23016_TW Alexander_BAR_20190822

Soil and Soil Gas Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

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TABLE OF CONTENTS
1.0 INTRODUCTION .............................................................................................................................. 1
1.1 SITE ENVIRONMENTAL HISTORY .............................................................................................................................. 1
1.2 SAMPLING OBJECTIVES .......................................................................................................................................... 1
2.0 SCOPE OF WORK .......................................................................................................................... 1
3.0 SAMPLING METHODOLOGY ........................................................................................................ 2
3.1 HEALTH AND SAFETY PLANNING, AND, SITE AND UTILITY CLEARING................................................................................ 2
3.2 SOIL GAS SAMPLING ............................................................................................................................................. 2
3.3 SOIL SAMPLING .................................................................................................................................................... 3
3.4 SAMPLE POINT LOCATING ...................................................................................................................................... 3
3.5 SOIL BORING ABANDONMENT ................................................................................................................................ 4
4.0 PHYSICAL SITE CHARACTERISTICS .......................................................................................... 4
4.1 TOPOGRAPHY AND SURFACE WATER DRAINAGE ......................................................................................................... 4
4.2 SITE GEOLOGY ..................................................................................................................................................... 4
4.3 SITE HYDROGEOLOGY ............................................................................................................................................ 4
5.0 LABORATORY ANALYTICAL RESULTS ...................................................................................... 4
5.1 SOIL GAS VOC ANALYTICAL RESULTS ....................................................................................................................... 5
5.1.1 VOCs....................................................................................................................................................... 5
5.1.2 Vapor Intrusion Risk Calculator Results ................................................................................................ 5
5.2 SOIL ANALYTICAL RESULTS ..................................................................................................................................... 5
5.2.1 VOCs....................................................................................................................................................... 5
5.2.2 SVOCS .................................................................................................................................................... 5
5.2.3 Metals .................................................................................................................................................... 5
5.2.4 Soil Direct Contact Exposure Risk Calculator Results ........................................................................... 6
5.3 FIELD AND LABORATORY PROCEDURE QA/QC ........................................................................................................... 6
6.0 INVESTIGATION DERIVED WASTE (IDW) MANAGEMENT ........................................................ 6
7.0 FINDINGS ........................................................................................................................................ 6
8.0 CONCLUSIONS AND RECOMMENDATIONS ............................................................................... 7
9.0 REFERENCES ................................................................................................................................. 7

DRAWINGS

Drawing 1 Topographic Site Map
Drawing 2 Soil Gas and Soil Sample Location Map

TABLES

Table 1 Soil Gas and Soil Sample Locations and Analysis
Table 2 Soil Gas Analytical Results – Building 1
Table 3 Soil Gas Analytical Results – Building 2
Table 4 Soil Gas Analytical Results – Building 3
Table 5 Soil Gas Analytical Results – Building 4
Table 6 Soil Analytical Results
Soil and Soil Gas Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

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APPENDICES

Appendix A Weck Total Volatile Organic Compound (VOC) 2017 Plume Map (prepared by Amec
Foster Wheeler)
Appendix B Field Notes
Appendix C Laboratory Analytical Reports
Appendix E Risk Calculator - Summary of Risk Assessment Output
Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

Page 1 of 8

1.0 INTRODUCTION
The John R. McAdams Company, Inc. (McAdams) is pleased to submit this Soil Gas and Soil Sampling Work
Plan for the TW Alexander Flex Property located southwest of the intersection of TW Alexander Drive and
S Miami Boulevard in Durham, North Carolina (herein referred to as the “subject site”). The subject site is
comprised of Durham County Parcel Identification Numbers (PINs) 0749-03-31-9242, 0749-03-41-4159,
0749-04-51-1176, 0749-04-50-1918, 0749-03-40-3468, and 0748-01-49-4407 and consists of +/- 51.15
acres of land. The subject site is identified as North Carolina Brownfield Program (NCBP) 23016-19-032.
The subject site is depicted on Drawing 1.

1.1 Site Environmental History
The subject site was historically used for agricultural and residential purposes, and currently consists of
undeveloped woodland owned by IBM. Merritt – IB1, LLC is planning to purchase and redevelop the
subject site as a single-story commercial flex space.

The site is located downgradient of a volatile organic compound (VOC) (i.e., chlorinated solvent and other
VOCs) plume that originates on the north adjacent former Edward Weck, Inc. facility (EPA ID NCD 001 493
931) located at 2917 Weck Drive in Durham, North Carolina. Corrective Action activities for the plume are
being managed under the North Carolina Registered Environmental Consultant (REC) Program. A total
VOC map prepared by others that depicts the extent and orientation of the plume on the subject site (as
of 2017) is presented in Appendix A.

1.2 Sampling Objectives
Soil gas and soil sampling activities performed were conducted to meet the following objectives:

• Obtain data to evaluate if a vapor intrusion mitigation system (VIMS) is required for all or a portion
of the proposed buildings, and if so, to use the data to support the VIMS design process.
• Obtain soil data to evaluate if a potential exposure risk is present to construction workers.
• Evaluate soils for beneficial reuse conditions at the site prior to construction.

Work performed as part of this assessment was conducted in general accordance with NCBP approved
Soil Gas and Soil Sampling Work Plan (Rev 2), dated June 12, 2019 (McAdams).

2.0 SCOPE OF WORK
The scope of work included the advancement of 24 soil borings to allow for the collection of soil gas and
soil samples on the subject site. As shown in Drawing 2, soil boring locations were distributed within the
footprint of each of the four proposed buildings.

A soil gas sample was collected at each of the 24 soil boring locations. Soil gas samples were collected at
a depth of approximately 6 feet below (current) land surface (BLS) and analyzed in accordance with Table
1.
Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

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Soil samples were also collected from the one- to two-foot BLS sample interval from borings located within
the footprint of each (of the four) proposed buildings as depicted on Drawing 2 and submitted for
laboratory analysis as summarized in Table 1.

3.0 SAMPLING METHODOLOGY
On July 10 and 11, 2019 McAdams oversaw Quantex Environmental Drilling of Clayton, North Carolina
advance 24 borings (SG-1 through SG-24) (Drawing 2) using direct push technology to a depth of six feet
BLS to allow for the collection and analysis of soil gas and soil samples using the methods summarized in
Table 1. Field notes, including a description of soil encountered in each boring are presented in Appendix
B. Laboratory analytical results are summarized in Tables 2 through 6. Laboratory analytical reports are
provided in Appendix C. An electronic data deliverable (EDD) of laboratory data is also being submitted
to the NCBP under separate cover in conjunction with this report.

3.1 Health and Safety Planning, and, Site and Utility Clearing
Prior to the start of work, McAdams updated the site-specific Health and Safety Plan in general accordance
with the Occupation Safety and Health Administration (OSHA) rules (29 CFR 1910.120). To address
potential underground utilities, McAdams contacted the North Carolina 811 one-call system a minimum
of 72 hours before beginning the assessment to notify member utilities of the subsurface work.
Concurrent with vegetative clearing on July 8 through 10, 2019, McAdams performed a subsurface utility
exploration (SUE) survey to clear sample locations/areas of utilities.

3.2 Soil Gas Sampling
On July 11, 12 and 19, 2019, soil gas sampling was conducted in general accordance with North Carolina
Department of Environmental Quality (NCDEQ), Division of Waste Management (DWM), Vapor Intrusion
Guidance (March 2018).

Soil gas sample ports were installed in each borehole by inserting and lowering a steel mesh vapor
sampling implant affixed to an inert ¼-inch outer diameter Teflon tube into the borehole to six feet BLS.
The implant was encased with driller’s sand. Bentonite was added and hydrated with distilled water to
create a seal at the top of the borehole. A plug was inserted onto the end of the section of tubing
extending out of the ground and the borehole was allowed to stabilize for a minimum of approximately
24-hours, before sampling.

A disposable 100 milliliter (mL) syringe and fittings were used to purge a minimum of three volumes of
soil gas from each location prior to sample location. Purge volumes were recorded for each borehole
(Appendix B). A helium tracer compound was introduced through a shroud over the borehole and
sampling train to check the sampling set-up for leaks. Helium concentration of less than 50 parts per
million (ppm) were used to indicate an adequate seal has been achieved at each implant/sample point.

Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

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A laboratory supplied one-Liter Summa canister attached to the tubing was used to collect the soil gas
samples after the system leak check had been performed. A flow regulator choke placed on each canister
was used to obtain a flow rate of no more than 200 milliliters per minute during sampling. Each summa
canister was closed while the canister still had a negative pressure. Soil gas samples were submitted to
the Pace Analytical Services, LLC (Pace) laboratoy located in Minneapolis, Minnesota for the full VOC
analyte list using U.S. EPA Method TO-15.

3.3 Soil Sampling
Soil from each of the 24 borings advanced during soil gas sampling was scanned continuously for evidence
of total VOCs using a Photoionization Detector (PID) and generally classified in conformance with the
Unified Soil Classification System (USCS) (Appendix B).

A soil sample was collected from the one- to two-foot interval from the following borings (Drawing 2):

• Proposed Building 1 Footprint: B-3 and B-8
• Proposed Building 2 Footprint: B-10 and B-12
• Proposed Building 3 Footprint: B-15 and B-17
• Proposed Building 4 Footprint: B-19 and B-24

Each of the eight grab samples was placed in appropriately labeled laboratory supplied bottle ware
designated for VOC analysis by EPA Method 8260B.

Remaining soil from the one- to two- foot sample interval (from the two borings located within each
proposed building footprint) was homogenized in a decontaminated stainless-steel bowl to allow for
composite soil sampling. The four composite soil samples (Blgd-1, Bldg-2, Bldg-3 and Bldg-4) were placed
into laboratory supplied bottle ware for analysis of semi volatile organic compounds (SVOCs) using EPA
Method 8270C and Resource Conservation Recovery Act (RCRA) Metals using EPA Methods 6010C and
6020B. Soil samples were sealed, placed on ice, stored in dedicated coolers and submitted to Pace located
in Huntersville, North Carolina for laboratory analysis.

Additional hexavalent chromium follow-on analysis by EPA Method 7199 (Table 1) was conducted on
composite sample Bldg-3, as it was reported with the highest concentration of total chromium compared
to Bldg-1, Bldg-2 and Bldg-4.

3.4 Sample Point Locating
A handheld GPS unit and field measurements was utilized to locate the soil boring/soil gas sample points
as depicted on Drawing 2.

Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

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3.5 Soil Boring Abandonment
Soil borings were abandoned using bentonite and concrete in accordance with procedures for boring/well
abandonment outlined in 15A NCAC 02C .0113.

4.0 PHYSICAL SITE CHARACTERISTICS
4.1 Topography and Surface Water Drainage
According to United States Geological Survey (USGS) Topographic Quadrangle of Southeast Durham,
North Carolina site elevations range from approximately 370 to 345 feet above mean sea level (msl)
(Drawing 1). Based on topography, surface drainage is expected to generally flow southeast towards
Stirrup Iron Creek.

4.2 Site Geology
The site is in the Piedmont Physiographic Province. The Piedmont is characterized by gently rolling
topography and deeply weathered bedrock. Dendritic (tree-like) surface drainage patterns generally allow
for good drainage within this region. The region is characterized by a soil veneer derived from weathered
rock, or saprolite, which overlies bedrock.

According to the North Carolina Geological Survey Section of the North Carolina Department of Natural
Resources and Community Development Geology of North Carolina (1985) map, Triassic Basin, Durham-
Sanford Subbasin sedimentary rocks lie beneath the site. These rocks are described as Triassic Period
interbedded conglomerates, fanglomerates, sandstones and mudstones of the undivided Chatham Group.

Based on field notes (Appendix B) soil overburden generally consisted of approximately 6 inches of topsoil,
overlying silty clay (0.5 to 2 feet BLS) and clayey silt (2 to 6 feet BLS) of varying color.

4.3 Site Hydrogeology
Groundwater elevations and flow directions are site-specific. Groundwater flow direction generally
mimics the overlying site topography, flowing from higher to lower land surface elevations. Site-specific
groundwater flow direction can be influenced by impermeable surfaces, the proximity of nearby drainage
features, sinkholes, creeks, swamps, and pumped groundwater wells. Fractures, joints, bedding planes
and other discontinuities in the underlying rock can also affect the groundwater conditions. Based on a
review of available information, shallow groundwater is expected to converge southwest in the east
portion of the site and southeast in the western portion of the at Stirrup Iron Creek.

5.0 LABORATORY ANALYTICAL RESULTS
Tabulated soil gas and soil sample results presented in Tables 2 through 6 were compared to the NCDEQ,
DWM, Inactive Hazardous Sites Branch (IHSB), Vapor Intrusion Screening Levels (VISLs) (February 2018)
and Preliminary Soil Remediation Goals (PSRGs) (May 2019), respectively. Soil gas and soil sample results
are also depicted on Drawing 2. Associated Level II Quality Assurance (QA)/Quality Control (QC) analytical
reports are provided in Appendix C.
Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

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5.1 Soil Gas VOC Analytical Results
Soil gas results for Buildings 1 through 4 are tabulated in Tables 2 through 5, respectively.

5.1.1 VOCs
As is summarized in corresponding Tables, no VOCs were detected at concentrations greater than
associated Non-Residential Soil Gas VISLs in Building footprints 1 through 4. Compounds with detectable
concentrations were primarily associated with petroleum- and solvent-related compounds, and, were
reported at least one order of magnitude below associated Non-Residential Soil Gas VISLs.

5.1.2 Vapor Intrusion Risk Calculator Results
Vapor Intrusion Risk Calculator - Summary of Risk Assessment Outputs for each building, presented in
Appendix D, indicated the following for the non-residential worker soil gas to indoor air pathway:

• Building 1 – Carcinogenic Risk: 2.9 x 10-6; Hazard Index: 7.9 x 10-2;
• Building 2 – Carcinogenic Risk: 2.4 x 10-5; Hazard Index: 7.0 x 10-1;
• Building 3 – Carcinogenic Risk: 3.3 x 10-6; Hazard Index: 8.7 x 10-2; and,
• Building 4 – Carcinogenic Risk: 3.1 x 10-5; Hazard Index: 8.8 x 10-1.

Based on risk calculator results a vapor intrusion risk does not appear to be present for a non-residential
worker in proposed Buildings 1 through 4.

5.2 Soil Analytical Results
Soil sample analytical results are tabulated in Table 6. Below is a summary of soil sample results by
analytical suite.

5.2.1 VOCs
Acetone was reported at a detectable concentration below the Industrial/Commercial PSRGs in sample
SG-24 1’ (Building 4), and, based on its concentration and anamolous detection is likely a laboratory
artifact. No other VOCs were reported with detectable concentrations above the reporting limit.

5.2.2 SVOCS
No SVOCs were reported with detectable concentrations above the reporting limit.

5.2.3 Metals
Total chromium was detected at concentrations ranging between 10.7 milligrams per kilogram (mg/kg)
and 27.2 mg.kg in composite samples collected from Buildings 1 through 4 (BLDG-1 through BLDG-4).
Hexavalent chromium was reported at a detectable concentration below the Industrial/Commercial
PSRGs in composite sample BLDG-3. Total arsenic, barium, lead, mercury and selenium were also reported
at detectable concetrations below the associated Industrical/Commerical PSRGs. Detected
Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

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concentrations of metals appear to be within the background metals range for soils in North Carolina as
published in Elements in North American Soils by Dragun and Chekiri, 2005 (Table 6).

5.2.4 Soil Direct Contact Exposure Risk Calculator Results
Soil direct contact exposure Risk Calculator - Summary of Risk Assessment Outputs for the site (Appendix
D) indicated the following:

• Non-residential worker soil direct contact pathway - Carcinogenic Risk: 9.4 x 10-7; Hazard Index:
5.7 x 10-3;
• Construction worker soil direct contact pathway – Carcinogenic Risk: 7.1 x 10-7; Hazard Index: 5.7
x 10-2; and
• Recreator/Trespasser soil direct contact pathway – Carcinogenic Risk: 5.5 x 10-6; Hazard Index: 4.2
x 10-2.

Risk calculator results suggest that a direct contact exposure soil risk is not present for non-residential
workers, construction workers, or a recreators/trespassers at the site.

5.3 Field and Laboratory Procedure QA/QC
Blind duplicate results for soil gas sample DUP-1 (Table 3) and soil sample SG-DUP-1 (Table 6) were within
10 standard deviations of results reported for soil gas sample SG-11 and soil sample SG-12 1’, respectively.

6.0 INVESTIGATION DERIVED WASTE (IDW) MANAGEMENT
Because no evidence of potential impacts was identified using field screening methods, soil cuttings were
spread onto the ground in general accordance with applicable regulatory guidance.

7.0 FINDINGS
Based on the results of this assessment McAdams offers the following findings:

• Soil at the site generally consists of approximately 6 inches of topsoil, overlying silty clay (0.5 to 2
feet BLS) and clayey silt (2 to 6 feet BLS) of varying color. Field screening results did not reveal
evidence of impacts in soil.
• No VOCs were detected at concentrations greater than associated Non-Residential Soil Gas VISLs
in Building footprints 1 through 4. Compounds with detectable concentrations were primarily
associated with petroleum- and solvent-related compounds, and, were reported at least one
order of magnitude below associated Non-Residential Soil Gas VISLs.
• Risk calculator results suggest that an unacceptable vapor intrusion risk is unlikely to be present
for a non-residential worker in proposed Buildings 1 through 4.
• With the exception of a detection of acetone below the Industrial/Commercial PSRG (which is
likely a laboratory artifact), no VOCs or SVOCs were reported at detectable concentrations above
the reporting limit.
Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

Page 7 of 8

• Total chromium was detected in every soil sample collected. Follow-on hexavalent chromium
analysis, with concentrations below the associated Industrial/Commercial PSRG, suggested that
total chromium is predominantly present in its trivalent state at the site.
• In addition to total chromium, several other metals were reported at detectable concentrations
below associated Industrial/Commercial PSRGs. Concentrations of metals reported fall within the
background metals range for soils in North Carolina (Dragun and Chekiri, 2005).
• Risk calculator results suggest that a direct contact soil exposure risk is not present for non-
residential workers, construction workers, or a recreators/trespassers at the site.

8.0 CONCLUSIONS AND RECOMMENDATIONS
Soil gas results suggest that a VIMS will not be required for any of the proposed buildings. Additional soil
gas/indoor air sampling may be required once the buildings are constructed per NCBP protocol to confirm
the findings of this assessment in the event VIMS are not installed.

Soil results suggest that special handling or additional personal protection equipment beyond that of what
would typically be required at a construction site will not be necessary for construction workers during
site redevelopment for disturbance of soils above the water table. Due to the presence of contaminants
of concern in the water table, specialized handling of soils below the water table will be required (as
applicable).

Finally, results suggest that unsaturated soil meets the criteria for potential export to be classified as
beneficial fill per Issue 15: Soil Import/Export of the Brownfields Program Guidelines and Issue Resolutions
document (dated December 2017), and can be used on other sites following approval from the NCBP. An
Environmental Management Plan (EMP) will be required by the NCBP to develop procedures for managing
soils at the site during construction.

9.0 REFERENCES

Dragun and Chekiri, Elements in North American Soils, 2005.

McAdams, Soil Gas and Soil Sampling Work Plan (Rev 2), TW Alexander Flex Property, Durham, Durham
County, North Carolina, NCBP Project No. 23016-19-032, June 12, 2019.

McAdams, Phase I Environmental Site Assessment, 1105 & 1107 West Main Street and 1024 & 1026
West Peabody Street, Durham, North Carolina, July 18, 2017

NCDEQ, DWM, IHSB, Vapor Intrusion Screening Levels, February 2018.

NCDEQ, DWM, IHSB, Preliminary Soil Remediation Goals Table, last updated in May 2019.

Soil Gas and Soil Sampling Report
TW Alexander Flex Property
NCBP Project No. 23016-19-032
August 22, 2019

Page 8 of 8

NCDEQ, DWM, Vapor Intrusion Guidance (March 2018).

NCDEQ, IHSB, Guidelines for Assessment and Cleanup, (October 2015).

North Carolina Geologic Survey, Geologic Map of North Carolina, 1985.

United States Geological Survey (USGS), Topographic Quadrangles of Northwest and Southwest Durham,
North Carolina, 2016.

DRAWINGS
0 1,000 2,000Feet1 inch = 2,000 feet
¯
DRAWING 1. LOCATION MAPTW ALEXANDER FLEX PROPERTYTW ALEXANDER AND S MIAMI BLVDDURHAM, NORTH CAROLINA
DWG NO:DATE:JOB NO:DRAWN BY:DRAFT CHECK:ENG. CHECK:APPROVAL:FILE LOC:
3/12/2019MPP-18020VG
X:\Projects\MPP18020\GIS\ENVIRONMENTAL\NCBP_APPLICATIONI\LOCATION_MAP
NOTES:1. BASE MAP FROM USGS TOPOGRAPHIC QUADRANGLE OFSOUTHWEST DURHAM, NC; 1998 AND SOUTHEAST DURHAM, NC; 1998.
LEGEND
SUBJECT PROPERTY
CLIENT
REVISIONS
PROJECT NO.MPP-18020
FILENAME
CHECKED BY
DRAWN BY
SCALE
DATE 06. 07. 2019
N0.DATE
X:\Projects\MPP\MPP-18020\Land\Earthworks\EW7.dwg, 5/28/2019 9:46:57 AM, Harrell, GrayThe John R. McAdams Company, Inc.
2905 Meridian Parkway
Durham, NC 27713
phone [phone]
fax [phone]
license number: C-0293
www.mcadamsco.com
FLEX BUILDINGS - TW ALEXANDERADMINISTRATIVE SITE PLAN - LEVEL 4DURHAM, NORTH CAROLINA 27703SHEET
PLAN INFORMATION
MERRITT PROPERTIES
2066 LORD BALTIMORE DIVE
BALTIMORE, MARYLAND 21244
PRELIMINARY DRAWING - NOT RELEASED FOR CONSTRUCTION
BUILDING
FFE = 369.50
BUILDING
FFE=366.25
BUILDING
FFE=366.50
BUILDING
FFE=371.00
GRAPHIC SCALE
0 50 100 200
1 inch = 100 ft.
1"=100'

TABLES
Sample ID Sample Objective Proposed Sample Depth (FT BLS)Analytical Method QA/QC
SG-1 through SG-8 VI Assessment under Proposed Building 1 5 to 10 - Full VOC list by EPA Method TO-15 --
SG-9 through SG-14 VI Assessment under Proposed Building 2 5 to 10 - Full VOC list by EPA Method TO-15 --
SG-15 through SG-18 VI Assessment under Proposed Building 3 5 to 10 - Full VOC list by EPA Method TO-15 --
SG-19 through SG-24 VI Assessment under Proposed Building 4 5 to 10 - Full VOC list by EPA Method TO-15 --
SG DUP-1 QA/QC 5 to 10 - Full VOC list by EPA Method TO-15 Blind Duplicate Sample
B-3 and B-8 / Bldg-1 Soil Assessment under Proposed Building 1 1 to 2
- Grab Samples (B-3 and B-8) VOCs by EPA Method 8260B
- Composite Sample (Bldg-1) SVOCs by EPA Method 8270C and RCRA Metals EPA Methods 6010C, 6020B*--
B-10 and B-12 / Bldg-2 Soil Assessment under Proposed Building 2 1 to 2
- Grab Samples (B-10 and B-12) VOCs by EPA Method 8260B
- Composite Sample (Bldg-2) SVOCs by EPA Method 8270C and RCRA Metals EPA Methods 6010C, 6020B*--
B-15 and B-17 / Bldg-3 Soil Assessment under Proposed Building 3 1 to 2
- Grab Samples (B-15 and B-17) VOCs by EPA Method 8260B
- Composite Sample (Bldg-3) SVOCs by EPA Method 8270C and RCRA Metals EPA Methods 6010C, 6020B*--
B-19 and B-24 / Bldg-4 Soil Assessment under Proposed Building 4 1 to 2
- Grab Samples (B-19 and B-24) VOCs by EPA Method 8260B
- Composite Sample (Bldg-4) SVOCs by EPA Method 8270C and RCRA Metals EPA Methods 6010C, 6020B*--
B DUP-1 QA/QC 1 to 2
- Grab Sample VOCs by EPA Method 8260B
- Composite Sample SVOCs by EPA Method 8270C and RCRA Metals EPA Methods 6010C, 6020B Blind Duplicate Sample
Trip Blank QA/QC N/A - VOCs by EPA Method 8260B Trip Blank
Notes:
VOCs = Volatile Organic Compounds
SVOCs = Semi-Volatile Organic Compounds
RCRA = Resource Conservation Recovery Act
VI = Vapor Intrusion
FT BLS = Feet Below Land Surface
QA/QC = Quality Assurance/Quality Control
*Laboratory will be notified on the chain of custody to anlayze the composite sample (Bldg-1, Bldg-2, Bldg-3 or Bldg-4) with the highest concentration of total chromium for hexavalent chromium by EPA Method 7199
TABLE 1
SOIL GAS AND SOIL SAMPLE LOCATIONS AND ANALYSIS
TW ALEXANDER FLEX PROPERTY (NCBP Project No. 23016-19-032)
DURHAM, NORTH CAROLINA
MCADAMS PROJECT NO. MPP-18020
SAMPLE ID SG-1 SG-2 SG-3 SG-4 SG-5 SG-6 SG-7 SG-8
DATE SAMPLED 07/11/19 07/11/19 07/11/19 07/11/19 07/11/19 07/11/19 07/11/19 07/11/19
1,1,1-Trichloroethane <2.2 <3.6 <2.2 <2.2 <2.2 <1.9 <2.2 <2.2 440,000
1,1,2,2-Tetrachloroethane <1.4 <2.3 <1.4 <1.4 <1.4 <1.2 <1.4 <1.4 210
1,1,2-Trichloroethane <1.1 <1.8 <1.1 <1.1 <1.1 <0.97 <1.1 <1.1 18
1,1,2-Trichlorotrifluoroethane <3.2 <5.1 <3.0 <3.0 <3.0 <2.7 <3.2 <3.2 440,000
1,1-Dichloroethane <1.7 <2.7 <1.6 <1.6 <1.6 <1.4 <1.7 2.4 7,700
1,1-Dichloroethene <1.6 <2.6 <1.6 <1.6 <1.6 <1.4 <1.6 <1.6 18,000
1,2,4-Trichlorobenzene <15.2 <24.6 <14.6 <14.6 <14.6 <13.1 <15.2 <15.2 180
1,2,4-Trimethylbenzene 7.2 3.5 5.8 7.9 5.8 21.3 14.2 29.9 5,300
1,2-Dibromoethane (EDB)<1.6 <2.5 <1.5 <1.5 <1.5 <1.4 <1.6 <1.6 20
1,2-Dichlorobenzene <2.5 <4.0 <2.4 <2.4 <2.4 <2.1 <2.5 <2.5 18,000
1,2-Dichloroethane <0.83 <1.3 <0.80 <0.80 <0.80 <0.72 <0.83 <0.83 470
1,2-Dichloropropane <1.9 <3.1 <1.8 <1.8 <1.8 <1.6 <1.9 <1.9 350
1,3,5-Trimethylbenzene 5.6 <3.3 3.6 4.8 2.2 9.1 7.2 12.9 5,300
1,3-Butadiene <0.91 <1.5 <0.87 <0.87 <0.87 <0.78 <0.91 <0.91 180
1,3-Dichlorobenzene 3.8 <4.0 4.6 5.2 14.6 20.8 9.9 10.5 NE
1,4-Dichlorobenzene <6.2 <10 <5.9 <5.9 <5.9 <5.3 <6.2 <6.2 1,100
2-Butanone (MEK)<6.1 <9.8 <5.8 6.9 6.3 6.5 6.5 11.4 440,000
2-Hexanone <8.4 <13.6 <8.1 <8.1 <8.1 <7.2 <8.4 <8.4 2,600
4-Ethyltoluene <5.0 <8.2 <4.8 <4.8 <4.8 5.2 5.4 8.7 NE
4-Methyl-2-pentanone (MIBK)<8.4 <13.6 <8.1 <8.1 <8.1 <7.2 <8.4 12.3 260,000
Acetone 18.4 37.9 21.9 28.4 36.3 36.4 41.6 58.8 2,700,000
Benzene 3.4 1.8 14.7 10.1 5.4 5.3 16.3 29.9 1,600
Bromodichloromethane <2.7 <4.4 <2.6 <2.6 <2.6 <2.4 <2.7 <2.7 330
Bromoform <10.6 <17.1 <10.2 <10.2 <10.2 <9.1 <10.6 <10.6 11,000
Bromomethane <1.6 <2.6 <1.5 <1.5 <1.5 <1.4 <1.6 1.9 330
Carbon disulfide 1.6 <2.1 3.8 5.1 2.9 4.5 22.9 30.3 61,000
Carbon tetrachloride <2.6 <4.2 <2.5 <2.5 <2.5 <2.2 <2.6 <2.6 2,000
Chlorobenzene <1.9 <3.1 <1.8 <1.8 <1.8 <1.6 <1.9 <1.9 4,400
Chloroethane <1.1 <1.7 <1.0 <1.0 <1.0 <0.93 <1.1 6.9 880,000
Chloroform 20 5.8 8.3 8.6 <0.96 2.1 4.2 11 530
Chloromethane <0.85 <1.4 <0.81 1.1 1.6 <0.73 1.1 13.9 7,900
Cyclohexane 4.1 <5.7 13.3 5.3 4.7 5.2 <3.5 <3.5 530,000
Dibromochloromethane <3.5 <5.6 <3.4 <3.4 <3.4 <3.0 <3.5 <3.5 NE
Dichlorodifluoromethane <2.0 <3.3 2.1 2.0 2.4 <1.8 <2.0 2.1 8,800
Dichlorotetrafluoroethane <2.9 <4.6 <2.8 <2.8 <2.8 <2.5 <2.9 <2.9 NE
Ethyl acetate 2.1 <2.4 2.7 2.7 3.3 2.1 3.5 3.1 6,100
Ethylbenzene 5.4 <2.9 9.8 10.6 4.8 12.2 14.7 27.3 4,900
Hexachloro-1,3-butadiene <10.9 <17.7 <10.5 <10.5 <10.5 <9.4 <10.9 <10.9 560
Methyl-tert-butyl ether <7.4 <11.9 <7.1 <7.1 <7.1 <6.4 <7.4 <7.4 47,000
Methylene Chloride <7.1 341 <6.8 <6.8 <6.8 <6.1 <7.1 <7.1 53,000
Naphthalene <5.4 <8.7 <5.2 <5.2 <5.2 <4.6 <5.4 <5.4 260
Propylene 8.6 11.8 19.4 53.9 16.9 14.8 332 E 98.2 260,000
Styrene 3.3 <2.8 6.9 35.1 <1.7 1440 <1.7 5.9 88,000
Tetrachloroethene <1.4 <2.2 <1.3 <1.3 <1.3 <1.2 <1.4 <1.4 3,500
Tetrahydrofuran <1.2 <2.0 <1.2 <1.2 <1.2 <1.0 <1.2 <1.2 180,000
Toluene 26.2 12.9 83.2 70.7 33.3 42.2 99.5 187 440,000
Trichloroethene <1.1 <1.8 <1.1 <1.1 <1.1 <0.95 <1.1 <1.1 180
Trichlorofluoromethane <2.3 <3.7 <2.2 <2.2 <2.2 <2.0 <2.3 <2.3 NE
Vinyl acetate <1.4 <2.3 <1.4 <1.4 <1.4 <1.2 <1.4 <1.4 18,000
Vinyl chloride <0.53 <0.85 <0.50 <0.50 <0.50 <0.45 <0.53 2.1 2,800
cis-1,2-Dichloroethene <1.6 <2.6 <1.6 <1.6 <1.6 <1.4 <1.6 7.2 NE
cis-1,3-Dichloropropene <1.9 <3.0 <1.8 <1.8 <1.8 <1.6 <1.9 <1.9 NE
m&p-Xylene 22.7 8.5 34.5 38.5 15.8 44.9 55.4 113 8,800
n-Heptane 5.3 <2.7 25.9 13.2 7.4 9.2 21.5 38.5 35,000
n-Hexane 4.7 26.3 27.5 13.9 10.1 10.4 37.3 43.9 61,000
o-Xylene 6.5 3.1 9.1 10.1 5.5 10 16 31.6 8,800
trans-1,2-Dichloroethene <1.6 <2.6 <1.6 <1.6 <1.6 <1.4 <1.6 <1.6 NE
trans-1,3-Dichloropropene <1.9 <3.0 <1.8 <1.8 <1.8 <1.6 <1.9 <1.9 1,800
Notes:
ug/m3 = milligram per kilogram
< # = Not detected above the Reporting Limit (RL)
E = Analyte concentration exceeded the calibration range, the reported result is estimated
Bolded Values = Concentrations detected above their respective IHSB Non-Residential Soil Gas Screening Limits (February 2018)
Non-Residential Soil Gas
Screening Level
EPA METHOD TO-15 (ug/m3)
TABLE 2
SOIL GAS ANALYTICAL RESULTS - BUILDING 1
JULY 2019
TW ALEXANDER FLEX, SOIL GAS SAMPLING (NCBP Project No. 23016-19-032)
DURHAM, NORTH CAROLINA
MCADAMS PROJECT NO. MPP-18020
SAMPLE ID SG-9 SG-10 SG-11 *DUP-1 SG-12 SG-13 SG-14
DATE SAMPLED 07/12/19 07/12/19 07/12/19 07/12/19 07/12/19 07/12/19 07/19/19
1,1,1-Trichloroethane <2.3 <2.2 <2.2 <2.3 <4.5 <11.2 <37.3 440,000
1,1,2,2-Tetrachloroethane <1.5 <1.4 <1.4 <1.5 <2.8 <7.0 <23.5 210
1,1,2-Trichloroethane <1.2 <1.1 <1.1 <1.2 <2.2 <5.6 <18.6 18
1,1,2-Trichlorotrifluoroethane <3.3 <3.2 <3.2 <3.3 <6.3 <15.8 <52.4 440,000
1,1-Dichloroethane <1.7 <1.7 <1.7 <1.7 <3.3 <8.3 <27.7 7,700
1,1-Dichloroethene <1.7 <1.6 <1.6 <1.7 <3.3 <8.1 <27.1 18,000
1,2,4-Trichlorobenzene <15.8 <15.2 <15.2 <15.8 <30.5 <76.2 <253 180
1,2,4-Trimethylbenzene 6.1 10.8 6.7 6.4 19.4 22.6 141 5,300
1,2-Dibromoethane (EDB)<1.6 <1.6 <1.6 <1.6 <3.2 <7.9 <26.2 20
1,2-Dichlorobenzene <2.6 <2.5 <2.5 <2.6 <4.9 <12.3 <41.0 18,000
1,2-Dichloroethane <0.86 <0.83 <0.83 <0.86 <1.7 <4.2 <13.8 470
1,2-Dichloropropane <2.0 <1.9 <1.9 <2.0 <3.8 <9.5 <31.6 350
1,3,5-Trimethylbenzene 2.1 4.6 <2.0 <2.1 8.5 <10.1 62.1 5,300
1,3-Butadiene <0.94 <0.91 <0.91 <0.94 <1.8 <4.5 <15.1 180
1,3-Dichlorobenzene 18 23.6 26.1 19.3 29.3 33.3 <41.0 NE
1,4-Dichlorobenzene <6.4 <6.2 <6.2 <6.4 <12.4 <30.9 <103 1,100
2-Butanone (MEK)13 <6.1 12.3 16.3 <12.1 <30.3 <101 440,000
2-Hexanone <8.7 <8.4 <8.4 <8.7 <16.8 <42.0 <140 2,600
4-Ethyltoluene <5.2 <5.0 <5.0 <5.2 <10.1 <25.2 <84.0 NE
4-Methyl-2-pentanone (MIBK)<8.7 <8.4 <8.4 <8.7 <16.8 <42.0 <140 260,000
Acetone 53.1 52.1 52.2 62.1 51.1 58.8 <81.0 2,700,000
Benzene 11.4 25.3 0.95 1.1 50.3 28.2 <10.9 1,600
Bromodichloromethane <2.9 <2.7 <2.7 <2.9 <5.5 <13.7 <45.7 330
Bromoform <11 <10.6 <10.6 <11 <21.2 <53 <176 11,000
Bromomethane <1.7 <1.6 <1.6 <1.7 <3.2 <8.0 <26.5 330
Carbon disulfide 3.3 10.1 <1.3 <1.3 7.0 12.1 <21.3 61,000
Carbon tetrachloride <2.7 <2.6 <2.6 <2.7 <5.2 <12.9 <43.0 2,000
Chlorobenzene <2.0 <1.9 <1.9 <2.0 <3.8 <9.5 <31.4 4,400
Chloroethane <1.1 <1.1 <1.1 <1.1 9.3 <5.4 <18.0 880,000
Chloroform 3.7 2.2 <1.0 <1.0 5.1 7.9 <16.7 530
Chloromethane 7 <0.85 <0.85 <0.88 58.2 8.9 <14.1 7,900
Cyclohexane 9.4 <3.5 6.6 6.0 21.2 20.6 <58.8 530,000
Dibromochloromethane <3.6 <3.5 <3.5 <3.6 <7.0 <17.5 <58.1 NE
Dichlorodifluoromethane 2.7 2.5 <2.0 <2.1 <4.1 <10.2 <33.9 8,800
Dichlorotetrafluoroethane <3.0 <2.9 <2.9 <3.0 <5.7 <14.3 <47.7 NE
Ethyl acetate 4.3 <1.5 4.4 <1.5 <3.0 <7.4 <24.6 6,100
Ethylbenzene 5.9 17.6 3.1 3.2 36.3 28.4 38.7 4,900
Hexachloro-1,3-butadiene <11.4 <10.9 <10.9 <11.4 <21.9 <54.7 <182 560
Methyl-tert-butyl ether <7.7 <7.4 <7.4 <7.7 <14.8 <37 <123 47,000
Methylene Chloride <7.4 <7.1 <7.1 <7.4 16.9 <35.7 <119 53,000
Naphthalene <5.6 <5.4 <5.4 <5.6 <10.7 <26.9 <89.4 260
Propylene 77.9 288 <0.71 <0.74 606 E 113 85.8 260,000
Styrene 8.1 405 7.1 <1.8 <3.5 204 <29.1 88,000
Tetrachloroethene <1.4 <1.4 2.1 <1.4 <2.8 <7.0 <23.2 3,500
Tetrahydrofuran <1.3 <1.2 <1.2 <1.3 <2.4 <6.1 <20.2 180,000
Toluene 37.5 139 9.2 9.9 142 152 118 440,000
Trichloroethene <1.1 <1.1 <1.1 <1.1 <2.2 <5.5 <18.3 180
Trichlorofluoromethane <2.4 <2.3 <2.3 <2.4 <4.6 <11.5 <38.3 NE
Vinyl acetate <1.5 <1.4 <1.4 <1.5 <2.9 <7.2 <24.1 18,000
Vinyl chloride 2.2 <0.53 <0.53 <0.55 24.8 6.9 <8.7 2,800
cis-1,2-Dichloroethene <1.7 <1.6 <1.6 <1.7 <3.3 <8.1 <27.1 NE
cis-1,3-Dichloropropene <1.9 <1.9 <1.9 <1.9 <3.7 <9.3 <31.0 NE
m&p-Xylene 19.1 64.2 11.1 11.5 92.1 104 182 8,800
n-Heptane 13.1 39.3 <1.7 <1.7 30.6 38.9 <28.0 35,000
n-Hexane 24.1 78.4 <1.4 <1.5 72.5 59.6 <24.1 61,000
o-Xylene 6.1 15.8 4.7 5.0 25.2 29.3 63.8 8,800
trans-1,2-Dichloroethene <1.7 <1.6 <1.6 <1.7 <3.3 <8.1 <27.1 NE
trans-1,3-Dichloropropene <1.9 <1.9 <1.9 <1.9 <3.7 <9.3 <31.0 1,800
Notes:
ug/m3 = milligram per kilogram
< # = Not detected above the Reporting Limit (RL)
E = Analyte concentration exceeded the calibration range, the reported result is estimated
* DUP-1 is a duplicate of SG-11
Bolded Values = Concentrations detected above their respective IHSB Non-Residential Soil Gas Screening Limits (February 2018)
Non-Residential Soil Gas
Screening Level
EPA METHOD TO-15 (ug/m3)
TABLE 3
SOIL GAS ANALYTICAL RESULTS - BUILDING 2
JULY 2019
TW ALEXANDER FLEX, SOIL GAS SAMPLING (NCBP Project No. 23016-19-032)
DURHAM, NORTH CAROLINA
MCADAMS PROJECT NO. MPP-18020
SAMPLE ID SG-15 SG-16 SG-17 SG-18
DATE SAMPLED 07/12/19 07/12/19 07/12/19 07/12/19
1,1,1-Trichloroethane <2.4 <2.2 <4.5 <2.2 440,000
1,1,2,2-Tetrachloroethane <1.5 <1.4 <2.8 <1.4 210
1,1,2-Trichloroethane <1.2 <1.1 <2.2 <1.1 18
1,1,2-Trichlorotrifluoroethane <3.4 <3 <6.3 <3.0 440,000
1,1-Dichloroethane <1.8 <1.6 <3.3 <1.6 7,700
1,1-Dichloroethene <1.8 <1.6 <3.3 <1.6 18,000
1,2,4-Trichlorobenzene <16.5 <14.6 <30.5 <14.6 180
1,2,4-Trimethylbenzene 8.3 6.9 7.8 6.3 5,300
1,2-Dibromoethane (EDB)<1.7 <1.5 <3.2 <1.5 20
1,2-Dichlorobenzene <2.7 <2.4 <4.9 <2.4 18,000
1,2-Dichloroethane <0.9 <0.8 <1.7 <0.8 470
1,2-Dichloropropane <2.1 <1.8 <3.8 <1.8 350
1,3,5-Trimethylbenzene 3.2 2.4 <4.0 <1.9 5,300
1,3-Butadiene <0.99 <0.87 <1.8 <0.87 180
1,3-Dichlorobenzene 12.3 12.2 17.7 9.3 NE
1,4-Dichlorobenzene <6.7 <5.9 <12.4 <5.9 1,100
2-Butanone (MEK)<6.6 9.6 <12.1 6.7 440,000
2-Hexanone <9.1 <8.1 <16.8 <8.1 2,600
4-Ethyltoluene <5.5 <4.8 <10.1 <4.8 NE
4-Methyl-2-pentanone (MIBK)<9.1 <8.1 <16.8 <8.1 260,000
Acetone 44.2 <4.7 <9.7 51.6 2,700,000
Benzene 22.9 15.6 34.8 31.8 1,600
Bromodichloromethane <3.0 <2.6 <5.5 <2.6 330
Bromoform <11.5 <10.2 <21.2 <10.2 11,000
Bromomethane <1.7 <1.5 <3.2 <1.5 330
Carbon disulfide 6.3 13.1 22.4 22.7 61,000
Carbon tetrachloride <2.8 <2.5 <5.2 <2.5 2,000
Chlorobenzene <2.0 <1.8 <3.8 <1.8 4,400
Chloroethane 7.1 <1.0 <2.2 <1.0 880,000
Chloroform 6.5 1.0 4.1 3.7 530
Chloromethane 13.3 <0.81 <1.7 11.6 7,900
Cyclohexane 13.8 <3.4 <7.1 <3.4 530,000
Dibromochloromethane <3.8 <3.4 <7.0 <3.4 NE
Dichlorodifluoromethane 2.9 2.4 <4.1 2.3 8,800
Dichlorotetrafluoroethane <3.1 <2.8 <5.7 <2.8 NE
Ethyl acetate 4.3 5.1 <3.0 <1.4 6,100
Ethylbenzene 12 7.8 18.3 9.2 4,900
Hexachloro-1,3-butadiene <11.9 <10.5 <21.9 <10.5 560
Methyl-tert-butyl ether <8.0 <7.1 <14.8 <7.1 47,000
Methylene Chloride 14.2 <6.8 <14.3 <6.8 53,000
Naphthalene <5.8 <5.2 <10.7 <5.2 260
Propylene 189 E 453 E 1000 E 4740 260,000
Styrene <1.9 2.5 <3.5 5.4 88,000
Tetrachloroethene <1.5 <1.3 <2.8 <1.3 3,500
Tetrahydrofuran <1.3 <1.2 <2.4 <1.2 180,000
Toluene 92.6 52.6 98.9 71.7 440,000
Trichloroethene <1.2 <1.1 <2.2 <1.1 180
Trichlorofluoromethane <2.5 <2.2 <4.6 <2.2 NE
Vinyl acetate <1.6 <1.4 <2.9 <1.4 18,000
Vinyl chloride 4.7 <0.5 <1.1 <0.5 2,800
cis-1,2-Dichloroethene <1.8 <1.6 <3.3 <1.6 NE
cis-1,3-Dichloropropene <2.0 <1.8 <3.7 <1.8 NE
m&p-Xylene 41.5 25.7 39.4 28.1 8,800
n-Heptane 25.7 32.9 56.5 51.9 35,000
n-Hexane 42.7 107 160 154 61,000
o-Xylene 11.4 7.9 11 8.5 8,800
trans-1,2-Dichloroethene <1.8 <1.6 <3.3 <1.6 NE
trans-1,3-Dichloropropene <2.0 <1.8 <3.7 <1.8 1,800
Notes:
ug/m3 = milligram per kilogram
< # = Not detected above the Reporting Limit (RL)
E = Analyte concentration exceeded the calibration range, the reported result is estimated
Bolded Values = Concentrations detected above their respective IHSB Non-Residential Soil Gas Screening Limits (February 2018)
Non-Residential Soil Gas
Screening Level
EPA METHOD TO-15 (ug/m3)
TABLE 4
SOIL GAS ANALYTICAL RESULTS - BUILDING 3
JULY 2019
TW ALEXANDER FLEX, SOIL GAS SAMPLING (NCBP Project No. 23016-19-032)
DURHAM, NORTH CAROLINA
MCADAMS PROJECT NO. MPP-18020
SAMPLE ID SG-19 SG-20 SG-21 SG-22 SG-23 SG-24
DATE SAMPLED 07/11/19 07/11/19 07/11/19 07/11/19 07/11/19 07/11/19
1,1,1-Trichloroethane <47.4 <2.2 <2.2 <2.3 <2.2 <2.2 440,000
1,1,2,2-Tetrachloroethane <29.8 <1.4 <1.4 <1.5 <1.4 <1.4 210
1,1,2-Trichloroethane <23.7 <1.1 <1.1 <1.2 <1.1 <1.1 18
1,1,2-Trichlorotrifluoroethane <66.6 <3.2 <3.2 <3.3 <3.2 <3.2 440,000
1,1-Dichloroethane <35.1 <1.7 <1.7 <1.7 <1.7 <1.7 7,700
1,1-Dichloroethene <34.4 <1.6 <1.6 <1.7 <1.6 <1.6 18,000
1,2,4-Trichlorobenzene <322 <15.2 <15.2 <15.8 <15.2 <15.2 180
1,2,4-Trimethylbenzene 67.4 20.2 4.0 17.6 <2.0 12.5 5,300
1,2-Dibromoethane (EDB)<33.3 <1.6 <1.6 <1.6 <1.6 <1.6 20
1,2-Dichlorobenzene <52.1 <2.5 <2.5 <2.6 <2.5 <2.5 18,000
1,2-Dichloroethane <17.5 <0.83 <0.83 <0.86 <0.83 <0.83 470
1,2-Dichloropropane <40.1 <1.9 <1.9 <2.0 <1.9 <1.9 350
1,3,5-Trimethylbenzene 64.8 10.9 <2.0 8.7 <2.0 <2.0 5,300
1,3-Butadiene <19.2 <0.91 <0.91 <0.94 <0.91 <0.91 180
1,3-Dichlorobenzene <52.1 10.6 4.1 24.2 <2.5 36.1 NE
1,4-Dichlorobenzene <131 <6.2 <6.2 <6.4 <6.2 <6.2 1,100
2-Butanone (MEK)<128 <6.1 6.5 <6.3 8.1 15.9 440,000
2-Hexanone <178 <8.4 <8.4 <8.7 <8.4 <8.4 2,600
4-Ethyltoluene <107 <5.0 <5.0 5.4 <5.0 <5.0 NE
4-Methyl-2-pentanone (MIBK)<178 9.5 11.8 <8.7 <8.4 <8.4 260,000
Acetone 150 30.7 63.4 35.4 86.8 111 2,700,000
Benzene 29.2 28.3 45.7 14.4 27.8 67.5 1,600
Bromodichloromethane <58.1 <2.7 <2.7 <2.9 <2.7 <2.7 330
Bromoform <224 <10.6 <10.6 <11 <10.6 <10.6 11,000
Bromomethane <33.7 <1.6 <1.6 <1.7 <1.6 <1.6 330
Carbon disulfide 31.2 12.2 118 1.9 34.3 777 61,000
Carbon tetrachloride <54.7 <2.6 <2.6 <2.7 <2.6 <2.6 2,000
Chlorobenzene <40.0 <1.9 <1.9 <2.0 <1.9 <1.9 4,400
Chloroethane <22.9 <1.1 3.4 <1.1 5.3 <1.1 880,000
Chloroform <21.2 26.4 19.1 4.1 36.6 31.1 530
Chloromethane <17.9 <0.85 8.1 0.89 5.8 <0.85 7,900
Cyclohexane <74.7 18 <3.5 6.3 17.4 <3.5 530,000
Dibromochloromethane <73.9 <3.5 <3.5 <3.6 <3.5 <3.5 NE
Dichlorodifluoromethane <43.1 2.3 <2.0 <2.1 2.2 4.0 8,800
Dichlorotetrafluoroethane <60.6 <2.9 <2.9 <3.0 <2.9 <2.9 NE
Ethyl acetate <31.3 2.9 2.6 2.9 <1.5 5.1 6,100
Ethylbenzene 66.9 25.4 28.8 20 38.8 62.7 4,900
Hexachloro-1,3-butadiene <231 <10.9 <10.9 <11.4 <10.9 <10.9 560
Methyl-tert-butyl ether <156 <7.4 <7.4 <7.7 <7.4 <7.4 47,000
Methylene Chloride <151 <7.1 10.5 10.9 <7.1 13.6 53,000
Naphthalene <114 <5.4 <5.4 <5.6 <5.4 <5.4 260
Propylene 466 305 E 6,470 9.2 194 E 2,920 260,000
Styrene <37 6.6 62.4 12 17.9 10.1 88,000
Tetrachloroethene <29.4 <1.4 <1.4 <1.4 7.1 14.8 3,500
Tetrahydrofuran <25.6 <1.2 <1.2 <1.3 <1.2 <1.2 180,000
Toluene 300 167 188 122 221 412 440,000
Trichloroethene <23.3 <1.1 <1.1 <1.1 <1.1 2.2 180
Trichlorofluoromethane <48.7 <2.3 <2.3 <2.4 <2.3 2.7 NE
Vinyl acetate <76.4 <1.4 <1.4 <1.5 <1.4 <1.4 18,000
Vinyl chloride <11.1 1.1 4.6 <0.55 2.2 <0.53 2,800
cis-1,2-Dichloroethene <34.4 <1.6 <1.6 <1.7 <1.6 <1.6 NE
cis-1,3-Dichloropropene <39.4 <1.9 <1.9 <1.9 <1.9 <1.9 NE
m&p-Xylene 266 94.8 109 77.3 145 204 8,800
n-Heptane <35.6 36.6 66.9 16.4 48 133 35,000
n-Hexane 86.8 69.3 170 15.5 51.3 359 61,000
o-Xylene 80.2 26.6 28.2 21.7 41.8 65.9 8,800
trans-1,2-Dichloroethene <34.4 <1.6 <1.6 <1.7 <1.6 <1.6 NE
trans-1,3-Dichloropropene <39.4 <1.9 <1.9 <1.9 <1.9 <1.9 1,800
Notes:
ug/m3 = milligram per kilogram
< # = Not detected above the Reporting Limit (RL)
E = Analyte concentration exceeded the calibration range, the reported result is estimated
Bolded Values = Concentrations detected above their respective IHSB Non-Residential Soil Gas Screening Limits (February 2018)
Non-Residential Soil Gas
Screening Level
EPA METHOD TO-15 (ug/m3)
TABLE 5
SOIL GAS ANALYTICAL RESULTS - BUILDING 4
JULY 2019
TW ALEXANDER FLEX, SOIL GAS SAMPLING (NCBP Project No. 23016-19-032)
DURHAM, NORTH CAROLINA
MCADAMS PROJECT NO. MPP-18020
SAMPLE ID SG-3 1'SG-8 1'SG-10 1'SG-12 1'SG-DUP-1*SG-15 1'SG-18 1'SG-19 1'SG-24 1'BLDG-1 BLDG-2 BLDG-3 BLDG-DUP-1*BLDG-4
DATE SAMPLED 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019 7/10/2019
SAMPLE DEPTH (FT BLS)1 1 1 1 1 1 1 1 1 1 - 2 0 - 6 0 - 6 0 - 6 0 - 6
EPA METHOD 8260D (mg/kg)
Acetone <0.0906 <0.0886 <0.105 <0.094 <0.105 <0.0856 <0.0998 0.118 <0.09 NA NA NA NA NA 140,000 25 ----
EPA METHOD 8270E (mg/kg)
NO COMPOUNDS DETECTED NA NA NA NA NA NA NA NA NA --------
EPA METHOD 6010D, 7471B, and 7199A (mg/kg)
Arsenic (Total)NA NA NA NA NA NA NA NA NA 1.4 1.7 1.4 1.8 0.92 M1 3.0 5.8 1.0 - 18 4.8
Barium (Total)NA NA NA NA NA NA NA NA NA 53.6 37.9 138 76 64.3 47,000 580 50 - 1,000 356
Chromium (Total)(1)NA NA NA NA NA NA NA NA NA 12.3 14.7 27.2 11.5 10.7 ----7.0 - 300 65
Hexavalent Chromium(1)NA NA NA NA NA NA NA NA NA NA NA 2.2 NA NA 6.5 3.8 ----
Trivalent Chromium(1)NA NA NA NA NA NA NA NA NA NE NE 25 NE NE 350,000 360,000 ----
Lead (Total)NA NA NA NA NA NA NA NA NA 6.9 9.1 15 11.6 11.5 800 270 Non-Detect - 50 16
Mercury (Total)NA NA NA NA NA NA NA NA NA 0.014 <0.0047 0.0088 <0.0038 0.0096 9.7 1.0 0.03 - 0.52 0.121
Selenium (Total)NA NA NA NA NA NA NA NA NA <0.97 <1.0 1.2 <1.1 <0.87 M1 1,200 2.1 Non-detect - 0.8 0.42
Notes:
mg/kg = milligram per kilogram
FT BLS = feet below land surface
NA = Not Analyzed
NE = Not Estimated
< # = Not detected above the reporting limit (RL)
SG-DUP-1 is a duplicate of SG-12 1'; BLDG-SUP-1 is a duplicate of BLGD-3
MS-1 = Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery
Bolded Values = Concentrations detected above their respective Industrial/Commercial PSRG
Underlined Values = Concentrations detected above their respective Protection of Groundwater PSRG
(1) Trivalent Chromium concentration was estimated by subtracting Hexavalent Chromium concentration
(2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005
TABLE 6
SOIL ANALYTICAL RESULTS
JULY 2019
TW ALEXANDER FLEX, SOIL GAS SAMPLING (NCBP Project No. 23016-19-032)
DURHAM, NORTH CAROLINA
MCADAMS PROJECT NO. MPP-18020
NO COMPOUNDS DETECTED
Ind./Comm. PSRG Protection of
Groundwater PSRG
Inactive Hazardous Sites Branch PSRGs (May
2019)Regional Background Metals in Soil(2)
Range Mean
BUILDING 1 BUILDING 3 BUILDING 4BUILDING 2

APPENDIX A
777
77107107207310
280
26
<0.15
0.59<0.15
5.9 (5/16)
<0.5 (5/16)
<1 (historical)
29
370
0.43J
3.6
1.4 190
MW-1
MW-2
MW-3
MW-5MW-7
MW-8
MW-9
MW-10
MW-11 MW-12
MW-14
MW-15
EMW-1
EMW-2
EMW-3
CW-3S
AD-50
M-1-55
M-2-100
M-3-50
M-5-50
M-6-55
M-10-50
CW-6S
MW-19
M-4-150
M-4-50R
MW-6
MW-22 MW-21
MW-20
CW-5S
CW-4Dike
CW-4S
MW-16S
W-AW-01
9G1859
9G1858
9G1857
9G1856
9G1855
9G1801
SW-2
SW-3
9G1800
9G1802
X XXX
0 175 350
Abandoned
Water Supply
LEGEND
Monitor Well, Shallow
Monitor Well, Deep
Surface Water Sample Location
Groundwater Flow DirectionProperty LineSanitary SewerStorm SewerSurface Water
Conc. Units =ug/L
NC2L Std. Contour is Bold
DATE:
DRAWN BY:
LOCATION: P:\Comm-Ind\Projects\Clients A to F\demaximis
SCALE:
CHECKED BY:
PROJECT:1" = 350'
J. Smith S. Knox
6480177131
demaximis, inc.CLIENT:
SITE:
TITLE:FIGURE
7b1/30/2018Edward Weck, Inc.2917 Weck Drive, Durham, NCNCD001493931
Amec Foster WheelerEnvironment & Infrastructure, Inc.4021 Stirrup Creek Drive, Suite 100
Durham, NC 27703(919) 381-9900
Weck Site
IBM M-Area
Stirrup IronCreek
Diabase Dike
Diabase Dike
Fault
UWBZ DCE Isoconcentration Map
NC2L = 350 ug/L
November 2017
7
27
47
67
87
107
127
147
167
187
207
227
247
267
287
307
327
DCE ug/L

APPENDIX B
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APPENDIX C
#=CL#
August 02, 2019
LIMS USE: FR - ERIC HOWARD
LIMS OBJECT ID: 92436815
92436815
Project:
Pace Project No.:
RE:
Eric Howard
McAdams Co
2905 Meridian Parkway
Durham, NC 27713
MPP18020; Soil Gas Sampling
Dear Eric Howard:
Enclosed are the analytical results for sample(s) received by the laboratory on July 15, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
cc:Vicky Garlington, McAdams Co
Accounts Payable, McAdams Co
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 81
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
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Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 81
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92436815001 SG-24 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815002 SG-19 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815003 SG-3 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815004 SG-8 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815005 SG-10 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815006 SG-15 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815007 SG-18 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815008 SG-12 1'EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815009 SG-DUP-1 EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92436815010 TRIP BLANK EPA 8260D 63 PASI-CCL
92436815011 BLDG-4 EPA 6010D 7 PASI-ADS
EPA 7471B 1 PASI-AJMW1
EPA 8270E 150 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92436815012 BLDG-1 EPA 6010D 7 PASI-ADS
EPA 7471B 1 PASI-AJMW1
EPA 8270E 150 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92436815013 BLDG-3 EPA 6010D 7 PASI-ADS
EPA 7471B 1 PASI-AJMW1
EPA 8270E 150 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
EPA 7199 1 PASI-OALD
92436815014 BLDG-2 EPA 6010D 7 PASI-ADS
EPA 7471B 1 PASI-AJMW1
EPA 8270E 150 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
92436815015 BLDG-DUP-1 EPA 6010D 7 PASI-ADS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 81
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7471B 1 PASI-AJMW1
EPA 8270E 150 PASI-CBPJ
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-24 1'Lab ID:92436815001 Collected:07/10/19 09:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/16/19 18:36 67-64-107/16/19 13:3990.0 1
Benzene ND ug/kg 07/16/19 18:36 71-43-207/16/19 13:394.5 1
Bromobenzene ND ug/kg 07/16/19 18:36 108-86-107/16/19 13:394.5 1
Bromochloromethane ND ug/kg 07/16/19 18:36 74-97-507/16/19 13:394.5 1
Bromodichloromethane ND ug/kg 07/16/19 18:36 75-27-407/16/19 13:394.5 1
Bromoform ND ug/kg 07/16/19 18:36 75-25-207/16/19 13:394.5 1
Bromomethane ND ug/kg 07/16/19 18:36 74-83-907/16/19 13:399.0 1
2-Butanone (MEK)ND ug/kg 07/16/19 18:36 78-93-307/16/19 13:3990.0 1
n-Butylbenzene ND ug/kg 07/16/19 18:36 104-51-807/16/19 13:394.5 1
sec-Butylbenzene ND ug/kg 07/16/19 18:36 135-98-807/16/19 13:394.5 1
tert-Butylbenzene ND ug/kg 07/16/19 18:36 98-06-607/16/19 13:394.5 1
Carbon tetrachloride ND ug/kg 07/16/19 18:36 56-23-507/16/19 13:394.5 1
Chlorobenzene ND ug/kg 07/16/19 18:36 108-90-707/16/19 13:394.5 1
Chloroethane ND ug/kg 07/16/19 18:36 75-00-307/16/19 13:399.0 1
Chloroform ND ug/kg 07/16/19 18:36 67-66-307/16/19 13:394.5 1
Chloromethane ND ug/kg 07/16/19 18:36 74-87-307/16/19 13:399.0 1
2-Chlorotoluene ND ug/kg 07/16/19 18:36 95-49-807/16/19 13:394.5 1
4-Chlorotoluene ND ug/kg 07/16/19 18:36 106-43-407/16/19 13:394.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/16/19 18:36 96-12-807/16/19 13:394.5 1
Dibromochloromethane ND ug/kg 07/16/19 18:36 124-48-107/16/19 13:394.5 1
1,2-Dibromoethane (EDB)ND ug/kg 07/16/19 18:36 106-93-407/16/19 13:394.5 1
Dibromomethane ND ug/kg 07/16/19 18:36 74-95-307/16/19 13:394.5 1
1,2-Dichlorobenzene ND ug/kg 07/16/19 18:36 95-50-107/16/19 13:394.5 1
1,3-Dichlorobenzene ND ug/kg 07/16/19 18:36 541-73-107/16/19 13:394.5 1
1,4-Dichlorobenzene ND ug/kg 07/16/19 18:36 106-46-707/16/19 13:394.5 1
Dichlorodifluoromethane ND ug/kg 07/16/19 18:36 75-71-807/16/19 13:399.0 1
1,1-Dichloroethane ND ug/kg 07/16/19 18:36 75-34-307/16/19 13:394.5 1
1,2-Dichloroethane ND ug/kg 07/16/19 18:36 107-06-207/16/19 13:394.5 1
1,1-Dichloroethene ND ug/kg 07/16/19 18:36 75-35-407/16/19 13:394.5 1
cis-1,2-Dichloroethene ND ug/kg 07/16/19 18:36 156-59-207/16/19 13:394.5 1
trans-1,2-Dichloroethene ND ug/kg 07/16/19 18:36 156-60-507/16/19 13:394.5 1
1,2-Dichloropropane ND ug/kg 07/16/19 18:36 78-87-507/16/19 13:394.5 1
1,3-Dichloropropane ND ug/kg 07/16/19 18:36 142-28-907/16/19 13:394.5 1
2,2-Dichloropropane ND ug/kg 07/16/19 18:36 594-20-707/16/19 13:394.5 1
1,1-Dichloropropene ND ug/kg 07/16/19 18:36 563-58-607/16/19 13:394.5 1
cis-1,3-Dichloropropene ND ug/kg 07/16/19 18:36 10061-01-507/16/19 13:394.5 1
trans-1,3-Dichloropropene ND ug/kg 07/16/19 18:36 10061-02-607/16/19 13:394.5 1
Diisopropyl ether ND ug/kg 07/16/19 18:36 108-20-307/16/19 13:394.5 1
Ethylbenzene ND ug/kg 07/16/19 18:36 100-41-407/16/19 13:394.5 1
Hexachloro-1,3-butadiene ND ug/kg 07/16/19 18:36 87-68-307/16/19 13:394.5 1
2-Hexanone ND ug/kg 07/16/19 18:36 591-78-607/16/19 13:3945.0 1
Isopropylbenzene (Cumene)ND ug/kg 07/16/19 18:36 98-82-807/16/19 13:394.5 1
p-Isopropyltoluene ND ug/kg 07/16/19 18:36 99-87-607/16/19 13:394.5 1
Methylene Chloride ND ug/kg 07/16/19 18:36 75-09-2 v207/16/19 13:3918.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/16/19 18:36 108-10-107/16/19 13:3945.0 1
Methyl-tert-butyl ether ND ug/kg 07/16/19 18:36 1634-04-407/16/19 13:394.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-24 1'Lab ID:92436815001 Collected:07/10/19 09:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/16/19 18:36 91-20-307/16/19 13:394.5 1
n-Propylbenzene ND ug/kg 07/16/19 18:36 103-65-107/16/19 13:394.5 1
Styrene ND ug/kg 07/16/19 18:36 100-42-507/16/19 13:394.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/16/19 18:36 630-20-607/16/19 13:394.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/16/19 18:36 79-34-507/16/19 13:394.5 1
Tetrachloroethene ND ug/kg 07/16/19 18:36 127-18-407/16/19 13:394.5 1
Toluene ND ug/kg 07/16/19 18:36 108-88-307/16/19 13:394.5 1
1,2,3-Trichlorobenzene ND ug/kg 07/16/19 18:36 87-61-607/16/19 13:394.5 1
1,2,4-Trichlorobenzene ND ug/kg 07/16/19 18:36 120-82-107/16/19 13:394.5 1
1,1,1-Trichloroethane ND ug/kg 07/16/19 18:36 71-55-607/16/19 13:394.5 1
1,1,2-Trichloroethane ND ug/kg 07/16/19 18:36 79-00-507/16/19 13:394.5 1
Trichloroethene ND ug/kg 07/16/19 18:36 79-01-607/16/19 13:394.5 1
Trichlorofluoromethane ND ug/kg 07/16/19 18:36 75-69-407/16/19 13:394.5 1
1,2,3-Trichloropropane ND ug/kg 07/16/19 18:36 96-18-407/16/19 13:394.5 1
1,2,4-Trimethylbenzene ND ug/kg 07/16/19 18:36 95-63-607/16/19 13:394.5 1
1,3,5-Trimethylbenzene ND ug/kg 07/16/19 18:36 108-67-807/16/19 13:394.5 1
Vinyl acetate ND ug/kg 07/16/19 18:36 108-05-407/16/19 13:3945.0 1
Vinyl chloride ND ug/kg 07/16/19 18:36 75-01-407/16/19 13:399.0 1
Xylene (Total)ND ug/kg 07/16/19 18:36 1330-20-707/16/19 13:399.0 1
m&p-Xylene ND ug/kg 07/16/19 18:36 179601-23-107/16/19 13:399.0 1
o-Xylene ND ug/kg 07/16/19 18:36 95-47-607/16/19 13:394.5 1
Surrogates
Toluene-d8 (S)99 %07/16/19 18:36 2037-26-507/16/19 13:3970-130 1
4-Bromofluorobenzene (S)103 %07/16/19 18:36 460-00-407/16/19 13:3970-130 1
1,2-Dichloroethane-d4 (S)106 %07/16/19 18:36 17060-07-007/16/19 13:3970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.9 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-19 1'Lab ID:92436815002 Collected:07/10/19 11:15 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone 118 ug/kg 07/16/19 19:02 67-64-107/16/19 13:3986.9 1
Benzene ND ug/kg 07/16/19 19:02 71-43-207/16/19 13:394.3 1
Bromobenzene ND ug/kg 07/16/19 19:02 108-86-107/16/19 13:394.3 1
Bromochloromethane ND ug/kg 07/16/19 19:02 74-97-507/16/19 13:394.3 1
Bromodichloromethane ND ug/kg 07/16/19 19:02 75-27-407/16/19 13:394.3 1
Bromoform ND ug/kg 07/16/19 19:02 75-25-207/16/19 13:394.3 1
Bromomethane ND ug/kg 07/16/19 19:02 74-83-907/16/19 13:398.7 1
2-Butanone (MEK)ND ug/kg 07/16/19 19:02 78-93-307/16/19 13:3986.9 1
n-Butylbenzene ND ug/kg 07/16/19 19:02 104-51-807/16/19 13:394.3 1
sec-Butylbenzene ND ug/kg 07/16/19 19:02 135-98-807/16/19 13:394.3 1
tert-Butylbenzene ND ug/kg 07/16/19 19:02 98-06-607/16/19 13:394.3 1
Carbon tetrachloride ND ug/kg 07/16/19 19:02 56-23-507/16/19 13:394.3 1
Chlorobenzene ND ug/kg 07/16/19 19:02 108-90-707/16/19 13:394.3 1
Chloroethane ND ug/kg 07/16/19 19:02 75-00-307/16/19 13:398.7 1
Chloroform ND ug/kg 07/16/19 19:02 67-66-307/16/19 13:394.3 1
Chloromethane ND ug/kg 07/16/19 19:02 74-87-307/16/19 13:398.7 1
2-Chlorotoluene ND ug/kg 07/16/19 19:02 95-49-807/16/19 13:394.3 1
4-Chlorotoluene ND ug/kg 07/16/19 19:02 106-43-407/16/19 13:394.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/16/19 19:02 96-12-807/16/19 13:394.3 1
Dibromochloromethane ND ug/kg 07/16/19 19:02 124-48-107/16/19 13:394.3 1
1,2-Dibromoethane (EDB)ND ug/kg 07/16/19 19:02 106-93-407/16/19 13:394.3 1
Dibromomethane ND ug/kg 07/16/19 19:02 74-95-307/16/19 13:394.3 1
1,2-Dichlorobenzene ND ug/kg 07/16/19 19:02 95-50-107/16/19 13:394.3 1
1,3-Dichlorobenzene ND ug/kg 07/16/19 19:02 541-73-107/16/19 13:394.3 1
1,4-Dichlorobenzene ND ug/kg 07/16/19 19:02 106-46-707/16/19 13:394.3 1
Dichlorodifluoromethane ND ug/kg 07/16/19 19:02 75-71-807/16/19 13:398.7 1
1,1-Dichloroethane ND ug/kg 07/16/19 19:02 75-34-307/16/19 13:394.3 1
1,2-Dichloroethane ND ug/kg 07/16/19 19:02 107-06-207/16/19 13:394.3 1
1,1-Dichloroethene ND ug/kg 07/16/19 19:02 75-35-407/16/19 13:394.3 1
cis-1,2-Dichloroethene ND ug/kg 07/16/19 19:02 156-59-207/16/19 13:394.3 1
trans-1,2-Dichloroethene ND ug/kg 07/16/19 19:02 156-60-507/16/19 13:394.3 1
1,2-Dichloropropane ND ug/kg 07/16/19 19:02 78-87-507/16/19 13:394.3 1
1,3-Dichloropropane ND ug/kg 07/16/19 19:02 142-28-907/16/19 13:394.3 1
2,2-Dichloropropane ND ug/kg 07/16/19 19:02 594-20-707/16/19 13:394.3 1
1,1-Dichloropropene ND ug/kg 07/16/19 19:02 563-58-607/16/19 13:394.3 1
cis-1,3-Dichloropropene ND ug/kg 07/16/19 19:02 10061-01-507/16/19 13:394.3 1
trans-1,3-Dichloropropene ND ug/kg 07/16/19 19:02 10061-02-607/16/19 13:394.3 1
Diisopropyl ether ND ug/kg 07/16/19 19:02 108-20-307/16/19 13:394.3 1
Ethylbenzene ND ug/kg 07/16/19 19:02 100-41-407/16/19 13:394.3 1
Hexachloro-1,3-butadiene ND ug/kg 07/16/19 19:02 87-68-307/16/19 13:394.3 1
2-Hexanone ND ug/kg 07/16/19 19:02 591-78-607/16/19 13:3943.4 1
Isopropylbenzene (Cumene)ND ug/kg 07/16/19 19:02 98-82-807/16/19 13:394.3 1
p-Isopropyltoluene ND ug/kg 07/16/19 19:02 99-87-607/16/19 13:394.3 1
Methylene Chloride ND ug/kg 07/16/19 19:02 75-09-2 v207/16/19 13:3917.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/16/19 19:02 108-10-107/16/19 13:3943.4 1
Methyl-tert-butyl ether ND ug/kg 07/16/19 19:02 1634-04-407/16/19 13:394.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-19 1'Lab ID:92436815002 Collected:07/10/19 11:15 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/16/19 19:02 91-20-307/16/19 13:394.3 1
n-Propylbenzene ND ug/kg 07/16/19 19:02 103-65-107/16/19 13:394.3 1
Styrene ND ug/kg 07/16/19 19:02 100-42-507/16/19 13:394.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/16/19 19:02 630-20-607/16/19 13:394.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/16/19 19:02 79-34-507/16/19 13:394.3 1
Tetrachloroethene ND ug/kg 07/16/19 19:02 127-18-407/16/19 13:394.3 1
Toluene ND ug/kg 07/16/19 19:02 108-88-307/16/19 13:394.3 1
1,2,3-Trichlorobenzene ND ug/kg 07/16/19 19:02 87-61-607/16/19 13:394.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/16/19 19:02 120-82-107/16/19 13:394.3 1
1,1,1-Trichloroethane ND ug/kg 07/16/19 19:02 71-55-607/16/19 13:394.3 1
1,1,2-Trichloroethane ND ug/kg 07/16/19 19:02 79-00-507/16/19 13:394.3 1
Trichloroethene ND ug/kg 07/16/19 19:02 79-01-607/16/19 13:394.3 1
Trichlorofluoromethane ND ug/kg 07/16/19 19:02 75-69-407/16/19 13:394.3 1
1,2,3-Trichloropropane ND ug/kg 07/16/19 19:02 96-18-407/16/19 13:394.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/16/19 19:02 95-63-607/16/19 13:394.3 1
1,3,5-Trimethylbenzene ND ug/kg 07/16/19 19:02 108-67-807/16/19 13:394.3 1
Vinyl acetate ND ug/kg 07/16/19 19:02 108-05-407/16/19 13:3943.4 1
Vinyl chloride ND ug/kg 07/16/19 19:02 75-01-407/16/19 13:398.7 1
Xylene (Total)ND ug/kg 07/16/19 19:02 1330-20-707/16/19 13:398.7 1
m&p-Xylene ND ug/kg 07/16/19 19:02 179601-23-107/16/19 13:398.7 1
o-Xylene ND ug/kg 07/16/19 19:02 95-47-607/16/19 13:394.3 1
Surrogates
Toluene-d8 (S)99 %07/16/19 19:02 2037-26-507/16/19 13:3970-130 1
4-Bromofluorobenzene (S)101 %07/16/19 19:02 460-00-407/16/19 13:3970-130 1
1,2-Dichloroethane-d4 (S)103 %07/16/19 19:02 17060-07-007/16/19 13:3970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.6 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-3 1'Lab ID:92436815003 Collected:07/10/19 13:40 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/16/19 19:27 67-64-107/16/19 13:3990.6 1
Benzene ND ug/kg 07/16/19 19:27 71-43-207/16/19 13:394.5 1
Bromobenzene ND ug/kg 07/16/19 19:27 108-86-107/16/19 13:394.5 1
Bromochloromethane ND ug/kg 07/16/19 19:27 74-97-507/16/19 13:394.5 1
Bromodichloromethane ND ug/kg 07/16/19 19:27 75-27-407/16/19 13:394.5 1
Bromoform ND ug/kg 07/16/19 19:27 75-25-207/16/19 13:394.5 1
Bromomethane ND ug/kg 07/16/19 19:27 74-83-907/16/19 13:399.1 1
2-Butanone (MEK)ND ug/kg 07/16/19 19:27 78-93-307/16/19 13:3990.6 1
n-Butylbenzene ND ug/kg 07/16/19 19:27 104-51-807/16/19 13:394.5 1
sec-Butylbenzene ND ug/kg 07/16/19 19:27 135-98-807/16/19 13:394.5 1
tert-Butylbenzene ND ug/kg 07/16/19 19:27 98-06-607/16/19 13:394.5 1
Carbon tetrachloride ND ug/kg 07/16/19 19:27 56-23-507/16/19 13:394.5 1
Chlorobenzene ND ug/kg 07/16/19 19:27 108-90-707/16/19 13:394.5 1
Chloroethane ND ug/kg 07/16/19 19:27 75-00-307/16/19 13:399.1 1
Chloroform ND ug/kg 07/16/19 19:27 67-66-307/16/19 13:394.5 1
Chloromethane ND ug/kg 07/16/19 19:27 74-87-307/16/19 13:399.1 1
2-Chlorotoluene ND ug/kg 07/16/19 19:27 95-49-807/16/19 13:394.5 1
4-Chlorotoluene ND ug/kg 07/16/19 19:27 106-43-407/16/19 13:394.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/16/19 19:27 96-12-807/16/19 13:394.5 1
Dibromochloromethane ND ug/kg 07/16/19 19:27 124-48-107/16/19 13:394.5 1
1,2-Dibromoethane (EDB)ND ug/kg 07/16/19 19:27 106-93-407/16/19 13:394.5 1
Dibromomethane ND ug/kg 07/16/19 19:27 74-95-307/16/19 13:394.5 1
1,2-Dichlorobenzene ND ug/kg 07/16/19 19:27 95-50-107/16/19 13:394.5 1
1,3-Dichlorobenzene ND ug/kg 07/16/19 19:27 541-73-107/16/19 13:394.5 1
1,4-Dichlorobenzene ND ug/kg 07/16/19 19:27 106-46-707/16/19 13:394.5 1
Dichlorodifluoromethane ND ug/kg 07/16/19 19:27 75-71-807/16/19 13:399.1 1
1,1-Dichloroethane ND ug/kg 07/16/19 19:27 75-34-307/16/19 13:394.5 1
1,2-Dichloroethane ND ug/kg 07/16/19 19:27 107-06-207/16/19 13:394.5 1
1,1-Dichloroethene ND ug/kg 07/16/19 19:27 75-35-407/16/19 13:394.5 1
cis-1,2-Dichloroethene ND ug/kg 07/16/19 19:27 156-59-207/16/19 13:394.5 1
trans-1,2-Dichloroethene ND ug/kg 07/16/19 19:27 156-60-507/16/19 13:394.5 1
1,2-Dichloropropane ND ug/kg 07/16/19 19:27 78-87-507/16/19 13:394.5 1
1,3-Dichloropropane ND ug/kg 07/16/19 19:27 142-28-907/16/19 13:394.5 1
2,2-Dichloropropane ND ug/kg 07/16/19 19:27 594-20-707/16/19 13:394.5 1
1,1-Dichloropropene ND ug/kg 07/16/19 19:27 563-58-607/16/19 13:394.5 1
cis-1,3-Dichloropropene ND ug/kg 07/16/19 19:27 10061-01-507/16/19 13:394.5 1
trans-1,3-Dichloropropene ND ug/kg 07/16/19 19:27 10061-02-607/16/19 13:394.5 1
Diisopropyl ether ND ug/kg 07/16/19 19:27 108-20-307/16/19 13:394.5 1
Ethylbenzene ND ug/kg 07/16/19 19:27 100-41-407/16/19 13:394.5 1
Hexachloro-1,3-butadiene ND ug/kg 07/16/19 19:27 87-68-307/16/19 13:394.5 1
2-Hexanone ND ug/kg 07/16/19 19:27 591-78-607/16/19 13:3945.3 1
Isopropylbenzene (Cumene)ND ug/kg 07/16/19 19:27 98-82-807/16/19 13:394.5 1
p-Isopropyltoluene ND ug/kg 07/16/19 19:27 99-87-607/16/19 13:394.5 1
Methylene Chloride ND ug/kg 07/16/19 19:27 75-09-2 v207/16/19 13:3918.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/16/19 19:27 108-10-107/16/19 13:3945.3 1
Methyl-tert-butyl ether ND ug/kg 07/16/19 19:27 1634-04-407/16/19 13:394.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-3 1'Lab ID:92436815003 Collected:07/10/19 13:40 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/16/19 19:27 91-20-307/16/19 13:394.5 1
n-Propylbenzene ND ug/kg 07/16/19 19:27 103-65-107/16/19 13:394.5 1
Styrene ND ug/kg 07/16/19 19:27 100-42-507/16/19 13:394.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/16/19 19:27 630-20-607/16/19 13:394.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/16/19 19:27 79-34-507/16/19 13:394.5 1
Tetrachloroethene ND ug/kg 07/16/19 19:27 127-18-407/16/19 13:394.5 1
Toluene ND ug/kg 07/16/19 19:27 108-88-307/16/19 13:394.5 1
1,2,3-Trichlorobenzene ND ug/kg 07/16/19 19:27 87-61-607/16/19 13:394.5 1
1,2,4-Trichlorobenzene ND ug/kg 07/16/19 19:27 120-82-107/16/19 13:394.5 1
1,1,1-Trichloroethane ND ug/kg 07/16/19 19:27 71-55-607/16/19 13:394.5 1
1,1,2-Trichloroethane ND ug/kg 07/16/19 19:27 79-00-507/16/19 13:394.5 1
Trichloroethene ND ug/kg 07/16/19 19:27 79-01-607/16/19 13:394.5 1
Trichlorofluoromethane ND ug/kg 07/16/19 19:27 75-69-407/16/19 13:394.5 1
1,2,3-Trichloropropane ND ug/kg 07/16/19 19:27 96-18-407/16/19 13:394.5 1
1,2,4-Trimethylbenzene ND ug/kg 07/16/19 19:27 95-63-607/16/19 13:394.5 1
1,3,5-Trimethylbenzene ND ug/kg 07/16/19 19:27 108-67-807/16/19 13:394.5 1
Vinyl acetate ND ug/kg 07/16/19 19:27 108-05-407/16/19 13:3945.3 1
Vinyl chloride ND ug/kg 07/16/19 19:27 75-01-407/16/19 13:399.1 1
Xylene (Total)ND ug/kg 07/16/19 19:27 1330-20-707/16/19 13:399.1 1
m&p-Xylene ND ug/kg 07/16/19 19:27 179601-23-107/16/19 13:399.1 1
o-Xylene ND ug/kg 07/16/19 19:27 95-47-607/16/19 13:394.5 1
Surrogates
Toluene-d8 (S)101 %07/16/19 19:27 2037-26-507/16/19 13:3970-130 1
4-Bromofluorobenzene (S)105 %07/16/19 19:27 460-00-407/16/19 13:3970-130 1
1,2-Dichloroethane-d4 (S)103 %07/16/19 19:27 17060-07-007/16/19 13:3970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.3 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-8 1'Lab ID:92436815004 Collected:07/10/19 14:15 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/16/19 19:53 67-64-107/16/19 13:3988.6 1
Benzene ND ug/kg 07/16/19 19:53 71-43-207/16/19 13:394.4 1
Bromobenzene ND ug/kg 07/16/19 19:53 108-86-107/16/19 13:394.4 1
Bromochloromethane ND ug/kg 07/16/19 19:53 74-97-507/16/19 13:394.4 1
Bromodichloromethane ND ug/kg 07/16/19 19:53 75-27-407/16/19 13:394.4 1
Bromoform ND ug/kg 07/16/19 19:53 75-25-207/16/19 13:394.4 1
Bromomethane ND ug/kg 07/16/19 19:53 74-83-907/16/19 13:398.9 1
2-Butanone (MEK)ND ug/kg 07/16/19 19:53 78-93-307/16/19 13:3988.6 1
n-Butylbenzene ND ug/kg 07/16/19 19:53 104-51-807/16/19 13:394.4 1
sec-Butylbenzene ND ug/kg 07/16/19 19:53 135-98-807/16/19 13:394.4 1
tert-Butylbenzene ND ug/kg 07/16/19 19:53 98-06-607/16/19 13:394.4 1
Carbon tetrachloride ND ug/kg 07/16/19 19:53 56-23-507/16/19 13:394.4 1
Chlorobenzene ND ug/kg 07/16/19 19:53 108-90-707/16/19 13:394.4 1
Chloroethane ND ug/kg 07/16/19 19:53 75-00-307/16/19 13:398.9 1
Chloroform ND ug/kg 07/16/19 19:53 67-66-307/16/19 13:394.4 1
Chloromethane ND ug/kg 07/16/19 19:53 74-87-307/16/19 13:398.9 1
2-Chlorotoluene ND ug/kg 07/16/19 19:53 95-49-807/16/19 13:394.4 1
4-Chlorotoluene ND ug/kg 07/16/19 19:53 106-43-407/16/19 13:394.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/16/19 19:53 96-12-807/16/19 13:394.4 1
Dibromochloromethane ND ug/kg 07/16/19 19:53 124-48-107/16/19 13:394.4 1
1,2-Dibromoethane (EDB)ND ug/kg 07/16/19 19:53 106-93-407/16/19 13:394.4 1
Dibromomethane ND ug/kg 07/16/19 19:53 74-95-307/16/19 13:394.4 1
1,2-Dichlorobenzene ND ug/kg 07/16/19 19:53 95-50-107/16/19 13:394.4 1
1,3-Dichlorobenzene ND ug/kg 07/16/19 19:53 541-73-107/16/19 13:394.4 1
1,4-Dichlorobenzene ND ug/kg 07/16/19 19:53 106-46-707/16/19 13:394.4 1
Dichlorodifluoromethane ND ug/kg 07/16/19 19:53 75-71-807/16/19 13:398.9 1
1,1-Dichloroethane ND ug/kg 07/16/19 19:53 75-34-307/16/19 13:394.4 1
1,2-Dichloroethane ND ug/kg 07/16/19 19:53 107-06-207/16/19 13:394.4 1
1,1-Dichloroethene ND ug/kg 07/16/19 19:53 75-35-407/16/19 13:394.4 1
cis-1,2-Dichloroethene ND ug/kg 07/16/19 19:53 156-59-207/16/19 13:394.4 1
trans-1,2-Dichloroethene ND ug/kg 07/16/19 19:53 156-60-507/16/19 13:394.4 1
1,2-Dichloropropane ND ug/kg 07/16/19 19:53 78-87-507/16/19 13:394.4 1
1,3-Dichloropropane ND ug/kg 07/16/19 19:53 142-28-907/16/19 13:394.4 1
2,2-Dichloropropane ND ug/kg 07/16/19 19:53 594-20-707/16/19 13:394.4 1
1,1-Dichloropropene ND ug/kg 07/16/19 19:53 563-58-607/16/19 13:394.4 1
cis-1,3-Dichloropropene ND ug/kg 07/16/19 19:53 10061-01-507/16/19 13:394.4 1
trans-1,3-Dichloropropene ND ug/kg 07/16/19 19:53 10061-02-607/16/19 13:394.4 1
Diisopropyl ether ND ug/kg 07/16/19 19:53 108-20-307/16/19 13:394.4 1
Ethylbenzene ND ug/kg 07/16/19 19:53 100-41-407/16/19 13:394.4 1
Hexachloro-1,3-butadiene ND ug/kg 07/16/19 19:53 87-68-307/16/19 13:394.4 1
2-Hexanone ND ug/kg 07/16/19 19:53 591-78-607/16/19 13:3944.3 1
Isopropylbenzene (Cumene)ND ug/kg 07/16/19 19:53 98-82-807/16/19 13:394.4 1
p-Isopropyltoluene ND ug/kg 07/16/19 19:53 99-87-607/16/19 13:394.4 1
Methylene Chloride ND ug/kg 07/16/19 19:53 75-09-2 v207/16/19 13:3917.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/16/19 19:53 108-10-107/16/19 13:3944.3 1
Methyl-tert-butyl ether ND ug/kg 07/16/19 19:53 1634-04-407/16/19 13:394.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-8 1'Lab ID:92436815004 Collected:07/10/19 14:15 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/16/19 19:53 91-20-307/16/19 13:394.4 1
n-Propylbenzene ND ug/kg 07/16/19 19:53 103-65-107/16/19 13:394.4 1
Styrene ND ug/kg 07/16/19 19:53 100-42-507/16/19 13:394.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/16/19 19:53 630-20-607/16/19 13:394.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/16/19 19:53 79-34-507/16/19 13:394.4 1
Tetrachloroethene ND ug/kg 07/16/19 19:53 127-18-407/16/19 13:394.4 1
Toluene ND ug/kg 07/16/19 19:53 108-88-307/16/19 13:394.4 1
1,2,3-Trichlorobenzene ND ug/kg 07/16/19 19:53 87-61-607/16/19 13:394.4 1
1,2,4-Trichlorobenzene ND ug/kg 07/16/19 19:53 120-82-107/16/19 13:394.4 1
1,1,1-Trichloroethane ND ug/kg 07/16/19 19:53 71-55-607/16/19 13:394.4 1
1,1,2-Trichloroethane ND ug/kg 07/16/19 19:53 79-00-507/16/19 13:394.4 1
Trichloroethene ND ug/kg 07/16/19 19:53 79-01-607/16/19 13:394.4 1
Trichlorofluoromethane ND ug/kg 07/16/19 19:53 75-69-407/16/19 13:394.4 1
1,2,3-Trichloropropane ND ug/kg 07/16/19 19:53 96-18-407/16/19 13:394.4 1
1,2,4-Trimethylbenzene ND ug/kg 07/16/19 19:53 95-63-607/16/19 13:394.4 1
1,3,5-Trimethylbenzene ND ug/kg 07/16/19 19:53 108-67-807/16/19 13:394.4 1
Vinyl acetate ND ug/kg 07/16/19 19:53 108-05-407/16/19 13:3944.3 1
Vinyl chloride ND ug/kg 07/16/19 19:53 75-01-407/16/19 13:398.9 1
Xylene (Total)ND ug/kg 07/16/19 19:53 1330-20-707/16/19 13:398.9 1
m&p-Xylene ND ug/kg 07/16/19 19:53 179601-23-107/16/19 13:398.9 1
o-Xylene ND ug/kg 07/16/19 19:53 95-47-607/16/19 13:394.4 1
Surrogates
Toluene-d8 (S)101 %07/16/19 19:53 2037-26-507/16/19 13:3970-130 1
4-Bromofluorobenzene (S)103 %07/16/19 19:53 460-00-407/16/19 13:3970-130 1
1,2-Dichloroethane-d4 (S)103 %07/16/19 19:53 17060-07-007/16/19 13:3970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.8 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-10 1'Lab ID:92436815005 Collected:07/11/19 09:10 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/16/19 20:18 67-64-107/16/19 13:391051
Benzene ND ug/kg 07/16/19 20:18 71-43-207/16/19 13:395.3 1
Bromobenzene ND ug/kg 07/16/19 20:18 108-86-107/16/19 13:395.3 1
Bromochloromethane ND ug/kg 07/16/19 20:18 74-97-507/16/19 13:395.3 1
Bromodichloromethane ND ug/kg 07/16/19 20:18 75-27-407/16/19 13:395.3 1
Bromoform ND ug/kg 07/16/19 20:18 75-25-207/16/19 13:395.3 1
Bromomethane ND ug/kg 07/16/19 20:18 74-83-907/16/19 13:3910.5 1
2-Butanone (MEK)ND ug/kg 07/16/19 20:18 78-93-307/16/19 13:391051
n-Butylbenzene ND ug/kg 07/16/19 20:18 104-51-807/16/19 13:395.3 1
sec-Butylbenzene ND ug/kg 07/16/19 20:18 135-98-807/16/19 13:395.3 1
tert-Butylbenzene ND ug/kg 07/16/19 20:18 98-06-607/16/19 13:395.3 1
Carbon tetrachloride ND ug/kg 07/16/19 20:18 56-23-507/16/19 13:395.3 1
Chlorobenzene ND ug/kg 07/16/19 20:18 108-90-707/16/19 13:395.3 1
Chloroethane ND ug/kg 07/16/19 20:18 75-00-307/16/19 13:3910.5 1
Chloroform ND ug/kg 07/16/19 20:18 67-66-307/16/19 13:395.3 1
Chloromethane ND ug/kg 07/16/19 20:18 74-87-307/16/19 13:3910.5 1
2-Chlorotoluene ND ug/kg 07/16/19 20:18 95-49-807/16/19 13:395.3 1
4-Chlorotoluene ND ug/kg 07/16/19 20:18 106-43-407/16/19 13:395.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/16/19 20:18 96-12-807/16/19 13:395.3 1
Dibromochloromethane ND ug/kg 07/16/19 20:18 124-48-107/16/19 13:395.3 1
1,2-Dibromoethane (EDB)ND ug/kg 07/16/19 20:18 106-93-407/16/19 13:395.3 1
Dibromomethane ND ug/kg 07/16/19 20:18 74-95-307/16/19 13:395.3 1
1,2-Dichlorobenzene ND ug/kg 07/16/19 20:18 95-50-107/16/19 13:395.3 1
1,3-Dichlorobenzene ND ug/kg 07/16/19 20:18 541-73-107/16/19 13:395.3 1
1,4-Dichlorobenzene ND ug/kg 07/16/19 20:18 106-46-707/16/19 13:395.3 1
Dichlorodifluoromethane ND ug/kg 07/16/19 20:18 75-71-807/16/19 13:3910.5 1
1,1-Dichloroethane ND ug/kg 07/16/19 20:18 75-34-307/16/19 13:395.3 1
1,2-Dichloroethane ND ug/kg 07/16/19 20:18 107-06-207/16/19 13:395.3 1
1,1-Dichloroethene ND ug/kg 07/16/19 20:18 75-35-407/16/19 13:395.3 1
cis-1,2-Dichloroethene ND ug/kg 07/16/19 20:18 156-59-207/16/19 13:395.3 1
trans-1,2-Dichloroethene ND ug/kg 07/16/19 20:18 156-60-507/16/19 13:395.3 1
1,2-Dichloropropane ND ug/kg 07/16/19 20:18 78-87-507/16/19 13:395.3 1
1,3-Dichloropropane ND ug/kg 07/16/19 20:18 142-28-907/16/19 13:395.3 1
2,2-Dichloropropane ND ug/kg 07/16/19 20:18 594-20-707/16/19 13:395.3 1
1,1-Dichloropropene ND ug/kg 07/16/19 20:18 563-58-607/16/19 13:395.3 1
cis-1,3-Dichloropropene ND ug/kg 07/16/19 20:18 10061-01-507/16/19 13:395.3 1
trans-1,3-Dichloropropene ND ug/kg 07/16/19 20:18 10061-02-607/16/19 13:395.3 1
Diisopropyl ether ND ug/kg 07/16/19 20:18 108-20-307/16/19 13:395.3 1
Ethylbenzene ND ug/kg 07/16/19 20:18 100-41-407/16/19 13:395.3 1
Hexachloro-1,3-butadiene ND ug/kg 07/16/19 20:18 87-68-307/16/19 13:395.3 1
2-Hexanone ND ug/kg 07/16/19 20:18 591-78-607/16/19 13:3952.7 1
Isopropylbenzene (Cumene)ND ug/kg 07/16/19 20:18 98-82-807/16/19 13:395.3 1
p-Isopropyltoluene ND ug/kg 07/16/19 20:18 99-87-607/16/19 13:395.3 1
Methylene Chloride ND ug/kg 07/16/19 20:18 75-09-2 v207/16/19 13:3921.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/16/19 20:18 108-10-107/16/19 13:3952.7 1
Methyl-tert-butyl ether ND ug/kg 07/16/19 20:18 1634-04-407/16/19 13:395.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-10 1'Lab ID:92436815005 Collected:07/11/19 09:10 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/16/19 20:18 91-20-307/16/19 13:395.3 1
n-Propylbenzene ND ug/kg 07/16/19 20:18 103-65-107/16/19 13:395.3 1
Styrene ND ug/kg 07/16/19 20:18 100-42-507/16/19 13:395.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/16/19 20:18 630-20-607/16/19 13:395.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/16/19 20:18 79-34-507/16/19 13:395.3 1
Tetrachloroethene ND ug/kg 07/16/19 20:18 127-18-407/16/19 13:395.3 1
Toluene ND ug/kg 07/16/19 20:18 108-88-307/16/19 13:395.3 1
1,2,3-Trichlorobenzene ND ug/kg 07/16/19 20:18 87-61-607/16/19 13:395.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/16/19 20:18 120-82-107/16/19 13:395.3 1
1,1,1-Trichloroethane ND ug/kg 07/16/19 20:18 71-55-607/16/19 13:395.3 1
1,1,2-Trichloroethane ND ug/kg 07/16/19 20:18 79-00-507/16/19 13:395.3 1
Trichloroethene ND ug/kg 07/16/19 20:18 79-01-607/16/19 13:395.3 1
Trichlorofluoromethane ND ug/kg 07/16/19 20:18 75-69-407/16/19 13:395.3 1
1,2,3-Trichloropropane ND ug/kg 07/16/19 20:18 96-18-407/16/19 13:395.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/16/19 20:18 95-63-607/16/19 13:395.3 1
1,3,5-Trimethylbenzene ND ug/kg 07/16/19 20:18 108-67-807/16/19 13:395.3 1
Vinyl acetate ND ug/kg 07/16/19 20:18 108-05-407/16/19 13:3952.7 1
Vinyl chloride ND ug/kg 07/16/19 20:18 75-01-407/16/19 13:3910.5 1
Xylene (Total)ND ug/kg 07/16/19 20:18 1330-20-707/16/19 13:3910.5 1
m&p-Xylene ND ug/kg 07/16/19 20:18 179601-23-107/16/19 13:3910.5 1
o-Xylene ND ug/kg 07/16/19 20:18 95-47-607/16/19 13:395.3 1
Surrogates
Toluene-d8 (S)100 %07/16/19 20:18 2037-26-507/16/19 13:3970-130 1
4-Bromofluorobenzene (S)103 %07/16/19 20:18 460-00-407/16/19 13:3970-130 1
1,2-Dichloroethane-d4 (S)103 %07/16/19 20:18 17060-07-007/16/19 13:3970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.3 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-15 1'Lab ID:92436815006 Collected:07/11/19 09:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/17/19 14:28 67-64-107/17/19 11:3585.6 1
Benzene ND ug/kg 07/17/19 14:28 71-43-207/17/19 11:354.3 1
Bromobenzene ND ug/kg 07/17/19 14:28 108-86-107/17/19 11:354.3 1
Bromochloromethane ND ug/kg 07/17/19 14:28 74-97-507/17/19 11:354.3 1
Bromodichloromethane ND ug/kg 07/17/19 14:28 75-27-407/17/19 11:354.3 1
Bromoform ND ug/kg 07/17/19 14:28 75-25-207/17/19 11:354.3 1
Bromomethane ND ug/kg 07/17/19 14:28 74-83-907/17/19 11:358.6 1
2-Butanone (MEK)ND ug/kg 07/17/19 14:28 78-93-307/17/19 11:3585.6 1
n-Butylbenzene ND ug/kg 07/17/19 14:28 104-51-807/17/19 11:354.3 1
sec-Butylbenzene ND ug/kg 07/17/19 14:28 135-98-807/17/19 11:354.3 1
tert-Butylbenzene ND ug/kg 07/17/19 14:28 98-06-607/17/19 11:354.3 1
Carbon tetrachloride ND ug/kg 07/17/19 14:28 56-23-507/17/19 11:354.3 1
Chlorobenzene ND ug/kg 07/17/19 14:28 108-90-707/17/19 11:354.3 1
Chloroethane ND ug/kg 07/17/19 14:28 75-00-307/17/19 11:358.6 1
Chloroform ND ug/kg 07/17/19 14:28 67-66-307/17/19 11:354.3 1
Chloromethane ND ug/kg 07/17/19 14:28 74-87-307/17/19 11:358.6 1
2-Chlorotoluene ND ug/kg 07/17/19 14:28 95-49-807/17/19 11:354.3 1
4-Chlorotoluene ND ug/kg 07/17/19 14:28 106-43-407/17/19 11:354.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/17/19 14:28 96-12-807/17/19 11:354.3 1
Dibromochloromethane ND ug/kg 07/17/19 14:28 124-48-107/17/19 11:354.3 1
1,2-Dibromoethane (EDB)ND ug/kg 07/17/19 14:28 106-93-407/17/19 11:354.3 1
Dibromomethane ND ug/kg 07/17/19 14:28 74-95-307/17/19 11:354.3 1
1,2-Dichlorobenzene ND ug/kg 07/17/19 14:28 95-50-107/17/19 11:354.3 1
1,3-Dichlorobenzene ND ug/kg 07/17/19 14:28 541-73-107/17/19 11:354.3 1
1,4-Dichlorobenzene ND ug/kg 07/17/19 14:28 106-46-707/17/19 11:354.3 1
Dichlorodifluoromethane ND ug/kg 07/17/19 14:28 75-71-807/17/19 11:358.6 1
1,1-Dichloroethane ND ug/kg 07/17/19 14:28 75-34-307/17/19 11:354.3 1
1,2-Dichloroethane ND ug/kg 07/17/19 14:28 107-06-207/17/19 11:354.3 1
1,1-Dichloroethene ND ug/kg 07/17/19 14:28 75-35-407/17/19 11:354.3 1
cis-1,2-Dichloroethene ND ug/kg 07/17/19 14:28 156-59-207/17/19 11:354.3 1
trans-1,2-Dichloroethene ND ug/kg 07/17/19 14:28 156-60-507/17/19 11:354.3 1
1,2-Dichloropropane ND ug/kg 07/17/19 14:28 78-87-507/17/19 11:354.3 1
1,3-Dichloropropane ND ug/kg 07/17/19 14:28 142-28-907/17/19 11:354.3 1
2,2-Dichloropropane ND ug/kg 07/17/19 14:28 594-20-707/17/19 11:354.3 1
1,1-Dichloropropene ND ug/kg 07/17/19 14:28 563-58-607/17/19 11:354.3 1
cis-1,3-Dichloropropene ND ug/kg 07/17/19 14:28 10061-01-507/17/19 11:354.3 1
trans-1,3-Dichloropropene ND ug/kg 07/17/19 14:28 10061-02-607/17/19 11:354.3 1
Diisopropyl ether ND ug/kg 07/17/19 14:28 108-20-307/17/19 11:354.3 1
Ethylbenzene ND ug/kg 07/17/19 14:28 100-41-407/17/19 11:354.3 1
Hexachloro-1,3-butadiene ND ug/kg 07/17/19 14:28 87-68-3 IK07/17/19 11:354.3 1
2-Hexanone ND ug/kg 07/17/19 14:28 591-78-607/17/19 11:3542.8 1
Isopropylbenzene (Cumene)ND ug/kg 07/17/19 14:28 98-82-807/17/19 11:354.3 1
p-Isopropyltoluene ND ug/kg 07/17/19 14:28 99-87-607/17/19 11:354.3 1
Methylene Chloride ND ug/kg 07/17/19 14:28 75-09-207/17/19 11:3517.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/17/19 14:28 108-10-107/17/19 11:3542.8 1
Methyl-tert-butyl ether ND ug/kg 07/17/19 14:28 1634-04-407/17/19 11:354.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-15 1'Lab ID:92436815006 Collected:07/11/19 09:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/17/19 14:28 91-20-307/17/19 11:354.3 1
n-Propylbenzene ND ug/kg 07/17/19 14:28 103-65-107/17/19 11:354.3 1
Styrene ND ug/kg 07/17/19 14:28 100-42-507/17/19 11:354.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/17/19 14:28 630-20-607/17/19 11:354.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/17/19 14:28 79-34-507/17/19 11:354.3 1
Tetrachloroethene ND ug/kg 07/17/19 14:28 127-18-407/17/19 11:354.3 1
Toluene ND ug/kg 07/17/19 14:28 108-88-307/17/19 11:354.3 1
1,2,3-Trichlorobenzene ND ug/kg 07/17/19 14:28 87-61-607/17/19 11:354.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/17/19 14:28 120-82-107/17/19 11:354.3 1
1,1,1-Trichloroethane ND ug/kg 07/17/19 14:28 71-55-607/17/19 11:354.3 1
1,1,2-Trichloroethane ND ug/kg 07/17/19 14:28 79-00-507/17/19 11:354.3 1
Trichloroethene ND ug/kg 07/17/19 14:28 79-01-607/17/19 11:354.3 1
Trichlorofluoromethane ND ug/kg 07/17/19 14:28 75-69-407/17/19 11:354.3 1
1,2,3-Trichloropropane ND ug/kg 07/17/19 14:28 96-18-407/17/19 11:354.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/17/19 14:28 95-63-607/17/19 11:354.3 1
1,3,5-Trimethylbenzene ND ug/kg 07/17/19 14:28 108-67-807/17/19 11:354.3 1
Vinyl acetate ND ug/kg 07/17/19 14:28 108-05-407/17/19 11:3542.8 1
Vinyl chloride ND ug/kg 07/17/19 14:28 75-01-407/17/19 11:358.6 1
Xylene (Total)ND ug/kg 07/17/19 14:28 1330-20-707/17/19 11:358.6 1
m&p-Xylene ND ug/kg 07/17/19 14:28 179601-23-107/17/19 11:358.6 1
o-Xylene ND ug/kg 07/17/19 14:28 95-47-607/17/19 11:354.3 1
Surrogates
Toluene-d8 (S)100 %07/17/19 14:28 2037-26-507/17/19 11:3570-130 1
4-Bromofluorobenzene (S)100 %07/17/19 14:28 460-00-407/17/19 11:3570-130 1
1,2-Dichloroethane-d4 (S)105 %07/17/19 14:28 17060-07-007/17/19 11:3570-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.8 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-18 1'Lab ID:92436815007 Collected:07/11/19 10:20 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/17/19 14:54 67-64-107/17/19 11:3599.8 1
Benzene ND ug/kg 07/17/19 14:54 71-43-207/17/19 11:355.0 1
Bromobenzene ND ug/kg 07/17/19 14:54 108-86-107/17/19 11:355.0 1
Bromochloromethane ND ug/kg 07/17/19 14:54 74-97-507/17/19 11:355.0 1
Bromodichloromethane ND ug/kg 07/17/19 14:54 75-27-407/17/19 11:355.0 1
Bromoform ND ug/kg 07/17/19 14:54 75-25-207/17/19 11:355.0 1
Bromomethane ND ug/kg 07/17/19 14:54 74-83-907/17/19 11:35101
2-Butanone (MEK)ND ug/kg 07/17/19 14:54 78-93-307/17/19 11:3599.8 1
n-Butylbenzene ND ug/kg 07/17/19 14:54 104-51-807/17/19 11:355.0 1
sec-Butylbenzene ND ug/kg 07/17/19 14:54 135-98-807/17/19 11:355.0 1
tert-Butylbenzene ND ug/kg 07/17/19 14:54 98-06-607/17/19 11:355.0 1
Carbon tetrachloride ND ug/kg 07/17/19 14:54 56-23-507/17/19 11:355.0 1
Chlorobenzene ND ug/kg 07/17/19 14:54 108-90-707/17/19 11:355.0 1
Chloroethane ND ug/kg 07/17/19 14:54 75-00-307/17/19 11:35101
Chloroform ND ug/kg 07/17/19 14:54 67-66-307/17/19 11:355.0 1
Chloromethane ND ug/kg 07/17/19 14:54 74-87-307/17/19 11:35101
2-Chlorotoluene ND ug/kg 07/17/19 14:54 95-49-807/17/19 11:355.0 1
4-Chlorotoluene ND ug/kg 07/17/19 14:54 106-43-407/17/19 11:355.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/17/19 14:54 96-12-807/17/19 11:355.0 1
Dibromochloromethane ND ug/kg 07/17/19 14:54 124-48-107/17/19 11:355.0 1
1,2-Dibromoethane (EDB)ND ug/kg 07/17/19 14:54 106-93-407/17/19 11:355.0 1
Dibromomethane ND ug/kg 07/17/19 14:54 74-95-307/17/19 11:355.0 1
1,2-Dichlorobenzene ND ug/kg 07/17/19 14:54 95-50-107/17/19 11:355.0 1
1,3-Dichlorobenzene ND ug/kg 07/17/19 14:54 541-73-107/17/19 11:355.0 1
1,4-Dichlorobenzene ND ug/kg 07/17/19 14:54 106-46-707/17/19 11:355.0 1
Dichlorodifluoromethane ND ug/kg 07/17/19 14:54 75-71-807/17/19 11:35101
1,1-Dichloroethane ND ug/kg 07/17/19 14:54 75-34-307/17/19 11:355.0 1
1,2-Dichloroethane ND ug/kg 07/17/19 14:54 107-06-207/17/19 11:355.0 1
1,1-Dichloroethene ND ug/kg 07/17/19 14:54 75-35-407/17/19 11:355.0 1
cis-1,2-Dichloroethene ND ug/kg 07/17/19 14:54 156-59-207/17/19 11:355.0 1
trans-1,2-Dichloroethene ND ug/kg 07/17/19 14:54 156-60-507/17/19 11:355.0 1
1,2-Dichloropropane ND ug/kg 07/17/19 14:54 78-87-507/17/19 11:355.0 1
1,3-Dichloropropane ND ug/kg 07/17/19 14:54 142-28-907/17/19 11:355.0 1
2,2-Dichloropropane ND ug/kg 07/17/19 14:54 594-20-707/17/19 11:355.0 1
1,1-Dichloropropene ND ug/kg 07/17/19 14:54 563-58-607/17/19 11:355.0 1
cis-1,3-Dichloropropene ND ug/kg 07/17/19 14:54 10061-01-507/17/19 11:355.0 1
trans-1,3-Dichloropropene ND ug/kg 07/17/19 14:54 10061-02-607/17/19 11:355.0 1
Diisopropyl ether ND ug/kg 07/17/19 14:54 108-20-307/17/19 11:355.0 1
Ethylbenzene ND ug/kg 07/17/19 14:54 100-41-407/17/19 11:355.0 1
Hexachloro-1,3-butadiene ND ug/kg 07/17/19 14:54 87-68-3 IK07/17/19 11:355.0 1
2-Hexanone ND ug/kg 07/17/19 14:54 591-78-607/17/19 11:3549.9 1
Isopropylbenzene (Cumene)ND ug/kg 07/17/19 14:54 98-82-807/17/19 11:355.0 1
p-Isopropyltoluene ND ug/kg 07/17/19 14:54 99-87-607/17/19 11:355.0 1
Methylene Chloride ND ug/kg 07/17/19 14:54 75-09-207/17/19 11:3520.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/17/19 14:54 108-10-107/17/19 11:3549.9 1
Methyl-tert-butyl ether ND ug/kg 07/17/19 14:54 1634-04-407/17/19 11:355.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-18 1'Lab ID:92436815007 Collected:07/11/19 10:20 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/17/19 14:54 91-20-307/17/19 11:355.0 1
n-Propylbenzene ND ug/kg 07/17/19 14:54 103-65-107/17/19 11:355.0 1
Styrene ND ug/kg 07/17/19 14:54 100-42-507/17/19 11:355.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/17/19 14:54 630-20-607/17/19 11:355.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/17/19 14:54 79-34-507/17/19 11:355.0 1
Tetrachloroethene ND ug/kg 07/17/19 14:54 127-18-407/17/19 11:355.0 1
Toluene ND ug/kg 07/17/19 14:54 108-88-307/17/19 11:355.0 1
1,2,3-Trichlorobenzene ND ug/kg 07/17/19 14:54 87-61-607/17/19 11:355.0 1
1,2,4-Trichlorobenzene ND ug/kg 07/17/19 14:54 120-82-107/17/19 11:355.0 1
1,1,1-Trichloroethane ND ug/kg 07/17/19 14:54 71-55-607/17/19 11:355.0 1
1,1,2-Trichloroethane ND ug/kg 07/17/19 14:54 79-00-507/17/19 11:355.0 1
Trichloroethene ND ug/kg 07/17/19 14:54 79-01-607/17/19 11:355.0 1
Trichlorofluoromethane ND ug/kg 07/17/19 14:54 75-69-407/17/19 11:355.0 1
1,2,3-Trichloropropane ND ug/kg 07/17/19 14:54 96-18-407/17/19 11:355.0 1
1,2,4-Trimethylbenzene ND ug/kg 07/17/19 14:54 95-63-607/17/19 11:355.0 1
1,3,5-Trimethylbenzene ND ug/kg 07/17/19 14:54 108-67-807/17/19 11:355.0 1
Vinyl acetate ND ug/kg 07/17/19 14:54 108-05-407/17/19 11:3549.9 1
Vinyl chloride ND ug/kg 07/17/19 14:54 75-01-407/17/19 11:35101
Xylene (Total)ND ug/kg 07/17/19 14:54 1330-20-707/17/19 11:35101
m&p-Xylene ND ug/kg 07/17/19 14:54 179601-23-107/17/19 11:35101
o-Xylene ND ug/kg 07/17/19 14:54 95-47-607/17/19 11:355.0 1
Surrogates
Toluene-d8 (S)101 %07/17/19 14:54 2037-26-507/17/19 11:3570-130 1
4-Bromofluorobenzene (S)108 %07/17/19 14:54 460-00-407/17/19 11:3570-130 1
1,2-Dichloroethane-d4 (S)111 %07/17/19 14:54 17060-07-007/17/19 11:3570-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.0 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-12 1'Lab ID:92436815008 Collected:07/11/19 10:45 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/17/19 15:19 67-64-107/17/19 11:3594.0 1
Benzene ND ug/kg 07/17/19 15:19 71-43-207/17/19 11:354.7 1
Bromobenzene ND ug/kg 07/17/19 15:19 108-86-107/17/19 11:354.7 1
Bromochloromethane ND ug/kg 07/17/19 15:19 74-97-507/17/19 11:354.7 1
Bromodichloromethane ND ug/kg 07/17/19 15:19 75-27-407/17/19 11:354.7 1
Bromoform ND ug/kg 07/17/19 15:19 75-25-207/17/19 11:354.7 1
Bromomethane ND ug/kg 07/17/19 15:19 74-83-907/17/19 11:359.4 1
2-Butanone (MEK)ND ug/kg 07/17/19 15:19 78-93-307/17/19 11:3594.0 1
n-Butylbenzene ND ug/kg 07/17/19 15:19 104-51-807/17/19 11:354.7 1
sec-Butylbenzene ND ug/kg 07/17/19 15:19 135-98-807/17/19 11:354.7 1
tert-Butylbenzene ND ug/kg 07/17/19 15:19 98-06-607/17/19 11:354.7 1
Carbon tetrachloride ND ug/kg 07/17/19 15:19 56-23-507/17/19 11:354.7 1
Chlorobenzene ND ug/kg 07/17/19 15:19 108-90-707/17/19 11:354.7 1
Chloroethane ND ug/kg 07/17/19 15:19 75-00-307/17/19 11:359.4 1
Chloroform ND ug/kg 07/17/19 15:19 67-66-307/17/19 11:354.7 1
Chloromethane ND ug/kg 07/17/19 15:19 74-87-307/17/19 11:359.4 1
2-Chlorotoluene ND ug/kg 07/17/19 15:19 95-49-807/17/19 11:354.7 1
4-Chlorotoluene ND ug/kg 07/17/19 15:19 106-43-407/17/19 11:354.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/17/19 15:19 96-12-807/17/19 11:354.7 1
Dibromochloromethane ND ug/kg 07/17/19 15:19 124-48-107/17/19 11:354.7 1
1,2-Dibromoethane (EDB)ND ug/kg 07/17/19 15:19 106-93-407/17/19 11:354.7 1
Dibromomethane ND ug/kg 07/17/19 15:19 74-95-307/17/19 11:354.7 1
1,2-Dichlorobenzene ND ug/kg 07/17/19 15:19 95-50-107/17/19 11:354.7 1
1,3-Dichlorobenzene ND ug/kg 07/17/19 15:19 541-73-107/17/19 11:354.7 1
1,4-Dichlorobenzene ND ug/kg 07/17/19 15:19 106-46-707/17/19 11:354.7 1
Dichlorodifluoromethane ND ug/kg 07/17/19 15:19 75-71-807/17/19 11:359.4 1
1,1-Dichloroethane ND ug/kg 07/17/19 15:19 75-34-307/17/19 11:354.7 1
1,2-Dichloroethane ND ug/kg 07/17/19 15:19 107-06-207/17/19 11:354.7 1
1,1-Dichloroethene ND ug/kg 07/17/19 15:19 75-35-407/17/19 11:354.7 1
cis-1,2-Dichloroethene ND ug/kg 07/17/19 15:19 156-59-207/17/19 11:354.7 1
trans-1,2-Dichloroethene ND ug/kg 07/17/19 15:19 156-60-507/17/19 11:354.7 1
1,2-Dichloropropane ND ug/kg 07/17/19 15:19 78-87-507/17/19 11:354.7 1
1,3-Dichloropropane ND ug/kg 07/17/19 15:19 142-28-907/17/19 11:354.7 1
2,2-Dichloropropane ND ug/kg 07/17/19 15:19 594-20-707/17/19 11:354.7 1
1,1-Dichloropropene ND ug/kg 07/17/19 15:19 563-58-607/17/19 11:354.7 1
cis-1,3-Dichloropropene ND ug/kg 07/17/19 15:19 10061-01-507/17/19 11:354.7 1
trans-1,3-Dichloropropene ND ug/kg 07/17/19 15:19 10061-02-607/17/19 11:354.7 1
Diisopropyl ether ND ug/kg 07/17/19 15:19 108-20-307/17/19 11:354.7 1
Ethylbenzene ND ug/kg 07/17/19 15:19 100-41-407/17/19 11:354.7 1
Hexachloro-1,3-butadiene ND ug/kg 07/17/19 15:19 87-68-3 IK07/17/19 11:354.7 1
2-Hexanone ND ug/kg 07/17/19 15:19 591-78-607/17/19 11:3547.0 1
Isopropylbenzene (Cumene)ND ug/kg 07/17/19 15:19 98-82-807/17/19 11:354.7 1
p-Isopropyltoluene ND ug/kg 07/17/19 15:19 99-87-607/17/19 11:354.7 1
Methylene Chloride ND ug/kg 07/17/19 15:19 75-09-207/17/19 11:3518.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/17/19 15:19 108-10-107/17/19 11:3547.0 1
Methyl-tert-butyl ether ND ug/kg 07/17/19 15:19 1634-04-407/17/19 11:354.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
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Page 19 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-12 1'Lab ID:92436815008 Collected:07/11/19 10:45 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/17/19 15:19 91-20-307/17/19 11:354.7 1
n-Propylbenzene ND ug/kg 07/17/19 15:19 103-65-107/17/19 11:354.7 1
Styrene ND ug/kg 07/17/19 15:19 100-42-507/17/19 11:354.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/17/19 15:19 630-20-607/17/19 11:354.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/17/19 15:19 79-34-507/17/19 11:354.7 1
Tetrachloroethene ND ug/kg 07/17/19 15:19 127-18-407/17/19 11:354.7 1
Toluene ND ug/kg 07/17/19 15:19 108-88-307/17/19 11:354.7 1
1,2,3-Trichlorobenzene ND ug/kg 07/17/19 15:19 87-61-607/17/19 11:354.7 1
1,2,4-Trichlorobenzene ND ug/kg 07/17/19 15:19 120-82-107/17/19 11:354.7 1
1,1,1-Trichloroethane ND ug/kg 07/17/19 15:19 71-55-607/17/19 11:354.7 1
1,1,2-Trichloroethane ND ug/kg 07/17/19 15:19 79-00-507/17/19 11:354.7 1
Trichloroethene ND ug/kg 07/17/19 15:19 79-01-607/17/19 11:354.7 1
Trichlorofluoromethane ND ug/kg 07/17/19 15:19 75-69-407/17/19 11:354.7 1
1,2,3-Trichloropropane ND ug/kg 07/17/19 15:19 96-18-407/17/19 11:354.7 1
1,2,4-Trimethylbenzene ND ug/kg 07/17/19 15:19 95-63-607/17/19 11:354.7 1
1,3,5-Trimethylbenzene ND ug/kg 07/17/19 15:19 108-67-807/17/19 11:354.7 1
Vinyl acetate ND ug/kg 07/17/19 15:19 108-05-407/17/19 11:3547.0 1
Vinyl chloride ND ug/kg 07/17/19 15:19 75-01-407/17/19 11:359.4 1
Xylene (Total)ND ug/kg 07/17/19 15:19 1330-20-707/17/19 11:359.4 1
m&p-Xylene ND ug/kg 07/17/19 15:19 179601-23-107/17/19 11:359.4 1
o-Xylene ND ug/kg 07/17/19 15:19 95-47-607/17/19 11:354.7 1
Surrogates
Toluene-d8 (S)103 %07/17/19 15:19 2037-26-507/17/19 11:3570-130 1
4-Bromofluorobenzene (S)100 %07/17/19 15:19 460-00-407/17/19 11:3570-130 1
1,2-Dichloroethane-d4 (S)101 %07/17/19 15:19 17060-07-007/17/19 11:3570-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.8 %07/15/19 16:150.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 20 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-DUP-1 Lab ID:92436815009 Collected:07/11/19 00:01 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 07/17/19 15:45 67-64-107/17/19 11:351051
Benzene ND ug/kg 07/17/19 15:45 71-43-207/17/19 11:355.2 1
Bromobenzene ND ug/kg 07/17/19 15:45 108-86-107/17/19 11:355.2 1
Bromochloromethane ND ug/kg 07/17/19 15:45 74-97-507/17/19 11:355.2 1
Bromodichloromethane ND ug/kg 07/17/19 15:45 75-27-407/17/19 11:355.2 1
Bromoform ND ug/kg 07/17/19 15:45 75-25-207/17/19 11:355.2 1
Bromomethane ND ug/kg 07/17/19 15:45 74-83-907/17/19 11:3510.5 1
2-Butanone (MEK)ND ug/kg 07/17/19 15:45 78-93-307/17/19 11:351051
n-Butylbenzene ND ug/kg 07/17/19 15:45 104-51-807/17/19 11:355.2 1
sec-Butylbenzene ND ug/kg 07/17/19 15:45 135-98-807/17/19 11:355.2 1
tert-Butylbenzene ND ug/kg 07/17/19 15:45 98-06-607/17/19 11:355.2 1
Carbon tetrachloride ND ug/kg 07/17/19 15:45 56-23-507/17/19 11:355.2 1
Chlorobenzene ND ug/kg 07/17/19 15:45 108-90-707/17/19 11:355.2 1
Chloroethane ND ug/kg 07/17/19 15:45 75-00-307/17/19 11:3510.5 1
Chloroform ND ug/kg 07/17/19 15:45 67-66-307/17/19 11:355.2 1
Chloromethane ND ug/kg 07/17/19 15:45 74-87-307/17/19 11:3510.5 1
2-Chlorotoluene ND ug/kg 07/17/19 15:45 95-49-807/17/19 11:355.2 1
4-Chlorotoluene ND ug/kg 07/17/19 15:45 106-43-407/17/19 11:355.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/17/19 15:45 96-12-807/17/19 11:355.2 1
Dibromochloromethane ND ug/kg 07/17/19 15:45 124-48-107/17/19 11:355.2 1
1,2-Dibromoethane (EDB)ND ug/kg 07/17/19 15:45 106-93-407/17/19 11:355.2 1
Dibromomethane ND ug/kg 07/17/19 15:45 74-95-307/17/19 11:355.2 1
1,2-Dichlorobenzene ND ug/kg 07/17/19 15:45 95-50-107/17/19 11:355.2 1
1,3-Dichlorobenzene ND ug/kg 07/17/19 15:45 541-73-107/17/19 11:355.2 1
1,4-Dichlorobenzene ND ug/kg 07/17/19 15:45 106-46-707/17/19 11:355.2 1
Dichlorodifluoromethane ND ug/kg 07/17/19 15:45 75-71-807/17/19 11:3510.5 1
1,1-Dichloroethane ND ug/kg 07/17/19 15:45 75-34-307/17/19 11:355.2 1
1,2-Dichloroethane ND ug/kg 07/17/19 15:45 107-06-207/17/19 11:355.2 1
1,1-Dichloroethene ND ug/kg 07/17/19 15:45 75-35-407/17/19 11:355.2 1
cis-1,2-Dichloroethene ND ug/kg 07/17/19 15:45 156-59-207/17/19 11:355.2 1
trans-1,2-Dichloroethene ND ug/kg 07/17/19 15:45 156-60-507/17/19 11:355.2 1
1,2-Dichloropropane ND ug/kg 07/17/19 15:45 78-87-507/17/19 11:355.2 1
1,3-Dichloropropane ND ug/kg 07/17/19 15:45 142-28-907/17/19 11:355.2 1
2,2-Dichloropropane ND ug/kg 07/17/19 15:45 594-20-707/17/19 11:355.2 1
1,1-Dichloropropene ND ug/kg 07/17/19 15:45 563-58-607/17/19 11:355.2 1
cis-1,3-Dichloropropene ND ug/kg 07/17/19 15:45 10061-01-507/17/19 11:355.2 1
trans-1,3-Dichloropropene ND ug/kg 07/17/19 15:45 10061-02-607/17/19 11:355.2 1
Diisopropyl ether ND ug/kg 07/17/19 15:45 108-20-307/17/19 11:355.2 1
Ethylbenzene ND ug/kg 07/17/19 15:45 100-41-407/17/19 11:355.2 1
Hexachloro-1,3-butadiene ND ug/kg 07/17/19 15:45 87-68-3 IK07/17/19 11:355.2 1
2-Hexanone ND ug/kg 07/17/19 15:45 591-78-607/17/19 11:3552.4 1
Isopropylbenzene (Cumene)ND ug/kg 07/17/19 15:45 98-82-807/17/19 11:355.2 1
p-Isopropyltoluene ND ug/kg 07/17/19 15:45 99-87-607/17/19 11:355.2 1
Methylene Chloride ND ug/kg 07/17/19 15:45 75-09-207/17/19 11:3520.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/17/19 15:45 108-10-107/17/19 11:3552.4 1
Methyl-tert-butyl ether ND ug/kg 07/17/19 15:45 1634-04-407/17/19 11:355.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:SG-DUP-1 Lab ID:92436815009 Collected:07/11/19 00:01 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Naphthalene ND ug/kg 07/17/19 15:45 91-20-307/17/19 11:355.2 1
n-Propylbenzene ND ug/kg 07/17/19 15:45 103-65-107/17/19 11:355.2 1
Styrene ND ug/kg 07/17/19 15:45 100-42-507/17/19 11:355.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/17/19 15:45 630-20-607/17/19 11:355.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/17/19 15:45 79-34-507/17/19 11:355.2 1
Tetrachloroethene ND ug/kg 07/17/19 15:45 127-18-407/17/19 11:355.2 1
Toluene ND ug/kg 07/17/19 15:45 108-88-307/17/19 11:355.2 1
1,2,3-Trichlorobenzene ND ug/kg 07/17/19 15:45 87-61-607/17/19 11:355.2 1
1,2,4-Trichlorobenzene ND ug/kg 07/17/19 15:45 120-82-107/17/19 11:355.2 1
1,1,1-Trichloroethane ND ug/kg 07/17/19 15:45 71-55-607/17/19 11:355.2 1
1,1,2-Trichloroethane ND ug/kg 07/17/19 15:45 79-00-507/17/19 11:355.2 1
Trichloroethene ND ug/kg 07/17/19 15:45 79-01-607/17/19 11:355.2 1
Trichlorofluoromethane ND ug/kg 07/17/19 15:45 75-69-407/17/19 11:355.2 1
1,2,3-Trichloropropane ND ug/kg 07/17/19 15:45 96-18-407/17/19 11:355.2 1
1,2,4-Trimethylbenzene ND ug/kg 07/17/19 15:45 95-63-607/17/19 11:355.2 1
1,3,5-Trimethylbenzene ND ug/kg 07/17/19 15:45 108-67-807/17/19 11:355.2 1
Vinyl acetate ND ug/kg 07/17/19 15:45 108-05-407/17/19 11:3552.4 1
Vinyl chloride ND ug/kg 07/17/19 15:45 75-01-407/17/19 11:3510.5 1
Xylene (Total)ND ug/kg 07/17/19 15:45 1330-20-707/17/19 11:3510.5 1
m&p-Xylene ND ug/kg 07/17/19 15:45 179601-23-107/17/19 11:3510.5 1
o-Xylene ND ug/kg 07/17/19 15:45 95-47-607/17/19 11:355.2 1
Surrogates
Toluene-d8 (S)100 %07/17/19 15:45 2037-26-507/17/19 11:3570-130 1
4-Bromofluorobenzene (S)103 %07/17/19 15:45 460-00-407/17/19 11:3570-130 1
1,2-Dichloroethane-d4 (S)102 %07/17/19 15:45 17060-07-007/17/19 11:3570-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.0 %07/15/19 16:160.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:TRIP BLANK Lab ID:92436815010 Collected:07/10/19 00:00 Received:07/15/19 12:59 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 07/16/19 12:42 67-64-125.0 1
Benzene ND ug/L 07/16/19 12:42 71-43-21.0 1
Bromobenzene ND ug/L 07/16/19 12:42 108-86-11.0 1
Bromochloromethane ND ug/L 07/16/19 12:42 74-97-51.0 1
Bromodichloromethane ND ug/L 07/16/19 12:42 75-27-41.0 1
Bromoform ND ug/L 07/16/19 12:42 75-25-21.0 1
Bromomethane ND ug/L 07/16/19 12:42 74-83-9 v12.0 1
2-Butanone (MEK)ND ug/L 07/16/19 12:42 78-93-35.0 1
Carbon tetrachloride ND ug/L 07/16/19 12:42 56-23-51.0 1
Chlorobenzene ND ug/L 07/16/19 12:42 108-90-71.0 1
Chloroethane ND ug/L 07/16/19 12:42 75-00-31.0 1
Chloroform ND ug/L 07/16/19 12:42 67-66-35.0 1
Chloromethane ND ug/L 07/16/19 12:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 07/16/19 12:42 95-49-81.0 1
4-Chlorotoluene ND ug/L 07/16/19 12:42 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 07/16/19 12:42 96-12-85.0 1
Dibromochloromethane ND ug/L 07/16/19 12:42 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 07/16/19 12:42 106-93-41.0 1
Dibromomethane ND ug/L 07/16/19 12:42 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 07/16/19 12:42 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 07/16/19 12:42 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 07/16/19 12:42 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 07/16/19 12:42 75-71-81.0 1
1,1-Dichloroethane ND ug/L 07/16/19 12:42 75-34-31.0 1
1,2-Dichloroethane ND ug/L 07/16/19 12:42 107-06-21.0 1
1,1-Dichloroethene ND ug/L 07/16/19 12:42 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 07/16/19 12:42 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 07/16/19 12:42 156-60-51.0 1
1,2-Dichloropropane ND ug/L 07/16/19 12:42 78-87-51.0 1
1,3-Dichloropropane ND ug/L 07/16/19 12:42 142-28-91.0 1
2,2-Dichloropropane ND ug/L 07/16/19 12:42 594-20-71.0 1
1,1-Dichloropropene ND ug/L 07/16/19 12:42 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 07/16/19 12:42 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 07/16/19 12:42 10061-02-61.0 1
Diisopropyl ether ND ug/L 07/16/19 12:42 108-20-31.0 1
Ethylbenzene ND ug/L 07/16/19 12:42 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 07/16/19 12:42 87-68-31.0 1
2-Hexanone ND ug/L 07/16/19 12:42 591-78-65.0 1
p-Isopropyltoluene ND ug/L 07/16/19 12:42 99-87-61.0 1
Methylene Chloride ND ug/L 07/16/19 12:42 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 07/16/19 12:42 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 07/16/19 12:42 1634-04-41.0 1
Naphthalene ND ug/L 07/16/19 12:42 91-20-31.0 1
Styrene ND ug/L 07/16/19 12:42 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 07/16/19 12:42 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 07/16/19 12:42 79-34-51.0 1
Tetrachloroethene ND ug/L 07/16/19 12:42 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:TRIP BLANK Lab ID:92436815010 Collected:07/10/19 00:00 Received:07/15/19 12:59 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Toluene ND ug/L 07/16/19 12:42 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 07/16/19 12:42 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 07/16/19 12:42 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 07/16/19 12:42 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 07/16/19 12:42 79-00-51.0 1
Trichloroethene ND ug/L 07/16/19 12:42 79-01-61.0 1
Trichlorofluoromethane ND ug/L 07/16/19 12:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 07/16/19 12:42 96-18-41.0 1
Vinyl acetate ND ug/L 07/16/19 12:42 108-05-42.0 1
Vinyl chloride ND ug/L 07/16/19 12:42 75-01-41.0 1
Xylene (Total)ND ug/L 07/16/19 12:42 1330-20-71.0 1
m&p-Xylene ND ug/L 07/16/19 12:42 179601-23-12.0 1
o-Xylene ND ug/L 07/16/19 12:42 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %07/16/19 12:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %07/16/19 12:42 17060-07-070-130 1
Toluene-d8 (S)104 %07/16/19 12:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-4 Lab ID:92436815011 Collected:07/10/19 11:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 0.92 mg/kg 07/20/19 17:24 7440-38-2 M107/19/19 10:540.87 1
Barium 64.3 mg/kg 07/20/19 17:24 7440-39-307/19/19 10:540.43 1
Cadmium ND mg/kg 07/21/19 17:13 7440-43-907/19/19 10:540.087 1
Chromium 10.7 mg/kg 07/20/19 17:24 7440-47-307/19/19 10:540.43 1
Lead 11.5 mg/kg 07/20/19 17:24 7439-92-107/19/19 10:540.43 1
Selenium ND mg/kg 07/20/19 17:24 7782-49-2 M107/19/19 10:540.87 1
Silver ND mg/kg 07/20/19 17:24 7440-22-407/19/19 10:540.43 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0096 mg/kg 07/16/19 12:37 7439-97-607/16/19 10:250.0025 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 07/19/19 11:56 83-32-907/17/19 15:453891
Acenaphthylene ND ug/kg 07/19/19 11:56 208-96-807/17/19 15:453891
Acetophenone ND ug/kg 07/19/19 11:56 98-86-207/17/19 15:453891
2-Acetylaminofluorene ND ug/kg 07/19/19 11:56 53-96-307/17/19 15:457771
4-Aminobiphenyl ND ug/kg 07/19/19 11:56 92-67-1 M1,v207/17/19 15:4538901
Aniline ND ug/kg 07/19/19 11:56 62-53-3 R107/17/19 15:453891
Anthracene ND ug/kg 07/19/19 11:56 120-12-707/17/19 15:453891
Aramite ND ug/kg 07/19/19 11:56 140-57-8 M107/17/19 15:4538901
Atrazine ND ug/kg 07/19/19 11:56 1912-24-9 L207/17/19 15:457771
Benzal chloride ND ug/kg 07/19/19 11:56 98-87-307/17/19 15:4511801
Benzaldehyde ND ug/kg 07/19/19 11:56 100-52-707/17/19 15:457771
Benzidine ND ug/kg 07/19/19 11:56 92-87-5 M107/17/19 15:4519401
Benzo(a)anthracene ND ug/kg 07/19/19 11:56 56-55-307/17/19 15:453891
Benzo(a)pyrene ND ug/kg 07/19/19 11:56 50-32-807/17/19 15:453891
Benzo(b)fluoranthene ND ug/kg 07/19/19 11:56 205-99-207/17/19 15:453891
Benzo(g,h,i)perylene ND ug/kg 07/19/19 11:56 191-24-207/17/19 15:453891
Benzo(k)fluoranthene ND ug/kg 07/19/19 11:56 207-08-907/17/19 15:453891
Benzoic Acid ND ug/kg 07/19/19 11:56 65-85-007/17/19 15:4519401
Benzophenone ND ug/kg 07/19/19 11:56 119-61-907/17/19 15:453891
Benzyl alcohol ND ug/kg 07/19/19 11:56 100-51-607/17/19 15:457771
Biphenyl (Diphenyl)ND ug/kg 07/19/19 11:56 92-52-407/17/19 15:453891
4-Bromophenylphenyl ether ND ug/kg 07/19/19 11:56 101-55-307/17/19 15:453891
Butylbenzylphthalate ND ug/kg 07/19/19 11:56 85-68-707/17/19 15:453891
Caprolactam ND ug/kg 07/19/19 11:56 105-60-2 L207/17/19 15:453891
Carbazole ND ug/kg 07/19/19 11:56 86-74-807/17/19 15:453891
4-Chloro-3-methylphenol ND ug/kg 07/19/19 11:56 59-50-707/17/19 15:457771
4-Chloroaniline ND ug/kg 07/19/19 11:56 106-47-807/17/19 15:4519401
Chlorobenzilate ND ug/kg 07/19/19 11:56 510-15-607/17/19 15:453891
bis(2-Chloroethoxy)methane ND ug/kg 07/19/19 11:56 111-91-107/17/19 15:453891
bis(2-Chloroethyl) ether ND ug/kg 07/19/19 11:56 111-44-407/17/19 15:453891
2-Chloronaphthalene ND ug/kg 07/19/19 11:56 91-58-707/17/19 15:453891
2-Chlorophenol ND ug/kg 07/19/19 11:56 95-57-807/17/19 15:453891
4-Chlorophenylphenyl ether ND ug/kg 07/19/19 11:56 7005-72-307/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-4 Lab ID:92436815011 Collected:07/10/19 11:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Chrysene ND ug/kg 07/19/19 11:56 218-01-907/17/19 15:453891
n-Decane ND ug/kg 07/19/19 11:56 124-18-5 M107/17/19 15:453891
Diallate ND ug/kg 07/19/19 11:56 2303-16-407/17/19 15:453891
Dibenz(a,h)anthracene ND ug/kg 07/19/19 11:56 53-70-307/17/19 15:453891
Dibenzo(a,e)pyrene ND ug/kg 07/19/19 11:56 192-65-4 M107/17/19 15:4511801
Dibenzofuran ND ug/kg 07/19/19 11:56 132-64-907/17/19 15:453891
2,3-Dibromo-1-propanol phosph ND ug/kg 07/19/19 11:56 126-72-7 IC,L1,M007/17/19 15:4529401
1,2-Dichlorobenzene ND ug/kg 07/19/19 11:56 95-50-107/17/19 15:453891
1,3-Dichlorobenzene ND ug/kg 07/19/19 11:56 541-73-107/17/19 15:453891
1,4-Dichlorobenzene ND ug/kg 07/19/19 11:56 106-46-707/17/19 15:453891
3,3'-Dichlorobenzidine ND ug/kg 07/19/19 11:56 91-94-107/17/19 15:4519401
2,4-Dichlorophenol ND ug/kg 07/19/19 11:56 120-83-207/17/19 15:453891
2,6-Dichlorophenol ND ug/kg 07/19/19 11:56 87-65-0 M107/17/19 15:453891
2,3-Dichloroaniline ND ug/kg 07/19/19 11:56 608-27-5 M107/17/19 15:453891
Diethylphthalate ND ug/kg 07/19/19 11:56 84-66-207/17/19 15:453891
Dimethoate ND ug/kg 07/19/19 11:56 60-51-5 IC,L1,M007/17/19 15:457771
P-Dimethylaminoazobenzene ND ug/kg 07/19/19 11:56 60-11-7 M107/17/19 15:457771
7,12-Dimethylbenz(a)anthracene ND ug/kg 07/19/19 11:56 57-97-6 M107/17/19 15:453891
3,3'-Dimethylbenzidine ND ug/kg 07/19/19 11:56 119-93-7 M107/17/19 15:4538901
2,4-Dimethylphenol ND ug/kg 07/19/19 11:56 105-67-907/17/19 15:453891
a,a-Dimethylphenylethylamine ND ug/kg 07/19/19 11:56 122-09-8 M107/17/19 15:4519401
Dimethylphthalate ND ug/kg 07/19/19 11:56 131-11-307/17/19 15:453891
Di-n-butylphthalate ND ug/kg 07/19/19 11:56 84-74-207/17/19 15:453891
4,6-Dinitro-2-methylphenol ND ug/kg 07/19/19 11:56 534-52-1 v107/17/19 15:457771
1,3-Dinitrobenzene ND ug/kg 07/19/19 11:56 99-65-007/17/19 15:457771
1,4-Dinitrobenzene ND ug/kg 07/19/19 11:56 100-25-407/17/19 15:453891
2,4-Dinitrophenol ND ug/kg 07/19/19 11:56 51-28-507/17/19 15:4519401
2,4-Dinitrotoluene ND ug/kg 07/19/19 11:56 121-14-207/17/19 15:453891
2,6-Dinitrotoluene ND ug/kg 07/19/19 11:56 606-20-207/17/19 15:453891
Di-n-octylphthalate ND ug/kg 07/19/19 11:56 117-84-007/17/19 15:453891
Dinoseb ND ug/kg 07/19/19 11:56 88-85-707/17/19 15:457771
Diphenylamine ND ug/kg 07/19/19 11:56 122-39-407/17/19 15:453891
Diphenyl ether (Phenyl ether)ND ug/kg 07/19/19 11:56 101-84-8 M107/17/19 15:455891
1,2-Diphenylhydrazine ND ug/kg 07/19/19 11:56 122-66-707/17/19 15:453891
Disulfoton ND ug/kg 07/19/19 11:56 298-04-407/17/19 15:457771
bis(2-Ethylhexyl)phthalate ND ug/kg 07/19/19 11:56 117-81-707/17/19 15:453891
Ethyl methanesulfonate ND ug/kg 07/19/19 11:56 62-50-0 M107/17/19 15:457771
Famphur ND ug/kg 07/19/19 11:56 52-85-7 L207/17/19 15:4519401
Fluoranthene ND ug/kg 07/19/19 11:56 206-44-007/17/19 15:453891
Fluorene ND ug/kg 07/19/19 11:56 86-73-707/17/19 15:453891
Hexachloro-1,3-butadiene ND ug/kg 07/19/19 11:56 87-68-3 R107/17/19 15:453891
Hexachlorobenzene ND ug/kg 07/19/19 11:56 118-74-107/17/19 15:453891
Hexachlorocyclopentadiene ND ug/kg 07/19/19 11:56 77-47-4 R107/17/19 15:453891
Hexachloroethane ND ug/kg 07/19/19 11:56 67-72-1 R107/17/19 15:453891
Hexachlorophene ND ug/kg 07/19/19 11:56 70-30-4 M107/17/19 15:4538901
Hexachloropropene ND ug/kg 07/19/19 11:56 1888-71-707/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-4 Lab ID:92436815011 Collected:07/10/19 11:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 07/19/19 11:56 193-39-507/17/19 15:453891
Isodrin ND ug/kg 07/19/19 11:56 465-73-6 M107/17/19 15:457771
Isophorone ND ug/kg 07/19/19 11:56 78-59-107/17/19 15:453891
Isosafrole ND ug/kg 07/19/19 11:56 120-58-107/17/19 15:453891
Kepone ND ug/kg 07/19/19 11:56 143-50-0 M107/17/19 15:4519401
Methapyrilene ND ug/kg 07/19/19 11:56 91-80-5 M107/17/19 15:4519401
3-Methylcholanthrene ND ug/kg 07/19/19 11:56 56-49-507/17/19 15:453891
4,4'-Methylene-bis(2-chloroani ND ug/kg 07/19/19 11:56 101-14-407/17/19 15:4511801
Methyl methanesulfonate ND ug/kg 07/19/19 11:56 66-27-307/17/19 15:457771
1-Methylnaphthalene ND ug/kg 07/19/19 11:56 90-12-007/17/19 15:453891
2-Methylnaphthalene ND ug/kg 07/19/19 11:56 91-57-607/17/19 15:453891
2-Methyl-5-nitroaniline ND ug/kg 07/19/19 11:56 99-55-8 M107/17/19 15:453891
Methyl parathion ND ug/kg 07/19/19 11:56 298-00-0 L107/17/19 15:457771
2-Methylphenol(o-Cresol)ND ug/kg 07/19/19 11:56 95-48-707/17/19 15:453891
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/19/19 11:56 15831-10-407/17/19 15:453891
1-Naphthalenamine ND ug/kg 07/19/19 11:56 134-32-7 M107/17/19 15:457771
2-Naphthalenamine ND ug/kg 07/19/19 11:56 91-59-8 M107/17/19 15:457771
Naphthalene ND ug/kg 07/19/19 11:56 91-20-307/17/19 15:453891
1,4-Naphthoquinone ND ug/kg 07/19/19 11:56 130-15-4 IC,L1,M007/17/19 15:4538901
2-Nitroaniline ND ug/kg 07/19/19 11:56 88-74-407/17/19 15:4519401
3-Nitroaniline ND ug/kg 07/19/19 11:56 99-09-207/17/19 15:4519401
4-Nitroaniline ND ug/kg 07/19/19 11:56 100-01-607/17/19 15:457771
Nitrobenzene ND ug/kg 07/19/19 11:56 98-95-307/17/19 15:453891
2-Nitrophenol ND ug/kg 07/19/19 11:56 88-75-507/17/19 15:453891
4-Nitrophenol ND ug/kg 07/19/19 11:56 100-02-707/17/19 15:4519401
4-Nitroquinoline-n-oxide ND ug/kg 07/19/19 11:56 56-57-5 M107/17/19 15:4519401
5-Nitro-o-toluidine ND ug/kg 07/19/19 11:56 99-55-807/17/19 15:453891
N-Nitrosodiethylamine ND ug/kg 07/19/19 11:56 55-18-507/17/19 15:457771
N-Nitrosodimethylamine ND ug/kg 07/19/19 11:56 62-75-9 R107/17/19 15:453891
N-Nitroso-di-n-butylamine ND ug/kg 07/19/19 11:56 924-16-307/17/19 15:453891
N-Nitroso-di-n-propylamine ND ug/kg 07/19/19 11:56 621-64-707/17/19 15:453891
N-Nitrosodiphenylamine ND ug/kg 07/19/19 11:56 86-30-607/17/19 15:453891
N-Nitrosomethylethylamine ND ug/kg 07/19/19 11:56 10595-95-607/17/19 15:453891
N-Nitrosomorpholine ND ug/kg 07/19/19 11:56 59-89-207/17/19 15:453891
N-Nitrosopiperidine ND ug/kg 07/19/19 11:56 100-75-407/17/19 15:457771
N-Nitrosopyrrolidine ND ug/kg 07/19/19 11:56 930-55-207/17/19 15:457771
n-Octadecane ND ug/kg 07/19/19 11:56 593-45-307/17/19 15:453891
O,O,O-Triethylphosphorothioate ND ug/kg 07/19/19 11:56 126-68-1 M107/17/19 15:4519401
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/19/19 11:56 108-60-107/17/19 15:453891
Parathion (Ethyl parathion)ND ug/kg 07/19/19 11:56 56-38-207/17/19 15:457771
Pentachlorobenzene ND ug/kg 07/19/19 11:56 608-93-507/17/19 15:453891
Pentachloroethane ND ug/kg 07/19/19 11:56 76-01-7 M107/17/19 15:457771
Pentachloronitrobenzene ND ug/kg 07/19/19 11:56 82-68-807/17/19 15:457771
Pentachlorophenol ND ug/kg 07/19/19 11:56 87-86-507/17/19 15:4519401
Phenacetin ND ug/kg 07/19/19 11:56 62-44-207/17/19 15:457771
Phenanthrene ND ug/kg 07/19/19 11:56 85-01-807/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-4 Lab ID:92436815011 Collected:07/10/19 11:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Phenol ND ug/kg 07/19/19 11:56 108-95-207/17/19 15:453891
p-Phenylenediamine ND ug/kg 07/19/19 11:56 106-50-307/17/19 15:457771
Phorate ND ug/kg 07/19/19 11:56 298-02-207/17/19 15:457771
Phthalic anhydride ND ug/kg 07/19/19 11:56 85-44-907/17/19 15:4529401
2-Picoline ND ug/kg 07/19/19 11:56 109-06-8 M107/17/19 15:453891
Pronamide ND ug/kg 07/19/19 11:56 23950-58-507/17/19 15:457771
Pyrene ND ug/kg 07/19/19 11:56 129-00-007/17/19 15:453891
Pyridine ND ug/kg 07/19/19 11:56 110-86-1 M107/17/19 15:453891
Safrole ND ug/kg 07/19/19 11:56 94-59-707/17/19 15:457771
Sulfotepp (Thiodiphosphoric Ac ND ug/kg 07/19/19 11:56 3689-24-507/17/19 15:457771
Terpineol ND ug/kg 07/19/19 11:56 98-55-5 M107/17/19 15:453891
1,2,4,5-Tetrachlorobenzene ND ug/kg 07/19/19 11:56 95-94-307/17/19 15:453891
2,3,4,6-Tetrachlorophenol ND ug/kg 07/19/19 11:56 58-90-207/17/19 15:453891
Thionazin ND ug/kg 07/19/19 11:56 297-97-207/17/19 15:457771
O-Toluidine ND ug/kg 07/19/19 11:56 95-53-4 M107/17/19 15:453891
1,2,4-Trichlorobenzene ND ug/kg 07/19/19 11:56 120-82-107/17/19 15:453891
2,4,5-Trichlorophenol ND ug/kg 07/19/19 11:56 95-95-407/17/19 15:453891
2,4,6-Trichlorophenol ND ug/kg 07/19/19 11:56 88-06-207/17/19 15:453891
1,3,5-Trinitrobenzene ND ug/kg 07/19/19 11:56 99-35-407/17/19 15:453891
Surrogates
2-Fluorobiphenyl (S)61 %07/19/19 11:56 321-60-807/17/19 15:4530-110 1
Terphenyl-d14 (S)70 %07/19/19 11:56 1718-51-007/17/19 15:4528-110 1
Phenol-d6 (S)66 %07/19/19 11:56 13127-88-307/17/19 15:4522-110 1
2-Fluorophenol (S)66 %07/19/19 11:56 367-12-407/17/19 15:4513-110 1
2,4,6-Tribromophenol (S)70 %07/19/19 11:56 118-79-607/17/19 15:4527-110 1
Nitrobenzene-d5 (S)71 %07/19/19 11:56 4165-60-007/17/19 15:4523-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.5 %07/16/19 14:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-1 Lab ID:92436815012 Collected:07/10/19 15:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 1.4 mg/kg 07/20/19 17:36 7440-38-207/19/19 10:540.97 1
Barium 53.6 mg/kg 07/20/19 17:36 7440-39-307/19/19 10:540.49 1
Cadmium ND mg/kg 07/21/19 17:25 7440-43-907/19/19 10:540.097 1
Chromium 12.3 mg/kg 07/20/19 17:36 7440-47-307/19/19 10:540.49 1
Lead 6.9 mg/kg 07/20/19 17:36 7439-92-107/19/19 10:540.49 1
Selenium ND mg/kg 07/20/19 17:36 7782-49-207/19/19 10:540.97 1
Silver ND mg/kg 07/20/19 17:36 7440-22-407/19/19 10:540.49 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.014 mg/kg 07/16/19 12:39 7439-97-607/16/19 10:250.0052 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 07/19/19 13:30 83-32-907/17/19 15:453891
Acenaphthylene ND ug/kg 07/19/19 13:30 208-96-807/17/19 15:453891
Acetophenone ND ug/kg 07/19/19 13:30 98-86-207/17/19 15:453891
2-Acetylaminofluorene ND ug/kg 07/19/19 13:30 53-96-307/17/19 15:457781
4-Aminobiphenyl ND ug/kg 07/19/19 13:30 92-67-1 v207/17/19 15:4538901
Aniline ND ug/kg 07/19/19 13:30 62-53-307/17/19 15:453891
Anthracene ND ug/kg 07/19/19 13:30 120-12-707/17/19 15:453891
Aramite ND ug/kg 07/19/19 13:30 140-57-807/17/19 15:4538901
Atrazine ND ug/kg 07/19/19 13:30 1912-24-9 L207/17/19 15:457781
Benzal chloride ND ug/kg 07/19/19 13:30 98-87-307/17/19 15:4511801
Benzaldehyde ND ug/kg 07/19/19 13:30 100-52-707/17/19 15:457781
Benzidine ND ug/kg 07/19/19 13:30 92-87-507/17/19 15:4519501
Benzo(a)anthracene ND ug/kg 07/19/19 13:30 56-55-307/17/19 15:453891
Benzo(a)pyrene ND ug/kg 07/19/19 13:30 50-32-807/17/19 15:453891
Benzo(b)fluoranthene ND ug/kg 07/19/19 13:30 205-99-207/17/19 15:453891
Benzo(g,h,i)perylene ND ug/kg 07/19/19 13:30 191-24-207/17/19 15:453891
Benzo(k)fluoranthene ND ug/kg 07/19/19 13:30 207-08-907/17/19 15:453891
Benzoic Acid ND ug/kg 07/19/19 13:30 65-85-007/17/19 15:4519501
Benzophenone ND ug/kg 07/19/19 13:30 119-61-907/17/19 15:453891
Benzyl alcohol ND ug/kg 07/19/19 13:30 100-51-607/17/19 15:457781
Biphenyl (Diphenyl)ND ug/kg 07/19/19 13:30 92-52-407/17/19 15:453891
4-Bromophenylphenyl ether ND ug/kg 07/19/19 13:30 101-55-307/17/19 15:453891
Butylbenzylphthalate ND ug/kg 07/19/19 13:30 85-68-707/17/19 15:453891
Caprolactam ND ug/kg 07/19/19 13:30 105-60-2 L207/17/19 15:453891
Carbazole ND ug/kg 07/19/19 13:30 86-74-807/17/19 15:453891
4-Chloro-3-methylphenol ND ug/kg 07/19/19 13:30 59-50-707/17/19 15:457781
4-Chloroaniline ND ug/kg 07/19/19 13:30 106-47-807/17/19 15:4519501
Chlorobenzilate ND ug/kg 07/19/19 13:30 510-15-607/17/19 15:453891
bis(2-Chloroethoxy)methane ND ug/kg 07/19/19 13:30 111-91-107/17/19 15:453891
bis(2-Chloroethyl) ether ND ug/kg 07/19/19 13:30 111-44-407/17/19 15:453891
2-Chloronaphthalene ND ug/kg 07/19/19 13:30 91-58-707/17/19 15:453891
2-Chlorophenol ND ug/kg 07/19/19 13:30 95-57-807/17/19 15:453891
4-Chlorophenylphenyl ether ND ug/kg 07/19/19 13:30 7005-72-307/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-1 Lab ID:92436815012 Collected:07/10/19 15:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Chrysene ND ug/kg 07/19/19 13:30 218-01-907/17/19 15:453891
n-Decane ND ug/kg 07/19/19 13:30 124-18-507/17/19 15:453891
Diallate ND ug/kg 07/19/19 13:30 2303-16-407/17/19 15:453891
Dibenz(a,h)anthracene ND ug/kg 07/19/19 13:30 53-70-307/17/19 15:453891
Dibenzo(a,e)pyrene ND ug/kg 07/19/19 13:30 192-65-407/17/19 15:4511801
Dibenzofuran ND ug/kg 07/19/19 13:30 132-64-907/17/19 15:453891
2,3-Dibromo-1-propanol phosph ND ug/kg 07/19/19 13:30 126-72-7 IC,L107/17/19 15:4529501
1,2-Dichlorobenzene ND ug/kg 07/19/19 13:30 95-50-107/17/19 15:453891
1,3-Dichlorobenzene ND ug/kg 07/19/19 13:30 541-73-107/17/19 15:453891
1,4-Dichlorobenzene ND ug/kg 07/19/19 13:30 106-46-707/17/19 15:453891
3,3'-Dichlorobenzidine ND ug/kg 07/19/19 13:30 91-94-107/17/19 15:4519501
2,4-Dichlorophenol ND ug/kg 07/19/19 13:30 120-83-207/17/19 15:453891
2,6-Dichlorophenol ND ug/kg 07/19/19 13:30 87-65-007/17/19 15:453891
2,3-Dichloroaniline ND ug/kg 07/19/19 13:30 608-27-507/17/19 15:453891
Diethylphthalate ND ug/kg 07/19/19 13:30 84-66-207/17/19 15:453891
Dimethoate ND ug/kg 07/19/19 13:30 60-51-5 IC,L107/17/19 15:457781
P-Dimethylaminoazobenzene ND ug/kg 07/19/19 13:30 60-11-707/17/19 15:457781
7,12-Dimethylbenz(a)anthracene ND ug/kg 07/19/19 13:30 57-97-607/17/19 15:453891
3,3'-Dimethylbenzidine ND ug/kg 07/19/19 13:30 119-93-707/17/19 15:4538901
2,4-Dimethylphenol ND ug/kg 07/19/19 13:30 105-67-907/17/19 15:453891
a,a-Dimethylphenylethylamine ND ug/kg 07/19/19 13:30 122-09-807/17/19 15:4519501
Dimethylphthalate ND ug/kg 07/19/19 13:30 131-11-307/17/19 15:453891
Di-n-butylphthalate ND ug/kg 07/19/19 13:30 84-74-207/17/19 15:453891
4,6-Dinitro-2-methylphenol ND ug/kg 07/19/19 13:30 534-52-1 v107/17/19 15:457781
1,3-Dinitrobenzene ND ug/kg 07/19/19 13:30 99-65-007/17/19 15:457781
1,4-Dinitrobenzene ND ug/kg 07/19/19 13:30 100-25-407/17/19 15:453891
2,4-Dinitrophenol ND ug/kg 07/19/19 13:30 51-28-507/17/19 15:4519501
2,4-Dinitrotoluene ND ug/kg 07/19/19 13:30 121-14-207/17/19 15:453891
2,6-Dinitrotoluene ND ug/kg 07/19/19 13:30 606-20-207/17/19 15:453891
Di-n-octylphthalate ND ug/kg 07/19/19 13:30 117-84-007/17/19 15:453891
Dinoseb ND ug/kg 07/19/19 13:30 88-85-707/17/19 15:457781
Diphenylamine ND ug/kg 07/19/19 13:30 122-39-407/17/19 15:453891
Diphenyl ether (Phenyl ether)ND ug/kg 07/19/19 13:30 101-84-807/17/19 15:455891
1,2-Diphenylhydrazine ND ug/kg 07/19/19 13:30 122-66-707/17/19 15:453891
Disulfoton ND ug/kg 07/19/19 13:30 298-04-407/17/19 15:457781
bis(2-Ethylhexyl)phthalate ND ug/kg 07/19/19 13:30 117-81-707/17/19 15:453891
Ethyl methanesulfonate ND ug/kg 07/19/19 13:30 62-50-007/17/19 15:457781
Famphur ND ug/kg 07/19/19 13:30 52-85-7 L207/17/19 15:4519501
Fluoranthene ND ug/kg 07/19/19 13:30 206-44-007/17/19 15:453891
Fluorene ND ug/kg 07/19/19 13:30 86-73-707/17/19 15:453891
Hexachloro-1,3-butadiene ND ug/kg 07/19/19 13:30 87-68-307/17/19 15:453891
Hexachlorobenzene ND ug/kg 07/19/19 13:30 118-74-107/17/19 15:453891
Hexachlorocyclopentadiene ND ug/kg 07/19/19 13:30 77-47-407/17/19 15:453891
Hexachloroethane ND ug/kg 07/19/19 13:30 67-72-107/17/19 15:453891
Hexachlorophene ND ug/kg 07/19/19 13:30 70-30-407/17/19 15:4538901
Hexachloropropene ND ug/kg 07/19/19 13:30 1888-71-707/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-1 Lab ID:92436815012 Collected:07/10/19 15:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 07/19/19 13:30 193-39-507/17/19 15:453891
Isodrin ND ug/kg 07/19/19 13:30 465-73-607/17/19 15:457781
Isophorone ND ug/kg 07/19/19 13:30 78-59-107/17/19 15:453891
Isosafrole ND ug/kg 07/19/19 13:30 120-58-107/17/19 15:453891
Kepone ND ug/kg 07/19/19 13:30 143-50-007/17/19 15:4519501
Methapyrilene ND ug/kg 07/19/19 13:30 91-80-507/17/19 15:4519501
3-Methylcholanthrene ND ug/kg 07/19/19 13:30 56-49-507/17/19 15:453891
4,4'-Methylene-bis(2-chloroani ND ug/kg 07/19/19 13:30 101-14-407/17/19 15:4511801
Methyl methanesulfonate ND ug/kg 07/19/19 13:30 66-27-307/17/19 15:457781
1-Methylnaphthalene ND ug/kg 07/19/19 13:30 90-12-007/17/19 15:453891
2-Methylnaphthalene ND ug/kg 07/19/19 13:30 91-57-607/17/19 15:453891
2-Methyl-5-nitroaniline ND ug/kg 07/19/19 13:30 99-55-807/17/19 15:453891
Methyl parathion ND ug/kg 07/19/19 13:30 298-00-0 L107/17/19 15:457781
2-Methylphenol(o-Cresol)ND ug/kg 07/19/19 13:30 95-48-707/17/19 15:453891
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/19/19 13:30 15831-10-407/17/19 15:453891
1-Naphthalenamine ND ug/kg 07/19/19 13:30 134-32-707/17/19 15:457781
2-Naphthalenamine ND ug/kg 07/19/19 13:30 91-59-807/17/19 15:457781
Naphthalene ND ug/kg 07/19/19 13:30 91-20-307/17/19 15:453891
1,4-Naphthoquinone ND ug/kg 07/19/19 13:30 130-15-4 IC,L107/17/19 15:4538901
2-Nitroaniline ND ug/kg 07/19/19 13:30 88-74-407/17/19 15:4519501
3-Nitroaniline ND ug/kg 07/19/19 13:30 99-09-207/17/19 15:4519501
4-Nitroaniline ND ug/kg 07/19/19 13:30 100-01-607/17/19 15:457781
Nitrobenzene ND ug/kg 07/19/19 13:30 98-95-307/17/19 15:453891
2-Nitrophenol ND ug/kg 07/19/19 13:30 88-75-507/17/19 15:453891
4-Nitrophenol ND ug/kg 07/19/19 13:30 100-02-707/17/19 15:4519501
4-Nitroquinoline-n-oxide ND ug/kg 07/19/19 13:30 56-57-507/17/19 15:4519501
5-Nitro-o-toluidine ND ug/kg 07/19/19 13:30 99-55-807/17/19 15:453891
N-Nitrosodiethylamine ND ug/kg 07/19/19 13:30 55-18-507/17/19 15:457781
N-Nitrosodimethylamine ND ug/kg 07/19/19 13:30 62-75-907/17/19 15:453891
N-Nitroso-di-n-butylamine ND ug/kg 07/19/19 13:30 924-16-307/17/19 15:453891
N-Nitroso-di-n-propylamine ND ug/kg 07/19/19 13:30 621-64-707/17/19 15:453891
N-Nitrosodiphenylamine ND ug/kg 07/19/19 13:30 86-30-607/17/19 15:453891
N-Nitrosomethylethylamine ND ug/kg 07/19/19 13:30 10595-95-607/17/19 15:453891
N-Nitrosomorpholine ND ug/kg 07/19/19 13:30 59-89-207/17/19 15:453891
N-Nitrosopiperidine ND ug/kg 07/19/19 13:30 100-75-407/17/19 15:457781
N-Nitrosopyrrolidine ND ug/kg 07/19/19 13:30 930-55-207/17/19 15:457781
n-Octadecane ND ug/kg 07/19/19 13:30 593-45-307/17/19 15:453891
O,O,O-Triethylphosphorothioate ND ug/kg 07/19/19 13:30 126-68-107/17/19 15:4519501
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/19/19 13:30 108-60-107/17/19 15:453891
Parathion (Ethyl parathion)ND ug/kg 07/19/19 13:30 56-38-207/17/19 15:457781
Pentachlorobenzene ND ug/kg 07/19/19 13:30 608-93-507/17/19 15:453891
Pentachloroethane ND ug/kg 07/19/19 13:30 76-01-707/17/19 15:457781
Pentachloronitrobenzene ND ug/kg 07/19/19 13:30 82-68-807/17/19 15:457781
Pentachlorophenol ND ug/kg 07/19/19 13:30 87-86-507/17/19 15:4519501
Phenacetin ND ug/kg 07/19/19 13:30 62-44-207/17/19 15:457781
Phenanthrene ND ug/kg 07/19/19 13:30 85-01-807/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-1 Lab ID:92436815012 Collected:07/10/19 15:30 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Phenol ND ug/kg 07/19/19 13:30 108-95-207/17/19 15:453891
p-Phenylenediamine ND ug/kg 07/19/19 13:30 106-50-307/17/19 15:457781
Phorate ND ug/kg 07/19/19 13:30 298-02-207/17/19 15:457781
Phthalic anhydride ND ug/kg 07/19/19 13:30 85-44-907/17/19 15:4529501
2-Picoline ND ug/kg 07/19/19 13:30 109-06-807/17/19 15:453891
Pronamide ND ug/kg 07/19/19 13:30 23950-58-507/17/19 15:457781
Pyrene ND ug/kg 07/19/19 13:30 129-00-007/17/19 15:453891
Pyridine ND ug/kg 07/19/19 13:30 110-86-107/17/19 15:453891
Safrole ND ug/kg 07/19/19 13:30 94-59-707/17/19 15:457781
Sulfotepp (Thiodiphosphoric Ac ND ug/kg 07/19/19 13:30 3689-24-507/17/19 15:457781
Terpineol ND ug/kg 07/19/19 13:30 98-55-507/17/19 15:453891
1,2,4,5-Tetrachlorobenzene ND ug/kg 07/19/19 13:30 95-94-307/17/19 15:453891
2,3,4,6-Tetrachlorophenol ND ug/kg 07/19/19 13:30 58-90-207/17/19 15:453891
Thionazin ND ug/kg 07/19/19 13:30 297-97-207/17/19 15:457781
O-Toluidine ND ug/kg 07/19/19 13:30 95-53-407/17/19 15:453891
1,2,4-Trichlorobenzene ND ug/kg 07/19/19 13:30 120-82-107/17/19 15:453891
2,4,5-Trichlorophenol ND ug/kg 07/19/19 13:30 95-95-407/17/19 15:453891
2,4,6-Trichlorophenol ND ug/kg 07/19/19 13:30 88-06-207/17/19 15:453891
1,3,5-Trinitrobenzene ND ug/kg 07/19/19 13:30 99-35-407/17/19 15:453891
Surrogates
2-Fluorobiphenyl (S)56 %07/19/19 13:30 321-60-807/17/19 15:4530-110 1
Terphenyl-d14 (S)66 %07/19/19 13:30 1718-51-007/17/19 15:4528-110 1
Phenol-d6 (S)61 %07/19/19 13:30 13127-88-307/17/19 15:4522-110 1
2-Fluorophenol (S)62 %07/19/19 13:30 367-12-407/17/19 15:4513-110 1
2,4,6-Tribromophenol (S)64 %07/19/19 13:30 118-79-607/17/19 15:4527-110 1
Nitrobenzene-d5 (S)67 %07/19/19 13:30 4165-60-007/17/19 15:4523-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.7 %07/16/19 14:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-3 Lab ID:92436815013 Collected:07/11/19 11:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 1.4 mg/kg 07/20/19 17:39 7440-38-207/19/19 10:541.1 1
Barium 138 mg/kg 07/20/19 17:39 7440-39-307/19/19 10:540.53 1
Cadmium ND mg/kg 07/21/19 17:28 7440-43-907/19/19 10:540.11 1
Chromium 27.2 mg/kg 07/20/19 17:39 7440-47-307/19/19 10:540.53 1
Lead 15.0 mg/kg 07/20/19 17:39 7439-92-107/19/19 10:540.53 1
Selenium 1.2 mg/kg 07/20/19 17:39 7782-49-207/19/19 10:541.1 1
Silver ND mg/kg 07/20/19 17:39 7440-22-407/19/19 10:540.53 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury 0.0088 mg/kg 07/16/19 12:42 7439-97-607/16/19 10:250.0041 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 07/19/19 14:01 83-32-907/17/19 15:454091
Acenaphthylene ND ug/kg 07/19/19 14:01 208-96-807/17/19 15:454091
Acetophenone ND ug/kg 07/19/19 14:01 98-86-207/17/19 15:454091
2-Acetylaminofluorene ND ug/kg 07/19/19 14:01 53-96-307/17/19 15:458191
4-Aminobiphenyl ND ug/kg 07/19/19 14:01 92-67-1 v107/17/19 15:4540901
Aniline ND ug/kg 07/19/19 14:01 62-53-307/17/19 15:454091
Anthracene ND ug/kg 07/19/19 14:01 120-12-707/17/19 15:454091
Aramite ND ug/kg 07/19/19 14:01 140-57-807/17/19 15:4540901
Atrazine ND ug/kg 07/19/19 14:01 1912-24-9 L207/17/19 15:458191
Benzal chloride ND ug/kg 07/19/19 14:01 98-87-307/17/19 15:4512401
Benzaldehyde ND ug/kg 07/19/19 14:01 100-52-707/17/19 15:458191
Benzidine ND ug/kg 07/19/19 14:01 92-87-507/17/19 15:4520501
Benzo(a)anthracene ND ug/kg 07/19/19 14:01 56-55-307/17/19 15:454091
Benzo(a)pyrene ND ug/kg 07/19/19 14:01 50-32-807/17/19 15:454091
Benzo(b)fluoranthene ND ug/kg 07/19/19 14:01 205-99-207/17/19 15:454091
Benzo(g,h,i)perylene ND ug/kg 07/19/19 14:01 191-24-207/17/19 15:454091
Benzo(k)fluoranthene ND ug/kg 07/19/19 14:01 207-08-907/17/19 15:454091
Benzoic Acid ND ug/kg 07/19/19 14:01 65-85-007/17/19 15:4520501
Benzophenone ND ug/kg 07/19/19 14:01 119-61-907/17/19 15:454091
Benzyl alcohol ND ug/kg 07/19/19 14:01 100-51-607/17/19 15:458191
Biphenyl (Diphenyl)ND ug/kg 07/19/19 14:01 92-52-407/17/19 15:454091
4-Bromophenylphenyl ether ND ug/kg 07/19/19 14:01 101-55-307/17/19 15:454091
Butylbenzylphthalate ND ug/kg 07/19/19 14:01 85-68-707/17/19 15:454091
Caprolactam ND ug/kg 07/19/19 14:01 105-60-2 L207/17/19 15:454091
Carbazole ND ug/kg 07/19/19 14:01 86-74-807/17/19 15:454091
4-Chloro-3-methylphenol ND ug/kg 07/19/19 14:01 59-50-707/17/19 15:458191
4-Chloroaniline ND ug/kg 07/19/19 14:01 106-47-807/17/19 15:4520501
Chlorobenzilate ND ug/kg 07/19/19 14:01 510-15-607/17/19 15:454091
bis(2-Chloroethoxy)methane ND ug/kg 07/19/19 14:01 111-91-107/17/19 15:454091
bis(2-Chloroethyl) ether ND ug/kg 07/19/19 14:01 111-44-407/17/19 15:454091
2-Chloronaphthalene ND ug/kg 07/19/19 14:01 91-58-707/17/19 15:454091
2-Chlorophenol ND ug/kg 07/19/19 14:01 95-57-807/17/19 15:454091
4-Chlorophenylphenyl ether ND ug/kg 07/19/19 14:01 7005-72-307/17/19 15:454091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-3 Lab ID:92436815013 Collected:07/11/19 11:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Chrysene ND ug/kg 07/19/19 14:01 218-01-907/17/19 15:454091
n-Decane ND ug/kg 07/19/19 14:01 124-18-507/17/19 15:454091
Diallate ND ug/kg 07/19/19 14:01 2303-16-407/17/19 15:454091
Dibenz(a,h)anthracene ND ug/kg 07/19/19 14:01 53-70-307/17/19 15:454091
Dibenzo(a,e)pyrene ND ug/kg 07/19/19 14:01 192-65-407/17/19 15:4512401
Dibenzofuran ND ug/kg 07/19/19 14:01 132-64-907/17/19 15:454091
2,3-Dibromo-1-propanol phosph ND ug/kg 07/19/19 14:01 126-72-7 IC,L107/17/19 15:4531001
1,2-Dichlorobenzene ND ug/kg 07/19/19 14:01 95-50-107/17/19 15:454091
1,3-Dichlorobenzene ND ug/kg 07/19/19 14:01 541-73-107/17/19 15:454091
1,4-Dichlorobenzene ND ug/kg 07/19/19 14:01 106-46-707/17/19 15:454091
3,3'-Dichlorobenzidine ND ug/kg 07/19/19 14:01 91-94-107/17/19 15:4520501
2,4-Dichlorophenol ND ug/kg 07/19/19 14:01 120-83-207/17/19 15:454091
2,6-Dichlorophenol ND ug/kg 07/19/19 14:01 87-65-007/17/19 15:454091
2,3-Dichloroaniline ND ug/kg 07/19/19 14:01 608-27-507/17/19 15:454091
Diethylphthalate ND ug/kg 07/19/19 14:01 84-66-207/17/19 15:454091
Dimethoate ND ug/kg 07/19/19 14:01 60-51-5 IC,L107/17/19 15:458191
P-Dimethylaminoazobenzene ND ug/kg 07/19/19 14:01 60-11-707/17/19 15:458191
7,12-Dimethylbenz(a)anthracene ND ug/kg 07/19/19 14:01 57-97-607/17/19 15:454091
3,3'-Dimethylbenzidine ND ug/kg 07/19/19 14:01 119-93-707/17/19 15:4540901
2,4-Dimethylphenol ND ug/kg 07/19/19 14:01 105-67-907/17/19 15:454091
a,a-Dimethylphenylethylamine ND ug/kg 07/19/19 14:01 122-09-807/17/19 15:4520501
Dimethylphthalate ND ug/kg 07/19/19 14:01 131-11-307/17/19 15:454091
Di-n-butylphthalate ND ug/kg 07/19/19 14:01 84-74-207/17/19 15:454091
4,6-Dinitro-2-methylphenol ND ug/kg 07/19/19 14:01 534-52-1 v107/17/19 15:458191
1,3-Dinitrobenzene ND ug/kg 07/19/19 14:01 99-65-007/17/19 15:458191
1,4-Dinitrobenzene ND ug/kg 07/19/19 14:01 100-25-407/17/19 15:454091
2,4-Dinitrophenol ND ug/kg 07/19/19 14:01 51-28-507/17/19 15:4520501
2,4-Dinitrotoluene ND ug/kg 07/19/19 14:01 121-14-207/17/19 15:454091
2,6-Dinitrotoluene ND ug/kg 07/19/19 14:01 606-20-207/17/19 15:454091
Di-n-octylphthalate ND ug/kg 07/19/19 14:01 117-84-007/17/19 15:454091
Dinoseb ND ug/kg 07/19/19 14:01 88-85-707/17/19 15:458191
Diphenylamine ND ug/kg 07/19/19 14:01 122-39-407/17/19 15:454091
Diphenyl ether (Phenyl ether)ND ug/kg 07/19/19 14:01 101-84-807/17/19 15:456201
1,2-Diphenylhydrazine ND ug/kg 07/19/19 14:01 122-66-707/17/19 15:454091
Disulfoton ND ug/kg 07/19/19 14:01 298-04-407/17/19 15:458191
bis(2-Ethylhexyl)phthalate ND ug/kg 07/19/19 14:01 117-81-707/17/19 15:454091
Ethyl methanesulfonate ND ug/kg 07/19/19 14:01 62-50-007/17/19 15:458191
Famphur ND ug/kg 07/19/19 14:01 52-85-7 L207/17/19 15:4520501
Fluoranthene ND ug/kg 07/19/19 14:01 206-44-007/17/19 15:454091
Fluorene ND ug/kg 07/19/19 14:01 86-73-707/17/19 15:454091
Hexachloro-1,3-butadiene ND ug/kg 07/19/19 14:01 87-68-307/17/19 15:454091
Hexachlorobenzene ND ug/kg 07/19/19 14:01 118-74-107/17/19 15:454091
Hexachlorocyclopentadiene ND ug/kg 07/19/19 14:01 77-47-407/17/19 15:454091
Hexachloroethane ND ug/kg 07/19/19 14:01 67-72-107/17/19 15:454091
Hexachlorophene ND ug/kg 07/19/19 14:01 70-30-407/17/19 15:4540901
Hexachloropropene ND ug/kg 07/19/19 14:01 1888-71-707/17/19 15:454091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-3 Lab ID:92436815013 Collected:07/11/19 11:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 07/19/19 14:01 193-39-507/17/19 15:454091
Isodrin ND ug/kg 07/19/19 14:01 465-73-607/17/19 15:458191
Isophorone ND ug/kg 07/19/19 14:01 78-59-107/17/19 15:454091
Isosafrole ND ug/kg 07/19/19 14:01 120-58-107/17/19 15:454091
Kepone ND ug/kg 07/19/19 14:01 143-50-007/17/19 15:4520501
Methapyrilene ND ug/kg 07/19/19 14:01 91-80-507/17/19 15:4520501
3-Methylcholanthrene ND ug/kg 07/19/19 14:01 56-49-507/17/19 15:454091
4,4'-Methylene-bis(2-chloroani ND ug/kg 07/19/19 14:01 101-14-407/17/19 15:4512401
Methyl methanesulfonate ND ug/kg 07/19/19 14:01 66-27-307/17/19 15:458191
1-Methylnaphthalene ND ug/kg 07/19/19 14:01 90-12-007/17/19 15:454091
2-Methylnaphthalene ND ug/kg 07/19/19 14:01 91-57-607/17/19 15:454091
2-Methyl-5-nitroaniline ND ug/kg 07/19/19 14:01 99-55-807/17/19 15:454091
Methyl parathion ND ug/kg 07/19/19 14:01 298-00-0 L107/17/19 15:458191
2-Methylphenol(o-Cresol)ND ug/kg 07/19/19 14:01 95-48-707/17/19 15:454091
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/19/19 14:01 15831-10-407/17/19 15:454091
1-Naphthalenamine ND ug/kg 07/19/19 14:01 134-32-707/17/19 15:458191
2-Naphthalenamine ND ug/kg 07/19/19 14:01 91-59-807/17/19 15:458191
Naphthalene ND ug/kg 07/19/19 14:01 91-20-307/17/19 15:454091
1,4-Naphthoquinone ND ug/kg 07/19/19 14:01 130-15-4 IC,L107/17/19 15:4540901
2-Nitroaniline ND ug/kg 07/19/19 14:01 88-74-407/17/19 15:4520501
3-Nitroaniline ND ug/kg 07/19/19 14:01 99-09-207/17/19 15:4520501
4-Nitroaniline ND ug/kg 07/19/19 14:01 100-01-607/17/19 15:458191
Nitrobenzene ND ug/kg 07/19/19 14:01 98-95-307/17/19 15:454091
2-Nitrophenol ND ug/kg 07/19/19 14:01 88-75-507/17/19 15:454091
4-Nitrophenol ND ug/kg 07/19/19 14:01 100-02-707/17/19 15:4520501
4-Nitroquinoline-n-oxide ND ug/kg 07/19/19 14:01 56-57-507/17/19 15:4520501
5-Nitro-o-toluidine ND ug/kg 07/19/19 14:01 99-55-807/17/19 15:454091
N-Nitrosodiethylamine ND ug/kg 07/19/19 14:01 55-18-507/17/19 15:458191
N-Nitrosodimethylamine ND ug/kg 07/19/19 14:01 62-75-907/17/19 15:454091
N-Nitroso-di-n-butylamine ND ug/kg 07/19/19 14:01 924-16-307/17/19 15:454091
N-Nitroso-di-n-propylamine ND ug/kg 07/19/19 14:01 621-64-707/17/19 15:454091
N-Nitrosodiphenylamine ND ug/kg 07/19/19 14:01 86-30-607/17/19 15:454091
N-Nitrosomethylethylamine ND ug/kg 07/19/19 14:01 10595-95-607/17/19 15:454091
N-Nitrosomorpholine ND ug/kg 07/19/19 14:01 59-89-207/17/19 15:454091
N-Nitrosopiperidine ND ug/kg 07/19/19 14:01 100-75-407/17/19 15:458191
N-Nitrosopyrrolidine ND ug/kg 07/19/19 14:01 930-55-207/17/19 15:458191
n-Octadecane ND ug/kg 07/19/19 14:01 593-45-307/17/19 15:454091
O,O,O-Triethylphosphorothioate ND ug/kg 07/19/19 14:01 126-68-107/17/19 15:4520501
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/19/19 14:01 108-60-107/17/19 15:454091
Parathion (Ethyl parathion)ND ug/kg 07/19/19 14:01 56-38-207/17/19 15:458191
Pentachlorobenzene ND ug/kg 07/19/19 14:01 608-93-507/17/19 15:454091
Pentachloroethane ND ug/kg 07/19/19 14:01 76-01-707/17/19 15:458191
Pentachloronitrobenzene ND ug/kg 07/19/19 14:01 82-68-807/17/19 15:458191
Pentachlorophenol ND ug/kg 07/19/19 14:01 87-86-507/17/19 15:4520501
Phenacetin ND ug/kg 07/19/19 14:01 62-44-207/17/19 15:458191
Phenanthrene ND ug/kg 07/19/19 14:01 85-01-807/17/19 15:454091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-3 Lab ID:92436815013 Collected:07/11/19 11:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Phenol ND ug/kg 07/19/19 14:01 108-95-207/17/19 15:454091
p-Phenylenediamine ND ug/kg 07/19/19 14:01 106-50-307/17/19 15:458191
Phorate ND ug/kg 07/19/19 14:01 298-02-207/17/19 15:458191
Phthalic anhydride ND ug/kg 07/19/19 14:01 85-44-907/17/19 15:4531001
2-Picoline ND ug/kg 07/19/19 14:01 109-06-807/17/19 15:454091
Pronamide ND ug/kg 07/19/19 14:01 23950-58-507/17/19 15:458191
Pyrene ND ug/kg 07/19/19 14:01 129-00-007/17/19 15:454091
Pyridine ND ug/kg 07/19/19 14:01 110-86-107/17/19 15:454091
Safrole ND ug/kg 07/19/19 14:01 94-59-707/17/19 15:458191
Sulfotepp (Thiodiphosphoric Ac ND ug/kg 07/19/19 14:01 3689-24-507/17/19 15:458191
Terpineol ND ug/kg 07/19/19 14:01 98-55-507/17/19 15:454091
1,2,4,5-Tetrachlorobenzene ND ug/kg 07/19/19 14:01 95-94-307/17/19 15:454091
2,3,4,6-Tetrachlorophenol ND ug/kg 07/19/19 14:01 58-90-207/17/19 15:454091
Thionazin ND ug/kg 07/19/19 14:01 297-97-207/17/19 15:458191
O-Toluidine ND ug/kg 07/19/19 14:01 95-53-407/17/19 15:454091
1,2,4-Trichlorobenzene ND ug/kg 07/19/19 14:01 120-82-107/17/19 15:454091
2,4,5-Trichlorophenol ND ug/kg 07/19/19 14:01 95-95-407/17/19 15:454091
2,4,6-Trichlorophenol ND ug/kg 07/19/19 14:01 88-06-207/17/19 15:454091
1,3,5-Trinitrobenzene ND ug/kg 07/19/19 14:01 99-35-407/17/19 15:454091
Surrogates
2-Fluorobiphenyl (S)68 %07/19/19 14:01 321-60-807/17/19 15:4530-110 1
Terphenyl-d14 (S)68 %07/19/19 14:01 1718-51-007/17/19 15:4528-110 1
Phenol-d6 (S)66 %07/19/19 14:01 13127-88-307/17/19 15:4522-110 1
2-Fluorophenol (S)67 %07/19/19 14:01 367-12-407/17/19 15:4513-110 1
2,4,6-Tribromophenol (S)75 %07/19/19 14:01 118-79-607/17/19 15:4527-110 1
Nitrobenzene-d5 (S)73 %07/19/19 14:01 4165-60-007/17/19 15:4523-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.7 %07/16/19 14:240.10 1
Analytical Method: EPA 7199 Preparation Method: EPA 30607199 Hexavalent Chromium Soil
Chromium, Hexavalent 2.2 mg/kg 08/01/19 15:28 18540-29-907/31/19 16:150.81 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-2 Lab ID:92436815014 Collected:07/11/19 13:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 1.7 mg/kg 07/20/19 17:48 7440-38-207/19/19 10:541.0 1
Barium 97.9 mg/kg 07/20/19 17:48 7440-39-307/19/19 10:540.51 1
Cadmium ND mg/kg 07/21/19 17:37 7440-43-907/19/19 10:540.10 1
Chromium 14.7 mg/kg 07/20/19 17:48 7440-47-307/19/19 10:540.51 1
Lead 9.1 mg/kg 07/20/19 17:48 7439-92-107/19/19 10:540.51 1
Selenium ND mg/kg 07/20/19 17:48 7782-49-207/19/19 10:541.0 1
Silver ND mg/kg 07/20/19 17:48 7440-22-407/19/19 10:540.51 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury ND mg/kg 07/16/19 12:44 7439-97-607/16/19 10:250.0047 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 07/19/19 14:33 83-32-907/17/19 15:454071
Acenaphthylene ND ug/kg 07/19/19 14:33 208-96-807/17/19 15:454071
Acetophenone ND ug/kg 07/19/19 14:33 98-86-207/17/19 15:454071
2-Acetylaminofluorene ND ug/kg 07/19/19 14:33 53-96-307/17/19 15:458141
4-Aminobiphenyl ND ug/kg 07/19/19 14:33 92-67-1 v207/17/19 15:4540701
Aniline ND ug/kg 07/19/19 14:33 62-53-307/17/19 15:454071
Anthracene ND ug/kg 07/19/19 14:33 120-12-707/17/19 15:454071
Aramite ND ug/kg 07/19/19 14:33 140-57-807/17/19 15:4540701
Atrazine ND ug/kg 07/19/19 14:33 1912-24-9 L207/17/19 15:458141
Benzal chloride ND ug/kg 07/19/19 14:33 98-87-307/17/19 15:4512301
Benzaldehyde ND ug/kg 07/19/19 14:33 100-52-707/17/19 15:458141
Benzidine ND ug/kg 07/19/19 14:33 92-87-507/17/19 15:4520301
Benzo(a)anthracene ND ug/kg 07/19/19 14:33 56-55-307/17/19 15:454071
Benzo(a)pyrene ND ug/kg 07/19/19 14:33 50-32-807/17/19 15:454071
Benzo(b)fluoranthene ND ug/kg 07/19/19 14:33 205-99-207/17/19 15:454071
Benzo(g,h,i)perylene ND ug/kg 07/19/19 14:33 191-24-207/17/19 15:454071
Benzo(k)fluoranthene ND ug/kg 07/19/19 14:33 207-08-907/17/19 15:454071
Benzoic Acid ND ug/kg 07/19/19 14:33 65-85-007/17/19 15:4520301
Benzophenone ND ug/kg 07/19/19 14:33 119-61-907/17/19 15:454071
Benzyl alcohol ND ug/kg 07/19/19 14:33 100-51-607/17/19 15:458141
Biphenyl (Diphenyl)ND ug/kg 07/19/19 14:33 92-52-407/17/19 15:454071
4-Bromophenylphenyl ether ND ug/kg 07/19/19 14:33 101-55-307/17/19 15:454071
Butylbenzylphthalate ND ug/kg 07/19/19 14:33 85-68-707/17/19 15:454071
Caprolactam ND ug/kg 07/19/19 14:33 105-60-2 L207/17/19 15:454071
Carbazole ND ug/kg 07/19/19 14:33 86-74-807/17/19 15:454071
4-Chloro-3-methylphenol ND ug/kg 07/19/19 14:33 59-50-707/17/19 15:458141
4-Chloroaniline ND ug/kg 07/19/19 14:33 106-47-807/17/19 15:4520301
Chlorobenzilate ND ug/kg 07/19/19 14:33 510-15-607/17/19 15:454071
bis(2-Chloroethoxy)methane ND ug/kg 07/19/19 14:33 111-91-107/17/19 15:454071
bis(2-Chloroethyl) ether ND ug/kg 07/19/19 14:33 111-44-407/17/19 15:454071
2-Chloronaphthalene ND ug/kg 07/19/19 14:33 91-58-707/17/19 15:454071
2-Chlorophenol ND ug/kg 07/19/19 14:33 95-57-807/17/19 15:454071
4-Chlorophenylphenyl ether ND ug/kg 07/19/19 14:33 7005-72-307/17/19 15:454071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-2 Lab ID:92436815014 Collected:07/11/19 13:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Chrysene ND ug/kg 07/19/19 14:33 218-01-907/17/19 15:454071
n-Decane ND ug/kg 07/19/19 14:33 124-18-507/17/19 15:454071
Diallate ND ug/kg 07/19/19 14:33 2303-16-407/17/19 15:454071
Dibenz(a,h)anthracene ND ug/kg 07/19/19 14:33 53-70-307/17/19 15:454071
Dibenzo(a,e)pyrene ND ug/kg 07/19/19 14:33 192-65-407/17/19 15:4512301
Dibenzofuran ND ug/kg 07/19/19 14:33 132-64-907/17/19 15:454071
2,3-Dibromo-1-propanol phosph ND ug/kg 07/19/19 14:33 126-72-7 IC,L107/17/19 15:4530801
1,2-Dichlorobenzene ND ug/kg 07/19/19 14:33 95-50-107/17/19 15:454071
1,3-Dichlorobenzene ND ug/kg 07/19/19 14:33 541-73-107/17/19 15:454071
1,4-Dichlorobenzene ND ug/kg 07/19/19 14:33 106-46-707/17/19 15:454071
3,3'-Dichlorobenzidine ND ug/kg 07/19/19 14:33 91-94-107/17/19 15:4520301
2,4-Dichlorophenol ND ug/kg 07/19/19 14:33 120-83-207/17/19 15:454071
2,6-Dichlorophenol ND ug/kg 07/19/19 14:33 87-65-007/17/19 15:454071
2,3-Dichloroaniline ND ug/kg 07/19/19 14:33 608-27-507/17/19 15:454071
Diethylphthalate ND ug/kg 07/19/19 14:33 84-66-207/17/19 15:454071
Dimethoate ND ug/kg 07/19/19 14:33 60-51-5 IC,L107/17/19 15:458141
P-Dimethylaminoazobenzene ND ug/kg 07/19/19 14:33 60-11-707/17/19 15:458141
7,12-Dimethylbenz(a)anthracene ND ug/kg 07/19/19 14:33 57-97-607/17/19 15:454071
3,3'-Dimethylbenzidine ND ug/kg 07/19/19 14:33 119-93-707/17/19 15:4540701
2,4-Dimethylphenol ND ug/kg 07/19/19 14:33 105-67-907/17/19 15:454071
a,a-Dimethylphenylethylamine ND ug/kg 07/19/19 14:33 122-09-807/17/19 15:4520301
Dimethylphthalate ND ug/kg 07/19/19 14:33 131-11-307/17/19 15:454071
Di-n-butylphthalate ND ug/kg 07/19/19 14:33 84-74-207/17/19 15:454071
4,6-Dinitro-2-methylphenol ND ug/kg 07/19/19 14:33 534-52-1 v107/17/19 15:458141
1,3-Dinitrobenzene ND ug/kg 07/19/19 14:33 99-65-007/17/19 15:458141
1,4-Dinitrobenzene ND ug/kg 07/19/19 14:33 100-25-407/17/19 15:454071
2,4-Dinitrophenol ND ug/kg 07/19/19 14:33 51-28-507/17/19 15:4520301
2,4-Dinitrotoluene ND ug/kg 07/19/19 14:33 121-14-207/17/19 15:454071
2,6-Dinitrotoluene ND ug/kg 07/19/19 14:33 606-20-207/17/19 15:454071
Di-n-octylphthalate ND ug/kg 07/19/19 14:33 117-84-007/17/19 15:454071
Dinoseb ND ug/kg 07/19/19 14:33 88-85-707/17/19 15:458141
Diphenylamine ND ug/kg 07/19/19 14:33 122-39-407/17/19 15:454071
Diphenyl ether (Phenyl ether)ND ug/kg 07/19/19 14:33 101-84-807/17/19 15:456171
1,2-Diphenylhydrazine ND ug/kg 07/19/19 14:33 122-66-707/17/19 15:454071
Disulfoton ND ug/kg 07/19/19 14:33 298-04-407/17/19 15:458141
bis(2-Ethylhexyl)phthalate ND ug/kg 07/19/19 14:33 117-81-707/17/19 15:454071
Ethyl methanesulfonate ND ug/kg 07/19/19 14:33 62-50-007/17/19 15:458141
Famphur ND ug/kg 07/19/19 14:33 52-85-7 L207/17/19 15:4520301
Fluoranthene ND ug/kg 07/19/19 14:33 206-44-007/17/19 15:454071
Fluorene ND ug/kg 07/19/19 14:33 86-73-707/17/19 15:454071
Hexachloro-1,3-butadiene ND ug/kg 07/19/19 14:33 87-68-307/17/19 15:454071
Hexachlorobenzene ND ug/kg 07/19/19 14:33 118-74-107/17/19 15:454071
Hexachlorocyclopentadiene ND ug/kg 07/19/19 14:33 77-47-407/17/19 15:454071
Hexachloroethane ND ug/kg 07/19/19 14:33 67-72-107/17/19 15:454071
Hexachlorophene ND ug/kg 07/19/19 14:33 70-30-407/17/19 15:4540701
Hexachloropropene ND ug/kg 07/19/19 14:33 1888-71-707/17/19 15:454071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-2 Lab ID:92436815014 Collected:07/11/19 13:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 07/19/19 14:33 193-39-507/17/19 15:454071
Isodrin ND ug/kg 07/19/19 14:33 465-73-607/17/19 15:458141
Isophorone ND ug/kg 07/19/19 14:33 78-59-107/17/19 15:454071
Isosafrole ND ug/kg 07/19/19 14:33 120-58-107/17/19 15:454071
Kepone ND ug/kg 07/19/19 14:33 143-50-007/17/19 15:4520301
Methapyrilene ND ug/kg 07/19/19 14:33 91-80-507/17/19 15:4520301
3-Methylcholanthrene ND ug/kg 07/19/19 14:33 56-49-507/17/19 15:454071
4,4'-Methylene-bis(2-chloroani ND ug/kg 07/19/19 14:33 101-14-407/17/19 15:4512301
Methyl methanesulfonate ND ug/kg 07/19/19 14:33 66-27-307/17/19 15:458141
1-Methylnaphthalene ND ug/kg 07/19/19 14:33 90-12-007/17/19 15:454071
2-Methylnaphthalene ND ug/kg 07/19/19 14:33 91-57-607/17/19 15:454071
2-Methyl-5-nitroaniline ND ug/kg 07/19/19 14:33 99-55-807/17/19 15:454071
Methyl parathion ND ug/kg 07/19/19 14:33 298-00-0 L107/17/19 15:458141
2-Methylphenol(o-Cresol)ND ug/kg 07/19/19 14:33 95-48-707/17/19 15:454071
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/19/19 14:33 15831-10-407/17/19 15:454071
1-Naphthalenamine ND ug/kg 07/19/19 14:33 134-32-707/17/19 15:458141
2-Naphthalenamine ND ug/kg 07/19/19 14:33 91-59-807/17/19 15:458141
Naphthalene ND ug/kg 07/19/19 14:33 91-20-307/17/19 15:454071
1,4-Naphthoquinone ND ug/kg 07/19/19 14:33 130-15-4 IC,L107/17/19 15:4540701
2-Nitroaniline ND ug/kg 07/19/19 14:33 88-74-407/17/19 15:4520301
3-Nitroaniline ND ug/kg 07/19/19 14:33 99-09-207/17/19 15:4520301
4-Nitroaniline ND ug/kg 07/19/19 14:33 100-01-607/17/19 15:458141
Nitrobenzene ND ug/kg 07/19/19 14:33 98-95-307/17/19 15:454071
2-Nitrophenol ND ug/kg 07/19/19 14:33 88-75-507/17/19 15:454071
4-Nitrophenol ND ug/kg 07/19/19 14:33 100-02-707/17/19 15:4520301
4-Nitroquinoline-n-oxide ND ug/kg 07/19/19 14:33 56-57-507/17/19 15:4520301
5-Nitro-o-toluidine ND ug/kg 07/19/19 14:33 99-55-807/17/19 15:454071
N-Nitrosodiethylamine ND ug/kg 07/19/19 14:33 55-18-507/17/19 15:458141
N-Nitrosodimethylamine ND ug/kg 07/19/19 14:33 62-75-907/17/19 15:454071
N-Nitroso-di-n-butylamine ND ug/kg 07/19/19 14:33 924-16-307/17/19 15:454071
N-Nitroso-di-n-propylamine ND ug/kg 07/19/19 14:33 621-64-707/17/19 15:454071
N-Nitrosodiphenylamine ND ug/kg 07/19/19 14:33 86-30-607/17/19 15:454071
N-Nitrosomethylethylamine ND ug/kg 07/19/19 14:33 10595-95-607/17/19 15:454071
N-Nitrosomorpholine ND ug/kg 07/19/19 14:33 59-89-207/17/19 15:454071
N-Nitrosopiperidine ND ug/kg 07/19/19 14:33 100-75-407/17/19 15:458141
N-Nitrosopyrrolidine ND ug/kg 07/19/19 14:33 930-55-207/17/19 15:458141
n-Octadecane ND ug/kg 07/19/19 14:33 593-45-307/17/19 15:454071
O,O,O-Triethylphosphorothioate ND ug/kg 07/19/19 14:33 126-68-107/17/19 15:4520301
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/19/19 14:33 108-60-107/17/19 15:454071
Parathion (Ethyl parathion)ND ug/kg 07/19/19 14:33 56-38-207/17/19 15:458141
Pentachlorobenzene ND ug/kg 07/19/19 14:33 608-93-507/17/19 15:454071
Pentachloroethane ND ug/kg 07/19/19 14:33 76-01-707/17/19 15:458141
Pentachloronitrobenzene ND ug/kg 07/19/19 14:33 82-68-807/17/19 15:458141
Pentachlorophenol ND ug/kg 07/19/19 14:33 87-86-507/17/19 15:4520301
Phenacetin ND ug/kg 07/19/19 14:33 62-44-207/17/19 15:458141
Phenanthrene ND ug/kg 07/19/19 14:33 85-01-807/17/19 15:454071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 39 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-2 Lab ID:92436815014 Collected:07/11/19 13:00 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Phenol ND ug/kg 07/19/19 14:33 108-95-207/17/19 15:454071
p-Phenylenediamine ND ug/kg 07/19/19 14:33 106-50-307/17/19 15:458141
Phorate ND ug/kg 07/19/19 14:33 298-02-207/17/19 15:458141
Phthalic anhydride ND ug/kg 07/19/19 14:33 85-44-907/17/19 15:4530801
2-Picoline ND ug/kg 07/19/19 14:33 109-06-807/17/19 15:454071
Pronamide ND ug/kg 07/19/19 14:33 23950-58-507/17/19 15:458141
Pyrene ND ug/kg 07/19/19 14:33 129-00-007/17/19 15:454071
Pyridine ND ug/kg 07/19/19 14:33 110-86-107/17/19 15:454071
Safrole ND ug/kg 07/19/19 14:33 94-59-707/17/19 15:458141
Sulfotepp (Thiodiphosphoric Ac ND ug/kg 07/19/19 14:33 3689-24-507/17/19 15:458141
Terpineol ND ug/kg 07/19/19 14:33 98-55-507/17/19 15:454071
1,2,4,5-Tetrachlorobenzene ND ug/kg 07/19/19 14:33 95-94-307/17/19 15:454071
2,3,4,6-Tetrachlorophenol ND ug/kg 07/19/19 14:33 58-90-207/17/19 15:454071
Thionazin ND ug/kg 07/19/19 14:33 297-97-207/17/19 15:458141
O-Toluidine ND ug/kg 07/19/19 14:33 95-53-407/17/19 15:454071
1,2,4-Trichlorobenzene ND ug/kg 07/19/19 14:33 120-82-107/17/19 15:454071
2,4,5-Trichlorophenol ND ug/kg 07/19/19 14:33 95-95-407/17/19 15:454071
2,4,6-Trichlorophenol ND ug/kg 07/19/19 14:33 88-06-207/17/19 15:454071
1,3,5-Trinitrobenzene ND ug/kg 07/19/19 14:33 99-35-407/17/19 15:454071
Surrogates
2-Fluorobiphenyl (S)70 %07/19/19 14:33 321-60-807/17/19 15:4530-110 1
Terphenyl-d14 (S)72 %07/19/19 14:33 1718-51-007/17/19 15:4528-110 1
Phenol-d6 (S)67 %07/19/19 14:33 13127-88-307/17/19 15:4522-110 1
2-Fluorophenol (S)67 %07/19/19 14:33 367-12-407/17/19 15:4513-110 1
2,4,6-Tribromophenol (S)77 %07/19/19 14:33 118-79-607/17/19 15:4527-110 1
Nitrobenzene-d5 (S)73 %07/19/19 14:33 4165-60-007/17/19 15:4523-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.0 %07/16/19 14:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-DUP-1 Lab ID:92436815015 Collected:07/11/19 00:01 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3050B6010 MET ICP
Arsenic 1.8 mg/kg 07/20/19 17:51 7440-38-207/19/19 10:541.1 1
Barium 76.0 mg/kg 07/20/19 17:51 7440-39-307/19/19 10:540.54 1
Cadmium ND mg/kg 07/21/19 17:41 7440-43-907/19/19 10:540.11 1
Chromium 11.5 mg/kg 07/20/19 17:51 7440-47-307/19/19 10:540.54 1
Lead 11.6 mg/kg 07/20/19 17:51 7439-92-107/19/19 10:540.54 1
Selenium ND mg/kg 07/20/19 17:51 7782-49-207/19/19 10:541.1 1
Silver ND mg/kg 07/20/19 17:51 7440-22-407/19/19 10:540.54 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B7471 Mercury
Mercury ND mg/kg 07/16/19 12:47 7439-97-607/16/19 10:250.0038 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 07/19/19 15:05 83-32-907/17/19 15:453891
Acenaphthylene ND ug/kg 07/19/19 15:05 208-96-807/17/19 15:453891
Acetophenone ND ug/kg 07/19/19 15:05 98-86-207/17/19 15:453891
2-Acetylaminofluorene ND ug/kg 07/19/19 15:05 53-96-307/17/19 15:457781
4-Aminobiphenyl ND ug/kg 07/19/19 15:05 92-67-1 v207/17/19 15:4538901
Aniline ND ug/kg 07/19/19 15:05 62-53-307/17/19 15:453891
Anthracene ND ug/kg 07/19/19 15:05 120-12-707/17/19 15:453891
Aramite ND ug/kg 07/19/19 15:05 140-57-807/17/19 15:4538901
Atrazine ND ug/kg 07/19/19 15:05 1912-24-9 L207/17/19 15:457781
Benzal chloride ND ug/kg 07/19/19 15:05 98-87-307/17/19 15:4511801
Benzaldehyde ND ug/kg 07/19/19 15:05 100-52-707/17/19 15:457781
Benzidine ND ug/kg 07/19/19 15:05 92-87-507/17/19 15:4519501
Benzo(a)anthracene ND ug/kg 07/19/19 15:05 56-55-307/17/19 15:453891
Benzo(a)pyrene ND ug/kg 07/19/19 15:05 50-32-807/17/19 15:453891
Benzo(b)fluoranthene ND ug/kg 07/19/19 15:05 205-99-207/17/19 15:453891
Benzo(g,h,i)perylene ND ug/kg 07/19/19 15:05 191-24-207/17/19 15:453891
Benzo(k)fluoranthene ND ug/kg 07/19/19 15:05 207-08-907/17/19 15:453891
Benzoic Acid ND ug/kg 07/19/19 15:05 65-85-007/17/19 15:4519501
Benzophenone ND ug/kg 07/19/19 15:05 119-61-907/17/19 15:453891
Benzyl alcohol ND ug/kg 07/19/19 15:05 100-51-607/17/19 15:457781
Biphenyl (Diphenyl)ND ug/kg 07/19/19 15:05 92-52-407/17/19 15:453891
4-Bromophenylphenyl ether ND ug/kg 07/19/19 15:05 101-55-307/17/19 15:453891
Butylbenzylphthalate ND ug/kg 07/19/19 15:05 85-68-707/17/19 15:453891
Caprolactam ND ug/kg 07/19/19 15:05 105-60-2 L207/17/19 15:453891
Carbazole ND ug/kg 07/19/19 15:05 86-74-807/17/19 15:453891
4-Chloro-3-methylphenol ND ug/kg 07/19/19 15:05 59-50-707/17/19 15:457781
4-Chloroaniline ND ug/kg 07/19/19 15:05 106-47-807/17/19 15:4519501
Chlorobenzilate ND ug/kg 07/19/19 15:05 510-15-607/17/19 15:453891
bis(2-Chloroethoxy)methane ND ug/kg 07/19/19 15:05 111-91-107/17/19 15:453891
bis(2-Chloroethyl) ether ND ug/kg 07/19/19 15:05 111-44-407/17/19 15:453891
2-Chloronaphthalene ND ug/kg 07/19/19 15:05 91-58-707/17/19 15:453891
2-Chlorophenol ND ug/kg 07/19/19 15:05 95-57-807/17/19 15:453891
4-Chlorophenylphenyl ether ND ug/kg 07/19/19 15:05 7005-72-307/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-DUP-1 Lab ID:92436815015 Collected:07/11/19 00:01 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Chrysene ND ug/kg 07/19/19 15:05 218-01-907/17/19 15:453891
n-Decane ND ug/kg 07/19/19 15:05 124-18-507/17/19 15:453891
Diallate ND ug/kg 07/19/19 15:05 2303-16-407/17/19 15:453891
Dibenz(a,h)anthracene ND ug/kg 07/19/19 15:05 53-70-307/17/19 15:453891
Dibenzo(a,e)pyrene ND ug/kg 07/19/19 15:05 192-65-407/17/19 15:4511801
Dibenzofuran ND ug/kg 07/19/19 15:05 132-64-907/17/19 15:453891
2,3-Dibromo-1-propanol phosph ND ug/kg 07/19/19 15:05 126-72-7 IC,L107/17/19 15:4529501
1,2-Dichlorobenzene ND ug/kg 07/19/19 15:05 95-50-107/17/19 15:453891
1,3-Dichlorobenzene ND ug/kg 07/19/19 15:05 541-73-107/17/19 15:453891
1,4-Dichlorobenzene ND ug/kg 07/19/19 15:05 106-46-707/17/19 15:453891
3,3'-Dichlorobenzidine ND ug/kg 07/19/19 15:05 91-94-107/17/19 15:4519501
2,4-Dichlorophenol ND ug/kg 07/19/19 15:05 120-83-207/17/19 15:453891
2,6-Dichlorophenol ND ug/kg 07/19/19 15:05 87-65-007/17/19 15:453891
2,3-Dichloroaniline ND ug/kg 07/19/19 15:05 608-27-507/17/19 15:453891
Diethylphthalate ND ug/kg 07/19/19 15:05 84-66-207/17/19 15:453891
Dimethoate ND ug/kg 07/19/19 15:05 60-51-5 IC,L107/17/19 15:457781
P-Dimethylaminoazobenzene ND ug/kg 07/19/19 15:05 60-11-707/17/19 15:457781
7,12-Dimethylbenz(a)anthracene ND ug/kg 07/19/19 15:05 57-97-607/17/19 15:453891
3,3'-Dimethylbenzidine ND ug/kg 07/19/19 15:05 119-93-707/17/19 15:4538901
2,4-Dimethylphenol ND ug/kg 07/19/19 15:05 105-67-907/17/19 15:453891
a,a-Dimethylphenylethylamine ND ug/kg 07/19/19 15:05 122-09-807/17/19 15:4519501
Dimethylphthalate ND ug/kg 07/19/19 15:05 131-11-307/17/19 15:453891
Di-n-butylphthalate ND ug/kg 07/19/19 15:05 84-74-207/17/19 15:453891
4,6-Dinitro-2-methylphenol ND ug/kg 07/19/19 15:05 534-52-1 v107/17/19 15:457781
1,3-Dinitrobenzene ND ug/kg 07/19/19 15:05 99-65-007/17/19 15:457781
1,4-Dinitrobenzene ND ug/kg 07/19/19 15:05 100-25-407/17/19 15:453891
2,4-Dinitrophenol ND ug/kg 07/19/19 15:05 51-28-507/17/19 15:4519501
2,4-Dinitrotoluene ND ug/kg 07/19/19 15:05 121-14-207/17/19 15:453891
2,6-Dinitrotoluene ND ug/kg 07/19/19 15:05 606-20-207/17/19 15:453891
Di-n-octylphthalate ND ug/kg 07/19/19 15:05 117-84-007/17/19 15:453891
Dinoseb ND ug/kg 07/19/19 15:05 88-85-707/17/19 15:457781
Diphenylamine ND ug/kg 07/19/19 15:05 122-39-407/17/19 15:453891
Diphenyl ether (Phenyl ether)ND ug/kg 07/19/19 15:05 101-84-807/17/19 15:455901
1,2-Diphenylhydrazine ND ug/kg 07/19/19 15:05 122-66-707/17/19 15:453891
Disulfoton ND ug/kg 07/19/19 15:05 298-04-407/17/19 15:457781
bis(2-Ethylhexyl)phthalate ND ug/kg 07/19/19 15:05 117-81-707/17/19 15:453891
Ethyl methanesulfonate ND ug/kg 07/19/19 15:05 62-50-007/17/19 15:457781
Famphur ND ug/kg 07/19/19 15:05 52-85-7 L207/17/19 15:4519501
Fluoranthene ND ug/kg 07/19/19 15:05 206-44-007/17/19 15:453891
Fluorene ND ug/kg 07/19/19 15:05 86-73-707/17/19 15:453891
Hexachloro-1,3-butadiene ND ug/kg 07/19/19 15:05 87-68-307/17/19 15:453891
Hexachlorobenzene ND ug/kg 07/19/19 15:05 118-74-107/17/19 15:453891
Hexachlorocyclopentadiene ND ug/kg 07/19/19 15:05 77-47-407/17/19 15:453891
Hexachloroethane ND ug/kg 07/19/19 15:05 67-72-107/17/19 15:453891
Hexachlorophene ND ug/kg 07/19/19 15:05 70-30-407/17/19 15:4538901
Hexachloropropene ND ug/kg 07/19/19 15:05 1888-71-707/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-DUP-1 Lab ID:92436815015 Collected:07/11/19 00:01 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Indeno(1,2,3-cd)pyrene ND ug/kg 07/19/19 15:05 193-39-507/17/19 15:453891
Isodrin ND ug/kg 07/19/19 15:05 465-73-607/17/19 15:457781
Isophorone ND ug/kg 07/19/19 15:05 78-59-107/17/19 15:453891
Isosafrole ND ug/kg 07/19/19 15:05 120-58-107/17/19 15:453891
Kepone ND ug/kg 07/19/19 15:05 143-50-007/17/19 15:4519501
Methapyrilene ND ug/kg 07/19/19 15:05 91-80-507/17/19 15:4519501
3-Methylcholanthrene ND ug/kg 07/19/19 15:05 56-49-507/17/19 15:453891
4,4'-Methylene-bis(2-chloroani ND ug/kg 07/19/19 15:05 101-14-407/17/19 15:4511801
Methyl methanesulfonate ND ug/kg 07/19/19 15:05 66-27-307/17/19 15:457781
1-Methylnaphthalene ND ug/kg 07/19/19 15:05 90-12-007/17/19 15:453891
2-Methylnaphthalene ND ug/kg 07/19/19 15:05 91-57-607/17/19 15:453891
2-Methyl-5-nitroaniline ND ug/kg 07/19/19 15:05 99-55-807/17/19 15:453891
Methyl parathion ND ug/kg 07/19/19 15:05 298-00-0 L107/17/19 15:457781
2-Methylphenol(o-Cresol)ND ug/kg 07/19/19 15:05 95-48-707/17/19 15:453891
3&4-Methylphenol(m&p Cresol)ND ug/kg 07/19/19 15:05 15831-10-407/17/19 15:453891
1-Naphthalenamine ND ug/kg 07/19/19 15:05 134-32-707/17/19 15:457781
2-Naphthalenamine ND ug/kg 07/19/19 15:05 91-59-807/17/19 15:457781
Naphthalene ND ug/kg 07/19/19 15:05 91-20-307/17/19 15:453891
1,4-Naphthoquinone ND ug/kg 07/19/19 15:05 130-15-4 IC,L107/17/19 15:4538901
2-Nitroaniline ND ug/kg 07/19/19 15:05 88-74-407/17/19 15:4519501
3-Nitroaniline ND ug/kg 07/19/19 15:05 99-09-207/17/19 15:4519501
4-Nitroaniline ND ug/kg 07/19/19 15:05 100-01-607/17/19 15:457781
Nitrobenzene ND ug/kg 07/19/19 15:05 98-95-307/17/19 15:453891
2-Nitrophenol ND ug/kg 07/19/19 15:05 88-75-507/17/19 15:453891
4-Nitrophenol ND ug/kg 07/19/19 15:05 100-02-707/17/19 15:4519501
4-Nitroquinoline-n-oxide ND ug/kg 07/19/19 15:05 56-57-507/17/19 15:4519501
5-Nitro-o-toluidine ND ug/kg 07/19/19 15:05 99-55-807/17/19 15:453891
N-Nitrosodiethylamine ND ug/kg 07/19/19 15:05 55-18-507/17/19 15:457781
N-Nitrosodimethylamine ND ug/kg 07/19/19 15:05 62-75-907/17/19 15:453891
N-Nitroso-di-n-butylamine ND ug/kg 07/19/19 15:05 924-16-307/17/19 15:453891
N-Nitroso-di-n-propylamine ND ug/kg 07/19/19 15:05 621-64-707/17/19 15:453891
N-Nitrosodiphenylamine ND ug/kg 07/19/19 15:05 86-30-607/17/19 15:453891
N-Nitrosomethylethylamine ND ug/kg 07/19/19 15:05 10595-95-607/17/19 15:453891
N-Nitrosomorpholine ND ug/kg 07/19/19 15:05 59-89-207/17/19 15:453891
N-Nitrosopiperidine ND ug/kg 07/19/19 15:05 100-75-407/17/19 15:457781
N-Nitrosopyrrolidine ND ug/kg 07/19/19 15:05 930-55-207/17/19 15:457781
n-Octadecane ND ug/kg 07/19/19 15:05 593-45-307/17/19 15:453891
O,O,O-Triethylphosphorothioate ND ug/kg 07/19/19 15:05 126-68-107/17/19 15:4519501
2,2'-Oxybis(1-chloropropane)ND ug/kg 07/19/19 15:05 108-60-107/17/19 15:453891
Parathion (Ethyl parathion)ND ug/kg 07/19/19 15:05 56-38-207/17/19 15:457781
Pentachlorobenzene ND ug/kg 07/19/19 15:05 608-93-507/17/19 15:453891
Pentachloroethane ND ug/kg 07/19/19 15:05 76-01-707/17/19 15:457781
Pentachloronitrobenzene ND ug/kg 07/19/19 15:05 82-68-807/17/19 15:457781
Pentachlorophenol ND ug/kg 07/19/19 15:05 87-86-507/17/19 15:4519501
Phenacetin ND ug/kg 07/19/19 15:05 62-44-207/17/19 15:457781
Phenanthrene ND ug/kg 07/19/19 15:05 85-01-807/17/19 15:453891
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 81
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Sample:BLDG-DUP-1 Lab ID:92436815015 Collected:07/11/19 00:01 Received:07/15/19 12:59 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Phenol ND ug/kg 07/19/19 15:05 108-95-207/17/19 15:453891
p-Phenylenediamine ND ug/kg 07/19/19 15:05 106-50-307/17/19 15:457781
Phorate ND ug/kg 07/19/19 15:05 298-02-207/17/19 15:457781
Phthalic anhydride ND ug/kg 07/19/19 15:05 85-44-907/17/19 15:4529501
2-Picoline ND ug/kg 07/19/19 15:05 109-06-807/17/19 15:453891
Pronamide ND ug/kg 07/19/19 15:05 23950-58-507/17/19 15:457781
Pyrene ND ug/kg 07/19/19 15:05 129-00-007/17/19 15:453891
Pyridine ND ug/kg 07/19/19 15:05 110-86-107/17/19 15:453891
Safrole ND ug/kg 07/19/19 15:05 94-59-707/17/19 15:457781
Sulfotepp (Thiodiphosphoric Ac ND ug/kg 07/19/19 15:05 3689-24-507/17/19 15:457781
Terpineol ND ug/kg 07/19/19 15:05 98-55-507/17/19 15:453891
1,2,4,5-Tetrachlorobenzene ND ug/kg 07/19/19 15:05 95-94-307/17/19 15:453891
2,3,4,6-Tetrachlorophenol ND ug/kg 07/19/19 15:05 58-90-207/17/19 15:453891
Thionazin ND ug/kg 07/19/19 15:05 297-97-207/17/19 15:457781
O-Toluidine ND ug/kg 07/19/19 15:05 95-53-407/17/19 15:453891
1,2,4-Trichlorobenzene ND ug/kg 07/19/19 15:05 120-82-107/17/19 15:453891
2,4,5-Trichlorophenol ND ug/kg 07/19/19 15:05 95-95-407/17/19 15:453891
2,4,6-Trichlorophenol ND ug/kg 07/19/19 15:05 88-06-207/17/19 15:453891
1,3,5-Trinitrobenzene ND ug/kg 07/19/19 15:05 99-35-407/17/19 15:453891
Surrogates
2-Fluorobiphenyl (S)68 %07/19/19 15:05 321-60-807/17/19 15:4530-110 1
Terphenyl-d14 (S)71 %07/19/19 15:05 1718-51-007/17/19 15:4528-110 1
Phenol-d6 (S)63 %07/19/19 15:05 13127-88-307/17/19 15:4522-110 1
2-Fluorophenol (S)62 %07/19/19 15:05 367-12-407/17/19 15:4513-110 1
2,4,6-Tribromophenol (S)78 %07/19/19 15:05 118-79-607/17/19 15:4527-110 1
Nitrobenzene-d5 (S)67 %07/19/19 15:05 4165-60-007/17/19 15:4523-110 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.6 %07/16/19 14:240.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
486565
EPA 7471B
EPA 7471B
7471 Mercury
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2627545
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0060 07/16/19 11:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2627546LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0800.083 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2627547MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92436507001
2627548
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg 1.3 78 75-12576 21.30.63 1.7 1.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
487340
EPA 3050B
EPA 6010D
6010 MET
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2631108
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.0 07/20/19 17:18
Barium mg/kg ND 0.50 07/20/19 17:18
Cadmium mg/kg ND 0.10 07/21/19 17:06
Chromium mg/kg ND 0.50 07/20/19 17:18
Lead mg/kg ND 0.50 07/20/19 17:18
Selenium mg/kg ND 1.0 07/20/19 17:18
Silver mg/kg ND 0.50 07/20/19 17:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2631109LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 41.450 83 80-120
Barium mg/kg 46.650 93 80-120
Cadmium mg/kg 45.850 92 80-120
Chromium mg/kg 46.650 93 80-120
Lead mg/kg 45.250 90 80-120
Selenium mg/kg 42.850 86 80-120
Silver mg/kg 23.325 93 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2631110MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92436815011
2631111
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg M142.1 73 75-12574 342.70.92 31.5 32.4
Barium mg/kg 42.1 105 75-125101 142.764.3 109 108
Cadmium mg/kg 42.1 86 75-12586 242.7ND 36.1 37.0
Chromium mg/kg 42.1 97 75-125100 342.710.7 51.8 53.4
Lead mg/kg 42.1 85 75-12578 542.711.5 47.3 45.0
Selenium mg/kg M142.1 69 75-12569 142.7ND 29.1 29.5
Silver mg/kg 21.1 92 75-12593 321.4ND 19.4 19.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
486612
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92436815001, 92436815002, 92436815003, 92436815004, 92436815005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2627701
Associated Lab Samples:92436815001, 92436815002, 92436815003, 92436815004, 92436815005
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/16/19 11:46
1,1,1-Trichloroethane ug/kg ND 5.0 07/16/19 11:46
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/16/19 11:46
1,1,2-Trichloroethane ug/kg ND 5.0 07/16/19 11:46
1,1-Dichloroethane ug/kg ND 5.0 07/16/19 11:46
1,1-Dichloroethene ug/kg ND 5.0 07/16/19 11:46
1,1-Dichloropropene ug/kg ND 5.0 07/16/19 11:46
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/16/19 11:46
1,2,3-Trichloropropane ug/kg ND 5.0 07/16/19 11:46
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/16/19 11:46
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/16/19 11:46
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/16/19 11:46
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/16/19 11:46
1,2-Dichlorobenzene ug/kg ND 5.0 07/16/19 11:46
1,2-Dichloroethane ug/kg ND 5.0 07/16/19 11:46
1,2-Dichloropropane ug/kg ND 5.0 07/16/19 11:46
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/16/19 11:46
1,3-Dichlorobenzene ug/kg ND 5.0 07/16/19 11:46
1,3-Dichloropropane ug/kg ND 5.0 07/16/19 11:46
1,4-Dichlorobenzene ug/kg ND 5.0 07/16/19 11:46
2,2-Dichloropropane ug/kg ND 5.0 07/16/19 11:46
2-Butanone (MEK)ug/kg ND 100 07/16/19 11:46
2-Chlorotoluene ug/kg ND 5.0 07/16/19 11:46
2-Hexanone ug/kg ND 50.0 07/16/19 11:46
4-Chlorotoluene ug/kg ND 5.0 07/16/19 11:46
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/16/19 11:46
Acetone ug/kg ND 100 07/16/19 11:46
Benzene ug/kg ND 5.0 07/16/19 11:46
Bromobenzene ug/kg ND 5.0 07/16/19 11:46
Bromochloromethane ug/kg ND 5.0 07/16/19 11:46
Bromodichloromethane ug/kg ND 5.0 07/16/19 11:46
Bromoform ug/kg ND 5.0 07/16/19 11:46
Bromomethane ug/kg ND 10.0 07/16/19 11:46
Carbon tetrachloride ug/kg ND 5.0 07/16/19 11:46
Chlorobenzene ug/kg ND 5.0 07/16/19 11:46
Chloroethane ug/kg ND 10.0 07/16/19 11:46
Chloroform ug/kg ND 5.0 07/16/19 11:46
Chloromethane ug/kg ND 10.0 07/16/19 11:46
cis-1,2-Dichloroethene ug/kg ND 5.0 07/16/19 11:46
cis-1,3-Dichloropropene ug/kg ND 5.0 07/16/19 11:46
Dibromochloromethane ug/kg ND 5.0 07/16/19 11:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2627701
Associated Lab Samples:92436815001, 92436815002, 92436815003, 92436815004, 92436815005
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.0 07/16/19 11:46
Dichlorodifluoromethane ug/kg ND 10.0 07/16/19 11:46
Diisopropyl ether ug/kg ND 5.0 07/16/19 11:46
Ethylbenzene ug/kg ND 5.0 07/16/19 11:46
Hexachloro-1,3-butadiene ug/kg ND 5.0 07/16/19 11:46
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/16/19 11:46
m&p-Xylene ug/kg ND 10.0 07/16/19 11:46
Methyl-tert-butyl ether ug/kg ND 5.0 07/16/19 11:46
Methylene Chloride ug/kg ND 20.0 v207/16/19 11:46
n-Butylbenzene ug/kg ND 5.0 07/16/19 11:46
n-Propylbenzene ug/kg ND 5.0 07/16/19 11:46
Naphthalene ug/kg ND 5.0 07/16/19 11:46
o-Xylene ug/kg ND 5.0 07/16/19 11:46
p-Isopropyltoluene ug/kg ND 5.0 07/16/19 11:46
sec-Butylbenzene ug/kg ND 5.0 07/16/19 11:46
Styrene ug/kg ND 5.0 07/16/19 11:46
tert-Butylbenzene ug/kg ND 5.0 07/16/19 11:46
Tetrachloroethene ug/kg ND 5.0 07/16/19 11:46
Toluene ug/kg ND 5.0 07/16/19 11:46
trans-1,2-Dichloroethene ug/kg ND 5.0 07/16/19 11:46
trans-1,3-Dichloropropene ug/kg ND 5.0 07/16/19 11:46
Trichloroethene ug/kg ND 5.0 07/16/19 11:46
Trichlorofluoromethane ug/kg ND 5.0 07/16/19 11:46
Vinyl acetate ug/kg ND 50.0 07/16/19 11:46
Vinyl chloride ug/kg ND 10.0 07/16/19 11:46
Xylene (Total)ug/kg ND 10.0 07/16/19 11:46
1,2-Dichloroethane-d4 (S)%96 70-132 07/16/19 11:46
4-Bromofluorobenzene (S)%100 70-130 07/16/19 11:46
Toluene-d8 (S)%99 70-130 07/16/19 11:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2627702LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2627703
1,1,1,2-Tetrachloroethane ug/kg 52.750 105 70-13010552.7 0 30
1,1,1-Trichloroethane ug/kg 45.150 90 70-1309447.1 4 30
1,1,2,2-Tetrachloroethane ug/kg 48.350 97 55-1309748.5 0 30
1,1,2-Trichloroethane ug/kg 48.850 98 70-1309648.0 2 30
1,1-Dichloroethane ug/kg 47.350 95 68-1309447.0 1 30
1,1-Dichloroethene ug/kg 48.450 97 70-1309848.9 1 30
1,1-Dichloropropene ug/kg 45.550 91 70-1309245.9 1 30
1,2,3-Trichlorobenzene ug/kg 47.150 94 70-1309648.0 2 30
1,2,3-Trichloropropane ug/kg 49.550 99 70-13010150.3 2 30
1,2,4-Trichlorobenzene ug/kg 49.250 98 70-1309949.4 1 30
1,2,4-Trimethylbenzene ug/kg 47.350 95 69-1309647.8 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2627702LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2627703
1,2-Dibromo-3-chloropropane ug/kg 52.050 104 57-14110653.2 2 30
1,2-Dibromoethane (EDB)ug/kg 49.750 99 70-1309949.5 0 30
1,2-Dichlorobenzene ug/kg 48.150 96 70-1309748.6 1 30
1,2-Dichloroethane ug/kg 44.950 90 70-1309346.3 3 30
1,2-Dichloropropane ug/kg 47.450 95 70-1309246.2 3 30
1,3,5-Trimethylbenzene ug/kg 47.350 95 70-1309547.4 0 30
1,3-Dichlorobenzene ug/kg 49.250 98 70-1309849.2 0 30
1,3-Dichloropropane ug/kg 50.350 101 70-13010049.8 1 30
1,4-Dichlorobenzene ug/kg 48.250 96 70-1309748.6 1 30
2,2-Dichloropropane ug/kg 49.450 99 70-1309949.7 1 30
2-Butanone (MEK)ug/kg 81.5J100 82 60-1307978.9J 30
2-Chlorotoluene ug/kg 46.950 94 70-1309547.6 2 30
2-Hexanone ug/kg 81.8100 82 70-1328281.6 0 30
4-Chlorotoluene ug/kg 46.550 93 70-1309648.0 3 30
4-Methyl-2-pentanone (MIBK)ug/kg 81.8100 82 69-1308080.0 2 30
Acetone ug/kg 87.5J100 87 49-1488080.1J 30
Benzene ug/kg 47.050 94 70-1309647.9 2 30
Bromobenzene ug/kg 48.850 98 70-13010050.0 2 30
Bromochloromethane ug/kg 52.650 105 70-13010250.8 4 30
Bromodichloromethane ug/kg 49.350 99 70-1309949.6 1 30
Bromoform ug/kg 52.850 106 68-13610653.0 0 30
Bromomethane ug/kg 57.450 115 60-14011658.2 1 30
Carbon tetrachloride ug/kg 49.550 99 70-13010049.9 1 30
Chlorobenzene ug/kg 47.550 95 70-1309849.2 3 30
Chloroethane ug/kg 58.950 118 51-14711859.2 0 30
Chloroform ug/kg 51.350 103 70-1309447.2 8 30
Chloromethane ug/kg 41.050 82 48-1308341.4 1 30
cis-1,2-Dichloroethene ug/kg 46.050 92 70-1309246.2 0 30
cis-1,3-Dichloropropene ug/kg 49.350 99 70-13010050.1 2 30
Dibromochloromethane ug/kg 49.650 99 70-13010150.5 2 30
Dibromomethane ug/kg 50.150 100 70-13010753.3 6 30
Dichlorodifluoromethane ug/kg 52.750 105 49-13010452.2 1 30
Diisopropyl ether ug/kg 40.950 82 66-1308240.8 0 30
Ethylbenzene ug/kg 47.450 95 70-1309647.9 1 30
Hexachloro-1,3-butadiene ug/kg 47.650 95 70-1309848.8 2 30
Isopropylbenzene (Cumene)ug/kg 48.750 97 70-1309848.9 0 30
m&p-Xylene ug/kg 97.4100 97 70-1309998.8 1 30
Methyl-tert-butyl ether ug/kg 48.950 98 70-1309346.6 5 30
Methylene Chloride ug/kg 39.0 v3507850-1377939.3 1 30
n-Butylbenzene ug/kg 48.950 98 70-1309848.9 0 30
n-Propylbenzene ug/kg 49.050 98 70-1309848.9 0 30
Naphthalene ug/kg 45.050 90 70-1319346.6 4 30
o-Xylene ug/kg 47.350 95 70-1309748.4 2 30
p-Isopropyltoluene ug/kg 47.550 95 70-1309647.9 1 30
sec-Butylbenzene ug/kg 49.750 99 70-13010050.2 1 30
Styrene ug/kg 47.650 95 70-1309547.6 0 30
tert-Butylbenzene ug/kg 44.050 88 69-1308944.3 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2627702LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2627703
Tetrachloroethene ug/kg 49.450 99 56-1309949.4 0 30
Toluene ug/kg 47.450 95 70-1309446.9 1 30
trans-1,2-Dichloroethene ug/kg 46.850 94 70-1309245.8 2 30
trans-1,3-Dichloropropene ug/kg 50.250 100 70-1309949.3 2 30
Trichloroethene ug/kg 51.150 102 70-14110150.3 2 30
Trichlorofluoromethane ug/kg 50.450 101 67-1309949.4 2 30
Vinyl acetate ug/kg 102100 102 10-1369191.3 11 30
Vinyl chloride ug/kg 51.550 103 67-1309949.4 4 30
Xylene (Total)ug/kg 145150 96 70-13098147 2 30
1,2-Dichloroethane-d4 (S)%94 70-13288
4-Bromofluorobenzene (S)%99 70-130100
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
486855
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92436815006, 92436815007, 92436815008, 92436815009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2628675
Associated Lab Samples:92436815006, 92436815007, 92436815008, 92436815009
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/17/19 14:03
1,1,1-Trichloroethane ug/kg ND 5.0 07/17/19 14:03
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/17/19 14:03
1,1,2-Trichloroethane ug/kg ND 5.0 07/17/19 14:03
1,1-Dichloroethane ug/kg ND 5.0 07/17/19 14:03
1,1-Dichloroethene ug/kg ND 5.0 07/17/19 14:03
1,1-Dichloropropene ug/kg ND 5.0 07/17/19 14:03
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/17/19 14:03
1,2,3-Trichloropropane ug/kg ND 5.0 07/17/19 14:03
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/17/19 14:03
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/17/19 14:03
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/17/19 14:03
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/17/19 14:03
1,2-Dichlorobenzene ug/kg ND 5.0 07/17/19 14:03
1,2-Dichloroethane ug/kg ND 5.0 07/17/19 14:03
1,2-Dichloropropane ug/kg ND 5.0 07/17/19 14:03
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/17/19 14:03
1,3-Dichlorobenzene ug/kg ND 5.0 07/17/19 14:03
1,3-Dichloropropane ug/kg ND 5.0 07/17/19 14:03
1,4-Dichlorobenzene ug/kg ND 5.0 07/17/19 14:03
2,2-Dichloropropane ug/kg ND 5.0 07/17/19 14:03
2-Butanone (MEK)ug/kg ND 100 07/17/19 14:03
2-Chlorotoluene ug/kg ND 5.0 07/17/19 14:03
2-Hexanone ug/kg ND 50.0 07/17/19 14:03
4-Chlorotoluene ug/kg ND 5.0 07/17/19 14:03
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/17/19 14:03
Acetone ug/kg ND 100 07/17/19 14:03
Benzene ug/kg ND 5.0 07/17/19 14:03
Bromobenzene ug/kg ND 5.0 07/17/19 14:03
Bromochloromethane ug/kg ND 5.0 07/17/19 14:03
Bromodichloromethane ug/kg ND 5.0 07/17/19 14:03
Bromoform ug/kg ND 5.0 07/17/19 14:03
Bromomethane ug/kg ND 10.0 07/17/19 14:03
Carbon tetrachloride ug/kg ND 5.0 07/17/19 14:03
Chlorobenzene ug/kg ND 5.0 07/17/19 14:03
Chloroethane ug/kg ND 10.0 07/17/19 14:03
Chloroform ug/kg ND 5.0 07/17/19 14:03
Chloromethane ug/kg ND 10.0 07/17/19 14:03
cis-1,2-Dichloroethene ug/kg ND 5.0 07/17/19 14:03
cis-1,3-Dichloropropene ug/kg ND 5.0 07/17/19 14:03
Dibromochloromethane ug/kg ND 5.0 07/17/19 14:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2628675
Associated Lab Samples:92436815006, 92436815007, 92436815008, 92436815009
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.0 07/17/19 14:03
Dichlorodifluoromethane ug/kg ND 10.0 07/17/19 14:03
Diisopropyl ether ug/kg ND 5.0 07/17/19 14:03
Ethylbenzene ug/kg ND 5.0 07/17/19 14:03
Hexachloro-1,3-butadiene ug/kg ND 5.0 IK07/17/19 14:03
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/17/19 14:03
m&p-Xylene ug/kg ND 10.0 07/17/19 14:03
Methyl-tert-butyl ether ug/kg ND 5.0 07/17/19 14:03
Methylene Chloride ug/kg ND 20.0 07/17/19 14:03
n-Butylbenzene ug/kg ND 5.0 07/17/19 14:03
n-Propylbenzene ug/kg ND 5.0 07/17/19 14:03
Naphthalene ug/kg ND 5.0 07/17/19 14:03
o-Xylene ug/kg ND 5.0 07/17/19 14:03
p-Isopropyltoluene ug/kg ND 5.0 07/17/19 14:03
sec-Butylbenzene ug/kg ND 5.0 07/17/19 14:03
Styrene ug/kg ND 5.0 07/17/19 14:03
tert-Butylbenzene ug/kg ND 5.0 07/17/19 14:03
Tetrachloroethene ug/kg ND 5.0 07/17/19 14:03
Toluene ug/kg ND 5.0 07/17/19 14:03
trans-1,2-Dichloroethene ug/kg ND 5.0 07/17/19 14:03
trans-1,3-Dichloropropene ug/kg ND 5.0 07/17/19 14:03
Trichloroethene ug/kg ND 5.0 07/17/19 14:03
Trichlorofluoromethane ug/kg ND 5.0 07/17/19 14:03
Vinyl acetate ug/kg ND 50.0 07/17/19 14:03
Vinyl chloride ug/kg ND 10.0 07/17/19 14:03
Xylene (Total)ug/kg ND 10.0 07/17/19 14:03
1,2-Dichloroethane-d4 (S)%104 70-132 07/17/19 14:03
4-Bromofluorobenzene (S)%101 70-130 07/17/19 14:03
Toluene-d8 (S)%99 70-130 07/17/19 14:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2628676LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2628677
1,1,1,2-Tetrachloroethane ug/kg 53.550 107 70-13010049.8 7 30
1,1,1-Trichloroethane ug/kg 47.850 96 70-1309246.0 4 30
1,1,2,2-Tetrachloroethane ug/kg 52.350 105 55-1309949.6 5 30
1,1,2-Trichloroethane ug/kg 50.750 101 70-13010150.3 1 30
1,1-Dichloroethane ug/kg 48.250 96 68-1309346.6 3 30
1,1-Dichloroethene ug/kg 51.950 104 70-13010049.8 4 30
1,1-Dichloropropene ug/kg 46.350 93 70-1308743.7 6 30
1,2,3-Trichlorobenzene ug/kg 47.650 95 70-1308844.1 8 30
1,2,3-Trichloropropane ug/kg 55.450 111 70-13010251.0 8 30
1,2,4-Trichlorobenzene ug/kg 45.850 92 70-1308542.6 7 30
1,2,4-Trimethylbenzene ug/kg 47.450 95 69-1309044.8 6 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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Huntersville, NC 28078
[phone]
Page 52 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2628676LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2628677
1,2-Dibromo-3-chloropropane ug/kg 56.550 113 57-14110552.5 7 30
1,2-Dibromoethane (EDB)ug/kg 54.150 108 70-13010150.6 7 30
1,2-Dichlorobenzene ug/kg 48.350 97 70-1309145.7 5 30
1,2-Dichloroethane ug/kg 49.350 99 70-1309446.9 5 30
1,2-Dichloropropane ug/kg 49.650 99 70-1309748.5 2 30
1,3,5-Trimethylbenzene ug/kg 48.650 97 70-1309045.2 7 30
1,3-Dichlorobenzene ug/kg 46.250 92 70-1308844.2 5 30
1,3-Dichloropropane ug/kg 53.450 107 70-13010250.9 5 30
1,4-Dichlorobenzene ug/kg 46.350 93 70-1308843.8 5 30
2,2-Dichloropropane ug/kg 48.150 96 70-1309045.1 6 30
2-Butanone (MEK)ug/kg 96.9J100 97 60-1309494.4J 30
2-Chlorotoluene ug/kg 47.250 94 70-1309045.1 5 30
2-Hexanone ug/kg 105100 105 70-132101101 4 30
4-Chlorotoluene ug/kg 47.150 94 70-1308944.3 6 30
4-Methyl-2-pentanone (MIBK)ug/kg 102100 102 69-130102102 0 30
Acetone ug/kg 117100 117 49-148110110 6 30
Benzene ug/kg 49.750 99 70-1309648.0 3 30
Bromobenzene ug/kg 49.350 99 70-1309346.5 6 30
Bromochloromethane ug/kg 47.750 95 70-1309145.7 4 30
Bromodichloromethane ug/kg 50.750 101 70-1309648.0 5 30
Bromoform ug/kg 55.750 111 68-13610552.7 6 30
Bromomethane ug/kg 64.450 129 60-14010653.1 19 30
Carbon tetrachloride ug/kg 47.750 95 70-1309245.9 4 30
Chlorobenzene ug/kg 49.250 98 70-1309145.7 7 30
Chloroethane ug/kg 53.550 107 51-14710049.9 7 30
Chloroform ug/kg 48.050 96 70-1309145.5 5 30
Chloromethane ug/kg 52.350 105 48-13010050.1 4 30
cis-1,2-Dichloroethene ug/kg 48.750 97 70-1309346.7 4 30
cis-1,3-Dichloropropene ug/kg 51.750 103 70-13010150.6 2 30
Dibromochloromethane ug/kg 53.650 107 70-1309748.7 10 30
Dibromomethane ug/kg 51.950 104 70-1309949.5 5 30
Dichlorodifluoromethane ug/kg 53.150 106 49-13010351.5 3 30
Diisopropyl ether ug/kg 50.950 102 66-13010150.3 1 30
Ethylbenzene ug/kg 49.350 99 70-1309246.0 7 30
Hexachloro-1,3-butadiene ug/kg 49.5 IK509970-1309246.1 7 30
Isopropylbenzene (Cumene)ug/kg 50.250 100 70-1309346.4 8 30
m&p-Xylene ug/kg 99.5100 99 70-1309291.7 8 30
Methyl-tert-butyl ether ug/kg 51.050 102 70-1309849.2 4 30
Methylene Chloride ug/kg 55.750 111 50-13710552.6 6 30
n-Butylbenzene ug/kg 46.650 93 70-1308944.4 5 30
n-Propylbenzene ug/kg 47.550 95 70-1309045.0 5 30
Naphthalene ug/kg 50.050 100 70-1319346.7 7 30
o-Xylene ug/kg 50.050 100 70-1309145.7 9 30
p-Isopropyltoluene ug/kg 47.650 95 70-1309045.0 6 30
sec-Butylbenzene ug/kg 49.250 98 70-1309446.8 5 30
Styrene ug/kg 50.450 101 70-1309346.3 9 30
tert-Butylbenzene ug/kg 43.050 86 69-1308140.3 7 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 53 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2628676LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2628677
Tetrachloroethene ug/kg 49.750 99 56-1309145.6 9 30
Toluene ug/kg 47.750 95 70-1309246.2 3 30
trans-1,2-Dichloroethene ug/kg 50.150 100 70-1309346.7 7 30
trans-1,3-Dichloropropene ug/kg 51.050 102 70-1309949.5 3 30
Trichloroethene ug/kg 48.150 96 70-1419245.9 5 30
Trichlorofluoromethane ug/kg 50.550 101 67-1309748.5 4 30
Vinyl acetate ug/kg 69.3100 69 10-1366868.4 1 30
Vinyl chloride ug/kg 51.650 103 67-13010050.0 3 30
Xylene (Total)ug/kg 149150 100 70-13092137 8 30
1,2-Dichloroethane-d4 (S)%98 70-13297
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%97 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
486667
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples:92436815010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2627971
Associated Lab Samples:92436815010
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 07/16/19 11:50
1,1,1-Trichloroethane ug/L ND 1.0 07/16/19 11:50
1,1,2,2-Tetrachloroethane ug/L ND 1.0 07/16/19 11:50
1,1,2-Trichloroethane ug/L ND 1.0 07/16/19 11:50
1,1-Dichloroethane ug/L ND 1.0 07/16/19 11:50
1,1-Dichloroethene ug/L ND 1.0 07/16/19 11:50
1,1-Dichloropropene ug/L ND 1.0 07/16/19 11:50
1,2,3-Trichlorobenzene ug/L ND 1.0 07/16/19 11:50
1,2,3-Trichloropropane ug/L ND 1.0 07/16/19 11:50
1,2,4-Trichlorobenzene ug/L ND 1.0 07/16/19 11:50
1,2-Dibromo-3-chloropropane ug/L ND 5.0 07/16/19 11:50
1,2-Dibromoethane (EDB)ug/L ND 1.0 07/16/19 11:50
1,2-Dichlorobenzene ug/L ND 1.0 07/16/19 11:50
1,2-Dichloroethane ug/L ND 1.0 07/16/19 11:50
1,2-Dichloropropane ug/L ND 1.0 07/16/19 11:50
1,3-Dichlorobenzene ug/L ND 1.0 07/16/19 11:50
1,3-Dichloropropane ug/L ND 1.0 07/16/19 11:50
1,4-Dichlorobenzene ug/L ND 1.0 07/16/19 11:50
2,2-Dichloropropane ug/L ND 1.0 07/16/19 11:50
2-Butanone (MEK)ug/L ND 5.0 07/16/19 11:50
2-Chlorotoluene ug/L ND 1.0 07/16/19 11:50
2-Hexanone ug/L ND 5.0 07/16/19 11:50
4-Chlorotoluene ug/L ND 1.0 07/16/19 11:50
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 07/16/19 11:50
Acetone ug/L ND 25.0 07/16/19 11:50
Benzene ug/L ND 1.0 07/16/19 11:50
Bromobenzene ug/L ND 1.0 07/16/19 11:50
Bromochloromethane ug/L ND 1.0 07/16/19 11:50
Bromodichloromethane ug/L ND 1.0 07/16/19 11:50
Bromoform ug/L ND 1.0 07/16/19 11:50
Bromomethane ug/L ND 2.0 v107/16/19 11:50
Carbon tetrachloride ug/L ND 1.0 07/16/19 11:50
Chlorobenzene ug/L ND 1.0 07/16/19 11:50
Chloroethane ug/L ND 1.0 07/16/19 11:50
Chloroform ug/L ND 5.0 07/16/19 11:50
Chloromethane ug/L ND 1.0 07/16/19 11:50
cis-1,2-Dichloroethene ug/L ND 1.0 07/16/19 11:50
cis-1,3-Dichloropropene ug/L ND 1.0 07/16/19 11:50
Dibromochloromethane ug/L ND 1.0 07/16/19 11:50
Dibromomethane ug/L ND 1.0 07/16/19 11:50
Dichlorodifluoromethane ug/L ND 1.0 07/16/19 11:50
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2627971
Associated Lab Samples:92436815010
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 07/16/19 11:50
Ethylbenzene ug/L ND 1.0 07/16/19 11:50
Hexachloro-1,3-butadiene ug/L ND 1.0 07/16/19 11:50
m&p-Xylene ug/L ND 2.0 07/16/19 11:50
Methyl-tert-butyl ether ug/L ND 1.0 07/16/19 11:50
Methylene Chloride ug/L ND 5.0 07/16/19 11:50
Naphthalene ug/L ND 1.0 07/16/19 11:50
o-Xylene ug/L ND 1.0 07/16/19 11:50
p-Isopropyltoluene ug/L ND 1.0 07/16/19 11:50
Styrene ug/L ND 1.0 07/16/19 11:50
Tetrachloroethene ug/L ND 1.0 07/16/19 11:50
Toluene ug/L ND 1.0 07/16/19 11:50
trans-1,2-Dichloroethene ug/L ND 1.0 07/16/19 11:50
trans-1,3-Dichloropropene ug/L ND 1.0 07/16/19 11:50
Trichloroethene ug/L ND 1.0 07/16/19 11:50
Trichlorofluoromethane ug/L ND 1.0 07/16/19 11:50
Vinyl acetate ug/L ND 2.0 07/16/19 11:50
Vinyl chloride ug/L ND 1.0 07/16/19 11:50
Xylene (Total)ug/L ND 1.0 07/16/19 11:50
1,2-Dichloroethane-d4 (S)%107 70-130 07/16/19 11:50
4-Bromofluorobenzene (S)%105 70-130 07/16/19 11:50
Toluene-d8 (S)%104 70-130 07/16/19 11:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2627972LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.550 101 70-130
1,1,1-Trichloroethane ug/L 49.950 100 70-130
1,1,2,2-Tetrachloroethane ug/L 50.350 101 70-130
1,1,2-Trichloroethane ug/L 50.750 101 70-130
1,1-Dichloroethane ug/L 52.150 104 70-130
1,1-Dichloroethene ug/L 54.850 110 70-130
1,1-Dichloropropene ug/L 49.850 100 70-130
1,2,3-Trichlorobenzene ug/L 51.550 103 70-130
1,2,3-Trichloropropane ug/L 51.850 104 70-130
1,2,4-Trichlorobenzene ug/L 49.350 99 70-130
1,2-Dibromo-3-chloropropane ug/L 49.150 98 70-130
1,2-Dibromoethane (EDB)ug/L 50.450 101 70-130
1,2-Dichlorobenzene ug/L 48.350 97 70-130
1,2-Dichloroethane ug/L 48.650 97 70-130
1,2-Dichloropropane ug/L 50.150 100 70-130
1,3-Dichlorobenzene ug/L 49.250 98 70-130
1,3-Dichloropropane ug/L 51.750 103 70-131
1,4-Dichlorobenzene ug/L 48.450 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2627972LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 53.050 106 69-130
2-Butanone (MEK)ug/L 100100 100 64-135
2-Chlorotoluene ug/L 49.650 99 70-130
2-Hexanone ug/L 101100 101 66-135
4-Chlorotoluene ug/L 49.750 99 70-130
4-Methyl-2-pentanone (MIBK)ug/L 103100 103 70-130
Acetone ug/L 101100 101 61-157
Benzene ug/L 50.950 102 70-130
Bromobenzene ug/L 50.250 100 70-130
Bromochloromethane ug/L 49.350 99 70-130
Bromodichloromethane ug/L 52.450 105 70-130
Bromoform ug/L 51.850 104 70-130
Bromomethane ug/L 62.4 v15012538-130
Carbon tetrachloride ug/L 51.950 104 70-130
Chlorobenzene ug/L 48.850 98 70-130
Chloroethane ug/L 46.750 93 37-142
Chloroform ug/L 50.450 101 70-130
Chloromethane ug/L 47.950 96 48-130
cis-1,2-Dichloroethene ug/L 50.850 102 70-130
cis-1,3-Dichloropropene ug/L 54.150 108 70-130
Dibromochloromethane ug/L 51.450 103 70-130
Dibromomethane ug/L 49.750 99 70-130
Dichlorodifluoromethane ug/L 57.450 115 53-134
Diisopropyl ether ug/L 52.050 104 70-135
Ethylbenzene ug/L 49.150 98 70-130
Hexachloro-1,3-butadiene ug/L 50.750 101 68-132
m&p-Xylene ug/L 97.9100 98 70-130
Methyl-tert-butyl ether ug/L 52.350 105 70-130
Methylene Chloride ug/L 50.450 101 67-132
Naphthalene ug/L 50.450 101 70-130
o-Xylene ug/L 49.150 98 70-131
p-Isopropyltoluene ug/L 51.750 103 70-130
Styrene ug/L 49.250 98 70-130
Tetrachloroethene ug/L 49.950 100 69-130
Toluene ug/L 48.450 97 70-130
trans-1,2-Dichloroethene ug/L 53.250 106 70-130
trans-1,3-Dichloropropene ug/L 52.850 106 70-130
Trichloroethene ug/L 49.950 100 70-130
Trichlorofluoromethane ug/L 54.250 108 63-130
Vinyl acetate ug/L 114100 114 55-143
Vinyl chloride ug/L 52.550 105 70-131
Xylene (Total)ug/L 147150 98 70-130
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2627974MATRIX SPIKE SAMPLE:
MSSpike
Result
92436785013
1,1,1,2-Tetrachloroethane ug/L 19.620 98 73-134<1.0
1,1,1-Trichloroethane ug/L 19.520 97 82-143<1.0
1,1,2,2-Tetrachloroethane ug/L 19.020 95 70-136<1.0
1,1,2-Trichloroethane ug/L 19.720 98 70-135<1.0
1,1-Dichloroethane ug/L 19.920 99 70-139<1.0
1,1-Dichloroethene ug/L 20.720 103 70-154<1.0
1,1-Dichloropropene ug/L 19.320 97 70-149<1.0
1,2,3-Trichlorobenzene ug/L 20.120 100 70-135<1.0
1,2,3-Trichloropropane ug/L 19.420 97 71-137<1.0
1,2,4-Trichlorobenzene ug/L 19.220 96 73-140<1.0
1,2-Dibromo-3-chloropropane ug/L 18.820 94 65-134<5.0
1,2-Dibromoethane (EDB)ug/L 19.920 100 70-137<1.0
1,2-Dichlorobenzene ug/L 19.620 98 70-133<1.0
1,2-Dichloroethane ug/L 18.220 91 70-137<1.0
1,2-Dichloropropane ug/L 20.520 103 70-140<1.0
1,3-Dichlorobenzene ug/L 19.520 97 70-135<1.0
1,3-Dichloropropane ug/L 21.020 105 70-143<1.0
1,4-Dichlorobenzene ug/L 19.520 98 70-133<1.0
2,2-Dichloropropane ug/L 19.320 97 61-148<1.0
2-Butanone (MEK)ug/L 37.040 87 60-139<5.0
2-Chlorotoluene ug/L 19.420 97 70-144<1.0
2-Hexanone ug/L 38.040 95 65-138<5.0
4-Chlorotoluene ug/L 19.820 99 70-137<1.0
4-Methyl-2-pentanone (MIBK)ug/L 38.040 95 65-135<5.0
Acetone ug/L 53.740 61 60-14829.2
Benzene ug/L 20.920 104 70-151<1.0
Bromobenzene ug/L 20.020 100 70-136<1.0
Bromochloromethane ug/L 19.320 96 70-141<1.0
Bromodichloromethane ug/L 20.420 102 70-138<1.0
Bromoform ug/L 19.420 97 63-130<1.0
Bromomethane ug/L 14.820 74 15-152<2.0
Carbon tetrachloride ug/L 21.220 106 70-143<1.0
Chlorobenzene ug/L 20.020 100 70-138<1.0
Chloroethane ug/L 21.520 107 52-163<1.0
Chloroform ug/L 20.120 97 70-139<5.0
Chloromethane ug/L 21.120 105 41-139<1.0
cis-1,2-Dichloroethene ug/L 19.620 98 70-141<1.0
cis-1,3-Dichloropropene ug/L 20.820 104 70-137<1.0
Dibromochloromethane ug/L 19.620 98 70-134<1.0
Dibromomethane ug/L 19.620 98 70-138<1.0
Dichlorodifluoromethane ug/L 21.020 105 47-155<1.0
Diisopropyl ether ug/L 19.220 96 63-144<1.0
Ethylbenzene ug/L 20.120 101 66-153<1.0
Hexachloro-1,3-butadiene ug/L 20.120 100 65-149<1.0
m&p-Xylene ug/L 41.140 103 69-152<2.0
Methyl-tert-butyl ether ug/L 19.020 95 54-156<1.0
Methylene Chloride ug/L 19.820 99 42-159<5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 58 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2627974MATRIX SPIKE SAMPLE:
MSSpike
Result
92436785013
Naphthalene ug/L 19.420 97 61-148<1.0
o-Xylene ug/L 20.420 102 70-148<1.0
p-Isopropyltoluene ug/L 20.120 101 70-146<1.0
Styrene ug/L 20.320 102 70-135<1.0
Tetrachloroethene ug/L 20.620 103 59-143<1.0
Toluene ug/L 19.720 99 59-148<1.0
trans-1,2-Dichloroethene ug/L 20.120 101 70-146<1.0
trans-1,3-Dichloropropene ug/L 20.220 101 70-135<1.0
Trichloroethene ug/L 24.220 106 70-1473.1
Trichlorofluoromethane ug/L 19.620 98 70-148<1.0
Vinyl acetate ug/L 35.940 90 49-151<2.0
Vinyl chloride ug/L 21.220 106 70-156<1.0
Xylene (Total)ug/L 61.460 102 63-158<1.0
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92436785012
2627973SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND<1.0
1,1,1-Trichloroethane ug/L ND<1.0
1,1,2,2-Tetrachloroethane ug/L ND<1.0
1,1,2-Trichloroethane ug/L ND<1.0
1,1-Dichloroethane ug/L ND<1.0
1,1-Dichloroethene ug/L ND<1.0
1,1-Dichloropropene ug/L ND<1.0
1,2,3-Trichlorobenzene ug/L ND<1.0
1,2,3-Trichloropropane ug/L ND<1.0
1,2,4-Trichlorobenzene ug/L ND<1.0
1,2-Dibromo-3-chloropropane ug/L ND<5.0
1,2-Dibromoethane (EDB)ug/L ND<1.0
1,2-Dichlorobenzene ug/L ND<1.0
1,2-Dichloroethane ug/L ND<1.0
1,2-Dichloropropane ug/L ND<1.0
1,3-Dichlorobenzene ug/L ND<1.0
1,3-Dichloropropane ug/L ND<1.0
1,4-Dichlorobenzene ug/L ND<1.0
2,2-Dichloropropane ug/L ND<1.0
2-Butanone (MEK)ug/L ND<5.0
2-Chlorotoluene ug/L ND<1.0
2-Hexanone ug/L ND<5.0
4-Chlorotoluene ug/L ND<1.0
4-Methyl-2-pentanone (MIBK)ug/L ND<5.0
Acetone ug/L 18J36.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92436785012
2627973SAMPLE DUPLICATE:
Benzene ug/L ND<1.0
Bromobenzene ug/L ND<1.0
Bromochloromethane ug/L ND<1.0
Bromodichloromethane ug/L ND<1.0
Bromoform ug/L ND<1.0
Bromomethane ug/L ND<2.0
Carbon tetrachloride ug/L ND<1.0
Chlorobenzene ug/L ND<1.0
Chloroethane ug/L ND<1.0
Chloroform ug/L ND<5.0
Chloromethane ug/L ND<1.0
cis-1,2-Dichloroethene ug/L ND<1.0
cis-1,3-Dichloropropene ug/L ND<1.0
Dibromochloromethane ug/L ND<1.0
Dibromomethane ug/L ND<1.0
Dichlorodifluoromethane ug/L ND<1.0
Diisopropyl ether ug/L ND<1.0
Ethylbenzene ug/L ND<1.0
Hexachloro-1,3-butadiene ug/L ND<1.0
m&p-Xylene ug/L ND<2.0
Methyl-tert-butyl ether ug/L ND<1.0
Methylene Chloride ug/L ND<5.0
Naphthalene ug/L ND<1.0
o-Xylene ug/L ND<1.0
p-Isopropyltoluene ug/L ND<1.0
Styrene ug/L ND<1.0
Tetrachloroethene ug/L ND<1.0
Toluene ug/L ND<1.0
trans-1,2-Dichloroethene ug/L ND<1.0
trans-1,3-Dichloropropene ug/L ND<1.0
Trichloroethene ug/L 5.3 166.3
Trichlorofluoromethane ug/L ND<1.0
Vinyl acetate ug/L ND<2.0
Vinyl chloride ug/L ND<1.0
Xylene (Total)ug/L ND<1.0
1,2-Dichloroethane-d4 (S)%95108
4-Bromofluorobenzene (S)%100106
Toluene-d8 (S)%103104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
486914
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2628908
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Matrix:Solid
Analyzed
1,2,4,5-Tetrachlorobenzene ug/kg ND 334 07/19/19 10:53
1,2,4-Trichlorobenzene ug/kg ND 334 07/19/19 10:53
1,2-Dichlorobenzene ug/kg ND 334 07/19/19 10:53
1,2-Diphenylhydrazine ug/kg ND 334 07/19/19 10:53
1,3,5-Trinitrobenzene ug/kg ND 334 07/19/19 10:53
1,3-Dichlorobenzene ug/kg ND 334 07/19/19 10:53
1,3-Dinitrobenzene ug/kg ND 669 07/19/19 10:53
1,4-Dichlorobenzene ug/kg ND 334 07/19/19 10:53
1,4-Dinitrobenzene ug/kg ND 334 07/19/19 10:53
1,4-Naphthoquinone ug/kg ND 3340 IC07/19/19 10:53
1-Methylnaphthalene ug/kg ND 334 07/19/19 10:53
1-Naphthalenamine ug/kg ND 669 07/19/19 10:53
2,2'-Oxybis(1-chloropropane)ug/kg ND 334 07/19/19 10:53
2,3,4,6-Tetrachlorophenol ug/kg ND 334 07/19/19 10:53
2,3-Dibromo-1-propanol phosph ug/kg ND 2530 IC07/19/19 10:53
2,3-Dichloroaniline ug/kg ND 334 07/19/19 10:53
2,4,5-Trichlorophenol ug/kg ND 334 07/19/19 10:53
2,4,6-Trichlorophenol ug/kg ND 334 07/19/19 10:53
2,4-Dichlorophenol ug/kg ND 334 07/19/19 10:53
2,4-Dimethylphenol ug/kg ND 334 07/19/19 10:53
2,4-Dinitrophenol ug/kg ND 1670 07/19/19 10:53
2,4-Dinitrotoluene ug/kg ND 334 07/19/19 10:53
2,6-Dichlorophenol ug/kg ND 334 07/19/19 10:53
2,6-Dinitrotoluene ug/kg ND 334 07/19/19 10:53
2-Acetylaminofluorene ug/kg ND 669 07/19/19 10:53
2-Chloronaphthalene ug/kg ND 334 07/19/19 10:53
2-Chlorophenol ug/kg ND 334 07/19/19 10:53
2-Methyl-5-nitroaniline ug/kg ND 334 07/19/19 10:53
2-Methylnaphthalene ug/kg ND 334 07/19/19 10:53
2-Methylphenol(o-Cresol)ug/kg ND 334 07/19/19 10:53
2-Naphthalenamine ug/kg ND 669 07/19/19 10:53
2-Nitroaniline ug/kg ND 1670 07/19/19 10:53
2-Nitrophenol ug/kg ND 334 07/19/19 10:53
2-Picoline ug/kg ND 334 07/19/19 10:53
3&4-Methylphenol(m&p Cresol)ug/kg ND 334 07/19/19 10:53
3,3'-Dichlorobenzidine ug/kg ND 1670 07/19/19 10:53
3,3'-Dimethylbenzidine ug/kg ND 3340 07/19/19 10:53
3-Methylcholanthrene ug/kg ND 334 07/19/19 10:53
3-Nitroaniline ug/kg ND 1670 07/19/19 10:53
4,4'-Methylene-bis(2-chloroani ug/kg ND 1010 07/19/19 10:53
4,6-Dinitro-2-methylphenol ug/kg ND 669 v107/19/19 10:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2628908
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Matrix:Solid
Analyzed
4-Aminobiphenyl ug/kg ND 3340 v207/19/19 10:53
4-Bromophenylphenyl ether ug/kg ND 334 07/19/19 10:53
4-Chloro-3-methylphenol ug/kg ND 669 07/19/19 10:53
4-Chloroaniline ug/kg ND 1670 07/19/19 10:53
4-Chlorophenylphenyl ether ug/kg ND 334 07/19/19 10:53
4-Nitroaniline ug/kg ND 669 07/19/19 10:53
4-Nitrophenol ug/kg ND 1670 07/19/19 10:53
4-Nitroquinoline-n-oxide ug/kg ND 1670 07/19/19 10:53
5-Nitro-o-toluidine ug/kg ND 334 07/19/19 10:53
7,12-Dimethylbenz(a)anthracene ug/kg ND 334 07/19/19 10:53
a,a-Dimethylphenylethylamine ug/kg ND 1670 07/19/19 10:53
Acenaphthene ug/kg ND 334 07/19/19 10:53
Acenaphthylene ug/kg ND 334 07/19/19 10:53
Acetophenone ug/kg ND 334 07/19/19 10:53
Aniline ug/kg ND 334 07/19/19 10:53
Anthracene ug/kg ND 334 07/19/19 10:53
Aramite ug/kg ND 3340 07/19/19 10:53
Atrazine ug/kg ND 669 07/19/19 10:53
Benzal chloride ug/kg ND 1010 07/19/19 10:53
Benzaldehyde ug/kg ND 669 07/19/19 10:53
Benzidine ug/kg ND 1670 07/19/19 10:53
Benzo(a)anthracene ug/kg ND 334 07/19/19 10:53
Benzo(a)pyrene ug/kg ND 334 07/19/19 10:53
Benzo(b)fluoranthene ug/kg ND 334 07/19/19 10:53
Benzo(g,h,i)perylene ug/kg ND 334 07/19/19 10:53
Benzo(k)fluoranthene ug/kg ND 334 07/19/19 10:53
Benzoic Acid ug/kg ND 1670 07/19/19 10:53
Benzophenone ug/kg ND 334 07/19/19 10:53
Benzyl alcohol ug/kg ND 669 07/19/19 10:53
Biphenyl (Diphenyl)ug/kg ND 334 07/19/19 10:53
bis(2-Chloroethoxy)methane ug/kg ND 334 07/19/19 10:53
bis(2-Chloroethyl) ether ug/kg ND 334 07/19/19 10:53
bis(2-Ethylhexyl)phthalate ug/kg ND 334 07/19/19 10:53
Butylbenzylphthalate ug/kg ND 334 07/19/19 10:53
Caprolactam ug/kg ND 334 07/19/19 10:53
Carbazole ug/kg ND 334 07/19/19 10:53
Chlorobenzilate ug/kg ND 334 07/19/19 10:53
Chrysene ug/kg ND 334 07/19/19 10:53
Di-n-butylphthalate ug/kg ND 334 07/19/19 10:53
Di-n-octylphthalate ug/kg ND 334 07/19/19 10:53
Diallate ug/kg ND 334 07/19/19 10:53
Dibenz(a,h)anthracene ug/kg ND 334 07/19/19 10:53
Dibenzo(a,e)pyrene ug/kg ND 1010 07/19/19 10:53
Dibenzofuran ug/kg ND 334 07/19/19 10:53
Diethylphthalate ug/kg ND 334 07/19/19 10:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2628908
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Matrix:Solid
Analyzed
Dimethoate ug/kg ND 669 IC07/19/19 10:53
Dimethylphthalate ug/kg ND 334 07/19/19 10:53
Dinoseb ug/kg ND 669 07/19/19 10:53
Diphenyl ether (Phenyl ether)ug/kg ND 507 07/19/19 10:53
Diphenylamine ug/kg ND 334 07/19/19 10:53
Disulfoton ug/kg ND 669 07/19/19 10:53
Ethyl methanesulfonate ug/kg ND 669 07/19/19 10:53
Famphur ug/kg ND 1670 07/19/19 10:53
Fluoranthene ug/kg ND 334 07/19/19 10:53
Fluorene ug/kg ND 334 07/19/19 10:53
Hexachloro-1,3-butadiene ug/kg ND 334 07/19/19 10:53
Hexachlorobenzene ug/kg ND 334 07/19/19 10:53
Hexachlorocyclopentadiene ug/kg ND 334 07/19/19 10:53
Hexachloroethane ug/kg ND 334 07/19/19 10:53
Hexachlorophene ug/kg ND 3340 07/19/19 10:53
Hexachloropropene ug/kg ND 334 07/19/19 10:53
Indeno(1,2,3-cd)pyrene ug/kg ND 334 07/19/19 10:53
Isodrin ug/kg ND 669 07/19/19 10:53
Isophorone ug/kg ND 334 07/19/19 10:53
Isosafrole ug/kg ND 334 07/19/19 10:53
Kepone ug/kg ND 1670 07/19/19 10:53
Methapyrilene ug/kg ND 1670 07/19/19 10:53
Methyl methanesulfonate ug/kg ND 669 07/19/19 10:53
Methyl parathion ug/kg ND 669 07/19/19 10:53
n-Decane ug/kg ND 334 07/19/19 10:53
N-Nitroso-di-n-butylamine ug/kg ND 334 07/19/19 10:53
N-Nitroso-di-n-propylamine ug/kg ND 334 07/19/19 10:53
N-Nitrosodiethylamine ug/kg ND 669 07/19/19 10:53
N-Nitrosodimethylamine ug/kg ND 334 07/19/19 10:53
N-Nitrosodiphenylamine ug/kg ND 334 07/19/19 10:53
N-Nitrosomethylethylamine ug/kg ND 334 07/19/19 10:53
N-Nitrosomorpholine ug/kg ND 334 07/19/19 10:53
N-Nitrosopiperidine ug/kg ND 669 07/19/19 10:53
N-Nitrosopyrrolidine ug/kg ND 669 07/19/19 10:53
n-Octadecane ug/kg ND 334 07/19/19 10:53
Naphthalene ug/kg ND 334 07/19/19 10:53
Nitrobenzene ug/kg ND 334 07/19/19 10:53
O,O,O-Triethylphosphorothioate ug/kg ND 1670 07/19/19 10:53
O-Toluidine ug/kg ND 334 07/19/19 10:53
P-Dimethylaminoazobenzene ug/kg ND 669 07/19/19 10:53
p-Phenylenediamine ug/kg ND 669 07/19/19 10:53
Parathion (Ethyl parathion)ug/kg ND 669 07/19/19 10:53
Pentachlorobenzene ug/kg ND 334 07/19/19 10:53
Pentachloroethane ug/kg ND 669 07/19/19 10:53
Pentachloronitrobenzene ug/kg ND 669 07/19/19 10:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2628908
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Matrix:Solid
Analyzed
Pentachlorophenol ug/kg ND 1670 07/19/19 10:53
Phenacetin ug/kg ND 669 07/19/19 10:53
Phenanthrene ug/kg ND 334 07/19/19 10:53
Phenol ug/kg ND 334 07/19/19 10:53
Phorate ug/kg ND 669 07/19/19 10:53
Phthalic anhydride ug/kg ND 2530 07/19/19 10:53
Pronamide ug/kg ND 669 07/19/19 10:53
Pyrene ug/kg ND 334 07/19/19 10:53
Pyridine ug/kg ND 334 07/19/19 10:53
Safrole ug/kg ND 669 07/19/19 10:53
Sulfotepp (Thiodiphosphoric Ac ug/kg ND 669 07/19/19 10:53
Terpineol ug/kg ND 334 07/19/19 10:53
Thionazin ug/kg ND 669 07/19/19 10:53
2,4,6-Tribromophenol (S)%71 27-110 07/19/19 10:53
2-Fluorobiphenyl (S)%68 30-110 07/19/19 10:53
2-Fluorophenol (S)%64 13-110 07/19/19 10:53
Nitrobenzene-d5 (S)%69 23-110 07/19/19 10:53
Phenol-d6 (S)%65 22-110 07/19/19 10:53
Terphenyl-d14 (S)%68 28-110 07/19/19 10:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2628909LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4,5-Tetrachlorobenzene ug/kg 14901680 88 24-130
1,2,4-Trichlorobenzene ug/kg 13401680 80 52-130
1,2-Dichlorobenzene ug/kg 13401680 80 51-130
1,2-Diphenylhydrazine ug/kg 15501680 92 24-159
1,3,5-Trinitrobenzene ug/kg 21401680 127 61-130
1,3-Dichlorobenzene ug/kg 13501680 80 50-130
1,3-Dinitrobenzene ug/kg 15801680 94 66-130
1,4-Dichlorobenzene ug/kg 13801680 82 49-130
1,4-Dinitrobenzene ug/kg 17201680 102 47-130
1,4-Naphthoquinone ug/kg 2490J IC,L1168014810-137
1-Methylnaphthalene ug/kg 14001680 83 55-130
1-Naphthalenamine ug/kg 11501680 68 45-130
2,2'-Oxybis(1-chloropropane)ug/kg 15501680 92 30-130
2,3,4,6-Tetrachlorophenol ug/kg 17301680 103 24-200
2,3-Dibromo-1-propanol phosph ug/kg 17900 IC,L1673026510-160
2,3-Dichloroaniline ug/kg 13601680 81 46-145
2,4,5-Trichlorophenol ug/kg 13901680 83 55-130
2,4,6-Trichlorophenol ug/kg 15501680 92 57-130
2,4-Dichlorophenol ug/kg 14601680 87 56-130
2,4-Dimethylphenol ug/kg 14901680 89 51-130
2,4-Dinitrophenol ug/kg 85608420 102 27-133
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2628909LABORATORY CONTROL SAMPLE:
LCSSpike
2,4-Dinitrotoluene ug/kg 13901680 83 61-130
2,6-Dichlorophenol ug/kg 15701680 93 55-130
2,6-Dinitrotoluene ug/kg 15201680 90 60-130
2-Acetylaminofluorene ug/kg 11501680 68 47-130
2-Chloronaphthalene ug/kg 15601680 93 52-130
2-Chlorophenol ug/kg 15701680 93 54-130
2-Methyl-5-nitroaniline ug/kg 11801680 70 70-141
2-Methylnaphthalene ug/kg 14501680 86 54-130
2-Methylphenol(o-Cresol)ug/kg 15201680 90 51-130
2-Naphthalenamine ug/kg 9491680 56 37-130
2-Nitroaniline ug/kg 28603370 85 51-130
2-Nitrophenol ug/kg 15601680 93 49-130
2-Picoline ug/kg 13201680 79 10-130
3&4-Methylphenol(m&p Cresol)ug/kg 16601680 98 11-163
3,3'-Dichlorobenzidine ug/kg 26203370 78 10-132
3,3'-Dimethylbenzidine ug/kg 1720J3370 51 10-130
3-Methylcholanthrene ug/kg 21701680 129 48-130
3-Nitroaniline ug/kg 28203370 84 55-130
4,4'-Methylene-bis(2-chloroani ug/kg 20503370 61 58-130
4,6-Dinitro-2-methylphenol ug/kg 4020 v1337011947-142
4-Aminobiphenyl ug/kg 1030J v216806110-130
4-Bromophenylphenyl ether ug/kg 15201680 91 59-130
4-Chloro-3-methylphenol ug/kg 29703370 88 55-130
4-Chloroaniline ug/kg 26703370 79 54-130
4-Chlorophenylphenyl ether ug/kg 14701680 87 58-130
4-Nitroaniline ug/kg 26603370 79 54-130
4-Nitrophenol ug/kg 73808420 88 48-130
4-Nitroquinoline-n-oxide ug/kg 25803370 77 30-130
5-Nitro-o-toluidine ug/kg 11801680 70 46-130
7,12-Dimethylbenz(a)anthracene ug/kg 16401680 97 62-130
a,a-Dimethylphenylethylamine ug/kg 762J1680 45 10-160
Acenaphthene ug/kg 14101680 84 60-130
Acenaphthylene ug/kg 14301680 85 60-130
Acetophenone ug/kg 15401680 92 50-130
Aniline ug/kg 12901680 76 43-130
Anthracene ug/kg 14901680 88 63-130
Aramite ug/kg ND3370 45 34-130
Atrazine ug/kg 400J L216802466-130
Benzal chloride ug/kg 13601680 81 43-130
Benzaldehyde ug/kg 11201680 67 10-130
Benzidine ug/kg 1520J3370 45 10-130
Benzo(a)anthracene ug/kg 14901680 88 59-130
Benzo(a)pyrene ug/kg 15101680 90 57-130
Benzo(b)fluoranthene ug/kg 16401680 97 54-130
Benzo(g,h,i)perylene ug/kg 15701680 93 59-130
Benzo(k)fluoranthene ug/kg 14901680 89 54-130
Benzoic Acid ug/kg 53408420 63 19-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2628909LABORATORY CONTROL SAMPLE:
LCSSpike
Benzophenone ug/kg 16201680 96 56-130
Benzyl alcohol ug/kg 29903370 89 50-130
Biphenyl (Diphenyl)ug/kg 14301680 85 53-130
bis(2-Chloroethoxy)methane ug/kg 15101680 90 54-130
bis(2-Chloroethyl) ether ug/kg 15301680 91 48-130
bis(2-Ethylhexyl)phthalate ug/kg 15801680 94 45-134
Butylbenzylphthalate ug/kg 15001680 89 46-138
Caprolactam ug/kg 576 L216803443-130
Carbazole ug/kg 13601680 81 60-130
Chlorobenzilate ug/kg 19001680 113 66-130
Chrysene ug/kg 13501680 80 58-130
Di-n-butylphthalate ug/kg 14501680 86 60-130
Di-n-octylphthalate ug/kg 14401680 85 53-130
Diallate ug/kg 15401680 92 69-130
Dibenz(a,h)anthracene ug/kg 15401680 91 59-130
Dibenzo(a,e)pyrene ug/kg ND1680 58 49-130
Dibenzofuran ug/kg 13901680 83 60-130
Diethylphthalate ug/kg 14001680 83 60-130
Dimethoate ug/kg 2430 IC,L1168014467-133
Dimethylphthalate ug/kg 14301680 85 60-130
Dinoseb ug/kg 18101680 107 30-139
Diphenyl ether (Phenyl ether)ug/kg 13101680 78 10-159
Diphenylamine ug/kg 15101680 90 59-130
Disulfoton ug/kg 15001680 89 55-139
Ethyl methanesulfonate ug/kg 16201680 96 39-144
Famphur ug/kg ND L23370710-200
Fluoranthene ug/kg 14501680 86 65-130
Fluorene ug/kg 14001680 83 63-130
Hexachloro-1,3-butadiene ug/kg 13301680 79 46-130
Hexachlorobenzene ug/kg 14501680 86 58-130
Hexachlorocyclopentadiene ug/kg 9581680 57 23-130
Hexachloroethane ug/kg 13701680 81 47-130
Hexachlorophene ug/kg 1090016800 65 10-131
Hexachloropropene ug/kg 14801680 88 35-149
Indeno(1,2,3-cd)pyrene ug/kg 15401680 92 60-130
Isodrin ug/kg 14501680 86 70-130
Isophorone ug/kg 13901680 82 49-130
Isosafrole ug/kg 11701680 69 57-130
Kepone ug/kg ND3370 10 10-147
Methapyrilene ug/kg ND1680 32 10-166
Methyl methanesulfonate ug/kg 19401680 115 23-138
Methyl parathion ug/kg 2280 L1168013557-130
n-Decane ug/kg 14001680 83 21-130
N-Nitroso-di-n-butylamine ug/kg 10301680 61 36-130
N-Nitroso-di-n-propylamine ug/kg 15201680 90 47-130
N-Nitrosodiethylamine ug/kg 11901680 71 47-130
N-Nitrosodimethylamine ug/kg 14601680 87 45-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2628909LABORATORY CONTROL SAMPLE:
LCSSpike
N-Nitrosodiphenylamine ug/kg 15101680 90 59-130
N-Nitrosomethylethylamine ug/kg 11701680 70 48-130
N-Nitrosomorpholine ug/kg 12201680 72 37-150
N-Nitrosopiperidine ug/kg 11801680 70 61-130
N-Nitrosopyrrolidine ug/kg 11401680 68 51-130
n-Octadecane ug/kg 13601680 81 47-130
Naphthalene ug/kg 14601680 87 55-130
Nitrobenzene ug/kg 14001680 83 49-130
O,O,O-Triethylphosphorothioate ug/kg ND1680 85 29-175
O-Toluidine ug/kg 11701680 69 10-151
P-Dimethylaminoazobenzene ug/kg 7101680 42 14-130
p-Phenylenediamine ug/kg 14601680 86 60-160
Parathion (Ethyl parathion)ug/kg 16301680 97 61-130
Pentachlorobenzene ug/kg 15101680 90 48-130
Pentachloroethane ug/kg 14401680 85 35-141
Pentachloronitrobenzene ug/kg 17101680 102 68-131
Pentachlorophenol ug/kg 32803370 98 10-132
Phenacetin ug/kg 14601680 86 62-130
Phenanthrene ug/kg 14801680 88 62-130
Phenol ug/kg 15301680 91 46-130
Phorate ug/kg 21701680 129 59-130
Phthalic anhydride ug/kg ND
Pronamide ug/kg 14701680 88 66-130
Pyrene ug/kg 16001680 95 53-130
Pyridine ug/kg 12601680 75 37-130
Safrole ug/kg 14501680 86 51-130
Sulfotepp (Thiodiphosphoric Ac ug/kg 15501680 92 10-160
Terpineol ug/kg 13701680 82 39-130
Thionazin ug/kg 15501680 92 43-146
2,4,6-Tribromophenol (S)%95 27-110
2-Fluorobiphenyl (S)%82 30-110
2-Fluorophenol (S)%82 13-110
Nitrobenzene-d5 (S)%85 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%85 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2628910MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92436815011
2628911
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4,5-Tetrachlorobenzene ug/kg 2010 84 16-13067 241990ND16901330
1,2,4-Trichlorobenzene ug/kg 2010 72 18-13054 291990ND14401080
1,2-Dichlorobenzene ug/kg 2010 68 14-13054 261990ND13801070
1,2-Diphenylhydrazine ug/kg 2010 83 23-13078 91990ND16801540
1,3,5-Trinitrobenzene ug/kg 2010 111 70-130105 71990ND22402090
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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Huntersville, NC 28078
[phone]
Page 67 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2628910MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92436815011
2628911
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,3-Dichlorobenzene ug/kg 2010 69 12-13052 301990ND13901030
1,3-Dinitrobenzene ug/kg 2010 84 70-13076 121990ND16901500
1,4-Dichlorobenzene ug/kg 2010 71 10-13054 291990ND14301070
1,4-Dinitrobenzene ug/kg 2010 92 17-13084 101990ND18501660
1,4-Naphthoquinone ug/kg IC,M0201014270-1301291990ND2870J2550J
1-Methylnaphthalene ug/kg 2010 73 12-13058 241990ND14701160
1-Naphthalenamine ug/kg M120104770-13042 121990ND945835
2,2'-Oxybis(1-chloropropane)ug/kg 2010 78 10-13060 271990ND15701200
2,3,4,6-Tetrachlorophenol ug/kg 2010 94 10-20082 151990ND19001630
2,3-Dibromo-1-propanol
phosph
ug/kg IC,M0806035310-194323 107930ND2840025600
2,3-Dichloroaniline ug/kg M120107570-13063 191990ND15001250
2,4,5-Trichlorophenol ug/kg 2010 76 13-13065 171990ND15301290
2,4,6-Trichlorophenol ug/kg 2010 85 17-13072 171990ND17001430
2,4-Dichlorophenol ug/kg 2010 78 10-13061 251990ND15701220
2,4-Dimethylphenol ug/kg 2010 78 10-13062 241990ND15801230
2,4-Dinitrophenol ug/kg 10100 96 10-13086 139910ND97008520
2,4-Dinitrotoluene ug/kg 2010 73 24-13067 111990ND14801330
2,6-Dichlorophenol ug/kg M120108370-13069 211990ND16801360
2,6-Dinitrotoluene ug/kg 2010 80 23-13071 141990ND16201410
2-Acetylaminofluorene ug/kg 2010 65 10-13059 111990ND13101170
2-Chloronaphthalene ug/kg 2010 87 19-13069 241990ND17501380
2-Chlorophenol ug/kg 2010 79 10-13060 291990ND16001190
2-Methyl-5-nitroaniline ug/kg M120106170-13057 81990ND12201130
2-Methylnaphthalene ug/kg 2010 76 18-13061 241990ND15301210
2-Methylphenol(o-Cresol)ug/kg 2010 76 10-13058 281990ND15301150
2-Naphthalenamine ug/kg M120101770-13051990ND333JND
2-Nitroaniline ug/kg 4040 77 17-13069 123960ND30902750
2-Nitrophenol ug/kg 2010 84 10-13063 301990ND17001250
2-Picoline ug/kg M12010770-13021990NDNDND
3&4-Methylphenol(m&p
Cresol)ug/kg 2010 79 10-13064 241990ND16001260
3,3'-Dichlorobenzidine ug/kg 4040 66 10-13056 183960ND26502220
3,3'-Dimethylbenzidine ug/kg M14040570-13013960ND202JND
3-Methylcholanthrene ug/kg 2010 117 10-130107 111990ND23702120
3-Nitroaniline ug/kg 4040 73 24-13065 143960ND29502570
4,4'-Methylene-bis(2-chloroani ug/kg 4040 53 10-13149 113960ND21501930
4,6-Dinitro-2-methylphenol ug/kg v1404011010-15299 123960ND44503940
4-Aminobiphenyl ug/kg M1,v220103170-130311990ND627J615J
4-Bromophenylphenyl ether ug/kg 2010 83 29-13072 161990ND16701420
4-Chloro-3-methylphenol ug/kg 4040 77 17-13068 153960ND31202680
4-Chloroaniline ug/kg 4040 67 14-13056 193960ND27002230
4-Chlorophenylphenyl ether ug/kg 2010 77 25-13068 151990ND15601340
4-Nitroaniline ug/kg 4040 67 22-13062 83960ND26802470
4-Nitrophenol ug/kg 10100 74 10-13067 129910ND74906660
4-Nitroquinoline-n-oxide ug/kg M140407570-13068 113960ND30202710
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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Huntersville, NC 28078
[phone]
Page 68 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2628910MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92436815011
2628911
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
5-Nitro-o-toluidine ug/kg 2010 61 10-13057 81990ND12201130
7,12-
Dimethylbenz(a)anthracene ug/kg M120108070-13068 171990ND16001360
a,a-Dimethylphenylethylamine ug/kg M12010270-13011990NDNDND
Acenaphthene ug/kg 2010 76 20-13066 161990ND15401300
Acenaphthylene ug/kg 2010 78 25-13067 171990ND15701320
Acetophenone ug/kg 2010 78 15-13061 251990ND15701220
Aniline ug/kg R120105210-13034 431990ND1050677
Anthracene ug/kg 2010 79 29-13072 121990ND16001420
Aramite ug/kg M140403970-130363960NDNDND
Atrazine ug/kg 2010 38 10-156401990ND764J801
Benzal chloride ug/kg 2010 73 21-130571990ND1470ND
Benzaldehyde ug/kg 2010 72 10-13060 191990ND14401190
Benzidine ug/kg M14040370-13003960NDNDND
Benzo(a)anthracene ug/kg 2010 78 19-13070 121990ND15701390
Benzo(a)pyrene ug/kg 2010 79 12-13071 121990ND16001410
Benzo(b)fluoranthene ug/kg 2010 83 14-13074 131990ND16701470
Benzo(g,h,i)perylene ug/kg 2010 87 10-13074 171990ND17501470
Benzo(k)fluoranthene ug/kg 2010 77 14-13069 121990ND15501360
Benzoic Acid ug/kg 10100 75 10-13063 209910ND75606210
Benzophenone ug/kg 2010 86 70-13083 61990ND17401640
Benzyl alcohol ug/kg 4040 74 13-13058 253960ND29702320
Biphenyl (Diphenyl)ug/kg 2010 79 17-13065 211990ND15901280
bis(2-Chloroethoxy)methane ug/kg 2010 79 16-13061 261990ND15901220
bis(2-Chloroethyl) ether ug/kg 2010 78 11-13059 301990ND15801170
bis(2-Ethylhexyl)phthalate ug/kg 2010 80 21-13071 131990ND16101410
Butylbenzylphthalate ug/kg 2010 78 23-13070 131990ND15801380
Caprolactam ug/kg 2010 19 10-134181990ND390J363J
Carbazole ug/kg 2010 71 29-13064 111990ND14301280
Chlorobenzilate ug/kg 2010 98 70-13087 141990ND19801720
Chrysene ug/kg 2010 71 22-13064 121990ND14401280
Di-n-butylphthalate ug/kg 2010 74 30-13068 111990ND14901340
Di-n-octylphthalate ug/kg 2010 77 23-14268 141990ND15501350
Diallate ug/kg 2010 84 70-13077 101990ND16901530
Dibenz(a,h)anthracene ug/kg 2010 85 10-13071 201990ND17201410
Dibenzo(a,e)pyrene ug/kg M120105270-130471990NDNDND
Dibenzofuran ug/kg 2010 75 24-13067 131990ND15201340
Diethylphthalate ug/kg 2010 72 26-13065 121990ND14501280
Dimethoate ug/kg IC,M0201014070-130133 71990ND28202630
Dimethylphthalate ug/kg 2010 75 22-13067 131990ND15201330
Dinoseb ug/kg 2010 98 10-14688 121990ND19701740
Diphenyl ether (Phenyl ether)ug/kg M120107270-13059 211990ND14401160
Diphenylamine ug/kg 2010 82 42-13073 131990ND16501450
Disulfoton ug/kg 2010 80 70-13076 61990ND16101510
Ethyl methanesulfonate ug/kg M120108270-13064 261990ND16501270
Famphur ug/kg 4040 42 10-199473960ND1680J1850J
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2628910MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92436815011
2628911
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Fluoranthene ug/kg 2010 75 33-13068 111990ND15101340
Fluorene ug/kg 2010 74 22-13067 131990ND15001320
Hexachloro-1,3-butadiene ug/kg R120107113-13053 311990ND14201050
Hexachlorobenzene ug/kg 2010 78 29-13067 171990ND15701330
Hexachlorocyclopentadiene ug/kg R120108010-13059 331990ND16101160
Hexachloroethane ug/kg R120107010-13052 311990ND14201030
Hexachlorophene ug/kg M1201007270-13064 1119900ND1620014400
Hexachloropropene ug/kg 2010 85 10-13965 281990ND17101290
Indeno(1,2,3-cd)pyrene ug/kg 2010 85 10-13073 171990ND17201450
Isodrin ug/kg M120107670-13069 121990ND15301360
Isophorone ug/kg 2010 72 13-13058 231990ND14601150
Isosafrole ug/kg 2010 65 24-13056 171990ND13001100
Kepone ug/kg M140402370-130293960NDNDND
Methapyrilene ug/kg M12010010-13001990NDNDND
Methyl methanesulfonate ug/kg 2010 97 70-13075 281990ND19601480
Methyl parathion ug/kg 2010 126 70-130117 81990ND25302330
n-Decane ug/kg M120107070-13054 271990ND14101070
N-Nitroso-di-n-butylamine ug/kg 2010 53 21-13046 161990ND1080917
N-Nitroso-di-n-propylamine ug/kg 2010 76 12-13061 231990ND15401210
N-Nitrosodiethylamine ug/kg 2010 60 18-13047 251990ND1210941
N-Nitrosodimethylamine ug/kg R120107511-13052 381990ND15101030
N-Nitrosodiphenylamine ug/kg 2010 82 15-13073 131990ND16501450
N-Nitrosomethylethylamine ug/kg 2010 60 10-13046 271990ND1200917
N-Nitrosomorpholine ug/kg 2010 66 10-13750 281990ND1320995
N-Nitrosopiperidine ug/kg 2010 61 28-13050 211990ND1240999
N-Nitrosopyrrolidine ug/kg 2010 56 25-13048 171990ND1130956
n-Octadecane ug/kg 2010 75 70-13070 91990ND15201390
Naphthalene ug/kg 2010 77 15-13061 251990ND15501200
Nitrobenzene ug/kg 2010 75 12-13057 291990ND15001120
O,O,O-
Triethylphosphorothioate
ug/kg M120107570-130581990NDNDND
O-Toluidine ug/kg M120104970-13038 281990ND994750
P-Dimethylaminoazobenzene ug/kg M120103870-130331990NDNDND
p-Phenylenediamine ug/kg 2010 75 70-13070 81990ND15101390
Parathion (Ethyl parathion)ug/kg 2010 84 70-13077 101990ND16901520
Pentachlorobenzene ug/kg 2010 83 23-13072 151990ND16701440
Pentachloroethane ug/kg M120107570-13057 291990ND15001130
Pentachloronitrobenzene ug/kg 2010 92 19-13183 111990ND18401650
Pentachlorophenol ug/kg 4040 89 10-13077 173960ND36103030
Phenacetin ug/kg 2010 75 10-13070 81990ND15101390
Phenanthrene ug/kg 2010 78 27-13071 111990ND15701420
Phenol ug/kg 2010 76 10-13060 261990ND15301180
Phorate ug/kg 2010 115 70-130110 61990ND23302190
Phthalic anhydride ug/kg ND ND ND
Pronamide ug/kg 2010 78 10-16673 81990ND15701450
Pyrene ug/kg 2010 82 19-13074 121990ND16501460
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2628910MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92436815011
2628911
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Pyridine ug/kg M120101410-13051990ND280JND
Safrole ug/kg 2010 76 46-13062 231990ND15401230
Sulfotepp (Thiodiphosphoric
Ac ug/kg 2010 83 70-13073 141990ND16601440
Terpineol ug/kg M120107370-13059 231990ND14601170
Thionazin ug/kg 2010 80 70-13074 101990ND16201470
2,4,6-Tribromophenol (S)%85 27-11073
2-Fluorobiphenyl (S)%74 30-11062
2-Fluorophenol (S)%69 13-11054
Nitrobenzene-d5 (S)%76 23-11059
Phenol-d6 (S)%66 22-11053
Terphenyl-d14 (S)%71 28-11065
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
486455
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92436815001, 92436815002, 92436815003, 92436815004, 92436815005, 92436815006, 92436815007,
92436815008, 92436815009
Parameter Units
Dup
Result QualifiersRPDResult
92436740004
2627281SAMPLE DUPLICATE:
Percent Moisture %17.0 516.3
Parameter Units
Dup
Result QualifiersRPDResult
92436827005
2627282SAMPLE DUPLICATE:
Percent Moisture %18.2 617.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
486673
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92436815011, 92436815012, 92436815013, 92436815014, 92436815015
Parameter Units
Dup
Result QualifiersRPDResult
92436747041
2627991SAMPLE DUPLICATE:
Percent Moisture %35.5 738.0
Parameter Units
Dup
Result QualifiersRPDResult
92436833001
2627992SAMPLE DUPLICATE:
Percent Moisture %68.8 068.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 81
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
558234
EPA 3060
EPA 7199
7199 Hexavelent Chromium Soil
Associated Lab Samples:92436815013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3029480
Associated Lab Samples:92436815013
Matrix:Solid
Analyzed
Chromium, Hexavalent mg/kg ND 0.65 08/01/19 13:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3029481LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 40.740.3 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3029483MATRIX SPIKE SAMPLE:
MSSpike
Result
20113369001
Chromium, Hexavalent mg/kg 67.951.7 99 75-12513.1
Parameter Units
Dup
Result QualifiersRPDResult
20113369001
3029482SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 20.6 1913.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 81
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
The initial calibration for this compound was outside of method control limits. The result is estimated.IC
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 81
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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[phone]
Page 76 of 81
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92436815
MPP18020; Soil Gas Sampling
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92436815011 487340 487479BLDG-4 EPA 3050B EPA 6010D
92436815012 487340 487479BLDG-1 EPA 3050B EPA 6010D
92436815013 487340 487479BLDG-3 EPA 3050B EPA 6010D
92436815014 487340 487479BLDG-2 EPA 3050B EPA 6010D
92436815015 487340 487479BLDG-DUP-1 EPA 3050B EPA 6010D
92436815011 486565 486615BLDG-4 EPA 7471B EPA 7471B
92436815012 486565 486615BLDG-1 EPA 7471B EPA 7471B
92436815013 486565 486615BLDG-3 EPA 7471B EPA 7471B
92436815014 486565 486615BLDG-2 EPA 7471B EPA 7471B
92436815015 486565 486615BLDG-DUP-1 EPA 7471B EPA 7471B
92436815011 486914 487109BLDG-4 EPA 3546 EPA 8270E
92436815012 486914 487109BLDG-1 EPA 3546 EPA 8270E
92436815013 486914 487109BLDG-3 EPA 3546 EPA 8270E
92436815014 486914 487109BLDG-2 EPA 3546 EPA 8270E
92436815015 486914 487109BLDG-DUP-1 EPA 3546 EPA 8270E
92436815001 486612 486617SG-24 1'EPA 5035A EPA 8260D
92436815002 486612 486617SG-19 1'EPA 5035A EPA 8260D
92436815003 486612 486617SG-3 1'EPA 5035A EPA 8260D
92436815004 486612 486617SG-8 1'EPA 5035A EPA 8260D
92436815005 486612 486617SG-10 1'EPA 5035A EPA 8260D
92436815006 486855 486862SG-15 1'EPA 5035A EPA 8260D
92436815007 486855 486862SG-18 1'EPA 5035A EPA 8260D
92436815008 486855 486862SG-12 1'EPA 5035A EPA 8260D
92436815009 486855 486862SG-DUP-1 EPA 5035A EPA 8260D
92436815010 486667TRIP BLANK EPA 8260D
92436815001 486455SG-24 1'ASTM D2974-87
92436815002 486455SG-19 1'ASTM D2974-87
92436815003 486455SG-3 1'ASTM D2974-87
92436815004 486455SG-8 1'ASTM D2974-87
92436815005 486455SG-10 1'ASTM D2974-87
92436815006 486455SG-15 1'ASTM D2974-87
92436815007 486455SG-18 1'ASTM D2974-87
92436815008 486455SG-12 1'ASTM D2974-87
92436815009 486455SG-DUP-1 ASTM D2974-87
92436815011 486673BLDG-4 ASTM D2974-87
92436815012 486673BLDG-1 ASTM D2974-87
92436815013 486673BLDG-3 ASTM D2974-87
92436815014 486673BLDG-2 ASTM D2974-87
92436815015 486673BLDG-DUP-1 ASTM D2974-87
92436815013 558234 558966BLDG-3 EPA 3060 EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/02/2019 12:00 PM
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#=CL#
July 29, 2019
LIMS USE: FR - ERIC HOWARD
LIMS OBJECT ID: 92437876
92437876
Project:
Pace Project No.:
RE:
Eric Howard
McAdams Co
2905 Meridian Parkway
Durham, NC 27713
RTP Flex
Dear Eric Howard:
Enclosed are the analytical results for sample(s) received by the laboratory on July 20, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
cc:Vicky Garlington, McAdams Co
Accounts Payable, McAdams Co
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 158
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92437876
RTP Flex
Minnesota Certification IDs
1700 Elm Street SE, Minneapolis, MN 55414-2485
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
CNMI Saipan Certification #: MP0003
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605
Georgia Certification #: 959
Guam EPA Certification #: MN00064
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: 03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Massachusetts Certification #: M-MN064
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Certifcation #: via MN 027-053-137
Minnesota Petrofund Certification #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92437876
RTP Flex
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92437876001 SG-19 (2435)TO-15 58 PASI-MCH1
92437876002 SG-20 (2441)TO-15 58 PASI-MMG2
92437876003 SG-21 (1348)TO-15 58 PASI-MMG2
92437876004 SG-22 (2215)TO-15 58 PASI-MMG2
92437876005 SG-23 (3229)TO-15 58 PASI-MMG2
92437876006 SG-24 (2789)TO-15 58 PASI-MMG2
92437876007 SG-8 (3227)TO-15 58 PASI-MMG2
92437876008 SG-7 (2650)TO-15 58 PASI-MMG2
92437876009 SG-6 (3294)TO-15 58 PASI-MMG2
92437876010 SG-5 (2243)TO-15 58 PASI-MMG2
92437876011 SG-4 (2924)TO-15 58 PASI-MMG2
92437876012 SG-3 (1792)TO-15 58 PASI-MMG2
92437876013 SG-2 (2878)TO-15 58 PASI-MMG2
92437876014 SG-1 (2194)TO-15 58 PASI-MMG2
92437876015 SG-18 (2002)TO-15 58 PASI-MMG2
92437876016 SG-17 (2001)TO-15 58 PASI-MMLS
92437876017 SG-16 (2147)TO-15 58 PASI-MMLS
92437876018 SG-15 (3266)TO-15 58 PASI-MMLS
92437876019 SG-10 (2788)TO-15 58 PASI-MMLS
92437876020 SG-9 (2226)TO-15 58 PASI-MMLS
92437876021 SG-11 (3182)TO-15 58 PASI-MMLS
92437876022 SG-13 (3065)TO-15 58 PASI-MMLS
92437876023 SG-12 (2076)TO-15 58 PASI-MMLS
92437876025 DUP-1 (3175)TO-15 58 PASI-MMLS
92437876026 SG-14 (3527) re-test TO-15 58 PASI-MMLS
REPORT OF LABORATORY ANALYSIS
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Page 3 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-19 (2435)Lab ID:92437876001 Collected:07/11/19 12:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 150 ug/m3 07/24/19 11:28 67-64-110342.7
Benzene 29.2 ug/m3 07/24/19 11:28 71-43-213.9 42.7
Bromodichloromethane ND ug/m3 07/24/19 11:28 75-27-458.1 42.7
Bromoform ND ug/m3 07/24/19 11:28 75-25-222442.7
Bromomethane ND ug/m3 07/24/19 11:28 74-83-933.7 42.7
1,3-Butadiene ND ug/m3 07/24/19 11:28 106-99-019.2 42.7
2-Butanone (MEK)ND ug/m3 07/24/19 11:28 78-93-312842.7
Carbon disulfide 31.2 ug/m3 07/24/19 11:28 75-15-027.0 42.7
Carbon tetrachloride ND ug/m3 07/24/19 11:28 56-23-554.7 42.7
Chlorobenzene ND ug/m3 07/24/19 11:28 108-90-740.0 42.7
Chloroethane ND ug/m3 07/24/19 11:28 75-00-322.9 42.7
Chloroform ND ug/m3 07/24/19 11:28 67-66-321.2 42.7
Chloromethane ND ug/m3 07/24/19 11:28 74-87-317.9 42.7
Cyclohexane ND ug/m3 07/24/19 11:28 110-82-774.7 42.7
Dibromochloromethane ND ug/m3 07/24/19 11:28 124-48-173.9 42.7
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:28 106-93-433.3 42.7
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:28 95-50-152.1 42.7
1,3-Dichlorobenzene ND ug/m3 07/24/19 11:28 541-73-152.1 42.7
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:28 106-46-713142.7
Dichlorodifluoromethane ND ug/m3 07/24/19 11:28 75-71-843.1 42.7
1,1-Dichloroethane ND ug/m3 07/24/19 11:28 75-34-335.1 42.7
1,2-Dichloroethane ND ug/m3 07/24/19 11:28 107-06-217.5 42.7
1,1-Dichloroethene ND ug/m3 07/24/19 11:28 75-35-434.4 42.7
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:28 156-59-234.4 42.7
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:28 156-60-534.4 42.7
1,2-Dichloropropane ND ug/m3 07/24/19 11:28 78-87-540.1 42.7
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:28 10061-01-539.4 42.7
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:28 10061-02-639.4 42.7
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:28 76-14-260.6 42.7
Ethyl acetate ND ug/m3 07/24/19 11:28 141-78-631.3 42.7
Ethylbenzene 66.9 ug/m3 07/24/19 11:28 100-41-437.7 42.7
4-Ethyltoluene ND ug/m3 07/24/19 11:28 622-96-810742.7
n-Heptane ND ug/m3 07/24/19 11:28 142-82-535.6 42.7
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:28 87-68-323142.7
n-Hexane 86.8 ug/m3 07/24/19 11:28 110-54-330.6 42.7
2-Hexanone ND ug/m3 07/24/19 11:28 591-78-617842.7
Methylene Chloride ND ug/m3 07/24/19 11:28 75-09-215142.7
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 11:28 108-10-117842.7
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:28 1634-04-415642.7
Naphthalene ND ug/m3 07/24/19 11:28 91-20-311442.7
Propylene 466 ug/m3 07/24/19 11:28 115-07-114.9 42.7
Styrene ND ug/m3 07/24/19 11:28 100-42-537.0 42.7
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:28 79-34-529.8 42.7
Tetrachloroethene ND ug/m3 07/24/19 11:28 127-18-429.4 42.7
Tetrahydrofuran ND ug/m3 07/24/19 11:28 109-99-925.6 42.7
Toluene 300 ug/m3 07/24/19 11:28 108-88-332.7 42.7
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:28 120-82-132242.7
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-19 (2435)Lab ID:92437876001 Collected:07/11/19 12:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:28 71-55-647.4 42.7
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:28 79-00-523.7 42.7
Trichloroethene ND ug/m3 07/24/19 11:28 79-01-623.3 42.7
Trichlorofluoromethane ND ug/m3 07/24/19 11:28 75-69-448.7 42.7
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:28 76-13-166.6 42.7
1,2,4-Trimethylbenzene 67.4 ug/m3 07/24/19 11:28 95-63-642.7 42.7
1,3,5-Trimethylbenzene 64.8 ug/m3 07/24/19 11:28 108-67-842.7 42.7
Vinyl acetate ND ug/m3 07/24/19 11:28 108-05-476.4 42.7
Vinyl chloride ND ug/m3 07/24/19 11:28 75-01-411.1 42.7
m&p-Xylene 266 ug/m3 07/24/19 11:28 179601-23-175.6 42.7
o-Xylene 80.2 ug/m3 07/24/19 11:28 95-47-637.7 42.7
REPORT OF LABORATORY ANALYSIS
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Page 5 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-20 (2441)Lab ID:92437876002 Collected:07/11/19 12:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 30.7 ug/m3 07/24/19 11:00 67-64-14.9 2.02
Benzene 28.3 ug/m3 07/24/19 11:00 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 11:00 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 11:00 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 11:00 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 11:00 106-99-00.91 2.02
2-Butanone (MEK)ND ug/m3 07/24/19 11:00 78-93-36.1 2.02
Carbon disulfide 12.2 ug/m3 07/24/19 11:00 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 11:00 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 11:00 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 11:00 75-00-31.1 2.02
Chloroform 26.4 ug/m3 07/24/19 11:00 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 11:00 74-87-30.85 2.02
Cyclohexane 18.0 ug/m3 07/24/19 11:00 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 11:00 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:00 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:00 95-50-12.5 2.02
1,3-Dichlorobenzene 10.6 ug/m3 07/24/19 11:00 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:00 106-46-76.2 2.02
Dichlorodifluoromethane 2.3 ug/m3 07/24/19 11:00 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 11:00 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 11:00 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 11:00 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:00 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:00 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 11:00 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:00 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:00 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:00 76-14-22.9 2.02
Ethyl acetate 2.9 ug/m3 07/24/19 11:00 141-78-61.5 2.02
Ethylbenzene 25.4 ug/m3 07/24/19 11:00 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 11:00 622-96-85.0 2.02
n-Heptane 36.6 ug/m3 07/24/19 11:00 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:00 87-68-310.9 2.02
n-Hexane 69.3 ug/m3 07/24/19 11:00 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 11:00 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 11:00 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)9.5 ug/m3 07/24/19 11:00 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:00 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 11:00 91-20-35.4 2.02
Propylene 305 ug/m3 07/24/19 11:00 115-07-1 E0.71 2.02
Styrene 6.6 ug/m3 07/24/19 11:00 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:00 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 11:00 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 11:00 109-99-91.2 2.02
Toluene 167 ug/m3 07/24/19 11:00 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:00 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-20 (2441)Lab ID:92437876002 Collected:07/11/19 12:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:00 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:00 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 11:00 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 11:00 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:00 76-13-13.2 2.02
1,2,4-Trimethylbenzene 20.2 ug/m3 07/24/19 11:00 95-63-62.0 2.02
1,3,5-Trimethylbenzene 10.9 ug/m3 07/24/19 11:00 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 11:00 108-05-41.4 2.02
Vinyl chloride 1.1 ug/m3 07/24/19 11:00 75-01-40.53 2.02
m&p-Xylene 94.8 ug/m3 07/24/19 11:00 179601-23-13.6 2.02
o-Xylene 26.6 ug/m3 07/24/19 11:00 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
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Page 7 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-21 (1348)Lab ID:92437876003 Collected:07/11/19 13:10 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 63.4 ug/m3 07/24/19 11:29 67-64-14.9 2.02
Benzene 45.7 ug/m3 07/24/19 11:29 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 11:29 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 11:29 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 11:29 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 11:29 106-99-00.91 2.02
2-Butanone (MEK)6.5 ug/m3 07/24/19 11:29 78-93-36.1 2.02
Carbon disulfide 118 ug/m3 07/24/19 11:29 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 11:29 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 11:29 108-90-71.9 2.02
Chloroethane 3.4 ug/m3 07/24/19 11:29 75-00-31.1 2.02
Chloroform 19.1 ug/m3 07/24/19 11:29 67-66-31.0 2.02
Chloromethane 8.1 ug/m3 07/24/19 11:29 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 11:29 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 11:29 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:29 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:29 95-50-12.5 2.02
1,3-Dichlorobenzene 4.1 ug/m3 07/24/19 11:29 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:29 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 11:29 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 11:29 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 11:29 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 11:29 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:29 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:29 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 11:29 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:29 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:29 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:29 76-14-22.9 2.02
Ethyl acetate 2.6 ug/m3 07/24/19 11:29 141-78-61.5 2.02
Ethylbenzene 28.8 ug/m3 07/24/19 11:29 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 11:29 622-96-85.0 2.02
n-Heptane 66.9 ug/m3 07/24/19 11:29 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:29 87-68-310.9 2.02
n-Hexane 170 ug/m3 07/24/19 11:29 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 11:29 591-78-68.4 2.02
Methylene Chloride 10.5 ug/m3 07/24/19 11:29 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)11.8 ug/m3 07/24/19 11:29 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:29 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 11:29 91-20-35.4 2.02
Propylene 6470 ug/m3 07/25/19 12:03 115-07-1113323.2
Styrene 62.4 ug/m3 07/24/19 11:29 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:29 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 11:29 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 11:29 109-99-91.2 2.02
Toluene 188 ug/m3 07/24/19 11:29 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:29 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 8 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-21 (1348)Lab ID:92437876003 Collected:07/11/19 13:10 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:29 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:29 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 11:29 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 11:29 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:29 76-13-13.2 2.02
1,2,4-Trimethylbenzene 4.0 ug/m3 07/24/19 11:29 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 11:29 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 11:29 108-05-41.4 2.02
Vinyl chloride 4.6 ug/m3 07/24/19 11:29 75-01-40.53 2.02
m&p-Xylene 109 ug/m3 07/24/19 11:29 179601-23-13.6 2.02
o-Xylene 28.2 ug/m3 07/24/19 11:29 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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9800 Kincey Ave. Suite 100
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Page 9 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-22 (2215)Lab ID:92437876004 Collected:07/11/19 13:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 35.4 ug/m3 07/24/19 11:58 67-64-15.1 2.1
Benzene 14.4 ug/m3 07/24/19 11:58 71-43-20.68 2.1
Bromodichloromethane ND ug/m3 07/24/19 11:58 75-27-42.9 2.1
Bromoform ND ug/m3 07/24/19 11:58 75-25-211.0 2.1
Bromomethane ND ug/m3 07/24/19 11:58 74-83-91.7 2.1
1,3-Butadiene ND ug/m3 07/24/19 11:58 106-99-00.94 2.1
2-Butanone (MEK)ND ug/m3 07/24/19 11:58 78-93-36.3 2.1
Carbon disulfide 1.9 ug/m3 07/24/19 11:58 75-15-01.3 2.1
Carbon tetrachloride ND ug/m3 07/24/19 11:58 56-23-52.7 2.1
Chlorobenzene ND ug/m3 07/24/19 11:58 108-90-72.0 2.1
Chloroethane ND ug/m3 07/24/19 11:58 75-00-31.1 2.1
Chloroform 4.1 ug/m3 07/24/19 11:58 67-66-31.0 2.1
Chloromethane 0.89 ug/m3 07/24/19 11:58 74-87-30.88 2.1
Cyclohexane 6.3 ug/m3 07/24/19 11:58 110-82-73.7 2.1
Dibromochloromethane ND ug/m3 07/24/19 11:58 124-48-13.6 2.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:58 106-93-41.6 2.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:58 95-50-12.6 2.1
1,3-Dichlorobenzene 24.2 ug/m3 07/24/19 11:58 541-73-12.6 2.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:58 106-46-76.4 2.1
Dichlorodifluoromethane ND ug/m3 07/24/19 11:58 75-71-82.1 2.1
1,1-Dichloroethane ND ug/m3 07/24/19 11:58 75-34-31.7 2.1
1,2-Dichloroethane ND ug/m3 07/24/19 11:58 107-06-20.86 2.1
1,1-Dichloroethene ND ug/m3 07/24/19 11:58 75-35-41.7 2.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:58 156-59-21.7 2.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:58 156-60-51.7 2.1
1,2-Dichloropropane ND ug/m3 07/24/19 11:58 78-87-52.0 2.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:58 10061-01-51.9 2.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:58 10061-02-61.9 2.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:58 76-14-23.0 2.1
Ethyl acetate 2.9 ug/m3 07/24/19 11:58 141-78-61.5 2.1
Ethylbenzene 20.0 ug/m3 07/24/19 11:58 100-41-41.9 2.1
4-Ethyltoluene 5.4 ug/m3 07/24/19 11:58 622-96-85.2 2.1
n-Heptane 16.4 ug/m3 07/24/19 11:58 142-82-51.7 2.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:58 87-68-311.4 2.1
n-Hexane 15.5 ug/m3 07/24/19 11:58 110-54-31.5 2.1
2-Hexanone ND ug/m3 07/24/19 11:58 591-78-68.7 2.1
Methylene Chloride 10.9 ug/m3 07/24/19 11:58 75-09-27.4 2.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 11:58 108-10-18.7 2.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:58 1634-04-47.7 2.1
Naphthalene ND ug/m3 07/24/19 11:58 91-20-35.6 2.1
Propylene 9.2 ug/m3 07/24/19 11:58 115-07-10.74 2.1
Styrene 12.0 ug/m3 07/24/19 11:58 100-42-51.8 2.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:58 79-34-51.5 2.1
Tetrachloroethene ND ug/m3 07/24/19 11:58 127-18-41.4 2.1
Tetrahydrofuran ND ug/m3 07/24/19 11:58 109-99-91.3 2.1
Toluene 122 ug/m3 07/24/19 11:58 108-88-31.6 2.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:58 120-82-115.8 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 10 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-22 (2215)Lab ID:92437876004 Collected:07/11/19 13:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:58 71-55-62.3 2.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:58 79-00-51.2 2.1
Trichloroethene ND ug/m3 07/24/19 11:58 79-01-61.1 2.1
Trichlorofluoromethane ND ug/m3 07/24/19 11:58 75-69-42.4 2.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:58 76-13-13.3 2.1
1,2,4-Trimethylbenzene 17.6 ug/m3 07/24/19 11:58 95-63-62.1 2.1
1,3,5-Trimethylbenzene 8.7 ug/m3 07/24/19 11:58 108-67-82.1 2.1
Vinyl acetate ND ug/m3 07/24/19 11:58 108-05-41.5 2.1
Vinyl chloride ND ug/m3 07/24/19 11:58 75-01-40.55 2.1
m&p-Xylene 77.3 ug/m3 07/24/19 11:58 179601-23-13.7 2.1
o-Xylene 21.7 ug/m3 07/24/19 11:58 95-47-61.9 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-23 (3229)Lab ID:92437876005 Collected:07/11/19 14:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 86.8 ug/m3 07/24/19 12:27 67-64-14.9 2.02
Benzene 27.8 ug/m3 07/24/19 12:27 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 12:27 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 12:27 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 12:27 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 12:27 106-99-00.91 2.02
2-Butanone (MEK)8.1 ug/m3 07/24/19 12:27 78-93-36.1 2.02
Carbon disulfide 34.3 ug/m3 07/24/19 12:27 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 12:27 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 12:27 108-90-71.9 2.02
Chloroethane 5.3 ug/m3 07/24/19 12:27 75-00-31.1 2.02
Chloroform 36.6 ug/m3 07/24/19 12:27 67-66-31.0 2.02
Chloromethane 5.8 ug/m3 07/24/19 12:27 74-87-30.85 2.02
Cyclohexane 17.4 ug/m3 07/24/19 12:27 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 12:27 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 12:27 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 12:27 95-50-12.5 2.02
1,3-Dichlorobenzene ND ug/m3 07/24/19 12:27 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 12:27 106-46-76.2 2.02
Dichlorodifluoromethane 2.2 ug/m3 07/24/19 12:27 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 12:27 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 12:27 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 12:27 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 12:27 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 12:27 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 12:27 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 12:27 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 12:27 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 12:27 76-14-22.9 2.02
Ethyl acetate ND ug/m3 07/24/19 12:27 141-78-61.5 2.02
Ethylbenzene 38.8 ug/m3 07/24/19 12:27 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 12:27 622-96-85.0 2.02
n-Heptane 48.0 ug/m3 07/24/19 12:27 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 12:27 87-68-310.9 2.02
n-Hexane 51.3 ug/m3 07/24/19 12:27 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 12:27 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 12:27 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 12:27 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 12:27 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 12:27 91-20-35.4 2.02
Propylene 194 ug/m3 07/24/19 12:27 115-07-1 E0.71 2.02
Styrene 17.9 ug/m3 07/24/19 12:27 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 12:27 79-34-51.4 2.02
Tetrachloroethene 7.1 ug/m3 07/24/19 12:27 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 12:27 109-99-91.2 2.02
Toluene 221 ug/m3 07/24/19 12:27 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 12:27 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-23 (3229)Lab ID:92437876005 Collected:07/11/19 14:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 12:27 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 12:27 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 12:27 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 12:27 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 12:27 76-13-13.2 2.02
1,2,4-Trimethylbenzene ND ug/m3 07/24/19 12:27 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 12:27 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 12:27 108-05-41.4 2.02
Vinyl chloride 2.2 ug/m3 07/24/19 12:27 75-01-40.53 2.02
m&p-Xylene 145 ug/m3 07/24/19 12:27 179601-23-13.6 2.02
o-Xylene 41.8 ug/m3 07/24/19 12:27 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 13 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-24 (2789)Lab ID:92437876006 Collected:07/11/19 14:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 111 ug/m3 07/24/19 13:02 67-64-14.9 2.02
Benzene 67.5 ug/m3 07/24/19 13:02 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 13:02 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 13:02 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 13:02 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 13:02 106-99-00.91 2.02
2-Butanone (MEK)15.9 ug/m3 07/24/19 13:02 78-93-36.1 2.02
Carbon disulfide 777 ug/m3 07/25/19 11:36 75-15-0102161.6
Carbon tetrachloride ND ug/m3 07/24/19 13:02 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 13:02 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 13:02 75-00-31.1 2.02
Chloroform 31.1 ug/m3 07/24/19 13:02 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 13:02 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 13:02 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 13:02 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 13:02 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 13:02 95-50-12.5 2.02
1,3-Dichlorobenzene 36.1 ug/m3 07/24/19 13:02 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 13:02 106-46-76.2 2.02
Dichlorodifluoromethane 4.0 ug/m3 07/24/19 13:02 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 13:02 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 13:02 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 13:02 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 13:02 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 13:02 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 13:02 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 13:02 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 13:02 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 13:02 76-14-22.9 2.02
Ethyl acetate 5.1 ug/m3 07/24/19 13:02 141-78-61.5 2.02
Ethylbenzene 62.7 ug/m3 07/24/19 13:02 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 13:02 622-96-85.0 2.02
n-Heptane 133 ug/m3 07/24/19 13:02 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 13:02 87-68-310.9 2.02
n-Hexane 359 ug/m3 07/25/19 11:36 110-54-3116161.6
2-Hexanone ND ug/m3 07/24/19 13:02 591-78-68.4 2.02
Methylene Chloride 13.6 ug/m3 07/24/19 13:02 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 13:02 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 13:02 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 13:02 91-20-35.4 2.02
Propylene 2920 ug/m3 07/25/19 11:36 115-07-156.6 161.6
Styrene 10.1 ug/m3 07/24/19 13:02 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 13:02 79-34-51.4 2.02
Tetrachloroethene 14.8 ug/m3 07/24/19 13:02 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 13:02 109-99-91.2 2.02
Toluene 412 ug/m3 07/25/19 11:36 108-88-3124161.6
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 13:02 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-24 (2789)Lab ID:92437876006 Collected:07/11/19 14:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 13:02 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 13:02 79-00-51.1 2.02
Trichloroethene 2.2 ug/m3 07/24/19 13:02 79-01-61.1 2.02
Trichlorofluoromethane 2.7 ug/m3 07/24/19 13:02 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 13:02 76-13-13.2 2.02
1,2,4-Trimethylbenzene 12.5 ug/m3 07/24/19 13:02 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 13:02 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 13:02 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 13:02 75-01-40.53 2.02
m&p-Xylene 204 ug/m3 07/24/19 13:02 179601-23-13.6 2.02
o-Xylene 65.9 ug/m3 07/24/19 13:02 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 15 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-8 (3227)Lab ID:92437876007 Collected:07/11/19 17:05 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 58.8 ug/m3 07/24/19 13:31 67-64-14.9 2.02
Benzene 29.9 ug/m3 07/24/19 13:31 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 13:31 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 13:31 75-25-210.6 2.02
Bromomethane 1.9 ug/m3 07/24/19 13:31 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 13:31 106-99-00.91 2.02
2-Butanone (MEK)11.4 ug/m3 07/24/19 13:31 78-93-36.1 2.02
Carbon disulfide 30.3 ug/m3 07/24/19 13:31 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 13:31 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 13:31 108-90-71.9 2.02
Chloroethane 6.9 ug/m3 07/24/19 13:31 75-00-31.1 2.02
Chloroform 11.0 ug/m3 07/24/19 13:31 67-66-31.0 2.02
Chloromethane 13.9 ug/m3 07/24/19 13:31 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 13:31 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 13:31 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 13:31 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 13:31 95-50-12.5 2.02
1,3-Dichlorobenzene 10.5 ug/m3 07/24/19 13:31 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 13:31 106-46-76.2 2.02
Dichlorodifluoromethane 2.1 ug/m3 07/24/19 13:31 75-71-82.0 2.02
1,1-Dichloroethane 2.4 ug/m3 07/24/19 13:31 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 13:31 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 13:31 75-35-41.6 2.02
cis-1,2-Dichloroethene 7.2 ug/m3 07/24/19 13:31 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 13:31 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 13:31 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 13:31 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 13:31 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 13:31 76-14-22.9 2.02
Ethyl acetate 3.1 ug/m3 07/24/19 13:31 141-78-61.5 2.02
Ethylbenzene 27.3 ug/m3 07/24/19 13:31 100-41-41.8 2.02
4-Ethyltoluene 8.7 ug/m3 07/24/19 13:31 622-96-85.0 2.02
n-Heptane 38.5 ug/m3 07/24/19 13:31 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 13:31 87-68-310.9 2.02
n-Hexane 43.9 ug/m3 07/24/19 13:31 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 13:31 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 13:31 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)12.3 ug/m3 07/24/19 13:31 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 13:31 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 13:31 91-20-35.4 2.02
Propylene 98.2 ug/m3 07/24/19 13:31 115-07-10.71 2.02
Styrene 5.9 ug/m3 07/24/19 13:31 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 13:31 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 13:31 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 13:31 109-99-91.2 2.02
Toluene 187 ug/m3 07/24/19 13:31 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 13:31 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
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Page 16 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-8 (3227)Lab ID:92437876007 Collected:07/11/19 17:05 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 13:31 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 13:31 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 13:31 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 13:31 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 13:31 76-13-13.2 2.02
1,2,4-Trimethylbenzene 29.9 ug/m3 07/24/19 13:31 95-63-62.0 2.02
1,3,5-Trimethylbenzene 12.9 ug/m3 07/24/19 13:31 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 13:31 108-05-41.4 2.02
Vinyl chloride 2.1 ug/m3 07/24/19 13:31 75-01-40.53 2.02
m&p-Xylene 113 ug/m3 07/24/19 13:31 179601-23-13.6 2.02
o-Xylene 31.6 ug/m3 07/24/19 13:31 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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9800 Kincey Ave. Suite 100
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Page 17 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-7 (2650)Lab ID:92437876008 Collected:07/11/19 17:25 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 41.6 ug/m3 07/24/19 14:00 67-64-14.9 2.02
Benzene 16.3 ug/m3 07/24/19 14:00 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 14:00 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 14:00 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 14:00 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 14:00 106-99-00.91 2.02
2-Butanone (MEK)6.5 ug/m3 07/24/19 14:00 78-93-36.1 2.02
Carbon disulfide 22.9 ug/m3 07/24/19 14:00 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 14:00 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 14:00 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 14:00 75-00-31.1 2.02
Chloroform 4.2 ug/m3 07/24/19 14:00 67-66-31.0 2.02
Chloromethane 1.1 ug/m3 07/24/19 14:00 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 14:00 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 14:00 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 14:00 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 14:00 95-50-12.5 2.02
1,3-Dichlorobenzene 9.9 ug/m3 07/24/19 14:00 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 14:00 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 14:00 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 14:00 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 14:00 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 14:00 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 14:00 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 14:00 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 14:00 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 14:00 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 14:00 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 14:00 76-14-22.9 2.02
Ethyl acetate 3.5 ug/m3 07/24/19 14:00 141-78-61.5 2.02
Ethylbenzene 14.7 ug/m3 07/24/19 14:00 100-41-41.8 2.02
4-Ethyltoluene 5.4 ug/m3 07/24/19 14:00 622-96-85.0 2.02
n-Heptane 21.5 ug/m3 07/24/19 14:00 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 14:00 87-68-310.9 2.02
n-Hexane 37.3 ug/m3 07/24/19 14:00 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 14:00 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 14:00 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 14:00 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 14:00 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 14:00 91-20-35.4 2.02
Propylene 332 ug/m3 07/24/19 14:00 115-07-1 E0.71 2.02
Styrene ND ug/m3 07/24/19 14:00 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 14:00 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 14:00 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 14:00 109-99-91.2 2.02
Toluene 99.5 ug/m3 07/24/19 14:00 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 14:00 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-7 (2650)Lab ID:92437876008 Collected:07/11/19 17:25 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 14:00 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 14:00 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 14:00 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 14:00 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 14:00 76-13-13.2 2.02
1,2,4-Trimethylbenzene 14.2 ug/m3 07/24/19 14:00 95-63-62.0 2.02
1,3,5-Trimethylbenzene 7.2 ug/m3 07/24/19 14:00 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 14:00 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 14:00 75-01-40.53 2.02
m&p-Xylene 55.4 ug/m3 07/24/19 14:00 179601-23-13.6 2.02
o-Xylene 16.0 ug/m3 07/24/19 14:00 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-6 (3294)Lab ID:92437876009 Collected:07/11/19 17:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 36.4 ug/m3 07/24/19 14:29 67-64-14.2 1.74
Benzene 5.3 ug/m3 07/24/19 14:29 71-43-20.57 1.74
Bromodichloromethane ND ug/m3 07/24/19 14:29 75-27-42.4 1.74
Bromoform ND ug/m3 07/24/19 14:29 75-25-29.1 1.74
Bromomethane ND ug/m3 07/24/19 14:29 74-83-91.4 1.74
1,3-Butadiene ND ug/m3 07/24/19 14:29 106-99-00.78 1.74
2-Butanone (MEK)6.5 ug/m3 07/24/19 14:29 78-93-35.2 1.74
Carbon disulfide 4.5 ug/m3 07/24/19 14:29 75-15-01.1 1.74
Carbon tetrachloride ND ug/m3 07/24/19 14:29 56-23-52.2 1.74
Chlorobenzene ND ug/m3 07/24/19 14:29 108-90-71.6 1.74
Chloroethane ND ug/m3 07/24/19 14:29 75-00-30.93 1.74
Chloroform 2.1 ug/m3 07/24/19 14:29 67-66-30.86 1.74
Chloromethane ND ug/m3 07/24/19 14:29 74-87-30.73 1.74
Cyclohexane 5.2 ug/m3 07/24/19 14:29 110-82-73.0 1.74
Dibromochloromethane ND ug/m3 07/24/19 14:29 124-48-13.0 1.74
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 14:29 106-93-41.4 1.74
1,2-Dichlorobenzene ND ug/m3 07/24/19 14:29 95-50-12.1 1.74
1,3-Dichlorobenzene 20.8 ug/m3 07/24/19 14:29 541-73-12.1 1.74
1,4-Dichlorobenzene ND ug/m3 07/24/19 14:29 106-46-75.3 1.74
Dichlorodifluoromethane ND ug/m3 07/24/19 14:29 75-71-81.8 1.74
1,1-Dichloroethane ND ug/m3 07/24/19 14:29 75-34-31.4 1.74
1,2-Dichloroethane ND ug/m3 07/24/19 14:29 107-06-20.72 1.74
1,1-Dichloroethene ND ug/m3 07/24/19 14:29 75-35-41.4 1.74
cis-1,2-Dichloroethene ND ug/m3 07/24/19 14:29 156-59-21.4 1.74
trans-1,2-Dichloroethene ND ug/m3 07/24/19 14:29 156-60-51.4 1.74
1,2-Dichloropropane ND ug/m3 07/24/19 14:29 78-87-51.6 1.74
cis-1,3-Dichloropropene ND ug/m3 07/24/19 14:29 10061-01-51.6 1.74
trans-1,3-Dichloropropene ND ug/m3 07/24/19 14:29 10061-02-61.6 1.74
Dichlorotetrafluoroethane ND ug/m3 07/24/19 14:29 76-14-22.5 1.74
Ethyl acetate 2.1 ug/m3 07/24/19 14:29 141-78-61.3 1.74
Ethylbenzene 12.2 ug/m3 07/24/19 14:29 100-41-41.5 1.74
4-Ethyltoluene 5.2 ug/m3 07/24/19 14:29 622-96-84.4 1.74
n-Heptane 9.2 ug/m3 07/24/19 14:29 142-82-51.4 1.74
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 14:29 87-68-39.4 1.74
n-Hexane 10.4 ug/m3 07/24/19 14:29 110-54-31.2 1.74
2-Hexanone ND ug/m3 07/24/19 14:29 591-78-67.2 1.74
Methylene Chloride ND ug/m3 07/24/19 14:29 75-09-26.1 1.74
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 14:29 108-10-17.2 1.74
Methyl-tert-butyl ether ND ug/m3 07/24/19 14:29 1634-04-46.4 1.74
Naphthalene ND ug/m3 07/24/19 14:29 91-20-34.6 1.74
Propylene 14.8 ug/m3 07/24/19 14:29 115-07-10.61 1.74
Styrene 1440 ug/m3 07/25/19 11:09 100-42-545.2 52.2
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 14:29 79-34-51.2 1.74
Tetrachloroethene ND ug/m3 07/24/19 14:29 127-18-41.2 1.74
Tetrahydrofuran ND ug/m3 07/24/19 14:29 109-99-91.0 1.74
Toluene 42.2 ug/m3 07/24/19 14:29 108-88-31.3 1.74
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 14:29 120-82-113.1 1.74
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-6 (3294)Lab ID:92437876009 Collected:07/11/19 17:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 14:29 71-55-61.9 1.74
1,1,2-Trichloroethane ND ug/m3 07/24/19 14:29 79-00-50.97 1.74
Trichloroethene ND ug/m3 07/24/19 14:29 79-01-60.95 1.74
Trichlorofluoromethane ND ug/m3 07/24/19 14:29 75-69-42.0 1.74
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 14:29 76-13-12.7 1.74
1,2,4-Trimethylbenzene 21.3 ug/m3 07/24/19 14:29 95-63-61.7 1.74
1,3,5-Trimethylbenzene 9.1 ug/m3 07/24/19 14:29 108-67-81.7 1.74
Vinyl acetate ND ug/m3 07/24/19 14:29 108-05-41.2 1.74
Vinyl chloride ND ug/m3 07/24/19 14:29 75-01-40.45 1.74
m&p-Xylene 44.9 ug/m3 07/24/19 14:29 179601-23-13.1 1.74
o-Xylene 10 ug/m3 07/24/19 14:29 95-47-61.5 1.74
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-5 (2243)Lab ID:92437876010 Collected:07/11/19 18:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 36.3 ug/m3 07/24/19 14:58 67-64-14.7 1.94
Benzene 5.4 ug/m3 07/24/19 14:58 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 14:58 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 14:58 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 14:58 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 14:58 106-99-00.87 1.94
2-Butanone (MEK)6.3 ug/m3 07/24/19 14:58 78-93-35.8 1.94
Carbon disulfide 2.9 ug/m3 07/24/19 14:58 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 14:58 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 14:58 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 14:58 75-00-31.0 1.94
Chloroform ND ug/m3 07/24/19 14:58 67-66-30.96 1.94
Chloromethane 1.6 ug/m3 07/24/19 14:58 74-87-30.81 1.94
Cyclohexane 4.7 ug/m3 07/24/19 14:58 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 14:58 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 14:58 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 14:58 95-50-12.4 1.94
1,3-Dichlorobenzene 14.6 ug/m3 07/24/19 14:58 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 14:58 106-46-75.9 1.94
Dichlorodifluoromethane 2.4 ug/m3 07/24/19 14:58 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 14:58 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 14:58 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 14:58 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 14:58 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 14:58 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 14:58 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 14:58 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 14:58 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 14:58 76-14-22.8 1.94
Ethyl acetate 3.3 ug/m3 07/24/19 14:58 141-78-61.4 1.94
Ethylbenzene 4.8 ug/m3 07/24/19 14:58 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 14:58 622-96-84.8 1.94
n-Heptane 7.4 ug/m3 07/24/19 14:58 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 14:58 87-68-310.5 1.94
n-Hexane 10.1 ug/m3 07/24/19 14:58 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 14:58 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 14:58 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 14:58 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 14:58 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 14:58 91-20-35.2 1.94
Propylene 16.9 ug/m3 07/24/19 14:58 115-07-10.68 1.94
Styrene ND ug/m3 07/25/19 10:12 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 14:58 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 14:58 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 14:58 109-99-91.2 1.94
Toluene 33.3 ug/m3 07/24/19 14:58 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 14:58 120-82-114.6 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
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Page 22 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-5 (2243)Lab ID:92437876010 Collected:07/11/19 18:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 14:58 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 14:58 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 14:58 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 14:58 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 14:58 76-13-13.0 1.94
1,2,4-Trimethylbenzene 5.8 ug/m3 07/24/19 14:58 95-63-61.9 1.94
1,3,5-Trimethylbenzene 2.2 ug/m3 07/24/19 14:58 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 14:58 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 14:58 75-01-40.50 1.94
m&p-Xylene 15.8 ug/m3 07/24/19 14:58 179601-23-13.4 1.94
o-Xylene 5.5 ug/m3 07/24/19 14:58 95-47-61.7 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 23 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-4 (2924)Lab ID:92437876011 Collected:07/11/19 18:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 28.4 ug/m3 07/24/19 15:27 67-64-14.7 1.94
Benzene 10.1 ug/m3 07/24/19 15:27 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 15:27 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 15:27 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 15:27 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 15:27 106-99-00.87 1.94
2-Butanone (MEK)6.9 ug/m3 07/24/19 15:27 78-93-35.8 1.94
Carbon disulfide 5.1 ug/m3 07/24/19 15:27 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 15:27 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 15:27 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 15:27 75-00-31.0 1.94
Chloroform 8.6 ug/m3 07/24/19 15:27 67-66-30.96 1.94
Chloromethane 1.1 ug/m3 07/24/19 15:27 74-87-30.81 1.94
Cyclohexane 5.3 ug/m3 07/24/19 15:27 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 15:27 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 15:27 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 15:27 95-50-12.4 1.94
1,3-Dichlorobenzene 5.2 ug/m3 07/24/19 15:27 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 15:27 106-46-75.9 1.94
Dichlorodifluoromethane 2.0 ug/m3 07/24/19 15:27 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 15:27 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 15:27 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 15:27 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 15:27 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 15:27 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 15:27 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 15:27 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 15:27 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 15:27 76-14-22.8 1.94
Ethyl acetate 2.7 ug/m3 07/24/19 15:27 141-78-61.4 1.94
Ethylbenzene 10.6 ug/m3 07/24/19 15:27 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 15:27 622-96-84.8 1.94
n-Heptane 13.2 ug/m3 07/24/19 15:27 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 15:27 87-68-310.5 1.94
n-Hexane 13.9 ug/m3 07/24/19 15:27 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 15:27 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 15:27 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 15:27 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 15:27 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 15:27 91-20-35.2 1.94
Propylene 53.9 ug/m3 07/24/19 15:27 115-07-10.68 1.94
Styrene 35.1 ug/m3 07/24/19 15:27 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 15:27 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 15:27 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 15:27 109-99-91.2 1.94
Toluene 70.7 ug/m3 07/24/19 15:27 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 15:27 120-82-114.6 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 24 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-4 (2924)Lab ID:92437876011 Collected:07/11/19 18:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 15:27 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 15:27 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 15:27 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 15:27 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 15:27 76-13-13.0 1.94
1,2,4-Trimethylbenzene 7.9 ug/m3 07/24/19 15:27 95-63-61.9 1.94
1,3,5-Trimethylbenzene 4.8 ug/m3 07/24/19 15:27 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 15:27 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 15:27 75-01-40.50 1.94
m&p-Xylene 38.5 ug/m3 07/24/19 15:27 179601-23-13.4 1.94
o-Xylene 10.1 ug/m3 07/24/19 15:27 95-47-61.7 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-3 (1792)Lab ID:92437876012 Collected:07/11/19 18:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 21.9 ug/m3 07/24/19 15:56 67-64-14.7 1.94
Benzene 14.7 ug/m3 07/24/19 15:56 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 15:56 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 15:56 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 15:56 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 15:56 106-99-00.87 1.94
2-Butanone (MEK)ND ug/m3 07/24/19 15:56 78-93-35.8 1.94
Carbon disulfide 3.8 ug/m3 07/24/19 15:56 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 15:56 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 15:56 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 15:56 75-00-31.0 1.94
Chloroform 8.3 ug/m3 07/24/19 15:56 67-66-30.96 1.94
Chloromethane ND ug/m3 07/24/19 15:56 74-87-30.81 1.94
Cyclohexane 13.3 ug/m3 07/24/19 15:56 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 15:56 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 15:56 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 15:56 95-50-12.4 1.94
1,3-Dichlorobenzene 4.6 ug/m3 07/24/19 15:56 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 15:56 106-46-75.9 1.94
Dichlorodifluoromethane 2.1 ug/m3 07/24/19 15:56 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 15:56 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 15:56 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 15:56 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 15:56 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 15:56 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 15:56 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 15:56 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 15:56 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 15:56 76-14-22.8 1.94
Ethyl acetate 2.7 ug/m3 07/24/19 15:56 141-78-61.4 1.94
Ethylbenzene 9.8 ug/m3 07/24/19 15:56 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 15:56 622-96-84.8 1.94
n-Heptane 25.9 ug/m3 07/24/19 15:56 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 15:56 87-68-310.5 1.94
n-Hexane 27.5 ug/m3 07/24/19 15:56 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 15:56 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 15:56 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 15:56 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 15:56 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 15:56 91-20-35.2 1.94
Propylene 19.4 ug/m3 07/24/19 15:56 115-07-10.68 1.94
Styrene 6.9 ug/m3 07/24/19 15:56 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 15:56 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 15:56 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 15:56 109-99-91.2 1.94
Toluene 83.2 ug/m3 07/24/19 15:56 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 15:56 120-82-114.6 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-3 (1792)Lab ID:92437876012 Collected:07/11/19 18:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 15:56 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 15:56 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 15:56 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 15:56 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 15:56 76-13-13.0 1.94
1,2,4-Trimethylbenzene 5.8 ug/m3 07/24/19 15:56 95-63-61.9 1.94
1,3,5-Trimethylbenzene 3.6 ug/m3 07/24/19 15:56 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 15:56 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 15:56 75-01-40.50 1.94
m&p-Xylene 34.5 ug/m3 07/24/19 15:56 179601-23-13.4 1.94
o-Xylene 9.1 ug/m3 07/24/19 15:56 95-47-61.7 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-2 (2878)Lab ID:92437876013 Collected:07/11/19 19:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 37.9 ug/m3 07/26/19 00:55 67-64-17.9 3.26
Benzene 1.8 ug/m3 07/26/19 00:55 71-43-21.1 3.26
Bromodichloromethane ND ug/m3 07/26/19 00:55 75-27-44.4 3.26
Bromoform ND ug/m3 07/26/19 00:55 75-25-217.1 3.26
Bromomethane ND ug/m3 07/26/19 00:55 74-83-92.6 3.26
1,3-Butadiene ND ug/m3 07/26/19 00:55 106-99-01.5 3.26
2-Butanone (MEK)ND ug/m3 07/26/19 00:55 78-93-39.8 3.26
Carbon disulfide ND ug/m3 07/26/19 00:55 75-15-02.1 3.26
Carbon tetrachloride ND ug/m3 07/26/19 00:55 56-23-54.2 3.26
Chlorobenzene ND ug/m3 07/26/19 00:55 108-90-73.1 3.26
Chloroethane ND ug/m3 07/26/19 00:55 75-00-31.7 3.26
Chloroform 5.8 ug/m3 07/26/19 00:55 67-66-31.6 3.26
Chloromethane ND ug/m3 07/26/19 00:55 74-87-31.4 3.26
Cyclohexane ND ug/m3 07/26/19 00:55 110-82-75.7 3.26
Dibromochloromethane ND ug/m3 07/26/19 00:55 124-48-15.6 3.26
1,2-Dibromoethane (EDB)ND ug/m3 07/26/19 00:55 106-93-42.5 3.26
1,2-Dichlorobenzene ND ug/m3 07/26/19 00:55 95-50-14.0 3.26
1,3-Dichlorobenzene ND ug/m3 07/26/19 00:55 541-73-14.0 3.26
1,4-Dichlorobenzene ND ug/m3 07/26/19 00:55 106-46-7103.26
Dichlorodifluoromethane ND ug/m3 07/26/19 00:55 75-71-83.3 3.26
1,1-Dichloroethane ND ug/m3 07/26/19 00:55 75-34-32.7 3.26
1,2-Dichloroethane ND ug/m3 07/26/19 00:55 107-06-21.3 3.26
1,1-Dichloroethene ND ug/m3 07/26/19 00:55 75-35-42.6 3.26
cis-1,2-Dichloroethene ND ug/m3 07/26/19 00:55 156-59-22.6 3.26
trans-1,2-Dichloroethene ND ug/m3 07/26/19 00:55 156-60-52.6 3.26
1,2-Dichloropropane ND ug/m3 07/26/19 00:55 78-87-53.1 3.26
cis-1,3-Dichloropropene ND ug/m3 07/26/19 00:55 10061-01-53.0 3.26
trans-1,3-Dichloropropene ND ug/m3 07/26/19 00:55 10061-02-63.0 3.26
Dichlorotetrafluoroethane ND ug/m3 07/26/19 00:55 76-14-24.6 3.26
Ethyl acetate ND ug/m3 07/26/19 00:55 141-78-62.4 3.26
Ethylbenzene ND ug/m3 07/26/19 00:55 100-41-42.9 3.26
4-Ethyltoluene ND ug/m3 07/26/19 00:55 622-96-88.2 3.26
n-Heptane ND ug/m3 07/26/19 00:55 142-82-52.7 3.26
Hexachloro-1,3-butadiene ND ug/m3 07/26/19 00:55 87-68-317.7 3.26
n-Hexane 26.3 ug/m3 07/26/19 00:55 110-54-32.3 3.26
2-Hexanone ND ug/m3 07/26/19 00:55 591-78-613.6 3.26
Methylene Chloride 341 ug/m3 07/26/19 00:55 75-09-211.5 3.26
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/19 00:55 108-10-113.6 3.26
Methyl-tert-butyl ether ND ug/m3 07/26/19 00:55 1634-04-411.9 3.26
Naphthalene ND ug/m3 07/26/19 00:55 91-20-38.7 3.26
Propylene 11.8 ug/m3 07/26/19 00:55 115-07-11.1 3.26
Styrene ND ug/m3 07/26/19 00:55 100-42-52.8 3.26
1,1,2,2-Tetrachloroethane ND ug/m3 07/26/19 00:55 79-34-52.3 3.26
Tetrachloroethene ND ug/m3 07/26/19 00:55 127-18-42.2 3.26
Tetrahydrofuran ND ug/m3 07/26/19 00:55 109-99-92.0 3.26
Toluene 12.9 ug/m3 07/26/19 00:55 108-88-32.5 3.26
1,2,4-Trichlorobenzene ND ug/m3 07/26/19 00:55 120-82-124.6 3.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-2 (2878)Lab ID:92437876013 Collected:07/11/19 19:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/26/19 00:55 71-55-63.6 3.26
1,1,2-Trichloroethane ND ug/m3 07/26/19 00:55 79-00-51.8 3.26
Trichloroethene ND ug/m3 07/26/19 00:55 79-01-61.8 3.26
Trichlorofluoromethane ND ug/m3 07/26/19 00:55 75-69-43.7 3.26
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/19 00:55 76-13-15.1 3.26
1,2,4-Trimethylbenzene 3.5 ug/m3 07/26/19 00:55 95-63-63.3 3.26
1,3,5-Trimethylbenzene ND ug/m3 07/26/19 00:55 108-67-83.3 3.26
Vinyl acetate ND ug/m3 07/26/19 00:55 108-05-42.3 3.26
Vinyl chloride ND ug/m3 07/26/19 00:55 75-01-40.85 3.26
m&p-Xylene 8.5 ug/m3 07/26/19 00:55 179601-23-15.8 3.26
o-Xylene 3.1 ug/m3 07/26/19 00:55 95-47-62.9 3.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-1 (2194)Lab ID:92437876014 Collected:07/11/19 19:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 18.4 ug/m3 07/24/19 16:55 67-64-14.9 2.02
Benzene 3.4 ug/m3 07/24/19 16:55 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 16:55 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 16:55 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 16:55 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 16:55 106-99-00.91 2.02
2-Butanone (MEK)ND ug/m3 07/24/19 16:55 78-93-36.1 2.02
Carbon disulfide 1.6 ug/m3 07/24/19 16:55 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 16:55 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 16:55 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 16:55 75-00-31.1 2.02
Chloroform 20.0 ug/m3 07/24/19 16:55 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 16:55 74-87-30.85 2.02
Cyclohexane 4.1 ug/m3 07/24/19 16:55 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 16:55 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 16:55 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 16:55 95-50-12.5 2.02
1,3-Dichlorobenzene 3.8 ug/m3 07/24/19 16:55 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 16:55 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 16:55 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 16:55 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 16:55 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 16:55 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 16:55 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 16:55 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 16:55 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 16:55 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 16:55 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 16:55 76-14-22.9 2.02
Ethyl acetate 2.1 ug/m3 07/24/19 16:55 141-78-61.5 2.02
Ethylbenzene 5.4 ug/m3 07/24/19 16:55 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 16:55 622-96-85.0 2.02
n-Heptane 5.3 ug/m3 07/24/19 16:55 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 16:55 87-68-310.9 2.02
n-Hexane 4.7 ug/m3 07/24/19 16:55 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 16:55 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 16:55 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 16:55 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 16:55 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 16:55 91-20-35.4 2.02
Propylene 8.6 ug/m3 07/24/19 16:55 115-07-10.71 2.02
Styrene 3.3 ug/m3 07/24/19 16:55 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 16:55 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 16:55 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 16:55 109-99-91.2 2.02
Toluene 26.2 ug/m3 07/24/19 16:55 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 16:55 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 30 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-1 (2194)Lab ID:92437876014 Collected:07/11/19 19:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 16:55 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 16:55 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 16:55 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 16:55 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 16:55 76-13-13.2 2.02
1,2,4-Trimethylbenzene 7.2 ug/m3 07/24/19 16:55 95-63-62.0 2.02
1,3,5-Trimethylbenzene 5.6 ug/m3 07/24/19 16:55 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 16:55 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 16:55 75-01-40.53 2.02
m&p-Xylene 22.7 ug/m3 07/24/19 16:55 179601-23-13.6 2.02
o-Xylene 6.5 ug/m3 07/24/19 16:55 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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Page 31 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-18 (2002)Lab ID:92437876015 Collected:07/12/19 08:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 51.6 ug/m3 07/24/19 17:24 67-64-14.7 1.94
Benzene 31.8 ug/m3 07/24/19 17:24 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 17:24 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 17:24 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 17:24 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 17:24 106-99-00.87 1.94
2-Butanone (MEK)6.7 ug/m3 07/24/19 17:24 78-93-35.8 1.94
Carbon disulfide 22.7 ug/m3 07/24/19 17:24 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 17:24 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 17:24 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 17:24 75-00-31.0 1.94
Chloroform 3.7 ug/m3 07/24/19 17:24 67-66-30.96 1.94
Chloromethane 11.6 ug/m3 07/24/19 17:24 74-87-30.81 1.94
Cyclohexane ND ug/m3 07/24/19 17:24 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 17:24 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 17:24 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 17:24 95-50-12.4 1.94
1,3-Dichlorobenzene 9.3 ug/m3 07/24/19 17:24 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 17:24 106-46-75.9 1.94
Dichlorodifluoromethane 2.3 ug/m3 07/24/19 17:24 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 17:24 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 17:24 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 17:24 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 17:24 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 17:24 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 17:24 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 17:24 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 17:24 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 17:24 76-14-22.8 1.94
Ethyl acetate ND ug/m3 07/24/19 17:24 141-78-61.4 1.94
Ethylbenzene 9.2 ug/m3 07/24/19 17:24 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 17:24 622-96-84.8 1.94
n-Heptane 51.9 ug/m3 07/24/19 17:24 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 17:24 87-68-310.5 1.94
n-Hexane 154 ug/m3 07/24/19 17:24 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 17:24 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 17:24 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 17:24 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 17:24 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 17:24 91-20-35.2 1.94
Propylene 4740 ug/m3 07/25/19 12:30 115-07-1109310.4
Styrene 5.4 ug/m3 07/24/19 17:24 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 17:24 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 17:24 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 17:24 109-99-91.2 1.94
Toluene 71.7 ug/m3 07/24/19 17:24 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 17:24 120-82-114.6 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-18 (2002)Lab ID:92437876015 Collected:07/12/19 08:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 17:24 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 17:24 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 17:24 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 17:24 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 17:24 76-13-13.0 1.94
1,2,4-Trimethylbenzene 6.3 ug/m3 07/24/19 17:24 95-63-61.9 1.94
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 17:24 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 17:24 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 17:24 75-01-40.50 1.94
m&p-Xylene 28.1 ug/m3 07/24/19 17:24 179601-23-13.4 1.94
o-Xylene 8.5 ug/m3 07/24/19 17:24 95-47-61.7 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-17 (2001)Lab ID:92437876016 Collected:07/12/19 08:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone ND ug/m3 07/25/19 22:20 67-64-19.7 4.04
Benzene 34.8 ug/m3 07/25/19 22:20 71-43-21.3 4.04
Bromodichloromethane ND ug/m3 07/25/19 22:20 75-27-45.5 4.04
Bromoform ND ug/m3 07/25/19 22:20 75-25-221.2 4.04
Bromomethane ND ug/m3 07/25/19 22:20 74-83-93.2 4.04
1,3-Butadiene ND ug/m3 07/25/19 22:20 106-99-01.8 4.04
2-Butanone (MEK)ND ug/m3 07/25/19 22:20 78-93-312.1 4.04
Carbon disulfide 22.4 ug/m3 07/25/19 22:20 75-15-02.6 4.04
Carbon tetrachloride ND ug/m3 07/25/19 22:20 56-23-55.2 4.04
Chlorobenzene ND ug/m3 07/25/19 22:20 108-90-73.8 4.04
Chloroethane ND ug/m3 07/25/19 22:20 75-00-32.2 4.04
Chloroform 4.1 ug/m3 07/25/19 22:20 67-66-32.0 4.04
Chloromethane ND ug/m3 07/25/19 22:20 74-87-31.7 4.04
Cyclohexane ND ug/m3 07/25/19 22:20 110-82-77.1 4.04
Dibromochloromethane ND ug/m3 07/25/19 22:20 124-48-17.0 4.04
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 22:20 106-93-43.2 4.04
1,2-Dichlorobenzene ND ug/m3 07/25/19 22:20 95-50-14.9 4.04
1,3-Dichlorobenzene 17.7 ug/m3 07/25/19 22:20 541-73-14.9 4.04
1,4-Dichlorobenzene ND ug/m3 07/25/19 22:20 106-46-712.4 4.04
Dichlorodifluoromethane ND ug/m3 07/25/19 22:20 75-71-84.1 4.04
1,1-Dichloroethane ND ug/m3 07/25/19 22:20 75-34-33.3 4.04
1,2-Dichloroethane ND ug/m3 07/25/19 22:20 107-06-21.7 4.04
1,1-Dichloroethene ND ug/m3 07/25/19 22:20 75-35-43.3 4.04
cis-1,2-Dichloroethene ND ug/m3 07/25/19 22:20 156-59-23.3 4.04
trans-1,2-Dichloroethene ND ug/m3 07/25/19 22:20 156-60-53.3 4.04
1,2-Dichloropropane ND ug/m3 07/25/19 22:20 78-87-53.8 4.04
cis-1,3-Dichloropropene ND ug/m3 07/25/19 22:20 10061-01-53.7 4.04
trans-1,3-Dichloropropene ND ug/m3 07/25/19 22:20 10061-02-63.7 4.04
Dichlorotetrafluoroethane ND ug/m3 07/25/19 22:20 76-14-25.7 4.04
Ethyl acetate ND ug/m3 07/25/19 22:20 141-78-63.0 4.04
Ethylbenzene 18.3 ug/m3 07/25/19 22:20 100-41-43.6 4.04
4-Ethyltoluene ND ug/m3 07/25/19 22:20 622-96-810.1 4.04
n-Heptane 56.5 ug/m3 07/25/19 22:20 142-82-53.4 4.04
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 22:20 87-68-321.9 4.04
n-Hexane 160 ug/m3 07/25/19 22:20 110-54-32.9 4.04
2-Hexanone ND ug/m3 07/25/19 22:20 591-78-616.8 4.04
Methylene Chloride ND ug/m3 07/25/19 22:20 75-09-214.3 4.04
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 22:20 108-10-116.8 4.04
Methyl-tert-butyl ether ND ug/m3 07/25/19 22:20 1634-04-414.8 4.04
Naphthalene ND ug/m3 07/25/19 22:20 91-20-310.7 4.04
Propylene 1000 ug/m3 07/25/19 22:20 115-07-1 E1.4 4.04
Styrene ND ug/m3 07/25/19 22:20 100-42-53.5 4.04
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 22:20 79-34-52.8 4.04
Tetrachloroethene ND ug/m3 07/25/19 22:20 127-18-42.8 4.04
Tetrahydrofuran ND ug/m3 07/25/19 22:20 109-99-92.4 4.04
Toluene 98.9 ug/m3 07/25/19 22:20 108-88-33.1 4.04
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 22:20 120-82-130.5 4.04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-17 (2001)Lab ID:92437876016 Collected:07/12/19 08:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/25/19 22:20 71-55-64.5 4.04
1,1,2-Trichloroethane ND ug/m3 07/25/19 22:20 79-00-52.2 4.04
Trichloroethene ND ug/m3 07/25/19 22:20 79-01-62.2 4.04
Trichlorofluoromethane ND ug/m3 07/25/19 22:20 75-69-44.6 4.04
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 22:20 76-13-16.3 4.04
1,2,4-Trimethylbenzene 7.8 ug/m3 07/25/19 22:20 95-63-64.0 4.04
1,3,5-Trimethylbenzene ND ug/m3 07/25/19 22:20 108-67-84.0 4.04
Vinyl acetate ND ug/m3 07/25/19 22:20 108-05-42.9 4.04
Vinyl chloride ND ug/m3 07/25/19 22:20 75-01-41.1 4.04
m&p-Xylene 39.4 ug/m3 07/25/19 22:20 179601-23-17.2 4.04
o-Xylene 11.0 ug/m3 07/25/19 22:20 95-47-63.6 4.04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-16 (2147)Lab ID:92437876017 Collected:07/12/19 09:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone ND ug/m3 07/24/19 19:58 67-64-14.7 1.94
Benzene 15.6 ug/m3 07/24/19 19:58 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 19:58 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 19:58 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 19:58 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 19:58 106-99-00.87 1.94
2-Butanone (MEK)9.6 ug/m3 07/24/19 19:58 78-93-35.8 1.94
Carbon disulfide 13.1 ug/m3 07/24/19 19:58 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 19:58 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 19:58 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 19:58 75-00-31.0 1.94
Chloroform 1.0 ug/m3 07/24/19 19:58 67-66-30.96 1.94
Chloromethane ND ug/m3 07/24/19 19:58 74-87-30.81 1.94
Cyclohexane ND ug/m3 07/24/19 19:58 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 19:58 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 19:58 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 19:58 95-50-12.4 1.94
1,3-Dichlorobenzene 12.2 ug/m3 07/24/19 19:58 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 19:58 106-46-75.9 1.94
Dichlorodifluoromethane 2.4 ug/m3 07/24/19 19:58 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 19:58 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 19:58 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 19:58 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 19:58 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 19:58 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 19:58 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 19:58 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 19:58 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 19:58 76-14-22.8 1.94
Ethyl acetate 5.1 ug/m3 07/24/19 19:58 141-78-61.4 1.94
Ethylbenzene 7.8 ug/m3 07/24/19 19:58 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 19:58 622-96-84.8 1.94
n-Heptane 32.9 ug/m3 07/24/19 19:58 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 19:58 87-68-310.5 1.94
n-Hexane 107 ug/m3 07/24/19 19:58 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 19:58 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 19:58 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 19:58 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 19:58 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 19:58 91-20-35.2 1.94
Propylene 453 ug/m3 07/24/19 19:58 115-07-1 E0.68 1.94
Styrene 2.5 ug/m3 07/25/19 19:20 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 19:58 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 19:58 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 19:58 109-99-91.2 1.94
Toluene 52.6 ug/m3 07/24/19 19:58 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 19:58 120-82-114.6 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 36 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-16 (2147)Lab ID:92437876017 Collected:07/12/19 09:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 19:58 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 19:58 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 19:58 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 19:58 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 19:58 76-13-13.0 1.94
1,2,4-Trimethylbenzene 6.9 ug/m3 07/24/19 19:58 95-63-61.9 1.94
1,3,5-Trimethylbenzene 2.4 ug/m3 07/24/19 19:58 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 19:58 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 19:58 75-01-40.50 1.94
m&p-Xylene 25.7 ug/m3 07/24/19 19:58 179601-23-13.4 1.94
o-Xylene 7.9 ug/m3 07/24/19 19:58 95-47-61.7 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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9800 Kincey Ave. Suite 100
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Page 37 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-15 (3266)Lab ID:92437876018 Collected:07/12/19 09:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 44.2 ug/m3 07/25/19 21:19 67-64-15.3 2.19
Benzene 22.9 ug/m3 07/25/19 21:19 71-43-20.71 2.19
Bromodichloromethane ND ug/m3 07/25/19 21:19 75-27-43.0 2.19
Bromoform ND ug/m3 07/25/19 21:19 75-25-211.5 2.19
Bromomethane ND ug/m3 07/25/19 21:19 74-83-91.7 2.19
1,3-Butadiene ND ug/m3 07/25/19 21:19 106-99-00.99 2.19
2-Butanone (MEK)ND ug/m3 07/25/19 21:19 78-93-36.6 2.19
Carbon disulfide 6.3 ug/m3 07/25/19 21:19 75-15-01.4 2.19
Carbon tetrachloride ND ug/m3 07/25/19 21:19 56-23-52.8 2.19
Chlorobenzene ND ug/m3 07/25/19 21:19 108-90-72.0 2.19
Chloroethane 7.1 ug/m3 07/25/19 21:19 75-00-31.2 2.19
Chloroform 6.5 ug/m3 07/25/19 21:19 67-66-31.1 2.19
Chloromethane 13.3 ug/m3 07/25/19 21:19 74-87-30.92 2.19
Cyclohexane 13.8 ug/m3 07/25/19 21:19 110-82-73.8 2.19
Dibromochloromethane ND ug/m3 07/25/19 21:19 124-48-13.8 2.19
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 21:19 106-93-41.7 2.19
1,2-Dichlorobenzene ND ug/m3 07/25/19 21:19 95-50-12.7 2.19
1,3-Dichlorobenzene 12.3 ug/m3 07/25/19 21:19 541-73-12.7 2.19
1,4-Dichlorobenzene ND ug/m3 07/25/19 21:19 106-46-76.7 2.19
Dichlorodifluoromethane 2.9 ug/m3 07/25/19 21:19 75-71-82.2 2.19
1,1-Dichloroethane ND ug/m3 07/25/19 21:19 75-34-31.8 2.19
1,2-Dichloroethane ND ug/m3 07/25/19 21:19 107-06-20.90 2.19
1,1-Dichloroethene ND ug/m3 07/25/19 21:19 75-35-41.8 2.19
cis-1,2-Dichloroethene ND ug/m3 07/25/19 21:19 156-59-21.8 2.19
trans-1,2-Dichloroethene ND ug/m3 07/25/19 21:19 156-60-51.8 2.19
1,2-Dichloropropane ND ug/m3 07/25/19 21:19 78-87-52.1 2.19
cis-1,3-Dichloropropene ND ug/m3 07/25/19 21:19 10061-01-52.0 2.19
trans-1,3-Dichloropropene ND ug/m3 07/25/19 21:19 10061-02-62.0 2.19
Dichlorotetrafluoroethane ND ug/m3 07/25/19 21:19 76-14-23.1 2.19
Ethyl acetate 4.3 ug/m3 07/25/19 21:19 141-78-61.6 2.19
Ethylbenzene 12.0 ug/m3 07/25/19 21:19 100-41-41.9 2.19
4-Ethyltoluene ND ug/m3 07/25/19 21:19 622-96-85.5 2.19
n-Heptane 25.7 ug/m3 07/25/19 21:19 142-82-51.8 2.19
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 21:19 87-68-311.9 2.19
n-Hexane 42.7 ug/m3 07/25/19 21:19 110-54-31.6 2.19
2-Hexanone ND ug/m3 07/25/19 21:19 591-78-69.1 2.19
Methylene Chloride 14.2 ug/m3 07/25/19 21:19 75-09-27.7 2.19
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 21:19 108-10-19.1 2.19
Methyl-tert-butyl ether ND ug/m3 07/25/19 21:19 1634-04-48.0 2.19
Naphthalene ND ug/m3 07/25/19 21:19 91-20-35.8 2.19
Propylene 189 ug/m3 07/25/19 21:19 115-07-1 E0.77 2.19
Styrene ND ug/m3 07/25/19 21:19 100-42-51.9 2.19
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 21:19 79-34-51.5 2.19
Tetrachloroethene ND ug/m3 07/25/19 21:19 127-18-41.5 2.19
Tetrahydrofuran ND ug/m3 07/25/19 21:19 109-99-91.3 2.19
Toluene 92.6 ug/m3 07/25/19 21:19 108-88-31.7 2.19
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 21:19 120-82-116.5 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 38 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-15 (3266)Lab ID:92437876018 Collected:07/12/19 09:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/25/19 21:19 71-55-62.4 2.19
1,1,2-Trichloroethane ND ug/m3 07/25/19 21:19 79-00-51.2 2.19
Trichloroethene ND ug/m3 07/25/19 21:19 79-01-61.2 2.19
Trichlorofluoromethane ND ug/m3 07/25/19 21:19 75-69-42.5 2.19
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 21:19 76-13-13.4 2.19
1,2,4-Trimethylbenzene 8.3 ug/m3 07/25/19 21:19 95-63-62.2 2.19
1,3,5-Trimethylbenzene 3.2 ug/m3 07/25/19 21:19 108-67-82.2 2.19
Vinyl acetate ND ug/m3 07/25/19 21:19 108-05-41.6 2.19
Vinyl chloride 4.7 ug/m3 07/25/19 21:19 75-01-40.57 2.19
m&p-Xylene 41.5 ug/m3 07/25/19 21:19 179601-23-13.9 2.19
o-Xylene 11.4 ug/m3 07/25/19 21:19 95-47-61.9 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 39 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-10 (2788)Lab ID:92437876019 Collected:07/12/19 10:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 52.1 ug/m3 07/24/19 19:28 67-64-14.9 2.02
Benzene 25.3 ug/m3 07/24/19 19:28 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 19:28 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 19:28 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 19:28 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 19:28 106-99-00.91 2.02
2-Butanone (MEK)ND ug/m3 07/24/19 19:28 78-93-36.1 2.02
Carbon disulfide 10.1 ug/m3 07/24/19 19:28 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 19:28 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 19:28 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 19:28 75-00-31.1 2.02
Chloroform 2.2 ug/m3 07/24/19 19:28 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 19:28 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 19:28 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 19:28 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 19:28 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 19:28 95-50-12.5 2.02
1,3-Dichlorobenzene 23.6 ug/m3 07/24/19 19:28 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 19:28 106-46-76.2 2.02
Dichlorodifluoromethane 2.5 ug/m3 07/24/19 19:28 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 19:28 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 19:28 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 19:28 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 19:28 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 19:28 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 19:28 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 19:28 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 19:28 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 19:28 76-14-22.9 2.02
Ethyl acetate ND ug/m3 07/24/19 19:28 141-78-61.5 2.02
Ethylbenzene 17.6 ug/m3 07/24/19 19:28 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 19:28 622-96-85.0 2.02
n-Heptane 39.3 ug/m3 07/24/19 19:28 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 19:28 87-68-310.9 2.02
n-Hexane 78.4 ug/m3 07/24/19 19:28 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 19:28 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 19:28 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 19:28 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 19:28 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 19:28 91-20-35.4 2.02
Propylene 288 ug/m3 07/25/19 20:19 115-07-17.1 20.2
Styrene 405 ug/m3 07/25/19 20:19 100-42-517.5 20.2
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 19:28 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 19:28 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 19:28 109-99-91.2 2.02
Toluene 139 ug/m3 07/24/19 19:28 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 19:28 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-10 (2788)Lab ID:92437876019 Collected:07/12/19 10:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 19:28 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 19:28 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 19:28 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 19:28 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 19:28 76-13-13.2 2.02
1,2,4-Trimethylbenzene 10.8 ug/m3 07/24/19 19:28 95-63-62.0 2.02
1,3,5-Trimethylbenzene 4.6 ug/m3 07/24/19 19:28 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 19:28 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 19:28 75-01-40.53 2.02
m&p-Xylene 64.2 ug/m3 07/24/19 19:28 179601-23-13.6 2.02
o-Xylene 15.8 ug/m3 07/24/19 19:28 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 41 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-9 (2226)Lab ID:92437876020 Collected:07/12/19 10:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 53.1 ug/m3 07/24/19 20:28 67-64-15.1 2.1
Benzene 11.4 ug/m3 07/24/19 20:28 71-43-20.68 2.1
Bromodichloromethane ND ug/m3 07/24/19 20:28 75-27-42.9 2.1
Bromoform ND ug/m3 07/24/19 20:28 75-25-211.0 2.1
Bromomethane ND ug/m3 07/24/19 20:28 74-83-91.7 2.1
1,3-Butadiene ND ug/m3 07/24/19 20:28 106-99-00.94 2.1
2-Butanone (MEK)13.0 ug/m3 07/24/19 20:28 78-93-36.3 2.1
Carbon disulfide 3.3 ug/m3 07/24/19 20:28 75-15-01.3 2.1
Carbon tetrachloride ND ug/m3 07/24/19 20:28 56-23-52.7 2.1
Chlorobenzene ND ug/m3 07/24/19 20:28 108-90-72.0 2.1
Chloroethane ND ug/m3 07/24/19 20:28 75-00-31.1 2.1
Chloroform 3.7 ug/m3 07/24/19 20:28 67-66-31.0 2.1
Chloromethane 7.0 ug/m3 07/24/19 20:28 74-87-30.88 2.1
Cyclohexane 9.4 ug/m3 07/24/19 20:28 110-82-73.7 2.1
Dibromochloromethane ND ug/m3 07/24/19 20:28 124-48-13.6 2.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 20:28 106-93-41.6 2.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 20:28 95-50-12.6 2.1
1,3-Dichlorobenzene 18.0 ug/m3 07/24/19 20:28 541-73-12.6 2.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 20:28 106-46-76.4 2.1
Dichlorodifluoromethane 2.7 ug/m3 07/24/19 20:28 75-71-82.1 2.1
1,1-Dichloroethane ND ug/m3 07/24/19 20:28 75-34-31.7 2.1
1,2-Dichloroethane ND ug/m3 07/24/19 20:28 107-06-20.86 2.1
1,1-Dichloroethene ND ug/m3 07/24/19 20:28 75-35-41.7 2.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 20:28 156-59-21.7 2.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 20:28 156-60-51.7 2.1
1,2-Dichloropropane ND ug/m3 07/24/19 20:28 78-87-52.0 2.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 20:28 10061-01-51.9 2.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 20:28 10061-02-61.9 2.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 20:28 76-14-23.0 2.1
Ethyl acetate 4.3 ug/m3 07/24/19 20:28 141-78-61.5 2.1
Ethylbenzene 5.9 ug/m3 07/24/19 20:28 100-41-41.9 2.1
4-Ethyltoluene ND ug/m3 07/24/19 20:28 622-96-85.2 2.1
n-Heptane 13.1 ug/m3 07/24/19 20:28 142-82-51.7 2.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 20:28 87-68-311.4 2.1
n-Hexane 24.1 ug/m3 07/24/19 20:28 110-54-31.5 2.1
2-Hexanone ND ug/m3 07/24/19 20:28 591-78-68.7 2.1
Methylene Chloride ND ug/m3 07/24/19 20:28 75-09-27.4 2.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 20:28 108-10-18.7 2.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 20:28 1634-04-47.7 2.1
Naphthalene ND ug/m3 07/24/19 20:28 91-20-35.6 2.1
Propylene 77.9 ug/m3 07/24/19 20:28 115-07-10.74 2.1
Styrene 8.1 ug/m3 07/24/19 20:28 100-42-51.8 2.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 20:28 79-34-51.5 2.1
Tetrachloroethene ND ug/m3 07/24/19 20:28 127-18-41.4 2.1
Tetrahydrofuran ND ug/m3 07/24/19 20:28 109-99-91.3 2.1
Toluene 37.5 ug/m3 07/24/19 20:28 108-88-31.6 2.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 20:28 120-82-115.8 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-9 (2226)Lab ID:92437876020 Collected:07/12/19 10:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 20:28 71-55-62.3 2.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 20:28 79-00-51.2 2.1
Trichloroethene ND ug/m3 07/24/19 20:28 79-01-61.1 2.1
Trichlorofluoromethane ND ug/m3 07/24/19 20:28 75-69-42.4 2.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 20:28 76-13-13.3 2.1
1,2,4-Trimethylbenzene 6.1 ug/m3 07/24/19 20:28 95-63-62.1 2.1
1,3,5-Trimethylbenzene 2.1 ug/m3 07/24/19 20:28 108-67-82.1 2.1
Vinyl acetate ND ug/m3 07/24/19 20:28 108-05-41.5 2.1
Vinyl chloride 2.2 ug/m3 07/24/19 20:28 75-01-40.55 2.1
m&p-Xylene 19.1 ug/m3 07/24/19 20:28 179601-23-13.7 2.1
o-Xylene 6.1 ug/m3 07/24/19 20:28 95-47-61.9 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 43 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-11 (3182)Lab ID:92437876021 Collected:07/12/19 11:03 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 52.2 ug/m3 07/24/19 18:27 67-64-14.9 2.02
Benzene 0.95 ug/m3 07/24/19 18:27 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 18:27 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 18:27 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 18:27 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 18:27 106-99-00.91 2.02
2-Butanone (MEK)12.3 ug/m3 07/24/19 18:27 78-93-36.1 2.02
Carbon disulfide ND ug/m3 07/24/19 18:27 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 18:27 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 18:27 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 18:27 75-00-31.1 2.02
Chloroform ND ug/m3 07/24/19 18:27 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 18:27 74-87-30.85 2.02
Cyclohexane 6.6 ug/m3 07/24/19 18:27 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 18:27 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 18:27 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 18:27 95-50-12.5 2.02
1,3-Dichlorobenzene 26.1 ug/m3 07/24/19 18:27 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 18:27 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 18:27 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 18:27 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 18:27 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 18:27 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 18:27 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 18:27 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 18:27 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 18:27 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 18:27 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 18:27 76-14-22.9 2.02
Ethyl acetate 4.4 ug/m3 07/24/19 18:27 141-78-61.5 2.02
Ethylbenzene 3.1 ug/m3 07/24/19 18:27 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 18:27 622-96-85.0 2.02
n-Heptane ND ug/m3 07/24/19 18:27 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 18:27 87-68-310.9 2.02
n-Hexane ND ug/m3 07/24/19 18:27 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 18:27 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 18:27 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 18:27 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 18:27 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 18:27 91-20-35.4 2.02
Propylene ND ug/m3 07/24/19 18:27 115-07-10.71 2.02
Styrene 7.1 ug/m3 07/24/19 18:27 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 18:27 79-34-51.4 2.02
Tetrachloroethene 2.1 ug/m3 07/24/19 18:27 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 18:27 109-99-91.2 2.02
Toluene 9.2 ug/m3 07/24/19 18:27 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 18:27 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 44 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-11 (3182)Lab ID:92437876021 Collected:07/12/19 11:03 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 18:27 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 18:27 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 18:27 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 18:27 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 18:27 76-13-13.2 2.02
1,2,4-Trimethylbenzene 6.7 ug/m3 07/24/19 18:27 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 18:27 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 18:27 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 18:27 75-01-40.53 2.02
m&p-Xylene 11.1 ug/m3 07/24/19 18:27 179601-23-13.6 2.02
o-Xylene 4.7 ug/m3 07/24/19 18:27 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 45 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-13 (3065)Lab ID:92437876022 Collected:07/12/19 11:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 58.8 ug/m3 07/24/19 20:57 67-64-124.3 10.1
Benzene 28.2 ug/m3 07/24/19 20:57 71-43-23.3 10.1
Bromodichloromethane ND ug/m3 07/24/19 20:57 75-27-413.7 10.1
Bromoform ND ug/m3 07/24/19 20:57 75-25-253.0 10.1
Bromomethane ND ug/m3 07/24/19 20:57 74-83-98.0 10.1
1,3-Butadiene ND ug/m3 07/24/19 20:57 106-99-04.5 10.1
2-Butanone (MEK)ND ug/m3 07/24/19 20:57 78-93-330.3 10.1
Carbon disulfide 12.1 ug/m3 07/24/19 20:57 75-15-06.4 10.1
Carbon tetrachloride ND ug/m3 07/24/19 20:57 56-23-512.9 10.1
Chlorobenzene ND ug/m3 07/24/19 20:57 108-90-79.5 10.1
Chloroethane ND ug/m3 07/24/19 20:57 75-00-35.4 10.1
Chloroform 7.9 ug/m3 07/24/19 20:57 67-66-35.0 10.1
Chloromethane 8.9 ug/m3 07/24/19 20:57 74-87-34.2 10.1
Cyclohexane 20.6 ug/m3 07/24/19 20:57 110-82-717.7 10.1
Dibromochloromethane ND ug/m3 07/24/19 20:57 124-48-117.5 10.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 20:57 106-93-47.9 10.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 20:57 95-50-112.3 10.1
1,3-Dichlorobenzene 33.3 ug/m3 07/24/19 20:57 541-73-112.3 10.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 20:57 106-46-730.9 10.1
Dichlorodifluoromethane ND ug/m3 07/24/19 20:57 75-71-810.2 10.1
1,1-Dichloroethane ND ug/m3 07/24/19 20:57 75-34-38.3 10.1
1,2-Dichloroethane ND ug/m3 07/24/19 20:57 107-06-24.2 10.1
1,1-Dichloroethene ND ug/m3 07/24/19 20:57 75-35-48.1 10.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 20:57 156-59-28.1 10.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 20:57 156-60-58.1 10.1
1,2-Dichloropropane ND ug/m3 07/24/19 20:57 78-87-59.5 10.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 20:57 10061-01-59.3 10.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 20:57 10061-02-69.3 10.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 20:57 76-14-214.3 10.1
Ethyl acetate ND ug/m3 07/24/19 20:57 141-78-67.4 10.1
Ethylbenzene 28.4 ug/m3 07/24/19 20:57 100-41-48.9 10.1
4-Ethyltoluene ND ug/m3 07/24/19 20:57 622-96-825.2 10.1
n-Heptane 38.9 ug/m3 07/24/19 20:57 142-82-58.4 10.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 20:57 87-68-354.7 10.1
n-Hexane 59.6 ug/m3 07/24/19 20:57 110-54-37.2 10.1
2-Hexanone ND ug/m3 07/24/19 20:57 591-78-642.0 10.1
Methylene Chloride ND ug/m3 07/24/19 20:57 75-09-235.7 10.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 20:57 108-10-142.0 10.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 20:57 1634-04-437.0 10.1
Naphthalene ND ug/m3 07/24/19 20:57 91-20-326.9 10.1
Propylene 113 ug/m3 07/24/19 20:57 115-07-13.5 10.1
Styrene 204 ug/m3 07/24/19 20:57 100-42-58.7 10.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 20:57 79-34-57.0 10.1
Tetrachloroethene ND ug/m3 07/24/19 20:57 127-18-47.0 10.1
Tetrahydrofuran ND ug/m3 07/24/19 20:57 109-99-96.1 10.1
Toluene 152 ug/m3 07/24/19 20:57 108-88-37.7 10.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 20:57 120-82-176.2 10.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-13 (3065)Lab ID:92437876022 Collected:07/12/19 11:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 20:57 71-55-611.2 10.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 20:57 79-00-55.6 10.1
Trichloroethene ND ug/m3 07/24/19 20:57 79-01-65.5 10.1
Trichlorofluoromethane ND ug/m3 07/24/19 20:57 75-69-411.5 10.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 20:57 76-13-115.8 10.1
1,2,4-Trimethylbenzene 22.6 ug/m3 07/24/19 20:57 95-63-610.1 10.1
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 20:57 108-67-810.1 10.1
Vinyl acetate ND ug/m3 07/24/19 20:57 108-05-47.2 10.1
Vinyl chloride 6.9 ug/m3 07/24/19 20:57 75-01-42.6 10.1
m&p-Xylene 104 ug/m3 07/24/19 20:57 179601-23-117.9 10.1
o-Xylene 29.3 ug/m3 07/24/19 20:57 95-47-68.9 10.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-12 (2076)Lab ID:92437876023 Collected:07/12/19 11:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 51.1 ug/m3 07/25/19 21:50 67-64-19.7 4.04
Benzene 50.3 ug/m3 07/25/19 21:50 71-43-21.3 4.04
Bromodichloromethane ND ug/m3 07/25/19 21:50 75-27-45.5 4.04
Bromoform ND ug/m3 07/25/19 21:50 75-25-221.2 4.04
Bromomethane ND ug/m3 07/25/19 21:50 74-83-93.2 4.04
1,3-Butadiene ND ug/m3 07/25/19 21:50 106-99-01.8 4.04
2-Butanone (MEK)ND ug/m3 07/25/19 21:50 78-93-312.1 4.04
Carbon disulfide 7.0 ug/m3 07/25/19 21:50 75-15-02.6 4.04
Carbon tetrachloride ND ug/m3 07/25/19 21:50 56-23-55.2 4.04
Chlorobenzene ND ug/m3 07/25/19 21:50 108-90-73.8 4.04
Chloroethane 9.3 ug/m3 07/25/19 21:50 75-00-32.2 4.04
Chloroform 5.1 ug/m3 07/25/19 21:50 67-66-32.0 4.04
Chloromethane 58.2 ug/m3 07/25/19 21:50 74-87-31.7 4.04
Cyclohexane 21.2 ug/m3 07/25/19 21:50 110-82-77.1 4.04
Dibromochloromethane ND ug/m3 07/25/19 21:50 124-48-17.0 4.04
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 21:50 106-93-43.2 4.04
1,2-Dichlorobenzene ND ug/m3 07/25/19 21:50 95-50-14.9 4.04
1,3-Dichlorobenzene 29.3 ug/m3 07/25/19 21:50 541-73-14.9 4.04
1,4-Dichlorobenzene ND ug/m3 07/25/19 21:50 106-46-712.4 4.04
Dichlorodifluoromethane ND ug/m3 07/25/19 21:50 75-71-84.1 4.04
1,1-Dichloroethane ND ug/m3 07/25/19 21:50 75-34-33.3 4.04
1,2-Dichloroethane ND ug/m3 07/25/19 21:50 107-06-21.7 4.04
1,1-Dichloroethene ND ug/m3 07/25/19 21:50 75-35-43.3 4.04
cis-1,2-Dichloroethene ND ug/m3 07/25/19 21:50 156-59-23.3 4.04
trans-1,2-Dichloroethene ND ug/m3 07/25/19 21:50 156-60-53.3 4.04
1,2-Dichloropropane ND ug/m3 07/25/19 21:50 78-87-53.8 4.04
cis-1,3-Dichloropropene ND ug/m3 07/25/19 21:50 10061-01-53.7 4.04
trans-1,3-Dichloropropene ND ug/m3 07/25/19 21:50 10061-02-63.7 4.04
Dichlorotetrafluoroethane ND ug/m3 07/25/19 21:50 76-14-25.7 4.04
Ethyl acetate ND ug/m3 07/25/19 21:50 141-78-63.0 4.04
Ethylbenzene 36.3 ug/m3 07/25/19 21:50 100-41-43.6 4.04
4-Ethyltoluene ND ug/m3 07/25/19 21:50 622-96-810.1 4.04
n-Heptane 30.6 ug/m3 07/25/19 21:50 142-82-53.4 4.04
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 21:50 87-68-321.9 4.04
n-Hexane 72.5 ug/m3 07/25/19 21:50 110-54-32.9 4.04
2-Hexanone ND ug/m3 07/25/19 21:50 591-78-616.8 4.04
Methylene Chloride 16.9 ug/m3 07/25/19 21:50 75-09-214.3 4.04
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 21:50 108-10-116.8 4.04
Methyl-tert-butyl ether ND ug/m3 07/25/19 21:50 1634-04-414.8 4.04
Naphthalene ND ug/m3 07/25/19 21:50 91-20-310.7 4.04
Propylene 606 ug/m3 07/25/19 21:50 115-07-1 E1.4 4.04
Styrene ND ug/m3 07/25/19 21:50 100-42-53.5 4.04
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 21:50 79-34-52.8 4.04
Tetrachloroethene ND ug/m3 07/25/19 21:50 127-18-42.8 4.04
Tetrahydrofuran ND ug/m3 07/25/19 21:50 109-99-92.4 4.04
Toluene 142 ug/m3 07/25/19 21:50 108-88-33.1 4.04
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 21:50 120-82-130.5 4.04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-12 (2076)Lab ID:92437876023 Collected:07/12/19 11:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/25/19 21:50 71-55-64.5 4.04
1,1,2-Trichloroethane ND ug/m3 07/25/19 21:50 79-00-52.2 4.04
Trichloroethene ND ug/m3 07/25/19 21:50 79-01-62.2 4.04
Trichlorofluoromethane ND ug/m3 07/25/19 21:50 75-69-44.6 4.04
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 21:50 76-13-16.3 4.04
1,2,4-Trimethylbenzene 19.4 ug/m3 07/25/19 21:50 95-63-64.0 4.04
1,3,5-Trimethylbenzene 8.5 ug/m3 07/25/19 21:50 108-67-84.0 4.04
Vinyl acetate ND ug/m3 07/25/19 21:50 108-05-42.9 4.04
Vinyl chloride 24.8 ug/m3 07/25/19 21:50 75-01-41.1 4.04
m&p-Xylene 92.1 ug/m3 07/25/19 21:50 179601-23-17.2 4.04
o-Xylene 25.2 ug/m3 07/25/19 21:50 95-47-63.6 4.04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 49 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:DUP-1 (3175)Lab ID:92437876025 Collected:07/12/19 00:06 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 62.1 ug/m3 07/24/19 18:57 67-64-15.1 2.1
Benzene 1.1 ug/m3 07/24/19 18:57 71-43-20.68 2.1
Bromodichloromethane ND ug/m3 07/24/19 18:57 75-27-42.9 2.1
Bromoform ND ug/m3 07/24/19 18:57 75-25-211.0 2.1
Bromomethane ND ug/m3 07/24/19 18:57 74-83-91.7 2.1
1,3-Butadiene ND ug/m3 07/24/19 18:57 106-99-00.94 2.1
2-Butanone (MEK)16.3 ug/m3 07/24/19 18:57 78-93-36.3 2.1
Carbon disulfide ND ug/m3 07/24/19 18:57 75-15-01.3 2.1
Carbon tetrachloride ND ug/m3 07/24/19 18:57 56-23-52.7 2.1
Chlorobenzene ND ug/m3 07/24/19 18:57 108-90-72.0 2.1
Chloroethane ND ug/m3 07/24/19 18:57 75-00-31.1 2.1
Chloroform ND ug/m3 07/24/19 18:57 67-66-31.0 2.1
Chloromethane ND ug/m3 07/24/19 18:57 74-87-30.88 2.1
Cyclohexane 6.0 ug/m3 07/24/19 18:57 110-82-73.7 2.1
Dibromochloromethane ND ug/m3 07/24/19 18:57 124-48-13.6 2.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 18:57 106-93-41.6 2.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 18:57 95-50-12.6 2.1
1,3-Dichlorobenzene 19.3 ug/m3 07/24/19 18:57 541-73-12.6 2.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 18:57 106-46-76.4 2.1
Dichlorodifluoromethane ND ug/m3 07/24/19 18:57 75-71-82.1 2.1
1,1-Dichloroethane ND ug/m3 07/24/19 18:57 75-34-31.7 2.1
1,2-Dichloroethane ND ug/m3 07/24/19 18:57 107-06-20.86 2.1
1,1-Dichloroethene ND ug/m3 07/24/19 18:57 75-35-41.7 2.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 18:57 156-59-21.7 2.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 18:57 156-60-51.7 2.1
1,2-Dichloropropane ND ug/m3 07/24/19 18:57 78-87-52.0 2.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 18:57 10061-01-51.9 2.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 18:57 10061-02-61.9 2.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 18:57 76-14-23.0 2.1
Ethyl acetate ND ug/m3 07/24/19 18:57 141-78-61.5 2.1
Ethylbenzene 3.2 ug/m3 07/24/19 18:57 100-41-41.9 2.1
4-Ethyltoluene ND ug/m3 07/24/19 18:57 622-96-85.2 2.1
n-Heptane ND ug/m3 07/24/19 18:57 142-82-51.7 2.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 18:57 87-68-311.4 2.1
n-Hexane ND ug/m3 07/24/19 18:57 110-54-31.5 2.1
2-Hexanone ND ug/m3 07/24/19 18:57 591-78-68.7 2.1
Methylene Chloride ND ug/m3 07/24/19 18:57 75-09-27.4 2.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 18:57 108-10-18.7 2.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 18:57 1634-04-47.7 2.1
Naphthalene ND ug/m3 07/24/19 18:57 91-20-35.6 2.1
Propylene ND ug/m3 07/24/19 18:57 115-07-10.74 2.1
Styrene ND ug/m3 07/24/19 18:57 100-42-51.8 2.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 18:57 79-34-51.5 2.1
Tetrachloroethene ND ug/m3 07/24/19 18:57 127-18-41.4 2.1
Tetrahydrofuran ND ug/m3 07/24/19 18:57 109-99-91.3 2.1
Toluene 9.9 ug/m3 07/24/19 18:57 108-88-31.6 2.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 18:57 120-82-115.8 2.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 50 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:DUP-1 (3175)Lab ID:92437876025 Collected:07/12/19 00:06 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 18:57 71-55-62.3 2.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 18:57 79-00-51.2 2.1
Trichloroethene ND ug/m3 07/24/19 18:57 79-01-61.1 2.1
Trichlorofluoromethane ND ug/m3 07/24/19 18:57 75-69-42.4 2.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 18:57 76-13-13.3 2.1
1,2,4-Trimethylbenzene 6.4 ug/m3 07/24/19 18:57 95-63-62.1 2.1
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 18:57 108-67-82.1 2.1
Vinyl acetate ND ug/m3 07/24/19 18:57 108-05-41.5 2.1
Vinyl chloride ND ug/m3 07/24/19 18:57 75-01-40.55 2.1
m&p-Xylene 11.5 ug/m3 07/24/19 18:57 179601-23-13.7 2.1
o-Xylene 5.0 ug/m3 07/24/19 18:57 95-47-61.9 2.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 51 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-14 (3527) re-test Lab ID:92437876026 Collected:07/19/19 15:20 Received:07/20/19 09:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone ND ug/m3 07/25/19 22:50 67-64-181.0 33.6
Benzene ND ug/m3 07/25/19 22:50 71-43-210.9 33.6
Bromodichloromethane ND ug/m3 07/25/19 22:50 75-27-445.7 33.6
Bromoform ND ug/m3 07/25/19 22:50 75-25-217633.6
Bromomethane ND ug/m3 07/25/19 22:50 74-83-926.5 33.6
1,3-Butadiene ND ug/m3 07/25/19 22:50 106-99-015.1 33.6
2-Butanone (MEK)ND ug/m3 07/25/19 22:50 78-93-310133.6
Carbon disulfide ND ug/m3 07/25/19 22:50 75-15-021.3 33.6
Carbon tetrachloride ND ug/m3 07/25/19 22:50 56-23-543.0 33.6
Chlorobenzene ND ug/m3 07/25/19 22:50 108-90-731.4 33.6
Chloroethane ND ug/m3 07/25/19 22:50 75-00-318.0 33.6
Chloroform ND ug/m3 07/25/19 22:50 67-66-316.7 33.6
Chloromethane ND ug/m3 07/25/19 22:50 74-87-314.1 33.6
Cyclohexane ND ug/m3 07/25/19 22:50 110-82-758.8 33.6
Dibromochloromethane ND ug/m3 07/25/19 22:50 124-48-158.1 33.6
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 22:50 106-93-426.2 33.6
1,2-Dichlorobenzene ND ug/m3 07/25/19 22:50 95-50-141.0 33.6
1,3-Dichlorobenzene ND ug/m3 07/25/19 22:50 541-73-141.0 33.6
1,4-Dichlorobenzene ND ug/m3 07/25/19 22:50 106-46-710333.6
Dichlorodifluoromethane ND ug/m3 07/25/19 22:50 75-71-833.9 33.6
1,1-Dichloroethane ND ug/m3 07/25/19 22:50 75-34-327.7 33.6
1,2-Dichloroethane ND ug/m3 07/25/19 22:50 107-06-213.8 33.6
1,1-Dichloroethene ND ug/m3 07/25/19 22:50 75-35-427.1 33.6
cis-1,2-Dichloroethene ND ug/m3 07/25/19 22:50 156-59-227.1 33.6
trans-1,2-Dichloroethene ND ug/m3 07/25/19 22:50 156-60-527.1 33.6
1,2-Dichloropropane ND ug/m3 07/25/19 22:50 78-87-531.6 33.6
cis-1,3-Dichloropropene ND ug/m3 07/25/19 22:50 10061-01-531.0 33.6
trans-1,3-Dichloropropene ND ug/m3 07/25/19 22:50 10061-02-631.0 33.6
Dichlorotetrafluoroethane ND ug/m3 07/25/19 22:50 76-14-247.7 33.6
Ethyl acetate ND ug/m3 07/25/19 22:50 141-78-624.6 33.6
Ethylbenzene 38.7 ug/m3 07/25/19 22:50 100-41-429.7 33.6
4-Ethyltoluene ND ug/m3 07/25/19 22:50 622-96-884.0 33.6
n-Heptane ND ug/m3 07/25/19 22:50 142-82-528.0 33.6
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 22:50 87-68-318233.6
n-Hexane ND ug/m3 07/25/19 22:50 110-54-324.1 33.6
2-Hexanone ND ug/m3 07/25/19 22:50 591-78-614033.6
Methylene Chloride ND ug/m3 07/25/19 22:50 75-09-211933.6
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 22:50 108-10-114033.6
Methyl-tert-butyl ether ND ug/m3 07/25/19 22:50 1634-04-412333.6
Naphthalene ND ug/m3 07/25/19 22:50 91-20-389.4 33.6
Propylene 85.8 ug/m3 07/25/19 22:50 115-07-111.8 33.6
Styrene ND ug/m3 07/25/19 22:50 100-42-529.1 33.6
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 22:50 79-34-523.5 33.6
Tetrachloroethene ND ug/m3 07/25/19 22:50 127-18-423.2 33.6
Tetrahydrofuran ND ug/m3 07/25/19 22:50 109-99-920.2 33.6
Toluene 118 ug/m3 07/25/19 22:50 108-88-325.7 33.6
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 22:50 120-82-125333.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 52 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92437876
RTP Flex
Sample:SG-14 (3527) re-test Lab ID:92437876026 Collected:07/19/19 15:20 Received:07/20/19 09:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/25/19 22:50 71-55-637.3 33.6
1,1,2-Trichloroethane ND ug/m3 07/25/19 22:50 79-00-518.6 33.6
Trichloroethene ND ug/m3 07/25/19 22:50 79-01-618.3 33.6
Trichlorofluoromethane ND ug/m3 07/25/19 22:50 75-69-438.3 33.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 22:50 76-13-152.4 33.6
1,2,4-Trimethylbenzene 141 ug/m3 07/25/19 22:50 95-63-633.6 33.6
1,3,5-Trimethylbenzene 62.1 ug/m3 07/25/19 22:50 108-67-833.6 33.6
Vinyl acetate ND ug/m3 07/25/19 22:50 108-05-424.1 33.6
Vinyl chloride ND ug/m3 07/25/19 22:50 75-01-48.7 33.6
m&p-Xylene 182 ug/m3 07/25/19 22:50 179601-23-159.5 33.6
o-Xylene 63.8 ug/m3 07/25/19 22:50 95-47-629.7 33.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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[phone]
Page 53 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621628
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876002, 92437876003, 92437876004, 92437876005, 92437876006, 92437876007, 92437876008,
92437876009, 92437876010, 92437876011, 92437876012, 92437876014, 92437876015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355758
Associated Lab Samples:92437876002, 92437876003, 92437876004, 92437876005, 92437876006, 92437876007, 92437876008,
92437876009, 92437876010, 92437876011, 92437876012, 92437876014, 92437876015
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 07/24/19 08:59
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 07/24/19 08:59
1,1,2-Trichloroethane ug/m3 ND 0.56 07/24/19 08:59
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 07/24/19 08:59
1,1-Dichloroethane ug/m3 ND 0.82 07/24/19 08:59
1,1-Dichloroethene ug/m3 ND 0.81 07/24/19 08:59
1,2,4-Trichlorobenzene ug/m3 ND 7.5 07/24/19 08:59
1,2,4-Trimethylbenzene ug/m3 ND 1.0 07/24/19 08:59
1,2-Dibromoethane (EDB)ug/m3 ND 0.78 07/24/19 08:59
1,2-Dichlorobenzene ug/m3 ND 1.2 07/24/19 08:59
1,2-Dichloroethane ug/m3 ND 0.41 07/24/19 08:59
1,2-Dichloropropane ug/m3 ND 0.94 07/24/19 08:59
1,3,5-Trimethylbenzene ug/m3 ND 1.0 07/24/19 08:59
1,3-Butadiene ug/m3 ND 0.45 07/24/19 08:59
1,3-Dichlorobenzene ug/m3 ND 1.2 07/24/19 08:59
1,4-Dichlorobenzene ug/m3 ND 3.1 07/24/19 08:59
2-Butanone (MEK)ug/m3 ND 3.0 07/24/19 08:59
2-Hexanone ug/m3 ND 4.2 07/24/19 08:59
4-Ethyltoluene ug/m3 ND 2.5 07/24/19 08:59
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 07/24/19 08:59
Acetone ug/m3 ND 2.4 07/24/19 08:59
Benzene ug/m3 ND 0.32 07/24/19 08:59
Bromodichloromethane ug/m3 ND 1.4 07/24/19 08:59
Bromoform ug/m3 ND 5.2 07/24/19 08:59
Bromomethane ug/m3 ND 0.79 07/24/19 08:59
Carbon disulfide ug/m3 ND 0.63 07/24/19 08:59
Carbon tetrachloride ug/m3 ND 1.3 07/24/19 08:59
Chlorobenzene ug/m3 ND 0.94 07/24/19 08:59
Chloroethane ug/m3 ND 0.54 07/24/19 08:59
Chloroform ug/m3 ND 0.50 07/24/19 08:59
Chloromethane ug/m3 ND 0.42 07/24/19 08:59
cis-1,2-Dichloroethene ug/m3 ND 0.81 07/24/19 08:59
cis-1,3-Dichloropropene ug/m3 ND 0.92 07/24/19 08:59
Cyclohexane ug/m3 ND 1.8 07/24/19 08:59
Dibromochloromethane ug/m3 ND 1.7 07/24/19 08:59
Dichlorodifluoromethane ug/m3 ND 1.0 07/24/19 08:59
Dichlorotetrafluoroethane ug/m3 ND 1.4 07/24/19 08:59
Ethyl acetate ug/m3 ND 0.73 07/24/19 08:59
Ethylbenzene ug/m3 ND 0.88 07/24/19 08:59
Hexachloro-1,3-butadiene ug/m3 ND 5.4 07/24/19 08:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355758
Associated Lab Samples:92437876002, 92437876003, 92437876004, 92437876005, 92437876006, 92437876007, 92437876008,
92437876009, 92437876010, 92437876011, 92437876012, 92437876014, 92437876015
Matrix:Air
Analyzed
m&p-Xylene ug/m3 ND 1.8 07/24/19 08:59
Methyl-tert-butyl ether ug/m3 ND 3.7 07/24/19 08:59
Methylene Chloride ug/m3 ND 3.5 07/24/19 08:59
n-Heptane ug/m3 ND 0.83 07/24/19 08:59
n-Hexane ug/m3 ND 0.72 07/24/19 08:59
Naphthalene ug/m3 ND 2.7 07/24/19 08:59
o-Xylene ug/m3 ND 0.88 07/24/19 08:59
Propylene ug/m3 ND 0.35 07/24/19 08:59
Styrene ug/m3 ND 0.87 07/24/19 08:59
Tetrachloroethene ug/m3 ND 0.69 07/24/19 08:59
Tetrahydrofuran ug/m3 ND 0.60 07/24/19 08:59
Toluene ug/m3 ND 0.77 07/24/19 08:59
trans-1,2-Dichloroethene ug/m3 ND 0.81 07/24/19 08:59
trans-1,3-Dichloropropene ug/m3 ND 0.92 07/24/19 08:59
Trichloroethene ug/m3 ND 0.55 07/24/19 08:59
Trichlorofluoromethane ug/m3 ND 1.1 07/24/19 08:59
Vinyl acetate ug/m3 ND 0.72 07/24/19 08:59
Vinyl chloride ug/m3 ND 0.26 07/24/19 08:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355759LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 54.355.5 98 70-130
1,1,2,2-Tetrachloroethane ug/m3 73.769.8 106 70-132
1,1,2-Trichloroethane ug/m3 54.555.5 98 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 75.777.9 97 70-130
1,1-Dichloroethane ug/m3 39.341.1 96 70-130
1,1-Dichloroethene ug/m3 39.140.3 97 70-130
1,2,4-Trichlorobenzene ug/m3 75.275.4 100 56-130
1,2,4-Trimethylbenzene ug/m3 54.550 109 70-134
1,2-Dibromoethane (EDB)ug/m3 78.878.1 101 70-130
1,2-Dichlorobenzene ug/m3 65.561.1 107 70-132
1,2-Dichloroethane ug/m3 39.441.1 96 70-130
1,2-Dichloropropane ug/m3 44.547 95 70-130
1,3,5-Trimethylbenzene ug/m3 49.050 98 70-132
1,3-Butadiene ug/m3 21.822.5 97 65-130
1,3-Dichlorobenzene ug/m3 64.861.1 106 70-137
1,4-Dichlorobenzene ug/m3 66.361.1 108 70-134
2-Butanone (MEK)ug/m3 26.330 88 70-130
2-Hexanone ug/m3 41.241.6 99 70-135
4-Ethyltoluene ug/m3 53.350 107 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 42.141.6 101 70-131
Acetone ug/m3 107121 89 67-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355759LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/m3 34.932.5 107 70-130
Bromodichloromethane ug/m3 67.868.1 100 70-130
Bromoform ug/m3 104105 99 70-132
Bromomethane ug/m3 37.939.5 96 69-130
Carbon disulfide ug/m3 31.131.6 98 56-137
Carbon tetrachloride ug/m3 62.264 97 66-131
Chlorobenzene ug/m3 45.246.8 97 70-130
Chloroethane ug/m3 24.026.8 90 70-130
Chloroform ug/m3 48.049.6 97 70-130
Chloromethane ug/m3 19.821 94 66-130
cis-1,2-Dichloroethene ug/m3 38.740.3 96 70-130
cis-1,3-Dichloropropene ug/m3 45.746.1 99 70-133
Cyclohexane ug/m3 33.335 95 68-132
Dibromochloromethane ug/m3 89.486.6 103 70-130
Dichlorodifluoromethane ug/m3 47.450.3 94 70-130
Dichlorotetrafluoroethane ug/m3 68.471 96 70-130
Ethyl acetate ug/m3 34.836.6 95 69-130
Ethylbenzene ug/m3 41.744.1 94 67-131
Hexachloro-1,3-butadiene ug/m3 113108 105 66-137
m&p-Xylene ug/m3 82.188.3 93 70-132
Methyl-tert-butyl ether ug/m3 35.236.6 96 70-130
Methylene Chloride ug/m3 161177 91 65-130
n-Heptane ug/m3 38.141.7 91 65-130
n-Hexane ug/m3 32.535.8 91 66-130
Naphthalene ug/m3 52.453.3 98 56-130
o-Xylene ug/m3 41.744.1 95 70-130
Propylene ug/m3 15.517.5 89 67-130
Styrene ug/m3 46.943.3 108 69-136
Tetrachloroethene ug/m3 75.068.9 109 70-130
Tetrahydrofuran ug/m3 27.730 92 68-131
Toluene ug/m3 36.238.3 94 70-130
trans-1,2-Dichloroethene ug/m3 38.640.3 96 70-130
trans-1,3-Dichloropropene ug/m3 46.346.1 100 70-134
Trichloroethene ug/m3 58.954.6 108 70-130
Trichlorofluoromethane ug/m3 53.557.1 94 65-130
Vinyl acetate ug/m3 33.135.8 92 61-133
Vinyl chloride ug/m3 24.126 93 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484068001
3357274SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484068001
3357274SAMPLE DUPLICATE:
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 42.9 242.1
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 11.2 410.7
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 3.0 23.1
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 6.2 45.9
2-Hexanone ug/m3 1.7JND
4-Ethyltoluene ug/m3 12.0 1810.0
4-Methyl-2-pentanone (MIBK)ug/m3 3.5JND
Acetone ug/m3 21.8 021.8
Benzene ug/m3 5.0 54.7
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.3 02.3
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 19.2 418.5
Chloromethane ug/m3 .45JND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 3.9 73.6
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.5 12.5
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 11.6 111.4
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 56.3 156.5
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 2.9JND
n-Heptane ug/m3 4.3 64.0
n-Hexane ug/m3 6.9 66.5
Naphthalene ug/m3 5.1 54.8
o-Xylene ug/m3 19.1 118.9
Propylene ug/m3 85.4 E185.9
Styrene ug/m3 3.0 82.7
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 3.0 33.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 57 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484068001
3357274SAMPLE DUPLICATE:
Toluene ug/m3 42.6 142.9
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.5JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
10484068002
3357275SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 24.4 224.8
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 6.1 86.6
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 1.8JND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 5.3JND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 6.9 27.1
4-Methyl-2-pentanone (MIBK)ug/m3 2.2JND
Acetone ug/m3 22.0 222.6
Benzene ug/m3 4.5 24.6
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.6 112.9
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 4.0 43.8
Chloromethane ug/m3 .65JND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 2.7JND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 58 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484068002
3357275SAMPLE DUPLICATE:
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 4.5 14.6
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 8.7 39.0
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 41.1 342.2
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 6.9ND
n-Heptane ug/m3 2.7 62.6
n-Hexane ug/m3 4.2 14.1
Naphthalene ug/m3 3.7JND
o-Xylene ug/m3 14.3 415.0
Propylene ug/m3 29.3 430.5
Styrene ug/m3 2.3 22.2
Tetrachloroethene ug/m3 1.2JND
Tetrahydrofuran ug/m3 2.2 22.2
Toluene ug/m3 28.8 129.0
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.3JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Huntersville, NC 28078
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Page 59 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621640
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355839
Associated Lab Samples:92437876001
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 0.56 07/24/19 09:54
1,1,2,2-Tetrachloroethane ug/m3 ND 0.35 07/24/19 09:54
1,1,2-Trichloroethane ug/m3 ND 0.28 07/24/19 09:54
1,1,2-Trichlorotrifluoroethane ug/m3 ND 0.78 07/24/19 09:54
1,1-Dichloroethane ug/m3 ND 0.41 07/24/19 09:54
1,1-Dichloroethene ug/m3 ND 0.40 07/24/19 09:54
1,2,4-Trichlorobenzene ug/m3 ND 3.8 07/24/19 09:54
1,2,4-Trimethylbenzene ug/m3 ND 0.50 07/24/19 09:54
1,2-Dibromoethane (EDB)ug/m3 ND 0.39 07/24/19 09:54
1,2-Dichlorobenzene ug/m3 ND 0.61 07/24/19 09:54
1,2-Dichloroethane ug/m3 ND 0.21 07/24/19 09:54
1,2-Dichloropropane ug/m3 ND 0.47 07/24/19 09:54
1,3,5-Trimethylbenzene ug/m3 ND 0.50 07/24/19 09:54
1,3-Butadiene ug/m3 ND 0.22 07/24/19 09:54
1,3-Dichlorobenzene ug/m3 ND 0.61 07/24/19 09:54
1,4-Dichlorobenzene ug/m3 ND 1.5 07/24/19 09:54
2-Butanone (MEK)ug/m3 ND 1.5 07/24/19 09:54
2-Hexanone ug/m3 ND 2.1 07/24/19 09:54
4-Ethyltoluene ug/m3 ND 1.2 07/24/19 09:54
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 07/24/19 09:54
Acetone ug/m3 ND 1.2 07/24/19 09:54
Benzene ug/m3 ND 0.16 07/24/19 09:54
Bromodichloromethane ug/m3 ND 0.68 07/24/19 09:54
Bromoform ug/m3 ND 2.6 07/24/19 09:54
Bromomethane ug/m3 ND 0.39 07/24/19 09:54
Carbon disulfide ug/m3 ND 0.32 07/24/19 09:54
Carbon tetrachloride ug/m3 ND 0.64 07/24/19 09:54
Chlorobenzene ug/m3 ND 0.47 07/24/19 09:54
Chloroethane ug/m3 ND 0.27 07/24/19 09:54
Chloroform ug/m3 ND 0.25 07/24/19 09:54
Chloromethane ug/m3 ND 0.21 07/24/19 09:54
cis-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 09:54
cis-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 09:54
Cyclohexane ug/m3 ND 0.88 07/24/19 09:54
Dibromochloromethane ug/m3 ND 0.86 07/24/19 09:54
Dichlorodifluoromethane ug/m3 ND 0.50 07/24/19 09:54
Dichlorotetrafluoroethane ug/m3 ND 0.71 07/24/19 09:54
Ethyl acetate ug/m3 ND 0.37 07/24/19 09:54
Ethylbenzene ug/m3 ND 0.44 07/24/19 09:54
Hexachloro-1,3-butadiene ug/m3 ND 2.7 07/24/19 09:54
m&p-Xylene ug/m3 ND 0.88 07/24/19 09:54
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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9800 Kincey Ave. Suite 100
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Page 60 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355839
Associated Lab Samples:92437876001
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 1.8 07/24/19 09:54
Methylene Chloride ug/m3 ND 1.8 07/24/19 09:54
n-Heptane ug/m3 ND 0.42 07/24/19 09:54
n-Hexane ug/m3 ND 0.36 07/24/19 09:54
Naphthalene ug/m3 ND 1.3 07/24/19 09:54
o-Xylene ug/m3 ND 0.44 07/24/19 09:54
Propylene ug/m3 ND 0.18 07/24/19 09:54
Styrene ug/m3 ND 0.43 07/24/19 09:54
Tetrachloroethene ug/m3 ND 0.34 07/24/19 09:54
Tetrahydrofuran ug/m3 ND 0.30 07/24/19 09:54
Toluene ug/m3 ND 0.38 07/24/19 09:54
trans-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 09:54
trans-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 09:54
Trichloroethene ug/m3 ND 0.27 07/24/19 09:54
Trichlorofluoromethane ug/m3 ND 0.57 07/24/19 09:54
Vinyl acetate ug/m3 ND 0.89 MN07/24/19 09:54
Vinyl chloride ug/m3 ND 0.13 07/24/19 09:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355840LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 62.755.5 113 70-130
1,1,2,2-Tetrachloroethane ug/m3 72.569.8 104 70-132
1,1,2-Trichloroethane ug/m3 58.755.5 106 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 86.177.9 111 70-130
1,1-Dichloroethane ug/m3 44.941.1 109 70-130
1,1-Dichloroethene ug/m3 43.840.3 109 70-130
1,2,4-Trichlorobenzene ug/m3 73.875.4 98 56-130
1,2,4-Trimethylbenzene ug/m3 56.950 114 70-134
1,2-Dibromoethane (EDB)ug/m3 89.278.1 114 70-130
1,2-Dichlorobenzene ug/m3 70.561.1 115 70-132
1,2-Dichloroethane ug/m3 46.641.1 113 70-130
1,2-Dichloropropane ug/m3 54.747 116 70-130
1,3,5-Trimethylbenzene ug/m3 56.750 113 70-132
1,3-Butadiene ug/m3 26.122.5 116 65-130
1,3-Dichlorobenzene ug/m3 71.061.1 116 70-137
1,4-Dichlorobenzene ug/m3 72.461.1 118 70-134
2-Butanone (MEK)ug/m3 30.630 102 70-130
2-Hexanone ug/m3 46.441.6 111 70-135
4-Ethyltoluene ug/m3 57.650 115 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 44.741.6 107 70-131
Acetone ug/m3 117121 97 67-130
Benzene ug/m3 35.132.5 108 70-130
Bromodichloromethane ug/m3 77.068.1 113 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355840LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 111105 106 70-132
Bromomethane ug/m3 46.239.5 117 69-130
Carbon disulfide ug/m3 35.231.6 111 56-137
Carbon tetrachloride ug/m3 71.264 111 66-131
Chlorobenzene ug/m3 51.846.8 111 70-130
Chloroethane ug/m3 33.926.8 126 70-130
Chloroform ug/m3 55.149.6 111 70-130
Chloromethane ug/m3 24.421 116 66-130
cis-1,2-Dichloroethene ug/m3 43.140.3 107 70-130
cis-1,3-Dichloropropene ug/m3 51.946.1 112 70-133
Cyclohexane ug/m3 37.635 107 68-132
Dibromochloromethane ug/m3 10586.6 121 70-130
Dichlorodifluoromethane ug/m3 56.650.3 113 70-130
Dichlorotetrafluoroethane ug/m3 82.371 116 70-130
Ethyl acetate ug/m3 41.536.6 113 69-130
Ethylbenzene ug/m3 51.544.1 117 67-131
Hexachloro-1,3-butadiene ug/m3 128108 118 66-137
m&p-Xylene ug/m3 10488.3 117 70-132
Methyl-tert-butyl ether ug/m3 40.736.6 111 70-130
Methylene Chloride ug/m3 184177 104 65-130
n-Heptane ug/m3 44.341.7 106 65-130
n-Hexane ug/m3 38.735.8 108 66-130
Naphthalene ug/m3 51.253.3 96 56-130
o-Xylene ug/m3 50.944.1 115 70-130
Propylene ug/m3 18.017.5 103 67-130
Styrene ug/m3 49.443.3 114 69-136
Tetrachloroethene ug/m3 73.368.9 106 70-130
Tetrahydrofuran ug/m3 31.030 103 68-131
Toluene ug/m3 43.138.3 113 70-130
trans-1,2-Dichloroethene ug/m3 45.040.3 112 70-130
trans-1,3-Dichloropropene ug/m3 54.146.1 117 70-134
Trichloroethene ug/m3 58.454.6 107 70-130
Trichlorofluoromethane ug/m3 66.257.1 116 65-130
Vinyl acetate ug/m3 37.535.8 105 61-133
Vinyl chloride ug/m3 31.226 120 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484111004
3357227SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 62 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484111004
3357227SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 NDND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 17.8 218.2
Benzene ug/m3 0.55ND
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 NDND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.4 41.4
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.7 62.9
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 NDND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 55.5 457.6
n-Heptane ug/m3 .81JND
n-Hexane ug/m3 4.8 35.0
Naphthalene ug/m3 NDND
o-Xylene ug/m3 NDND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 NDND
Toluene ug/m3 1.8 21.8
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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[phone]
Page 63 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484111004
3357227SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.5JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
75112382002
3357229SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 2.2 82.4
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 .76JND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 2.6JND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 27.9 328.7
Benzene ug/m3 1.9 22.0
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 NDND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 1.2 51.3
Chloromethane ug/m3 1.6 01.6
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 3.2 33.3
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 3.0 13.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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9800 Kincey Ave. Suite 100
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Page 64 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
75112382002
3357229SAMPLE DUPLICATE:
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 17.2 618.4
Ethylbenzene ug/m3 .93JND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 2.6JND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 4.5JND
n-Heptane ug/m3 1.5 01.5
n-Hexane ug/m3 4.7 44.9
Naphthalene ug/m3 NDND
o-Xylene ug/m3 1.1JND
Propylene ug/m3 NDND
Styrene ug/m3 1.8 51.9
Tetrachloroethene ug/m3 .99JND
Tetrahydrofuran ug/m3 NDND
Toluene ug/m3 4.2 74.5
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 5.6 35.7
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621644
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876017, 92437876019, 92437876020, 92437876021, 92437876022, 92437876025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355846
Associated Lab Samples:92437876017, 92437876019, 92437876020, 92437876021, 92437876022, 92437876025
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 0.56 07/24/19 10:45
1,1,2,2-Tetrachloroethane ug/m3 ND 0.35 07/24/19 10:45
1,1,2-Trichloroethane ug/m3 ND 0.28 07/24/19 10:45
1,1,2-Trichlorotrifluoroethane ug/m3 ND 0.78 07/24/19 10:45
1,1-Dichloroethane ug/m3 ND 0.41 07/24/19 10:45
1,1-Dichloroethene ug/m3 ND 0.40 07/24/19 10:45
1,2,4-Trichlorobenzene ug/m3 ND 3.8 07/24/19 10:45
1,2,4-Trimethylbenzene ug/m3 ND 0.50 07/24/19 10:45
1,2-Dibromoethane (EDB)ug/m3 ND 0.39 07/24/19 10:45
1,2-Dichlorobenzene ug/m3 ND 0.61 07/24/19 10:45
1,2-Dichloroethane ug/m3 ND 0.21 07/24/19 10:45
1,2-Dichloropropane ug/m3 ND 0.47 07/24/19 10:45
1,3,5-Trimethylbenzene ug/m3 ND 0.50 07/24/19 10:45
1,3-Butadiene ug/m3 ND 0.22 07/24/19 10:45
1,3-Dichlorobenzene ug/m3 ND 0.61 07/24/19 10:45
1,4-Dichlorobenzene ug/m3 ND 1.5 07/24/19 10:45
2-Butanone (MEK)ug/m3 ND 1.5 07/24/19 10:45
2-Hexanone ug/m3 ND 2.1 07/24/19 10:45
4-Ethyltoluene ug/m3 ND 1.2 07/24/19 10:45
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 07/24/19 10:45
Acetone ug/m3 ND 1.2 07/24/19 10:45
Benzene ug/m3 ND 0.16 07/24/19 10:45
Bromodichloromethane ug/m3 ND 0.68 07/24/19 10:45
Bromoform ug/m3 ND 2.6 07/24/19 10:45
Bromomethane ug/m3 ND 0.39 07/24/19 10:45
Carbon disulfide ug/m3 ND 0.32 07/24/19 10:45
Carbon tetrachloride ug/m3 ND 0.64 07/24/19 10:45
Chlorobenzene ug/m3 ND 0.47 07/24/19 10:45
Chloroethane ug/m3 ND 0.27 07/24/19 10:45
Chloroform ug/m3 ND 0.25 07/24/19 10:45
Chloromethane ug/m3 ND 0.21 07/24/19 10:45
cis-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 10:45
cis-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 10:45
Cyclohexane ug/m3 ND 0.88 07/24/19 10:45
Dibromochloromethane ug/m3 ND 0.86 07/24/19 10:45
Dichlorodifluoromethane ug/m3 ND 0.50 07/24/19 10:45
Dichlorotetrafluoroethane ug/m3 ND 0.71 07/24/19 10:45
Ethyl acetate ug/m3 ND 0.37 07/24/19 10:45
Ethylbenzene ug/m3 ND 0.44 07/24/19 10:45
Hexachloro-1,3-butadiene ug/m3 ND 2.7 07/24/19 10:45
m&p-Xylene ug/m3 ND 0.88 07/24/19 10:45
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355846
Associated Lab Samples:92437876017, 92437876019, 92437876020, 92437876021, 92437876022, 92437876025
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 1.8 07/24/19 10:45
Methylene Chloride ug/m3 ND 1.8 07/24/19 10:45
n-Heptane ug/m3 ND 0.42 07/24/19 10:45
n-Hexane ug/m3 ND 0.36 07/24/19 10:45
Naphthalene ug/m3 ND 1.3 07/24/19 10:45
o-Xylene ug/m3 ND 0.44 07/24/19 10:45
Propylene ug/m3 ND 0.18 07/24/19 10:45
Styrene ug/m3 ND 0.43 07/24/19 10:45
Tetrachloroethene ug/m3 ND 0.34 07/24/19 10:45
Tetrahydrofuran ug/m3 ND 0.30 07/24/19 10:45
Toluene ug/m3 ND 0.38 07/24/19 10:45
trans-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 10:45
trans-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 10:45
Trichloroethene ug/m3 ND 0.27 07/24/19 10:45
Trichlorofluoromethane ug/m3 ND 0.57 07/24/19 10:45
Vinyl acetate ug/m3 ND 0.36 07/24/19 10:45
Vinyl chloride ug/m3 ND 0.13 07/24/19 10:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355847LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 63.055.5 114 70-130
1,1,2,2-Tetrachloroethane ug/m3 79.069.8 113 70-132
1,1,2-Trichloroethane ug/m3 65.755.5 118 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 90.277.9 116 70-130
1,1-Dichloroethane ug/m3 45.841.1 111 70-130
1,1-Dichloroethene ug/m3 48.440.3 120 70-130
1,2,4-Trichlorobenzene ug/m3 69.675.4 92 56-130
1,2,4-Trimethylbenzene ug/m3 57.150 114 70-134
1,2-Dibromoethane (EDB)ug/m3 90.378.1 116 70-130
1,2-Dichlorobenzene ug/m3 70.361.1 115 70-132
1,2-Dichloroethane ug/m3 47.641.1 116 70-130
1,2-Dichloropropane ug/m3 55.347 118 70-130
1,3,5-Trimethylbenzene ug/m3 53.550 107 70-132
1,3-Butadiene ug/m3 30.4 CH,L322.5 135 65-130
1,3-Dichlorobenzene ug/m3 71.361.1 117 70-137
1,4-Dichlorobenzene ug/m3 71.661.1 117 70-134
2-Butanone (MEK)ug/m3 28.130 94 70-130
2-Hexanone ug/m3 50.941.6 122 70-135
4-Ethyltoluene ug/m3 56.450 113 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 48.341.6 116 70-131
Acetone ug/m3 128121 106 67-130
Benzene ug/m3 35.032.5 108 70-130
Bromodichloromethane ug/m3 77.068.1 113 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 67 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355847LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 128105 122 70-132
Bromomethane ug/m3 50.139.5 127 69-130
Carbon disulfide ug/m3 35.031.6 111 56-137
Carbon tetrachloride ug/m3 72.464 113 66-131
Chlorobenzene ug/m3 49.546.8 106 70-130
Chloroethane ug/m3 36.0 CH,L326.8 134 70-130
Chloroform ug/m3 55.149.6 111 70-130
Chloromethane ug/m3 25.221 120 66-130
cis-1,2-Dichloroethene ug/m3 43.140.3 107 70-130
cis-1,3-Dichloropropene ug/m3 53.046.1 115 70-133
Cyclohexane ug/m3 38.335 109 68-132
Dibromochloromethane ug/m3 10286.6 118 70-130
Dichlorodifluoromethane ug/m3 51.350.3 102 70-130
Dichlorotetrafluoroethane ug/m3 84.171 118 70-130
Ethyl acetate ug/m3 40.236.6 110 69-130
Ethylbenzene ug/m3 49.344.1 112 67-131
Hexachloro-1,3-butadiene ug/m3 121108 111 66-137
m&p-Xylene ug/m3 96.488.3 109 70-132
Methyl-tert-butyl ether ug/m3 40.536.6 110 70-130
Methylene Chloride ug/m3 185177 105 65-130
n-Heptane ug/m3 45.741.7 110 65-130
n-Hexane ug/m3 38.035.8 106 66-130
Naphthalene ug/m3 49.653.3 93 56-130
o-Xylene ug/m3 46.544.1 105 70-130
Propylene ug/m3 17.617.5 101 67-130
Styrene ug/m3 50.343.3 116 69-136
Tetrachloroethene ug/m3 80.468.9 117 70-130
Tetrahydrofuran ug/m3 34.930 117 68-131
Toluene ug/m3 41.338.3 108 70-130
trans-1,2-Dichloroethene ug/m3 44.240.3 110 70-130
trans-1,3-Dichloropropene ug/m3 55.446.1 120 70-134
Trichloroethene ug/m3 61.954.6 113 70-130
Trichlorofluoromethane ug/m3 67.157.1 118 65-130
Vinyl acetate ug/m3 40.435.8 113 61-133
Vinyl chloride ug/m3 33.126 127 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484108001
3356244SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 68 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484108001
3356244SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 7.3 27.5
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 22.2 924.4
Benzene ug/m3 0.93 60.99
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 6.8 86.3
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.3 81.4
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 20.6 220.9
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.5 42.5
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 4.1 24.2
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 12.2 512.9
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 14.5 214.2
n-Heptane ug/m3 6.0 06.0
n-Hexane ug/m3 38.3 339.3
Naphthalene ug/m3 NDND
o-Xylene ug/m3 2.4 42.3
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 3.5 13.5
Toluene ug/m3 74.4 175.1
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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[phone]
Page 69 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484108001
3356244SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 1.0ND
Trichlorofluoromethane ug/m3 2.9 163.4
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
10484108002
3356272SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 3.2JND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 16.3 914.9
Benzene ug/m3 .26JND
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.1 32.0
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.5 21.5
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.5 22.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 70 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484108002
3356272SAMPLE DUPLICATE:
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 NDND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 3.5JND
n-Heptane ug/m3 3.4 23.3
n-Hexane ug/m3 .96JND
Naphthalene ug/m3 NDND
o-Xylene ug/m3 NDND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 4.1 14.2
Toluene ug/m3 137 1136
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 .55JND
Trichlorofluoromethane ug/m3 1.4JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 71 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621953
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357278
Associated Lab Samples:92437876013
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 07/25/19 08:18
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 07/25/19 08:18
1,1,2-Trichloroethane ug/m3 ND 0.56 07/25/19 08:18
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 07/25/19 08:18
1,1-Dichloroethane ug/m3 ND 0.82 07/25/19 08:18
1,1-Dichloroethene ug/m3 ND 0.81 07/25/19 08:18
1,2,4-Trichlorobenzene ug/m3 ND 7.5 07/25/19 08:18
1,2,4-Trimethylbenzene ug/m3 ND 1.0 07/25/19 08:18
1,2-Dibromoethane (EDB)ug/m3 ND 0.78 07/25/19 08:18
1,2-Dichlorobenzene ug/m3 ND 1.2 07/25/19 08:18
1,2-Dichloroethane ug/m3 ND 0.41 07/25/19 08:18
1,2-Dichloropropane ug/m3 ND 0.94 07/25/19 08:18
1,3,5-Trimethylbenzene ug/m3 ND 1.0 07/25/19 08:18
1,3-Butadiene ug/m3 ND 0.45 07/25/19 08:18
1,3-Dichlorobenzene ug/m3 ND 1.2 07/25/19 08:18
1,4-Dichlorobenzene ug/m3 ND 3.1 07/25/19 08:18
2-Butanone (MEK)ug/m3 ND 3.0 07/25/19 08:18
2-Hexanone ug/m3 ND 4.2 07/25/19 08:18
4-Ethyltoluene ug/m3 ND 2.5 07/25/19 08:18
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 07/25/19 08:18
Acetone ug/m3 ND 2.4 07/25/19 08:18
Benzene ug/m3 ND 0.32 07/25/19 08:18
Bromodichloromethane ug/m3 ND 1.4 07/25/19 08:18
Bromoform ug/m3 ND 5.2 07/25/19 08:18
Bromomethane ug/m3 ND 0.79 07/25/19 08:18
Carbon disulfide ug/m3 ND 0.63 07/25/19 08:18
Carbon tetrachloride ug/m3 ND 1.3 07/25/19 08:18
Chlorobenzene ug/m3 ND 0.94 07/25/19 08:18
Chloroethane ug/m3 ND 0.54 07/25/19 08:18
Chloroform ug/m3 ND 0.50 07/25/19 08:18
Chloromethane ug/m3 ND 0.42 07/25/19 08:18
cis-1,2-Dichloroethene ug/m3 ND 0.81 07/25/19 08:18
cis-1,3-Dichloropropene ug/m3 ND 0.92 07/25/19 08:18
Cyclohexane ug/m3 ND 1.8 07/25/19 08:18
Dibromochloromethane ug/m3 ND 1.7 07/25/19 08:18
Dichlorodifluoromethane ug/m3 ND 1.0 07/25/19 08:18
Dichlorotetrafluoroethane ug/m3 ND 1.4 07/25/19 08:18
Ethyl acetate ug/m3 ND 0.73 07/25/19 08:18
Ethylbenzene ug/m3 ND 0.88 07/25/19 08:18
Hexachloro-1,3-butadiene ug/m3 ND 5.4 07/25/19 08:18
m&p-Xylene ug/m3 ND 1.8 07/25/19 08:18
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 72 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357278
Associated Lab Samples:92437876013
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 3.7 07/25/19 08:18
Methylene Chloride ug/m3 ND 3.5 07/25/19 08:18
n-Heptane ug/m3 ND 0.83 07/25/19 08:18
n-Hexane ug/m3 ND 0.72 07/25/19 08:18
Naphthalene ug/m3 ND 2.7 07/25/19 08:18
o-Xylene ug/m3 ND 0.88 07/25/19 08:18
Propylene ug/m3 ND 0.35 07/25/19 08:18
Styrene ug/m3 ND 0.87 07/25/19 08:18
Tetrachloroethene ug/m3 ND 0.69 07/25/19 08:18
Tetrahydrofuran ug/m3 ND 0.60 07/25/19 08:18
Toluene ug/m3 ND 0.77 07/25/19 08:18
trans-1,2-Dichloroethene ug/m3 ND 0.81 07/25/19 08:18
trans-1,3-Dichloropropene ug/m3 ND 0.92 07/25/19 08:18
Trichloroethene ug/m3 ND 0.55 07/25/19 08:18
Trichlorofluoromethane ug/m3 ND 1.1 07/25/19 08:18
Vinyl acetate ug/m3 ND 0.72 07/25/19 08:18
Vinyl chloride ug/m3 ND 0.26 07/25/19 08:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357279LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 55.155.5 99 70-130
1,1,2,2-Tetrachloroethane ug/m3 73.569.8 105 70-132
1,1,2-Trichloroethane ug/m3 55.455.5 100 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 76.877.9 99 70-130
1,1-Dichloroethane ug/m3 40.541.1 98 70-130
1,1-Dichloroethene ug/m3 39.940.3 99 70-130
1,2,4-Trichlorobenzene ug/m3 80.975.4 107 56-130
1,2,4-Trimethylbenzene ug/m3 55.550 111 70-134
1,2-Dibromoethane (EDB)ug/m3 80.678.1 103 70-130
1,2-Dichlorobenzene ug/m3 67.561.1 111 70-132
1,2-Dichloroethane ug/m3 40.041.1 97 70-130
1,2-Dichloropropane ug/m3 45.447 97 70-130
1,3,5-Trimethylbenzene ug/m3 50.050 100 70-132
1,3-Butadiene ug/m3 21.622.5 96 65-130
1,3-Dichlorobenzene ug/m3 67.661.1 111 70-137
1,4-Dichlorobenzene ug/m3 69.061.1 113 70-134
2-Butanone (MEK)ug/m3 26.330 88 70-130
2-Hexanone ug/m3 41.941.6 101 70-135
4-Ethyltoluene ug/m3 54.250 109 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 42.841.6 103 70-131
Acetone ug/m3 108121 90 67-130
Benzene ug/m3 35.532.5 109 70-130
Bromodichloromethane ug/m3 68.568.1 101 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/29/2019 10:30 AM
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Page 73 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357279LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 102105 97 70-132
Bromomethane ug/m3 38.039.5 96 69-130
Carbon disulfide ug/m3 31.631.6 100 56-137
Carbon tetrachloride ug/m3 64.364 101 66-131
Chlorobenzene ug/m3 46.546.8 99 70-130
Chloroethane ug/m3 25.226.8 94 70-130
Chloroform ug/m3 48.449.6 98 70-130
Chloromethane ug/m3 20.021 96 66-130
cis-1,2-Dichloroethene ug/m3 39.240.3 97 70-130
cis-1,3-Dichloropropene ug/m3 46.346.1 100 70-133
Cyclohexane ug/m3 33.635 96 68-132
Dibromochloromethane ug/m3 91.086.6 105 70-130
Dichlorodifluoromethane ug/m3 47.650.3 95 70-130
Dichlorotetrafluoroethane ug/m3 68.471 96 70-130
Ethyl acetate ug/m3 35.536.6 97 69-130
Ethylbenzene ug/m3 42.344.1 96 67-131
Hexachloro-1,3-butadiene ug/m3 118108 109 66-137
m&p-Xylene ug/m3 83.588.3 95 70-132
Methyl-tert-butyl ether ug/m3 36.036.6 98 70-130
Methylene Chloride ug/m3 164177 93 65-130
n-Heptane ug/m3 38.941.7 93 65-130
n-Hexane ug/m3 33.035.8 92 66-130
Naphthalene ug/m3 54.253.3 102 56-130
o-Xylene ug/m3 42.244.1 96 70-130
Propylene ug/m3 15.817.5 91 67-130
Styrene ug/m3 47.943.3 111 69-136
Tetrachloroethene ug/m3 75.868.9 110 70-130
Tetrahydrofuran ug/m3 27.730 93 68-131
Toluene ug/m3 37.138.3 97 70-130
trans-1,2-Dichloroethene ug/m3 38.840.3 96 70-130
trans-1,3-Dichloropropene ug/m3 46.746.1 101 70-134
Trichloroethene ug/m3 59.854.6 110 70-130
Trichlorofluoromethane ug/m3 54.757.1 96 65-130
Vinyl acetate ug/m3 31.835.8 89 61-133
Vinyl chloride ug/m3 24.526 94 70-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
622036
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876016, 92437876018, 92437876023, 92437876026
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357701
Associated Lab Samples:92437876016, 92437876018, 92437876023, 92437876026
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 0.56 07/25/19 16:53
1,1,2,2-Tetrachloroethane ug/m3 ND 0.35 07/25/19 16:53
1,1,2-Trichloroethane ug/m3 ND 0.28 07/25/19 16:53
1,1,2-Trichlorotrifluoroethane ug/m3 ND 0.78 07/25/19 16:53
1,1-Dichloroethane ug/m3 ND 0.41 07/25/19 16:53
1,1-Dichloroethene ug/m3 ND 0.40 07/25/19 16:53
1,2,4-Trichlorobenzene ug/m3 ND 3.8 07/25/19 16:53
1,2,4-Trimethylbenzene ug/m3 ND 0.50 07/25/19 16:53
1,2-Dibromoethane (EDB)ug/m3 ND 0.39 07/25/19 16:53
1,2-Dichlorobenzene ug/m3 ND 0.61 07/25/19 16:53
1,2-Dichloroethane ug/m3 ND 0.21 07/25/19 16:53
1,2-Dichloropropane ug/m3 ND 0.47 07/25/19 16:53
1,3,5-Trimethylbenzene ug/m3 ND 0.50 07/25/19 16:53
1,3-Butadiene ug/m3 ND 0.22 07/25/19 16:53
1,3-Dichlorobenzene ug/m3 ND 0.61 07/25/19 16:53
1,4-Dichlorobenzene ug/m3 ND 1.5 07/25/19 16:53
2-Butanone (MEK)ug/m3 ND 1.5 07/25/19 16:53
2-Hexanone ug/m3 ND 2.1 07/25/19 16:53
4-Ethyltoluene ug/m3 ND 1.2 07/25/19 16:53
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 07/25/19 16:53
Acetone ug/m3 ND 1.2 07/25/19 16:53
Benzene ug/m3 ND 0.16 07/25/19 16:53
Bromodichloromethane ug/m3 ND 0.68 07/25/19 16:53
Bromoform ug/m3 ND 2.6 07/25/19 16:53
Bromomethane ug/m3 ND 0.39 07/25/19 16:53
Carbon disulfide ug/m3 ND 0.32 07/25/19 16:53
Carbon tetrachloride ug/m3 ND 0.64 07/25/19 16:53
Chlorobenzene ug/m3 ND 0.47 07/25/19 16:53
Chloroethane ug/m3 ND 0.27 07/25/19 16:53
Chloroform ug/m3 ND 0.25 07/25/19 16:53
Chloromethane ug/m3 ND 0.21 07/25/19 16:53
cis-1,2-Dichloroethene ug/m3 ND 0.40 07/25/19 16:53
cis-1,3-Dichloropropene ug/m3 ND 0.46 07/25/19 16:53
Cyclohexane ug/m3 ND 0.88 07/25/19 16:53
Dibromochloromethane ug/m3 ND 0.86 07/25/19 16:53
Dichlorodifluoromethane ug/m3 ND 0.50 07/25/19 16:53
Dichlorotetrafluoroethane ug/m3 ND 0.71 07/25/19 16:53
Ethyl acetate ug/m3 ND 0.37 07/25/19 16:53
Ethylbenzene ug/m3 ND 0.44 07/25/19 16:53
Hexachloro-1,3-butadiene ug/m3 ND 2.7 07/25/19 16:53
m&p-Xylene ug/m3 ND 0.88 07/25/19 16:53
REPORT OF LABORATORY ANALYSIS
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Page 75 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357701
Associated Lab Samples:92437876016, 92437876018, 92437876023, 92437876026
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 1.8 07/25/19 16:53
Methylene Chloride ug/m3 ND 1.8 07/25/19 16:53
n-Heptane ug/m3 ND 0.42 07/25/19 16:53
n-Hexane ug/m3 ND 0.36 07/25/19 16:53
Naphthalene ug/m3 ND 1.3 07/25/19 16:53
o-Xylene ug/m3 ND 0.44 07/25/19 16:53
Propylene ug/m3 ND 0.18 07/25/19 16:53
Styrene ug/m3 ND 0.43 07/25/19 16:53
Tetrachloroethene ug/m3 ND 0.34 07/25/19 16:53
Tetrahydrofuran ug/m3 ND 0.30 07/25/19 16:53
Toluene ug/m3 ND 0.38 07/25/19 16:53
trans-1,2-Dichloroethene ug/m3 ND 0.40 07/25/19 16:53
trans-1,3-Dichloropropene ug/m3 ND 0.46 07/25/19 16:53
Trichloroethene ug/m3 ND 0.27 07/25/19 16:53
Trichlorofluoromethane ug/m3 ND 0.57 07/25/19 16:53
Vinyl acetate ug/m3 ND 0.36 07/25/19 16:53
Vinyl chloride ug/m3 ND 0.13 07/25/19 16:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357702LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 56.555.5 102 70-130
1,1,2,2-Tetrachloroethane ug/m3 73.769.8 106 70-132
1,1,2-Trichloroethane ug/m3 58.655.5 106 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 80.077.9 103 70-130
1,1-Dichloroethane ug/m3 41.141.1 100 70-130
1,1-Dichloroethene ug/m3 39.840.3 99 70-130
1,2,4-Trichlorobenzene ug/m3 68.975.4 91 56-130
1,2,4-Trimethylbenzene ug/m3 54.650 109 70-134
1,2-Dibromoethane (EDB)ug/m3 79.578.1 102 70-130
1,2-Dichlorobenzene ug/m3 66.961.1 109 70-132
1,2-Dichloroethane ug/m3 41.841.1 102 70-130
1,2-Dichloropropane ug/m3 48.347 103 70-130
1,3,5-Trimethylbenzene ug/m3 51.050 102 70-132
1,3-Butadiene ug/m3 23.222.5 103 65-130
1,3-Dichlorobenzene ug/m3 66.361.1 109 70-137
1,4-Dichlorobenzene ug/m3 67.761.1 111 70-134
2-Butanone (MEK)ug/m3 25.030 83 70-130
2-Hexanone ug/m3 41.641.6 100 70-135
4-Ethyltoluene ug/m3 53.850 108 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 41.841.6 100 70-131
Acetone ug/m3 94.8121 79 67-130
Benzene ug/m3 32.332.5 100 70-130
Bromodichloromethane ug/m3 71.568.1 105 70-130
REPORT OF LABORATORY ANALYSIS
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Page 76 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357702LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 119105 113 70-132
Bromomethane ug/m3 38.139.5 97 69-130
Carbon disulfide ug/m3 34.531.6 109 56-137
Carbon tetrachloride ug/m3 68.764 107 66-131
Chlorobenzene ug/m3 46.646.8 100 70-130
Chloroethane ug/m3 26.326.8 98 70-130
Chloroform ug/m3 49.449.6 99 70-130
Chloromethane ug/m3 20.121 96 66-130
cis-1,2-Dichloroethene ug/m3 41.940.3 104 70-130
cis-1,3-Dichloropropene ug/m3 48.746.1 106 70-133
Cyclohexane ug/m3 35.235 100 68-132
Dibromochloromethane ug/m3 92.586.6 107 70-130
Dichlorodifluoromethane ug/m3 47.950.3 95 70-130
Dichlorotetrafluoroethane ug/m3 69.871 98 70-130
Ethyl acetate ug/m3 36.336.6 99 69-130
Ethylbenzene ug/m3 46.644.1 106 67-131
Hexachloro-1,3-butadiene ug/m3 112108 103 66-137
m&p-Xylene ug/m3 90.988.3 103 70-132
Methyl-tert-butyl ether ug/m3 37.136.6 101 70-130
Methylene Chloride ug/m3 182177 103 65-130
n-Heptane ug/m3 41.141.7 99 65-130
n-Hexane ug/m3 33.935.8 95 66-130
Naphthalene ug/m3 47.653.3 89 56-130
o-Xylene ug/m3 43.944.1 100 70-130
Propylene ug/m3 16.117.5 92 67-130
Styrene ug/m3 48.243.3 111 69-136
Tetrachloroethene ug/m3 71.368.9 103 70-130
Tetrahydrofuran ug/m3 30.830 103 68-131
Toluene ug/m3 39.138.3 102 70-130
trans-1,2-Dichloroethene ug/m3 41.940.3 104 70-130
trans-1,3-Dichloropropene ug/m3 50.846.1 110 70-134
Trichloroethene ug/m3 57.754.6 106 70-130
Trichlorofluoromethane ug/m3 55.957.1 98 65-130
Vinyl acetate ug/m3 36.335.8 101 61-133
Vinyl chloride ug/m3 25.426 98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484249003
3358693SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 77 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484249003
3358693SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 3.0 52.9
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 7.8 58.2
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 17.4 616.4
Benzene ug/m3 NDND
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.1 12.0
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.2 41.2
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.4 02.4
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 2.2JND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 16.7 116.6
n-Heptane ug/m3 NDND
n-Hexane ug/m3 4.3 44.2
Naphthalene ug/m3 NDND
o-Xylene ug/m3 .97JND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 NDND
Toluene ug/m3 2.5 02.5
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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Page 78 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484249003
3358693SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.2JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
10484249004
3358694SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 1.6JND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 ND7.2
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 21.6 121.8
Benzene ug/m3 2.2 12.2
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 NDND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.3 151.1
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.4 22.3
REPORT OF LABORATORY ANALYSIS
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Page 79 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92437876
RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484249004
3358694SAMPLE DUPLICATE:
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 NDND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 12.0 011.9
n-Heptane ug/m3 NDND
n-Hexane ug/m3 5.3 65.0
Naphthalene ug/m3 NDND
o-Xylene ug/m3 NDND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 1.3JND
Tetrahydrofuran ug/m3 1.6 21.5
Toluene ug/m3 1.7 61.6
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.2JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
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Page 80 of 158
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92437876
RTP Flex
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples.L3
The reporting limit has been raised in accordance with Minnesota Statutes 4740.2100 Subpart 8. C, D. Reporting Limit
Evaluation Rule.MN
REPORT OF LABORATORY ANALYSIS
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Page 81 of 158
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92437876
RTP Flex
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92437876001 621640SG-19 (2435)TO-15
92437876002 621628SG-20 (2441)TO-15
92437876003 621628SG-21 (1348)TO-15
92437876004 621628SG-22 (2215)TO-15
92437876005 621628SG-23 (3229)TO-15
92437876006 621628SG-24 (2789)TO-15
92437876007 621628SG-8 (3227)TO-15
92437876008 621628SG-7 (2650)TO-15
92437876009 621628SG-6 (3294)TO-15
92437876010 621628SG-5 (2243)TO-15
92437876011 621628SG-4 (2924)TO-15
92437876012 621628SG-3 (1792)TO-15
92437876013 621953SG-2 (2878)TO-15
92437876014 621628SG-1 (2194)TO-15
92437876015 621628SG-18 (2002)TO-15
92437876016 622036SG-17 (2001)TO-15
92437876017 621644SG-16 (2147)TO-15
92437876018 622036SG-15 (3266)TO-15
92437876019 621644SG-10 (2788)TO-15
92437876020 621644SG-9 (2226)TO-15
92437876021 621644SG-11 (3182)TO-15
92437876022 621644SG-13 (3065)TO-15
92437876023 622036SG-12 (2076)TO-15
92437876025 621644DUP-1 (3175)TO-15
92437876026 622036SG-14 (3527) re-test TO-15
REPORT OF LABORATORY ANALYSIS
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Page 82 of 158
Page 83 of 158
Page 84 of 158
Page 85 of 158
Page 86 of 158
#=CL#
July 26, 2019
LIMS USE: FR - BONNIE VANG
LIMS OBJECT ID: 10484053
10484053
Project:
Pace Project No.:
RE:
Bonnie Vang
Pace Analytical Charlotte
9800 Kincey Ave.
Suite 100
Huntersville, NC 28078
92437876 RTP Flex
Dear Bonnie Vang:
Enclosed are the analytical results for sample(s) received by the laboratory on July 20, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ryan Thibault
[e-mail]
Project Manager
[phone]
Enclosures
cc:Client Service - Charlotte, Pace Analytical Charlotte
REPORT OF LABORATORY ANALYSIS
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1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 1 of 72Page 87 of 158
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Minnesota Certification IDs
1700 Elm Street SE, Minneapolis, MN 55414-2485
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
CNMI Saipan Certification #: MP0003
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8+Wyoming DW Certification #: via MN 027-
053-137
Florida Certification #: E87605
Georgia Certification #: 959
Guam EPA Certification #: MN00064
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: 03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Massachusetts Certification #: M-MN064
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Certifcation #: via MN 027-053-137
Minnesota Petrofund Certification #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 2 of 72Page 88 of 158
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92437876001 SG-19 (2435)TO-15 58 PASI-MCH1
92437876002 SG-20 (2441)TO-15 58 PASI-MMG2
92437876003 SG-21 (1348)TO-15 58 PASI-MMG2
92437876004 SG-22 (2215)TO-15 58 PASI-MMG2
92437876005 SG-23 (3229)TO-15 58 PASI-MMG2
92437876006 SG-24 (2789)TO-15 58 PASI-MMG2
92437876007 SG-8 (3227)TO-15 58 PASI-MMG2
92437876008 SG-7 (2650)TO-15 58 PASI-MMG2
92437876009 SG-6 (3294)TO-15 58 PASI-MMG2
92437876010 SG-5 (2243)TO-15 58 PASI-MMG2
92437876011 SG-4 (2924)TO-15 58 PASI-MMG2
92437876012 SG-3 (1792)TO-15 58 PASI-MMG2
92437876013 SG-2 (2878)TO-15 58 PASI-MMG2
92437876014 SG-1 (2194)TO-15 58 PASI-MMG2
92437876015 SG-18 (2002)TO-15 58 PASI-MMG2
92437876016 SG-17 (2001)TO-15 58 PASI-MMLS
92437876017 SG-16 (2147)TO-15 58 PASI-MMLS
92437876018 SG-15 (3266)TO-15 58 PASI-MMLS
92437876019 SG-10 (2788)TO-15 58 PASI-MMLS
92437876020 SG-9 (2226)TO-15 58 PASI-MMLS
92437876021 SG-11 (3182)TO-15 58 PASI-MMLS
92437876022 SG-13 (3065)TO-15 58 PASI-MMLS
92437876023 SG-12 (2076)TO-15 58 PASI-MMLS
92437876025 DUP-1 (3175)TO-15 58 PASI-MMLS
92437876026 SG-14 (3527) re-test TO-15 58 PASI-MMLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 3 of 72Page 89 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-19 (2435)Lab ID:92437876001 Collected:07/11/19 12:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 150 ug/m3 07/24/19 11:28 67-64-110342.7
Benzene 29.2 ug/m3 07/24/19 11:28 71-43-213.9 42.7
Bromodichloromethane ND ug/m3 07/24/19 11:28 75-27-458.1 42.7
Bromoform ND ug/m3 07/24/19 11:28 75-25-222442.7
Bromomethane ND ug/m3 07/24/19 11:28 74-83-933.7 42.7
1,3-Butadiene ND ug/m3 07/24/19 11:28 106-99-019.2 42.7
2-Butanone (MEK)ND ug/m3 07/24/19 11:28 78-93-312842.7
Carbon disulfide 31.2 ug/m3 07/24/19 11:28 75-15-027.0 42.7
Carbon tetrachloride ND ug/m3 07/24/19 11:28 56-23-554.7 42.7
Chlorobenzene ND ug/m3 07/24/19 11:28 108-90-740.0 42.7
Chloroethane ND ug/m3 07/24/19 11:28 75-00-322.9 42.7
Chloroform ND ug/m3 07/24/19 11:28 67-66-321.2 42.7
Chloromethane ND ug/m3 07/24/19 11:28 74-87-317.9 42.7
Cyclohexane ND ug/m3 07/24/19 11:28 110-82-774.7 42.7
Dibromochloromethane ND ug/m3 07/24/19 11:28 124-48-173.9 42.7
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:28 106-93-433.3 42.7
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:28 95-50-152.1 42.7
1,3-Dichlorobenzene ND ug/m3 07/24/19 11:28 541-73-152.1 42.7
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:28 106-46-713142.7
Dichlorodifluoromethane ND ug/m3 07/24/19 11:28 75-71-843.1 42.7
1,1-Dichloroethane ND ug/m3 07/24/19 11:28 75-34-335.1 42.7
1,2-Dichloroethane ND ug/m3 07/24/19 11:28 107-06-217.5 42.7
1,1-Dichloroethene ND ug/m3 07/24/19 11:28 75-35-434.4 42.7
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:28 156-59-234.4 42.7
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:28 156-60-534.4 42.7
1,2-Dichloropropane ND ug/m3 07/24/19 11:28 78-87-540.1 42.7
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:28 10061-01-539.4 42.7
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:28 10061-02-639.4 42.7
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:28 76-14-260.6 42.7
Ethyl acetate ND ug/m3 07/24/19 11:28 141-78-631.3 42.7
Ethylbenzene 66.9 ug/m3 07/24/19 11:28 100-41-437.7 42.7
4-Ethyltoluene ND ug/m3 07/24/19 11:28 622-96-810742.7
n-Heptane ND ug/m3 07/24/19 11:28 142-82-535.6 42.7
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:28 87-68-323142.7
n-Hexane 86.8 ug/m3 07/24/19 11:28 110-54-330.6 42.7
2-Hexanone ND ug/m3 07/24/19 11:28 591-78-617842.7
Methylene Chloride ND ug/m3 07/24/19 11:28 75-09-215142.7
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 11:28 108-10-117842.7
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:28 1634-04-415642.7
Naphthalene ND ug/m3 07/24/19 11:28 91-20-311442.7
Propylene 466 ug/m3 07/24/19 11:28 115-07-114.9 42.7
Styrene ND ug/m3 07/24/19 11:28 100-42-537.0 42.7
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:28 79-34-529.8 42.7
Tetrachloroethene ND ug/m3 07/24/19 11:28 127-18-429.4 42.7
Tetrahydrofuran ND ug/m3 07/24/19 11:28 109-99-925.6 42.7
Toluene 300 ug/m3 07/24/19 11:28 108-88-332.7 42.7
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:28 120-82-132242.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 4 of 72Page 90 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-19 (2435)Lab ID:92437876001 Collected:07/11/19 12:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:28 71-55-647.4 42.7
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:28 79-00-523.7 42.7
Trichloroethene ND ug/m3 07/24/19 11:28 79-01-623.3 42.7
Trichlorofluoromethane ND ug/m3 07/24/19 11:28 75-69-448.7 42.7
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:28 76-13-166.6 42.7
1,2,4-Trimethylbenzene 67.4 ug/m3 07/24/19 11:28 95-63-642.7 42.7
1,3,5-Trimethylbenzene 64.8 ug/m3 07/24/19 11:28 108-67-842.7 42.7
Vinyl acetate ND ug/m3 07/24/19 11:28 108-05-476.4 42.7
Vinyl chloride ND ug/m3 07/24/19 11:28 75-01-411.1 42.7
m&p-Xylene 266 ug/m3 07/24/19 11:28 179601-23-175.6 42.7
o-Xylene 80.2 ug/m3 07/24/19 11:28 95-47-637.7 42.7
Sample:SG-20 (2441)Lab ID:92437876002 Collected:07/11/19 12:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 30.7 ug/m3 07/24/19 11:00 67-64-14.9 2.02
Benzene 28.3 ug/m3 07/24/19 11:00 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 11:00 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 11:00 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 11:00 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 11:00 106-99-00.91 2.02
2-Butanone (MEK)ND ug/m3 07/24/19 11:00 78-93-36.1 2.02
Carbon disulfide 12.2 ug/m3 07/24/19 11:00 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 11:00 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 11:00 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 11:00 75-00-31.1 2.02
Chloroform 26.4 ug/m3 07/24/19 11:00 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 11:00 74-87-30.85 2.02
Cyclohexane 18.0 ug/m3 07/24/19 11:00 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 11:00 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:00 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:00 95-50-12.5 2.02
1,3-Dichlorobenzene 10.6 ug/m3 07/24/19 11:00 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:00 106-46-76.2 2.02
Dichlorodifluoromethane 2.3 ug/m3 07/24/19 11:00 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 11:00 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 11:00 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 11:00 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:00 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:00 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 11:00 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:00 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:00 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:00 76-14-22.9 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 5 of 72Page 91 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-20 (2441)Lab ID:92437876002 Collected:07/11/19 12:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate 2.9 ug/m3 07/24/19 11:00 141-78-61.5 2.02
Ethylbenzene 25.4 ug/m3 07/24/19 11:00 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 11:00 622-96-85.0 2.02
n-Heptane 36.6 ug/m3 07/24/19 11:00 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:00 87-68-310.9 2.02
n-Hexane 69.3 ug/m3 07/24/19 11:00 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 11:00 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 11:00 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)9.5 ug/m3 07/24/19 11:00 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:00 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 11:00 91-20-35.4 2.02
Propylene 305 ug/m3 07/24/19 11:00 115-07-1 E0.71 2.02
Styrene 6.6 ug/m3 07/24/19 11:00 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:00 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 11:00 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 11:00 109-99-91.2 2.02
Toluene 167 ug/m3 07/24/19 11:00 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:00 120-82-115.2 2.02
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:00 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:00 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 11:00 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 11:00 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:00 76-13-13.2 2.02
1,2,4-Trimethylbenzene 20.2 ug/m3 07/24/19 11:00 95-63-62.0 2.02
1,3,5-Trimethylbenzene 10.9 ug/m3 07/24/19 11:00 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 11:00 108-05-41.4 2.02
Vinyl chloride 1.1 ug/m3 07/24/19 11:00 75-01-40.53 2.02
m&p-Xylene 94.8 ug/m3 07/24/19 11:00 179601-23-13.6 2.02
o-Xylene 26.6 ug/m3 07/24/19 11:00 95-47-61.8 2.02
Sample:SG-21 (1348)Lab ID:92437876003 Collected:07/11/19 13:10 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 63.4 ug/m3 07/24/19 11:29 67-64-14.9 2.02
Benzene 45.7 ug/m3 07/24/19 11:29 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 11:29 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 11:29 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 11:29 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 11:29 106-99-00.91 2.02
2-Butanone (MEK)6.5 ug/m3 07/24/19 11:29 78-93-36.1 2.02
Carbon disulfide 118 ug/m3 07/24/19 11:29 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 11:29 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 11:29 108-90-71.9 2.02
Chloroethane 3.4 ug/m3 07/24/19 11:29 75-00-31.1 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 6 of 72Page 92 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-21 (1348)Lab ID:92437876003 Collected:07/11/19 13:10 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform 19.1 ug/m3 07/24/19 11:29 67-66-31.0 2.02
Chloromethane 8.1 ug/m3 07/24/19 11:29 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 11:29 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 11:29 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:29 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:29 95-50-12.5 2.02
1,3-Dichlorobenzene 4.1 ug/m3 07/24/19 11:29 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:29 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 11:29 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 11:29 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 11:29 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 11:29 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:29 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:29 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 11:29 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:29 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:29 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:29 76-14-22.9 2.02
Ethyl acetate 2.6 ug/m3 07/24/19 11:29 141-78-61.5 2.02
Ethylbenzene 28.8 ug/m3 07/24/19 11:29 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 11:29 622-96-85.0 2.02
n-Heptane 66.9 ug/m3 07/24/19 11:29 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:29 87-68-310.9 2.02
n-Hexane 170 ug/m3 07/24/19 11:29 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 11:29 591-78-68.4 2.02
Methylene Chloride 10.5 ug/m3 07/24/19 11:29 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)11.8 ug/m3 07/24/19 11:29 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:29 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 11:29 91-20-35.4 2.02
Propylene 6470 ug/m3 07/25/19 12:03 115-07-1113323.2
Styrene 62.4 ug/m3 07/24/19 11:29 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:29 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 11:29 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 11:29 109-99-91.2 2.02
Toluene 188 ug/m3 07/24/19 11:29 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:29 120-82-115.2 2.02
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:29 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:29 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 11:29 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 11:29 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:29 76-13-13.2 2.02
1,2,4-Trimethylbenzene 4.0 ug/m3 07/24/19 11:29 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 11:29 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 11:29 108-05-41.4 2.02
Vinyl chloride 4.6 ug/m3 07/24/19 11:29 75-01-40.53 2.02
m&p-Xylene 109 ug/m3 07/24/19 11:29 179601-23-13.6 2.02
o-Xylene 28.2 ug/m3 07/24/19 11:29 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 7 of 72Page 93 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-22 (2215)Lab ID:92437876004 Collected:07/11/19 13:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 35.4 ug/m3 07/24/19 11:58 67-64-15.1 2.1
Benzene 14.4 ug/m3 07/24/19 11:58 71-43-20.68 2.1
Bromodichloromethane ND ug/m3 07/24/19 11:58 75-27-42.9 2.1
Bromoform ND ug/m3 07/24/19 11:58 75-25-211.0 2.1
Bromomethane ND ug/m3 07/24/19 11:58 74-83-91.7 2.1
1,3-Butadiene ND ug/m3 07/24/19 11:58 106-99-00.94 2.1
2-Butanone (MEK)ND ug/m3 07/24/19 11:58 78-93-36.3 2.1
Carbon disulfide 1.9 ug/m3 07/24/19 11:58 75-15-01.3 2.1
Carbon tetrachloride ND ug/m3 07/24/19 11:58 56-23-52.7 2.1
Chlorobenzene ND ug/m3 07/24/19 11:58 108-90-72.0 2.1
Chloroethane ND ug/m3 07/24/19 11:58 75-00-31.1 2.1
Chloroform 4.1 ug/m3 07/24/19 11:58 67-66-31.0 2.1
Chloromethane 0.89 ug/m3 07/24/19 11:58 74-87-30.88 2.1
Cyclohexane 6.3 ug/m3 07/24/19 11:58 110-82-73.7 2.1
Dibromochloromethane ND ug/m3 07/24/19 11:58 124-48-13.6 2.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 11:58 106-93-41.6 2.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 11:58 95-50-12.6 2.1
1,3-Dichlorobenzene 24.2 ug/m3 07/24/19 11:58 541-73-12.6 2.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 11:58 106-46-76.4 2.1
Dichlorodifluoromethane ND ug/m3 07/24/19 11:58 75-71-82.1 2.1
1,1-Dichloroethane ND ug/m3 07/24/19 11:58 75-34-31.7 2.1
1,2-Dichloroethane ND ug/m3 07/24/19 11:58 107-06-20.86 2.1
1,1-Dichloroethene ND ug/m3 07/24/19 11:58 75-35-41.7 2.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 11:58 156-59-21.7 2.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 11:58 156-60-51.7 2.1
1,2-Dichloropropane ND ug/m3 07/24/19 11:58 78-87-52.0 2.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 11:58 10061-01-51.9 2.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 11:58 10061-02-61.9 2.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 11:58 76-14-23.0 2.1
Ethyl acetate 2.9 ug/m3 07/24/19 11:58 141-78-61.5 2.1
Ethylbenzene 20.0 ug/m3 07/24/19 11:58 100-41-41.9 2.1
4-Ethyltoluene 5.4 ug/m3 07/24/19 11:58 622-96-85.2 2.1
n-Heptane 16.4 ug/m3 07/24/19 11:58 142-82-51.7 2.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 11:58 87-68-311.4 2.1
n-Hexane 15.5 ug/m3 07/24/19 11:58 110-54-31.5 2.1
2-Hexanone ND ug/m3 07/24/19 11:58 591-78-68.7 2.1
Methylene Chloride 10.9 ug/m3 07/24/19 11:58 75-09-27.4 2.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 11:58 108-10-18.7 2.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 11:58 1634-04-47.7 2.1
Naphthalene ND ug/m3 07/24/19 11:58 91-20-35.6 2.1
Propylene 9.2 ug/m3 07/24/19 11:58 115-07-10.74 2.1
Styrene 12.0 ug/m3 07/24/19 11:58 100-42-51.8 2.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 11:58 79-34-51.5 2.1
Tetrachloroethene ND ug/m3 07/24/19 11:58 127-18-41.4 2.1
Tetrahydrofuran ND ug/m3 07/24/19 11:58 109-99-91.3 2.1
Toluene 122 ug/m3 07/24/19 11:58 108-88-31.6 2.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 11:58 120-82-115.8 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 8 of 72Page 94 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-22 (2215)Lab ID:92437876004 Collected:07/11/19 13:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 11:58 71-55-62.3 2.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 11:58 79-00-51.2 2.1
Trichloroethene ND ug/m3 07/24/19 11:58 79-01-61.1 2.1
Trichlorofluoromethane ND ug/m3 07/24/19 11:58 75-69-42.4 2.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 11:58 76-13-13.3 2.1
1,2,4-Trimethylbenzene 17.6 ug/m3 07/24/19 11:58 95-63-62.1 2.1
1,3,5-Trimethylbenzene 8.7 ug/m3 07/24/19 11:58 108-67-82.1 2.1
Vinyl acetate ND ug/m3 07/24/19 11:58 108-05-41.5 2.1
Vinyl chloride ND ug/m3 07/24/19 11:58 75-01-40.55 2.1
m&p-Xylene 77.3 ug/m3 07/24/19 11:58 179601-23-13.7 2.1
o-Xylene 21.7 ug/m3 07/24/19 11:58 95-47-61.9 2.1
Sample:SG-23 (3229)Lab ID:92437876005 Collected:07/11/19 14:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 86.8 ug/m3 07/24/19 12:27 67-64-14.9 2.02
Benzene 27.8 ug/m3 07/24/19 12:27 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 12:27 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 12:27 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 12:27 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 12:27 106-99-00.91 2.02
2-Butanone (MEK)8.1 ug/m3 07/24/19 12:27 78-93-36.1 2.02
Carbon disulfide 34.3 ug/m3 07/24/19 12:27 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 12:27 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 12:27 108-90-71.9 2.02
Chloroethane 5.3 ug/m3 07/24/19 12:27 75-00-31.1 2.02
Chloroform 36.6 ug/m3 07/24/19 12:27 67-66-31.0 2.02
Chloromethane 5.8 ug/m3 07/24/19 12:27 74-87-30.85 2.02
Cyclohexane 17.4 ug/m3 07/24/19 12:27 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 12:27 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 12:27 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 12:27 95-50-12.5 2.02
1,3-Dichlorobenzene ND ug/m3 07/24/19 12:27 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 12:27 106-46-76.2 2.02
Dichlorodifluoromethane 2.2 ug/m3 07/24/19 12:27 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 12:27 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 12:27 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 12:27 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 12:27 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 12:27 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 12:27 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 12:27 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 12:27 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 12:27 76-14-22.9 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 9 of 72Page 95 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-23 (3229)Lab ID:92437876005 Collected:07/11/19 14:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate ND ug/m3 07/24/19 12:27 141-78-61.5 2.02
Ethylbenzene 38.8 ug/m3 07/24/19 12:27 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 12:27 622-96-85.0 2.02
n-Heptane 48.0 ug/m3 07/24/19 12:27 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 12:27 87-68-310.9 2.02
n-Hexane 51.3 ug/m3 07/24/19 12:27 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 12:27 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 12:27 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 12:27 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 12:27 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 12:27 91-20-35.4 2.02
Propylene 194 ug/m3 07/24/19 12:27 115-07-1 E0.71 2.02
Styrene 17.9 ug/m3 07/24/19 12:27 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 12:27 79-34-51.4 2.02
Tetrachloroethene 7.1 ug/m3 07/24/19 12:27 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 12:27 109-99-91.2 2.02
Toluene 221 ug/m3 07/24/19 12:27 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 12:27 120-82-115.2 2.02
1,1,1-Trichloroethane ND ug/m3 07/24/19 12:27 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 12:27 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 12:27 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 12:27 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 12:27 76-13-13.2 2.02
1,2,4-Trimethylbenzene ND ug/m3 07/24/19 12:27 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 12:27 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 12:27 108-05-41.4 2.02
Vinyl chloride 2.2 ug/m3 07/24/19 12:27 75-01-40.53 2.02
m&p-Xylene 145 ug/m3 07/24/19 12:27 179601-23-13.6 2.02
o-Xylene 41.8 ug/m3 07/24/19 12:27 95-47-61.8 2.02
Sample:SG-24 (2789)Lab ID:92437876006 Collected:07/11/19 14:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 111 ug/m3 07/24/19 13:02 67-64-14.9 2.02
Benzene 67.5 ug/m3 07/24/19 13:02 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 13:02 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 13:02 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 13:02 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 13:02 106-99-00.91 2.02
2-Butanone (MEK)15.9 ug/m3 07/24/19 13:02 78-93-36.1 2.02
Carbon disulfide 777 ug/m3 07/25/19 11:36 75-15-0102161.6
Carbon tetrachloride ND ug/m3 07/24/19 13:02 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 13:02 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 13:02 75-00-31.1 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 10 of 72Page 96 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-24 (2789)Lab ID:92437876006 Collected:07/11/19 14:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform 31.1 ug/m3 07/24/19 13:02 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 13:02 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 13:02 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 13:02 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 13:02 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 13:02 95-50-12.5 2.02
1,3-Dichlorobenzene 36.1 ug/m3 07/24/19 13:02 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 13:02 106-46-76.2 2.02
Dichlorodifluoromethane 4.0 ug/m3 07/24/19 13:02 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 13:02 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 13:02 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 13:02 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 13:02 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 13:02 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 13:02 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 13:02 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 13:02 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 13:02 76-14-22.9 2.02
Ethyl acetate 5.1 ug/m3 07/24/19 13:02 141-78-61.5 2.02
Ethylbenzene 62.7 ug/m3 07/24/19 13:02 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 13:02 622-96-85.0 2.02
n-Heptane 133 ug/m3 07/24/19 13:02 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 13:02 87-68-310.9 2.02
n-Hexane 359 ug/m3 07/25/19 11:36 110-54-3116161.6
2-Hexanone ND ug/m3 07/24/19 13:02 591-78-68.4 2.02
Methylene Chloride 13.6 ug/m3 07/24/19 13:02 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 13:02 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 13:02 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 13:02 91-20-35.4 2.02
Propylene 2920 ug/m3 07/25/19 11:36 115-07-156.6 161.6
Styrene 10.1 ug/m3 07/24/19 13:02 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 13:02 79-34-51.4 2.02
Tetrachloroethene 14.8 ug/m3 07/24/19 13:02 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 13:02 109-99-91.2 2.02
Toluene 412 ug/m3 07/25/19 11:36 108-88-3124161.6
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 13:02 120-82-115.2 2.02
1,1,1-Trichloroethane ND ug/m3 07/24/19 13:02 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 13:02 79-00-51.1 2.02
Trichloroethene 2.2 ug/m3 07/24/19 13:02 79-01-61.1 2.02
Trichlorofluoromethane 2.7 ug/m3 07/24/19 13:02 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 13:02 76-13-13.2 2.02
1,2,4-Trimethylbenzene 12.5 ug/m3 07/24/19 13:02 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 13:02 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 13:02 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 13:02 75-01-40.53 2.02
m&p-Xylene 204 ug/m3 07/24/19 13:02 179601-23-13.6 2.02
o-Xylene 65.9 ug/m3 07/24/19 13:02 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 11 of 72Page 97 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-8 (3227)Lab ID:92437876007 Collected:07/11/19 17:05 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 58.8 ug/m3 07/24/19 13:31 67-64-14.9 2.02
Benzene 29.9 ug/m3 07/24/19 13:31 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 13:31 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 13:31 75-25-210.6 2.02
Bromomethane 1.9 ug/m3 07/24/19 13:31 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 13:31 106-99-00.91 2.02
2-Butanone (MEK)11.4 ug/m3 07/24/19 13:31 78-93-36.1 2.02
Carbon disulfide 30.3 ug/m3 07/24/19 13:31 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 13:31 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 13:31 108-90-71.9 2.02
Chloroethane 6.9 ug/m3 07/24/19 13:31 75-00-31.1 2.02
Chloroform 11.0 ug/m3 07/24/19 13:31 67-66-31.0 2.02
Chloromethane 13.9 ug/m3 07/24/19 13:31 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 13:31 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 13:31 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 13:31 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 13:31 95-50-12.5 2.02
1,3-Dichlorobenzene 10.5 ug/m3 07/24/19 13:31 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 13:31 106-46-76.2 2.02
Dichlorodifluoromethane 2.1 ug/m3 07/24/19 13:31 75-71-82.0 2.02
1,1-Dichloroethane 2.4 ug/m3 07/24/19 13:31 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 13:31 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 13:31 75-35-41.6 2.02
cis-1,2-Dichloroethene 7.2 ug/m3 07/24/19 13:31 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 13:31 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 13:31 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 13:31 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 13:31 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 13:31 76-14-22.9 2.02
Ethyl acetate 3.1 ug/m3 07/24/19 13:31 141-78-61.5 2.02
Ethylbenzene 27.3 ug/m3 07/24/19 13:31 100-41-41.8 2.02
4-Ethyltoluene 8.7 ug/m3 07/24/19 13:31 622-96-85.0 2.02
n-Heptane 38.5 ug/m3 07/24/19 13:31 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 13:31 87-68-310.9 2.02
n-Hexane 43.9 ug/m3 07/24/19 13:31 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 13:31 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 13:31 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)12.3 ug/m3 07/24/19 13:31 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 13:31 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 13:31 91-20-35.4 2.02
Propylene 98.2 ug/m3 07/24/19 13:31 115-07-10.71 2.02
Styrene 5.9 ug/m3 07/24/19 13:31 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 13:31 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 13:31 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 13:31 109-99-91.2 2.02
Toluene 187 ug/m3 07/24/19 13:31 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 13:31 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 12 of 72Page 98 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-8 (3227)Lab ID:92437876007 Collected:07/11/19 17:05 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 13:31 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 13:31 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 13:31 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 13:31 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 13:31 76-13-13.2 2.02
1,2,4-Trimethylbenzene 29.9 ug/m3 07/24/19 13:31 95-63-62.0 2.02
1,3,5-Trimethylbenzene 12.9 ug/m3 07/24/19 13:31 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 13:31 108-05-41.4 2.02
Vinyl chloride 2.1 ug/m3 07/24/19 13:31 75-01-40.53 2.02
m&p-Xylene 113 ug/m3 07/24/19 13:31 179601-23-13.6 2.02
o-Xylene 31.6 ug/m3 07/24/19 13:31 95-47-61.8 2.02
Sample:SG-7 (2650)Lab ID:92437876008 Collected:07/11/19 17:25 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 41.6 ug/m3 07/24/19 14:00 67-64-14.9 2.02
Benzene 16.3 ug/m3 07/24/19 14:00 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 14:00 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 14:00 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 14:00 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 14:00 106-99-00.91 2.02
2-Butanone (MEK)6.5 ug/m3 07/24/19 14:00 78-93-36.1 2.02
Carbon disulfide 22.9 ug/m3 07/24/19 14:00 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 14:00 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 14:00 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 14:00 75-00-31.1 2.02
Chloroform 4.2 ug/m3 07/24/19 14:00 67-66-31.0 2.02
Chloromethane 1.1 ug/m3 07/24/19 14:00 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 14:00 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 14:00 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 14:00 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 14:00 95-50-12.5 2.02
1,3-Dichlorobenzene 9.9 ug/m3 07/24/19 14:00 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 14:00 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 14:00 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 14:00 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 14:00 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 14:00 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 14:00 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 14:00 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 14:00 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 14:00 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 14:00 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 14:00 76-14-22.9 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 13 of 72Page 99 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-7 (2650)Lab ID:92437876008 Collected:07/11/19 17:25 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate 3.5 ug/m3 07/24/19 14:00 141-78-61.5 2.02
Ethylbenzene 14.7 ug/m3 07/24/19 14:00 100-41-41.8 2.02
4-Ethyltoluene 5.4 ug/m3 07/24/19 14:00 622-96-85.0 2.02
n-Heptane 21.5 ug/m3 07/24/19 14:00 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 14:00 87-68-310.9 2.02
n-Hexane 37.3 ug/m3 07/24/19 14:00 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 14:00 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 14:00 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 14:00 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 14:00 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 14:00 91-20-35.4 2.02
Propylene 332 ug/m3 07/24/19 14:00 115-07-1 E0.71 2.02
Styrene ND ug/m3 07/24/19 14:00 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 14:00 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 14:00 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 14:00 109-99-91.2 2.02
Toluene 99.5 ug/m3 07/24/19 14:00 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 14:00 120-82-115.2 2.02
1,1,1-Trichloroethane ND ug/m3 07/24/19 14:00 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 14:00 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 14:00 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 14:00 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 14:00 76-13-13.2 2.02
1,2,4-Trimethylbenzene 14.2 ug/m3 07/24/19 14:00 95-63-62.0 2.02
1,3,5-Trimethylbenzene 7.2 ug/m3 07/24/19 14:00 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 14:00 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 14:00 75-01-40.53 2.02
m&p-Xylene 55.4 ug/m3 07/24/19 14:00 179601-23-13.6 2.02
o-Xylene 16.0 ug/m3 07/24/19 14:00 95-47-61.8 2.02
Sample:SG-6 (3294)Lab ID:92437876009 Collected:07/11/19 17:50 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 36.4 ug/m3 07/24/19 14:29 67-64-14.2 1.74
Benzene 5.3 ug/m3 07/24/19 14:29 71-43-20.57 1.74
Bromodichloromethane ND ug/m3 07/24/19 14:29 75-27-42.4 1.74
Bromoform ND ug/m3 07/24/19 14:29 75-25-29.1 1.74
Bromomethane ND ug/m3 07/24/19 14:29 74-83-91.4 1.74
1,3-Butadiene ND ug/m3 07/24/19 14:29 106-99-00.78 1.74
2-Butanone (MEK)6.5 ug/m3 07/24/19 14:29 78-93-35.2 1.74
Carbon disulfide 4.5 ug/m3 07/24/19 14:29 75-15-01.1 1.74
Carbon tetrachloride ND ug/m3 07/24/19 14:29 56-23-52.2 1.74
Chlorobenzene ND ug/m3 07/24/19 14:29 108-90-71.6 1.74
Chloroethane ND ug/m3 07/24/19 14:29 75-00-30.93 1.74
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 14 of 72Page 100 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-6 (3294)Lab ID:92437876009 Collected:07/11/19 17:50 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform 2.1 ug/m3 07/24/19 14:29 67-66-30.86 1.74
Chloromethane ND ug/m3 07/24/19 14:29 74-87-30.73 1.74
Cyclohexane 5.2 ug/m3 07/24/19 14:29 110-82-73.0 1.74
Dibromochloromethane ND ug/m3 07/24/19 14:29 124-48-13.0 1.74
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 14:29 106-93-41.4 1.74
1,2-Dichlorobenzene ND ug/m3 07/24/19 14:29 95-50-12.1 1.74
1,3-Dichlorobenzene 20.8 ug/m3 07/24/19 14:29 541-73-12.1 1.74
1,4-Dichlorobenzene ND ug/m3 07/24/19 14:29 106-46-75.3 1.74
Dichlorodifluoromethane ND ug/m3 07/24/19 14:29 75-71-81.8 1.74
1,1-Dichloroethane ND ug/m3 07/24/19 14:29 75-34-31.4 1.74
1,2-Dichloroethane ND ug/m3 07/24/19 14:29 107-06-20.72 1.74
1,1-Dichloroethene ND ug/m3 07/24/19 14:29 75-35-41.4 1.74
cis-1,2-Dichloroethene ND ug/m3 07/24/19 14:29 156-59-21.4 1.74
trans-1,2-Dichloroethene ND ug/m3 07/24/19 14:29 156-60-51.4 1.74
1,2-Dichloropropane ND ug/m3 07/24/19 14:29 78-87-51.6 1.74
cis-1,3-Dichloropropene ND ug/m3 07/24/19 14:29 10061-01-51.6 1.74
trans-1,3-Dichloropropene ND ug/m3 07/24/19 14:29 10061-02-61.6 1.74
Dichlorotetrafluoroethane ND ug/m3 07/24/19 14:29 76-14-22.5 1.74
Ethyl acetate 2.1 ug/m3 07/24/19 14:29 141-78-61.3 1.74
Ethylbenzene 12.2 ug/m3 07/24/19 14:29 100-41-41.5 1.74
4-Ethyltoluene 5.2 ug/m3 07/24/19 14:29 622-96-84.4 1.74
n-Heptane 9.2 ug/m3 07/24/19 14:29 142-82-51.4 1.74
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 14:29 87-68-39.4 1.74
n-Hexane 10.4 ug/m3 07/24/19 14:29 110-54-31.2 1.74
2-Hexanone ND ug/m3 07/24/19 14:29 591-78-67.2 1.74
Methylene Chloride ND ug/m3 07/24/19 14:29 75-09-26.1 1.74
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 14:29 108-10-17.2 1.74
Methyl-tert-butyl ether ND ug/m3 07/24/19 14:29 1634-04-46.4 1.74
Naphthalene ND ug/m3 07/24/19 14:29 91-20-34.6 1.74
Propylene 14.8 ug/m3 07/24/19 14:29 115-07-10.61 1.74
Styrene 1440 ug/m3 07/25/19 11:09 100-42-545.2 52.2
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 14:29 79-34-51.2 1.74
Tetrachloroethene ND ug/m3 07/24/19 14:29 127-18-41.2 1.74
Tetrahydrofuran ND ug/m3 07/24/19 14:29 109-99-91.0 1.74
Toluene 42.2 ug/m3 07/24/19 14:29 108-88-31.3 1.74
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 14:29 120-82-113.1 1.74
1,1,1-Trichloroethane ND ug/m3 07/24/19 14:29 71-55-61.9 1.74
1,1,2-Trichloroethane ND ug/m3 07/24/19 14:29 79-00-50.97 1.74
Trichloroethene ND ug/m3 07/24/19 14:29 79-01-60.95 1.74
Trichlorofluoromethane ND ug/m3 07/24/19 14:29 75-69-42.0 1.74
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 14:29 76-13-12.7 1.74
1,2,4-Trimethylbenzene 21.3 ug/m3 07/24/19 14:29 95-63-61.7 1.74
1,3,5-Trimethylbenzene 9.1 ug/m3 07/24/19 14:29 108-67-81.7 1.74
Vinyl acetate ND ug/m3 07/24/19 14:29 108-05-41.2 1.74
Vinyl chloride ND ug/m3 07/24/19 14:29 75-01-40.45 1.74
m&p-Xylene 44.9 ug/m3 07/24/19 14:29 179601-23-13.1 1.74
o-Xylene 10 ug/m3 07/24/19 14:29 95-47-61.5 1.74
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 15 of 72Page 101 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-5 (2243)Lab ID:92437876010 Collected:07/11/19 18:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 36.3 ug/m3 07/24/19 14:58 67-64-14.7 1.94
Benzene 5.4 ug/m3 07/24/19 14:58 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 14:58 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 14:58 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 14:58 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 14:58 106-99-00.87 1.94
2-Butanone (MEK)6.3 ug/m3 07/24/19 14:58 78-93-35.8 1.94
Carbon disulfide 2.9 ug/m3 07/24/19 14:58 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 14:58 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 14:58 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 14:58 75-00-31.0 1.94
Chloroform ND ug/m3 07/24/19 14:58 67-66-30.96 1.94
Chloromethane 1.6 ug/m3 07/24/19 14:58 74-87-30.81 1.94
Cyclohexane 4.7 ug/m3 07/24/19 14:58 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 14:58 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 14:58 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 14:58 95-50-12.4 1.94
1,3-Dichlorobenzene 14.6 ug/m3 07/24/19 14:58 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 14:58 106-46-75.9 1.94
Dichlorodifluoromethane 2.4 ug/m3 07/24/19 14:58 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 14:58 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 14:58 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 14:58 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 14:58 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 14:58 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 14:58 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 14:58 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 14:58 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 14:58 76-14-22.8 1.94
Ethyl acetate 3.3 ug/m3 07/24/19 14:58 141-78-61.4 1.94
Ethylbenzene 4.8 ug/m3 07/24/19 14:58 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 14:58 622-96-84.8 1.94
n-Heptane 7.4 ug/m3 07/24/19 14:58 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 14:58 87-68-310.5 1.94
n-Hexane 10.1 ug/m3 07/24/19 14:58 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 14:58 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 14:58 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 14:58 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 14:58 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 14:58 91-20-35.2 1.94
Propylene 16.9 ug/m3 07/24/19 14:58 115-07-10.68 1.94
Styrene ND ug/m3 07/25/19 10:12 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 14:58 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 14:58 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 14:58 109-99-91.2 1.94
Toluene 33.3 ug/m3 07/24/19 14:58 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 14:58 120-82-114.6 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 16 of 72Page 102 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-5 (2243)Lab ID:92437876010 Collected:07/11/19 18:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 14:58 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 14:58 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 14:58 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 14:58 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 14:58 76-13-13.0 1.94
1,2,4-Trimethylbenzene 5.8 ug/m3 07/24/19 14:58 95-63-61.9 1.94
1,3,5-Trimethylbenzene 2.2 ug/m3 07/24/19 14:58 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 14:58 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 14:58 75-01-40.50 1.94
m&p-Xylene 15.8 ug/m3 07/24/19 14:58 179601-23-13.4 1.94
o-Xylene 5.5 ug/m3 07/24/19 14:58 95-47-61.7 1.94
Sample:SG-4 (2924)Lab ID:92437876011 Collected:07/11/19 18:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 28.4 ug/m3 07/24/19 15:27 67-64-14.7 1.94
Benzene 10.1 ug/m3 07/24/19 15:27 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 15:27 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 15:27 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 15:27 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 15:27 106-99-00.87 1.94
2-Butanone (MEK)6.9 ug/m3 07/24/19 15:27 78-93-35.8 1.94
Carbon disulfide 5.1 ug/m3 07/24/19 15:27 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 15:27 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 15:27 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 15:27 75-00-31.0 1.94
Chloroform 8.6 ug/m3 07/24/19 15:27 67-66-30.96 1.94
Chloromethane 1.1 ug/m3 07/24/19 15:27 74-87-30.81 1.94
Cyclohexane 5.3 ug/m3 07/24/19 15:27 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 15:27 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 15:27 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 15:27 95-50-12.4 1.94
1,3-Dichlorobenzene 5.2 ug/m3 07/24/19 15:27 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 15:27 106-46-75.9 1.94
Dichlorodifluoromethane 2.0 ug/m3 07/24/19 15:27 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 15:27 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 15:27 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 15:27 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 15:27 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 15:27 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 15:27 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 15:27 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 15:27 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 15:27 76-14-22.8 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 17 of 72Page 103 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-4 (2924)Lab ID:92437876011 Collected:07/11/19 18:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate 2.7 ug/m3 07/24/19 15:27 141-78-61.4 1.94
Ethylbenzene 10.6 ug/m3 07/24/19 15:27 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 15:27 622-96-84.8 1.94
n-Heptane 13.2 ug/m3 07/24/19 15:27 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 15:27 87-68-310.5 1.94
n-Hexane 13.9 ug/m3 07/24/19 15:27 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 15:27 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 15:27 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 15:27 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 15:27 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 15:27 91-20-35.2 1.94
Propylene 53.9 ug/m3 07/24/19 15:27 115-07-10.68 1.94
Styrene 35.1 ug/m3 07/24/19 15:27 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 15:27 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 15:27 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 15:27 109-99-91.2 1.94
Toluene 70.7 ug/m3 07/24/19 15:27 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 15:27 120-82-114.6 1.94
1,1,1-Trichloroethane ND ug/m3 07/24/19 15:27 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 15:27 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 15:27 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 15:27 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 15:27 76-13-13.0 1.94
1,2,4-Trimethylbenzene 7.9 ug/m3 07/24/19 15:27 95-63-61.9 1.94
1,3,5-Trimethylbenzene 4.8 ug/m3 07/24/19 15:27 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 15:27 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 15:27 75-01-40.50 1.94
m&p-Xylene 38.5 ug/m3 07/24/19 15:27 179601-23-13.4 1.94
o-Xylene 10.1 ug/m3 07/24/19 15:27 95-47-61.7 1.94
Sample:SG-3 (1792)Lab ID:92437876012 Collected:07/11/19 18:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 21.9 ug/m3 07/24/19 15:56 67-64-14.7 1.94
Benzene 14.7 ug/m3 07/24/19 15:56 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 15:56 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 15:56 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 15:56 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 15:56 106-99-00.87 1.94
2-Butanone (MEK)ND ug/m3 07/24/19 15:56 78-93-35.8 1.94
Carbon disulfide 3.8 ug/m3 07/24/19 15:56 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 15:56 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 15:56 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 15:56 75-00-31.0 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 18 of 72Page 104 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-3 (1792)Lab ID:92437876012 Collected:07/11/19 18:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform 8.3 ug/m3 07/24/19 15:56 67-66-30.96 1.94
Chloromethane ND ug/m3 07/24/19 15:56 74-87-30.81 1.94
Cyclohexane 13.3 ug/m3 07/24/19 15:56 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 15:56 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 15:56 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 15:56 95-50-12.4 1.94
1,3-Dichlorobenzene 4.6 ug/m3 07/24/19 15:56 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 15:56 106-46-75.9 1.94
Dichlorodifluoromethane 2.1 ug/m3 07/24/19 15:56 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 15:56 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 15:56 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 15:56 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 15:56 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 15:56 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 15:56 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 15:56 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 15:56 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 15:56 76-14-22.8 1.94
Ethyl acetate 2.7 ug/m3 07/24/19 15:56 141-78-61.4 1.94
Ethylbenzene 9.8 ug/m3 07/24/19 15:56 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 15:56 622-96-84.8 1.94
n-Heptane 25.9 ug/m3 07/24/19 15:56 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 15:56 87-68-310.5 1.94
n-Hexane 27.5 ug/m3 07/24/19 15:56 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 15:56 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 15:56 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 15:56 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 15:56 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 15:56 91-20-35.2 1.94
Propylene 19.4 ug/m3 07/24/19 15:56 115-07-10.68 1.94
Styrene 6.9 ug/m3 07/24/19 15:56 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 15:56 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 15:56 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 15:56 109-99-91.2 1.94
Toluene 83.2 ug/m3 07/24/19 15:56 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 15:56 120-82-114.6 1.94
1,1,1-Trichloroethane ND ug/m3 07/24/19 15:56 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 15:56 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 15:56 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 15:56 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 15:56 76-13-13.0 1.94
1,2,4-Trimethylbenzene 5.8 ug/m3 07/24/19 15:56 95-63-61.9 1.94
1,3,5-Trimethylbenzene 3.6 ug/m3 07/24/19 15:56 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 15:56 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 15:56 75-01-40.50 1.94
m&p-Xylene 34.5 ug/m3 07/24/19 15:56 179601-23-13.4 1.94
o-Xylene 9.1 ug/m3 07/24/19 15:56 95-47-61.7 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 19 of 72Page 105 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-2 (2878)Lab ID:92437876013 Collected:07/11/19 19:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 37.9 ug/m3 07/26/19 00:55 67-64-17.9 3.26
Benzene 1.8 ug/m3 07/26/19 00:55 71-43-21.1 3.26
Bromodichloromethane ND ug/m3 07/26/19 00:55 75-27-44.4 3.26
Bromoform ND ug/m3 07/26/19 00:55 75-25-217.1 3.26
Bromomethane ND ug/m3 07/26/19 00:55 74-83-92.6 3.26
1,3-Butadiene ND ug/m3 07/26/19 00:55 106-99-01.5 3.26
2-Butanone (MEK)ND ug/m3 07/26/19 00:55 78-93-39.8 3.26
Carbon disulfide ND ug/m3 07/26/19 00:55 75-15-02.1 3.26
Carbon tetrachloride ND ug/m3 07/26/19 00:55 56-23-54.2 3.26
Chlorobenzene ND ug/m3 07/26/19 00:55 108-90-73.1 3.26
Chloroethane ND ug/m3 07/26/19 00:55 75-00-31.7 3.26
Chloroform 5.8 ug/m3 07/26/19 00:55 67-66-31.6 3.26
Chloromethane ND ug/m3 07/26/19 00:55 74-87-31.4 3.26
Cyclohexane ND ug/m3 07/26/19 00:55 110-82-75.7 3.26
Dibromochloromethane ND ug/m3 07/26/19 00:55 124-48-15.6 3.26
1,2-Dibromoethane (EDB)ND ug/m3 07/26/19 00:55 106-93-42.5 3.26
1,2-Dichlorobenzene ND ug/m3 07/26/19 00:55 95-50-14.0 3.26
1,3-Dichlorobenzene ND ug/m3 07/26/19 00:55 541-73-14.0 3.26
1,4-Dichlorobenzene ND ug/m3 07/26/19 00:55 106-46-7103.26
Dichlorodifluoromethane ND ug/m3 07/26/19 00:55 75-71-83.3 3.26
1,1-Dichloroethane ND ug/m3 07/26/19 00:55 75-34-32.7 3.26
1,2-Dichloroethane ND ug/m3 07/26/19 00:55 107-06-21.3 3.26
1,1-Dichloroethene ND ug/m3 07/26/19 00:55 75-35-42.6 3.26
cis-1,2-Dichloroethene ND ug/m3 07/26/19 00:55 156-59-22.6 3.26
trans-1,2-Dichloroethene ND ug/m3 07/26/19 00:55 156-60-52.6 3.26
1,2-Dichloropropane ND ug/m3 07/26/19 00:55 78-87-53.1 3.26
cis-1,3-Dichloropropene ND ug/m3 07/26/19 00:55 10061-01-53.0 3.26
trans-1,3-Dichloropropene ND ug/m3 07/26/19 00:55 10061-02-63.0 3.26
Dichlorotetrafluoroethane ND ug/m3 07/26/19 00:55 76-14-24.6 3.26
Ethyl acetate ND ug/m3 07/26/19 00:55 141-78-62.4 3.26
Ethylbenzene ND ug/m3 07/26/19 00:55 100-41-42.9 3.26
4-Ethyltoluene ND ug/m3 07/26/19 00:55 622-96-88.2 3.26
n-Heptane ND ug/m3 07/26/19 00:55 142-82-52.7 3.26
Hexachloro-1,3-butadiene ND ug/m3 07/26/19 00:55 87-68-317.7 3.26
n-Hexane 26.3 ug/m3 07/26/19 00:55 110-54-32.3 3.26
2-Hexanone ND ug/m3 07/26/19 00:55 591-78-613.6 3.26
Methylene Chloride 341 ug/m3 07/26/19 00:55 75-09-211.5 3.26
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/26/19 00:55 108-10-113.6 3.26
Methyl-tert-butyl ether ND ug/m3 07/26/19 00:55 1634-04-411.9 3.26
Naphthalene ND ug/m3 07/26/19 00:55 91-20-38.7 3.26
Propylene 11.8 ug/m3 07/26/19 00:55 115-07-11.1 3.26
Styrene ND ug/m3 07/26/19 00:55 100-42-52.8 3.26
1,1,2,2-Tetrachloroethane ND ug/m3 07/26/19 00:55 79-34-52.3 3.26
Tetrachloroethene ND ug/m3 07/26/19 00:55 127-18-42.2 3.26
Tetrahydrofuran ND ug/m3 07/26/19 00:55 109-99-92.0 3.26
Toluene 12.9 ug/m3 07/26/19 00:55 108-88-32.5 3.26
1,2,4-Trichlorobenzene ND ug/m3 07/26/19 00:55 120-82-124.6 3.26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 20 of 72Page 106 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-2 (2878)Lab ID:92437876013 Collected:07/11/19 19:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/26/19 00:55 71-55-63.6 3.26
1,1,2-Trichloroethane ND ug/m3 07/26/19 00:55 79-00-51.8 3.26
Trichloroethene ND ug/m3 07/26/19 00:55 79-01-61.8 3.26
Trichlorofluoromethane ND ug/m3 07/26/19 00:55 75-69-43.7 3.26
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/26/19 00:55 76-13-15.1 3.26
1,2,4-Trimethylbenzene 3.5 ug/m3 07/26/19 00:55 95-63-63.3 3.26
1,3,5-Trimethylbenzene ND ug/m3 07/26/19 00:55 108-67-83.3 3.26
Vinyl acetate ND ug/m3 07/26/19 00:55 108-05-42.3 3.26
Vinyl chloride ND ug/m3 07/26/19 00:55 75-01-40.85 3.26
m&p-Xylene 8.5 ug/m3 07/26/19 00:55 179601-23-15.8 3.26
o-Xylene 3.1 ug/m3 07/26/19 00:55 95-47-62.9 3.26
Sample:SG-1 (2194)Lab ID:92437876014 Collected:07/11/19 19:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 18.4 ug/m3 07/24/19 16:55 67-64-14.9 2.02
Benzene 3.4 ug/m3 07/24/19 16:55 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 16:55 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 16:55 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 16:55 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 16:55 106-99-00.91 2.02
2-Butanone (MEK)ND ug/m3 07/24/19 16:55 78-93-36.1 2.02
Carbon disulfide 1.6 ug/m3 07/24/19 16:55 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 16:55 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 16:55 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 16:55 75-00-31.1 2.02
Chloroform 20.0 ug/m3 07/24/19 16:55 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 16:55 74-87-30.85 2.02
Cyclohexane 4.1 ug/m3 07/24/19 16:55 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 16:55 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 16:55 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 16:55 95-50-12.5 2.02
1,3-Dichlorobenzene 3.8 ug/m3 07/24/19 16:55 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 16:55 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 16:55 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 16:55 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 16:55 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 16:55 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 16:55 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 16:55 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 16:55 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 16:55 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 16:55 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 16:55 76-14-22.9 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 21 of 72Page 107 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-1 (2194)Lab ID:92437876014 Collected:07/11/19 19:45 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate 2.1 ug/m3 07/24/19 16:55 141-78-61.5 2.02
Ethylbenzene 5.4 ug/m3 07/24/19 16:55 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 16:55 622-96-85.0 2.02
n-Heptane 5.3 ug/m3 07/24/19 16:55 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 16:55 87-68-310.9 2.02
n-Hexane 4.7 ug/m3 07/24/19 16:55 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 16:55 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 16:55 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 16:55 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 16:55 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 16:55 91-20-35.4 2.02
Propylene 8.6 ug/m3 07/24/19 16:55 115-07-10.71 2.02
Styrene 3.3 ug/m3 07/24/19 16:55 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 16:55 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 16:55 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 16:55 109-99-91.2 2.02
Toluene 26.2 ug/m3 07/24/19 16:55 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 16:55 120-82-115.2 2.02
1,1,1-Trichloroethane ND ug/m3 07/24/19 16:55 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 16:55 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 16:55 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 16:55 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 16:55 76-13-13.2 2.02
1,2,4-Trimethylbenzene 7.2 ug/m3 07/24/19 16:55 95-63-62.0 2.02
1,3,5-Trimethylbenzene 5.6 ug/m3 07/24/19 16:55 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 16:55 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 16:55 75-01-40.53 2.02
m&p-Xylene 22.7 ug/m3 07/24/19 16:55 179601-23-13.6 2.02
o-Xylene 6.5 ug/m3 07/24/19 16:55 95-47-61.8 2.02
Sample:SG-18 (2002)Lab ID:92437876015 Collected:07/12/19 08:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 51.6 ug/m3 07/24/19 17:24 67-64-14.7 1.94
Benzene 31.8 ug/m3 07/24/19 17:24 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 17:24 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 17:24 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 17:24 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 17:24 106-99-00.87 1.94
2-Butanone (MEK)6.7 ug/m3 07/24/19 17:24 78-93-35.8 1.94
Carbon disulfide 22.7 ug/m3 07/24/19 17:24 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 17:24 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 17:24 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 17:24 75-00-31.0 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 22 of 72Page 108 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-18 (2002)Lab ID:92437876015 Collected:07/12/19 08:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform 3.7 ug/m3 07/24/19 17:24 67-66-30.96 1.94
Chloromethane 11.6 ug/m3 07/24/19 17:24 74-87-30.81 1.94
Cyclohexane ND ug/m3 07/24/19 17:24 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 17:24 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 17:24 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 17:24 95-50-12.4 1.94
1,3-Dichlorobenzene 9.3 ug/m3 07/24/19 17:24 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 17:24 106-46-75.9 1.94
Dichlorodifluoromethane 2.3 ug/m3 07/24/19 17:24 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 17:24 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 17:24 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 17:24 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 17:24 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 17:24 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 17:24 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 17:24 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 17:24 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 17:24 76-14-22.8 1.94
Ethyl acetate ND ug/m3 07/24/19 17:24 141-78-61.4 1.94
Ethylbenzene 9.2 ug/m3 07/24/19 17:24 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 17:24 622-96-84.8 1.94
n-Heptane 51.9 ug/m3 07/24/19 17:24 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 17:24 87-68-310.5 1.94
n-Hexane 154 ug/m3 07/24/19 17:24 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 17:24 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 17:24 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 17:24 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 17:24 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 17:24 91-20-35.2 1.94
Propylene 4740 ug/m3 07/25/19 12:30 115-07-1109310.4
Styrene 5.4 ug/m3 07/24/19 17:24 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 17:24 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 17:24 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 17:24 109-99-91.2 1.94
Toluene 71.7 ug/m3 07/24/19 17:24 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 17:24 120-82-114.6 1.94
1,1,1-Trichloroethane ND ug/m3 07/24/19 17:24 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 17:24 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 17:24 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 17:24 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 17:24 76-13-13.0 1.94
1,2,4-Trimethylbenzene 6.3 ug/m3 07/24/19 17:24 95-63-61.9 1.94
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 17:24 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 17:24 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 17:24 75-01-40.50 1.94
m&p-Xylene 28.1 ug/m3 07/24/19 17:24 179601-23-13.4 1.94
o-Xylene 8.5 ug/m3 07/24/19 17:24 95-47-61.7 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 23 of 72Page 109 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-17 (2001)Lab ID:92437876016 Collected:07/12/19 08:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone ND ug/m3 07/25/19 22:20 67-64-19.7 4.04
Benzene 34.8 ug/m3 07/25/19 22:20 71-43-21.3 4.04
Bromodichloromethane ND ug/m3 07/25/19 22:20 75-27-45.5 4.04
Bromoform ND ug/m3 07/25/19 22:20 75-25-221.2 4.04
Bromomethane ND ug/m3 07/25/19 22:20 74-83-93.2 4.04
1,3-Butadiene ND ug/m3 07/25/19 22:20 106-99-01.8 4.04
2-Butanone (MEK)ND ug/m3 07/25/19 22:20 78-93-312.1 4.04
Carbon disulfide 22.4 ug/m3 07/25/19 22:20 75-15-02.6 4.04
Carbon tetrachloride ND ug/m3 07/25/19 22:20 56-23-55.2 4.04
Chlorobenzene ND ug/m3 07/25/19 22:20 108-90-73.8 4.04
Chloroethane ND ug/m3 07/25/19 22:20 75-00-32.2 4.04
Chloroform 4.1 ug/m3 07/25/19 22:20 67-66-32.0 4.04
Chloromethane ND ug/m3 07/25/19 22:20 74-87-31.7 4.04
Cyclohexane ND ug/m3 07/25/19 22:20 110-82-77.1 4.04
Dibromochloromethane ND ug/m3 07/25/19 22:20 124-48-17.0 4.04
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 22:20 106-93-43.2 4.04
1,2-Dichlorobenzene ND ug/m3 07/25/19 22:20 95-50-14.9 4.04
1,3-Dichlorobenzene 17.7 ug/m3 07/25/19 22:20 541-73-14.9 4.04
1,4-Dichlorobenzene ND ug/m3 07/25/19 22:20 106-46-712.4 4.04
Dichlorodifluoromethane ND ug/m3 07/25/19 22:20 75-71-84.1 4.04
1,1-Dichloroethane ND ug/m3 07/25/19 22:20 75-34-33.3 4.04
1,2-Dichloroethane ND ug/m3 07/25/19 22:20 107-06-21.7 4.04
1,1-Dichloroethene ND ug/m3 07/25/19 22:20 75-35-43.3 4.04
cis-1,2-Dichloroethene ND ug/m3 07/25/19 22:20 156-59-23.3 4.04
trans-1,2-Dichloroethene ND ug/m3 07/25/19 22:20 156-60-53.3 4.04
1,2-Dichloropropane ND ug/m3 07/25/19 22:20 78-87-53.8 4.04
cis-1,3-Dichloropropene ND ug/m3 07/25/19 22:20 10061-01-53.7 4.04
trans-1,3-Dichloropropene ND ug/m3 07/25/19 22:20 10061-02-63.7 4.04
Dichlorotetrafluoroethane ND ug/m3 07/25/19 22:20 76-14-25.7 4.04
Ethyl acetate ND ug/m3 07/25/19 22:20 141-78-63.0 4.04
Ethylbenzene 18.3 ug/m3 07/25/19 22:20 100-41-43.6 4.04
4-Ethyltoluene ND ug/m3 07/25/19 22:20 622-96-810.1 4.04
n-Heptane 56.5 ug/m3 07/25/19 22:20 142-82-53.4 4.04
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 22:20 87-68-321.9 4.04
n-Hexane 160 ug/m3 07/25/19 22:20 110-54-32.9 4.04
2-Hexanone ND ug/m3 07/25/19 22:20 591-78-616.8 4.04
Methylene Chloride ND ug/m3 07/25/19 22:20 75-09-214.3 4.04
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 22:20 108-10-116.8 4.04
Methyl-tert-butyl ether ND ug/m3 07/25/19 22:20 1634-04-414.8 4.04
Naphthalene ND ug/m3 07/25/19 22:20 91-20-310.7 4.04
Propylene 1000 ug/m3 07/25/19 22:20 115-07-1 E1.4 4.04
Styrene ND ug/m3 07/25/19 22:20 100-42-53.5 4.04
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 22:20 79-34-52.8 4.04
Tetrachloroethene ND ug/m3 07/25/19 22:20 127-18-42.8 4.04
Tetrahydrofuran ND ug/m3 07/25/19 22:20 109-99-92.4 4.04
Toluene 98.9 ug/m3 07/25/19 22:20 108-88-33.1 4.04
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 22:20 120-82-130.5 4.04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 24 of 72Page 110 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-17 (2001)Lab ID:92437876016 Collected:07/12/19 08:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/25/19 22:20 71-55-64.5 4.04
1,1,2-Trichloroethane ND ug/m3 07/25/19 22:20 79-00-52.2 4.04
Trichloroethene ND ug/m3 07/25/19 22:20 79-01-62.2 4.04
Trichlorofluoromethane ND ug/m3 07/25/19 22:20 75-69-44.6 4.04
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 22:20 76-13-16.3 4.04
1,2,4-Trimethylbenzene 7.8 ug/m3 07/25/19 22:20 95-63-64.0 4.04
1,3,5-Trimethylbenzene ND ug/m3 07/25/19 22:20 108-67-84.0 4.04
Vinyl acetate ND ug/m3 07/25/19 22:20 108-05-42.9 4.04
Vinyl chloride ND ug/m3 07/25/19 22:20 75-01-41.1 4.04
m&p-Xylene 39.4 ug/m3 07/25/19 22:20 179601-23-17.2 4.04
o-Xylene 11.0 ug/m3 07/25/19 22:20 95-47-63.6 4.04
Sample:SG-16 (2147)Lab ID:92437876017 Collected:07/12/19 09:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone ND ug/m3 07/24/19 19:58 67-64-14.7 1.94
Benzene 15.6 ug/m3 07/24/19 19:58 71-43-20.63 1.94
Bromodichloromethane ND ug/m3 07/24/19 19:58 75-27-42.6 1.94
Bromoform ND ug/m3 07/24/19 19:58 75-25-210.2 1.94
Bromomethane ND ug/m3 07/24/19 19:58 74-83-91.5 1.94
1,3-Butadiene ND ug/m3 07/24/19 19:58 106-99-00.87 1.94
2-Butanone (MEK)9.6 ug/m3 07/24/19 19:58 78-93-35.8 1.94
Carbon disulfide 13.1 ug/m3 07/24/19 19:58 75-15-01.2 1.94
Carbon tetrachloride ND ug/m3 07/24/19 19:58 56-23-52.5 1.94
Chlorobenzene ND ug/m3 07/24/19 19:58 108-90-71.8 1.94
Chloroethane ND ug/m3 07/24/19 19:58 75-00-31.0 1.94
Chloroform 1.0 ug/m3 07/24/19 19:58 67-66-30.96 1.94
Chloromethane ND ug/m3 07/24/19 19:58 74-87-30.81 1.94
Cyclohexane ND ug/m3 07/24/19 19:58 110-82-73.4 1.94
Dibromochloromethane ND ug/m3 07/24/19 19:58 124-48-13.4 1.94
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 19:58 106-93-41.5 1.94
1,2-Dichlorobenzene ND ug/m3 07/24/19 19:58 95-50-12.4 1.94
1,3-Dichlorobenzene 12.2 ug/m3 07/24/19 19:58 541-73-12.4 1.94
1,4-Dichlorobenzene ND ug/m3 07/24/19 19:58 106-46-75.9 1.94
Dichlorodifluoromethane 2.4 ug/m3 07/24/19 19:58 75-71-82.0 1.94
1,1-Dichloroethane ND ug/m3 07/24/19 19:58 75-34-31.6 1.94
1,2-Dichloroethane ND ug/m3 07/24/19 19:58 107-06-20.80 1.94
1,1-Dichloroethene ND ug/m3 07/24/19 19:58 75-35-41.6 1.94
cis-1,2-Dichloroethene ND ug/m3 07/24/19 19:58 156-59-21.6 1.94
trans-1,2-Dichloroethene ND ug/m3 07/24/19 19:58 156-60-51.6 1.94
1,2-Dichloropropane ND ug/m3 07/24/19 19:58 78-87-51.8 1.94
cis-1,3-Dichloropropene ND ug/m3 07/24/19 19:58 10061-01-51.8 1.94
trans-1,3-Dichloropropene ND ug/m3 07/24/19 19:58 10061-02-61.8 1.94
Dichlorotetrafluoroethane ND ug/m3 07/24/19 19:58 76-14-22.8 1.94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 25 of 72Page 111 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-16 (2147)Lab ID:92437876017 Collected:07/12/19 09:20 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate 5.1 ug/m3 07/24/19 19:58 141-78-61.4 1.94
Ethylbenzene 7.8 ug/m3 07/24/19 19:58 100-41-41.7 1.94
4-Ethyltoluene ND ug/m3 07/24/19 19:58 622-96-84.8 1.94
n-Heptane 32.9 ug/m3 07/24/19 19:58 142-82-51.6 1.94
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 19:58 87-68-310.5 1.94
n-Hexane 107 ug/m3 07/24/19 19:58 110-54-31.4 1.94
2-Hexanone ND ug/m3 07/24/19 19:58 591-78-68.1 1.94
Methylene Chloride ND ug/m3 07/24/19 19:58 75-09-26.8 1.94
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 19:58 108-10-18.1 1.94
Methyl-tert-butyl ether ND ug/m3 07/24/19 19:58 1634-04-47.1 1.94
Naphthalene ND ug/m3 07/24/19 19:58 91-20-35.2 1.94
Propylene 453 ug/m3 07/24/19 19:58 115-07-1 E0.68 1.94
Styrene 2.5 ug/m3 07/25/19 19:20 100-42-51.7 1.94
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 19:58 79-34-51.4 1.94
Tetrachloroethene ND ug/m3 07/24/19 19:58 127-18-41.3 1.94
Tetrahydrofuran ND ug/m3 07/24/19 19:58 109-99-91.2 1.94
Toluene 52.6 ug/m3 07/24/19 19:58 108-88-31.5 1.94
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 19:58 120-82-114.6 1.94
1,1,1-Trichloroethane ND ug/m3 07/24/19 19:58 71-55-62.2 1.94
1,1,2-Trichloroethane ND ug/m3 07/24/19 19:58 79-00-51.1 1.94
Trichloroethene ND ug/m3 07/24/19 19:58 79-01-61.1 1.94
Trichlorofluoromethane ND ug/m3 07/24/19 19:58 75-69-42.2 1.94
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 19:58 76-13-13.0 1.94
1,2,4-Trimethylbenzene 6.9 ug/m3 07/24/19 19:58 95-63-61.9 1.94
1,3,5-Trimethylbenzene 2.4 ug/m3 07/24/19 19:58 108-67-81.9 1.94
Vinyl acetate ND ug/m3 07/24/19 19:58 108-05-41.4 1.94
Vinyl chloride ND ug/m3 07/24/19 19:58 75-01-40.50 1.94
m&p-Xylene 25.7 ug/m3 07/24/19 19:58 179601-23-13.4 1.94
o-Xylene 7.9 ug/m3 07/24/19 19:58 95-47-61.7 1.94
Sample:SG-15 (3266)Lab ID:92437876018 Collected:07/12/19 09:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 44.2 ug/m3 07/25/19 21:19 67-64-15.3 2.19
Benzene 22.9 ug/m3 07/25/19 21:19 71-43-20.71 2.19
Bromodichloromethane ND ug/m3 07/25/19 21:19 75-27-43.0 2.19
Bromoform ND ug/m3 07/25/19 21:19 75-25-211.5 2.19
Bromomethane ND ug/m3 07/25/19 21:19 74-83-91.7 2.19
1,3-Butadiene ND ug/m3 07/25/19 21:19 106-99-00.99 2.19
2-Butanone (MEK)ND ug/m3 07/25/19 21:19 78-93-36.6 2.19
Carbon disulfide 6.3 ug/m3 07/25/19 21:19 75-15-01.4 2.19
Carbon tetrachloride ND ug/m3 07/25/19 21:19 56-23-52.8 2.19
Chlorobenzene ND ug/m3 07/25/19 21:19 108-90-72.0 2.19
Chloroethane 7.1 ug/m3 07/25/19 21:19 75-00-31.2 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 26 of 72Page 112 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-15 (3266)Lab ID:92437876018 Collected:07/12/19 09:40 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform 6.5 ug/m3 07/25/19 21:19 67-66-31.1 2.19
Chloromethane 13.3 ug/m3 07/25/19 21:19 74-87-30.92 2.19
Cyclohexane 13.8 ug/m3 07/25/19 21:19 110-82-73.8 2.19
Dibromochloromethane ND ug/m3 07/25/19 21:19 124-48-13.8 2.19
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 21:19 106-93-41.7 2.19
1,2-Dichlorobenzene ND ug/m3 07/25/19 21:19 95-50-12.7 2.19
1,3-Dichlorobenzene 12.3 ug/m3 07/25/19 21:19 541-73-12.7 2.19
1,4-Dichlorobenzene ND ug/m3 07/25/19 21:19 106-46-76.7 2.19
Dichlorodifluoromethane 2.9 ug/m3 07/25/19 21:19 75-71-82.2 2.19
1,1-Dichloroethane ND ug/m3 07/25/19 21:19 75-34-31.8 2.19
1,2-Dichloroethane ND ug/m3 07/25/19 21:19 107-06-20.90 2.19
1,1-Dichloroethene ND ug/m3 07/25/19 21:19 75-35-41.8 2.19
cis-1,2-Dichloroethene ND ug/m3 07/25/19 21:19 156-59-21.8 2.19
trans-1,2-Dichloroethene ND ug/m3 07/25/19 21:19 156-60-51.8 2.19
1,2-Dichloropropane ND ug/m3 07/25/19 21:19 78-87-52.1 2.19
cis-1,3-Dichloropropene ND ug/m3 07/25/19 21:19 10061-01-52.0 2.19
trans-1,3-Dichloropropene ND ug/m3 07/25/19 21:19 10061-02-62.0 2.19
Dichlorotetrafluoroethane ND ug/m3 07/25/19 21:19 76-14-23.1 2.19
Ethyl acetate 4.3 ug/m3 07/25/19 21:19 141-78-61.6 2.19
Ethylbenzene 12.0 ug/m3 07/25/19 21:19 100-41-41.9 2.19
4-Ethyltoluene ND ug/m3 07/25/19 21:19 622-96-85.5 2.19
n-Heptane 25.7 ug/m3 07/25/19 21:19 142-82-51.8 2.19
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 21:19 87-68-311.9 2.19
n-Hexane 42.7 ug/m3 07/25/19 21:19 110-54-31.6 2.19
2-Hexanone ND ug/m3 07/25/19 21:19 591-78-69.1 2.19
Methylene Chloride 14.2 ug/m3 07/25/19 21:19 75-09-27.7 2.19
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 21:19 108-10-19.1 2.19
Methyl-tert-butyl ether ND ug/m3 07/25/19 21:19 1634-04-48.0 2.19
Naphthalene ND ug/m3 07/25/19 21:19 91-20-35.8 2.19
Propylene 189 ug/m3 07/25/19 21:19 115-07-1 E0.77 2.19
Styrene ND ug/m3 07/25/19 21:19 100-42-51.9 2.19
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 21:19 79-34-51.5 2.19
Tetrachloroethene ND ug/m3 07/25/19 21:19 127-18-41.5 2.19
Tetrahydrofuran ND ug/m3 07/25/19 21:19 109-99-91.3 2.19
Toluene 92.6 ug/m3 07/25/19 21:19 108-88-31.7 2.19
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 21:19 120-82-116.5 2.19
1,1,1-Trichloroethane ND ug/m3 07/25/19 21:19 71-55-62.4 2.19
1,1,2-Trichloroethane ND ug/m3 07/25/19 21:19 79-00-51.2 2.19
Trichloroethene ND ug/m3 07/25/19 21:19 79-01-61.2 2.19
Trichlorofluoromethane ND ug/m3 07/25/19 21:19 75-69-42.5 2.19
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 21:19 76-13-13.4 2.19
1,2,4-Trimethylbenzene 8.3 ug/m3 07/25/19 21:19 95-63-62.2 2.19
1,3,5-Trimethylbenzene 3.2 ug/m3 07/25/19 21:19 108-67-82.2 2.19
Vinyl acetate ND ug/m3 07/25/19 21:19 108-05-41.6 2.19
Vinyl chloride 4.7 ug/m3 07/25/19 21:19 75-01-40.57 2.19
m&p-Xylene 41.5 ug/m3 07/25/19 21:19 179601-23-13.9 2.19
o-Xylene 11.4 ug/m3 07/25/19 21:19 95-47-61.9 2.19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 27 of 72Page 113 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-10 (2788)Lab ID:92437876019 Collected:07/12/19 10:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 52.1 ug/m3 07/24/19 19:28 67-64-14.9 2.02
Benzene 25.3 ug/m3 07/24/19 19:28 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 19:28 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 19:28 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 19:28 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 19:28 106-99-00.91 2.02
2-Butanone (MEK)ND ug/m3 07/24/19 19:28 78-93-36.1 2.02
Carbon disulfide 10.1 ug/m3 07/24/19 19:28 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 19:28 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 19:28 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 19:28 75-00-31.1 2.02
Chloroform 2.2 ug/m3 07/24/19 19:28 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 19:28 74-87-30.85 2.02
Cyclohexane ND ug/m3 07/24/19 19:28 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 19:28 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 19:28 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 19:28 95-50-12.5 2.02
1,3-Dichlorobenzene 23.6 ug/m3 07/24/19 19:28 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 19:28 106-46-76.2 2.02
Dichlorodifluoromethane 2.5 ug/m3 07/24/19 19:28 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 19:28 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 19:28 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 19:28 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 19:28 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 19:28 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 19:28 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 19:28 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 19:28 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 19:28 76-14-22.9 2.02
Ethyl acetate ND ug/m3 07/24/19 19:28 141-78-61.5 2.02
Ethylbenzene 17.6 ug/m3 07/24/19 19:28 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 19:28 622-96-85.0 2.02
n-Heptane 39.3 ug/m3 07/24/19 19:28 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 19:28 87-68-310.9 2.02
n-Hexane 78.4 ug/m3 07/24/19 19:28 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 19:28 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 19:28 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 19:28 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 19:28 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 19:28 91-20-35.4 2.02
Propylene 288 ug/m3 07/25/19 20:19 115-07-17.1 20.2
Styrene 405 ug/m3 07/25/19 20:19 100-42-517.5 20.2
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 19:28 79-34-51.4 2.02
Tetrachloroethene ND ug/m3 07/24/19 19:28 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 19:28 109-99-91.2 2.02
Toluene 139 ug/m3 07/24/19 19:28 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 19:28 120-82-115.2 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 28 of 72Page 114 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-10 (2788)Lab ID:92437876019 Collected:07/12/19 10:15 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 19:28 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 19:28 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 19:28 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 19:28 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 19:28 76-13-13.2 2.02
1,2,4-Trimethylbenzene 10.8 ug/m3 07/24/19 19:28 95-63-62.0 2.02
1,3,5-Trimethylbenzene 4.6 ug/m3 07/24/19 19:28 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 19:28 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 19:28 75-01-40.53 2.02
m&p-Xylene 64.2 ug/m3 07/24/19 19:28 179601-23-13.6 2.02
o-Xylene 15.8 ug/m3 07/24/19 19:28 95-47-61.8 2.02
Sample:SG-9 (2226)Lab ID:92437876020 Collected:07/12/19 10:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 53.1 ug/m3 07/24/19 20:28 67-64-15.1 2.1
Benzene 11.4 ug/m3 07/24/19 20:28 71-43-20.68 2.1
Bromodichloromethane ND ug/m3 07/24/19 20:28 75-27-42.9 2.1
Bromoform ND ug/m3 07/24/19 20:28 75-25-211.0 2.1
Bromomethane ND ug/m3 07/24/19 20:28 74-83-91.7 2.1
1,3-Butadiene ND ug/m3 07/24/19 20:28 106-99-00.94 2.1
2-Butanone (MEK)13.0 ug/m3 07/24/19 20:28 78-93-36.3 2.1
Carbon disulfide 3.3 ug/m3 07/24/19 20:28 75-15-01.3 2.1
Carbon tetrachloride ND ug/m3 07/24/19 20:28 56-23-52.7 2.1
Chlorobenzene ND ug/m3 07/24/19 20:28 108-90-72.0 2.1
Chloroethane ND ug/m3 07/24/19 20:28 75-00-31.1 2.1
Chloroform 3.7 ug/m3 07/24/19 20:28 67-66-31.0 2.1
Chloromethane 7.0 ug/m3 07/24/19 20:28 74-87-30.88 2.1
Cyclohexane 9.4 ug/m3 07/24/19 20:28 110-82-73.7 2.1
Dibromochloromethane ND ug/m3 07/24/19 20:28 124-48-13.6 2.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 20:28 106-93-41.6 2.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 20:28 95-50-12.6 2.1
1,3-Dichlorobenzene 18.0 ug/m3 07/24/19 20:28 541-73-12.6 2.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 20:28 106-46-76.4 2.1
Dichlorodifluoromethane 2.7 ug/m3 07/24/19 20:28 75-71-82.1 2.1
1,1-Dichloroethane ND ug/m3 07/24/19 20:28 75-34-31.7 2.1
1,2-Dichloroethane ND ug/m3 07/24/19 20:28 107-06-20.86 2.1
1,1-Dichloroethene ND ug/m3 07/24/19 20:28 75-35-41.7 2.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 20:28 156-59-21.7 2.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 20:28 156-60-51.7 2.1
1,2-Dichloropropane ND ug/m3 07/24/19 20:28 78-87-52.0 2.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 20:28 10061-01-51.9 2.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 20:28 10061-02-61.9 2.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 20:28 76-14-23.0 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 29 of 72Page 115 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-9 (2226)Lab ID:92437876020 Collected:07/12/19 10:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate 4.3 ug/m3 07/24/19 20:28 141-78-61.5 2.1
Ethylbenzene 5.9 ug/m3 07/24/19 20:28 100-41-41.9 2.1
4-Ethyltoluene ND ug/m3 07/24/19 20:28 622-96-85.2 2.1
n-Heptane 13.1 ug/m3 07/24/19 20:28 142-82-51.7 2.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 20:28 87-68-311.4 2.1
n-Hexane 24.1 ug/m3 07/24/19 20:28 110-54-31.5 2.1
2-Hexanone ND ug/m3 07/24/19 20:28 591-78-68.7 2.1
Methylene Chloride ND ug/m3 07/24/19 20:28 75-09-27.4 2.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 20:28 108-10-18.7 2.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 20:28 1634-04-47.7 2.1
Naphthalene ND ug/m3 07/24/19 20:28 91-20-35.6 2.1
Propylene 77.9 ug/m3 07/24/19 20:28 115-07-10.74 2.1
Styrene 8.1 ug/m3 07/24/19 20:28 100-42-51.8 2.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 20:28 79-34-51.5 2.1
Tetrachloroethene ND ug/m3 07/24/19 20:28 127-18-41.4 2.1
Tetrahydrofuran ND ug/m3 07/24/19 20:28 109-99-91.3 2.1
Toluene 37.5 ug/m3 07/24/19 20:28 108-88-31.6 2.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 20:28 120-82-115.8 2.1
1,1,1-Trichloroethane ND ug/m3 07/24/19 20:28 71-55-62.3 2.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 20:28 79-00-51.2 2.1
Trichloroethene ND ug/m3 07/24/19 20:28 79-01-61.1 2.1
Trichlorofluoromethane ND ug/m3 07/24/19 20:28 75-69-42.4 2.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 20:28 76-13-13.3 2.1
1,2,4-Trimethylbenzene 6.1 ug/m3 07/24/19 20:28 95-63-62.1 2.1
1,3,5-Trimethylbenzene 2.1 ug/m3 07/24/19 20:28 108-67-82.1 2.1
Vinyl acetate ND ug/m3 07/24/19 20:28 108-05-41.5 2.1
Vinyl chloride 2.2 ug/m3 07/24/19 20:28 75-01-40.55 2.1
m&p-Xylene 19.1 ug/m3 07/24/19 20:28 179601-23-13.7 2.1
o-Xylene 6.1 ug/m3 07/24/19 20:28 95-47-61.9 2.1
Sample:SG-11 (3182)Lab ID:92437876021 Collected:07/12/19 11:03 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 52.2 ug/m3 07/24/19 18:27 67-64-14.9 2.02
Benzene 0.95 ug/m3 07/24/19 18:27 71-43-20.66 2.02
Bromodichloromethane ND ug/m3 07/24/19 18:27 75-27-42.7 2.02
Bromoform ND ug/m3 07/24/19 18:27 75-25-210.6 2.02
Bromomethane ND ug/m3 07/24/19 18:27 74-83-91.6 2.02
1,3-Butadiene ND ug/m3 07/24/19 18:27 106-99-00.91 2.02
2-Butanone (MEK)12.3 ug/m3 07/24/19 18:27 78-93-36.1 2.02
Carbon disulfide ND ug/m3 07/24/19 18:27 75-15-01.3 2.02
Carbon tetrachloride ND ug/m3 07/24/19 18:27 56-23-52.6 2.02
Chlorobenzene ND ug/m3 07/24/19 18:27 108-90-71.9 2.02
Chloroethane ND ug/m3 07/24/19 18:27 75-00-31.1 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 30 of 72Page 116 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-11 (3182)Lab ID:92437876021 Collected:07/12/19 11:03 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform ND ug/m3 07/24/19 18:27 67-66-31.0 2.02
Chloromethane ND ug/m3 07/24/19 18:27 74-87-30.85 2.02
Cyclohexane 6.6 ug/m3 07/24/19 18:27 110-82-73.5 2.02
Dibromochloromethane ND ug/m3 07/24/19 18:27 124-48-13.5 2.02
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 18:27 106-93-41.6 2.02
1,2-Dichlorobenzene ND ug/m3 07/24/19 18:27 95-50-12.5 2.02
1,3-Dichlorobenzene 26.1 ug/m3 07/24/19 18:27 541-73-12.5 2.02
1,4-Dichlorobenzene ND ug/m3 07/24/19 18:27 106-46-76.2 2.02
Dichlorodifluoromethane ND ug/m3 07/24/19 18:27 75-71-82.0 2.02
1,1-Dichloroethane ND ug/m3 07/24/19 18:27 75-34-31.7 2.02
1,2-Dichloroethane ND ug/m3 07/24/19 18:27 107-06-20.83 2.02
1,1-Dichloroethene ND ug/m3 07/24/19 18:27 75-35-41.6 2.02
cis-1,2-Dichloroethene ND ug/m3 07/24/19 18:27 156-59-21.6 2.02
trans-1,2-Dichloroethene ND ug/m3 07/24/19 18:27 156-60-51.6 2.02
1,2-Dichloropropane ND ug/m3 07/24/19 18:27 78-87-51.9 2.02
cis-1,3-Dichloropropene ND ug/m3 07/24/19 18:27 10061-01-51.9 2.02
trans-1,3-Dichloropropene ND ug/m3 07/24/19 18:27 10061-02-61.9 2.02
Dichlorotetrafluoroethane ND ug/m3 07/24/19 18:27 76-14-22.9 2.02
Ethyl acetate 4.4 ug/m3 07/24/19 18:27 141-78-61.5 2.02
Ethylbenzene 3.1 ug/m3 07/24/19 18:27 100-41-41.8 2.02
4-Ethyltoluene ND ug/m3 07/24/19 18:27 622-96-85.0 2.02
n-Heptane ND ug/m3 07/24/19 18:27 142-82-51.7 2.02
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 18:27 87-68-310.9 2.02
n-Hexane ND ug/m3 07/24/19 18:27 110-54-31.4 2.02
2-Hexanone ND ug/m3 07/24/19 18:27 591-78-68.4 2.02
Methylene Chloride ND ug/m3 07/24/19 18:27 75-09-27.1 2.02
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 18:27 108-10-18.4 2.02
Methyl-tert-butyl ether ND ug/m3 07/24/19 18:27 1634-04-47.4 2.02
Naphthalene ND ug/m3 07/24/19 18:27 91-20-35.4 2.02
Propylene ND ug/m3 07/24/19 18:27 115-07-10.71 2.02
Styrene 7.1 ug/m3 07/24/19 18:27 100-42-51.7 2.02
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 18:27 79-34-51.4 2.02
Tetrachloroethene 2.1 ug/m3 07/24/19 18:27 127-18-41.4 2.02
Tetrahydrofuran ND ug/m3 07/24/19 18:27 109-99-91.2 2.02
Toluene 9.2 ug/m3 07/24/19 18:27 108-88-31.5 2.02
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 18:27 120-82-115.2 2.02
1,1,1-Trichloroethane ND ug/m3 07/24/19 18:27 71-55-62.2 2.02
1,1,2-Trichloroethane ND ug/m3 07/24/19 18:27 79-00-51.1 2.02
Trichloroethene ND ug/m3 07/24/19 18:27 79-01-61.1 2.02
Trichlorofluoromethane ND ug/m3 07/24/19 18:27 75-69-42.3 2.02
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 18:27 76-13-13.2 2.02
1,2,4-Trimethylbenzene 6.7 ug/m3 07/24/19 18:27 95-63-62.0 2.02
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 18:27 108-67-82.0 2.02
Vinyl acetate ND ug/m3 07/24/19 18:27 108-05-41.4 2.02
Vinyl chloride ND ug/m3 07/24/19 18:27 75-01-40.53 2.02
m&p-Xylene 11.1 ug/m3 07/24/19 18:27 179601-23-13.6 2.02
o-Xylene 4.7 ug/m3 07/24/19 18:27 95-47-61.8 2.02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 31 of 72Page 117 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-13 (3065)Lab ID:92437876022 Collected:07/12/19 11:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 58.8 ug/m3 07/24/19 20:57 67-64-124.3 10.1
Benzene 28.2 ug/m3 07/24/19 20:57 71-43-23.3 10.1
Bromodichloromethane ND ug/m3 07/24/19 20:57 75-27-413.7 10.1
Bromoform ND ug/m3 07/24/19 20:57 75-25-253.0 10.1
Bromomethane ND ug/m3 07/24/19 20:57 74-83-98.0 10.1
1,3-Butadiene ND ug/m3 07/24/19 20:57 106-99-04.5 10.1
2-Butanone (MEK)ND ug/m3 07/24/19 20:57 78-93-330.3 10.1
Carbon disulfide 12.1 ug/m3 07/24/19 20:57 75-15-06.4 10.1
Carbon tetrachloride ND ug/m3 07/24/19 20:57 56-23-512.9 10.1
Chlorobenzene ND ug/m3 07/24/19 20:57 108-90-79.5 10.1
Chloroethane ND ug/m3 07/24/19 20:57 75-00-35.4 10.1
Chloroform 7.9 ug/m3 07/24/19 20:57 67-66-35.0 10.1
Chloromethane 8.9 ug/m3 07/24/19 20:57 74-87-34.2 10.1
Cyclohexane 20.6 ug/m3 07/24/19 20:57 110-82-717.7 10.1
Dibromochloromethane ND ug/m3 07/24/19 20:57 124-48-117.5 10.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 20:57 106-93-47.9 10.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 20:57 95-50-112.3 10.1
1,3-Dichlorobenzene 33.3 ug/m3 07/24/19 20:57 541-73-112.3 10.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 20:57 106-46-730.9 10.1
Dichlorodifluoromethane ND ug/m3 07/24/19 20:57 75-71-810.2 10.1
1,1-Dichloroethane ND ug/m3 07/24/19 20:57 75-34-38.3 10.1
1,2-Dichloroethane ND ug/m3 07/24/19 20:57 107-06-24.2 10.1
1,1-Dichloroethene ND ug/m3 07/24/19 20:57 75-35-48.1 10.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 20:57 156-59-28.1 10.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 20:57 156-60-58.1 10.1
1,2-Dichloropropane ND ug/m3 07/24/19 20:57 78-87-59.5 10.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 20:57 10061-01-59.3 10.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 20:57 10061-02-69.3 10.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 20:57 76-14-214.3 10.1
Ethyl acetate ND ug/m3 07/24/19 20:57 141-78-67.4 10.1
Ethylbenzene 28.4 ug/m3 07/24/19 20:57 100-41-48.9 10.1
4-Ethyltoluene ND ug/m3 07/24/19 20:57 622-96-825.2 10.1
n-Heptane 38.9 ug/m3 07/24/19 20:57 142-82-58.4 10.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 20:57 87-68-354.7 10.1
n-Hexane 59.6 ug/m3 07/24/19 20:57 110-54-37.2 10.1
2-Hexanone ND ug/m3 07/24/19 20:57 591-78-642.0 10.1
Methylene Chloride ND ug/m3 07/24/19 20:57 75-09-235.7 10.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 20:57 108-10-142.0 10.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 20:57 1634-04-437.0 10.1
Naphthalene ND ug/m3 07/24/19 20:57 91-20-326.9 10.1
Propylene 113 ug/m3 07/24/19 20:57 115-07-13.5 10.1
Styrene 204 ug/m3 07/24/19 20:57 100-42-58.7 10.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 20:57 79-34-57.0 10.1
Tetrachloroethene ND ug/m3 07/24/19 20:57 127-18-47.0 10.1
Tetrahydrofuran ND ug/m3 07/24/19 20:57 109-99-96.1 10.1
Toluene 152 ug/m3 07/24/19 20:57 108-88-37.7 10.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 20:57 120-82-176.2 10.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 32 of 72Page 118 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-13 (3065)Lab ID:92437876022 Collected:07/12/19 11:35 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/24/19 20:57 71-55-611.2 10.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 20:57 79-00-55.6 10.1
Trichloroethene ND ug/m3 07/24/19 20:57 79-01-65.5 10.1
Trichlorofluoromethane ND ug/m3 07/24/19 20:57 75-69-411.5 10.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 20:57 76-13-115.8 10.1
1,2,4-Trimethylbenzene 22.6 ug/m3 07/24/19 20:57 95-63-610.1 10.1
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 20:57 108-67-810.1 10.1
Vinyl acetate ND ug/m3 07/24/19 20:57 108-05-47.2 10.1
Vinyl chloride 6.9 ug/m3 07/24/19 20:57 75-01-42.6 10.1
m&p-Xylene 104 ug/m3 07/24/19 20:57 179601-23-117.9 10.1
o-Xylene 29.3 ug/m3 07/24/19 20:57 95-47-68.9 10.1
Sample:SG-12 (2076)Lab ID:92437876023 Collected:07/12/19 11:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 51.1 ug/m3 07/25/19 21:50 67-64-19.7 4.04
Benzene 50.3 ug/m3 07/25/19 21:50 71-43-21.3 4.04
Bromodichloromethane ND ug/m3 07/25/19 21:50 75-27-45.5 4.04
Bromoform ND ug/m3 07/25/19 21:50 75-25-221.2 4.04
Bromomethane ND ug/m3 07/25/19 21:50 74-83-93.2 4.04
1,3-Butadiene ND ug/m3 07/25/19 21:50 106-99-01.8 4.04
2-Butanone (MEK)ND ug/m3 07/25/19 21:50 78-93-312.1 4.04
Carbon disulfide 7.0 ug/m3 07/25/19 21:50 75-15-02.6 4.04
Carbon tetrachloride ND ug/m3 07/25/19 21:50 56-23-55.2 4.04
Chlorobenzene ND ug/m3 07/25/19 21:50 108-90-73.8 4.04
Chloroethane 9.3 ug/m3 07/25/19 21:50 75-00-32.2 4.04
Chloroform 5.1 ug/m3 07/25/19 21:50 67-66-32.0 4.04
Chloromethane 58.2 ug/m3 07/25/19 21:50 74-87-31.7 4.04
Cyclohexane 21.2 ug/m3 07/25/19 21:50 110-82-77.1 4.04
Dibromochloromethane ND ug/m3 07/25/19 21:50 124-48-17.0 4.04
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 21:50 106-93-43.2 4.04
1,2-Dichlorobenzene ND ug/m3 07/25/19 21:50 95-50-14.9 4.04
1,3-Dichlorobenzene 29.3 ug/m3 07/25/19 21:50 541-73-14.9 4.04
1,4-Dichlorobenzene ND ug/m3 07/25/19 21:50 106-46-712.4 4.04
Dichlorodifluoromethane ND ug/m3 07/25/19 21:50 75-71-84.1 4.04
1,1-Dichloroethane ND ug/m3 07/25/19 21:50 75-34-33.3 4.04
1,2-Dichloroethane ND ug/m3 07/25/19 21:50 107-06-21.7 4.04
1,1-Dichloroethene ND ug/m3 07/25/19 21:50 75-35-43.3 4.04
cis-1,2-Dichloroethene ND ug/m3 07/25/19 21:50 156-59-23.3 4.04
trans-1,2-Dichloroethene ND ug/m3 07/25/19 21:50 156-60-53.3 4.04
1,2-Dichloropropane ND ug/m3 07/25/19 21:50 78-87-53.8 4.04
cis-1,3-Dichloropropene ND ug/m3 07/25/19 21:50 10061-01-53.7 4.04
trans-1,3-Dichloropropene ND ug/m3 07/25/19 21:50 10061-02-63.7 4.04
Dichlorotetrafluoroethane ND ug/m3 07/25/19 21:50 76-14-25.7 4.04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 33 of 72Page 119 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-12 (2076)Lab ID:92437876023 Collected:07/12/19 11:55 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Ethyl acetate ND ug/m3 07/25/19 21:50 141-78-63.0 4.04
Ethylbenzene 36.3 ug/m3 07/25/19 21:50 100-41-43.6 4.04
4-Ethyltoluene ND ug/m3 07/25/19 21:50 622-96-810.1 4.04
n-Heptane 30.6 ug/m3 07/25/19 21:50 142-82-53.4 4.04
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 21:50 87-68-321.9 4.04
n-Hexane 72.5 ug/m3 07/25/19 21:50 110-54-32.9 4.04
2-Hexanone ND ug/m3 07/25/19 21:50 591-78-616.8 4.04
Methylene Chloride 16.9 ug/m3 07/25/19 21:50 75-09-214.3 4.04
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 21:50 108-10-116.8 4.04
Methyl-tert-butyl ether ND ug/m3 07/25/19 21:50 1634-04-414.8 4.04
Naphthalene ND ug/m3 07/25/19 21:50 91-20-310.7 4.04
Propylene 606 ug/m3 07/25/19 21:50 115-07-1 E1.4 4.04
Styrene ND ug/m3 07/25/19 21:50 100-42-53.5 4.04
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 21:50 79-34-52.8 4.04
Tetrachloroethene ND ug/m3 07/25/19 21:50 127-18-42.8 4.04
Tetrahydrofuran ND ug/m3 07/25/19 21:50 109-99-92.4 4.04
Toluene 142 ug/m3 07/25/19 21:50 108-88-33.1 4.04
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 21:50 120-82-130.5 4.04
1,1,1-Trichloroethane ND ug/m3 07/25/19 21:50 71-55-64.5 4.04
1,1,2-Trichloroethane ND ug/m3 07/25/19 21:50 79-00-52.2 4.04
Trichloroethene ND ug/m3 07/25/19 21:50 79-01-62.2 4.04
Trichlorofluoromethane ND ug/m3 07/25/19 21:50 75-69-44.6 4.04
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 21:50 76-13-16.3 4.04
1,2,4-Trimethylbenzene 19.4 ug/m3 07/25/19 21:50 95-63-64.0 4.04
1,3,5-Trimethylbenzene 8.5 ug/m3 07/25/19 21:50 108-67-84.0 4.04
Vinyl acetate ND ug/m3 07/25/19 21:50 108-05-42.9 4.04
Vinyl chloride 24.8 ug/m3 07/25/19 21:50 75-01-41.1 4.04
m&p-Xylene 92.1 ug/m3 07/25/19 21:50 179601-23-17.2 4.04
o-Xylene 25.2 ug/m3 07/25/19 21:50 95-47-63.6 4.04
Sample:DUP-1 (3175)Lab ID:92437876025 Collected:07/12/19 00:06 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone 62.1 ug/m3 07/24/19 18:57 67-64-15.1 2.1
Benzene 1.1 ug/m3 07/24/19 18:57 71-43-20.68 2.1
Bromodichloromethane ND ug/m3 07/24/19 18:57 75-27-42.9 2.1
Bromoform ND ug/m3 07/24/19 18:57 75-25-211.0 2.1
Bromomethane ND ug/m3 07/24/19 18:57 74-83-91.7 2.1
1,3-Butadiene ND ug/m3 07/24/19 18:57 106-99-00.94 2.1
2-Butanone (MEK)16.3 ug/m3 07/24/19 18:57 78-93-36.3 2.1
Carbon disulfide ND ug/m3 07/24/19 18:57 75-15-01.3 2.1
Carbon tetrachloride ND ug/m3 07/24/19 18:57 56-23-52.7 2.1
Chlorobenzene ND ug/m3 07/24/19 18:57 108-90-72.0 2.1
Chloroethane ND ug/m3 07/24/19 18:57 75-00-31.1 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 34 of 72Page 120 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:DUP-1 (3175)Lab ID:92437876025 Collected:07/12/19 00:06 Received:07/20/19 08:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Chloroform ND ug/m3 07/24/19 18:57 67-66-31.0 2.1
Chloromethane ND ug/m3 07/24/19 18:57 74-87-30.88 2.1
Cyclohexane 6.0 ug/m3 07/24/19 18:57 110-82-73.7 2.1
Dibromochloromethane ND ug/m3 07/24/19 18:57 124-48-13.6 2.1
1,2-Dibromoethane (EDB)ND ug/m3 07/24/19 18:57 106-93-41.6 2.1
1,2-Dichlorobenzene ND ug/m3 07/24/19 18:57 95-50-12.6 2.1
1,3-Dichlorobenzene 19.3 ug/m3 07/24/19 18:57 541-73-12.6 2.1
1,4-Dichlorobenzene ND ug/m3 07/24/19 18:57 106-46-76.4 2.1
Dichlorodifluoromethane ND ug/m3 07/24/19 18:57 75-71-82.1 2.1
1,1-Dichloroethane ND ug/m3 07/24/19 18:57 75-34-31.7 2.1
1,2-Dichloroethane ND ug/m3 07/24/19 18:57 107-06-20.86 2.1
1,1-Dichloroethene ND ug/m3 07/24/19 18:57 75-35-41.7 2.1
cis-1,2-Dichloroethene ND ug/m3 07/24/19 18:57 156-59-21.7 2.1
trans-1,2-Dichloroethene ND ug/m3 07/24/19 18:57 156-60-51.7 2.1
1,2-Dichloropropane ND ug/m3 07/24/19 18:57 78-87-52.0 2.1
cis-1,3-Dichloropropene ND ug/m3 07/24/19 18:57 10061-01-51.9 2.1
trans-1,3-Dichloropropene ND ug/m3 07/24/19 18:57 10061-02-61.9 2.1
Dichlorotetrafluoroethane ND ug/m3 07/24/19 18:57 76-14-23.0 2.1
Ethyl acetate ND ug/m3 07/24/19 18:57 141-78-61.5 2.1
Ethylbenzene 3.2 ug/m3 07/24/19 18:57 100-41-41.9 2.1
4-Ethyltoluene ND ug/m3 07/24/19 18:57 622-96-85.2 2.1
n-Heptane ND ug/m3 07/24/19 18:57 142-82-51.7 2.1
Hexachloro-1,3-butadiene ND ug/m3 07/24/19 18:57 87-68-311.4 2.1
n-Hexane ND ug/m3 07/24/19 18:57 110-54-31.5 2.1
2-Hexanone ND ug/m3 07/24/19 18:57 591-78-68.7 2.1
Methylene Chloride ND ug/m3 07/24/19 18:57 75-09-27.4 2.1
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/24/19 18:57 108-10-18.7 2.1
Methyl-tert-butyl ether ND ug/m3 07/24/19 18:57 1634-04-47.7 2.1
Naphthalene ND ug/m3 07/24/19 18:57 91-20-35.6 2.1
Propylene ND ug/m3 07/24/19 18:57 115-07-10.74 2.1
Styrene ND ug/m3 07/24/19 18:57 100-42-51.8 2.1
1,1,2,2-Tetrachloroethane ND ug/m3 07/24/19 18:57 79-34-51.5 2.1
Tetrachloroethene ND ug/m3 07/24/19 18:57 127-18-41.4 2.1
Tetrahydrofuran ND ug/m3 07/24/19 18:57 109-99-91.3 2.1
Toluene 9.9 ug/m3 07/24/19 18:57 108-88-31.6 2.1
1,2,4-Trichlorobenzene ND ug/m3 07/24/19 18:57 120-82-115.8 2.1
1,1,1-Trichloroethane ND ug/m3 07/24/19 18:57 71-55-62.3 2.1
1,1,2-Trichloroethane ND ug/m3 07/24/19 18:57 79-00-51.2 2.1
Trichloroethene ND ug/m3 07/24/19 18:57 79-01-61.1 2.1
Trichlorofluoromethane ND ug/m3 07/24/19 18:57 75-69-42.4 2.1
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/24/19 18:57 76-13-13.3 2.1
1,2,4-Trimethylbenzene 6.4 ug/m3 07/24/19 18:57 95-63-62.1 2.1
1,3,5-Trimethylbenzene ND ug/m3 07/24/19 18:57 108-67-82.1 2.1
Vinyl acetate ND ug/m3 07/24/19 18:57 108-05-41.5 2.1
Vinyl chloride ND ug/m3 07/24/19 18:57 75-01-40.55 2.1
m&p-Xylene 11.5 ug/m3 07/24/19 18:57 179601-23-13.7 2.1
o-Xylene 5.0 ug/m3 07/24/19 18:57 95-47-61.9 2.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 35 of 72Page 121 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-14 (3527) re-test Lab ID:92437876026 Collected:07/19/19 15:20 Received:07/20/19 09:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
Acetone ND ug/m3 07/25/19 22:50 67-64-181.0 33.6
Benzene ND ug/m3 07/25/19 22:50 71-43-210.9 33.6
Bromodichloromethane ND ug/m3 07/25/19 22:50 75-27-445.7 33.6
Bromoform ND ug/m3 07/25/19 22:50 75-25-217633.6
Bromomethane ND ug/m3 07/25/19 22:50 74-83-926.5 33.6
1,3-Butadiene ND ug/m3 07/25/19 22:50 106-99-015.1 33.6
2-Butanone (MEK)ND ug/m3 07/25/19 22:50 78-93-310133.6
Carbon disulfide ND ug/m3 07/25/19 22:50 75-15-021.3 33.6
Carbon tetrachloride ND ug/m3 07/25/19 22:50 56-23-543.0 33.6
Chlorobenzene ND ug/m3 07/25/19 22:50 108-90-731.4 33.6
Chloroethane ND ug/m3 07/25/19 22:50 75-00-318.0 33.6
Chloroform ND ug/m3 07/25/19 22:50 67-66-316.7 33.6
Chloromethane ND ug/m3 07/25/19 22:50 74-87-314.1 33.6
Cyclohexane ND ug/m3 07/25/19 22:50 110-82-758.8 33.6
Dibromochloromethane ND ug/m3 07/25/19 22:50 124-48-158.1 33.6
1,2-Dibromoethane (EDB)ND ug/m3 07/25/19 22:50 106-93-426.2 33.6
1,2-Dichlorobenzene ND ug/m3 07/25/19 22:50 95-50-141.0 33.6
1,3-Dichlorobenzene ND ug/m3 07/25/19 22:50 541-73-141.0 33.6
1,4-Dichlorobenzene ND ug/m3 07/25/19 22:50 106-46-710333.6
Dichlorodifluoromethane ND ug/m3 07/25/19 22:50 75-71-833.9 33.6
1,1-Dichloroethane ND ug/m3 07/25/19 22:50 75-34-327.7 33.6
1,2-Dichloroethane ND ug/m3 07/25/19 22:50 107-06-213.8 33.6
1,1-Dichloroethene ND ug/m3 07/25/19 22:50 75-35-427.1 33.6
cis-1,2-Dichloroethene ND ug/m3 07/25/19 22:50 156-59-227.1 33.6
trans-1,2-Dichloroethene ND ug/m3 07/25/19 22:50 156-60-527.1 33.6
1,2-Dichloropropane ND ug/m3 07/25/19 22:50 78-87-531.6 33.6
cis-1,3-Dichloropropene ND ug/m3 07/25/19 22:50 10061-01-531.0 33.6
trans-1,3-Dichloropropene ND ug/m3 07/25/19 22:50 10061-02-631.0 33.6
Dichlorotetrafluoroethane ND ug/m3 07/25/19 22:50 76-14-247.7 33.6
Ethyl acetate ND ug/m3 07/25/19 22:50 141-78-624.6 33.6
Ethylbenzene 38.7 ug/m3 07/25/19 22:50 100-41-429.7 33.6
4-Ethyltoluene ND ug/m3 07/25/19 22:50 622-96-884.0 33.6
n-Heptane ND ug/m3 07/25/19 22:50 142-82-528.0 33.6
Hexachloro-1,3-butadiene ND ug/m3 07/25/19 22:50 87-68-318233.6
n-Hexane ND ug/m3 07/25/19 22:50 110-54-324.1 33.6
2-Hexanone ND ug/m3 07/25/19 22:50 591-78-614033.6
Methylene Chloride ND ug/m3 07/25/19 22:50 75-09-211933.6
4-Methyl-2-pentanone (MIBK)ND ug/m3 07/25/19 22:50 108-10-114033.6
Methyl-tert-butyl ether ND ug/m3 07/25/19 22:50 1634-04-412333.6
Naphthalene ND ug/m3 07/25/19 22:50 91-20-389.4 33.6
Propylene 85.8 ug/m3 07/25/19 22:50 115-07-111.8 33.6
Styrene ND ug/m3 07/25/19 22:50 100-42-529.1 33.6
1,1,2,2-Tetrachloroethane ND ug/m3 07/25/19 22:50 79-34-523.5 33.6
Tetrachloroethene ND ug/m3 07/25/19 22:50 127-18-423.2 33.6
Tetrahydrofuran ND ug/m3 07/25/19 22:50 109-99-920.2 33.6
Toluene 118 ug/m3 07/25/19 22:50 108-88-325.7 33.6
1,2,4-Trichlorobenzene ND ug/m3 07/25/19 22:50 120-82-125333.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 36 of 72Page 122 of 158
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Sample:SG-14 (3527) re-test Lab ID:92437876026 Collected:07/19/19 15:20 Received:07/20/19 09:45 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: TO-15TO15 MSV AIR
1,1,1-Trichloroethane ND ug/m3 07/25/19 22:50 71-55-637.3 33.6
1,1,2-Trichloroethane ND ug/m3 07/25/19 22:50 79-00-518.6 33.6
Trichloroethene ND ug/m3 07/25/19 22:50 79-01-618.3 33.6
Trichlorofluoromethane ND ug/m3 07/25/19 22:50 75-69-438.3 33.6
1,1,2-Trichlorotrifluoroethane ND ug/m3 07/25/19 22:50 76-13-152.4 33.6
1,2,4-Trimethylbenzene 141 ug/m3 07/25/19 22:50 95-63-633.6 33.6
1,3,5-Trimethylbenzene 62.1 ug/m3 07/25/19 22:50 108-67-833.6 33.6
Vinyl acetate ND ug/m3 07/25/19 22:50 108-05-424.1 33.6
Vinyl chloride ND ug/m3 07/25/19 22:50 75-01-48.7 33.6
m&p-Xylene 182 ug/m3 07/25/19 22:50 179601-23-159.5 33.6
o-Xylene 63.8 ug/m3 07/25/19 22:50 95-47-629.7 33.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 37 of 72Page 123 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621628
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876002, 92437876003, 92437876004, 92437876005, 92437876006, 92437876007, 92437876008,
92437876009, 92437876010, 92437876011, 92437876012, 92437876014, 92437876015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355758
Associated Lab Samples:92437876002, 92437876003, 92437876004, 92437876005, 92437876006, 92437876007, 92437876008,
92437876009, 92437876010, 92437876011, 92437876012, 92437876014, 92437876015
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 07/24/19 08:59
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 07/24/19 08:59
1,1,2-Trichloroethane ug/m3 ND 0.56 07/24/19 08:59
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 07/24/19 08:59
1,1-Dichloroethane ug/m3 ND 0.82 07/24/19 08:59
1,1-Dichloroethene ug/m3 ND 0.81 07/24/19 08:59
1,2,4-Trichlorobenzene ug/m3 ND 7.5 07/24/19 08:59
1,2,4-Trimethylbenzene ug/m3 ND 1.0 07/24/19 08:59
1,2-Dibromoethane (EDB)ug/m3 ND 0.78 07/24/19 08:59
1,2-Dichlorobenzene ug/m3 ND 1.2 07/24/19 08:59
1,2-Dichloroethane ug/m3 ND 0.41 07/24/19 08:59
1,2-Dichloropropane ug/m3 ND 0.94 07/24/19 08:59
1,3,5-Trimethylbenzene ug/m3 ND 1.0 07/24/19 08:59
1,3-Butadiene ug/m3 ND 0.45 07/24/19 08:59
1,3-Dichlorobenzene ug/m3 ND 1.2 07/24/19 08:59
1,4-Dichlorobenzene ug/m3 ND 3.1 07/24/19 08:59
2-Butanone (MEK)ug/m3 ND 3.0 07/24/19 08:59
2-Hexanone ug/m3 ND 4.2 07/24/19 08:59
4-Ethyltoluene ug/m3 ND 2.5 07/24/19 08:59
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 07/24/19 08:59
Acetone ug/m3 ND 2.4 07/24/19 08:59
Benzene ug/m3 ND 0.32 07/24/19 08:59
Bromodichloromethane ug/m3 ND 1.4 07/24/19 08:59
Bromoform ug/m3 ND 5.2 07/24/19 08:59
Bromomethane ug/m3 ND 0.79 07/24/19 08:59
Carbon disulfide ug/m3 ND 0.63 07/24/19 08:59
Carbon tetrachloride ug/m3 ND 1.3 07/24/19 08:59
Chlorobenzene ug/m3 ND 0.94 07/24/19 08:59
Chloroethane ug/m3 ND 0.54 07/24/19 08:59
Chloroform ug/m3 ND 0.50 07/24/19 08:59
Chloromethane ug/m3 ND 0.42 07/24/19 08:59
cis-1,2-Dichloroethene ug/m3 ND 0.81 07/24/19 08:59
cis-1,3-Dichloropropene ug/m3 ND 0.92 07/24/19 08:59
Cyclohexane ug/m3 ND 1.8 07/24/19 08:59
Dibromochloromethane ug/m3 ND 1.7 07/24/19 08:59
Dichlorodifluoromethane ug/m3 ND 1.0 07/24/19 08:59
Dichlorotetrafluoroethane ug/m3 ND 1.4 07/24/19 08:59
Ethyl acetate ug/m3 ND 0.73 07/24/19 08:59
Ethylbenzene ug/m3 ND 0.88 07/24/19 08:59
Hexachloro-1,3-butadiene ug/m3 ND 5.4 07/24/19 08:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
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Minneapolis, MN 55414
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355758
Associated Lab Samples:92437876002, 92437876003, 92437876004, 92437876005, 92437876006, 92437876007, 92437876008,
92437876009, 92437876010, 92437876011, 92437876012, 92437876014, 92437876015
Matrix:Air
Analyzed
m&p-Xylene ug/m3 ND 1.8 07/24/19 08:59
Methyl-tert-butyl ether ug/m3 ND 3.7 07/24/19 08:59
Methylene Chloride ug/m3 ND 3.5 07/24/19 08:59
n-Heptane ug/m3 ND 0.83 07/24/19 08:59
n-Hexane ug/m3 ND 0.72 07/24/19 08:59
Naphthalene ug/m3 ND 2.7 07/24/19 08:59
o-Xylene ug/m3 ND 0.88 07/24/19 08:59
Propylene ug/m3 ND 0.35 07/24/19 08:59
Styrene ug/m3 ND 0.87 07/24/19 08:59
Tetrachloroethene ug/m3 ND 0.69 07/24/19 08:59
Tetrahydrofuran ug/m3 ND 0.60 07/24/19 08:59
Toluene ug/m3 ND 0.77 07/24/19 08:59
trans-1,2-Dichloroethene ug/m3 ND 0.81 07/24/19 08:59
trans-1,3-Dichloropropene ug/m3 ND 0.92 07/24/19 08:59
Trichloroethene ug/m3 ND 0.55 07/24/19 08:59
Trichlorofluoromethane ug/m3 ND 1.1 07/24/19 08:59
Vinyl acetate ug/m3 ND 0.72 07/24/19 08:59
Vinyl chloride ug/m3 ND 0.26 07/24/19 08:59
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355759LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 54.355.5 98 70-130
1,1,2,2-Tetrachloroethane ug/m3 73.769.8 106 70-132
1,1,2-Trichloroethane ug/m3 54.555.5 98 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 75.777.9 97 70-130
1,1-Dichloroethane ug/m3 39.341.1 96 70-130
1,1-Dichloroethene ug/m3 39.140.3 97 70-130
1,2,4-Trichlorobenzene ug/m3 75.275.4 100 56-130
1,2,4-Trimethylbenzene ug/m3 54.550 109 70-134
1,2-Dibromoethane (EDB)ug/m3 78.878.1 101 70-130
1,2-Dichlorobenzene ug/m3 65.561.1 107 70-132
1,2-Dichloroethane ug/m3 39.441.1 96 70-130
1,2-Dichloropropane ug/m3 44.547 95 70-130
1,3,5-Trimethylbenzene ug/m3 49.050 98 70-132
1,3-Butadiene ug/m3 21.822.5 97 65-130
1,3-Dichlorobenzene ug/m3 64.861.1 106 70-137
1,4-Dichlorobenzene ug/m3 66.361.1 108 70-134
2-Butanone (MEK)ug/m3 26.330 88 70-130
2-Hexanone ug/m3 41.241.6 99 70-135
4-Ethyltoluene ug/m3 53.350 107 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 42.141.6 101 70-131
Acetone ug/m3 107121 89 67-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 39 of 72Page 125 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355759LABORATORY CONTROL SAMPLE:
LCSSpike
Benzene ug/m3 34.932.5 107 70-130
Bromodichloromethane ug/m3 67.868.1 100 70-130
Bromoform ug/m3 104105 99 70-132
Bromomethane ug/m3 37.939.5 96 69-130
Carbon disulfide ug/m3 31.131.6 98 56-137
Carbon tetrachloride ug/m3 62.264 97 66-131
Chlorobenzene ug/m3 45.246.8 97 70-130
Chloroethane ug/m3 24.026.8 90 70-130
Chloroform ug/m3 48.049.6 97 70-130
Chloromethane ug/m3 19.821 94 66-130
cis-1,2-Dichloroethene ug/m3 38.740.3 96 70-130
cis-1,3-Dichloropropene ug/m3 45.746.1 99 70-133
Cyclohexane ug/m3 33.335 95 68-132
Dibromochloromethane ug/m3 89.486.6 103 70-130
Dichlorodifluoromethane ug/m3 47.450.3 94 70-130
Dichlorotetrafluoroethane ug/m3 68.471 96 70-130
Ethyl acetate ug/m3 34.836.6 95 69-130
Ethylbenzene ug/m3 41.744.1 94 67-131
Hexachloro-1,3-butadiene ug/m3 113108 105 66-137
m&p-Xylene ug/m3 82.188.3 93 70-132
Methyl-tert-butyl ether ug/m3 35.236.6 96 70-130
Methylene Chloride ug/m3 161177 91 65-130
n-Heptane ug/m3 38.141.7 91 65-130
n-Hexane ug/m3 32.535.8 91 66-130
Naphthalene ug/m3 52.453.3 98 56-130
o-Xylene ug/m3 41.744.1 95 70-130
Propylene ug/m3 15.517.5 89 67-130
Styrene ug/m3 46.943.3 108 69-136
Tetrachloroethene ug/m3 75.068.9 109 70-130
Tetrahydrofuran ug/m3 27.730 92 68-131
Toluene ug/m3 36.238.3 94 70-130
trans-1,2-Dichloroethene ug/m3 38.640.3 96 70-130
trans-1,3-Dichloropropene ug/m3 46.346.1 100 70-134
Trichloroethene ug/m3 58.954.6 108 70-130
Trichlorofluoromethane ug/m3 53.557.1 94 65-130
Vinyl acetate ug/m3 33.135.8 92 61-133
Vinyl chloride ug/m3 24.126 93 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484068001
3357274SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 40 of 72Page 126 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484068001
3357274SAMPLE DUPLICATE:
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 42.9 242.1
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 11.2 410.7
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 3.0 23.1
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 6.2 45.9
2-Hexanone ug/m3 1.7JND
4-Ethyltoluene ug/m3 12.0 1810.0
4-Methyl-2-pentanone (MIBK)ug/m3 3.5JND
Acetone ug/m3 21.8 021.8
Benzene ug/m3 5.0 54.7
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.3 02.3
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 19.2 418.5
Chloromethane ug/m3 .45JND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 3.9 73.6
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.5 12.5
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 11.6 111.4
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 56.3 156.5
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 2.9JND
n-Heptane ug/m3 4.3 64.0
n-Hexane ug/m3 6.9 66.5
Naphthalene ug/m3 5.1 54.8
o-Xylene ug/m3 19.1 118.9
Propylene ug/m3 85.4 E185.9
Styrene ug/m3 3.0 82.7
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 3.0 33.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 41 of 72Page 127 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484068001
3357274SAMPLE DUPLICATE:
Toluene ug/m3 42.6 142.9
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.5JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
10484068002
3357275SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 24.4 224.8
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 6.1 86.6
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 1.8JND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 5.3JND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 6.9 27.1
4-Methyl-2-pentanone (MIBK)ug/m3 2.2JND
Acetone ug/m3 22.0 222.6
Benzene ug/m3 4.5 24.6
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.6 112.9
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 4.0 43.8
Chloromethane ug/m3 .65JND
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 2.7JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 42 of 72Page 128 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484068002
3357275SAMPLE DUPLICATE:
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 4.5 14.6
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 8.7 39.0
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 41.1 342.2
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 6.9ND
n-Heptane ug/m3 2.7 62.6
n-Hexane ug/m3 4.2 14.1
Naphthalene ug/m3 3.7JND
o-Xylene ug/m3 14.3 415.0
Propylene ug/m3 29.3 430.5
Styrene ug/m3 2.3 22.2
Tetrachloroethene ug/m3 1.2JND
Tetrahydrofuran ug/m3 2.2 22.2
Toluene ug/m3 28.8 129.0
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.3JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 43 of 72Page 129 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621640
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355839
Associated Lab Samples:92437876001
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 0.56 07/24/19 09:54
1,1,2,2-Tetrachloroethane ug/m3 ND 0.35 07/24/19 09:54
1,1,2-Trichloroethane ug/m3 ND 0.28 07/24/19 09:54
1,1,2-Trichlorotrifluoroethane ug/m3 ND 0.78 07/24/19 09:54
1,1-Dichloroethane ug/m3 ND 0.41 07/24/19 09:54
1,1-Dichloroethene ug/m3 ND 0.40 07/24/19 09:54
1,2,4-Trichlorobenzene ug/m3 ND 3.8 07/24/19 09:54
1,2,4-Trimethylbenzene ug/m3 ND 0.50 07/24/19 09:54
1,2-Dibromoethane (EDB)ug/m3 ND 0.39 07/24/19 09:54
1,2-Dichlorobenzene ug/m3 ND 0.61 07/24/19 09:54
1,2-Dichloroethane ug/m3 ND 0.21 07/24/19 09:54
1,2-Dichloropropane ug/m3 ND 0.47 07/24/19 09:54
1,3,5-Trimethylbenzene ug/m3 ND 0.50 07/24/19 09:54
1,3-Butadiene ug/m3 ND 0.22 07/24/19 09:54
1,3-Dichlorobenzene ug/m3 ND 0.61 07/24/19 09:54
1,4-Dichlorobenzene ug/m3 ND 1.5 07/24/19 09:54
2-Butanone (MEK)ug/m3 ND 1.5 07/24/19 09:54
2-Hexanone ug/m3 ND 2.1 07/24/19 09:54
4-Ethyltoluene ug/m3 ND 1.2 07/24/19 09:54
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 07/24/19 09:54
Acetone ug/m3 ND 1.2 07/24/19 09:54
Benzene ug/m3 ND 0.16 07/24/19 09:54
Bromodichloromethane ug/m3 ND 0.68 07/24/19 09:54
Bromoform ug/m3 ND 2.6 07/24/19 09:54
Bromomethane ug/m3 ND 0.39 07/24/19 09:54
Carbon disulfide ug/m3 ND 0.32 07/24/19 09:54
Carbon tetrachloride ug/m3 ND 0.64 07/24/19 09:54
Chlorobenzene ug/m3 ND 0.47 07/24/19 09:54
Chloroethane ug/m3 ND 0.27 07/24/19 09:54
Chloroform ug/m3 ND 0.25 07/24/19 09:54
Chloromethane ug/m3 ND 0.21 07/24/19 09:54
cis-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 09:54
cis-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 09:54
Cyclohexane ug/m3 ND 0.88 07/24/19 09:54
Dibromochloromethane ug/m3 ND 0.86 07/24/19 09:54
Dichlorodifluoromethane ug/m3 ND 0.50 07/24/19 09:54
Dichlorotetrafluoroethane ug/m3 ND 0.71 07/24/19 09:54
Ethyl acetate ug/m3 ND 0.37 07/24/19 09:54
Ethylbenzene ug/m3 ND 0.44 07/24/19 09:54
Hexachloro-1,3-butadiene ug/m3 ND 2.7 07/24/19 09:54
m&p-Xylene ug/m3 ND 0.88 07/24/19 09:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 44 of 72Page 130 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355839
Associated Lab Samples:92437876001
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 1.8 07/24/19 09:54
Methylene Chloride ug/m3 ND 1.8 07/24/19 09:54
n-Heptane ug/m3 ND 0.42 07/24/19 09:54
n-Hexane ug/m3 ND 0.36 07/24/19 09:54
Naphthalene ug/m3 ND 1.3 07/24/19 09:54
o-Xylene ug/m3 ND 0.44 07/24/19 09:54
Propylene ug/m3 ND 0.18 07/24/19 09:54
Styrene ug/m3 ND 0.43 07/24/19 09:54
Tetrachloroethene ug/m3 ND 0.34 07/24/19 09:54
Tetrahydrofuran ug/m3 ND 0.30 07/24/19 09:54
Toluene ug/m3 ND 0.38 07/24/19 09:54
trans-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 09:54
trans-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 09:54
Trichloroethene ug/m3 ND 0.27 07/24/19 09:54
Trichlorofluoromethane ug/m3 ND 0.57 07/24/19 09:54
Vinyl acetate ug/m3 ND 0.89 MN07/24/19 09:54
Vinyl chloride ug/m3 ND 0.13 07/24/19 09:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355840LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 62.755.5 113 70-130
1,1,2,2-Tetrachloroethane ug/m3 72.569.8 104 70-132
1,1,2-Trichloroethane ug/m3 58.755.5 106 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 86.177.9 111 70-130
1,1-Dichloroethane ug/m3 44.941.1 109 70-130
1,1-Dichloroethene ug/m3 43.840.3 109 70-130
1,2,4-Trichlorobenzene ug/m3 73.875.4 98 56-130
1,2,4-Trimethylbenzene ug/m3 56.950 114 70-134
1,2-Dibromoethane (EDB)ug/m3 89.278.1 114 70-130
1,2-Dichlorobenzene ug/m3 70.561.1 115 70-132
1,2-Dichloroethane ug/m3 46.641.1 113 70-130
1,2-Dichloropropane ug/m3 54.747 116 70-130
1,3,5-Trimethylbenzene ug/m3 56.750 113 70-132
1,3-Butadiene ug/m3 26.122.5 116 65-130
1,3-Dichlorobenzene ug/m3 71.061.1 116 70-137
1,4-Dichlorobenzene ug/m3 72.461.1 118 70-134
2-Butanone (MEK)ug/m3 30.630 102 70-130
2-Hexanone ug/m3 46.441.6 111 70-135
4-Ethyltoluene ug/m3 57.650 115 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 44.741.6 107 70-131
Acetone ug/m3 117121 97 67-130
Benzene ug/m3 35.132.5 108 70-130
Bromodichloromethane ug/m3 77.068.1 113 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
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Page 45 of 72Page 131 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355840LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 111105 106 70-132
Bromomethane ug/m3 46.239.5 117 69-130
Carbon disulfide ug/m3 35.231.6 111 56-137
Carbon tetrachloride ug/m3 71.264 111 66-131
Chlorobenzene ug/m3 51.846.8 111 70-130
Chloroethane ug/m3 33.926.8 126 70-130
Chloroform ug/m3 55.149.6 111 70-130
Chloromethane ug/m3 24.421 116 66-130
cis-1,2-Dichloroethene ug/m3 43.140.3 107 70-130
cis-1,3-Dichloropropene ug/m3 51.946.1 112 70-133
Cyclohexane ug/m3 37.635 107 68-132
Dibromochloromethane ug/m3 10586.6 121 70-130
Dichlorodifluoromethane ug/m3 56.650.3 113 70-130
Dichlorotetrafluoroethane ug/m3 82.371 116 70-130
Ethyl acetate ug/m3 41.536.6 113 69-130
Ethylbenzene ug/m3 51.544.1 117 67-131
Hexachloro-1,3-butadiene ug/m3 128108 118 66-137
m&p-Xylene ug/m3 10488.3 117 70-132
Methyl-tert-butyl ether ug/m3 40.736.6 111 70-130
Methylene Chloride ug/m3 184177 104 65-130
n-Heptane ug/m3 44.341.7 106 65-130
n-Hexane ug/m3 38.735.8 108 66-130
Naphthalene ug/m3 51.253.3 96 56-130
o-Xylene ug/m3 50.944.1 115 70-130
Propylene ug/m3 18.017.5 103 67-130
Styrene ug/m3 49.443.3 114 69-136
Tetrachloroethene ug/m3 73.368.9 106 70-130
Tetrahydrofuran ug/m3 31.030 103 68-131
Toluene ug/m3 43.138.3 113 70-130
trans-1,2-Dichloroethene ug/m3 45.040.3 112 70-130
trans-1,3-Dichloropropene ug/m3 54.146.1 117 70-134
Trichloroethene ug/m3 58.454.6 107 70-130
Trichlorofluoromethane ug/m3 66.257.1 116 65-130
Vinyl acetate ug/m3 37.535.8 105 61-133
Vinyl chloride ug/m3 31.226 120 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484111004
3357227SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 46 of 72Page 132 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484111004
3357227SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 NDND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 17.8 218.2
Benzene ug/m3 0.55ND
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 NDND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.4 41.4
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.7 62.9
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 NDND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 55.5 457.6
n-Heptane ug/m3 .81JND
n-Hexane ug/m3 4.8 35.0
Naphthalene ug/m3 NDND
o-Xylene ug/m3 NDND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 NDND
Toluene ug/m3 1.8 21.8
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 47 of 72Page 133 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484111004
3357227SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.5JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
75112382002
3357229SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 2.2 82.4
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 .76JND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 2.6JND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 27.9 328.7
Benzene ug/m3 1.9 22.0
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 NDND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 1.2 51.3
Chloromethane ug/m3 1.6 01.6
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 3.2 33.3
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 3.0 13.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 48 of 72Page 134 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
75112382002
3357229SAMPLE DUPLICATE:
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 17.2 618.4
Ethylbenzene ug/m3 .93JND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 2.6JND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 4.5JND
n-Heptane ug/m3 1.5 01.5
n-Hexane ug/m3 4.7 44.9
Naphthalene ug/m3 NDND
o-Xylene ug/m3 1.1JND
Propylene ug/m3 NDND
Styrene ug/m3 1.8 51.9
Tetrachloroethene ug/m3 .99JND
Tetrahydrofuran ug/m3 NDND
Toluene ug/m3 4.2 74.5
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 5.6 35.7
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 49 of 72Page 135 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621644
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876017, 92437876019, 92437876020, 92437876021, 92437876022, 92437876025
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355846
Associated Lab Samples:92437876017, 92437876019, 92437876020, 92437876021, 92437876022, 92437876025
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 0.56 07/24/19 10:45
1,1,2,2-Tetrachloroethane ug/m3 ND 0.35 07/24/19 10:45
1,1,2-Trichloroethane ug/m3 ND 0.28 07/24/19 10:45
1,1,2-Trichlorotrifluoroethane ug/m3 ND 0.78 07/24/19 10:45
1,1-Dichloroethane ug/m3 ND 0.41 07/24/19 10:45
1,1-Dichloroethene ug/m3 ND 0.40 07/24/19 10:45
1,2,4-Trichlorobenzene ug/m3 ND 3.8 07/24/19 10:45
1,2,4-Trimethylbenzene ug/m3 ND 0.50 07/24/19 10:45
1,2-Dibromoethane (EDB)ug/m3 ND 0.39 07/24/19 10:45
1,2-Dichlorobenzene ug/m3 ND 0.61 07/24/19 10:45
1,2-Dichloroethane ug/m3 ND 0.21 07/24/19 10:45
1,2-Dichloropropane ug/m3 ND 0.47 07/24/19 10:45
1,3,5-Trimethylbenzene ug/m3 ND 0.50 07/24/19 10:45
1,3-Butadiene ug/m3 ND 0.22 07/24/19 10:45
1,3-Dichlorobenzene ug/m3 ND 0.61 07/24/19 10:45
1,4-Dichlorobenzene ug/m3 ND 1.5 07/24/19 10:45
2-Butanone (MEK)ug/m3 ND 1.5 07/24/19 10:45
2-Hexanone ug/m3 ND 2.1 07/24/19 10:45
4-Ethyltoluene ug/m3 ND 1.2 07/24/19 10:45
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 07/24/19 10:45
Acetone ug/m3 ND 1.2 07/24/19 10:45
Benzene ug/m3 ND 0.16 07/24/19 10:45
Bromodichloromethane ug/m3 ND 0.68 07/24/19 10:45
Bromoform ug/m3 ND 2.6 07/24/19 10:45
Bromomethane ug/m3 ND 0.39 07/24/19 10:45
Carbon disulfide ug/m3 ND 0.32 07/24/19 10:45
Carbon tetrachloride ug/m3 ND 0.64 07/24/19 10:45
Chlorobenzene ug/m3 ND 0.47 07/24/19 10:45
Chloroethane ug/m3 ND 0.27 07/24/19 10:45
Chloroform ug/m3 ND 0.25 07/24/19 10:45
Chloromethane ug/m3 ND 0.21 07/24/19 10:45
cis-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 10:45
cis-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 10:45
Cyclohexane ug/m3 ND 0.88 07/24/19 10:45
Dibromochloromethane ug/m3 ND 0.86 07/24/19 10:45
Dichlorodifluoromethane ug/m3 ND 0.50 07/24/19 10:45
Dichlorotetrafluoroethane ug/m3 ND 0.71 07/24/19 10:45
Ethyl acetate ug/m3 ND 0.37 07/24/19 10:45
Ethylbenzene ug/m3 ND 0.44 07/24/19 10:45
Hexachloro-1,3-butadiene ug/m3 ND 2.7 07/24/19 10:45
m&p-Xylene ug/m3 ND 0.88 07/24/19 10:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 50 of 72Page 136 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3355846
Associated Lab Samples:92437876017, 92437876019, 92437876020, 92437876021, 92437876022, 92437876025
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 1.8 07/24/19 10:45
Methylene Chloride ug/m3 ND 1.8 07/24/19 10:45
n-Heptane ug/m3 ND 0.42 07/24/19 10:45
n-Hexane ug/m3 ND 0.36 07/24/19 10:45
Naphthalene ug/m3 ND 1.3 07/24/19 10:45
o-Xylene ug/m3 ND 0.44 07/24/19 10:45
Propylene ug/m3 ND 0.18 07/24/19 10:45
Styrene ug/m3 ND 0.43 07/24/19 10:45
Tetrachloroethene ug/m3 ND 0.34 07/24/19 10:45
Tetrahydrofuran ug/m3 ND 0.30 07/24/19 10:45
Toluene ug/m3 ND 0.38 07/24/19 10:45
trans-1,2-Dichloroethene ug/m3 ND 0.40 07/24/19 10:45
trans-1,3-Dichloropropene ug/m3 ND 0.46 07/24/19 10:45
Trichloroethene ug/m3 ND 0.27 07/24/19 10:45
Trichlorofluoromethane ug/m3 ND 0.57 07/24/19 10:45
Vinyl acetate ug/m3 ND 0.36 07/24/19 10:45
Vinyl chloride ug/m3 ND 0.13 07/24/19 10:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355847LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 63.055.5 114 70-130
1,1,2,2-Tetrachloroethane ug/m3 79.069.8 113 70-132
1,1,2-Trichloroethane ug/m3 65.755.5 118 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 90.277.9 116 70-130
1,1-Dichloroethane ug/m3 45.841.1 111 70-130
1,1-Dichloroethene ug/m3 48.440.3 120 70-130
1,2,4-Trichlorobenzene ug/m3 69.675.4 92 56-130
1,2,4-Trimethylbenzene ug/m3 57.150 114 70-134
1,2-Dibromoethane (EDB)ug/m3 90.378.1 116 70-130
1,2-Dichlorobenzene ug/m3 70.361.1 115 70-132
1,2-Dichloroethane ug/m3 47.641.1 116 70-130
1,2-Dichloropropane ug/m3 55.347 118 70-130
1,3,5-Trimethylbenzene ug/m3 53.550 107 70-132
1,3-Butadiene ug/m3 30.4 CH,L322.5 135 65-130
1,3-Dichlorobenzene ug/m3 71.361.1 117 70-137
1,4-Dichlorobenzene ug/m3 71.661.1 117 70-134
2-Butanone (MEK)ug/m3 28.130 94 70-130
2-Hexanone ug/m3 50.941.6 122 70-135
4-Ethyltoluene ug/m3 56.450 113 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 48.341.6 116 70-131
Acetone ug/m3 128121 106 67-130
Benzene ug/m3 35.032.5 108 70-130
Bromodichloromethane ug/m3 77.068.1 113 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 51 of 72Page 137 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355847LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 128105 122 70-132
Bromomethane ug/m3 50.139.5 127 69-130
Carbon disulfide ug/m3 35.031.6 111 56-137
Carbon tetrachloride ug/m3 72.464 113 66-131
Chlorobenzene ug/m3 49.546.8 106 70-130
Chloroethane ug/m3 36.0 CH,L326.8 134 70-130
Chloroform ug/m3 55.149.6 111 70-130
Chloromethane ug/m3 25.221 120 66-130
cis-1,2-Dichloroethene ug/m3 43.140.3 107 70-130
cis-1,3-Dichloropropene ug/m3 53.046.1 115 70-133
Cyclohexane ug/m3 38.335 109 68-132
Dibromochloromethane ug/m3 10286.6 118 70-130
Dichlorodifluoromethane ug/m3 51.350.3 102 70-130
Dichlorotetrafluoroethane ug/m3 84.171 118 70-130
Ethyl acetate ug/m3 40.236.6 110 69-130
Ethylbenzene ug/m3 49.344.1 112 67-131
Hexachloro-1,3-butadiene ug/m3 121108 111 66-137
m&p-Xylene ug/m3 96.488.3 109 70-132
Methyl-tert-butyl ether ug/m3 40.536.6 110 70-130
Methylene Chloride ug/m3 185177 105 65-130
n-Heptane ug/m3 45.741.7 110 65-130
n-Hexane ug/m3 38.035.8 106 66-130
Naphthalene ug/m3 49.653.3 93 56-130
o-Xylene ug/m3 46.544.1 105 70-130
Propylene ug/m3 17.617.5 101 67-130
Styrene ug/m3 50.343.3 116 69-136
Tetrachloroethene ug/m3 80.468.9 117 70-130
Tetrahydrofuran ug/m3 34.930 117 68-131
Toluene ug/m3 41.338.3 108 70-130
trans-1,2-Dichloroethene ug/m3 44.240.3 110 70-130
trans-1,3-Dichloropropene ug/m3 55.446.1 120 70-134
Trichloroethene ug/m3 61.954.6 113 70-130
Trichlorofluoromethane ug/m3 67.157.1 118 65-130
Vinyl acetate ug/m3 40.435.8 113 61-133
Vinyl chloride ug/m3 33.126 127 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484108001
3356244SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 52 of 72Page 138 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484108001
3356244SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 7.3 27.5
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 22.2 924.4
Benzene ug/m3 0.93 60.99
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 6.8 86.3
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.3 81.4
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 20.6 220.9
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.5 42.5
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 4.1 24.2
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 12.2 512.9
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 14.5 214.2
n-Heptane ug/m3 6.0 06.0
n-Hexane ug/m3 38.3 339.3
Naphthalene ug/m3 NDND
o-Xylene ug/m3 2.4 42.3
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 3.5 13.5
Toluene ug/m3 74.4 175.1
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 53 of 72Page 139 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484108001
3356244SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 1.0ND
Trichlorofluoromethane ug/m3 2.9 163.4
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
10484108002
3356272SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 3.2JND
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 16.3 914.9
Benzene ug/m3 .26JND
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.1 32.0
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.5 21.5
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.5 22.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 54 of 72Page 140 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484108002
3356272SAMPLE DUPLICATE:
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 NDND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 3.5JND
n-Heptane ug/m3 3.4 23.3
n-Hexane ug/m3 .96JND
Naphthalene ug/m3 NDND
o-Xylene ug/m3 NDND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 4.1 14.2
Toluene ug/m3 137 1136
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 .55JND
Trichlorofluoromethane ug/m3 1.4JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 55 of 72Page 141 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
621953
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357278
Associated Lab Samples:92437876013
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 1.1 07/25/19 08:18
1,1,2,2-Tetrachloroethane ug/m3 ND 0.70 07/25/19 08:18
1,1,2-Trichloroethane ug/m3 ND 0.56 07/25/19 08:18
1,1,2-Trichlorotrifluoroethane ug/m3 ND 1.6 07/25/19 08:18
1,1-Dichloroethane ug/m3 ND 0.82 07/25/19 08:18
1,1-Dichloroethene ug/m3 ND 0.81 07/25/19 08:18
1,2,4-Trichlorobenzene ug/m3 ND 7.5 07/25/19 08:18
1,2,4-Trimethylbenzene ug/m3 ND 1.0 07/25/19 08:18
1,2-Dibromoethane (EDB)ug/m3 ND 0.78 07/25/19 08:18
1,2-Dichlorobenzene ug/m3 ND 1.2 07/25/19 08:18
1,2-Dichloroethane ug/m3 ND 0.41 07/25/19 08:18
1,2-Dichloropropane ug/m3 ND 0.94 07/25/19 08:18
1,3,5-Trimethylbenzene ug/m3 ND 1.0 07/25/19 08:18
1,3-Butadiene ug/m3 ND 0.45 07/25/19 08:18
1,3-Dichlorobenzene ug/m3 ND 1.2 07/25/19 08:18
1,4-Dichlorobenzene ug/m3 ND 3.1 07/25/19 08:18
2-Butanone (MEK)ug/m3 ND 3.0 07/25/19 08:18
2-Hexanone ug/m3 ND 4.2 07/25/19 08:18
4-Ethyltoluene ug/m3 ND 2.5 07/25/19 08:18
4-Methyl-2-pentanone (MIBK)ug/m3 ND 4.2 07/25/19 08:18
Acetone ug/m3 ND 2.4 07/25/19 08:18
Benzene ug/m3 ND 0.32 07/25/19 08:18
Bromodichloromethane ug/m3 ND 1.4 07/25/19 08:18
Bromoform ug/m3 ND 5.2 07/25/19 08:18
Bromomethane ug/m3 ND 0.79 07/25/19 08:18
Carbon disulfide ug/m3 ND 0.63 07/25/19 08:18
Carbon tetrachloride ug/m3 ND 1.3 07/25/19 08:18
Chlorobenzene ug/m3 ND 0.94 07/25/19 08:18
Chloroethane ug/m3 ND 0.54 07/25/19 08:18
Chloroform ug/m3 ND 0.50 07/25/19 08:18
Chloromethane ug/m3 ND 0.42 07/25/19 08:18
cis-1,2-Dichloroethene ug/m3 ND 0.81 07/25/19 08:18
cis-1,3-Dichloropropene ug/m3 ND 0.92 07/25/19 08:18
Cyclohexane ug/m3 ND 1.8 07/25/19 08:18
Dibromochloromethane ug/m3 ND 1.7 07/25/19 08:18
Dichlorodifluoromethane ug/m3 ND 1.0 07/25/19 08:18
Dichlorotetrafluoroethane ug/m3 ND 1.4 07/25/19 08:18
Ethyl acetate ug/m3 ND 0.73 07/25/19 08:18
Ethylbenzene ug/m3 ND 0.88 07/25/19 08:18
Hexachloro-1,3-butadiene ug/m3 ND 5.4 07/25/19 08:18
m&p-Xylene ug/m3 ND 1.8 07/25/19 08:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 56 of 72Page 142 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357278
Associated Lab Samples:92437876013
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 3.7 07/25/19 08:18
Methylene Chloride ug/m3 ND 3.5 07/25/19 08:18
n-Heptane ug/m3 ND 0.83 07/25/19 08:18
n-Hexane ug/m3 ND 0.72 07/25/19 08:18
Naphthalene ug/m3 ND 2.7 07/25/19 08:18
o-Xylene ug/m3 ND 0.88 07/25/19 08:18
Propylene ug/m3 ND 0.35 07/25/19 08:18
Styrene ug/m3 ND 0.87 07/25/19 08:18
Tetrachloroethene ug/m3 ND 0.69 07/25/19 08:18
Tetrahydrofuran ug/m3 ND 0.60 07/25/19 08:18
Toluene ug/m3 ND 0.77 07/25/19 08:18
trans-1,2-Dichloroethene ug/m3 ND 0.81 07/25/19 08:18
trans-1,3-Dichloropropene ug/m3 ND 0.92 07/25/19 08:18
Trichloroethene ug/m3 ND 0.55 07/25/19 08:18
Trichlorofluoromethane ug/m3 ND 1.1 07/25/19 08:18
Vinyl acetate ug/m3 ND 0.72 07/25/19 08:18
Vinyl chloride ug/m3 ND 0.26 07/25/19 08:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357279LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 55.155.5 99 70-130
1,1,2,2-Tetrachloroethane ug/m3 73.569.8 105 70-132
1,1,2-Trichloroethane ug/m3 55.455.5 100 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 76.877.9 99 70-130
1,1-Dichloroethane ug/m3 40.541.1 98 70-130
1,1-Dichloroethene ug/m3 39.940.3 99 70-130
1,2,4-Trichlorobenzene ug/m3 80.975.4 107 56-130
1,2,4-Trimethylbenzene ug/m3 55.550 111 70-134
1,2-Dibromoethane (EDB)ug/m3 80.678.1 103 70-130
1,2-Dichlorobenzene ug/m3 67.561.1 111 70-132
1,2-Dichloroethane ug/m3 40.041.1 97 70-130
1,2-Dichloropropane ug/m3 45.447 97 70-130
1,3,5-Trimethylbenzene ug/m3 50.050 100 70-132
1,3-Butadiene ug/m3 21.622.5 96 65-130
1,3-Dichlorobenzene ug/m3 67.661.1 111 70-137
1,4-Dichlorobenzene ug/m3 69.061.1 113 70-134
2-Butanone (MEK)ug/m3 26.330 88 70-130
2-Hexanone ug/m3 41.941.6 101 70-135
4-Ethyltoluene ug/m3 54.250 109 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 42.841.6 103 70-131
Acetone ug/m3 108121 90 67-130
Benzene ug/m3 35.532.5 109 70-130
Bromodichloromethane ug/m3 68.568.1 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 57 of 72Page 143 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357279LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 102105 97 70-132
Bromomethane ug/m3 38.039.5 96 69-130
Carbon disulfide ug/m3 31.631.6 100 56-137
Carbon tetrachloride ug/m3 64.364 101 66-131
Chlorobenzene ug/m3 46.546.8 99 70-130
Chloroethane ug/m3 25.226.8 94 70-130
Chloroform ug/m3 48.449.6 98 70-130
Chloromethane ug/m3 20.021 96 66-130
cis-1,2-Dichloroethene ug/m3 39.240.3 97 70-130
cis-1,3-Dichloropropene ug/m3 46.346.1 100 70-133
Cyclohexane ug/m3 33.635 96 68-132
Dibromochloromethane ug/m3 91.086.6 105 70-130
Dichlorodifluoromethane ug/m3 47.650.3 95 70-130
Dichlorotetrafluoroethane ug/m3 68.471 96 70-130
Ethyl acetate ug/m3 35.536.6 97 69-130
Ethylbenzene ug/m3 42.344.1 96 67-131
Hexachloro-1,3-butadiene ug/m3 118108 109 66-137
m&p-Xylene ug/m3 83.588.3 95 70-132
Methyl-tert-butyl ether ug/m3 36.036.6 98 70-130
Methylene Chloride ug/m3 164177 93 65-130
n-Heptane ug/m3 38.941.7 93 65-130
n-Hexane ug/m3 33.035.8 92 66-130
Naphthalene ug/m3 54.253.3 102 56-130
o-Xylene ug/m3 42.244.1 96 70-130
Propylene ug/m3 15.817.5 91 67-130
Styrene ug/m3 47.943.3 111 69-136
Tetrachloroethene ug/m3 75.868.9 110 70-130
Tetrahydrofuran ug/m3 27.730 93 68-131
Toluene ug/m3 37.138.3 97 70-130
trans-1,2-Dichloroethene ug/m3 38.840.3 96 70-130
trans-1,3-Dichloropropene ug/m3 46.746.1 101 70-134
Trichloroethene ug/m3 59.854.6 110 70-130
Trichlorofluoromethane ug/m3 54.757.1 96 65-130
Vinyl acetate ug/m3 31.835.8 89 61-133
Vinyl chloride ug/m3 24.526 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 58 of 72Page 144 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
622036
TO-15
TO-15
TO15 MSV AIR Low Level
Associated Lab Samples:92437876016, 92437876018, 92437876023, 92437876026
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357701
Associated Lab Samples:92437876016, 92437876018, 92437876023, 92437876026
Matrix:Air
Analyzed
1,1,1-Trichloroethane ug/m3 ND 0.56 07/25/19 16:53
1,1,2,2-Tetrachloroethane ug/m3 ND 0.35 07/25/19 16:53
1,1,2-Trichloroethane ug/m3 ND 0.28 07/25/19 16:53
1,1,2-Trichlorotrifluoroethane ug/m3 ND 0.78 07/25/19 16:53
1,1-Dichloroethane ug/m3 ND 0.41 07/25/19 16:53
1,1-Dichloroethene ug/m3 ND 0.40 07/25/19 16:53
1,2,4-Trichlorobenzene ug/m3 ND 3.8 07/25/19 16:53
1,2,4-Trimethylbenzene ug/m3 ND 0.50 07/25/19 16:53
1,2-Dibromoethane (EDB)ug/m3 ND 0.39 07/25/19 16:53
1,2-Dichlorobenzene ug/m3 ND 0.61 07/25/19 16:53
1,2-Dichloroethane ug/m3 ND 0.21 07/25/19 16:53
1,2-Dichloropropane ug/m3 ND 0.47 07/25/19 16:53
1,3,5-Trimethylbenzene ug/m3 ND 0.50 07/25/19 16:53
1,3-Butadiene ug/m3 ND 0.22 07/25/19 16:53
1,3-Dichlorobenzene ug/m3 ND 0.61 07/25/19 16:53
1,4-Dichlorobenzene ug/m3 ND 1.5 07/25/19 16:53
2-Butanone (MEK)ug/m3 ND 1.5 07/25/19 16:53
2-Hexanone ug/m3 ND 2.1 07/25/19 16:53
4-Ethyltoluene ug/m3 ND 1.2 07/25/19 16:53
4-Methyl-2-pentanone (MIBK)ug/m3 ND 2.1 07/25/19 16:53
Acetone ug/m3 ND 1.2 07/25/19 16:53
Benzene ug/m3 ND 0.16 07/25/19 16:53
Bromodichloromethane ug/m3 ND 0.68 07/25/19 16:53
Bromoform ug/m3 ND 2.6 07/25/19 16:53
Bromomethane ug/m3 ND 0.39 07/25/19 16:53
Carbon disulfide ug/m3 ND 0.32 07/25/19 16:53
Carbon tetrachloride ug/m3 ND 0.64 07/25/19 16:53
Chlorobenzene ug/m3 ND 0.47 07/25/19 16:53
Chloroethane ug/m3 ND 0.27 07/25/19 16:53
Chloroform ug/m3 ND 0.25 07/25/19 16:53
Chloromethane ug/m3 ND 0.21 07/25/19 16:53
cis-1,2-Dichloroethene ug/m3 ND 0.40 07/25/19 16:53
cis-1,3-Dichloropropene ug/m3 ND 0.46 07/25/19 16:53
Cyclohexane ug/m3 ND 0.88 07/25/19 16:53
Dibromochloromethane ug/m3 ND 0.86 07/25/19 16:53
Dichlorodifluoromethane ug/m3 ND 0.50 07/25/19 16:53
Dichlorotetrafluoroethane ug/m3 ND 0.71 07/25/19 16:53
Ethyl acetate ug/m3 ND 0.37 07/25/19 16:53
Ethylbenzene ug/m3 ND 0.44 07/25/19 16:53
Hexachloro-1,3-butadiene ug/m3 ND 2.7 07/25/19 16:53
m&p-Xylene ug/m3 ND 0.88 07/25/19 16:53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 59 of 72Page 145 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3357701
Associated Lab Samples:92437876016, 92437876018, 92437876023, 92437876026
Matrix:Air
Analyzed
Methyl-tert-butyl ether ug/m3 ND 1.8 07/25/19 16:53
Methylene Chloride ug/m3 ND 1.8 07/25/19 16:53
n-Heptane ug/m3 ND 0.42 07/25/19 16:53
n-Hexane ug/m3 ND 0.36 07/25/19 16:53
Naphthalene ug/m3 ND 1.3 07/25/19 16:53
o-Xylene ug/m3 ND 0.44 07/25/19 16:53
Propylene ug/m3 ND 0.18 07/25/19 16:53
Styrene ug/m3 ND 0.43 07/25/19 16:53
Tetrachloroethene ug/m3 ND 0.34 07/25/19 16:53
Tetrahydrofuran ug/m3 ND 0.30 07/25/19 16:53
Toluene ug/m3 ND 0.38 07/25/19 16:53
trans-1,2-Dichloroethene ug/m3 ND 0.40 07/25/19 16:53
trans-1,3-Dichloropropene ug/m3 ND 0.46 07/25/19 16:53
Trichloroethene ug/m3 ND 0.27 07/25/19 16:53
Trichlorofluoromethane ug/m3 ND 0.57 07/25/19 16:53
Vinyl acetate ug/m3 ND 0.36 07/25/19 16:53
Vinyl chloride ug/m3 ND 0.13 07/25/19 16:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357702LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/m3 56.555.5 102 70-130
1,1,2,2-Tetrachloroethane ug/m3 73.769.8 106 70-132
1,1,2-Trichloroethane ug/m3 58.655.5 106 70-130
1,1,2-Trichlorotrifluoroethane ug/m3 80.077.9 103 70-130
1,1-Dichloroethane ug/m3 41.141.1 100 70-130
1,1-Dichloroethene ug/m3 39.840.3 99 70-130
1,2,4-Trichlorobenzene ug/m3 68.975.4 91 56-130
1,2,4-Trimethylbenzene ug/m3 54.650 109 70-134
1,2-Dibromoethane (EDB)ug/m3 79.578.1 102 70-130
1,2-Dichlorobenzene ug/m3 66.961.1 109 70-132
1,2-Dichloroethane ug/m3 41.841.1 102 70-130
1,2-Dichloropropane ug/m3 48.347 103 70-130
1,3,5-Trimethylbenzene ug/m3 51.050 102 70-132
1,3-Butadiene ug/m3 23.222.5 103 65-130
1,3-Dichlorobenzene ug/m3 66.361.1 109 70-137
1,4-Dichlorobenzene ug/m3 67.761.1 111 70-134
2-Butanone (MEK)ug/m3 25.030 83 70-130
2-Hexanone ug/m3 41.641.6 100 70-135
4-Ethyltoluene ug/m3 53.850 108 70-138
4-Methyl-2-pentanone (MIBK)ug/m3 41.841.6 100 70-131
Acetone ug/m3 94.8121 79 67-130
Benzene ug/m3 32.332.5 100 70-130
Bromodichloromethane ug/m3 71.568.1 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 60 of 72Page 146 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3357702LABORATORY CONTROL SAMPLE:
LCSSpike
Bromoform ug/m3 119105 113 70-132
Bromomethane ug/m3 38.139.5 97 69-130
Carbon disulfide ug/m3 34.531.6 109 56-137
Carbon tetrachloride ug/m3 68.764 107 66-131
Chlorobenzene ug/m3 46.646.8 100 70-130
Chloroethane ug/m3 26.326.8 98 70-130
Chloroform ug/m3 49.449.6 99 70-130
Chloromethane ug/m3 20.121 96 66-130
cis-1,2-Dichloroethene ug/m3 41.940.3 104 70-130
cis-1,3-Dichloropropene ug/m3 48.746.1 106 70-133
Cyclohexane ug/m3 35.235 100 68-132
Dibromochloromethane ug/m3 92.586.6 107 70-130
Dichlorodifluoromethane ug/m3 47.950.3 95 70-130
Dichlorotetrafluoroethane ug/m3 69.871 98 70-130
Ethyl acetate ug/m3 36.336.6 99 69-130
Ethylbenzene ug/m3 46.644.1 106 67-131
Hexachloro-1,3-butadiene ug/m3 112108 103 66-137
m&p-Xylene ug/m3 90.988.3 103 70-132
Methyl-tert-butyl ether ug/m3 37.136.6 101 70-130
Methylene Chloride ug/m3 182177 103 65-130
n-Heptane ug/m3 41.141.7 99 65-130
n-Hexane ug/m3 33.935.8 95 66-130
Naphthalene ug/m3 47.653.3 89 56-130
o-Xylene ug/m3 43.944.1 100 70-130
Propylene ug/m3 16.117.5 92 67-130
Styrene ug/m3 48.243.3 111 69-136
Tetrachloroethene ug/m3 71.368.9 103 70-130
Tetrahydrofuran ug/m3 30.830 103 68-131
Toluene ug/m3 39.138.3 102 70-130
trans-1,2-Dichloroethene ug/m3 41.940.3 104 70-130
trans-1,3-Dichloropropene ug/m3 50.846.1 110 70-134
Trichloroethene ug/m3 57.754.6 106 70-130
Trichlorofluoromethane ug/m3 55.957.1 98 65-130
Vinyl acetate ug/m3 36.335.8 101 61-133
Vinyl chloride ug/m3 25.426 98 70-130
Parameter Units
Dup
Result QualifiersRPDResult
10484249003
3358693SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 61 of 72Page 147 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484249003
3358693SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 3.0 52.9
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 NDND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 7.8 58.2
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 17.4 616.4
Benzene ug/m3 NDND
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 2.1 12.0
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.2 41.2
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.4 02.4
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 2.2JND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 16.7 116.6
n-Heptane ug/m3 NDND
n-Hexane ug/m3 4.3 44.2
Naphthalene ug/m3 NDND
o-Xylene ug/m3 .97JND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 NDND
Tetrahydrofuran ug/m3 NDND
Toluene ug/m3 2.5 02.5
trans-1,2-Dichloroethene ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 62 of 72Page 148 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484249003
3358693SAMPLE DUPLICATE:
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.2JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
Parameter Units
Dup
Result QualifiersRPDResult
10484249004
3358694SAMPLE DUPLICATE:
1,1,1-Trichloroethane ug/m3 NDND
1,1,2,2-Tetrachloroethane ug/m3 NDND
1,1,2-Trichloroethane ug/m3 NDND
1,1,2-Trichlorotrifluoroethane ug/m3 NDND
1,1-Dichloroethane ug/m3 NDND
1,1-Dichloroethene ug/m3 NDND
1,2,4-Trichlorobenzene ug/m3 NDND
1,2,4-Trimethylbenzene ug/m3 NDND
1,2-Dibromoethane (EDB)ug/m3 NDND
1,2-Dichlorobenzene ug/m3 NDND
1,2-Dichloroethane ug/m3 NDND
1,2-Dichloropropane ug/m3 1.6JND
1,3,5-Trimethylbenzene ug/m3 NDND
1,3-Butadiene ug/m3 NDND
1,3-Dichlorobenzene ug/m3 NDND
1,4-Dichlorobenzene ug/m3 NDND
2-Butanone (MEK)ug/m3 ND7.2
2-Hexanone ug/m3 NDND
4-Ethyltoluene ug/m3 NDND
4-Methyl-2-pentanone (MIBK)ug/m3 NDND
Acetone ug/m3 21.6 121.8
Benzene ug/m3 2.2 12.2
Bromodichloromethane ug/m3 NDND
Bromoform ug/m3 NDND
Bromomethane ug/m3 NDND
Carbon disulfide ug/m3 NDND
Carbon tetrachloride ug/m3 NDND
Chlorobenzene ug/m3 NDND
Chloroethane ug/m3 NDND
Chloroform ug/m3 NDND
Chloromethane ug/m3 1.3 151.1
cis-1,2-Dichloroethene ug/m3 NDND
cis-1,3-Dichloropropene ug/m3 NDND
Cyclohexane ug/m3 NDND
Dibromochloromethane ug/m3 NDND
Dichlorodifluoromethane ug/m3 2.4 22.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 63 of 72Page 149 of 158
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
10484249004
3358694SAMPLE DUPLICATE:
Dichlorotetrafluoroethane ug/m3 NDND
Ethyl acetate ug/m3 NDND
Ethylbenzene ug/m3 NDND
Hexachloro-1,3-butadiene ug/m3 NDND
m&p-Xylene ug/m3 NDND
Methyl-tert-butyl ether ug/m3 NDND
Methylene Chloride ug/m3 12.0 011.9
n-Heptane ug/m3 NDND
n-Hexane ug/m3 5.3 65.0
Naphthalene ug/m3 NDND
o-Xylene ug/m3 NDND
Propylene ug/m3 NDND
Styrene ug/m3 NDND
Tetrachloroethene ug/m3 1.3JND
Tetrahydrofuran ug/m3 1.6 21.5
Toluene ug/m3 1.7 61.6
trans-1,2-Dichloroethene ug/m3 NDND
trans-1,3-Dichloropropene ug/m3 NDND
Trichloroethene ug/m3 NDND
Trichlorofluoromethane ug/m3 1.2JND
Vinyl acetate ug/m3 NDND
Vinyl chloride ug/m3 NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 64 of 72Page 150 of 158
#=QL#
QUALIFIERS
Pace Project No.:
Project:
10484053
92437876 RTP Flex
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - MinneapolisPASI-M
ANALYTE QUALIFIERS
The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.CH
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples.L3
The reporting limit has been raised in accordance with Minnesota Statutes 4740.2100 Subpart 8. C, D. Reporting Limit
Evaluation Rule.MN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 65 of 72Page 151 of 158
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
10484053
92437876 RTP Flex
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92437876001 621640SG-19 (2435)TO-15
92437876002 621628SG-20 (2441)TO-15
92437876003 621628SG-21 (1348)TO-15
92437876004 621628SG-22 (2215)TO-15
92437876005 621628SG-23 (3229)TO-15
92437876006 621628SG-24 (2789)TO-15
92437876007 621628SG-8 (3227)TO-15
92437876008 621628SG-7 (2650)TO-15
92437876009 621628SG-6 (3294)TO-15
92437876010 621628SG-5 (2243)TO-15
92437876011 621628SG-4 (2924)TO-15
92437876012 621628SG-3 (1792)TO-15
92437876013 621953SG-2 (2878)TO-15
92437876014 621628SG-1 (2194)TO-15
92437876015 621628SG-18 (2002)TO-15
92437876016 622036SG-17 (2001)TO-15
92437876017 621644SG-16 (2147)TO-15
92437876018 622036SG-15 (3266)TO-15
92437876019 621644SG-10 (2788)TO-15
92437876020 621644SG-9 (2226)TO-15
92437876021 621644SG-11 (3182)TO-15
92437876022 621644SG-13 (3065)TO-15
92437876023 622036SG-12 (2076)TO-15
92437876025 621644DUP-1 (3175)TO-15
92437876026 622036SG-14 (3527) re-test TO-15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/26/2019 03:00 PM
Pace Analytical Services, LLC
1700 Elm Street - Suite 200
Minneapolis, MN 55414
[phone]
Page 66 of 72Page 152 of 158
001 002 003 004 005 006 007 008009 010 011012 013 014 015 016 017018 0197/22/19 RTPage 67 of 72Page 153 of 158
020 021 022023024 025 7/22/19 RT7/20/19 0845---Page 68 of 72Page 154 of 158
7/22/19
Page 69 of 72Page 155 of 158
7/22/19
Page 70 of 72Page 156 of 158
Page 71 of 72Page 157 of 158
7/23/19
Page 72 of 72Page 158 of 158

APPENDIX D

Risk for Individual Pathways Output Form 1A
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID: NCBP Project No. 23016-19-032
Exposure Unit ID:
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil 9.4E-07 5.7E-03 NO
Groundwater Use*NC NC NC
Construction Worker Soil 7.1E-07 5.7E-02 NO
Soil 5.5E-06 4.2E-02 NO
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID: NCBP Project No. 23016-19-032
Exposure Unit ID: Building 1
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.9E-06 7.9E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID: NCBP Project No. 23016-19-032
Exposure Unit ID: Building 2
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 2.4E-05 7.0E-01 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID: NCBP Project No. 23016-19-032
Exposure Unit ID: Building 3
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.3E-06 8.7E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID: NCBP Project No. 23016-19-032
Exposure Unit ID: Building 4
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.1E-05 8.8E-01 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator