21047_High Point Multi Stadium_PIIR_20190912

Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019

TABLE OF CONTENTS
1.0 BACKGROUND INFORMATION ............................................................................. 1
2.0 FIELD ACTIVITIES .................................................................................................. 6
3.0 RESULTS ................................................................................................................ 9
4.0 GROUNDWATER FLOW DIRECTION .................................................................. 10
5.0 CONCLUSIONS ..................................................................................................... 10
6.0 RECOMMENDATIONS .......................................................................................... 11
7.0 QUALIFICATIONS OF REPORT ........................................................................... 11

FIGURES
Figure 1 Site Location Map
Figure 2 Sample Locations Overlaid on Historical Development Figure 3 Sample Locations Overlaid on Proposed Development
Figure 4 Groundwater Flow Direction Map
TABLES
Table 1 Temporary Well Construction Data Table 2 Summary of Soil Sample Analytical Results
Table 3 Summary of Groundwater Sample Analytical Results Table 4 Summary of Soil Gas Sample Analytical Results APPENDICES
Appendix A Historical Sample Location Maps
Appendix B Photo Log Appendix C Soil Boring Logs
Appendix D Monitoring Well Construction Diagrams
Appendix E Laboratory Analytical Results and Chain of Custody Records Appendix F Field Notes

Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
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1.0 BACKGROUND INFORMATION

On October 17, 2017, the North Carolina Department of Environmental Quality (NCDEQ) determined that the High Point Multi Stadium project (the “Site”) was eligible for entry into the
North Carolina Brownfields Program (NCBP). The Site is located in downtown High Point, Guilford County (Figure 1) and is generally enclosed by Gatewood Avenue to the north, Lindsay Street to the west, English Street to the south, and Elm Street to the east. The Site is comprised
of a number of parcels (some of which have been combined to facilitate development). Subject
to NCBP’s oversight and approvals, the northern approximate half of the Site has been developed with a multi-use baseball stadium and includes approximately 6 acres (Phase I
Development). The remainder of the Site will be developed with mixture of retail, office, hotel, and residential uses (Phase II Development Parcels). The City of High Point, with notice to and approval by the NCBP, recently removed certain of the Phase II Development Parcels from the
Brownfields Application. The parcels included in the Brownfields Application are shown on Figure 2 and Figure 3. These parcels are referred to as the “Brownfields Property.”

A description of the parcels and an overview of their assessments to date follow:
Parcel 1
Parcel 1 located at 210 Church Avenue, 207-215 Gatewood, and 305-307 Elm Street is the
location of the former High Point Enterprise.
ECS performed a Phase I Environmental Site Assessment (ESA) of the former High Point
Enterprise in February 2016. ECS identified the past use of the property as a printing company
and paint factory as a recognized environmental condition (REC). ECS also identified a former auto repair garage located east of the site and a former gasoline station located south of the site
as off-site RECs. ECS performed a Phase II ESA on the former High Point News and Record property in May
2016. On May 5, 2016, ECS mobilized to the site to observe and document the advancement of
seven soil borings (GP-1, GP-2, GP-3, GP-4, GP-5, GP-6, and GP-7) and conduct the collection of soil samples for laboratory analysis. One duplicate sample was also collected (DUP-1) at the
GP-1 location. The soil samples were focused in the western portion of the site in the area formerly operated as the paint factory. The soil samples were analyzed for volatile organic compounds (VOCs) using EPA Method 8260/3035 and semi-volatile organic compounds
(SVOCs) using EPA Method 8270. Two petroleum related constituents, benzo(a)anthracene and benzo(a)pyrene (BaP) were detected at concentrations above their respective NCDWQ Division of
Waste Management (DWM) Inactive Hazardous Sites Branch (IHSB) Protection of Groundwater
Preliminary Soil Remediation Goals (PSRGs). These constituents were detected in soil samples GP-4, GP-5 and GP-6. Neither VOCs nor SVOCs were detected at concentrations above the
laboratory reporting limits in soil samples GP-1, GP-2, or GP-3.
On May 5, 2016, six Type II monitoring wells were installed on the High Point Enterprise parcel
using hollow-stem auger drilling techniques (MW-1, MW-2, MW-3, MW-4, MW-5 and MW-5D). The depth to groundwater was consistent across the site ranging from approximately 2.75 feet to 4.50 feet below the tops of the well casings. Groundwater samples from the monitoring wells
Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
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were analyzed for VOCs using EPA Method 6200B, SVOCs using EPA Method 8270, and
Resource Conservation and Recovery Action (RCRA) Metals using EPA Method 6010/7174. Four
chlorinated VOCs, tetrachloroethylene (PCE), trichloroethylene (TCE), cis-1,2-dichloroethylene (cis-1,2-DCE), and vinyl chloride, were detected at concentrations above their respective North
Carolina 2L Groundwater Quality Standards (NC2LGWQS) in monitoring wells MW-2, MW-3, and
MW-4.
On September 15, 2016, ECS mobilized to the site to collect sub-slab soil gas samples (SSG-01
through SSG-10) at the High Point Enterprise property. The sub-slab soil gas samples were focused across the rear (north) of the building, closest to MW-3. Laboratory analysis detected
TCE in sample SSG-07 at a concentration of 230 micrograms per cubic meter (ug/m3). This concentration exceeds both the residential and non-residential NCDEQ DWM Vapor Intrusion Screening Levels (VISLs) of 13.9 ug/m3 and 175 ug/m3, respectively. VOCs were not detected in
the remaining samples above the laboratory reporting limit. Sample locations and laboratory analytical tables from previous investigations can be found in Appendix A.
Parcel 2
Parcel 2 located at 206 Church Avenue has been developed since 1932 with a building
originally used as a residence and later converted into a doctor’s office. ECS performed a Phase I ESA of this property in September 2017. ECS identified an abandoned heating oil
UST located on the property as a REC.
On November 22, 2017, ECS contracted a North Carolina licensed drilling contractor to drill fifteen
(GP-1 through GP-15) soil borings using direct push technology (DPT) to a depth of up to 15 feet
below ground surface (bgs) in the areas of recognized environmental conditions and proposed utility pathways. One boring, GP-2, was drilled on Parcel 2 in an area where the UST was
identified. The sample was packaged and submitted to a North Carolina certified laboratory to be analyzed for VOCs and SVOCs using EPA Methods 8260 and 8270, respectively, and total RCRA metals using EPA Methods 6020/7470/7471. Laboratory analysis of the sample collected from
GP-2 did not detect VOCs or SVOCs above the laboratory reporting limits. Laboratory analysis
detected arsenic at a concentration above the residential PSRG.
The previously abandoned heating oil UST was removed on February 22, 2018. Laboratory analysis did not detect VOCs or SVOCs above the laboratory reporting limits. Laboratory analysis of soil samples collected from the sidewalls and base of the UST excavation detected
mercury, barium, chromium, selenium, and lead below the residential PSRGs. Laboratory analysis of one sidewall soil sample detected mercury above the Residential PSRG. Laboratory
analysis of four soil samples detected arsenic above the Residential PSRG with the
concentration in two samples above the Industrial/Commercial PSRG. The concentration of metals detected in the soil samples is consistent with concentrations of similar metals detected
across the site.

Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
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Parcel 4

Parcel 4 located at 300 Church Avenue was developed with single-family residences from at least 1906 until 1969. In 1969, a building was constructed on the site and its occupants included
Wagner Tire Service, Piedmont Truck Tires, and Club Cu.
ECS performed a Phase I ESA of the property in September 2017. ECS identified multiple on-
site RECs including the historical use of the property as an automobile garage, the three
underground hydraulic lifts located in the garage, the two removed underground hydraulic lifts, and the pit located in the garage as RECs. ECS also identified the former gasoline station
located east of the property (Parcel 8) and the former dry cleaning facility located southeast of the property (Parcel 9) as off-site RECs.
On February 28, 2018, ECS observed the removal of six underground hydraulic lifts and one 1,000-gallon heating oil UST from Parcel 4. The lifts and associated lift tanks and heating oil UST were removed and disposed of by DH Griffin Wrecking Company. A soil sample was
collected from each hydraulic lift and lift tank excavation and analyzed for SVOCs. Following removal of the heating oil UST, sidewall and base samples were collected and analyzed for
SVOCs and VOCs. The analysis did not detect VOCs or SVOCs above the IHSB PSRGs.
Parcels 7 & 11 (Portions no longer included in the BFA)

ECS performed a Phase I ESA on the properties located at 207, 209, and 211 Pine Street, 208 N. Lindsay Street, and 500, 504, and 508 West English Street in September 2017. ECS
identified on-site RECs including the use of the property as a machine shop since 1951. ECS
identified off-site RECs including the former dry cleaning facility located east of the site (Parcel 9), the former dry cleaning facility located south of the site (off-site across English Street), and
the gasoline station (Parcel 12) located southwest of the site. Parcel 11 has not yet been assessed. On August 13, 2019, the City of High Point confirmed that Parcel 11 and the portions of Parcel 7 south of Parcel 11 have been dropped from the Brownfields application.
Parcel 8
Parcel 8 located at 215 Church Avenue was undeveloped from at least 1902 until 1950. From 1950 until 1965, a gasoline station was located on the northwestern corner of the property. In 1965, a building was constructed on the property. Occupants of the site have included
Enterprise Offset Printing, Mac Panel Company, Stone Printing Company, Suz’s Software, and RK Stewart & Son Contractors.

ECS performed a Phase I ESA on the property in September 2017. ECS identified the former use of the property as a gasoline station as a REC.

On November 22, 2017, ECS contracted with a North Carolina licensed drilling contractor to drill fifteen soil borings (GP-1 through GP-15) using DPT to a depth of up to 15 feet bgs in the areas of
RECs and proposed utility pathways. One boring, GP-12, was drilled on Parcel 8 in an area where
the USTs were postulated to have been located at the former gasoline station. The sample was packaged and submitted to a North Carolina certified laboratory to be analyzed for VOCs and
Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
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SVOCs using EPA Methods 8260 and 8270, respectively and total RCRA metals using EPA
Methods 6020/7470/7471. Laboratory analysis of the sample collected from GP-12 detected
eight VOCs associated with petroleum products above the laboratory reporting limit, and one VOC, naphthalene, above the Residential PSRG.

On January 30, 2018, three gasoline USTs associated with the former gasoline station were discovered during excavation of a storm water retention pond. The USTs were removed and
samples were collected. Laboratory analysis did not detect VOCs, SVOCs, or RCRA metals
above the residential PSRGs. The soil removed during the excavation of the storm water pond and USTs was stored onsite to be used as beneficial fill.
Parcels 9 & 10

Parcel 9 located at 216 Pine Street was owned by DR Management USA, Inc. and is covered by
an approved Brownfields Agreement (Adam Millis Facility, Brownfields Project No. 15013-11-041). The parcel was undeveloped from at least 1902 until 1950. From 1950 until 2005, the
parcel was developed with a commercial building and two single-family residences. The commercial building was occupied by a hosiery mill and Mac Panel Company Machine Shop. Since 2005, the parcel has been undeveloped and consists of a parking lot. Parcel 10 is located
at 201 Church Avenue and was owned by United Way of Greater High Point, Inc. The parcel consisted of undeveloped land from at least 1902 until 1911. From 1911 until 1960 the parcel
consisted of single-family residences. In 1960, a new building was constructed on the parcel
and has been occupied by Mendenhall-Moore Realtors and the United Way of High Point since construction.

ECS performed a Phase I ESA of the properties in September 2017. ECS identified the former use of the property located at 216 Pine Street as a hosiery mill and machine shop as an on-site REC.
Two off-site RECs were identified which included the former Adam Millis Hosiery Mill located to the
southeast and the former dry cleaning facility located to the southeast.
Parcels 1 through 10 and Utility Corridors On November 22, 2017, ECS contracted with a North Carolina licensed drilling contractor to drill
fifteen (GP-1 through GP-15) soil borings using DPT to a depth of up to 15 feet below in the areas of RECs on parcels 1 through 10 and proposed utility pathways. On December 5, 2017, ECS and the drilling subcontractor returned to the site to install an additional boring (GP-16) in the right of
way of Gatewood Avenue. Soil samples were collected at 5-foot intervals to boring termination. The soil samples were classified in the field by an ECS professional and screened for volatile
organic vapors using a FID/PID. The soil sample from each boring showing the greatest FID/PID
reading and collected from above the water table was selected for analysis. If no organic vapor readings were detected, or the readings were essentially the same, then the sample from a depth
of two feet was selected for analysis. The samples collected for analysis were collected from
depths ranging from 2 to 6 feet below grade. Each sample was packaged and submitted to a North Carolina certified laboratory to be analyzed for VOCs and SVOCs using EPA Methods 8260 and
8270, respectively, and total RCRA metals using EPA Methods 6020/7470/7471. A Level II QA/QC
package was requested from the laboratory.
Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
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Following completion of the soil borings described above, ECS had the drilling contractor
advance the borings (if needed) to intercept the water table and install temporary monitoring
wells. The temporary monitoring wells were purged and sampled. The depth to the water table ranged between approximately 5 and 13 feet below the top of casing. Each sample was packaged
and submitted to a North Carolina certified laboratory to be analyzed for VOCs and SVOCs using
EPA Methods 8260 and 8270, respectively and total RCRA metals using EPA Methods 6010/7470/7471. Subsequent to sampling activities, the temporary and permanent monitoring
wells installed on the High Point Enterprise property were abandoned by the driller in accordance
with North Carolina Administrative Code 2C (NCAC 2C) standards.
Laboratory analysis of soil sample GP-12 (Parcel 12) by EPA Method 8260 detected eight VOCs above the laboratory reporting limit and one VOC, naphthalene, above the Residential PSRG. Laboratory analysis of fourteen of the sixteen soil samples detected arsenic at
concentrations above the Residential PSRG of 0.68 mg/Kg. Arsenic was detected in GP-3 and GP-4 at a concentration above the Industrial Health-Based PSRG of 3.0 mg/Kg. The arsenic in the samples likely reflects naturally occurring concentrations of arsenic.
TCE was detected in the groundwater samples collected from temporary monitoring wells TW-5, -6, -7, -11, and -16 above the NC2LGWQS. TCE was detected above the laboratory reporting
limits, but below the NC2LGWQS in samples collected from temporary monitoring wells TW- 3, -4, -12, and -13. PCE was detected in the groundwater samples collected from temporary
monitoring wells TW-11 and TW-12 above the NC2LGWQS.
Multiple EPA Method 8260 targeted analytes were detected above the NC2LGWQS in the
sample collected from temporary monitoring well TW-12. Several VOCs associated with the
degradation of PCE and TCE were also detected in the samples collected from temporary monitoring wells TW-6 and -7. Three EPA Method 8270 targeted analytes including, 1-
methylnaphthalene, 2-methylnaphthalene, and naphthalene were detected in the sample collected from temporary monitoring well TW-12 at concentrations above their respective NC2LGWQS.

Arsenic was detected in eight of the fifteen groundwater samples above its NC2LGWQS. Barium was detected in each of the samples, of which eight of the fifteen samples were
detected above the NC2LGWQS. Total chromium was detected in each of the samples above the NC2LGWQS. Lead was detected in each above the NC2LGWQS. Mercury was detected in sample TW-1 above the NC2LGWQS.
Parcel 12 (No longer included in the BFA)

ECS performed a Phase I ESA of the property located at 516 West English Street and 204 N. Lindsay Street in September 2017. ECS identified the former use of the property as a gasoline
station since at least 1950 as an on-site REC. One off-site REC was identified which was the
release from the gasoline station formerly located on the property to the southeast and up-gradient of the site. On August 13, 2019, the City of High Point confirmed that Parcel 12 has
been dropped from the Brownfields application.

Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
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The USTs associated with the gasoline station were removed from the site in October 2018. A
Limited Site Assessment (LSA) was conducted on the property in October 2018 after the UST
removal. Soil samples collected from the former UST basin were analyzed for VOCs, SVOCs, EPH, and VPH. Various aliphatics and aromatics were detected in the soil samples above the
Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs), but below the
Residential Standards. One monitoring well was installed in the area of the former UST basin. The groundwater sample was analyzed for VOCs, SVOCs, lead, VPH, and EPH. Five VOCs
were detected in the groundwater sample above the NC2LGWQS, but below the GCLs. The site
received a letter of No Further Action from the NCDEQ on November 9, 2018 with a restriction on groundwater use.
Parcel 13

ECS performed a Transaction Screen Process (TSP) of the properties located at 210 and 212
North Lindsay Street in September 2017. ECS identified the former J’s Mart gasoline station located approximately 175 feet southeast and topographically upgradient of the subject property
as an off-site REC. Parcels 14 through 17
McAdams performed a Phase I ESA that included these parcels (listed as Parcel H in their
report) in May of 2019. McAdams identified the residual groundwater contamination associated
with the southern adjacent and upgradient PERCO and J’s Mart facilities to be off-site RECs for the parcels. McAdams also identified the potential for TCE to migrate through utility corridors
and other potential vapor intrusion preferential pathways as an off-site REC. 2.0 FIELD ACTIVITIES
The following sections describe field activities that were conducted on August 14 through 16, 2019 by ECS. Field activities were conducted in accordance with the NCDEQ approved Work
Plan dated July 29, 2019 and Revised on August 9, 2019, and NCBP’s agreement that no
further assessment was required on the parcels recently removed from the Brownfields Application.
Prior to conducting field activities, ECS contacted the public utility locator service (North Carolina One-Call Center) to identify and mark utilities prior to performing sampling activities.
The field activities included the collection of five (5) soil samples using a Geoprobe® drill rig equipped with DPT, the installation and sampling of four (4) temporary groundwater monitoring
wells, and the installation and sampling of seven (7) soil gas monitoring points at the site. Site
photographs are included in Appendix B.
2.1 Soil Sampling
On August 14, 2019, ECS contracted with 3D Environmental Investigations, LLC (3D) to
advance five soil borings (GP-1, GP-2, GP-8, GP-9, and GP-12) on Parcels 10, 4, 14-15, 17, and 10, respectively using the DTP drill rig. The approximate locations of the soil samples are shown on Figure 2 and Figure 3. Soil boring logs are included in Appendix C. The soil
Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
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samples were collected continuously from the ground surface to the termination depth of each
boring. Soil borings GP-1 and GP-12 were advanced to 4 feet bgs due to redevelopment plans
including the installation of concrete footers extending to approximately 4 feet bgs in the vicinity. The remaining samples (GP-2, GP-8, and GP-9) were drilled to a depth of 2 feet bgs in order to
assess the near surface soil quality. The soil samples were classified and field screened for
relative levels of volatile organic vapors using a PID.
Soil samples were collected for laboratory analysis from borings GP-2, GP-8, and GP-9 from 0-
2 feet bgs, and from GP-1 and GP-12 from depths of 0-2 feet bgs and 2-4 feet bgs in accordance with the work plan. Immediately after collection, the soil samples were transferred
into laboratory supplied/preserved sample containers. The sample containers were labeled, placed into protective packaging material, and placed into a cooler with ice to maintain the
samples at approximately 4° Celsius (°C). The samples were submitted to Pace Analytical
Laboratories (Pace) located in Huntersville, North Carolina to be analyzed for SVOCs using EPA Method 8270, total RCRA metals by EPA Methods 6020/7471 and for VOCs using EPA Method
8260. The soil sample with the highest detected total chromium concentration (Dup-3) was also
analyzed for hexavalent chromium (chromium VI) using EPA Method 7199.
2.2 Groundwater Sampling
During the advancement of the soil borings, four temporary monitoring wells (GW-1, GW-2, GW-
8, and GW-9) were installed on the subject site by 3D. The approximate locations of the temporary monitoring wells are shown on Figure 2 and Figure 3. The temporary monitoring
wells were advanced to depths ranging from 18 to 25 feet bgs. On August 15, 2019,
groundwater samples were collected from each well.
Each temporary monitoring well was constructed with a one-inch inner diameter Schedule 40
PVC flush-threaded riser and well screen to create the monitoring wells. A 15-foot length of 0.010-inch slotted well screen was installed in the monitoring wells. The screens were installed
to a depth such that the screened interval intersected the estimated groundwater surface. A
solid section of PVC riser was placed above the screened interval and extended to a point just above the ground surface. Well construction data is shown on Table 1. Monitoring well
construction diagrams are shown in Appendix D.
Prior to monitoring well sampling activities, the static groundwater elevation was measured
using a decontaminated water level meter. Depth to groundwater in the monitoring wells ranged
from 12.81 feet below the top of casing (ft. btoc) in monitoring well GW-1 to 22.44 ft. btoc in monitoring well GW-9.
Purging and sampling were accomplished using a peristaltic pump and new length of polyethylene tubing using low-flow sampling techniques as indicated in the work plan.
Immediately after collection, the groundwater samples were transferred into laboratory supplied/preserved sample containers. The sample containers were labeled, placed into
protective packaging material, and placed into a cooler with ice to maintain the samples at
approximately 4°C. The samples were submitted to Pace to be analyzed for SVOCs using EPA Method 8270, total RCRA metals by EPA Methods 6020/7470, and for VOCs using EPA Method
8260.
Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
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2.3 Soil Gas Sampling

On August 16, 2019 ECS collected seven soil-gas samples (SG-1 through SG-5, SG-9, and SG-10) at the subject site. The soil gas sampling was conducted in general accordance with the
NCDEQ Vapor Intrusion Guidance (March 2018). The soil gas sampling points were installed by
3D using DPT. Once each boring has reached termination depth 5 feet bgs, dedicated Nylafow tubing and an air stone were lowered into the boring. Coarse filter sand was placed around and
approximately 5 inches above the air stone. The remaining space above the sand consisted of
bentonite granules which was hydrated with distilled water. The soil gas probes were allowed to stabilize for approximately 24 hours before sample collection.
A dedicated syringe was used at each sample location and connected to the tubing to purge the tubing. Approximately three volumes of the tubing was purged prior to sample collection. The
tubing was connected to a 1-liter Summa canister, which was used to collect the sample. The Summa canister was fitted with a flow regulator. The flow rate for both purging and sample collection was approximately 0.2 liters per minute (LPM). The vacuum in the canister was
recorded before and after sample collection. Sample collection was terminated when the vacuum reached approximately 5 inches of mercury (in-Hg).

Prior to collecting the soil gas samples, laboratory-grade helium gas was used as a quality assurance control measure to confirm the integrity of the probe seal and sampling train at each
sample location. A plastic shroud (approximately 18 quarts) was placed and sealed over the
sampling train and sampling point, and then purged with commercial grade helium. The purge point tubing and tracer gas tubing was placed through the cylinder wall via rubber grommets.
The shroud was pressed to the ground with a heavy weight. During the purging stage, the
shroud was flooded with laboratory grade helium via the hose placed through the its wall. The probe point and sampling train was purged using a syringe and discharged into a tedlar bag. A
Model MGD-2002 Multi-Gas Leak detector was used to measure helium from the Tedlar bag. The process was repeated for three intervals. A helium concentration of less than ten percent helium of the shroud concentration was considered acceptable. If concentrations greater than
ten percent helium was measured, the probe tube seal was resealed and the leak detection process was repeated until acceptable levels of less than ten percent were recorded by the detector.
After the leak test was determined to have passed quality assurance criteria, the valve on the
summa canister was opened. The vacuum in the canister was measured and recorded at the
beginning and the end of the sampling cycle. Following sample collection, the probes were removed and the borings filled with grout. The samples were submitted to H&P Mobile
Geochemistry, Inc. (H&P) located in Carlsbad, California to be analyzed for VOCs using EPA
Method TO-15. ECS maintained proper chain-of-custody (COC) procedures throughout the sample collection and transportation process.

Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
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3.0 RESULTS 3.1 Soil Analytical Results

Laboratory analysis did not detect VOCs at concentrations above the laboratory detection limits in the soil samples collected. Laboratory analysis of soil sample GP-1 collected from a depth of
2-4 feet bgs detected pyrene at a concentration above the laboratory detection limits but below
the NCDEQ IHSB Residential and Industrial/Commercial PSRGs. Laboratory analysis of soil samples GP-1, GP-2, GP-8, GP-9, and GP-12 detected barium, total chromium, mercury, and
lead at concentrations above the laboratory detection limits but below their respective PSRGs. Laboratory analysis of soil sample DUP-3 did not detect chromium VI above the laboratory detection limits. Laboratory analysis of soil sample GP-8 detected arsenic at a concentration
above the Residential and Industrial/Commercial PSRGs.
SAMPLE
ID
TARGET ANALYTES EXCEEDING RESIDENTIAL AND
INDUSTRIAL/COMMERCIAL PSRGs
GP-8 Arsenic
A summary of the soil laboratory analytical results are included in Table 2. The laboratory
analytical data sheets and chain of custody records are shown in Appendix E.
3.2 Groundwater Analytical Results
Laboratory analysis did not detect VOCs, SVOCs, arsenic, cadmium, selenium, or silver at concentrations above the laboratory detection limits in the groundwater samples collected.
Laboratory analysis detected barium at concentrations above the laboratory detection limits but
below the NC2LGWQS in the groundwater samples collected. Laboratory analysis of groundwater sample GW-2 detected lead at a concentration above the laboratory detection
limits but below the NC2LGWQS. Laboratory analysis of groundwater samples GW-1 and GW-2 detected total chromium at concentrations above its NC2LGWQS but below its EPA Maximum Contaminant Level (MCL). A summary of the groundwater laboratory analytical results are
included in Table 3. The laboratory analytical data sheets and chain of custody records are shown in Appendix E.

SAMPLE
ID TARGET ANALYTES EXCEEDING NC2LGWQS
GW-1 Chromium (Total)
GW-2 Chromium (Total)
3.3 Soil Gas Analytical Results Laboratory analysis detected three (3) VOCs in soil gas sample SG-1, eight (8) VOCs in soil gas
samples SG-2 and SG-4, fourteen (14) VOCs in soil gas sample SG-5, ten (10) VOCs in soil gas sample SG-9, and nine (9) VOCs in soil gas sample SG-10 at concentrations above the
Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
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laboratory reporting limits but below their respective NCDEQ Residential and Non-Residential
Vapor Intrusion Screening Levels (VISLs). Laboratory analysis of soil gas sample SG-3
detected benzene and ethylbenzene at concentrations above their respective NCDEQ Residential VISL but below their respective Non-Residential VISLs. A summary of the
groundwater laboratory analytical results are included in Table 4. The laboratory analytical data sheets and chain of custody records are shown in Appendix E.
SAMPLE ID TARGET ANALYTES EXCEEDING RESIDENTIAL VISLs
SG-3 Benzene, Ethylbenzene
4.0 GROUNDWATER FLOW DIRECTION
The relative elevation of the top of temporary wells GW-2, GW-8, and GW-9 were measured to
the nearest 0.01 feet using a level and rod. The elevations were measured relative to an arbitrary benchmark, which was assigned an elevation of 100 feet. The relative elevation of the
top of casing for each well and the measurement of the depth to groundwater surface from the
top of the well casing were used to determine the relative elevation of groundwater at each well location (Table 1). The groundwater elevations as determined on August 15, 2019 were used to
prepare a potentiometric map of the groundwater surface in the assessment area of the site (Figure 4). The groundwater flow direction is generally to the northwest across the site.

5.0 CONCLUSIONS
Based on the field observation and laboratory analytical results of this assessment, ECS
concludes the following:
• Laboratory analysis of one soil sample detected arsenic at a concentration above the Residential and Industrial/Commercial PSRGs. It is ECS’s opinion that the arsenic detected is
naturally occurring. Dragun and Chekiri Elements in North American Soils – Second Edition
indicates that the concentration of arsenic present in North Carolina soil ranges from 1.0 mg/kg to 18 mg/kg

• Laboratory analysis of two groundwater samples detected total chromium at concentrations
above the NC2LGWQS but below its EPA MCL. The concentration of total chromium detected
may be attributed to the naturally occurring concentrations of these metals in the soil.
• Laboratory analysis of one soil gas sample detected benzene and ethylbenzene at concentrations above their respective NCDEQ Residential VISLs but below their respective
Non-Residential VISLs.

• The laboratory quality control data was reviewed and is acceptable for the intended purposes of
this report.
Environmental Services Report High Point Multi Stadium - Phase II Development Parcels Brownfields Project No. 21047-17-041
Gatewood Avenue and Church Street High Point, Guilford County, North Carolina
ECS Project No. 49-5318F September 12, 2019
11
6.0 RECOMMENDATIONS

ECS recommends submitting this report to the Brownfields Project Manager. Based on these results and the planned redevelopment, ECS does not believe that further assessment is
warranted on the Phase II Development Parcels.
7.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those normally employed in assessment projects of this type. Our evaluation of site conditions has
been based on our understanding of the site project information and the data obtained during our previous assessment and field activities.

FIGURES
SOURCE:

USGS TOPOGRAPHIC MAP
HIGH POINT WEST AND HIGH POINT EAST,
NORTH CAROLINA QUADRANGLES, DATED
1969 AND REVISED 1987

FIGURE 1
SITE LOCATION MAP

HIGH POINT MULTI STADIUM
GATEWOOD AVENUE, CHURCH AVENUE,
AND PINE STREET
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-5318-F
SITE
BROWNFIELD PROPERTY BOUNDARY
2,000’
SOURCE:

GUILFORD COUNTY GIS WEBSITE
AERIAL PHOTOGRAPH, DATED 2014 AND
ECS NOTES

FIGURE 2
SAMPLE LOCATIONS OVERLAID ON
HISTORICAL DEVELOPMENT

HIGH POINT MULTI STADIUM
GATEWOOD AVENUE, CHURCH AVENUE,
AND PINE STREET
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-5318-F 140’
Legend
Brownfield Property Boundary
Soil Gas Sample Location
Soil/Groundwater Sample Location
Soil Sample Location
SG-1
SG-2
SG-3
SG-4
SG-5
SG-9
SG-10
GP-1/GW-1
GP-2/GW-2
GP-8/GW-8
GP-9/GW-9
GP-12
SOURCE:

CITY OF HIGH POINT
AND ECS NOTES

NOT TO SCALE

FIGURE 3
SAMLE LOCATIONS OVERLAID ON
PROPOSED DEVELOPMENT

HIGH POINT MULTI USE STADIUM
GATEWOOD AVENUE, CHURCH AVENUE,
AND PINE STREET
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-5318A
Legend
Brownfield Property Boundary
Soil Gas Sample Location
Soil/Groundwater Sample Location
Soil Sample Location
SG-1
SG-2
SG-3
SG-4
SG-5
SG-9
SG-10
GP-1/GW-1
GP-2/GW-2
GP-8/GW-8
GP-9/GW-9
GP-12
SOURCE:

GUILFORD COUNTY GIS WEBSITE
AERIAL PHOTOGRAPH, DATED 2014 AND
ECS NOTES

FIGURE 4
GROUNDWATER FLOW DIRECTION MAP

HIGH POINT MULTI STADIUM
GATEWOOD AVENUE, CHURCH AVENUE,
AND PINE STREET
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-5318-F 140’
Legend
Brownfield Property Boundary
Groundwater Sample Location 77.XX
Relative Groundwater Elevation
Inferred Groundwater Flow Direction
GP-1/GW-1
GP-2/GW-2
GP-8/GW-8
GP-9/GW-9
(76.68)
(77.37)
(77.14)
76
76
77
77
(Not Measured)
TABLES
TABLE 1: Temporary Well Construction Data
High Point Multi Stadium
Gatewood Avenue and Church Street
High Point, Guilford County, NC
Brownfields Project ID: 21047-17-041
ECS Project No. 49-5318-F
WELL ID #WELL DEPTH
(ft.)
SCREEN LENGTH
(ft.)
TOP OF CASING
ELEVATION (ft.)
DATE WATER
LEVEL MEASURED DEPTH TO WATER GROUNDWATER
ELEVATION* (ft.)
GW-1 18 15 -8/15/2019 12.81 -
GW-2 25 15 93.15 8/15/2019 16.47 76.68
GW-8 25 15 97.58 8/15/2019 20.21 77.37
GW-9 25 15 99.58 8/15/2019 22.44 77.14
* Relative to an arbitrary benchmark of 100 feet above mean sea level
TABLE 2: SUMMARY OF SOIL ANALYTICAL RESULTS
High Point Multi Stadium
Gatewood Avenue and Church Street
High Point, Guilford County, NC
Brownfields Project ID: 21047-17-041
ECS Project No. 49-5318-F
Parameter
Sample ID GP-2 GP-8 GP-9 DUP-3
Collection Depth (feet bgs)0-2 2-4 0-2 0-2 0-2 0-2 2-4 2-4
Collection Date
VOCs by EPA 8260D
All Targeted Compounds ND ND ND ND ND ND ND ND ----
SVOCs by EPA 8270E
Pyrene <2.0 0.50 <1.9 <2.3 <0.44 <0.39 <0.45 <0.49 360 4,500
Metals by EPA 6020 and EPA 7471
Barium 80.6 108 104 33.2 23.1 23.3 176 191 3,100 47,000
Total Chromium 71.6 80.2 41.6 42.3 107 139 104 206 23,000 350,000
Chromium (III)NA NA NA NA NA NA NA NA 23,000 350,000
Chromium (VI)--------------ND 0.31 6.5
Arsenic <3.8 <4.1 <3.4 5.4 <4.1 <3.6 <4.1 <4.5 0.68 3
Lead 27.9 33.7 10.6 58.6 9.1 7.3 8.0 <4.5 400 800
Selenium <3.8 <4.1 <3.4 <4.2 <4.1 <3.6 <4.1 6.6 78 1,200
Mercury 0.12 0.037 0.044 0.19 0.28 <0.018 0.045 <0.023 2.3 9.7
Notes:
mg/kg = milligrams per kilogram (mg/kg), parts per million (ppm)
Feet bgs = Feet below ground surface
NA = Not Analyzed
ND = Not Detected
BOLD = Concentration Exceeds the Residential PSRG
Underline = Concentration Exceeds the Industrial PSRG
IHSB = Inactive Hazardous Sites Branch
PSRG = Preliminary Soil Remediation Goal
Dup-3 is a duplicate of GP-12 collected from 2-4 feet bgs
IHSB
Residential
Health Based
PSRG
IHSB
Industrial
Commercial
Health Based
PSRG
Comparison CriteriaSAMPLE LOCATION
8/14/19
GP-1 GP-12
High Point Multi Stadium
Gatewood Avenue and Church Street
High Point, Guilford County, NC
Brownfields Project ID: 21047-17-041
ECS Project No. 49-5318-F
Sample ID GW-1 GW-2 GW-8
Sample Date
Method (Parameter)
All Targeted Compounds ND ND ND ND ND ----
Method (Parameter)
All Targeted Compounds ND ND ND ND ND ----
Method (Parameter)
Arsenic <10 <10 <10 <10 <10 10 100
Barium 77.2 232 24.1 37.3 32.2 700 2,000
Cadmium <1.0 <1.0 <1.0 <1.0 <1.0 2 5
Chromium 25.7 32.9 <5.0 6.9 <5.0 10 100
Lead <5.0 7.4 <5.0 <5.0 <5.0 15 15
Selenium <10 <10 <10 <10 <10 20 50
Silver <5.0 <5.0 <5.0 <5.0 <5.0 20 50
Method (Parameter)
Mercury <0.20 <0.20 <0.20 <0.20 <0.20 1 2
Notes:
Results presented in parts per billion (ug/L)
NC2LGWQS = North Carolina 2L Groundwater Quality Standard
(µg/L) = Micrograms per Liter
ND = Not detected above the laboratory detection limit Limit
NE = Not Established
Bold = Detected above the NC2LGWQS
TABLE 3: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
GW-9/Dup-1
8/15/2019 EPA MCL
EPA Method 7470A
NC2LGWQS
EPA Method 8260
EPA Method 8270
EPA Method 6010D
High Point Multi Stadium
Gatewood Avenue and Church Street
High Point, Guilford County, NC
Brownfields Project ID: 21047-17-041
ECS Project No. 49-5318-F
Sample ID SG-1 SG-2 SG-3 SG-4 SG-5 SG-9 Dup-2 SG-10
Sample Date
Method (Parameter)
Benzene <16 54 490 22 51 45 48 27 120 1,600
2-Butanone (MEK)<30 <30 <30 <30 110 <30 <30 <30 35,000 440,000
2-Hexanone (MBK)<8.3 <8.3 <8.3 <8.3 31 <8.3 <8.3 <8.3 210 2,600
Chloromethane <10 26 <10 13 4.3 4.8 4.5 6.3 630 7,900
Carbon Disulfide <6.3 47 49 140 13 22 23 13 4,900 61,000
Chloroform <4.9 <4.9 <4.9 <4.9 <4.9 5.3 6.9 6.3 41 530
Ethylbenzene <4.4 57 710 78 6.0 9.2 10 5.6 370 4,900
4-Ethyltoluene <25 25 200 38 <25 <25 <25 <25 ----
Styrene <4.3 <4.3 <4.3 <4.3 12 12 10 5.2 6,950 87,600
Toluene <3.8 87 90 61 29 32 34 27 35,000 440,000
Dichlorodifluoromethane (F12)130 <5.0 39 <5.0 50 <5.0 <5.0 <5.0 700 8,800
Dichlorotetrafluoromethane (F114)<7.1 <7.1 <7.1 <7.1 93 <7.1 <7.1 <7.1 ----
Trichlorofluoromethane (F11)49,000 <5.6 <5.6 <5.6 6.9 <5.6 7.5 <5.6 ----
Vinyl Chloride <2.6 <2.6 <2.6 <2.6 5.8 8.5 6.1 <2.6 56 2,800
1,2,4-Trimethylbenzene <5.0 39 370 62 7.5 9.0 8.0 5.4 420 5,300
1,3,5-Trimethylbenzene <25 <25 330 <25 <25 <25 <25 <25 420 5,300
Total Xylenes 250 231 690 285 25.5 35 37 21.7 700 8,800
Notes:
Results presented in micrograms per cubic meter (ug/m3)
NCDEQ Division of Waste Management Residential and Non-Residential Vapor Intrusion Screening Levels dated February 2018
VISL = Vapor Intrusion Screening Level
ug/m3 = Micrograms per Cubic Meter
-- = No Established VISL
BRL = Below Reporting Level
Bold = Detected Above the Residential SGSL
Residential
VISLs
Non-Residential
VISLsEPA TO-15
Table 4 Summary of Soil Gas Sample Analytical Results
8/16/2019
APPENDIX A
APPENDIX B
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 1: View of Block C assessment area looking west. Note marked utilities.
Photograph 2: View of GP-12 soil boring location looking west.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 3: View of GP-12 soil boring location looking northeast.
Photograph 4: View of SG-1 soil gas sample location looking northeast.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 5: Additional view of SG-1 looking northwest.
Photograph 6: View of GP-1/GW-1 location looking northeast.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 7: View of GP-1/GW-1 sample location looking southeast.
Photograph 8: Macro cores associated with GP-1/GW-1 location. Refusal was encountered at 18 feet bgs.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 9: View of macro core associated with SG-2. Note gray staining from 4-5 feet bgs (photo left).
Photograph 10: View of SG-2 soil gas sample location behind center field wall looking west.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 11: View of SG-2 soil gas sample location behind center field wall looking east.
Photograph 12: View of soil gas sample vapor point installation at location identified as SG-2.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 13: View of soil gas sample location SG-3 looking southeast.
Photograph 14: View of soil gas sample location SG-3 looking west.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 15: View of soil gas sample location SG-4 looking northwest.
Photograph 16: View of soil gas sample location SG-4 looking west.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 17: View of soil gas sample location SG-10 looking southwest.
Photograph 18: View of soil gas sample location SG-10 looking northeast.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 19: View of sample location GP-9/GW-9 looking north.
Photograph 20: View of sample location GP-9/GW-9 looking southwest.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 21: View of macro cores produced from installation of GP-9/GW-9.
Photograph 22: View of GP-8/GW-8 temporary well installation.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 23: View of GP-8/GW-8 location looking southwest.
Photograph 24: View of GP-8/GW-8 location looking northwest.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 25: View of SG-9 location looking southeast.
Photograph 26: View of well development activities occurring at location GP-2/GW-3. View looking southwest.
PHOTOGRAPH LOG
High Point Multi Stadium
Gatewood Avenue, Church Avenue, and Pine Street
High Point, Guilford County, North Carolina
ECS Project No. 49-5318-F
Photograph 27: Soil boring cuttings and well development water were drummed as IDW for future disposal.
Photograph 28: Soil Gas Shroud Set-up at location SG-10.
APPENDIX C
APPENDIX D
APPENDIX E
ECS Southeast, LLP - Greensboro
Greensboro, NC 27407
4811 Koger Blvd.
Randy Cavallier
Enclosed is the analytical report for the above referenced project. The data herein applies to
samples as received by H&P Mobile Geochemistry, Inc. on 19-Aug-19 which were analyzed in
accordance with the attached Chain of Custody record(s).
The results for all sample analyses and required QA/QC analyses are presented in the following
sections and summarized in the documents:
• Sample Summary
• Case Narrative (if applicable)
• Sample Results
• Quality Control Summary
• Notes and Definitions / Appendix
• Chain of Custody
• Sampling Logs (if applicable)
Unless otherwise noted, I certify that all analyses were performed and reviewed in compliance with
our Quality Systems Manual and Standard Operating Procedures. This report shall not be
reproduced, except in full, without the written approval of H&P Mobile Geochemistry, Inc.
We at H&P Mobile Geochemistry, Inc. sincerely appreciate the opportunity to provide analytical
services to you on this project. If you have any questions or concerns regarding this analytical report,
please contact me at your convenience at 760-804-9678.
Sincerely,
21 August 2019
Janis La Roux
Laboratory Director
H&P Mobile Geochemistry, Inc. is certified under the California ELAP and the National Environmental
Laboratory Accreditation Conference (NELAC). H&P is approved as an Environmental Testing Laboratory and
Mobile Laboratory in accordance with the DoD-ELAP Program and ISO/IEC 17025:2005 programs,
accreditation number 69070 for EPA Method TO-15, H&P Method TO-15, EPA Method 8260B and H&P 8260SV.
Client Project: HP Stadium Phase II / High Point
H&P Project: ECS081919-11
Dear Randy Cavallier:
P 1.800.834.9888 / 760.804.9678 F 760.804.9159 W handpmg.com
2470 Impala Drive, Carlsbad, CA 92010 & Field Office - Signal Hill, CAQuality. Accuracy. Experience.
Geochemistry Inc.Mobile
Page 1 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
SG-10 E908093-01 Vapor 16-Aug-19 19-Aug-19
SG-9 E908093-02 Vapor 16-Aug-19 19-Aug-19
SG-5 E908093-03 Vapor 16-Aug-19 19-Aug-19
SG-1 E908093-04 Vapor 16-Aug-19 19-Aug-19
SG-2 E908093-05 Vapor 16-Aug-19 19-Aug-19
SG-3 E908093-06 Vapor 16-Aug-19 19-Aug-19
SG-4 E908093-07 Vapor 16-Aug-19 19-Aug-19
Dup-2 E908093-08 Vapor 16-Aug-19 19-Aug-19
Page 2 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
DETECTIONS SUMMARY
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-01SG-10
Notes
Reporting
Chloromethane 6.3 2.1 ug/m3 EPA TO-15
Carbon disulfide 13 6.3 ug/m3 EPA TO-15
Chloroform 6.3 4.9 ug/m3 EPA TO-15
Benzene 27 3.2 ug/m3 EPA TO-15
Toluene 27 3.8 ug/m3 EPA TO-15
Ethylbenzene 5.6 4.4 ug/m3 EPA TO-15
m,p-Xylene 15 8.8 ug/m3 EPA TO-15
Styrene 5.2 4.3 ug/m3 EPA TO-15
o-Xylene 6.7 4.4 ug/m3 EPA TO-15
1,2,4-Trimethylbenzene 5.4 5.0 ug/m3 EPA TO-15
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-02SG-9
Notes
Reporting
Chloromethane 4.8 2.1 ug/m3 EPA TO-15
Vinyl chloride 8.5 2.6 ug/m3 EPA TO-15
Carbon disulfide 22 6.3 ug/m3 EPA TO-15
Chloroform 5.3 4.9 ug/m3 EPA TO-15
Benzene 45 3.2 ug/m3 EPA TO-15
Toluene 32 3.8 ug/m3 EPA TO-15
Ethylbenzene 9.2 4.4 ug/m3 EPA TO-15
m,p-Xylene 24 8.8 ug/m3 EPA TO-15
Styrene 12 4.3 ug/m3 EPA TO-15
o-Xylene 11 4.4 ug/m3 EPA TO-15
1,2,4-Trimethylbenzene 9.0 5.0 ug/m3 EPA TO-15
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-03SG-5
Notes
Reporting
Dichlorodifluoromethane (F12)50 5.0 ug/m3 EPA TO-15
Chloromethane 4.3 2.1 ug/m3 EPA TO-15
Dichlorotetrafluoroethane (F114)93 7.1 ug/m3 EPA TO-15
Vinyl chloride 5.8 2.6 ug/m3 EPA TO-15
Trichlorofluoromethane (F11)6.9 5.6 ug/m3 EPA TO-15
Carbon disulfide 13 6.3 ug/m3 EPA TO-15
2-Butanone (MEK)110 30 ug/m3 EPA TO-15
Benzene 51 3.2 ug/m3 EPA TO-15
Page 3 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-03SG-5
Notes
Reporting
Toluene 29 3.8 ug/m3 EPA TO-15
2-Hexanone (MBK)31 8.3 ug/m3 EPA TO-15
Ethylbenzene 6.0 4.4 ug/m3 EPA TO-15
m,p-Xylene 16 8.8 ug/m3 EPA TO-15
Styrene 12 4.3 ug/m3 EPA TO-15
o-Xylene 9.5 4.4 ug/m3 EPA TO-15
1,2,4-Trimethylbenzene 7.5 5.0 ug/m3 EPA TO-15
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-04SG-1
Notes
Reporting
Dichlorodifluoromethane (F12)130 130 ug/m3 EPA TO-15
Trichlorofluoromethane (F11)49000 140 ug/m3 EPA TO-15
m,p-Xylene 250 220 ug/m3 EPA TO-15
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-05SG-2
Notes
Reporting
Chloromethane 26 10 ug/m3 EPA TO-15
Carbon disulfide 47 32 ug/m3 EPA TO-15
Benzene 54 16 ug/m3 EPA TO-15
Toluene 87 19 ug/m3 EPA TO-15
Ethylbenzene 57 22 ug/m3 EPA TO-15
m,p-Xylene 180 44 ug/m3 EPA TO-15
o-Xylene 51 22 ug/m3 EPA TO-15
4-Ethyltoluene 25 25 ug/m3 EPA TO-15
1,2,4-Trimethylbenzene 39 25 ug/m3 EPA TO-15
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-06SG-3
Notes
Reporting
Dichlorodifluoromethane (F12)39 25 ug/m3 EPA TO-15
Carbon disulfide 49 32 ug/m3 EPA TO-15
Benzene 490 16 ug/m3 EPA TO-15
Toluene 90 19 ug/m3 EPA TO-15
Ethylbenzene 710 22 ug/m3 EPA TO-15
m,p-Xylene 560 44 ug/m3 EPA TO-15
o-Xylene 130 22 ug/m3 EPA TO-15
4-Ethyltoluene 200 25 ug/m3 EPA TO-15
Page 4 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-06SG-3
Notes
Reporting
1,3,5-Trimethylbenzene 330 25 ug/m3 EPA TO-15
1,2,4-Trimethylbenzene 370 25 ug/m3 EPA TO-15
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-07SG-4
Notes
Reporting
Chloromethane 13 10 ug/m3 EPA TO-15
Carbon disulfide 140 32 ug/m3 EPA TO-15
Benzene 22 16 ug/m3 EPA TO-15
Toluene 61 19 ug/m3 EPA TO-15
Ethylbenzene 78 22 ug/m3 EPA TO-15
m,p-Xylene 210 44 ug/m3 EPA TO-15
o-Xylene 75 22 ug/m3 EPA TO-15
4-Ethyltoluene 38 25 ug/m3 EPA TO-15
1,2,4-Trimethylbenzene 62 25 ug/m3 EPA TO-15
Sample ID:Laboratory ID:
Analyte Result Limit Units Method
E908093-08Dup-2
Notes
Reporting
Chloromethane 4.5 2.1 ug/m3 EPA TO-15
Vinyl chloride 6.1 2.6 ug/m3 EPA TO-15
Trichlorofluoromethane (F11)7.5 5.6 ug/m3 EPA TO-15
Carbon disulfide 23 6.3 ug/m3 EPA TO-15
Chloroform 6.9 4.9 ug/m3 EPA TO-15
Benzene 48 3.2 ug/m3 EPA TO-15
Toluene 34 3.8 ug/m3 EPA TO-15
Ethylbenzene 10 4.4 ug/m3 EPA TO-15
m,p-Xylene 25 8.8 ug/m3 EPA TO-15
Styrene 10 4.3 ug/m3 EPA TO-15
o-Xylene 12 4.4 ug/m3 EPA TO-15
1,2,4-Trimethylbenzene 8.0 5.0 ug/m3 EPA TO-15
Page 5 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-10 (E908093-01) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920051Dichlorodifluoromethane (F12)5.0ND
"""""Chloromethane "2.16.3
""""""Dichlorotetrafluoroethane (F114)7.1ND
""""""Vinyl chloride 2.6ND
""""""Bromomethane 16ND
""""""Chloroethane 8.0ND
""""""Trichlorofluoromethane (F11)5.6ND
""""""1,1-Dichloroethene 4.0ND
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND
""""""Methylene chloride (Dichloromethane)3.5ND
"""""Carbon disulfide "6.313
""""""trans-1,2-Dichloroethene 8.0ND
""""""1,1-Dichloroethane 4.1ND
""""""2-Butanone (MEK)30ND
""""""cis-1,2-Dichloroethene 4.0ND
"""""Chloroform "4.96.3
""""""1,1,1-Trichloroethane 5.5ND
""""""1,2-Dichloroethane (EDC)4.1ND
"""""Benzene "3.227
""""""Carbon tetrachloride 6.4ND
""""""Trichloroethene 5.5ND
""""""1,2-Dichloropropane 9.4ND
""""""Bromodichloromethane 6.8ND
""""""cis-1,3-Dichloropropene 4.6ND
""""""4-Methyl-2-pentanone (MIBK)8.3ND
""""""trans-1,3-Dichloropropene 4.6ND
"""""Toluene "3.827
""""""1,1,2-Trichloroethane 5.5ND
""""""2-Hexanone (MBK)8.3ND
""""""Dibromochloromethane 8.6ND
""""""Tetrachloroethene 6.9ND
""""""1,2-Dibromoethane (EDB)7.8ND
""""""1,1,1,2-Tetrachloroethane 7.0ND
""""""Chlorobenzene 4.7ND
"""""Ethylbenzene "4.45.6
"""""m,p-Xylene "8.815
"""""Styrene "4.35.2
"""""o-Xylene "4.46.7
Page 6 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-10 (E908093-01) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920051Bromoform10ND
""""""1,1,2,2-Tetrachloroethane 7.0ND
""""""4-Ethyltoluene 5.0ND
""""""1,3,5-Trimethylbenzene 5.0ND
"""""1,2,4-Trimethylbenzene "5.05.4
""""""1,3-Dichlorobenzene 12ND
""""""1,4-Dichlorobenzene 12ND
""""""1,2-Dichlorobenzene 12ND
""""""1,2,4-Trichlorobenzene 38ND
""""""Hexachlorobutadiene 54ND
""""104 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""104 % 78-125Surrogate: Toluene-d8
""""98.0 % 77-127Surrogate: 4-Bromofluorobenzene
SG-9 (E908093-02) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920051Dichlorodifluoromethane (F12)5.0ND
"""""Chloromethane "2.14.8
""""""Dichlorotetrafluoroethane (F114)7.1ND
"""""Vinyl chloride "2.68.5
""""""Bromomethane 16ND
""""""Chloroethane 8.0ND
""""""Trichlorofluoromethane (F11)5.6ND
""""""1,1-Dichloroethene 4.0ND
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND
""""""Methylene chloride (Dichloromethane)3.5ND
"""""Carbon disulfide "6.322
""""""trans-1,2-Dichloroethene 8.0ND
""""""1,1-Dichloroethane 4.1ND
""""""2-Butanone (MEK)30ND
""""""cis-1,2-Dichloroethene 4.0ND
"""""Chloroform "4.95.3
""""""1,1,1-Trichloroethane 5.5ND
""""""1,2-Dichloroethane (EDC)4.1ND
"""""Benzene "3.245
""""""Carbon tetrachloride 6.4ND
""""""Trichloroethene 5.5ND
""""""1,2-Dichloropropane 9.4ND
Page 7 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-9 (E908093-02) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920051Bromodichloromethane6.8ND
""""""cis-1,3-Dichloropropene 4.6ND
""""""4-Methyl-2-pentanone (MIBK)8.3ND
""""""trans-1,3-Dichloropropene 4.6ND
"""""Toluene "3.832
""""""1,1,2-Trichloroethane 5.5ND
""""""2-Hexanone (MBK)8.3ND
""""""Dibromochloromethane 8.6ND
""""""Tetrachloroethene 6.9ND
""""""1,2-Dibromoethane (EDB)7.8ND
""""""1,1,1,2-Tetrachloroethane 7.0ND
""""""Chlorobenzene 4.7ND
"""""Ethylbenzene "4.49.2
"""""m,p-Xylene "8.824
"""""Styrene "4.312
"""""o-Xylene "4.411
""""""Bromoform 10ND
""""""1,1,2,2-Tetrachloroethane 7.0ND
""""""4-Ethyltoluene 5.0ND
""""""1,3,5-Trimethylbenzene 5.0ND
"""""1,2,4-Trimethylbenzene "5.09.0
""""""1,3-Dichlorobenzene 12ND
""""""1,4-Dichlorobenzene 12ND
""""""1,2-Dichlorobenzene 12ND
""""""1,2,4-Trichlorobenzene 38ND
""""""Hexachlorobutadiene 54ND
""""97.1 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""104 % 78-125Surrogate: Toluene-d8
""""102 % 77-127Surrogate: 4-Bromofluorobenzene
Page 8 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-5 (E908093-03) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EH92005 20-Aug-19 20-Aug-19ug/m3 1Dichlorodifluoromethane (F12)EPA TO-155.050
"""""Chloromethane "2.14.3
"""""Dichlorotetrafluoroethane (F114)"7.193
"""""Vinyl chloride "2.65.8
""""""Bromomethane 16ND
""""""Chloroethane 8.0ND
"""""Trichlorofluoromethane (F11)"5.66.9
""""""1,1-Dichloroethene 4.0ND
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND
""""""Methylene chloride (Dichloromethane)3.5ND
"""""Carbon disulfide "6.313
""""""trans-1,2-Dichloroethene 8.0ND
""""""1,1-Dichloroethane 4.1ND
"""""2-Butanone (MEK)"30110
""""""cis-1,2-Dichloroethene 4.0ND
""""""Chloroform 4.9ND
""""""1,1,1-Trichloroethane 5.5ND
""""""1,2-Dichloroethane (EDC)4.1ND
"""""Benzene "3.251
""""""Carbon tetrachloride 6.4ND
""""""Trichloroethene 5.5ND
""""""1,2-Dichloropropane 9.4ND
""""""Bromodichloromethane 6.8ND
""""""cis-1,3-Dichloropropene 4.6ND
""""""4-Methyl-2-pentanone (MIBK)8.3ND
""""""trans-1,3-Dichloropropene 4.6ND
"""""Toluene "3.829
""""""1,1,2-Trichloroethane 5.5ND
"""""2-Hexanone (MBK)"8.331
""""""Dibromochloromethane 8.6ND
""""""Tetrachloroethene 6.9ND
""""""1,2-Dibromoethane (EDB)7.8ND
""""""1,1,1,2-Tetrachloroethane 7.0ND
""""""Chlorobenzene 4.7ND
"""""Ethylbenzene "4.46.0
"""""m,p-Xylene "8.816
"""""Styrene "4.312
"""""o-Xylene "4.49.5
Page 9 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-5 (E908093-03) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920051Bromoform10ND
""""""1,1,2,2-Tetrachloroethane 7.0ND
""""""4-Ethyltoluene 5.0ND
""""""1,3,5-Trimethylbenzene 5.0ND
"""""1,2,4-Trimethylbenzene "5.07.5
""""""1,3-Dichlorobenzene 12ND
""""""1,4-Dichlorobenzene 12ND
""""""1,2-Dichlorobenzene 12ND
""""""1,2,4-Trichlorobenzene 38ND
""""""Hexachlorobutadiene 54ND
""""95.0 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""102 % 78-125Surrogate: Toluene-d8
""""102 % 77-127Surrogate: 4-Bromofluorobenzene
SG-1 (E908093-04) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EH92005 20-Aug-19 20-Aug-19ug/m3 25Dichlorodifluoromethane (F12)EPA TO-15130130
""""""Chloromethane 52ND
""""""Dichlorotetrafluoroethane (F114)180ND
""""""Vinyl chloride 65ND
""""""Bromomethane 390ND
""""""Chloroethane 200ND
"""""Trichlorofluoromethane (F11)"14049000
""""""1,1-Dichloroethene 100ND
""""""1,1,2-Trichlorotrifluoroethane (F113)190ND
""""""Methylene chloride (Dichloromethane)88ND
""""""Carbon disulfide 160ND
""""""trans-1,2-Dichloroethene 200ND
""""""1,1-Dichloroethane 100ND
""""""2-Butanone (MEK)750ND
""""""cis-1,2-Dichloroethene 100ND
""""""Chloroform 120ND
""""""1,1,1-Trichloroethane 140ND
""""""1,2-Dichloroethane (EDC)100ND
""""""Benzene 81ND
""""""Carbon tetrachloride 160ND
""""""Trichloroethene 140ND
""""""1,2-Dichloropropane 230ND
Page 10 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-1 (E908093-04) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH9200525Bromodichloromethane170ND
""""""cis-1,3-Dichloropropene 120ND
""""""4-Methyl-2-pentanone (MIBK)210ND
""""""trans-1,3-Dichloropropene 120ND
""""""Toluene 95ND
""""""1,1,2-Trichloroethane 140ND
""""""2-Hexanone (MBK)210ND
""""""Dibromochloromethane 220ND
""""""Tetrachloroethene 170ND
""""""1,2-Dibromoethane (EDB)190ND
""""""1,1,1,2-Tetrachloroethane 170ND
""""""Chlorobenzene 120ND
""""""Ethylbenzene 110ND
"""""m,p-Xylene "220250
""""""Styrene 110ND
""""""o-Xylene 110ND
""""""Bromoform 260ND
""""""1,1,2,2-Tetrachloroethane 170ND
""""""4-Ethyltoluene 120ND
""""""1,3,5-Trimethylbenzene 120ND
""""""1,2,4-Trimethylbenzene 120ND
""""""1,3-Dichlorobenzene 300ND
""""""1,4-Dichlorobenzene 300ND
""""""1,2-Dichlorobenzene 300ND
""""""1,2,4-Trichlorobenzene 940ND
""""""Hexachlorobutadiene 1300ND
""""95.0 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""106 % 78-125Surrogate: Toluene-d8
""""98.0 % 77-127Surrogate: 4-Bromofluorobenzene
Page 11 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-2 (E908093-05) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920055Dichlorodifluoromethane (F12)25ND
"""""Chloromethane "1026
""""""Dichlorotetrafluoroethane (F114)35ND
""""""Vinyl chloride 13ND
""""""Bromomethane 79ND
""""""Chloroethane 40ND
""""""Trichlorofluoromethane (F11)28ND
""""""1,1-Dichloroethene 20ND
""""""1,1,2-Trichlorotrifluoroethane (F113)39ND
""""""Methylene chloride (Dichloromethane)18ND
"""""Carbon disulfide "3247
""""""trans-1,2-Dichloroethene 40ND
""""""1,1-Dichloroethane 21ND
""""""2-Butanone (MEK)150ND
""""""cis-1,2-Dichloroethene 20ND
""""""Chloroform 25ND
""""""1,1,1-Trichloroethane 28ND
""""""1,2-Dichloroethane (EDC)21ND
"""""Benzene "1654
""""""Carbon tetrachloride 32ND
""""""Trichloroethene 27ND
""""""1,2-Dichloropropane 47ND
""""""Bromodichloromethane 34ND
""""""cis-1,3-Dichloropropene 23ND
""""""4-Methyl-2-pentanone (MIBK)41ND
""""""trans-1,3-Dichloropropene 23ND
"""""Toluene "1987
""""""1,1,2-Trichloroethane 28ND
""""""2-Hexanone (MBK)41ND
""""""Dibromochloromethane 43ND
""""""Tetrachloroethene 34ND
""""""1,2-Dibromoethane (EDB)39ND
""""""1,1,1,2-Tetrachloroethane 35ND
""""""Chlorobenzene 23ND
"""""Ethylbenzene "2257
"""""m,p-Xylene "44180
""""""Styrene 22ND
"""""o-Xylene "2251
Page 12 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-2 (E908093-05) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920055Bromoform52ND
""""""1,1,2,2-Tetrachloroethane 35ND
"""""4-Ethyltoluene "2525
""""""1,3,5-Trimethylbenzene 25ND
"""""1,2,4-Trimethylbenzene "2539
""""""1,3-Dichlorobenzene 61ND
""""""1,4-Dichlorobenzene 61ND
""""""1,2-Dichlorobenzene 61ND
""""""1,2,4-Trichlorobenzene 190ND
""""""Hexachlorobutadiene 270ND
""""95.5 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""110 % 78-125Surrogate: Toluene-d8
""""97.8 % 77-127Surrogate: 4-Bromofluorobenzene
SG-3 (E908093-06) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EH92005 20-Aug-19 20-Aug-19ug/m3 5Dichlorodifluoromethane (F12)EPA TO-152539
""""""Chloromethane 10ND
""""""Dichlorotetrafluoroethane (F114)35ND
""""""Vinyl chloride 13ND
""""""Bromomethane 79ND
""""""Chloroethane 40ND
""""""Trichlorofluoromethane (F11)28ND
""""""1,1-Dichloroethene 20ND
""""""1,1,2-Trichlorotrifluoroethane (F113)39ND
""""""Methylene chloride (Dichloromethane)18ND
"""""Carbon disulfide "3249
""""""trans-1,2-Dichloroethene 40ND
""""""1,1-Dichloroethane 21ND
""""""2-Butanone (MEK)150ND
""""""cis-1,2-Dichloroethene 20ND
""""""Chloroform 25ND
""""""1,1,1-Trichloroethane 28ND
""""""1,2-Dichloroethane (EDC)21ND
"""""Benzene "16490
""""""Carbon tetrachloride 32ND
""""""Trichloroethene 27ND
""""""1,2-Dichloropropane 47ND
Page 13 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-3 (E908093-06) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920055Bromodichloromethane34ND
""""""cis-1,3-Dichloropropene 23ND
""""""4-Methyl-2-pentanone (MIBK)41ND
""""""trans-1,3-Dichloropropene 23ND
"""""Toluene "1990
""""""1,1,2-Trichloroethane 28ND
""""""2-Hexanone (MBK)41ND
""""""Dibromochloromethane 43ND
""""""Tetrachloroethene 34ND
""""""1,2-Dibromoethane (EDB)39ND
""""""1,1,1,2-Tetrachloroethane 35ND
""""""Chlorobenzene 23ND
"""""Ethylbenzene "22710
"""""m,p-Xylene "44560
""""""Styrene 22ND
"""""o-Xylene "22130
""""""Bromoform 52ND
""""""1,1,2,2-Tetrachloroethane 35ND
"""""4-Ethyltoluene "25200
"""""1,3,5-Trimethylbenzene "25330
"""""1,2,4-Trimethylbenzene "25370
""""""1,3-Dichlorobenzene 61ND
""""""1,4-Dichlorobenzene 61ND
""""""1,2-Dichlorobenzene 61ND
""""""1,2,4-Trichlorobenzene 190ND
""""""Hexachlorobutadiene 270ND
""""98.3 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""107 % 78-125Surrogate: Toluene-d8
""""110 % 77-127Surrogate: 4-Bromofluorobenzene
Page 14 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-4 (E908093-07) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920055Dichlorodifluoromethane (F12)25ND
"""""Chloromethane "1013
""""""Dichlorotetrafluoroethane (F114)35ND
""""""Vinyl chloride 13ND
""""""Bromomethane 79ND
""""""Chloroethane 40ND
""""""Trichlorofluoromethane (F11)28ND
""""""1,1-Dichloroethene 20ND
""""""1,1,2-Trichlorotrifluoroethane (F113)39ND
""""""Methylene chloride (Dichloromethane)18ND
"""""Carbon disulfide "32140
""""""trans-1,2-Dichloroethene 40ND
""""""1,1-Dichloroethane 21ND
""""""2-Butanone (MEK)150ND
""""""cis-1,2-Dichloroethene 20ND
""""""Chloroform 25ND
""""""1,1,1-Trichloroethane 28ND
""""""1,2-Dichloroethane (EDC)21ND
"""""Benzene "1622
""""""Carbon tetrachloride 32ND
""""""Trichloroethene 27ND
""""""1,2-Dichloropropane 47ND
""""""Bromodichloromethane 34ND
""""""cis-1,3-Dichloropropene 23ND
""""""4-Methyl-2-pentanone (MIBK)41ND
""""""trans-1,3-Dichloropropene 23ND
"""""Toluene "1961
""""""1,1,2-Trichloroethane 28ND
""""""2-Hexanone (MBK)41ND
""""""Dibromochloromethane 43ND
""""""Tetrachloroethene 34ND
""""""1,2-Dibromoethane (EDB)39ND
""""""1,1,1,2-Tetrachloroethane 35ND
""""""Chlorobenzene 23ND
"""""Ethylbenzene "2278
"""""m,p-Xylene "44210
""""""Styrene 22ND
"""""o-Xylene "2275
Page 15 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
SG-4 (E908093-07) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920055Bromoform52ND
""""""1,1,2,2-Tetrachloroethane 35ND
"""""4-Ethyltoluene "2538
""""""1,3,5-Trimethylbenzene 25ND
"""""1,2,4-Trimethylbenzene "2562
""""""1,3-Dichlorobenzene 61ND
""""""1,4-Dichlorobenzene 61ND
""""""1,2-Dichlorobenzene 61ND
""""""1,2,4-Trichlorobenzene 190ND
""""""Hexachlorobutadiene 270ND
""""94.7 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""112 % 78-125Surrogate: Toluene-d8
""""93.4 % 77-127Surrogate: 4-Bromofluorobenzene
Dup-2 (E908093-08) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920051Dichlorodifluoromethane (F12)5.0ND
"""""Chloromethane "2.14.5
""""""Dichlorotetrafluoroethane (F114)7.1ND
"""""Vinyl chloride "2.66.1
""""""Bromomethane 16ND
""""""Chloroethane 8.0ND
"""""Trichlorofluoromethane (F11)"5.67.5
""""""1,1-Dichloroethene 4.0ND
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND
""""""Methylene chloride (Dichloromethane)3.5ND
"""""Carbon disulfide "6.323
""""""trans-1,2-Dichloroethene 8.0ND
""""""1,1-Dichloroethane 4.1ND
""""""2-Butanone (MEK)30ND
""""""cis-1,2-Dichloroethene 4.0ND
"""""Chloroform "4.96.9
""""""1,1,1-Trichloroethane 5.5ND
""""""1,2-Dichloroethane (EDC)4.1ND
"""""Benzene "3.248
""""""Carbon tetrachloride 6.4ND
""""""Trichloroethene 5.5ND
""""""1,2-Dichloropropane 9.4ND
Page 16 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes Factor
Dup-2 (E908093-08) Vapor Sampled: 16-Aug-19 Received: 19-Aug-19
EPA TO-1520-Aug-19 20-Aug-19ug/m3 EH920051Bromodichloromethane6.8ND
""""""cis-1,3-Dichloropropene 4.6ND
""""""4-Methyl-2-pentanone (MIBK)8.3ND
""""""trans-1,3-Dichloropropene 4.6ND
"""""Toluene "3.834
""""""1,1,2-Trichloroethane 5.5ND
""""""2-Hexanone (MBK)8.3ND
""""""Dibromochloromethane 8.6ND
""""""Tetrachloroethene 6.9ND
""""""1,2-Dibromoethane (EDB)7.8ND
""""""1,1,1,2-Tetrachloroethane 7.0ND
""""""Chlorobenzene 4.7ND
"""""Ethylbenzene "4.410
"""""m,p-Xylene "8.825
"""""Styrene "4.310
"""""o-Xylene "4.412
""""""Bromoform 10ND
""""""1,1,2,2-Tetrachloroethane 7.0ND
""""""4-Ethyltoluene 5.0ND
""""""1,3,5-Trimethylbenzene 5.0ND
"""""1,2,4-Trimethylbenzene "5.08.0
""""""1,3-Dichlorobenzene 12ND
""""""1,4-Dichlorobenzene 12ND
""""""1,2-Dichlorobenzene 12ND
""""""1,2,4-Trichlorobenzene 38ND
""""""Hexachlorobutadiene 54ND
""""94.4 % 76-134Surrogate: 1,2-Dichloroethane-d4
""""105 % 78-125Surrogate: Toluene-d8
""""99.7 % 77-127Surrogate: 4-Bromofluorobenzene
Page 17 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EH92005 - TO-15
Blank (EH92005-BLK1)Prepared & Analyzed: 20-Aug-19
Dichlorodifluoromethane (F12)ug/m35.0ND
Chloromethane "2.1ND
Dichlorotetrafluoroethane (F114)"7.1ND
Vinyl chloride "2.6ND
Bromomethane "16ND
Chloroethane "8.0ND
Trichlorofluoromethane (F11)"5.6ND
1,1-Dichloroethene "4.0ND
1,1,2-Trichlorotrifluoroethane (F113)"7.7ND
Methylene chloride (Dichloromethane)"3.5ND
Carbon disulfide "6.3ND
trans-1,2-Dichloroethene "8.0ND
1,1-Dichloroethane "4.1ND
2-Butanone (MEK)"30ND
cis-1,2-Dichloroethene "4.0ND
Chloroform "4.9ND
1,1,1-Trichloroethane "5.5ND
1,2-Dichloroethane (EDC)"4.1ND
Benzene "3.2ND
Carbon tetrachloride "6.4ND
Trichloroethene "5.5ND
1,2-Dichloropropane "9.4ND
Bromodichloromethane "6.8ND
cis-1,3-Dichloropropene "4.6ND
4-Methyl-2-pentanone (MIBK)"8.3ND
trans-1,3-Dichloropropene "4.6ND
Toluene "3.8ND
1,1,2-Trichloroethane "5.5ND
2-Hexanone (MBK)"8.3ND
Dibromochloromethane "8.6ND
Tetrachloroethene "6.9ND
1,2-Dibromoethane (EDB)"7.8ND
1,1,1,2-Tetrachloroethane "7.0ND
Chlorobenzene "4.7ND
Page 18 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EH92005 - TO-15
Blank (EH92005-BLK1)Prepared & Analyzed: 20-Aug-19
Ethylbenzene ug/m34.4ND
m,p-Xylene "8.8ND
Styrene "4.3ND
o-Xylene "4.4ND
Bromoform "10ND
1,1,2,2-Tetrachloroethane "7.0ND
4-Ethyltoluene "5.0ND
1,3,5-Trimethylbenzene "5.0ND
1,2,4-Trimethylbenzene "5.0ND
1,3-Dichlorobenzene "12ND
1,4-Dichlorobenzene "12ND
1,2-Dichlorobenzene "12ND
1,2,4-Trichlorobenzene "38ND
Hexachlorobutadiene "54ND
" 214 76-134Surrogate: 1,2-Dichloroethane-d4 102219
" 208 78-125Surrogate: Toluene-d8 99.6207
" 363 77-127Surrogate: 4-Bromofluorobenzene 95.6347
LCS (EH92005-BS1)Prepared & Analyzed: 20-Aug-19
Dichlorodifluoromethane (F12)ug/m3 101 59-1281045.0110
Vinyl chloride " 52.0 64-12793.72.649
Chloroethane " 53.6 63-12784.88.045
Trichlorofluoromethane (F11)" 113 62-12685.95.697
1,1-Dichloroethene " 80.8 61-13389.54.072
1,1,2-Trichlorotrifluoroethane (F113)" 155 66-12690.67.7140
Methylene chloride (Dichloromethane)" 70.8 62-11583.33.559
trans-1,2-Dichloroethene " 80.8 67-12488.18.071
1,1-Dichloroethane " 82.4 68-12687.74.172
cis-1,2-Dichloroethene " 80.0 70-12192.44.074
Chloroform " 99.2 68-12389.44.989
1,1,1-Trichloroethane " 111 68-12594.35.5100
1,2-Dichloroethane (EDC)" 82.4 65-12892.64.176
Benzene " 64.8 69-11989.33.258
Page 19 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EH92005 - TO-15
LCS (EH92005-BS1)Prepared & Analyzed: 20-Aug-19
Carbon tetrachloride ug/m3 128 68-13291.26.4120
Trichloroethene " 110 71-12392.25.5100
Toluene " 76.8 66-11986.93.867
1,1,2-Trichloroethane " 111 73-11991.75.5100
Tetrachloroethene " 138 66-12496.76.9130
1,1,1,2-Tetrachloroethane " 140 67-12997.17.0140
Ethylbenzene " 88.4 70-1241064.493
m,p-Xylene " 88.4 61-1341028.890
o-Xylene " 88.4 67-1251024.491
1,1,2,2-Tetrachloroethane " 140 65-12796.57.0140
" 214 76-134Surrogate: 1,2-Dichloroethane-d4 105224
" 208 78-125Surrogate: Toluene-d8 100208
" 363 77-127Surrogate: 4-Bromofluorobenzene 108391
LCS Dup (EH92005-BSD1)Prepared & Analyzed: 20-Aug-19
Dichlorodifluoromethane (F12)ug/m3 101 2559-128103 1.645.0100
Vinyl chloride " 52.0 2564-12792.3 1.452.648
Chloroethane " 53.6 2563-12769.2 20.38.037
Trichlorofluoromethane (F11)" 113 2562-12684.7 1.405.696
1,1-Dichloroethene " 80.8 2561-13389.9 0.5004.073
1,1,2-Trichlorotrifluoroethane (F113)" 155 2566-12690.1 0.5507.7140
Methylene chloride (Dichloromethane)" 70.8 2562-11584.7 1.663.560
trans-1,2-Dichloroethene " 80.8 2567-12488.8 0.8448.072
1,1-Dichloroethane " 82.4 2568-12688.5 0.9624.173
cis-1,2-Dichloroethene " 80.0 2570-12192.3 0.1094.074
Chloroform " 99.2 2568-12388.7 0.7834.988
1,1,1-Trichloroethane " 111 2568-12593.4 0.8995.5100
1,2-Dichloroethane (EDC)" 82.4 2565-12890.7 2.074.175
Benzene " 64.8 2569-11990.1 0.8913.258
Carbon tetrachloride " 128 2568-13293.3 2.336.4120
Trichloroethene " 110 2571-12393.3 1.185.5100
Toluene " 76.8 2566-11986.5 0.5163.866
1,1,2-Trichloroethane " 111 2573-11991.7 0.005.5100
Page 20 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EH92005 - TO-15
LCS Dup (EH92005-BSD1)Prepared & Analyzed: 20-Aug-19
Tetrachloroethene ug/m3 138 2566-12496.9 0.2066.9130
1,1,1,2-Tetrachloroethane " 140 2567-12997.6 0.5637.0140
Ethylbenzene " 88.4 2570-124109 3.204.496
m,p-Xylene " 88.4 2561-134106 3.948.893
o-Xylene " 88.4 2567-125105 2.874.493
1,1,2,2-Tetrachloroethane " 140 2565-12798.8 2.347.0140
" 214 76-134Surrogate: 1,2-Dichloroethane-d4 103220
" 208 78-125Surrogate: Toluene-d8 100208
" 363 77-127Surrogate: 4-Bromofluorobenzene 110399
Page 21 of 22
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Greensboro
4811 Koger Blvd.
ECS081919-11
HP Stadium Phase II / High Point
Randy CavallierGreensboro, NC 27407 21-Aug-19 12:03
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
H&P Mobile
Geochemistry Inc.
Notes and Definitions
Percent Recovery
Relative Percent DifferenceRPD
%REC
Method Detection LimitMDL
Analyte NOT DETECTED at or above the reporting limitND
Leak Check CompoundLCC
Appendix
H&P Mobile Geochemistry, Inc. is approved as an Environmental Testing Laboratory and Mobile Laboratory in accordance with the DoD-ELAP Program
and ISO/IEC 17025:2005 programs through PJLA, accreditation number 69070 for EPA Method TO-15, H&P Method TO-15, EPA Method 8260B and
H&P 8260SV.
H&P is approved by the State of California as an Environmental Laboratory and Mobile Laboratory in conformance with the Environmental Laboratory
Accreditation Program (ELAP) for the category of Volatile and Semi-Volatile Organic Chemistry of Hazardous Waste, certification numbers 2740, 2741,
2743 & 2745.
H&P is approved by the State of Louisiana Department of Environmental Quality under the National Environmental Laboratory Accreditation Conference
(NELAC) certification number 04138
The complete list of stationary and mobile laboratory certifications along with the fields of testing (FOTs) and analyte lists are available at
www.handpmg.com/about/certifications.
All soil results are reported in wet weight.
Page 22 of 22
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Z Geochemistry, Inc.
2470 Impala Drive, Carlsbad, CA 92010
& Field Office - Signal Hill, CA
W handpmg.com E info©handpmg.com

DATE: F11 Wi
Page Hof 1 VAPOR I AIR Chain of Custody

Lab Client and Project Information
Lab Client/Consultant: E 6., 3. 0 ,41-1,„.11 LLp Project Name / #: I R 5-42J; /°1A--te 71-
Lab Client Project Manager: . `t c'i 1 . . 141? IS 1 ir,e Project Location: , iv v.„:1___
Lab Client Address:Report
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Lab Client City, State, Zip: c, d y CLA4 i/AkS
Phone Number: -S? b TA't -2/ C U
Reporting Requirements Turnaround Time Sampler Information
[Standard Report q Level III
q Excel EDD q Other EDD:
q Level IV q Standard (7 days for preliminary
report, 10 days for final report)
Rush (specify): q f Ivy
Sampler(s). /1
( ''4/-".
Signature:
/
q CA Geotracker Global ID: Date: ,.ht,/ i i
Sample Receipt (Lab Use Only)
Date Recd (ii [11 Control #. tq-oto (13,0
H&P Project # EcSfAll I
Lab Work Order # q a J1 fl 3
Sample Intact: f Yes [11 No q See Notes Below
Receipt Gauge ID: 3o005 Temp: 1„R-I-.
Outside Lab:
Receipt Notes/Tracking #:
1-1(00 Ctitri
Lab PM Initials: Os'
Additional Instructions to Laboratory:
* Preferred V09.mits (please choose one):
q p.g/L µg/m3 q ppbv q ppmv
FIELD POINT SAMPLE TYPE Indoor Air (IA), Ambient
NAME DATE TIME Air (M), Subslab (SS),
(if applicable) mm/dd/yy 24hr clock Soil Vapor (SV) SAMPLE NAME
CONTAINER
SIZE & TYPE
400mL/1L/6L
Summa, Tedlar,
Tube, etc.
C >
W 10 0 -C CO
CO 0_ c0 q Methane by EPA 8015m -Z7-5
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Approved/Relinquished by: 7: 5 Time: / 7 tic,
Approved/Relinquished by: Corrrzi Dlef: Time:
Approved/Relinquished by Company: Date: Time:
Company. Date Time:

*atEl Timei s. riov\
Received by: Company: Date: Time:
1:;:rk:k
Received by4.1)rli
Received by.
Connt;,,f)
'Approval constitutes as authorization to proceed with analysis and acceptance of conditions on back Appendix 6A1, Rev 1/9/2019, Effective 1/21/2019
#=CL#
August 21, 2019
LIMS USE: FR - RANDY CAVALLIER
LIMS OBJECT ID: 92441752
92441752
Project:
Pace Project No.:
RE:
Mr. Randy Cavallier
ECS Southeast, LLP
4811 Koger Blvd.
Greensboro, NC 27407
HP Stadium Phase 2
Dear Mr. Cavallier:
Enclosed are the analytical results for sample(s) received by the laboratory on August 16, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 39
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 39
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92441752001 GW-9 MS/MSD EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92441752002 GW-8 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92441752003 GW-2 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92441752004 GW-1 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
92441752005 Dup-1 EPA 6010D 7 PASI-ASH1
EPA 7470A 1 PASI-AJMW1
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-9 MS/MSD Lab ID:92441752001 Collected:08/15/19 13:50 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/21/19 10:55 7440-38-208/20/19 17:3410.0 1
Barium 37.3 ug/L 08/21/19 10:55 7440-39-308/20/19 17:345.0 1
Cadmium ND ug/L 08/21/19 10:55 7440-43-908/20/19 17:341.0 1
Chromium 6.9 ug/L 08/21/19 10:55 7440-47-308/20/19 17:345.0 1
Lead ND ug/L 08/21/19 10:55 7439-92-108/20/19 17:345.0 1
Selenium ND ug/L 08/21/19 10:55 7782-49-208/20/19 17:3410.0 1
Silver ND ug/L 08/21/19 10:55 7440-22-408/20/19 17:345.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/21/19 09:24 7439-97-608/20/19 13:540.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/20/19 17:07 83-32-908/20/19 16:4010.0 1
Acenaphthylene ND ug/L 08/20/19 17:07 208-96-808/20/19 16:4010.0 1
Aniline ND ug/L 08/20/19 17:07 62-53-308/20/19 16:4010.0 1
Anthracene ND ug/L 08/20/19 17:07 120-12-708/20/19 16:4010.0 1
Benzo(a)anthracene ND ug/L 08/20/19 17:07 56-55-308/20/19 16:4010.0 1
Benzo(a)pyrene ND ug/L 08/20/19 17:07 50-32-808/20/19 16:4010.0 1
Benzo(b)fluoranthene ND ug/L 08/20/19 17:07 205-99-208/20/19 16:4010.0 1
Benzo(g,h,i)perylene ND ug/L 08/20/19 17:07 191-24-208/20/19 16:4010.0 1
Benzo(k)fluoranthene ND ug/L 08/20/19 17:07 207-08-908/20/19 16:4010.0 1
Benzoic Acid ND ug/L 08/20/19 17:07 65-85-008/20/19 16:4050.0 1
Benzyl alcohol ND ug/L 08/20/19 17:07 100-51-608/20/19 16:4020.0 1
4-Bromophenylphenyl ether ND ug/L 08/20/19 17:07 101-55-308/20/19 16:4010.0 1
Butylbenzylphthalate ND ug/L 08/20/19 17:07 85-68-708/20/19 16:4010.0 1
4-Chloro-3-methylphenol ND ug/L 08/20/19 17:07 59-50-708/20/19 16:4020.0 1
4-Chloroaniline ND ug/L 08/20/19 17:07 106-47-808/20/19 16:4020.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/20/19 17:07 111-91-108/20/19 16:4010.0 1
bis(2-Chloroethyl) ether ND ug/L 08/20/19 17:07 111-44-408/20/19 16:4010.0 1
2-Chloronaphthalene ND ug/L 08/20/19 17:07 91-58-708/20/19 16:4010.0 1
2-Chlorophenol ND ug/L 08/20/19 17:07 95-57-808/20/19 16:4010.0 1
4-Chlorophenylphenyl ether ND ug/L 08/20/19 17:07 7005-72-308/20/19 16:4010.0 1
Chrysene ND ug/L 08/20/19 17:07 218-01-908/20/19 16:4010.0 1
Dibenz(a,h)anthracene ND ug/L 08/20/19 17:07 53-70-308/20/19 16:4010.0 1
Dibenzofuran ND ug/L 08/20/19 17:07 132-64-908/20/19 16:4010.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 17:07 95-50-108/20/19 16:4010.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 17:07 541-73-108/20/19 16:4010.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 17:07 106-46-708/20/19 16:4010.0 1
3,3'-Dichlorobenzidine ND ug/L 08/20/19 17:07 91-94-108/20/19 16:4020.0 1
2,4-Dichlorophenol ND ug/L 08/20/19 17:07 120-83-208/20/19 16:4010.0 1
Diethylphthalate ND ug/L 08/20/19 17:07 84-66-208/20/19 16:4010.0 1
2,4-Dimethylphenol ND ug/L 08/20/19 17:07 105-67-908/20/19 16:4010.0 1
Dimethylphthalate ND ug/L 08/20/19 17:07 131-11-308/20/19 16:4010.0 1
Di-n-butylphthalate ND ug/L 08/20/19 17:07 84-74-208/20/19 16:4010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/20/19 17:07 534-52-108/20/19 16:4020.0 1
2,4-Dinitrophenol ND ug/L 08/20/19 17:07 51-28-508/20/19 16:4050.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-9 MS/MSD Lab ID:92441752001 Collected:08/15/19 13:50 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dinitrotoluene ND ug/L 08/20/19 17:07 121-14-208/20/19 16:4010.0 1
2,6-Dinitrotoluene ND ug/L 08/20/19 17:07 606-20-208/20/19 16:4010.0 1
Di-n-octylphthalate ND ug/L 08/20/19 17:07 117-84-008/20/19 16:4010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/20/19 17:07 117-81-708/20/19 16:406.0 1
Fluoranthene ND ug/L 08/20/19 17:07 206-44-008/20/19 16:4010.0 1
Fluorene ND ug/L 08/20/19 17:07 86-73-708/20/19 16:4010.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 17:07 87-68-308/20/19 16:4010.0 1
Hexachlorobenzene ND ug/L 08/20/19 17:07 118-74-108/20/19 16:4010.0 1
Hexachlorocyclopentadiene ND ug/L 08/20/19 17:07 77-47-408/20/19 16:4010.0 1
Hexachloroethane ND ug/L 08/20/19 17:07 67-72-108/20/19 16:4010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/20/19 17:07 193-39-508/20/19 16:4010.0 1
Isophorone ND ug/L 08/20/19 17:07 78-59-108/20/19 16:4010.0 1
1-Methylnaphthalene ND ug/L 08/20/19 17:07 90-12-008/20/19 16:4010.0 1
2-Methylnaphthalene ND ug/L 08/20/19 17:07 91-57-608/20/19 16:4010.0 1
2-Methylphenol(o-Cresol)ND ug/L 08/20/19 17:07 95-48-708/20/19 16:4010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/20/19 17:07 15831-10-408/20/19 16:4010.0 1
Naphthalene ND ug/L 08/20/19 17:07 91-20-308/20/19 16:4010.0 1
2-Nitroaniline ND ug/L 08/20/19 17:07 88-74-408/20/19 16:4020.0 1
3-Nitroaniline ND ug/L 08/20/19 17:07 99-09-208/20/19 16:4020.0 1
4-Nitroaniline ND ug/L 08/20/19 17:07 100-01-608/20/19 16:4020.0 1
Nitrobenzene ND ug/L 08/20/19 17:07 98-95-308/20/19 16:4010.0 1
2-Nitrophenol ND ug/L 08/20/19 17:07 88-75-508/20/19 16:4010.0 1
4-Nitrophenol ND ug/L 08/20/19 17:07 100-02-708/20/19 16:4050.0 1
N-Nitrosodimethylamine ND ug/L 08/20/19 17:07 62-75-908/20/19 16:4010.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/20/19 17:07 621-64-708/20/19 16:4010.0 1
N-Nitrosodiphenylamine ND ug/L 08/20/19 17:07 86-30-608/20/19 16:4010.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/20/19 17:07 108-60-108/20/19 16:4010.0 1
Pentachlorophenol ND ug/L 08/20/19 17:07 87-86-508/20/19 16:4025.0 1
Phenanthrene ND ug/L 08/20/19 17:07 85-01-808/20/19 16:4010.0 1
Phenol ND ug/L 08/20/19 17:07 108-95-208/20/19 16:4010.0 1
Pyrene ND ug/L 08/20/19 17:07 129-00-008/20/19 16:4010.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 17:07 120-82-108/20/19 16:4010.0 1
2,4,5-Trichlorophenol ND ug/L 08/20/19 17:07 95-95-408/20/19 16:4010.0 1
2,4,6-Trichlorophenol ND ug/L 08/20/19 17:07 88-06-208/20/19 16:4010.0 1
Surrogates
Nitrobenzene-d5 (S)43 %08/20/19 17:07 4165-60-008/20/19 16:4013-130 1
2-Fluorobiphenyl (S)40 %08/20/19 17:07 321-60-808/20/19 16:4013-130 1
Terphenyl-d14 (S)98 %08/20/19 17:07 1718-51-008/20/19 16:4025-130 1
Phenol-d6 (S)23 %08/20/19 17:07 13127-88-308/20/19 16:4010-130 1
2-Fluorophenol (S)33 %08/20/19 17:07 367-12-408/20/19 16:4010-130 1
2,4,6-Tribromophenol (S)64 %08/20/19 17:07 118-79-608/20/19 16:4010-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/20/19 16:37 67-64-125.0 1
Benzene ND ug/L 08/20/19 16:37 71-43-21.0 1
Bromobenzene ND ug/L 08/20/19 16:37 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/19 16:37 74-97-51.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-9 MS/MSD Lab ID:92441752001 Collected:08/15/19 13:50 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Bromodichloromethane ND ug/L 08/20/19 16:37 75-27-41.0 1
Bromoform ND ug/L 08/20/19 16:37 75-25-21.0 1
Bromomethane ND ug/L 08/20/19 16:37 74-83-9 v2,v32.0 1
2-Butanone (MEK)ND ug/L 08/20/19 16:37 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/19 16:37 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/19 16:37 108-90-71.0 1
Chloroethane ND ug/L 08/20/19 16:37 75-00-31.0 1
Chloroform ND ug/L 08/20/19 16:37 67-66-35.0 1
Chloromethane ND ug/L 08/20/19 16:37 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/20/19 16:37 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/19 16:37 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/19 16:37 96-12-85.0 1
Dibromochloromethane ND ug/L 08/20/19 16:37 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/19 16:37 106-93-41.0 1
Dibromomethane ND ug/L 08/20/19 16:37 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 16:37 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 16:37 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 16:37 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/19 16:37 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/19 16:37 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/19 16:37 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/19 16:37 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/19 16:37 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/19 16:37 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/19 16:37 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/19 16:37 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/19 16:37 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/19 16:37 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/19 16:37 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/19 16:37 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/19 16:37 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/19 16:37 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 16:37 87-68-31.0 1
2-Hexanone ND ug/L 08/20/19 16:37 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/19 16:37 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/19 16:37 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/19 16:37 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/19 16:37 1634-04-41.0 1
Naphthalene ND ug/L 08/20/19 16:37 91-20-31.0 1
Styrene ND ug/L 08/20/19 16:37 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/19 16:37 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/19 16:37 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/19 16:37 127-18-41.0 1
Toluene ND ug/L 08/20/19 16:37 108-88-3 v21.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/19 16:37 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 16:37 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/19 16:37 71-55-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-9 MS/MSD Lab ID:92441752001 Collected:08/15/19 13:50 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
1,1,2-Trichloroethane ND ug/L 08/20/19 16:37 79-00-51.0 1
Trichloroethene ND ug/L 08/20/19 16:37 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/19 16:37 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/19 16:37 96-18-4 v31.0 1
Vinyl acetate ND ug/L 08/20/19 16:37 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/19 16:37 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/19 16:37 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/19 16:37 179601-23-12.0 1
o-Xylene ND ug/L 08/20/19 16:37 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)87 %08/20/19 16:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %08/20/19 16:37 17060-07-070-130 1
Toluene-d8 (S)111 %08/20/19 16:37 2037-26-570-130 1
Sample:GW-8 Lab ID:92441752002 Collected:08/15/19 14:25 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/21/19 11:08 7440-38-208/20/19 17:3410.0 1
Barium 24.1 ug/L 08/21/19 11:08 7440-39-308/20/19 17:345.0 1
Cadmium ND ug/L 08/21/19 11:08 7440-43-908/20/19 17:341.0 1
Chromium ND ug/L 08/21/19 11:08 7440-47-308/20/19 17:345.0 1
Lead ND ug/L 08/21/19 11:08 7439-92-108/20/19 17:345.0 1
Selenium ND ug/L 08/21/19 11:08 7782-49-208/20/19 17:3410.0 1
Silver ND ug/L 08/21/19 11:08 7440-22-408/20/19 17:345.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/21/19 09:31 7439-97-608/20/19 13:540.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/20/19 17:58 83-32-908/20/19 16:4010.0 1
Acenaphthylene ND ug/L 08/20/19 17:58 208-96-808/20/19 16:4010.0 1
Aniline ND ug/L 08/20/19 17:58 62-53-308/20/19 16:4010.0 1
Anthracene ND ug/L 08/20/19 17:58 120-12-708/20/19 16:4010.0 1
Benzo(a)anthracene ND ug/L 08/20/19 17:58 56-55-308/20/19 16:4010.0 1
Benzo(a)pyrene ND ug/L 08/20/19 17:58 50-32-808/20/19 16:4010.0 1
Benzo(b)fluoranthene ND ug/L 08/20/19 17:58 205-99-208/20/19 16:4010.0 1
Benzo(g,h,i)perylene ND ug/L 08/20/19 17:58 191-24-208/20/19 16:4010.0 1
Benzo(k)fluoranthene ND ug/L 08/20/19 17:58 207-08-908/20/19 16:4010.0 1
Benzoic Acid ND ug/L 08/20/19 17:58 65-85-008/20/19 16:4050.0 1
Benzyl alcohol ND ug/L 08/20/19 17:58 100-51-608/20/19 16:4020.0 1
4-Bromophenylphenyl ether ND ug/L 08/20/19 17:58 101-55-308/20/19 16:4010.0 1
Butylbenzylphthalate ND ug/L 08/20/19 17:58 85-68-708/20/19 16:4010.0 1
4-Chloro-3-methylphenol ND ug/L 08/20/19 17:58 59-50-708/20/19 16:4020.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-8 Lab ID:92441752002 Collected:08/15/19 14:25 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
4-Chloroaniline ND ug/L 08/20/19 17:58 106-47-808/20/19 16:4020.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/20/19 17:58 111-91-108/20/19 16:4010.0 1
bis(2-Chloroethyl) ether ND ug/L 08/20/19 17:58 111-44-408/20/19 16:4010.0 1
2-Chloronaphthalene ND ug/L 08/20/19 17:58 91-58-708/20/19 16:4010.0 1
2-Chlorophenol ND ug/L 08/20/19 17:58 95-57-808/20/19 16:4010.0 1
4-Chlorophenylphenyl ether ND ug/L 08/20/19 17:58 7005-72-308/20/19 16:4010.0 1
Chrysene ND ug/L 08/20/19 17:58 218-01-908/20/19 16:4010.0 1
Dibenz(a,h)anthracene ND ug/L 08/20/19 17:58 53-70-308/20/19 16:4010.0 1
Dibenzofuran ND ug/L 08/20/19 17:58 132-64-908/20/19 16:4010.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 17:58 95-50-108/20/19 16:4010.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 17:58 541-73-108/20/19 16:4010.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 17:58 106-46-708/20/19 16:4010.0 1
3,3'-Dichlorobenzidine ND ug/L 08/20/19 17:58 91-94-108/20/19 16:4020.0 1
2,4-Dichlorophenol ND ug/L 08/20/19 17:58 120-83-208/20/19 16:4010.0 1
Diethylphthalate ND ug/L 08/20/19 17:58 84-66-208/20/19 16:4010.0 1
2,4-Dimethylphenol ND ug/L 08/20/19 17:58 105-67-908/20/19 16:4010.0 1
Dimethylphthalate ND ug/L 08/20/19 17:58 131-11-308/20/19 16:4010.0 1
Di-n-butylphthalate ND ug/L 08/20/19 17:58 84-74-208/20/19 16:4010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/20/19 17:58 534-52-108/20/19 16:4020.0 1
2,4-Dinitrophenol ND ug/L 08/20/19 17:58 51-28-508/20/19 16:4050.0 1
2,4-Dinitrotoluene ND ug/L 08/20/19 17:58 121-14-208/20/19 16:4010.0 1
2,6-Dinitrotoluene ND ug/L 08/20/19 17:58 606-20-208/20/19 16:4010.0 1
Di-n-octylphthalate ND ug/L 08/20/19 17:58 117-84-008/20/19 16:4010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/20/19 17:58 117-81-708/20/19 16:406.0 1
Fluoranthene ND ug/L 08/20/19 17:58 206-44-008/20/19 16:4010.0 1
Fluorene ND ug/L 08/20/19 17:58 86-73-708/20/19 16:4010.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 17:58 87-68-308/20/19 16:4010.0 1
Hexachlorobenzene ND ug/L 08/20/19 17:58 118-74-108/20/19 16:4010.0 1
Hexachlorocyclopentadiene ND ug/L 08/20/19 17:58 77-47-408/20/19 16:4010.0 1
Hexachloroethane ND ug/L 08/20/19 17:58 67-72-108/20/19 16:4010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/20/19 17:58 193-39-508/20/19 16:4010.0 1
Isophorone ND ug/L 08/20/19 17:58 78-59-108/20/19 16:4010.0 1
1-Methylnaphthalene ND ug/L 08/20/19 17:58 90-12-008/20/19 16:4010.0 1
2-Methylnaphthalene ND ug/L 08/20/19 17:58 91-57-608/20/19 16:4010.0 1
2-Methylphenol(o-Cresol)ND ug/L 08/20/19 17:58 95-48-708/20/19 16:4010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/20/19 17:58 15831-10-408/20/19 16:4010.0 1
Naphthalene ND ug/L 08/20/19 17:58 91-20-308/20/19 16:4010.0 1
2-Nitroaniline ND ug/L 08/20/19 17:58 88-74-408/20/19 16:4020.0 1
3-Nitroaniline ND ug/L 08/20/19 17:58 99-09-208/20/19 16:4020.0 1
4-Nitroaniline ND ug/L 08/20/19 17:58 100-01-608/20/19 16:4020.0 1
Nitrobenzene ND ug/L 08/20/19 17:58 98-95-308/20/19 16:4010.0 1
2-Nitrophenol ND ug/L 08/20/19 17:58 88-75-508/20/19 16:4010.0 1
4-Nitrophenol ND ug/L 08/20/19 17:58 100-02-708/20/19 16:4050.0 1
N-Nitrosodimethylamine ND ug/L 08/20/19 17:58 62-75-908/20/19 16:4010.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/20/19 17:58 621-64-708/20/19 16:4010.0 1
N-Nitrosodiphenylamine ND ug/L 08/20/19 17:58 86-30-608/20/19 16:4010.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/20/19 17:58 108-60-108/20/19 16:4010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-8 Lab ID:92441752002 Collected:08/15/19 14:25 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Pentachlorophenol ND ug/L 08/20/19 17:58 87-86-508/20/19 16:4025.0 1
Phenanthrene ND ug/L 08/20/19 17:58 85-01-808/20/19 16:4010.0 1
Phenol ND ug/L 08/20/19 17:58 108-95-208/20/19 16:4010.0 1
Pyrene ND ug/L 08/20/19 17:58 129-00-008/20/19 16:4010.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 17:58 120-82-108/20/19 16:4010.0 1
2,4,5-Trichlorophenol ND ug/L 08/20/19 17:58 95-95-408/20/19 16:4010.0 1
2,4,6-Trichlorophenol ND ug/L 08/20/19 17:58 88-06-208/20/19 16:4010.0 1
Surrogates
Nitrobenzene-d5 (S)62 %08/20/19 17:58 4165-60-008/20/19 16:4013-130 1
2-Fluorobiphenyl (S)60 %08/20/19 17:58 321-60-808/20/19 16:4013-130 1
Terphenyl-d14 (S)92 %08/20/19 17:58 1718-51-008/20/19 16:4025-130 1
Phenol-d6 (S)36 %08/20/19 17:58 13127-88-308/20/19 16:4010-130 1
2-Fluorophenol (S)50 %08/20/19 17:58 367-12-408/20/19 16:4010-130 1
2,4,6-Tribromophenol (S)68 %08/20/19 17:58 118-79-608/20/19 16:4010-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/20/19 16:55 67-64-125.0 1
Benzene ND ug/L 08/20/19 16:55 71-43-21.0 1
Bromobenzene ND ug/L 08/20/19 16:55 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/19 16:55 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/19 16:55 75-27-41.0 1
Bromoform ND ug/L 08/20/19 16:55 75-25-21.0 1
Bromomethane ND ug/L 08/20/19 16:55 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/20/19 16:55 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/19 16:55 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/19 16:55 108-90-71.0 1
Chloroethane ND ug/L 08/20/19 16:55 75-00-31.0 1
Chloroform ND ug/L 08/20/19 16:55 67-66-35.0 1
Chloromethane ND ug/L 08/20/19 16:55 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/20/19 16:55 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/19 16:55 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/19 16:55 96-12-85.0 1
Dibromochloromethane ND ug/L 08/20/19 16:55 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/19 16:55 106-93-41.0 1
Dibromomethane ND ug/L 08/20/19 16:55 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 16:55 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 16:55 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 16:55 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/19 16:55 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/19 16:55 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/19 16:55 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/19 16:55 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/19 16:55 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/19 16:55 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/19 16:55 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/19 16:55 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/19 16:55 594-20-71.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-8 Lab ID:92441752002 Collected:08/15/19 14:25 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
1,1-Dichloropropene ND ug/L 08/20/19 16:55 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/19 16:55 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/19 16:55 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/19 16:55 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/19 16:55 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 16:55 87-68-31.0 1
2-Hexanone ND ug/L 08/20/19 16:55 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/19 16:55 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/19 16:55 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/19 16:55 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/19 16:55 1634-04-41.0 1
Naphthalene ND ug/L 08/20/19 16:55 91-20-31.0 1
Styrene ND ug/L 08/20/19 16:55 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/19 16:55 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/19 16:55 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/19 16:55 127-18-41.0 1
Toluene ND ug/L 08/20/19 16:55 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/19 16:55 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 16:55 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/19 16:55 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/19 16:55 79-00-51.0 1
Trichloroethene ND ug/L 08/20/19 16:55 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/19 16:55 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/19 16:55 96-18-4 v21.0 1
Vinyl acetate ND ug/L 08/20/19 16:55 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/19 16:55 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/19 16:55 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/19 16:55 179601-23-12.0 1
o-Xylene ND ug/L 08/20/19 16:55 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)96 %08/20/19 16:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)95 %08/20/19 16:55 17060-07-070-130 1
Toluene-d8 (S)101 %08/20/19 16:55 2037-26-570-130 1
Sample:GW-2 Lab ID:92441752003 Collected:08/15/19 15:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/21/19 11:14 7440-38-208/20/19 17:3410.0 1
Barium 232 ug/L 08/21/19 11:14 7440-39-308/20/19 17:345.0 1
Cadmium ND ug/L 08/21/19 11:14 7440-43-908/20/19 17:341.0 1
Chromium 32.9 ug/L 08/21/19 11:14 7440-47-308/20/19 17:345.0 1
Lead 7.4 ug/L 08/21/19 11:14 7439-92-108/20/19 17:345.0 1
Selenium ND ug/L 08/21/19 11:14 7782-49-208/20/19 17:3410.0 1
Silver ND ug/L 08/21/19 11:14 7440-22-408/20/19 17:345.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-2 Lab ID:92441752003 Collected:08/15/19 15:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/21/19 09:34 7439-97-608/20/19 13:540.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/20/19 18:48 83-32-908/20/19 16:4010.0 1
Acenaphthylene ND ug/L 08/20/19 18:48 208-96-808/20/19 16:4010.0 1
Aniline ND ug/L 08/20/19 18:48 62-53-308/20/19 16:4010.0 1
Anthracene ND ug/L 08/20/19 18:48 120-12-708/20/19 16:4010.0 1
Benzo(a)anthracene ND ug/L 08/20/19 18:48 56-55-308/20/19 16:4010.0 1
Benzo(a)pyrene ND ug/L 08/20/19 18:48 50-32-808/20/19 16:4010.0 1
Benzo(b)fluoranthene ND ug/L 08/20/19 18:48 205-99-208/20/19 16:4010.0 1
Benzo(g,h,i)perylene ND ug/L 08/20/19 18:48 191-24-208/20/19 16:4010.0 1
Benzo(k)fluoranthene ND ug/L 08/20/19 18:48 207-08-908/20/19 16:4010.0 1
Benzoic Acid ND ug/L 08/20/19 18:48 65-85-008/20/19 16:4050.0 1
Benzyl alcohol ND ug/L 08/20/19 18:48 100-51-608/20/19 16:4020.0 1
4-Bromophenylphenyl ether ND ug/L 08/20/19 18:48 101-55-308/20/19 16:4010.0 1
Butylbenzylphthalate ND ug/L 08/20/19 18:48 85-68-708/20/19 16:4010.0 1
4-Chloro-3-methylphenol ND ug/L 08/20/19 18:48 59-50-708/20/19 16:4020.0 1
4-Chloroaniline ND ug/L 08/20/19 18:48 106-47-808/20/19 16:4020.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/20/19 18:48 111-91-108/20/19 16:4010.0 1
bis(2-Chloroethyl) ether ND ug/L 08/20/19 18:48 111-44-408/20/19 16:4010.0 1
2-Chloronaphthalene ND ug/L 08/20/19 18:48 91-58-708/20/19 16:4010.0 1
2-Chlorophenol ND ug/L 08/20/19 18:48 95-57-808/20/19 16:4010.0 1
4-Chlorophenylphenyl ether ND ug/L 08/20/19 18:48 7005-72-308/20/19 16:4010.0 1
Chrysene ND ug/L 08/20/19 18:48 218-01-908/20/19 16:4010.0 1
Dibenz(a,h)anthracene ND ug/L 08/20/19 18:48 53-70-308/20/19 16:4010.0 1
Dibenzofuran ND ug/L 08/20/19 18:48 132-64-908/20/19 16:4010.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 18:48 95-50-108/20/19 16:4010.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 18:48 541-73-108/20/19 16:4010.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 18:48 106-46-708/20/19 16:4010.0 1
3,3'-Dichlorobenzidine ND ug/L 08/20/19 18:48 91-94-108/20/19 16:4020.0 1
2,4-Dichlorophenol ND ug/L 08/20/19 18:48 120-83-208/20/19 16:4010.0 1
Diethylphthalate ND ug/L 08/20/19 18:48 84-66-208/20/19 16:4010.0 1
2,4-Dimethylphenol ND ug/L 08/20/19 18:48 105-67-908/20/19 16:4010.0 1
Dimethylphthalate ND ug/L 08/20/19 18:48 131-11-308/20/19 16:4010.0 1
Di-n-butylphthalate ND ug/L 08/20/19 18:48 84-74-208/20/19 16:4010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/20/19 18:48 534-52-108/20/19 16:4020.0 1
2,4-Dinitrophenol ND ug/L 08/20/19 18:48 51-28-508/20/19 16:4050.0 1
2,4-Dinitrotoluene ND ug/L 08/20/19 18:48 121-14-208/20/19 16:4010.0 1
2,6-Dinitrotoluene ND ug/L 08/20/19 18:48 606-20-208/20/19 16:4010.0 1
Di-n-octylphthalate ND ug/L 08/20/19 18:48 117-84-008/20/19 16:4010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/20/19 18:48 117-81-708/20/19 16:406.0 1
Fluoranthene ND ug/L 08/20/19 18:48 206-44-008/20/19 16:4010.0 1
Fluorene ND ug/L 08/20/19 18:48 86-73-708/20/19 16:4010.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 18:48 87-68-308/20/19 16:4010.0 1
Hexachlorobenzene ND ug/L 08/20/19 18:48 118-74-108/20/19 16:4010.0 1
Hexachlorocyclopentadiene ND ug/L 08/20/19 18:48 77-47-408/20/19 16:4010.0 1
Hexachloroethane ND ug/L 08/20/19 18:48 67-72-108/20/19 16:4010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-2 Lab ID:92441752003 Collected:08/15/19 15:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Indeno(1,2,3-cd)pyrene ND ug/L 08/20/19 18:48 193-39-508/20/19 16:4010.0 1
Isophorone ND ug/L 08/20/19 18:48 78-59-108/20/19 16:4010.0 1
1-Methylnaphthalene ND ug/L 08/20/19 18:48 90-12-008/20/19 16:4010.0 1
2-Methylnaphthalene ND ug/L 08/20/19 18:48 91-57-608/20/19 16:4010.0 1
2-Methylphenol(o-Cresol)ND ug/L 08/20/19 18:48 95-48-708/20/19 16:4010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/20/19 18:48 15831-10-408/20/19 16:4010.0 1
Naphthalene ND ug/L 08/20/19 18:48 91-20-308/20/19 16:4010.0 1
2-Nitroaniline ND ug/L 08/20/19 18:48 88-74-408/20/19 16:4020.0 1
3-Nitroaniline ND ug/L 08/20/19 18:48 99-09-208/20/19 16:4020.0 1
4-Nitroaniline ND ug/L 08/20/19 18:48 100-01-608/20/19 16:4020.0 1
Nitrobenzene ND ug/L 08/20/19 18:48 98-95-308/20/19 16:4010.0 1
2-Nitrophenol ND ug/L 08/20/19 18:48 88-75-508/20/19 16:4010.0 1
4-Nitrophenol ND ug/L 08/20/19 18:48 100-02-708/20/19 16:4050.0 1
N-Nitrosodimethylamine ND ug/L 08/20/19 18:48 62-75-908/20/19 16:4010.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/20/19 18:48 621-64-708/20/19 16:4010.0 1
N-Nitrosodiphenylamine ND ug/L 08/20/19 18:48 86-30-608/20/19 16:4010.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/20/19 18:48 108-60-108/20/19 16:4010.0 1
Pentachlorophenol ND ug/L 08/20/19 18:48 87-86-508/20/19 16:4025.0 1
Phenanthrene ND ug/L 08/20/19 18:48 85-01-808/20/19 16:4010.0 1
Phenol ND ug/L 08/20/19 18:48 108-95-208/20/19 16:4010.0 1
Pyrene ND ug/L 08/20/19 18:48 129-00-008/20/19 16:4010.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 18:48 120-82-108/20/19 16:4010.0 1
2,4,5-Trichlorophenol ND ug/L 08/20/19 18:48 95-95-408/20/19 16:4010.0 1
2,4,6-Trichlorophenol ND ug/L 08/20/19 18:48 88-06-208/20/19 16:4010.0 1
Surrogates
Nitrobenzene-d5 (S)81 %08/20/19 18:48 4165-60-008/20/19 16:4013-130 1
2-Fluorobiphenyl (S)77 %08/20/19 18:48 321-60-808/20/19 16:4013-130 1
Terphenyl-d14 (S)109 %08/20/19 18:48 1718-51-008/20/19 16:4025-130 1
Phenol-d6 (S)44 %08/20/19 18:48 13127-88-308/20/19 16:4010-130 1
2-Fluorophenol (S)63 %08/20/19 18:48 367-12-408/20/19 16:4010-130 1
2,4,6-Tribromophenol (S)76 %08/20/19 18:48 118-79-608/20/19 16:4010-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/20/19 17:13 67-64-125.0 1
Benzene ND ug/L 08/20/19 17:13 71-43-21.0 1
Bromobenzene ND ug/L 08/20/19 17:13 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/19 17:13 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/19 17:13 75-27-41.0 1
Bromoform ND ug/L 08/20/19 17:13 75-25-21.0 1
Bromomethane ND ug/L 08/20/19 17:13 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/20/19 17:13 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/19 17:13 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/19 17:13 108-90-71.0 1
Chloroethane ND ug/L 08/20/19 17:13 75-00-31.0 1
Chloroform ND ug/L 08/20/19 17:13 67-66-35.0 1
Chloromethane ND ug/L 08/20/19 17:13 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/20/19 17:13 95-49-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-2 Lab ID:92441752003 Collected:08/15/19 15:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
4-Chlorotoluene ND ug/L 08/20/19 17:13 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/19 17:13 96-12-85.0 1
Dibromochloromethane ND ug/L 08/20/19 17:13 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/19 17:13 106-93-41.0 1
Dibromomethane ND ug/L 08/20/19 17:13 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 17:13 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 17:13 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 17:13 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/19 17:13 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/19 17:13 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/19 17:13 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/19 17:13 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/19 17:13 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/19 17:13 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/19 17:13 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/19 17:13 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/19 17:13 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/19 17:13 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/19 17:13 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/19 17:13 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/19 17:13 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/19 17:13 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 17:13 87-68-31.0 1
2-Hexanone ND ug/L 08/20/19 17:13 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/19 17:13 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/19 17:13 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/19 17:13 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/19 17:13 1634-04-41.0 1
Naphthalene ND ug/L 08/20/19 17:13 91-20-31.0 1
Styrene ND ug/L 08/20/19 17:13 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/19 17:13 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/19 17:13 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/19 17:13 127-18-41.0 1
Toluene ND ug/L 08/20/19 17:13 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/19 17:13 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 17:13 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/19 17:13 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/19 17:13 79-00-51.0 1
Trichloroethene ND ug/L 08/20/19 17:13 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/19 17:13 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/19 17:13 96-18-4 v21.0 1
Vinyl acetate ND ug/L 08/20/19 17:13 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/19 17:13 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/19 17:13 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/19 17:13 179601-23-12.0 1
o-Xylene ND ug/L 08/20/19 17:13 95-47-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-2 Lab ID:92441752003 Collected:08/15/19 15:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Surrogates
4-Bromofluorobenzene (S)100 %08/20/19 17:13 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %08/20/19 17:13 17060-07-070-130 1
Toluene-d8 (S)99 %08/20/19 17:13 2037-26-570-130 1
Sample:GW-1 Lab ID:92441752004 Collected:08/15/19 16:05 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/21/19 11:24 7440-38-208/20/19 17:3410.0 1
Barium 77.2 ug/L 08/21/19 11:24 7440-39-308/20/19 17:345.0 1
Cadmium ND ug/L 08/21/19 11:24 7440-43-908/20/19 17:341.0 1
Chromium 25.7 ug/L 08/21/19 11:24 7440-47-308/20/19 17:345.0 1
Lead ND ug/L 08/21/19 11:24 7439-92-108/20/19 17:345.0 1
Selenium ND ug/L 08/21/19 11:24 7782-49-208/20/19 17:3410.0 1
Silver ND ug/L 08/21/19 11:24 7440-22-408/20/19 17:345.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/21/19 09:36 7439-97-608/20/19 13:540.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/20/19 19:13 83-32-908/20/19 16:4010.0 1
Acenaphthylene ND ug/L 08/20/19 19:13 208-96-808/20/19 16:4010.0 1
Aniline ND ug/L 08/20/19 19:13 62-53-308/20/19 16:4010.0 1
Anthracene ND ug/L 08/20/19 19:13 120-12-708/20/19 16:4010.0 1
Benzo(a)anthracene ND ug/L 08/20/19 19:13 56-55-308/20/19 16:4010.0 1
Benzo(a)pyrene ND ug/L 08/20/19 19:13 50-32-808/20/19 16:4010.0 1
Benzo(b)fluoranthene ND ug/L 08/20/19 19:13 205-99-208/20/19 16:4010.0 1
Benzo(g,h,i)perylene ND ug/L 08/20/19 19:13 191-24-208/20/19 16:4010.0 1
Benzo(k)fluoranthene ND ug/L 08/20/19 19:13 207-08-908/20/19 16:4010.0 1
Benzoic Acid ND ug/L 08/20/19 19:13 65-85-008/20/19 16:4050.0 1
Benzyl alcohol ND ug/L 08/20/19 19:13 100-51-608/20/19 16:4020.0 1
4-Bromophenylphenyl ether ND ug/L 08/20/19 19:13 101-55-308/20/19 16:4010.0 1
Butylbenzylphthalate ND ug/L 08/20/19 19:13 85-68-708/20/19 16:4010.0 1
4-Chloro-3-methylphenol ND ug/L 08/20/19 19:13 59-50-708/20/19 16:4020.0 1
4-Chloroaniline ND ug/L 08/20/19 19:13 106-47-808/20/19 16:4020.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/20/19 19:13 111-91-108/20/19 16:4010.0 1
bis(2-Chloroethyl) ether ND ug/L 08/20/19 19:13 111-44-408/20/19 16:4010.0 1
2-Chloronaphthalene ND ug/L 08/20/19 19:13 91-58-708/20/19 16:4010.0 1
2-Chlorophenol ND ug/L 08/20/19 19:13 95-57-808/20/19 16:4010.0 1
4-Chlorophenylphenyl ether ND ug/L 08/20/19 19:13 7005-72-308/20/19 16:4010.0 1
Chrysene ND ug/L 08/20/19 19:13 218-01-908/20/19 16:4010.0 1
Dibenz(a,h)anthracene ND ug/L 08/20/19 19:13 53-70-308/20/19 16:4010.0 1
Dibenzofuran ND ug/L 08/20/19 19:13 132-64-908/20/19 16:4010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-1 Lab ID:92441752004 Collected:08/15/19 16:05 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
1,2-Dichlorobenzene ND ug/L 08/20/19 19:13 95-50-108/20/19 16:4010.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 19:13 541-73-108/20/19 16:4010.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 19:13 106-46-708/20/19 16:4010.0 1
3,3'-Dichlorobenzidine ND ug/L 08/20/19 19:13 91-94-108/20/19 16:4020.0 1
2,4-Dichlorophenol ND ug/L 08/20/19 19:13 120-83-208/20/19 16:4010.0 1
Diethylphthalate ND ug/L 08/20/19 19:13 84-66-208/20/19 16:4010.0 1
2,4-Dimethylphenol ND ug/L 08/20/19 19:13 105-67-908/20/19 16:4010.0 1
Dimethylphthalate ND ug/L 08/20/19 19:13 131-11-308/20/19 16:4010.0 1
Di-n-butylphthalate ND ug/L 08/20/19 19:13 84-74-208/20/19 16:4010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/20/19 19:13 534-52-108/20/19 16:4020.0 1
2,4-Dinitrophenol ND ug/L 08/20/19 19:13 51-28-508/20/19 16:4050.0 1
2,4-Dinitrotoluene ND ug/L 08/20/19 19:13 121-14-208/20/19 16:4010.0 1
2,6-Dinitrotoluene ND ug/L 08/20/19 19:13 606-20-208/20/19 16:4010.0 1
Di-n-octylphthalate ND ug/L 08/20/19 19:13 117-84-008/20/19 16:4010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/20/19 19:13 117-81-708/20/19 16:406.0 1
Fluoranthene ND ug/L 08/20/19 19:13 206-44-008/20/19 16:4010.0 1
Fluorene ND ug/L 08/20/19 19:13 86-73-708/20/19 16:4010.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 19:13 87-68-308/20/19 16:4010.0 1
Hexachlorobenzene ND ug/L 08/20/19 19:13 118-74-108/20/19 16:4010.0 1
Hexachlorocyclopentadiene ND ug/L 08/20/19 19:13 77-47-408/20/19 16:4010.0 1
Hexachloroethane ND ug/L 08/20/19 19:13 67-72-108/20/19 16:4010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/20/19 19:13 193-39-508/20/19 16:4010.0 1
Isophorone ND ug/L 08/20/19 19:13 78-59-108/20/19 16:4010.0 1
1-Methylnaphthalene ND ug/L 08/20/19 19:13 90-12-008/20/19 16:4010.0 1
2-Methylnaphthalene ND ug/L 08/20/19 19:13 91-57-608/20/19 16:4010.0 1
2-Methylphenol(o-Cresol)ND ug/L 08/20/19 19:13 95-48-708/20/19 16:4010.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/20/19 19:13 15831-10-408/20/19 16:4010.0 1
Naphthalene ND ug/L 08/20/19 19:13 91-20-308/20/19 16:4010.0 1
2-Nitroaniline ND ug/L 08/20/19 19:13 88-74-408/20/19 16:4020.0 1
3-Nitroaniline ND ug/L 08/20/19 19:13 99-09-208/20/19 16:4020.0 1
4-Nitroaniline ND ug/L 08/20/19 19:13 100-01-608/20/19 16:4020.0 1
Nitrobenzene ND ug/L 08/20/19 19:13 98-95-308/20/19 16:4010.0 1
2-Nitrophenol ND ug/L 08/20/19 19:13 88-75-508/20/19 16:4010.0 1
4-Nitrophenol ND ug/L 08/20/19 19:13 100-02-708/20/19 16:4050.0 1
N-Nitrosodimethylamine ND ug/L 08/20/19 19:13 62-75-908/20/19 16:4010.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/20/19 19:13 621-64-708/20/19 16:4010.0 1
N-Nitrosodiphenylamine ND ug/L 08/20/19 19:13 86-30-608/20/19 16:4010.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/20/19 19:13 108-60-108/20/19 16:4010.0 1
Pentachlorophenol ND ug/L 08/20/19 19:13 87-86-508/20/19 16:4025.0 1
Phenanthrene ND ug/L 08/20/19 19:13 85-01-808/20/19 16:4010.0 1
Phenol ND ug/L 08/20/19 19:13 108-95-208/20/19 16:4010.0 1
Pyrene ND ug/L 08/20/19 19:13 129-00-008/20/19 16:4010.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 19:13 120-82-108/20/19 16:4010.0 1
2,4,5-Trichlorophenol ND ug/L 08/20/19 19:13 95-95-408/20/19 16:4010.0 1
2,4,6-Trichlorophenol ND ug/L 08/20/19 19:13 88-06-208/20/19 16:4010.0 1
Surrogates
Nitrobenzene-d5 (S)39 %08/20/19 19:13 4165-60-008/20/19 16:4013-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-1 Lab ID:92441752004 Collected:08/15/19 16:05 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Surrogates
2-Fluorobiphenyl (S)38 %08/20/19 19:13 321-60-808/20/19 16:4013-130 1
Terphenyl-d14 (S)74 %08/20/19 19:13 1718-51-008/20/19 16:4025-130 1
Phenol-d6 (S)20 %08/20/19 19:13 13127-88-308/20/19 16:4010-130 1
2-Fluorophenol (S)28 %08/20/19 19:13 367-12-408/20/19 16:4010-130 1
2,4,6-Tribromophenol (S)37 %08/20/19 19:13 118-79-608/20/19 16:4010-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/20/19 17:32 67-64-125.0 1
Benzene ND ug/L 08/20/19 17:32 71-43-21.0 1
Bromobenzene ND ug/L 08/20/19 17:32 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/19 17:32 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/19 17:32 75-27-41.0 1
Bromoform ND ug/L 08/20/19 17:32 75-25-21.0 1
Bromomethane ND ug/L 08/20/19 17:32 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/20/19 17:32 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/19 17:32 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/19 17:32 108-90-71.0 1
Chloroethane ND ug/L 08/20/19 17:32 75-00-31.0 1
Chloroform ND ug/L 08/20/19 17:32 67-66-35.0 1
Chloromethane ND ug/L 08/20/19 17:32 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/20/19 17:32 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/19 17:32 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/19 17:32 96-12-85.0 1
Dibromochloromethane ND ug/L 08/20/19 17:32 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/19 17:32 106-93-41.0 1
Dibromomethane ND ug/L 08/20/19 17:32 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 17:32 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 17:32 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 17:32 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/19 17:32 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/19 17:32 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/19 17:32 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/19 17:32 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/19 17:32 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/19 17:32 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/19 17:32 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/19 17:32 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/19 17:32 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/19 17:32 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/19 17:32 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/19 17:32 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/19 17:32 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/19 17:32 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 17:32 87-68-31.0 1
2-Hexanone ND ug/L 08/20/19 17:32 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/19 17:32 99-87-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:GW-1 Lab ID:92441752004 Collected:08/15/19 16:05 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Methylene Chloride ND ug/L 08/20/19 17:32 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/19 17:32 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/19 17:32 1634-04-41.0 1
Naphthalene ND ug/L 08/20/19 17:32 91-20-31.0 1
Styrene ND ug/L 08/20/19 17:32 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/19 17:32 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/19 17:32 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/19 17:32 127-18-41.0 1
Toluene ND ug/L 08/20/19 17:32 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/19 17:32 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 17:32 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/19 17:32 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/19 17:32 79-00-51.0 1
Trichloroethene ND ug/L 08/20/19 17:32 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/19 17:32 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/19 17:32 96-18-4 v21.0 1
Vinyl acetate ND ug/L 08/20/19 17:32 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/19 17:32 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/19 17:32 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/19 17:32 179601-23-12.0 1
o-Xylene ND ug/L 08/20/19 17:32 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)81 %08/20/19 17:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %08/20/19 17:32 17060-07-070-130 1
Toluene-d8 (S)130 %08/20/19 17:32 2037-26-570-130 1
Sample:Dup-1 Lab ID:92441752005 Collected:08/15/19 00:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6010D Preparation Method: EPA 3010A6010 MET ICP
Arsenic ND ug/L 08/21/19 11:27 7440-38-208/20/19 17:3410.0 1
Barium 32.2 ug/L 08/21/19 11:27 7440-39-308/20/19 17:345.0 1
Cadmium ND ug/L 08/21/19 11:27 7440-43-908/20/19 17:341.0 1
Chromium ND ug/L 08/21/19 11:27 7440-47-308/20/19 17:345.0 1
Lead ND ug/L 08/21/19 11:27 7439-92-108/20/19 17:345.0 1
Selenium ND ug/L 08/21/19 11:27 7782-49-208/20/19 17:3410.0 1
Silver ND ug/L 08/21/19 11:27 7440-22-408/20/19 17:345.0 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A7470 Mercury
Mercury ND ug/L 08/21/19 09:38 7439-97-608/20/19 13:540.20 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 08/20/19 19:39 83-32-908/20/19 16:4010.0 1
Acenaphthylene ND ug/L 08/20/19 19:39 208-96-808/20/19 16:4010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:Dup-1 Lab ID:92441752005 Collected:08/15/19 00:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Aniline ND ug/L 08/20/19 19:39 62-53-308/20/19 16:4010.0 1
Anthracene ND ug/L 08/20/19 19:39 120-12-708/20/19 16:4010.0 1
Benzo(a)anthracene ND ug/L 08/20/19 19:39 56-55-308/20/19 16:4010.0 1
Benzo(a)pyrene ND ug/L 08/20/19 19:39 50-32-808/20/19 16:4010.0 1
Benzo(b)fluoranthene ND ug/L 08/20/19 19:39 205-99-208/20/19 16:4010.0 1
Benzo(g,h,i)perylene ND ug/L 08/20/19 19:39 191-24-208/20/19 16:4010.0 1
Benzo(k)fluoranthene ND ug/L 08/20/19 19:39 207-08-908/20/19 16:4010.0 1
Benzoic Acid ND ug/L 08/20/19 19:39 65-85-008/20/19 16:4050.0 1
Benzyl alcohol ND ug/L 08/20/19 19:39 100-51-608/20/19 16:4020.0 1
4-Bromophenylphenyl ether ND ug/L 08/20/19 19:39 101-55-308/20/19 16:4010.0 1
Butylbenzylphthalate ND ug/L 08/20/19 19:39 85-68-708/20/19 16:4010.0 1
4-Chloro-3-methylphenol ND ug/L 08/20/19 19:39 59-50-708/20/19 16:4020.0 1
4-Chloroaniline ND ug/L 08/20/19 19:39 106-47-808/20/19 16:4020.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/20/19 19:39 111-91-108/20/19 16:4010.0 1
bis(2-Chloroethyl) ether ND ug/L 08/20/19 19:39 111-44-408/20/19 16:4010.0 1
2-Chloronaphthalene ND ug/L 08/20/19 19:39 91-58-708/20/19 16:4010.0 1
2-Chlorophenol ND ug/L 08/20/19 19:39 95-57-808/20/19 16:4010.0 1
4-Chlorophenylphenyl ether ND ug/L 08/20/19 19:39 7005-72-308/20/19 16:4010.0 1
Chrysene ND ug/L 08/20/19 19:39 218-01-908/20/19 16:4010.0 1
Dibenz(a,h)anthracene ND ug/L 08/20/19 19:39 53-70-308/20/19 16:4010.0 1
Dibenzofuran ND ug/L 08/20/19 19:39 132-64-908/20/19 16:4010.0 1
1,2-Dichlorobenzene ND ug/L 08/20/19 19:39 95-50-108/20/19 16:4010.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 19:39 541-73-108/20/19 16:4010.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 19:39 106-46-708/20/19 16:4010.0 1
3,3'-Dichlorobenzidine ND ug/L 08/20/19 19:39 91-94-108/20/19 16:4020.0 1
2,4-Dichlorophenol ND ug/L 08/20/19 19:39 120-83-208/20/19 16:4010.0 1
Diethylphthalate ND ug/L 08/20/19 19:39 84-66-208/20/19 16:4010.0 1
2,4-Dimethylphenol ND ug/L 08/20/19 19:39 105-67-908/20/19 16:4010.0 1
Dimethylphthalate ND ug/L 08/20/19 19:39 131-11-308/20/19 16:4010.0 1
Di-n-butylphthalate ND ug/L 08/20/19 19:39 84-74-208/20/19 16:4010.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/20/19 19:39 534-52-108/20/19 16:4020.0 1
2,4-Dinitrophenol ND ug/L 08/20/19 19:39 51-28-508/20/19 16:4050.0 1
2,4-Dinitrotoluene ND ug/L 08/20/19 19:39 121-14-208/20/19 16:4010.0 1
2,6-Dinitrotoluene ND ug/L 08/20/19 19:39 606-20-208/20/19 16:4010.0 1
Di-n-octylphthalate ND ug/L 08/20/19 19:39 117-84-008/20/19 16:4010.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/20/19 19:39 117-81-708/20/19 16:406.0 1
Fluoranthene ND ug/L 08/20/19 19:39 206-44-008/20/19 16:4010.0 1
Fluorene ND ug/L 08/20/19 19:39 86-73-708/20/19 16:4010.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 19:39 87-68-308/20/19 16:4010.0 1
Hexachlorobenzene ND ug/L 08/20/19 19:39 118-74-108/20/19 16:4010.0 1
Hexachlorocyclopentadiene ND ug/L 08/20/19 19:39 77-47-408/20/19 16:4010.0 1
Hexachloroethane ND ug/L 08/20/19 19:39 67-72-108/20/19 16:4010.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/20/19 19:39 193-39-508/20/19 16:4010.0 1
Isophorone ND ug/L 08/20/19 19:39 78-59-108/20/19 16:4010.0 1
1-Methylnaphthalene ND ug/L 08/20/19 19:39 90-12-008/20/19 16:4010.0 1
2-Methylnaphthalene ND ug/L 08/20/19 19:39 91-57-608/20/19 16:4010.0 1
2-Methylphenol(o-Cresol)ND ug/L 08/20/19 19:39 95-48-708/20/19 16:4010.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:Dup-1 Lab ID:92441752005 Collected:08/15/19 00:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
3&4-Methylphenol(m&p Cresol)ND ug/L 08/20/19 19:39 15831-10-408/20/19 16:4010.0 1
Naphthalene ND ug/L 08/20/19 19:39 91-20-308/20/19 16:4010.0 1
2-Nitroaniline ND ug/L 08/20/19 19:39 88-74-408/20/19 16:4020.0 1
3-Nitroaniline ND ug/L 08/20/19 19:39 99-09-208/20/19 16:4020.0 1
4-Nitroaniline ND ug/L 08/20/19 19:39 100-01-608/20/19 16:4020.0 1
Nitrobenzene ND ug/L 08/20/19 19:39 98-95-308/20/19 16:4010.0 1
2-Nitrophenol ND ug/L 08/20/19 19:39 88-75-508/20/19 16:4010.0 1
4-Nitrophenol ND ug/L 08/20/19 19:39 100-02-708/20/19 16:4050.0 1
N-Nitrosodimethylamine ND ug/L 08/20/19 19:39 62-75-908/20/19 16:4010.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/20/19 19:39 621-64-708/20/19 16:4010.0 1
N-Nitrosodiphenylamine ND ug/L 08/20/19 19:39 86-30-608/20/19 16:4010.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/20/19 19:39 108-60-108/20/19 16:4010.0 1
Pentachlorophenol ND ug/L 08/20/19 19:39 87-86-508/20/19 16:4025.0 1
Phenanthrene ND ug/L 08/20/19 19:39 85-01-808/20/19 16:4010.0 1
Phenol ND ug/L 08/20/19 19:39 108-95-208/20/19 16:4010.0 1
Pyrene ND ug/L 08/20/19 19:39 129-00-008/20/19 16:4010.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 19:39 120-82-108/20/19 16:4010.0 1
2,4,5-Trichlorophenol ND ug/L 08/20/19 19:39 95-95-408/20/19 16:4010.0 1
2,4,6-Trichlorophenol ND ug/L 08/20/19 19:39 88-06-208/20/19 16:4010.0 1
Surrogates
Nitrobenzene-d5 (S)56 %08/20/19 19:39 4165-60-008/20/19 16:4013-130 1
2-Fluorobiphenyl (S)55 %08/20/19 19:39 321-60-808/20/19 16:4013-130 1
Terphenyl-d14 (S)92 %08/20/19 19:39 1718-51-008/20/19 16:4025-130 1
Phenol-d6 (S)27 %08/20/19 19:39 13127-88-308/20/19 16:4010-130 1
2-Fluorophenol (S)20 %08/20/19 19:39 367-12-408/20/19 16:4010-130 1
2,4,6-Tribromophenol (S)10 %08/20/19 19:39 118-79-608/20/19 16:4010-137 1
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 08/20/19 17:50 67-64-125.0 1
Benzene ND ug/L 08/20/19 17:50 71-43-21.0 1
Bromobenzene ND ug/L 08/20/19 17:50 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/19 17:50 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/19 17:50 75-27-41.0 1
Bromoform ND ug/L 08/20/19 17:50 75-25-21.0 1
Bromomethane ND ug/L 08/20/19 17:50 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 08/20/19 17:50 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/19 17:50 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/19 17:50 108-90-71.0 1
Chloroethane ND ug/L 08/20/19 17:50 75-00-31.0 1
Chloroform ND ug/L 08/20/19 17:50 67-66-35.0 1
Chloromethane ND ug/L 08/20/19 17:50 74-87-31.0 1
2-Chlorotoluene ND ug/L 08/20/19 17:50 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/19 17:50 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/19 17:50 96-12-85.0 1
Dibromochloromethane ND ug/L 08/20/19 17:50 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/19 17:50 106-93-41.0 1
Dibromomethane ND ug/L 08/20/19 17:50 74-95-31.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
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Page 19 of 39
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Sample:Dup-1 Lab ID:92441752005 Collected:08/15/19 00:00 Received:08/16/19 10:13 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
1,2-Dichlorobenzene ND ug/L 08/20/19 17:50 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/19 17:50 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/19 17:50 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/19 17:50 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/19 17:50 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/19 17:50 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/19 17:50 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/19 17:50 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/19 17:50 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/19 17:50 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/19 17:50 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/19 17:50 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/19 17:50 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/19 17:50 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/19 17:50 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/19 17:50 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/19 17:50 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/19 17:50 87-68-31.0 1
2-Hexanone ND ug/L 08/20/19 17:50 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/19 17:50 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/19 17:50 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/19 17:50 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/19 17:50 1634-04-41.0 1
Naphthalene ND ug/L 08/20/19 17:50 91-20-31.0 1
Styrene ND ug/L 08/20/19 17:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/19 17:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/19 17:50 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/19 17:50 127-18-4 v21.0 1
Toluene ND ug/L 08/20/19 17:50 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/19 17:50 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/19 17:50 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/19 17:50 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/19 17:50 79-00-51.0 1
Trichloroethene ND ug/L 08/20/19 17:50 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/19 17:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/19 17:50 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/19 17:50 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/19 17:50 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/19 17:50 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/19 17:50 179601-23-12.0 1
o-Xylene ND ug/L 08/20/19 17:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)109 %08/20/19 17:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %08/20/19 17:50 17060-07-070-130 1
Toluene-d8 (S)118 %08/20/19 17:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 20 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493353
EPA 7470A
EPA 7470A
7470 Mercury
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2659074
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 08/21/19 09:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2659075LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2659076MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92441752001
2659077
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury ug/L 2.5 104 75-125106 22.5ND 2.6 2.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493445
EPA 3010A
EPA 6010D
6010 MET
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2659611
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Matrix:Water
Analyzed
Arsenic ug/L ND 10.0 08/21/19 10:49
Barium ug/L ND 5.0 08/21/19 10:49
Cadmium ug/L ND 1.0 08/21/19 10:49
Chromium ug/L ND 5.0 08/21/19 10:49
Lead ug/L ND 5.0 08/21/19 10:49
Selenium ug/L ND 10.0 08/21/19 10:49
Silver ug/L ND 5.0 08/21/19 10:49
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2659612LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 489500 98 80-120
Barium ug/L 490500 98 80-120
Cadmium ug/L 493500 99 80-120
Chromium ug/L 483500 97 80-120
Lead ug/L 500500 100 80-120
Selenium ug/L 501500 100 80-120
Silver ug/L 251250 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2659613MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92441752001
2659614
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic ug/L 500 99 75-12598 1500ND494488
Barium ug/L 500 97 75-12595 250037.3 524 511
Cadmium ug/L 500 100 75-12599 1500ND500494
Chromium ug/L 500 97 75-12598 05006.9 493 495
Lead ug/L 500 99 75-12598 2500ND498490
Selenium ug/L 500 106 75-125104 1500ND528521
Silver ug/L 250 101 75-125101 0250ND253252
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493345
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2659040
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/20/19 15:05
1,1,1-Trichloroethane ug/L ND 1.0 08/20/19 15:05
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/20/19 15:05
1,1,2-Trichloroethane ug/L ND 1.0 08/20/19 15:05
1,1-Dichloroethane ug/L ND 1.0 08/20/19 15:05
1,1-Dichloroethene ug/L ND 1.0 08/20/19 15:05
1,1-Dichloropropene ug/L ND 1.0 08/20/19 15:05
1,2,3-Trichlorobenzene ug/L ND 1.0 08/20/19 15:05
1,2,3-Trichloropropane ug/L ND 1.0 v108/20/19 15:05
1,2,4-Trichlorobenzene ug/L ND 1.0 08/20/19 15:05
1,2-Dibromo-3-chloropropane ug/L ND 5.0 08/20/19 15:05
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/20/19 15:05
1,2-Dichlorobenzene ug/L ND 1.0 08/20/19 15:05
1,2-Dichloroethane ug/L ND 1.0 08/20/19 15:05
1,2-Dichloropropane ug/L ND 1.0 08/20/19 15:05
1,3-Dichlorobenzene ug/L ND 1.0 08/20/19 15:05
1,3-Dichloropropane ug/L ND 1.0 08/20/19 15:05
1,4-Dichlorobenzene ug/L ND 1.0 08/20/19 15:05
2,2-Dichloropropane ug/L ND 1.0 08/20/19 15:05
2-Butanone (MEK)ug/L ND 5.0 08/20/19 15:05
2-Chlorotoluene ug/L ND 1.0 08/20/19 15:05
2-Hexanone ug/L ND 5.0 08/20/19 15:05
4-Chlorotoluene ug/L ND 1.0 08/20/19 15:05
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/20/19 15:05
Acetone ug/L ND 25.0 08/20/19 15:05
Benzene ug/L ND 1.0 08/20/19 15:05
Bromobenzene ug/L ND 1.0 08/20/19 15:05
Bromochloromethane ug/L ND 1.0 08/20/19 15:05
Bromodichloromethane ug/L ND 1.0 08/20/19 15:05
Bromoform ug/L ND 1.0 08/20/19 15:05
Bromomethane ug/L ND 2.0 v208/20/19 15:05
Carbon tetrachloride ug/L ND 1.0 08/20/19 15:05
Chlorobenzene ug/L ND 1.0 08/20/19 15:05
Chloroethane ug/L ND 1.0 08/20/19 15:05
Chloroform ug/L ND 5.0 08/20/19 15:05
Chloromethane ug/L ND 1.0 08/20/19 15:05
cis-1,2-Dichloroethene ug/L ND 1.0 08/20/19 15:05
cis-1,3-Dichloropropene ug/L ND 1.0 08/20/19 15:05
Dibromochloromethane ug/L ND 1.0 08/20/19 15:05
Dibromomethane ug/L ND 1.0 08/20/19 15:05
Dichlorodifluoromethane ug/L ND 1.0 08/20/19 15:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2659040
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 08/20/19 15:05
Ethylbenzene ug/L ND 1.0 08/20/19 15:05
Hexachloro-1,3-butadiene ug/L ND 1.0 08/20/19 15:05
m&p-Xylene ug/L ND 2.0 08/20/19 15:05
Methyl-tert-butyl ether ug/L ND 1.0 08/20/19 15:05
Methylene Chloride ug/L ND 5.0 08/20/19 15:05
Naphthalene ug/L ND 1.0 08/20/19 15:05
o-Xylene ug/L ND 1.0 08/20/19 15:05
p-Isopropyltoluene ug/L ND 1.0 08/20/19 15:05
Styrene ug/L ND 1.0 08/20/19 15:05
Tetrachloroethene ug/L ND 1.0 08/20/19 15:05
Toluene ug/L ND 1.0 08/20/19 15:05
trans-1,2-Dichloroethene ug/L ND 1.0 08/20/19 15:05
trans-1,3-Dichloropropene ug/L ND 1.0 08/20/19 15:05
Trichloroethene ug/L ND 1.0 08/20/19 15:05
Trichlorofluoromethane ug/L ND 1.0 08/20/19 15:05
Vinyl acetate ug/L ND 2.0 08/20/19 15:05
Vinyl chloride ug/L ND 1.0 08/20/19 15:05
Xylene (Total)ug/L ND 1.0 08/20/19 15:05
1,2-Dichloroethane-d4 (S)%95 70-130 08/20/19 15:05
4-Bromofluorobenzene (S)%88 70-130 08/20/19 15:05
Toluene-d8 (S)%101 70-130 08/20/19 15:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2659041LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.250 110 70-130
1,1,1-Trichloroethane ug/L 57.750 115 70-130
1,1,2,2-Tetrachloroethane ug/L 50.950 102 70-130
1,1,2-Trichloroethane ug/L 60.850 122 70-130
1,1-Dichloroethane ug/L 56.450 113 70-130
1,1-Dichloroethene ug/L 58.450 117 70-130
1,1-Dichloropropene ug/L 51.5 IK5010370-130
1,2,3-Trichlorobenzene ug/L 52.150 104 70-130
1,2,3-Trichloropropane ug/L 56.6 v35011370-130
1,2,4-Trichlorobenzene ug/L 49.950 100 70-130
1,2-Dibromo-3-chloropropane ug/L 58.950 118 70-130
1,2-Dibromoethane (EDB)ug/L 57.850 116 70-130
1,2-Dichlorobenzene ug/L 52.050 104 70-130
1,2-Dichloroethane ug/L 53.150 106 70-130
1,2-Dichloropropane ug/L 55.750 111 70-130
1,3-Dichlorobenzene ug/L 51.750 103 70-130
1,3-Dichloropropane ug/L 58.150 116 70-131
1,4-Dichlorobenzene ug/L 47.550 95 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2659041LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 62.250 124 69-130
2-Butanone (MEK)ug/L 113100 113 64-135
2-Chlorotoluene ug/L 50.650 101 70-130
2-Hexanone ug/L 102100 102 66-135
4-Chlorotoluene ug/L 54.050 108 70-130
4-Methyl-2-pentanone (MIBK)ug/L 105100 105 70-130
Acetone ug/L 119100 119 61-157
Benzene ug/L 56.050 112 70-130
Bromobenzene ug/L 49.350 99 70-130
Bromochloromethane ug/L 57.450 115 70-130
Bromodichloromethane ug/L 60.9 IK5012270-130
Bromoform ug/L 56.150 112 70-130
Bromomethane ug/L 48.2 v3509638-130
Carbon tetrachloride ug/L 58.750 117 70-130
Chlorobenzene ug/L 49.450 99 70-130
Chloroethane ug/L 59.950 120 37-142
Chloroform ug/L 53.450 107 70-130
Chloromethane ug/L 49.650 99 48-130
cis-1,2-Dichloroethene ug/L 55.450 111 70-130
cis-1,3-Dichloropropene ug/L 51.650 103 70-130
Dibromochloromethane ug/L 53.750 107 70-130
Dibromomethane ug/L 52.550 105 70-130
Dichlorodifluoromethane ug/L 53.250 106 53-134
Diisopropyl ether ug/L 60.150 120 70-135
Ethylbenzene ug/L 50.050 100 70-130
Hexachloro-1,3-butadiene ug/L 50.750 101 68-132
m&p-Xylene ug/L 103100 103 70-130
Methyl-tert-butyl ether ug/L 54.7 IK5010970-130
Methylene Chloride ug/L 52.250 104 67-132
Naphthalene ug/L 54.550 109 70-130
o-Xylene ug/L 52.750 105 70-131
p-Isopropyltoluene ug/L 52.350 105 70-130
Styrene ug/L 50.750 101 70-130
Tetrachloroethene ug/L 51.050 102 69-130
Toluene ug/L 44.850 90 70-130
trans-1,2-Dichloroethene ug/L 60.050 120 70-130
trans-1,3-Dichloropropene ug/L 54.750 109 70-130
Trichloroethene ug/L 58.550 117 70-130
Trichlorofluoromethane ug/L 60.850 122 63-130
Vinyl acetate ug/L 109 IK10010955-143
Vinyl chloride ug/L 59.050 118 70-131
Xylene (Total)ug/L 155150 103 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%88 70-130
Toluene-d8 (S)%89 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2659042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92441752001
2659043
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 108 73-134114 620ND21.5 22.8
1,1,1-Trichloroethane ug/L 20 110 82-143115 520ND22.0 23.0
1,1,2,2-Tetrachloroethane ug/L 20 105 70-13699 520ND20.9 19.8
1,1,2-Trichloroethane ug/L 20 115 70-13588 2620ND23.0 17.7
1,1-Dichloroethane ug/L 20 109 70-139119 920ND21.8 23.8
1,1-Dichloroethene ug/L 20 114 70-154124 820ND22.8 24.8
1,1-Dichloropropene ug/L 20 95 70-14985 1220ND19.0 16.9
1,2,3-Trichlorobenzene ug/L 20 77 70-13588 1420ND15.3 17.6
1,2,3-Trichloropropane ug/L v32011171-137111 120ND22.1 22.3
1,2,4-Trichlorobenzene ug/L 20 87 73-14088 120ND17.4 17.6
1,2-Dibromo-3-chloropropane ug/L 20 107 65-134103 420ND21.5 20.7
1,2-Dibromoethane (EDB)ug/L 20 110 70-137108 220ND22.1 21.7
1,2-Dichlorobenzene ug/L 20 95 70-13393 220ND18.9 18.5
1,2-Dichloroethane ug/L 20 108 70-137118 920ND21.6 23.5
1,2-Dichloropropane ug/L 20 106 70-140107 120ND21.2 21.4
1,3-Dichlorobenzene ug/L 20 94 70-13593 120ND18.9 18.7
1,3-Dichloropropane ug/L 20 104 70-143102 320ND20.9 20.3
1,4-Dichlorobenzene ug/L 20 93 70-13394 120ND18.7 18.8
2,2-Dichloropropane ug/L 20 98 61-148105 620ND19.7 20.9
2-Butanone (MEK)ug/L 40 100 60-13993 740ND40.1 37.3
2-Chlorotoluene ug/L 20 99 70-14495 420ND19.8 19.0
2-Hexanone ug/L 40 105 65-138104 040ND41.8 41.7
4-Chlorotoluene ug/L 20 101 70-13796 520ND20.2 19.2
4-Methyl-2-pentanone (MIBK)ug/L 40 101 65-13584 1840ND40.5 33.8
Acetone ug/L 40 118 60-148124 540ND47.3 49.8
Benzene ug/L 20 105 70-151106 120ND21.0 21.1
Bromobenzene ug/L 20 103 70-136102 120ND20.6 20.4
Bromochloromethane ug/L 20 108 70-141100 820ND21.7 20.0
Bromodichloromethane ug/L 20 118 70-138124 520ND23.6 24.8
Bromoform ug/L 20 108 63-130117 820ND21.6 23.5
Bromomethane ug/L v3206915-15261 1320ND13.8 12.1
Carbon tetrachloride ug/L 20 117 70-143117 020ND23.4 23.3
Chlorobenzene ug/L 20 103 70-138102 120ND20.6 20.4
Chloroethane ug/L 20 116 52-163128 1020ND23.1 25.6
Chloroform ug/L 20 103 70-139106 220ND22.9 23.4
Chloromethane ug/L 20 89 41-139115 2520ND17.8 23.0
cis-1,2-Dichloroethene ug/L 20 110 70-141117 720ND21.9 23.4
cis-1,3-Dichloropropene ug/L 20 94 70-13784 1120ND18.8 16.8
Dibromochloromethane ug/L 20 98 70-134108 920ND19.6 21.6
Dibromomethane ug/L 20 106 70-138102 320ND21.2 20.5
Dichlorodifluoromethane ug/L 20 112 47-155125 1120ND22.4 25.1
Diisopropyl ether ug/L 20 109 63-144123 1120ND21.9 24.5
Ethylbenzene ug/L 20 104 66-153103 120ND20.8 20.6
Hexachloro-1,3-butadiene ug/L 20 91 65-14988 320ND18.2 17.7
m&p-Xylene ug/L 40 107 69-152103 440ND42.9 41.3
Methyl-tert-butyl ether ug/L 20 95 54-156109 1320ND19.0 21.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
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Huntersville, NC 28078
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Page 26 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2659042MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92441752001
2659043
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Methylene Chloride ug/L 20 110 42-159118 720ND22.1 23.6
Naphthalene ug/L 20 86 61-14888 320ND17.1 17.6
o-Xylene ug/L 20 105 70-148108 320ND21.0 21.5
p-Isopropyltoluene ug/L 20 99 70-14693 620ND19.8 18.6
Styrene ug/L 20 105 70-135103 220ND21.0 20.6
Tetrachloroethene ug/L 20 103 59-143105 220ND20.6 21.1
Toluene ug/L 20 104 59-14879 2720ND20.8 15.8
trans-1,2-Dichloroethene ug/L 20 115 70-146122 620ND22.9 24.4
trans-1,3-Dichloropropene ug/L 20 97 70-13585 1320ND19.4 16.9
Trichloroethene ug/L 20 111 70-14798 1220ND22.2 19.7
Trichlorofluoromethane ug/L 20 125 70-148121 320ND24.9 24.3
Vinyl acetate ug/L 40 88 49-15196 940ND35.1 38.4
Vinyl chloride ug/L 20 111 70-156136 2120ND22.1 27.2
Xylene (Total)ug/L 60 106 63-158105 260ND63.9 62.8
1,2-Dichloroethane-d4 (S)%106 70-130109
4-Bromofluorobenzene (S)%103 70-130108
Toluene-d8 (S)%99 70-13081
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493363
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2659136
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 08/20/19 09:42
1,2-Dichlorobenzene ug/L ND 10.0 08/20/19 09:42
1,3-Dichlorobenzene ug/L ND 10.0 08/20/19 09:42
1,4-Dichlorobenzene ug/L ND 10.0 08/20/19 09:42
1-Methylnaphthalene ug/L ND 10.0 08/20/19 09:42
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 08/20/19 09:42
2,4,5-Trichlorophenol ug/L ND 10.0 08/20/19 09:42
2,4,6-Trichlorophenol ug/L ND 10.0 08/20/19 09:42
2,4-Dichlorophenol ug/L ND 10.0 08/20/19 09:42
2,4-Dimethylphenol ug/L ND 10.0 08/20/19 09:42
2,4-Dinitrophenol ug/L ND 50.0 08/20/19 09:42
2,4-Dinitrotoluene ug/L ND 10.0 08/20/19 09:42
2,6-Dinitrotoluene ug/L ND 10.0 08/20/19 09:42
2-Chloronaphthalene ug/L ND 10.0 08/20/19 09:42
2-Chlorophenol ug/L ND 10.0 08/20/19 09:42
2-Methylnaphthalene ug/L ND 10.0 08/20/19 09:42
2-Methylphenol(o-Cresol)ug/L ND 10.0 08/20/19 09:42
2-Nitroaniline ug/L ND 20.0 08/20/19 09:42
2-Nitrophenol ug/L ND 10.0 08/20/19 09:42
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 08/20/19 09:42
3,3'-Dichlorobenzidine ug/L ND 20.0 08/20/19 09:42
3-Nitroaniline ug/L ND 20.0 08/20/19 09:42
4,6-Dinitro-2-methylphenol ug/L ND 20.0 08/20/19 09:42
4-Bromophenylphenyl ether ug/L ND 10.0 08/20/19 09:42
4-Chloro-3-methylphenol ug/L ND 20.0 08/20/19 09:42
4-Chloroaniline ug/L ND 20.0 08/20/19 09:42
4-Chlorophenylphenyl ether ug/L ND 10.0 08/20/19 09:42
4-Nitroaniline ug/L ND 20.0 08/20/19 09:42
4-Nitrophenol ug/L ND 50.0 08/20/19 09:42
Acenaphthene ug/L ND 10.0 08/20/19 09:42
Acenaphthylene ug/L ND 10.0 08/20/19 09:42
Aniline ug/L ND 10.0 08/20/19 09:42
Anthracene ug/L ND 10.0 08/20/19 09:42
Benzo(a)anthracene ug/L ND 10.0 08/20/19 09:42
Benzo(a)pyrene ug/L ND 10.0 08/20/19 09:42
Benzo(b)fluoranthene ug/L ND 10.0 08/20/19 09:42
Benzo(g,h,i)perylene ug/L ND 10.0 08/20/19 09:42
Benzo(k)fluoranthene ug/L ND 10.0 08/20/19 09:42
Benzoic Acid ug/L ND 50.0 08/20/19 09:42
Benzyl alcohol ug/L ND 20.0 08/20/19 09:42
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/20/19 09:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2659136
Associated Lab Samples:92441752001, 92441752002, 92441752003, 92441752004, 92441752005
Matrix:Water
Analyzed
bis(2-Chloroethyl) ether ug/L ND 10.0 08/20/19 09:42
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 08/20/19 09:42
Butylbenzylphthalate ug/L ND 10.0 08/20/19 09:42
Chrysene ug/L ND 10.0 08/20/19 09:42
Di-n-butylphthalate ug/L ND 10.0 08/20/19 09:42
Di-n-octylphthalate ug/L ND 10.0 08/20/19 09:42
Dibenz(a,h)anthracene ug/L ND 10.0 08/20/19 09:42
Dibenzofuran ug/L ND 10.0 08/20/19 09:42
Diethylphthalate ug/L ND 10.0 08/20/19 09:42
Dimethylphthalate ug/L ND 10.0 08/20/19 09:42
Fluoranthene ug/L ND 10.0 08/20/19 09:42
Fluorene ug/L ND 10.0 08/20/19 09:42
Hexachloro-1,3-butadiene ug/L ND 10.0 08/20/19 09:42
Hexachlorobenzene ug/L ND 10.0 08/20/19 09:42
Hexachlorocyclopentadiene ug/L ND 10.0 08/20/19 09:42
Hexachloroethane ug/L ND 10.0 08/20/19 09:42
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/20/19 09:42
Isophorone ug/L ND 10.0 08/20/19 09:42
N-Nitroso-di-n-propylamine ug/L ND 10.0 08/20/19 09:42
N-Nitrosodimethylamine ug/L ND 10.0 08/20/19 09:42
N-Nitrosodiphenylamine ug/L ND 10.0 08/20/19 09:42
Naphthalene ug/L ND 10.0 08/20/19 09:42
Nitrobenzene ug/L ND 10.0 08/20/19 09:42
Pentachlorophenol ug/L ND 25.0 08/20/19 09:42
Phenanthrene ug/L ND 10.0 08/20/19 09:42
Phenol ug/L ND 10.0 08/20/19 09:42
Pyrene ug/L ND 10.0 08/20/19 09:42
2,4,6-Tribromophenol (S)%41 10-137 08/20/19 09:42
2-Fluorobiphenyl (S)%62 13-130 08/20/19 09:42
2-Fluorophenol (S)%33 10-130 08/20/19 09:42
Nitrobenzene-d5 (S)%70 13-130 08/20/19 09:42
Phenol-d6 (S)%33 10-130 08/20/19 09:42
Terphenyl-d14 (S)%81 25-130 08/20/19 09:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2659137LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2659138
1,2,4-Trichlorobenzene ug/L 28.150 56 30-1305527.5 2 30
1,2-Dichlorobenzene ug/L 26.450 53 30-1305025.1 5 30
1,3-Dichlorobenzene ug/L 26.250 52 20-1304823.9 9 30
1,4-Dichlorobenzene ug/L 26.150 52 30-1305125.4 3 30
1-Methylnaphthalene ug/L 37.650 75 30-1307035.0 7 30
2,2'-Oxybis(1-chloropropane)ug/L 42.650 85 20-1308240.9 4 30
2,4,5-Trichlorophenol ug/L 36.050 72 40-1307236.2 1 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2659137LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2659138
2,4,6-Trichlorophenol ug/L 36.050 72 40-1307437.1 3 30
2,4-Dichlorophenol ug/L 38.250 76 31-1307838.9 2 30
2,4-Dimethylphenol ug/L 38.950 78 30-1308140.3 4 30
2,4-Dinitrophenol ug/L 187250 75 30-13081204 9 30
2,4-Dinitrotoluene ug/L 35.550 71 49-1307336.6 3 30
2,6-Dinitrotoluene ug/L 35.550 71 50-1307336.3 2 30
2-Chloronaphthalene ug/L 34.750 69 30-1306934.6 0 30
2-Chlorophenol ug/L 37.550 75 30-1307235.9 4 30
2-Methylnaphthalene ug/L 38.350 77 30-1307236.0 6 30
2-Methylphenol(o-Cresol)ug/L 34.350 69 30-1307235.9 4 30
2-Nitroaniline ug/L 81.0100 81 40-1308282.2 1 30
2-Nitrophenol ug/L 36.550 73 20-1307537.6 3 30
3&4-Methylphenol(m&p Cresol)ug/L 34.350 69 20-1306432.2 6 30
3,3'-Dichlorobenzidine ug/L 78.3100 78 10-1508383.4 6 30
3-Nitroaniline ug/L 82.2100 82 40-1308685.7 4 30
4,6-Dinitro-2-methylphenol ug/L 76.6100 77 40-1308080.5 5 30
4-Bromophenylphenyl ether ug/L 39.150 78 30-1308040.2 3 30
4-Chloro-3-methylphenol ug/L 80.2100 80 30-1307776.9 4 30
4-Chloroaniline ug/L 87.0100 87 20-1308585.1 2 30
4-Chlorophenylphenyl ether ug/L 37.250 74 20-1307738.3 3 30
4-Nitroaniline ug/L 82.2100 82 40-1308787.4 6 30
4-Nitrophenol ug/L 131250 52 10-13057143 8 30
Acenaphthene ug/L 36.050 72 30-1307235.9 0 30
Acenaphthylene ug/L 37.350 75 30-1307436.8 1 30
Aniline ug/L 35.050 70 20-1306532.4 8 30
Anthracene ug/L 41.450 83 50-1308743.5 5 30
Benzo(a)anthracene ug/L 44.850 90 50-1309246.1 3 30
Benzo(a)pyrene ug/L 43.150 86 50-1309145.7 6 30
Benzo(b)fluoranthene ug/L 43.850 88 50-1309949.7 13 30
Benzo(g,h,i)perylene ug/L 45.250 90 50-1309648.2 7 30
Benzo(k)fluoranthene ug/L 42.150 84 50-1309145.5 8 30
Benzoic Acid ug/L 118250 47 10-13050126 7 30
Benzyl alcohol ug/L 66.6100 67 20-1306766.5 0 30
bis(2-Chloroethoxy)methane ug/L 39.750 79 30-1307839.0 2 30
bis(2-Chloroethyl) ether ug/L 41.150 82 30-1307838.9 5 30
bis(2-Ethylhexyl)phthalate ug/L 42.650 85 50-1309145.4 6 30
Butylbenzylphthalate ug/L 42.650 85 50-1509446.9 10 30
Chrysene ug/L 45.350 91 50-1309346.5 3 30
Di-n-butylphthalate ug/L 40.350 81 50-1308643.1 6 30
Di-n-octylphthalate ug/L 39.050 78 50-1309848.9 23 30
Dibenz(a,h)anthracene ug/L 44.750 89 40-1309547.7 6 30
Dibenzofuran ug/L 36.050 72 40-1307235.8 1 30
Diethylphthalate ug/L 38.650 77 40-1308341.6 8 30
Dimethylphthalate ug/L 38.150 76 40-1308039.9 4 30
Fluoranthene ug/L 43.150 86 30-1309145.3 5 30
Fluorene ug/L 38.450 77 20-1307838.9 1 30
Hexachloro-1,3-butadiene ug/L 24.950 50 10-1304824.0 4 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2659137LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2659138
Hexachlorobenzene ug/L 34.150 68 30-1307235.8 5 30
Hexachlorocyclopentadiene ug/L 22.950 46 10-1504623.0 1 30
Hexachloroethane ug/L 23.050 46 10-1304623.0 0 30
Indeno(1,2,3-cd)pyrene ug/L 44.850 90 40-1309547.4 6 30
Isophorone ug/L 36.250 72 30-1307436.9 2 30
N-Nitroso-di-n-propylamine ug/L 41.050 82 30-1308040.2 2 30
N-Nitrosodimethylamine ug/L 32.450 65 10-1307135.3 9 30
N-Nitrosodiphenylamine ug/L 41.450 83 30-1308241.0 1 30
Naphthalene ug/L 36.750 73 20-1307436.9 1 30
Nitrobenzene ug/L 36.250 72 20-1307537.5 4 30
Pentachlorophenol ug/L 78.3100 78 10-1408787.3 11 30
Phenanthrene ug/L 41.150 82 50-1308542.7 4 30
Phenol ug/L 26.750 53 10-1304924.3 9 30
Pyrene ug/L 44.250 88 50-1309245.9 4 30
2,4,6-Tribromophenol (S)%75 10-13773
2-Fluorobiphenyl (S)%60 13-13058
2-Fluorophenol (S)%60 10-13059
Nitrobenzene-d5 (S)%72 13-13074
Phenol-d6 (S)%47 10-13045
Terphenyl-d14 (S)%81 25-13084
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2659139MATRIX SPIKE SAMPLE:
MSSpike
Result
92441752001
1,2,4-Trichlorobenzene ug/L 38.6100 39 30-130ND
1,2-Dichlorobenzene ug/L 38.8100 39 30-130ND
1,3-Dichlorobenzene ug/L 39.4100 39 20-130ND
1,4-Dichlorobenzene ug/L 39.1100 39 30-130ND
1-Methylnaphthalene ug/L 44.9100 45 30-130ND
2,2'-Oxybis(1-chloropropane)ug/L 46.9100 47 20-130ND
2,4,5-Trichlorophenol ug/L 44.1100 44 40-130ND
2,4,6-Trichlorophenol ug/L 43.7100 44 40-130ND
2,4-Dichlorophenol ug/L 40.8100 41 31-130ND
2,4-Dimethylphenol ug/L 43.4100 43 30-130ND
2,4-Dinitrophenol ug/L 303500 61 30-130ND
2,4-Dinitrotoluene ug/L 58.3100 58 49-130ND
2,6-Dinitrotoluene ug/L 51.1100 51 50-130ND
2-Chloronaphthalene ug/L 38.9100 39 30-130ND
2-Chlorophenol ug/L 41.1100 41 30-130ND
2-Methylnaphthalene ug/L 46.9100 47 30-130ND
2-Methylphenol(o-Cresol)ug/L 41.5100 41 30-130ND
2-Nitroaniline ug/L 118200 59 40-130ND
2-Nitrophenol ug/L 40.6100 41 20-130ND
3&4-Methylphenol(m&p Cresol)ug/L 37.7100 38 20-130ND
3,3'-Dichlorobenzidine ug/L 102200 51 10-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/21/2019 04:55 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 31 of 39
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2659139MATRIX SPIKE SAMPLE:
MSSpike
Result
92441752001
3-Nitroaniline ug/L 122200 61 40-130ND
4,6-Dinitro-2-methylphenol ug/L 137200 68 40-130ND
4-Bromophenylphenyl ether ug/L 64.4100 64 30-130ND
4-Chloro-3-methylphenol ug/L 95.2200 48 30-130ND
4-Chloroaniline ug/L 80.7200 40 20-130ND
4-Chlorophenylphenyl ether ug/L 53.3100 53 20-130ND
4-Nitroaniline ug/L 128200 64 40-130ND
4-Nitrophenol ug/L 194500 39 10-130ND
Acenaphthene ug/L 47.7100 48 30-130ND
Acenaphthylene ug/L 46.9100 47 30-130ND
Aniline ug/L 21.2100 21 20-130ND
Anthracene ug/L 72.5100 72 50-130ND
Benzo(a)anthracene ug/L 75.8100 76 50-130ND
Benzo(a)pyrene ug/L 75.2100 75 50-130ND
Benzo(b)fluoranthene ug/L 75.4100 75 50-130ND
Benzo(g,h,i)perylene ug/L 79.9100 80 50-130ND
Benzo(k)fluoranthene ug/L 74.9100 75 50-130ND
Benzoic Acid ug/L 141500 28 10-130ND
Benzyl alcohol ug/L 78.3200 39 20-130ND
bis(2-Chloroethoxy)methane ug/L 42.9100 43 30-130ND
bis(2-Chloroethyl) ether ug/L 45.3100 45 30-130ND
bis(2-Ethylhexyl)phthalate ug/L 72.7100 73 50-130ND
Butylbenzylphthalate ug/L 70.9100 71 50-150ND
Chrysene ug/L 78.2100 78 50-130ND
Di-n-butylphthalate ug/L 72.1100 72 50-130ND
Di-n-octylphthalate ug/L 70.8100 71 50-130ND
Dibenz(a,h)anthracene ug/L 79.0100 79 40-130ND
Dibenzofuran ug/L 47.5100 48 40-130ND
Diethylphthalate ug/L 63.6100 64 40-130ND
Dimethylphthalate ug/L 59.2100 59 40-130ND
Fluoranthene ug/L 76.4100 76 30-130ND
Fluorene ug/L 54.5100 54 20-130ND
Hexachloro-1,3-butadiene ug/L 36.1100 36 10-130ND
Hexachlorobenzene ug/L 57.6100 58 30-130ND
Hexachlorocyclopentadiene ug/L 32.9100 33 10-150ND
Hexachloroethane ug/L 36.5100 36 10-130ND
Indeno(1,2,3-cd)pyrene ug/L 79.2100 79 40-130ND
Isophorone ug/L 39.6100 40 30-130ND
N-Nitroso-di-n-propylamine ug/L 45.6100 46 30-130ND
N-Nitrosodimethylamine ug/L 39.5100 40 10-130ND
N-Nitrosodiphenylamine ug/L 68.4100 68 30-130ND
Naphthalene ug/L 46.4100 46 20-130ND
Nitrobenzene ug/L 41.1100 41 20-130ND
Pentachlorophenol ug/L 140200 70 10-140ND
Phenanthrene ug/L 71.7100 72 50-130ND
Phenol ug/L 27.2100 27 10-130ND
Pyrene ug/L 75.7100 76 50-130ND
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2659139MATRIX SPIKE SAMPLE:
MSSpike
Result
92441752001
2,4,6-Tribromophenol (S)%76 10-137
2-Fluorobiphenyl (S)%49 13-130
2-Fluorophenol (S)%39 10-130
Nitrobenzene-d5 (S)%50 13-130
Phenol-d6 (S)%31 10-130
Terphenyl-d14 (S)%82 25-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2659638MATRIX SPIKE SAMPLE:
MSSpike
Result
92441752002
1,2,4-Trichlorobenzene ug/L 18.050 36 30-130ND
1,2-Dichlorobenzene ug/L 17.950 36 30-130ND
1,3-Dichlorobenzene ug/L 17.950 36 20-130ND
1,4-Dichlorobenzene ug/L 17.850 36 30-130ND
1-Methylnaphthalene ug/L 21.950 44 30-130ND
2,2'-Oxybis(1-chloropropane)ug/L 22.350 45 20-130ND
2,4,5-Trichlorophenol ug/L 22.150 44 40-130ND
2,4,6-Trichlorophenol ug/L 22.350 45 40-130ND
2,4-Dichlorophenol ug/L 19.250 38 31-130ND
2,4-Dimethylphenol ug/L 19.650 39 30-130ND
2,4-Dinitrophenol ug/L 150250 60 30-130ND
2,4-Dinitrotoluene ug/L 29.250 58 49-130ND
2,6-Dinitrotoluene ug/L 26.150 52 50-130ND
2-Chloronaphthalene ug/L 19.550 39 30-130ND
2-Chlorophenol ug/L 18.150 36 30-130ND
2-Methylnaphthalene ug/L 22.650 45 30-130ND
2-Methylphenol(o-Cresol)ug/L 18.550 37 30-130ND
2-Nitroaniline ug/L 62.0100 62 40-130ND
2-Nitrophenol ug/L 18.550 37 20-130ND
3&4-Methylphenol(m&p Cresol)ug/L 16.550 33 20-130ND
3,3'-Dichlorobenzidine ug/L 52.0100 52 10-150ND
3-Nitroaniline ug/L 62.2100 62 40-130ND
4,6-Dinitro-2-methylphenol ug/L 68.0100 68 40-130ND
4-Bromophenylphenyl ether ug/L 31.850 64 30-130ND
4-Chloro-3-methylphenol ug/L 47.2100 47 30-130ND
4-Chloroaniline ug/L 39.2100 39 20-130ND
4-Chlorophenylphenyl ether ug/L 26.650 53 20-130ND
4-Nitroaniline ug/L 64.5100 64 40-130ND
4-Nitrophenol ug/L 92.0250 37 10-130ND
Acenaphthene ug/L 25.050 50 30-130ND
Acenaphthylene ug/L 25.050 50 30-130ND
Aniline ug/L 10.650 21 20-130ND
Anthracene ug/L 35.950 72 50-130ND
Benzo(a)anthracene ug/L 38.050 76 50-130ND
Benzo(a)pyrene ug/L 37.050 74 50-130ND
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2659638MATRIX SPIKE SAMPLE:
MSSpike
Result
92441752002
Benzo(b)fluoranthene ug/L 37.450 75 50-130ND
Benzo(g,h,i)perylene ug/L 38.150 76 50-130ND
Benzo(k)fluoranthene ug/L 37.150 74 50-130ND
Benzoic Acid ug/L 72.8250 29 10-130ND
Benzyl alcohol ug/L 37.0100 37 20-130ND
bis(2-Chloroethoxy)methane ug/L 21.350 43 30-130ND
bis(2-Chloroethyl) ether ug/L 20.650 41 30-130ND
bis(2-Ethylhexyl)phthalate ug/L 35.350 71 50-130ND
Butylbenzylphthalate ug/L 34.350 69 50-150ND
Chrysene ug/L 39.750 79 50-130ND
Di-n-butylphthalate ug/L 34.750 64 50-130ND
Di-n-octylphthalate ug/L 33.450 67 50-130ND
Dibenz(a,h)anthracene ug/L 38.050 76 40-130ND
Dibenzofuran ug/L 25.050 50 40-130ND
Diethylphthalate ug/L 30.650 61 40-130ND
Dimethylphthalate ug/L 29.550 59 40-130ND
Fluoranthene ug/L 37.550 75 30-130ND
Fluorene ug/L 28.050 56 20-130ND
Hexachloro-1,3-butadiene ug/L 16.950 34 10-130ND
Hexachlorobenzene ug/L 29.250 58 30-130ND
Hexachlorocyclopentadiene ug/L 15.650 31 10-150ND
Hexachloroethane ug/L 16.550 33 10-130ND
Indeno(1,2,3-cd)pyrene ug/L 37.650 75 40-130ND
Isophorone ug/L 20.550 41 30-130ND
N-Nitroso-di-n-propylamine ug/L 22.750 45 30-130ND
N-Nitrosodimethylamine ug/L 18.750 37 10-130ND
N-Nitrosodiphenylamine ug/L 32.150 64 30-130ND
Naphthalene ug/L 22.150 44 20-130ND
Nitrobenzene ug/L 19.650 39 20-130ND
Pentachlorophenol ug/L 67.5100 67 10-140ND
Phenanthrene ug/L 35.250 70 50-130ND
Phenol ug/L 11.250 22 10-130ND
Pyrene ug/L 39.450 79 50-130ND
2,4,6-Tribromophenol (S)%60 10-137
2-Fluorobiphenyl (S)%41 13-130
2-Fluorophenol (S)%28 10-130
Nitrobenzene-d5 (S)%40 13-130
Phenol-d6 (S)%21 10-130
Terphenyl-d14 (S)%72 25-130
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92441752
HP Stadium Phase 2
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92441752001 493445 493475GW-9 MS/MSD EPA 3010A EPA 6010D
92441752002 493445 493475GW-8 EPA 3010A EPA 6010D
92441752003 493445 493475GW-2 EPA 3010A EPA 6010D
92441752004 493445 493475GW-1 EPA 3010A EPA 6010D
92441752005 493445 493475Dup-1 EPA 3010A EPA 6010D
92441752001 493353 493397GW-9 MS/MSD EPA 7470A EPA 7470A
92441752002 493353 493397GW-8 EPA 7470A EPA 7470A
92441752003 493353 493397GW-2 EPA 7470A EPA 7470A
92441752004 493353 493397GW-1 EPA 7470A EPA 7470A
92441752005 493353 493397Dup-1 EPA 7470A EPA 7470A
92441752001 493363 493518GW-9 MS/MSD EPA 3510C EPA 8270E
92441752002 493363 493518GW-8 EPA 3510C EPA 8270E
92441752003 493363 493518GW-2 EPA 3510C EPA 8270E
92441752004 493363 493518GW-1 EPA 3510C EPA 8270E
92441752005 493363 493518Dup-1 EPA 3510C EPA 8270E
92441752001 493345GW-9 MS/MSD EPA 8260D
92441752002 493345GW-8 EPA 8260D
92441752003 493345GW-2 EPA 8260D
92441752004 493345GW-1 EPA 8260D
92441752005 493345Dup-1 EPA 8260D
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Page 36 of 39
Page 37 of 39
Page 38 of 39
Page 39 of 39
#=CL#
September 03, 2019
LIMS USE: FR - RANDY CAVALLIER
LIMS OBJECT ID: 92441608
92441608
Project:
Pace Project No.:
RE:
Mr. Randy Cavallier
ECS Southeast, LLP
4811 Koger Blvd.
Greensboro, NC 27407
High Point Ballfield 5318-F
Dear Mr. Cavallier:
Enclosed are the analytical results for sample(s) received by the laboratory on August 15, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Report revised to add Cr+6 by 7199 to Dup 3.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
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#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alaska DEC- CS/UST/LUST
Alabama Certification #: 41320
Arizona Certification# AZ0819
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
North Dakota Certification #: R-216
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FL01264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical National Certification IDs
12065 Lebanon Road, Mt. Juliet, TN 37122
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Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
REPORT OF LABORATORY ANALYSIS
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#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Pace Analytical National Certification IDs
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
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South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92441608001 GP-12 0-2'EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92441608002 GP-12 2-4'EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92441608003 DUP-3 EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANKBC
EPA 7199 1 PANGB
92441608004 GP-1 0-2'EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92441608005 GP-1 2-4'EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CPKS
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92441608006 GP-2 0-2'EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92441608007 GP-9 0-2'EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92441608008 GP-8 0-2'EPA 6020 7 PASI-OFDV
EPA 7471 1 PASI-ONMP
EPA 8270E 74 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
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#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 0-2'Lab ID:92441608001 Collected:08/14/19 09:56 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic ND mg/kg 08/23/19 09:30 7440-38-208/21/19 14:113.6 50
Barium 23.3 mg/kg 08/23/19 09:30 7440-39-308/21/19 14:113.6 50
Cadmium ND mg/kg 08/23/19 09:30 7440-43-908/21/19 14:110.44 50
Chromium 139 mg/kg 08/23/19 09:30 7440-47-308/21/19 14:113.6 50
Lead 7.3 mg/kg 08/23/19 09:30 7439-92-108/21/19 14:113.6 50
Selenium ND mg/kg 08/23/19 09:30 7782-49-208/21/19 14:113.6 50
Silver ND mg/kg 08/23/19 09:30 7440-22-4 N208/21/19 14:110.44 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 08/21/19 16:09 7439-97-608/21/19 10:350.018 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 11:26 83-32-908/17/19 15:340.39 1
Acenaphthylene ND mg/kg 08/20/19 11:26 208-96-808/17/19 15:340.39 1
Aniline ND mg/kg 08/20/19 11:26 62-53-308/17/19 15:340.39 1
Anthracene ND mg/kg 08/20/19 11:26 120-12-708/17/19 15:340.39 1
Benzo(a)anthracene ND mg/kg 08/20/19 11:26 56-55-308/17/19 15:340.39 1
Benzo(a)pyrene ND mg/kg 08/20/19 11:26 50-32-808/17/19 15:340.39 1
Benzo(b)fluoranthene ND mg/kg 08/20/19 11:26 205-99-208/17/19 15:340.39 1
Benzo(g,h,i)perylene ND mg/kg 08/20/19 11:26 191-24-208/17/19 15:340.39 1
Benzo(k)fluoranthene ND mg/kg 08/20/19 11:26 207-08-908/17/19 15:340.39 1
Benzoic Acid ND mg/kg 08/20/19 11:26 65-85-008/17/19 15:341.9 1
Benzyl alcohol ND mg/kg 08/20/19 11:26 100-51-608/17/19 15:340.78 1
4-Bromophenylphenyl ether ND mg/kg 08/20/19 11:26 101-55-308/17/19 15:340.39 1
Butylbenzylphthalate ND mg/kg 08/20/19 11:26 85-68-708/17/19 15:340.39 1
4-Chloro-3-methylphenol ND mg/kg 08/20/19 11:26 59-50-708/17/19 15:340.78 1
4-Chloroaniline ND mg/kg 08/20/19 11:26 106-47-808/17/19 15:341.9 1
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 11:26 111-91-108/17/19 15:340.39 1
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 11:26 111-44-408/17/19 15:340.39 1
2-Chloronaphthalene ND mg/kg 08/20/19 11:26 91-58-708/17/19 15:340.39 1
2-Chlorophenol ND mg/kg 08/20/19 11:26 95-57-808/17/19 15:340.39 1
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 11:26 7005-72-308/17/19 15:340.39 1
Chrysene ND mg/kg 08/20/19 11:26 218-01-908/17/19 15:340.39 1
Dibenz(a,h)anthracene ND mg/kg 08/20/19 11:26 53-70-308/17/19 15:340.39 1
Dibenzofuran ND mg/kg 08/20/19 11:26 132-64-908/17/19 15:340.39 1
1,2-Dichlorobenzene ND mg/kg 08/20/19 11:26 95-50-108/17/19 15:340.39 1
1,3-Dichlorobenzene ND mg/kg 08/20/19 11:26 541-73-108/17/19 15:340.39 1
1,4-Dichlorobenzene ND mg/kg 08/20/19 11:26 106-46-708/17/19 15:340.39 1
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 11:26 91-94-108/17/19 15:341.9 1
2,4-Dichlorophenol ND mg/kg 08/20/19 11:26 120-83-208/17/19 15:340.39 1
Diethylphthalate ND mg/kg 08/20/19 11:26 84-66-208/17/19 15:340.39 1
2,4-Dimethylphenol ND mg/kg 08/20/19 11:26 105-67-908/17/19 15:340.39 1
Dimethylphthalate ND mg/kg 08/20/19 11:26 131-11-308/17/19 15:340.39 1
Di-n-butylphthalate ND mg/kg 08/20/19 11:26 84-74-208/17/19 15:340.39 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 11:26 534-52-108/17/19 15:340.78 1
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 0-2'Lab ID:92441608001 Collected:08/14/19 09:56 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/20/19 11:26 51-28-508/17/19 15:341.9 1
2,4-Dinitrotoluene ND mg/kg 08/20/19 11:26 121-14-208/17/19 15:340.39 1
2,6-Dinitrotoluene ND mg/kg 08/20/19 11:26 606-20-208/17/19 15:340.39 1
Di-n-octylphthalate ND mg/kg 08/20/19 11:26 117-84-008/17/19 15:340.39 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 11:26 117-81-708/17/19 15:340.39 1
Fluoranthene ND mg/kg 08/20/19 11:26 206-44-008/17/19 15:340.39 1
Fluorene ND mg/kg 08/20/19 11:26 86-73-708/17/19 15:340.39 1
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 11:26 87-68-308/17/19 15:340.39 1
Hexachlorobenzene ND mg/kg 08/20/19 11:26 118-74-108/17/19 15:340.39 1
Hexachlorocyclopentadiene ND mg/kg 08/20/19 11:26 77-47-408/17/19 15:340.39 1
Hexachloroethane ND mg/kg 08/20/19 11:26 67-72-108/17/19 15:340.39 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 11:26 193-39-508/17/19 15:340.39 1
Isophorone ND mg/kg 08/20/19 11:26 78-59-108/17/19 15:340.39 1
1-Methylnaphthalene ND mg/kg 08/20/19 11:26 90-12-008/17/19 15:340.39 1
2-Methylnaphthalene ND mg/kg 08/20/19 11:26 91-57-608/17/19 15:340.39 1
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 11:26 95-48-708/17/19 15:340.39 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 11:26 15831-10-408/17/19 15:340.39 1
Naphthalene ND mg/kg 08/20/19 11:26 91-20-308/17/19 15:340.39 1
2-Nitroaniline ND mg/kg 08/20/19 11:26 88-74-408/17/19 15:341.9 1
3-Nitroaniline ND mg/kg 08/20/19 11:26 99-09-208/17/19 15:341.9 1
4-Nitroaniline ND mg/kg 08/20/19 11:26 100-01-608/17/19 15:340.78 1
Nitrobenzene ND mg/kg 08/20/19 11:26 98-95-308/17/19 15:340.39 1
2-Nitrophenol ND mg/kg 08/20/19 11:26 88-75-508/17/19 15:340.39 1
4-Nitrophenol ND mg/kg 08/20/19 11:26 100-02-708/17/19 15:341.9 1
N-Nitrosodimethylamine ND mg/kg 08/20/19 11:26 62-75-908/17/19 15:340.39 1
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 11:26 621-64-708/17/19 15:340.39 1
N-Nitrosodiphenylamine ND mg/kg 08/20/19 11:26 86-30-608/17/19 15:340.39 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 11:26 108-60-108/17/19 15:340.39 1
Pentachlorophenol ND mg/kg 08/20/19 11:26 87-86-508/17/19 15:341.9 1
Phenanthrene ND mg/kg 08/20/19 11:26 85-01-808/17/19 15:340.39 1
Phenol ND mg/kg 08/20/19 11:26 108-95-208/17/19 15:340.39 1
Pyrene ND mg/kg 08/20/19 11:26 129-00-008/17/19 15:340.39 1
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 11:26 120-82-108/17/19 15:340.39 1
2,4,5-Trichlorophenol ND mg/kg 08/20/19 11:26 95-95-408/17/19 15:340.39 1
2,4,6-Trichlorophenol ND mg/kg 08/20/19 11:26 88-06-208/17/19 15:340.39 1
Surrogates
Nitrobenzene-d5 (S)67 %08/20/19 11:26 4165-60-008/17/19 15:3423-110 1
2-Fluorobiphenyl (S)66 %08/20/19 11:26 321-60-808/17/19 15:3430-110 1
Terphenyl-d14 (S)83 %08/20/19 11:26 1718-51-008/17/19 15:3428-110 1
Phenol-d6 (S)61 %08/20/19 11:26 13127-88-308/17/19 15:3422-110 1
2-Fluorophenol (S)59 %08/20/19 11:26 367-12-408/17/19 15:3413-110 1
2,4,6-Tribromophenol (S)78 %08/20/19 11:26 118-79-608/17/19 15:3427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 16:42 67-64-108/19/19 14:090.081 1
Benzene ND mg/kg 08/19/19 16:42 71-43-208/19/19 14:090.0041 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 0-2'Lab ID:92441608001 Collected:08/14/19 09:56 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Bromobenzene ND mg/kg 08/19/19 16:42 108-86-108/19/19 14:090.0041 1
Bromochloromethane ND mg/kg 08/19/19 16:42 74-97-508/19/19 14:090.0041 1
Bromodichloromethane ND mg/kg 08/19/19 16:42 75-27-408/19/19 14:090.0041 1
Bromoform ND mg/kg 08/19/19 16:42 75-25-208/19/19 14:090.0041 1
Bromomethane ND mg/kg 08/19/19 16:42 74-83-908/19/19 14:090.0081 1
2-Butanone (MEK)ND mg/kg 08/19/19 16:42 78-93-308/19/19 14:090.081 1
n-Butylbenzene ND mg/kg 08/19/19 16:42 104-51-808/19/19 14:090.0041 1
sec-Butylbenzene ND mg/kg 08/19/19 16:42 135-98-808/19/19 14:090.0041 1
tert-Butylbenzene ND mg/kg 08/19/19 16:42 98-06-608/19/19 14:090.0041 1
Carbon tetrachloride ND mg/kg 08/19/19 16:42 56-23-508/19/19 14:090.0041 1
Chlorobenzene ND mg/kg 08/19/19 16:42 108-90-708/19/19 14:090.0041 1
Chloroethane ND mg/kg 08/19/19 16:42 75-00-308/19/19 14:090.0081 1
Chloroform ND mg/kg 08/19/19 16:42 67-66-308/19/19 14:090.0041 1
Chloromethane ND mg/kg 08/19/19 16:42 74-87-308/19/19 14:090.0081 1
2-Chlorotoluene ND mg/kg 08/19/19 16:42 95-49-808/19/19 14:090.0041 1
4-Chlorotoluene ND mg/kg 08/19/19 16:42 106-43-408/19/19 14:090.0041 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 16:42 96-12-808/19/19 14:090.0041 1
Dibromochloromethane ND mg/kg 08/19/19 16:42 124-48-108/19/19 14:090.0041 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 16:42 106-93-408/19/19 14:090.0041 1
Dibromomethane ND mg/kg 08/19/19 16:42 74-95-308/19/19 14:090.0041 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 16:42 95-50-108/19/19 14:090.0041 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 16:42 541-73-108/19/19 14:090.0041 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 16:42 106-46-708/19/19 14:090.0041 1
Dichlorodifluoromethane ND mg/kg 08/19/19 16:42 75-71-808/19/19 14:090.0081 1
1,1-Dichloroethane ND mg/kg 08/19/19 16:42 75-34-308/19/19 14:090.0041 1
1,2-Dichloroethane ND mg/kg 08/19/19 16:42 107-06-208/19/19 14:090.0041 1
1,1-Dichloroethene ND mg/kg 08/19/19 16:42 75-35-408/19/19 14:090.0041 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 16:42 156-59-208/19/19 14:090.0041 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 16:42 156-60-508/19/19 14:090.0041 1
1,2-Dichloropropane ND mg/kg 08/19/19 16:42 78-87-508/19/19 14:090.0041 1
1,3-Dichloropropane ND mg/kg 08/19/19 16:42 142-28-908/19/19 14:090.0041 1
2,2-Dichloropropane ND mg/kg 08/19/19 16:42 594-20-708/19/19 14:090.0041 1
1,1-Dichloropropene ND mg/kg 08/19/19 16:42 563-58-608/19/19 14:090.0041 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 16:42 10061-01-508/19/19 14:090.0041 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 16:42 10061-02-608/19/19 14:090.0041 1
Diisopropyl ether ND mg/kg 08/19/19 16:42 108-20-308/19/19 14:090.0041 1
Ethylbenzene ND mg/kg 08/19/19 16:42 100-41-408/19/19 14:090.0041 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 16:42 87-68-308/19/19 14:090.0041 1
2-Hexanone ND mg/kg 08/19/19 16:42 591-78-608/19/19 14:090.041 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 16:42 98-82-808/19/19 14:090.0041 1
p-Isopropyltoluene ND mg/kg 08/19/19 16:42 99-87-608/19/19 14:090.0041 1
Methylene Chloride ND mg/kg 08/19/19 16:42 75-09-208/19/19 14:090.016 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 16:42 108-10-108/19/19 14:090.041 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 16:42 1634-04-408/19/19 14:090.0041 1
Naphthalene ND mg/kg 08/19/19 16:42 91-20-308/19/19 14:090.0041 1
n-Propylbenzene ND mg/kg 08/19/19 16:42 103-65-108/19/19 14:090.0041 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 0-2'Lab ID:92441608001 Collected:08/14/19 09:56 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Styrene ND mg/kg 08/19/19 16:42 100-42-508/19/19 14:090.0041 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 16:42 630-20-608/19/19 14:090.0041 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 16:42 79-34-508/19/19 14:090.0041 1
Tetrachloroethene ND mg/kg 08/19/19 16:42 127-18-408/19/19 14:090.0041 1
Toluene ND mg/kg 08/19/19 16:42 108-88-308/19/19 14:090.0041 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 16:42 87-61-608/19/19 14:090.0041 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 16:42 120-82-108/19/19 14:090.0041 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 16:42 71-55-608/19/19 14:090.0041 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 16:42 79-00-508/19/19 14:090.0041 1
Trichloroethene ND mg/kg 08/19/19 16:42 79-01-608/19/19 14:090.0041 1
Trichlorofluoromethane ND mg/kg 08/19/19 16:42 75-69-408/19/19 14:090.0041 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 16:42 96-18-408/19/19 14:090.0041 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 16:42 95-63-608/19/19 14:090.0041 1
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 16:42 108-67-808/19/19 14:090.0041 1
Vinyl acetate ND mg/kg 08/19/19 16:42 108-05-408/19/19 14:090.041 1
Vinyl chloride ND mg/kg 08/19/19 16:42 75-01-408/19/19 14:090.0081 1
Xylene (Total)ND mg/kg 08/19/19 16:42 1330-20-708/19/19 14:090.0081 1
m&p-Xylene ND mg/kg 08/19/19 16:42 179601-23-108/19/19 14:090.0081 1
o-Xylene ND mg/kg 08/19/19 16:42 95-47-608/19/19 14:090.0041 1
Surrogates
Toluene-d8 (S)105 %08/19/19 16:42 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)100 %08/19/19 16:42 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)93 %08/19/19 16:42 17060-07-008/19/19 14:0970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 14.7 %08/16/19 17:040.10 1
Sample:GP-12 2-4'Lab ID:92441608002 Collected:08/14/19 10:08 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic ND mg/kg 08/23/19 09:33 7440-38-208/21/19 14:114.1 50
Barium 176 mg/kg 08/23/19 09:33 7440-39-308/21/19 14:114.1 50
Cadmium ND mg/kg 08/23/19 09:33 7440-43-908/21/19 14:110.49 50
Chromium 104 mg/kg 08/23/19 09:33 7440-47-308/21/19 14:114.1 50
Lead 8.0 mg/kg 08/23/19 09:33 7439-92-108/21/19 14:114.1 50
Selenium ND mg/kg 08/23/19 09:33 7782-49-208/21/19 14:114.1 50
Silver ND mg/kg 08/23/19 09:33 7440-22-4 N208/21/19 14:110.49 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.045 mg/kg 08/21/19 16:11 7439-97-608/21/19 10:350.022 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 2-4'Lab ID:92441608002 Collected:08/14/19 10:08 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 11:59 83-32-908/17/19 15:340.45 1
Acenaphthylene ND mg/kg 08/20/19 11:59 208-96-808/17/19 15:340.45 1
Aniline ND mg/kg 08/20/19 11:59 62-53-308/17/19 15:340.45 1
Anthracene ND mg/kg 08/20/19 11:59 120-12-708/17/19 15:340.45 1
Benzo(a)anthracene ND mg/kg 08/20/19 11:59 56-55-308/17/19 15:340.45 1
Benzo(a)pyrene ND mg/kg 08/20/19 11:59 50-32-808/17/19 15:340.45 1
Benzo(b)fluoranthene ND mg/kg 08/20/19 11:59 205-99-208/17/19 15:340.45 1
Benzo(g,h,i)perylene ND mg/kg 08/20/19 11:59 191-24-208/17/19 15:340.45 1
Benzo(k)fluoranthene ND mg/kg 08/20/19 11:59 207-08-908/17/19 15:340.45 1
Benzoic Acid ND mg/kg 08/20/19 11:59 65-85-008/17/19 15:342.3 1
Benzyl alcohol ND mg/kg 08/20/19 11:59 100-51-608/17/19 15:340.90 1
4-Bromophenylphenyl ether ND mg/kg 08/20/19 11:59 101-55-308/17/19 15:340.45 1
Butylbenzylphthalate ND mg/kg 08/20/19 11:59 85-68-708/17/19 15:340.45 1
4-Chloro-3-methylphenol ND mg/kg 08/20/19 11:59 59-50-708/17/19 15:340.90 1
4-Chloroaniline ND mg/kg 08/20/19 11:59 106-47-808/17/19 15:342.3 1
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 11:59 111-91-108/17/19 15:340.45 1
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 11:59 111-44-408/17/19 15:340.45 1
2-Chloronaphthalene ND mg/kg 08/20/19 11:59 91-58-708/17/19 15:340.45 1
2-Chlorophenol ND mg/kg 08/20/19 11:59 95-57-808/17/19 15:340.45 1
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 11:59 7005-72-308/17/19 15:340.45 1
Chrysene ND mg/kg 08/20/19 11:59 218-01-908/17/19 15:340.45 1
Dibenz(a,h)anthracene ND mg/kg 08/20/19 11:59 53-70-308/17/19 15:340.45 1
Dibenzofuran ND mg/kg 08/20/19 11:59 132-64-908/17/19 15:340.45 1
1,2-Dichlorobenzene ND mg/kg 08/20/19 11:59 95-50-108/17/19 15:340.45 1
1,3-Dichlorobenzene ND mg/kg 08/20/19 11:59 541-73-108/17/19 15:340.45 1
1,4-Dichlorobenzene ND mg/kg 08/20/19 11:59 106-46-708/17/19 15:340.45 1
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 11:59 91-94-108/17/19 15:342.3 1
2,4-Dichlorophenol ND mg/kg 08/20/19 11:59 120-83-208/17/19 15:340.45 1
Diethylphthalate ND mg/kg 08/20/19 11:59 84-66-208/17/19 15:340.45 1
2,4-Dimethylphenol ND mg/kg 08/20/19 11:59 105-67-908/17/19 15:340.45 1
Dimethylphthalate ND mg/kg 08/20/19 11:59 131-11-308/17/19 15:340.45 1
Di-n-butylphthalate ND mg/kg 08/20/19 11:59 84-74-208/17/19 15:340.45 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 11:59 534-52-108/17/19 15:340.90 1
2,4-Dinitrophenol ND mg/kg 08/20/19 11:59 51-28-508/17/19 15:342.3 1
2,4-Dinitrotoluene ND mg/kg 08/20/19 11:59 121-14-208/17/19 15:340.45 1
2,6-Dinitrotoluene ND mg/kg 08/20/19 11:59 606-20-208/17/19 15:340.45 1
Di-n-octylphthalate ND mg/kg 08/20/19 11:59 117-84-008/17/19 15:340.45 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 11:59 117-81-708/17/19 15:340.45 1
Fluoranthene ND mg/kg 08/20/19 11:59 206-44-008/17/19 15:340.45 1
Fluorene ND mg/kg 08/20/19 11:59 86-73-708/17/19 15:340.45 1
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 11:59 87-68-308/17/19 15:340.45 1
Hexachlorobenzene ND mg/kg 08/20/19 11:59 118-74-108/17/19 15:340.45 1
Hexachlorocyclopentadiene ND mg/kg 08/20/19 11:59 77-47-408/17/19 15:340.45 1
Hexachloroethane ND mg/kg 08/20/19 11:59 67-72-108/17/19 15:340.45 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 11:59 193-39-508/17/19 15:340.45 1
Isophorone ND mg/kg 08/20/19 11:59 78-59-108/17/19 15:340.45 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 2-4'Lab ID:92441608002 Collected:08/14/19 10:08 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
1-Methylnaphthalene ND mg/kg 08/20/19 11:59 90-12-008/17/19 15:340.45 1
2-Methylnaphthalene ND mg/kg 08/20/19 11:59 91-57-608/17/19 15:340.45 1
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 11:59 95-48-708/17/19 15:340.45 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 11:59 15831-10-408/17/19 15:340.45 1
Naphthalene ND mg/kg 08/20/19 11:59 91-20-308/17/19 15:340.45 1
2-Nitroaniline ND mg/kg 08/20/19 11:59 88-74-408/17/19 15:342.3 1
3-Nitroaniline ND mg/kg 08/20/19 11:59 99-09-208/17/19 15:342.3 1
4-Nitroaniline ND mg/kg 08/20/19 11:59 100-01-608/17/19 15:340.90 1
Nitrobenzene ND mg/kg 08/20/19 11:59 98-95-308/17/19 15:340.45 1
2-Nitrophenol ND mg/kg 08/20/19 11:59 88-75-508/17/19 15:340.45 1
4-Nitrophenol ND mg/kg 08/20/19 11:59 100-02-708/17/19 15:342.3 1
N-Nitrosodimethylamine ND mg/kg 08/20/19 11:59 62-75-908/17/19 15:340.45 1
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 11:59 621-64-708/17/19 15:340.45 1
N-Nitrosodiphenylamine ND mg/kg 08/20/19 11:59 86-30-608/17/19 15:340.45 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 11:59 108-60-108/17/19 15:340.45 1
Pentachlorophenol ND mg/kg 08/20/19 11:59 87-86-508/17/19 15:342.3 1
Phenanthrene ND mg/kg 08/20/19 11:59 85-01-808/17/19 15:340.45 1
Phenol ND mg/kg 08/20/19 11:59 108-95-208/17/19 15:340.45 1
Pyrene ND mg/kg 08/20/19 11:59 129-00-008/17/19 15:340.45 1
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 11:59 120-82-108/17/19 15:340.45 1
2,4,5-Trichlorophenol ND mg/kg 08/20/19 11:59 95-95-408/17/19 15:340.45 1
2,4,6-Trichlorophenol ND mg/kg 08/20/19 11:59 88-06-208/17/19 15:340.45 1
Surrogates
Nitrobenzene-d5 (S)69 %08/20/19 11:59 4165-60-008/17/19 15:3423-110 1
2-Fluorobiphenyl (S)68 %08/20/19 11:59 321-60-808/17/19 15:3430-110 1
Terphenyl-d14 (S)83 %08/20/19 11:59 1718-51-008/17/19 15:3428-110 1
Phenol-d6 (S)57 %08/20/19 11:59 13127-88-308/17/19 15:3422-110 1
2-Fluorophenol (S)55 %08/20/19 11:59 367-12-408/17/19 15:3413-110 1
2,4,6-Tribromophenol (S)74 %08/20/19 11:59 118-79-608/17/19 15:3427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 17:06 67-64-108/19/19 14:090.10 1
Benzene ND mg/kg 08/19/19 17:06 71-43-208/19/19 14:090.0052 1
Bromobenzene ND mg/kg 08/19/19 17:06 108-86-108/19/19 14:090.0052 1
Bromochloromethane ND mg/kg 08/19/19 17:06 74-97-508/19/19 14:090.0052 1
Bromodichloromethane ND mg/kg 08/19/19 17:06 75-27-408/19/19 14:090.0052 1
Bromoform ND mg/kg 08/19/19 17:06 75-25-208/19/19 14:090.0052 1
Bromomethane ND mg/kg 08/19/19 17:06 74-83-908/19/19 14:090.010 1
2-Butanone (MEK)ND mg/kg 08/19/19 17:06 78-93-308/19/19 14:090.10 1
n-Butylbenzene ND mg/kg 08/19/19 17:06 104-51-808/19/19 14:090.0052 1
sec-Butylbenzene ND mg/kg 08/19/19 17:06 135-98-808/19/19 14:090.0052 1
tert-Butylbenzene ND mg/kg 08/19/19 17:06 98-06-608/19/19 14:090.0052 1
Carbon tetrachloride ND mg/kg 08/19/19 17:06 56-23-508/19/19 14:090.0052 1
Chlorobenzene ND mg/kg 08/19/19 17:06 108-90-708/19/19 14:090.0052 1
Chloroethane ND mg/kg 08/19/19 17:06 75-00-308/19/19 14:090.010 1
Chloroform ND mg/kg 08/19/19 17:06 67-66-308/19/19 14:090.0052 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 2-4'Lab ID:92441608002 Collected:08/14/19 10:08 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Chloromethane ND mg/kg 08/19/19 17:06 74-87-308/19/19 14:090.010 1
2-Chlorotoluene ND mg/kg 08/19/19 17:06 95-49-808/19/19 14:090.0052 1
4-Chlorotoluene ND mg/kg 08/19/19 17:06 106-43-408/19/19 14:090.0052 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 17:06 96-12-808/19/19 14:090.0052 1
Dibromochloromethane ND mg/kg 08/19/19 17:06 124-48-108/19/19 14:090.0052 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 17:06 106-93-408/19/19 14:090.0052 1
Dibromomethane ND mg/kg 08/19/19 17:06 74-95-308/19/19 14:090.0052 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 17:06 95-50-108/19/19 14:090.0052 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 17:06 541-73-108/19/19 14:090.0052 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 17:06 106-46-708/19/19 14:090.0052 1
Dichlorodifluoromethane ND mg/kg 08/19/19 17:06 75-71-808/19/19 14:090.010 1
1,1-Dichloroethane ND mg/kg 08/19/19 17:06 75-34-308/19/19 14:090.0052 1
1,2-Dichloroethane ND mg/kg 08/19/19 17:06 107-06-208/19/19 14:090.0052 1
1,1-Dichloroethene ND mg/kg 08/19/19 17:06 75-35-408/19/19 14:090.0052 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 17:06 156-59-208/19/19 14:090.0052 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 17:06 156-60-508/19/19 14:090.0052 1
1,2-Dichloropropane ND mg/kg 08/19/19 17:06 78-87-508/19/19 14:090.0052 1
1,3-Dichloropropane ND mg/kg 08/19/19 17:06 142-28-908/19/19 14:090.0052 1
2,2-Dichloropropane ND mg/kg 08/19/19 17:06 594-20-708/19/19 14:090.0052 1
1,1-Dichloropropene ND mg/kg 08/19/19 17:06 563-58-608/19/19 14:090.0052 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 17:06 10061-01-508/19/19 14:090.0052 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 17:06 10061-02-608/19/19 14:090.0052 1
Diisopropyl ether ND mg/kg 08/19/19 17:06 108-20-308/19/19 14:090.0052 1
Ethylbenzene ND mg/kg 08/19/19 17:06 100-41-408/19/19 14:090.0052 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 17:06 87-68-308/19/19 14:090.0052 1
2-Hexanone ND mg/kg 08/19/19 17:06 591-78-608/19/19 14:090.052 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 17:06 98-82-808/19/19 14:090.0052 1
p-Isopropyltoluene ND mg/kg 08/19/19 17:06 99-87-608/19/19 14:090.0052 1
Methylene Chloride ND mg/kg 08/19/19 17:06 75-09-208/19/19 14:090.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 17:06 108-10-108/19/19 14:090.052 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 17:06 1634-04-408/19/19 14:090.0052 1
Naphthalene ND mg/kg 08/19/19 17:06 91-20-308/19/19 14:090.0052 1
n-Propylbenzene ND mg/kg 08/19/19 17:06 103-65-108/19/19 14:090.0052 1
Styrene ND mg/kg 08/19/19 17:06 100-42-508/19/19 14:090.0052 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 17:06 630-20-608/19/19 14:090.0052 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 17:06 79-34-508/19/19 14:090.0052 1
Tetrachloroethene ND mg/kg 08/19/19 17:06 127-18-408/19/19 14:090.0052 1
Toluene ND mg/kg 08/19/19 17:06 108-88-308/19/19 14:090.0052 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 17:06 87-61-608/19/19 14:090.0052 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 17:06 120-82-108/19/19 14:090.0052 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 17:06 71-55-608/19/19 14:090.0052 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 17:06 79-00-508/19/19 14:090.0052 1
Trichloroethene ND mg/kg 08/19/19 17:06 79-01-608/19/19 14:090.0052 1
Trichlorofluoromethane ND mg/kg 08/19/19 17:06 75-69-408/19/19 14:090.0052 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 17:06 96-18-408/19/19 14:090.0052 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 17:06 95-63-608/19/19 14:090.0052 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-12 2-4'Lab ID:92441608002 Collected:08/14/19 10:08 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 17:06 108-67-808/19/19 14:090.0052 1
Vinyl acetate ND mg/kg 08/19/19 17:06 108-05-408/19/19 14:090.052 1
Vinyl chloride ND mg/kg 08/19/19 17:06 75-01-408/19/19 14:090.010 1
Xylene (Total)ND mg/kg 08/19/19 17:06 1330-20-708/19/19 14:090.010 1
m&p-Xylene ND mg/kg 08/19/19 17:06 179601-23-108/19/19 14:090.010 1
o-Xylene ND mg/kg 08/19/19 17:06 95-47-608/19/19 14:090.0052 1
Surrogates
Toluene-d8 (S)103 %08/19/19 17:06 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)102 %08/19/19 17:06 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)96 %08/19/19 17:06 17060-07-008/19/19 14:0970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 26.7 %08/16/19 17:050.10 1
Sample:DUP-3 Lab ID:92441608003 Collected:08/14/19 10:22 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic ND mg/kg 08/23/19 09:36 7440-38-208/21/19 14:114.5 50
Barium 191 mg/kg 08/23/19 09:36 7440-39-308/21/19 14:114.5 50
Cadmium ND mg/kg 08/23/19 09:36 7440-43-908/21/19 14:110.54 50
Chromium 206 mg/kg 08/23/19 16:55 7440-47-308/21/19 14:119.0 100
Lead ND mg/kg 08/23/19 09:36 7439-92-108/21/19 14:114.5 50
Selenium 6.6 mg/kg 08/23/19 09:36 7782-49-208/21/19 14:114.5 50
Silver ND mg/kg 08/23/19 09:36 7440-22-4 N208/21/19 14:110.54 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury ND mg/kg 08/21/19 16:13 7439-97-608/21/19 10:350.023 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 12:38 83-32-908/17/19 15:340.49 1
Acenaphthylene ND mg/kg 08/20/19 12:38 208-96-808/17/19 15:340.49 1
Aniline ND mg/kg 08/20/19 12:38 62-53-308/17/19 15:340.49 1
Anthracene ND mg/kg 08/20/19 12:38 120-12-708/17/19 15:340.49 1
Benzo(a)anthracene ND mg/kg 08/20/19 12:38 56-55-308/17/19 15:340.49 1
Benzo(a)pyrene ND mg/kg 08/20/19 12:38 50-32-808/17/19 15:340.49 1
Benzo(b)fluoranthene ND mg/kg 08/20/19 12:38 205-99-208/17/19 15:340.49 1
Benzo(g,h,i)perylene ND mg/kg 08/20/19 12:38 191-24-208/17/19 15:340.49 1
Benzo(k)fluoranthene ND mg/kg 08/20/19 12:38 207-08-908/17/19 15:340.49 1
Benzoic Acid ND mg/kg 08/20/19 12:38 65-85-008/17/19 15:342.4 1
Benzyl alcohol ND mg/kg 08/20/19 12:38 100-51-608/17/19 15:340.97 1
4-Bromophenylphenyl ether ND mg/kg 08/20/19 12:38 101-55-308/17/19 15:340.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:DUP-3 Lab ID:92441608003 Collected:08/14/19 10:22 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Butylbenzylphthalate ND mg/kg 08/20/19 12:38 85-68-708/17/19 15:340.49 1
4-Chloro-3-methylphenol ND mg/kg 08/20/19 12:38 59-50-708/17/19 15:340.97 1
4-Chloroaniline ND mg/kg 08/20/19 12:38 106-47-808/17/19 15:342.4 1
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 12:38 111-91-108/17/19 15:340.49 1
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 12:38 111-44-408/17/19 15:340.49 1
2-Chloronaphthalene ND mg/kg 08/20/19 12:38 91-58-708/17/19 15:340.49 1
2-Chlorophenol ND mg/kg 08/20/19 12:38 95-57-808/17/19 15:340.49 1
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 12:38 7005-72-308/17/19 15:340.49 1
Chrysene ND mg/kg 08/20/19 12:38 218-01-908/17/19 15:340.49 1
Dibenz(a,h)anthracene ND mg/kg 08/20/19 12:38 53-70-308/17/19 15:340.49 1
Dibenzofuran ND mg/kg 08/20/19 12:38 132-64-908/17/19 15:340.49 1
1,2-Dichlorobenzene ND mg/kg 08/20/19 12:38 95-50-108/17/19 15:340.49 1
1,3-Dichlorobenzene ND mg/kg 08/20/19 12:38 541-73-108/17/19 15:340.49 1
1,4-Dichlorobenzene ND mg/kg 08/20/19 12:38 106-46-708/17/19 15:340.49 1
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 12:38 91-94-108/17/19 15:342.4 1
2,4-Dichlorophenol ND mg/kg 08/20/19 12:38 120-83-208/17/19 15:340.49 1
Diethylphthalate ND mg/kg 08/20/19 12:38 84-66-208/17/19 15:340.49 1
2,4-Dimethylphenol ND mg/kg 08/20/19 12:38 105-67-908/17/19 15:340.49 1
Dimethylphthalate ND mg/kg 08/20/19 12:38 131-11-308/17/19 15:340.49 1
Di-n-butylphthalate ND mg/kg 08/20/19 12:38 84-74-208/17/19 15:340.49 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 12:38 534-52-108/17/19 15:340.97 1
2,4-Dinitrophenol ND mg/kg 08/20/19 12:38 51-28-508/17/19 15:342.4 1
2,4-Dinitrotoluene ND mg/kg 08/20/19 12:38 121-14-208/17/19 15:340.49 1
2,6-Dinitrotoluene ND mg/kg 08/20/19 12:38 606-20-208/17/19 15:340.49 1
Di-n-octylphthalate ND mg/kg 08/20/19 12:38 117-84-008/17/19 15:340.49 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 12:38 117-81-708/17/19 15:340.49 1
Fluoranthene ND mg/kg 08/20/19 12:38 206-44-008/17/19 15:340.49 1
Fluorene ND mg/kg 08/20/19 12:38 86-73-708/17/19 15:340.49 1
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 12:38 87-68-308/17/19 15:340.49 1
Hexachlorobenzene ND mg/kg 08/20/19 12:38 118-74-108/17/19 15:340.49 1
Hexachlorocyclopentadiene ND mg/kg 08/20/19 12:38 77-47-408/17/19 15:340.49 1
Hexachloroethane ND mg/kg 08/20/19 12:38 67-72-108/17/19 15:340.49 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 12:38 193-39-508/17/19 15:340.49 1
Isophorone ND mg/kg 08/20/19 12:38 78-59-108/17/19 15:340.49 1
1-Methylnaphthalene ND mg/kg 08/20/19 12:38 90-12-008/17/19 15:340.49 1
2-Methylnaphthalene ND mg/kg 08/20/19 12:38 91-57-608/17/19 15:340.49 1
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 12:38 95-48-708/17/19 15:340.49 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 12:38 15831-10-408/17/19 15:340.49 1
Naphthalene ND mg/kg 08/20/19 12:38 91-20-308/17/19 15:340.49 1
2-Nitroaniline ND mg/kg 08/20/19 12:38 88-74-408/17/19 15:342.4 1
3-Nitroaniline ND mg/kg 08/20/19 12:38 99-09-208/17/19 15:342.4 1
4-Nitroaniline ND mg/kg 08/20/19 12:38 100-01-608/17/19 15:340.97 1
Nitrobenzene ND mg/kg 08/20/19 12:38 98-95-308/17/19 15:340.49 1
2-Nitrophenol ND mg/kg 08/20/19 12:38 88-75-508/17/19 15:340.49 1
4-Nitrophenol ND mg/kg 08/20/19 12:38 100-02-7 v208/17/19 15:342.4 1
N-Nitrosodimethylamine ND mg/kg 08/20/19 12:38 62-75-9 v108/17/19 15:340.49 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:DUP-3 Lab ID:92441608003 Collected:08/14/19 10:22 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 12:38 621-64-708/17/19 15:340.49 1
N-Nitrosodiphenylamine ND mg/kg 08/20/19 12:38 86-30-608/17/19 15:340.49 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 12:38 108-60-108/17/19 15:340.49 1
Pentachlorophenol ND mg/kg 08/20/19 12:38 87-86-508/17/19 15:342.4 1
Phenanthrene ND mg/kg 08/20/19 12:38 85-01-808/17/19 15:340.49 1
Phenol ND mg/kg 08/20/19 12:38 108-95-208/17/19 15:340.49 1
Pyrene ND mg/kg 08/20/19 12:38 129-00-008/17/19 15:340.49 1
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 12:38 120-82-108/17/19 15:340.49 1
2,4,5-Trichlorophenol ND mg/kg 08/20/19 12:38 95-95-408/17/19 15:340.49 1
2,4,6-Trichlorophenol ND mg/kg 08/20/19 12:38 88-06-208/17/19 15:340.49 1
Surrogates
Nitrobenzene-d5 (S)58 %08/20/19 12:38 4165-60-008/17/19 15:3423-110 1
2-Fluorobiphenyl (S)64 %08/20/19 12:38 321-60-808/17/19 15:3430-110 1
Terphenyl-d14 (S)93 %08/20/19 12:38 1718-51-008/17/19 15:3428-110 1
Phenol-d6 (S)62 %08/20/19 12:38 13127-88-308/17/19 15:3422-110 1
2-Fluorophenol (S)61 %08/20/19 12:38 367-12-408/17/19 15:3413-110 1
2,4,6-Tribromophenol (S)76 %08/20/19 12:38 118-79-608/17/19 15:3427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 17:31 67-64-108/19/19 14:090.11 1
Benzene ND mg/kg 08/19/19 17:31 71-43-208/19/19 14:090.0057 1
Bromobenzene ND mg/kg 08/19/19 17:31 108-86-108/19/19 14:090.0057 1
Bromochloromethane ND mg/kg 08/19/19 17:31 74-97-508/19/19 14:090.0057 1
Bromodichloromethane ND mg/kg 08/19/19 17:31 75-27-408/19/19 14:090.0057 1
Bromoform ND mg/kg 08/19/19 17:31 75-25-208/19/19 14:090.0057 1
Bromomethane ND mg/kg 08/19/19 17:31 74-83-908/19/19 14:090.011 1
2-Butanone (MEK)ND mg/kg 08/19/19 17:31 78-93-308/19/19 14:090.11 1
n-Butylbenzene ND mg/kg 08/19/19 17:31 104-51-808/19/19 14:090.0057 1
sec-Butylbenzene ND mg/kg 08/19/19 17:31 135-98-808/19/19 14:090.0057 1
tert-Butylbenzene ND mg/kg 08/19/19 17:31 98-06-608/19/19 14:090.0057 1
Carbon tetrachloride ND mg/kg 08/19/19 17:31 56-23-508/19/19 14:090.0057 1
Chlorobenzene ND mg/kg 08/19/19 17:31 108-90-708/19/19 14:090.0057 1
Chloroethane ND mg/kg 08/19/19 17:31 75-00-308/19/19 14:090.011 1
Chloroform ND mg/kg 08/19/19 17:31 67-66-308/19/19 14:090.0057 1
Chloromethane ND mg/kg 08/19/19 17:31 74-87-308/19/19 14:090.011 1
2-Chlorotoluene ND mg/kg 08/19/19 17:31 95-49-808/19/19 14:090.0057 1
4-Chlorotoluene ND mg/kg 08/19/19 17:31 106-43-408/19/19 14:090.0057 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 17:31 96-12-808/19/19 14:090.0057 1
Dibromochloromethane ND mg/kg 08/19/19 17:31 124-48-108/19/19 14:090.0057 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 17:31 106-93-408/19/19 14:090.0057 1
Dibromomethane ND mg/kg 08/19/19 17:31 74-95-308/19/19 14:090.0057 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 17:31 95-50-108/19/19 14:090.0057 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 17:31 541-73-108/19/19 14:090.0057 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 17:31 106-46-708/19/19 14:090.0057 1
Dichlorodifluoromethane ND mg/kg 08/19/19 17:31 75-71-808/19/19 14:090.011 1
1,1-Dichloroethane ND mg/kg 08/19/19 17:31 75-34-308/19/19 14:090.0057 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:DUP-3 Lab ID:92441608003 Collected:08/14/19 10:22 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
1,2-Dichloroethane ND mg/kg 08/19/19 17:31 107-06-208/19/19 14:090.0057 1
1,1-Dichloroethene ND mg/kg 08/19/19 17:31 75-35-408/19/19 14:090.0057 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 17:31 156-59-208/19/19 14:090.0057 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 17:31 156-60-508/19/19 14:090.0057 1
1,2-Dichloropropane ND mg/kg 08/19/19 17:31 78-87-508/19/19 14:090.0057 1
1,3-Dichloropropane ND mg/kg 08/19/19 17:31 142-28-908/19/19 14:090.0057 1
2,2-Dichloropropane ND mg/kg 08/19/19 17:31 594-20-708/19/19 14:090.0057 1
1,1-Dichloropropene ND mg/kg 08/19/19 17:31 563-58-608/19/19 14:090.0057 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 17:31 10061-01-508/19/19 14:090.0057 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 17:31 10061-02-608/19/19 14:090.0057 1
Diisopropyl ether ND mg/kg 08/19/19 17:31 108-20-308/19/19 14:090.0057 1
Ethylbenzene ND mg/kg 08/19/19 17:31 100-41-408/19/19 14:090.0057 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 17:31 87-68-308/19/19 14:090.0057 1
2-Hexanone ND mg/kg 08/19/19 17:31 591-78-608/19/19 14:090.057 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 17:31 98-82-808/19/19 14:090.0057 1
p-Isopropyltoluene ND mg/kg 08/19/19 17:31 99-87-608/19/19 14:090.0057 1
Methylene Chloride ND mg/kg 08/19/19 17:31 75-09-208/19/19 14:090.023 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 17:31 108-10-108/19/19 14:090.057 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 17:31 1634-04-408/19/19 14:090.0057 1
Naphthalene ND mg/kg 08/19/19 17:31 91-20-308/19/19 14:090.0057 1
n-Propylbenzene ND mg/kg 08/19/19 17:31 103-65-108/19/19 14:090.0057 1
Styrene ND mg/kg 08/19/19 17:31 100-42-508/19/19 14:090.0057 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 17:31 630-20-608/19/19 14:090.0057 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 17:31 79-34-508/19/19 14:090.0057 1
Tetrachloroethene ND mg/kg 08/19/19 17:31 127-18-408/19/19 14:090.0057 1
Toluene ND mg/kg 08/19/19 17:31 108-88-308/19/19 14:090.0057 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 17:31 87-61-608/19/19 14:090.0057 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 17:31 120-82-108/19/19 14:090.0057 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 17:31 71-55-608/19/19 14:090.0057 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 17:31 79-00-508/19/19 14:090.0057 1
Trichloroethene ND mg/kg 08/19/19 17:31 79-01-608/19/19 14:090.0057 1
Trichlorofluoromethane ND mg/kg 08/19/19 17:31 75-69-408/19/19 14:090.0057 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 17:31 96-18-408/19/19 14:090.0057 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 17:31 95-63-608/19/19 14:090.0057 1
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 17:31 108-67-808/19/19 14:090.0057 1
Vinyl acetate ND mg/kg 08/19/19 17:31 108-05-408/19/19 14:090.057 1
Vinyl chloride ND mg/kg 08/19/19 17:31 75-01-408/19/19 14:090.011 1
Xylene (Total)ND mg/kg 08/19/19 17:31 1330-20-708/19/19 14:090.011 1
m&p-Xylene ND mg/kg 08/19/19 17:31 179601-23-108/19/19 14:090.011 1
o-Xylene ND mg/kg 08/19/19 17:31 95-47-608/19/19 14:090.0057 1
Surrogates
Toluene-d8 (S)104 %08/19/19 17:31 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)102 %08/19/19 17:31 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)94 %08/19/19 17:31 17060-07-008/19/19 14:0970-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:DUP-3 Lab ID:92441608003 Collected:08/14/19 10:22 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 31.0 %08/16/19 17:050.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 65.3 %08/29/19 16:5808/29/19 16:491
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 08/30/19 16:43 18540-29-908/30/19 09:441.53 1
Sample:GP-1 0-2'Lab ID:92441608004 Collected:08/14/19 10:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic ND mg/kg 08/23/19 09:38 7440-38-208/21/19 14:113.8 50
Barium 80.6 mg/kg 08/23/19 09:38 7440-39-308/21/19 14:113.8 50
Cadmium ND mg/kg 08/23/19 09:38 7440-43-908/21/19 14:110.45 50
Chromium 71.6 mg/kg 08/23/19 09:38 7440-47-308/21/19 14:113.8 50
Lead 27.9 mg/kg 08/23/19 09:38 7439-92-108/21/19 14:113.8 50
Selenium ND mg/kg 08/23/19 09:38 7782-49-208/21/19 14:113.8 50
Silver ND mg/kg 08/23/19 09:38 7440-22-4 N208/21/19 14:110.45 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.12 mg/kg 08/21/19 16:16 7439-97-608/21/19 10:350.019 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 19:22 83-32-908/17/19 15:342.0 5
Acenaphthylene ND mg/kg 08/20/19 19:22 208-96-808/17/19 15:342.0 5
Aniline ND mg/kg 08/20/19 19:22 62-53-308/17/19 15:342.0 5
Anthracene ND mg/kg 08/20/19 19:22 120-12-708/17/19 15:342.0 5
Benzo(a)anthracene ND mg/kg 08/20/19 19:22 56-55-308/17/19 15:342.0 5
Benzo(a)pyrene ND mg/kg 08/20/19 19:22 50-32-808/17/19 15:342.0 5
Benzo(b)fluoranthene ND mg/kg 08/20/19 19:22 205-99-208/17/19 15:342.0 5
Benzo(g,h,i)perylene ND mg/kg 08/20/19 19:22 191-24-208/17/19 15:342.0 5
Benzo(k)fluoranthene ND mg/kg 08/20/19 19:22 207-08-908/17/19 15:342.0 5
Benzoic Acid ND mg/kg 08/20/19 19:22 65-85-008/17/19 15:3410.2 5
Benzyl alcohol ND mg/kg 08/20/19 19:22 100-51-608/17/19 15:344.1 5
4-Bromophenylphenyl ether ND mg/kg 08/20/19 19:22 101-55-308/17/19 15:342.0 5
Butylbenzylphthalate ND mg/kg 08/20/19 19:22 85-68-708/17/19 15:342.0 5
4-Chloro-3-methylphenol ND mg/kg 08/20/19 19:22 59-50-708/17/19 15:344.1 5
4-Chloroaniline ND mg/kg 08/20/19 19:22 106-47-808/17/19 15:3410.2 5
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 19:22 111-91-108/17/19 15:342.0 5
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 19:22 111-44-408/17/19 15:342.0 5
2-Chloronaphthalene ND mg/kg 08/20/19 19:22 91-58-708/17/19 15:342.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-1 0-2'Lab ID:92441608004 Collected:08/14/19 10:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2-Chlorophenol ND mg/kg 08/20/19 19:22 95-57-808/17/19 15:342.0 5
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 19:22 7005-72-308/17/19 15:342.0 5
Chrysene ND mg/kg 08/20/19 19:22 218-01-908/17/19 15:342.0 5
Dibenz(a,h)anthracene ND mg/kg 08/20/19 19:22 53-70-308/17/19 15:342.0 5
Dibenzofuran ND mg/kg 08/20/19 19:22 132-64-908/17/19 15:342.0 5
1,2-Dichlorobenzene ND mg/kg 08/20/19 19:22 95-50-108/17/19 15:342.0 5
1,3-Dichlorobenzene ND mg/kg 08/20/19 19:22 541-73-108/17/19 15:342.0 5
1,4-Dichlorobenzene ND mg/kg 08/20/19 19:22 106-46-708/17/19 15:342.0 5
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 19:22 91-94-108/17/19 15:3410.2 5
2,4-Dichlorophenol ND mg/kg 08/20/19 19:22 120-83-208/17/19 15:342.0 5
Diethylphthalate ND mg/kg 08/20/19 19:22 84-66-208/17/19 15:342.0 5
2,4-Dimethylphenol ND mg/kg 08/20/19 19:22 105-67-908/17/19 15:342.0 5
Dimethylphthalate ND mg/kg 08/20/19 19:22 131-11-308/17/19 15:342.0 5
Di-n-butylphthalate ND mg/kg 08/20/19 19:22 84-74-208/17/19 15:342.0 5
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 19:22 534-52-108/17/19 15:344.1 5
2,4-Dinitrophenol ND mg/kg 08/20/19 19:22 51-28-508/17/19 15:3410.2 5
2,4-Dinitrotoluene ND mg/kg 08/20/19 19:22 121-14-208/17/19 15:342.0 5
2,6-Dinitrotoluene ND mg/kg 08/20/19 19:22 606-20-208/17/19 15:342.0 5
Di-n-octylphthalate ND mg/kg 08/20/19 19:22 117-84-008/17/19 15:342.0 5
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 19:22 117-81-708/17/19 15:342.0 5
Fluoranthene ND mg/kg 08/20/19 19:22 206-44-008/17/19 15:342.0 5
Fluorene ND mg/kg 08/20/19 19:22 86-73-708/17/19 15:342.0 5
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 19:22 87-68-308/17/19 15:342.0 5
Hexachlorobenzene ND mg/kg 08/20/19 19:22 118-74-108/17/19 15:342.0 5
Hexachlorocyclopentadiene ND mg/kg 08/20/19 19:22 77-47-408/17/19 15:342.0 5
Hexachloroethane ND mg/kg 08/20/19 19:22 67-72-108/17/19 15:342.0 5
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 19:22 193-39-508/17/19 15:342.0 5
Isophorone ND mg/kg 08/20/19 19:22 78-59-108/17/19 15:342.0 5
1-Methylnaphthalene ND mg/kg 08/20/19 19:22 90-12-008/17/19 15:342.0 5
2-Methylnaphthalene ND mg/kg 08/20/19 19:22 91-57-608/17/19 15:342.0 5
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 19:22 95-48-708/17/19 15:342.0 5
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 19:22 15831-10-408/17/19 15:342.0 5
Naphthalene ND mg/kg 08/20/19 19:22 91-20-308/17/19 15:342.0 5
2-Nitroaniline ND mg/kg 08/20/19 19:22 88-74-408/17/19 15:3410.2 5
3-Nitroaniline ND mg/kg 08/20/19 19:22 99-09-208/17/19 15:3410.2 5
4-Nitroaniline ND mg/kg 08/20/19 19:22 100-01-608/17/19 15:344.1 5
Nitrobenzene ND mg/kg 08/20/19 19:22 98-95-308/17/19 15:342.0 5
2-Nitrophenol ND mg/kg 08/20/19 19:22 88-75-508/17/19 15:342.0 5
4-Nitrophenol ND mg/kg 08/20/19 19:22 100-02-708/17/19 15:3410.2 5
N-Nitrosodimethylamine ND mg/kg 08/20/19 19:22 62-75-908/17/19 15:342.0 5
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 19:22 621-64-708/17/19 15:342.0 5
N-Nitrosodiphenylamine ND mg/kg 08/20/19 19:22 86-30-608/17/19 15:342.0 5
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 19:22 108-60-108/17/19 15:342.0 5
Pentachlorophenol ND mg/kg 08/20/19 19:22 87-86-508/17/19 15:3410.2 5
Phenanthrene ND mg/kg 08/20/19 19:22 85-01-808/17/19 15:342.0 5
Phenol ND mg/kg 08/20/19 19:22 108-95-208/17/19 15:342.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-1 0-2'Lab ID:92441608004 Collected:08/14/19 10:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Pyrene ND mg/kg 08/20/19 19:22 129-00-008/17/19 15:342.0 5
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 19:22 120-82-108/17/19 15:342.0 5
2,4,5-Trichlorophenol ND mg/kg 08/20/19 19:22 95-95-408/17/19 15:342.0 5
2,4,6-Trichlorophenol ND mg/kg 08/20/19 19:22 88-06-208/17/19 15:342.0 5
Surrogates
Nitrobenzene-d5 (S)58 %08/20/19 19:22 4165-60-0 D308/17/19 15:3423-110 5
2-Fluorobiphenyl (S)65 %08/20/19 19:22 321-60-808/17/19 15:3430-110 5
Terphenyl-d14 (S)71 %08/20/19 19:22 1718-51-008/17/19 15:3428-110 5
Phenol-d6 (S)43 %08/20/19 19:22 13127-88-308/17/19 15:3422-110 5
2-Fluorophenol (S)15 %08/20/19 19:22 367-12-408/17/19 15:3413-110 5
2,4,6-Tribromophenol (S)10 %08/20/19 19:22 118-79-6 S008/17/19 15:3427-110 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 17:56 67-64-108/19/19 14:090.093 1
Benzene ND mg/kg 08/19/19 17:56 71-43-208/19/19 14:090.0047 1
Bromobenzene ND mg/kg 08/19/19 17:56 108-86-108/19/19 14:090.0047 1
Bromochloromethane ND mg/kg 08/19/19 17:56 74-97-508/19/19 14:090.0047 1
Bromodichloromethane ND mg/kg 08/19/19 17:56 75-27-408/19/19 14:090.0047 1
Bromoform ND mg/kg 08/19/19 17:56 75-25-208/19/19 14:090.0047 1
Bromomethane ND mg/kg 08/19/19 17:56 74-83-908/19/19 14:090.0093 1
2-Butanone (MEK)ND mg/kg 08/19/19 17:56 78-93-308/19/19 14:090.093 1
n-Butylbenzene ND mg/kg 08/19/19 17:56 104-51-808/19/19 14:090.0047 1
sec-Butylbenzene ND mg/kg 08/19/19 17:56 135-98-808/19/19 14:090.0047 1
tert-Butylbenzene ND mg/kg 08/19/19 17:56 98-06-608/19/19 14:090.0047 1
Carbon tetrachloride ND mg/kg 08/19/19 17:56 56-23-508/19/19 14:090.0047 1
Chlorobenzene ND mg/kg 08/19/19 17:56 108-90-708/19/19 14:090.0047 1
Chloroethane ND mg/kg 08/19/19 17:56 75-00-308/19/19 14:090.0093 1
Chloroform ND mg/kg 08/19/19 17:56 67-66-308/19/19 14:090.0047 1
Chloromethane ND mg/kg 08/19/19 17:56 74-87-308/19/19 14:090.0093 1
2-Chlorotoluene ND mg/kg 08/19/19 17:56 95-49-808/19/19 14:090.0047 1
4-Chlorotoluene ND mg/kg 08/19/19 17:56 106-43-408/19/19 14:090.0047 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 17:56 96-12-808/19/19 14:090.0047 1
Dibromochloromethane ND mg/kg 08/19/19 17:56 124-48-108/19/19 14:090.0047 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 17:56 106-93-408/19/19 14:090.0047 1
Dibromomethane ND mg/kg 08/19/19 17:56 74-95-308/19/19 14:090.0047 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 17:56 95-50-108/19/19 14:090.0047 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 17:56 541-73-108/19/19 14:090.0047 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 17:56 106-46-708/19/19 14:090.0047 1
Dichlorodifluoromethane ND mg/kg 08/19/19 17:56 75-71-808/19/19 14:090.0093 1
1,1-Dichloroethane ND mg/kg 08/19/19 17:56 75-34-308/19/19 14:090.0047 1
1,2-Dichloroethane ND mg/kg 08/19/19 17:56 107-06-208/19/19 14:090.0047 1
1,1-Dichloroethene ND mg/kg 08/19/19 17:56 75-35-408/19/19 14:090.0047 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 17:56 156-59-208/19/19 14:090.0047 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 17:56 156-60-508/19/19 14:090.0047 1
1,2-Dichloropropane ND mg/kg 08/19/19 17:56 78-87-508/19/19 14:090.0047 1
1,3-Dichloropropane ND mg/kg 08/19/19 17:56 142-28-908/19/19 14:090.0047 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-1 0-2'Lab ID:92441608004 Collected:08/14/19 10:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
2,2-Dichloropropane ND mg/kg 08/19/19 17:56 594-20-708/19/19 14:090.0047 1
1,1-Dichloropropene ND mg/kg 08/19/19 17:56 563-58-608/19/19 14:090.0047 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 17:56 10061-01-508/19/19 14:090.0047 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 17:56 10061-02-608/19/19 14:090.0047 1
Diisopropyl ether ND mg/kg 08/19/19 17:56 108-20-308/19/19 14:090.0047 1
Ethylbenzene ND mg/kg 08/19/19 17:56 100-41-408/19/19 14:090.0047 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 17:56 87-68-308/19/19 14:090.0047 1
2-Hexanone ND mg/kg 08/19/19 17:56 591-78-608/19/19 14:090.047 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 17:56 98-82-808/19/19 14:090.0047 1
p-Isopropyltoluene ND mg/kg 08/19/19 17:56 99-87-608/19/19 14:090.0047 1
Methylene Chloride ND mg/kg 08/19/19 17:56 75-09-208/19/19 14:090.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 17:56 108-10-108/19/19 14:090.047 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 17:56 1634-04-408/19/19 14:090.0047 1
Naphthalene ND mg/kg 08/19/19 17:56 91-20-308/19/19 14:090.0047 1
n-Propylbenzene ND mg/kg 08/19/19 17:56 103-65-108/19/19 14:090.0047 1
Styrene ND mg/kg 08/19/19 17:56 100-42-508/19/19 14:090.0047 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 17:56 630-20-608/19/19 14:090.0047 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 17:56 79-34-508/19/19 14:090.0047 1
Tetrachloroethene ND mg/kg 08/19/19 17:56 127-18-408/19/19 14:090.0047 1
Toluene ND mg/kg 08/19/19 17:56 108-88-308/19/19 14:090.0047 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 17:56 87-61-608/19/19 14:090.0047 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 17:56 120-82-108/19/19 14:090.0047 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 17:56 71-55-608/19/19 14:090.0047 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 17:56 79-00-508/19/19 14:090.0047 1
Trichloroethene ND mg/kg 08/19/19 17:56 79-01-608/19/19 14:090.0047 1
Trichlorofluoromethane ND mg/kg 08/19/19 17:56 75-69-408/19/19 14:090.0047 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 17:56 96-18-408/19/19 14:090.0047 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 17:56 95-63-608/19/19 14:090.0047 1
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 17:56 108-67-808/19/19 14:090.0047 1
Vinyl acetate ND mg/kg 08/19/19 17:56 108-05-408/19/19 14:090.047 1
Vinyl chloride ND mg/kg 08/19/19 17:56 75-01-408/19/19 14:090.0093 1
Xylene (Total)ND mg/kg 08/19/19 17:56 1330-20-708/19/19 14:090.0093 1
m&p-Xylene ND mg/kg 08/19/19 17:56 179601-23-108/19/19 14:090.0093 1
o-Xylene ND mg/kg 08/19/19 17:56 95-47-608/19/19 14:090.0047 1
Surrogates
Toluene-d8 (S)107 %08/19/19 17:56 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)100 %08/19/19 17:56 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)87 %08/19/19 17:56 17060-07-008/19/19 14:0970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.5 %08/16/19 17:050.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-1 2-4'Lab ID:92441608005 Collected:08/14/19 11:00 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic ND mg/kg 08/23/19 09:41 7440-38-208/21/19 14:114.1 50
Barium 108 mg/kg 08/23/19 09:41 7440-39-308/21/19 14:114.1 50
Cadmium ND mg/kg 08/23/19 09:41 7440-43-908/21/19 14:110.49 50
Chromium 80.2 mg/kg 08/23/19 09:41 7440-47-308/21/19 14:114.1 50
Lead 33.7 mg/kg 08/23/19 09:41 7439-92-108/21/19 14:114.1 50
Selenium ND mg/kg 08/23/19 09:41 7782-49-208/21/19 14:114.1 50
Silver ND mg/kg 08/23/19 09:41 7440-22-4 N208/21/19 14:110.49 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.037 mg/kg 08/21/19 16:18 7439-97-608/21/19 10:350.021 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 13:08 83-32-908/17/19 15:340.45 1
Acenaphthylene ND mg/kg 08/20/19 13:08 208-96-808/17/19 15:340.45 1
Aniline ND mg/kg 08/20/19 13:08 62-53-308/17/19 15:340.45 1
Anthracene ND mg/kg 08/20/19 13:08 120-12-708/17/19 15:340.45 1
Benzo(a)anthracene ND mg/kg 08/20/19 13:08 56-55-308/17/19 15:340.45 1
Benzo(a)pyrene ND mg/kg 08/20/19 13:08 50-32-808/17/19 15:340.45 1
Benzo(b)fluoranthene ND mg/kg 08/20/19 13:08 205-99-208/17/19 15:340.45 1
Benzo(g,h,i)perylene ND mg/kg 08/20/19 13:08 191-24-208/17/19 15:340.45 1
Benzo(k)fluoranthene ND mg/kg 08/20/19 13:08 207-08-908/17/19 15:340.45 1
Benzoic Acid ND mg/kg 08/20/19 13:08 65-85-008/17/19 15:342.3 1
Benzyl alcohol ND mg/kg 08/20/19 13:08 100-51-608/17/19 15:340.90 1
4-Bromophenylphenyl ether ND mg/kg 08/20/19 13:08 101-55-308/17/19 15:340.45 1
Butylbenzylphthalate ND mg/kg 08/20/19 13:08 85-68-708/17/19 15:340.45 1
4-Chloro-3-methylphenol ND mg/kg 08/20/19 13:08 59-50-708/17/19 15:340.90 1
4-Chloroaniline ND mg/kg 08/20/19 13:08 106-47-808/17/19 15:342.3 1
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 13:08 111-91-108/17/19 15:340.45 1
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 13:08 111-44-408/17/19 15:340.45 1
2-Chloronaphthalene ND mg/kg 08/20/19 13:08 91-58-708/17/19 15:340.45 1
2-Chlorophenol ND mg/kg 08/20/19 13:08 95-57-808/17/19 15:340.45 1
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 13:08 7005-72-308/17/19 15:340.45 1
Chrysene ND mg/kg 08/20/19 13:08 218-01-908/17/19 15:340.45 1
Dibenz(a,h)anthracene ND mg/kg 08/20/19 13:08 53-70-308/17/19 15:340.45 1
Dibenzofuran ND mg/kg 08/20/19 13:08 132-64-908/17/19 15:340.45 1
1,2-Dichlorobenzene ND mg/kg 08/20/19 13:08 95-50-108/17/19 15:340.45 1
1,3-Dichlorobenzene ND mg/kg 08/20/19 13:08 541-73-108/17/19 15:340.45 1
1,4-Dichlorobenzene ND mg/kg 08/20/19 13:08 106-46-708/17/19 15:340.45 1
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 13:08 91-94-108/17/19 15:342.3 1
2,4-Dichlorophenol ND mg/kg 08/20/19 13:08 120-83-208/17/19 15:340.45 1
Diethylphthalate ND mg/kg 08/20/19 13:08 84-66-208/17/19 15:340.45 1
2,4-Dimethylphenol ND mg/kg 08/20/19 13:08 105-67-908/17/19 15:340.45 1
Dimethylphthalate ND mg/kg 08/20/19 13:08 131-11-308/17/19 15:340.45 1
Di-n-butylphthalate ND mg/kg 08/20/19 13:08 84-74-208/17/19 15:340.45 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 13:08 534-52-108/17/19 15:340.90 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-1 2-4'Lab ID:92441608005 Collected:08/14/19 11:00 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND mg/kg 08/20/19 13:08 51-28-508/17/19 15:342.3 1
2,4-Dinitrotoluene ND mg/kg 08/20/19 13:08 121-14-208/17/19 15:340.45 1
2,6-Dinitrotoluene ND mg/kg 08/20/19 13:08 606-20-208/17/19 15:340.45 1
Di-n-octylphthalate ND mg/kg 08/20/19 13:08 117-84-008/17/19 15:340.45 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 13:08 117-81-708/17/19 15:340.45 1
Fluoranthene ND mg/kg 08/20/19 13:08 206-44-008/17/19 15:340.45 1
Fluorene ND mg/kg 08/20/19 13:08 86-73-708/17/19 15:340.45 1
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 13:08 87-68-308/17/19 15:340.45 1
Hexachlorobenzene ND mg/kg 08/20/19 13:08 118-74-108/17/19 15:340.45 1
Hexachlorocyclopentadiene ND mg/kg 08/20/19 13:08 77-47-408/17/19 15:340.45 1
Hexachloroethane ND mg/kg 08/20/19 13:08 67-72-108/17/19 15:340.45 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 13:08 193-39-508/17/19 15:340.45 1
Isophorone ND mg/kg 08/20/19 13:08 78-59-108/17/19 15:340.45 1
1-Methylnaphthalene ND mg/kg 08/20/19 13:08 90-12-008/17/19 15:340.45 1
2-Methylnaphthalene ND mg/kg 08/20/19 13:08 91-57-608/17/19 15:340.45 1
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 13:08 95-48-708/17/19 15:340.45 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 13:08 15831-10-408/17/19 15:340.45 1
Naphthalene ND mg/kg 08/20/19 13:08 91-20-308/17/19 15:340.45 1
2-Nitroaniline ND mg/kg 08/20/19 13:08 88-74-408/17/19 15:342.3 1
3-Nitroaniline ND mg/kg 08/20/19 13:08 99-09-208/17/19 15:342.3 1
4-Nitroaniline ND mg/kg 08/20/19 13:08 100-01-608/17/19 15:340.90 1
Nitrobenzene ND mg/kg 08/20/19 13:08 98-95-308/17/19 15:340.45 1
2-Nitrophenol ND mg/kg 08/20/19 13:08 88-75-508/17/19 15:340.45 1
4-Nitrophenol ND mg/kg 08/20/19 13:08 100-02-7 v208/17/19 15:342.3 1
N-Nitrosodimethylamine ND mg/kg 08/20/19 13:08 62-75-9 v108/17/19 15:340.45 1
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 13:08 621-64-708/17/19 15:340.45 1
N-Nitrosodiphenylamine ND mg/kg 08/20/19 13:08 86-30-608/17/19 15:340.45 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 13:08 108-60-108/17/19 15:340.45 1
Pentachlorophenol ND mg/kg 08/20/19 13:08 87-86-508/17/19 15:342.3 1
Phenanthrene ND mg/kg 08/20/19 13:08 85-01-808/17/19 15:340.45 1
Phenol ND mg/kg 08/20/19 13:08 108-95-208/17/19 15:340.45 1
Pyrene 0.50 mg/kg 08/20/19 13:08 129-00-008/17/19 15:340.45 1
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 13:08 120-82-108/17/19 15:340.45 1
2,4,5-Trichlorophenol ND mg/kg 08/20/19 13:08 95-95-408/17/19 15:340.45 1
2,4,6-Trichlorophenol ND mg/kg 08/20/19 13:08 88-06-208/17/19 15:340.45 1
Surrogates
Nitrobenzene-d5 (S)61 %08/20/19 13:08 4165-60-008/17/19 15:3423-110 1
2-Fluorobiphenyl (S)68 %08/20/19 13:08 321-60-808/17/19 15:3430-110 1
Terphenyl-d14 (S)96 %08/20/19 13:08 1718-51-008/17/19 15:3428-110 1
Phenol-d6 (S)64 %08/20/19 13:08 13127-88-308/17/19 15:3422-110 1
2-Fluorophenol (S)63 %08/20/19 13:08 367-12-408/17/19 15:3413-110 1
2,4,6-Tribromophenol (S)89 %08/20/19 13:08 118-79-608/17/19 15:3427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 18:21 67-64-108/19/19 14:090.11 1
Benzene ND mg/kg 08/19/19 18:21 71-43-208/19/19 14:090.0053 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-1 2-4'Lab ID:92441608005 Collected:08/14/19 11:00 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Bromobenzene ND mg/kg 08/19/19 18:21 108-86-108/19/19 14:090.0053 1
Bromochloromethane ND mg/kg 08/19/19 18:21 74-97-508/19/19 14:090.0053 1
Bromodichloromethane ND mg/kg 08/19/19 18:21 75-27-408/19/19 14:090.0053 1
Bromoform ND mg/kg 08/19/19 18:21 75-25-208/19/19 14:090.0053 1
Bromomethane ND mg/kg 08/19/19 18:21 74-83-908/19/19 14:090.011 1
2-Butanone (MEK)ND mg/kg 08/19/19 18:21 78-93-308/19/19 14:090.11 1
n-Butylbenzene ND mg/kg 08/19/19 18:21 104-51-808/19/19 14:090.0053 1
sec-Butylbenzene ND mg/kg 08/19/19 18:21 135-98-808/19/19 14:090.0053 1
tert-Butylbenzene ND mg/kg 08/19/19 18:21 98-06-608/19/19 14:090.0053 1
Carbon tetrachloride ND mg/kg 08/19/19 18:21 56-23-508/19/19 14:090.0053 1
Chlorobenzene ND mg/kg 08/19/19 18:21 108-90-708/19/19 14:090.0053 1
Chloroethane ND mg/kg 08/19/19 18:21 75-00-308/19/19 14:090.011 1
Chloroform ND mg/kg 08/19/19 18:21 67-66-308/19/19 14:090.0053 1
Chloromethane ND mg/kg 08/19/19 18:21 74-87-308/19/19 14:090.011 1
2-Chlorotoluene ND mg/kg 08/19/19 18:21 95-49-808/19/19 14:090.0053 1
4-Chlorotoluene ND mg/kg 08/19/19 18:21 106-43-408/19/19 14:090.0053 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 18:21 96-12-808/19/19 14:090.0053 1
Dibromochloromethane ND mg/kg 08/19/19 18:21 124-48-108/19/19 14:090.0053 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 18:21 106-93-408/19/19 14:090.0053 1
Dibromomethane ND mg/kg 08/19/19 18:21 74-95-308/19/19 14:090.0053 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 18:21 95-50-108/19/19 14:090.0053 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 18:21 541-73-108/19/19 14:090.0053 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 18:21 106-46-708/19/19 14:090.0053 1
Dichlorodifluoromethane ND mg/kg 08/19/19 18:21 75-71-808/19/19 14:090.011 1
1,1-Dichloroethane ND mg/kg 08/19/19 18:21 75-34-308/19/19 14:090.0053 1
1,2-Dichloroethane ND mg/kg 08/19/19 18:21 107-06-208/19/19 14:090.0053 1
1,1-Dichloroethene ND mg/kg 08/19/19 18:21 75-35-408/19/19 14:090.0053 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 18:21 156-59-208/19/19 14:090.0053 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 18:21 156-60-508/19/19 14:090.0053 1
1,2-Dichloropropane ND mg/kg 08/19/19 18:21 78-87-508/19/19 14:090.0053 1
1,3-Dichloropropane ND mg/kg 08/19/19 18:21 142-28-908/19/19 14:090.0053 1
2,2-Dichloropropane ND mg/kg 08/19/19 18:21 594-20-708/19/19 14:090.0053 1
1,1-Dichloropropene ND mg/kg 08/19/19 18:21 563-58-608/19/19 14:090.0053 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 18:21 10061-01-508/19/19 14:090.0053 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 18:21 10061-02-608/19/19 14:090.0053 1
Diisopropyl ether ND mg/kg 08/19/19 18:21 108-20-308/19/19 14:090.0053 1
Ethylbenzene ND mg/kg 08/19/19 18:21 100-41-408/19/19 14:090.0053 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 18:21 87-68-308/19/19 14:090.0053 1
2-Hexanone ND mg/kg 08/19/19 18:21 591-78-608/19/19 14:090.053 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 18:21 98-82-808/19/19 14:090.0053 1
p-Isopropyltoluene ND mg/kg 08/19/19 18:21 99-87-608/19/19 14:090.0053 1
Methylene Chloride ND mg/kg 08/19/19 18:21 75-09-208/19/19 14:090.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 18:21 108-10-108/19/19 14:090.053 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 18:21 1634-04-408/19/19 14:090.0053 1
Naphthalene ND mg/kg 08/19/19 18:21 91-20-308/19/19 14:090.0053 1
n-Propylbenzene ND mg/kg 08/19/19 18:21 103-65-108/19/19 14:090.0053 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-1 2-4'Lab ID:92441608005 Collected:08/14/19 11:00 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Styrene ND mg/kg 08/19/19 18:21 100-42-508/19/19 14:090.0053 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 18:21 630-20-608/19/19 14:090.0053 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 18:21 79-34-508/19/19 14:090.0053 1
Tetrachloroethene ND mg/kg 08/19/19 18:21 127-18-408/19/19 14:090.0053 1
Toluene ND mg/kg 08/19/19 18:21 108-88-308/19/19 14:090.0053 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 18:21 87-61-608/19/19 14:090.0053 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 18:21 120-82-108/19/19 14:090.0053 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 18:21 71-55-608/19/19 14:090.0053 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 18:21 79-00-508/19/19 14:090.0053 1
Trichloroethene ND mg/kg 08/19/19 18:21 79-01-608/19/19 14:090.0053 1
Trichlorofluoromethane ND mg/kg 08/19/19 18:21 75-69-408/19/19 14:090.0053 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 18:21 96-18-408/19/19 14:090.0053 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 18:21 95-63-608/19/19 14:090.0053 1
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 18:21 108-67-808/19/19 14:090.0053 1
Vinyl acetate ND mg/kg 08/19/19 18:21 108-05-408/19/19 14:090.053 1
Vinyl chloride ND mg/kg 08/19/19 18:21 75-01-408/19/19 14:090.011 1
Xylene (Total)ND mg/kg 08/19/19 18:21 1330-20-708/19/19 14:090.011 1
m&p-Xylene ND mg/kg 08/19/19 18:21 179601-23-108/19/19 14:090.011 1
o-Xylene ND mg/kg 08/19/19 18:21 95-47-608/19/19 14:090.0053 1
Surrogates
Toluene-d8 (S)107 %08/19/19 18:21 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)103 %08/19/19 18:21 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)81 %08/19/19 18:21 17060-07-008/19/19 14:0970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.4 %08/16/19 17:050.10 1
Sample:GP-2 0-2'Lab ID:92441608006 Collected:08/14/19 12:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic ND mg/kg 08/23/19 09:43 7440-38-208/21/19 14:113.4 50
Barium 104 mg/kg 08/23/19 09:43 7440-39-308/21/19 14:113.4 50
Cadmium ND mg/kg 08/23/19 09:43 7440-43-908/21/19 14:110.41 50
Chromium 41.6 mg/kg 08/23/19 09:43 7440-47-308/21/19 14:113.4 50
Lead 10.6 mg/kg 08/23/19 09:43 7439-92-108/21/19 14:113.4 50
Selenium ND mg/kg 08/23/19 09:43 7782-49-208/21/19 14:113.4 50
Silver ND mg/kg 08/23/19 09:43 7440-22-4 N208/21/19 14:110.41 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.044 mg/kg 08/21/19 16:20 7439-97-608/21/19 10:350.018 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-2 0-2'Lab ID:92441608006 Collected:08/14/19 12:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 19:55 83-32-908/17/19 15:341.9 5
Acenaphthylene ND mg/kg 08/20/19 19:55 208-96-808/17/19 15:341.9 5
Aniline ND mg/kg 08/20/19 19:55 62-53-308/17/19 15:341.9 5
Anthracene ND mg/kg 08/20/19 19:55 120-12-708/17/19 15:341.9 5
Benzo(a)anthracene ND mg/kg 08/20/19 19:55 56-55-308/17/19 15:341.9 5
Benzo(a)pyrene ND mg/kg 08/20/19 19:55 50-32-808/17/19 15:341.9 5
Benzo(b)fluoranthene ND mg/kg 08/20/19 19:55 205-99-208/17/19 15:341.9 5
Benzo(g,h,i)perylene ND mg/kg 08/20/19 19:55 191-24-208/17/19 15:341.9 5
Benzo(k)fluoranthene ND mg/kg 08/20/19 19:55 207-08-908/17/19 15:341.9 5
Benzoic Acid ND mg/kg 08/20/19 19:55 65-85-008/17/19 15:349.5 5
Benzyl alcohol ND mg/kg 08/20/19 19:55 100-51-608/17/19 15:343.8 5
4-Bromophenylphenyl ether ND mg/kg 08/20/19 19:55 101-55-308/17/19 15:341.9 5
Butylbenzylphthalate ND mg/kg 08/20/19 19:55 85-68-708/17/19 15:341.9 5
4-Chloro-3-methylphenol ND mg/kg 08/20/19 19:55 59-50-708/17/19 15:343.8 5
4-Chloroaniline ND mg/kg 08/20/19 19:55 106-47-808/17/19 15:349.5 5
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 19:55 111-91-108/17/19 15:341.9 5
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 19:55 111-44-408/17/19 15:341.9 5
2-Chloronaphthalene ND mg/kg 08/20/19 19:55 91-58-708/17/19 15:341.9 5
2-Chlorophenol ND mg/kg 08/20/19 19:55 95-57-808/17/19 15:341.9 5
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 19:55 7005-72-308/17/19 15:341.9 5
Chrysene ND mg/kg 08/20/19 19:55 218-01-908/17/19 15:341.9 5
Dibenz(a,h)anthracene ND mg/kg 08/20/19 19:55 53-70-308/17/19 15:341.9 5
Dibenzofuran ND mg/kg 08/20/19 19:55 132-64-908/17/19 15:341.9 5
1,2-Dichlorobenzene ND mg/kg 08/20/19 19:55 95-50-108/17/19 15:341.9 5
1,3-Dichlorobenzene ND mg/kg 08/20/19 19:55 541-73-108/17/19 15:341.9 5
1,4-Dichlorobenzene ND mg/kg 08/20/19 19:55 106-46-708/17/19 15:341.9 5
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 19:55 91-94-108/17/19 15:349.5 5
2,4-Dichlorophenol ND mg/kg 08/20/19 19:55 120-83-208/17/19 15:341.9 5
Diethylphthalate ND mg/kg 08/20/19 19:55 84-66-208/17/19 15:341.9 5
2,4-Dimethylphenol ND mg/kg 08/20/19 19:55 105-67-908/17/19 15:341.9 5
Dimethylphthalate ND mg/kg 08/20/19 19:55 131-11-308/17/19 15:341.9 5
Di-n-butylphthalate ND mg/kg 08/20/19 19:55 84-74-208/17/19 15:341.9 5
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 19:55 534-52-108/17/19 15:343.8 5
2,4-Dinitrophenol ND mg/kg 08/20/19 19:55 51-28-508/17/19 15:349.5 5
2,4-Dinitrotoluene ND mg/kg 08/20/19 19:55 121-14-208/17/19 15:341.9 5
2,6-Dinitrotoluene ND mg/kg 08/20/19 19:55 606-20-208/17/19 15:341.9 5
Di-n-octylphthalate ND mg/kg 08/20/19 19:55 117-84-008/17/19 15:341.9 5
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 19:55 117-81-708/17/19 15:341.9 5
Fluoranthene ND mg/kg 08/20/19 19:55 206-44-008/17/19 15:341.9 5
Fluorene ND mg/kg 08/20/19 19:55 86-73-708/17/19 15:341.9 5
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 19:55 87-68-308/17/19 15:341.9 5
Hexachlorobenzene ND mg/kg 08/20/19 19:55 118-74-108/17/19 15:341.9 5
Hexachlorocyclopentadiene ND mg/kg 08/20/19 19:55 77-47-408/17/19 15:341.9 5
Hexachloroethane ND mg/kg 08/20/19 19:55 67-72-108/17/19 15:341.9 5
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 19:55 193-39-508/17/19 15:341.9 5
Isophorone ND mg/kg 08/20/19 19:55 78-59-108/17/19 15:341.9 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-2 0-2'Lab ID:92441608006 Collected:08/14/19 12:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
1-Methylnaphthalene ND mg/kg 08/20/19 19:55 90-12-008/17/19 15:341.9 5
2-Methylnaphthalene ND mg/kg 08/20/19 19:55 91-57-608/17/19 15:341.9 5
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 19:55 95-48-708/17/19 15:341.9 5
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 19:55 15831-10-408/17/19 15:341.9 5
Naphthalene ND mg/kg 08/20/19 19:55 91-20-308/17/19 15:341.9 5
2-Nitroaniline ND mg/kg 08/20/19 19:55 88-74-408/17/19 15:349.5 5
3-Nitroaniline ND mg/kg 08/20/19 19:55 99-09-208/17/19 15:349.5 5
4-Nitroaniline ND mg/kg 08/20/19 19:55 100-01-608/17/19 15:343.8 5
Nitrobenzene ND mg/kg 08/20/19 19:55 98-95-308/17/19 15:341.9 5
2-Nitrophenol ND mg/kg 08/20/19 19:55 88-75-508/17/19 15:341.9 5
4-Nitrophenol ND mg/kg 08/20/19 19:55 100-02-708/17/19 15:349.5 5
N-Nitrosodimethylamine ND mg/kg 08/20/19 19:55 62-75-908/17/19 15:341.9 5
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 19:55 621-64-708/17/19 15:341.9 5
N-Nitrosodiphenylamine ND mg/kg 08/20/19 19:55 86-30-608/17/19 15:341.9 5
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 19:55 108-60-108/17/19 15:341.9 5
Pentachlorophenol ND mg/kg 08/20/19 19:55 87-86-508/17/19 15:349.5 5
Phenanthrene ND mg/kg 08/20/19 19:55 85-01-808/17/19 15:341.9 5
Phenol ND mg/kg 08/20/19 19:55 108-95-208/17/19 15:341.9 5
Pyrene ND mg/kg 08/20/19 19:55 129-00-008/17/19 15:341.9 5
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 19:55 120-82-108/17/19 15:341.9 5
2,4,5-Trichlorophenol ND mg/kg 08/20/19 19:55 95-95-408/17/19 15:341.9 5
2,4,6-Trichlorophenol ND mg/kg 08/20/19 19:55 88-06-208/17/19 15:341.9 5
Surrogates
Nitrobenzene-d5 (S)52 %08/20/19 19:55 4165-60-0 D308/17/19 15:3423-110 5
2-Fluorobiphenyl (S)60 %08/20/19 19:55 321-60-808/17/19 15:3430-110 5
Terphenyl-d14 (S)68 %08/20/19 19:55 1718-51-008/17/19 15:3428-110 5
Phenol-d6 (S)52 %08/20/19 19:55 13127-88-308/17/19 15:3422-110 5
2-Fluorophenol (S)50 %08/20/19 19:55 367-12-408/17/19 15:3413-110 5
2,4,6-Tribromophenol (S)69 %08/20/19 19:55 118-79-608/17/19 15:3427-110 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 18:45 67-64-108/19/19 14:090.080 1
Benzene ND mg/kg 08/19/19 18:45 71-43-208/19/19 14:090.0040 1
Bromobenzene ND mg/kg 08/19/19 18:45 108-86-108/19/19 14:090.0040 1
Bromochloromethane ND mg/kg 08/19/19 18:45 74-97-508/19/19 14:090.0040 1
Bromodichloromethane ND mg/kg 08/19/19 18:45 75-27-408/19/19 14:090.0040 1
Bromoform ND mg/kg 08/19/19 18:45 75-25-208/19/19 14:090.0040 1
Bromomethane ND mg/kg 08/19/19 18:45 74-83-908/19/19 14:090.0080 1
2-Butanone (MEK)ND mg/kg 08/19/19 18:45 78-93-308/19/19 14:090.080 1
n-Butylbenzene ND mg/kg 08/19/19 18:45 104-51-808/19/19 14:090.0040 1
sec-Butylbenzene ND mg/kg 08/19/19 18:45 135-98-808/19/19 14:090.0040 1
tert-Butylbenzene ND mg/kg 08/19/19 18:45 98-06-608/19/19 14:090.0040 1
Carbon tetrachloride ND mg/kg 08/19/19 18:45 56-23-508/19/19 14:090.0040 1
Chlorobenzene ND mg/kg 08/19/19 18:45 108-90-708/19/19 14:090.0040 1
Chloroethane ND mg/kg 08/19/19 18:45 75-00-308/19/19 14:090.0080 1
Chloroform ND mg/kg 08/19/19 18:45 67-66-308/19/19 14:090.0040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-2 0-2'Lab ID:92441608006 Collected:08/14/19 12:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Chloromethane ND mg/kg 08/19/19 18:45 74-87-308/19/19 14:090.0080 1
2-Chlorotoluene ND mg/kg 08/19/19 18:45 95-49-808/19/19 14:090.0040 1
4-Chlorotoluene ND mg/kg 08/19/19 18:45 106-43-408/19/19 14:090.0040 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 18:45 96-12-808/19/19 14:090.0040 1
Dibromochloromethane ND mg/kg 08/19/19 18:45 124-48-108/19/19 14:090.0040 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 18:45 106-93-408/19/19 14:090.0040 1
Dibromomethane ND mg/kg 08/19/19 18:45 74-95-308/19/19 14:090.0040 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 18:45 95-50-108/19/19 14:090.0040 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 18:45 541-73-108/19/19 14:090.0040 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 18:45 106-46-708/19/19 14:090.0040 1
Dichlorodifluoromethane ND mg/kg 08/19/19 18:45 75-71-808/19/19 14:090.0080 1
1,1-Dichloroethane ND mg/kg 08/19/19 18:45 75-34-308/19/19 14:090.0040 1
1,2-Dichloroethane ND mg/kg 08/19/19 18:45 107-06-208/19/19 14:090.0040 1
1,1-Dichloroethene ND mg/kg 08/19/19 18:45 75-35-408/19/19 14:090.0040 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 18:45 156-59-208/19/19 14:090.0040 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 18:45 156-60-508/19/19 14:090.0040 1
1,2-Dichloropropane ND mg/kg 08/19/19 18:45 78-87-508/19/19 14:090.0040 1
1,3-Dichloropropane ND mg/kg 08/19/19 18:45 142-28-908/19/19 14:090.0040 1
2,2-Dichloropropane ND mg/kg 08/19/19 18:45 594-20-708/19/19 14:090.0040 1
1,1-Dichloropropene ND mg/kg 08/19/19 18:45 563-58-608/19/19 14:090.0040 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 18:45 10061-01-508/19/19 14:090.0040 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 18:45 10061-02-608/19/19 14:090.0040 1
Diisopropyl ether ND mg/kg 08/19/19 18:45 108-20-308/19/19 14:090.0040 1
Ethylbenzene ND mg/kg 08/19/19 18:45 100-41-408/19/19 14:090.0040 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 18:45 87-68-308/19/19 14:090.0040 1
2-Hexanone ND mg/kg 08/19/19 18:45 591-78-608/19/19 14:090.040 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 18:45 98-82-808/19/19 14:090.0040 1
p-Isopropyltoluene ND mg/kg 08/19/19 18:45 99-87-608/19/19 14:090.0040 1
Methylene Chloride ND mg/kg 08/19/19 18:45 75-09-208/19/19 14:090.016 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 18:45 108-10-108/19/19 14:090.040 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 18:45 1634-04-408/19/19 14:090.0040 1
Naphthalene ND mg/kg 08/19/19 18:45 91-20-308/19/19 14:090.0040 1
n-Propylbenzene ND mg/kg 08/19/19 18:45 103-65-108/19/19 14:090.0040 1
Styrene ND mg/kg 08/19/19 18:45 100-42-508/19/19 14:090.0040 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 18:45 630-20-608/19/19 14:090.0040 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 18:45 79-34-508/19/19 14:090.0040 1
Tetrachloroethene ND mg/kg 08/19/19 18:45 127-18-408/19/19 14:090.0040 1
Toluene ND mg/kg 08/19/19 18:45 108-88-308/19/19 14:090.0040 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 18:45 87-61-608/19/19 14:090.0040 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 18:45 120-82-108/19/19 14:090.0040 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 18:45 71-55-608/19/19 14:090.0040 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 18:45 79-00-508/19/19 14:090.0040 1
Trichloroethene ND mg/kg 08/19/19 18:45 79-01-608/19/19 14:090.0040 1
Trichlorofluoromethane ND mg/kg 08/19/19 18:45 75-69-408/19/19 14:090.0040 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 18:45 96-18-408/19/19 14:090.0040 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 18:45 95-63-608/19/19 14:090.0040 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-2 0-2'Lab ID:92441608006 Collected:08/14/19 12:40 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 18:45 108-67-808/19/19 14:090.0040 1
Vinyl acetate ND mg/kg 08/19/19 18:45 108-05-408/19/19 14:090.040 1
Vinyl chloride ND mg/kg 08/19/19 18:45 75-01-408/19/19 14:090.0080 1
Xylene (Total)ND mg/kg 08/19/19 18:45 1330-20-708/19/19 14:090.0080 1
m&p-Xylene ND mg/kg 08/19/19 18:45 179601-23-108/19/19 14:090.0080 1
o-Xylene ND mg/kg 08/19/19 18:45 95-47-608/19/19 14:090.0040 1
Surrogates
Toluene-d8 (S)112 %08/19/19 18:45 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)101 %08/19/19 18:45 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)90 %08/19/19 18:45 17060-07-008/19/19 14:0970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.5 %08/16/19 17:050.10 1
Sample:GP-9 0-2'Lab ID:92441608007 Collected:08/14/19 13:57 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic ND mg/kg 08/23/19 09:46 7440-38-208/21/19 14:114.1 50
Barium 23.1 mg/kg 08/23/19 09:46 7440-39-308/21/19 14:114.1 50
Cadmium ND mg/kg 08/23/19 09:46 7440-43-908/21/19 14:110.49 50
Chromium 107 mg/kg 08/23/19 09:46 7440-47-308/21/19 14:114.1 50
Lead 9.1 mg/kg 08/23/19 09:46 7439-92-108/21/19 14:114.1 50
Selenium ND mg/kg 08/23/19 09:46 7782-49-208/21/19 14:114.1 50
Silver ND mg/kg 08/23/19 09:46 7440-22-4 N208/21/19 14:110.49 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.28 mg/kg 08/21/19 16:23 7439-97-608/21/19 10:350.021 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 12:32 83-32-908/17/19 15:340.44 1
Acenaphthylene ND mg/kg 08/20/19 12:32 208-96-808/17/19 15:340.44 1
Aniline ND mg/kg 08/20/19 12:32 62-53-308/17/19 15:340.44 1
Anthracene ND mg/kg 08/20/19 12:32 120-12-708/17/19 15:340.44 1
Benzo(a)anthracene ND mg/kg 08/20/19 12:32 56-55-308/17/19 15:340.44 1
Benzo(a)pyrene ND mg/kg 08/20/19 12:32 50-32-808/17/19 15:340.44 1
Benzo(b)fluoranthene ND mg/kg 08/20/19 12:32 205-99-208/17/19 15:340.44 1
Benzo(g,h,i)perylene ND mg/kg 08/20/19 12:32 191-24-208/17/19 15:340.44 1
Benzo(k)fluoranthene ND mg/kg 08/20/19 12:32 207-08-908/17/19 15:340.44 1
Benzoic Acid ND mg/kg 08/20/19 12:32 65-85-008/17/19 15:342.2 1
Benzyl alcohol ND mg/kg 08/20/19 12:32 100-51-608/17/19 15:340.87 1
4-Bromophenylphenyl ether ND mg/kg 08/20/19 12:32 101-55-308/17/19 15:340.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-9 0-2'Lab ID:92441608007 Collected:08/14/19 13:57 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Butylbenzylphthalate ND mg/kg 08/20/19 12:32 85-68-708/17/19 15:340.44 1
4-Chloro-3-methylphenol ND mg/kg 08/20/19 12:32 59-50-708/17/19 15:340.87 1
4-Chloroaniline ND mg/kg 08/20/19 12:32 106-47-808/17/19 15:342.2 1
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 12:32 111-91-108/17/19 15:340.44 1
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 12:32 111-44-408/17/19 15:340.44 1
2-Chloronaphthalene ND mg/kg 08/20/19 12:32 91-58-708/17/19 15:340.44 1
2-Chlorophenol ND mg/kg 08/20/19 12:32 95-57-808/17/19 15:340.44 1
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 12:32 7005-72-308/17/19 15:340.44 1
Chrysene ND mg/kg 08/20/19 12:32 218-01-908/17/19 15:340.44 1
Dibenz(a,h)anthracene ND mg/kg 08/20/19 12:32 53-70-308/17/19 15:340.44 1
Dibenzofuran ND mg/kg 08/20/19 12:32 132-64-908/17/19 15:340.44 1
1,2-Dichlorobenzene ND mg/kg 08/20/19 12:32 95-50-108/17/19 15:340.44 1
1,3-Dichlorobenzene ND mg/kg 08/20/19 12:32 541-73-108/17/19 15:340.44 1
1,4-Dichlorobenzene ND mg/kg 08/20/19 12:32 106-46-708/17/19 15:340.44 1
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 12:32 91-94-108/17/19 15:342.2 1
2,4-Dichlorophenol ND mg/kg 08/20/19 12:32 120-83-208/17/19 15:340.44 1
Diethylphthalate ND mg/kg 08/20/19 12:32 84-66-208/17/19 15:340.44 1
2,4-Dimethylphenol ND mg/kg 08/20/19 12:32 105-67-908/17/19 15:340.44 1
Dimethylphthalate ND mg/kg 08/20/19 12:32 131-11-308/17/19 15:340.44 1
Di-n-butylphthalate ND mg/kg 08/20/19 12:32 84-74-208/17/19 15:340.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 12:32 534-52-108/17/19 15:340.87 1
2,4-Dinitrophenol ND mg/kg 08/20/19 12:32 51-28-508/17/19 15:342.2 1
2,4-Dinitrotoluene ND mg/kg 08/20/19 12:32 121-14-208/17/19 15:340.44 1
2,6-Dinitrotoluene ND mg/kg 08/20/19 12:32 606-20-208/17/19 15:340.44 1
Di-n-octylphthalate ND mg/kg 08/20/19 12:32 117-84-008/17/19 15:340.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 12:32 117-81-708/17/19 15:340.44 1
Fluoranthene ND mg/kg 08/20/19 12:32 206-44-008/17/19 15:340.44 1
Fluorene ND mg/kg 08/20/19 12:32 86-73-708/17/19 15:340.44 1
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 12:32 87-68-308/17/19 15:340.44 1
Hexachlorobenzene ND mg/kg 08/20/19 12:32 118-74-108/17/19 15:340.44 1
Hexachlorocyclopentadiene ND mg/kg 08/20/19 12:32 77-47-408/17/19 15:340.44 1
Hexachloroethane ND mg/kg 08/20/19 12:32 67-72-108/17/19 15:340.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 12:32 193-39-508/17/19 15:340.44 1
Isophorone ND mg/kg 08/20/19 12:32 78-59-108/17/19 15:340.44 1
1-Methylnaphthalene ND mg/kg 08/20/19 12:32 90-12-008/17/19 15:340.44 1
2-Methylnaphthalene ND mg/kg 08/20/19 12:32 91-57-608/17/19 15:340.44 1
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 12:32 95-48-708/17/19 15:340.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 12:32 15831-10-408/17/19 15:340.44 1
Naphthalene ND mg/kg 08/20/19 12:32 91-20-308/17/19 15:340.44 1
2-Nitroaniline ND mg/kg 08/20/19 12:32 88-74-408/17/19 15:342.2 1
3-Nitroaniline ND mg/kg 08/20/19 12:32 99-09-208/17/19 15:342.2 1
4-Nitroaniline ND mg/kg 08/20/19 12:32 100-01-608/17/19 15:340.87 1
Nitrobenzene ND mg/kg 08/20/19 12:32 98-95-308/17/19 15:340.44 1
2-Nitrophenol ND mg/kg 08/20/19 12:32 88-75-508/17/19 15:340.44 1
4-Nitrophenol ND mg/kg 08/20/19 12:32 100-02-708/17/19 15:342.2 1
N-Nitrosodimethylamine ND mg/kg 08/20/19 12:32 62-75-908/17/19 15:340.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-9 0-2'Lab ID:92441608007 Collected:08/14/19 13:57 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 12:32 621-64-708/17/19 15:340.44 1
N-Nitrosodiphenylamine ND mg/kg 08/20/19 12:32 86-30-608/17/19 15:340.44 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 12:32 108-60-108/17/19 15:340.44 1
Pentachlorophenol ND mg/kg 08/20/19 12:32 87-86-508/17/19 15:342.2 1
Phenanthrene ND mg/kg 08/20/19 12:32 85-01-808/17/19 15:340.44 1
Phenol ND mg/kg 08/20/19 12:32 108-95-208/17/19 15:340.44 1
Pyrene ND mg/kg 08/20/19 12:32 129-00-008/17/19 15:340.44 1
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 12:32 120-82-108/17/19 15:340.44 1
2,4,5-Trichlorophenol ND mg/kg 08/20/19 12:32 95-95-408/17/19 15:340.44 1
2,4,6-Trichlorophenol ND mg/kg 08/20/19 12:32 88-06-208/17/19 15:340.44 1
Surrogates
Nitrobenzene-d5 (S)65 %08/20/19 12:32 4165-60-008/17/19 15:3423-110 1
2-Fluorobiphenyl (S)68 %08/20/19 12:32 321-60-808/17/19 15:3430-110 1
Terphenyl-d14 (S)82 %08/20/19 12:32 1718-51-008/17/19 15:3428-110 1
Phenol-d6 (S)60 %08/20/19 12:32 13127-88-308/17/19 15:3422-110 1
2-Fluorophenol (S)60 %08/20/19 12:32 367-12-408/17/19 15:3413-110 1
2,4,6-Tribromophenol (S)83 %08/20/19 12:32 118-79-608/17/19 15:3427-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 19:10 67-64-108/19/19 14:090.10 1
Benzene ND mg/kg 08/19/19 19:10 71-43-208/19/19 14:090.0051 1
Bromobenzene ND mg/kg 08/19/19 19:10 108-86-108/19/19 14:090.0051 1
Bromochloromethane ND mg/kg 08/19/19 19:10 74-97-508/19/19 14:090.0051 1
Bromodichloromethane ND mg/kg 08/19/19 19:10 75-27-408/19/19 14:090.0051 1
Bromoform ND mg/kg 08/19/19 19:10 75-25-208/19/19 14:090.0051 1
Bromomethane ND mg/kg 08/19/19 19:10 74-83-908/19/19 14:090.010 1
2-Butanone (MEK)ND mg/kg 08/19/19 19:10 78-93-308/19/19 14:090.10 1
n-Butylbenzene ND mg/kg 08/19/19 19:10 104-51-808/19/19 14:090.0051 1
sec-Butylbenzene ND mg/kg 08/19/19 19:10 135-98-808/19/19 14:090.0051 1
tert-Butylbenzene ND mg/kg 08/19/19 19:10 98-06-608/19/19 14:090.0051 1
Carbon tetrachloride ND mg/kg 08/19/19 19:10 56-23-508/19/19 14:090.0051 1
Chlorobenzene ND mg/kg 08/19/19 19:10 108-90-708/19/19 14:090.0051 1
Chloroethane ND mg/kg 08/19/19 19:10 75-00-308/19/19 14:090.010 1
Chloroform ND mg/kg 08/19/19 19:10 67-66-308/19/19 14:090.0051 1
Chloromethane ND mg/kg 08/19/19 19:10 74-87-308/19/19 14:090.010 1
2-Chlorotoluene ND mg/kg 08/19/19 19:10 95-49-808/19/19 14:090.0051 1
4-Chlorotoluene ND mg/kg 08/19/19 19:10 106-43-408/19/19 14:090.0051 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 19:10 96-12-808/19/19 14:090.0051 1
Dibromochloromethane ND mg/kg 08/19/19 19:10 124-48-108/19/19 14:090.0051 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 19:10 106-93-408/19/19 14:090.0051 1
Dibromomethane ND mg/kg 08/19/19 19:10 74-95-308/19/19 14:090.0051 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 19:10 95-50-108/19/19 14:090.0051 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 19:10 541-73-108/19/19 14:090.0051 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 19:10 106-46-708/19/19 14:090.0051 1
Dichlorodifluoromethane ND mg/kg 08/19/19 19:10 75-71-808/19/19 14:090.010 1
1,1-Dichloroethane ND mg/kg 08/19/19 19:10 75-34-308/19/19 14:090.0051 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-9 0-2'Lab ID:92441608007 Collected:08/14/19 13:57 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
1,2-Dichloroethane ND mg/kg 08/19/19 19:10 107-06-208/19/19 14:090.0051 1
1,1-Dichloroethene ND mg/kg 08/19/19 19:10 75-35-408/19/19 14:090.0051 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 19:10 156-59-208/19/19 14:090.0051 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 19:10 156-60-508/19/19 14:090.0051 1
1,2-Dichloropropane ND mg/kg 08/19/19 19:10 78-87-508/19/19 14:090.0051 1
1,3-Dichloropropane ND mg/kg 08/19/19 19:10 142-28-908/19/19 14:090.0051 1
2,2-Dichloropropane ND mg/kg 08/19/19 19:10 594-20-708/19/19 14:090.0051 1
1,1-Dichloropropene ND mg/kg 08/19/19 19:10 563-58-608/19/19 14:090.0051 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 19:10 10061-01-508/19/19 14:090.0051 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 19:10 10061-02-608/19/19 14:090.0051 1
Diisopropyl ether ND mg/kg 08/19/19 19:10 108-20-308/19/19 14:090.0051 1
Ethylbenzene ND mg/kg 08/19/19 19:10 100-41-408/19/19 14:090.0051 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 19:10 87-68-308/19/19 14:090.0051 1
2-Hexanone ND mg/kg 08/19/19 19:10 591-78-608/19/19 14:090.051 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 19:10 98-82-808/19/19 14:090.0051 1
p-Isopropyltoluene ND mg/kg 08/19/19 19:10 99-87-608/19/19 14:090.0051 1
Methylene Chloride ND mg/kg 08/19/19 19:10 75-09-208/19/19 14:090.020 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 19:10 108-10-108/19/19 14:090.051 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 19:10 1634-04-408/19/19 14:090.0051 1
Naphthalene ND mg/kg 08/19/19 19:10 91-20-308/19/19 14:090.0051 1
n-Propylbenzene ND mg/kg 08/19/19 19:10 103-65-108/19/19 14:090.0051 1
Styrene ND mg/kg 08/19/19 19:10 100-42-508/19/19 14:090.0051 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 19:10 630-20-608/19/19 14:090.0051 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 19:10 79-34-508/19/19 14:090.0051 1
Tetrachloroethene ND mg/kg 08/19/19 19:10 127-18-408/19/19 14:090.0051 1
Toluene ND mg/kg 08/19/19 19:10 108-88-308/19/19 14:090.0051 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 19:10 87-61-608/19/19 14:090.0051 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 19:10 120-82-108/19/19 14:090.0051 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 19:10 71-55-608/19/19 14:090.0051 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 19:10 79-00-508/19/19 14:090.0051 1
Trichloroethene ND mg/kg 08/19/19 19:10 79-01-608/19/19 14:090.0051 1
Trichlorofluoromethane ND mg/kg 08/19/19 19:10 75-69-408/19/19 14:090.0051 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 19:10 96-18-408/19/19 14:090.0051 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 19:10 95-63-608/19/19 14:090.0051 1
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 19:10 108-67-808/19/19 14:090.0051 1
Vinyl acetate ND mg/kg 08/19/19 19:10 108-05-408/19/19 14:090.051 1
Vinyl chloride ND mg/kg 08/19/19 19:10 75-01-408/19/19 14:090.010 1
Xylene (Total)ND mg/kg 08/19/19 19:10 1330-20-708/19/19 14:090.010 1
m&p-Xylene ND mg/kg 08/19/19 19:10 179601-23-108/19/19 14:090.010 1
o-Xylene ND mg/kg 08/19/19 19:10 95-47-608/19/19 14:090.0051 1
Surrogates
Toluene-d8 (S)112 %08/19/19 19:10 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)102 %08/19/19 19:10 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)92 %08/19/19 19:10 17060-07-008/19/19 14:0970-132 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-9 0-2'Lab ID:92441608007 Collected:08/14/19 13:57 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.9 %08/16/19 17:060.10 1
Sample:GP-8 0-2'Lab ID:92441608008 Collected:08/14/19 14:55 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS
Arsenic 5.4 mg/kg 08/23/19 09:48 7440-38-208/21/19 14:114.2 50
Barium 33.2 mg/kg 08/23/19 09:48 7440-39-308/21/19 14:114.2 50
Cadmium ND mg/kg 08/23/19 09:48 7440-43-908/21/19 14:110.51 50
Chromium 42.3 mg/kg 08/23/19 09:48 7440-47-308/21/19 14:114.2 50
Lead 58.6 mg/kg 08/23/19 09:48 7439-92-108/21/19 14:114.2 50
Selenium ND mg/kg 08/23/19 09:48 7782-49-208/21/19 14:114.2 50
Silver ND mg/kg 08/23/19 09:48 7440-22-4 N208/21/19 14:110.51 50
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.19 mg/kg 08/21/19 15:47 7439-97-608/21/19 10:350.022 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND mg/kg 08/20/19 20:28 83-32-908/17/19 15:342.3 5
Acenaphthylene ND mg/kg 08/20/19 20:28 208-96-808/17/19 15:342.3 5
Aniline ND mg/kg 08/20/19 20:28 62-53-308/17/19 15:342.3 5
Anthracene ND mg/kg 08/20/19 20:28 120-12-708/17/19 15:342.3 5
Benzo(a)anthracene ND mg/kg 08/20/19 20:28 56-55-308/17/19 15:342.3 5
Benzo(a)pyrene ND mg/kg 08/20/19 20:28 50-32-808/17/19 15:342.3 5
Benzo(b)fluoranthene ND mg/kg 08/20/19 20:28 205-99-208/17/19 15:342.3 5
Benzo(g,h,i)perylene ND mg/kg 08/20/19 20:28 191-24-208/17/19 15:342.3 5
Benzo(k)fluoranthene ND mg/kg 08/20/19 20:28 207-08-908/17/19 15:342.3 5
Benzoic Acid ND mg/kg 08/20/19 20:28 65-85-008/17/19 15:3411.3 5
Benzyl alcohol ND mg/kg 08/20/19 20:28 100-51-608/17/19 15:344.5 5
4-Bromophenylphenyl ether ND mg/kg 08/20/19 20:28 101-55-308/17/19 15:342.3 5
Butylbenzylphthalate ND mg/kg 08/20/19 20:28 85-68-708/17/19 15:342.3 5
4-Chloro-3-methylphenol ND mg/kg 08/20/19 20:28 59-50-708/17/19 15:344.5 5
4-Chloroaniline ND mg/kg 08/20/19 20:28 106-47-808/17/19 15:3411.3 5
bis(2-Chloroethoxy)methane ND mg/kg 08/20/19 20:28 111-91-108/17/19 15:342.3 5
bis(2-Chloroethyl) ether ND mg/kg 08/20/19 20:28 111-44-408/17/19 15:342.3 5
2-Chloronaphthalene ND mg/kg 08/20/19 20:28 91-58-708/17/19 15:342.3 5
2-Chlorophenol ND mg/kg 08/20/19 20:28 95-57-808/17/19 15:342.3 5
4-Chlorophenylphenyl ether ND mg/kg 08/20/19 20:28 7005-72-308/17/19 15:342.3 5
Chrysene ND mg/kg 08/20/19 20:28 218-01-908/17/19 15:342.3 5
Dibenz(a,h)anthracene ND mg/kg 08/20/19 20:28 53-70-308/17/19 15:342.3 5
Dibenzofuran ND mg/kg 08/20/19 20:28 132-64-908/17/19 15:342.3 5
1,2-Dichlorobenzene ND mg/kg 08/20/19 20:28 95-50-108/17/19 15:342.3 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-8 0-2'Lab ID:92441608008 Collected:08/14/19 14:55 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
1,3-Dichlorobenzene ND mg/kg 08/20/19 20:28 541-73-108/17/19 15:342.3 5
1,4-Dichlorobenzene ND mg/kg 08/20/19 20:28 106-46-708/17/19 15:342.3 5
3,3'-Dichlorobenzidine ND mg/kg 08/20/19 20:28 91-94-108/17/19 15:3411.3 5
2,4-Dichlorophenol ND mg/kg 08/20/19 20:28 120-83-208/17/19 15:342.3 5
Diethylphthalate ND mg/kg 08/20/19 20:28 84-66-208/17/19 15:342.3 5
2,4-Dimethylphenol ND mg/kg 08/20/19 20:28 105-67-908/17/19 15:342.3 5
Dimethylphthalate ND mg/kg 08/20/19 20:28 131-11-308/17/19 15:342.3 5
Di-n-butylphthalate ND mg/kg 08/20/19 20:28 84-74-208/17/19 15:342.3 5
4,6-Dinitro-2-methylphenol ND mg/kg 08/20/19 20:28 534-52-108/17/19 15:344.5 5
2,4-Dinitrophenol ND mg/kg 08/20/19 20:28 51-28-508/17/19 15:3411.3 5
2,4-Dinitrotoluene ND mg/kg 08/20/19 20:28 121-14-208/17/19 15:342.3 5
2,6-Dinitrotoluene ND mg/kg 08/20/19 20:28 606-20-208/17/19 15:342.3 5
Di-n-octylphthalate ND mg/kg 08/20/19 20:28 117-84-008/17/19 15:342.3 5
bis(2-Ethylhexyl)phthalate ND mg/kg 08/20/19 20:28 117-81-708/17/19 15:342.3 5
Fluoranthene ND mg/kg 08/20/19 20:28 206-44-008/17/19 15:342.3 5
Fluorene ND mg/kg 08/20/19 20:28 86-73-708/17/19 15:342.3 5
Hexachloro-1,3-butadiene ND mg/kg 08/20/19 20:28 87-68-308/17/19 15:342.3 5
Hexachlorobenzene ND mg/kg 08/20/19 20:28 118-74-108/17/19 15:342.3 5
Hexachlorocyclopentadiene ND mg/kg 08/20/19 20:28 77-47-408/17/19 15:342.3 5
Hexachloroethane ND mg/kg 08/20/19 20:28 67-72-108/17/19 15:342.3 5
Indeno(1,2,3-cd)pyrene ND mg/kg 08/20/19 20:28 193-39-508/17/19 15:342.3 5
Isophorone ND mg/kg 08/20/19 20:28 78-59-108/17/19 15:342.3 5
1-Methylnaphthalene ND mg/kg 08/20/19 20:28 90-12-008/17/19 15:342.3 5
2-Methylnaphthalene ND mg/kg 08/20/19 20:28 91-57-608/17/19 15:342.3 5
2-Methylphenol(o-Cresol)ND mg/kg 08/20/19 20:28 95-48-708/17/19 15:342.3 5
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/20/19 20:28 15831-10-408/17/19 15:342.3 5
Naphthalene ND mg/kg 08/20/19 20:28 91-20-308/17/19 15:342.3 5
2-Nitroaniline ND mg/kg 08/20/19 20:28 88-74-408/17/19 15:3411.3 5
3-Nitroaniline ND mg/kg 08/20/19 20:28 99-09-208/17/19 15:3411.3 5
4-Nitroaniline ND mg/kg 08/20/19 20:28 100-01-608/17/19 15:344.5 5
Nitrobenzene ND mg/kg 08/20/19 20:28 98-95-308/17/19 15:342.3 5
2-Nitrophenol ND mg/kg 08/20/19 20:28 88-75-508/17/19 15:342.3 5
4-Nitrophenol ND mg/kg 08/20/19 20:28 100-02-708/17/19 15:3411.3 5
N-Nitrosodimethylamine ND mg/kg 08/20/19 20:28 62-75-908/17/19 15:342.3 5
N-Nitroso-di-n-propylamine ND mg/kg 08/20/19 20:28 621-64-708/17/19 15:342.3 5
N-Nitrosodiphenylamine ND mg/kg 08/20/19 20:28 86-30-608/17/19 15:342.3 5
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/20/19 20:28 108-60-108/17/19 15:342.3 5
Pentachlorophenol ND mg/kg 08/20/19 20:28 87-86-508/17/19 15:3411.3 5
Phenanthrene ND mg/kg 08/20/19 20:28 85-01-808/17/19 15:342.3 5
Phenol ND mg/kg 08/20/19 20:28 108-95-208/17/19 15:342.3 5
Pyrene ND mg/kg 08/20/19 20:28 129-00-008/17/19 15:342.3 5
1,2,4-Trichlorobenzene ND mg/kg 08/20/19 20:28 120-82-108/17/19 15:342.3 5
2,4,5-Trichlorophenol ND mg/kg 08/20/19 20:28 95-95-408/17/19 15:342.3 5
2,4,6-Trichlorophenol ND mg/kg 08/20/19 20:28 88-06-208/17/19 15:342.3 5
Surrogates
Nitrobenzene-d5 (S)46 %08/20/19 20:28 4165-60-0 D308/17/19 15:3423-110 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-8 0-2'Lab ID:92441608008 Collected:08/14/19 14:55 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)55 %08/20/19 20:28 321-60-808/17/19 15:3430-110 5
Terphenyl-d14 (S)67 %08/20/19 20:28 1718-51-008/17/19 15:3428-110 5
Phenol-d6 (S)46 %08/20/19 20:28 13127-88-308/17/19 15:3422-110 5
2-Fluorophenol (S)44 %08/20/19 20:28 367-12-408/17/19 15:3413-110 5
2,4,6-Tribromophenol (S)67 %08/20/19 20:28 118-79-608/17/19 15:3427-110 5
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND mg/kg 08/19/19 19:35 67-64-108/19/19 14:090.11 1
Benzene ND mg/kg 08/19/19 19:35 71-43-208/19/19 14:090.0053 1
Bromobenzene ND mg/kg 08/19/19 19:35 108-86-108/19/19 14:090.0053 1
Bromochloromethane ND mg/kg 08/19/19 19:35 74-97-508/19/19 14:090.0053 1
Bromodichloromethane ND mg/kg 08/19/19 19:35 75-27-408/19/19 14:090.0053 1
Bromoform ND mg/kg 08/19/19 19:35 75-25-208/19/19 14:090.0053 1
Bromomethane ND mg/kg 08/19/19 19:35 74-83-908/19/19 14:090.011 1
2-Butanone (MEK)ND mg/kg 08/19/19 19:35 78-93-308/19/19 14:090.11 1
n-Butylbenzene ND mg/kg 08/19/19 19:35 104-51-808/19/19 14:090.0053 1
sec-Butylbenzene ND mg/kg 08/19/19 19:35 135-98-808/19/19 14:090.0053 1
tert-Butylbenzene ND mg/kg 08/19/19 19:35 98-06-608/19/19 14:090.0053 1
Carbon tetrachloride ND mg/kg 08/19/19 19:35 56-23-508/19/19 14:090.0053 1
Chlorobenzene ND mg/kg 08/19/19 19:35 108-90-708/19/19 14:090.0053 1
Chloroethane ND mg/kg 08/19/19 19:35 75-00-308/19/19 14:090.011 1
Chloroform ND mg/kg 08/19/19 19:35 67-66-308/19/19 14:090.0053 1
Chloromethane ND mg/kg 08/19/19 19:35 74-87-308/19/19 14:090.011 1
2-Chlorotoluene ND mg/kg 08/19/19 19:35 95-49-808/19/19 14:090.0053 1
4-Chlorotoluene ND mg/kg 08/19/19 19:35 106-43-408/19/19 14:090.0053 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/19/19 19:35 96-12-808/19/19 14:090.0053 1
Dibromochloromethane ND mg/kg 08/19/19 19:35 124-48-108/19/19 14:090.0053 1
1,2-Dibromoethane (EDB)ND mg/kg 08/19/19 19:35 106-93-408/19/19 14:090.0053 1
Dibromomethane ND mg/kg 08/19/19 19:35 74-95-308/19/19 14:090.0053 1
1,2-Dichlorobenzene ND mg/kg 08/19/19 19:35 95-50-108/19/19 14:090.0053 1
1,3-Dichlorobenzene ND mg/kg 08/19/19 19:35 541-73-108/19/19 14:090.0053 1
1,4-Dichlorobenzene ND mg/kg 08/19/19 19:35 106-46-708/19/19 14:090.0053 1
Dichlorodifluoromethane ND mg/kg 08/19/19 19:35 75-71-808/19/19 14:090.011 1
1,1-Dichloroethane ND mg/kg 08/19/19 19:35 75-34-308/19/19 14:090.0053 1
1,2-Dichloroethane ND mg/kg 08/19/19 19:35 107-06-208/19/19 14:090.0053 1
1,1-Dichloroethene ND mg/kg 08/19/19 19:35 75-35-408/19/19 14:090.0053 1
cis-1,2-Dichloroethene ND mg/kg 08/19/19 19:35 156-59-208/19/19 14:090.0053 1
trans-1,2-Dichloroethene ND mg/kg 08/19/19 19:35 156-60-508/19/19 14:090.0053 1
1,2-Dichloropropane ND mg/kg 08/19/19 19:35 78-87-508/19/19 14:090.0053 1
1,3-Dichloropropane ND mg/kg 08/19/19 19:35 142-28-908/19/19 14:090.0053 1
2,2-Dichloropropane ND mg/kg 08/19/19 19:35 594-20-708/19/19 14:090.0053 1
1,1-Dichloropropene ND mg/kg 08/19/19 19:35 563-58-608/19/19 14:090.0053 1
cis-1,3-Dichloropropene ND mg/kg 08/19/19 19:35 10061-01-508/19/19 14:090.0053 1
trans-1,3-Dichloropropene ND mg/kg 08/19/19 19:35 10061-02-608/19/19 14:090.0053 1
Diisopropyl ether ND mg/kg 08/19/19 19:35 108-20-308/19/19 14:090.0053 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 34 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Sample:GP-8 0-2'Lab ID:92441608008 Collected:08/14/19 14:55 Received:08/15/19 09:01 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Ethylbenzene ND mg/kg 08/19/19 19:35 100-41-408/19/19 14:090.0053 1
Hexachloro-1,3-butadiene ND mg/kg 08/19/19 19:35 87-68-308/19/19 14:090.0053 1
2-Hexanone ND mg/kg 08/19/19 19:35 591-78-608/19/19 14:090.053 1
Isopropylbenzene (Cumene)ND mg/kg 08/19/19 19:35 98-82-808/19/19 14:090.0053 1
p-Isopropyltoluene ND mg/kg 08/19/19 19:35 99-87-608/19/19 14:090.0053 1
Methylene Chloride ND mg/kg 08/19/19 19:35 75-09-208/19/19 14:090.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/19/19 19:35 108-10-108/19/19 14:090.053 1
Methyl-tert-butyl ether ND mg/kg 08/19/19 19:35 1634-04-408/19/19 14:090.0053 1
Naphthalene ND mg/kg 08/19/19 19:35 91-20-308/19/19 14:090.0053 1
n-Propylbenzene ND mg/kg 08/19/19 19:35 103-65-108/19/19 14:090.0053 1
Styrene ND mg/kg 08/19/19 19:35 100-42-508/19/19 14:090.0053 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/19/19 19:35 630-20-608/19/19 14:090.0053 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/19/19 19:35 79-34-508/19/19 14:090.0053 1
Tetrachloroethene ND mg/kg 08/19/19 19:35 127-18-408/19/19 14:090.0053 1
Toluene ND mg/kg 08/19/19 19:35 108-88-308/19/19 14:090.0053 1
1,2,3-Trichlorobenzene ND mg/kg 08/19/19 19:35 87-61-608/19/19 14:090.0053 1
1,2,4-Trichlorobenzene ND mg/kg 08/19/19 19:35 120-82-108/19/19 14:090.0053 1
1,1,1-Trichloroethane ND mg/kg 08/19/19 19:35 71-55-608/19/19 14:090.0053 1
1,1,2-Trichloroethane ND mg/kg 08/19/19 19:35 79-00-508/19/19 14:090.0053 1
Trichloroethene ND mg/kg 08/19/19 19:35 79-01-608/19/19 14:090.0053 1
Trichlorofluoromethane ND mg/kg 08/19/19 19:35 75-69-408/19/19 14:090.0053 1
1,2,3-Trichloropropane ND mg/kg 08/19/19 19:35 96-18-408/19/19 14:090.0053 1
1,2,4-Trimethylbenzene ND mg/kg 08/19/19 19:35 95-63-608/19/19 14:090.0053 1
1,3,5-Trimethylbenzene ND mg/kg 08/19/19 19:35 108-67-808/19/19 14:090.0053 1
Vinyl acetate ND mg/kg 08/19/19 19:35 108-05-408/19/19 14:090.053 1
Vinyl chloride ND mg/kg 08/19/19 19:35 75-01-408/19/19 14:090.011 1
Xylene (Total)ND mg/kg 08/19/19 19:35 1330-20-708/19/19 14:090.011 1
m&p-Xylene ND mg/kg 08/19/19 19:35 179601-23-108/19/19 14:090.011 1
o-Xylene ND mg/kg 08/19/19 19:35 95-47-608/19/19 14:090.0053 1
Surrogates
Toluene-d8 (S)109 %08/19/19 19:35 2037-26-508/19/19 14:0970-130 1
4-Bromofluorobenzene (S)103 %08/19/19 19:35 460-00-408/19/19 14:0970-130 1
1,2-Dichloroethane-d4 (S)95 %08/19/19 19:35 17060-07-008/19/19 14:0970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.1 %08/16/19 17:060.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
564376
EPA 7471
EPA 7471
7471 Mercury
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3064979
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.0096 08/21/19 13:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3064980LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0970.098 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3064981MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35490225001
3064982
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Mercury mg/kg M10.099 60 80-12075 120.1020.081 0.14 0.16
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
564525
EPA 3050
EPA 6020
6020 MET SOLID
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3065562
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Matrix:Solid
Analyzed
Arsenic mg/kg ND 1.2 08/23/19 08:44
Barium mg/kg ND 1.2 08/23/19 08:44
Cadmium mg/kg ND 0.15 08/23/19 08:44
Chromium mg/kg ND 1.2 08/23/19 08:44
Lead mg/kg ND 1.2 08/23/19 08:44
Selenium mg/kg ND 1.2 08/23/19 08:44
Silver mg/kg ND 0.15 N208/23/19 08:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3065563LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 30.230.5 99 80-120
Barium mg/kg 30.430.5 100 80-120
Cadmium mg/kg 3.03 98 80-120
Chromium mg/kg 31.230.5 102 80-120
Lead mg/kg 31.230.5 102 80-120
Selenium mg/kg 28.730.5 94 80-120
Silver mg/kg 3.2 N2310580-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3065564MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35490318001
3065565
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Arsenic mg/kg 36.9 115 75-12595 15379.4 51.8 44.5
Barium mg/kg 36.9 114 75-125100 93713.0 54.9 50.0
Cadmium mg/kg 3.72 98 75-12594 33.720.27 3.9 3.8
Chromium mg/kg 36.9 123 75-12589 153743.0 88.3 76.1
Lead mg/kg 36.9 108 75-12598 73715.5 55.4 51.8
Selenium mg/kg 36.9 97 75-12589 8372.6 38.5 35.4
Silver mg/kg N23.72 99 75-12595 43.720.072J 3.7 3.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
493171
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2658357
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/19/19 14:37
1,1,1-Trichloroethane mg/kg ND 0.0050 08/19/19 14:37
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/19/19 14:37
1,1,2-Trichloroethane mg/kg ND 0.0050 08/19/19 14:37
1,1-Dichloroethane mg/kg ND 0.0050 08/19/19 14:37
1,1-Dichloroethene mg/kg ND 0.0050 08/19/19 14:37
1,1-Dichloropropene mg/kg ND 0.0050 08/19/19 14:37
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/19/19 14:37
1,2,3-Trichloropropane mg/kg ND 0.0050 08/19/19 14:37
1,2,4-Trichlorobenzene mg/kg ND 0.0050 08/19/19 14:37
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/19/19 14:37
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/19/19 14:37
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/19/19 14:37
1,2-Dichlorobenzene mg/kg ND 0.0050 08/19/19 14:37
1,2-Dichloroethane mg/kg ND 0.0050 08/19/19 14:37
1,2-Dichloropropane mg/kg ND 0.0050 08/19/19 14:37
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/19/19 14:37
1,3-Dichlorobenzene mg/kg ND 0.0050 08/19/19 14:37
1,3-Dichloropropane mg/kg ND 0.0050 08/19/19 14:37
1,4-Dichlorobenzene mg/kg ND 0.0050 08/19/19 14:37
2,2-Dichloropropane mg/kg ND 0.0050 08/19/19 14:37
2-Butanone (MEK)mg/kg ND 0.10 08/19/19 14:37
2-Chlorotoluene mg/kg ND 0.0050 08/19/19 14:37
2-Hexanone mg/kg ND 0.050 08/19/19 14:37
4-Chlorotoluene mg/kg ND 0.0050 08/19/19 14:37
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/19/19 14:37
Acetone mg/kg ND 0.10 08/19/19 14:37
Benzene mg/kg ND 0.0050 08/19/19 14:37
Bromobenzene mg/kg ND 0.0050 08/19/19 14:37
Bromochloromethane mg/kg ND 0.0050 08/19/19 14:37
Bromodichloromethane mg/kg ND 0.0050 08/19/19 14:37
Bromoform mg/kg ND 0.0050 08/19/19 14:37
Bromomethane mg/kg ND 0.010 08/19/19 14:37
Carbon tetrachloride mg/kg ND 0.0050 08/19/19 14:37
Chlorobenzene mg/kg ND 0.0050 08/19/19 14:37
Chloroethane mg/kg ND 0.010 08/19/19 14:37
Chloroform mg/kg ND 0.0050 08/19/19 14:37
Chloromethane mg/kg ND 0.010 08/19/19 14:37
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/19/19 14:37
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/19/19 14:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2658357
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 08/19/19 14:37
Dibromomethane mg/kg ND 0.0050 08/19/19 14:37
Dichlorodifluoromethane mg/kg ND 0.010 08/19/19 14:37
Diisopropyl ether mg/kg ND 0.0050 08/19/19 14:37
Ethylbenzene mg/kg ND 0.0050 08/19/19 14:37
Hexachloro-1,3-butadiene mg/kg ND 0.0050 08/19/19 14:37
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/19/19 14:37
m&p-Xylene mg/kg ND 0.010 08/19/19 14:37
Methyl-tert-butyl ether mg/kg ND 0.0050 08/19/19 14:37
Methylene Chloride mg/kg ND 0.020 08/19/19 14:37
n-Butylbenzene mg/kg ND 0.0050 08/19/19 14:37
n-Propylbenzene mg/kg ND 0.0050 08/19/19 14:37
Naphthalene mg/kg ND 0.0050 08/19/19 14:37
o-Xylene mg/kg ND 0.0050 08/19/19 14:37
p-Isopropyltoluene mg/kg ND 0.0050 08/19/19 14:37
sec-Butylbenzene mg/kg ND 0.0050 08/19/19 14:37
Styrene mg/kg ND 0.0050 08/19/19 14:37
tert-Butylbenzene mg/kg ND 0.0050 08/19/19 14:37
Tetrachloroethene mg/kg ND 0.0050 08/19/19 14:37
Toluene mg/kg ND 0.0050 08/19/19 14:37
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/19/19 14:37
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/19/19 14:37
Trichloroethene mg/kg ND 0.0050 08/19/19 14:37
Trichlorofluoromethane mg/kg ND 0.0050 08/19/19 14:37
Vinyl acetate mg/kg ND 0.050 08/19/19 14:37
Vinyl chloride mg/kg ND 0.010 08/19/19 14:37
Xylene (Total)mg/kg ND 0.010 08/19/19 14:37
1,2-Dichloroethane-d4 (S)%87 70-132 08/19/19 14:37
4-Bromofluorobenzene (S)%101 70-130 08/19/19 14:37
Toluene-d8 (S)%103 70-130 08/19/19 14:37
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2658358LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.0570.05 115 70-130
1,1,1-Trichloroethane mg/kg 0.0560.05 111 70-130
1,1,2,2-Tetrachloroethane mg/kg 0.0550.05 110 55-130
1,1,2-Trichloroethane mg/kg 0.0580.05 115 70-130
1,1-Dichloroethane mg/kg 0.0530.05 106 68-130
1,1-Dichloroethene mg/kg 0.0580.05 117 70-130
1,1-Dichloropropene mg/kg 0.0580.05 116 70-130
1,2,3-Trichlorobenzene mg/kg 0.0560.05 112 70-130
1,2,3-Trichloropropane mg/kg 0.0560.05 113 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2658358LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 0.0550.05 111 70-130
1,2,4-Trimethylbenzene mg/kg 0.0570.05 114 69-130
1,2-Dibromo-3-chloropropane mg/kg 0.0580.05 117 57-141
1,2-Dibromoethane (EDB)mg/kg 0.0580.05 117 70-130
1,2-Dichlorobenzene mg/kg 0.0550.05 110 70-130
1,2-Dichloroethane mg/kg 0.0520.05 104 70-130
1,2-Dichloropropane mg/kg 0.0560.05 111 70-130
1,3,5-Trimethylbenzene mg/kg 0.0560.05 112 70-130
1,3-Dichlorobenzene mg/kg 0.0560.05 111 70-130
1,3-Dichloropropane mg/kg 0.0580.05 116 70-130
1,4-Dichlorobenzene mg/kg 0.0540.05 109 70-130
2,2-Dichloropropane mg/kg 0.0570.05 115 70-130
2-Butanone (MEK)mg/kg 0.110.1 108 60-130
2-Chlorotoluene mg/kg 0.0550.05 110 70-130
2-Hexanone mg/kg 0.110.1 114 70-132
4-Chlorotoluene mg/kg 0.0540.05 109 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 0.110.1 108 69-130
Acetone mg/kg 0.110.1 114 49-148
Benzene mg/kg 0.0590.05 119 70-130
Bromobenzene mg/kg 0.0560.05 112 70-130
Bromochloromethane mg/kg 0.0560.05 112 70-130
Bromodichloromethane mg/kg 0.0570.05 114 70-130
Bromoform mg/kg 0.0580.05 115 68-136
Bromomethane mg/kg 0.0560.05 111 60-140
Carbon tetrachloride mg/kg 0.0580.05 115 70-130
Chlorobenzene mg/kg 0.0560.05 111 70-130
Chloroethane mg/kg 0.0580.05 116 51-147
Chloroform mg/kg 0.0520.05 103 70-130
Chloromethane mg/kg 0.0490.05 99 48-130
cis-1,2-Dichloroethene mg/kg 0.0550.05 110 70-130
cis-1,3-Dichloropropene mg/kg 0.0600.05 121 70-130
Dibromochloromethane mg/kg 0.0570.05 114 70-130
Dibromomethane mg/kg 0.0570.05 113 70-130
Dichlorodifluoromethane mg/kg 0.0480.05 96 49-130
Diisopropyl ether mg/kg 0.0480.05 95 66-130
Ethylbenzene mg/kg 0.0570.05 114 70-130
Hexachloro-1,3-butadiene mg/kg 0.0580.05 116 70-130
Isopropylbenzene (Cumene)mg/kg 0.0580.05 116 70-130
m&p-Xylene mg/kg 0.110.1 114 70-130
Methyl-tert-butyl ether mg/kg 0.0530.05 106 70-130
Methylene Chloride mg/kg 0.0490.05 97 50-137
n-Butylbenzene mg/kg 0.0570.05 115 70-130
n-Propylbenzene mg/kg 0.0570.05 113 70-130
Naphthalene mg/kg 0.0550.05 111 70-131
o-Xylene mg/kg 0.0570.05 115 70-130
p-Isopropyltoluene mg/kg 0.0570.05 115 70-130
sec-Butylbenzene mg/kg 0.0580.05 115 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2658358LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene mg/kg 0.0570.05 114 70-130
tert-Butylbenzene mg/kg 0.0520.05 103 69-130
Tetrachloroethene mg/kg 0.0560.05 111 56-130
Toluene mg/kg 0.0560.05 113 70-130
trans-1,2-Dichloroethene mg/kg 0.0560.05 112 70-130
trans-1,3-Dichloropropene mg/kg 0.0590.05 118 70-130
Trichloroethene mg/kg 0.0580.05 117 70-141
Trichlorofluoromethane mg/kg 0.0520.05 105 67-130
Vinyl acetate mg/kg 0.100.1 104 10-136
Vinyl chloride mg/kg 0.0540.05 108 67-130
Xylene (Total)mg/kg 0.170.15 115 70-130
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2658360MATRIX SPIKE SAMPLE:
MSSpike
Result
92441608005
1,1,1,2-Tetrachloroethane mg/kg 0.0220.022 101 52-133ND
1,1,1-Trichloroethane mg/kg 0.0240.022 110 49-137ND
1,1,2,2-Tetrachloroethane mg/kg 0.0190.022 86 39-150ND
1,1,2-Trichloroethane mg/kg 0.0200.022 92 48-140ND
1,1-Dichloroethane mg/kg 0.0230.022 103 46-135ND
1,1-Dichloroethene mg/kg 0.0260.022 119 38-149ND
1,1-Dichloropropene mg/kg 0.0220.022 101 41-140ND
1,2,3-Trichlorobenzene mg/kg 0.0210.022 93 10-158ND
1,2,3-Trichloropropane mg/kg 0.0200.022 92 33-157ND
1,2,4-Trichlorobenzene mg/kg 0.0210.022 95 10-155ND
1,2,4-Trimethylbenzene mg/kg 0.0210.022 95 24-154ND
1,2-Dibromo-3-chloropropane mg/kg 0.0200.022 88 33-158ND
1,2-Dibromoethane (EDB)mg/kg 0.0200.022 92 40-136ND
1,2-Dichlorobenzene mg/kg 0.0220.022 97 27-146ND
1,2-Dichloroethane mg/kg 0.0210.022 97 49-140ND
1,2-Dichloropropane mg/kg 0.0220.022 101 44-143ND
1,3,5-Trimethylbenzene mg/kg 0.0220.022 101 40-144ND
1,3-Dichlorobenzene mg/kg 0.0220.022 98 33-140ND
1,3-Dichloropropane mg/kg 0.0200.022 92 47-147ND
1,4-Dichlorobenzene mg/kg 0.0220.022 99 35-139ND
2,2-Dichloropropane mg/kg 0.0230.022 105 41-140ND
2-Butanone (MEK)mg/kg .032J0.044 73 10-181ND
2-Chlorotoluene mg/kg 0.0230.022 102 38-147ND
2-Hexanone mg/kg .033J0.044 75 18-169ND
4-Chlorotoluene mg/kg 0.0220.022 97 36-145ND
4-Methyl-2-pentanone (MIBK)mg/kg .035J0.044 78 16-175ND
Acetone mg/kg .04J0.044 90 10-200ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2658360MATRIX SPIKE SAMPLE:
MSSpike
Result
92441608005
Benzene mg/kg 0.0230.022 104 46-136ND
Bromobenzene mg/kg 0.0220.022 101 38-149ND
Bromochloromethane mg/kg 0.0230.022 105 44-142ND
Bromodichloromethane mg/kg 0.0220.022 102 41-140ND
Bromoform mg/kg 0.0220.022 98 34-145ND
Bromomethane mg/kg 0.0200.022 91 14-162ND
Carbon tetrachloride mg/kg 0.0260.022 117 44-141ND
Chlorobenzene mg/kg 0.0230.022 102 39-141ND
Chloroethane mg/kg 0.0270.022 123 10-182ND
Chloroform mg/kg 0.0230.022 103 45-140ND
Chloromethane mg/kg 0.0220.022 98 19-149ND
cis-1,2-Dichloroethene mg/kg 0.0230.022 105 38-150ND
cis-1,3-Dichloropropene mg/kg 0.0230.022 106 30-144ND
Dibromochloromethane mg/kg 0.0210.022 95 36-145ND
Dibromomethane mg/kg 0.0230.022 104 41-145ND
Dichlorodifluoromethane mg/kg 0.0240.022 107 16-146ND
Diisopropyl ether mg/kg 0.0200.022 92 41-143ND
Ethylbenzene mg/kg 0.0230.022 104 35-144ND
Hexachloro-1,3-butadiene mg/kg 0.0220.022 100 10-160ND
Isopropylbenzene (Cumene)mg/kg 0.0240.022 107 30-152ND
m&p-Xylene mg/kg 0.0460.044 103 33-145ND
Methyl-tert-butyl ether mg/kg 0.0190.022 84 49-140ND
Methylene Chloride mg/kg .016J0.022 71 10-174ND
n-Butylbenzene mg/kg 0.0220.022 101 10-160ND
n-Propylbenzene mg/kg 0.0230.022 104 24-159ND
Naphthalene mg/kg 0.0200.022 89 10-171ND
o-Xylene mg/kg 0.0240.022 106 31-150ND
p-Isopropyltoluene mg/kg 0.0240.022 108 21-154ND
sec-Butylbenzene mg/kg 0.0230.022 106 19-159ND
Styrene mg/kg 0.0220.022 99 15-152ND
tert-Butylbenzene mg/kg 0.0200.022 90 31-141ND
Tetrachloroethene mg/kg 0.0230.022 104 19-141ND
Toluene mg/kg 0.0230.022 105 31-146ND
trans-1,2-Dichloroethene mg/kg 0.0240.022 108 28-157ND
trans-1,3-Dichloropropene mg/kg 0.0210.022 95 25-146ND
Trichloroethene mg/kg 0.0240.022 110 34-149ND
Trichlorofluoromethane mg/kg 0.0240.022 110 10-167ND
Vinyl acetate mg/kg .032J0.044 73 10-200ND
Vinyl chloride mg/kg 0.0220.022 100 36-155ND
Xylene (Total)mg/kg 0.0690.066 104 29-148ND
1,2-Dichloroethane-d4 (S)%94 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92441608001
2658359SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg .019JND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92441608001
2658359SAMPLE DUPLICATE:
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%8993
4-Bromofluorobenzene (S)%99100
Toluene-d8 (S)%100105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
492975
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2657365
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 08/19/19 21:55
1,2-Dichlorobenzene mg/kg ND 0.33 08/19/19 21:55
1,3-Dichlorobenzene mg/kg ND 0.33 08/19/19 21:55
1,4-Dichlorobenzene mg/kg ND 0.33 08/19/19 21:55
1-Methylnaphthalene mg/kg ND 0.33 08/19/19 21:55
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 08/19/19 21:55
2,4,5-Trichlorophenol mg/kg ND 0.33 08/19/19 21:55
2,4,6-Trichlorophenol mg/kg ND 0.33 08/19/19 21:55
2,4-Dichlorophenol mg/kg ND 0.33 08/19/19 21:55
2,4-Dimethylphenol mg/kg ND 0.33 08/19/19 21:55
2,4-Dinitrophenol mg/kg ND 1.7 v108/19/19 21:55
2,4-Dinitrotoluene mg/kg ND 0.33 08/19/19 21:55
2,6-Dinitrotoluene mg/kg ND 0.33 08/19/19 21:55
2-Chloronaphthalene mg/kg ND 0.33 08/19/19 21:55
2-Chlorophenol mg/kg ND 0.33 08/19/19 21:55
2-Methylnaphthalene mg/kg ND 0.33 08/19/19 21:55
2-Methylphenol(o-Cresol)mg/kg ND 0.33 08/19/19 21:55
2-Nitroaniline mg/kg ND 1.7 08/19/19 21:55
2-Nitrophenol mg/kg ND 0.33 08/19/19 21:55
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 08/19/19 21:55
3,3'-Dichlorobenzidine mg/kg ND 1.7 08/19/19 21:55
3-Nitroaniline mg/kg ND 1.7 08/19/19 21:55
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 08/19/19 21:55
4-Bromophenylphenyl ether mg/kg ND 0.33 08/19/19 21:55
4-Chloro-3-methylphenol mg/kg ND 0.66 08/19/19 21:55
4-Chloroaniline mg/kg ND 1.7 08/19/19 21:55
4-Chlorophenylphenyl ether mg/kg ND 0.33 08/19/19 21:55
4-Nitroaniline mg/kg ND 0.66 08/19/19 21:55
4-Nitrophenol mg/kg ND 1.7 08/19/19 21:55
Acenaphthene mg/kg ND 0.33 08/19/19 21:55
Acenaphthylene mg/kg ND 0.33 08/19/19 21:55
Aniline mg/kg ND 0.33 08/19/19 21:55
Anthracene mg/kg ND 0.33 08/19/19 21:55
Benzo(a)anthracene mg/kg ND 0.33 08/19/19 21:55
Benzo(a)pyrene mg/kg ND 0.33 08/19/19 21:55
Benzo(b)fluoranthene mg/kg ND 0.33 08/19/19 21:55
Benzo(g,h,i)perylene mg/kg ND 0.33 08/19/19 21:55
Benzo(k)fluoranthene mg/kg ND 0.33 08/19/19 21:55
Benzoic Acid mg/kg ND 1.7 v108/19/19 21:55
Benzyl alcohol mg/kg ND 0.66 08/19/19 21:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2657365
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 08/19/19 21:55
bis(2-Chloroethyl) ether mg/kg ND 0.33 08/19/19 21:55
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 08/19/19 21:55
Butylbenzylphthalate mg/kg ND 0.33 08/19/19 21:55
Chrysene mg/kg ND 0.33 08/19/19 21:55
Di-n-butylphthalate mg/kg ND 0.33 08/19/19 21:55
Di-n-octylphthalate mg/kg ND 0.33 08/19/19 21:55
Dibenz(a,h)anthracene mg/kg ND 0.33 08/19/19 21:55
Dibenzofuran mg/kg ND 0.33 08/19/19 21:55
Diethylphthalate mg/kg ND 0.33 08/19/19 21:55
Dimethylphthalate mg/kg ND 0.33 08/19/19 21:55
Fluoranthene mg/kg ND 0.33 08/19/19 21:55
Fluorene mg/kg ND 0.33 08/19/19 21:55
Hexachloro-1,3-butadiene mg/kg ND 0.33 08/19/19 21:55
Hexachlorobenzene mg/kg ND 0.33 08/19/19 21:55
Hexachlorocyclopentadiene mg/kg ND 0.33 08/19/19 21:55
Hexachloroethane mg/kg ND 0.33 08/19/19 21:55
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 08/19/19 21:55
Isophorone mg/kg ND 0.33 08/19/19 21:55
N-Nitroso-di-n-propylamine mg/kg ND 0.33 08/19/19 21:55
N-Nitrosodimethylamine mg/kg ND 0.33 08/19/19 21:55
N-Nitrosodiphenylamine mg/kg ND 0.33 08/19/19 21:55
Naphthalene mg/kg ND 0.33 08/19/19 21:55
Nitrobenzene mg/kg ND 0.33 08/19/19 21:55
Pentachlorophenol mg/kg ND 1.7 08/19/19 21:55
Phenanthrene mg/kg ND 0.33 08/19/19 21:55
Phenol mg/kg ND 0.33 08/19/19 21:55
Pyrene mg/kg ND 0.33 08/19/19 21:55
2,4,6-Tribromophenol (S)%90 27-110 08/19/19 21:55
2-Fluorobiphenyl (S)%75 30-110 08/19/19 21:55
2-Fluorophenol (S)%69 13-110 08/19/19 21:55
Nitrobenzene-d5 (S)%77 23-110 08/19/19 21:55
Phenol-d6 (S)%73 22-110 08/19/19 21:55
Terphenyl-d14 (S)%98 28-110 08/19/19 21:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2657366LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.7 73 52-130
1,2-Dichlorobenzene mg/kg 1.31.7 77 51-130
1,3-Dichlorobenzene mg/kg 1.31.7 77 50-130
1,4-Dichlorobenzene mg/kg 1.31.7 76 49-130
1-Methylnaphthalene mg/kg 1.31.7 79 55-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2657366LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.61.7 98 30-130
2,4,5-Trichlorophenol mg/kg 1.31.7 76 55-130
2,4,6-Trichlorophenol mg/kg 1.31.7 79 57-130
2,4-Dichlorophenol mg/kg 1.21.7 73 56-130
2,4-Dimethylphenol mg/kg 1.21.7 72 51-130
2,4-Dinitrophenol mg/kg 5.88.3 69 27-133
2,4-Dinitrotoluene mg/kg 1.11.7 68 61-130
2,6-Dinitrotoluene mg/kg 1.31.7 76 60-130
2-Chloronaphthalene mg/kg 1.31.7 77 52-130
2-Chlorophenol mg/kg 1.41.7 82 54-130
2-Methylnaphthalene mg/kg 1.41.7 82 54-130
2-Methylphenol(o-Cresol)mg/kg 1.31.7 76 51-130
2-Nitroaniline mg/kg 2.33.3 70 51-130
2-Nitrophenol mg/kg 1.41.7 82 49-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.21.7 72 11-163
3,3'-Dichlorobenzidine mg/kg 2.53.3 74 10-132
3-Nitroaniline mg/kg 2.53.3 75 55-130
4,6-Dinitro-2-methylphenol mg/kg 3.03.3 92 47-142
4-Bromophenylphenyl ether mg/kg 1.61.7 97 59-130
4-Chloro-3-methylphenol mg/kg 2.33.3 69 55-130
4-Chloroaniline mg/kg 2.73.3 80 54-130
4-Chlorophenylphenyl ether mg/kg 1.31.7 76 58-130
4-Nitroaniline mg/kg 2.43.3 72 54-130
4-Nitrophenol mg/kg 4.3 v38.3 52 48-130
Acenaphthene mg/kg 1.41.7 84 60-130
Acenaphthylene mg/kg 1.41.7 86 60-130
Aniline mg/kg 1.31.7 81 43-130
Anthracene mg/kg 1.61.7 96 63-130
Benzo(a)anthracene mg/kg 1.61.7 99 59-130
Benzo(a)pyrene mg/kg 1.61.7 95 57-130
Benzo(b)fluoranthene mg/kg 1.61.7 96 54-130
Benzo(g,h,i)perylene mg/kg 1.51.7 91 59-130
Benzo(k)fluoranthene mg/kg 1.71.7 102 54-130
Benzoic Acid mg/kg 4.98.3 60 19-130
Benzyl alcohol mg/kg 2.43.3 73 50-130
bis(2-Chloroethoxy)methane mg/kg 1.41.7 86 54-130
bis(2-Chloroethyl) ether mg/kg 1.51.7 90 48-130
bis(2-Ethylhexyl)phthalate mg/kg 1.81.7 109 45-134
Butylbenzylphthalate mg/kg 1.81.7 107 46-138
Chrysene mg/kg 1.71.7 102 58-130
Di-n-butylphthalate mg/kg 1.51.7 90 60-130
Di-n-octylphthalate mg/kg 1.71.7 102 53-130
Dibenz(a,h)anthracene mg/kg 1.51.7 91 59-130
Dibenzofuran mg/kg 1.31.7 76 60-130
Diethylphthalate mg/kg 1.21.7 73 60-130
Dimethylphthalate mg/kg 1.31.7 79 60-130
Fluoranthene mg/kg 1.41.7 87 65-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2657366LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.31.7 77 63-130
Hexachloro-1,3-butadiene mg/kg 1.11.7 68 46-130
Hexachlorobenzene mg/kg 1.51.7 87 58-130
Hexachlorocyclopentadiene mg/kg 1.21.7 75 23-130
Hexachloroethane mg/kg 1.21.7 74 47-130
Indeno(1,2,3-cd)pyrene mg/kg 1.51.7 92 60-130
Isophorone mg/kg 1.21.7 70 49-130
N-Nitroso-di-n-propylamine mg/kg 1.31.7 81 47-130
N-Nitrosodimethylamine mg/kg 1.5 v11.7 90 45-130
N-Nitrosodiphenylamine mg/kg 1.71.7 100 59-130
Naphthalene mg/kg 1.41.7 87 55-130
Nitrobenzene mg/kg 1.21.7 71 49-130
Pentachlorophenol mg/kg 2.83.3 85 10-132
Phenanthrene mg/kg 1.61.7 96 62-130
Phenol mg/kg 1.51.7 88 46-130
Pyrene mg/kg 1.91.7 113 53-130
2,4,6-Tribromophenol (S)%96 27-110
2-Fluorobiphenyl (S)%77 30-110
2-Fluorophenol (S)%81 13-110
Nitrobenzene-d5 (S)%70 23-110
Phenol-d6 (S)%79 22-110
Terphenyl-d14 (S)%99 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2657367MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92432117012
2657368
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene mg/kg 1.7 69 18-13070 11.6ND 1.1 1.1
1,2-Dichlorobenzene mg/kg 1.7 72 14-13071 31.6ND 1.2 1.2
1,3-Dichlorobenzene mg/kg 1.7 73 12-13071 31.6ND 1.2 1.2
1,4-Dichlorobenzene mg/kg 1.7 71 10-13069 51.6ND 1.2 1.1
1-Methylnaphthalene mg/kg 1.7 72 12-13074 21.6ND 1.2 1.2
2,2'-Oxybis(1-chloropropane)mg/kg 1.7 92 10-13091 21.6ND 1.5 1.5
2,4,5-Trichlorophenol mg/kg 1.7 71 13-13074 31.6ND 1.2 1.2
2,4,6-Trichlorophenol mg/kg 1.7 73 17-13076 21.6ND 1.2 1.2
2,4-Dichlorophenol mg/kg 1.7 64 10-13067 41.6ND 1.1 1.1
2,4-Dimethylphenol mg/kg 1.7 32 10-13041 231.6ND 0.54 0.67
2,4-Dinitrophenol mg/kg 8.3 69 10-13070 18.2ND 5.7 5.8
2,4-Dinitrotoluene mg/kg 1.7 64 24-13068 41.6ND 1.1 1.1
2,6-Dinitrotoluene mg/kg 1.7 73 23-13075 21.6ND 1.2 1.2
2-Chloronaphthalene mg/kg 1.7 72 19-13074 21.6ND 1.2 1.2
2-Chlorophenol mg/kg 1.7 72 10-13074 11.6ND 1.2 1.2
2-Methylnaphthalene mg/kg 1.7 76 18-13078 11.6ND 1.3 1.3
2-Methylphenol(o-Cresol)mg/kg 1.7 46 10-13053 111.6ND 0.77 0.86
2-Nitroaniline mg/kg 3.3 72 17-13070 43.3ND 2.4 2.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2657367MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92432117012
2657368
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
2-Nitrophenol mg/kg 1.7 75 10-13078 31.6ND 1.2 1.3
3&4-Methylphenol(m&p
Cresol)mg/kg 1.7 48 10-13053 91.6ND 0.80 0.87
3,3'-Dichlorobenzidine mg/kg 3.3 43 10-130473.3ND 1.4J ND
3-Nitroaniline mg/kg 3.3 71 24-13074 33.3ND 2.3 2.4
4,6-Dinitro-2-methylphenol mg/kg 3.3 89 10-15290 03.3ND 3.0 2.9
4-Bromophenylphenyl ether mg/kg 1.7 92 29-13091 21.6ND 1.5 1.5
4-Chloro-3-methylphenol mg/kg 3.3 57 17-13060 43.3ND 1.9 2.0
4-Chloroaniline mg/kg 3.3 65 14-13069 53.3ND 2.1 2.3
4-Chlorophenylphenyl ether mg/kg 1.7 72 25-13074 11.6ND 1.2 1.2
4-Nitroaniline mg/kg 3.3 67 22-13068 23.3ND 2.2 2.2
4-Nitrophenol mg/kg v38.3 48 10-13051 38.2ND 4.0 4.1
Acenaphthene mg/kg 1.7 79 20-13081 11.6ND 1.3 1.3
Acenaphthylene mg/kg 1.7 82 25-13084 21.6ND 1.4 1.4
Aniline mg/kg 1.7 30 10-13037 201.6ND 0.49 0.60
Anthracene mg/kg 1.7 91 29-13093 11.6ND 1.5 1.5
Benzo(a)anthracene mg/kg 1.7 93 19-13093 11.6ND 1.5 1.5
Benzo(a)pyrene mg/kg 1.7 87 12-13088 01.6ND 1.4 1.4
Benzo(b)fluoranthene mg/kg 1.7 86 14-13088 21.6ND 1.4 1.4
Benzo(g,h,i)perylene mg/kg 1.7 85 10-13087 11.6ND 1.4 1.4
Benzo(k)fluoranthene mg/kg 1.7 92 14-13093 01.6ND 1.5 1.5
Benzoic Acid mg/kg 8.3 47 10-13046 18.2ND 3.9 3.8
Benzyl alcohol mg/kg 3.3 66 13-13067 13.3ND 2.2 2.2
bis(2-Chloroethoxy)methane mg/kg 1.7 77 16-13081 41.6ND 1.3 1.3
bis(2-Chloroethyl) ether mg/kg 1.7 85 11-13084 21.6ND 1.4 1.4
bis(2-Ethylhexyl)phthalate mg/kg 1.7 97 21-130100 21.6ND 1.6 1.6
Butylbenzylphthalate mg/kg 1.7 98 23-130101 21.6ND 1.6 1.7
Chrysene mg/kg 1.7 97 22-13097 11.6ND 1.6 1.6
Di-n-butylphthalate mg/kg 1.7 82 30-13083 01.6ND 1.4 1.4
Di-n-octylphthalate mg/kg 1.7 92 23-14292 01.6ND 1.5 1.5
Dibenz(a,h)anthracene mg/kg 1.7 85 10-13086 01.6ND 1.4 1.4
Dibenzofuran mg/kg 1.7 73 24-13074 11.6ND 1.2 1.2
Diethylphthalate mg/kg 1.7 70 26-13072 21.6ND 1.2 1.2
Dimethylphthalate mg/kg 1.7 76 22-13079 21.6ND 1.3 1.3
Fluoranthene mg/kg 1.7 79 33-13081 11.6ND 1.3 1.3
Fluorene mg/kg 1.7 74 22-13076 11.6ND 1.2 1.2
Hexachloro-1,3-butadiene mg/kg 1.7 63 13-13062 21.6ND 1.0 1.0
Hexachlorobenzene mg/kg 1.7 84 29-13082 31.6ND 1.4 1.3
Hexachlorocyclopentadiene mg/kg 1.7 69 10-13068 11.6ND 1.1 1.1
Hexachloroethane mg/kg 1.7 68 10-13067 31.6ND 1.1 1.1
Indeno(1,2,3-cd)pyrene mg/kg 1.7 84 10-13086 21.6ND 1.4 1.4
Isophorone mg/kg 1.7 65 13-13067 21.6ND 1.1 1.1
N-Nitroso-di-n-propylamine mg/kg 1.7 73 12-13075 11.6ND 1.2 1.2
N-Nitrosodimethylamine mg/kg v11.7 82 11-13078 61.6ND 1.4 1.3
N-Nitrosodiphenylamine mg/kg 1.7 93 15-13093 11.6ND 1.5 1.5
Naphthalene mg/kg 1.7 81 15-13083 11.6ND 1.3 1.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
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Page 49 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2657367MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92432117012
2657368
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Nitrobenzene mg/kg 1.7 66 12-13066 01.6ND 1.1 1.1
Pentachlorophenol mg/kg 3.3 78 10-13078 03.3ND 2.6 2.6
Phenanthrene mg/kg 1.7 92 27-13093 01.6ND 1.5 1.5
Phenol mg/kg 1.7 66 10-13069 21.6ND 1.1 1.1
Pyrene mg/kg 1.7 111 19-130111 11.6ND 1.8 1.8
2,4,6-Tribromophenol (S)%84 27-11084
2-Fluorobiphenyl (S)%71 30-11071
2-Fluorophenol (S)%60 13-11060
Nitrobenzene-d5 (S)%65 23-11063
Phenol-d6 (S)%62 22-11062
Terphenyl-d14 (S)%91 28-11091
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 50 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
492915
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92441608001, 92441608002, 92441608003, 92441608004, 92441608005, 92441608006, 92441608007,
92441608008
Parameter Units
Dup
Result QualifiersRPDResult
92441608001
2657089SAMPLE DUPLICATE:
Percent Moisture %14.6 114.7
Parameter Units
Dup
Result QualifiersRPDResult
92441723004
2657090SAMPLE DUPLICATE:
Percent Moisture %19.6 518.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 51 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1337041
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92441608003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3446100-1
Associated Lab Samples:92441608003
Matrix:Solid
Analyzed
Total Solids %0.00100 08/29/19 16:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3446100-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result QualifiersRPDResult
L1133141-01
R3446100-3SAMPLE DUPLICATE:
Total Solids %83.6 1.8385.1
REPORT OF LABORATORY ANALYSIS
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Page 52 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1336581
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples:92441608003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3446154-1
Associated Lab Samples:92441608003
Matrix:Solid
Analyzed
Chromium, Hexavalent mg/kg ND 1.00 08/30/19 15:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3446154-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 9.3610.0 93.6 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3446154-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1133262-05
R3446154-6
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 24.6 95.7 75.0-12591.5 4.4824.6ND 23.5 22.5
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3446154-7MATRIX SPIKE SAMPLE:
MSSpike
Result
L1133262-05
Chromium, Hexavalent mg/kg 10701140 93.5 75.0-125ND
Parameter Units
Dup
Result QualifiersRPDResult
L1132009-01
R3446154-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00ND
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
[phone]
Page 53 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
BATCH QUALIFIERS
Batch: 564670
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.[1]
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
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Huntersville, NC 28078
[phone]
Page 54 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
ANALYTE QUALIFIERS
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/03/2019 08:14 AM
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92441608
High Point Ballfield 5318-F
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92441608001 564525 564670GP-12 0-2'EPA 3050 EPA 6020
92441608002 564525 564670GP-12 2-4'EPA 3050 EPA 6020
92441608003 564525 564670DUP-3 EPA 3050 EPA 6020
92441608004 564525 564670GP-1 0-2'EPA 3050 EPA 6020
92441608005 564525 564670GP-1 2-4'EPA 3050 EPA 6020
92441608006 564525 564670GP-2 0-2'EPA 3050 EPA 6020
92441608007 564525 564670GP-9 0-2'EPA 3050 EPA 6020
92441608008 564525 564670GP-8 0-2'EPA 3050 EPA 6020
92441608001 564376 564498GP-12 0-2'EPA 7471 EPA 7471
92441608002 564376 564498GP-12 2-4'EPA 7471 EPA 7471
92441608003 564376 564498DUP-3 EPA 7471 EPA 7471
92441608004 564376 564498GP-1 0-2'EPA 7471 EPA 7471
92441608005 564376 564498GP-1 2-4'EPA 7471 EPA 7471
92441608006 564376 564498GP-2 0-2'EPA 7471 EPA 7471
92441608007 564376 564498GP-9 0-2'EPA 7471 EPA 7471
92441608008 564376 564498GP-8 0-2'EPA 7471 EPA 7471
92441608001 492975 493156GP-12 0-2'EPA 3546 EPA 8270E
92441608002 492975 493156GP-12 2-4'EPA 3546 EPA 8270E
92441608003 492975 493156DUP-3 EPA 3546 EPA 8270E
92441608004 492975 493156GP-1 0-2'EPA 3546 EPA 8270E
92441608005 492975 493156GP-1 2-4'EPA 3546 EPA 8270E
92441608006 492975 493156GP-2 0-2'EPA 3546 EPA 8270E
92441608007 492975 493156GP-9 0-2'EPA 3546 EPA 8270E
92441608008 492975 493156GP-8 0-2'EPA 3546 EPA 8270E
92441608001 493171 493182GP-12 0-2'EPA 5035A EPA 8260D
92441608002 493171 493182GP-12 2-4'EPA 5035A EPA 8260D
92441608003 493171 493182DUP-3 EPA 5035A EPA 8260D
92441608004 493171 493182GP-1 0-2'EPA 5035A EPA 8260D
92441608005 493171 493182GP-1 2-4'EPA 5035A EPA 8260D
92441608006 493171 493182GP-2 0-2'EPA 5035A EPA 8260D
92441608007 493171 493182GP-9 0-2'EPA 5035A EPA 8260D
92441608008 493171 493182GP-8 0-2'EPA 5035A EPA 8260D
92441608001 492915GP-12 0-2'ASTM D2974-87
92441608002 492915GP-12 2-4'ASTM D2974-87
92441608003 492915DUP-3 ASTM D2974-87
92441608004 492915GP-1 0-2'ASTM D2974-87
92441608005 492915GP-1 2-4'ASTM D2974-87
92441608006 492915GP-2 0-2'ASTM D2974-87
92441608007 492915GP-9 0-2'ASTM D2974-87
92441608008 492915GP-8 0-2'ASTM D2974-87
92441608003 1337041 1337041DUP-3 SM 2540 G SM 2540G
92441608003 1336581 1336581DUP-3 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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Page 57 of 57
APPENDIX F