8602_Surry_MtAiry_MSWLF_CDLF_Spring2019GW_FID1358252_20190917

IDENR USE ONLY: I I ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event *:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are 'Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646,
Solid Waste Monitoring Data'Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Municipal Engineering Services Co., PA
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Jonathan Pfohl
E-mail: [e-mail]
Facility name: Facility Address:
LCIose
County Closed C&D and 237 Landfill Road
d MSW Landfill -Mt. Airy Mt. Airy, NC 27030
Phone: (91
NC Landfill Rule: Actual sampling dates (e.g.,
Permit # (.0500 or .1600) October 20-24, 2006)
May 15-17 & 20, 2019
.1600 August 29, 2019 MW-20
verification sample
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring �X Assessment Monitoring ❑X Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
Leachate monitoring data ElSurface water monitorina data
Notification attached?
Methane gas monitoring data
Corrective action data (specify) MNA parameters on 7 wells
Other(specify)
No. No groundwater or surface water standards were exceeded.
X Yes, a nocation of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levelsand a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that ther
,e
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Steven R. Gandy, Ph.D., P.E. Senior Project Manager [phone]
Facility Representative Name (Print) Title (Area Code) Telephone Number
Affix NC Licensed/ Professional Geologist Seal
ignature> Date `%%otRT (fill' ee
� C
P.O. BOX 97, Garner, NC 27529 ®�
v �
Facility Representative Address b o
S� );p
C-0281 ® W t 370
r A '°
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009 ®+�,,�j� �;�EEa •.••� ,`���
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Semi -Annual Water Quality Monitoring Report
with Corrective Action Update
Prepared for
Surry County Closed C&D and Closed MSWLF, Mt. Airy
Mt. Airy, North Carolina
May 2019
Permit Number: 86-02
MESCO Project Number: G19031.0
MUNICIPAL ENGINEERING
riniE"�SERVICES COMPANY, P.A.
6B SHIPWASH DRIVE, GARNER, NO 27529 - PHONE: [phone]
N;_;_Z000�0/_ P.D. Box 349, BOONE, NO 2B607 - PHONE: B28-262-1767
LICENSE NUMBER: C-02B1

Yn E
MUNICIPAL ENGINEERING
SERVICES COMPANY9 P.A.
GARNER, NO AND B❑❑NE, NO
September 17, 2019
Ms. Jaclynne Drummond
Solid Waste Section (SWS)
2090 US 70 Highway
Swannanoa, NC 28778
Re: Semi -Annual Water Quality Monitoring Report with Corrective Action Update
Surry County Closed C&D and Closed MSWLF, Mount Airy
Permit No. 86-02
MESCO Project No. G19031.0
Event Date(s): May 15-17 & 20, 2019
August 29, 2019 Verification sample MW-20
Dear Ms. Drummond:
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi -
Annual Water Quality Report with Corrective Action Update for the Spring 2019 event performed at the Surry County
closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy.
NCDEQ Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid
Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters
during an event performed on May 15-17 & 20, 2019 and a verification sample collected from MW-20 on August 29,
2019. During this event laboratory analytical results indicate volatile organic compounds (VOCs) in concentrations in
excess of 2L Standards continue to persist in samples collected from MW-9, MW-15, MW-16 and they have recently
emerged in sample MW-20. In response to the unprecedented detections of vinyl chloride in sample MW-20 and
fulfillment of Rule 15A NCAC 1313.1633(c)(1) a 14-Day Notification Report was filed with the SWS. No
constituents were detected in surface water samples above established NC 2B Standards. Corrective action to
remediate VOCs in groundwater is ongoing within all three areas of concern (AOC) as described in the most recent
Corrective Action Evaluation Report (CAER) and improvement has been observed with updated information
presented herein.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North
Carolina. The site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill
the site operated as an unlined sanitary landfill that consisted of two units.
68 Shipwash Drive • Garner, NC 27529 • ph: 919-772-5393 • fx: 919-772-1176 * www.mesco.com
LICENSE NUMBER: C-0281

The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The
first part stopped receiving waste prior to October 1991 and the second part stopped receiving waste prior to January
1, 1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the
Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008
at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity,
both the northern and the southern units are monitored and reported together.
During this event supplemental samples from both background wells MW-1 (closed) and MW-1 (Lined) were tested
in support of an Alternative Source Demonstration (ASD) for metals which is planned to be submitted to the NCDEQ
as approved by the NC SWS (DIN:28729).
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since
1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC
13B and as a condition of the post -closure portion of the permit to operate and memorandums this report contains
sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. This
report also contains a table of detections compared to Standards, field data results table, groundwater flow
directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost
aquifer, histograms of historical detections, statistical trend analysis, laboratory analytical reports with chains -of -
custody (C-O-C) and quality assurance/quality control data.
Sampling Procedures
The water quality monitoring program, current as of this event date, includes sampling locations and parameters as
outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:1320110 dated April 2019 and approved by the
SWS (DIN: 1320181) on May 1, 2019. Monitoring locations are shown on the enclosed potentiometric map (Sheet
2). MESCO personnel collected water samples from 18 downgradient groundwater monitoring wells (MW-3R,
MW-4, MW-6 through MW-11, MW-125, MW-13 through MW-17 and MW-19 through MW-23), one background
well (MW-1), four surface water locations (SW-1, SW-2, SW-3 and SW-4), and the water supply well
(SCALEHOUSE) that serves the facility. Data from three surface water points (SWN-1, SWN-2 and SW-C)
designated in the Water Quality Monitoring Plan for the adjacent lined MSWLF are presented because both permitted
landfills discharge into Stoney Creek. Quality control measures implemented during this event included the
quantification of potential artifact contaminants via equipment (EB) and field (FB) blanks. Samples were not
analyzed from the six injection wells (IW-1), (IW-2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-
6/1\4W-8) since they are exempt due to the presence of injectant residue which would yield unrepresentative water
quality results.
A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of
all monitoring locations were visually evaluated as documented on Table 2. The depth to water in each well was
electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or
bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the
well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated
locations. During well purging and surface water sample collection the required field parameters were recorded.
2

The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene
bailer. Samples were collected, kept on ice, and transported to a NC -certified laboratory under proper C-O-C
protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO),
temperature, oxidation reduction potential (ORP), specific conductance and turbidity. The field parameter data
indicates the monitored groundwater is slightly acidic, reducing conditions, with relatively low specific conductance
which is generally consistent relative to each other and congruent with data historically reported. Field parameter
data recorded at the surface water locations had low specific conductance and neutral pH which is consistent with
uncontaminated water. A summary of the field parameter data is presented in Table 3 and the field sampling data
sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratory (PACE) performed the laboratory analysis of groundwater and surface water samples for
the total recoverable constituents listed in 40 CFR Appendix I and 1,4-Dioxane. Environmental Conservation
Laboratories (ENCO) performed the analysis of the verification sample collected from MW-20 on August 28, 2019.
A sampling and analysis table summarizing the locations, constituents, and methods is presented on Table 4.
Laboratory results and C-O-Cs are contained in Appendix A.
Water samples were analyzed to the laboratory -established Method Detection Limits (MDL) and any value between
the MDL and laboratory -established Reporting Limit (RL) is qualified by the laboratory as an estimated concentration
hence qualified with a "J". Estimated concentrations are considered non -quantifiable and discretion should be made
prior to making decisions based solely on an approximate value. Table 5 summarizes constituents detected in
groundwater and QC samples compared to groundwater compliance standards which include SWS adopted
Groundwater Protection Standards (GWP), SWS adopted Interim Maximum Allowable Concentrations (IMAC) and
North Carolina Groundwater Standards (2L). Although not applicable for regulatory compliance purposes the
detections are also compared to the Maximum Contaminant Level (MCL) commonly referenced as the Federal
"Drinking Water Standard". Table 6 lists the constituents detected in surface water samples compared to the North
Carolina Surface Water Standards (213) for a Class C water -body and the MCL. Table 7 presents detections of
constituents and turbidity values of background samples compared to Standards which were obtained in support of a
future ASD for inorganics.
Quality Control Samples
No constituents were detected in either of the quality control samples (EB, FB).
Groundwater Samples Detected Above Standards
One or two metals were detected in quantifiable concentrations (> RL) above the NC 2L/IMAC Standard in samples
collected from 9 wells as shown on Table 5 and summarized below.
3

Metals Detected Above RDL and 2L/IMAC Standards in Groundwater
Cd
Co
cadmium
cobalt
2L/IMAC STD.
2
1
MW-6
3
52.9
MW-7
57.1
MW-9
29.5
230
MW-13
6.9
10.6
MW-14
3.5
MW-15
3.4
MW-16
305
MW-20
90.1
MW-22
14.4
Concentrations in ug/L.
VOC(s) were detected in quantifiable concentrations (> RDL) above the NC 2L Standard in samples collected from
four wells as shown on Table 5 and summarized below.
VOC(s) Detected Above 2L Standards in Groundwater
1,1-DCA
Benzene
1,2-DCA
1,4-DCB
VC
2L STD.
6
1
0.4
6
0.03
MW-9
1.32
12.38
MW-15
7.14
2.43
MW-16
1.28
1.23
6.2
2.33
MW-20 v
1.3
Concentrations in ug/L, — Verification Sample.
The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase
aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent which originated from an
anthropogenic source in levels above the EPA established maximum contaminant levels (MCLs) primary "Drinking
Water Standards" was vinyl chloride in samples MW-9, MW-15 and MW-16. A site map depicting the
concentrations and estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is
presented on Sheet 2.
The on -site water supply well (SCALEHOUSE) continues to lack detections above current groundwater or drinking
water Standards.
Surface Water Samples
No parameters were detected in concentrations above established 213 Groundwater Standards.
4

Corrective Action Update
Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three
designated areas of concern (AOC) (Northern, Southern and MW-11). A second Corrective Action Evaluation Report
(CAER) (DIN: 1320112) was submitted on April 30, 2019 which demonstrated that groundwater conditions continue
to improve, except for area near MW-9, which was approved by the the SWS on May 1, 2019 (DIN:1320182). A
historical summary of corrective actions performed to date are briefly described in the following sections.
MNAAnalysis (AOCs Northern, Southern and MW-11)
Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was
initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A revised
SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated during an
event performed in May 2013. MNA monitoring was limited to field paramaters (ORP, DO and turbidity) during this
event in compliance with the SAP. MNA parameters are presented on Table 3.
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion
with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011.
Similar substrates were injected into monitoring wells MW-4/1W-4 and MW-8/1W-6 on October 24-25, 2012. Details
of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013.
As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post -injection water quality
monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13,
MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background
well MW-1 was also performed in conjunction with this semi-annual event. Total aggregate VOC concentrations
reported during this event were lower at all locations and an increasing trend is not evident when compared to the
respective moving averages of the five events preceding injection in the selected wells downgradient of the injection
points (Figure 1).
MW-11 AOC Investigations
The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L
Standards. MW-I I is located within the compliance boundary near the northern property line which is hydraulically
upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before
adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been
detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and
chlorinated hydocarbons (solvents). VOCs were not detected above allowable Standards in samples collected from
MW-11 which is an improvement compared to previous events. MNA will continue at MW-11 and substrate injection
is no longer planned nor required as described in the most recent CAER.
5

Groundwater and Surface Water Characterization
A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both
saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet 2.
Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table
9. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the
tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate
average of 1,873 ft/yr in the wells screened in regolith and 554 ft/yr in the wells screened in the bedrock. The
consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of
the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the
geology of the Piedmont. Streams located within the facility boundaries were observed to be of moderate volume
and flow with low turbidity.
Findings
The inorganic detections are believed to be a product of erosion of natural deposits and not an anthropogenic source.
Total recoverable metals and associated turbidity levels collected during this, past and future events is planned to be
presented in an ASD-Addendum prior to April 1, 2020 as described in a work -plan dated January 25, 2018
(DIN:28728) which was approved by the SWS January 30, 2018 (DIN: 28729). In the interim, it's understood that
the observed inorganic exceedances do not constituent a compliance violation and additional assessment monitoring
or corrective action will not be implemented unless instructed otherwise.
The on -site supply well and the surface water points remain unimpacted as indicated by the lack of detections in
excess of the applicable Standards. The on -site supply well is not considered potable thus bottled water is provided
for consumption and "Non -Potable Water" warning signs were observed.
One or more Appendix I VOC(s) were detected above the 2L Standard in samples collected from the uppermost
aquifer at four locations (MW-9, MW-15, MW-16 and MW-20). Since the previous event in October 2018 the plume
appears to have advanced from the northern AOC to beyond MW-20. All VOC concentrations remain within their
own respective historically identified range except for the unprecedented exceedance in sample MW-20.
Qualitative evaluation of VOC concentrations indicate a general decreasing trend over time and distance from the
landfill. During this event total cumulative VOC concentrations decreased compared to their respective five event
averages preceding corrective action at most locations (Figure 2). Results of statistical temporal trend analysis,
using Sen's Slope Estimator at a 95% confidence level indicate that none of the individual well's cumulative VOC
concentrations have increased compared to when corrective action began 8 years ago except for MW-9. The Southern
AOC and site -wide cumulative VOC levels continue to exhibit a decreasing trend.
The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs
in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the
MW-11 AOC and 4 acres in the Southern AOC for a total facility wide area of approximately 4 acres (Sheet 2). The
total area impacted beyond the compliance boundary has retracted an estimated 50% (from 8 acres to 4 acres)
compared to when corrective action was initiated 9.5 years ago.
6

Evaluation of the most current water quality data continues to support assertions drawn in previous reports with the
exception that VOCs have now migrated beyond MW-20. A few VOCs persist in the upper portion of the aquifer but
concentrations are decreasing over time and distance away from the landfill. Samples collected from the local
discharge features, which are all located within the property boundaries, continue to lack contaminates above
allowable levels. Data continues to indicate that the plumes within each AOC have stabilized and/or decreasing and
there is adequate evidence that groundwater is naturally attenuating. Corrective action will continue per the approved
CAP with amendments described in the latest CAER.
Closing
Water quality monitoring and corrective action will continue with the next event scheduled for the fall of 2019. The
water supply well (SCALEHOUSE) is planned to be replaced at a different location in the near future. If you have
any questions regarding this report, please contact us at [phone] or by email at jpfohlnmesco.com.
Sincerely,
MUNICIPAL ENGINEERING SERVICES CO., P.A.
Jonathan Kohl
Environmental Specialist
Enclosures
cc: Ms. Jessica Montgomery
Surry County
Steven R. Gandy, Ph.D, P.E.
Senior Project Manger
7

Sheets

Topographic Map with Site Location
Surry County Landfill, Mt. Airy fl
237 Landfill Road
Mount Airy, NC 28621
Lat: 36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
0 Surry Co Property Line
O Closed Unlined C&D Landfill
O Closed Unlined Sanitary Landfill
O Active Lined MSW Landfill
SHEET 1

■ I M
237 LANDFILL ROAD
i
iw
,41
GWE=1131.38 =
JI
o_: SCALEHOUSE _ — / / // // — \
Lj
MW-9
Benzene - 1.32 / IIIVI II - CLOSED UNLINED MSW (8602-MSWLF-1983)
y
Vin I Chloride - 12.38 / ll 1 II l� II II — — \ - STOPPED RECEIVING WASTE BEFORE OCTOBER 9, 1991
1 V/ ��I I�
;l 11�V111 II vI ' / A✓ii\/l/��/� ' /�
ACTIVE LCID (NO PERMIT) <2 ACRES
MW-9 GWEIIIIII104910��-- o �� v �/ y/y
enzene-1.3\Vv\\ GWE=1061.09- =_o J/l /�� / /if/
M �/
MW-20 \V A(' ��� ��VA y __= _ %�_ _�`_ / > > \ \ \\ r l / MW 1
GWE=1063.58 \� ��\\ \V \ \ \ I I // GWE=1 10.
M �_— � �%�� / / v I IIIII l i//
SW-2
VV 1 \\ \A V A\\lll�l
V A 111 IIA\ I I /j __ _ _ _�� / / / / / / i TIRES BURIED UNDER SOIL AND GRASS
I III II II III
II II
I 1 l l I MW-7
,
II GWE=1062.19
l 1 1 II II I IIIIIIIIIIII(I(I II "Jill
JIllIl I/III/llI/ll/llll—
ICLOSE�D UNLINED
NLINED, ,C,.1&/lD\�(8�60_2--C�DL,FA-2001)IlSTOPPED RECEIVING C&D BEFORE JUNE 30, 2008
llCLOSURE REQUIREMENTS COMPLETED BEFORE MAY 30, 2009
I
(4v
/ll l
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Jill
IIII vvv v I I II
/IIII I I vvv v ' ll II I III I I �
,CLOSED C&D OVER CLOSED UNLINED MSW (8602-CDLF ON TOP OF MSW)
STOPPED RECEIVING C&D BEFORE MARCH 3, 2006
/%/ STOPPED RECEIVING MSW BY JAN. 1, 1999
LFG EXTRACTION SYSTEM
MW-12D*���/�/i/�,�ii/�/%%/_
IW-2 I�11111 \1� w�w� �wE=>�o27.05
GWE=1027.97
Jill Il�.
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oA
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ll I III II l IIIIMW-18 /
=974.69 /GWE
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WE_977.
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OW4-20 ��\�\\�\\\\\\\\\\\\�\� ��Q���=�/IIII l \II\\\ �� ���\\ -
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\\� \\\\\\\\\\\\� _—_�/� �I \\\\ 1,2-Dic oroe ane -1.23 \,L 1 \ ��\\III 1 \ \\ \ /%% Iw IW 5 f I l flll II 1 i� _ — r / i //// / /(� /; — /
GWE=1066.35 �\ \\\ \\�\ \ \ \\\�\�\\ \ �� — �� (III l� 2-Dichloro ro ane - 0.82 J MW„16 \� I IIIII ll \\\ // / / / f / 1 /I I I / /�� —� /\ / / \ i j/�/%ii�/�/ice//j//// // / J _ _ / / l/a OPERTY LINE
- - GWE=973.14
1,4 Dichlorobenzene 6.2
Vinyl Chloride - 2.33 /// ! /ii
SW-3
/
Benzene -1.28
MW-14////// MW-21
GWE=956.21
J1111IIIII
\
INACTIVE LINED —
//i PHASE 1
PTO 12/1/98
MONITORED SEPERATELY
ACTIVE LFG EXTRACTION
NOW OR FORMERLY
OWNED BY
JOHNNY COX
\�\\�\\I1111111{�111111\� (I1�\r�
\\� \��
v SWN-1 (-350 FT UPSTREAM)
\ / I
MW-15
1,1-Dichloroethane-7.14
1,2-Dichloroethane - 0.48
GWE=948.04 \l\ \\\\ \ — J //i=�� Vinyl Chloride - 2.43
GWE=949.22�������\\\
GWE=937.17� �( l l� \VAS _ - ��
� — — — � � ���) �� — � � NOW OR FORMERLY
STONEY CREEK l \ �� \' //i f�/7 OWNED BY
�—,940� 1 \� ����if / /
✓/ // / / % SHAWNA SUMMERS
v�j
SW-4
%�/\ \\ \ \�%�%/;!r- ; � i/ l l ' J \ � � ,� IIII Il II /III l /ll///// r ,; _���\ �✓ /�i//i
�-
/
LAGOON
SWN-2 (-1,420') & SW-C (-450')
DOWNSTREAM)
LEGEND
EXISTING TOPOGRAPHIC CONTOURS
EXISITING ROAD/PATH
EXISTING CHAINLINK FENCE
EXISTING STRUCTURE
PERENNIAL CREEK, STREAM, ETC.
INTERMITTANT CREEK, STREAM, ETC.
PROPERTY LINE
LINED MSWLF PHASE LIMITS
UNLINED WASTE LIMITS (APPROXIMATE)
COMPLIANCE BOUNDARY
1060 POTENTIOMETRIC GROUNDWATER CONTOUR (5/16-17/2019
GWE = 2626.85 GROUNDWATER POTENTIOMETRIC ELEVATION
*MW- ELEVATION NOT USED FOR CONTOURING
ESTIMATED EXTENT OF VOC VIOLATIONS (MAY 2019)
BEYOND COMPLIANCE BOUNDARY (-4 ACRES)
sw SURFACE WATER SAMPLING LOCATION
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DATE: 06118119
DRWN. BY: J. PFOHL
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SHEET 2 1 OF 1

Figures

Figure 1
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
October 22, 2009 - May 17, 2019
DOWNGRADIENT OF IW-2 (TOTAL CUMULATIVE VOC CONCENTRATIONS)
s.meo�re
DOWNGRADIENT OF IW4 (TOTAL CUMULATIVE VOC CONCENTRATIONS)
s.meoa
DOWNGRADIENT OF IW-3 (TOTAL CUMULATIVE VOC CONCENTRATIONS)
DOWNGRADIENT OF IW-5 (TOTAL CUMULATIVE VOC CONCENTRATIONS)
s�geou.
�wis ov«.,9
Baseline
Period (Oct.
2009-Oct.
2011)
Difference
Difference
Average of
Between
Between
first Five
Corrective
Most
Most
Statistical
Oct
May
Oct
May
Oct
Action
May
Recent &
Recent &
Trend* Between
2009
2010
2010
2011
2011
Events
2019
Baseline
Baseline
Oct. 2009-May
Well ID
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(uq/L)
(uq/L)
(G/D)
2019
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S & MW-13
MW-12S
0.00
0.00
0.00
0.00
5.40
1.08
0.00
-1.08
-100
HNo TrendH
MW-13
61.00
50.60
74.20
87.30
72.50
69.12
18.65
-50.47
-73
�Downward�
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R
0.00
0.00
1 0.00
0.00
0.00
0.00
0.00
0.00
0
HNo TrendH
MW-16
1137.90
113.60
135.70
121.20
116.30
124.94
33.71
-91.23
-73
. Downward
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14
15.20
15.60
15.60
8.20
17.00
14.32
2.47
-11.85
-83
HNo TrendH
MW-21
52.10
50.70
51.38
39.10
32.41
45.14
19.05
-26.09
-58
Downward.
MW-23
4.30
0.00
0.00
0.00
0.00
0.86
1.46
0.60
70
HNo TrendH
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19
MW-15
96.13
63.89
55.00
78.10
64.06
71.44
49.02
-22.42
-31
Downward.
MW-19
0.00
0.00
0.00
0.00
0.00
0.00
3.13
3.13
100
HNo TrendH
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
* = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Figure 2
Total Cumulative VOC Concentrations Time Series Graphs/Table
October 22, 2009 - May 17, 2019
Total Cumulative vO(--s
SOUTHERN AOC (TOTAL CUMULATIVE VOC CONCENTRATIONS) NORTHERN AOC (TOTAL CUMULATIVE VOC CONCENTRATIONS)
um we
0rv.,e plwis prmv pi"va u�wsi eerwie 1Aew�s +�nv.n ®rmis
-0-1-
AOC
Well ID
Oct
2009
May
2010
Oct
2010
May
2011
Oct
2011
Average of
first Five
Corrective
Action
Events
May 2019
Difference
Difference
Statistical Trend
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
N
Oct 2009 - May 2019
Background
MW-1
0.00
0.00
0.00
0.00
0.00
0.00
0
0.00
0
No Trend
IW-2 (MW-2)
105.25
207.00
207.93
159.90
79.10
151.84
79.10 NS
NS
NS
No Trend
IW-3 (MW-3RS)
202.90
127.50
127.50
144.00
127.60
145.90
127.60 NS
NS
NS
No Trend
MW-3R
0.00
0.00
0.00
0.00
0.00
0.00
0
0.00
0
No Trend
IW-4 (MW-4)
27.00
24.20
24.20
27.60
23.50
25.30
18.10 NS
NS
NS
No Trend
IW-5 (MW-5)
35.00
46.50
46.50
47.40
34.80
42.04
34.80 NS
NS
NS
No Trend
MW-12S
0.06
0.00
0.00
0.00
5.40
1.08
0
-1.08
-100
No Trend
MW-12D
0.00
0.00
0.00
0.00
0.00
0.00
0 NS
0.00
0
No Trend
MW-13
61.00
50.60
74.20
87.30
72.50
69.12
18.65
-50.47
-73
Downward
Southern
MW-14
15.20
15.60
15.60
8.20
17.00
14.32
2.47
-11.85
-83
Downward
MW-15
96.13
55.00
55.00
78.10
64.06
69.66
49.02
-20.64
-30
Downward
MW-16
137.90
113.60
135.70
121.20
116.30
124.94
33.71
-91.23
-73
Downward
MW-17
20.34
8.40
8.85
0.00
5.77
8.67
0.55
-8.12
-94
No Trend
MW-18
0.00
0.00
0.00
0.00
0.00
0.00
0 NS
0.00
0
No Trend
MW-19
0.00
0.00
0.00
0.00
0.00
0.00
3.13
3.13
100
No Trend
MW-21
52.10
50.70
51.38
39.10
32.41
45.14
19.05
-26.09
-58
Downward
MW-22
28.90
23.80
23.80
11.66
5.20
18.67
6.73
-11.94
-64
Downward
MW-23
4.30
0.00
0.00
0.00
0.00
0.86
1.46
0.60
70
No Trend
Combined Total
786.02
722.90
770.66
724.46
583.64
717.54
394.37
-323.17
-44
Downward
MW-6
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
100
No Trend
MW-7
7.40
9.40
11.20
9.70
8.80
9.30
2.71
-6.59
-71
Downward
IW-6 (MW-8)
22.00
23.90
16.00
12.30
12.60
17.36
10.20 NS
NS
NS
No Trend
Northern
MW-9
23.50
20.40
23.20
25.80
22.90
23.16
56.93
33.77
146
Upward
MW-20
0.00
0.00
0.00
0.00
0.00
0.00
18.05
18.05
100
No Trend
Combined Total
52.90
53.70
50.40
47.80
44.30
49.82
87.89
38.07
81
No Trend
MW-11
MW-11
10.10
6.00
6.00
5.44
23.20
10.15
0.50
-9.65
-95
No Trend
SITEWIDE
Combined Total
849.02
782.60
827.06
777.70
651.14
777.50
482.76
-294.74
-37
Downward
"s = Not sampled this event so most recent concentration shown and used in calculations
* = Statistical trend analysis via Sen's Slope Estimator on original and transformed log -normal at a 95% Confidence Level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Tables

Table 1
Groundwater Monitoring Well Construction Table
May 15-17, 2019
Monitoring Well
Date
Installed
Well
Diameter
Total Well
Depth
Top of Screen
Depth
Screen
Length
Geology of
Screened
Interval
Top of Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
Latitude
Longitude
(inches)
(ft bgs)
(ft bgs)
(ft)
(ft amsl)
(ft amsl)
(ft amsl)
(ft btoc)
MW-1
11/28/89
2
40
30
10
Clay
1134.35
1133.15
1110.79
23.56
36.439211
-80.568133
0-2 (was MW-2)
11/28/89
2
70
60
10
Clay
1068.86
1068.36
1027.97
40.89
36.435833
-80.568894
MW-3R
9/27/94
2
101
86
15
Rock
1017.50
1015.00
977.80
39.7
36.434725
-80.571989
IW-3 (was MW-3RS)
5/17/01
2
52
37
15
Rock
1020.57
1018.24
990.36
30.21
36.434656
-80.571858
IW-4 (was MW-4)
8/30/94
2
55.4
40.4
15
Rock
1026.26
1025.06
989.28
36.98
36.434686
-80.569200
0-5 (was MW-5)
8/27/94
2
63
48
15
Rock
1080.18
1077.78
<1039.50
>40.68
36.434614
-80.570436
MW-6
9/7/94
2
29.7
14.7
15
Rock
1067.67
1065.61
1045.26
22.41
36.437431
-80.571067
MW-7
8/23/94
2
23
8
15
Rock
1073.50
1071.50
1062.19
11.31
36.438439
-80.570722
IW-6 (was MW-8)
8/16/94
2
54
39
15
Rock
1088.45
1086.45
1049.10
39.35
36.439278
-80.570381
MW-9
8/22/94
2
43.8
28.8
15
Rock
1094.07
1092.07
1061.09
32.98
36.439289
-80.571508
MW-11
8/15/94
2
40
25
15
Rock
1151.80
1150.40
1131.38
20.42
36.441589
-80.569558
MW-12S
5/31/01
2
51
11
40
Rock
1025.80
1023.25
1012.81
12.99
36.435942
-80.567972
MW-12D
5/30/01
2
100
90
10
Rock
1027.05
1023.75
1027.05
0.00
36.435964
-80.567994
MW-13
5/30/06
2
35.78
20.78
15
Saprolite
1008.48
1005.75
985.28
23.20
36.435036
-80.568183
MW-14
5/30/06
2
48.03
33.03
15
Rock
1018.80
1016.11
986.96
31.84
36.434267
-80.569239
MW-15
6/22/06
2
57
42
15
Rock
1075.96
1073.23
1027.75
48.21
36.433797
-80.570467
MW-16
6/21/06
2
36.3
21.3
15
Rock
999.54
996.67
973.14
26.40
36.434536
-80.572117
MW-17
6/1/07
2
15.32
5.32
10
Rock
965.43
962.26
956.21
9.22
36.433558
-80.572517
MW-18
6/1/07
2
18.15
8.15
10
Saprolite
983.00
980.00
974.69
8.31
36.435453
-80.567050
MW-19
6/1/07
2
17.1
7.1
10
PWR
946.27
942.97
937.17
9.10
36.432231
-80.570556
MW-20
6/1/07
2
25.64
10.64
15
Rock
1082.19
1079.12
1063.58
18.61
36.439025
-80.571650
MW-21
6/1/07
2
15.41
5.41
10
Saprolite/PWR
965.36
962.22
960.76
4.60
36.434214
-80.568717
MW-22
6/1/07
2
16.04
6.04
10
Saprolite
953.40
950.23
949.22
4.18
36.432928
-80.571678
MW-23
6/1/07
2
17.1
7.1
10
Sandy Silt
955.31
952.09
948.04
7.27
36.432828
-80.569156
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 2
Field Observations of Monitoring Locations
May 15-17, 2019
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Comments
MW-1
Yes
Yes
Yes
Yes
Yes
Yes
IW-1
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11.
IW-2 (was MW-2)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11. No pad visible
MW-3R
Yes
Yes
Yes
Yes
Yes
Yes
IW-3 (was MW-3RS)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11.
IW-4 (was MW-4)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 10/24/12.
IW-5 (was MW-5)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11. Bailer would not descend
MW-6
Yes
Yes
Yes
Yes
Yes
Yes
MW-7
Yes
Yes
Yes
Yes
Yes
Yes
IW-6 (was MW-8)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 10/24/12. PR
MW-9
Yes
Yes
Yes
Yes
Yes
Yes
MW-11
Yes
Yes
Yes
Yes
Yes
Yes
MW-12S
Yes
Yes
Yes
Yes
Yes
Yes
MW-12D
Yes
Yes
Yes
Yes
Yes
Yes
Flowing artesian which is typical
MW-13
Yes
Yes
Yes
Yes
Yes
Yes
MW-14
Yes
Yes
Yes
Yes
Yes
Yes
MW-15
Yes
Yes
Yes
Yes
Yes
Yes
MW-16
Yes
Yes
Yes
Yes
Yes
Yes
Red purge water
MW-17
Yes
Yes
Yes
Yes
Yes
Yes
MW-18
Yes
Yes
Yes
Yes
Yes
Yes
MW-19
Yes
Yes
Yes
Yes
Yes
Yes
MW-20
Yes
Yes
Yes
Yes
Yes
Yes
MW-21
Yes
Yes
Yes
Yes
Yes
Yes
MW-22
Yes
Yes
Yes
Yes
Yes
Yes
Red purge water
MW-23
Yes
Yes
Yes
Yes
Yes
Yes
sW-1
Yes
Moderate gage height & flow
SW-2
Yes
Moderate gage height & flow
SW-3
Yes
Moderate gage height & flow
SW-4
Yes
Moderate gage height & flow
SW-c
Yes
Moderate gage height & flow
SW N-1
Yes
Moderate gage height & flow
SWN-2
Yes
Moderate gage height & flow
SCALEHOUSE
Yes
I Sample from spigot next to well which is typical
Any unusual field conditions, observations, or events:
Injection wells (IW-1, IW-2, IW-3, IW4, IW-5 and IW-6) exempt from laboratory analysis as approved by NC SWS on May 10, 2013 (DIN:18938)
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case
Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 3
Field Parameter Data Summary
May 15-17, 2019
Parameter
Units
Depth to
Water
ft (btoc)
Water
Elevation
TOC
Elevation Temp.
ft (arri C
ORP
DO
pH
SU
Specific
Conductance
umhos/cm
Turbidity
NTU
ft (amsl)
my
mg/L
MW-1
23.56
1110.79
1134.35
13.5
88
1.0
6.6
105
5.49
IW-2
40.89
1027.97
1068.86
NR
NR
NR
NR
NR
>1000
MW-3R
39.70
977.80
1017.50
15.7
31
1.1
6.8
283
5.47
IW-3
30.21
990.36
1020.57
NR
NR
NR
NR
NR
>1000
IW-4
36.98
989.28
1026.26
NR
NR
NR
NR
NR
>1000
IW-5
-40
<1040.18
1080.18
NR
NR
NR
NR
NR
NR
MW-6
22.41
1045.26
1067.67
12.5
121
1.2
6.1
225
5.25
MW-7
11.31
1062.19
1073.50
15.5
151
1.8
5.7
210
1.23
IW-6
39.35
1049.10
1088.45
NR
NR
NR
NR
NR
169
MW-9
32.98
1061.09
1094.07
15.6
31
0.8
6.4
422
1.81
MW-11
20.42
1131.38
1151.80
16.5
81
1.9
5.2
109
1.73
MW-12S
12.99
1012.81
1025.80
12.9
132
5.2
6.8
207
2.08
MW-12D
0.00
>1027.05
1027.05
NR
NR
NR
NR
NR
NR
MW-13
23.20
985.28
1008.48
14.2
NR
1.5
4.9
232
2.29
MW-14
31.84
986.96
1018.80
14.1
142
0.9
5.8
74
3.98
MW-15
48.21
1027.75
1075.96
15.1
168
1.3
5.5
111
7.22
MW-16
26.40
973.14
999.54
14.3
175
1.4
6.0
296
1.94
MW-17
9.22
956.21
965.43
13.1
NR
2.1
6.7
268
1.45
MW-18
8.31
974.69
983.00
NR
NR
NR
NR
NR
NR
MW-19
9.10
937.17
946.27
12.9
39
0.9
5.5
51
0.93
MW-20
18.61
1063.58
1082.19
13.4
76
0.9
5.8
123
6.07
MW-21
4.60
960.76
965.36
13.4
88
1.3
5.5
172
0.86
MW-22
4.18
949.22
953.40
16.0
77
1.1
6.1
309
0.87
MW-23
7.27
948.04
955.31
12.6
138
3.5
6.4
51
4.46
Scalehouse
na
na
na
15.1
101
3.1
7.8
81
NR
Minimum
0.00
937.17
946.27
12.5
31
0.8
4.9
51
0.86
Average
21.81
1010.04
1034.58
14.2
102
1.7
6.1
185
153
Maximum
48.21
1131.38
1151.80
16.5
175
5.2
7.8
422
>1000
SW-1
-
-
-
13.1
NR
8.1
6.8
97
6.59
SW-2
-
-
-
14.3
NR
7.3
6.9
74
11.1
SW-3
-
-
-
14.6
NR
8.1
7.1
89
7.48
SW-4
-
-
-
15.1
NR
8.1
6.9
131
4.63
SWN-1
-
-
-
14.5
107
9.8
6.9
31
3.94
SWN-2
-
-
-
15.3
105
9.3
6.9
38
4.61
Minimum
-
-
-
13.1
-
7.3
6.8
31
3.94
Average
-
-
-
14.5
-
8.5
6.9
77
6.39
Maximum
-
-
-
15.3
-
9.8
7.1
131
11.1
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
NR = No reading attempted
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 4
Sampling and Analysis Summary
May 16,17 & 20, 2019
App. I
10ther
MNA
Field Parameter
O
m
IL
c
_
Q
Q
o
5
7
a
a)
C
C0
cc
u)
7
Oof
;v
7
fl
c
a
>
a
o
-a
>
c
.>_
v
v0
U
N
S
�,
Q
o
i
CD
U)
f6
O
U
C
c`v
0
'p
a
0
E
c
a
`a
>>
4
LL
�`
>
L
Y
O
O
O
o
•r
x
o
`m
=
H
>_
w
o
Q
cn
cn
U
H
m
U
z
o
O
H
U
S
n
H
0
0
0
0
25
m
0
0
o
m
0
Y
o
o
O
v
Y
CoN
�
xx
XX
U
N
O
pp
O
m
m
�
�
�
LL
W
LL
U
Q
C�
Q
C9
to
=
O
O
O
O
_
O
No
Q
d
Q
d
N
�
N
�
N
�
a)
�
�p
2�
N
N
�
W
W
W
M
N
O
N
Y
O
N
M
Q
CO
Q
v7
CO
Q
M
iO
N
LO
N
LO
W
W
CO
N
M
2
2
fn
R
a-
0_
[L
2
2
2
N
N
N
N
N
J
J
J
Q
Q
O
Q
LL
W
W
J
W
0
0
(n
J
J
LL
LL
LL
LL
LL
LL
L.L
IW-1
Not sampled since exempt per NC SWS approved WQMP
MW-1
X X X I X X X X X X
IW-2
Not sampled since exempt per NC SWS approved WQMP
MW-3R
X X X I X X X X X X
IW-3
Not sampled since exempt per NC SWS approved WQMP
IW-4
Not sampled since exempt per NC SWS approved WQMP
IW-5
Not sampled since exempt per NC SWS approved WQMP
MW-6
X
X
X
I X
X
X
X
X
X
MW-7
X
X
X
I X
X
XI
X
X
X
IW-6
Not sampled since exempt per NC SWS approved WQMP
MW-9
X
X
X
X
X
X
X
MW-11
X
X
X
X
X
X
X
rX
MW-12S
X
X
X
X
X
X
X
MW-12D
Not sampled since exempt per NC SWS approved WQMP
MW-13
X
X
X
X
X
X
X
X
X
MW-14
X
X
X
X
X
X
X
X
X
MW-15
X
X
X
X
X
X
X
X
X
MW-16
X
X
X
X
X
X
X
X
X
MW-17
X
X
X
X
X
X
X
X
MW-18
Not sampled since exempt per NC SWS approved WQMP
MW-19
X
X
X
X
X
X
X
X
X
MW-20
X
X
X
X
X
X
X
X
X
MW-21
X
X
X
X
X
X
X
X
X
MW-22
X
X
X
X
X
X
X
X
X
MW-23
X
X
X
X
X
X
X
X
X
Scalehouse
X
X
X
X
X
X
X
X
SW-1
X
X
X
X
X
X
X
X
X
SW-2
X
X
X
X
X
X
X
X
X
SW-3
X
X
X
X
X
X
X
X
X
SW-4
X
X
X
X
X
X
X
X
X
SW-C
X
X
X
X
X
X
X
X
X
SWN-1
X
X
X
X
X
X
X
X
X
X
SWN-2
X
X
X
X
X
X
X
X
X
X
EB
X
X
X
FB
X
X
X
App I & II Lists = From current 40 CFR 258
Eight wells exempt from lab testing per NC SWS approved WQMP [FID:1320181]
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 5
Groundwater and QC Sample Detections
May 15-17, & 20, 2019
August 29, 2019 Verification sample MW-20
Parameter Name
MDL
RL
2L/GWP/IMAC
MCL
MW-1
MW-3R
MW-6
MW-7
MW-9
MW-11
MW-12S
MW-13
MW-14
MW-15
MW-16
MW-17
MW-19
MW-20
MW-20
(8/29/19)
MW-21
MW-22
MW-23
SCALEHOUSE
EB
FB
STANDARD
BG
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
WSW
QC
QC
Metals Tar eted 40CFR 258 Appendix I
Barium, total
1
5
700
2000
47 J
7.2 J
75.2 J
49.8 J
40.2 J
33.2 J
14.6 J
61.1 J
20.4 J
43.5 J
71 J
34.6 J
40.8 J
36.6 J
--
56 J
51 J
23.8 J
12.3 J
Beryllium, total
0.2
1
4
4
0.24 J
0.31 J
0.22 J
0.25 J
--
0.32 J
Cadmium, total
0.4
1
2
5
0.91 J
3 (N)
29.5 (N)
0.68 J
6.9 (N)
3.5 (N)
3.4 (N)
0.91 J
--
0.47 J
Chromium, total
1
5
10
100
1.7 J
1.4 J
3.8 J
2.7 J
11
--
2 J
Cobalt, total
1.1
5
1
NE
2.5 J
52.9 (N)
57.1 (N)
230 (N)
9.1 J
10.6 (N)
3.3 J
305 (N)
4.7 J
90.1 (N)
--
5.1 J
14.4 (N)
Copper, total
2.1
5
1000
1300
2.5 J
--
2.9 J
Lead, total
1.6
5
15
15
1.7 J
2.2 J
2 J
3.1 J
--
2 J
Nickel, total
0.9
5
100
NE
1.6J
3.7J
1.7J
7.1 J
2.3J
2.1 J
2.5J
151
6J
0.91 J
4J
--
1.4J
7.1 J
Thallium, total
0.06
0.1
0.28
2
0.62 J
0.14 J
0.3 J
0.09 J
0.08 J
0.09 J
0.29 J
0.07 J
0.51 J
--
0.11 J
Vanadium, total
1.3
5
0.3
NE
1.3 J
I
I
1
1 2.2 J
1.5 J
1.7 J
--
1.5 J
Zinc, total
1 3.9
1 101
1000
NE
1 9.3 J
1 11.6
6.2 J
4.5 J
10.5
1 6.2 J
11
10.4
7.3 J
8.8 J
--
18.2
5.8 J
VOCs (Targeted 40CFR 258 Appendix I and 1,4-Dioxane)
1,1-Dichloroethane
0.27
1
6
NE
1.24 J
1.64 J
1.12 J
7.14 (L)
0.69 J
1.07 J
1.04 J
2.68 J
0.9 J
0.56 J
1,2-Dichlorobenzene
0.29
1
20
NE
0.77 J
0.48 J
1.04 J
0.47 J
1,2-Dichloroethane
0.34
1
0.4
5
0.48 J
1.23 (L)
0.4 J
1,2-Dichloropropane
0.19
1
0.6
5
0.82 J
1,4-Dichlorobenzene
0.26
1
6
75
0.79 J
3.48
0.5 J
0.96 J
3.56
6.2 (L)
2.91
1.4
1.83
Benzene
0.15
1
1
5
1.32 (L)
0.46 J
1.28 (L)
1.15 (L)
0.58 J
0.33 J
Chlorobenzene
0.23
1
50
100
1.92 J
1.12 J
2.33 J
3.07
1.13 J
0.96 J
Chloroethane
0.49
5
3000
NE
1.3 J
0.53 J
0.69 J
cis-1,2-Dichloroethene
0.29
1
70
70
35.32
14.58
1.35 J
28.99
16.34
2.06 J
6.5
2.9
14.34
1.94 J
0.9 J
Methyl-Tert-Butyl Ether
0.37
1
20
NE
0.63 J
0.44 J
1.27
0.55 J
0.86 J
0.77 J
--
--
trans-1,2-Dichloroethene
0.25
1
100
100
0.46 J
Trichloroethene
0.22
1
3
5
0.84 J
2.2
0.77 J
Vinyl chloride
0.24
1
0.03
2
12.38 (L)
2.43 (L)
2.33 (L)
3.59 (L)
1.3 (L)
Turbidity (Field
Measured) (NTU)
Turbidity (NTU) 0.01 -- NE NE 5.49 5.47 5.25 1.23 1.81 1.73 2.08
1 2.29 3.98 7.22 1.94 1.45 0.93 1 6.07 -- 0.86 0.87 1 4.46 -- -- --
Notes:
Units ug/L unless shown otherwise, Blank cells means not detected above MDL, -- means parameter not analyzed, NE means not established
Bold Above Established 2L/GWP/IMAC Std. (Regulatory compliance Standard)
Highlighted Above Established MCL Drinking Water Std. (No regulatory significance)
BG= Background Well Sample, QC = Quality Control Sample, S = Sentinal Well Sample, WSW=Water Supply Well Sample.
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
RL = Reporting Limit established by the laboratory. The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix.
2L/GWP/IMAC Standard = NC 2L /GWP and IMAC Standards adopted and enforced by the NC SWS,
2L = NC 2L Groundater Standard 15A NCAC 02L .0202 adopted by NC SWS as a regulatory groundater Standard.
GWP=Groundwater Protection Standard adopted by NC SWS as a regulatory groundater Standard.
IMAC=Interim Maximum Allowable Concentration adopted by NC SWS as a regulatory groundater Standard.
MCL = Maximum Contaminant Level for drinking water established by the USEPA.
J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Prelilminary source is believed to be anthropogenic with Landfill Gas Wor leachate as suspected transport mechanism.
A definitive source of the detections was not determined as part of this report.
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 6
Surface Water Sample Detections
May 17, 2019
Parameter Name
MDL
RL
INC 2B
STD'
NC PVZ
MCL
SWN-1
SW-1
SW-2
I SW-3
SW-4
SW-C
SW-4
SWN-2
Upstream
Downstream
Downstream
Downstream
Downstream
Downstream
Downstream
Downstream
Metals arcieted 40CFR 258 Appendix
I
Barium, total
1
5
NE
200,000
2000
16 J
23.1 J
23.1 J
17.8 J
17.7 J
18.6 J
17.7 J
17.4 J
Cobalt, total
1.1
5
NE
4
NE
19.9
Hardness as CaCo3 (Field Measured)
Hardness (mg/L) 20 -- NE NE NE 20 20 60 20 30 20 30 20
Turbidity (Field Measured)
Turbidity (NTU) 0.01 -- 50 NE -- 3.94 6.59 11.1 7.48 4.63 5.03 4.63 4.61
VOCs (Targeted 40CFR 258 Appendix 1)
cis-1,2-Dichloroethene
0.29
1
NE
720
70
4.53 J
Vin I Chloride
0.15
1
2.4
NE
2
1.08
Notes:
Units ug/L unless indicated otherwise, Blank cells means Not Detected, NE means Standard Not Established
J = "J-qualified". Defined by the lab as "estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
Red Bold Above Applicable Established 2B Std.
Above Established Federal MCL Drinking Water Std.
Receiving surface waters are Stoney Creek (12-72-12) and Ararat River (12-72-(4.5) Both Class C. 03040101 (8-Digit HUC).
NC 2B STD = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters. Presumed NC SWS adopted the numerical Standard for regulatory compliance purposes.
NC 2B Standard for vinyl chloride was based on fresh and salt (All Class C & SC) fish consumption.
z NC PV= NC Protective Value. These criteria may be based on limited toxicological information and are offered as guidelines only. Contact DWR staff for further information.
NC PV for barium, cobalt & cis-1,2-Dichloroethene based on fresh and salt (All Class C & SC) fish consumption.
3 MCL= Maximum Contaminant Level. Federal "Drinking Water Standard". Shown for comparison purposes only. Not applicable for regulatory compliance purposes.
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1

Table 7
Groundwater Sample Detections (Background)
Designated Background Wells and those Approved by NC SWS* to Establish Background Conditions at the Site
May 17, 2019
Parameter Name
MDL
2L/GWP/IMAC MW-1
RL MCL
STANDARD � (Closed)
Metals (Appendix
MW-1
(Lined)
Barium, total
1
5
700
20001
13.7 J
47 J
Cadmium, total
0.4
1
2
5
0.91 J
Cobalt, total
1.1
5
1
NE
5.6 J
2.5 J
Copper, total
2.1
5
1000
1300
3 J
Lead, total
1.6
5
15
15
1.7 J
Nickel, total
0.9
5
100
NE
7.9 J
1.6 J
Thallium, total
0.06
0.1
0.28
2
0.08 J
Zinc, total
3.9
1 10
1 1000
NE
14.3
9.3 J
Turbidity (Measured in Lab)
Turbidity
0.5
1
1 NE
I NE
1 7.22
5.49
Units ug/L, Blank cells means Not Detected, -- means not tested
Red Bold Above Established 2L/GWP/IMAC Std. Regulatory compliance Standard
Highlighted Above Established MCL Drinking Water Std. No regulatory compliance significance.
MDL = Method Detection Limit, 2L = NC 2L Groundater Standard, GWP=Groundwater Protection Standard, IMAC=Interim Maximum Allowable Con
MCL = Maximum Contaminant Level Federal Standard for Drinking Water
J = "J-qualified". Estimated concentration above the adjusted MDL and below the adjusted reporting limit.
* = NC SWS Approved that data from wells MW-1 (Closed), MW-1 (Lined) and 22 other "OW42' wells may be used in support of an ASD for inorge
Surry County Landfill -Mt. Airy Page 1 of 1

Table 8
Hydrogeolofic Properties at Monitoring Well Locations
May 16-17, 2019
Well
Hydraulic Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater Average
Linear Velocity Rate
Flow
Direction
Minimum
Distance From
Upgradient
EOW
(ft)
Ground Water
Depth
Groundwater
Potentiometric
Elevation
Screened Interval
Lithology
(cm/second)
(ft/day)
(°/u)
(feet/feet)
(feet/year)
(feet btoc)
(feet amsl)
MW-1
4.30E-05
0.12
15
0.023
7
S61W
0
23.56
1110.79
Clay
IW-2
4.30E-05
0.12
15
0.105
31
S46W
-
40.89
1027.97
Clay
MW-7
8.10E-04
2.30
15
0.058
325
N64W
704
11.31
1062.19
PWR / Fractured Rock
IW-6
4.40E-04
1.25
15
0.035
105
S02W
-
39.35
1049.10
PWR/ Fractured Rock
MW-9
1.90E-04
0.54
15
0.103
135
S36E
614
32.98
1061.09
Sandy Silt
MW-13
2.06E-04
0.58
23
0.164
152
S40E
1,850
23.20
985.28
Saprolite
MW-18
2.04E-03
5.78
15
0.085
na
S21E
0
8.31
974.69
Saprolite
MW-19
1.10E-03
3.12
3
0.276
10,462
S21W
2,663
9.10
937.17
PWR
MW-21
1.28E-03
3.63
3
0.154
6,792
S67E
2,041
4.60
960.76
Saprolite/PWR
MW-22
9.88E-04
2.80
15
0.065
443
S28W
2,506
4.18
949.22
Saprolite
MW-23
3.04E-04
0.86
15
0.131
274
S30E
2,610
7.27
948.04
Sandy Silt
Minimum
4.30E-05
0.12
3
0.023
7
0
4.18
937.17
Average
6.77E-04
1.92
14
0.109
1,873
1,443
18.61
1006.03
Maximum
2.04E-03
5.78
23
0.276
10,462
2,663
40.89
1110.79
MW-3R
2.40E-04
0.68
5
na
na
S43W
1,994
39.70
977.80
Fractured Rock
IW-3
2.40E-05
0.07
5
0.137
68
S43W
-
30.21
990.36
Fractured Rock
IW-4
1.10E-04
0.31
5
0.172
392
S53E
36.98
989.28
Fractured Rock
IW-5
1.50E-05
0.04
5
-
-
>40.68
<1039.50
Fractured Rock
MW-6
1.90E-05
0.05
5
0.137
54
S82W
963
22.41
1045.26
Fractured Rock
MW-11
3.10E-04
0.88
5
0.153
984
S21W
0
20.42
1131.38
Fractured Rock
MW-12S
na
na
3
0.117
na
S22W
0
12.99
1012.81
Fractured Rock
MW-12D
1.30E-06
0.00
5
na
na
na
0
0.00
>1027.05
Fractured Rock
MW-14
7.45E-03
21.12
3
0.130
33,368
S85W
2,098
31.84
986.96
Fractured Rock
MW-15
7.21E-05
0.20
3
0.455
1,130
S12W
2,020
48.21
1027.75
Fractured Rock
MW-16
2.82E-05
0.08
3
0.106
103
S40W
2,089
26.40
973.14
Fractured Rock
MW-17
2.94E-04
0.83
3
0.095
961
S67W
2,547
9.22
956.21
Rock
MW-20
1.92E-04
0.54
3
0.112
741
S18W
692
18.61
1063.58
Rock
Minimum
1.30E-06
0.00
3
0.095
54
0
0.00
956.21
Average
7.30E-04
2.07
1 4
0.161
554
1,240
24.75
1014.05
Maximum
7.45E-03
21.12
1 5
1 0.455
1,130
2 547
48.21
1131.38
NOTE: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce.
Hydrologic gradient from water levels recorded on May 16-17, 2019.
Wells screened entirely in rock were not utilized for flow directions/gradients.
Screens that traverse both rock and regolith assumed flow in regolith dominates.
Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum.
na = Not available/applicable
Average Linear Velocity (Q) is defined by modified Darcy's equation:
o _ K A K= hydraulic conductivity
where n dl ne= effective porosity
e dh= head difference
dl= horizontal distance
Slurry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1

Appendix A
Laboratory Analysis Reports
Chains of Custody

lacieAnalXical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 05, 2019
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
ft*OL-'
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Maddie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 106

lacmnalytical' www.pacelabs.corn
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
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Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A21LA 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE SUMMARY
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92429865002
MW-3R
Water
05/17/19 09:20
05/20/19 11:26
92429865003
MW-6
Water
05/17/1916:31
05/20/19 11:26
92429865004
MW-7
Water
05/17/1916:35
05/20/19 11:26
92429865005
MW-9
Water
05/17/1917:05
05/20/19 11:26
92429865006
MW-11
Water
05/17/1917:11
05/20/19 11:26
92429865007
MW-12S
Water
05/17/1916:28
05/20/19 11:26
92429865008
MW-13
Water
05/17/1915:20
05/20/19 11:26
92429865009
MW-14
Water
05/17/1915:25
05/20/19 11:26
92429865010
MW-15
Water
05/17/19 09:25
05/20/19 11:26
92429865011
MW-16
Water
05/17/19 09:15
05/20/19 11:26
92429865012
MW-17
Water
05/17/1914:20
05/20/19 11:26
92429865013
MW-19
Water
05/17/1914:35
05/20/19 11:26
92429865014
MW-20
Water
05/17/1917:15
05/20/19 11:26
92429865015
MW-21
Water
05/17/1914:47
05/20/19 11:26
92429865016
MW-22
Water
05/17/1914:18
05/20/19 11:26
92429865017
MW-23
Water
05/17/1916:16
05/20/19 11:26
92429865018
SCALEHOUSE
Water
05/17/1915:03
05/20/19 11:26
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SURRY CLOSED -MT. AIRY
92429865
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92429865002
MW-3R
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865003
MW-6
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865004
MW-7
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865005
MW-9
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865006
MW-11
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865007
MW-12S
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865008
MW-13
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865009
MW-14
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865010
MW-15
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865011
MW-16
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865012
MW-17
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865013
MW-19
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865014
MW-20
EPA 601OD
SH1
14
PASI-A
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project:
SURRY CLOSED -MT. AIRY
Pace Project No.:
92429865
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865015
MW-21
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865016
MW-22
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865017
MW-23
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429865018
SCALEHOUSE
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-3R Lab ID: 92429865002 Collected: 05/17/19 09:20 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/03/19 23:53
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:53
7440-38-2
Barium
7.2
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:53
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/03/19 23:53
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/03/19 23:53
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:53
7440-47-3
Cobalt
ND
ug/L
5.0
1.1
1
06/03/19 12:21
06/03/19 23:53
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/03/19 23:53
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/03/19 23:53
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
06/03/19 12:21
06/03/19 23:53
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:53
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/03/19 23:53
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/03/19 23:53
7440-62-2
Zinc
ND
ug/L
10.0
3.9
1
06/03/19 12:21
06/03/19 23:53
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 05:54
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 05:30
05/28/19 05:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 05:30
05/28/19 05:30
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 05:30
05/28/19 05:30
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 05:30
05/28/19 05:30
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 05:30
05/28/19 05:30
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 05:30
05/28/19 05:30
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 05:30
05/28/19 05:30
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 05:30
05/28/19 05:30
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 05:30
05/28/19 05:30
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 05:30
05/28/19 05:30
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 05:30
05/28/19 05:30
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 05:30
05/28/19 05:30
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 05:30
05/28/19 05:30
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 05:30
05/28/19 05:30
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 05:30
05/28/19 05:30
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 05:30
05/28/19 05:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 05:30
05/28/19 05:30
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 05:30
05/28/19 05:30
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 05:30
05/28/19 05:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 05:30
05/28/19 05:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 05:30
05/28/19 05:30
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 05:30
05/28/19 05:30
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 05:30
05/28/19 05:30
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 05:30
05/28/19 05:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 05:30
05/28/19 05:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 05:30
05/28/19 05:30
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 05:30
05/28/19 05:30
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
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Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 106

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ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-3R Lab ID: 92429865002 Collected: 05/17/19 09:20 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 05:30
05/28/19 05:30
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 05:30
05/28/19 05:30
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 05:30
05/28/19 05:30
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 05:30
05/28/19 05:30
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 05:30
05/28/19 05:30
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 05:30
05/28/19 05:30
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 05:30
05/28/19 05:30
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 05:30
05/28/19 05:30
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 05:30
05/28/19 05:30
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 05:30
05/28/19 05:30
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 05:30
05/28/19 05:30
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 05:30
05/28/19 05:30
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 05:30
05/28/19 05:30
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 05:30
05/28/19 05:30
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 05:30
05/28/19 05:30
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 05:30
05/28/19 05:30
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 05:30
05/28/19 05:30
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 05:30
05/28/19 05:30
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 05:30
05/28/19 05:30
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 05:30
05/28/19 05:30
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 05:30
05/28/19 05:30
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 05:30
05/28/19 05:30
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 05:30
05/28/19 05:30
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 05:30
05/28/19 05:30
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 05:30
05/28/19 05:30
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 05:30
05/28/19 05:30
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 05:30
05/28/19 05:30
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 05:30
05/28/19 05:30
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 05:30
05/28/19 05:30
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 05:30
05/28/19 05:30
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 05:30
05/28/19 05:30
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 05:30
05/28/19 05:30
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 05:30
05/28/19 05:30
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 05:30
05/28/19 05:30
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 05:30
05/28/19 05:30
123-91-1
93.2
%
80.0-120
1
05/28/19 05:30
05/28/19 05:30
2037-26-5
101
%
77.0-126
1
05/28/19 05:30
05/28/19 05:30
460-00-4
87.1
%
70.0-130
1
05/28/19 05:30
05/28/19 05:30
17060-07-0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-6 Lab ID: 92429865003 Collected: 05/17/19 16:31 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/03/19 23:56
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:56
7440-38-2
Barium
75.2
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:56
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/03/19 23:56
7440-41-7
Cadmium
3.0
ug/L
1.0
0.40
1
06/03/19 12:21
06/03/19 23:56
7440-43-9
Chromium
1.7J
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:56
7440-47-3
Cobalt
52.9
ug/L
5.0
1.1
1
06/03/19 12:21
06/03/19 23:56
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/03/19 23:56
7440-50-8
Lead
2.2J
ug/L
5.0
1.6
1
06/03/19 12:21
06/03/19 23:56
7439-92-1
Nickel
3.7J
ug/L
5.0
0.90
1
06/03/19 12:21
06/03/19 23:56
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:56
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/03/19 23:56
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/03/19 23:56
7440-62-2
Zinc
11.6
ug/L
10.0
3.9
1
06/03/19 12:21
06/03/19 23:56
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.62
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:05
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 05:50
05/28/19 05:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 05:50
05/28/19 05:50
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 05:50
05/28/19 05:50
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 05:50
05/28/19 05:50
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 05:50
05/28/19 05:50
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 05:50
05/28/19 05:50
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 05:50
05/28/19 05:50
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 05:50
05/28/19 05:50
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 05:50
05/28/19 05:50
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 05:50
05/28/19 05:50
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 05:50
05/28/19 05:50
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 05:50
05/28/19 05:50
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 05:50
05/28/19 05:50
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 05:50
05/28/19 05:50
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 05:50
05/28/19 05:50
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 05:50
05/28/19 05:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 05:50
05/28/19 05:50
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 05:50
05/28/19 05:50
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 05:50
05/28/19 05:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 05:50
05/28/19 05:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 05:50
05/28/19 05:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 05:50
05/28/19 05:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 05:50
05/28/19 05:50
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 05:50
05/28/19 05:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 05:50
05/28/19 05:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 05:50
05/28/19 05:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 05:50
05/28/19 05:50
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-6 Lab ID: 92429865003 Collected: 05/17/19 16:31 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 05:50
05/28/19 05:50
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 05:50
05/28/19 05:50
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 05:50
05/28/19 05:50
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 05:50
05/28/19 05:50
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 05:50
05/28/19 05:50
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 05:50
05/28/19 05:50
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 05:50
05/28/19 05:50
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 05:50
05/28/19 05:50
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 05:50
05/28/19 05:50
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 05:50
05/28/19 05:50
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 05:50
05/28/19 05:50
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 05:50
05/28/19 05:50
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 05:50
05/28/19 05:50
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 05:50
05/28/19 05:50
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 05:50
05/28/19 05:50
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 05:50
05/28/19 05:50
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 05:50
05/28/19 05:50
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 05:50
05/28/19 05:50
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 05:50
05/28/19 05:50
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 05:50
05/28/19 05:50
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 05:50
05/28/19 05:50
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 05:50
05/28/19 05:50
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 05:50
05/28/19 05:50
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 05:50
05/28/19 05:50
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 05:50
05/28/19 05:50
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 05:50
05/28/19 05:50
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 05:50
05/28/19 05:50
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 05:50
05/28/19 05:50
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 05:50
05/28/19 05:50
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 05:50
05/28/19 05:50
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 05:50
05/28/19 05:50
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 05:50
05/28/19 05:50
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 05:50
05/28/19 05:50
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 05:50
05/28/19 05:50
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 05:50
05/28/19 05:50
123-91-1
90.6
%
80.0-120
1
05/28/19 05:50
05/28/19 05:50
2037-26-5
98.7
%
77.0-126
1
05/28/19 05:50
05/28/19 05:50
460-00-4
93.2
%
70.0-130
1
05/28/19 05:50
05/28/19 05:50
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-7 Lab ID: 92429865004 Collected: 05/17/19 16:35 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/03/19 23:59
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:59
7440-38-2
Barium
49.8
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:59
7440-39-3
Beryllium
0.24J
ug/L
1.0
0.20
1
06/03/19 12:21
06/03/19 23:59
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/03/19 23:59
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:59
7440-47-3
Cobalt
57.1
ug/L
5.0
1.1
1
06/03/19 12:21
06/03/19 23:59
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/03/19 23:59
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/03/19 23:59
7439-92-1
Nickel
1.7J
ug/L
5.0
0.90
1
06/03/19 12:21
06/03/19 23:59
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:59
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/03/19 23:59
7440-22-4
Vanadium
1.3J
ug/L
5.0
1.3
1
06/03/19 12:21
06/03/19 23:59
7440-62-2
Zinc
6.2J
ug/L
10.0
3.9
1
06/03/19 12:21
06/03/19 23:59
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.14
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:12
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 06:10
05/28/19 06:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 06:10
05/28/19 06:10
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 06:10
05/28/19 06:10
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 06:10
05/28/19 06:10
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 06:10
05/28/19 06:10
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 06:10
05/28/19 06:10
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 06:10
05/28/19 06:10
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 06:10
05/28/19 06:10
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 06:10
05/28/19 06:10
56-23-5
Chlorobenzene
1.92
ug/L
1.00
0.348
1
05/28/19 06:10
05/28/19 06:10
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 06:10
05/28/19 06:10
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 06:10
05/28/19 06:10
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 06:10
05/28/19 06:10
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 06:10
05/28/19 06:10
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 06:10
05/28/19 06:10
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 06:10
05/28/19 06:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 06:10
05/28/19 06:10
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 06:10
05/28/19 06:10
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 06:10
05/28/19 06:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 06:10
05/28/19 06:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 06:10
05/28/19 06:10
541-73-1
1,4-Dichlorobenzene
0.786J
ug/L
1.00
0.274
1
05/28/19 06:10
05/28/19 06:10
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 06:10
05/28/19 06:10
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 06:10
05/28/19 06:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 06:10
05/28/19 06:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 06:10
05/28/19 06:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 06:10
05/28/19 06:10
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
J
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-7 Lab ID: 92429865004 Collected: 05/17/19 16:35 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 06:10
05/28/19 06:10
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 06:10
05/28/19 06:10
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 06:10
05/28/19 06:10
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 06:10
05/28/19 06:10
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 06:10
05/28/19 06:10
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 06:10
05/28/19 06:10
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 06:10
05/28/19 06:10
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 06:10
05/28/19 06:10
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 06:10
05/28/19 06:10
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 06:10
05/28/19 06:10
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 06:10
05/28/19 06:10
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 06:10
05/28/19 06:10
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 06:10
05/28/19 06:10
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 06:10
05/28/19 06:10
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 06:10
05/28/19 06:10
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 06:10
05/28/19 06:10
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 06:10
05/28/19 06:10
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 06:10
05/28/19 06:10
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 06:10
05/28/19 06:10
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 06:10
05/28/19 06:10
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 06:10
05/28/19 06:10
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 06:10
05/28/19 06:10
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 06:10
05/28/19 06:10
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 06:10
05/28/19 06:10
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 06:10
05/28/19 06:10
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 06:10
05/28/19 06:10
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 06:10
05/28/19 06:10
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 06:10
05/28/19 06:10
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 06:10
05/28/19 06:10
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 06:10
05/28/19 06:10
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 06:10
05/28/19 06:10
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 06:10
05/28/19 06:10
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 06:10
05/28/19 06:10
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 06:10
05/28/19 06:10
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 06:10
05/28/19 06:10
123-91-1
91.0
%
80.0-120
1
05/28/19 06:10
05/28/19 06:10
2037-26-5
103
%
77.0-126
1
05/28/19 06:10
05/28/19 06:10
460-00-4
92.6
%
70.0-130
1
05/28/19 06:10
05/28/19 06:10
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 106

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-9 Lab ID: 92429865005 Collected: 05/17/19 17:05 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:02
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:02
7440-38-2
Barium
40.2
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:02
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:02
7440-41-7
Cadmium
29.5
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:02
7440-43-9
Chromium
1AJ
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:02
7440-47-3
Cobalt
230
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:02
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:02
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:02
7439-92-1
Nickel
7.1
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:02
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:02
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:02
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:02
7440-62-2
Zinc
4.5J
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:02
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.30
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:19
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 06:30
05/28/19 06:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 06:30
05/28/19 06:30
107-13-1
Benzene
1.32
ug/L
1.00
0.331
1
05/28/19 06:30
05/28/19 06:30
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 06:30
05/28/19 06:30
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 06:30
05/28/19 06:30
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 06:30
05/28/19 06:30
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 06:30
05/28/19 06:30
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 06:30
05/28/19 06:30
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 06:30
05/28/19 06:30
56-23-5
Chlorobenzene
1.12
ug/L
1.00
0.348
1
05/28/19 06:30
05/28/19 06:30
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 06:30
05/28/19 06:30
124-48-1
Chloroethane
1.30J
ug/L
5.00
0.453
1
05/28/19 06:30
05/28/19 06:30
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 06:30
05/28/19 06:30
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 06:30
05/28/19 06:30
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 06:30
05/28/19 06:30
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 06:30
05/28/19 06:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 06:30
05/28/19 06:30
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 06:30
05/28/19 06:30
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 06:30
05/28/19 06:30
74-95-3
1,2-Dichlorobenzene
0.769J
ug/L
1.00
0.349
1
05/28/19 06:30
05/28/19 06:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 06:30
05/28/19 06:30
541-73-1
1,4-Dichlorobenzene
3.48
ug/L
1.00
0.274
1
05/28/19 06:30
05/28/19 06:30
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 06:30
05/28/19 06:30
75-71-8
1,1-Dichloroethane
1.24
ug/L
1.00
0.259
1
05/28/19 06:30
05/28/19 06:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 06:30
05/28/19 06:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 06:30
05/28/19 06:30
75-35-4
cis-1,2-Dichloroethene
35.3
ug/L
1.00
0.260
1
05/28/19 06:30
05/28/19 06:30
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
J
CC
J
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-9 Lab ID: 92429865005 Collected: 05/17/19 17:05 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 06:30
05/28/19 06:30
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 06:30
05/28/19 06:30
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 06:30
05/28/19 06:30
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 06:30
05/28/19 06:30
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 06:30
05/28/19 06:30
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 06:30
05/28/19 06:30
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 06:30
05/28/19 06:30
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 06:30
05/28/19 06:30
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 06:30
05/28/19 06:30
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 06:30
05/28/19 06:30
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 06:30
05/28/19 06:30
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 06:30
05/28/19 06:30
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 06:30
05/28/19 06:30
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 06:30
05/28/19 06:30
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 06:30
05/28/19 06:30
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 06:30
05/28/19 06:30
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 06:30
05/28/19 06:30
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 06:30
05/28/19 06:30
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 06:30
05/28/19 06:30
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 06:30
05/28/19 06:30
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 06:30
05/28/19 06:30
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 06:30
05/28/19 06:30
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 06:30
05/28/19 06:30
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 06:30
05/28/19 06:30
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 06:30
05/28/19 06:30
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 06:30
05/28/19 06:30
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 06:30
05/28/19 06:30
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 06:30
05/28/19 06:30
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 06:30
05/28/19 06:30
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 06:30
05/28/19 06:30
108-05-4
12.4
ug/L
1.00
0.259
1
05/28/19 06:30
05/28/19 06:30
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 06:30
05/28/19 06:30
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 06:30
05/28/19 06:30
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 06:30
05/28/19 06:30
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 06:30
05/28/19 06:30
123-91-1
91.1
%
80.0-120
1
05/28/19 06:30
05/28/19 06:30
2037-26-5
101
%
77.0-126
1
05/28/19 06:30
05/28/19 06:30
460-00-4
93.4
%
70.0-130
1
05/28/19 06:30
05/28/19 06:30
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-11 Lab ID: 92429865006 Collected: 05/17/19 17:11 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:05
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:05
7440-38-2
Barium
33.2
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:05
7440-39-3
Beryllium
0.31J
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:05
7440-41-7
Cadmium
0.68J
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:05
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:05
7440-47-3
Cobalt
9.1
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:05
7440-48-4
Copper
2.5J
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:05
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:05
7439-92-1
Nickel
2.3J
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:05
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:05
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:05
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:05
7440-62-2
Zinc
10.5
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:05
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.0911
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:26
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 06:50
05/28/19 06:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 06:50
05/28/19 06:50
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 06:50
05/28/19 06:50
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 06:50
05/28/19 06:50
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 06:50
05/28/19 06:50
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 06:50
05/28/19 06:50
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 06:50
05/28/19 06:50
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 06:50
05/28/19 06:50
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 06:50
05/28/19 06:50
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 06:50
05/28/19 06:50
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 06:50
05/28/19 06:50
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 06:50
05/28/19 06:50
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 06:50
05/28/19 06:50
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 06:50
05/28/19 06:50
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 06:50
05/28/19 06:50
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 06:50
05/28/19 06:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 06:50
05/28/19 06:50
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 06:50
05/28/19 06:50
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 06:50
05/28/19 06:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 06:50
05/28/19 06:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 06:50
05/28/19 06:50
541-73-1
1,4-Dichlorobenzene
0.501J
ug/L
1.00
0.274
1
05/28/19 06:50
05/28/19 06:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 06:50
05/28/19 06:50
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 06:50
05/28/19 06:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 06:50
05/28/19 06:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 06:50
05/28/19 06:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 06:50
05/28/19 06:50
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
J
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-11 Lab ID: 92429865006 Collected: 05/17/19 17:11 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 06:50
05/28/19 06:50
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 06:50
05/28/19 06:50
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 06:50
05/28/19 06:50
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 06:50
05/28/19 06:50
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 06:50
05/28/19 06:50
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 06:50
05/28/19 06:50
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 06:50
05/28/19 06:50
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 06:50
05/28/19 06:50
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 06:50
05/28/19 06:50
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 06:50
05/28/19 06:50
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 06:50
05/28/19 06:50
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 06:50
05/28/19 06:50
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 06:50
05/28/19 06:50
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 06:50
05/28/19 06:50
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 06:50
05/28/19 06:50
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 06:50
05/28/19 06:50
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 06:50
05/28/19 06:50
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 06:50
05/28/19 06:50
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 06:50
05/28/19 06:50
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 06:50
05/28/19 06:50
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 06:50
05/28/19 06:50
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 06:50
05/28/19 06:50
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 06:50
05/28/19 06:50
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 06:50
05/28/19 06:50
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 06:50
05/28/19 06:50
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 06:50
05/28/19 06:50
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 06:50
05/28/19 06:50
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 06:50
05/28/19 06:50
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 06:50
05/28/19 06:50
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 06:50
05/28/19 06:50
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 06:50
05/28/19 06:50
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 06:50
05/28/19 06:50
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 06:50
05/28/19 06:50
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 06:50
05/28/19 06:50
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 06:50
05/28/19 06:50
123-91-1
92.8
%
80.0-120
1
05/28/19 06:50
05/28/19 06:50
2037-26-5
99.6
%
77.0-126
1
05/28/19 06:50
05/28/19 06:50
460-00-4
90.6
%
70.0-130
1
05/28/19 06:50
05/28/19 06:50
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 106

aceAnalXical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-12S Lab ID: 92429865007 Collected: 05/17/19 16:28 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:08
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:08
7440-38-2
Barium
14.6
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:08
7440-39-3
Beryllium
0.22J
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:08
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:08
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:08
7440-47-3
Cobalt
ND
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:08
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:08
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:08
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:08
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:08
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:08
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:08
7440-62-2
Zinc
ND
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:08
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:33
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 07:10
05/28/19 07:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 07:10
05/28/19 07:10
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 07:10
05/28/19 07:10
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 07:10
05/28/19 07:10
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 07:10
05/28/19 07:10
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 07:10
05/28/19 07:10
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 07:10
05/28/19 07:10
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 07:10
05/28/19 07:10
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 07:10
05/28/19 07:10
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 07:10
05/28/19 07:10
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 07:10
05/28/19 07:10
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 07:10
05/28/19 07:10
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 07:10
05/28/19 07:10
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 07:10
05/28/19 07:10
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 07:10
05/28/19 07:10
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 07:10
05/28/19 07:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 07:10
05/28/19 07:10
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 07:10
05/28/19 07:10
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 07:10
05/28/19 07:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 07:10
05/28/19 07:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 07:10
05/28/19 07:10
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 07:10
05/28/19 07:10
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 07:10
05/28/19 07:10
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 07:10
05/28/19 07:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 07:10
05/28/19 07:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 07:10
05/28/19 07:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 07:10
05/28/19 07:10
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-12S Lab ID: 92429865007 Collected: 05/17/19 16:28 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 07:10
05/28/19 07:10
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 07:10
05/28/19 07:10
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 07:10
05/28/19 07:10
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 07:10
05/28/19 07:10
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 07:10
05/28/19 07:10
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 07:10
05/28/19 07:10
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 07:10
05/28/19 07:10
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 07:10
05/28/19 07:10
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 07:10
05/28/19 07:10
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 07:10
05/28/19 07:10
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 07:10
05/28/19 07:10
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 07:10
05/28/19 07:10
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 07:10
05/28/19 07:10
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 07:10
05/28/19 07:10
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 07:10
05/28/19 07:10
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 07:10
05/28/19 07:10
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 07:10
05/28/19 07:10
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 07:10
05/28/19 07:10
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 07:10
05/28/19 07:10
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 07:10
05/28/19 07:10
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 07:10
05/28/19 07:10
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 07:10
05/28/19 07:10
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 07:10
05/28/19 07:10
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 07:10
05/28/19 07:10
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 07:10
05/28/19 07:10
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 07:10
05/28/19 07:10
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 07:10
05/28/19 07:10
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 07:10
05/28/19 07:10
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 07:10
05/28/19 07:10
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 07:10
05/28/19 07:10
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 07:10
05/28/19 07:10
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 07:10
05/28/19 07:10
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 07:10
05/28/19 07:10
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 07:10
05/28/19 07:10
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 07:10
05/28/19 07:10
123-91-1
91.4
%
80.0-120
1
05/28/19 07:10
05/28/19 07:10
2037-26-5
100
%
77.0-126
1
05/28/19 07:10
05/28/19 07:10
460-00-4
89.6
%
70.0-130
1
05/28/19 07:10
05/28/19 07:10
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 106

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-13 Lab ID: 92429865008 Collected: 05/17/19 15:20 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:11
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:11
7440-38-2
Barium
61.1
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:11
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:11
7440-41-7
Cadmium
6.9
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:11
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:11
7440-47-3
Cobalt
10.6
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:11
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:11
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:11
7439-92-1
Nickel
2.1J
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:11
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:11
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:11
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:11
7440-62-2
Zinc
6.2J
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:11
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.078J
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:37
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 07:30
05/28/19 07:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 07:30
05/28/19 07:30
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 07:30
05/28/19 07:30
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 07:30
05/28/19 07:30
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 07:30
05/28/19 07:30
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 07:30
05/28/19 07:30
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 07:30
05/28/19 07:30
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 07:30
05/28/19 07:30
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 07:30
05/28/19 07:30
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 07:30
05/28/19 07:30
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 07:30
05/28/19 07:30
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 07:30
05/28/19 07:30
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 07:30
05/28/19 07:30
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 07:30
05/28/19 07:30
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 07:30
05/28/19 07:30
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 07:30
05/28/19 07:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 07:30
05/28/19 07:30
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 07:30
05/28/19 07:30
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 07:30
05/28/19 07:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 07:30
05/28/19 07:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 07:30
05/28/19 07:30
541-73-1
1,4-Dichlorobenzene
0.957J
ug/L
1.00
0.274
1
05/28/19 07:30
05/28/19 07:30
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 07:30
05/28/19 07:30
75-71-8
1,1-Dichloroethane
1.64
ug/L
1.00
0.259
1
05/28/19 07:30
05/28/19 07:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 07:30
05/28/19 07:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 07:30
05/28/19 07:30
75-35-4
cis-1,2-Dichloroethene
14.6
ug/L
1.00
0.260
1
05/28/19 07:30
05/28/19 07:30
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
J
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 106

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-13 Lab ID: 92429865008 Collected: 05/17/19 15:20 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 07:30
05/28/19 07:30
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 07:30
05/28/19 07:30
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 07:30
05/28/19 07:30
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 07:30
05/28/19 07:30
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 07:30
05/28/19 07:30
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 07:30
05/28/19 07:30
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 07:30
05/28/19 07:30
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 07:30
05/28/19 07:30
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 07:30
05/28/19 07:30
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 07:30
05/28/19 07:30
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 07:30
05/28/19 07:30
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 07:30
05/28/19 07:30
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 07:30
05/28/19 07:30
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 07:30
05/28/19 07:30
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 07:30
05/28/19 07:30
108-10-1
0.626J
ug/L
1.00
0.367
1
05/28/19 07:30
05/28/19 07:30
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 07:30
05/28/19 07:30
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 07:30
05/28/19 07:30
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 07:30
05/28/19 07:30
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 07:30
05/28/19 07:30
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 07:30
05/28/19 07:30
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 07:30
05/28/19 07:30
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 07:30
05/28/19 07:30
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 07:30
05/28/19 07:30
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 07:30
05/28/19 07:30
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 07:30
05/28/19 07:30
79-00-5
0.841J
ug/L
1.00
0.398
1
05/28/19 07:30
05/28/19 07:30
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 07:30
05/28/19 07:30
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 07:30
05/28/19 07:30
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 07:30
05/28/19 07:30
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 07:30
05/28/19 07:30
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 07:30
05/28/19 07:30
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 07:30
05/28/19 07:30
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 07:30
05/28/19 07:30
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 07:30
05/28/19 07:30
123-91-1
89.7
%
80.0-120
1
05/28/19 07:30
05/28/19 07:30
2037-26-5
99.8
%
77.0-126
1
05/28/19 07:30
05/28/19 07:30
460-00-4
91.8
%
70.0-130
1
05/28/19 07:30
05/28/19 07:30
17060-07-0
REPORT OF LABORATORY ANALYSIS
J
J
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-14 Lab ID: 92429865009 Collected: 05/17/19 15:25 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:14
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:14
7440-38-2
Barium
20.4
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:14
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:14
7440-41-7
Cadmium
3.5
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:14
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:14
7440-47-3
Cobalt
ND
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:14
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:14
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:14
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:14
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:14
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:14
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:14
7440-62-2
Zinc
ND
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:14
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:51
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 07:50
05/28/19 07:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 07:50
05/28/19 07:50
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 07:50
05/28/19 07:50
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 07:50
05/28/19 07:50
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 07:50
05/28/19 07:50
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 07:50
05/28/19 07:50
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 07:50
05/28/19 07:50
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 07:50
05/28/19 07:50
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 07:50
05/28/19 07:50
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 07:50
05/28/19 07:50
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 07:50
05/28/19 07:50
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 07:50
05/28/19 07:50
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 07:50
05/28/19 07:50
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 07:50
05/28/19 07:50
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 07:50
05/28/19 07:50
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 07:50
05/28/19 07:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 07:50
05/28/19 07:50
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 07:50
05/28/19 07:50
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 07:50
05/28/19 07:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 07:50
05/28/19 07:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 07:50
05/28/19 07:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 07:50
05/28/19 07:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 07:50
05/28/19 07:50
75-71-8
1,1-Dichloroethane
1.12
ug/L
1.00
0.259
1
05/28/19 07:50
05/28/19 07:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 07:50
05/28/19 07:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 07:50
05/28/19 07:50
75-35-4
cis-1,2-Dichloroethene
1.35
ug/L
1.00
0.260
1
05/28/19 07:50
05/28/19 07:50
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
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Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 106

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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-14 Lab ID: 92429865009 Collected: 05/17/19 15:25 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 07:50
05/28/19 07:50
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 07:50
05/28/19 07:50
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 07:50
05/28/19 07:50
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 07:50
05/28/19 07:50
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 07:50
05/28/19 07:50
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 07:50
05/28/19 07:50
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 07:50
05/28/19 07:50
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 07:50
05/28/19 07:50
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 07:50
05/28/19 07:50
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 07:50
05/28/19 07:50
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 07:50
05/28/19 07:50
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 07:50
05/28/19 07:50
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 07:50
05/28/19 07:50
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 07:50
05/28/19 07:50
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 07:50
05/28/19 07:50
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 07:50
05/28/19 07:50
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 07:50
05/28/19 07:50
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 07:50
05/28/19 07:50
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 07:50
05/28/19 07:50
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 07:50
05/28/19 07:50
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 07:50
05/28/19 07:50
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 07:50
05/28/19 07:50
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 07:50
05/28/19 07:50
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 07:50
05/28/19 07:50
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 07:50
05/28/19 07:50
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 07:50
05/28/19 07:50
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 07:50
05/28/19 07:50
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 07:50
05/28/19 07:50
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 07:50
05/28/19 07:50
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 07:50
05/28/19 07:50
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 07:50
05/28/19 07:50
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 07:50
05/28/19 07:50
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 07:50
05/28/19 07:50
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 07:50
05/28/19 07:50
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 07:50
05/28/19 07:50
123-91-1
89.6
%
80.0-120
1
05/28/19 07:50
05/28/19 07:50
2037-26-5
95.6
%
77.0-126
1
05/28/19 07:50
05/28/19 07:50
460-00-4
88.6
%
70.0-130
1
05/28/19 07:50
05/28/19 07:50
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 106

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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-15 Lab ID: 92429865010 Collected: 05/17/19 09:25 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:18
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:18
7440-38-2
Barium
43.5
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:18
7440-39-3
Beryllium
0.25J
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:18
7440-41-7
Cadmium
3.4
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:18
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:18
7440-47-3
Cobalt
3.3J
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:18
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:18
7440-50-8
Lead
2.OJ
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:18
7439-92-1
Nickel
2.5J
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:18
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:18
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:18
7440-22-4
Vanadium
2.2J
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:18
7440-62-2
Zinc
11.0
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:18
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.086J
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 06:54
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 08:10
05/28/19 08:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 08:10
05/28/19 08:10
107-13-1
Benzene
0.459J
ug/L
1.00
0.331
1
05/28/19 08:10
05/28/19 08:10
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 08:10
05/28/19 08:10
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 08:10
05/28/19 08:10
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 08:10
05/28/19 08:10
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 08:10
05/28/19 08:10
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 08:10
05/28/19 08:10
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 08:10
05/28/19 08:10
56-23-5
Chlorobenzene
2.33
ug/L
1.00
0.348
1
05/28/19 08:10
05/28/19 08:10
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 08:10
05/28/19 08:10
124-48-1
Chloroethane
0.531J
ug/L
5.00
0.453
1
05/28/19 08:10
05/28/19 08:10
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 08:10
05/28/19 08:10
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 08:10
05/28/19 08:10
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 08:10
05/28/19 08:10
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 08:10
05/28/19 08:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 08:10
05/28/19 08:10
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 08:10
05/28/19 08:10
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 08:10
05/28/19 08:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 08:10
05/28/19 08:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 08:10
05/28/19 08:10
541-73-1
1,4-Dichlorobenzene
3.56
ug/L
1.00
0.274
1
05/28/19 08:10
05/28/19 08:10
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 08:10
05/28/19 08:10
75-71-8
1,1-Dichloroethane
7.14
ug/L
1.00
0.259
1
05/28/19 08:10
05/28/19 08:10
75-34-3
1,2-Dichloroethane
0.479J
ug/L
1.00
0.361
1
05/28/19 08:10
05/28/19 08:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 08:10
05/28/19 08:10
75-35-4
cis-1,2-Dichloroethene
29.0
ug/L
1.00
0.260
1
05/28/19 08:10
05/28/19 08:10
156-59-2
REPORT OF LABORATORY ANALYSIS
LO
J
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 106

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-15 Lab ID: 92429865010 Collected: 05/17/19 09:25 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
0.463J
ug/L
1.00
0.396
1
05/28/19 08:10
05/28/19 08:10
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 08:10
05/28/19 08:10
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 08:10
05/28/19 08:10
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 08:10
05/28/19 08:10
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 08:10
05/28/19 08:10
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 08:10
05/28/19 08:10
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 08:10
05/28/19 08:10
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 08:10
05/28/19 08:10
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 08:10
05/28/19 08:10
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 08:10
05/28/19 08:10
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 08:10
05/28/19 08:10
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 08:10
05/28/19 08:10
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 08:10
05/28/19 08:10
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 08:10
05/28/19 08:10
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 08:10
05/28/19 08:10
108-10-1
0.443J
ug/L
1.00
0.367
1
05/28/19 08:10
05/28/19 08:10
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 08:10
05/28/19 08:10
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 08:10
05/28/19 08:10
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 08:10
05/28/19 08:10
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 08:10
05/28/19 08:10
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 08:10
05/28/19 08:10
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 08:10
05/28/19 08:10
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 08:10
05/28/19 08:10
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 08:10
05/28/19 08:10
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 08:10
05/28/19 08:10
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 08:10
05/28/19 08:10
79-00-5
2.20
ug/L
1.00
0.398
1
05/28/19 08:10
05/28/19 08:10
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 08:10
05/28/19 08:10
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 08:10
05/28/19 08:10
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 08:10
05/28/19 08:10
108-05-4
2.43
ug/L
1.00
0.259
1
05/28/19 08:10
05/28/19 08:10
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 08:10
05/28/19 08:10
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 08:10
05/28/19 08:10
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 08:10
05/28/19 08:10
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 08:10
05/28/19 08:10
123-91-1
91.5
%
80.0-120
1
05/28/19 08:10
05/28/19 08:10
2037-26-5
103
%
77.0-126
1
05/28/19 08:10
05/28/19 08:10
460-00-4
86.1
%
70.0-130
1
05/28/19 08:10
05/28/19 08:10
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
J
J
Page 23 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-16 Lab ID: 92429865011 Collected: 05/17/19 09:15 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:33
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:33
7440-38-2
Barium
71.0
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:33
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:33
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:33
7440-43-9
Chromium
3.8J
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:33
7440-47-3
Cobalt
305
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:33
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:33
7440-50-8
Lead
3.1J
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:33
7439-92-1
Nickel
15.0
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:33
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:33
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:33
7440-22-4
Vanadium
1.5J
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:33
7440-62-2
Zinc
10.4
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:33
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.29
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:01
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 08:30
05/28/19 08:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 08:30
05/28/19 08:30
107-13-1
Benzene
1.28
ug/L
1.00
0.331
1
05/28/19 08:30
05/28/19 08:30
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 08:30
05/28/19 08:30
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 08:30
05/28/19 08:30
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 08:30
05/28/19 08:30
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 08:30
05/28/19 08:30
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 08:30
05/28/19 08:30
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 08:30
05/28/19 08:30
56-23-5
Chlorobenzene
3.07
ug/L
1.00
0.348
1
05/28/19 08:30
05/28/19 08:30
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 08:30
05/28/19 08:30
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 08:30
05/28/19 08:30
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 08:30
05/28/19 08:30
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 08:30
05/28/19 08:30
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 08:30
05/28/19 08:30
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 08:30
05/28/19 08:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 08:30
05/28/19 08:30
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 08:30
05/28/19 08:30
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 08:30
05/28/19 08:30
74-95-3
1,2-Dichlorobenzene
0.482J
ug/L
1.00
0.349
1
05/28/19 08:30
05/28/19 08:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 08:30
05/28/19 08:30
541-73-1
1,4-Dichlorobenzene
6.20
ug/L
1.00
0.274
1
05/28/19 08:30
05/28/19 08:30
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 08:30
05/28/19 08:30
75-71-8
1,1-Dichloroethane
0.688J
ug/L
1.00
0.259
1
05/28/19 08:30
05/28/19 08:30
75-34-3
1,2-Dichloroethane
1.23
ug/L
1.00
0.361
1
05/28/19 08:30
05/28/19 08:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 08:30
05/28/19 08:30
75-35-4
cis-1,2-Dichloroethene
16.3
ug/L
1.00
0.260
1
05/28/19 08:30
05/28/19 08:30
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
J
LO
J
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-16 Lab ID: 92429865011 Collected: 05/17/19 09:15 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 08:30
05/28/19 08:30
156-60-5
0.824J
ug/L
1.00
0.306
1
05/28/19 08:30
05/28/19 08:30
78-87-5 J
ND
ug/L
1.00
0.352
1
05/28/19 08:30
05/28/19 08:30
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 08:30
05/28/19 08:30
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 08:30
05/28/19 08:30
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 08:30
05/28/19 08:30
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 08:30
05/28/19 08:30
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 08:30
05/28/19 08:30
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 08:30
05/28/19 08:30
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 08:30
05/28/19 08:30
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 08:30
05/28/19 08:30
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 08:30
05/28/19 08:30
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 08:30
05/28/19 08:30
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 08:30
05/28/19 08:30
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 08:30
05/28/19 08:30
108-10-1
1.27
ug/L
1.00
0.367
1
05/28/19 08:30
05/28/19 08:30
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 08:30
05/28/19 08:30
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 08:30
05/28/19 08:30
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 08:30
05/28/19 08:30
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 08:30
05/28/19 08:30
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 08:30
05/28/19 08:30
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 08:30
05/28/19 08:30
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 08:30
05/28/19 08:30
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 08:30
05/28/19 08:30
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 08:30
05/28/19 08:30
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 08:30
05/28/19 08:30
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 08:30
05/28/19 08:30
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 08:30
05/28/19 08:30
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 08:30
05/28/19 08:30
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 08:30
05/28/19 08:30
108-05-4
2.33
ug/L
1.00
0.259
1
05/28/19 08:30
05/28/19 08:30
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 08:30
05/28/19 08:30
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 08:30
05/28/19 08:30
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 08:30
05/28/19 08:30
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 08:30
05/28/19 08:30
123-91-1
90.5
%
80.0-120
1
05/28/19 08:30
05/28/19 08:30
2037-26-5
100
%
77.0-126
1
05/28/19 08:30
05/28/19 08:30
460-00-4
93.0
%
70.0-130
1
05/28/19 08:30
05/28/19 08:30
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-17 Lab ID: 92429865012 Collected: 05/17/19 14:20 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:36
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:36
7440-38-2
Barium
34.6
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:36
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:36
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:36
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:36
7440-47-3
Cobalt
4.7J
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:36
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:36
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:36
7439-92-1
Nickel
6.0
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:36
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:36
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:36
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:36
7440-62-2
Zinc
ND
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:36
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.065J
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:08
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 08:50
05/28/19 08:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 08:50
05/28/19 08:50
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 08:50
05/28/19 08:50
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 08:50
05/28/19 08:50
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 08:50
05/28/19 08:50
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 08:50
05/28/19 08:50
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 08:50
05/28/19 08:50
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 08:50
05/28/19 08:50
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 08:50
05/28/19 08:50
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 08:50
05/28/19 08:50
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 08:50
05/28/19 08:50
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 08:50
05/28/19 08:50
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 08:50
05/28/19 08:50
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 08:50
05/28/19 08:50
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 08:50
05/28/19 08:50
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 08:50
05/28/19 08:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 08:50
05/28/19 08:50
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 08:50
05/28/19 08:50
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 08:50
05/28/19 08:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 08:50
05/28/19 08:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 08:50
05/28/19 08:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 08:50
05/28/19 08:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 08:50
05/28/19 08:50
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 08:50
05/28/19 08:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 08:50
05/28/19 08:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 08:50
05/28/19 08:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 08:50
05/28/19 08:50
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-17 Lab ID: 92429865012 Collected: 05/17/19 14:20 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 08:50
05/28/19 08:50
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 08:50
05/28/19 08:50
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 08:50
05/28/19 08:50
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 08:50
05/28/19 08:50
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 08:50
05/28/19 08:50
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 08:50
05/28/19 08:50
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 08:50
05/28/19 08:50
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 08:50
05/28/19 08:50
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 08:50
05/28/19 08:50
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 08:50
05/28/19 08:50
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 08:50
05/28/19 08:50
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 08:50
05/28/19 08:50
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 08:50
05/28/19 08:50
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 08:50
05/28/19 08:50
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 08:50
05/28/19 08:50
108-10-1
0.552J
ug/L
1.00
0.367
1
05/28/19 08:50
05/28/19 08:50
1634-04-4 J
ND
ug/L
5.00
1.00
1
05/28/19 08:50
05/28/19 08:50
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 08:50
05/28/19 08:50
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 08:50
05/28/19 08:50
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 08:50
05/28/19 08:50
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 08:50
05/28/19 08:50
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 08:50
05/28/19 08:50
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 08:50
05/28/19 08:50
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 08:50
05/28/19 08:50
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 08:50
05/28/19 08:50
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 08:50
05/28/19 08:50
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 08:50
05/28/19 08:50
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 08:50
05/28/19 08:50
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 08:50
05/28/19 08:50
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 08:50
05/28/19 08:50
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 08:50
05/28/19 08:50
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 08:50
05/28/19 08:50
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 08:50
05/28/19 08:50
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 08:50
05/28/19 08:50
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 08:50
05/28/19 08:50
123-91-1
91.7
%
80.0-120
1
05/28/19 08:50
05/28/19 08:50
2037-26-5
101
%
77.0-126
1
05/28/19 08:50
05/28/19 08:50
460-00-4
88.2
%
70.0-130
1
05/28/19 08:50
05/28/19 08:50
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-19 Lab ID: 92429865013 Collected: 05/17/19 14:35 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:39
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:39
7440-38-2
Barium
40.8
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:39
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:39
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:39
7440-43-9
Chromium
2.7J
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:39
7440-47-3
Cobalt
ND
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:39
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:39
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:39
7439-92-1
Nickel
0.911
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:39
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:39
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:39
7440-22-4
Vanadium
1.7J
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:39
7440-62-2
Zinc
7.3J
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:39
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:26
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 09:10
05/28/19 09:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 09:10
05/28/19 09:10
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 09:10
05/28/19 09:10
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 09:10
05/28/19 09:10
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 09:10
05/28/19 09:10
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 09:10
05/28/19 09:10
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 09:10
05/28/19 09:10
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 09:10
05/28/19 09:10
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 09:10
05/28/19 09:10
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 09:10
05/28/19 09:10
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 09:10
05/28/19 09:10
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 09:10
05/28/19 09:10
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 09:10
05/28/19 09:10
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 09:10
05/28/19 09:10
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 09:10
05/28/19 09:10
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 09:10
05/28/19 09:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 09:10
05/28/19 09:10
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 09:10
05/28/19 09:10
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 09:10
05/28/19 09:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 09:10
05/28/19 09:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 09:10
05/28/19 09:10
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 09:10
05/28/19 09:10
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 09:10
05/28/19 09:10
75-71-8
1,1-Dichloroethane
1.07
ug/L
1.00
0.259
1
05/28/19 09:10
05/28/19 09:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 09:10
05/28/19 09:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 09:10
05/28/19 09:10
75-35-4
cis-1,2-Dichloroethene
2.06
ug/L
1.00
0.260
1
05/28/19 09:10
05/28/19 09:10
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-19 Lab ID: 92429865013 Collected: 05/17/19 14:35 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 09:10
05/28/19 09:10
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 09:10
05/28/19 09:10
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 09:10
05/28/19 09:10
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 09:10
05/28/19 09:10
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 09:10
05/28/19 09:10
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 09:10
05/28/19 09:10
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 09:10
05/28/19 09:10
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 09:10
05/28/19 09:10
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 09:10
05/28/19 09:10
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 09:10
05/28/19 09:10
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 09:10
05/28/19 09:10
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 09:10
05/28/19 09:10
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 09:10
05/28/19 09:10
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 09:10
05/28/19 09:10
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 09:10
05/28/19 09:10
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 09:10
05/28/19 09:10
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 09:10
05/28/19 09:10
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 09:10
05/28/19 09:10
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 09:10
05/28/19 09:10
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 09:10
05/28/19 09:10
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 09:10
05/28/19 09:10
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 09:10
05/28/19 09:10
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 09:10
05/28/19 09:10
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 09:10
05/28/19 09:10
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 09:10
05/28/19 09:10
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 09:10
05/28/19 09:10
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 09:10
05/28/19 09:10
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 09:10
05/28/19 09:10
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 09:10
05/28/19 09:10
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 09:10
05/28/19 09:10
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 09:10
05/28/19 09:10
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 09:10
05/28/19 09:10
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 09:10
05/28/19 09:10
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 09:10
05/28/19 09:10
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 09:10
05/28/19 09:10
123-91-1
89.9
%
80.0-120
1
05/28/19 09:10
05/28/19 09:10
2037-26-5
99.4
%
77.0-126
1
05/28/19 09:10
05/28/19 09:10
460-00-4
89.3
%
70.0-130
1
05/28/19 09:10
05/28/19 09:10
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-20 Lab ID: 92429865014 Collected: 05/17/19 17:15 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:42
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:42
7440-38-2
Barium
36.6
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:42
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:42
7440-41-7
Cadmium
0.911
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:42
7440-43-9
Chromium
1.0J
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:42
7440-47-3
Cobalt
90.1
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:42
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:42
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:42
7439-92-1
Nickel
4.OJ
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:42
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:42
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:42
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:42
7440-62-2
Zinc
8.8J
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:42
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.51
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:30
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 09:30
05/28/19 09:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 09:30
05/28/19 09:30
107-13-1
Benzene
1.15
ug/L
1.00
0.331
1
05/28/19 09:30
05/28/19 09:30
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 09:30
05/28/19 09:30
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 09:30
05/28/19 09:30
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 09:30
05/28/19 09:30
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 09:30
05/28/19 09:30
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 09:30
05/28/19 09:30
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 09:30
05/28/19 09:30
56-23-5
Chlorobenzene
1.13
ug/L
1.00
0.348
1
05/28/19 09:30
05/28/19 09:30
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 09:30
05/28/19 09:30
124-48-1
Chloroethane
0.687J
ug/L
5.00
0.453
1
05/28/19 09:30
05/28/19 09:30
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 09:30
05/28/19 09:30
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 09:30
05/28/19 09:30
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 09:30
05/28/19 09:30
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 09:30
05/28/19 09:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 09:30
05/28/19 09:30
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 09:30
05/28/19 09:30
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 09:30
05/28/19 09:30
74-95-3
1,2-Dichlorobenzene
1.04
ug/L
1.00
0.349
1
05/28/19 09:30
05/28/19 09:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 09:30
05/28/19 09:30
541-73-1
1,4-Dichlorobenzene
2.91
ug/L
1.00
0.274
1
05/28/19 09:30
05/28/19 09:30
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 09:30
05/28/19 09:30
75-71-8
1,1-Dichloroethane
1.04
ug/L
1.00
0.259
1
05/28/19 09:30
05/28/19 09:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 09:30
05/28/19 09:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 09:30
05/28/19 09:30
75-35-4
cis-1,2-Dichloroethene
6.50
ug/L
1.00
0.260
1
05/28/19 09:30
05/28/19 09:30
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
J
CC
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-20 Lab ID: 92429865014 Collected: 05/17/19 17:15 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 09:30
05/28/19 09:30
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 09:30
05/28/19 09:30
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 09:30
05/28/19 09:30
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 09:30
05/28/19 09:30
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 09:30
05/28/19 09:30
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 09:30
05/28/19 09:30
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 09:30
05/28/19 09:30
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 09:30
05/28/19 09:30
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 09:30
05/28/19 09:30
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 09:30
05/28/19 09:30
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 09:30
05/28/19 09:30
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 09:30
05/28/19 09:30
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 09:30
05/28/19 09:30
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 09:30
05/28/19 09:30
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 09:30
05/28/19 09:30
108-10-1
ND
ug/L
1.00
0.367
1
05/28/19 09:30
05/28/19 09:30
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 09:30
05/28/19 09:30
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 09:30
05/28/19 09:30
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 09:30
05/28/19 09:30
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 09:30
05/28/19 09:30
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 09:30
05/28/19 09:30
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 09:30
05/28/19 09:30
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 09:30
05/28/19 09:30
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 09:30
05/28/19 09:30
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 09:30
05/28/19 09:30
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 09:30
05/28/19 09:30
79-00-5
ND
ug/L
1.00
0.398
1
05/28/19 09:30
05/28/19 09:30
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 09:30
05/28/19 09:30
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 09:30
05/28/19 09:30
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 09:30
05/28/19 09:30
108-05-4
3.59
ug/L
1.00
0.259
1
05/28/19 09:30
05/28/19 09:30
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 09:30
05/28/19 09:30
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 09:30
05/28/19 09:30
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 09:30
05/28/19 09:30
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 09:30
05/28/19 09:30
123-91-1
91.9
%
80.0-120
1
05/28/19 09:30
05/28/19 09:30
2037-26-5
101
%
77.0-126
1
05/28/19 09:30
05/28/19 09:30
460-00-4
88.4
%
70.0-130
1
05/28/19 09:30
05/28/19 09:30
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-21 Lab ID: 92429865015 Collected: 05/17/19 14:47 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:45
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:45
7440-38-2
Barium
56.0
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:45
7440-39-3
Beryllium
0.32J
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:45
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:45
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:45
7440-47-3
Cobalt
5.1
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:45
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:45
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:45
7439-92-1
Nickel
1AJ
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:45
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:45
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:45
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:45
7440-62-2
Zinc
ND
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:45
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:44
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 09:50
05/28/19 09:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 09:50
05/28/19 09:50
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 09:50
05/28/19 09:50
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 09:50
05/28/19 09:50
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 09:50
05/28/19 09:50
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 09:50
05/28/19 09:50
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 09:50
05/28/19 09:50
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 09:50
05/28/19 09:50
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 09:50
05/28/19 09:50
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 09:50
05/28/19 09:50
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 09:50
05/28/19 09:50
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 09:50
05/28/19 09:50
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 09:50
05/28/19 09:50
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 09:50
05/28/19 09:50
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 09:50
05/28/19 09:50
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 09:50
05/28/19 09:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 09:50
05/28/19 09:50
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 09:50
05/28/19 09:50
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 09:50
05/28/19 09:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 09:50
05/28/19 09:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 09:50
05/28/19 09:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 09:50
05/28/19 09:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 09:50
05/28/19 09:50
75-71-8
1,1-Dichloroethane
2.68
ug/L
1.00
0.259
1
05/28/19 09:50
05/28/19 09:50
75-34-3
1,2-Dichloroethane
0.400J
ug/L
1.00
0.361
1
05/28/19 09:50
05/28/19 09:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 09:50
05/28/19 09:50
75-35-4
cis-1,2-Dichloroethene
14.3
ug/L
1.00
0.260
1
05/28/19 09:50
05/28/19 09:50
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
J
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-21 Lab ID: 92429865015 Collected: 05/17/19 14:47 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/19 09:50
05/28/19 09:50
156-60-5
ND
ug/L
1.00
0.306
1
05/28/19 09:50
05/28/19 09:50
78-87-5
ND
ug/L
1.00
0.352
1
05/28/19 09:50
05/28/19 09:50
563-58-6
ND
ug/L
1.00
0.366
1
05/28/19 09:50
05/28/19 09:50
142-28-9
ND
ug/L
1.00
0.418
1
05/28/19 09:50
05/28/19 09:50
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/19 09:50
05/28/19 09:50
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/19 09:50
05/28/19 09:50
594-20-7
ND
ug/L
1.00
0.320
1
05/28/19 09:50
05/28/19 09:50
108-20-3
ND
ug/L
1.00
0.384
1
05/28/19 09:50
05/28/19 09:50
100-41-4
ND
ug/L
1.00
0.256
1
05/28/19 09:50
05/28/19 09:50
87-68-3
ND
ug/L
10.0
3.82
1
05/28/19 09:50
05/28/19 09:50
591-78-6
ND
ug/L
1.00
0.350
1
05/28/19 09:50
05/28/19 09:50
99-87-6
ND
ug/L
10.0
3.93
1
05/28/19 09:50
05/28/19 09:50
78-93-3
ND
ug/L
5.00
1.00
1
05/28/19 09:50
05/28/19 09:50
75-09-2
ND
ug/L
10.0
2.14
1
05/28/19 09:50
05/28/19 09:50
108-10-1
0.865J
ug/L
1.00
0.367
1
05/28/19 09:50
05/28/19 09:50
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/19 09:50
05/28/19 09:50
91-20-3
ND
ug/L
1.00
0.307
1
05/28/19 09:50
05/28/19 09:50
100-42-5
ND
ug/L
1.00
0.385
1
05/28/19 09:50
05/28/19 09:50
630-20-6
ND
ug/L
1.00
0.130
1
05/28/19 09:50
05/28/19 09:50
79-34-5
ND
ug/L
1.00
0.372
1
05/28/19 09:50
05/28/19 09:50
127-18-4
ND
ug/L
1.00
0.412
1
05/28/19 09:50
05/28/19 09:50
108-88-3
ND
ug/L
1.00
0.230
1
05/28/19 09:50
05/28/19 09:50
87-61-6
ND
ug/L
1.00
0.355
1
05/28/19 09:50
05/28/19 09:50
120-82-1
ND
ug/L
1.00
0.319
1
05/28/19 09:50
05/28/19 09:50
71-55-6
ND
ug/L
1.00
0.383
1
05/28/19 09:50
05/28/19 09:50
79-00-5
0.772J
ug/L
1.00
0.398
1
05/28/19 09:50
05/28/19 09:50
79-01-6
ND
ug/L
5.00
1.20
1
05/28/19 09:50
05/28/19 09:50
75-69-4
ND
ug/L
2.50
0.807
1
05/28/19 09:50
05/28/19 09:50
96-18-4
ND
ug/L
10.0
1.63
1
05/28/19 09:50
05/28/19 09:50
108-05-4
ND
ug/L
1.00
0.259
1
05/28/19 09:50
05/28/19 09:50
75-01-4
ND
ug/L
1.00
0.341
1
05/28/19 09:50
05/28/19 09:50
95-47-6
ND
ug/L
2.00
0.719
1
05/28/19 09:50
05/28/19 09:50
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/19 09:50
05/28/19 09:50
1330-20-7
ND
ug/L
100
36.0
1
05/28/19 09:50
05/28/19 09:50
123-91-1
92.6
%
80.0-120
1
05/28/19 09:50
05/28/19 09:50
2037-26-5
101
%
77.0-126
1
05/28/19 09:50
05/28/19 09:50
460-00-4
87.8
%
70.0-130
1
05/28/19 09:50
05/28/19 09:50
17060-07-0
REPORT OF LABORATORY ANALYSIS
J
J
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-22 Lab ID: 92429865016 Collected: 05/17/19 14:18 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:48
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:48
7440-38-2
Barium
51.0
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:48
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:48
7440-41-7
Cadmium
0.47J
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:48
7440-43-9
Chromium
2.OJ
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:48
7440-47-3
Cobalt
14.4
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:48
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:48
7440-50-8
Lead
2.OJ
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:48
7439-92-1
Nickel
7.1
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:48
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:48
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:48
7440-22-4
Vanadium
1.5J
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:48
7440-62-2
Zinc
18.2
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:48
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.11
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:47
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 10:10
05/28/19 10:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 10:10
05/28/19 10:10
107-13-1
Benzene
0.332J
ug/L
1.00
0.331
1
05/28/19 10:10
05/28/19 10:10
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 10:10
05/28/19 10:10
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 10:10
05/28/19 10:10
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 10:10
05/28/19 10:10
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 10:10
05/28/19 10:10
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 10:10
05/28/19 10:10
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 10:10
05/28/19 10:10
56-23-5
Chlorobenzene
0.958J
ug/L
1.00
0.348
1
05/28/19 10:10
05/28/19 10:10
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 10:10
05/28/19 10:10
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 10:10
05/28/19 10:10
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 10:10
05/28/19 10:10
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 10:10
05/28/19 10:10
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 10:10
05/28/19 10:10
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 10:10
05/28/19 10:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 10:10
05/28/19 10:10
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 10:10
05/28/19 10:10
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 10:10
05/28/19 10:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 10:10
05/28/19 10:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 10:10
05/28/19 10:10
541-73-1
1,4-Dichlorobenzene
1.83
ug/L
1.00
0.274
1
05/28/19 10:10
05/28/19 10:10
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 10:10
05/28/19 10:10
75-71-8
1,1-Dichloroethane
0.9001
ug/L
1.00
0.259
1
05/28/19 10:10
05/28/19 10:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 10:10
05/28/19 10:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 10:10
05/28/19 10:10
75-35-4
cis-1,2-Dichloroethene
1.94
ug/L
1.00
0.260
1
05/28/19 10:10
05/28/19 10:10
156-59-2
REPORT OF LABORATORY ANALYSIS
LO
J
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-22 Lab ID: 92429865016 Collected: 05/17/19 14:18 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1910:10
05/28/1910:10
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1910:10
05/28/1910:10
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1910:10
05/28/1910:10
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1910:10
05/28/1910:10
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1910:10
05/28/1910:10
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1910:10
05/28/1910:10
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1910:10
05/28/1910:10
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1910:10
05/28/1910:10
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1910:10
05/28/1910:10
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1910:10
05/28/1910:10
87-68-3
ND
ug/L
10.0
3.82
1
05/28/1910:10
05/28/1910:10
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1910:10
05/28/1910:10
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1910:10
05/28/1910:10
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1910:10
05/28/1910:10
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1910:10
05/28/1910:10
108-10-1
0.768J
ug/L
1.00
0.367
1
05/28/1910:10
05/28/1910:10
1634-04-4 J
ND
ug/L
5.00
1.00
1
05/28/1910:10
05/28/1910:10
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1910:10
05/28/1910:10
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1910:10
05/28/1910:10
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1910:10
05/28/1910:10
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1910:10
05/28/1910:10
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1910:10
05/28/1910:10
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1910:10
05/28/1910:10
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1910:10
05/28/1910:10
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1910:10
05/28/1910:10
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1910:10
05/28/1910:10
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1910:10
05/28/1910:10
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1910:10
05/28/1910:10
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1910:10
05/28/1910:10
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1910:10
05/28/1910:10
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1910:10
05/28/1910:10
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1910:10
05/28/1910:10
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1910:10
05/28/1910:10
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1910:10
05/28/1910:10
1330-20-7
ND
ug/L
100
36.0
1
05/28/1910:10
05/28/1910:10
123-91-1
88.9
%
80.0-120
1
05/28/1910:10
05/28/1910:10
2037-26-5
101
%
77.0-126
1
05/28/1910:10
05/28/1910:10
460-00-4
92.7
%
70.0-130
1
05/28/1910:10
05/28/1910:10
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 35 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-23
Lab ID:
92429865017
Collected:
05/17/19
16:16
Received: 05/20/19 11:26 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 601
OD Preparation Method: EPA 301 OA
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:52
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:52
7440-38-2
Barium
23.8
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:52
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:52
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:52
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:52
7440-47-3
Cobalt
ND
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:52
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:52
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:52
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:52
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:52
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:52
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:52
7440-62-2
Zinc
ND
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:52
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method:
EPA 3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:54
7440-28-0
VOA (GC/MS) 8260D
Analytical
Method: EPA 8260D
Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 10:30
05/28/19 10:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 10:30
05/28/19 10:30
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 10:30
05/28/19 10:30
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 10:30
05/28/19 10:30
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 10:30
05/28/19 10:30
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 10:30
05/28/19 10:30
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 10:30
05/28/19 10:30
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 10:30
05/28/19 10:30
74-83-9
CC
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 10:30
05/28/19 10:30
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 10:30
05/28/19 10:30
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 10:30
05/28/19 10:30
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 10:30
05/28/19 10:30
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 10:30
05/28/19 10:30
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 10:30
05/28/19 10:30
74-87-3
CC
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 10:30
05/28/19 10:30
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 10:30
05/28/19 10:30
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 10:30
05/28/19 10:30
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 10:30
05/28/19 10:30
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 10:30
05/28/19 10:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 10:30
05/28/19 10:30
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 10:30
05/28/19 10:30
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 10:30
05/28/19 10:30
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 10:30
05/28/19 10:30
75-71-8
LO
1,1-Dichloroethane
0.561J
ug/L
1.00
0.259
1
05/28/19 10:30
05/28/19 10:30
75-34-3
J
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 10:30
05/28/19 10:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 10:30
05/28/19 10:30
75-35-4
cis-1,2-Dichloroethene
0.896J
ug/L
1.00
0.260
1
05/28/19 10:30
05/28/19 10:30
156-59-2
J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: MW-23 Lab ID: 92429865017 Collected: 05/17/19 16:16 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1910:30
05/28/1910:30
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1910:30
05/28/1910:30
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1910:30
05/28/1910:30
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1910:30
05/28/1910:30
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1910:30
05/28/1910:30
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1910:30
05/28/1910:30
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1910:30
05/28/1910:30
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1910:30
05/28/1910:30
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1910:30
05/28/1910:30
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1910:30
05/28/1910:30
87-68-3
ND
ug/L
10.0
3.82
1
05/28/1910:30
05/28/1910:30
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1910:30
05/28/1910:30
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1910:30
05/28/1910:30
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1910:30
05/28/1910:30
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1910:30
05/28/1910:30
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1910:30
05/28/1910:30
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1910:30
05/28/1910:30
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1910:30
05/28/1910:30
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1910:30
05/28/1910:30
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1910:30
05/28/1910:30
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1910:30
05/28/1910:30
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1910:30
05/28/1910:30
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1910:30
05/28/1910:30
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1910:30
05/28/1910:30
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1910:30
05/28/1910:30
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1910:30
05/28/1910:30
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1910:30
05/28/1910:30
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1910:30
05/28/1910:30
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1910:30
05/28/1910:30
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1910:30
05/28/1910:30
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1910:30
05/28/1910:30
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1910:30
05/28/1910:30
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1910:30
05/28/1910:30
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1910:30
05/28/1910:30
1330-20-7
ND
ug/L
100
36.0
1
05/28/1910:30
05/28/1910:30
123-91-1
90.4
%
80.0-120
1
05/28/1910:30
05/28/1910:30
2037-26-5
100
%
77.0-126
1
05/28/1910:30
05/28/1910:30
460-00-4
92.0
%
70.0-130
1
05/28/1910:30
05/28/1910:30
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 37 of 106

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: SCALEHOUSE Lab ID: 92429865018 Collected: 05/17/19 15:03 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/04/19 00:55
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:55
7440-38-2
Barium
12.3
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:55
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/04/19 00:55
7440-41-7
Cadmium
ND
ug/L
1.0
0.40
1
06/03/19 12:21
06/04/19 00:55
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/04/19 00:55
7440-47-3
Cobalt
ND
ug/L
5.0
1.1
1
06/03/19 12:21
06/04/19 00:55
7440-48-4
Copper
2.9J
ug/L
5.0
2.1
1
06/03/19 12:21
06/04/19 00:55
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
06/03/19 12:21
06/04/19 00:55
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
06/03/19 12:21
06/04/19 00:55
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/04/19 00:55
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/04/19 00:55
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/04/19 00:55
7440-62-2
Zinc
5.8J
ug/L
10.0
3.9
1
06/03/19 12:21
06/04/19 00:55
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 07:58
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 10:50
05/28/19 10:50
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 10:50
05/28/19 10:50
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 10:50
05/28/19 10:50
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 10:50
05/28/19 10:50
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 10:50
05/28/19 10:50
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 10:50
05/28/19 10:50
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 10:50
05/28/19 10:50
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 10:50
05/28/19 10:50
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 10:50
05/28/19 10:50
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 10:50
05/28/19 10:50
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 10:50
05/28/19 10:50
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 10:50
05/28/19 10:50
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 10:50
05/28/19 10:50
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 10:50
05/28/19 10:50
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 10:50
05/28/19 10:50
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 10:50
05/28/19 10:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 10:50
05/28/19 10:50
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 10:50
05/28/19 10:50
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 10:50
05/28/19 10:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 10:50
05/28/19 10:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 10:50
05/28/19 10:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 10:50
05/28/19 10:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 10:50
05/28/19 10:50
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 10:50
05/28/19 10:50
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 10:50
05/28/19 10:50
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 10:50
05/28/19 10:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 10:50
05/28/19 10:50
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 106

aceAnalXical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Sample: SCALEHOUSE Lab ID: 92429865018 Collected: 05/17/19 15:03 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 03:55 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1910:50
05/28/1910:50
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1910:50
05/28/1910:50
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1910:50
05/28/1910:50
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1910:50
05/28/1910:50
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1910:50
05/28/1910:50
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1910:50
05/28/1910:50
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1910:50
05/28/1910:50
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1910:50
05/28/1910:50
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1910:50
05/28/1910:50
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1910:50
05/28/1910:50
87-68-3
ND
ug/L
10.0
3.82
1
05/28/1910:50
05/28/1910:50
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1910:50
05/28/1910:50
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1910:50
05/28/1910:50
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1910:50
05/28/1910:50
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1910:50
05/28/1910:50
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1910:50
05/28/1910:50
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1910:50
05/28/1910:50
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1910:50
05/28/1910:50
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1910:50
05/28/1910:50
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1910:50
05/28/1910:50
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1910:50
05/28/1910:50
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1910:50
05/28/1910:50
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1910:50
05/28/1910:50
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1910:50
05/28/1910:50
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1910:50
05/28/1910:50
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1910:50
05/28/1910:50
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1910:50
05/28/1910:50
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1910:50
05/28/1910:50
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1910:50
05/28/1910:50
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1910:50
05/28/1910:50
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1910:50
05/28/1910:50
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1910:50
05/28/1910:50
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1910:50
05/28/1910:50
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1910:50
05/28/1910:50
1330-20-7
ND
ug/L
100
36.0
1
05/28/1910:50
05/28/1910:50
123-91-1
92.0
%
80.0-120
1
05/28/1910:50
05/28/1910:50
2037-26-5
99.9
%
77.0-126
1
05/28/1910:50
05/28/1910:50
460-00-4
89.8
%
70.0-130
1
05/28/1910:50
05/28/1910:50
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 39 of 106

aceAnalXical
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
QC Batch: 478711 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92429865002, 92429865003, 92429865004, 92429865005, 92429865006, 92429865007, 92429865008,
92429865009,92429865010,92429865011,92429865012,92429865013,92429865014,92429865015,
92429865016,92429865017,92429865018
METHOD BLANK: 2591279 Matrix: Water
Associated Lab Samples: 92429865002, 92429865003, 92429865004, 92429865005, 92429865006, 92429865007, 92429865008,
92429865009,92429865010,92429865011,92429865012,92429865013,92429865014,92429865015,
92429865016,92429865017,92429865018
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
5.0
3.0
06/03/19 23:26
Arsenic
ug/L
ND
10.0
4.7
06/03/19 23:26
Barium
ug/L
ND
5.0
1.0
06/03/19 23:26
Beryllium
ug/L
ND
1.0
0.20
06/03/19 23:26
Cadmium
ug/L
ND
1.0
0.40
06/03/19 23:26
Chromium
ug/L
ND
5.0
1.0
06/03/19 23:26
Cobalt
ug/L
ND
5.0
1.1
06/03/19 23:26
Copper
ug/L
ND
5.0
2.1
06/03/19 23:26
Lead
ug/L
ND
5.0
1.6
06/03/19 23:26
Nickel
ug/L
ND
5.0
0.90
06/03/19 23:26
Selenium
ug/L
ND
10.0
4.7
06/03/19 23:26
Silver
ug/L
ND
5.0
2.5
06/03/19 23:26
Vanadium
ug/L
ND
5.0
1.3
06/03/19 23:26
Zinc
ug/L
ND
10.0
3.9
06/03/19 23:26
LABORATORY CONTROL SAMPLE:
Parameter
2591280
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
498
100
80-120
Arsenic
ug/L
500
480
96
80-120
Barium
ug/L
500
488
98
80-120
Beryllium
ug/L
500
497
99
80-120
Cadmium
ug/L
500
492
98
80-120
Chromium
ug/L
500
498
100
80-120
Cobalt
ug/L
500
497
99
80-120
Copper
ug/L
500
503
101
80-120
Lead
ug/L
500
487
97
80-120
Nickel
ug/L
500
490
98
80-120
Selenium
ug/L
500
497
99
80-120
Silver
ug/L
250
250
100
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
498
100
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
SURRY CLOSED -MT. AIRY
92429865
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE: 2591281
2591282
MS
MSD
92429865001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
470
472
94
94
75-125
1
20
Arsenic
ug/L
ND
500
500
475
475
95
95
75-125
0
20
Barium
ug/L
47.0
500
500
519
526
94
96
75-125
1
20
Beryllium
ug/L
ND
500
500
482
489
96
98
75-125
1
20
Cadmium
ug/L
0.911
500
500
489
494
98
99
75-125
1
20
Chromium
ug/L
ND
500
500
488
491
98
98
75-125
0
20
Cobalt
ug/L
2.5J
500
500
485
490
97
97
75-125
1
20
Copper
ug/L
ND
500
500
486
489
97
98
75-125
1
20
Lead
ug/L
1.7J
500
500
477
477
95
95
75-125
0
20
Nickel
ug/L
1.6J
500
500
479
483
95
96
75-125
1
20
Selenium
ug/L
ND
500
500
511
516
102
103
75-125
1
20
Silver
ug/L
ND
250
250
236
239
95
96
75-125
1
20
Vanadium
ug/L
ND
500
500
487
490
97
98
75-125
1
20
Zinc
ug/L
9.3J
500
500
509
511
100
100
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
QC Batch: 478573 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92429865002, 92429865003, 92429865004, 92429865005, 92429865006, 92429865007, 92429865008,
92429865009,92429865010,92429865011,92429865012,92429865013,92429865014,92429865015,
92429865016,92429865017,92429865018
METHOD BLANK: 2590560 Matrix: Water
Associated Lab Samples: 92429865002, 92429865003, 92429865004, 92429865005, 92429865006, 92429865007, 92429865008,
92429865009,92429865010,92429865011,92429865012,92429865013,92429865014,92429865015,
92429865016,92429865017,92429865018
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.060 06/06/19 05:08
LABORATORY CONTROL SAMPLE: 2590561
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10.1 101 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2590562 2590563
MS MSD
92429865001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 10.1 10.2 101 102 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC.
Page 42 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
QC Batch: 1287157 Analysis Method: EPA 8260D
QC Batch Method: 8260D Analysis Description: VOA (GC/MS) 8260D
Associated Lab Samples: 92429865002, 92429865003, 92429865004, 92429865005, 92429865006, 92429865007, 92429865008,
92429865009,92429865010,92429865011,92429865012,92429865013,92429865014,92429865015,
92429865016,92429865017,92429865018
METHOD BLANK: R3415400-3 Matrix: Water
Associated Lab Samples: 92429865002, 92429865003, 92429865004, 92429865005, 92429865006, 92429865007, 92429865008,
92429865009,92429865010,92429865011,92429865012,92429865013,92429865014,92429865015,
92429865016,92429865017,92429865018
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Acetone
ug/L
ND
50.0
10.0
05/28/19 04:50
Acrylonitrile
ug/L
ND
10.0
1.87
05/28/19 04:50
Benzene
ug/L
ND
1.00
0.331
05/28/19 04:50
Bromobenzene
ug/L
ND
1.00
0.352
05/28/19 04:50
Bromodichloromethane
ug/L
ND
1.00
0.380
05/28/19 04:50
Bromochloromethane
ug/L
ND
5.00
0.520
05/28/19 04:50
Bromoform
ug/L
ND
1.00
0.469
05/28/19 04:50
Bromomethane
ug/L
ND
5.00
0.866
05/28/19 04:50
Carbon tetrachloride
ug/L
ND
1.00
0.379
05/28/19 04:50
Chlorobenzene
ug/L
ND
1.00
0.348
05/28/19 04:50
Dibromochloromethane
ug/L
ND
1.00
0.327
05/28/19 04:50
Chloroethane
ug/L
ND
5.00
0.453
05/28/19 04:50
Chloroform
ug/L
ND
5.00
0.324
05/28/19 04:50
Chloromethane
ug/L
ND
2.50
0.276
05/28/19 04:50
2-Chlorotoluene
ug/L
ND
1.00
0.375
05/28/19 04:50
4-Chlorotoluene
ug/L
ND
1.00
0.351
05/28/19 04:50
1,2-Dibromo-3-chloropropane
ug/L
ND
5.00
1.33
05/28/19 04:50
1,2-Dibromoethane (EDB)
ug/L
ND
1.00
0.381
05/28/19 04:50
Dibromomethane
ug/L
ND
1.00
0.346
05/28/19 04:50
1,2-Dichlorobenzene
ug/L
ND
1.00
0.349
05/28/19 04:50
1,3-Dichlorobenzene
ug/L
ND
1.00
0.220
05/28/19 04:50
1,4-Dichlorobenzene
ug/L
ND
1.00
0.274
05/28/19 04:50
Dichlorodifluoromethane
ug/L
ND
5.00
0.551
05/28/19 04:50
1,1-Dichloroethane
ug/L
ND
1.00
0.259
05/28/19 04:50
1,2-Dichloroethane
ug/L
ND
1.00
0.361
05/28/19 04:50
1,1-Dichloroethene
ug/L
ND
1.00
0.398
05/28/19 04:50
cis-1,2-Dichloroethene
ug/L
ND
1.00
0.260
05/28/19 04:50
trans-1,2-Dichloroethene
ug/L
ND
1.00
0.396
05/28/19 04:50
1,2-Dichloropropane
ug/L
ND
1.00
0.306
05/28/19 04:50
1,1-Dichloropropene
ug/L
ND
1.00
0.352
05/28/19 04:50
1,3-Dichloropropane
ug/L
ND
1.00
0.366
05/28/19 04:50
cis-1,3-Dichloropropene
ug/L
ND
1.00
0.418
05/28/19 04:50
trans- 1,3-Dichloropropene
ug/L
ND
1.00
0.419
05/28/19 04:50
2,2-Dichloropropane
ug/L
ND
1.00
0.321
05/28/19 04:50
Diisopropyl ether
ug/L
ND
1.00
0.320
05/28/19 04:50
Ethylbenzene
ug/L
ND
1.00
0.384
05/28/19 04:50
Hexachloro-1,3-butadiene
ug/L
ND
1.00
0.256
05/28/19 04:50
2-Hexanone
ug/L
ND
10.0
3.82
05/28/19 04:50
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
METHOD BLANK: R3415400-3 Matrix: Water
Associated Lab Samples: 92429865002, 92429865003, 92429865004, 92429865005, 92429865006, 92429865007, 92429865008,
92429865009,92429865010,92429865011,92429865012,92429865013,92429865014,92429865015,
92429865016,92429865017,92429865018
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
p-Isopropyltoluene
ug/L
ND
1.00
0.350
05/28/19 04:50
2-Butanone (MEK)
ug/L
ND
10.0
3.93
05/28/19 04:50
Methylene Chloride
ug/L
ND
5.00
1.00
05/28/19 04:50
4-Methyl-2-pentanone (MIBK)
ug/L
ND
10.0
2.14
05/28/19 04:50
Methyl-tert-butyl ether
ug/L
ND
1.00
0.367
05/28/19 04:50
Naphthalene
ug/L
ND
5.00
1.00
05/28/19 04:50
Styrene
ug/L
ND
1.00
0.307
05/28/19 04:50
1,1,1,2-Tetrachloroethane
ug/L
ND
1.00
0.385
05/28/19 04:50
1,1,2,2-Tetrachloroethane
ug/L
ND
1.00
0.130
05/28/19 04:50
Tetrachloroethene
ug/L
ND
1.00
0.372
05/28/19 04:50
Toluene
ug/L
ND
1.00
0.412
05/28/19 04:50
1,2,3-Trichlorobenzene
ug/L
ND
1.00
0.230
05/28/19 04:50
1,2,4-Trichlorobenzene
ug/L
ND
1.00
0.355
05/28/19 04:50
1,1,1-Trichloroethane
ug/L
ND
1.00
0.319
05/28/19 04:50
1,1,2-Trichloroethane
ug/L
ND
1.00
0.383
05/28/19 04:50
Trichloroethene
ug/L
ND
1.00
0.398
05/28/19 04:50
Trichlorofluoromethane
ug/L
ND
5.00
1.20
05/28/19 04:50
1,2,3-Trichloropropane
ug/L
ND
2.50
0.807
05/28/19 04:50
Vinyl acetate
ug/L
ND
10.0
1.63
05/28/19 04:50
Vinyl chloride
ug/L
ND
1.00
0.259
05/28/19 04:50
Xylene (Total)
ug/L
ND
3.00
1.06
05/28/19 04:50
o-Xylene
ug/L
ND
1.00
0.341
05/28/19 04:50
m&p-Xylene
ug/L
ND
2.00
0.719
05/28/19 04:50
1,4-Dioxane (p-Dioxane)
ug/L
ND
100
36.0
05/28/19 04:50
Toluene-d8 (S)
%
93
80.0-120
05/28/19 04:50
4-Bromofluorobenzene (S)
%
98.8
77.0-126
05/28/19 04:50
1,2-Dichloroethane-d4 (S)
%
89.8
70.0-130
05/28/19 04:50
LABORATORY CONTROL SAMPLE:
R3415400-1
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Acetone
ug/L
125
134
107
19.0-160
Acrylonitrile
ug/L
125
148
118
55.0-149
Benzene
ug/L
25.0
28.2
113
70.0-123
Bromobenzene
ug/L
25.0
22.2
89.0
73.0-121
Bromodichloromethane
ug/L
25.0
28.6
115
75.0-120
Bromochloromethane
ug/L
25.0
24.7
98.7
76.0-122
Bromoform
ug/L
25.0
25.1
100
68.0-132
Bromomethane
ug/L
25.0
14.5
58.1
10.0-160
Carbon tetrachloride
ug/L
25.0
29.3
117
68.0-126
Chlorobenzene
ug/L
25.0
26.3
105
80.0-121
Dibromochloromethane
ug/L
25.0
25.7
103
77.0-125
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
LABORATORY CONTROL SAMPLE:
Parameter
R3415400-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloroethane
ug/L
25.0
26.2
105
47.0-150
Chloroform
ug/L
25.0
28.1
112
73.0-120
Chloromethane
ug/L
25.0
12.7
50.9
41.0-142
2-Chlorotoluene
ug/L
25.0
22.2
88.8
76.0-123
4-Chlorotoluene
ug/L
25.0
23.3
93.3
75.0-122
1,2-Dibromo-3-chloropropane
ug/L
25.0
21.8
87.4
58.0-134
1,2-Dibromoethane (EDB)
ug/L
25.0
27.1
109
80.0-122
Dibromomethane
ug/L
25.0
27.4
110
80.0-120
1,2-Dichlorobenzene
ug/L
25.0
24.6
98.5
79.0-121
1,3-Dichlorobenzene
ug/L
25.0
23.5
94.0
79.0-120
1,4-Dichlorobenzene
ug/L
25.0
22.9
91.5
79.0-120
Dichlorodifluoromethane
ug/L
25.0
12.4
49.5
51.0-149 LO
1,1-Dichloroethane
ug/L
25.0
28.3
113
70.0-126
1,2-Dichloroethane
ug/L
25.0
25.9
104
70.0-128
1,1-Dichloroethene
ug/L
25.0
30.5
122
71.0-124
cis-1,2-Dichloroethene
ug/L
25.0
28.0
112
73.0-120
trans-1,2-Dichloroethene
ug/L
25.0
30.0
120
73.0-120
1,2-Dichloropropane
ug/L
25.0
27.8
111
77.0-125
1,1-Dichloropropene
ug/L
25.0
29.9
119
74.0-126
1,3-Dichloropropane
ug/L
25.0
27.1
108
80.0-120
cis-1,3-Dichloropropene
ug/L
25.0
29.1
116
80.0-123
trans- 1,3-Dichloropropene
ug/L
25.0
25.8
103
78.0-124
2,2-Dichloropropane
ug/L
25.0
25.9
104
58.0-130
Diisopropyl ether
ug/L
25.0
27.5
110
58.0-138
Ethylbenzene
ug/L
25.0
27.0
108
79.0-123
Hexachloro-1,3-butadiene
ug/L
25.0
20.9
83.5
54.0-138
2-Hexanone
ug/L
125
136
109
67.0-149
p-Isopropyltoluene
ug/L
25.0
22.3
89.0
76.0-125
2-Butanone (MEK)
ug/L
125
130
104
44.0-160
Methylene Chloride
ug/L
25.0
27.3
109
67.0-120
4-Methyl-2-pentanone (MIBK)
ug/L
125
127
102
68.0-142
Methyl-tert-butyl ether
ug/L
25.0
28.8
115
68.0-125
Naphthalene
ug/L
25.0
22.2
88.8
54.0-135
Styrene
ug/L
25.0
28.0
112
73.0-130
1,1,1,2-Tetrachloroethane
ug/L
25.0
26.1
104
75.0-125
1,1,2,2-Tetrachloroethane
ug/L
25.0
23.1
92.4
65.0-130
Tetrachloroethene
ug/L
25.0
28.4
114
72.0-132
Toluene
ug/L
25.0
25.4
102
79.0-120
1,2,3-Trichlorobenzene
ug/L
25.0
22.3
89.1
50.0-138
1,2,4-Trichlorobenzene
ug/L
25.0
23.0
91.8
57.0-137
1,1,1-Trichloroethane
ug/L
25.0
29.8
119
73.0-124
1,1,2-Trichloroethane
ug/L
25.0
25.8
103
80.0-120
Trichloroethene
ug/L
25.0
30.5
122
78.0-124
Trichlorofluoromethane
ug/L
25.0
32.7
131
59.0-147
1,2,3-Trichloropropane
ug/L
25.0
23.9
95.7
73.0-130
Vinyl acetate
ug/L
125
113
90.7
11.0-160
Vinyl chloride
ug/L
25.0
31.6
126
67.0-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
LABORATORY CONTROL SAMPLE:
R3415400-1
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits
Xylene (Total)
ug/L
75.0
77.1 103
79.0-123
o-Xylene
ug/L
25.0
26.0 104
80.0-122
m&p-Xylene
ug/L
50.0
51.1 102
80.0-122
Toluene-d8 (S)
%
92.2
80.0-120
4-Bromofluorobenzene (S)
%
104
77.0-126
1,2-Dichloroethane-d4 (S)
%
86.0
70.0-130
LABORATORY CONTROL SAMPLE:
R3415400-2
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits
1,4-Dioxane (p-Dioxane)
ug/L
1000 988 98.8
13.0-160
Toluene-d8 (S)
%
92.0
80.0-120
4-Bromofluorobenzene (S)
%
100
77.0-126
1,2-Dichloroethane-d4 (S)
%
91.5
70.0-130
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC.
Page 46 of 106

Pace Analytical Services, LLC
aceAnalXical� 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PAN Pace Analytical National
PASI-A Pace Analytical Services - Asheville
ANALYTE QUALIFIERS
CC The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The result may be biased.
J Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92429865002
MW-311
EPA 3010A
478711
EPA 6010D
478791
92429865003
MW-6
EPA 3010A
478711
EPA 6010D
478791
92429865004
MW-7
EPA 3010A
478711
EPA 6010D
478791
92429865005
MW-9
EPA 3010A
478711
EPA 6010D
478791
92429865006
MW-11
EPA 3010A
478711
EPA 6010D
478791
92429865007
MW-12S
EPA 3010A
478711
EPA 6010D
478791
92429865008
MW-13
EPA 3010A
478711
EPA 6010D
478791
92429865009
MW-14
EPA 3010A
478711
EPA 6010D
478791
92429865010
MW-15
EPA 3010A
478711
EPA 6010D
478791
92429865011
MW-16
EPA 3010A
478711
EPA 6010D
478791
92429865012
MW-17
EPA 3010A
478711
EPA 6010D
478791
92429865013
MW-19
EPA 3010A
478711
EPA 6010D
478791
92429865014
MW-20
EPA 3010A
478711
EPA 6010D
478791
92429865015
MW-21
EPA 3010A
478711
EPA 6010D
478791
92429865016
MW-22
EPA 3010A
478711
EPA 6010D
478791
92429865017
MW-23
EPA 3010A
478711
EPA 6010D
478791
92429865018
SCALEHOUSE
EPA 3010A
478711
EPA 6010D
478791
92429865002
MW-3R
EPA 3010A
478573
EPA 6020B
478747
92429865003
MW-6
EPA 3010A
478573
EPA 6020B
478747
92429865004
MW-7
EPA 3010A
478573
EPA 6020B
478747
92429865005
MW-9
EPA 3010A
478573
EPA 6020B
478747
92429865006
MW-11
EPA 3010A
478573
EPA 6020B
478747
92429865007
MW-12S
EPA 3010A
478573
EPA 6020B
478747
92429865008
MW-13
EPA 3010A
478573
EPA 6020B
478747
92429865009
MW-14
EPA 3010A
478573
EPA 6020B
478747
92429865010
MW-15
EPA 3010A
478573
EPA 6020B
478747
92429865011
MW-16
EPA 3010A
478573
EPA 6020B
478747
92429865012
MW-17
EPA 3010A
478573
EPA 6020B
478747
92429865013
MW-19
EPA 3010A
478573
EPA 6020B
478747
92429865014
MW-20
EPA 3010A
478573
EPA 6020B
478747
92429865015
MW-21
EPA 3010A
478573
EPA 6020B
478747
92429865016
MW-22
EPA 3010A
478573
EPA 6020B
478747
92429865017
MW-23
EPA 3010A
478573
EPA 6020B
478747
92429865018
SCALEHOUSE
EPA 3010A
478573
EPA 6020B
478747
92429865002
MW-3R
8260D
1287157
EPA 8260D
1287157
92429865003
MW-6
8260D
1287157
EPA 8260D
1287157
92429865004
MW-7
8260D
1287157
EPA 8260D
1287157
92429865005
MW-9
8260D
1287157
EPA 8260D
1287157
92429865006
MW-11
8260D
1287157
EPA 8260D
1287157
92429865007
MW-12S
8260D
1287157
EPA 8260D
1287157
92429865008
MW-13
8260D
1287157
EPA 8260D
1287157
92429865009
MW-14
8260D
1287157
EPA 8260D
1287157
92429865010
MW-15
8260D
1287157
EPA 8260D
1287157
92429865011
MW-16
8260D
1287157
EPA 8260D
1287157
92429865012
MW-17
8260D
1287157
EPA 8260D
1287157
92429865013
MW-19
8260D
1287157
EPA 8260D
1287157
92429865014
MW-20
8260D
1287157
EPA 8260D
1287157
92429865015
MW-21
8260D
1287157
EPA 8260D
1287157
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 03:55 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: SURRY CLOSED -MT. AIRY
Pace Project No.: 92429865
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92429865016
MW-22
8260D
1287157
EPA 8260D
1287157
92429865017
MW-23
8260D
1287157
EPA 8260D
1287157
92429865018
SCALEHOUSE
8260D
1287157
EPA 8260D
1287157
Date: 07/05/2019 03:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 49 of 106

Document Name:
Document Revised: February 7, 2018
m
Analytical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh[ Mechanicsville)-1
Sarnple-Condition Client Name: WQ# : 92429865
Upon Receipt r Project
Courier: Fe x UP5 ❑USPS 1 ❑Client 92429665
❑ Commercial 9face ❑Other:
Custody Seal Present? []Yes No Seals Intact? [-]Yes 050
Packing Material: ❑Bubble Wrap 8ubble Bags ❑None ❑ Other
Thermometer.ff,IA 92TO48 Type of Ire: evvet ❑slue
Gu n ID:�,r
Cooler Temp ('C): V II ,, Correction Factor: Add/Subtract (°C) 0.0
Cooler Temp Corrected ('C): V'
USDA Regulated Soil flET N/A, water sample)
Did samples origin^ to in a quarantine zone within the United States: CA, NY, or SC (check maps)?
Div-
Date/initials Person Examining Contents:
Biofog�ical issue Frozen?
❑Yes F[No []N/A
[None
Temp should be above freezing to 6°C
[]samples out of temp criteria.samples an ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
inrlurfia¢ Hawaii and Puerto Rlcal? MYes FIINO
Comments/Discrepancy:
Chain of Custody Present?
Wes
❑No
❑N/A
1.
Samples Arrived within Hold Time? .
Yes
[]No
El N/A
2,
Short Hold Time Analysis (-C72 hr.)?
❑Yes
2f4o
❑NIA
3.
Rush Turn Around Time Requested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
Yes
❑No
❑N/A
5.
Correct Containers Used?
OJY
[:IN.❑N/A
6,
-Pace Containers Used?
Yes
[:]No
❑N/A
Containers Intact?
UYes
❑No
❑N/A
7.
Dissolved analysis: Samples Field filtered?
[]Yes.
[]No
B N/A
a.
Sample Labels Match COC?
es
❑Na
[]N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (55-6mm)?
Des
No
❑N/A
10.
Trip Blank Present?
[]Yes
j3ho
❑N/A
21.
Trip Blank Custody Seals Present?
[:]Yes
❑No
❑6/A
COMMENTS/SA 1MPLE DISCREPANCY Field Data Required? ❑Yes ❑No
I�t- rY I bV "I
I j 0UJ
Lot ID of solit containers:
CLIEN7 NOTIFICATION/RESOLUTION
c� �r YCl b tA'\ —�- s Vim-'
Person contacted: Ju- ual vw) K- c--YVt Date/Time: r:s ''� � — � q
Project Manager SCURF Review: Y-) Date: 1—I Ci
Project Manager SRF Review: f D Date: 5
Page 50 of 106

Document Name:
Document Revised: February 7, 2018
aceAnal Cc7� a
y"
Sample Condition Upon ReceiptlSCURI
Page 1 of 2
Document No.:
Issuing Authority,
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
*'"Bottom half of box is to list number of bottle
Projec WO# ; 92429865
PM: AMB Due Date: 06/04/19
r j CLIENT: 92-Municipal
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot N
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e.
out of hold, incorrect preservative, out of temp, incorrect containers.
Page 51 of 106

Document Name: Document Revised: February 7, 2018
A Sample Condition Upon Receipt(SCUR) Pagel of 2
aCeAndlyf cal Document No.: Issuing Autharity:
F-CAR-Cs-033-Rev.06 Pace Carolinas quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/80i5 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Projectit W0# ; 92429865
PM: AMB Due Dale: 06/04/19
CLIENT, 92-Municipal
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lot H
Note: Whenevefthere is a discrepancy affecting North Carolina compliance samples, a cepy of this form will ?resent to the North Carolina DEHNR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 52 of 106

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Page 53 of 106

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SAMPLE TEMP AT COLLECTION
# OF CONTAINERS
Unpreserved
H2SO4
HNO3
HCI
NaOH
Na2S203
Methanol
Other
Analyses Test
K x
VOCs-8260 App 1
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i 0
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o £ i° v
7 m' c Cu
T Da
oa 6 2 Ip
o y D
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Page 54 of 106

aceAnal ical ° A f �l A L Y T CAL REPORT
National Center for Testing & Innovation May 28, 2019
FTc
FSS
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1101589 [Cn]
Samples Received: 05/22/2019 FrProject Number: 92430082
Description: Surry Closed -Mt. Airy RC
Site: 001
GI
Report To: Angela Baioni
9800 Kincey Avenue, Suite 100 rAl
Huntersville, NC 28078
Fc
Entire Report Reviewed By: �vUnn �v, � �Lr'�
L�
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. i
41
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:28 1 of 52

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Fn
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
6
Sr: Sample Results
7
FS
MW-3R L1101589-02
7
[Cn]
MW-6 L1101589-03
9
MW-7 L1101589-04
11
FSr
MW-9 L1101589-05
13
MW-11 L1101589-06
15
RC
MW-12S L1101589-07
17
�GI
MW-13 L1101589-08
19
MW-14 L1101589-09
21
rAl
MW-15 L1101589-10
23
MW-16 L1101589-11
25
FSC
MW-17 L1101589-12
27
MW-19 L1101589-13
29
MW-20 L1101589-14
31
MW-21 L1101589-15
33
MW-22 L1101589-16
35
MW-23 L1101589-17
37
SCALEHOUSE L1101589-18
39
Qc: Quality Control Summary
41
Volatile Organic Compounds (GC/MS) by Method 8260D
41
GI: Glossary of Terms
45
Al: Accreditations & Locations
46
Sc: Sample Chain of Custody
47
Page 56 of 106
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589
05/28/19 16:28
2 of 52

SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
Collected by
Collected date/time
Received date/time
MW-3R L1101589-02 GW
05/17/1909:20
05/22/1908:45
FP1
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
FTC
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 05:30
05/28/19 05:30
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
M
MW-6 L1101589-03 GW
05/17/1916:31
05/22/1908:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
[Cn]
date/time
date/time
Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 05:50
05/28/19 05:50
BMB Mt. Juliet, TN
FSrVolatile
Collected by
Collected date/time
Received date/time
sQC
MW-7 L1101589-04 GW
05/17/1916:35
05/22/1908:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
GI
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 06:10
05/28/19 06:10
BMB Mt. Juliet, TN
FAI
Collected by
Collected date/time
Received date/time
MW-9 L1101589-05 GW
05/17/1917:05
05/22/1908:45
FSC
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 06:30
05/28/19 06:30
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-11 L1101589-06 GW
05/17/1917:11
05/22/1908:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 06:50
05/28/19 06:50
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-12S L1101589-07 GW
05/17/1916:28
05/22/1908:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 07:10
05/28/19 07:10
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-13 L1101589-08 GW
05/17/1915:20
05/22/1908:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 07:30
05/28/19 07:30
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-14 L1101589-09 GW
05/17/1915:25
05/22/1908:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 07:50
05/28/19 07:50
BMB Mt. Juliet, TN
Page 57 of 106
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC
92430082
L1101589
05/28/19 16:28 3 of 52

SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
Collected by
Collected date/time
Received date/time
MW-15 L1101589-10 GW
05/17/19 09:25
05/22/19 08:45
FP1
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
FTC
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 08:10
05/28/19 08:10
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
M
MW-16 L1101589-11 GW
05/17/19 09:15
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
[Cn]
date/time
date/time
Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 08:30
05/28/19 08:30
BMB Mt. Juliet, TN
FSrVolatile
Collected by
Collected date/time
Received date/time
sQC
MW-17 L1101589-12 GW
05/17/1914:20
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
GI
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 08:50
05/28/19 08:50
BMB Mt. Juliet, TN
FAI
Collected by
Collected date/time
Received date/time
MW-19 L1101589-13 GW
05/17/1914:35
05/22/1908:45
FSC
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 09:10
05/28/19 09:10
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-20 L1101589-14 GW
05/17/1917:15
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 09:30
05/28/19 09:30
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-21 L1101589-15 GW
05/17/1914:47
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/19 09:50
05/28/19 09:50
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-22 L1101589-16 GW
05/17/1914:18
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/1910:10
05/28/1910:10
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
MW-23 L1101589-17 GW
05/17/1916:16
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/1910:30
05/28/1910:30
BMB Mt. Juliet, TN
Page 58 of 106
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC
92430082
L1101589
05/28/19 16:28 4 of 52

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
SCALEHOUSE L1101589-18 GW 05/17/1915:03 05/22/1908:45 C
P
Method
Volatile Organic Compounds (GC/MS) by Method 8260D
Batch Dilution Preparation Analysis Analyst Location I—J
date/time date/time FT,]
WG1287157 1 05/28/1910:50 05/28/1910:50 BMB Mt. Juliet, TN
[Cn]
FSr
RC
F,
FAI
FSC
Page 59 of 106
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589 05/28/19 16:28 5 of 52

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
VV VV� � �t La�'_
Nancy McLain
Project Manager
FP1
FTC
FSS
FSr
FC-1
F,
FAI
FSC
Page 60 of 106
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589 05/28/19 16:28 6 of 52

MW-3R SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 09:20 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 05:30
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 05:30
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 05:30
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 05:30
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 05:30
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 05:30
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 05:30
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 05:30
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 05:30
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 05:30
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 05:30
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 05:30
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 05:30
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 05:30
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 05:30
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 05:30
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 05:30
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 05:30
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 05:30
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 05:30
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 05:30
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 05:30
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 05:30
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 05:30
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 05:30
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 05:30
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 05:30
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 05:30
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 05:30
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 05:30
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 05:30
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 05:30
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 05:30
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 05:30
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 05:30
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 05:30
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 05:30
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 05:30
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 05:30
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 05:30
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 05:30
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 05:30
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 05:30
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 05:30
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 05:30
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 05:30
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 05:30
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 05:30
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 05:30
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 05:30
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 05:30
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 05:30
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 05:30
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 05:30
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 05:30
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 05:30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 61 of 106
PAGE:
7 of 52

ONE LAB. NATIONWIDE.
MW-3R SAMPLE RESULTS - 02
Collected date/time: 05/17/19 09:20 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 05:30
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 05:30
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 05:30
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 05:30
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 05:30
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 05:30
WG1287157
(S) Toluene-d8
93.2
80.0-120
0512812019 0530
WG1287157
(S) 4-Bromof/uorobenzene
101
77.0-126
0512812019 05:30
WG1287157
(S 1,2-Dich/oroethane-d4
87.1
70.0-130
0512812019 0530
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
FP
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 62 of 106
PAGE:
8 of 52

MW-6 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 16:31 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 05:50
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 05:50
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 05:50
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 05:50
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 05:50
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 05:50
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 05:50
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 05:50
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 05:50
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 05:50
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 05:50
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 05:50
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 05:50
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 05:50
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 05:50
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 05:50
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 05:50
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 05:50
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 05:50
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 05:50
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 05:50
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 05:50
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 05:50
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 05:50
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 05:50
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 05:50
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 05:50
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 05:50
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 05:50
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 05:50
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 05:50
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 05:50
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 05:50
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 05:50
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 05:50
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 05:50
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 05:50
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 05:50
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 05:50
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 05:50
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 05:50
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 05:50
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 05:50
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 05:50
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 05:50
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 05:50
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 05:50
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 05:50
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 05:50
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 05:50
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 05:50
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 05:50
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 05:50
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 05:50
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 05:50
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 05:50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 63 of 106
PAGE:
9 of 52

ONE LAB. NATIONWIDE.
MW-6 SAMPLE RESULTS - 03
Collected date/time: 05/17/19 16:31 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 05:50
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 05:50
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 05:50
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 05:50
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 05:50
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 05:50
WG1287157
(S) Toluene-d8
90.6
80.0-120
0512812019 05.50
WG1287157
(S) 4-Bromof/uorobenzene
98.7
77.0-126
0512812019 05.50
WG1287157
(S) 1,2-Dich/oroethane-d4
93.2
70.0-130
0512812019 05.50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 64 of 106
PAGE:
10 of 52

MW-7 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 16:35 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 06:10
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 06:10
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 06:10
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 06:10
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 06:10
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 06:10
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 06:10
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 06:10
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 06:10
WG1287157
Chlorobenzene
1.92
0.348
1.00
1 05/28/2019 06:10
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 06:10
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 06:10
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 06:10
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 06:10
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 06:10
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 06:10
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 06:10
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 06:10
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 06:10
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 06:10
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 06:10
WG1287157
1,4-Dichlorobenzene
0.786
J
0.274
1.00
1 05/28/2019 06:10
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 06:10
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 06:10
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 06:10
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 06:10
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 06:10
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 06:10
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 06:10
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 06:10
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 06:10
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 06:10
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 06:10
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 06:10
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 06:10
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 06:10
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 06:10
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 06:10
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 06:10
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 06:10
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 06:10
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 06:10
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 06:10
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 06:10
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 06:10
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 06:10
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 06:10
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 06:10
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 06:10
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 06:10
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 06:10
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 06:10
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 06:10
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 06:10
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 06:10
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 06:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 65 of 106
PAGE:
11 of 52

ONE LAB. NATIONWIDE.
MW-7 SAMPLE RESULTS - 04
Collected date/time: 05/17/19 16:35 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 06:10
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 06:10
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 06:10
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 06:10
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 06:10
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 06:10
WG1287157
(S) Toluene-d8
91.0
80.0-120
0512812019 06:10
WG1287157
(S) 4-Bromof/uorobenzene
103
77.0-126
0512812019 06:10
WG1287157
(S)1,2-Dich/oroethane-d4
92.6
70.0-130
0512812019 06:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 66 of 106
PAGE:
12 of 52

MW-9 SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 17:05 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 06:30
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 06:30
WG1287157
Benzene
1.32
0.331
1.00
1 05/28/2019 06:30
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 06:30
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 06:30
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 06:30
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 06:30
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 06:30
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 06:30
WG1287157
Chlorobenzene
1.12
0.348
1.00
1 05/28/2019 06:30
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 06:30
WG1287157
Chloroethane
1.30
J
0.453
5.00
1 05/28/2019 06:30
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 06:30
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 06:30
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 06:30
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 06:30
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 06:30
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 06:30
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 06:30
WG1287157
1,2-Dichlorobenzene
0.769
J
0.349
1.00
1 05/28/2019 06:30
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 06:30
WG1287157
1,4-Dichlorobenzene
3.48
0.274
1.00
1 05/28/2019 06:30
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 06:30
WG1287157
1,1-Dichloroethane
1.24
0.259
1.00
1 05/28/2019 06:30
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 06:30
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 06:30
WG1287157
cis-1,2-Dichloroethene
35.3
0.260
1.00
1 05/28/2019 06:30
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 06:30
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 06:30
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 06:30
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 06:30
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 06:30
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 06:30
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 06:30
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 06:30
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 06:30
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 06:30
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 06:30
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 06:30
WG1287157
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 06:30
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 06:30
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 06:30
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 06:30
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 06:30
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 06:30
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 06:30
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 06:30
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 06:30
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 06:30
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 06:30
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 06:30
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 06:30
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 06:30
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 06:30
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 06:30
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 06:30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 67 of 106
PAGE:
13 of 52

ONE LAB. NATIONWIDE.
MW-9 SAMPLE RESULTS - 05
Collected date/time: 05/17/19 17:05 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 06:30
WG1287157
Vinyl chloride
12.4
0.259
1.00
1 05/28/2019 06:30
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 06:30
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 06:30
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 06:30
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 06:30
WG1287157
(S) Toluene-d8
91.1
80.0-120
0512812019 0630
WG1287157
(S) 4-Bromof/uorobenzene
101
77.0-126
0512812019 06:30
WG1287157
(S) 1,2-Dich/oroethane-d4
93.4
70.0-130
0512812019 0630
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 68 of 106
PAGE:
14 of 52

MW-11 SAMPLE RESULTS - 06 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 17:11 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 06:50
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 06:50
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 06:50
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 06:50
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 06:50
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 06:50
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 06:50
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 06:50
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 06:50
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 06:50
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 06:50
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 06:50
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 06:50
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 06:50
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 06:50
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 06:50
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 06:50
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 06:50
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 06:50
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 06:50
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 06:50
WG1287157
1,4-Dichlorobenzene
0.501
J
0.274
1.00
1 05/28/2019 06:50
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 06:50
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 06:50
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 06:50
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 06:50
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 06:50
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 06:50
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 06:50
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 06:50
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 06:50
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 06:50
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 06:50
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 06:50
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 06:50
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 06:50
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 06:50
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 06:50
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 06:50
WG1287157
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 06:50
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 06:50
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 06:50
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 06:50
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 06:50
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 06:50
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 06:50
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 06:50
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 06:50
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 06:50
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 06:50
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 06:50
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 06:50
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 06:50
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 06:50
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 06:50
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 06:50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 69 of 106
PAGE:
15 of 52

ONE LAB. NATIONWIDE.
MW-11 SAMPLE RESULTS - 06
Collected date/time: 05/17/19 17:11 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 06:50
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 06:50
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 06:50
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 06:50
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 06:50
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 06:50
WG1287157
(S) Toluene-d8
92.8
80.0-120
0512812019 06.50
WG1287157
(S) 4-Bromof/uorobenzene
99.6
77.0-126
0512812019 06.50
WG1287157
(S)1,2-Dich/oroethane-d4
90.6
70.0-130
0512812019 06.50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 70 of 106
PAGE:
16 of 52

M W-12 S SAMPLE RESULTS - 07 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 16:28 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 07:10
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 07:10
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 07:10
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 07:10
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 07:10
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 07:10
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 07:10
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 07:10
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 07:10
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 07:10
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 07:10
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 07:10
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 07:10
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 07:10
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 07:10
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 07:10
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 07:10
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 07:10
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 07:10
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 07:10
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 07:10
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 07:10
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 07:10
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 07:10
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 07:10
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 07:10
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 07:10
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 07:10
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 07:10
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 07:10
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 07:10
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 07:10
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 07:10
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 07:10
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 07:10
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 07:10
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 07:10
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 07:10
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 07:10
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 07:10
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 07:10
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 07:10
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 07:10
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 07:10
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 07:10
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 07:10
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 07:10
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 07:10
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 07:10
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 07:10
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 07:10
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 07:10
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 07:10
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 07:10
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 07:10
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 07:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 71 of 106
PAGE:
17 of 52

ONE LAB. NATIONWIDE.
MW-12S SAMPLE RESULTS - 07
Collected date/time: 05/17/19 16:28 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 07:10
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 07:10
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 07:10
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 07:10
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 07:10
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 07:10
WG1287157
(S) Toluene-d8
91.4
80.0-120
0512812019 07.10
WG1287157
(S) 4-Bromof/uorobenzene
100
77.0-126
0512812019 07:10
WG1287157
(S 1,2-Dich/oroethane-d4
89.6
70.0-130
0512812019 07.10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 72 of 106
PAGE:
18 of 52

M W-13 SAMPLE RESULTS - 08 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 15:20 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 07:30
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 07:30
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 07:30
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 07:30
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 07:30
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 07:30
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 07:30
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 07:30
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 07:30
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 07:30
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 07:30
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 07:30
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 07:30
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 07:30
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 07:30
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 07:30
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 07:30
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 07:30
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 07:30
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 07:30
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 07:30
WG1287157
1,4-Dichlorobenzene
0.957
J
0.274
1.00
1 05/28/2019 07:30
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 07:30
WG1287157
1,1-Dichloroethane
1.64
0.259
1.00
1 05/28/2019 07:30
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 07:30
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 07:30
WG1287157
cis-1,2-Dichloroethene
14.6
0.260
1.00
1 05/28/2019 07:30
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 07:30
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 07:30
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 07:30
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 07:30
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 07:30
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 07:30
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 07:30
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 07:30
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 07:30
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 07:30
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 07:30
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 07:30
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 07:30
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 07:30
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 07:30
WG1287157
Methyl tert-butyl ether
0.626
J
0.367
1.00
1 05/28/2019 07:30
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 07:30
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 07:30
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 07:30
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 07:30
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 07:30
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 07:30
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 07:30
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 07:30
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 07:30
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 07:30
WG1287157
Trichloroethene
0.841
J
0.398
1.00
1 05/28/2019 07:30
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 07:30
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 07:30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 73 of 106
PAGE:
19 of 52

ONE LAB. NATIONWIDE.
MW-13 SAMPLE RESULTS - 08
Collected date/time: 05/17/19 15:20 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 07:30
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 07:30
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 07:30
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 07:30
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 07:30
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 07:30
WG1287157
(S) Toluene-d8
89.7
80.0-120
0512812019 07.30
WG1287157
(S) 4-Bromof/uorobenzene
99.8
77.0-126
0512812019 07.30
WG1287157
(S 1,2-Dich/oroethane-d4
91.8
70.0-130
0512812019 07.30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 74 of 106
PAGE:
20 of 52

MW-14 SAMPLE RESULTS - 09 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 15:25 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 07:50
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 07:50
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 07:50
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 07:50
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 07:50
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 07:50
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 07:50
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 07:50
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 07:50
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 07:50
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 07:50
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 07:50
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 07:50
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 07:50
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 07:50
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 07:50
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 07:50
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 07:50
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 07:50
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 07:50
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 07:50
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 07:50
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 07:50
WG1287157
1,1-Dichloroethane
1.12
0.259
1.00
1 05/28/2019 07:50
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 07:50
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 07:50
WG1287157
cis-1,2-Dichloroethene
1.35
0.260
1.00
1 05/28/2019 07:50
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 07:50
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 07:50
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 07:50
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 07:50
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 07:50
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 07:50
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 07:50
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 07:50
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 07:50
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 07:50
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 07:50
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 07:50
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 07:50
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 07:50
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 07:50
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 07:50
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 07:50
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 07:50
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 07:50
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 07:50
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 07:50
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 07:50
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 07:50
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 07:50
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 07:50
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 07:50
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 07:50
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 07:50
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 07:50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 75 of 106
PAGE:
21 of 52

ONE LAB. NATIONWIDE.
MW-14 SAMPLE RESULTS - 09
Collected date/time: 05/17/19 15:25 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 07:50
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 07:50
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 07:50
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 07:50
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 07:50
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 07:50
WG1287157
(S) Toluene-d8
89.6
80.0-120
0512812019 07.50
WG1287157
(S) 4-Bromof/uorobenzene
95.6
77.0-126
0512812019 07:50
WG1287157
(S 1,2-Dich/oroethane-d4
88.6
70.0-130
0512812019 07.50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 76 of 106
PAGE:
22 of 52

M W-15 SAMPLE RESULTS - 10 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 09:25 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 08:10
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 08:10
WG1287157
Benzene
0.459
J
0.331
1.00
1 05/28/2019 08:10
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 08:10
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 08:10
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 08:10
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 08:10
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 08:10
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 08:10
WG1287157
Chlorobenzene
2.33
0.348
1.00
1 05/28/2019 08:10
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 08:10
WG1287157
Chloroethane
0.531
J
0.453
5.00
1 05/28/2019 08:10
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 08:10
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 08:10
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 08:10
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 08:10
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 08:10
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 08:10
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 08:10
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 08:10
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 08:10
WG1287157
1,4-Dichlorobenzene
3.56
0.274
1.00
1 05/28/2019 08:10
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 08:10
WG1287157
1,1-Dichloroethane
7.14
0.259
1.00
1 05/28/2019 08:10
WG1287157
1,2-Dichloroethane
0.479
J
0.361
1.00
1 05/28/2019 08:10
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 08:10
WG1287157
cis-1,2-Dichloroethene
29.0
0.260
1.00
1 05/28/2019 08:10
WG1287157
trans-1,2-Dichloroethene
0.463
J
0.396
1.00
1 05/28/2019 08:10
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 08:10
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 08:10
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 08:10
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 08:10
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 08:10
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 08:10
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 08:10
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 08:10
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 08:10
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 08:10
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 08:10
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 08:10
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 08:10
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 08:10
WG1287157
Methyl tert-butyl ether
0.443
J
0.367
1.00
1 05/28/2019 08:10
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 08:10
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 08:10
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 08:10
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 08:10
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 08:10
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 08:10
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 08:10
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 08:10
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 08:10
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 08:10
WG1287157
Trichloroethene
2.20
0.398
1.00
1 05/28/2019 08:10
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 08:10
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 08:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 77 of 106
PAGE:
23 of 52

ONE LAB. NATIONWIDE.
MW-15 SAMPLE RESULTS - 10
Collected date/time: 05/17/19 09:25 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 08:10
WG1287157
Vinyl chloride
2.43
0.259
1.00
1 05/28/2019 08:10
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 08:10
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 08:10
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 08:10
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 08:10
WG1287157
(S) Toluene-d8
91.5
80.0-120
0512812019 08.10
WG1287157
(S) 4-Bromof/uorobenzene
103
77.0-126
0512812019 08.10
WG1287157
(S)1,2-Dich/oroethane-d4
86.1
70.0-130
0512812019 08.10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
FP
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 78 of 106
PAGE:
24 of 52

MW-16 SAMPLE RESULTS - 11 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 09:15 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 08:30
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 08:30
WG1287157
Benzene
1.28
0.331
1.00
1 05/28/2019 08:30
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 08:30
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 08:30
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 08:30
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 08:30
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 08:30
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 08:30
WG1287157
Chlorobenzene
3.07
0.348
1.00
1 05/28/2019 08:30
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 08:30
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 08:30
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 08:30
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 08:30
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 08:30
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 08:30
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 08:30
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 08:30
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 08:30
WG1287157
1,2-Dichlorobenzene
0.482
J
0.349
1.00
1 05/28/2019 08:30
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 08:30
WG1287157
1,4-Dichlorobenzene
6.20
0.274
1.00
1 05/28/2019 08:30
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 08:30
WG1287157
1,1-Dichloroethane
0.688
J
0.259
1.00
1 05/28/2019 08:30
WG1287157
1,2-Dichloroethane
1.23
0.361
1.00
1 05/28/2019 08:30
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 08:30
WG1287157
cis-1,2-Dichloroethene
16.3
0.260
1.00
1 05/28/2019 08:30
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 08:30
WG1287157
1,2-Dichloropropane
0.824
J
0.306
1.00
1 05/28/2019 08:30
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 08:30
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 08:30
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 08:30
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 08:30
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 08:30
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 08:30
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 08:30
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 08:30
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 08:30
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 08:30
WG1287157
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 08:30
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 08:30
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 08:30
WG1287157
Methyl tert-butyl ether
1.27
0.367
1.00
1 05/28/2019 08:30
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 08:30
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 08:30
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 08:30
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 08:30
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 08:30
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 08:30
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 08:30
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 08:30
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 08:30
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 08:30
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 08:30
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 08:30
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 08:30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 79 of 106
PAGE:
25 of 52

ONE LAB. NATIONWIDE.
MW-16 SAMPLE RESULTS - 11
Collected date/time: 05/17/19 09:15 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 08:30
WG1287157
Vinyl chloride
2.33
0.259
1.00
1 05/28/2019 08:30
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 08:30
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 08:30
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 08:30
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 08:30
WG1287157
(S) Toluene-d8
90.5
80.0-120
0512812019 08.30
WG1287157
(S) 4-Bromof/uorobenzene
100
77.0-126
0512812019 08:30
WG1287157
(S) 1,2-Dich/oroethane-d4
93.0
70.0-130
0512812019 0830
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
FP
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 80 of 106
PAGE:
26 of 52

MW-17 SAMPLE RESULTS - 12 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 14:20 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 08:50
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 08:50
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 08:50
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 08:50
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 08:50
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 08:50
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 08:50
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 08:50
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 08:50
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 08:50
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 08:50
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 08:50
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 08:50
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 08:50
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 08:50
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 08:50
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 08:50
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 08:50
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 08:50
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 08:50
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 08:50
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 08:50
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 08:50
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 08:50
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 08:50
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 08:50
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 08:50
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 08:50
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 08:50
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 08:50
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 08:50
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 08:50
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 08:50
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 08:50
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 08:50
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 08:50
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 08:50
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 08:50
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 08:50
WG1287157
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 08:50
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 08:50
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 08:50
WG1287157
Methyl tert-butyl ether
0.552
J
0.367
1.00
1 05/28/2019 08:50
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 08:50
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 08:50
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 08:50
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 08:50
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 08:50
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 08:50
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 08:50
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 08:50
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 08:50
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 08:50
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 08:50
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 08:50
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 08:50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 81 of 106
PAGE:
27 of 52

ONE LAB. NATIONWIDE.
MW-17 SAMPLE RESULTS - 12
Collected date/time: 05/17/19 14:20 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 08:50
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 08:50
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 08:50
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 08:50
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 08:50
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 08:50
WG1287157
(S) Toluene-d8
91.7
80.0-120
0512812019 08.50
WG1287157
(S) 4-Bromof/uorobenzene
101
77.0-126
0512812019 08.50
WG1287157
(S) 1,2-Dich/oroethane-d4
88.2
70.0-130
0512812019 08.50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 82 of 106
PAGE:
28 of 52

M W-19 SAMPLE RESULTS - 13 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 14:35 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 09:10
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 09:10
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 09:10
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 09:10
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 09:10
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 09:10
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 09:10
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 09:10
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 09:10
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 09:10
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 09:10
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 09:10
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 09:10
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 09:10
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 09:10
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 09:10
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 09:10
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 09:10
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 09:10
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 09:10
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 09:10
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 09:10
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 09:10
WG1287157
1,1-Dichloroethane
1.07
0.259
1.00
1 05/28/2019 09:10
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 09:10
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 09:10
WG1287157
cis-1,2-Dichloroethene
2.06
0.260
1.00
1 05/28/2019 09:10
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 09:10
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 09:10
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 09:10
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 09:10
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 09:10
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 09:10
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 09:10
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 09:10
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 09:10
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 09:10
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 09:10
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 09:10
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 09:10
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 09:10
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 09:10
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 09:10
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 09:10
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 09:10
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 09:10
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 09:10
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 09:10
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 09:10
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 09:10
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 09:10
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 09:10
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 09:10
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 09:10
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 09:10
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 09:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 83 of 106
PAGE:
29 of 52

ONE LAB. NATIONWIDE.
MW-19 SAMPLE RESULTS - 13
Collected date/time: 05/17/19 14:35 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 09:10
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 09:10
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 09:10
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 09:10
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 09:10
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 09:10
WG1287157
(S Toluene-d8
89.9
80.0-120
0512812019 09.10
WG1287157
(S) 4-Bromof/uorobenzene
99.4
77.0-126
0512812019 09.10
WG1287157
(S 1,2-Dich/oroethane-d4
89.3
70.0-130
0512812019 09.10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 84 of 106
PAGE:
30 of 52

MW-20 SAMPLE RESULTS - 14 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 17:15 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 09:30
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 09:30
WG1287157
Benzene
1.15
0.331
1.00
1 05/28/2019 09:30
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 09:30
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 09:30
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 09:30
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 09:30
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 09:30
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 09:30
WG1287157
Chlorobenzene
1.13
0.348
1.00
1 05/28/2019 09:30
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 09:30
WG1287157
Chloroethane
0.687
J
0.453
5.00
1 05/28/2019 09:30
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 09:30
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 09:30
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 09:30
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 09:30
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 09:30
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 09:30
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 09:30
WG1287157
1,2-Dichlorobenzene
1.04
0.349
1.00
1 05/28/2019 09:30
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 09:30
WG1287157
1,4-Dichlorobenzene
2.91
0.274
1.00
1 05/28/2019 09:30
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 09:30
WG1287157
1,1-Dichloroethane
1.04
0.259
1.00
1 05/28/2019 09:30
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 09:30
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 09:30
WG1287157
cis-1,2-Dichloroethene
6.50
0.260
1.00
1 05/28/2019 09:30
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 09:30
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 09:30
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 09:30
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 09:30
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 09:30
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 09:30
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 09:30
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 09:30
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 09:30
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 09:30
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 09:30
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 09:30
WG1287157
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 09:30
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 09:30
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 09:30
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 09:30
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 09:30
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 09:30
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 09:30
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 09:30
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 09:30
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 09:30
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 09:30
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 09:30
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 09:30
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 09:30
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 09:30
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 09:30
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 09:30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 85 of 106
PAGE:
31 of 52

ONE LAB. NATIONWIDE.
MW-20 SAMPLE RESULTS - 14
Collected date/time: 05/17/19 17:15 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 09:30
WG1287157
Vinyl chloride
3.59
0.259
1.00
1 05/28/2019 09:30
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 09:30
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 09:30
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 09:30
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 09:30
WG1287157
(S) Toluene-d8
91.9
80.0-120
0512812019 0930
WG1287157
(S) 4-Bromof/uorobenzene
101
77.0-126
0512812019 09:30
WG1287157
(S) 1,2-Dich/oroethane-d4
88.4
70.0-130
0512812019 0930
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 86 of 106
PAGE:
32 of 52

MW-21 SAMPLE RESULTS - 15 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 14:47 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 09:50
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 09:50
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 09:50
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 09:50
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 09:50
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 09:50
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 09:50
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 09:50
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 09:50
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 09:50
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 09:50
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 09:50
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 09:50
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 09:50
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 09:50
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 09:50
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 09:50
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 09:50
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 09:50
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 09:50
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 09:50
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 09:50
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 09:50
WG1287157
1,1-Dichloroethane
2.68
0.259
1.00
1 05/28/2019 09:50
WG1287157
1,2-Dichloroethane
0.400
J
0.361
1.00
1 05/28/2019 09:50
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 09:50
WG1287157
cis-1,2-Dichloroethene
14.3
0.260
1.00
1 05/28/2019 09:50
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 09:50
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 09:50
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 09:50
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 09:50
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 09:50
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 09:50
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 09:50
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 09:50
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 09:50
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 09:50
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 09:50
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 09:50
WG1287157
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 09:50
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 09:50
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 09:50
WG1287157
Methyl tert-butyl ether
0.865
J
0.367
1.00
1 05/28/2019 09:50
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 09:50
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 09:50
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 09:50
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 09:50
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 09:50
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 09:50
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 09:50
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 09:50
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 09:50
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 09:50
WG1287157
Trichloroethene
0.772
J
0.398
1.00
1 05/28/2019 09:50
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 09:50
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 09:50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 87 of 106
PAGE:
33 of 52

ONE LAB. NATIONWIDE.
MW-21 SAMPLE RESULTS - 15
Collected date/time: 05/17/19 14:47 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 09:50
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 09:50
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 09:50
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 09:50
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 09:50
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 09:50
WG1287157
(S) Toluene-d8
92.6
80.0-120
0512812019 09.50
WG1287157
(S) 4-Bromof/uorobenzene
101
77.0-126
0512812019 09.50
WG1287157
(S) 1,2-Dich/oroethane-d4
87.8
70.0-130
0512812019 09.50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 88 of 106
PAGE:
34 of 52

MW-22 SAMPLE RESULTS - 16 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 14,18 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/201910:10
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/201910:10
WG1287157
Benzene
0.332
J
0.331
1.00
1 05/28/201910:10
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/201910:10
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/201910:10
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/201910:10
WG1287157
Bromoform
U
0.469
1.00
1 05/28/201910:10
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/201910:10
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/201910:10
WG1287157
Chlorobenzene
0.958
J
0.348
1.00
1 05/28/201910:10
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/201910:10
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/201910:10
WG1287157
Chloroform
U
0.324
5.00
1 05/28/201910:10
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/201910:10
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/201910:10
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/201910:10
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/201910:10
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/201910:10
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/201910:10
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/201910:10
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/201910:10
WG1287157
1,4-Dichlorobenzene
1.83
0.274
1.00
1 05/28/2019 10:10
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/201910:10
WG1287157
1,1-Dichloroethane
0.900
J
0.259
1.00
1 05/28/201910:10
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/201910:10
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/201910:10
WG1287157
cis-1,2-Dichloroethene
1.94
0.260
1.00
1 05/28/201910:10
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/201910:10
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/201910:10
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/201910:10
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/201910:10
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/201910:10
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/201910:10
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/201910:10
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/201910:10
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/201910:10
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/201910:10
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/201910:10
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/201910:10
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/201910:10
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/201910:10
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/201910:10
WG1287157
Methyl tert-butyl ether
0.768
J
0.367
1.00
1 05/28/201910:10
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/201910:10
WG1287157
Styrene
U
0.307
1.00
1 05/28/201910:10
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/201910:10
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/201910:10
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/201910:10
WG1287157
Toluene
U
0.412
1.00
1 05/28/201910:10
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/201910:10
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/201910:10
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/201910:10
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/201910:10
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/201910:10
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/201910:10
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/201910:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 89 of 106
PAGE:
35 of 52

ONE LAB. NATIONWIDE.
MW-22 SAMPLE RESULTS - 16
Collected date/time: 05/17/19 14:18 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201910:10
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/201910:10
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/201910:10
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/201910:10
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/201910:10
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/201910:10
WG1287157
(S) Toluene-d8
88.9
80.0-120
051281201910:10
WG1287157
(S 4-Bromof/uorobenzene
101
77.0-126
051281201910.10
WG1287157
(S 1,2-Dich/oroethane-d4
92.7
70.0-130
051281201910:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 90 of 106
PAGE:
36 of 52

MW-23 SAMPLE RESULTS - 17 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 16:16 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/201910:30
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/201910:30
WG1287157
Benzene
U
0.331
1.00
1 05/28/201910:30
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/201910:30
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/201910:30
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/201910:30
WG1287157
Bromoform
U
0.469
1.00
1 05/28/201910:30
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/201910:30
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/201910:30
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/201910:30
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/201910:30
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/201910:30
WG1287157
Chloroform
U
0.324
5.00
1 05/28/201910:30
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/201910:30
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/201910:30
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/201910:30
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/201910:30
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/201910:30
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/201910:30
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/201910:30
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/201910:30
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 10:30
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/201910:30
WG1287157
1,1-Dichloroethane
0.561
J
0.259
1.00
1 05/28/201910:30
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/201910:30
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/201910:30
WG1287157
cis-1,2-Dichloroethene
0.896
J
0.260
1.00
1 05/28/201910:30
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/201910:30
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/201910:30
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/201910:30
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/201910:30
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/201910:30
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/201910:30
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/201910:30
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/201910:30
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/201910:30
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/201910:30
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/201910:30
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/201910:30
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/201910:30
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/201910:30
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/201910:30
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/201910:30
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/201910:30
WG1287157
Styrene
U
0.307
1.00
1 05/28/201910:30
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/201910:30
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/201910:30
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/201910:30
WG1287157
Toluene
U
0.412
1.00
1 05/28/201910:30
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/201910:30
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/201910:30
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/201910:30
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/201910:30
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/201910:30
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/201910:30
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/201910:30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 91 of 106
PAGE:
37 of 52

ONE LAB. NATIONWIDE.
MW-23 SAMPLE RESULTS - 17
Collected date/time: 05/17/19 16:16 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201910:30
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/201910:30
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/201910:30
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/201910:30
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/201910:30
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/201910:30
WG1287157
(S) Toluene-d8
90.4
80.0-120
051281201910:30
WG1287157
(S) 4-Bromof/uorobenzene
100
77.0-126
051281201910.30
WG1287157
(S)1,2-Dich/oroethane-d4
92.0
70.0-130
051281201910.30
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 92 of 106
PAGE:
38 of 52

SCALEHOUSE SAMPLE RESULTS - 18 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 15:03 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/201910:50
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/201910:50
WG1287157
Benzene
U
0.331
1.00
1 05/28/201910:50
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/201910:50
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/201910:50
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/201910:50
WG1287157
Bromoform
U
0.469
1.00
1 05/28/201910:50
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/201910:50
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/201910:50
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/201910:50
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/201910:50
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/201910:50
WG1287157
Chloroform
U
0.324
5.00
1 05/28/201910:50
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/201910:50
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/201910:50
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/201910:50
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/201910:50
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/201910:50
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/201910:50
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/201910:50
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/201910:50
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 10:50
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/201910:50
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/201910:50
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/201910:50
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/201910:50
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/201910:50
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/201910:50
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/201910:50
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/201910:50
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/201910:50
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/201910:50
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/201910:50
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/201910:50
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/201910:50
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/201910:50
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/201910:50
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/201910:50
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/201910:50
WG1287157
2-Butanone(MEK)
U
3.93
10.0
1 05/28/201910:50
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/201910:50
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/201910:50
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/201910:50
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/201910:50
WG1287157
Styrene
U
0.307
1.00
1 05/28/201910:50
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/201910:50
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/201910:50
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/201910:50
WG1287157
Toluene
U
0.412
1.00
1 05/28/201910:50
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/201910:50
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/201910:50
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/201910:50
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/201910:50
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/201910:50
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/201910:50
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/201910:50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:28
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 93 of 106
PAGE:
39 of 52

ONE LAB. NATIONWIDE.
SCALEHOUSE SAMPLE RESULTS - 18
Collected date/time: 05/17/19 15:03 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201910:50
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/201910:50
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/201910:50
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/201910:50
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/201910:50
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/201910:50
WG1287157
(S) Toluene-d8
92.0
80.0-120
051281201910:50
WG1287157
(S) 4-Bromof/uorobenzene
99.9
77.0-126
051281201910.50
WG1287157
(S 1,2-Dich/oroethane-d4
89.8
70.0-130
0512812019 10:50
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:28
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 94 of 106
PAGE:
40 of 52

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101589-02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R3415400-3 05/28/19 04:50
MB Result
Analyte
ug/I
Acetone
U
Acrylonitrile
U
Benzene
U
Bromobenzene
U
Bromodichloromethane
U
Bromochloromethane
U
Bromoform
U
Bromomethane
U
Carbon tetrachloride
U
Chlorobenzene
U
Chlorodibromomethane
U
Chloroethane
U
Chloroform
U
Chloromethane
U
2-Chlorotoluene
U
4-Chlorotoluene
U
1,2-Dibromo-3-Chloropropane
U
1,2-Dibromoethane
U
Dibromomethane
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
Dichlorodifluoromethane
U
1,1-Dichloroethane
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
cis-1,2-Dichloroethene
U
trans-1,2-Dichloroethene
U
1,2-Dichloropropane
U
1,1-Dichloropropene
U
1,3-Dichloropropane
U
cis-1,3-Dichloropropene
U
trans-1,3-Dichloropropene
U
2,2-Dichloropropane
U
Di -isopropyl ether
U
Ethylbenzene
U
Hexachloro-1,3-butadiene
U
2-Hexanone
U
p-Isopropyltoluene
U
2-Butanone (MEK)
U
MB Qualifier MB MDL
MB RDL
ug/I
ug/I
10.0
50.0
1.87
10.0
0.331
1.00
0.352
1.00
0.380
1.00
0.520
5.00
0.469
1.00
0.866
5.00
0.379
1.00
0.348
1.00
0.327
1.00
0.453
5.00
0.324
5.00
0.276
2.50
0.375
1.00
0.351
1.00
1.33
5.00
0.381
1.00
0.346
1.00
0.349
1.00
0.220
1.00
0.274
1.00
0.551
5.00
0.259
1.00
0.361
1.00
0.398
1.00
0.260
1.00
0.396
1.00
0.306
1.00
0.352
1.00
0.366
1.00
0.418
1.00
0.419
1.00
0.321
1.00
0.320
1.00
0.384
1.00
0.256
1.00
3.82
10.0
0.350
1.00
3.93
10.0
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
Page 95 of 106
PAGE:
41 of 52
ACCOUNT:
Pace Analytical - Huntersville, NC
PROJECT: SDG: DATE/TIME:
92430082 L1101589 05/28/19 16:28

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101589-02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Method Blank (MB)
(MB) R3415400-3 05/28/19 04:50
MB Result
Analyte
ug/I
Methylene Chloride
U
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
Styrene
U
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
Vinyl acetate
U
Vinyl chloride
U
Xylenes, Total
U
o-Xylene
U
m&p-Xylenes
U
1,4-Dioxane
U
(S) Toluene-d8
93.0
(S) 4-Bromof/uorobenzene
98.8
(S) 1,2-Dich/oroethone-d4
89.8
MB Qualifier MB MDL
ug/I
Laboratory Control Sample (LCS)
1.00
2.14
0.367
1.00
0.307
0.385
0.130
0.372
0.412
0.230
0.355
0.319
0.383
0.398
1.20
0.807
1.63
0.259
1.06
0.341
0.719
36.0
MB RDL
ug/I
5.00
10.0
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
5.00
2.50
10.0
1.00
3.00
1.00
2.00
100
80.0-120
77.0-126
70.0-130
FP1
FTC]
IS-S]
[Cn]
rs-r
�GI
rAl
FSC
(LCS) R3415400-1 05/28/19 03:30
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte ug/I
ug/I
%
%
Acetone 125
134
107
19.0-160
Acrylonitrile 125
148
118
55.0-149
Benzene 25.0
28.2
113
70.0-123
Bromobenzene 25.0
22.2
89.0
73.0-121
Bromodichloromethane 25.0
28.6
115
75.0-120
Bromochloromethane 25.0
24.7
98.7
76.0-122
Bromoform 25.0
25.1
100
68.0-132
Bromomethane 25.0
14.5
58.1
10.0-160
Page 96 of 106
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville,
NC
92430082 L1101589 05/28/19 16:28 42 of 52

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101589-02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Laboratory Control Sample (LCS)
(LCS) R3415400-1 05/28/19 03:30
Spike Amount LCS Result
Analyte ug/I ug/I
Carbon tetrachloride
25.0
29.3
Chlorobenzene
25.0
26.3
Chlorodibromomethane
25.0
25.7
Chloroethane
25.0
26.2
Chloroform
25.0
28.1
Chloromethane
25.0
12.7
2-Chlorotoluene
25.0
22.2
4-Chlorotoluene
25.0
23.3
1,2-Dibromo-3-Chloropropane
25.0
21.8
1,2-Dibromoethane
25.0
27.1
Dibromomethane
25.0
27.4
1,2-Dichlorobenzene
25.0
24.6
1,3-Dichlorobenzene
25.0
23.5
1,4-Dichlorobenzene
25.0
22.9
Dichlorodifluoromethane
25.0
12.4
1,1-Dichloroethane
25.0
28.3
1,2-Dichloroethane
25.0
25.9
1,1-Dichloroethene
25.0
30.5
cis-1,2-Dichloroethene
25.0
28.0
trans-1,2-Dichloroethene
25.0
30.0
1,2-Dichloropropane
25.0
27.8
1,1-Dichloropropene
25.0
29.9
1,3-Dichloropropane
25.0
27.1
cis-1,3-Dichloropropene
25.0
29.1
trans-1,3-Dichloropropene
25.0
25.8
2,2-Dichloropropane
25.0
25.9
Di -isopropyl ether
25.0
27.5
Ethylbenzene
25.0
27.0
Hexachloro-1,3-butadiene
25.0
20.9
2-Hexanone
125
136
p-Isopropyltoluene
25.0
22.3
2-Butanone (MEK)
125
130
Methylene Chloride
25.0
27.3
4-Methyl-2-pentanone (MIBK)
125
127
Methyl tert-butyl ether
25.0
28.8
Naphthalene
25.0
22.2
Styrene
25.0
28.0
1,1,1,2-Tetrachloroethane
25.0
26.1
1,1,2,2-Tetrachloroethane
25.0
23.1
Tetrachloroethene
25.0
28.4
LCS Rec
117
105
103
105
112
50.9
88.8
93.3
87.4
109
110
98.5
94.0
91.5
49.5
113
104
122
112
120
119
108
116
103
104
110
108
83.5
109
89.0
104
109
102
115
88.8
112
104
92.4
114
Rec. Limits LCS Qualifier
68.0-126
80.0-121
77.0-125
47.0-150
73.0-120
41.0-142
76.0-123
75.0-122
58.0-134
80.0-122
80.0-120
79.0-121
79.0-120
79.0-120
51.0-149
70.0-126
70.0-128
71.0-124
73.0-120
73.0-120
77.0-125
74.0-126
80.0-120
80.0-123
78.0-124
58.0-130
58.0-138
79.0-123
54.0-138
67.0-149
76.0-125
44.0-160
67.0-120
68.0-142
68.0-125
54.0-135
73.0-130
75.0-125
65.0-130
72.0-132
J4
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
Page 97 of 106
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:28 43 of 52

WG1287157
Volatile Organic Compounds (GC/MS) by Method 8260D
Laboratory Control Sample (LCS)
(LCS) R3415400-1 05/28/19 03:30
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Toluene
25.0
25.4
1,2,3-Trichlorobenzene
25.0
22.3
1,2,4-Trichlorobenzene
25.0
23.0
1,1,1-Trichloroethane
25.0
29.8
1,1,2-Trichloroethane
25.0
25.8
Trichloroethene
25.0
30.5
Trichlorofluoromethane
25.0
32.7
1,2,3-Trichloropropane
25.0
23.9
Vinyl acetate
125
113
Vinyl chloride
25.0
31.6
Xylenes, Total
75.0
77.1
o-Xylene
25.0
26.0
m&p-Xylenes
50.0
51.1
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethane-d4
Laboratory Control Sample (LCS)
LCS Rec.
102
89.1
91.8
119
103
122
131
95.7
90.7
126
103
104
102
92.2
104
86.0
QUALITY CONTROL SUMMARY
L1101589-02,03,04,05,06,07,08,09,10,11,12,13,14,15,16,17,18
Rec. Limits LCS Qualifier
79.0-120
50.0-138
57.0-137
73.0-124
80.0-120
78.0-124
59.0-147
73.0-130
11.0-160
67.0-131
79.0-123
80.0-122
80.0-122
80.0-120
77.0-126
70.0-130
ONE LAB. NATIONWIDE.
FP1
FTC]
IS-S]
[Cn]
rs-r
�GI
rAl
FSC
(LCS) R3415400-2 05/28/19 04:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
1,4-Dioxane 1000 988 98.8 13.0-160
(S) Toluene-d8 92.0 80.0-120
(S)4-Bromofluorobenzene 100 77.0-126
(S)1,2-Dich/oroethane-d4 91.5 70.0-130
Page 98 of 106
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:28 44 of 52

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
CP
IP
FTC
MDL
Method Detection Limit.
RDL
Reported Detection Limit.
FSS
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
[Cn]
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
FSr
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
Fc
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
FAI
duplicated within these ranges.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
FSC
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
JO JO: The identification of the analyte is acceptable, but the reported concentration is an estimate. The calibration met
method criteria.
J4 The associated batch QC was outside the established quality control range for accuracy.
Page 99 of 106
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589 05/28/19 16:28 45 of 52

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT NO
OR MN
T ID T WI NY
SD
WY MI
NV
T NE IA OH T PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
W 11110
� NM O� AR N Sc
T MS A`7L GA
T TX * LA
T
AK T T
q FL
wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:28
ME
Page 100 of 106
PAGE:
46 of 52

1164
Chain of Custody
❑ Samples were sent directly to the Subcontracting Laboratory. State Of Origin: NC
Cert. Needed: ❑ Yes ❑ No
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Workorder: 92429865 Workorder Name: SUKKY CLOSED -MT. . AIRY Owner Received Date: er/_uizV 19 Ke5urts r11equeareu oy, uj-rre-u is
lie :T "¢l'-- Requested Analysis==r
Angela Baioni
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100 Pace National zV
Huntersville, NC 28078 12065 Lebanon Rd
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Phone [phone]
Mt Juliet, TN 37122 e
615-758-5858
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Containers
Sample Collect g_
Item sample II] Type Date1T-ime _ Lab 0.. Matrix z LAB USE ONLY
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1 PS 51171201916:05 92429865001 Water X L 1 14 _el
2 MW-3R PS 511712019 09:20 92429865002 Water X '06
3 VW-6 PS 5/171201916:31 92429865003 Water X U
4 MW-7 PS 5/17/201916:35 924298656D4 Water X b
5 MW-9 PS 5117/201917:D5 92429865005 Water X 41
6 Mw-11 PS 51171201917:11 92429865006 Water X
17 MW-12S PS 5/17/201916:28 92429865007 Water X 0-7
8 MW-13 PS 5/171201915:20 92429865008 Water X to
9 MW-14 PS 5/17/201915:25 92429865009 Water X Oq
10 MW-15 PS 5117/2019 09:25 92429865010 Water X i
11 MW-16 PS 5/17/2019 09 15 92429865011 Water X 1 {
12 MW-17 PS 511712019 14,20 92429865012 Water X I rl
13 MW-19 PS 51171201914:35 92429865013 Water X
14 Mw-20 PS 5/17/201917:15 92429865014 Water X 1
15 MW-21 PS 5/171201914:47 92429865015 Water X
16 Mw-22 PS 5117/201914:18 92429865016 Water X �p
17 Mw-23 PS 5/171201916:16 92429865017 Water X t
18 SCALEHOUSE PS 5/171201915:03 92429865018 Water X 1
114,w 5'0> 7MM M
Tuesday, May 21, 2019 1:55:39 PM FMT-ALL-C-002rev.00 24March2009 Page 1N dlbt 2
114,w 5'0> 7MM M
Tuesday, May 21, 2019 1:55:39 PM FMT-ALL-C-002rev.00 24March2009 Page 1N dlbt 2

Transfers Released By DatefTime Received By DaterTime
2
3
Cooler Tem erature on Receipt - °C Custody Seal Y or N Received on Ice � or N Samples Intac Y or N
***In order to maintain client confidentiality, location/name of the sampling sit ampler's name and signature may not be provided on this COC document.
This chain of custody is considered complete as is since this information is available in the owner laboratory.
-1 a i Pp
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ZO SCREEN: <0.5 MR/hf
Tuesday, May 21, 2019 1:55:41 PM FMT-ALL-C-002rev.00 24March2009 Par 2 of 2
Page 10of 106

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ac6Analytical�
www.pecefabs.wM
Ship To:
INTER —LABORATORY WORK ORDER # 92430082
(To be completed by sending lab)
Sending Project No
92430082
Receiving Project No
Check Box for Consolidated Invoice
',�:
Date Prepared
05l28/19
REQUESTED COMPLETION DATE
6/4/2019
Sending Region
1R92-Charlotte
Sending Project Mgr.
Angela Baioni
Receiving-Regi
IR850-Pace-Natk=1
-Ext r—i I -Client
Municipa Engineering Services
State of Sample Origin
NC
QC Deliverable
STD REPORT
Ali questions snouia De aaaressed to sending project manager.
Requested Reportable Units Report Wet or Dry Weight? Dry Weight
Cert. Needed
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Chain of Custody Included: EYes ENo Return Samples to Sending Region: Dyes �o
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Tuesday, May 28, 2019 4:24:42 PM FMT-ALL-C-001 rev.00 24March2009 POW 1MID61106

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Pace Analytical Nationalfor • & Innovation
CoolerReceipt i
Client: SDG#: I f o l
Cooler Received/Opened On: 5/1,L-/19 Temperature:
Received By: Jordan Harris
Signature:
Receipt Check List NP
Yes
No
COC Seal Present / Intact? i
COC Signed / Accurate?
/
Bottles arrive intact?
-i
Correct bottles used?
Sufficient volume sent?
If Applicable
VOA Zero headspace?
Preservation Correct / Checked?
Page 106 of 106

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 10, 2019
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry Closed MW1
Pace Project No.: 92430082
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory between May 20, 2019
and May 22, 2019. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
A revised report is being submitted on 6/10/19 because the metals did not initially report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
owa-
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Maddie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
r
e
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without the written consent of Pace Analytical Services, LLC.
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aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Project: Surry Closed MW1
Pace Project No.: 92430082
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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SAMPLE SUMMARY
Project: Surry Closed MW1
Pace Project No.: 92430082
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92430082001
92429865001
1
MW-1
Water
Water
05/20/19 09:58
05/17/1916:05
05/22/19 09:57
05/20/1911:26
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Surry Closed MW1
Pace Project No.: 92430082
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92429865001 MW-1 EPA 601OD SH1 14 PASI-A
EPA 6020E JOR 1 PASI-A
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project:
Surry Closed MW1
Pace Project No.:
92430082
Sample: MW-1
Lab ID:
92429865001
Collected:
05/17/19 16:05
Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 6010D
Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
06/03/19 12:21
06/03/19 23:33
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:33
7440-38-2
Barium
47.0
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:33
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
06/03/19 12:21
06/03/19 23:33
7440-41-7
Cadmium
0.911
ug/L
1.0
0.40
1
06/03/19 12:21
06/03/19 23:33
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
06/03/19 12:21
06/03/19 23:33
7440-47-3
Cobalt
2.5J
ug/L
5.0
1.1
1
06/03/19 12:21
06/03/19 23:33
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
06/03/19 12:21
06/03/19 23:33
7440-50-8
Lead
1.7J
ug/L
5.0
1.6
1
06/03/19 12:21
06/03/19 23:33
7439-92-1
Nickel
1.6J
ug/L
5.0
0.90
1
06/03/19 12:21
06/03/19 23:33
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
06/03/19 12:21
06/03/19 23:33
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
06/03/19 12:21
06/03/19 23:33
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
06/03/19 12:21
06/03/19 23:33
7440-62-2
Zinc
9.3J
ug/L
10.0
3.9
1
06/03/19 12:21
06/03/19 23:33
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method:
EPA 3010A
Thallium
ND
ug/L
0.10
0.060
1
06/03/19 09:01
06/06/19 05:22
7440-28-0
REPORT OF LABORATORY ANALYSIS
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Date: 06/10/2019 02:09 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 31

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed MW1
Pace Project No.: 92430082
QC Batch: 478711 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92429865001
METHOD BLANK: 2591279
Associated Lab Samples: 92429865001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
06/03/19 23:26
Arsenic
ug/L
ND
10.0
4.7
06/03/19 23:26
Barium
ug/L
ND
5.0
1.0
06/03/19 23:26
Beryllium
ug/L
ND
1.0
0.20
06/03/19 23:26
Cadmium
ug/L
ND
1.0
0.40
06/03/19 23:26
Chromium
ug/L
ND
5.0
1.0
06/03/19 23:26
Cobalt
ug/L
ND
5.0
1.1
06/03/19 23:26
Copper
ug/L
ND
5.0
2.1
06/03/19 23:26
Lead
ug/L
ND
5.0
1.6
06/03/19 23:26
Nickel
ug/L
ND
5.0
0.90
06/03/19 23:26
Selenium
ug/L
ND
10.0
4.7
06/03/19 23:26
Silver
ug/L
ND
5.0
2.5
06/03/19 23:26
Vanadium
ug/L
ND
5.0
1.3
06/03/19 23:26
Zinc
ug/L
ND
10.0
3.9
06/03/19 23:26
LABORATORY CONTROL SAMPLE:
Parameter
2591280
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
498
100
80-120
Arsenic
ug/L
500
480
96
80-120
Barium
ug/L
500
488
98
80-120
Beryllium
ug/L
500
497
99
80-120
Cadmium
ug/L
500
492
98
80-120
Chromium
ug/L
500
498
100
80-120
Cobalt
ug/L
500
497
99
80-120
Copper
ug/L
500
503
101
80-120
Lead
ug/L
500
487
97
80-120
Nickel
ug/L
500
490
98
80-120
Selenium
ug/L
500
497
99
80-120
Silver
ug/L
250
250
100
80-120
Vanadium
ug/L
500
496
99
80-120
Zinc
ug/L
500
498
100
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2591281 2591282
MS MSD
92429865001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 470 472 94 94 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/10/2019 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 31

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry Closed MW1
92430082
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2591281
2591282
MS
MSD
92429865001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
475
475
95
95
75-125
0
20
Barium
ug/L
47.0
500
500
519
526
94
96
75-125
1
20
Beryllium
ug/L
ND
500
500
482
489
96
98
75-125
1
20
Cadmium
ug/L
0.911
500
500
489
494
98
99
75-125
1
20
Chromium
ug/L
ND
500
500
488
491
98
98
75-125
0
20
Cobalt
ug/L
2.5J
500
500
485
490
97
97
75-125
1
20
Copper
ug/L
ND
500
500
486
489
97
98
75-125
1
20
Lead
ug/L
1.7J
500
500
477
477
95
95
75-125
0
20
Nickel
ug/L
1.6J
500
500
479
483
95
96
75-125
1
20
Selenium
ug/L
ND
500
500
511
516
102
103
75-125
1
20
Silver
ug/L
ND
250
250
236
239
95
96
75-125
1
20
Vanadium
ug/L
ND
500
500
487
490
97
98
75-125
1
20
Zinc
ug/L
9.3J
500
500
509
511
100
100
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2019 02:09 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 31

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Surry Closed MW1
Pace Project No.: 92430082
QC Batch: 478573
Analysis Method:
EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description:
6020 MET
Associated Lab Samples: 92429865001
METHOD BLANK: 2590560
Matrix: Water
Associated Lab Samples: 92429865001
Blank Reporting
Parameter Units
Result Limit
MDL
Analyzed Qualifiers
Thallium ug/L
ND 0.10 0.060 06/06/19 05:08
LABORATORY CONTROL SAMPLE: 2590561
Spike LCS
LCS
% Rec
Parameter Units
Conc. Result
% Rec
Limits Qualifiers
Thallium ug/L
10 10.1
101
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2590562 2590563
MS MSD
92429865001
Spike Spike MS
MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result
% Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND
10 10 10.1
10.2
101 102 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Surry Closed MW1
Pace Project No.: 92430082
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Surry Closed MW1
Pace Project No.: 92430082
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92429865001 MW-1 EPA 3010A 478711 EPA 6010D 478791
92429865001 MW-1 EPA 3010A 478573 EPA 6020B 478747
Date: 06/10/2019 02:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 31

Document Name: Document Revised: February 7, 2018
m Sample Condition Upon Receipt(SOUR) Page 1 of 2
atl�And Gad Document No,: Issuing Authority:
F-CAR-CS•033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersviile Raleigh❑ ` MechanicsvilieF]
GfientName: WO# : 92430082
Upon Receiptf Project #:
1
Courier: Fe x UPS []LISPS []Client II I II� 4I I�l I �lI I� �II
❑ Commercial 0ace ❑other; 92430062
Custody Seal Present? ❑Yes No Seals intact? Oyes Oro (}�
Date/initials Person Examining Corttenls:�—'
Packing Material: ❑Bubble Wrap aubble Bags ❑None ❑ Other
Thermometer;
92 O4$ Type of Ice: E ret ❑Blue
ff R Gun ID:
Cooler Terrip (T). �•� Carrectlon Factor: Add/Subtract J'Q (,o
Cooler Temp Corrected ('C): .
USDA Regulated Sail 0"N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
Fly.., r
Biolog�ical issue Frozen?
[]Yes ETNo []N/A
Temp should be above fPeezing to VC
❑Samples outoftemp criteria. Samples an ice, coaling process
hasbegun
Did samples originate from a foreign source (internationally,
inrludineHawaii and Puerto Rlcol? MYes rlNo
Comments/Dscrepancy:
Chain of Custody Present?
res
❑No
❑N/a
1.
Samples Arrived within Hold Time?
Yes
❑No
❑NIA
2,
Short Hold Time Analysis (<72 hr.)?
OVes
210
❑N/A 1
3,
Rush Turn Around Time Requested?
❑Yes
EIN.
❑N/A
4,
Sufficient Volume?
54s
❑No
❑NIA
S.
Correct Containers Used?
e
[]No
❑N/A
6.
-Pace Containers Used?
Yes
❑No
❑N/A
Containers Intact?
EfYes
❑NO
NIA
7.
Dissolved analysis: Samples Field Filtered?
❑Yes .
[]No
NIA
B.
Sample Labels Match COC?
©es
❑No
[]N/A
9.
-includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
❑yes
No
[]N/A
10.
Trip Blank Present?
[-]Yes ,21
No
-]N/Ail.
Trip Blank Custody Seals Present?
[--]Yes
ONO
[AA
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes Ono
w ifp' z✓-Z I is ocl�
Lot ID of split containers:
CLIENT NOTIFICATION/RI SOLUTION
Parson contacted: .� �)(Q ) Datejflme:
Project Manager SCURF Review: T✓
Project Manager SRF Review:
Date: J5 I —I q
Date: S7�� 1 -1 q
Page 11 of 31

Document Name:
Sample Condition Upon Recei
Document No.'
F-CAR-05-033•Aev,06
Document Revised: February 7, 2013
Page 1 of 2
Issuing Authority,
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlofination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform,TOC, Oil and Grease, DRO/8015 (water) DOC, UNg
"Bottom half of box is to list number of bottle
Projec WO# : 92430082
r� I
PM: AMB Due Date: 06/04/19
CLIENT: 92-Municipal
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pH Adjustment Log for Preserved Samples
Sample ED
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 4
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form wid he sent to the North Carolina DFHNR Certification Office U.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 12 of 31

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Page 13 of 31

aceAnal ical ° A f �l A L Y T CAL REPORT
National Center for Testing & Innovation May 28, 2019
FTc
FSS
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1101589 [Cn]
Samples Received: 05/22/2019 FrProject Number: 92430082
Description: Surry Closed -Mt. Airy RC
Site: 001
GI
Report To: Angela Baioni
9800 Kincey Avenue, Suite 100 rAl
Huntersville, NC 28078
Fc
Entire Report Reviewed By: �vUnn �v, � �Lr'�
L�
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. i
41
Page 14 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:03 1 of 18
A

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
MW-1 L1101589-01
Qc: Quality Control Summary
Volatile Organic Compounds (GC/MS) by Method 8260D
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
CID
2
3
4
FS5
5
[Cn]
7
7
Fr
11
12
RC
13
F,
rAI
FSC
Page 15 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589 05/28/19 16:03 2 of 18

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
MW-1 L1101589-01 GW 05/17/1916:05 05/22/1908:45 C
P
Method
Volatile Organic Compounds (GC/MS) by Method 8260D
Batch Dilution Preparation Analysis Analyst Location I—J
date/time date/time FT,]
WG1287157 1 05/28/19 05:10 05/28/19 05:10 BMB Mt. Juliet, TN
[Cn]
FSr
RC
F,
FAI
FSC
Page 16 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589 05/28/19 16:03 3 of 18

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
VV VV� � �t La�'_
Nancy McLain
Project Manager
FP1
FTC
FSS
FSr
FC-1
F,
FAI
FSC
Page 17 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589 05/28/19 16:03 4 of 18

M W-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 16:05 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 05:10
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/2019 05:10
WG1287157
Benzene
U
0.331
1.00
1 05/28/2019 05:10
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/2019 05:10
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/2019 05:10
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 05:10
WG1287157
Bromoform
U
0.469
1.00
1 05/28/2019 05:10
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 05:10
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 05:10
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/2019 05:10
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 05:10
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/2019 05:10
WG1287157
Chloroform
U
0.324
5.00
1 05/28/2019 05:10
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 05:10
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 05:10
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 05:10
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 05:10
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 05:10
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/2019 05:10
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 05:10
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 05:10
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 05:10
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/2019 05:10
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 05:10
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 05:10
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 05:10
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 05:10
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 05:10
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 05:10
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 05:10
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 05:10
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 05:10
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 05:10
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 05:10
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 05:10
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/2019 05:10
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/2019 05:10
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/2019 05:10
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 05:10
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 05:10
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/2019 05:10
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 05:10
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 05:10
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/2019 05:10
WG1287157
Styrene
U
0.307
1.00
1 05/28/2019 05:10
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 05:10
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 05:10
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 05:10
WG1287157
Toluene
U
0.412
1.00
1 05/28/2019 05:10
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 05:10
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 05:10
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 05:10
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 05:10
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/2019 05:10
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 05:10
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 05:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92430082
L1101589
05/28/19 16:03
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 18 of 31
PAGE:
5of18

ONE LAB. NATIONWIDE.
MW-1 SAMPLE RESULTS - 01
Collected date/time: 05/17/19 16:05 L1101589
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/2019 05:10
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/2019 05:10
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/2019 05:10
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/2019 05:10
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/2019 05:10
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/2019 05:10
WG1287157
(S) Toluene-d8
91.3
80.0-120
0512812019 05.10
WG1287157
(S) 4-Bromof/uorobenzene
98.8
77.0-126
0512812019 05.10
WG1287157
(S 1,2-Dich/oroethane-d4
90.5
70.0-130
0512812019 05.10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92430082
L1101589
05/28/19 16:03
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 19 of 31
PAGE:
6 ofIS

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101589-01
Method Blank (MB)
(MB) R3415400-3 05/28/19 04:50
MB Result
Analyte
ug/I
Acetone
U
Acrylonitrile
U
Benzene
U
Bromobenzene
U
Bromodichloromethane
U
Bromochloromethane
U
Bromoform
U
Bromomethane
U
Carbon tetrachloride
U
Chlorobenzene
U
Chlorodibromomethane
U
Chloroethane
U
Chloroform
U
Chloromethane
U
2-Chlorotoluene
U
4-Chlorotoluene
U
1,2-Dibromo-3-Chloropropane
U
1,2-Dibromoethane
U
Dibromomethane
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
Dichlorodifluoromethane
U
1,1-Dichloroethane
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
cis-1,2-Dichloroethene
U
trans-1,2-Dichloroethene
U
1,2-Dichloropropane
U
1,1-Dichloropropene
U
1,3-Dichloropropane
U
cis-1,3-Dichloropropene
U
trans-1,3-Dichloropropene
U
2,2-Dichloropropane
U
Di -isopropyl ether
U
Ethylbenzene
U
Hexachloro-1,3-butadiene
U
2-Hexanone
U
p-Isopropyltoluene
U
2-Butanone (MEK)
U
MB Qualifier MB MDL
ug/I
10.0
1.87
0.331
0.352
0.380
0.520
0.469
0.866
0.379
0.348
0.327
0.453
0.324
0.276
0.375
0.351
1.33
0.381
0.346
0.349
0.220
0.274
0.551
0.259
0.361
0.398
0.260
0.396
0.306
0.352
0.366
0.418
0.419
0.321
0.320
0.384
0.256
3.82
0.350
3.93
MB RDL
ug/I
50.0
10.0
1.00
1.00
1.00
5.00
1.00
5.00
1.00
1.00
1.00
5.00
5.00
2.50
1.00
1.00
5.00
1.00
1.00
1.00
1.00
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
10.0
1.00
10.0
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
Page 20 of 31
PAGE:
7of18
ACCOUNT:
Pace Analytical - Huntersville, NC
PROJECT: SDG: DATE/TIME:
92430082 L1101589 05/28/19 16:03

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101589-01
Method Blank (MB)
(MB) R3415400-3 05/28/19 04:50
MB Result
Analyte
ug/I
Methylene Chloride
U
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
Styrene
U
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
Vinyl acetate
U
Vinyl chloride
U
Xylenes, Total
U
o-Xylene
U
m&p-Xylenes
U
1,4-Dioxane
U
(S) Toluene-d8
93.0
(S) 4-Bromof/uorobenzene
98.8
(S) 1,2-Dich/oroethone-d4
89.8
MB Qualifier MB MDL
ug/I
Laboratory Control Sample (LCS)
1.00
2.14
0.367
1.00
0.307
0.385
0.130
0.372
0.412
0.230
0.355
0.319
0.383
0.398
1.20
0.807
1.63
0.259
1.06
0.341
0.719
36.0
MB RDL
ug/I
5.00
10.0
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
5.00
2.50
10.0
1.00
3.00
1.00
2.00
100
80.0-120
77.0-126
70.0-130
(LCS) R3415400-1 05/28/19 03:30
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
Acetone
125
134
107
19.0-160
Acrylonitrile
125
148
118
55.0-149
Benzene
25.0
28.2
113
70.0-123
Bromobenzene
25.0
22.2
89.0
73.0-121
Bromodichloromethane
25.0
28.6
115
75.0-120
Bromochloromethane
25.0
24.7
98.7
76.0-122
Bromoform
25.0
25.1
100
68.0-132
Bromomethane
25.0
14.5
58.1
10.0-160
Page 21 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:03 8 of 18

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101589-01
Laboratory Control Sample (LCS)
(LCS) R3415400-1 05/28/19 03:30
Spike Amount LCS Result
Analyte ug/I ug/I
Carbon tetrachloride
25.0
29.3
Chlorobenzene
25.0
26.3
Chlorodibromomethane
25.0
25.7
Chloroethane
25.0
26.2
Chloroform
25.0
28.1
Chloromethane
25.0
12.7
2-Chlorotoluene
25.0
22.2
4-Chlorotoluene
25.0
23.3
1,2-Dibromo-3-Chloropropane
25.0
21.8
1,2-Dibromoethane
25.0
27.1
Dibromomethane
25.0
27.4
1,2-Dichlorobenzene
25.0
24.6
1,3-Dichlorobenzene
25.0
23.5
1,4-Dichlorobenzene
25.0
22.9
Dichlorodifluoromethane
25.0
12.4
1,1-Dichloroethane
25.0
28.3
1,2-Dichloroethane
25.0
25.9
1,1-Dichloroethene
25.0
30.5
cis-1,2-Dichloroethene
25.0
28.0
trans-1,2-Dichloroethene
25.0
30.0
1,2-Dichloropropane
25.0
27.8
1,1-Dichloropropene
25.0
29.9
1,3-Dichloropropane
25.0
27.1
cis-1,3-Dichloropropene
25.0
29.1
trans-1,3-Dichloropropene
25.0
25.8
2,2-Dichloropropane
25.0
25.9
Di -isopropyl ether
25.0
27.5
Ethylbenzene
25.0
27.0
Hexachloro-1,3-butadiene
25.0
20.9
2-Hexanone
125
136
p-Isopropyltoluene
25.0
22.3
2-Butanone (MEK)
125
130
Methylene Chloride
25.0
27.3
4-Methyl-2-pentanone (MIBK)
125
127
Methyl tert-butyl ether
25.0
28.8
Naphthalene
25.0
22.2
Styrene
25.0
28.0
1,1,1,2-Tetrachloroethane
25.0
26.1
1,1,2,2-Tetrachloroethane
25.0
23.1
Tetrachloroethene
25.0
28.4
LCS Rec
117
105
103
105
112
50.9
88.8
93.3
87.4
109
110
98.5
94.0
91.5
49.5
113
104
122
112
120
119
108
116
103
104
110
108
83.5
109
89.0
104
109
102
115
88.8
112
104
92.4
114
Rec. Limits LCS Qualifier
68.0-126
80.0-121
77.0-125
47.0-150
73.0-120
41.0-142
76.0-123
75.0-122
58.0-134
80.0-122
80.0-120
79.0-121
79.0-120
79.0-120
51.0-149
70.0-126
70.0-128
71.0-124
73.0-120
73.0-120
77.0-125
74.0-126
80.0-120
80.0-123
78.0-124
58.0-130
58.0-138
79.0-123
54.0-138
67.0-149
76.0-125
44.0-160
67.0-120
68.0-142
68.0-125
54.0-135
73.0-130
75.0-125
65.0-130
72.0-132
J4
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
Page 22 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:03 9 of 18

WG1287157
Volatile Organic Compounds (GC/MS) by Method 8260D
Laboratory Control Sample (LCS)
(LCS) R3415400-1 05/28/19 03:30
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Toluene
25.0
25.4
1,2,3-Trichlorobenzene
25.0
22.3
1,2,4-Trichlorobenzene
25.0
23.0
1,1,1-Trichloroethane
25.0
29.8
1,1,2-Trichloroethane
25.0
25.8
Trichloroethene
25.0
30.5
Trichlorofluoromethane
25.0
32.7
1,2,3-Trichloropropane
25.0
23.9
Vinyl acetate
125
113
Vinyl chloride
25.0
31.6
Xylenes, Total
75.0
77.1
o-Xylene
25.0
26.0
m&p-Xylenes
50.0
51.1
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethane-d4
Laboratory Control Sample (LCS)
LCS Rec.
102
89.1
91.8
119
103
122
131
95.7
90.7
126
103
104
102
92.2
104
86.0
QUALITY CONTROL SUMMARY
L1101589-01
Rec. Limits LCS Qualifier
79.0-120
50.0-138
57.0-137
73.0-124
80.0-120
78.0-124
59.0-147
73.0-130
11.0-160
67.0-131
79.0-123
80.0-122
80.0-122
80.0-120
77.0-126
70.0-130
ONE LAB. NATIONWIDE.
FP1
FTC]
IS-S]
4
Cn
rs-r
�GI
rAl
FSC
(LCS) R3415400-2 05/28/19 04:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
1,4-Dioxane 1000 988 98.8 13.0-160
(S) Toluene-d8 92.0 80.0-120
(S)4-Bromofluorobenzene 100 77.0-126
(S)1,2-Dich/oroethane-d4 91.5 70.0-130
Page 23 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:03 10 of 18

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
CP
IP
FTC
MDL
Method Detection Limit.
RDL
Reported Detection Limit.
FSS
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
[Cn]
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
FSr
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
Fc
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
FAI
duplicated within these ranges.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
FSC
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
JO JO: The identification of the analyte is acceptable, but the reported concentration is an estimate. The calibration met
method criteria.
J4 The associated batch QC was outside the established quality control range for accuracy.
Page 24 of 31
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92430082 L1101589 05/28/19 16:03 11 of 18

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
NewJersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT NO
OR MN
T ID T WI NY
SD
WY MI
NV
T NE IA OH T PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
W 11110
� NM O� AR N Sc
T MS A`7L GA
T TX * LA
T
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wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME:
Pace Analytical - Huntersville, NC 92430082 L1101589 05/28/19 16:03
ME
Page 25 of 31
PAGE:
12 of18

1164
Chain of Custody
❑ Samples were sent directly to the Subcontracting Laboratory. State Of Origin: NC
Cert. Needed: ❑ Yes ❑ No
_
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Workorder: 92429865 Workorder Name: SUKKY CLOSED -MT. . AIRY Owner Received Date: er/_uizV 19 Ke5urts r11equeareu oy, uj-rre-u is
lie :T "¢l'-- Requested Analysis==r
Angela Baioni
Pace Analytical Charlotte
9800 Kincey Ave. Suite 100 Pace National zV
Huntersville, NC 28078 12065 Lebanon Rd
x
Phone [phone]
Mt Juliet, TN 37122 e
615-758-5858
`v
Containers
Sample Collect g_
Item sample II] Type Date1T-ime _ Lab 0.. Matrix z LAB USE ONLY
,e -
1 PS 51171201916:05 92429865001 Water X L 1 14 _el
2 MW-3R PS 511712019 09:20 92429865002 Water X '06
3 VW-6 PS 5/171201916:31 92429865003 Water X U
4 MW-7 PS 5/17/201916:35 924298656D4 Water X b
5 MW-9 PS 5117/201917:D5 92429865005 Water X 41
6 Mw-11 PS 51171201917:11 92429865006 Water X
17 MW-12S PS 5/17/201916:28 92429865007 Water X 0-7
8 MW-13 PS 5/171201915:20 92429865008 Water X to
9 MW-14 PS 5/17/201915:25 92429865009 Water X Oq
10 MW-15 PS 5117/2019 09:25 92429865010 Water X i
11 MW-16 PS 5/17/2019 09 15 92429865011 Water X 1 {
12 MW-17 PS 511712019 14,20 92429865012 Water X I rl
13 MW-19 PS 51171201914:35 92429865013 Water X
14 Mw-20 PS 5/17/201917:15 92429865014 Water X 1
15 MW-21 PS 5/171201914:47 92429865015 Water X
16 Mw-22 PS 5117/201914:18 92429865016 Water X �p
17 Mw-23 PS 5/171201916:16 92429865017 Water X t
18 SCALEHOUSE PS 5/171201915:03 92429865018 Water X 1
114,w 5'0> 7MM M
Tuesday, May 21, 2019 1:55:39 PM FMT-ALL-C-002rev.00 24March2009 paPa% 1 T, 2
114,w 5'0> 7MM M
Tuesday, May 21, 2019 1:55:39 PM FMT-ALL-C-002rev.00 24March2009 paPa% 1 T, 2

Transfers Released By DatefTime Received By DaterTime
2
3
Cooler Tem erature on Receipt - °C Custody Seal Y or N Received on Ice � or N Samples Intac Y or N
***In order to maintain client confidentiality, location/name of the sampling sit ampler's name and signature may not be provided on this COC document.
This chain of custody is considered complete as is since this information is available in the owner laboratory.
-1 a i Pp
1•i A-C/
ZO SCREEN: <0.5 MR/hf
Tuesday, May 21, 2019 1:55:41 PM FMT-ALL-C-002rev.00 24March2009 Page 2 of 2
Page 27 of 31

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Ship To:
INTER —LABORATORY WORK ORDER # 92430082
(To be completed by sending lab)
Sending Project No
92430082
Receiving Project No
Check Box for Consolidated Invoice
',�:
Date Prepared
05l28/19
REQUESTED COMPLETION DATE
6/4/2019
Sending Region
1R92-Charlotte
Sending Project Mgr.
Angela Baioni
Receiving-Regi
IR850-Pace-Natk=1
-Ext r—i I -Client
Municipa Engineering Services
State of Sample Origin
NC
QC Deliverable
STD REPORT
Ali questions snouia De aaaressed to sending project manager.
Requested Reportable Units Report Wet or Dry Weight? Dry Weight
Cert. Needed
REQ17ES jE�]
Method Dertptlolt "'`
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TOTAL
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$11.0
Chain of Custody Included: EYes ENo Return Samples to Sending Region: Dyes �o
Matrix: EDrinking Water Soil Water Air EOther (identify)
s r: CQNIRMATION;OF WOR�CCOMPL 1' „D. z ` aaz=
Date Completed: Receiving Project Manager:
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Original sent to the receiving lab - Copy kept at the sending lab.
When work completed: Original sent to the ABM at the receiving laboratory. Copies are made to corporate as needed.
Tuesday, May 28, 2019 4:24:42 PM FMT-ALL-C-001 rev.00 24March2009 PaftJ A & 31

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Cooler Received/Opened On: 5/1,L-/19 Temperature:
Received By: Jordan Harris
Signature:
Receipt Check List NP
Yes
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COC Seal Present / Intact? i
COC Signed / Accurate?
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Bottles arrive intact?
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Correct bottles used?
Sufficient volume sent?
If Applicable
VOA Zero headspace?
Preservation Correct / Checked?
Page 31 of 31

lacieAnalXical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
July 05, 2019
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Maddie German, Municipal Engineering Services
r.Q _Kok
Q
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 65

lacmnalytical' www.pacelabs.corn
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Pace Analytical National Certification IDs
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: A130792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TNO03
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification M CERT0086
Nebraska Certification #: NE-OS-15-05
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TNO02
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LA000356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A21-A 2926.01
A21-A-ISO 17025 Certification #: 1461.01
A21-A-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92429863001
SW-1
Water
05/17/1911:19
05/20/1911:26
92429863002
SW-2
Water
05/17/1912:00
05/20/1911:26
92429863003
SW-3
Water
05/17/1914:35
05/20/1911:26
92429863004
SW-4
Water
05/17/1916:15
05/20/1911:26
92429863005
SWN-1
Water
05/17/1915:34
05/20/1911:26
92429863006
SWN-2
Water
05/17/1916:53
05/20/1911:26
92429863007
SW-C
Water
05/17/19 08:43
05/20/19 11:26
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SURRY MSWLF SWS
92429863
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92429863001
SW-1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
DWR
65
PAN
92429863002
SW-2
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
DWR
65
PAN
92429863003
SW-3
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
DWR
65
PAN
92429863004
SW-4
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
DWR
65
PAN
92429863005
SWN-1
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
DWR
65
PAN
92429863006
SWN-2
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
BMB
65
PAN
92429863007
SW-C
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
DWR
65
PAN
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-1
Lab ID:
92429863001
Collected:
05/17/19
11:19
Received: 05/20/19 11:26 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 601
OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
05/31/19 00:08
05/31/19 19:45
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:45
7440-38-2
Barium
23.1
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 19:45
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 19:45
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7440-47-3
Cobalt
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7440-50-8
Lead
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7439-92-1
Nickel
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:45
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7440-22-4
Vanadium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:45
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:45
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method:
EPA 3010A
Thallium
ND
ug/L
0.10
0.060
1
06/01/19 01:19
06/06/19 03:58
7440-28-0
VOA (GC/MS) 8260D
Analytical
Method: EPA 8260D
Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 17:15
05/28/19 17:15
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 17:15
05/28/19 17:15
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 17:15
05/28/19 17:15
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 17:15
05/28/19 17:15
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 17:15
05/28/19 17:15
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 17:15
05/28/19 17:15
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 17:15
05/28/19 17:15
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 17:15
05/28/19 17:15
74-83-9 CC
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 17:15
05/28/19 17:15
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 17:15
05/28/19 17:15
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 17:15
05/28/19 17:15
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 17:15
05/28/19 17:15
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 17:15
05/28/19 17:15
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 17:15
05/28/19 17:15
74-87-3 CC
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 17:15
05/28/19 17:15
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 17:15
05/28/19 17:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 17:15
05/28/19 17:15
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 17:15
05/28/19 17:15
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 17:15
05/28/19 17:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 17:15
05/28/19 17:15
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 17:15
05/28/19 17:15
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 17:15
05/28/19 17:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 17:15
05/28/19 17:15
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 17:15
05/28/19 17:15
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 17:15
05/28/19 17:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 17:15
05/28/19 17:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 17:15
05/28/19 17:15
156-59-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-1 Lab ID: 92429863001 Collected: 05/17/19 11:19 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 02:15 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1917:15
05/28/1917:15
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1917:15
05/28/1917:15
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1917:15
05/28/1917:15
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1917:15
05/28/1917:15
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1917:15
05/28/1917:15
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1917:15
05/28/1917:15
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1917:15
05/28/1917:15
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1917:15
05/28/1917:15
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1917:15
05/28/1917:15
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1917:15
05/28/1917:15
87-68-3 CC
ND
ug/L
10.0
3.82
1
05/28/1917:15
05/28/1917:15
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1917:15
05/28/1917:15
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1917:15
05/28/1917:15
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1917:15
05/28/1917:15
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1917:15
05/28/1917:15
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1917:15
05/28/1917:15
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1917:15
05/28/1917:15
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1917:15
05/28/1917:15
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1917:15
05/28/1917:15
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1917:15
05/28/1917:15
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1917:15
05/28/1917:15
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1917:15
05/28/1917:15
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1917:15
05/28/1917:15
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1917:15
05/28/1917:15
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1917:15
05/28/1917:15
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1917:15
05/28/1917:15
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1917:15
05/28/1917:15
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1917:15
05/28/1917:15
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1917:15
05/28/1917:15
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1917:15
05/28/1917:15
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1917:15
05/28/1917:15
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1917:15
05/28/1917:15
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1917:15
05/28/1917:15
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1917:15
05/28/1917:15
1330-20-7
ND
ug/L
100
36.0
1
05/28/1917:15
05/28/1917:15
123-91-1
90.3
%
80.0-120
1
05/28/1917:15
05/28/1917:15
2037-26-5
98.3
%
77.0-126
1
05/28/1917:15
05/28/1917:15
460-00-4
88.6
%
70.0-130
1
05/28/1917:15
05/28/1917:15
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-2
Lab ID:
92429863002
Collected:
05/17/19
12:00
Received: 05/20/19 11:26 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 601
OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
05/31/19 00:08
05/31/19 19:54
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:54
7440-38-2
Barium
23.1
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 19:54
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 19:54
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7440-47-3
Cobalt
19.9
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7440-50-8
Lead
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7439-92-1
Nickel
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:54
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7440-22-4
Vanadium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:54
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:54
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method:
EPA 3010A
Thallium
ND
ug/L
0.10
0.060
1
06/01/19 01:19
06/06/19 04:01
7440-28-0
VOA (GC/MS) 8260D
Analytical
Method: EPA 8260D
Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 17:35
05/28/19 17:35
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 17:35
05/28/19 17:35
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 17:35
05/28/19 17:35
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 17:35
05/28/19 17:35
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 17:35
05/28/19 17:35
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 17:35
05/28/19 17:35
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 17:35
05/28/19 17:35
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 17:35
05/28/19 17:35
74-83-9 CC
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 17:35
05/28/19 17:35
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 17:35
05/28/19 17:35
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 17:35
05/28/19 17:35
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 17:35
05/28/19 17:35
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 17:35
05/28/19 17:35
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 17:35
05/28/19 17:35
74-87-3 CC
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 17:35
05/28/19 17:35
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 17:35
05/28/19 17:35
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 17:35
05/28/19 17:35
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 17:35
05/28/19 17:35
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 17:35
05/28/19 17:35
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 17:35
05/28/19 17:35
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 17:35
05/28/19 17:35
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 17:35
05/28/19 17:35
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 17:35
05/28/19 17:35
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 17:35
05/28/19 17:35
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 17:35
05/28/19 17:35
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 17:35
05/28/19 17:35
75-35-4
cis-1,2-Dichloroethene
4.53
ug/L
1.00
0.260
1
05/28/19 17:35
05/28/19 17:35
156-59-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-2 Lab ID: 92429863002 Collected: 05/17/19 12:00 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 02:15 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1917:35
05/28/1917:35
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1917:35
05/28/1917:35
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1917:35
05/28/1917:35
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1917:35
05/28/1917:35
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1917:35
05/28/1917:35
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1917:35
05/28/1917:35
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1917:35
05/28/1917:35
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1917:35
05/28/1917:35
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1917:35
05/28/1917:35
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1917:35
05/28/1917:35
87-68-3 CC
ND
ug/L
10.0
3.82
1
05/28/1917:35
05/28/1917:35
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1917:35
05/28/1917:35
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1917:35
05/28/1917:35
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1917:35
05/28/1917:35
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1917:35
05/28/1917:35
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1917:35
05/28/1917:35
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1917:35
05/28/1917:35
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1917:35
05/28/1917:35
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1917:35
05/28/1917:35
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1917:35
05/28/1917:35
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1917:35
05/28/1917:35
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1917:35
05/28/1917:35
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1917:35
05/28/1917:35
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1917:35
05/28/1917:35
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1917:35
05/28/1917:35
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1917:35
05/28/1917:35
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1917:35
05/28/1917:35
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1917:35
05/28/1917:35
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1917:35
05/28/1917:35
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1917:35
05/28/1917:35
108-05-4
1.08
ug/L
1.00
0.259
1
05/28/1917:35
05/28/1917:35
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1917:35
05/28/1917:35
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1917:35
05/28/1917:35
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1917:35
05/28/1917:35
1330-20-7
ND
ug/L
100
36.0
1
05/28/1917:35
05/28/1917:35
123-91-1
91.3
%
80.0-120
1
05/28/1917:35
05/28/1917:35
2037-26-5
100
%
77.0-126
1
05/28/1917:35
05/28/1917:35
460-00-4
88.0
%
70.0-130
1
05/28/1917:35
05/28/1917:35
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-3
Lab ID:
92429863003
Collected:
05/17/19
14:35
Received: 05/20/19 11:26 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical
Method: EPA 601
OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
05/31/19 00:08
05/31/19 19:57
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:57
7440-38-2
Barium
17.8
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 19:57
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 19:57
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7440-47-3
Cobalt
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7440-50-8
Lead
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7439-92-1
Nickel
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:57
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7440-22-4
Vanadium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 19:57
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 19:57
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020E
Preparation Method:
EPA 3010A
Thallium
ND
ug/L
0.10
0.060
1
06/01/19 01:19
06/06/19 04:08
7440-28-0
VOA (GC/MS) 8260D
Analytical
Method: EPA 8260D
Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 17:55
05/28/19 17:55
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 17:55
05/28/19 17:55
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 17:55
05/28/19 17:55
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 17:55
05/28/19 17:55
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 17:55
05/28/19 17:55
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 17:55
05/28/19 17:55
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 17:55
05/28/19 17:55
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 17:55
05/28/19 17:55
74-83-9 CC
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 17:55
05/28/19 17:55
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 17:55
05/28/19 17:55
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 17:55
05/28/19 17:55
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 17:55
05/28/19 17:55
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 17:55
05/28/19 17:55
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 17:55
05/28/19 17:55
74-87-3 CC
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 17:55
05/28/19 17:55
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 17:55
05/28/19 17:55
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 17:55
05/28/19 17:55
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 17:55
05/28/19 17:55
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 17:55
05/28/19 17:55
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 17:55
05/28/19 17:55
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 17:55
05/28/19 17:55
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 17:55
05/28/19 17:55
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 17:55
05/28/19 17:55
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 17:55
05/28/19 17:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 17:55
05/28/19 17:55
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 17:55
05/28/19 17:55
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 17:55
05/28/19 17:55
156-59-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-3 Lab ID: 92429863003 Collected: 05/17/19 14:35 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 02:15 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1917:55
05/28/1917:55
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1917:55
05/28/1917:55
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1917:55
05/28/1917:55
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1917:55
05/28/1917:55
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1917:55
05/28/1917:55
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1917:55
05/28/1917:55
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1917:55
05/28/1917:55
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1917:55
05/28/1917:55
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1917:55
05/28/1917:55
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1917:55
05/28/1917:55
87-68-3 CC
ND
ug/L
10.0
3.82
1
05/28/1917:55
05/28/1917:55
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1917:55
05/28/1917:55
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1917:55
05/28/1917:55
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1917:55
05/28/1917:55
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1917:55
05/28/1917:55
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1917:55
05/28/1917:55
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1917:55
05/28/1917:55
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1917:55
05/28/1917:55
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1917:55
05/28/1917:55
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1917:55
05/28/1917:55
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1917:55
05/28/1917:55
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1917:55
05/28/1917:55
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1917:55
05/28/1917:55
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1917:55
05/28/1917:55
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1917:55
05/28/1917:55
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1917:55
05/28/1917:55
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1917:55
05/28/1917:55
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1917:55
05/28/1917:55
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1917:55
05/28/1917:55
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1917:55
05/28/1917:55
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1917:55
05/28/1917:55
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1917:55
05/28/1917:55
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1917:55
05/28/1917:55
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1917:55
05/28/1917:55
1330-20-7
ND
ug/L
100
36.0
1
05/28/1917:55
05/28/1917:55
123-91-1
92.6
%
80.0-120
1
05/28/1917:55
05/28/1917:55
2037-26-5
102
%
77.0-126
1
05/28/1917:55
05/28/1917:55
460-00-4
89.2
%
70.0-130
1
05/28/1917:55
05/28/1917:55
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-4 Lab ID: 92429863004 Collected: 05/17/19 16:15 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
05/31/19 00:08
05/31/19 20:00
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:00
7440-38-2
Barium
17.7
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:00
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:00
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7440-47-3
Cobalt
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7440-50-8
Lead
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7439-92-1
Nickel
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:00
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7440-22-4
Vanadium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:00
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:00
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/01/19 01:19
06/06/19 04:12
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 18:15
05/28/19 18:15
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 18:15
05/28/19 18:15
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 18:15
05/28/19 18:15
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 18:15
05/28/19 18:15
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 18:15
05/28/19 18:15
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 18:15
05/28/19 18:15
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 18:15
05/28/19 18:15
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 18:15
05/28/19 18:15
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 18:15
05/28/19 18:15
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 18:15
05/28/19 18:15
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 18:15
05/28/19 18:15
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 18:15
05/28/19 18:15
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 18:15
05/28/19 18:15
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 18:15
05/28/19 18:15
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 18:15
05/28/19 18:15
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 18:15
05/28/19 18:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 18:15
05/28/19 18:15
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 18:15
05/28/19 18:15
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 18:15
05/28/19 18:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 18:15
05/28/19 18:15
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 18:15
05/28/19 18:15
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 18:15
05/28/19 18:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 18:15
05/28/19 18:15
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 18:15
05/28/19 18:15
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 18:15
05/28/19 18:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 18:15
05/28/19 18:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 18:15
05/28/19 18:15
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-4 Lab ID: 92429863004 Collected: 05/17/19 16:15 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 02:15 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1918:15
05/28/1918:15
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1918:15
05/28/1918:15
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1918:15
05/28/1918:15
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1918:15
05/28/1918:15
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1918:15
05/28/1918:15
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1918:15
05/28/1918:15
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1918:15
05/28/1918:15
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1918:15
05/28/1918:15
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1918:15
05/28/1918:15
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1918:15
05/28/1918:15
87-68-3 CC
ND
ug/L
10.0
3.82
1
05/28/1918:15
05/28/1918:15
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1918:15
05/28/1918:15
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1918:15
05/28/1918:15
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1918:15
05/28/1918:15
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1918:15
05/28/1918:15
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1918:15
05/28/1918:15
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1918:15
05/28/1918:15
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1918:15
05/28/1918:15
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1918:15
05/28/1918:15
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1918:15
05/28/1918:15
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1918:15
05/28/1918:15
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1918:15
05/28/1918:15
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1918:15
05/28/1918:15
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1918:15
05/28/1918:15
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1918:15
05/28/1918:15
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1918:15
05/28/1918:15
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1918:15
05/28/1918:15
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1918:15
05/28/1918:15
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1918:15
05/28/1918:15
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1918:15
05/28/1918:15
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1918:15
05/28/1918:15
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1918:15
05/28/1918:15
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1918:15
05/28/1918:15
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1918:15
05/28/1918:15
1330-20-7
ND
ug/L
100
36.0
1
05/28/1918:15
05/28/1918:15
123-91-1
89.0
%
80.0-120
1
05/28/1918:15
05/28/1918:15
2037-26-5
99.5
%
77.0-126
1
05/28/1918:15
05/28/1918:15
460-00-4
86.5
%
70.0-130
1
05/28/1918:15
05/28/1918:15
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SWN-1 Lab ID: 92429863005 Collected: 05/17/19 15:34 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
05/31/19 00:08
05/31/19 20:03
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:03
7440-38-2
Barium
16.0
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:03
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:03
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7440-47-3
Cobalt
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7440-50-8
Lead
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7439-92-1
Nickel
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:03
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7440-22-4
Vanadium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:03
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:03
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/01/19 01:19
06/06/19 04:15
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 18:35
05/28/19 18:35
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 18:35
05/28/19 18:35
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 18:35
05/28/19 18:35
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 18:35
05/28/19 18:35
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 18:35
05/28/19 18:35
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 18:35
05/28/19 18:35
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 18:35
05/28/19 18:35
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 18:35
05/28/19 18:35
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 18:35
05/28/19 18:35
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 18:35
05/28/19 18:35
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 18:35
05/28/19 18:35
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 18:35
05/28/19 18:35
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 18:35
05/28/19 18:35
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 18:35
05/28/19 18:35
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 18:35
05/28/19 18:35
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 18:35
05/28/19 18:35
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 18:35
05/28/19 18:35
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 18:35
05/28/19 18:35
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 18:35
05/28/19 18:35
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 18:35
05/28/19 18:35
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 18:35
05/28/19 18:35
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 18:35
05/28/19 18:35
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 18:35
05/28/19 18:35
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 18:35
05/28/19 18:35
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 18:35
05/28/19 18:35
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 18:35
05/28/19 18:35
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 18:35
05/28/19 18:35
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SWN-1 Lab ID: 92429863005 Collected: 05/17/19 15:34 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 02:15 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1918:35
05/28/1918:35
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1918:35
05/28/1918:35
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1918:35
05/28/1918:35
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1918:35
05/28/1918:35
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1918:35
05/28/1918:35
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1918:35
05/28/1918:35
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1918:35
05/28/1918:35
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1918:35
05/28/1918:35
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1918:35
05/28/1918:35
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1918:35
05/28/1918:35
87-68-3 CC
ND
ug/L
10.0
3.82
1
05/28/1918:35
05/28/1918:35
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1918:35
05/28/1918:35
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1918:35
05/28/1918:35
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1918:35
05/28/1918:35
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1918:35
05/28/1918:35
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1918:35
05/28/1918:35
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1918:35
05/28/1918:35
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1918:35
05/28/1918:35
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1918:35
05/28/1918:35
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1918:35
05/28/1918:35
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1918:35
05/28/1918:35
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1918:35
05/28/1918:35
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1918:35
05/28/1918:35
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1918:35
05/28/1918:35
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1918:35
05/28/1918:35
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1918:35
05/28/1918:35
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1918:35
05/28/1918:35
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1918:35
05/28/1918:35
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1918:35
05/28/1918:35
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1918:35
05/28/1918:35
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1918:35
05/28/1918:35
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1918:35
05/28/1918:35
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1918:35
05/28/1918:35
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1918:35
05/28/1918:35
1330-20-7
ND
ug/L
100
36.0
1
05/28/1918:35
05/28/1918:35
123-91-1
98.2
%
80.0-120
1
05/28/1918:35
05/28/1918:35
2037-26-5
84.2
%
77.0-126
1
05/28/1918:35
05/28/1918:35
460-00-4
69.7
%
70.0-130
1
05/28/1918:35
05/28/1918:35
17060-07-0 SR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 65

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SWN-2 Lab ID: 92429863006 Collected: 05/17/19 16:53 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
05/31/19 00:08
05/31/19 20:06
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:06
7440-38-2
Barium
17.4
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:06
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:06
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7440-47-3
Cobalt
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7440-50-8
Lead
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7439-92-1
Nickel
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:06
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7440-22-4
Vanadium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:06
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:06
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/01/19 01:19
06/06/19 04:19
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 11:10
05/28/19 11:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 11:10
05/28/19 11:10
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 11:10
05/28/19 11:10
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 11:10
05/28/19 11:10
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 11:10
05/28/19 11:10
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 11:10
05/28/19 11:10
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 11:10
05/28/19 11:10
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 11:10
05/28/19 11:10
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 11:10
05/28/19 11:10
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 11:10
05/28/19 11:10
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 11:10
05/28/19 11:10
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 11:10
05/28/19 11:10
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 11:10
05/28/19 11:10
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 11:10
05/28/19 11:10
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 11:10
05/28/19 11:10
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 11:10
05/28/19 11:10
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 11:10
05/28/19 11:10
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 11:10
05/28/19 11:10
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 11:10
05/28/19 11:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 11:10
05/28/19 11:10
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 11:10
05/28/19 11:10
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 11:10
05/28/19 11:10
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 11:10
05/28/19 11:10
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 11:10
05/28/19 11:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 11:10
05/28/19 11:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 11:10
05/28/19 11:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 11:10
05/28/19 11:10
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
LO
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 65

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SWN-2 Lab ID: 92429863006 Collected: 05/17/19 16:53 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 02:15 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1911:10
05/28/1911:10
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1911:10
05/28/1911:10
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1911:10
05/28/1911:10
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1911:10
05/28/1911:10
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1911:10
05/28/1911:10
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1911:10
05/28/1911:10
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1911:10
05/28/1911:10
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1911:10
05/28/1911:10
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1911:10
05/28/1911:10
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1911:10
05/28/1911:10
87-68-3
ND
ug/L
10.0
3.82
1
05/28/1911:10
05/28/1911:10
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1911:10
05/28/1911:10
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1911:10
05/28/1911:10
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1911:10
05/28/1911:10
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1911:10
05/28/1911:10
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1911:10
05/28/1911:10
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1911:10
05/28/1911:10
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1911:10
05/28/1911:10
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1911:10
05/28/1911:10
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1911:10
05/28/1911:10
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1911:10
05/28/1911:10
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1911:10
05/28/1911:10
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1911:10
05/28/1911:10
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1911:10
05/28/1911:10
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1911:10
05/28/1911:10
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1911:10
05/28/1911:10
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1911:10
05/28/1911:10
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1911:10
05/28/1911:10
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1911:10
05/28/1911:10
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1911:10
05/28/1911:10
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1911:10
05/28/1911:10
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1911:10
05/28/1911:10
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1911:10
05/28/1911:10
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1911:10
05/28/1911:10
1330-20-7
ND
ug/L
100
36.0
1
05/28/1911:10
05/28/1911:10
123-91-1
91.8
%
80.0-120
1
05/28/1911:10
05/28/1911:10
2037-26-5
102
%
77.0-126
1
05/28/1911:10
05/28/1911:10
460-00-4
89.1
%
70.0-130
1
05/28/1911:10
05/28/1911:10
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-C Lab ID: 92429863007 Collected: 05/17/19 08:43 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
05/31/19 00:08
05/31/19 20:09
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:09
7440-38-2
Barium
18.6
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:09
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/31/19 00:08
05/31/19 20:09
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7440-47-3
Cobalt
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7440-50-8
Lead
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7439-92-1
Nickel
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:09
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7440-22-4
Vanadium
ND
ug/L
5.0
2.5
1
05/31/19 00:08
05/31/19 20:09
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/31/19 00:08
05/31/19 20:09
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
06/01/19 01:19
06/06/19 04:22
7440-28-0
VOA (GC/MS) 8260D
Analytical Method: EPA 8260D Preparation Method: 8260D
Acetone
ND
ug/L
50.0
10.0
1
05/28/19 18:55
05/28/19 18:55
67-64-1
Acrylonitrile
ND
ug/L
10.0
1.87
1
05/28/19 18:55
05/28/19 18:55
107-13-1
Benzene
ND
ug/L
1.00
0.331
1
05/28/19 18:55
05/28/19 18:55
71-43-2
Bromobenzene
ND
ug/L
1.00
0.352
1
05/28/19 18:55
05/28/19 18:55
108-86-1
Bromochloromethane
ND
ug/L
5.00
0.520
1
05/28/19 18:55
05/28/19 18:55
74-97-5
Bromodichloromethane
ND
ug/L
1.00
0.380
1
05/28/19 18:55
05/28/19 18:55
75-27-4
Bromoform
ND
ug/L
1.00
0.469
1
05/28/19 18:55
05/28/19 18:55
75-25-2
Bromomethane
ND
ug/L
5.00
0.866
1
05/28/19 18:55
05/28/19 18:55
74-83-9
Carbon tetrachloride
ND
ug/L
1.00
0.379
1
05/28/19 18:55
05/28/19 18:55
56-23-5
Chlorobenzene
ND
ug/L
1.00
0.348
1
05/28/19 18:55
05/28/19 18:55
108-90-7
Dibromochloromethane
ND
ug/L
1.00
0.327
1
05/28/19 18:55
05/28/19 18:55
124-48-1
Chloroethane
ND
ug/L
5.00
0.453
1
05/28/19 18:55
05/28/19 18:55
75-00-3
Chloroform
ND
ug/L
5.00
0.324
1
05/28/19 18:55
05/28/19 18:55
67-66-3
Chloromethane
ND
ug/L
2.50
0.276
1
05/28/19 18:55
05/28/19 18:55
74-87-3
2-Chlorotoluene
ND
ug/L
1.00
0.375
1
05/28/19 18:55
05/28/19 18:55
95-49-8
4-Chlorotoluene
ND
ug/L
1.00
0.351
1
05/28/19 18:55
05/28/19 18:55
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.00
1.33
1
05/28/19 18:55
05/28/19 18:55
96-12-8
1,2-Dibromoethane (EDB)
ND
ug/L
1.00
0.381
1
05/28/19 18:55
05/28/19 18:55
106-93-4
Dibromomethane
ND
ug/L
1.00
0.346
1
05/28/19 18:55
05/28/19 18:55
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.00
0.349
1
05/28/19 18:55
05/28/19 18:55
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.00
0.220
1
05/28/19 18:55
05/28/19 18:55
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.00
0.274
1
05/28/19 18:55
05/28/19 18:55
106-46-7
Dichlorodifluoromethane
ND
ug/L
5.00
0.551
1
05/28/19 18:55
05/28/19 18:55
75-71-8
1,1-Dichloroethane
ND
ug/L
1.00
0.259
1
05/28/19 18:55
05/28/19 18:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.00
0.361
1
05/28/19 18:55
05/28/19 18:55
107-06-2
1,1-Dichloroethene
ND
ug/L
1.00
0.398
1
05/28/19 18:55
05/28/19 18:55
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.00
0.260
1
05/28/19 18:55
05/28/19 18:55
156-59-2
REPORT OF LABORATORY ANALYSIS
CC
CC
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
Sample: SW-C Lab ID: 92429863007 Collected: 05/17/19 08:43 Received: 05/20/19 11:26 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
VOA (GC/MS) 8260D
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
2,2-Dichloropropane
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
o-Xylene
m&p-Xylene
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Date: 07/05/2019 02:15 PM
Analytical Method: EPA 8260D Preparation Method: 8260D
ND
ug/L
1.00
0.396
1
05/28/1918:55
05/28/1918:55
156-60-5
ND
ug/L
1.00
0.306
1
05/28/1918:55
05/28/1918:55
78-87-5
ND
ug/L
1.00
0.352
1
05/28/1918:55
05/28/1918:55
563-58-6
ND
ug/L
1.00
0.366
1
05/28/1918:55
05/28/1918:55
142-28-9
ND
ug/L
1.00
0.418
1
05/28/1918:55
05/28/1918:55
10061-01-5
ND
ug/L
1.00
0.419
1
05/28/1918:55
05/28/1918:55
10061-02-6
ND
ug/L
1.00
0.321
1
05/28/1918:55
05/28/1918:55
594-20-7
ND
ug/L
1.00
0.320
1
05/28/1918:55
05/28/1918:55
108-20-3
ND
ug/L
1.00
0.384
1
05/28/1918:55
05/28/1918:55
100-41-4
ND
ug/L
1.00
0.256
1
05/28/1918:55
05/28/1918:55
87-68-3 CC
ND
ug/L
10.0
3.82
1
05/28/1918:55
05/28/1918:55
591-78-6
ND
ug/L
1.00
0.350
1
05/28/1918:55
05/28/1918:55
99-87-6
ND
ug/L
10.0
3.93
1
05/28/1918:55
05/28/1918:55
78-93-3
ND
ug/L
5.00
1.00
1
05/28/1918:55
05/28/1918:55
75-09-2
ND
ug/L
10.0
2.14
1
05/28/1918:55
05/28/1918:55
108-10-1
ND
ug/L
1.00
0.367
1
05/28/1918:55
05/28/1918:55
1634-04-4
ND
ug/L
5.00
1.00
1
05/28/1918:55
05/28/1918:55
91-20-3
ND
ug/L
1.00
0.307
1
05/28/1918:55
05/28/1918:55
100-42-5
ND
ug/L
1.00
0.385
1
05/28/1918:55
05/28/1918:55
630-20-6
ND
ug/L
1.00
0.130
1
05/28/1918:55
05/28/1918:55
79-34-5
ND
ug/L
1.00
0.372
1
05/28/1918:55
05/28/1918:55
127-18-4
ND
ug/L
1.00
0.412
1
05/28/1918:55
05/28/1918:55
108-88-3
ND
ug/L
1.00
0.230
1
05/28/1918:55
05/28/1918:55
87-61-6
ND
ug/L
1.00
0.355
1
05/28/1918:55
05/28/1918:55
120-82-1
ND
ug/L
1.00
0.319
1
05/28/1918:55
05/28/1918:55
71-55-6
ND
ug/L
1.00
0.383
1
05/28/1918:55
05/28/1918:55
79-00-5
ND
ug/L
1.00
0.398
1
05/28/1918:55
05/28/1918:55
79-01-6
ND
ug/L
5.00
1.20
1
05/28/1918:55
05/28/1918:55
75-69-4
ND
ug/L
2.50
0.807
1
05/28/1918:55
05/28/1918:55
96-18-4
ND
ug/L
10.0
1.63
1
05/28/1918:55
05/28/1918:55
108-05-4
ND
ug/L
1.00
0.259
1
05/28/1918:55
05/28/1918:55
75-01-4
ND
ug/L
1.00
0.341
1
05/28/1918:55
05/28/1918:55
95-47-6
ND
ug/L
2.00
0.719
1
05/28/1918:55
05/28/1918:55
179601-23-1
ND
ug/L
3.00
1.06
1
05/28/1918:55
05/28/1918:55
1330-20-7
ND
ug/L
100
36.0
1
05/28/1918:55
05/28/1918:55
123-91-1
91.4
%
80.0-120
1
05/28/1918:55
05/28/1918:55
2037-26-5
101
%
77.0-126
1
05/28/1918:55
05/28/1918:55
460-00-4
90.7
%
70.0-130
1
05/28/1918:55
05/28/1918:55
17060-07-0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 18 of 65

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QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
QC Batch: 478300 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92429863001, 92429863002, 92429863003, 92429863004, 92429863005, 92429863006, 92429863007
METHOD BLANK: 2589492 Matrix: Water
Associated Lab Samples: 92429863001, 92429863002, 92429863003, 92429863004, 92429863005, 92429863006, 92429863007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
5.0
3.9
05/31/1919:09
Arsenic
ug/L
ND
10.0
5.0
05/31/1919:09
Barium
ug/L
ND
5.0
2.5
05/31/1919:09
Beryllium
ug/L
ND
1.0
0.50
05/31/1919:09
Cadmium
ug/L
ND
1.0
0.50
05/31/1919:09
Chromium
ug/L
ND
5.0
2.5
05/31/1919:09
Cobalt
ug/L
ND
5.0
2.5
05/31/1919:09
Copper
ug/L
ND
5.0
2.5
05/31/1919:09
Lead
ug/L
ND
5.0
2.5
05/31/1919:09
Nickel
ug/L
ND
5.0
2.5
05/31/1919:09
Selenium
ug/L
ND
10.0
5.0
05/31/1919:09
Silver
ug/L
ND
5.0
2.5
05/31/1919:09
Vanadium
ug/L
ND
5.0
2.5
05/31/1919:09
Zinc
ug/L
ND
10.0
5.0
05/31/1919:09
LABORATORY CONTROL SAMPLE:
Parameter
2589493
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
487
97
80-120
Arsenic
ug/L
500
466
93
80-120
Barium
ug/L
500
495
99
80-120
Beryllium
ug/L
500
496
99
80-120
Cadmium
ug/L
500
489
98
80-120
Chromium
ug/L
500
497
99
80-120
Cobalt
ug/L
500
490
98
80-120
Copper
ug/L
500
502
100
80-120
Lead
ug/L
500
484
97
80-120
Nickel
ug/L
500
486
97
80-120
Selenium
ug/L
500
481
96
80-120
Silver
ug/L
250
251
100
80-120
Vanadium
ug/L
500
497
99
80-120
Zinc
ug/L
500
478
96
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2589494 2589495
MS MSD
92429561004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 486 499 97 100 75-125 3 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 65

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
SURRY MSWLF SWS
92429863
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2589494
2589495
MS
MSD
92429561004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
485
496
97
99
75-125
2
20
Barium
ug/L
253
500
500
750
759
99
101
75-125
1
20
Beryllium
ug/L
ND
500
500
502
515
100
103
75-125
2
20
Cadmium
ug/L
ND
500
500
483
489
97
98
75-125
1
20
Chromium
ug/L
ND
500
500
497
506
99
101
75-125
2
20
Cobalt
ug/L
21.4
500
500
507
515
97
99
75-125
1
20
Copper
ug/L
ND
500
500
526
537
105
107
75-125
2
20
Lead
ug/L
ND
500
500
480
488
96
98
75-125
2
20
Nickel
ug/L
5.2
500
500
486
495
96
98
75-125
2
20
Selenium
ug/L
ND
500
500
515
521
103
104
75-125
1
20
Silver
ug/L
ND
250
250
250
255
100
102
75-125
2
20
Vanadium
ug/L
ND
500
500
508
518
102
104
75-125
2
20
Zinc
ug/L
ND
500
500
475
482
94
96
75-125
2
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
QC Batch: 478331 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92429863001, 92429863002, 92429863003, 92429863004, 92429863005, 92429863006, 92429863007
METHOD BLANK: 2589562 Matrix: Water
Associated Lab Samples: 92429863001, 92429863002, 92429863003, 92429863004, 92429863005, 92429863006, 92429863007
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.060 06/06/19 02:29
LABORATORY CONTROL SAMPLE: 2589563
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2589564 2589565
MS MSD
92429561004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 9.6 10.0 96 100 75-125 4 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
QC Batch: 1287157 Analysis Method: EPA 8260D
QC Batch Method: 8260D Analysis Description: VOA (GC/MS) 8260D
Associated Lab Samples: 92429863006
METHOD BLANK: R3415400-3
Associated Lab Samples: 92429863006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Acetone
ug/L
ND
50.0
10.0
05/28/19 04:50
Acrylonitrile
ug/L
ND
10.0
1.87
05/28/19 04:50
Benzene
ug/L
ND
1.00
0.331
05/28/19 04:50
Bromobenzene
ug/L
ND
1.00
0.352
05/28/19 04:50
Bromodichloromethane
ug/L
ND
1.00
0.380
05/28/19 04:50
Bromochloromethane
ug/L
ND
5.00
0.520
05/28/19 04:50
Bromoform
ug/L
ND
1.00
0.469
05/28/19 04:50
Bromomethane
ug/L
ND
5.00
0.866
05/28/19 04:50
Carbon tetrachloride
ug/L
ND
1.00
0.379
05/28/19 04:50
Chlorobenzene
ug/L
ND
1.00
0.348
05/28/19 04:50
Dibromochloromethane
ug/L
ND
1.00
0.327
05/28/19 04:50
Chloroethane
ug/L
ND
5.00
0.453
05/28/19 04:50
Chloroform
ug/L
ND
5.00
0.324
05/28/19 04:50
Chloromethane
ug/L
ND
2.50
0.276
05/28/19 04:50
2-Chlorotoluene
ug/L
ND
1.00
0.375
05/28/19 04:50
4-Chlorotoluene
ug/L
ND
1.00
0.351
05/28/19 04:50
1,2-Dibromo-3-chloropropane
ug/L
ND
5.00
1.33
05/28/19 04:50
1,2-Dibromoethane (EDB)
ug/L
ND
1.00
0.381
05/28/19 04:50
Dibromomethane
ug/L
ND
1.00
0.346
05/28/19 04:50
1,2-Dichlorobenzene
ug/L
ND
1.00
0.349
05/28/19 04:50
1,3-Dichlorobenzene
ug/L
ND
1.00
0.220
05/28/19 04:50
1,4-Dichlorobenzene
ug/L
ND
1.00
0.274
05/28/19 04:50
Dichlorodifluoromethane
ug/L
ND
5.00
0.551
05/28/19 04:50
1,1-Dichloroethane
ug/L
ND
1.00
0.259
05/28/19 04:50
1,2-Dichloroethane
ug/L
ND
1.00
0.361
05/28/19 04:50
1,1-Dichloroethene
ug/L
ND
1.00
0.398
05/28/19 04:50
cis-1,2-Dichloroethene
ug/L
ND
1.00
0.260
05/28/19 04:50
trans-1,2-Dichloroethene
ug/L
ND
1.00
0.396
05/28/19 04:50
1,2-Dichloropropane
ug/L
ND
1.00
0.306
05/28/19 04:50
1,1-Dichloropropene
ug/L
ND
1.00
0.352
05/28/19 04:50
1,3-Dichloropropane
ug/L
ND
1.00
0.366
05/28/19 04:50
cis-1,3-Dichloropropene
ug/L
ND
1.00
0.418
05/28/19 04:50
trans- 1,3-Dichloropropene
ug/L
ND
1.00
0.419
05/28/19 04:50
2,2-Dichloropropane
ug/L
ND
1.00
0.321
05/28/19 04:50
Diisopropyl ether
ug/L
ND
1.00
0.320
05/28/19 04:50
Ethylbenzene
ug/L
ND
1.00
0.384
05/28/19 04:50
Hexachloro-1,3-butadiene
ug/L
ND
1.00
0.256
05/28/19 04:50
2-Hexanone
ug/L
ND
10.0
3.82
05/28/19 04:50
p-Isopropyltoluene
ug/L
ND
1.00
0.350
05/28/19 04:50
2-Butanone (MEK)
ug/L
ND
10.0
3.93
05/28/19 04:50
Methylene Chloride
ug/L
ND
5.00
1.00
05/28/19 04:50
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 65

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
METHOD BLANK: R3415400-3
Associated Lab Samples: 92429863006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
4-Methyl-2-pentanone (MIBK)
ug/L
ND
10.0
2.14
05/28/19 04:50
Methyl-tert-butyl ether
ug/L
ND
1.00
0.367
05/28/19 04:50
Naphthalene
ug/L
ND
5.00
1.00
05/28/19 04:50
Styrene
ug/L
ND
1.00
0.307
05/28/19 04:50
1,1,1,2-Tetrachloroethane
ug/L
ND
1.00
0.385
05/28/19 04:50
1,1,2,2-Tetrachloroethane
ug/L
ND
1.00
0.130
05/28/19 04:50
Tetrachloroethene
ug/L
ND
1.00
0.372
05/28/19 04:50
Toluene
ug/L
ND
1.00
0.412
05/28/19 04:50
1,2,3-Trichlorobenzene
ug/L
ND
1.00
0.230
05/28/19 04:50
1,2,4-Trichlorobenzene
ug/L
ND
1.00
0.355
05/28/19 04:50
1,1,1-Trichloroethane
ug/L
ND
1.00
0.319
05/28/19 04:50
1,1,2-Trichloroethane
ug/L
ND
1.00
0.383
05/28/19 04:50
Trichloroethene
ug/L
ND
1.00
0.398
05/28/19 04:50
Trichlorofluoromethane
ug/L
ND
5.00
1.20
05/28/19 04:50
1,2,3-Trichloropropane
ug/L
ND
2.50
0.807
05/28/19 04:50
Vinyl acetate
ug/L
ND
10.0
1.63
05/28/19 04:50
Vinyl chloride
ug/L
ND
1.00
0.259
05/28/19 04:50
Xylene (Total)
ug/L
ND
3.00
1.06
05/28/19 04:50
o-Xylene
ug/L
ND
1.00
0.341
05/28/19 04:50
m&p-Xylene
ug/L
ND
2.00
0.719
05/28/19 04:50
1,4-Dioxane (p-Dioxane)
ug/L
ND
100
36.0
05/28/19 04:50
Toluene-d8 (S)
%
93
80.0-120
05/28/19 04:50
4-Bromofluorobenzene (S)
%
98.8
77.0-126
05/28/19 04:50
1,2-Dichloroethane-d4 (S)
%
89.8
70.0-130
05/28/19 04:50
LABORATORY CONTROL SAMPLE:
Parameter
R3415400-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Acetone
ug/L
125
134
107
19.0-160
Acrylonitrile
ug/L
125
148
118
55.0-149
Benzene
ug/L
25.0
28.2
113
70.0-123
Bromobenzene
ug/L
25.0
22.2
89.0
73.0-121
Bromodichloromethane
ug/L
25.0
28.6
115
75.0-120
Bromochloromethane
ug/L
25.0
24.7
98.7
76.0-122
Bromoform
ug/L
25.0
25.1
100
68.0-132
Bromomethane
ug/L
25.0
14.5
58.1
10.0-160
Carbon tetrachloride
ug/L
25.0
29.3
117
68.0-126
Chlorobenzene
ug/L
25.0
26.3
105
80.0-121
Dibromochloromethane
ug/L
25.0
25.7
103
77.0-125
Chloroethane
ug/L
25.0
26.2
105
47.0-150
Chloroform
ug/L
25.0
28.1
112
73.0-120
Chloromethane
ug/L
25.0
12.7
50.9
41.0-142
2-Chlorotoluene
ug/L
25.0
22.2
88.8
76.0-123
4-Chlorotoluene
ug/L
25.0
23.3
93.3
75.0-122
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
LABORATORY CONTROL SAMPLE:
Parameter
R3415400-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2-Dibromo-3-chloropropane
ug/L
25.0
21.8
87.4
58.0-134
1,2-Dibromoethane (EDB)
ug/L
25.0
27.1
109
80.0-122
Dibromomethane
ug/L
25.0
27.4
110
80.0-120
1,2-Dichlorobenzene
ug/L
25.0
24.6
98.5
79.0-121
1,3-Dichlorobenzene
ug/L
25.0
23.5
94.0
79.0-120
1,4-Dichlorobenzene
ug/L
25.0
22.9
91.5
79.0-120
Dichlorodifluoromethane
ug/L
25.0
12.4
49.5
51.0-149 LO
1,1-Dichloroethane
ug/L
25.0
28.3
113
70.0-126
1,2-Dichloroethane
ug/L
25.0
25.9
104
70.0-128
1,1-Dichloroethene
ug/L
25.0
30.5
122
71.0-124
cis-1,2-Dichloroethene
ug/L
25.0
28.0
112
73.0-120
trans-1,2-Dichloroethene
ug/L
25.0
30.0
120
73.0-120
1,2-Dichloropropane
ug/L
25.0
27.8
111
77.0-125
1,1-Dichloropropene
ug/L
25.0
29.9
119
74.0-126
1,3-Dichloropropane
ug/L
25.0
27.1
108
80.0-120
cis-1,3-Dichloropropene
ug/L
25.0
29.1
116
80.0-123
trans- 1,3-Dichloropropene
ug/L
25.0
25.8
103
78.0-124
2,2-Dichloropropane
ug/L
25.0
25.9
104
58.0-130
Diisopropyl ether
ug/L
25.0
27.5
110
58.0-138
Ethylbenzene
ug/L
25.0
27.0
108
79.0-123
Hexachloro-1,3-butadiene
ug/L
25.0
20.9
83.5
54.0-138
2-Hexanone
ug/L
125
136
109
67.0-149
p-Isopropyltoluene
ug/L
25.0
22.3
89.0
76.0-125
2-Butanone (MEK)
ug/L
125
130
104
44.0-160
Methylene Chloride
ug/L
25.0
27.3
109
67.0-120
4-Methyl-2-pentanone (MIBK)
ug/L
125
127
102
68.0-142
Methyl-tert-butyl ether
ug/L
25.0
28.8
115
68.0-125
Naphthalene
ug/L
25.0
22.2
88.8
54.0-135
Styrene
ug/L
25.0
28.0
112
73.0-130
1,1,1,2-Tetrachloroethane
ug/L
25.0
26.1
104
75.0-125
1,1,2,2-Tetrachloroethane
ug/L
25.0
23.1
92.4
65.0-130
Tetrachloroethene
ug/L
25.0
28.4
114
72.0-132
Toluene
ug/L
25.0
25.4
102
79.0-120
1,2,3-Trichlorobenzene
ug/L
25.0
22.3
89.1
50.0-138
1,2,4-Trichlorobenzene
ug/L
25.0
23.0
91.8
57.0-137
1,1,1-Trichloroethane
ug/L
25.0
29.8
119
73.0-124
1,1,2-Trichloroethane
ug/L
25.0
25.8
103
80.0-120
Trichloroethene
ug/L
25.0
30.5
122
78.0-124
Trichlorofluoromethane
ug/L
25.0
32.7
131
59.0-147
1,2,3-Trichloropropane
ug/L
25.0
23.9
95.7
73.0-130
Vinyl acetate
ug/L
125
113
90.7
11.0-160
Vinyl chloride
ug/L
25.0
31.6
126
67.0-131
Xylene (Total)
ug/L
75.0
77.1
103
79.0-123
o-Xylene
ug/L
25.0
26.0
104
80.0-122
m&p-Xylene
ug/L
50.0
51.1
102
80.0-122
Toluene-d8 (S)
%
92.2
80.0-120
4-Bromofluorobenzene (S)
%
104
77.0-126
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 65

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
LABORATORY CONTROL SAMPLE: R3415400-1
Parameter Units
1,2-Dichloroethane-d4 (S) %
LABORATORY CONTROL SAMPLE:
R3415400-2
Parameter
Units
1,4-Dioxane (p-Dioxane)
ug/L
Toluene-d8 (S)
%
4-Bromofluorobenzene (S)
%
1,2-Dichloroethane-d4 (S)
%
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
86.0 70.0-130
Spike LCS
Conc. Result
1000 988
LCS
% Rec
% Rec
Limits Qualifiers
98.8
13.0-160
92.0
80.0-120
100
77.0-126
91.5
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
QC Batch: 1287536 Analysis Method: EPA 8260D
QC Batch Method: 8260D Analysis Description: VOA (GC/MS) 8260D
Associated Lab Samples: 92429863001, 92429863002, 92429863003, 92429863004, 92429863005, 92429863007
METHOD BLANK: R3416175-3 Matrix: Water
Associated Lab Samples: 92429863001, 92429863002, 92429863003, 92429863004, 92429863005, 92429863007
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Acetone
ug/L
ND
50.0
10.0
05/28/19 15:13
Acrylonitrile
ug/L
ND
10.0
1.87
05/28/19 15:13
Benzene
ug/L
ND
1.00
0.331
05/28/19 15:13
Bromobenzene
ug/L
ND
1.00
0.352
05/28/19 15:13
Bromodichloromethane
ug/L
ND
1.00
0.380
05/28/19 15:13
Bromochloromethane
ug/L
ND
5.00
0.520
05/28/19 15:13
Bromoform
ug/L
ND
1.00
0.469
05/28/19 15:13
Bromomethane
ug/L
ND
5.00
0.866
05/28/19 15:13
Carbon tetrachloride
ug/L
ND
1.00
0.379
05/28/19 15:13
Chlorobenzene
ug/L
ND
1.00
0.348
05/28/19 15:13
Dibromochloromethane
ug/L
ND
1.00
0.327
05/28/19 15:13
Chloroethane
ug/L
ND
5.00
0.453
05/28/19 15:13
Chloroform
ug/L
ND
5.00
0.324
05/28/19 15:13
Chloromethane
ug/L
ND
2.50
0.276
05/28/19 15:13
2-Chlorotoluene
ug/L
ND
1.00
0.375
05/28/19 15:13
4-Chlorotoluene
ug/L
ND
1.00
0.351
05/28/19 15:13
1,2-Dibromo-3-chloropropane
ug/L
ND
5.00
1.33
05/28/19 15:13
1,2-Dibromoethane (EDB)
ug/L
ND
1.00
0.381
05/28/19 15:13
Dibromomethane
ug/L
ND
1.00
0.346
05/28/19 15:13
1,2-Dichlorobenzene
ug/L
ND
1.00
0.349
05/28/19 15:13
1,3-Dichlorobenzene
ug/L
ND
1.00
0.220
05/28/19 15:13
1,4-Dichlorobenzene
ug/L
ND
1.00
0.274
05/28/19 15:13
Dichlorodifluoromethane
ug/L
ND
5.00
0.551
05/28/19 15:13
1,1-Dichloroethane
ug/L
ND
1.00
0.259
05/28/19 15:13
1,2-Dichloroethane
ug/L
ND
1.00
0.361
05/28/19 15:13
1,1-Dichloroethene
ug/L
ND
1.00
0.398
05/28/19 15:13
cis-1,2-Dichloroethene
ug/L
ND
1.00
0.260
05/28/19 15:13
trans-1,2-Dichloroethene
ug/L
ND
1.00
0.396
05/28/19 15:13
1,2-Dichloropropane
ug/L
ND
1.00
0.306
05/28/19 15:13
1,1-Dichloropropene
ug/L
ND
1.00
0.352
05/28/19 15:13
1,3-Dichloropropane
ug/L
ND
1.00
0.366
05/28/19 15:13
cis-1,3-Dichloropropene
ug/L
ND
1.00
0.418
05/28/19 15:13
trans- 1,3-Dichloropropene
ug/L
ND
1.00
0.419
05/28/19 15:13
2,2-Dichloropropane
ug/L
ND
1.00
0.321
05/28/19 15:13
Diisopropyl ether
ug/L
ND
1.00
0.320
05/28/19 15:13
Ethylbenzene
ug/L
ND
1.00
0.384
05/28/19 15:13
Hexachloro-1,3-butadiene
ug/L
ND
1.00
0.256
05/28/19 15:13
2-Hexanone
ug/L
ND
10.0
3.82
05/28/19 15:13
p-Isopropyltoluene
ug/L
ND
1.00
0.350
05/28/19 15:13
2-Butanone (MEK)
ug/L
ND
10.0
3.93
05/28/19 15:13
Methylene Chloride
ug/L
ND
5.00
1.00
05/28/19 15:13
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
METHOD BLANK: R3416175-3 Matrix: Water
Associated Lab Samples: 92429863001, 92429863002, 92429863003, 92429863004, 92429863005, 92429863007
Blank Reporting
Parameter Units Result Limit MDL Analyzed
4-Methyl-2-pentanone (MIBK)
ug/L
ND
10.0
2.14
05/28/19 15:13
Methyl-tert-butyl ether
ug/L
ND
1.00
0.367
05/28/19 15:13
Naphthalene
ug/L
ND
5.00
1.00
05/28/19 15:13
Styrene
ug/L
ND
1.00
0.307
05/28/19 15:13
1,1,1,2-Tetrachloroethane
ug/L
ND
1.00
0.385
05/28/19 15:13
1,1,2,2-Tetrachloroethane
ug/L
ND
1.00
0.130
05/28/19 15:13
Tetrachloroethene
ug/L
ND
1.00
0.372
05/28/19 15:13
Toluene
ug/L
ND
1.00
0.412
05/28/19 15:13
1,2,3-Trichlorobenzene
ug/L
ND
1.00
0.230
05/28/19 15:13
1,2,4-Trichlorobenzene
ug/L
ND
1.00
0.355
05/28/19 15:13
1,1,1-Trichloroethane
ug/L
ND
1.00
0.319
05/28/19 15:13
1,1,2-Trichloroethane
ug/L
ND
1.00
0.383
05/28/19 15:13
Trichloroethene
ug/L
ND
1.00
0.398
05/28/19 15:13
Trichlorofluoromethane
ug/L
ND
5.00
1.20
05/28/19 15:13
1,2,3-Trichloropropane
ug/L
ND
2.50
0.807
05/28/19 15:13
Vinyl acetate
ug/L
ND
10.0
1.63
05/28/19 15:13
Vinyl chloride
ug/L
ND
1.00
0.259
05/28/19 15:13
Xylene (Total)
ug/L
ND
3.00
1.06
05/28/19 15:13
o-Xylene
ug/L
ND
1.00
0.341
05/28/19 15:13
m&p-Xylene
ug/L
ND
2.00
0.719
05/28/19 15:13
1,4-Dioxane (p-Dioxane)
ug/L
ND
100
36.0
05/28/19 15:13
Toluene-d8 (S)
%
90.2
80.0-120
05/28/19 15:13
4-Bromofluorobenzene (S)
%
96.6
77.0-126
05/28/19 15:13
1,2-Dichloroethane-d4 (S)
%
86.2
70.0-130
05/28/19 15:13
LABORATORY CONTROL SAMPLE:
Parameter
R3416175-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Acetone
ug/L
125
143
114
19.0-160
Acrylonitrile
ug/L
125
149
120
55.0-149
Benzene
ug/L
25.0
26.7
107
70.0-123
Bromobenzene
ug/L
25.0
22.1
88.5
73.0-121
Bromodichloromethane
ug/L
25.0
27.3
109
75.0-120
Bromochloromethane
ug/L
25.0
23.8
95.3
76.0-122
Bromoform
ug/L
25.0
24.1
96.4
68.0-132
Bromomethane
ug/L
25.0
12.9
51.7
10.0-160
Carbon tetrachloride
ug/L
25.0
27.1
108
68.0-126
Chlorobenzene
ug/L
25.0
24.5
98.1
80.0-121
Dibromochloromethane
ug/L
25.0
24.7
99.0
77.0-125
Chloroethane
ug/L
25.0
23.1
92.3
47.0-150
Chloroform
ug/L
25.0
26.9
108
73.0-120
Chloromethane
ug/L
25.0
16.0
63.9
41.0-142
2-Chlorotoluene
ug/L
25.0
22.0
87.9
76.0-123
4-Chlorotoluene
ug/L
25.0
23.2
92.8
75.0-122
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
LABORATORY CONTROL SAMPLE:
Parameter
R3416175-1
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/L
25.0
22.4
89.6
58.0-134
1,2-Dibromoethane (EDB)
ug/L
25.0
25.1
100
80.0-122
Dibromomethane
ug/L
25.0
26.6
107
80.0-120
1,2-Dichlorobenzene
ug/L
25.0
24.4
97.6
79.0-121
1,3-Dichlorobenzene
ug/L
25.0
23.1
92.4
79.0-120
1,4-Dichlorobenzene
ug/L
25.0
22.6
90.6
79.0-120
Dichlorodifluoromethane
ug/L
25.0
27.7
111
51.0-149
1,1-Dichloroethane
ug/L
25.0
26.5
106
70.0-126
1,2-Dichloroethane
ug/L
25.0
24.7
98.9
70.0-128
1,1-Dichloroethene
ug/L
25.0
27.2
109
71.0-124
cis-1,2-Dichloroethene
ug/L
25.0
27.7
111
73.0-120
trans-1,2-Dichloroethene
ug/L
25.0
28.0
112
73.0-120
1,2-Dichloropropane
ug/L
25.0
26.9
107
77.0-125
1,1-Dichloropropene
ug/L
25.0
27.5
110
74.0-126
1,3-Dichloropropane
ug/L
25.0
25.2
101
80.0-120
cis-1,3-Dichloropropene
ug/L
25.0
28.1
112
80.0-123
trans- 1,3-Dichloropropene
ug/L
25.0
24.1
96.5
78.0-124
2,2-Dichloropropane
ug/L
25.0
25.5
102
58.0-130
Diisopropyl ether
ug/L
25.0
26.8
107
58.0-138
Ethylbenzene
ug/L
25.0
24.9
99.7
79.0-123
Hexachloro-1,3-butadiene
ug/L
25.0
20.4
81.7
54.0-138
2-Hexanone
ug/L
125
137
110
67.0-149
p-Isopropyltoluene
ug/L
25.0
21.8
87.4
76.0-125
2-Butanone (MEK)
ug/L
125
139
111
44.0-160
Methylene Chloride
ug/L
25.0
26.3
105
67.0-120
4-Methyl-2-pentanone (MIBK)
ug/L
125
126
100
68.0-142
Methyl-tert-butyl ether
ug/L
25.0
27.8
111
68.0-125
Naphthalene
ug/L
25.0
22.6
90.2
54.0-135
Styrene
ug/L
25.0
24.7
98.7
73.0-130
1,1,1,2-Tetrachloroethane
ug/L
25.0
24.6
98.4
75.0-125
1,1,2,2-Tetrachloroethane
ug/L
25.0
23.3
93.3
65.0-130
Tetrachloroethene
ug/L
25.0
25.5
102
72.0-132
Toluene
ug/L
25.0
23.7
94.7
79.0-120
1,2,3-Trichlorobenzene
ug/L
25.0
22.4
89.4
50.0-138
1,2,4-Trichlorobenzene
ug/L
25.0
23.2
92.9
57.0-137
1,1,1-Trichloroethane
ug/L
25.0
27.5
110
73.0-124
1,1,2-Trichloroethane
ug/L
25.0
24.2
96.9
80.0-120
Trichloroethene
ug/L
25.0
28.1
112
78.0-124
Trichlorofluoromethane
ug/L
25.0
28.7
115
59.0-147
1,2,3-Trichloropropane
ug/L
25.0
24.4
97.6
73.0-130
Vinyl acetate
ug/L
125
134
107
11.0-160
Vinyl chloride
ug/L
25.0
27.6
111
67.0-131
Xylene (Total)
ug/L
75.0
71.6
95.5
79.0-123
o-Xylene
ug/L
25.0
24.1
96.3
80.0-122
m&p-Xylene
ug/L
50.0
47.5
95.0
80.0-122
Toluene-d8 (S)
%
90.3
80.0-120
4-Bromofluorobenzene (S)
%
102
77.0-126
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
LABORATORY CONTROL SAMPLE: R3416175-1
Parameter Units
1,2-Dichloroethane-d4 (S) %
LABORATORY CONTROL SAMPLE:
R3416175-2
Parameter
Units
1,4-Dioxane (p-Dioxane)
ug/L
Toluene-d8 (S)
%
4-Bromofluorobenzene (S)
%
1,2-Dichloroethane-d4 (S)
%
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
100 70.0-130
Spike LCS
Conc. Result
1000 1100
LCS
% Rec
% Rec
Limits Qualifiers
110
13.0-160
90.6
80.0-120
100
77.0-126
86.4
70.0-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: SURRY MSWLF SWS
Pace Project No.: 92429863
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PAN Pace Analytical National
PASI-A Pace Analytical Services - Asheville
ANALYTE QUALIFIERS
CC The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The result may be biased.
LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
SR Surrogate recovery was below laboratory control limits. Results may be biased low.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 65

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
SURRY MSWLF SWS
Pace Project No.:
92429863
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92429863001
SW-1
EPA 3010A
478300
EPA 6010D
478326
92429863002
SW-2
EPA 3010A
478300
EPA 6010D
478326
92429863003
SW-3
EPA 3010A
478300
EPA 6010D
478326
92429863004
SW-4
EPA 3010A
478300
EPA 6010D
478326
92429863005
SWN-1
EPA 3010A
478300
EPA 6010D
478326
92429863006
SWN-2
EPA 3010A
478300
EPA 6010D
478326
92429863007
SW-C
EPA 3010A
478300
EPA 6010D
478326
92429863001
SW-1
EPA 3010A
478331
EPA 6020B
478572
92429863002
SW-2
EPA 3010A
478331
EPA 6020B
478572
92429863003
SW-3
EPA 3010A
478331
EPA 6020B
478572
92429863004
SW-4
EPA 3010A
478331
EPA 6020B
478572
92429863005
SWN-1
EPA 3010A
478331
EPA 6020B
478572
92429863006
SWN-2
EPA 3010A
478331
EPA 6020B
478572
92429863007
SW-C
EPA 3010A
478331
EPA 6020B
478572
92429863001
SW-1
8260D
1287536
EPA 8260D
1287536
92429863002
SW-2
8260D
1287536
EPA 8260D
1287536
92429863003
SW-3
8260D
1287536
EPA 8260D
1287536
92429863004
SW-4
8260D
1287536
EPA 8260D
1287536
92429863005
SWN-1
8260D
1287536
EPA 8260D
1287536
92429863006
SWN-2
8260D
1287157
EPA 8260D
1287157
92429863007
SW-C
8260D
1287536
EPA 8260D
1287536
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/05/2019 02:15 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 65

m
aeeAnalyfic
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.,
F•CAR-CS-033•itev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[:]Greenwood ❑ Huntersville 2--'Raleigh[] Methanitsville❑
Client Name: Wp# : 92429863
Upon Receipt P��d YI ii,` . ad L Y)c��C� .
Project i3
Courier: Fe Ex i []UPS /❑USPS❑Client
Commercial ace ❑Other: 92429653
� �
Custody Seal Present? []Yes No Seals Intact? []Yes la '
{late/Initials Person Examining Content d:- f 5 7C
Packing Material: ❑Bubble Wrap 081bble Bags ❑None ❑ Other Biological Tissue Frozen?
Therrrtomete►: [-]yes 2 o ❑N/A
1A Gun ID:
92Ta48 Type of ice: let ❑Blue ❑None
Cooler Temp ('Q: Correction Factor: Add/Subtract (°C) 0.0
� Temp should be above freezing to 6°C
Cooler Temp Corrected ('C): �' ! ❑5amples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (ZJ/N/A, water sample)
Did samples on - to in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
I—IVPa YINo including Hawaii and Puerto R1col7 ❑Yes ❑No
Comments/Discrepancy:
Chain of Custody Present?
Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
ON.
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
Oyes
Mo
❑NJA
3.
Rush Turn Around Time Requested?
❑Oyes.No
❑N/A
4,
Sufficient Volume?
BY.
❑Na
❑NJA
S.
Correct Containers Used?
41
ON.
[-]NIA
6.
-Pace Containers Used?
[]]Yes
❑No
❑N/A
Containers Intact?
0 e5
ON.
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
Z`NJA
S.
Sample Labels Match COC?
ZYes
❑No
❑NJA
9.
-includes Date/Time/ID/Analysis Matrix:
Headspace in VDA Vials (?5-6mm)?
❑Yes
0 Ca
❑NJA
10.
Trip Blank Present?
❑Yes
o
❑NJA
11.
Trip Blank Custody Seals Present?
❑Yes
❑No
❑K/
COMMENTS/SAMPLE DISCREPANCY Field Data Required? []Yes ❑No
CZ
Lot ID of split containers:
CLII NT NOT IFICATION/RESOLUTION
Person contacted: JpiaAtf a I ') ►l_l Date/Time: �uT ffig- I—[ "f
r_
Project Manager SCURF Review: Y
Project Manager SRF Review:
Date: 1� ` I '1
Date:- 1 _-( Pf
Page 32 of 65

Document Name:
Document Revised: February 7, 2013
a
aceAnalytical
Sample Condition Upon Receipti[SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-0-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
WO#:92429863
PM: AMB Due Date: 06/0 14/ 9
CLIENT: 92-Municipal
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot d
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina ❑EHNR Certification Office (i.e.
out of hold, incorrect preservative, out of temp, incorrect containers.
Page 33 of 65

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Page 34 of 65

aceAnal ical ° A f �l A L Y T CAL REPORT
National Center for Testing & Innovation May 30, 2019
FTc
FSS
Pace Analytical - Huntersville, NC
Sample Delivery Group: L1101602 [Cn]
Samples Received: 05/22/2019 FrProject Number: 92429863
Description: SURRY MSWLF SWS FC
Site: 001
GI
Report To: Angela Baioni
9800 Kincey Avenue, Suite 100 rAl
Huntersville, NC 28078
Fc
Entire Report Reviewed By: �vUnn �v, �. L
L111-�
Nancy McLain
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National
is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. i
41
Page 35 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913.43 1 of 31
A

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
SW-1 L1101602-01
SW-2 L1101602-02
SW-3 L1101602-03
SW-4 L1101602-04
SWN-1 L1101602-05
SWN-2 L1101602-06
SW-C L1101602-07
Qc: Quality Control Summary
Volatile Organic Compounds (GC/MS) by Method 8260D
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
CID
2
3
4
FS5
5
[Cn]
7
9
Fr
11
13
RC
15
�GI
17
19
rAI
19
27
FSC
28
29
Page 36 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92429863 L1101602 05/30/1913:43 2 of 31

SAMPLE
SUMMARY
ONE LAB. NATIONWIDE.
Collected by
Collected date/time
Received date/time
SW-1 L1101602-01 GW
05/17/1911:19
05/22/19 08:45
FP1
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
FTC
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287536
1
05/28/1917:15
05/28/1917:15
DWR Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
M
SW-2 L1101602-02 GW
05/17/1912:00
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
[Cn]
date/time
date/time
Organic Compounds (GC/MS) by Method 8260D
WG1287536
1
05/28/1917:35
05/28/1917:35
DWR Mt. Juliet, TN
FSrVolatile
Collected by
Collected date/time
Received date/time
6QC
SW-3 L1101602-03 GW
05/17/1914:35
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
GI
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287536
1
05/28/1917:55
05/28/1917:55
DWR Mt. Juliet, TN
FAI
Collected by
Collected date/time
Received date/time
SW-4 L1101602-04 GW
05/17/1916:15
05/22/1908:45
FSC
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287536
1
05/28/1918:15
05/28/1918:15
DWR Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
SWN-1 L1101602-05 GW
05/17/1915:34
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287536
1
05/28/1918:35
05/28/1918:35
DWR Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
SWN-2 L1101602-06 GW
05/17/1916:53
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287157
1
05/28/1911:10
05/28/1911:10
BMB Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
SW-C L1101602-07 GW
05/17/19 08:43
05/22/19 08:45
Method
Batch
Dilution
Preparation
Analysis
Analyst Location
date/time
date/time
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1287536
1
05/28/1918:55
05/28/1918:55
DWR Mt. Juliet, TN
Page 37 of 65
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC
92429863
L1101602
05/30/1913:43 3 of 31

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
VV VV� � �t La�'_
Nancy McLain
Project Manager
FP1
FTC
FSS
FSr
FC-1
F,
FAI
FSC
Page 38 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92429863 L1101602 05/30/1913:43 4 of 31

SW-1 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 11:19 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 17:15
WG1287536
Acrylonitrile
U
1.87
10.0
1 05/28/2019 17:15
WG1287536
Benzene
U
0.331
1.00
1 05/28/2019 17:15
WG1287536
Bromobenzene
U
0.352
1.00
1 05/28/2019 17:15
WG1287536
Bromochloromethane
U
0.520
5.00
1 05/28/2019 17:15
WG1287536
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 17:15
WG1287536
Bromoform
U
0.469
1.00
1 05/28/2019 17:15
WG1287536
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 17:15
WG1287536
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 17:15
WG1287536
Chlorobenzene
U
0.348
1.00
1 05/28/2019 17:15
WG1287536
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 17:15
WG1287536
Chloroethane
U
0.453
5.00
1 05/28/2019 17:15
WG1287536
Chloroform
U
0.324
5.00
1 05/28/2019 17:15
WG1287536
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 17:15
WG1287536
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 17:15
WG1287536
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 17:15
WG1287536
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 17:15
WG1287536
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 17:15
WG1287536
Dibromomethane
U
0.346
1.00
1 05/28/2019 17:15
WG1287536
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 17:15
WG1287536
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 17:15
WG1287536
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 17:15
WG1287536
Dichlorodifluoromethane
U
0.551
5.00
1 05/28/2019 17:15
WG1287536
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 17:15
WG1287536
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 17:15
WG1287536
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 17:15
WG1287536
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 17:15
WG1287536
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 17:15
WG1287536
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 17:15
WG1287536
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 17:15
WG1287536
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 17:15
WG1287536
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 17:15
WG1287536
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 17:15
WG1287536
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 17:15
WG1287536
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 17:15
WG1287536
Ethylbenzene
U
0.384
1.00
1 05/28/2019 17:15
WG1287536
Hexachloro-1,3-butadiene
U
J0
0.256
1.00
1 05/28/2019 17:15
WG1287536
2-Hexanone
U
3.82
10.0
1 05/28/2019 17:15
WG1287536
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 17:15
WG1287536
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 17:15
WG1287536
Methylene Chloride
U
1.00
5.00
1 05/28/2019 17:15
WG1287536
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 17:15
WG1287536
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 17:15
WG1287536
Naphthalene
U
1.00
5.00
1 05/28/2019 17:15
WG1287536
Styrene
U
0.307
1.00
1 05/28/2019 17:15
WG1287536
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 17:15
WG1287536
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 17:15
WG1287536
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 17:15
WG1287536
Toluene
U
0.412
1.00
1 05/28/2019 17:15
WG1287536
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 17:15
WG1287536
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 17:15
WG1287536
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 17:15
WG1287536
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 17:15
WG1287536
Trichloroethene
U
0.398
1.00
1 05/28/2019 17:15
WG1287536
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 17:15
WG1287536
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 17:15
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 39 of 65
PAGE:
5 of 31

ONE LAB. NATIONWIDE.
SW-1 SAMPLE RESULTS - 01
Collected date/time: 05/17/19 11:19 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201917:15
WG1287536
Vinyl chloride
U
0.259
1.00
1 05/28/201917:15
WG1287536
o-Xylene
U
0.341
1.00
1 05/28/201917:15
WG1287536
m&p-Xylene
U
0.719
2.00
1 05/28/201917:15
WG1287536
Xylenes, Total
U
1.06
3.00
1 05/28/201917:15
WG1287536
1,4-Dioxane
U
36.0
100
1 05/28/201917:15
WG1287536
(S) Toluene-d8
90.3
80.0-120
051281201917.75
WG1287536
(S 4-Bromof/uorobenzene
98.3
77.0-126
051281201917.75
WG1287536
(S 1,2-Dich/oroethane-d4
88.6
70.0-130
0512812019 17.75
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 40 of 65
PAGE:
6 of 31

SW-2 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 12:00 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/201917:35
WG1287536
Acrylonitrile
U
1.87
10.0
1 05/28/201917:35
WG1287536
Benzene
U
0.331
1.00
1 05/28/201917:35
WG1287536
Bromobenzene
U
0.352
1.00
1 05/28/201917:35
WG1287536
Bromochloromethane
U
0.520
5.00
1 05/28/201917:35
WG1287536
Bromodichloromethane
U
0.380
1.00
1 05/28/201917:35
WG1287536
Bromoform
U
0.469
1.00
1 05/28/201917:35
WG1287536
Bromomethane
U
J0
0.866
5.00
1 05/28/201917:35
WG1287536
Carbon tetrachloride
U
0.379
1.00
1 05/28/201917:35
WG1287536
Chlorobenzene
U
0.348
1.00
1 05/28/201917:35
WG1287536
Chlorodibromomethane
U
0.327
1.00
1 05/28/201917:35
WG1287536
Chloroethane
U
0.453
5.00
1 05/28/201917:35
WG1287536
Chloroform
U
0.324
5.00
1 05/28/201917:35
WG1287536
Chloromethane
U
J0
0.276
2.50
1 05/28/201917:35
WG1287536
2-Chlorotoluene
U
0.375
1.00
1 05/28/201917:35
WG1287536
4-Chlorotoluene
U
0.351
1.00
1 05/28/201917:35
WG1287536
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/201917:35
WG1287536
1,2-Dibromoethane
U
0.381
1.00
1 05/28/201917:35
WG1287536
Dibromomethane
U
0.346
1.00
1 05/28/201917:35
WG1287536
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/201917:35
WG1287536
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/201917:35
WG1287536
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 17:35
WG1287536
Dichlorodifluoromethane
U
0.551
5.00
1 05/28/201917:35
WG1287536
1,1-Dichloroethane
U
0.259
1.00
1 05/28/201917:35
WG1287536
1,2-Dichloroethane
U
0.361
1.00
1 05/28/201917:35
WG1287536
1,1-Dichloroethene
U
0.398
1.00
1 05/28/201917:35
WG1287536
cis-1,2-Dichloroethene
4.53
0.260
1.00
1 05/28/201917:35
WG1287536
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/201917:35
WG1287536
1,2-Dichloropropane
U
0.306
1.00
1 05/28/201917:35
WG1287536
1,1-Dichloropropene
U
0.352
1.00
1 05/28/201917:35
WG1287536
1,3-Dichloropropane
U
0.366
1.00
1 05/28/201917:35
WG1287536
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/201917:35
WG1287536
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/201917:35
WG1287536
2,2-Dichloropropane
U
0.321
1.00
1 05/28/201917:35
WG1287536
Di -isopropyl ether
U
0.320
1.00
1 05/28/201917:35
WG1287536
Ethylbenzene
U
0.384
1.00
1 05/28/201917:35
WG1287536
Hexachloro-1,3-butadiene
U
J0
0.256
1.00
1 05/28/201917:35
WG1287536
2-Hexanone
U
3.82
10.0
1 05/28/201917:35
WG1287536
p-Isopropyltoluene
U
0.350
1.00
1 05/28/201917:35
WG1287536
2-Butanone (MEK)
U
3.93
10.0
1 05/28/201917:35
WG1287536
Methylene Chloride
U
1.00
5.00
1 05/28/201917:35
WG1287536
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/201917:35
WG1287536
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/201917:35
WG1287536
Naphthalene
U
1.00
5.00
1 05/28/201917:35
WG1287536
Styrene
U
0.307
1.00
1 05/28/201917:35
WG1287536
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/201917:35
WG1287536
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/201917:35
WG1287536
Tetrachloroethene
U
0.372
1.00
1 05/28/201917:35
WG1287536
Toluene
U
0.412
1.00
1 05/28/201917:35
WG1287536
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/201917:35
WG1287536
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/201917:35
WG1287536
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/201917:35
WG1287536
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/201917:35
WG1287536
Trichloroethene
U
0.398
1.00
1 05/28/201917:35
WG1287536
Trichlorofluoromethane
U
1.20
5.00
1 05/28/201917:35
WG1287536
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/201917:35
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 41 of 65
PAGE:
7of31

ONE LAB. NATIONWIDE.
SW-2 SAMPLE RESULTS - 02
Collected date/time: 05/17/19 12:00 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201917:35
WG1287536
Vinyl chloride
1.08
0.259
1.00
1 05/28/201917:35
WG1287536
o-Xylene
IJ
0.341
1.00
1 05/28/201917:35
WG1287536
m&p-Xylene
U
0.719
2.00
1 05/28/201917:35
WG1287536
Xylenes, Total
IJ
1.06
3.00
1 05/28/201917:35
WG1287536
1,4-Dioxane
U
36.0
100
1 05/28/201917:35
WG1287536
(S) Toluene-d8
91.3
80.0-120
051281201917.35
WG1287536
(S 4-Bromof/uorobenzene
100
77.0-126
051281201917.35
WG1287536
(S) 1,2-Dich/oroethane-d4
88.0
70.0-130
0512812019 17.35
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 42 of 65
PAGE:
8 of 31

SW-3 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 14:35 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 17:55
WG1287536
Acrylonitrile
U
1.87
10.0
1 05/28/2019 17:55
WG1287536
Benzene
U
0.331
1.00
1 05/28/2019 17:55
WG1287536
Bromobenzene
U
0.352
1.00
1 05/28/2019 17:55
WG1287536
Bromochloromethane
U
0.520
5.00
1 05/28/2019 17:55
WG1287536
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 17:55
WG1287536
Bromoform
U
0.469
1.00
1 05/28/2019 17:55
WG1287536
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 17:55
WG1287536
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 17:55
WG1287536
Chlorobenzene
U
0.348
1.00
1 05/28/2019 17:55
WG1287536
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 17:55
WG1287536
Chloroethane
U
0.453
5.00
1 05/28/2019 17:55
WG1287536
Chloroform
U
0.324
5.00
1 05/28/2019 17:55
WG1287536
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 17:55
WG1287536
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 17:55
WG1287536
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 17:55
WG1287536
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 17:55
WG1287536
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 17:55
WG1287536
Dibromomethane
U
0.346
1.00
1 05/28/2019 17:55
WG1287536
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 17:55
WG1287536
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 17:55
WG1287536
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 17:55
WG1287536
Dichlorodifluoromethane
U
0.551
5.00
1 05/28/2019 17:55
WG1287536
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 17:55
WG1287536
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 17:55
WG1287536
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 17:55
WG1287536
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 17:55
WG1287536
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 17:55
WG1287536
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 17:55
WG1287536
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 17:55
WG1287536
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 17:55
WG1287536
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 17:55
WG1287536
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 17:55
WG1287536
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 17:55
WG1287536
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 17:55
WG1287536
Ethylbenzene
U
0.384
1.00
1 05/28/2019 17:55
WG1287536
Hexachloro-1,3-butadiene
U
J0
0.256
1.00
1 05/28/2019 17:55
WG1287536
2-Hexanone
U
3.82
10.0
1 05/28/2019 17:55
WG1287536
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 17:55
WG1287536
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 17:55
WG1287536
Methylene Chloride
U
1.00
5.00
1 05/28/2019 17:55
WG1287536
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 17:55
WG1287536
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 17:55
WG1287536
Naphthalene
U
1.00
5.00
1 05/28/2019 17:55
WG1287536
Styrene
U
0.307
1.00
1 05/28/2019 17:55
WG1287536
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 17:55
WG1287536
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 17:55
WG1287536
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 17:55
WG1287536
Toluene
U
0.412
1.00
1 05/28/2019 17:55
WG1287536
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 17:55
WG1287536
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 17:55
WG1287536
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 17:55
WG1287536
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 17:55
WG1287536
Trichloroethene
U
0.398
1.00
1 05/28/2019 17:55
WG1287536
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 17:55
WG1287536
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 17:55
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 43 of 65
PAGE:
9 of 31

ONE LAB. NATIONWIDE.
SW-3 SAMPLE RESULTS - 03
Collected date/time: 05/17/19 14:35 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201917:55
WG1287536
Vinyl chloride
U
0.259
1.00
1 05/28/201917:55
WG1287536
o-Xylene
U
0.341
1.00
1 05/28/201917:55
WG1287536
m&p-Xylene
U
0.719
2.00
1 05/28/201917:55
WG1287536
Xylenes, Total
U
1.06
3.00
1 05/28/201917:55
WG1287536
1,4-Dioxane
U
36.0
100
1 05/28/2019 17:55
WG1287536
(S) Toluene-d8
92.6
80.0-120
051281201917:55
WG1287536
(S 4-Bromof/uorobenzene
102
77.0-126
051281201917:55
WG1287536
(S 1,2-Dich/oroethane-d4
89.2
70.0-130
0512812019 17:55
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 44 of 65
PAGE:
10 of 31

SW-4 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 16:15 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 18:15
WG1287536
Acrylonitrile
U
1.87
10.0
1 05/28/2019 18:15
WG1287536
Benzene
U
0.331
1.00
1 05/28/2019 18:15
WG1287536
Bromobenzene
U
0.352
1.00
1 05/28/2019 18:15
WG1287536
Bromochloromethane
U
0.520
5.00
1 05/28/2019 18:15
WG1287536
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 18:15
WG1287536
Bromoform
U
0.469
1.00
1 05/28/2019 18:15
WG1287536
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 18:15
WG1287536
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 18:15
WG1287536
Chlorobenzene
U
0.348
1.00
1 05/28/2019 18:15
WG1287536
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 18:15
WG1287536
Chloroethane
U
0.453
5.00
1 05/28/2019 18:15
WG1287536
Chloroform
U
0.324
5.00
1 05/28/2019 18:15
WG1287536
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 18:15
WG1287536
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 18:15
WG1287536
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 18:15
WG1287536
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 18:15
WG1287536
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 18:15
WG1287536
Dibromomethane
U
0.346
1.00
1 05/28/2019 18:15
WG1287536
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 18:15
WG1287536
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 18:15
WG1287536
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 18:15
WG1287536
Dichlorodifluoromethane
U
0.551
5.00
1 05/28/2019 18:15
WG1287536
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 18:15
WG1287536
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 18:15
WG1287536
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 18:15
WG1287536
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 18:15
WG1287536
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 18:15
WG1287536
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 18:15
WG1287536
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 18:15
WG1287536
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 18:15
WG1287536
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 18:15
WG1287536
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 18:15
WG1287536
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 18:15
WG1287536
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 18:15
WG1287536
Ethylbenzene
U
0.384
1.00
1 05/28/2019 18:15
WG1287536
Hexachloro-1,3-butadiene
U
J0
0.256
1.00
1 05/28/2019 18:15
WG1287536
2-Hexanone
U
3.82
10.0
1 05/28/2019 18:15
WG1287536
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 18:15
WG1287536
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 18:15
WG1287536
Methylene Chloride
U
1.00
5.00
1 05/28/2019 18:15
WG1287536
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 18:15
WG1287536
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 18:15
WG1287536
Naphthalene
U
1.00
5.00
1 05/28/2019 18:15
WG1287536
Styrene
U
0.307
1.00
1 05/28/2019 18:15
WG1287536
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 18:15
WG1287536
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 18:15
WG1287536
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 18:15
WG1287536
Toluene
U
0.412
1.00
1 05/28/2019 18:15
WG1287536
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 18:15
WG1287536
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 18:15
WG1287536
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 18:15
WG1287536
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 18:15
WG1287536
Trichloroethene
U
0.398
1.00
1 05/28/2019 18:15
WG1287536
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 18:15
WG1287536
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 18:15
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 45 of 65
PAGE:
11 of 31

ONE LAB. NATIONWIDE.
SW-4 SAMPLE RESULTS - 04
Collected date/time: 05/17/19 16:15 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201918:15
WG1287536
Vinyl chloride
U
0.259
1.00
1 05/28/201918:15
WG1287536
o-Xylene
U
0.341
1.00
1 05/28/2019 18:15
WG1287536
m&p-Xylene
U
0.719
2.00
1 05/28/201918:15
WG1287536
Xylenes, Total
U
1.06
3.00
1 05/28/201918:15
WG1287536
1,4-Dioxane
U
36.0
100
1 05/28/201918:15
WG1287536
(S) Toluene-d8
89.0
80.0-120
051281201918.15
WG1287536
(S) 4-Bromof/uorobenzene
99.5
77.0-126
051281201918.15
WG1287536
(S 1,2-Dich/oroethane-d4
86.5
70.0-130
0512812019 18.15
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, INC
92429863
L1101602
05/30/1913:43
Fp
FTc
FS
Fn
N
Fc
F,
FAI
FSC
Page 46 of 65
PAGE:
12 of 31

S W N -1 SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 15:34 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 18:35
WG1287536
Acrylonitrile
U
1.87
10.0
1 05/28/2019 18:35
WG1287536
Benzene
U
0.331
1.00
1 05/28/2019 18:35
WG1287536
Bromobenzene
U
0.352
1.00
1 05/28/2019 18:35
WG1287536
Bromochloromethane
U
0.520
5.00
1 05/28/2019 18:35
WG1287536
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 18:35
WG1287536
Bromoform
U
0.469
1.00
1 05/28/2019 18:35
WG1287536
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 18:35
WG1287536
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 18:35
WG1287536
Chlorobenzene
U
0.348
1.00
1 05/28/2019 18:35
WG1287536
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 18:35
WG1287536
Chloroethane
U
0.453
5.00
1 05/28/2019 18:35
WG1287536
Chloroform
U
0.324
5.00
1 05/28/2019 18:35
WG1287536
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 18:35
WG1287536
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 18:35
WG1287536
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 18:35
WG1287536
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 18:35
WG1287536
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 18:35
WG1287536
Dibromomethane
U
0.346
1.00
1 05/28/2019 18:35
WG1287536
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 18:35
WG1287536
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 18:35
WG1287536
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 18:35
WG1287536
Dichlorodifluoromethane
U
0.551
5.00
1 05/28/2019 18:35
WG1287536
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 18:35
WG1287536
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 18:35
WG1287536
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 18:35
WG1287536
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 18:35
WG1287536
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 18:35
WG1287536
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 18:35
WG1287536
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 18:35
WG1287536
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 18:35
WG1287536
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 18:35
WG1287536
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 18:35
WG1287536
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 18:35
WG1287536
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 18:35
WG1287536
Ethylbenzene
U
0.384
1.00
1 05/28/2019 18:35
WG1287536
Hexachloro-1,3-butadiene
U
J0
0.256
1.00
1 05/28/2019 18:35
WG1287536
2-Hexanone
U
3.82
10.0
1 05/28/2019 18:35
WG1287536
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 18:35
WG1287536
2-Butanone (MEK)
U
3.93
10.0
1 05/28/2019 18:35
WG1287536
Methylene Chloride
U
1.00
5.00
1 05/28/2019 18:35
WG1287536
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 18:35
WG1287536
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 18:35
WG1287536
Naphthalene
U
1.00
5.00
1 05/28/2019 18:35
WG1287536
Styrene
U
0.307
1.00
1 05/28/2019 18:35
WG1287536
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 18:35
WG1287536
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 18:35
WG1287536
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 18:35
WG1287536
Toluene
U
0.412
1.00
1 05/28/2019 18:35
WG1287536
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 18:35
WG1287536
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 18:35
WG1287536
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 18:35
WG1287536
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 18:35
WG1287536
Trichloroethene
U
0.398
1.00
1 05/28/2019 18:35
WG1287536
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 18:35
WG1287536
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 18:35
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 47 of 65
PAGE:
13 of 31

ONE LAB. NATIONWIDE.
SWN-1 SAMPLE RESULTS - 05
Collected date/time: 05/17/19 15:34 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
Result
ug/I
Qualifier MDL
ug/I
RDL
ug/I
Dilution Analysis
date / time
Batch
Vinyl acetate
U
1.63
10.0
1 05/28/201918:35
WG1287536
Vinyl chloride
U
0.259
1.00
1 05/28/201918:35
WG1287536
o-Xylene
U
0.341
1.00
1 05/28/2019 18:35
WG1287536
m&p-Xylene
U
0.719
2.00
1 05/28/201918:35
WG1287536
Xylenes, Total
U
1.06
3.00
1 05/28/201918:35
WG1287536
1,4-Dioxane
U
36.0
100
1 05/28/201918:35
WG1287536
(S) Toluene-d8
98.2
80.0-120
051281201918:35
WG1287536
(S) 4-Bromof/uorobenzene
84.2
77.0-126
051281201918.35
WG1287536
(S)1,2-Dich/oroethane-d4
69.7
J2
70.0-130
051281201918:35
WG1287536
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 48 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43 14 of 31

S W N- 2 SAMPLE RESULTS - 06 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 16:53 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/201911:10
WG1287157
Acrylonitrile
U
1.87
10.0
1 05/28/201911:10
WG1287157
Benzene
U
0.331
1.00
1 05/28/201911:10
WG1287157
Bromobenzene
U
0.352
1.00
1 05/28/201911:10
WG1287157
Bromochloromethane
U
0.520
5.00
1 05/28/201911:10
WG1287157
Bromodichloromethane
U
0.380
1.00
1 05/28/201911:10
WG1287157
Bromoform
U
0.469
1.00
1 05/28/201911:10
WG1287157
Bromomethane
U
J0
0.866
5.00
1 05/28/201911:10
WG1287157
Carbon tetrachloride
U
0.379
1.00
1 05/28/201911:10
WG1287157
Chlorobenzene
U
0.348
1.00
1 05/28/201911:10
WG1287157
Chlorodibromomethane
U
0.327
1.00
1 05/28/201911:10
WG1287157
Chloroethane
U
0.453
5.00
1 05/28/201911:10
WG1287157
Chloroform
U
0.324
5.00
1 05/28/201911:10
WG1287157
Chloromethane
U
J0
0.276
2.50
1 05/28/201911:10
WG1287157
2-Chlorotoluene
U
0.375
1.00
1 05/28/201911:10
WG1287157
4-Chlorotoluene
U
0.351
1.00
1 05/28/201911:10
WG1287157
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/201911:10
WG1287157
1,2-Dibromoethane
U
0.381
1.00
1 05/28/201911:10
WG1287157
Dibromomethane
U
0.346
1.00
1 05/28/201911:10
WG1287157
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/201911:10
WG1287157
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/201911:10
WG1287157
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/201911:10
WG1287157
Dichlorodifluoromethane
U
J4
0.551
5.00
1 05/28/201911:10
WG1287157
1,1-Dichloroethane
U
0.259
1.00
1 05/28/201911:10
WG1287157
1,2-Dichloroethane
U
0.361
1.00
1 05/28/201911:10
WG1287157
1,1-Dichloroethene
U
0.398
1.00
1 05/28/201911:10
WG1287157
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/201911:10
WG1287157
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/201911:10
WG1287157
1,2-Dichloropropane
U
0.306
1.00
1 05/28/201911:10
WG1287157
1,1-Dichloropropene
U
0.352
1.00
1 05/28/201911:10
WG1287157
1,3-Dichloropropane
U
0.366
1.00
1 05/28/201911:10
WG1287157
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/201911:10
WG1287157
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/201911:10
WG1287157
2,2-Dichloropropane
U
0.321
1.00
1 05/28/201911:10
WG1287157
Di -isopropyl ether
U
0.320
1.00
1 05/28/201911:10
WG1287157
Ethylbenzene
U
0.384
1.00
1 05/28/201911:10
WG1287157
Hexachloro-1,3-butadiene
U
0.256
1.00
1 05/28/201911:10
WG1287157
2-Hexanone
U
3.82
10.0
1 05/28/201911:10
WG1287157
p-Isopropyltoluene
U
0.350
1.00
1 05/28/201911:10
WG1287157
2-Butanone (MEK)
U
3.93
10.0
1 05/28/201911:10
WG1287157
Methylene Chloride
U
1.00
5.00
1 05/28/201911:10
WG1287157
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/201911:10
WG1287157
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/201911:10
WG1287157
Naphthalene
U
1.00
5.00
1 05/28/201911:10
WG1287157
Styrene
U
0.307
1.00
1 05/28/201911:10
WG1287157
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/201911:10
WG1287157
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/201911:10
WG1287157
Tetrachloroethene
U
0.372
1.00
1 05/28/201911:10
WG1287157
Toluene
U
0.412
1.00
1 05/28/201911:10
WG1287157
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/201911:10
WG1287157
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/201911:10
WG1287157
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/201911:10
WG1287157
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/201911:10
WG1287157
Trichloroethene
U
0.398
1.00
1 05/28/201911:10
WG1287157
Trichlorofluoromethane
U
1.20
5.00
1 05/28/201911:10
WG1287157
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/201911:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 49 of 65
PAGE:
15 of 31

ONE LAB. NATIONWIDE.
SWN-2 SAMPLE RESULTS - 06
Collected date/time: 05/17/19 16:53 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201911:10
WG1287157
Vinyl chloride
U
0.259
1.00
1 05/28/201911:10
WG1287157
o-Xylene
U
0.341
1.00
1 05/28/201911:10
WG1287157
m&p-Xylene
U
0.719
2.00
1 05/28/201911:10
WG1287157
Xylenes, Total
U
1.06
3.00
1 05/28/201911:10
WG1287157
1,4-Dioxane
U
36.0
100
1 05/28/201911:10
WG1287157
(S Toluene-d8
91.8
80.0-120
051281201911:10
WG1287157
(S 4-Bromof/uorobenzene
102
77.0-126
051281201911:10
WG1287157
(S 1,2-Dich/oroethane-d4
89.1
70.0-130
051281201911:10
WG1287157
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 50 of 65
PAGE:
16 of 31

SW-C SAMPLE RESULTS - 07 ONE LAB. NATIONWIDE.
Collected date/time: 05/17/19 08:43 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Acetone
U
10.0
50.0
1 05/28/2019 18:55
WG1287536
Acrylonitrile
U
1.87
10.0
1 05/28/2019 18:55
WG1287536
Benzene
U
0.331
1.00
1 05/28/2019 18:55
WG1287536
Bromobenzene
U
0.352
1.00
1 05/28/2019 18:55
WG1287536
Bromochloromethane
U
0.520
5.00
1 05/28/2019 18:55
WG1287536
Bromodichloromethane
U
0.380
1.00
1 05/28/2019 18:55
WG1287536
Bromoform
U
0.469
1.00
1 05/28/2019 18:55
WG1287536
Bromomethane
U
J0
0.866
5.00
1 05/28/2019 18:55
WG1287536
Carbon tetrachloride
U
0.379
1.00
1 05/28/2019 18:55
WG1287536
Chlorobenzene
U
0.348
1.00
1 05/28/2019 18:55
WG1287536
Chlorodibromomethane
U
0.327
1.00
1 05/28/2019 18:55
WG1287536
Chloroethane
U
0.453
5.00
1 05/28/2019 18:55
WG1287536
Chloroform
U
0.324
5.00
1 05/28/2019 18:55
WG1287536
Chloromethane
U
J0
0.276
2.50
1 05/28/2019 18:55
WG1287536
2-Chlorotoluene
U
0.375
1.00
1 05/28/2019 18:55
WG1287536
4-Chlorotoluene
U
0.351
1.00
1 05/28/2019 18:55
WG1287536
1,2-Dibromo-3-Chloropropane
U
1.33
5.00
1 05/28/2019 18:55
WG1287536
1,2-Dibromoethane
U
0.381
1.00
1 05/28/2019 18:55
WG1287536
Dibromomethane
U
0.346
1.00
1 05/28/2019 18:55
WG1287536
1,2-Dichlorobenzene
U
0.349
1.00
1 05/28/2019 18:55
WG1287536
1,3-Dichlorobenzene
U
0.220
1.00
1 05/28/2019 18:55
WG1287536
1,4-Dichlorobenzene
U
0.274
1.00
1 05/28/2019 18:55
WG1287536
Dichlorodifluoromethane
U
0.551
5.00
1 05/28/2019 18:55
WG1287536
1,1-Dichloroethane
U
0.259
1.00
1 05/28/2019 18:55
WG1287536
1,2-Dichloroethane
U
0.361
1.00
1 05/28/2019 18:55
WG1287536
1,1-Dichloroethene
U
0.398
1.00
1 05/28/2019 18:55
WG1287536
cis-1,2-Dichloroethene
U
0.260
1.00
1 05/28/2019 18:55
WG1287536
trans-1,2-Dichloroethene
U
0.396
1.00
1 05/28/2019 18:55
WG1287536
1,2-Dichloropropane
U
0.306
1.00
1 05/28/2019 18:55
WG1287536
1,1-Dichloropropene
U
0.352
1.00
1 05/28/2019 18:55
WG1287536
1,3-Dichloropropane
U
0.366
1.00
1 05/28/2019 18:55
WG1287536
cis-1,3-Dichloropropene
U
0.418
1.00
1 05/28/2019 18:55
WG1287536
trans-1,3-Dichloropropene
U
0.419
1.00
1 05/28/2019 18:55
WG1287536
2,2-Dichloropropane
U
0.321
1.00
1 05/28/2019 18:55
WG1287536
Di -isopropyl ether
U
0.320
1.00
1 05/28/2019 18:55
WG1287536
Ethylbenzene
U
0.384
1.00
1 05/28/2019 18:55
WG1287536
Hexachloro-1,3-butadiene
U
J0
0.256
1.00
1 05/28/2019 18:55
WG1287536
2-Hexanone
U
3.82
10.0
1 05/28/2019 18:55
WG1287536
p-Isopropyltoluene
U
0.350
1.00
1 05/28/2019 18:55
WG1287536
2-Butanone(MEK)
U
3.93
10.0
1 05/28/2019 18:55
WG1287536
Methylene Chloride
U
1.00
5.00
1 05/28/2019 18:55
WG1287536
4-Methyl-2-pentanone (MIBK)
U
2.14
10.0
1 05/28/2019 18:55
WG1287536
Methyl tert-butyl ether
U
0.367
1.00
1 05/28/2019 18:55
WG1287536
Naphthalene
U
1.00
5.00
1 05/28/2019 18:55
WG1287536
Styrene
U
0.307
1.00
1 05/28/2019 18:55
WG1287536
1,1,1,2-Tetrachloroethane
U
0.385
1.00
1 05/28/2019 18:55
WG1287536
1,1,2,2-Tetrachloroethane
U
0.130
1.00
1 05/28/2019 18:55
WG1287536
Tetrachloroethene
U
0.372
1.00
1 05/28/2019 18:55
WG1287536
Toluene
U
0.412
1.00
1 05/28/2019 18:55
WG1287536
1,2,3-Trichlorobenzene
U
0.230
1.00
1 05/28/2019 18:55
WG1287536
1,2,4-Trichlorobenzene
U
0.355
1.00
1 05/28/2019 18:55
WG1287536
1,1,1-Trichloroethane
U
0.319
1.00
1 05/28/2019 18:55
WG1287536
1,1,2-Trichloroethane
U
0.383
1.00
1 05/28/2019 18:55
WG1287536
Trichloroethene
U
0.398
1.00
1 05/28/2019 18:55
WG1287536
Trichlorofluoromethane
U
1.20
5.00
1 05/28/2019 18:55
WG1287536
1,2,3-Trichloropropane
U
0.807
2.50
1 05/28/2019 18:55
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
FP1
FTc
FSS
4
Cn
FC]
F q,
FAI
FSC
Page 51 of 65
PAGE:
17 of 31

ONE LAB. NATIONWIDE.
SW-C SAMPLE RESULTS - 07
Collected date/time: 05/17/19 08:43 L1101602
Volatile Organic Compounds (GC/MS) by Method 8260D
Result Qualifier
MDL
RDL
Dilution Analysis
Batch
Analyte
ug/I
ug/I
ug/I
date / time
Vinyl acetate
U
1.63
10.0
1 05/28/201918:55
WG1287536
Vinyl chloride
U
0.259
1.00
1 05/28/201918:55
WG1287536
o-Xylene
U
0.341
1.00
1 05/28/2019 18:55
WG1287536
m&p-Xylene
U
0.719
2.00
1 05/28/201918:55
WG1287536
Xylenes, Total
U
1.06
3.00
1 05/28/201918:55
WG1287536
1,4-Dioxane
U
36.0
100
1 05/28/201918:55
WG1287536
(S) Toluene-d8
91.4
80.0-120
051281201918:55
WG1287536
(S) 4-Bromof/uorobenzene
101
77.0-126
051281201918:55
WG1287536
(S)1,2-Dich/oroethane-d4
90.7
70.0-130
051281201918:55
WG1287536
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
Pace Analytical
- Huntersville, NC
92429863
L1101602
05/30/1913:43
Fp
FTc
FS
Fn
Fc
F,
FAI
FSC
Page 52 of 65
PAGE:
18 of 31

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101602-06
Method Blank (MB)
(MB) R3415400-3 05/28/19 04:50
MB Result
Analyte
ug/I
Acetone
U
Acrylonitrile
U
Benzene
U
Bromobenzene
U
Bromodichloromethane
U
Bromochloromethane
U
Bromoform
U
Bromomethane
U
Carbon tetrachloride
U
Chlorobenzene
U
Chlorodibromomethane
U
Chloroethane
U
Chloroform
U
Chloromethane
U
2-Chlorotoluene
U
4-Chlorotoluene
U
1,2-Dibromo-3-Chloropropane
U
1,2-Dibromoethane
U
Dibromomethane
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
Dichlorodifluoromethane
U
1,1-Dichloroethane
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
cis-1,2-Dichloroethene
U
trans-1,2-Dichloroethene
U
1,2-Dichloropropane
U
1,1-Dichloropropene
U
1,3-Dichloropropane
U
cis-1,3-Dichloropropene
U
trans-1,3-Dichloropropene
U
2,2-Dichloropropane
U
Di -isopropyl ether
U
Ethylbenzene
U
Hexachloro-1,3-butadiene
U
2-Hexanone
U
p-Isopropyltoluene
U
2-Butanone (MEK)
U
MB Qualifier MB MDL
ug/I
10.0
1.87
0.331
0.352
0.380
0.520
0.469
0.866
0.379
0.348
0.327
0.453
0.324
0.276
0.375
0.351
1.33
0.381
0.346
0.349
0.220
0.274
0.551
0.259
0.361
0.398
0.260
0.396
0.306
0.352
0.366
0.418
0.419
0.321
0.320
0.384
0.256
3.82
0.350
3.93
MB RDL
ug/I
50.0
10.0
1.00
1.00
1.00
5.00
1.00
5.00
1.00
1.00
1.00
5.00
5.00
2.50
1.00
1.00
5.00
1.00
1.00
1.00
1.00
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
10.0
1.00
10.0
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
Page 53 of 65
PAGE:
19 of 31
ACCOUNT:
Pace Analytical - Huntersville, NC
PROJECT: SDG: DATE/TIME:
92429863 L1101602 05/30/1913:43

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101602-06
Method Blank (MB)
(MB) R3415400-3 05/28/19 04:50
MB Result
Analyte
ug/I
Methylene Chloride
U
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
Styrene
U
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
Vinyl acetate
U
Vinyl chloride
U
Xylenes, Total
U
o-Xylene
U
m&p-Xylenes
U
1,4-Dioxane
U
(S) Toluene-d8
93.0
(S) 4-Bromof/uorobenzene
98.8
(S) 1,2-Dich/oroethone-d4
89.8
MB Qualifier MB MDL
ug/I
Laboratory Control Sample (LCS)
1.00
2.14
0.367
1.00
0.307
0.385
0.130
0.372
0.412
0.230
0.355
0.319
0.383
0.398
1.20
0.807
1.63
0.259
1.06
0.341
0.719
36.0
MB RDL
ug/I
5.00
10.0
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
5.00
2.50
10.0
1.00
3.00
1.00
2.00
100
80.0-120
77.0-126
70.0-130
(LCS) R3415400-1 05/28/19 03:30
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
Acetone
125
134
107
19.0-160
Acrylonitrile
125
148
118
55.0-149
Benzene
25.0
28.2
113
70.0-123
Bromobenzene
25.0
22.2
89.0
73.0-121
Bromodichloromethane
25.0
28.6
115
75.0-120
Bromochloromethane
25.0
24.7
98.7
76.0-122
Bromoform
25.0
25.1
100
68.0-132
Bromomethane
25.0
14.5
58.1
10.0-160
Page 54 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43 20 of 31

WG1287157 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101602-06
Laboratory Control Sample (LCS)
(LCS) R3415400-1 05/28/19 03:30
Spike Amount LCS Result
Analyte ug/I ug/I
Carbon tetrachloride
25.0
29.3
Chlorobenzene
25.0
26.3
Chlorodibromomethane
25.0
25.7
Chloroethane
25.0
26.2
Chloroform
25.0
28.1
Chloromethane
25.0
12.7
2-Chlorotoluene
25.0
22.2
4-Chlorotoluene
25.0
23.3
1,2-Dibromo-3-Chloropropane
25.0
21.8
1,2-Dibromoethane
25.0
27.1
Dibromomethane
25.0
27.4
1,2-Dichlorobenzene
25.0
24.6
1,3-Dichlorobenzene
25.0
23.5
1,4-Dichlorobenzene
25.0
22.9
Dichlorodifluoromethane
25.0
12.4
1,1-Dichloroethane
25.0
28.3
1,2-Dichloroethane
25.0
25.9
1,1-Dichloroethene
25.0
30.5
cis-1,2-Dichloroethene
25.0
28.0
trans-1,2-Dichloroethene
25.0
30.0
1,2-Dichloropropane
25.0
27.8
1,1-Dichloropropene
25.0
29.9
1,3-Dichloropropane
25.0
27.1
cis-1,3-Dichloropropene
25.0
29.1
trans-1,3-Dichloropropene
25.0
25.8
2,2-Dichloropropane
25.0
25.9
Di -isopropyl ether
25.0
27.5
Ethylbenzene
25.0
27.0
Hexachloro-1,3-butadiene
25.0
20.9
2-Hexanone
125
136
p-Isopropyltoluene
25.0
22.3
2-Butanone (MEK)
125
130
Methylene Chloride
25.0
27.3
4-Methyl-2-pentanone (MIBK)
125
127
Methyl tert-butyl ether
25.0
28.8
Naphthalene
25.0
22.2
Styrene
25.0
28.0
1,1,1,2-Tetrachloroethane
25.0
26.1
1,1,2,2-Tetrachloroethane
25.0
23.1
Tetrachloroethene
25.0
28.4
LCS Rec
117
105
103
105
112
50.9
88.8
93.3
87.4
109
110
98.5
94.0
91.5
49.5
113
104
122
112
120
119
108
116
103
104
110
108
83.5
109
89.0
104
109
102
115
88.8
112
104
92.4
114
Rec. Limits LCS Qualifier
68.0-126
80.0-121
77.0-125
47.0-150
73.0-120
41.0-142
76.0-123
75.0-122
58.0-134
80.0-122
80.0-120
79.0-121
79.0-120
79.0-120
51.0-149
70.0-126
70.0-128
71.0-124
73.0-120
73.0-120
77.0-125
74.0-126
80.0-120
80.0-123
78.0-124
58.0-130
58.0-138
79.0-123
54.0-138
67.0-149
76.0-125
44.0-160
67.0-120
68.0-142
68.0-125
54.0-135
73.0-130
75.0-125
65.0-130
72.0-132
J4
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
Page 55 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43 21 of 31

WG1287157
Volatile Organic Compounds (GC/MS) by Method 8260D
Laboratory Control Sample (LCS)
(LCS) R3415400-1 05/28/19 03:30
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Toluene
25.0
25.4
1,2,3-Trichlorobenzene
25.0
22.3
1,2,4-Trichlorobenzene
25.0
23.0
1,1,1-Trichloroethane
25.0
29.8
1,1,2-Trichloroethane
25.0
25.8
Trichloroethene
25.0
30.5
Trichlorofluoromethane
25.0
32.7
1,2,3-Trichloropropane
25.0
23.9
Vinyl acetate
125
113
Vinyl chloride
25.0
31.6
Xylenes, Total
75.0
77.1
o-Xylene
25.0
26.0
m&p-Xylenes
50.0
51.1
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethane-d4
Laboratory Control Sample (LCS)
LCS Rec.
102
89.1
91.8
119
103
122
131
95.7
90.7
126
103
104
102
92.2
104
86.0
QUALITY CONTROL SUMMARY
L1101602-06
Rec. Limits LCS Qualifier
79.0-120
50.0-138
57.0-137
73.0-124
80.0-120
78.0-124
59.0-147
73.0-130
11.0-160
67.0-131
79.0-123
80.0-122
80.0-122
80.0-120
77.0-126
70.0-130
ONE LAB. NATIONWIDE.
FP1
FTC]
IS-S]
4
Cn
rs-r
�GI
rAl
FSC
(LCS) R3415400-2 05/28/19 04:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
1,4-Dioxane 1000 988 98.8 13.0-160
(S) Toluene-d8 92.0 80.0-120
(S)4-Bromofluorobenzene 100 77.0-126
(S)1,2-Dich/oroethane-d4 91.5 70.0-130
Page 56 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43 22 of 31

WG1287536 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101602-01,02,03,04,05,07
Method Blank (MB)
(MB) R3416175-3 05/28/1915:13
MB Result
Analyte
ug/I
Acetone
U
Acrylonitrile
U
Benzene
U
Bromobenzene
U
Bromodichloromethane
U
Bromochloromethane
U
Bromoform
U
Bromomethane
U
Carbon tetrachloride
U
Chlorobenzene
U
Chlorodibromomethane
U
Chloroethane
U
Chloroform
U
Chloromethane
U
2-Chlorotoluene
U
4-Chlorotoluene
U
1,2-Dibromo-3-Chloropropane
U
1,2-Dibromoethane
U
Dibromomethane
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
Dichlorodifluoromethane
U
1,1-Dichloroethane
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
cis-1,2-Dichloroethene
U
trans-1,2-Dichloroethene
U
1,2-Dichloropropane
U
1,1-Dichloropropene
U
1,3-Dichloropropane
U
cis-1,3-Dichloropropene
U
trans-1,3-Dichloropropene
U
2,2-Dichloropropane
U
Di -isopropyl ether
U
Ethylbenzene
U
Hexachloro-1,3-butadiene
U
2-Hexanone
U
p-Isopropyltoluene
U
2-Butanone (MEK)
U
MB Qualifier MB MDL
MB RDL
ug/I
ug/I
10.0
50.0
1.87
10.0
0.331
1.00
0.352
1.00
0.380
1.00
0.520
5.00
0.469
1.00
0.866
5.00
0.379
1.00
0.348
1.00
0.327
1.00
0.453
5.00
0.324
5.00
0.276
2.50
0.375
1.00
0.351
1.00
1.33
5.00
0.381
1.00
0.346
1.00
0.349
1.00
0.220
1.00
0.274
1.00
0.551
5.00
0.259
1.00
0.361
1.00
0.398
1.00
0.260
1.00
0.396
1.00
0.306
1.00
0.352
1.00
0.366
1.00
0.418
1.00
0.419
1.00
0.321
1.00
0.320
1.00
0.384
1.00
0.256
1.00
3.82
10.0
0.350
1.00
3.93
10.0
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
Page 57 of 65
PAGE:
23 of 31
ACCOUNT:
Pace Analytical - Huntersville, NC
PROJECT: SDG: DATE/TIME:
92429863 L1101602 05/30/1913:43

WG1287536
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
(MB) R3416175-3 05/28/1915:13
MB Result
Analyte
ug/I
Methylene Chloride
U
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
Styrene
U
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
Vinyl acetate
U
Vinyl chloride
U
Xylenes, Total
U
o-Xylene
U
m&p-Xylenes
U
1,4-Dioxane
U
(S) Toluene-d8
90.2
(S) 4-Bromof/uorobenzene
96.6
(S) 1,2-Dich/oroethone-d4
86.2
MB Qualifier MB MDL
ug/I
Laboratory Control Sample (LCS)
1.00
2.14
0.367
1.00
0.307
0.385
0.130
0.372
0.412
0.230
0.355
0.319
0.383
0.398
1.20
0.807
1.63
0.259
1.06
0.341
0.719
36.0
QUALITY CONTROL SUMMARY
L1101602-01,02,03,04,05,07
MB RDL
ug/I
5.00
10.0
1.00
5.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
1.00
5.00
2.50
10.0
1.00
3.00
1.00
2.00
100
80.0-120
77.0-126
70.0-130
(LCS) R3416175-1 05/28/1913:53
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
Acetone
125
143
114
19.0-160
Acrylonitrile
125
149
120
55.0-149
Benzene
25.0
26.7
107
70.0-123
Bromobenzene
25.0
22.1
88.5
73.0-121
Bromodichloromethane
25.0
27.3
109
75.0-120
Bromochloromethane
25.0
23.8
95.3
76.0-122
Bromoform
25.0
24.1
96.4
68.0-132
Bromomethane
25.0
12.9
51.7
10.0-160
ONE LAB. NATIONWIDE.
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC
Page 58 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43 24 of 31

WG1287536 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1101602-01,02,03,04,05,07
Laboratory Control Sample (LCS)
(LCS) R3416175-1 05/28/1913:53
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
ug/I
ug/I
%
%
Carbon tetrachloride
25.0
27.1
108
68.0-126
Chlorobenzene
25.0
24.5
98.1
80.0-121
Chlorodibromomethane
25.0
24.7
99.0
77.0-125
Chloroethane
25.0
23.1
92.3
47.0-150
Chloroform
25.0
26.9
108
73.0-120
Chloromethane
25.0
16.0
63.9
41.0-142
2-Chlorotoluene
25.0
22.0
87.9
76.0-123
4-Chlorotoluene
25.0
23.2
92.8
75.0-122
1,2-Dibromo-3-Chloropropane
25.0
22.4
89.6
58.0-134
1,2-Dibromoethane
25.0
25.1
100
80.0-122
Dibromomethane
25.0
26.6
107
80.0-120
1,2-Dichlorobenzene
25.0
24.4
97.6
79.0-121
1,3-Dichlorobenzene
25.0
23.1
92.4
79.0-120
1,4-Dichlorobenzene
25.0
22.6
90.6
79.0-120
Dichlorodifluoromethane
25.0
27.7
111
51.0-149
1,1-Dichloroethane
25.0
26.5
106
70.0-126
1,2-Dichloroethane
25.0
24.7
98.9
70.0-128
1,1-Dichloroethene
25.0
27.2
109
71.0-124
cis-1,2-Dichloroethene
25.0
27.7
111
73.0-120
trans-1,2-Dichloroethene
25.0
28.0
112
73.0-120
1,2-Dichloropropane
25.0
26.9
107
77.0-125
1,1-Dichloropropene
25.0
27.5
110
74.0-126
1,3-Dichloropropane
25.0
25.2
101
80.0-120
cis-1,3-Dichloropropene
25.0
28.1
112
80.0-123
trans-1,3-Dichloropropene
25.0
24.1
96.5
78.0-124
2,2-Dichloropropane
25.0
25.5
102
58.0-130
Di -isopropyl ether
25.0
26.8
107
58.0-138
Ethylbenzene
25.0
24.9
99.7
79.0-123
Hexachloro-1,3-butadiene
25.0
20.4
81.7
54.0-138
2-Hexanone
125
137
110
67.0-149
p-Isopropyltoluene
25.0
21.8
87.4
76.0-125
2-Butanone (MEK)
125
139
111
44.0-160
Methylene Chloride
25.0
26.3
105
67.0-120
4-Methyl-2-pentanone (MIBK)
125
126
100
68.0-142
Methyl tert-butyl ether
25.0
27.8
111
68.0-125
Naphthalene
25.0
22.6
90.2
54.0-135
Styrene
25.0
24.7
98.7
73.0-130
1,1,1,2-Tetrachloroethane
25.0
24.6
98.4
75.0-125
1,1,2,2-Tetrachloroethane
25.0
23.3
93.3
65.0-130
Tetrachloroethene
25.0
25.5
102
72.0-132
FP1
FTC]
IS-S]
4
Cn
rs-r
�GI
rAl
FSC
Page 59 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43 25 of 31

WG1287536
Volatile Organic Compounds (GC/MS) by Method 8260D
Laboratory Control Sample (LCS)
(LCS) R3416175-1 05/28/1913:53
Spike Amount
LCS Result
Analyte
ug/I
ug/I
Toluene
25.0
23.7
1,2,3-Trichlorobenzene
25.0
22.4
1,2,4-Trichlorobenzene
25.0
23.2
1,1,1-Trichloroethane
25.0
27.5
1,1,2-Trichloroethane
25.0
24.2
Trichloroethene
25.0
28.1
Trichlorofluoromethane
25.0
28.7
1,2,3-Trichloropropane
25.0
24.4
Vinyl acetate
125
134
Vinyl chloride
25.0
27.6
Xylenes, Total
75.0
71.6
o-Xylene
25.0
24.1
m&p-Xylenes
50.0
47.5
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethane-d4
Laboratory Control Sample (LCS)
LCS Rec
94.7
89.4
92.9
110
96.9
112
115
97.6
107
95.5
96.3
95.0
90.3
102
100
QUALITY CONTROL SUMMARY
L1101602-01,02,03,04,05,07
Rec. Limits LCS Qualifier
79.0-120
50.0-138
57.0-137
73.0-124
80.0-120
78.0-124
59.0-147
73.0-130
11.0-160
67.0-131
79.0-123
80.0-122
80.0-122
80.0-120
77.0-126
70.0-130
ONE LAB. NATIONWIDE.
FP1
FTC]
IS-S]
4
Cn
rs-r
�GI
rAl
FSC
(LCS) R3416175-2 05/28/1914:33
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte ug/I ug/I % %
1,4-Dioxane 1000 1100 110 13.0-160
(S) Toluene-d8 90.6 80.0-120
(S)4-Bromofluorobenzene 100 77.0-126
(S)1,2-Dich/oroethane-d4 86.4 70.0-130
Page 60 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43 26 of 31

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Abbreviations and Definitions
CP
IP
FTC
MDL
Method Detection Limit.
RDL
Reported Detection Limit.
FSS
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
[Cn]
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
FSr
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
Fc
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
FAI
duplicated within these ranges.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
FSC
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
JO JO: The identification of the analyte is acceptable, but the reported concentration is an estimate. The calibration met
method criteria.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J4 The associated batch QC was outside the established quality control range for accuracy.
Page 61 of 65
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pace Analytical - Huntersville, INC 92429863 L1101602 05/30/1913:43 27 of 31

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
MT ND
OR MN
T ID T WI NY
SD
WY MI
NV
T NE IA OH T PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
W 11110
� NM O� AR N Sc
T MS A`7L GA
T TX * LA
T
AK T T
q FL
wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME:
Pace Analytical - Huntersville, NC 92429863 L1101602 05/30/1913:43
ME
Page 62 of 65
PAGE:
28 of 31

Chain of Custody
❑ Samples were sent directly to the Subcontracting Laboratory.
Workorder: 92429863 Workorder Name: SURRY MSWLF SWS
sRepQit o- - Subcont
Angela Mom
Pace Analytical Charlotte Pace National
9800 Kincey Ave. Suite 100 12065 Lebanon Rd
Huntersville, NC 28078
Phone [phone] Mt Juliet, TN 37122
615-758-5858
Item
Sarmp{e IB
1
SW-1
2
w-2
3
SW-3
4
SvV-4
5
SWN-1
6
SWN-2
7
SW-C
Released By
sample
Collect
Type' .
aateMme _
Lab iD
Matrix
FS
5/17/20191ry1:19
92429863001
Water
PS
5117/201912:00
92429863002
Water
PS
51171201914:35
92429863003
Water
1
PS
5117/201916:15
92429863004
Water
1
PS
5117/201915:34
92429863005
Water
PS
51171201916:53
92429863006
Water
PS
5/17/2019 08:43
92429863007
Water
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Dat rme=' - ecelved By
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ace Analytical
State Of Origin: -Q$c�jdj)sxc�m
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Cert. Needed: ❑ No
Owner Received Date: 5/20/2019 Results Requested By: 614/2().19
81111111111F-77---� -Reauested Anal
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2
X
Date/Time
LAB USE ONLY
G1 6d -6I
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Cooler Temperature on Receipt 0.9-•1:0C[Custody Seal Y or N =eceived on Ice Y r N Samples Intact',Im-
. Y r N
***In order to maintain client confide iallty, location/name of the sampling site, sampler's name and signature may not be provided on this COC document.
This chain of custody is considered complete as is since this information is available in the owner laboratory.
RAD S�-7E`N: <0.5 mWhr
u
Tuesday, May 21, 2D19 1:58:47 PM FMT-ALL-C-002rev.00 24March2009 Page 1 of 1
Page 63 of 65

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Pace Analytical National Centerfor TestingsInnovation
Cooler Receipt Form
i S°c#:
Lved/opened
On: 51ZL/19 Temperature:Jordan
Harris
E
Receipt Check List NP
Yes
No
COC Seal Present / Intact?
COC Signed / Accurate?
f
Bottles arrive intact?
Correct bottles used?
Sufficient volume sent?
If Applicable
VOA Zero headspace?
Preservation Correct / Checked?
Page 65 of 65

Environmental Conservation Laboratories, Inc.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: [phone] FAX: [phone]
Thursday, September 12, 2019
Municipal Engineering Services (M0001)
Attn: Jonathan Pfohl
68 Shipwash Drive
Garner, NC 27529
RE: Laboratory Results for
Project Number: [none], Project Name/Desc: Surry Co. Closed LF
ENCO Workorder(s): CC14875
Dear Jonathan Pfohl,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Wednesday, September 4, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
00, (/ L- - C�- A
Chuck Smith
Project Manager
Enclosure(s)
(� �C—O
www.encolabs.com
The total number of pages in this report, including this page is 9.

(� 0a
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MW-20 Lab ID: CC14875-01 Sampled: 08/29/19 16:00 Received: 09/04/19 16:39
Parameter Preparation Hold Date/Time(s)
EPA 8260D EPA 5030B_MS 09/12/19
Pren Date/Time(s) Analysis Date/Time(s)
09/05/19 08:47 09/06/19 00:48
Page 2 of 9

(� 0a
www.encolabs.com
NORTH CAROLINA SWS SAMPLE DETECTION SUMMARY
lient ID: MW-20
Lab ID:
CC14875-01
Analyte
Results
Flag
DF
MDL
MRL
NC SWSL
Units
Method Notes
- - - - - - - - - - - - -
1,2-Dichlorobenzene
- - - - - - - - - -
0.47
- - -
3
-
1
- - - -
0.19
- - - - -
1.0
- - - - -
NE
- - - -
ug/L
- - - - - - - - - - - -
EPA 8260D
1,4-Dichlorobenzene
1.4
1
0.19
1.0
NE
ug/L
EPA 8260D
Benzene
0.58
3
1
0.15
1.0
NE
ug/L
EPA 8260D
cis- 1,2-Dichloroethene
2.9
1
0.15
1.0
NE
ug/L
EPA 8260D
Vinyl chloride
1.3
1
0.32
1.0
NE
ug/L
EPA 8260D
Page 3 of 9

(� �C-o
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-20 Lab Sample ID: CC14875-01 Received: 09/04/19 16:39
Matrix: Ground Water Sampled: 08/29/19 16:00 Work Order: CC14875
Project: Surry Co. Closed LF Sampled By: J. Pfohl
Volatile Organic Compounds by GCMS
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
^ - ENCO Cary certified analyte [NC 591]
Analyte iCAS Number]
Results
Flan
Units
DF
MDL
MRL NC SWSL
Method
Analyzed
ft Notes
1,1,1,2-Tetrachloroethane [630-20-6] ^
0.17
u
ug/L
1
0.17
1.0
EPA 8260D
09/06/19 00:48
REF
1,1,1-Trichloroethane [71-55-6] ^
0.12
u
ug/L
1
0.12
1.0
EPA 8260D
09/06/19 00:48
REF
1,1,2,2-Tetrachloroethane [79-34-5] ^
0.28
u
ug/L
1
0.28
1.0
EPA 8260D
09/06/19 00:48
REF
1,1,2-Trichloroethane [79-00-5] ^
0.14
u
ug/L
1
0.14
1.0
EPA 8260D
09/06/19 00:48
REF
1,1-Dichloroethane [75-34-3] ^
0.13
u
ug/L
1
0.13
1.0
EPA 8260D
09/06/19 00:48
REF
1,1-Dichloroethene [75-35-4] ^
0.21
u
ug/L
1
0.21
1.0
EPA 8260D
09/06/19 00:48
REF
1,2,3-Trichloropropane [96-18-4] ^
0.23
u
ug/L
1
0.23
1.0
EPA 8260D
09/06/19 00:48
REF
1,2-Dibromo-3-chloropropane [96-12-8] ^
0.48
u
ug/L
1
0.48
1.0
EPA 8260D
09/06/19 00:48
REF
1,2-Dibromoethane [106-93-4] ^
0.66
u
ug/L
1
0.66
1.0
EPA 8260D
09/06/19 00:48
REF
1,2-Dichlorobenzene [95-50-1] ^
0.47
ug/L
1
0.19
1.0
EPA 8260D
09/06/19 00:48
REF
1,2-Dichloroethane [107-06-2] ^
0.21
u
ug/L
1
0.21
1.0
EPA 8260D
09/06/19 00:48
REF
1,2-Dichloropropane [78-87-5] ^
0.10
u
ug/L
1
0.10
1.0
EPA 8260D
09/06/19 00:48
REF
1,4-Dichlorobenzene [106-46-7] ^
1.4
ug/L
1
0.19
1.0
EPA 8260D
09/06/19 00:48
REF
2-Butanone [78-93-3] ^
1.3
u
ug/L
1
1.3
5.0
EPA 8260D
09/06/19 00:48
REF
2-Hexanone [591-78-6] ^
0.88
u
ug/L
1
0.88
5.0
EPA 8260D
09/06/19 00:48
REF
4-Methyl-2-pentanone [108-10-1] ^
1.1
u
ug/L
1
1.1
5.0
EPA 8260D
09/06/19 00:48
REF
Acetone [67-64-1] ^
10
u
ug/L
1
10
20
EPA 8260D
09/06/19 00:48
REF
Acrylonitrile [107-13-1] ^
3.5
u
ug/L
1
3.5
10
EPA 8260D
09/06/19 00:48
REF
Benzene [71-43-2] ^
0.58
ug/L
1
0.15
1.0
EPA 8260D
09/06/19 00:48
REF
Bromochloromethane [74-97-5] ^
0.48
u
ug/L
1
0.48
1.0
EPA 8260D
09/06/19 00:48
REF
Bromodichloromethane [75-27-4] ^
0.17
u
ug/L
1
0.17
1.0
EPA 8260D
09/06/19 00:48
REF
Bromoform [75-25-2] ^
0.22
u
ug/L
1
0.22
1.0
EPA 8260D
09/06/19 00:48
REF
Bromomethane [74-83-9] ^
0.14
u
ug/L
1
0.14
1.0
EPA 8260D
09/06/19 00:48
REF
Carbon disulfide [75-15-0] ^
1.5
u
ug/L
1
1.5
5.0
EPA 8260D
09/06/19 00:48
REF
Carbon tetrachloride [56-23-5] ^
0.17
u
ug/L
1
0.17
1.0
EPA 8260D
09/06/19 00:48
REF
Chlorobenzene [108-90-7] ^
0.17
u
ug/L
1
0.17
1.0
EPA 8260D
09/06/19 00:48
REF
Chloroethane [75-00-3] ^
0.23
u
ug/L
1
0.23
1.0
EPA 8260D
09/06/19 00:48
REF
Chloroform [67-66-3] ^
0.18
u
ug/L
1
0.18
1.0
EPA 8260D
09/06/19 00:48
REF
Chloromethane [74-87-3] ^
0.13
u
ug/L
1
0.13
1.0
EPA 8260D
09/06/19 00:48
REF
cis-1,2-Dichloroethene [156-59-2] ^
2.9
ug/L
1
0.15
1.0
EPA 8260D
09/06/19 00:48
REF
cis-1,3-Dichloropropene [10061-01-5] ^
0.20
u
ug/L
1
0.20
1.0
EPA 8260D
09/06/19 00:48
REF
Dibromochloromethane [124-48-1] ^
0.17
u
ug/L
1
0.17
1.0
EPA 8260D
09/06/19 00:48
REF
Dibromomethane [74-95-3] ^
0.27
u
ug/L
1
0.27
1.0
EPA 8260D
09/06/19 00:48
REF
Ethylbenzene [100-41-4] ^
0.13
u
ug/L
1
0.13
1.0
EPA 8260D
09/06/19 00:48
REF
Iodomethane [74-88-4] ^
1.7
u
ug/L
1
1.7
5.0
EPA 8260D
09/06/19 00:48
REF
Methylene chloride [75-09-2] ^
0.23
u
ug/L
1
0.23
1.0
EPA 8260D
09/06/19 00:48
REF
Styrene [100-42-5] ^
0.11
u
ug/L
1
0.11
1.0
EPA 8260D
09/06/19 00:48
REF
Tetrachloroethene [127-18-4] ^
0.17
u
ug/L
1
0.17
1.0
EPA 8260D
09/06/19 00:48
REF
Toluene [108-88-3] ^
0.14
u
ug/L
1
0.14
1.0
EPA 8260D
09/06/19 00:48
REF
trans-1,2-Dichloroethene [156-60-5] ^
0.21
u
ug/L
1
0.21
1.0
EPA 8260D
09/06/19 00:48
REF
trans-1,3-Dichloropropene [10061-02-6] ^
0.15
u
ug/L
1
0.15
1.0
EPA 8260D
09/06/19 00:48
REF
trans-1,4-Dichloro-2-butene [110-57-6] ^
0.70
u
ug/L
1
0.70
1.0
EPA 8260D
09/06/19 00:48
REF
Trichloroethene [79-01-6] ^
0.15
u
ug/L
1
0.15
1.0
EPA 8260D
09/06/19 00:48
REF
Trichlorofluoromethane [75-69-4] ^
0.24
u
ug/L
1
0.24
1.0
EPA 8260D
09/06/19 00:48
REF
Vinyl acetate [108-05-4] ^
0.95
u
ug/L
1
0.95
5.0
EPA 8260D
09/06/19 00:48
REF QL-02,
QV-01
Vinyl chloride [75-01-4] ^
1.3
ug/L
1
0.32
1.0
EPA 8260D
09/06/19 00:48
REF
Xylenes(Total) [1330-20-7] ^
0.45
u
ug/L
1
0.45
3.0
EPA 8260D
09/06/19 00:48
REF
Page 4 of 9

Description: MW-20
Matrix: Ground Water
Project: Surry Co. Closed LF
Lab Sample ID: CC14875-01
Sampled: 08/ 29/ 19 16: 00
Sampled By: I Pfohl
(� �Eo
www.encolabs.com
Received: 09/04/ 19 16:39
Work Order: CC14875
Volatile Organic Compounds by GCMS
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -
^ - ENCO Cary certified anaiyte [NC 591]
Analvte iCAS Numberl Results Flag Ynits DF MDL MRL NC SWSL Method Analyzed Notes
Surrogates Results DF Spike Lvi % Rec % Rec Limits Batch Method Analyzed By Notes
4-8romofluorobenzene 49 1 50.0 98 % 53-136
Dibromofluoromethane 52 1 50.0 104 % 67-129
Toluene-d8 53 1 50.0 105 % 59-134
This report relates only to the sample as received by the laboratory, and may only be reproduced in full.
9105007 EPA 8260D 09106119 00:48 REF
9105007 EPA 8260D 09106119 00:48 REF
9105007 EPA 8260D 09106119 00:48 REF
Page 5 of 9

QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 9105007 - EPA 5030E MS
(� 0a
www.encolabs.com
Blank (9I05007-BLK3)
Prepared: 09/05/2019 08:47 Analyzed: 09/05/2019 17:00
�Analyte
Spike Source %REC RPD
Result
Flag
MRL
Units Level Result %REC Limits RPD Limit Notes
1,1,1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
5urrogate:4-Bromofluorobenzene 49 ug/L 50.0 96 53-136
Page 6 of 9

QUALITY CONTROL
Volatile Organic Compounds by GCMS - Quality Control
Batch 9105007 - EPA 5030B MS
(� �C-O
www.encolabs.com
Blank (9I05007-BLK3) Continued
Prepared: 09/05/2019 08:47 Analyzed: 09/05/2019 17:00
Spike
Source
%REC
RPD
Analyte
Result
Flag
MRL
Level
Result
%REC
Limits RPD
Limit
Notes
Surrogate: Dibromofluoromethane
51
ug/L
50.0
101
67-129
Surrogate: Toluene-d8
52
ug/L
50.0
104
59-134
- - - - - - - - - - - - - -
LCS (9I05007-BS1)
- - - -
- - -
- - - -
- - - -
- - - - - - - - - - - - - - - - - - - -
Prepared: 09/05/2019 08:47 Analyzed: 09/05/2019 14:23
- - - -
- - - -
Spike
Source
%REC
RPD
Analyte
Result
Flag
MRL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
1,1-Dichloroethene
20
1.0
ug/L
20.0
98
75-133
Benzene
21
1.0
ug/L
20.0
104
80-134
Chlorobenzene
20
1.0
ug/L
20.0
99
80-120
Toluene
19
1.0
ug/L
20.0
97
71-120
Trichloroethene
19
1.0
ug/L
20.0
95
74-120
- - - - - - - - - - - - - -
Matrix Spike (9I05007-MS1)
- - - -
- - -
- - - -
- - - -
- - - - - - - - - - - - - - - - - - - -
Prepared: 09/05/2019 08:47 Analyzed: 09/05/2019 14:55
- - - -
- - - -
Source: CC13453-03
�Analyte
Mow
-units
Spike
Source
%REC
RPD
Result
Level
Result
%REC
Limits RPD
Limit
Notes
1,1-Dichloroethene
2.1
1.0
ug/L
20.0
0.21 U
11
75-133
QM-07
Benzene
2.0
1.0
ug/L
20.0
0.15 U
10
80-134
QM-07
Chlorobenzene
1.8
1.0
ug/L
20.0
0.17 U
9
80-120
QM-07
Toluene
1.8
1.0
ug/L
20.0
0.14 U
9
71-120
QM-07
Trichloroethene
1.8
1.0
ug/L
20.0
0.15 U
9
74-120
QM-07
- - - - - -
Matrix Spike Dup (9I05007-MSD1)
- - - -
- - -
- - -
-
- - - - - - - - - - - - -
Prepared: 09/05/2019 08:47 Analyzed: 09/05/2019 15:26
Source:CC13453-03
�Analyte
Spike
Source
%REC
RPD
Flag
MRL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
1,1-Dichloroethene
2.9
1.0
ug/L
20.0
0.21 U
14
75-133 30
20
QM-07,
QM-11
Benzene
2.1
1.0
ug/L
20.0
0.15 U
11
80-134 7
17
QM-07
Chlorobenzene
1.8
1.0
ug/L
20.0
0.17 U
9
80-120 4
16
QM-07
Toluene
1.9
1.0
ug/L
20.0
0.14 U
10
71-120 8
17
QM-07
Trichloroethene
- - - - - - - - - - - - - -
2.1
- - - -
- - -
1.0
- - - -
ug/L
- - - -
20.0
- - - -
0.15 U
- - - -
10
- - - -
74-120 13
- - - - - - - -
22
- - - -
QM-07
- - - -
Page 7 of 9

(� 0a
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.
QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based
on acceptable LCS recovery.
QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
Page 8 of 9

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&

lacieAnalXical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 07, 2019
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Blanks
Pace Project No.: 92430139
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on May 22, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
ft*OL-'
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: Maddie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Blanks
Pace Project No.: 92430139
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Blanks
Pace Project No.: 92430139
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92430139001
92430139002
EB
FIB
Water
Water
05/20/1910:05
05/20/1910:40
05/22/1910:30
05/22/1910:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 20

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Blanks
92430139
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92430139001
EB
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92430139002
FIB
EPA 601OD
SH1
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 20

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ANALYTICAL RESULTS
Project: Blanks
Pace Project No.: 92430139
Sample: EB Lab ID: 92430139001 Collected: 05/20/19 10:05 Received: 05/22/19 10:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 06/07/2019 01:17 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
06/04/19 01:27
06/04/19 23:53
7440-36-0
ND
ug/L
10.0
4.7
1
06/04/19 01:27
06/04/19 23:53
7440-38-2
ND
ug/L
5.0
1.0
1
06/04/19 01:27
06/04/19 23:53
7440-39-3
ND
ug/L
1.0
0.20
1
06/04/19 01:27
06/04/19 23:53
7440-41-7
ND
ug/L
1.0
0.40
1
06/04/19 01:27
06/04/19 23:53
7440-43-9
ND
ug/L
5.0
1.0
1
06/04/19 01:27
06/04/19 23:53
7440-47-3
ND
ug/L
5.0
1.1
1
06/04/19 01:27
06/04/19 23:53
7440-48-4
ND
ug/L
5.0
2.1
1
06/04/19 01:27
06/04/19 23:53
7440-50-8
ND
ug/L
5.0
1.6
1
06/04/19 01:27
06/04/19 23:53
7439-92-1
ND
ug/L
5.0
0.90
1
06/04/19 01:27
06/04/19 23:53
7440-02-0
ND
ug/L
10.0
4.7
1
06/04/19 01:27
06/04/19 23:53
7782-49-2
ND
ug/L
5.0
2.5
1
06/04/19 01:27
06/04/19 23:53
7440-22-4
ND
ug/L
5.0
1.3
1
06/04/19 01:27
06/04/19 23:53
7440-62-2
ND
ug/L
10.0
3.9
1
06/04/19 01:27
06/04/19 23:53
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 06/06/19 03:06 06/07/19 07:50 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
05/28/19 23:34
67-64-1
ND
ug/L
10.0
0.90
1
05/28/19 23:34
107-13-1
ND
ug/L
1.0
0.15
1
05/28/19 23:34
71-43-2
ND
ug/L
1.0
0.34
1
05/28/19 23:34
74-97-5
ND
ug/L
1.0
0.26
1
05/28/19 23:34
75-27-4
ND
ug/L
1.0
0.62
1
05/28/19 23:34
75-25-2
ND
ug/L
2.0
0.62
1
05/28/19 23:34
74-83-9
ND
ug/L
5.0
3.3
1
05/28/19 23:34
78-93-3
ND
ug/L
2.0
0.40
1
05/28/19 23:34
75-15-0
ND
ug/L
1.0
0.22
1
05/28/19 23:34
56-23-5
ND
ug/L
1.0
0.23
1
05/28/19 23:34
108-90-7
ND
ug/L
1.0
0.49
1
05/28/19 23:34
75-00-3
ND
ug/L
5.0
2.3
1
05/28/19 23:34
67-66-3
ND
ug/L
1.0
0.39
1
05/28/19 23:34
74-87-3
ND
ug/L
5.0
0.26
1
05/28/19 23:34
96-12-8
ND
ug/L
1.0
0.41
1
05/28/19 23:34
124-48-1
ND
ug/L
1.0
0.26
1
05/28/19 23:34
106-93-4
ND
ug/L
1.0
0.46
1
05/28/19 23:34
74-95-3
ND
ug/L
1.0
0.29
1
05/28/19 23:34
95-50-1
ND
ug/L
1.0
0.26
1
05/28/19 23:34
106-46-7
ND
ug/L
1.0
0.54
1
05/28/19 23:34
110-57-6
ND
ug/L
1.0
0.27
1
05/28/19 23:34
75-34-3
ND
ug/L
1.0
0.34
1
05/28/19 23:34
107-06-2
ND
ug/L
1.0
0.24
1
05/28/19 23:34
75-35-4
ND
ug/L
1.0
0.29
1
05/28/19 23:34
156-59-2
ND
ug/L
1.0
0.25
1
05/28/19 23:34
156-60-5
ND
ug/L
1.0
0.19
1
05/28/19 23:34
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 20

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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: Blanks
Pace Project No.: 92430139
Sample: EB
Lab ID:
92430139001
Collected:
05/20/19 10:05
Received: 05/22/19 10:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
05/28/19 23:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
05/28/19 23:34
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
05/28/19 23:34
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
05/28/19 23:34
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
05/28/19 23:34
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
05/28/19 23:34
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
05/28/19 23:34
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
05/28/19 23:34
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
05/28/19 23:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
05/28/19 23:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
05/28/19 23:34
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
05/28/19 23:34
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
05/28/19 23:34
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
05/28/19 23:34
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
05/28/19 23:34
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
05/28/19 23:34
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
05/28/19 23:34
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
05/28/19 23:34
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
05/28/19 23:34
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
05/28/19 23:34
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
05/28/19 23:34
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
05/28/19 23:34
460-00-4
1,2-Dichloroethane-d4 (S)
118
%
70-130
1
05/28/19 23:34
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
05/28/19 23:34
2037-26-5
Date: 06/07/2019 01:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 20

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ANALYTICAL RESULTS
Project: Blanks
Pace Project No.: 92430139
Sample: FIB Lab ID: 92430139002 Collected: 05/20/19 10:40 Received: 05/22/19 10:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 06/07/2019 01:17 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
06/04/19 01:27
06/04/19 23:56
7440-36-0
ND
ug/L
10.0
4.7
1
06/04/19 01:27
06/04/19 23:56
7440-38-2
ND
ug/L
5.0
1.0
1
06/04/19 01:27
06/04/19 23:56
7440-39-3
ND
ug/L
1.0
0.20
1
06/04/19 01:27
06/04/19 23:56
7440-41-7
ND
ug/L
1.0
0.40
1
06/04/19 01:27
06/04/19 23:56
7440-43-9
ND
ug/L
5.0
1.0
1
06/04/19 01:27
06/04/19 23:56
7440-47-3
ND
ug/L
5.0
1.1
1
06/04/19 01:27
06/04/19 23:56
7440-48-4
ND
ug/L
5.0
2.1
1
06/04/19 01:27
06/04/19 23:56
7440-50-8
ND
ug/L
5.0
1.6
1
06/04/19 01:27
06/04/19 23:56
7439-92-1
ND
ug/L
5.0
0.90
1
06/04/19 01:27
06/04/19 23:56
7440-02-0
ND
ug/L
10.0
4.7
1
06/04/19 01:27
06/04/19 23:56
7782-49-2
ND
ug/L
5.0
2.5
1
06/04/19 01:27
06/04/19 23:56
7440-22-4
ND
ug/L
5.0
1.3
1
06/04/19 01:27
06/04/19 23:56
7440-62-2
ND
ug/L
10.0
3.9
1
06/04/19 01:27
06/04/19 23:56
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 06/06/19 03:06 06/07/19 07:53 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
05/28/19 23:51
67-64-1
ND
ug/L
10.0
0.90
1
05/28/19 23:51
107-13-1
ND
ug/L
1.0
0.15
1
05/28/19 23:51
71-43-2
ND
ug/L
1.0
0.34
1
05/28/19 23:51
74-97-5
ND
ug/L
1.0
0.26
1
05/28/19 23:51
75-27-4
ND
ug/L
1.0
0.62
1
05/28/19 23:51
75-25-2
ND
ug/L
2.0
0.62
1
05/28/19 23:51
74-83-9
ND
ug/L
5.0
3.3
1
05/28/19 23:51
78-93-3
ND
ug/L
2.0
0.40
1
05/28/19 23:51
75-15-0
ND
ug/L
1.0
0.22
1
05/28/19 23:51
56-23-5
ND
ug/L
1.0
0.23
1
05/28/19 23:51
108-90-7
ND
ug/L
1.0
0.49
1
05/28/19 23:51
75-00-3
ND
ug/L
5.0
2.3
1
05/28/19 23:51
67-66-3
ND
ug/L
1.0
0.39
1
05/28/19 23:51
74-87-3
ND
ug/L
5.0
0.26
1
05/28/19 23:51
96-12-8
ND
ug/L
1.0
0.41
1
05/28/19 23:51
124-48-1
ND
ug/L
1.0
0.26
1
05/28/19 23:51
106-93-4
ND
ug/L
1.0
0.46
1
05/28/19 23:51
74-95-3
ND
ug/L
1.0
0.29
1
05/28/19 23:51
95-50-1
ND
ug/L
1.0
0.26
1
05/28/19 23:51
106-46-7
ND
ug/L
1.0
0.54
1
05/28/19 23:51
110-57-6
ND
ug/L
1.0
0.27
1
05/28/19 23:51
75-34-3
ND
ug/L
1.0
0.34
1
05/28/19 23:51
107-06-2
ND
ug/L
1.0
0.24
1
05/28/19 23:51
75-35-4
ND
ug/L
1.0
0.29
1
05/28/19 23:51
156-59-2
ND
ug/L
1.0
0.25
1
05/28/19 23:51
156-60-5
ND
ug/L
1.0
0.19
1
05/28/19 23:51
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 20

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Blanks
Pace Project No.: 92430139
Sample: FIB
Lab ID:
92430139002
Collected:
05/20/19 10:40
Received: 05/22/19 10:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
05/28/19 23:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
05/28/19 23:51
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
05/28/19 23:51
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
05/28/19 23:51
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
05/28/19 23:51
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
05/28/19 23:51
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
05/28/19 23:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
05/28/19 23:51
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
05/28/19 23:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
05/28/19 23:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
05/28/19 23:51
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
05/28/19 23:51
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
05/28/19 23:51
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
05/28/19 23:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
05/28/19 23:51
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
05/28/19 23:51
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
05/28/19 23:51
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
05/28/19 23:51
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
05/28/19 23:51
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
05/28/19 23:51
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
05/28/19 23:51
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
05/28/19 23:51
460-00-4
1,2-Dichloroethane-d4 (S)
115
%
70-130
1
05/28/19 23:51
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
05/28/19 23:51
2037-26-5
Date: 06/07/2019 01:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 20

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QUALITY CONTROL DATA
Project: Blanks
Pace Project No.: 92430139
QC Batch: 478817 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92430139001, 92430139002
METHOD BLANK: 2591748
Associated Lab Samples: 92430139001, 92430139002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
06/04/19 22:43
Arsenic
ug/L
ND
10.0
4.7
06/04/19 22:43
Barium
ug/L
ND
5.0
1.0
06/04/19 22:43
Beryllium
ug/L
ND
1.0
0.20
06/04/19 22:43
Cadmium
ug/L
ND
1.0
0.40
06/04/19 22:43
Chromium
ug/L
ND
5.0
1.0
06/04/19 22:43
Cobalt
ug/L
ND
5.0
1.1
06/04/19 22:43
Copper
ug/L
ND
5.0
2.1
06/04/19 22:43
Lead
ug/L
ND
5.0
1.6
06/04/19 22:43
Nickel
ug/L
ND
5.0
0.90
06/04/19 22:43
Selenium
ug/L
ND
10.0
4.7
06/04/19 22:43
Silver
ug/L
ND
5.0
2.5
06/04/19 22:43
Vanadium
ug/L
ND
5.0
1.3
06/04/19 22:43
Zinc
ug/L
ND
10.0
3.9
06/04/19 22:43
LABORATORY CONTROL SAMPLE:
Parameter
2591749
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
450
90
80-120
Arsenic
ug/L
500
426
85
80-120
Barium
ug/L
500
471
94
80-120
Beryllium
ug/L
500
470
94
80-120
Cadmium
ug/L
500
453
91
80-120
Chromium
ug/L
500
463
93
80-120
Cobalt
ug/L
500
450
90
80-120
Copper
ug/L
500
461
92
80-120
Lead
ug/L
500
445
89
80-120
Nickel
ug/L
500
450
90
80-120
Selenium
ug/L
500
445
89
80-120
Silver
ug/L
250
236
94
80-120
Vanadium
ug/L
500
457
91
80-120
Zinc
ug/L
500
450
90
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2591750 2591751
MS MSD
92430136001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 483 494 97 99 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2019 01:17 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Blanks
Pace Project No.: 92430139
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2591750
2591751
MS
MSD
92430136001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
474
478
95
95
75-125
1
20
Barium
ug/L
83.7
500
500
601
602
103
104
75-125
0
20
Beryllium
ug/L
ND
500
500
518
519
104
104
75-125
0
20
Cadmium
ug/L
0.51J
500
500
508
511
102
102
75-125
1
20
Chromium
ug/L
ND
500
500
516
518
103
103
75-125
0
20
Cobalt
ug/L
ND
500
500
493
492
99
98
75-125
0
20
Copper
ug/L
ND
500
500
511
513
102
103
75-125
0
20
Lead
ug/L
ND
500
500
487
487
97
97
75-125
0
20
Nickel
ug/L
ND
500
500
495
498
99
99
75-125
0
20
Selenium
ug/L
ND
500
500
518
529
104
106
75-125
2
20
Silver
ug/L
ND
250
250
249
248
99
99
75-125
0
20
Vanadium
ug/L
1AJ
500
500
505
509
101
101
75-125
1
20
Zinc
ug/L
ND
500
500
501
488
100
97
75-125
3
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2019 01:17 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Blanks
Pace Project No.: 92430139
QC Batch: 478972
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92430139001, 92430139002
METHOD BLANK: 2592353
Matrix: Water
Associated Lab Samples: 92430139001, 92430139002
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed Qualifiers
Thallium ug/L
ND 0.10 0.060 06/07/19 01:34
LABORATORY CONTROL SAMPLE: 2592354
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 10.1 101
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2592355 2592356
MS MSD
92430136001
Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND
10 10 9.9 9.9
99 99 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2019 01:17 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Blanks
Pace Project No.: 92430139
QC Batch: 477720 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92430139001, 92430139002
METHOD BLANK: 2586764
Associated Lab Samples: 92430139001, 92430139002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
05/28/19 23:17
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
05/28/19 23:17
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
05/28/19 23:17
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
05/28/19 23:17
1,1-Dichloroethane
ug/L
ND
1.0
0.27
05/28/19 23:17
1,1-Dichloroethene
ug/L
ND
1.0
0.24
05/28/19 23:17
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
05/28/19 23:17
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
0.26
05/28/19 23:17
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.26
05/28/19 23:17
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
05/28/19 23:17
1,2-Dichloroethane
ug/L
ND
1.0
0.34
05/28/19 23:17
1,2-Dichloropropane
ug/L
ND
1.0
0.19
05/28/19 23:17
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
05/28/19 23:17
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
05/28/19 23:17
2-Butanone (MEK)
ug/L
ND
5.0
3.3
05/28/19 23:17
2-Hexanone
ug/L
ND
5.0
0.57
05/28/19 23:17
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
05/28/19 23:17
Acetone
ug/L
ND
25.0
6.2
05/28/19 23:17
Acrylonitrile
ug/L
ND
10.0
0.90
05/28/19 23:17
Benzene
ug/L
ND
1.0
0.15
05/28/19 23:17
Bromochloromethane
ug/L
ND
1.0
0.34
05/28/19 23:17
Bromodichloromethane
ug/L
ND
1.0
0.26
05/28/19 23:17
Bromoform
ug/L
ND
1.0
0.62
05/28/19 23:17
Bromomethane
ug/L
ND
2.0
0.62
05/28/19 23:17
Carbon disulfide
ug/L
ND
2.0
0.40
05/28/19 23:17
Carbon tetrachloride
ug/L
ND
1.0
0.22
05/28/19 23:17
Chlorobenzene
ug/L
ND
1.0
0.23
05/28/19 23:17
Chloroethane
ug/L
ND
1.0
0.49
05/28/19 23:17
Chloroform
ug/L
ND
5.0
2.3
05/28/19 23:17
Chloromethane
ug/L
ND
1.0
0.39
05/28/19 23:17
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
05/28/19 23:17
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
05/28/19 23:17
Dibromochloromethane
ug/L
ND
1.0
0.41
05/28/19 23:17
Dibromomethane
ug/L
ND
1.0
0.46
05/28/19 23:17
Ethylbenzene
ug/L
ND
1.0
0.26
05/28/19 23:17
lodomethane
ug/L
ND
20.0
12.5
05/28/19 23:17
Methylene Chloride
ug/L
ND
5.0
3.7
05/28/19 23:17
Styrene
ug/L
ND
1.0
0.27
05/28/19 23:17
Tetrachloroethene
ug/L
ND
1.0
0.16
05/28/19 23:17
Toluene
ug/L
ND
1.0
0.24
05/28/19 23:17
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
05/28/19 23:17
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2019 01:17 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Blanks
Pace Project No.: 92430139
METHOD BLANK: 2586764
Associated Lab Samples: 92430139001, 92430139002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit MDL
trans- 1,3-Dichloropropene
ug/L
ND
1.0
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
Trichloroethene
ug/L
ND
1.0
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl acetate
ug/L
ND
2.0
Vinyl chloride
ug/L
ND
1.0
Xylene (Total)
ug/L
ND
1.0
1,2-Dichloroethane-d4 (S)
%
116
70-130
4-Bromofluorobenzene (S)
%
105
70-130
Toluene-d8 (S)
%
103
70-130
Analyzed
0.31 05/28/19 23:17
0.54 05/28/19 23:17
0.22 05/28/19 23:17
0.31 05/28/19 23:17
1.4 05/28/19 23:17
0.24 05/28/19 23:17
0.63 05/28/19 23:17
05/28/19 23:17
05/28/19 23:17
05/28/19 23:17
LABORATORY CONTROL SAMPLE:
Parameter
2586765
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
58.9
118
70-130
1,1,1-Trichloroethane
ug/L
50
59.3
119
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
54.4
109
70-130
1,1,2-Trichloroethane
ug/L
50
56.4
113
70-130
1,1-Dichloroethane
ug/L
50
60.3
121
70-130
1,1-Dichloroethene
ug/L
50
61.3
123
70-130
1,2,3-Trichloropropane
ug/L
50
56.1
112
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
57.8
116
70-130
1,2-Dibromoethane (EDB)
ug/L
50
53.6
107
70-130
1,2-Dichlorobenzene
ug/L
50
53.3
107
70-130
1,2-Dichloroethane
ug/L
50
55.3
111
70-130
1,2-Dichloropropane
ug/L
50
56.6
113
70-130
1,4-Dichlorobenzene
ug/L
50
53.7
107
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1190
119
59-169
2-Butanone (MEK)
ug/L
100
119
119
64-135
2-Hexanone
ug/L
100
117
117
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
114
114
70-130
Acetone
ug/L
100
141
141
61-157
Acrylonitrile
ug/L
250
286
115
61-143
Benzene
ug/L
50
55.9
112
70-130
Bromochloromethane
ug/L
50
57.4
115
70-130
Bromodichloromethane
ug/L
50
61.2
122
70-130
Bromoform
ug/L
50
46.3
93
70-130
Bromomethane
ug/L
50
60.0
120
38-130
Carbon disulfide
ug/L
50
62.6
125
68-130
Carbon tetrachloride
ug/L
50
56.5
113
70-130
Chlorobenzene
ug/L
50
52.8
106
70-130
Chloroethane
ug/L
50
70.1
140
37-142
Chloroform
ug/L
50
59.4
119
70-130
Chloromethane
ug/L
50
61.7
123
48-130
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2019 01:17 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Blanks
Pace Project No.: 92430139
LABORATORY CONTROL SAMPLE:
Parameter
2586765
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
cis-1,2-Dichloroethene
ug/L
50
59.4
119
70-130
cis-1,3-Dichloropropene
ug/L
50
59.2
118
70-130
Dibromochloromethane
ug/L
50
57.9
116
70-130
Dibromomethane
ug/L
50
53.0
106
70-130
Ethylbenzene
ug/L
50
54.9
110
70-130
lodomethane
ug/L
100
109
109
40-130
Methylene Chloride
ug/L
50
58.9
118
67-132
Styrene
ug/L
50
55.3
111
70-130
Tetrachloroethene
ug/L
50
52.0
104
69-130
Toluene
ug/L
50
55.5
111
70-130
trans-1,2-Dichloroethene
ug/L
50
59.3
119
70-130
trans- 1,3-Dichloropropene
ug/L
50
57.5
115
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
83.2
166
35-189
Trichloroethene
ug/L
50
54.1
108
70-130
Trichlorofluoromethane
ug/L
50
58.2
116
63-130
Vinyl acetate
ug/L
100
119
119
55-143
Vinyl chloride
ug/L
50
61.2
122
70-131
Xylene (Total)
ug/L
150
165
110
70-130
1,2-Dichloroethane-d4 (S)
%
105
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2586766
MS
92430136011 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2586767
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
22.3
21.9
112
109
73-134
2
30
1,1,1-Trichloroethane
ug/L
ND
20
20
25.4
25.4
127
127
82-143
0
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
22.5
22.2
113
111
70-136
1
30
1,1,2-Trichloroethane
ug/L
ND
20
20
22.9
22.2
115
111
70-135
3
30
1,1-Dichloroethane
ug/L
ND
20
20
26.2
25.7
131
129
70-139
2
30
1,1-Dichloroethene
ug/L
ND
20
20
27.1
26.3
135
132
70-154
3
30
1,2,3-Trichloropropane
ug/L
ND
20
20
23.3
22.6
116
113
71-137
3
30
1,2-Dibromo-3-
ug/L
ND
20
20
20.2
19.8
101
99
65-134
2
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.7
21.8
109
109
70-137
0
30
1,2-Dichlorobenzene
ug/L
ND
20
20
19.5
20.3
98
101
70-133
4
30
1,2-Dichloroethane
ug/L
ND
20
20
24.4
24.7
122
123
70-137
1
30
1,2-Dichloropropane
ug/L
ND
20
20
24.0
23.3
120
117
70-140
3
30
1,4-Dichlorobenzene
ug/L
ND
20
20
19.8
20.4
99
102
70-133
3
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
400
484
482
121
121
53-168
0
30
2-Butanone (MEK)
ug/L
ND
40
40
50.7
51.9
127
130
60-139
2
30
2-Hexanone
ug/L
ND
40
40
45.5
47.1
114
118
65-138
4
30
4-Methyl-2-pentanone
ug/L
ND
40
40
48.3
45.6
121
114
65-135
6
30
(MIBK)
Acetone
ug/L
ND
40
40
58.8
60.1
147
150
60-148
2
30 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
Date: 06/07/2019 01:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Blanks
Pace Project No.: 92430139
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2586766
2586767
MS
MSD
92430136011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acrylonitrile
ug/L
ND
100
100
123
117
123
117
64-147
4
30
Benzene
ug/L
ND
20
20
23.4
23.0
117
115
70-151
1
30
Bromochloromethane
ug/L
ND
20
20
24.0
22.9
120
114
70-141
5
30
Bromodichloromethane
ug/L
ND
20
20
23.8
23.4
119
117
70-138
1
30
Bromoform
ug/L
ND
20
20
18.7
17.9
94
90
63-130
4
30
Bromomethane
ug/L
ND
20
20
23.2
23.5
116
118
15-152
1
30
Carbon disulfide
ug/L
ND
20
20
25.3
25.8
126
129
69-149
2
30
Carbon tetrachloride
ug/L
ND
20
20
22.6
22.0
113
110
70-143
3
30
Chlorobenzene
ug/L
ND
20
20
21.1
21.2
105
106
70-138
0
30
Chloroethane
ug/L
ND
20
20
28.3
26.1
142
131
52-163
8
30
Chloroform
ug/L
ND
20
20
25.0
25.2
125
126
70-139
1
30
Chloromethane
ug/L
ND
20
20
26.2
26.3
131
132
41-139
0
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
25.3
25.6
127
128
70-141
1
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
22.5
23.0
113
115
70-137
2
30
Dibromochloromethane
ug/L
ND
20
20
18.4
18.4
92
92
70-134
0
30
Dibromomethane
ug/L
ND
20
20
20.4
19.5
102
97
70-138
5
30
Ethylbenzene
ug/L
ND
20
20
22.4
21.8
112
109
66-153
3
30
lodomethane
ug/L
ND
40
40
41.9
40.7
105
102
20-138
3
30
Methylene Chloride
ug/L
ND
20
20
26.2
26.1
131
131
42-159
0
30
Styrene
ug/L
ND
20
20
21.2
20.9
106
104
70-135
2
30
Tetrachloroethene
ug/L
ND
20
20
20.4
19.2
102
96
59-143
6
30
Toluene
ug/L
ND
20
20
22.4
21.9
112
109
59-148
2
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
25.6
25.3
128
126
70-146
1
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
22.3
22.1
111
111
70-135
1
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
19.9
19.1
100
95
47-135
4
30
Trichloroethene
ug/L
ND
20
20
21.0
20.7
105
103
70-147
2
30
Trichlorofluoromethane
ug/L
ND
20
20
23.8
23.3
119
116
70-148
2
30
Vinyl acetate
ug/L
ND
40
40
44.4
44.4
111
111
49-151
0
30
Vinyl chloride
ug/L
ND
20
20
26.8
27.0
134
135
70-156
1
30
Xylene (Total)
ug/L
ND
60
60
66.3
64.7
111
108
63-158
2
30
1,2-Dichloroethane-d4 (S)
%
114
115
70-130
4-Bromofluorobenzene (S)
%
107
106
70-130
Toluene-d8 (S)
%
103
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2019 01:17 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Blanks
Pace Project No.: 92430139
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/07/2019 01:17 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Blanks
Pace Project No.: 92430139
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92430139001
EB
EPA 3010A
478817
EPA 6010D
478828
92430139002
FB
EPA 3010A
478817
EPA 6010D
478828
92430139001
EB
EPA 3010A
478972
EPA 6020B
479340
92430139002
FB
EPA 3010A
478972
EPA 6020B
479340
92430139001
EB
EPA 8260D
477720
92430139002
FB
EPA 8260D
477720
Date: 06/07/2019 01:17 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 20

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Recel t(SCUR) I Page 1 of 2
aCe2Amlyffa Document No.: Issuing Authiodty:
F•CAR-CS-033-Rev.06 Pace Carolinas Quality office
-
laboratory receiving samples:
Asheville 0 Eden❑
client Name:
Courier:
❑ Commercial
Custody Sea[ Present? []Yes Q No Seals intact? ❑Yes []No
Greenwood ❑
Huntersville ❑ Raleigh[, Mechanimille❑
Project#: W0# : 92430139
�CI� II I ill it II II Il I III I III
92430139
51XV1`j
Packing Material: ❑Bubble Wrap • ❑8ubbie Bags one ❑ oihar Biological Tissae�ozen?
//
Thermometer: ryr, Type of ice: Q(Wet []Blue❑None []Yes ❑No �JN/A
❑IRGun ID:9 IT
Cooler Tamp ('C): Correction Factor: Add/Subtract ('C)
Temp should be above freezing to 6'C
Cooler Temp Corrected ('C): ❑5amp:es out of temp crlteria. Samples an ice, coating process
hasbegun
USDA Regulated Soil (IA, water sample)
Did samples originate in a quarantine zone within the United States; CA, NY, or SC (check maps)? Did samples originate from a foreign source {intemationally,
-- rI— Including Hawsli and Puerto Rico)? ❑Yes []Nc,
Chain of Custody Present?
Samples Arrived within Hold Time?
Short Hold Time Analysis (<72 hr.)7
Rush Turn Around Time Requested?
5ufficlent Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CDC?
-Includes Date/T1me/ID/Analysis Ma
adspace in V0A Vials (>5-6mm)?
o Blank Present?
3 Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
Na ❑N/A 1
N N/A 2.
N N/A 3.
No N/A 4-
❑No N/A S•
[:]No [iN/A 6.
No ❑ 47
❑No N/
❑No ❑N/
❑No fA 10.
❑No N`A la.
Lot ID of split containers;
CLIENT NOTIFICATION/RESOLUVON
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
DAte/Tlme;
Yr L�.�f
M wD
Field Data Required? ❑Yes ❑No
Date:
Date:
Page 18 of 20

rfi 81ceAI alytical F
Document Name:
Bottle Identification Form
Document No.:
F-CAR-CS-043-Rev.00
*Check mark top half of box if pH and/or dechlorination is Project ##
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/801S (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Document issued: March 14, 2019
Page 1 of 1
Issuing Authority:
Pace Carolinas Qualitv Office
wo#:92430139
PM: AMB Due Date: 06/06/19
CLIENT: 92-Municipal
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Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation I Amount of Preservative Lot #
adjusted added
Note: whenever there Is a discrepancy affecting North Carolina compliance samples, a copy ofthis form wilt be sent to the North Carolina DEHNR Certification Office (i.e
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 19 of 20

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Page 20 of 20

Appendix B
Field Sampling Parameter Data Sheet(s)

Field Sampling Data Sheet
Project: Surry Co Closed C&D and Closed MSWLF-Mt. Airy odrnWiers.
Sampling
Parameters
Water
Quality
Parameters
(Stabilized)
Depth to
p
Water
Depth to
p
Water
Volume
Sample
Goes
Dry
Total
Depth
Total
Comments
DO
ORP
Temp.
Specific
Cond.
Tg/
�
CH4
Gas
MonitoringPure
Pure
g
Collect
Collect
Point
Date
t
Time
Date
Time
(BTOP)
(STOP)
Purged
Type
During
Measured
as
Depth
Expected
(mg/L)
pH
©
(us/cm
(mg/L)
.n
Vapors
i
1
rAL t�
Static
Collection
(Gal)
Purge
expected
' )7
MW-1
;tw
7�
t)
i
40
IW-2
,
-
-
68.08
-
-
ag
t
IW-3
52
-
-
-
-
-
IW-4
-
-
!a r '
-
57
-
-
IW-6
-
-
��
-
64
MW-6
CIi`
31
MW-7
�. ,
t
25
f o
IW-6
-
-
-
-
-
56
-
-
MW-9
((;`�b?v
46
MW-11
40
e
P
MW-12D
-
-
-
100
-
-
-
MW 12S
r.
n
r
£_"�?
"
�;,
4
, (
°r r
J
1a
51
35.78
fs
°t
a
_
MW 13//
MW-14
ram,'
t'"
', S
xj� .'
h,
48.03
r
3®
f , 1
''
56.98
36.28
°'-# t
-
t`
''
IJ
MW-15,
MVV-16
17}i
15.32
i%ri.
MW
-��
MW-18
-
18.15
-
-
-
MW-19
_,,...
17.1
25.64
15.41
(�-0
�`'
"
?�°,�<'
o
6.
MW 20
MW 21
°I'
J
v;
�"
,i
16,04
f�ed
0
W
�.
MW 22
17.1
ill
MW 23
i ! r"
w
SCALEHOUSE
_
r 1
; r)}
_. (4,
.:
222
SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained

�' • # � .
��r� �
rvl uniclPnl U IJ�L�� FnN� ccrtne �
.. c.,,..�. nc, m.,,,n. rvc
Project: Surry Co Closed C&D over Closed MSWLF &Active Subtitle DLined- Mt Airy (Shared Surface Watersl Samplers: y , C `_. , '.
Sampling
Parameters
Water
Quality
Parameters
(Stabilized)
Goes
Total
Specific
�
CH4
Monitorin g
Collect
Collect
Visual
Parameters
Visual
Sample
Dry
Depth
DO
Temp.
Cond.
Hardness
Gas
Point
Date
Time
Flow Rate
to be
Guage
Type
During
Measured
Comments
m /L
( g )
ORP
pH
©
(mg/L )
�
�
Va ors
analyzed
Ht.
as
(us/cm
E—
m
(PP )
` t
�
for
Purge
expected
SW-2
�i�
a
I
a `
—
—
`�l -°�
—
..
�ij
� i � `
-
SW-3
���
�i�{
r �.
,`
�
�
?
� �'
� `�
�'
-
SW-4
� , r
�
I
-
-
t
SWN-1
�,,*�
I
4t
:�.
-
-
It'?r�
f.��
=2r'�
I,
-
SWN-2
���
i�3
'�,��,
I
,�
-
-
�`
t�`�
��
I� 4 �
°:�
��
° . �r `
-
/+
. _
�,
�:
SS B=Stainless Steel Baler, D B=Disposable Baler, P=Low flow Pump, PD=Purged Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained