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HomeMy WebLinkAboutMO-8166_36757_CA_MRP_20190729_Groundwater Monitoring ReportHighlands 7 \ Environmental Solutions, InC. 8410-D Falls of Neuse Road; Raleigh, NC 27615 Phone: 919-848-3155 / Fax: 919-848-4265 / www. highlandsenvironmental. com July 29, 2019 Ms. Trudy Beverly NCDENR — Mooresville Regional Office 610 East Center Ave., Suite 301 Mooresville, NC 28115 Subject: Submittal of July 2019 Groundwater Monitoring Report Amoco #9 — Monroe Oil Company; Concord, North Carolina NCDENR Incident #36757 Project #68027 Dear Ms. Beverly: On behalf of our client (EMC Insurance Companies and Monroe Oil Company), please find enclosed an original copy of our Groundwater Monitoring Report for the Amoco #9, located at 7810 Lyles Lane, in Concord, North Carolina. If there are any questions regarding this correspondence, or the project in general, please contact Joe Beaman at (919) 848-3155. Sincerely, Highlands Environmental Solutions, Inc. bri k Senior Environmental Scientist Enclosure cc: Ms. Suzie Gibson — EMC Insurance Companies Mr. Olin Furr — Monroe Oil Company File Senior GROUNDWATER MONITORING REPORT JULY 2019 Amoco #9 7810 Lyles Lane Concord, Cabarrus County, North Carolina 28027 NCDEQ Incident #36757 HES Project #: 68027 July 26, 2019 Prepared for: Mr. Olin Furr Monroe Oil Company 519 East Franklin Street Monroe, North Carolina 28112 Ms. Suzie Gibson EMC Insurance Companies P.O. Box 621210 Charlotte, NC 28262-0120 Prepared by: Highlands Environmental Solutions, Inc. 8410-D Falls of Neuse Road Raleigh, North Carolina 27615 Scientist ei J e Beaman, P.G., RSM Principal Geologist Environmental Solutions, Inc. Groundwater Monitoring Report — July 2019 Amoco #9; 7810 Lyles Lane; Concord, NC Paae i TABLE OF CONTENTS 1.0 BACKGROUND AND GENERAL SITE INFORMATION........................................................1 2.0 SITE INVESTIGATION............................................................................................................ 5 2.1 Monitoring Well Installation and Site Survey........................................................................5 2.2 Water Level Measurements................................................................................................. 6 2.3 Monitoring Well Sampling....................................................................................................6 3.0 DISCUSSION...........................................................................................................................8 4.0 CERTIFICATION AND LIMITATIONS...................................................................................10 Appendix A - Figures Figure 1 — Site Location Diagram Figure 2 — Topographic Location Diagram Figure 3 — Site Diagram Figure 4 — Water Table Surface Diagram — July 2019 Figure 5 — Benzene Isoconcentration Diagram — July 2019 Figure 6 — MTBE Isoconcentration Diagram — July 2019 Figure 7 — 2L Exceedance Diagram — July 2019 Appendix B - Tables Table 1 — Well Construction and Water Table Elevations Table 2 — Summary of Groundwater Analytical Data — Volatile Organics Table 2a — Summary of Groundwater Analytical Data — VPH Appendix C - Copy of Laboratory Analytical Data Report and Chain -of -Custody Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 1 1.0 BACKGROUND AND GENERAL SITE INFORMATION The Amoco #9 site is located at 7810 Lyles Lane in Concord, Cabarrus County, North Carolina. The site is currently identified with Cabarrus County parcel identification number 4589-92-4798. The property is owned by the Bermuda Company, and the UST systems are currently owned and operated by Monroe Oil Company (Monroe) as a convenience store and gasoline station. The McDonalds Corporation also operates a McDonald's restaurant on the subject property. The site location is depicted as Figure 1 and Figure 2, included in Appendix A. Monroe currently operates two UST systems at the subject site. UST #1 is a 25,000-gallon compartmentalized UST, which contains regular gasoline (15,000 gallon) and premium gasoline (10,000 gallon). UST #2 is a 3,000 single compartment UST, which contains diesel fuel. According to Monroe representatives, during the night of September 25, 2009, a school activity bus collided with Dispenser #1 located at the site. The collision resulted in damage to the dispenser system, which resulted in the release of gasoline. The gasoline was not released to the ground surface; instead, the fuel was released to secondary containment sumps associated with the UST system. The driver of the vehicle that collided with the fuel dispenser left the scene of the incident; however, the incident was witnessed by other individuals at the site and the owner of the vehicle was identified. Based on information provided by EMC Insurance Companies, the incident eyewitness identified the school activity bus as being from Mount Zion Christian Academy in Durham, North Carolina. During the incident, the released fuel entered the containment sumps beneath the fuel dispenser, and back - flowed into the secondary containment sumps located atop the USTs. Approximately 304 gallons of fuel were recovered from the secondary containment sumps; however, at least one of the containment sumps (atop the USTs) was cracked, which allowed the fuel to be released to the backfill within the UST basin. Following the completion of incident response activities, Monroe noted a discrepancy of approximately 296 gallons between the apparent volume of recovered fuel and the UST inventory. Monroe then contacted their insurance provider (EMC Insurance Companies). EMC contacted Highlands Environmental Solutions, Inc. (HES) on October 20, 2009, to provide environmental services to investigate the incident and to assess for residual petroleum impacts at the site. On behalf of Monroe Oil Company, HES prepared and submitted a UST-61 Release Notification Form to the NCDEQ for the incident on October 21, 2009. HES conducted a site check investigation, which included the collection of soil samples from several borings around the damaged fuel dispenser and UST basin. Field and laboratory data collected during soil sampling and subsequent analysis indicated the presence of petroleum -impacted soil/backfill material inside the UST basin. HES reported the results of the investigation in a Site Check Report submitted to the North Carolina Department of Environmental Quality (NCDEQ) on January 5, 2010. Following review of the Site Check Report, the NCDEQ sent a Notice of Regulatory Requirements (NORR) dated January 20, 2010, to Monroe Oil Company. HES personnel mobilized to the field on March 31, 2010, to address the issues presented within the NORR. Additional soil borings were advanced around the perimeter of the UST basin, at each submersible pump secondary containment sump, and under the previously damaged fuel dispenser. Soil samples collected during subsequent assessment activities were submitted for laboratory analysis of gasoline range organics (GRO), and diesel range organics (DRO). Selected soil samples collected around the perimeter of the UST basin were analyzed for volatile organic compounds (VOCs), and volatile petroleum hydrocarbons (VPH). During subsequent site assessment activities, HES also installed one groundwater monitoring well (MW-1) immediately downgradient of the UST basin, and collected a groundwater sample for analysis of VOCs, VPH, and lead. Free -product was detected on the water surface at a thickness of 0.09 feet in the groundwater monitoring well. VOCs and VPH were also detected in monitoring well MW-1 at concentrations above the North Carolina Groundwater Quality Standard (NCGWQS). VOCs were also detected in monitoring well MW-1 at concentrations above Gross Contamination Levels for Groundwater. GRO and DRO were detected in soil samples collected during environmental assessment activities at concentrations greater than the North Groundwater Monitoring Report - July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 2 Carolina State Action Limit in six, and three of the soil samples respectively. VOCs and/or semi -volatile organic compounds (SVOCs) were detected at concentrations greater than their respective Soil -to - Groundwater, Residential, and Industrial/Commercial North Carolina Maximum Soil Contaminant Concentrations (MSCCs) in four soil samples. On August 18, 2010, HES installed three additional groundwater monitoring wells (MW-2, MW-3, MW-4), and collected a groundwater sample from each well for analysis of VOCs, VPH, and lead. Free -product was not detected on the water surface of MW-2, MW-3, or MW-4. VOCs were detected in MW-2 and MW-3 at concentrations greater than their respective North Carolina Administrative Code Subchapter 2L Groundwater Quality Standards (NCAC 2L Standards). VPH and lead were not detected in MW-2, MW-3, and MW-4 at concentrations greater than their respective NCAC 2L Standards. On February 23 and 24, 2011, HES installed five additional groundwater monitoring wells (MW-1D, MW-5, MW-6, MW-7, and MW-8), and replaced monitoring well MW-1 with a two-inch EPA type II well. HES collected a groundwater sample from each well for analysis of VOCs, VPH, and lead. Also, on February 23 and 24, 2011, HES advanced four soil borings near the dispenser island adjacent to the UST basin (SB-1, SB-2, SB-3, and SB-4). One soil boring (SB-5) was advanced near the Northwest corner of the UST basin, and one soil boring (SB-6) was advanced near the Southwest corner of the UST basin. HES collected six soil samples (SB-1, SB-2, SB-3, SB-4, SB-5, and SB-6) for laboratory analysis of VOCs and VPH. To date, two active liquid petroleum hydrocarbons (LPH) recovery events have been performed at the site. The first recovery event was a manual (i.e. bailing) event performed on MW-1 on October 13, 2010. During this event, LPH was measured at a thickness of 0.07 feet. Approximately 22 gallons of liquid (product and groundwater) was recovered from monitoring well MW-1 during this event. All recovered liquids were containerized in a 55-gallon drum at the site. Following completion of the event, the thickness of LPH in the well demonstrated no measurable change. A second LPH recovery event (Aggressive Fluid Vapor Recovery - AFVR) was performed at the site on July 14, 2011. During the AFVR event, HES utilized a vacuum truck to recover liquids and vapor from the well. The wellhead was sealed to maximize vacuum pressures in the well, which enhanced the recovery of volatilized gasoline (i.e. vapors). During the recovery event, HES depressed the water table surface local to the well, to maximize LPH recovery. During the AFVR event, HES personnel monitored liquid levels in nearby monitoring wells, as well as, temperature, airflow, relative humidity, and the total concentration of VOCs in the effluent air stream from the vacuum truck. Monitoring well MW-1 was evacuated of liquid and the AFVR event was performed for approximately 8 hours. A total of 1,239 gallons of liquid (free product and groundwater) were removed from monitoring well MW-1. The purpose of this recovery event was to aggressively remove most of the liquid from the well, and to determine if LPH returned to the well following the event. On October 26 and 27, 2011, HES installed two additional groundwater monitoring wells (MW-9 and MW-10). HES collected a groundwater sample from each well at the site for laboratory analysis of VOCs, VPH, and lead. A two-inch passive skimmer was installed in MW-1 on April 11, 2012. At that time product thickness was measured at 0.08 feet prior to the installation of the passive skimmer. HES personnel have monitored the passive skimmer monthly since it was installed. The amount of liquid and product located in the collection chamber of the passive skimmer recorded each month is as follows: ■ May 25, 2012 - Approximately 8.0 inches of total liquid (product and water) were removed and approximately 0.1 inch of liquid in the chamber appeared to be product. ■ June 14, 2012 - Approximately 4.0 inches of total liquid (product and water) were removed and approximately 1.5 inches of the liquid appeared to be product. ■ July 20, 2012 - Approximately 8.0 inches of total liquid (product and water) were removed and approximately 1.5 inches of the liquid appeared to be product. Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 3 ■ August 16, 2012 - Approximately 8.0 inches of total liquid (product and water) were removed and approximately 1.25 inches of the liquid appeared to be product. ■ August 29, 2012 - Approximately 7.0 inches of total liquid (product and water) were removed and approximately 1.5 inches of the liquid appeared to be product. ■ September 17, 2012, approximately 8.0 inches of total liquid was removed (product and water) and approximately 1.5 inches of the liquid appeared to be product. ■ October 2, 2012, approximately 7.0 inches of total liquid was removed (product and water) and approximately 1.25 inches of the liquid appeared to be product. ■ November 8, 2012, approximately 8.0 inches of total liquid was removed (product and water) and approximately 1.5 inches of the liquid appeared to be product. ■ December 12, 2012, approximately 8.0 inches of total liquid was removed (product and water) and approximately 1.25 inches of the liquid appeared to be product. ■ March 14, 2013, approximately 8.0 inches of total liquid was removed (product and water) and approximately 1.5 inches of the liquid appeared to be product. ■ April 25, 2013, approximately 6.5 inches of total liquid was removed (product and water) and approximately 1.55 inches of the liquid appeared to be product. ■ May 29, 2013, approximately 5.0 inches of total liquid was removed (product and water) and approximately 2.0 inches of the liquid appeared to be product. ■ June 25, 2013, approximately 6.0 inches of total liquid was removed (product and water) and approximately 1.75 inches of the liquid appeared to be product. ■ July 25, 2013, approximately 4.5 inches of total liquid was removed (product and water) and approximately 1.5 inches of the liquid appeared to be product. ■ August 15, 2013, approximately 5.0 inches of total liquid was removed (product and water) and approximately 1.25 inches of the liquid appeared to be product. ■ September 18, 2013, approximately 6.0 inches of total liquid was removed (product and water) and approximately 1.5 inches of the liquid appeared to be product. ■ October 8, 2013, approximately 7.0 inches of total liquid was removed, and there did not appear to be product in the skimmer. ■ November 18, 2013, approximately 8.0 inches of total liquid was removed, and there did not appear to be product in the skimmer. ■ December 10, 2013, approximately 8.0 inches of total liquid was removed, and there did not appear to be product in the skimmer. ■ January 27, 2014, approximately 8.0 inches of total liquid was removed, and there did not appear to be product in the skimmer. ■ March 20-21, 2014, approximately 12 inches of total liquid was removed, and there did not appear to be product in the skimmer. Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 4 ■ September 25, 2014; approximately 12 inches of total liquid was removed, and there did not appear to be product in the skimmer. ■ June 2015: No recoverable product present within the passive skimmer. The passive skimmer was removed. On September 17, 2012, HES installed an additional groundwater monitoring well (MW-11). HES collected a groundwater sample from each well at the site for laboratory analysis of VOCs, VPH, and Lead. On February 20, 2019, HES installed three groundwater monitoring wells MW-1 R and MW-1 DR, (replacement wells for MW-1 and MW-1 D, respectively) s and MW-12. A site diagram depicting the locations of monitoring wells on site is depicted as Figure 3. Adjacent properties consist of commercial land uses and do not show evidence of impact by the subject release. All properties within 1500 feet of the site utilize municipal water supplies for potable water. Three water supply wells (used for irrigation purposes) are located within 1500 feet of the release area. The closest irrigation well is located approximately 90 feet Northwest of the UST basin, and has been out of service for approximately seven years. The other two irrigation wells are located more than 1000 feet to the Southeast of the site. Surface water bodies are not located within 250 feet of the release area. Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 5 2.0 SITE INVESTIGATION 2.1 Monitoring Well Installation and Site Survey Monitoring well MW-1 was installed on April 1, 2010. Probe Technologies (Probe) was subcontracted for well installation. The well installation location is depicted on Figure 3. MW-1 was installed to a total depth of 30 feet below the ground surface and was constructed as a one -inch well. The well was constructed of Schedule 40 PVC casing and manufactured well screen (25 feet). A sand filter pack was installed to a depth approximately two feet above the top of the well screen. The remaining annulus was backfilled with a neat Portland cement grout, and the well was completed with a flush -mount steel cover and locking cap. Monitoring wells MW-2, MW-3, and MW-4 were installed on August 18, 2010. HES again subcontracted Probe for drilling services. The well installation locations are depicted on Figure 3. The borings for these wells were advanced using the same methodology and extended to depths of 20 feet below ground surface. The monitoring wells were constructed of two-inch Schedule 40 PVC manufactured well screen (15 feet) and casing. A sand filter pack was installed to a depth approximately one foot above the top of the well screens. The remaining annulus was backfilled with concrete, and the wells were completed with a flush -mount steel covers and locking caps. Additional details regarding well construction are presented as Table 1, included in Appendix B. Monitoring wells MW-5, MW-6, MW-7, and MW-8 were installed between February 22, 2011, and February24, 2011. HES again contracted Probe for drilling services. The well installation locations are depicted on Figure 3. The borings for these wells were advanced using the same methodology and extended to depths of 20 feet below ground surface, with the exception of monitoring well MW-1 D, that extended to a depth of 40 feet below ground surface. Monitoring wells MW-5, MW-6, MW-7, and MW-8 were constructed of two-inch Schedule 40 PVC manufactured well screen (15 feet) and casing. A sand filter pack was installed to a depth approximately one foot above the top of the well screens. The remaining annulus was backfilled with a neat Portland cement grout, and the wells were completed with a flush -mount steel covers and locking caps. On February 23, 2011, monitoring well MW-1 was replaced and installed as two-inch well. Monitoring well MW-1 was installed to a depth of 20 feet below ground surface and constructed of two-inch Schedule 40 PVC manufactured well screen (15 feet) and casing. A sand filter pack was installed to a depth approximately one foot above the top of the well screen. The remaining annulus was backfilled with concrete, and the wells were completed with a flush -mount steel cover and locking cap. Monitoring well MW-1 D was installed as an EPA Type III telescoping well on February 23, 2011. The well was constructed of thirty feet of four -inch Schedule 40 PVC surface casing and grouted in -place. The grout was allowed to cure for twelve hours prior to installing the one -inch Schedule 40 PVC. The one -inch PVC was installed to forty feet below grade, and MW-1 D was constructed with five feet of Schedule 40 pre -packed well screen. A sand filter pack was installed to a depth approximately one foot above the top of the well screen. A bentonite seal was installed atop the well screen to a depth of twenty-five feet below grade. The remaining annulus was backfilled with a neat Portland cement grout, and the well was completed with a flush -mount steel cover and locking cap. Monitoring wells MW-9 and MW-10 were installed on October 26, 2011. HES again contracted Probe for drilling services. The well installation locations are depicted on Figure 3. The borings for these wells were advanced using the same methodology and extended to depths of 20 feet below ground surface. Monitoring wells MW-9 and MW-10 were constructed of two-inch Schedule 40 PVC manufactured well screen (15 feet) and casing. A sand filter pack was installed to a depth approximately one foot above the top of the well screens. The remaining annulus was backfilled with a neat Portland cement grout, and the wells were completed with a flush -mount steel covers and locking caps. Monitoring well MW-11 was installed on September 17, 2012. HES again contracted Probe for drilling services. The well installation location is depicted on Figure 3. The boring for monitoring well MW-11 was advanced using the same methodology and extended to a depth of 44.0 feet below the ground surface. Monitoring well MW-11 was constructed of two-inch Schedule 40 PVC manufactured well screen (20 feet) and casing. A sand filter pack was installed to a depth approximately one foot above the top of the well screens. Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 6 The remaining annulus was backfilled with a neat Portland cement grout, and the well was completed with a flush -mount steel cover and locking cap. Monitoring wells MW-1 R, MW-1 DR, and MW-12 were installed on February 20, 2019. Wells MW-1 R and MW- 1 DR were replacement wells for monitoring wells MW-1 and MW-1 D (respectively that were previously damaged. HES again contracted IET for drilling services. The well installation location is depicted on Figure 3. The boring for monitoring well MW-1 R was advanced using the same methodology and extended to a depth of 20.0 feet below the ground surface. MW-12 was advanced using the same methodology and extended to a depth of 17.0 feet below the ground surface. Monitoring well MW-1 DR was installed as an EPA Type III telescoping well on February 20, 2019. MW-1 DR was constructed of forty feet of four -inch Schedule 40 PVC surface casing and grouted in -place. The grout was allowed to cure for twelve hours prior to installing the two-inch Schedule 40 PVC. The two-inch PVC was installed to thirty-five feet below grade, and MW-1 D was constructed with five feet of Schedule 40 pre -packed well screen. Monitoring well MW-1 R was constructed of two-inch Schedule 40 PVC manufactured well screen (20 feet) and casing. Monitoring well MW- 12 was constructed of two-inch Schedule 40 PVC manufactured well screen (17 feet) and casing. A sand filter pack was installed to a depth approximately one foot above the top of the well screens. The remaining annulus was backfilled with a neat Portland cement grout, and the well was completed with a flush -mount steel cover and locking cap. Following completion of well construction, the depth to liquid in each well was determined using a Testwell Oil/Water Interface Meter. The well volume was calculated, and the wells were developed by the use of bailers. All recovered liquids were visually examined for the presence of free -product and/or hydrocarbon sheens. Free product was not observed in any of the wells on site, and all liquids generated during well development were discharged to paved areas on the property, in accordance with NCDEQ regulations. The wells were allowed to recover for two hours before sampling. All monitoring well locations are depicted on Figure 3. 2.2 Water Level Measurements The July 2019 groundwater monitoring activities were performed at the site on July 11, 2019. Monitoring well MW-9 was gauged and sampled on Jul 17, 2019 (the well was not accessible during July 11 sampling event. During the groundwater monitoring event, monitoring wells MW-7 and MW-8 were found to be damaged and could be neither gauged nor sampled. The damage appeared to have occurred during site repaving activities. Depth -to -liquid data were collected from the remaining monitoring wells at the site. An electronic oil -water interface probe was utilized to collect the depth -to -liquid data, and all depth -to -liquid measurements were referenced to the top of each well casing. The oil -water interface probe was cleaned between each use, and the least impacted wells were checked first, while the two most impacted wells were checked last. Water level data were utilized to create a graphical representation of the water table surface in the surficial aquifer (Figure 4). Depth -to -liquid and well construction data are summarized on Table 1 (in Appendix B). 2.3 Monitoring Well Sampling During the July 11, 2019 monitoring event, groundwater samples were collected from monitoring wells MW- 1 R, MW-1 DR, MW-2, MW-3, MW-4, MW-5, MW-6, MW-9 (sampled on July 17, 2019), MW-10, MW-11, and MW-12. As noted earlier, monitoring wells MW-7 and MW-8 were unable to be sampled during the sampling event due to apparent damage. Using the depth -to -water and total -well -depth data, the well -volumes of each monitoring well were calculated, and three times that volume was to be removed prior to sampling each well in order to collect a current representative groundwater sample. HES personnel used new, non -reactive sampling gloves, a new dedicated disposable bailer, and new nylon rope in each of the wells during purging. After removing three well -volumes of water or bailing the wells dry three times (whichever occurred first), the groundwater samples were collected from each well. To collect the groundwater sample, the dedicated bailer was carefully lowered to a depth just beneath the water level in the well. The bailer was allowed to fill, and then the bailer was recovered. The groundwater samples were placed in labeled, pre -preserved, laboratory - supplied containers, maintained on ice, and transferred to a courier for a North Carolina -certified laboratory (Con -test Analytical Laboratories — ConTest, NC Certification #652). The courier then shipped the samples Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 7 under proper chain -of -custody protocol to the laboratory for analysis of VOCs, by Method 6200D; and VPH by the MADEP Method. Laboratory analytical data for groundwater samples collected on July 11, 2019, are summarized on Table 2 and Table 2a. A copy of the complete laboratory analytical data report for the July 2019 sampling event is included in Appendix C. Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 8 3.0 DISCUSSION The Amoco #9 site is a retail gasoline and convenience store located at 7810 Lyles Lane, in Concord, Cabarrus County, North Carolina. A petroleum release occurred at the site in September 2009, due to a third -party motor vehicle colliding with a petroleum dispenser at the site (dispenser #1). The third party has been identified, and EMC Insurance is investigating the identified third party for insurance coverage. The subject site is zoned and utilized for commercial use. Adjacent properties are zoned and utilized for commercial land uses. Underground utilities are located on site. Underground utilities (piping and electrical lines) associated with the UST systems transect the UST basin at the site. Public utilities observed in the area of the property included electrical, telephone, cable television and public water and sewer service, however, these utilities do not transect the petroleum -impacted area of the site. Surface water bodies are not located within a 250-foot radius of the site. The closest surface water feature is a drainage ditch situated approximately 360 feet northwest of the UST basin. The property slopes to the south, therefore, stormwater from the site and adjacent properties would be expected to flow towards the south. The surface water body was neither impacted nor significantly threatened by the subject release. The site is not located within a wellhead protection area. One water supply well, formerly used for irrigation purposes, is located within 250 feet of the UST basin. Based on information provided by the owner of this well, the well is damaged and not currently in service. No other water supply wells were identified within 1000 feet of the site. The subject site and all adjacent properties utilize public water supplies for potable water. Groundwater in the shallow aquifer beneath the site has historically been inferred to flow predominantly toward the south. However, water level data suggests the water table beneath the Amoco #9 property itself is locally influenced. This is most likely due to natural and/or manmade structures in the subsurface. Local mounding of the water table near the UST basin is not considered to be unusual, given the differences between the hydraulic conductivity and porosity of the UST basin backfill materials, and the native soil at the site. A total of eleven monitoring wells have been installed at the site, to include eleven EPA Type II), and one EPA Type III monitoring wells. The most recent groundwater monitoring event was completed on July 11, 2019. During this event, one groundwater sample was collected from each monitoring well at the site utilizing disposable bailers, with the exception of MW-7 MW-8 which were damaged. During the most recent monitoring event, none of the monitoring wells contained any free product. During the July 2019 monitoring event, several dissolved phase petroleum constituents were detected in site monitoring wells at concentrations greater than their respective NCAC 2L Standard as follows: MW-1 R — VOCs - Benzene at 270 ug/L - Ethylbenzene at 700 ug/L - Isopropylbenzene at 98 ug/L - Naphthalene at 320 ug/L - n-Propylbenzene at 130 ug/L - 1,2,4-Trimethylbenzene at 860 ug/L - Xylenes at 2600 ug/L - C5-C8 Aliphatics at 2600 ug/L - C9-C10 Aromatics at 4200 ug/L MW-1 DR — VOCs - Acetone at 1200ug/L - Benzene at 1.3 ug/L - MTBE at 27 ug/L Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 9 • MW-10 — VOcs - MTBE at 35 ug/L Historically, the bulk of the dissolved -phase petroleum plume in groundwater beneath the site is situated on the Amoco #9 site in the vicinity of the initial spill area, with the geometry of the plume being enlarged toward the South and Southeast. A diagram depicting the benzene and MTBE plumes are included as Figure 5 and 6, respectively. Additionally, a diagram depicting NCAC 2L Standard exceedances is included as Figure 7. HES prepared and submitted a Corrective Action Plan (CAP) for this site. This CAP has been reviewed and approved by the NCDEQ — Mooresville Regional Office. The technology to be utilized at the site is an approved technology. An agreement with the property owner (The Bermuda Corporation) is being negotiated for the implementation of the CAP. HES recommends the following: • Implementation of the proposed CAP. • Continued semi-annual groundwater monitoring. The site has been assigned a "high" risk ranking due to the presence of a former irrigation well within 250 feet of the source area. This well is out of service, and was sampled during the December 2018 sampling event, with no detectable concentrations of petroleum hydrocarbons. If this well was properly abandoned, then the site would qualify as "low" risk, and the incident could receive regulatory closure via a Notice of Residual Petroleum on the property. Groundwater Monitoring Report — July 2019 Monroe Oil Company; 7810 Lyles Lane; Concord, NC Page 10 4.0 CERTIFICATION AND LIMITATION Highlands Environmental Solutions, Inc. (HES) has performed the investigation documented in this report in a professional manner using generally accepted professional practices. This report shall not be construed to create any warranty regarding the property on which the investigation was conducted. This report is a representation and presentation of the findings and conclusions of HES based upon observations made at the time of site reconnaissance visits; personal interviews; research of available documents (records, maps, etc.) held by the appropriate government and private agencies; and and/or analytical data for samples collected during the course of the investigation. This report is subject to the limitation of historical documentation, and the availability and accuracy of pertinent records. HES shall not be responsible for conditions, or consequences, arising from relevant facts that were concealed, withheld or not fully disclosed to HES at the time the investigation was performed. The scope of work for this investigation was not sufficient, nor intended, to: Fully assess the extent of contaminated media at the site; develop or implement a remedial action plan for the site; or to fully assess the risk posed by contaminated media at the site. This report is intended solely for the use of Monroe Oil Company, Inc.; EMC Insurance Companies, Inc.; the North Carolina Department of Environmental Quality; their agents; and consultants. The information provided in this report is relevant to the dates of our site and research activities and should not be relied upon to represent conditions at future dates. With reference to applicable technical requirements, I certify that the work described herein has been performed in accordance with industry standards and practices by me, or under my direct supervision. Highlands Environmental Solutions, Inc. Bobby J. Beaman, P.G., RSM Principal Geologist NC Licensed Geologist #1468 Appendix A r� r� i Concord Regional Airport -85 Exit 1-85 Exit Approximate Scale 0 0.5 miles Base diagram from Microsoft Streets and Trips Plus Highlands Environmental Solutions, Inc. I Site Location I Rocky River Golf Club 1.0 Concord Charlotte Motor Speedway f 4 T Incident Location Diagram Project Name Groundwater Monitoring Report Monroe Oil Company Site; Concord, NC Client EMC Insurance / Monroe Oil Company Project # Drawn by 68027 BF Scale Date Fig. # As Shown July 2019 1 {a} f\ �; I � � '� '� 1 • ice; � f ti k V IL f t F Site Location T `" - rr•. +� } � "f 111 , I 1 le Up di mum 7tj� F k r - � - � J'y r i r J y L �s.{y i t , 1 - � ` r-z�+ } F• r � � ti r~ rz � '�•p � 4 Approximate Scale 0 0.75 miles IBase diagram from1984 Mallard Creek USGS 7.5 Minute Topographic Map Highlands Environmental Solutions, Inc. Project Name 1.5 Topographic Diagram T Groundwater Monitoring Report Monroe Oil Company Site; Concord, NC Client EMC Insurance / Monroe Oil Company Project # Drawn by 68027 BF Scale Date Fig. # As Shown July 2019 2 Appendix B Table 1 Well Construction and Liquid Level Data Monroe Oil Company / Amoco #9 Concord, North Carolina HES Job Number -68027 Well ID Date Installed Well Casing Depth (ft. BGS) Screened Interval (f[. BGS) Depth of Well (ft. BGS) Top of Casing Elevation (ft. MSL) Date Water Level Measured Depth to Water from Top of Casing (ft.) Free Pduct Thicrokness (ft.) Groundwater Elevation (ft. above MSL) Comments MW-1 3I31I10 30' 10-30 30.0 198.95 8120/10 12.30 0.09 186.73 10/13/10 11.35 0.07 187.66 311111 12.64 0.08 186.38 7/13/11 13.01 0.05 185.98 7115/11 13.61 0.05 185.38 10/26/11 11.69 0.08 187.33 6114/12 13.68 0.08 185.34 8/29/12 12.72 0.02 186.25 3113/13 13.05 0.02 185.92 7/25/13 13.19 0.02 185.77 10/16/13 12.21 0.00 186.74 Sheen on water in skimmer 11/25/13 11.48 0.00 187.47 No product in skimmer 12/19/13 11.72 0.00 187.23 No product in skimmer 1/2114 12.14 0.00 186.81 No product in skimmer 2/18/14 10.49 0.00 188.46 No product in skimmer 3/21/14 10.36 0.00 188.59 No product in skimmer 9125/14 12.08 0.00 186.87 No product in skimmer 6/30/15 13.28 0.00 185.67 No product in skimmer 6130/16 12.19 0.00 186.76 No product in skimmer 1/13/17 11.25 0.00 187.70 7127/17 13.06 0.00 185.89 3/20/18 nm nm nm Well Damaged Unable to Sample 7119/18 nm nm nm Well Damaged Unable to Sample 12/18/18 nm nm nm Well Damaged Unable to Sample MW-1R 2/20/19 20 10-20 20 198.55 7111/19 11.56 0.00 186.99 replacement well for MW-1 MW-2 8118/10 20' 5-20 20.0 199.84 8120/10 14.29 0.00 185.55 10/13/10 12.64 0.00 187.20 3/ 1 /11 14.51 0.00 185.33 7/13/11 14.67 0.00 185.17 7115/11 14.85 0.00 184.99 10/26/11 13.83 0.00 186.01 6114/12 14.13 0.00 185.71 8/29/12 14.58 0.00 185.26 3113/13 14.22 0.00 185.62 7/25/13 13.67 0.00 186.17 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 1/2114 nm nm nm 2/18/14 nm nm nm 3/21/14 10.98 0.00 188.86 9125/14 14.30 0.00 185.54 6/30/15 11.22 0.00 188.62 6130/16 13.88 0.00 185.96 1/13/17 14.23 0.00 185.61 7127/17 14.70 0.00 185.14 3/20/18 10.31 0.00 189.53 7119/18 14.65 0.00 185.19 12/18/18 6.55 0.00 193.29 7111/19 11.77 0.00 188.07 Notes: "ft BGS"= Feet Below Ground Surface "ft MSL" = Feet above Mean Sea Level "nm= not measured All elevah'ons are referenced to a benchmark of assumed elevation 10.00 ft. MSL established at the site. 1 of 5 Table 1 (cont'd) Well ID Date Installed Well Casing De th p (f[. BGS) Screened Interval (ft. BGS ) Depth of Well (k. BGS) Top o Casing Elevation (ft. MSL) Date Water Level Measured Depth to Water from Top of Casing (k.) Free Product Thickness (f[ Groundwater Elevation (ft. above MSL.) ) Comments MW-3 8/18/10 20' 5-20 20.0 197.04 8/20/10 13.01 0.00 184.03 10/13/10 12.85 0.00 184.19 3/ 1 /11 14.31 0.00 182.73 7113/11 13.39 0.00 183.65 7/15/11 13.55 0.00 183.49 10/26/11 13.33 0.00 183.71 6/14/12 13.78 0.00 183.26 8129/12 13.16 0.00 183.88 3/13/13 14.95 0.00 182.09 7125/13 13.83 0.00 183.21 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 112114 nm nm nm 2118/14 nm nm nm 3121/14 14.60 0.00 182.44 9/25/14 13.19 0.00 183.85 6130/15 13.72 0.00 183.32 6/30/16 12.68 0.00 184.36 1112/17 14.26 0.00 182.78 7/27/17 14.07 0.00 182.97 3120/18 14.18 0.00 182.86 7/19/18 13.48 0.00 183.56 12/18/18 12.41 0.00 184.63 7/11/19 11.36 0.00 185.68 MW-4 8/18/10 20' 5-20 20.0 198.25 8120/10 13.15 0.00 185.10 10/13/10 13.67 0.00 184.58 311/11 15.40 0.00 182.85 7/13/11 13.55 0.00 184.70 7115/11 13.81 0.00 184.44 10/26/ 11 13.71 0.00 184.54 6114/12 13.73 0.00 184.52 8/29/12 13.48 0.00 184.77 3113/13 15.30 0.00 182.95 7/25/13 13.49 0.00 184.76 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 1/2114 nm nm nm 2/18/14 nm nm nm 3/21/14 14.68 0.00 183.57 9125/14 13.80 0.00 184.45 6/30/15 13.93 0.00 184.32 6130/16 13.49 0.00 184.76 1/12/17 15.00 0.00 183.25 7127/17 13.61 0.00 184.64 3/20/18 13.87 0.00 184.38 7119/18 13.32 0.00 184.93 12/18/18 13.00 0.00 185.25 7111/19 11.79 0.00 186.46 NOta3: "It tlUi = Feet tlelow U-rd S-- Tt MSL-= Feef above Mean Sea Level =notm ured All a/evab'ons are referenced fo a benchmark of assumed elevation 10.00 ff. MSL established at the site. 2 of Table 1 (cont'd) Well ID Date Installed Well Casing De Depth p (ft. BGS) Screened Interval (ft. BGS ) Depth of Well (ft. BGS) Top of Casing Elevation (ft. MSL) Date Water Level Measured Depth to Water from Top of Casing (ft.) Free Pduct Thicro Thickness (ft.) Groundwater Elevation (ft. above MSL ) Comments MW-ID 2/23/11 40' 35-40 40.0 198.77 311111 25.92 0.00 172.85 7113/11 26.35 0.00 172.42 7115/11 26.49 0.00 172.28 10/26/11 26.10 0.00 172.67 6114/12 32.41 0.00 166.36 8129/12 33.60 0.00 165.17 3113/13 31.06 0.00 167.71 7125/13 34.94 0.00 163.83 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 112114 nm nm nm 2/18/14 nm nm nm 3121/14 29.69 0.00 169.08 9125/14 25.70 0.00 173.07 6130/15 37.14 0.00 161.63 6130/16 35.01 0.00 163.76 1112/17 30.59 0.00 168.18 7127/17 37.43 0.00 161.34 3120/18 nm nm nm Well Damaged Unable to Sample 7119/18 nm nm nm Well Damaged Unable to Sample 12/18/18 nm nm nm Well Damaged Unable to Sample MW-1 DR 2/20/19 35 35-40 40.0 198.53 711/19 23.02 0.00 175.51 replacement well for MW-1D MW-5 2124/11 20' 5-20 20.0 197.27 3/1/11 14.10 0.00 183.17 7113/11 13.32 0.00 183.95 7/15/11 13.46 0.00 183.81 10/26/11 13.21 0.00 184.06 6/14/12 13.69 0.00 183.58 8129/12 13.11 0.00 184.16 3/13/13 14.78 0.00 182.49 7125/13 13.76 0.00 183.51 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 112114 nm nm nm 2118/14 nm nm nm 3121/14 13.70 0.00 183.57 9/25/14 13.07 0.00 184.20 6130/15 13.77 0.00 183.50 6/30/16 12.64 0.00 184.63 1112/17 13.95 0.00 183.32 7/27/17 13.56 0.00 183.71 3120/18 13.70 0.00 183.57 7/19/18 13.32 0.00 183.95 12/18/18 11.35 0.00 185.92 7/11/19 11.05 0.00 186.22 MW-6 2/24/11 20' 5-20 20.0 198.94 311111 15.42 0.00 183.52 7/13/11 15.63 0.00 185.48 7115/11 13.46 0.00 185.48 10/26/11 14.97 0.00 183.97 6114/12 15.48 0.00 183.46 8/29/12 15.11 0.00 183.83 3113/13 16.13 0.00 182.81 7/25/14 15.86 0.00 183.08 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 1/2114 nm nm nm 2/18/14 nm nm nm 3/21/14 13.84 0.00 185.10 9125/14 14.80 0.00 184.14 6/30/15 15.63 0.00 183.31 6130/16 14.47 0.00 184.47 1/12/17 14.67 0.00 184.27 7127/17 15.36 0.00 183.58 3/20/18 13.71 0.00 185.23 7119/18 14.92 0.00 184.02 12/18/18 9.57 0.00 189.37 7111/19 11.42 0.00 187.52 Notes: "ft BGS"= Feet Below Ground Surface "ft MSL" = Feet above Mean Sea Level "non= not measured All elevations are referenced to a benchmark of assumed elevation 10.00 ft. MSL established at the site. 3 of Table 1 tcont'dl Well ID Date Installed Well Casing Depth (ft. BGS) Screened Interval (f[. BGS) Depth of Well (ft. BGS) Top of Casing Elevation (ft. MSL) Date Water Level Measured Depth to Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft. above MSL) Comments MW-7 2/23/11 20' 5-20 20.0 199.74 3/1/11 16.54 0.00 183.20 7113/11 16.62 0.00 182.53 7/15/11 17.21 0.00 182.53 10/26/11 16.72 0.00 183.02 6/14/12 14.70 0.00 185.04 8129/12 14.62 0.00 185.12 3/13/13 15.80 0.00 183.94 7125/13 13.78 0.00 185.96 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 112114 nm nm nm 2118/14 nm nm nm 3121/14 12.64 0.00 187.10 9/25/14 11.23 0.00 188.51 6130/15 13.28 0.00 186.46 6/30/16 6.68 0.00 193.06 1112/17 13.23 0.00 186.51 7/27/17 14.39 0.00 185.35 3120/18 nm nm Nm Well Damaged Unable to Sample 7/19/18 nm nm Nm Well Damaged Unable to Sample 12/18/18 nm nm Nm Well Damaged Unable to Sample 7/11/19 nm nm Nm Well Damaged Unable to Sample MW-8 2/23/11 20' 5-20 20.0 197.92 311111 13.93 0.00 183.99 7/13/11 13.07 0.00 184.85 7115/11 13.22 0.00 184.70 10/26/11 13.02 0.00 184.90 6114/12 11.80 0.00 186.12 8/29/12 12.80 0.00 185.12 3113/13 14.21 0.00 183.71 7/25/13 13.50 0.00 184.42 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 1/2114 nm nm nm 2/18/14 nm nm nm 3/21/14 Dry Dry Dry 9125/14 well Damaged Unable to Sample 6/30/15 6130/16 1/12/17 7127/17 3/20/18 7119/18 12/18/18 7111/19 MW-9 10/26/11 20' 5-20 20.0 200.34 10/26/11 17.30 0.00 183.04 6114/12 17.46 0.00 182.88 8/29/12 16.97 0.00 183.37 3113/13 18.41 0.00 181.93 7/25/13 17.54 0.00 182.80 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 1/2114 nm nm nm 2/18/14 nm nm nm 3/21/14 17.46 0.00 182.88 9125/14 16.58 0.00 183.76 6/30/15 17.31 0.00 183.03 6130/16 16.09 0.00 184.25 1/12/17 17.49 0.00 182.85 7127/17 17.53 0.00 182.81 3/20/18 17.92 0.00 182.42 7119/18 17.71 0.00 182.63 12/18/18 16.06 0.00 184.28 7115/19 15.08 0.00 185.26 Notes: "R BGS" = Feet Below Ground Surface "ft MSL" = Feet above Mean Sea Level "nm= not measured All elevations are referenced to a benchmark of assumed elevation 10.00 ft. MSL established at the site. 4 of Table 1 (cont'd) Well ID Date Installed Well Casing Depth (ft. BGS) Screened Interval (f[. BGS) Depth of Well (ft. BGS) Top of Casing Elevation (ft. MSL) Data Water Level Measured Depth to Top of Casing (ft.) Free Product Thickness (ft.) Groundwater Elevation (ft. above MSL) Comments MW-10 10/26/11 20' 5-20 20.0 198.09 10/26/11 16.38 0.00 181.71 6114/12 13.57 0.00 184.52 8/29/12 12.80 0.00 185.29 3113/13 14.61 0.00 183.48 7/25/13 13.51 0.00 184.58 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 1/2114 nm nm nm 2/18/14 nm nm nm 3/21/14 14.19 0.00 183.90 9125/14 12.50 0.00 185.59 6/30/15 13.33 0.00 184.76 6130/15 12.02 0.00 186.07 1/12/17 14.59 0.00 183.50 7127/17 13.35 0.00 184.74 3/20/18 nm nm nm Well Damaged Unable to Sample 7119/18 13.18 0.00 184.91 12/18/18 12.69 0.00 185.40 7111/19 10.64 0.00 187.45 MW-11 9/17/2012 44' 24-44 44.0 194.84 9/17/12 29.42 0.00 165.42 3113/13 29.95 0.00 164.89 7/25/13 29.04 0.00 165.80 10/16/13 nm nm nm 11/25/13 nm nm nm 12/19/13 nm nm nm 1/2114 nm nm nm 2/18/14 nm nm nm 3/21/14 28.20 0.00 166.64 9125/14 28.28 0.00 166.56 6/30/15 28.30 0.00 166.54 6130/16 27.51 0.00 167.33 1/12/17 27.52 0.00 167.32 7127/17 27.98 0.00 166.86 3/20/18 27.90 0.00 166.94 7/19/18 28.15 0.00 166.69 12/18/18 26.98 0.00 167.86 7111/19 26.35 0.00 168.49 MW-12 2/20/2019 17 10-17 17.0 196.39 7/11/19 10.32 0.00 186.07 Notes: "t BGS"= Feet Below Gnnmd surface 9f MSL" = Feet above Mean Sea Level = not measured All elevations are referenced to a benchmark orassumed elevation 10.00 R. MSL established at the site. 50f5 Table 2 Groundwater Monitoring Report Monroe Oil Company; Concord, NC HES Project # 68027 Summary of Groundwater Analytical Data (VOCS) Analytical Method Volatile Organic Compounds Contaminate of Concern (ugA4 a' m d N E ° O m O c N m C y N N rN, W O U d q E O E O O _° U E ° y L E ° U0 O N n - C Y o 5, cS K co N y Oa N y C iO . L L d O CCy °, N r2 LU W M T y y O N a L Uo i L m« L Ao Z aW o Il C L E o m LN tCNC ~ N c >` E ~ a c dN� ESam ~ N XT aCQ O Eo u L R O Ol O Q le ID Date Collected 3/31/2010 na 13,200 ND na na 14,100 ND NO ND NO ND na 100,000 NO ND 21,900 na NO NO NO ND NO 33,500 55,500 ND 653,000 ND 373,000 105,000 726,000 ND 8/20/2010 na na NO na na na na na NO NO ND na na na na na na na ND na na na na na ND na NO na na na na 2/24/2011 NO 1,300 NO NO NO NO NO NO NO NO ND NO 2,400 NO NO 390 NO NO NO NO ND 690 3,300 540 ND 40,000 ND 5,700 1,500 26,300 ND 10/26/2011 na na NO na na na na na NO NO ND na na na na na ND na ND na na na na na ND na ND na na na na 8/29/2012 NO 58.2 J NO NO 90.7 J 70.7 J NO NO NO NO ND NO 1,720 NO ND 342 NO NO NO NO ND 382 J 857 583 ND 7,740 NO 7,170 2,020 23,800 ND 7/25/2013 NO ND NO NO 521 321 NO NO NO NO ND NO 2,150 NO NO 1,120 262 NO ND NO ND NO 2,000 2,000 ND 531 ND 13,900 3,950 29,100 NO 3/21/2014 NO 33 J NO NO 86 J 16 J NO NO NO NO NO NO 900 NO NO 180 17 J NO NO NO ND NO 350 270 ND 460 ND 3,900 1,000 11,200 NO MW-1 9/25/2014 NO 10 J NO NO 110 22 J NO NO NO NO NO NO 630 NO NO 200 20 J na ND NO na ND 370 L 320 na 55 ND 4,400 1,100 6,000 ND 6/30/2015 NO NO NO NO 200 38 NO NO NO NO ND NO 400 ND NO 58 40 NO ND NO ND NO 470 180 ND ND ND 5,400 1,300 2800 ND 6/30/2016 ND NO NO NO 16 9 ND NO ND NO ND NO 75 NO NO 48 8.6 NO ND NO ND NO 210 88 ND ND ND 1200 380 329 ND 1/1312017 NO 26 NO NO NO 13 ND NO NO NO ND NO 65 ND NO 55 14.0 NO ND NO ND NO 170 110 NO 8.2 NO 1600 470 196 NO 7/27/2017 NO 42 NO NO 110 16 J NO NO NO NO ND NO 49 ND NO 91 64.0 NO ND NO ND NO 220 120 NO NO NO 1500 300 52 NO 3/20/2018 DAMAGED 7/19/2018 12/18/2018 MW-1R 7/1112019 ND 270 NO NO 20 9.0 J NO NO NO NO NO NO 700 3.6 J ND 98 4.6 J NO ND 16 ND NO 320 130 ND 100 ND 860 270 2600 ND 3/1/2011 31 6 NO 4.5 1 0.27 NO NO NO NO NO 94 6.7 ND NO 1.8 0.37 9.3 ND ND ND NO 6.2 2.8 ND 39 ND 38 9.4 73 ND 10/26/2011 2.8 2.5 NO NO NO 0.11 NO 0.42 NO NO NO NO 1 0.14 NO 0.73 NO NO NO 8.7 NO NO 1.2 0.33 NO 0.23 ND 3.0 1.4 0.11 NO 9/5/2012 NO NO NO NO NO NO NO NO NO NO ND NO NO NO NO NO NO NO ND NO ND NO ND NO ND ND ND NO NO NO NO 7/25/2013 NO 3.2 NO NO NO NO NO NO NO ND ND NO NO NO ND NO ND NO ND 14.4 ND ND NO NO ND ND ND NO NO NO NO 3/31/2014 NO 2.7 NO NO NO 0.11 J NO NO NO ND ND NO NO 0.31 J ND NO ND NO ND 15 NO ND 0.13 J NO 0.61 ND NO NO NO NO NO 9/25/2014 6.1 J 3.4 NO NO NO NO NO NO NO NO NO NO NO 0.31 J ND NO ND na ND 19 na NO NO NO na ND ND NO NO NO NO MW-1D 6/30/2015 NO 5.1 NO NO NO NO NO NO NO NO NO NO NO 0.24J NO NO ND NO ND 13 ND NO NO NO NO ND NO NO NO NO NO 6/30/2016 NO 3.6 NO NO NO NO NO NO NO NO NO NO NO 1.00 NO NO ND NO ND 78 NO NO NO NO NO NO NO NO NO NO NO 1/13/2017 NO 6.5 NO NO NO NO NO NO NO NO NO NO NO 1.10 NO NO ND NO ND 84 NO NO NO NO NO NO NO 0.27 J NO 0.47 J NO 7/27/2017 NO NO NO NO NO NO NO NO NO NO ND NO NO 0.66 NO NO ND NO ND 27 NO NO NO NO NO NO NO 0.27 J NO 0.47 J NO 3/20/2018 DAMAGED 7/19/2018 12/18/2019 MW-1DR 7/11/2019 1200 1.3 NO 2.3 J NO NO NO NO NO NO ND ND 2.1 0.56 NO 0.71 ND NO NO 27 NO NO NO 0.44 J NO 5.7 ND 1.7 1.1 16.5 ND NCAC 2L Standard (ug/L) 6,000 1 none 4,000 70 70 70 3 70 70 4,000 550 70.00 280 70 none 20 100 20 none 5 6 70 none 600 0.2 400 400 500 CS NCDEQ GCL (ug/L) 6000000 5,000 none 4000000 6,900 8,500 15,000 3,000 70,000 70,000 none 84,500 70000 280,000 25,000 none 20,000 100,000 20,000 none 5,000 6,000 30,000 none 260,000 200 28,500 25,000 85,500 CS Notes: Bold indicates results above NCAC 2L Standard. Red denotes concentration greater than GCL. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit / Not Detected J = an estimated quantity that is between the method detection limit and the reporting limit L = Laboratory -fortified blank/Jaboratory control sample recovery and duplicate recovery are outside of control limits. Reported value is likely to be biased on the low side. nm = not measured na = not analyzed CS = Compound Specific ig/L = micrograms per liter Table 2 Groundwater Monitoring Report Monroe Oil Company; Concord, NC HES Project # 68027 Summary of Groundwater Analytical Data (VOCS) Analytical Method --I- Volatile Organic Compounds Contaminate of Concern (ug/L4 U m d A o :u O m C m N y m O N C N a C d A E U L L p O w W o. o. O N C 0 m O -5, y T C N C a O C y L V L W O W. m0. i= :r 1 'OLU O L L) a N A Z _ d E O O N NN m E C� m E _ x a 0 CcEUN.O ; MA JO iLQ�WUa' O °1 O Sample ID Date Collected 8/20/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND 7.94 ND 2.14 ND 50.7 ND ND ND ND ND ND ND ND ND ND ND ND ND 2/24/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.0 ND ND ND ND ND 12 ND ND ND ND ND .12 ND ND ND ND ND 10/26/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.71 ND ND ND 4.1 ND ND ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND 0.60 J ND ND ND ND ND 5 5 ND ND ND ND ND ND ND ND ND 0.48 J ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.49 J ND ND ND na ND 6.4 na ND ND ND na ND ND ND ND ND ND MW-2 6/30/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 6/30/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/13/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.35 J ND ND ND ND ND 2.0 ND ND ND ND ND ND ND ND ND ND ND 7/27/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/20/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.6 ND ND ND ND ND ND ND ND ND ND ND 7/19/2018 ND ND ND ND ND ND ND ND ND ND 0.62 ND ND ND ND ND ND ND ND 0.72 ND ND ND ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/11/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 8/20/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND 16.5 ND ND ND 176 ND ND ND ND ND ND ND ND ND ND ND ND ND 2/24/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND 11 ND ND ND ND ND 100 ND ND ND ND ND ND ND ND ND ND ND 10/26/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND 4.8 ND ND ND ND ND 58.3 ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND 6.5 ND ND ND ND ND 98.7 ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.0 ND ND ND ND ND 74.6 ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.1 ND ND ND ND ND 71 ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.2 ND ND ND na ND 48 na ND ND ND na ND ND ND ND ND ND MW-3 6/30/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 120 ND ND ND ND ND ND ND ND ND ND ND 6/30/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.93 ND ND ND ND ND 74 ND ND ND ND ND ND ND ND ND ND ND 1/13/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.10 ND ND ND ND ND 120 ND ND ND ND ND ND ND ND ND ND ND 7/27/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.00 ND ND ND ND ND 71 ND ND ND ND ND ND ND ND ND ND ND 3/20/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.10 ND ND ND ND ND 99 ND ND ND ND ND ND ND ND ND ND ND 7/19/2018 ND ND ND ND ND ND ND ND ND ND 0.75 ND ND 0.68 ND ND ND ND ND 77 ND ND ND ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.87 ND ND ND ND ND 43 ND ND ND ND ND ND ND ND ND ND ND 7/11/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2.9 ND ND ND ND ND ND ND ND ND ND ND NCAC 2L Standard (ug/L) 6,000 1 none 4,000 70 70 70 3 70 70 3 4,000 550 70.00 280 70 none 20 100 20 none 5 6 70 none 600 0.2 400 400 500 CS NCDENR GCL (ug/L) 6000000 5,000 none 4000000 6,900 8,500 15,000 3,000 70,000 70,000 3,000 none 84,500 70000 280,000 25,000 none 20,000 100,000 20,000 none 5,000 6,000 30,000 none 260,000 200 28,500 25,000 85,500 CS Notes: Bold indicates results above NCAC 2L Standard. Red denotes concentration greater than GCL. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit / Not Detected J = an estimated quantity that is between the method detection limit and the reporting limit L = Laboratory -fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value is likely to be biased on the low side. nm = not measured na = not analyzed CS = Compound Specific ug/L = micrograms per liter Table 2 Groundwater Monitoring Report Monroe Oil Company; Concord, NC HES Project # 68027 Summary of Groundwater Analytical Data (VOCS) Analytical Method --I- Volatile Organic Compounds Contaminate of Concern (ug/L4 d d a A y N A C y N C a O L a NN W 'OLU C� N C N C W O 0 iL�W L O 0 C y O W. O CcEUN.O o a E p w o. m T m0. L L) _ d m m ; MA Sample ID Date Collected U m C m L o. O �. V is :r N O E E _ x JO Ua' :u O m O O N C L 1 A Z E 6 N LO E C �' N O N O 21 N Q O m U 8/20/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2/24/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/26/2011 ND ND ND ND ND ND ND 0.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND na ND ND na ND ND ND na ND ND ND ND ND ND MW-4 6/30/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.1 ND ND ND ND ND ND ND ND ND ND ND 6/30/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/13/2017 ND ND ND ND ND ND ND ND ND 0.41 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/27/2017 ND ND ND ND ND ND ND ND ND 0.53 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/20/2018 ND ND ND ND ND ND ND ND ND 0.22 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/19/2018 ND ND ND ND ND ND ND ND ND ND 0.75 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/11/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/1/2011 4.7 0.15 ND ND ND ND ND ND ND ND ND ND ND 5.0 ND ND ND ND ND 22 ND ND ND ND ND ND ND ND ND ND ND 10/26/2011 ND ND ND ND ND ND ND 0.27 ND ND ND ND ND 2.9 ND ND ND ND ND 12.8 ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND 13.2 ND ND ND ND ND 42.2 0.59 J ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND 8.5 ND ND ND ND ND 28.4 ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.3 ND ND ND ND ND 5.2 ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND 3.3 ND ND ND ND 7.5 na ND ND ND na ND ND ND ND ND ND na MW-5 6/30/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.5 ND ND ND ND ND 6.8 ND ND ND ND ND ND ND ND ND ND ND 6/30/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.8 ND ND ND ND ND 2.8 ND ND ND ND ND ND ND ND ND ND ND 1/13/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND 3.1 ND ND ND ND ND 2.6 ND ND ND ND ND ND ND ND ND ND ND 7/27/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND 3.0 ND ND ND ND ND 1.4 ND ND ND ND ND ND ND ND ND ND ND 3/20/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND 2.0 ND ND ND ND ND 1.8 ND ND ND ND ND ND ND ND ND ND ND 7/19/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND 0.9 ND ND ND ND ND 1.4 ND ND ND ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/11/2019 ND 0.25 J ND ND ND ND ND ND ND ND ND ND ND 0.48 J ND ND ND ND ND 1 ND ND ND ND ND ND ND ND ND ND ND NCAC 2L Standard (ug/L) 6,000 1 none 4,000 70 70 70 3 70 70 3 4,000 550 70.00 280 70 none 20 100 20 none 5 6 70 none 600 0.2 400 400 500 CS NCDENR GCL (ug/L) 6000000 1,000 none 4000000 6,900 8,100 15,000 3,000 70,000 70,000 3,000 none 84,500 70000 280,000 25,000 none 20,000 100,000 20,000 none 5,000 6,000 30,000 none 260,000 200 28,500 25,000 85,500 CS Notes: Bold indicates results above NCAC 2L Standard. Red denotes concentration greater than GCL. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit / Not Detected J = an estimated quantity that is between the method detection limit and the reporting limit L = Laboratory -fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value is likely to be biased on the low side. nm = not measured na = not analyzed CS = Compound Specific ug/L = micrograms per liter Table 2 Groundwater Monitoring Report Monroe Oil Company; Concord, NC HES Project # 68027 Summary of Groundwater Analytical Data (VOCs) Analytical Method --I- Volatile Organic Compounds Contaminate of Concern (ug/L4 d d a A y N A C y N C a O L a NN W 'OLU C� N C N C L O W 0 C O O 0 CcEUN.O iL�W o a E w o. m y O W. m0. L L) d m m ; Sample ID Date Collected U C m p o. O �. T V i= :r N _ O E E _ x MA Ua' JO m :u O m O L O N C L 1 A Z E 6 N LO E C �' N O N O 21 N O � Q 3/1/2011 7 0.18 ND ND ND ND ND ND ND ND ND ND ND 15 ND 0.15 ND ND ND 110 ND ND ND ND ND ND ND ND ND ND ND 10/26/2011 ND ND ND ND ND ND ND ND ND ND ND ND ND 18.8 ND ND ND ND ND 24.1 ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND 12.2 ND 0.32 J ND ND ND 12.5 ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND 0.5 J ND ND ND 0.48 J ND ND ND ND ND ND 0.47 J 4.2 ND 2.2 ND ND ND 6.5 ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 5.8 J ND ND ND ND ND ND ND ND ND ND ND ND 2.0 ND 0.21 J ND ND 1.5 J 1.8 ND ND ND ND ND 0.1 J ND 0.34 J ND 0.64 J ND 9/25/2014 15 J ND ND ND ND 1.5 ND ND ND ND ND ND ND 19 ND 2.3 ND na ND 7.2 na ND ND ND na ND ND ND ND ND ND 6/30/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND 21 ND ND ND ND ND 9.4 ND ND ND ND ND ND ND ND ND ND ND MW-6 6/30/2016 ND ND ND ND ND 0.96 ND ND ND ND ND ND ND 6.70 ND ND ND ND ND 9.4 2.7 ND ND ND ND ND ND ND ND ND ND 1/13/2017 ND ND ND ND 0.22 J 3.90 0.23 J ND ND ND ND ND ND 3.10 ND 0.39 J ND ND ND 1.7 ND ND ND ND ND 0.77 ND ND ND ND ND 7/27/2017 ND ND ND ND ND 3.2 0.18 J ND ND ND ND ND ND 2.10 ND 0.24 J ND ND ND 0.56 ND ND ND ND ND ND ND ND ND ND ND 3/20/2018 ND ND ND ND ND 0.78 ND ND ND ND ND ND ND 6.30 ND ND ND ND ND 2.9 ND ND ND ND ND ND ND ND ND ND ND 7/19/2018 ND 0.36 ND ND ND 4.2 0.20 ND ND ND ND ND ND 3.00 ND 0.26 J ND ND ND 2.7 ND ND ND ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND 0.47 ND ND ND ND ND ND ND 2.20 ND ND ND ND ND 1.9 ND ND ND ND ND ND ND ND ND ND ND 7/11/2019 20 J 0.21 J ND ND ND 3.5 ND ND ND ND ND ND ND 2.20 ND ND ND ND ND 1.7 ND ND ND ND ND ND ND 0.23 J ND ND ND 3/1/2011 ND ND ND ND ND 3.4 ND 1.2 ND ND ND ND ND .28 ND ND ND ND ND 54 ND ND ND ND ND .12 ND ND ND ND ND 10/26/2011 ND ND ND ND ND ND ND 0.31 ND ND ND ND ND ND ND ND ND ND ND 18.7 ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 12.6 ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.9 ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 5.3 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND na ND 0.35 J na ND ND ND na ND ND ND ND ND ND 6/30/2015 12 ND ND ND ND ND ND ND ND 0.39 ND ND ND ND ND ND ND ND ND 1.1 ND ND ND ND ND ND ND ND ND ND ND MW-7 6/30/2016 DRY 1 /13/2017 DRY 7/27/2017 9.8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.52 ND ND ND ND ND 3/20/2018 7/19/2018 Damaged 12/18/2018 7/11 /2019 NCAC 2L Standard (ug/L) 6,000 1 none 4,000 70 70 70 3 70 70 3 4,000 550 70.00 280 70 none 20 100 20 none 5 6 70 none 600 0.2 400 400 500 - NCDENR GCL (ug/L) 6000000 5,000 none 4000000 6,W0 8,500 15,000 3,000 10,000 70,000 3,000 none 84,500 70000 280,000 25,000 none 20,000 100,000 20,000 none 5,000 6,000 30,000 none 260,000 200 28,500 25,000 85,500 - Notes: Bold indicates results above NCAC 2L Standard. Red denotes concentration greater than GCL. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit / Not Detected J = an estimated quantity that is between the method detection limit and the reporting limit L = Laboratory -fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value is likely to be biased on the low side. nm = not measured na = not analyzed CS = Compound Specific ug/L = micrograms per liter Table 2 Groundwater Monitoring Report Monroe Oil Company; Concord, NC HES Project # 68027 Summary of Groundwater Analytical Data (VOCS) Analytical Method --I- Volatile Organic Compounds Contaminate of Concern (ug/L4 U m d A o :u O C m N y m O N C N a C d A E L L p O w W o. o. O N C 0 m O �. y T C N C a O C y L V L W O W. m0. is :r 1 'OLU O L L) a N A Z _ d E O O w NN m E C� m E cli� _ x a 0 CcEUN.O iL�WUa' ; MA JO O °1 Q O Sample ID Date Collected 3/1/2011 7.3 ND ND ND ND ND ND ND ND ND ND ND ND .32 ND ND ND ND ND 47 ND ND ND ND ND .17 ND ND ND ND ND 10/26/2011 6.5 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 20.1 ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 5.1 ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 27.2 ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY DRY MW-8 9/25/2014 Damaged 6/30/2015 6/30/2016 1 /13/2017 7/27/2017 3/20/2018 7/19/2018 12/18/2018 7/11 /2019 10/27/2011 7.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.17 ND ND ND ND ND ND ND ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.68 J ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.45 J ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND na ND 1.6 na ND ND ND na ND ND ND ND ND ND 6/30/2015 ND ND 3.8 ND ND ND ND ND 2.4 21 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-9 6/30/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3.6 ND ND ND ND ND ND ND ND ND ND ND 1/13/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.8 ND ND ND ND ND ND ND ND ND ND ND 7/27/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.77 ND ND ND ND ND ND ND ND ND ND ND 3/20/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.365 ND ND ND ND ND ND ND ND ND ND ND 7/19/2018 ND ND ND ND ND ND ND ND ND ND 0.63 ND ND ND ND ND ND ND ND 1.2 ND ND ND ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.7 ND ND ND ND ND ND ND ND ND ND ND 7/15/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.7 ND ND ND ND ND ND ND ND ND ND ND NCAC 2L Standard (ug/L) 6,000 1 none 4,000 70 70 70 3 70 70 3 4,000 550 70.00 280 70 none 20 100 20 none 5 6 70 none 600 0.2 400 400 500 CS NCDENR GCL (ug/L) 6000000 5,000 none 4000000 6,900 8,500 15,000 3,000 70,000 70,000 3,000 none 84,500 70000 280,000 25,000 none 20,000 100,000 20,000 none 5,000 6,000 30,000 none 260,000 200 28,500 25,000 85,500 CS Notes: Bold indicates results above NCAC 2L Standard. Red denotes concentration greater than GCL. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit / Not Detected J = an estimated quantity that is between the method detection limit and the reporting limit L = Laboratory -fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value is likely to be biased on the low side. nm = not measured na = not analyzed CS = Compound Specific ug/L = micrograms per liter Table 2 Groundwater Monitoring Report Monroe Oil Company; Concord, NC HES Project # 68027 Summary of Groundwater Analytical Data (VOCS) Analytical Method --I- Volatile Organic Compounds Contaminate of Concern (ug/L4 d d a A y N A C y N C a O L a W 'OLU C� N C N C W O a~NN 0 iL�W L O 0 C y O W. O CcEN.O o a E p w o. m T m0. L L) _ d m m ; MA Sample ID Date Collected U m C m L o. O �. V is :r N O E E _ x JO Ua' :u O m O O N C L 1 A Z E 6 N 2O E C �' N O N O 21 N r cli� Q O 10/27/2011 20.2 ND ND ND ND ND ND ND ND ND ND ND ND ND 1.8 ND ND ND ND 1.8 ND ND 0.16 ND ND ND 0.93 ND ND ND ND 8/29/2012 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 4.9 ND ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 17.0 ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 26 ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND na ND 34 na ND ND ND na ND ND ND ND ND ND 6/30/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 72 ND ND ND ND ND ND ND ND ND ND ND MW-10 6/30/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 40 ND ND ND ND ND ND ND ND ND ND ND 1/13/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 95 ND ND ND ND ND ND ND ND ND ND ND 7/27/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 65 ND ND ND ND ND ND ND ND ND ND ND 3/20/2018 DAMAGED 7/19/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 42 ND ND ND ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND ND ND ND ND 2.3 ND ND ND ND ND ND ND ND ND 8.9 ND ND ND ND ND ND ND ND ND ND ND 7/11/2019 ND ND ND ND ND ND ND ND ND 1.4 ND ND ND ND ND ND ND ND ND 35 ND ND ND ND ND ND ND ND ND ND ND 9/17/2012 24.4 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.59J ND ND ND ND ND ND ND ND ND ND 7/25/2013 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/21/2014 5.1 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.91 ND ND ND ND ND ND ND ND ND ND ND 9/25/2014 5.6 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND na ND 1 NA ND ND ND na ND ND ND ND ND ND 6/30/2015 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.7 ND ND ND ND ND ND ND ND ND ND ND 6/30/2016 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.4 ND ND ND ND ND ND ND ND ND ND ND MW-11 1/13/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.3 ND ND ND ND ND ND ND ND ND ND ND 7/27/2017 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.4 ND ND 0.74 ND ND ND ND ND ND ND ND 3/20/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2 ND ND 0.74 ND ND ND ND ND ND ND ND 7/19/2018 ND ND ND ND ND ND ND ND ND ND 0.94 ND ND ND ND ND ND ND ND 3.2 ND ND 0.74 ND ND ND ND ND ND ND ND 12/18/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.6 ND ND ND ND ND ND ND ND ND ND ND 7/11/2019 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.62 ND ND ND ND ND ND ND ND ND ND ND MW-12 7/11/2019 ND ND ND ND ND 0.53 ND ND ND ND ND ND ND 1.40 ND ND ND ND ND 1.2 ND ND ND ND ND ND ND ND ND ND ND WSW 12/18/2018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NCAC 2L Standard (ug/L) 6,000 1 none 4,000 70 70 70 3 70 70 3 4,000 550 70.00 280 70 none 20 100 20 none 5 6 70 none 600 0.2 400 400 500 CS NCDENR GCL (ug/L) 6000000 1,000 none 4000000 6,900 8,500 15,000 3,000 70,000 70,000 3,000 none 84,500 70000 280,000 25,000 none 20,000 100,000 20,000 none 5,000 6,000 30,000 none 260,000 200 28,500 25,000 85,500 CS Notes: Bold indicates results above NCAC 2L Standard. Red denotes concentration greater than GCL. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit / Not Detected J = an estimated quantity that is between the method detection limit and the reporting limit L = Laboratory -fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value is likely to be biased on the low side. nm = not measured na = not analyzed CS = Compound Specific ug/L = micrograms per liter Table 2a Groundwater Monitoring Report Monroe Oil Company; Concord, NC Summary of Groundwater Analytical Data (VPH & Lead Data) Analytical Method --*' VPH 3030C Constituent of Concern (ug/L) N U @ U N U -U iC L w U C1 U V - N o U T U Sample ID Date Collected 3/31/2010 na na na na 8/20/2010 na na na na 2/24/2011 54,000 10,000 28,000 0.017 10/26/2011 na na na na 8/29/2012 11,400 42,900 40,000 ND 7/25/2013 ND 27,500 27,700 NO 3/21/2014 4,400 ND 16,000 1.11 MW-1 9/25/2014 2,800 NO 9,700 NA 6/30/2015 2,100 ND 9,800 NA 6/30/2016 1,500 NO 6,700 NA 1/13/2017 ND 2,300 5,700 NA 7/27/2017 1,500 ND 6,200 NA 3/20/2018 Damaged 7/19/2018 12/18/2018 MW-1R 7/11/2019 1600 2700 4200 NA 3/1/2011 ND ND 150 5.9 10/26/2011 53.3 57.1 48.7 ND 9/5/2012 ND ND ND ND 7/25/2013 ND ND ND ND 3/21/2014 ND ND ND ND 9/25/2014 ND ND ND NA MW-1D 6/30/2015 ND ND ND NA 6/30/2016 ND ND ND NA 1/13/2017 ND ND ND NA 7/27/2017 ND ND ND NA 3/20/2018 Damaged 7/19/2018 12/18/2018 MW-1DR 7/11/2019 ND 120 ND ND 8/20/2010 ND NO ND ND 2/24/2011 ND ND ND 0.038 10/26/2011 67 NO ND 19.7 8/29/2012 ND ND ND 5.3 7/25/2013 ND ND ND ND 3/21/2014 ND ND ND 6.2 9/25/2014 ND NO ND NA MW-2 6/30/2015 ND ND ND NA 6/30/2016 ND ND ND NA 1/13/2017 ND ND ND NA 7/27/2017 ND ND ND NA 3/20/2018 ND ND ND NA 7/19/2018 ND ND ND NA 12/18/2018 ND ND ND NA 7/11/2019 ND NO ND NA NCAC 2L Standard (ug/L) 420 4,200 210 15 NCDENR GCL (ug/L) - - - 15,000 Notes: Bold indicates results above NCAC 2L Standard. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit/ Not Detected na = not analyzed CS = Compound Specific ug/L = micrograms per liter Table 2a Groundwater Monitoring Report Monroe Oil Company; Concord, NC Summary of Groundwater Analytical Data (VPH & Lead Data) Analytical Method --*' VPH 3030C Constituent of Concern (ug/L) N U @ U N U -U f0 L w U c6 U V - l0 o U C6 U Sample ID Date Collected 8/20/2010 198 ND ND ND 2/24/2011 ND ND ND 0.049 10/26/2011 ND NO ND 17.3 8/29/2012 87.9 J ND NO ND 7/25/2013 51.1 J NO ND NO 3/21/2014 ND ND NO 14 9/25/2014 ND NO ND NA MW-3 6/30/2015 130 ND NO NA 6/30/2016 ND NO ND NA 1/13/2017 ND ND NO NA 7/27/2017 ND NO ND NA 3/20/2018 130 ND NO NA 7/19/2018 110 NO ND NA 12/18/2018 ND ND NO NA 7/11/2019 ND NO ND NA 8/20/2010 ND ND ND ND 2/24/2011 ND NO ND NO 10/26/2011 ND ND ND 10.7 8/29/2012 104 NO ND ND 7/25/2013 ND ND NO ND 3/21/2014 ND NO ND 3.6 J 9/25/2014 ND ND NO NA MWA 6/30/2015 ND NO ND NA 6/30/2016 ND ND NO NA 1/13/2017 ND NO ND NA 7/27/2017 ND ND NO NA 3/20/2018 ND NO ND NA 7/19/2018 ND ND NO NA 12/18/2018 ND NO ND NA 7/11/2019 ND ND NO NA 3/1/2011 ND NO ND 6.2 10/26/2011 ND ND NO 27.1 8/29/2012 56.9 J NO ND ND 7/25/2013 81.6 J 42.0 J 102 ND 3/21/2014 ND ND ND 2.3 J 9/25/2014 ND ND NO NA MW-5 6/30/2015 ND NO ND NA 6/30/2016 ND ND NO NA 1/13/2017 ND NO ND NA 7/27/2017 ND ND NO NA 3/20/2018 ND NO ND NA 7/19/2018 ND ND NO NA 12/18/2018 ND NO ND NA 7/11/2019 ND ND NO NA NCAC 2L Standard (ug/L) 420 4,200 210 15 NCDENR GCL (ug/L) - - - 15,000 Notes: Bold indicates results above NCAC 2L Standard. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit/ Not Detected NA = Not Analyzed CS = Compound Specific ug/L = micrograms per liter Table 2a Groundwater Monitoring Report Monroe Oil Company; Concord, NC Summary of Groundwater Analytical Data (VPH & Lead Data) Analytical Method --*' VPH 3030C Constituent of Concern (ug/L) N U @ U N U -U f0 L w U Ci U V - l0 o U C6 U Sample ID Date Collected 3/1/2011 ND ND ND 61 10/26/2011 67.9 ND ND <5.0 8/29/2012 ND NO ND ND 7/25/2013 152 68.6 J 35.3 J 24.5 3/21/2014 210 150 ND 5.7 9/25/2014 300 250 250 NA MW-6 6/30/2015 260 NO 260 NA 6/30/2016 ND ND 110 NA 1/13/2017 ND NO 110 NA 7/27/2017 ND ND 140 NA 3/20/2018 ND NO ND NA 7/19/2018 ND 110 NO NA 12/18/2018 ND 110 ND NA 7/11/2019 NO ND NO NA 3/1/2011 110 NO ND 23 10/26/2011 ND ND NO 126 8/29/2012 ND NO ND 29.2 7/25/2013 ND ND ND ND 3/21/2014 ND NO ND 18 9/25/2014 ND ND NO NA MW-7 6/30/2015 ND NO ND NA 6/30/2015 ND ND NO NA 1/13/2017 ND NO ND NA 7/27/2017 ND ND ND NA 3/20/2018 Damaged 7/19/2018 12/18/2018 7/11/2019 3/1/2011 ND ND ND 18 10/26/2011 ND ND ND 30.1 8/29/2012 36.5 J NO ND NO 7/25/2013 ND ND NO ND 3/21/2014 Dry Dry Dry Dry MW-8 9/25/2014 Damaged 6/30/2015 6/30/2016 1/13/2017 7/27/2017 3/20/2018 7/19/2018 12/18/2018 7/11/2019 NCAC 2L Standard (ug/L) 420 4,200 210 15 NCDENR GCL (ug/L) - - - 15,000 Notes: Bolo indicates results above NCAC 2L Standard. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit/ Not Detected NA = Not Analyzed CS = Compound Specific ug/L = micrograms perliter Table 2a Groundwater Monitoring Report Monroe Oil Company; Concord, NC Summary of Groundwater Analytical Data (VPH & Lead Data) Analytical Method --*' VPH 3030C Constituent of Concern (ug/L) N U @ U N U -U f0 L w U Ct U V - l0 o U C6 U Sample ID Date Collected 10/27/2011 ND ND ND <5.0 8/29/2012 ND ND NO 16.4 7/25/2013 ND NO ND ND 3/21/2014 ND ND NO 7.5 9/25/2014 ND NO ND NA 6/30/2015 ND ND NO NA MW-9 6/30/2016 ND NO ND NA 1/13/2017 ND ND 110 NA 7/27/2017 ND NO ND NA 3/20/2018 ND ND NO NA 7/19/2018 ND NO ND NA 12/18/2018 ND ND NO NA 7/15/2019 ND NO ND NA 10/27/2011 ND ND ND <5.0 8/29/2012 35.9 J NO ND 38.2 7/25/2013 ND ND ND ND 3/21/2014 ND NO ND 38 9/25/2014 ND ND ND NA 6/30/2015 110 NO ND NA MW-10 6/30/2016 ND ND NO NA 1/13/2017 ND NO ND NA 7/27/2017 ND ND ND NA 3/20/2018 Damaged 7/19/2018 ND ND NO NA 12/18/2018 ND NO ND NA 7/11/2019 ND ND NO NA 9/17/2012 ND NO ND 489 7/25/2013 ND ND NO 6.7 3/21/2014 ND NO ND 60 9/25/2014 ND ND NO NA 6/30/2015 ND NO ND NA MW-11 6/30/2016 ND ND NO NA 1/13/2017 ND NO ND NA 7/27/2017 ND ND NO NA 3/20/2018 ND NO ND NA 7/19/2018 ND ND NO NA 12/18/2018 ND NO ND NA 7/11/2019 ND ND NO NA MW-12 7/11/2019 ND NO ND NA WSW 12/18/2018 ND ND ND NA NCAC 2L Standard (ug/L) 420 4,200 210 15 NCDENR GCL(ug/L) - - - 15,000 Notes: Bold indicates results above NCAC 2L Standard. NCAC 2L = North Carolina groundwater standards under 15A NCAC 2L.0202 NCDENR GCL = North Carolina Department of Environment and Natural Resources Gross Contamination Level ND = Below Quantitation Limit/ Not Detected NA = Not Analyzed CS = Compound Specific ug/L = micrograms per liter Appendix C icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 July 18, 2019 Bill Frederick Highlands Environmental Solutions, Inc. 8410-D Falls of Neuse Raleigh, NC 27615 Project Location: Concord, NC Client Job Number: Project Number: 68027 Laboratory Work Order Number: 19GO558 Enclosed are results of analyses for samples received by the laboratory on July 11, 2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 48 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 19G0558-01 19G0558-02 19G0558-03 19G0558-04 19G0558-05 19G0558-06 19G0558-07 19G0558-08 19G0558-09 19G0558-10 Sample Preparation Information QC Data Volatile Organic Compounds by GC/ 4S B235492 Petroleum Hydrocarbons Analyses - VPH B235440 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 5 5 8 11 14 17 20 23 26 29 32 35 36 36 36 40 40 42 43 46 Page 2 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Highlands Environmental Solutions, Inc. 8410-D Falls of Neuse REPORT DATE: 7/18/2019 Raleigh, NC 27615 PURCHASE ORDER NUMBER: ATTN: Bill Frederick PROJECT NUMBER: 68027 ANALYTICAL SUMMARY WORK ORDER NUMBER: 19GO558 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Concord, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB MW-11 19GO558-01 Ground Water MW-2 19GO558-02 Ground Water MW-6 19GO558-03 Ground Water MW-5 19GO558-04 Ground Water MW-1R 19GO558-05 Ground Water MW-lDR 19GO558-06 Ground Water MW-3 19GO558-07 Ground Water MW-12 19GO558-08 Ground Water MW-10 19GO558-09 Ground Water MW-4 19GO558-10 Ground Water MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B Page 3 of 48 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method 6200B elevated reporting limit for sample 19G0558-05 due to high concentrations of target compounds. For method MA VPH only hydrocarbon ranges were requested and reported. MADEP-VPH-Feb 2018 Rev 2.1 Qualifications 5-17 Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less than the reporting limit and bias is on the high side. Analyte & Samples(s) Qualified: 2,5-Dibromotoluene (FID) 19G0558-02[MW-2] 2,5-Dibromotoluene (PID) 19G0558-02[MW-2] SM21-22 6200B Qualifications: L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Acetone B235492-BSDI RL-11 Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: 19G0558-05[MW-1R] MADEP-VPH-Feb 2018 Rev 2.1 No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain -of -custody form unless specified in this narrative. Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. d� Lisa A. Worthington Technical Representative Page 4 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-11 Sampled: 7/11/2019 08:55 Sample ID: 19GO558-01 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Benzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Diisopropyl Ether (RIPE) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Methyl tert-Butyl Ether (MTBE) 0.62 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Page 5 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-11 Sampled: 7/11/2019 08:55 Sample ID: 19GO558-01 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:40 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:40 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.3 70-130 7/15/19 20:40 Toluene-d8 98.1 70-130 7/15/19 20:40 4-Bromofluorobenzene 99.4 70-130 7/15/19 20:40 Page 6 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-11 Sampled: 7/11/2019 08:55 Sample ID: 19G0558-01 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 1:44 KMB Rev 2.1 C5-C8Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 1:44 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 1:44 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 1:44 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 1:44 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 98.6 70-130 7/14/19 1:44 2,5-Dibromotoluene (PID) 96.9 70-130 7/14/19 1:44 Page 7 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-2 Sampled: 7/11/2019 09:25 Sample ID: 19GO558-02 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Benzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:01 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:01 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:01 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Diisopropyl Ether (RIPE) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Methyl tert-Butyl Ether (MTBE) ND 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Page 8 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-2 Sampled: 7/11/2019 09:25 Sample ID: 19GO558-02 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:01 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:01 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:01 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:01 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:01 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:01 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.3 70-130 7/15/19 18:01 Toluene-d8 97.6 70-130 7/15/19 18:01 4-Bromofluorobenzene 99.5 70-130 7/15/19 18:01 Page 9 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-2 Sampled: 7/11/2019 09:25 Sample ID: 19GO558-02 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 3:12 KMB Rev 2.1 C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 3:12 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 3:12 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 3:12 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 3:12 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 137 * 70-130 S-17 7/14/19 3:12 2,5-Dibromotoluene (PID) 138 * 70-130 S-17 7/14/19 3:12 Page 10 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-6 Sampled: 7/11/2019 09:45 Sample ID: 19GO558-03 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 20 50 3.8 µg/L 1 J SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Benzene 0.21 0.50 0.18 µg/L 1 J SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF sec-Butylbenzene 3.5 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Diisopropyl Ether (RIPE) 3.4 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Methyl tert-Butyl Ether (MTBE) 1.7 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Page 11 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-6 Sampled: 7/11/2019 09:45 Sample ID: 19GO558-03 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,2,4-Trimethylbenzene 0.23 0.50 0.18 µg/L 1 J SM21-22 6200B 7/15/19 7/15/19 21:06 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:06 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:06 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.2 70-130 7/15/19 21:06 Toluene-d8 99.8 70-130 7/15/19 21:06 4-Bromofluorobenzene 98.8 70-130 7/15/19 21:06 Page 12 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-6 Sampled: 7/11/2019 09:45 Sample ID: 19G0558-03 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 3:42 KMB Rev 2.1 C5-C8Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 3:42 KMB Rev 2.1 Unadjusted C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 3:42 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 3:42 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 3:42 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 101 70-130 7/14/19 3:42 2,5-Dibromotoluene (PID) 97.2 70-130 7/14/19 3:42 Page 13 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-5 Sampled: 7/11/2019 10:10 Sample ID: 19GO558-04 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Benzene 0.25 0.50 0.18 µg/L 1 J SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:28 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:28 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:28 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Diisopropyl Ether (RIPE) 0.48 0.50 0.17 µg/L 1 J SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Methyl tert-Butyl Ether (MTBE) 1.0 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Page 14 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-5 Sampled: 7/11/2019 10:10 Sample ID: 19GO558-04 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:28 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:28 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:28 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:28 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:28 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:28 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.2 70-130 7/15/19 18:28 Toluene-d8 98.7 70-130 7/15/19 18:28 4-Bromofluorobenzene 100 70-130 7/15/19 18:28 Page 15 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-5 Sampled: 7/11/2019 10:10 Sample ID: 19G0558-04 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 4:11 KMB Rev 2.1 C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 4:11 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 4:11 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 4:11 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 4:11 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 97.8 70-130 7/14/19 4:11 2,5-Dibromotoluene (PID) 96.8 70-130 7/14/19 4:11 Page 16 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-1R Sampled: 7/11/2019 10:40 Sample ID: 19GO558-05 Samnle Matrix: Ground Water Sample Flags: RL-II Volatile Organic Compounds by GUMS Analyte Results RL DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 1000 76 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Benzene 270 10 3.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Bromobenzene ND 10 3.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Bromochloromethane ND 10 6.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Bromodichloromethane ND 10 3.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Bromoform ND 10 9.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Bromomethane ND 40 16 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 2-Butanone (MEK) ND 100 39 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF n-Butylbenzene 20 10 4.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF sec-Butylbenzene 9.0 10 3.2 µg/L 20 J SM21-22 6200B 7/15/19 7/15/19 21:59 MFF tert-Butylbenzene ND 10 3.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Carbon Tetrachloride ND 10 2.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Chlorobenzene ND 10 3.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Ethanol ND 1000 210 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Chlorodibromomethane ND 10 4.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Chloroethane ND 10 7.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Chloroform ND 10 3.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Chloromethane ND 20 9.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 2-Chlorotoluene ND 10 2.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 4-Chlorotoluene ND 10 2.8 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2-Dibromoethane (EDB) ND 10 3.8 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2-Dichlorobenzene ND 10 3.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,3-Dichlorobenzene ND 10 2.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,4-Dichlorobenzene ND 10 2.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Dichlorodifluoromethane (Freon 12) ND 10 5.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,1-Dichloroethane ND 10 3.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2-Dichloroethane ND 10 8.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,1-Dichloroethylene ND 10 6.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF cis-1,2-Dichloroethylene ND 10 2.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF trans-1,2-Dichloroethylene ND 10 6.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2-Dichloropropane ND 10 4.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,3-Dichloropropane ND 10 2.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 2,2-Dichloropropane ND 10 4.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1, 1 -Dichloropropene ND 10 3.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF cis-1,3-Dichloropropene ND 10 2.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF trans-1,3-Dichloropropene ND 10 4.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Diisopropyl Ether (RIPE) 3.6 10 3.4 µg/L 20 J SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Ethylbenzene 700 10 2.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 2-Hexanone (MBK) ND 100 30 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Isopropylbenzene (Cumene) 98 10 3.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF p-Isopropyltoluene (p-Cymene) 4.6 10 4.0 µg/L 20 J SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Methyl tert-Butyl Ether (MTBE) 16 10 5.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Methylene Chloride ND 100 6.8 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 4-Methyl-2-pentanone (MIBK) ND 100 33 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Page 17 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-1R Sampled: 7/11/2019 10:40 Samnle ID: 19GO558-05 Samnle Matrix: Ground Water Sample Flags: RL-11 Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene 320 10 6.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF n-Propylbenzene 130 10 2.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Styrene ND 10 2.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,1,2,2-Tetrachloroethane ND 10 4.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Tetrachloroethylene ND 10 3.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Toluene 100 10 2.8 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2,3-Trichlorobenzene ND 20 11 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2,4-Trichlorobenzene ND 10 8.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,l,l-Trichloroethane ND 10 4.0 µg/L 20 SM21-226200B 7/15/19 7/15/19 21:59 MFF 1,1,2-Trichloroethane ND 10 3.2 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Trichloroethylene ND 10 4.8 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Trichlorofluoromethane (Freon 11) ND 10 6.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2,3-Trichloropropane ND 10 5.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,2,4-Trimethylbenzene 860 10 3.6 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF 1,3,5-Trimethylbenzene 270 10 2.8 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Vinyl Acetate ND 400 200 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Vinyl Chloride ND 10 9.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF m+p Xylene 1400 20 6.0 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF o-Xylene 1200 10 3.4 µg/L 20 SM21-22 6200B 7/15/19 7/15/19 21:59 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 97.2 70-130 7/15/19 21:59 Toluene-d8 98.7 70-130 7/15/19 21:59 4-Bromofluorobenzene 99.8 70-130 7/15/19 21:59 Page 18 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-1R Sampled: 7/11/2019 10:40 Sample ID: 19G0558-05 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics 2000 500 µg/L 5 MADEP-VPH-Feb 2018 7/13/19 7/14/19 8:06 KMB Rev 2.1 C5-C8 Aliphatics 1600 500 µg/L 5 MADEP-VPH-Feb 2018 7/13/19 7/14/19 8:06 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics 9700 500 µg/L 5 MADEP-VPH-Feb 2018 7/13/19 7/14/19 8:06 KMB Rev 2.1 C9-C 12 Aliphatics 2700 500 µg/L 5 MADEP-VPH-Feb2018 7/13/19 7/14/19 8:06 KMB Rev 2.1 C9-C10Aromatics 4200 500 µg/L 5 MADEP-VPH-Feb2018 7/13/19 7/14/19 8:06 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 109 70-130 7/14/19 8:06 2,5-Dibromotoluene (PID) 104 70-130 7/14/19 8:06 Page 19 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-1DR Sampled: 7/11/2019 11:10 Sample ID: 19GO558-06 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone 120 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Benzene 1.3 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 2-Butanone (MEK) 2.3 5.0 1.9 µg/L 1 J SM21-22 6200B 7/15/19 7/15/19 19:21 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:21 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:21 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Diisopropyl Ether (RIPE) 0.56 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Ethylbenzene 2.1 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Isopropylbenzene (Cumene) 0.71 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Methyl tert-Butyl Ether (MTBE) 27 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Page 20 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-1DR Sampled: 7/11/2019 11:10 Sample ID: 19GO558-06 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF n-Propylbenzene 0.44 0.50 0.13 µg/L 1 J SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:21 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Toluene 5.7 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:21 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:21 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,2,4-Trimethylbenzene 1.7 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF 1,3,5-Trimethylbenzene 1.1 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:21 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:21 MFF m+p Xylene 9.9 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF o-Xylene 6.6 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:21 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.9 70-130 7/15/19 19:21 Toluene-d8 98.5 70-130 7/15/19 19:21 4-Bromofluorobenzene 101 70-130 7/15/19 19:21 Page 21 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-1DR Sampled: 7/11/2019 11:10 Sample ID: 19G0558-06 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 6:38 KMB Rev 2.1 C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 6:38 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics 130 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 6:38 KMB Rev 2.1 C9-C 12 Aliphatics 120 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 6:38 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 6:38 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 113 70-130 7/14/19 6:38 2,5-Dibromotoluene (PID) 101 70-130 7/14/19 6:38 Page 22 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-3 Sampled: 7/11/2019 11:40 Sample ID: 19GO558-07 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Benzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Diisopropyl Ether (RIPE) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Methyl tert-Butyl Ether (MTBE) 2.9 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Page 23 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-3 Sampled: 7/11/2019 11:40 Sample ID: 19GO558-07 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 21:33 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 21:33 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.4 70-130 7/15/19 21:33 Toluene-d8 98.9 70-130 7/15/19 21:33 4-Bromofluorobenzene 101 70-130 7/15/19 21:33 Page 24 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-3 Sampled: 7/11/2019 11:40 Sample ID: 19G0558-07 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 4:41 KMB Rev 2.1 C5-C8Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 4:41 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 4:41 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 4:41 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 4:41 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 104 70-130 7/14/19 4:41 2,5-Dibromotoluene (PID) 100 70-130 7/14/19 4:41 Page 25 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-12 Sampled: 7/11/2019 12:10 Sample ID: 19GO558-08 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Benzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF sec-Butylbenzene 0.53 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:47 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:47 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:47 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Diisopropyl Ether (RIPE) 1.4 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Methyl tert-Butyl Ether (MTBE) 1.2 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Page 26 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-12 Sampled: 7/11/2019 12:10 Sample ID: 19GO558-08 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:47 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:47 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:47 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-226200B 7/15/19 7/15/19 19:47 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 19:47 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 19:47 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 99.6 70-130 7/15/19 19:47 Toluene-d8 99.0 70-130 7/15/19 19:47 4-Bromofluorobenzene 101 70-130 7/15/19 19:47 Page 27 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-12 Sampled: 7/11/2019 12:10 Sample ID: 19G0558-08 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 5:10 KMB Rev 2.1 C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 5:10 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 5:10 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 5:10 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 5:10 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 99.2 70-130 7/14/19 5:10 2,5-Dibromotoluene (PID) 99.6 70-130 7/14/19 5:10 Page 28 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-10 Sampled: 7/11/2019 12:35 Sample ID: 19GO558-09 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Benzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Chloroform 1.4 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Diisopropyl Ether (RIPE) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Methyl tert-Butyl Ether (MTBE) 35 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Page 29 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-10 Sampled: 7/11/2019 12:35 Sample ID: 19GO558-09 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 20:13 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 20:13 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.3 70-130 7/15/19 20:13 Toluene-d8 98.8 70-130 7/15/19 20:13 4-Bromofluorobenzene 98.0 70-130 7/15/19 20:13 Page 30 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-10 Sampled: 7/11/2019 12:35 Sample ID: 19G0558-09 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 5:40 KMB Rev 2.1 C5-C8Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 5:40 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 5:40 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 5:40 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 5:40 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 107 70-130 7/14/19 5:40 2,5-Dibromotoluene (PID) 102 70-130 7/14/19 5:40 Page 31 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-4 Sampled: 7/11/2019 13:15 Sample ID: 19GO558-10 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Benzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Bromochloromethane ND 0.50 0.32 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Bromomethane ND 2.0 0.78 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Ethanol ND 50 11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Chloromethane ND 1.0 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:54 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:54 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:54 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Diisopropyl Ether (RIPE) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Methyl tert-Butyl Ether (MTBE) ND 0.50 0.25 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Page 32 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO558 Date Received: 7/11/2019 Field Sample #: MW-4 Sampled: 7/11/2019 13:15 Sample ID: 19GO558-10 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:54 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:54 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:54 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Vinyl Acetate ND 20 10 µg/L 1 SM21-226200B 7/15/19 7/15/19 18:54 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/15/19 7/15/19 18:54 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/15/19 7/15/19 18:54 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 98.6 70-130 7/15/19 18:54 Toluene-d8 97.3 70-130 7/15/19 18:54 4-Bromofluorobenzene 97.8 70-130 7/15/19 18:54 Page 33 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0558 Date Received: 7/11/2019 Field Sample #: MW-4 Sampled: 7/11/2019 13:15 Sample ID: 19G0558-10 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 6:09 KMB Rev 2.1 C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 6:09 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/13/19 7/14/19 6:09 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 6:09 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/13/19 7/14/19 6:09 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 98.6 70-130 7/14/19 6:09 2,5-Dibromotoluene (PID) 95.6 70-130 7/14/19 6:09 Page 34 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1 Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 19G0558-01 [MW-11] B235440 5 5.00 07/13/19 19G0558-02[MW-2] B235440 5 5.00 07/13/19 19G0558-03 [MW-6] B235440 5 5.00 07/13/19 19G0558-04[MW-5] B235440 5 5.00 07/13/19 19G0558-05 [MW-1R] B235440 1 5.00 07/13/19 19G0558-06 [MW-1DR] B235440 5 5.00 07/13/19 19G0558-07[MW-3] B235440 5 5.00 07/13/19 19G0558-08 [MW-12] B235440 5 5.00 07/13/19 19G0558-09 [MW-10] B235440 5 5.00 07/13/19 19G0558-10[MW-4] B235440 5 5.00 07/13/19 Prep Method: SW-846 5030B-SM21-22 6200B Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 19G0558-01[MW-11] B235492 5 5.00 07/15/19 19G0558-02[MW-2] B235492 5 5.00 07/15/19 19G0558-03[MW-6] B235492 5 5.00 07/15/19 19G0558-04[MW-5] B235492 5 5.00 07/15/19 19G0558-05 [MW-1R] B235492 0.25 5.00 07/15/19 19G0558-06 [MW-1DR] B235492 5 5.00 07/15/19 19G0558-07[MW-3] B235492 5 5.00 07/15/19 19G0558-08[MW-12] B235492 5 5.00 07/15/19 19G0558-09[MW-10] B235492 5 5.00 07/15/19 19G0558-10[MW-4] B235492 5 5.00 07/15/19 Page 35 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235492 - SW-846 5030B Blank (B235492-BLK1) Prepared & Analyzed: 07/15/19 Acetone ND 50 µg/L Benzene ND 0.50 µg/L Bromobenzene ND 0.50 µg/L Bromochloromethane ND 0.50 µg/L Bromodichloromethane ND 0.50 µg/L Bromoform ND 0.50 µg/L Bromomethane ND 1.0 µg/L 2-Butanone (MEK) ND 5.0 µg/L n-Butylbenzene ND 0.50 µg/L sec-Butylbenzene ND 0.50 µg/L tert-Butylbenzene ND 0.50 µg/L Carbon Tetrachloride ND 0.50 µg/L Chlorobenzene ND 0.50 µg/L Ethanol ND 50 µg/L Chlorodibromomethane ND 0.50 µg/L Chloroethane ND 0.50 µg/L Chloroform ND 0.50 µg/L Chloromethane ND 0.60 µg/L 2-Chlorotoluene ND 0.50 µg/L 4-Chlorotoluene ND 0.50 µg/L 1,2-Dibromoethane (EDB) ND 0.50 µg/L 1,2-Dichlorobenzene ND 0.50 µg/L 1,3-Dichlorobenzene ND 0.50 µg/L 1,4-Dichlorobenzene ND 0.50 µg/L Dichlorodifluoromethane (Freon 12) ND 0.50 µg/L 1,1-Dichloroethane ND 0.50 µg/L 1,2-Dichloroethane ND 0.50 µg/L 1,1-Dichloroethylene ND 0.50 µg/L cis-1,2-Dichloroethylene ND 0.50 µg/L trans-1,2-Dichloroethylene ND 0.50 µg/L 1,2-Dichloropropane ND 0.50 µg/L 1,3-Dichloropropane ND 0.50 µg/L 2,2-Dichloropropane ND 0.50 µg/L 1,1-Dichloropropene ND 0.50 µg/L cis- 1,3 -Dichloropropene ND 0.50 µg/L trans- 1, 3 -Dichloropropene ND 0.50 µg/L Diisopropyl Ether (RIPE) ND 0.50 µg/L Ethylbenzene ND 0.50 µg/L 2-Hexanone (MBK) ND 5.0 µg/L Isopropylbenzene (Cumene) ND 0.50 µg/L p-Isopropyltoluene (p-Cymene) ND 0.50 µg/L Methyl tert-Butyl Ether (MTBE) ND 0.50 µg/L Methylene Chloride ND 5.0 µg/L 4-Methyl-2-pentanone (MIBK) ND 5.0 µg/L Naphthalene ND 0.50 µg/L n-Propylbenzene ND 0.50 µg/L Styrene ND 0.50 µg/L 1,1,2,2-Tetrachloroethane ND 0.50 µg/L Tetrachloroethylene ND 0.50 µg/L Toluene ND 0.50 µg/L 1,2,3-Trichlorobenzene ND 1.0 µg/L 1,2,4-Trichlorobenzene ND 0.50 µg/L Page 36 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235492 - SW-846 5030B Blank (B235492-BLK1) Prepared & Analyzed: 07/15/19 1, 1, 1 -Trichloroethane ND 0.50 µg/L 1,1,2-Tichloroethane ND 0.50 µg/L Trichloroethylene ND 0.50 µg/L Trichlorofluoromethane (Freon 11) ND 0.50 µg/L 1,2,3-Tichloropropane ND 0.50 µg/L 1,2,4-Trimethylbenzene ND 0.50 µg/L 1,3,5-Trimethylbenzene ND 0.50 µg/L Vinyl Acetate ND 20 µg/L Vinyl Chloride ND 0.50 µg/L m+p Xylene ND 1.0 µg/L o-Xylene ND 0.50 µg/L Surrogate:l,2-Dichloroethane-d4 Surrogate: Toluene-d8 Surrogate:4-Bromofluorobenzene LCS (B235492-BS1) 25.3 24.9 24.4 µg/L µg/L µg/L 25.0 101 25.0 99.8 25.0 97.4 Prepared & Analyzed: 07/15/19 70-130 70-130 70-130 Acetone 120 50 µg/L 100 120 70-130 t Benzene 10.3 0.50 µg/L 10.0 103 70-130 Bromobenzene 10.4 0.50 µg/L 10.0 104 70-130 Bromochloromethane 10.6 0.50 µg/L 10.0 106 70-130 Bromodichloromethane 11.2 0.50 µg/L 10.0 112 70-130 Bromoform 10.9 0.50 µg/L 10.0 109 70-130 Bromomethane 8.68 1.0 µg/L 10.0 86.8 60-140 t 2-Butanone(MEK) 100 5.0 µg/L 100 100 70-130 t n-Butylbenzene 10.4 0.50 µg/L 10.0 104 70-130 sec-Butylbenzene 10.8 0.50 µg/L 10.0 108 70-130 tert-Butylbenzene 10.3 0.50 µg/L 10.0 103 70-130 Carbon Tetrachloride 10.8 0.50 µg/L 10.0 108 70-130 Chlorobenzene 11.3 0.50 µg/L 10.0 113 70-130 Ethanol 104 50 µg/L 100 104 70-130 Chlorodibromomethane 11.0 0.50 µg/L 10.0 110 70-130 Chloroethane 11.5 0.50 µg/L 10.0 115 60-140 Chloroform 10.5 0.50 µg/L 10.0 105 70-130 Chloromethane 8.50 0.60 µg/L 10.0 85.0 60-140 t 2-Chlorotoluene 10.9 0.50 µg/L 10.0 109 70-130 4-Chlorotoluene 11.1 0.50 µg/L 10.0 111 70-130 1,2-Dibromoethane (EDB) 11.4 0.50 µg/L 10.0 114 70-130 1,2-Dichlorobenzene 11.0 0.50 µg/L 10.0 110 70-130 1,3-Dichlorobenzene 11.1 0.50 µg/L 10.0 111 70-130 1,4-Dichlorobenzene 11.0 0.50 µg/L 10.0 110 70-130 Dichlorodifluoromethane (Freon 12) 7.12 0.50 µg/L 10.0 71.2 60-140 I 1,1-Dichloroethane 9.98 0.50 µg/L 10.0 99.8 70-130 1,2-Dichloroethane 11.1 0.50 µg/L 10.0 ill 70-130 1,1-Dichloroethylene 11.9 0.50 µg/L 10.0 119 70-130 cis-1,2-Dichloroethylene 10.6 0.50 µg/L 10.0 106 70-130 trans-1,2-Dichloroethylene 11.1 0.50 µg/L 10.0 ill 70-130 1,2-Dichloropropane 10.5 0.50 µg/L 10.0 105 70-130 1,3-Dichloropropane 10.4 0.50 µg/L 10.0 104 70-130 2,2-Dichloropropane 10.2 0.50 µg/L 10.0 102 70-130 1,1-Dichloropropene 10.2 0.50 µg/L 10.0 102 70-130 cis- 1,3 -Dichloropropene 10.4 0.50 µg/L 10.0 104 70-130 trans- 1, 3 -Dichloropropene 10.3 0.50 µg/L 10.0 103 70-130 Page 37 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235492 - SW-846 5030B LCS (B235492-BSI) Prepared & Analyzed: 07/15/19 Diisopropyl Ether(DIPE) 9.94 0.50 µg/L 10.0 99.4 70-130 Ethylbenzene 10.9 0.50 µg/L 10.0 109 70-130 2-Hexanone (MBK) 103 5.0 µg/L 100 103 70-130 t Isopropylbenzene(Cumene) 11.2 0.50 µg/L 10.0 112 70-130 p-Isopropyholuene(p-Cymene) 10.6 0.50 µg/L 10.0 106 70-130 Methyl tert-Butyl Ether (MTBE) 11.3 0.50 µg/L 10.0 113 70-130 Methylene Chloride 11.8 5.0 µg/L 10.0 118 70-130 4-Methyl-2-pentanone (MIBK) 104 5.0 µg/L 100 104 70-130 t Naphthalene 10.2 0.50 µg/L 10.0 102 70-130 t n-Propylbenzene 11.2 0.50 µg/L 10.0 112 70-130 Styrene 11_0 0.50 µg/L 10.0 110 70-130 1,1,2,2-Tetrachloroethane 11.8 0.50 µg/L 10.0 118 70-130 Tetrachloroethylene 12.0 0.50 µg/L 10.0 120 70-130 Toluene 11.0 0.50 µg/L 10.0 110 70-130 1,2,3-Trichlorobenzene 10.5 1.0 µg/L 10.0 105 70-130 1,2,4-Trichlorobenzene 10.8 0.50 µg/L 10.0 108 70-130 1, 1, 1 -Trichloroethane 10.9 0.50 µg/L 10.0 109 70-130 1,1,2-Trichloroethane 11.7 0.50 µg/L 10.0 117 70-130 Trichloroethylene 11.2 0.50 µg/L 10.0 112 70-130 Trichlorofluoromethane (Freon 11) 10.8 0.50 µg/L 10.0 108 70-130 1,2,3-Trichloropropane 11.0 0.50 µg/L 10.0 110 70-130 1,2,4-Trimethylbenzene 9.68 0.50 µg/L 10.0 96.8 70-130 1,3,5-Trimethylbenzene 10.5 0.50 µg/L 10.0 105 70-130 Vinyl Acetate 90.5 20 µg/L 100 90.5 70-130 Vinyl Chloride 9.48 0.50 µg/L 10.0 94.8 60-140 f m+p Xylene 21.8 1.0 µg/L 20.0 109 70-130 o-Xylene 11.2 0.50 µg/L 10.0 112 70-130 Surrogate:l,2-Dichloroethane-d4 24.6 µg/L 25.0 98.3 70-130 Surrogate: Toluene-d8 25.2 µg/L 25.0 101 70-130 Surrogate:4-Bromofluorobenzene 24.8 µg/L 25.0 99.2 70-130 LCS Dup (B235492-BSD1) Prepared & Analyzed: 07/15/19 Acetone 138 50 µg/L 100 138 * 70-130 13.7 25 L-07 t Benzene 10.1 0.50 µg/L 10.0 101 70-130 2.15 25 Bromobenzene 10.6 0.50 µg/L 10.0 106 70-130 1.24 25 Bromochloromethane 10.7 0.50 µg/L 10.0 107 70-130 1.60 25 Bromodichloromethane 11.0 0.50 µg/L 10.0 110 70-130 2.16 25 Bromoform 10.8 0.50 µg/L 10.0 108 70-130 1.39 25 Bromomethane 9.50 1.0 µg/L 10.0 95.0 60-140 9.02 25 t 2-Butanone(MEK) 103 5.0 µg/L 100 103 70-130 2.99 25 t n-Butylbenzene 10.2 0.50 µg/L 10.0 102 70-130 1.55 25 sec-Butylbenzene 10.6 0.50 µg/L 10.0 106 70-130 1.77 25 tert-Butylbenzene 10.2 0.50 µg/L 10.0 102 70-130 1.08 25 Carbon Tetrachloride 10.9 0.50 µg/L 10.0 109 70-130 1.01 25 Chlorobenzene 11.0 0.50 µg/L 10.0 110 70-130 3.23 25 Ethanol 116 50 µg/L 100 116 70-130 10.1 25 Chlorodibromomethane 10.8 0.50 µg/L 10.0 108 70-130 1.55 25 Chloroethane 11.5 0.50 µg/L 10.0 115 60-140 0.261 25 Chloroform 10.6 0.50 µg/L 10.0 106 70-130 0.853 25 Chloromethane 8.75 0.60 µg/L 10.0 87.5 60-140 2.90 25 2-Chlorotoluene 10.5 0.50 µg/L 10.0 105 70-130 3.72 25 4-Chlorotoluene 10.7 0.50 µg/L 10.0 107 70-130 3.21 25 Page 38 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235492 - SW-846 5030B LCS Dup (B235492-BSD1) Prepared & Analyzed: 07/15/19 1,2-Dibromoethane (EDB) 11.1 0.50 µg/L 10.0 111 70-130 2.93 25 1,2-Dichlorobenzene 11.3 0.50 µg/L 10.0 113 70-130 1.97 25 1,3-Dichlorobenzene 10.9 0.50 µg/L 10.0 109 70-130 2.09 25 1,4-Dichlorobenzene 10.8 0.50 µg/L 10.0 108 70-130 1.84 25 Dichlorodifluoromethane (Freon 12) 7.10 0.50 µg/L 10.0 71.0 60-140 0.281 25 t 1,1-Dichloroethane 10.2 0.50 µg/L 10.0 102 70-130 2.18 25 1,2-Dichloroethane 11.0 0.50 µg/L 10.0 110 70-130 0.723 25 1,1-Dichloroethylene 11.9 0.50 µg/L 10.0 119 70-130 0.0840 25 cis-1,2-Dichloroethylene 10.4 0.50 µg/L 10.0 104 70-130 1.81 25 trans-1,2-Dichloroethylene 10.8 0.50 µg/L 10.0 108 70-130 2.64 25 1,2-Dichloropropane 10.3 0.50 µg/L 10.0 103 70-130 2.22 25 1,3-Dichloropropane 10.2 0.50 µg/L 10.0 102 70-130 1.95 25 2,2-Dichloropropane 10.2 0.50 µg/L 10.0 102 70-130 0.785 25 f 1,1-Dichloropropene 10.2 0.50 µg/L 10.0 102 70-130 0.0980 25 cis-1,3-Dichloropropene 10.3 0.50 µg/L 10.0 103 70-130 1.26 25 trans- 1, 3 -Dichloropropene 10.4 0.50 µg/L 10.0 104 70-130 1.45 25 Diisopropyl Ether(DIPE) 9.93 0.50 µg/L 10.0 99.3 70-130 0.101 25 Ethylbenzene 10.7 0.50 µg/L 10.0 107 70-130 2.41 25 2-Hexanone (MBK) 103 5.0 µg/L 100 103 70-130 0.360 25 f Isopropylbenzene(Cumene) 10.9 0.50 µg/L 10.0 109 70-130 2.27 25 p-Isopropyltoluene(p-Cymene) 10.1 0.50 µg/L 10.0 101 70-130 3.96 25 Methyl tert-Butyl Ether (MTBE) 11.4 0.50 µg/L 10.0 114 70-130 1.41 25 Methylene Chloride 11.7 5.0 µg/L 10.0 117 70-130 0.851 25 4-Methyl-2-pentanone (MIBK) 102 5.0 µg/L 100 102 70-130 1.44 25 t Naphthalene 9.98 0.50 µg/L 10.0 99.8 70-130 2.08 25 f n-Propylbenzene 10.9 0.50 µg/L 10.0 109 70-130 2.63 25 Styrene 10.6 0.50 µg/L 10.0 106 70-130 3.71 25 1,1,2,2-Tetrachloroethane 11.5 0.50 µg/L 10.0 115 70-130 2.74 25 Tetrachloroethylene 11.8 0.50 µg/L 10.0 118 70-130 1.85 25 Toluene 10.7 0.50 µg/L 10.0 107 70-130 3.03 25 1,2,3-Trichlorobenzene 10.2 1.0 µg/L 10.0 102 70-130 2.60 25 1,2,4-Trichlorobenzene 10.6 0.50 µg/L 10.0 106 70-130 1.97 25 1, 1, 1 -Trichloroethane 10.7 0.50 µg/L 10.0 107 70-130 1.94 25 1,1,2-Trichloroethane 11.5 0.50 µg/L 10.0 115 70-130 1.64 25 Trichloroethylene 10.8 0.50 µg/L 10.0 108 70-130 4.27 25 Trichlorofluoromethane (Freon 11) 10.8 0.50 µg/L 10.0 108 70-130 0.278 25 1,2,3-Trichloropropane 10.1 0.50 µg/L 10.0 101 70-130 8.42 25 1,2,4-Trimethylbenzene 9.75 0.50 µg/L 10.0 97.5 70-130 0.721 25 1,3,5-Trimethylbenzene 10.5 0.50 µg/L 10.0 105 70-130 0.381 25 Vinyl Acetate 89.7 20 µg/L 100 89.7 70-130 0.943 25 Vinyl Chloride 9.76 0.50 µg/L 10.0 97.6 60-140 2.91 25 t m+p Xylene 21.6 1.0 µg/L 20.0 108 70-130 0.553 25 o-Xylene 10.8 0.50 µg/L 10.0 108 70-130 3.28 25 Surrogate: 1,2-Dichloroethane-d4 25.2 µg/L 25.0 101 70-130 Surrogate: Toluene-d8 25.0 µg/L 25.0 100 70-130 Surrogate:4-Bromofluorobenzene 24.3 µg/L 25.0 97.3 70-130 Page 39 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235440 - MA VPH Blank (B235440-BLK1) Prepared & Analyzed: 07/13/19 Unadjusted C5-C8 Aliphatics ND 100 µg/L C5-C8 Aliphatics ND 100 µg/L Unadjusted C9-C12 Aliphatics ND 100 µg/L C9-C 12 Aliphatics ND 100 µg/L C9-C10Aromatics ND 100 µg/L Benzene ND 1.0 µg/L Butylcyclohexane ND 1.0 µg/L Decane ND 1.0 µg/L Ethylbenzene ND 1.0 µg/L Methyl tert-Butyl Ether (MTBE) ND 1.0 µg/L 2-Methylpentane ND 1.0 µg/L Naphthalene ND 5.0 µg/L Nonane ND 1.0 µg/L Pentane ND 1.0 µg/L Toluene ND 1.0 µg/L 1,2,4-Trimethylbenzene ND 1.0 µg/L 2,2,4-Trimethylpentane ND 1.0 µg/L m+p Xylene ND 2.0 µg/L o-Xylene ND 1.0 µg/L Surrogate:2,5-Dibromotoluene (FID) 38.7 µg/L 40.0 96.8 70-130 Surrogate: 2,5-Dibromotoluene (PID) 37.6 µg/L 40.0 94.1 70-130 LCS (B235440-BS1) Prepared & Analyzed: 07/13/19 Benzene 46.1 1.0 µg/L 50.0 92.2 70-130 Butylcyclohexane 54.6 1•0 µg/L 50.0 109 70-130 Decane 43.1 1.0 µg/L 50.0 86.2 70-130 Ethylbenzene 46.7 1.0 µg/L 50.0 93.4 70-130 Methyl tert-Butyl Ether (MTBE) 44.3 1.0 µg/L 50.0 88.6 70-130 2-Methylpentane 40.7 1.0 µg/L 50.0 81.5 70-130 Naphthalene 47.4 5.0 µg/L 50.0 94.7 70-130 Nonane 51.7 1.0 µg/L 50.0 103 70-130 Pentane 35.1 1.0 µg/L 50.0 70.3 70-130 Toluene 46.3 1.0 µg/L 50.0 92.7 70-130 1,2,4-Trimethylbenzene 47.0 1.0 µg/L 50.0 94.0 70-130 2,2,4-Trimethylpentane 40.1 1.0 µg/L 50.0 80.1 70-130 m+p Xylene 94.2 2.0 µg/L 100 94.2 70-130 o-Xylene 47.1 1.0 µg/L 50.0 94.3 70-130 Surrogate:2,5-Dibromotoluene (FID) 41.3 µg/L 40.0 103 70-130 Surrogate:2,5-Dibromotoluene (PID) 41.0 µg/L 40.0 103 70-130 LCS Dup (B235440-BSD1) Prepared & Analyzed: 07/13/19 Benzene 45.6 1.0 µg/L 50.0 91.2 70-130 1.14 Butylcyclohexane 54.0 1.0 µg/L 50.0 108 70-130 1.14 Decane 41.9 1.0 µg/L 50.0 83.9 70-130 2.79 Ethylbenzene 46.4 1.0 µg/L 50.0 92.7 70-130 0.677 Methyl tert-Butyl Ether (MTBE) 42.9 1.0 µg/L 50.0 85.7 70-130 3.33 2-Methylpentane 39.9 1.0 µg/L 50.0 79.8 70-130 2.12 Naphthalene 44.8 5.0 µg/L 50.0 89.6 70-130 5.55 Nonane 50.5 1.0 µg/L 50.0 101 70-130 2.37 Pentane 36.2 1.0 µg/L 50.0 72.5 70-130 3.10 Toluene 46.1 1.0 µg/L 50.0 92.2 70-130 0.567 1,2,4-Trimethylbenzene 46.5 1.0 µg/L 50.0 93.0 70-130 1.05 25 25 25 25 25 25 25 25 25 25 25 Page 40 of 48 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235440 - MA VPH LCS Dup (B235440-BSD1) Prepared & Analyzed: 07/13/19 2,2,4-Trimethylpentane 40.2 1.0 µg/L 50.0 80.4 70-130 0.329 25 m+p Xylene 93.7 2.0 µg/L 100 93.7 70-130 0.467 25 o-Xylene 46.7 1.0 µg/L 50.0 93.5 70-130 0.822 25 Surrogate:2,5-Dibromotoluene (FID) 41.9 µg/L 40.0 105 70-130 Surrogate:2,5-Dibromotoluene (PID) 39.7 µg/L 40.0 99.1 70-130 Page 41 of 48 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 * FAX 413/525-6405 " TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. RL-11 Elevated reporting limit due to high concentration of target compounds. 5-17 Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less than the reporting limit and bias is on the high side. Page 42 of 48 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications MADEP-VPH-Feb 2018 Rev 2.1 in Water Unadjusted C5-C8 Aliphatics CT,NC,ME,NH-P C5-C8 Aliphatics CT,NC,ME,NH-P Unadjusted C9-C12 Aliphatics CT,NC,ME,NH-P C9-C12 Aliphatics CT,NC,ME,NH-P C9-C10 Aromatics CT,NC,ME,NH-P Benzene CT,NC,ME,NH-P Ethylbenzene CT,NC,ME,NH-P Methyl tert-Butyl Ether (MTBE) CT,NC,ME,NH-P Naphthalene CT,NC,ME,NH-P Toluene CT,NC,ME,NH-P m+p Xylene CT,NC,ME,NH-P o-Xylene CT,NC,ME,NH-P SM21-22 6200B in Water Acetone NC Benzene NC Bromobenzene NC Bromochloromethane NC Bromodichloromethane NC Bromoform NC Bromomethane NC 2-Butanone (MEK) NC n-Butylbenzene NC sec-Butylbenzene NC tert-Butylbenzene NC Carbon Tetrachloride NC Chlorobenzene NC Ethanol NC Chlorodibromomethane NC Chloroethane NC Chloroform NC Chloromethane NC 2-Chlorotoluene NC 4-Chlorotoluene NC 1,2-Dibromoethane (EDB) NC 1,2-Dichlorobenzene NC 1,3-Dichlorobenzene NC 1,4-Dichlorobenzene NC Dichlorodifluoromethane (Freon 12) NC 1,1-Dichloroethane NC 1,2-Dichloroethane NC 1,1-Dichloroethylene NC cis-1,2-Dichloroethylene NC trans-1,2-Dichloroethylene NC 1,2-Dichloropropane NC 1,3-Dichloropropane NC 2,2-Dichloropropane NC Page 43 of 48 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SM21-22 6200B in Water 1,1-Dichloropropene NC cis-1,3-Dichloropropene NC trans-1,3-Dichloropropene NC Diisopropyl Ether (DIPE) NC Ethylbenzene NC 2-Hexanone (MBK) NC Isopropylbenzene (Cumene) NC p-Isopropyltoluene (p-Cymene) NC Methyl tert-Butyl Ether (MTBE) NC Methylene Chloride NC 4-Methyl-2-pentanone (MIBK) NC Naphthalene NC n-Propylbenzene NC Styrene NC 1,1,2,2-Tetrachloroethane NC Tetrachloroethylene NC Toluene NC 1,2,3-Trichlorobenzene NC 1,2,4-Trichlorobenzene NC 1, 1, 1 -Trichloroethane NC 1,1,2-Trichloroethane NC Trichloroethylene NC Trichlorofluoromethane (Freon 11) NC 1,2,3-Trichloropropane NC 1,2,4-Trimethylbenzene NC 1,3,5-Trimethylbenzene NC Vinyl Acetate NC Vinyl Chloride NC m+p Xylene NC o-Xylene NC Page 44 of 48 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/1/2020 MA Massachusetts DEP M-MA100 06/30/2020 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2020 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2020 RI Rhode Island Department of Health LAO00112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2020 FL Florida Department of Health E871027 NELAP 06/30/2020 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2020 ME State of Maine 2011028 06/9/2021 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2020 NC-DW North Carolina Department of Health 25703 07/31/2019 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2020 Page 45 of 48 Table of Contents m c I a —aN+ P ^ . O 7 U�•2 •� c � 4 NO C0O0NOU t.ONi a) '8 Nn"C'L N _C Q.'7 a O_ iII II it N it 11IIfU h P a)P 6 O U ❑ ❑ a NN N010 N>N El Eloo. ❑ C P c j co o c 3 ME J g o e Let ❑ o E r T n ro ro m Ell] a... q w w M w u U C O N u C N cu 0 P .. ❑❑ C o ro m I. Q OI a C? rri �' X W �I } 11 ❑ ❑ O a r q N ti W2 s 1 { F III��-III-_II� III��-III-_II� a z L3 u a :i 41 ., E L E `Z� Nj 61 P G N Pape 46 of 48 7/1212019 Track your package or shipment with FedEx Tracking ' 775693535227� Delivered Friday 7/12/20 9 at 9: i am FROM `lafeighj NC LDS Origin i ermr)E:'s RALEIGH, NC Multiple -piece Shipment Shipment Facts TRACKING NUM13ER 775693535227 WEIGHT 15 Ibs 16.8 kgs TOTAL PIECES 2 SHIPPER REFERENCE 8,l DELIVERED Signed for by B BECCA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY 2 Piece shipment SERVICE FedEX Priority Overnight DIMENSIONS 24x14x14in. TOTAL SHIPMENT WEIGHT 15 lbs / 6.8 kgs PACKAGING Your Packaging TO CAST E 0NGiAF11.k�0W, MA US F)e sulfa`; ior� I..ocat ion WINDSOR LOCKS, CT MASTER TRACKING NUMBER 715693535S25 DELIVERED TO shipping/Receiving TERMS -1 F_'Hd Party SPECIAL HANDLING SECTION Deliver Weekday, Additional ldaca`Iing ' iurciurge Table of Contents cTAMhA€rn TDAKI..ZIT '2ZWJP nATF7 err€€A€ nF€ €xicRv Page 47of48 https://www,fedex.com/apps/fedextrack/?action=track&tracknumbe rs=775693535227&locale=en—US&r-ntry_code=us Table of Contents Client Received By How were the samples received? 044 Date In Cooler t No Cooler Direct from Sampling L, it `) Time Cl V -f-- On lee No Ice Ambient Melted Ice Were samples within By Gun # Actual Temp - t Temperature? 2-6°C By Blank # Actual Temp - Was Custody Seal Intact? f Were Samples Tampered with? — Was COC Relinquished ? Does Chain Agree With Samples? Are there broken/leaking/loose caps on any samples? E Is COC in ink/ Legible? T Were samples received within holding time? �— Did COC include all Client Analysis rt ` Sampler Name pertinent Information? Project ID`s Collection Dates/Times ^ Are Sample labels filled out and legible? Are there Lab to Filters? Who was notified? Are there Rushes? Who was notified? Are there Short Holds? Who was notified? Is there enough Volume? ; Is there Headspace where applicable?� MS/MSD? Proper Media/Containers Used? Is splitting samples required? Were trip blanks received? On COC? f_ Do all samples have the proper pH? ps Acid Base Unp- 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- tit 500 mL Amb. 500 mL Plastic 8oz Amb/Clear Meoh- 250 mL Amb. 250 mL Plastic 4oz Amb/Clear Bisulfate- Flashpoint Col./Bacteria 2oz Amb/Clear Dl- Other Glass Other Plastic Encore Thiosulfate- I SOC Kit I Plastic Bag Frozen: Sulfuric- I Perchlorate 1 1 Zinlock Unp- 1 Liter Amb. 1 Liter Plastic 16 oz Amb. HCL- 500 mL Amb. 500 mL Plastic 8oz Amb/Clear Meoh- 250 mL Amb. 250 mL Plastic 4oz Amb/Clear Bisulfate- Col./Bacteria Flashpoint___ 2oz Amb/Clear DI- Other Plastic Other Glass Encore Thiosulfate-I SOC Kit Plastic Bag Frozen: Sulfuric- I Perchlorate Ziolock icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 July 22, 2019 Bill Frederick Highlands Environmental Solutions, Inc. 8410-D Falls of Neuse Raleigh, NC 27615 Project Location: Concord, NC Client Job Number: Project Number: 68027 Laboratory Work Order Number: 19GO697 Enclosed are results of analyses for samples received by the laboratory on July 15, 2019. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 21 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 19G0697-01 Sample Preparation Information QC Data Volatile Organic Compounds by GC/ 4S B235633 Petroleum Hydrocarbons Analyses - VPH B235707 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 5 5 8 9 9 9 13 13 15 16 19 Page 2 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Highlands Environmental Solutions, Inc. 8410-D Falls of Neuse REPORT DATE: 7/22/2019 Raleigh, NC 27615 PURCHASE ORDER NUMBER: ATTN: Bill Frederick PROJECT NUMBER: 68027 ANALYTICAL SUMMARY WORK ORDER NUMBER: 19GO697 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: Concord, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB MW-9 19GO697-01 Ground Water MADEP-VPH-Feb 2018 Rev 2.1 SM21-22 6200B Page 3 of 21 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method MA VPH only hydrocarbon ranges were requested and reported. SM21-22 6200B Qualifications: R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: Bromomethane 19G0697-01[MW-9], B235633-BLKI, B235633-BS1, B235633-BSDI MADEP-VPH-Feb 2018 Rev 2.1 No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain -of -custody form unless specified in this narrative. Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Tod E. Kopyscinski Laboratory Director Page 4 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO697 Date Received: 7/15/2019 Field Sample #: MW-9 Sampled: 7/15/2019 09:00 Sample ID: 19GO697-01 Samnle Matrix: Ground Water Analyte Results RL Volatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 50 3.8 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Benzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Bromobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Bromochloromethane ND 1.0 0.32 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Bromodichloromethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Bromoform ND 0.50 0.46 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Bromomethane ND 5.0 0.78 µg/L 1 R-05 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 2-Butanone (MEK) ND 5.0 1.9 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF n-Butylbenzene ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF sec-Butylbenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF tert-Butylbenzene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Carbon Tetrachloride ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Chlorobenzene ND 0.50 0.15 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Ethanol ND 100 11 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Chlorodibromomethane ND 0.50 0.21 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Chloroethane ND 0.50 0.35 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Chloroform ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Chloromethane ND 0.60 0.45 µg/L I SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 2-Chlorotoluene ND 0.50 0.12 µg/L I SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 4-Chlorotoluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2-Dibromoethane (EDB) ND 0.50 0.19 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2-Dichlorobenzene ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,3-Dichlorobenzene ND 0.50 0.12 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,4-Dichlorobenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Dichlorodifluoromethane (Freon 12) ND 0.50 0.26 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,1-Dichloroethane ND 0.50 0.16 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2-Dichloroethane ND 0.50 0.41 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,1-Dichloroethylene ND 0.50 0.32 µg/L 1 SM21-226200B 7/16/19 7/17/19 15:16 MFF cis-1,2-Dichloroethylene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF trans-1,2-Dichloroethylene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,3-Dichloropropane ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 2,2-Dichloropropane ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1, 1 -Dichloropropene ND 0.50 0.16 µg/L 1 SM21-226200B 7/16/19 7/17/19 15:16 MFF cis-1,3-Dichloropropene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF trans-1,3-Dichloropropene ND 0.50 0.23 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Diisopropyl Ether (RIPE) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Ethylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 2-Hexanone (MBK) ND 5.0 1.5 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Isopropylbenzene (Cumene) ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF p-Isopropyltoluene (p-Cymene) ND 0.50 0.20 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Methyl tert-Butyl Ether (MTBE) 2.0 0.50 0.25 µg/L I SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Methylene Chloride ND 5.0 0.34 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 4-Methyl-2-pentanone (MIBK) ND 5.0 1.7 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Page 5 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19GO697 Date Received: 7/15/2019 Field Sample #: MW-9 Sampled: 7/15/2019 09:00 Sample ID: 19GO697-01 Samnle Matrix: Ground Water Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Naphthalene ND 0.50 0.31 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF n-Propylbenzene ND 0.50 0.13 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Styrene ND 0.50 0.11 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,1,2,2-Tetrachloroethane ND 0.50 0.22 µg/L 1 SM21-226200B 7/16/19 7/17/19 15:16 MFF Tetrachloroethylene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Toluene ND 0.50 0.14 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2,3-Trichlorobenzene ND 1.0 0.57 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2,4-Trichlorobenzene ND 0.50 0.40 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1, 1, 1 -Trichloroethane ND 0.50 0.20 µg/L 1 SM21-226200B 7/16/19 7/17/19 15:16 MFF 1,1,2-Trichloroethane ND 0.50 0.16 µg/L 1 SM21-226200B 7/16/19 7/17/19 15:16 MFF Trichloroethylene ND 0.50 0.24 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Trichlorofluoromethane (Freon 11) ND 0.50 0.33 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2,3-Trichloropropane ND 0.50 0.25 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,2,4-Trimethylbenzene ND 0.50 0.18 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF 1,3,5-Trimethylbenzene ND 0.50 0.14 µg/L I SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Vinyl Acetate ND 20 10 µg/L I SM21-226200B 7/16/19 7/17/19 15:16 MFF Vinyl Chloride ND 0.50 0.45 µg/L I SM21-22 6200B 7/16/19 7/17/19 15:16 MFF m+p Xylene ND 1.0 0.30 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF o-Xylene ND 0.50 0.17 µg/L 1 SM21-22 6200B 7/16/19 7/17/19 15:16 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 91.9 70-130 7/17/19 15:16 Toluene-d8 110 70-130 7/17/19 15:16 4-Bromofluorobenzene 97.8 70-130 7/17/19 15:16 Page 6 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: Concord, NC Sample Description: Work Order: 19G0697 Date Received: 7/15/2019 Field Sample #: MW-9 Sampled: 7/15/2019 09:00 Sample ID: 19G0697-01 Samnle Matrix: Ground Water Petroleum Hydrocarbons Analyses - VPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Unadjusted C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/17/19 7/17/19 16:00 KMB Rev 2.1 C5-C8 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/17/19 7/17/19 16:00 KMB Rev 2.1 Unadjusted C9-C12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb 2018 7/17/19 7/17/19 16:00 KMB Rev 2.1 C9-C 12 Aliphatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/17/19 7/17/19 16:00 KMB Rev 2.1 C9-C10Aromatics ND 100 µg/L 1 MADEP-VPH-Feb2018 7/17/19 7/17/19 16:00 KMB Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 104 70-130 7/17/19 16:00 2,5-Dibromotoluene (PID) 94.2 70-130 7/17/19 16:00 Page 7 of 21 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1 Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 19G0697-01 [MW-9] B235707 5 5.00 07/17/19 Prep Method: SW-846 5030B-SM21-22 6200B Lab Number [Field ID] Batch Initial [mL] Final [mL] Date 19G0697-01 [MW-9] B235633 5 5.00 07/16/19 Page 8 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235633 - SW-846 5030B Blank (B235633-BLK1) Prepared: 07/16/19 Analyzed: 07/17/19 Acetone ND 50 µg/L Benzene ND 0.50 µg/L Bromobenzene ND 0.50 µg/L Bromochloromethane ND 0.50 µg/L Bromodichloromethane ND 0.50 µg/L Bromoform ND 0.50 µg/L Bromomethane ND 1.0 µg/L 2-Butanone (MEK) ND 5.0 µg/L n-Butylbenzene ND 0.50 µg/L sec-Butylbenzene ND 0.50 µg/L tert-Butylbenzene ND 0.50 µg/L Carbon Tetrachloride ND 0.50 µg/L Chlorobenzene ND 0.50 µg/L Ethanol ND 50 µg/L Chlorodibromomethane ND 0.50 µg/L Chloroethane ND 0.50 µg/L Chloroform ND 0.50 µg/L Chloromethane ND 0.60 µg/L 2-Chlorotoluene ND 0.50 µg/L 4-Chlorotoluene ND 0.50 µg/L 1,2-Dibromoethane (EDB) ND 0.50 µg/L 1,2-Dichlorobenzene ND 0.50 µg/L 1,3-Dichlorobenzene ND 0.50 µg/L 1,4-Dichlorobenzene ND 0.50 µg/L Dichlorodifluoromethane (Freon 12) ND 0.50 µg/L 1,1-Dichloroethane ND 0.50 µg/L 1,2-Dichloroethane ND 0.50 µg/L 1,1-Dichloroethylene ND 0.50 µg/L cis-1,2-Dichloroethylene ND 0.50 µg/L trans-1,2-Dichloroethylene ND 0.50 µg/L 1,2-Dichloropropane ND 0.50 µg/L 1,3-Dichloropropane ND 0.50 µg/L 2,2-Dichloropropane ND 0.50 µg/L 1,1-Dichloropropene ND 0.50 µg/L cis- 1,3 -Dichloropropene ND 0.50 µg/L trans- 1, 3 -Dichloropropene ND 0.50 µg/L Diisopropyl Ether (RIPE) ND 0.50 µg/L Ethylbenzene ND 0.50 µg/L 2-Hexanone (MBK) ND 5.0 µg/L Isopropylbenzene(Cumene) ND 0.50 µg/L p-Isopropyltoluene (p-Cymene) ND 0.50 µg/L Methyl tert-Butyl Ether (MTBE) ND 0.50 µg/L Methylene Chloride ND 5.0 µg/L 4-Methyl-2-pentanone (MIBK) ND 5.0 µg/L Naphthalene ND 0.50 µg/L n-Propylbenzene ND 0.50 µg/L Styrene ND 0.50 µg/L 1,1,2,2-Tetrachloroethane ND 0.50 µg/L Tetrachloroethylene ND 0.50 µg/L Toluene ND 0.50 µg/L 1,2,3-Trichlorobenzene ND 1.0 µg/L 1,2,4-Trichlorobenzene ND 0.50 µg/L R-05 Page 9 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235633 - SW-846 5030B Blank (B235633-BLK1) Prepared: 07/16/19 Analyzed: 07/17/19 1, 1, 1 -Trichloroethane ND 0.50 µg/L 1,1,2-Tichloroethane ND 0.50 µg/L Trichloroethylene ND 0.50 µg/L Trichlorofluoromethane (Freon 11) ND 0.50 µg/L 1,2,3-Tichloropropane ND 0.50 µg/L 1,2,4-Trimethylbenzene ND 0.50 µg/L 1,3,5-Trimethylbenzene ND 0.50 µg/L Vinyl Acetate ND 20 µg/L Vinyl Chloride ND 0.50 µg/L m+p Xylene ND 1.0 µg/L o-Xylene ND 0.50 µg/L Surrogate:l,2-Dichloroethane-d4 Surrogate: Toluene-d8 Surrogate:4-Bromofluorobenzene LCS (B235633-BS1) 22.2 27.7 24.6 µg/L µg/L µg/L 25.0 88.9 25.0 ill 25.0 98.4 Prepared: 07/16/19 Analyzed: 07/17/19 70-130 70-130 70-130 Acetone 86.3 50 µg/L 100 86.3 70-130 t Benzene 9.53 0.50 µg/L 10.0 95.3 70-130 Bromobenzene 9.68 0.50 µg/L 10.0 96.8 70-130 Bromochloromethane 9.80 0.50 µg/L 10.0 98.0 70-130 Bromodichloromethane 8.82 0.50 µg/L 10.0 88.2 70-130 Bromoform 8.71 0.50 µg/L 10.0 87.1 70-130 Bromomethane 10.3 1.0 µg/L 10.0 103 60-140 R-05 t 2-Butanone(MEK) 114 5.0 µg/L 100 114 70-130 t n-Butylbenzene 7.84 0.50 µg/L 10.0 78.4 70-130 sec-Butylbenzene 8.17 0.50 µg/L 10.0 81.7 70-130 tert-Butylbenzene 8.57 0.50 µg/L 10.0 85.7 70-130 Carbon Tetrachloride 8.60 0.50 µg/L 10.0 86.0 70-130 Chlorobenzene 9.60 0.50 µg/L 10.0 96.0 70-130 Ethanol ill 50 µg/L 100 ill 70-130 Chlorodibromomethane 9.67 0.50 µg/L 10.0 96.7 70-130 Chloroethane 8.39 0.50 µg/L 10.0 83.9 60-140 Chloroform 8.51 0.50 µg/L 10.0 85.1 70-130 Chloromethane 8.72 0.60 µg/L 10.0 87.2 60-140 t 2-Chlorotoluene 8.73 0.50 µg/L 10.0 87.3 70-130 4-Chlorotoluene 8.58 0.50 µg/L 10.0 85.8 70-130 1,2-Dibromoethane (EDB) 9.17 0.50 µg/L 10.0 91.7 70-130 1,2-Dichlorobenzene 8.94 0.50 µg/L 10.0 89.4 70-130 1,3-Dichlorobenzene 8.98 0.50 µg/L 10.0 89.8 70-130 1,4-Dichlorobenzene 8.78 0.50 µg/L 10.0 87.8 70-130 Dichlorodifluoromethane (Freon 12) 9.69 0.50 µg/L 10.0 96.9 60-140 I 1,1-Dichloroethane 9.91 0.50 µg/L 10.0 99.1 70-130 1,2-Dichloroethane 9.12 0.50 µg/L 10.0 91.2 70-130 1,1-Dichloroethylene 8.13 0.50 µg/L 10.0 81.3 70-130 cis-1,2-Dichloroethylene 9.59 0.50 µg/L 10.0 95.9 70-130 trans-1,2-Dichloroethylene 10.1 0.50 µg/L 10.0 101 70-130 1,2-Dichloropropane 10.9 0.50 µg/L 10.0 109 70-130 1,3-Dichloropropane 9.62 0.50 µg/L 10.0 96.2 70-130 2,2-Dichloropropane 8.50 0.50 µg/L 10.0 85.0 70-130 1,1-Dichloropropene 8.89 0.50 µg/L 10.0 88.9 70-130 cis- 1,3 -Dichloropropene 9.21 0.50 µg/L 10.0 92.1 70-130 trans- 1, 3 -Dichloropropene 8.66 0.50 µg/L 10.0 86.6 70-130 Page 10 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 * FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235633 - SW-846 5030B LCS (B235633-BSI) Prepared: 07/16/19 Analyzed: 07/17/19 Diisopropyl Ether(DIPE) 11.0 0.50 µg/L 10.0 110 70-130 Ethylbenzene 9.92 0.50 µg/L 10.0 95.2 70-130 2-Hexanone (MBK) 117 5.0 µg/L 100 117 70-130 t Isopropylbenzene (Cumene) 9.66 0.50 µg/L 10.0 96.6 70-130 p-Isopropyholuene(p-Cymene) 8.74 0.50 µg/L 10.0 87.4 70-130 Methyl tert-Butyl Ether (MTBE) 8.43 0.50 µg/L 10.0 84.3 70-130 Methylene Chloride 10.7 5.0 µg/L 10.0 107 70-130 4-Methyl-2-pentanone (MIBK) 118 5.0 µg/L 100 118 70-130 t Naphthalene 8.78 0.50 µg/L 10.0 87.8 70-130 t n-Propylbenzene 8.75 0.50 µg/L 10.0 87.5 70-130 Styrene 9.53 0.50 µg/L 10.0 95.3 70-130 1,1,2,2-Tetrachloroethane 9.64 0.50 µg/L 10.0 96.4 70-130 Tetrachloroethylene 10.6 0.50 µg/L 10.0 106 70-130 Toluene 9.54 0.50 µg/L 10.0 95.4 70-130 1,2,3-Trichlorobenzene 8.83 1.0 µg/L 10.0 88.3 70-130 1,2,4-Trichlorobenzene 8.85 0.50 µg/L 10.0 88.5 70-130 1, 1, 1 -Trichloroethane 8.49 0.50 µg/L 10.0 84.9 70-130 1,1,2-Trichloroethane 9.77 0.50 µg/L 10.0 97.7 70-130 Trichloroethylene 9.54 0.50 µg/L 10.0 95.4 70-130 Trichlorofluoromethane (Freon 11) 7.74 0.50 µg/L 10.0 77.4 70-130 1,2,3-Trichloropropane 9.61 0.50 µg/L 10.0 96.1 70-130 1,2,4-Trimethylbenzene 8.77 0.50 µg/L 10.0 87.7 70-130 1,3,5-Trimethylbenzene 9.03 0.50 µg/L 10.0 90.3 70-130 Vinyl Acetate 123 20 µg/L 100 123 70-130 Vinyl Chloride 9.29 0.50 µg/L 10.0 92.9 60-140 f m+p Xylene 18.3 1.0 µg/L 20.0 91.6 70-130 o-Xylene 8.99 0.50 µg/L 10.0 89.9 70-130 Surrogate:l,2-Dichloroethane-d4 22.1 µg/L 25.0 88.4 70-130 Surrogate: Toluene-d8 26.1 µg/L 25.0 105 70-130 Surrogate:4-Bromofluorobenzene 26.7 µg/L 25.0 107 70-130 LCS Dup (B235633-BSD1) Prepared: 07/16/19 Analyzed: 07/17/19 Acetone 86.4 50 µg/L 100 86.4 70-130 0.139 25 t Benzene 9.20 0.50 µg/L 10.0 92.0 70-130 3.52 25 Bromobenzene 9.76 0.50 µg/L 10.0 97.6 70-130 0.823 25 Bromochloromethane 9.92 0.50 µg/L 10.0 99.2 70-130 1.22 25 Bromodichloromethane 8.80 0.50 µg/L 10.0 88.0 70-130 0.227 25 Bromoform 8.63 0.50 µg/L 10.0 86.3 70-130 0.923 25 Bromomethane 7.67 1.0 µg/L 10.0 76.7 60-140 29.6 * 25 R-05 t 2-Butanone(MEK) 111 5.0 µg/L 100 Ill 70-130 3.00 25 t n-Butylbenzene 7.75 0.50 µg/L 10.0 77.5 70-130 1.15 25 sec-Butylbenzene 8.02 0.50 µg/L 10.0 80.2 70-130 1.85 25 tert-Butylbenzene 8.36 0.50 µg/L 10.0 83.6 70-130 2.48 25 Carbon Tetrachloride 8.13 0.50 µg/L 10.0 81.3 70-130 5.62 25 Chlorobenzene 9.44 0.50 µg/L 10.0 94.4 70-130 1.68 25 Ethanol 113 50 µg/L 100 113 70-130 2.35 25 Chlorodibromomethane 9.25 0.50 µg/L 10.0 92.5 70-130 4.44 25 Chloroethane 8.13 0.50 µg/L 10.0 81.3 60-140 3.15 25 Chloroform 8.21 0.50 µg/L 10.0 82.1 70-130 3.59 25 Chloromethane 8.12 0.60 µg/L 10.0 81.2 60-140 7.13 25 2-Chlorotoluene 8.51 0.50 µg/L 10.0 85.1 70-130 2.55 25 4-Chlorotoluene 8.42 0.50 µg/L 10.0 84.2 70-130 1.88 25 Page 11 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235633 - SW-846 5030B LCS Dup (B235633-BSD1) Prepared: 07/16/19 Analyzed: 07/17/19 1,2-Dibromoethane (EDB) 8.94 0.50 µg/L 10.0 89.4 70-130 2.54 25 1,2-Dichlorobenzene 9.02 0.50 µg/L 10.0 90.2 70-130 0.891 25 1,3-Dichlorobenzene 8.69 0.50 µg/L 10.0 86.9 70-130 3.28 25 1,4-Dichlorobenzene 8.78 0.50 µg/L 10.0 87.8 70-130 0.00 25 Dichlorodifluoromethane (Freon 12) 8.95 0.50 µg/L 10.0 89.5 60-140 7.94 25 t 1,1-Dichloroethane 9.64 0.50 µg/L 10.0 96.4 70-130 2.76 25 1,2-Dichloroethane 8.85 0.50 µg/L 10.0 88.5 70-130 3.01 25 1,1-Dichloroethylene 7.88 0.50 µg/L 10.0 78.8 70-130 3.12 25 cis-1,2-Dichloroethylene 9.35 0.50 µg/L 10.0 93.5 70-130 2.53 25 trans-1,2-Dichloroethylene 9.65 0.50 µg/L 10.0 96.5 70-130 4.95 25 1,2-Dichloropropane 10.5 0.50 µg/L 10.0 105 70-130 3.73 25 1,3-Dichloropropane 9.31 0.50 µg/L 10.0 93.1 70-130 3.28 25 2,2-Dichloropropane 8.09 0.50 µg/L 10.0 80.9 70-130 4.94 25 f 1,1-Dichloropropene 8.36 0.50 µg/L 10.0 83.6 70-130 6.14 25 cis-1,3-Dichloropropene 9.06 0.50 µg/L 10.0 90.6 70-130 1.64 25 trans- 1, 3 -Dichloropropene 8.32 0.50 µg/L 10.0 83.2 70-130 4.00 25 Diisopropyl Ether(DIPE) 10.6 0.50 µg/L 10.0 106 70-130 3.43 25 Ethylbenzene 9.17 0.50 µg/L 10.0 91.7 70-130 3.75 25 2-Hexanone (MBK) 115 5.0 µg/L 100 115 70-130 1.83 25 f Isopropylbenzene(Cumene) 9.34 0.50 µg/L 10.0 93.4 70-130 3.37 25 p-Isopropyltoluene (p-Cymene) 8.47 0.50 µg/L 10.0 84.7 70-130 3.14 25 Methyl tert-Butyl Ether (MTBE) 8.22 0.50 µg/L 10.0 82.2 70-130 2.52 25 Methylene Chloride 10.4 5.0 µg/L 10.0 104 70-130 2.18 25 4-Methyl-2-pentanone (MIBK) 116 5.0 µg/L 100 116 70-130 1.64 25 t Naphthalene 10.2 0.50 µg/L 10.0 102 70-130 14.5 25 f n-Propylbenzene 8.94 0.50 µg/L 10.0 85.4 70-130 2.43 25 Styrene 9.30 0.50 µg/L 10.0 93.0 70-130 2.44 25 1,1,2,2-Tetrachloroethane 9.62 0.50 µg/L 10.0 96.2 70-130 0.208 25 Tetrachloroethylene 9.71 0.50 µg/L 10.0 97.1 70-130 8.58 25 Toluene 9.24 0.50 µg/L 10.0 92.4 70-130 3.19 25 1,2,3-Trichlorobenzene 10.0 1.0 µg/L 10.0 100 70-130 12.8 25 1,2,4-Trichlorobenzene 9.50 0.50 µg/L 10.0 95.0 70-130 7.08 25 1, 1, 1 -Trichloroethane 8.18 0.50 µg/L 10.0 81.8 70-130 3.72 25 1,1,2-Trichloroethane 9.53 0.50 µg/L 10.0 95.3 70-130 2.49 25 Trichloroethylene 9.10 0.50 µg/L 10.0 91.0 70-130 4.72 25 Trichlorofluoromethane (Freon 11) 7.50 0.50 µg/L 10.0 75.0 70-130 3.15 25 1,2,3-Trichloropropane 9.49 0.50 µg/L 10.0 94.9 70-130 1.26 25 1,2,4-Trimethylbenzene 8.95 0.50 µg/L 10.0 85.5 70-130 2.54 25 1,3,5-Trimethylbenzene 8.81 0.50 µg/L 10.0 88.1 70-130 2.47 25 Vinyl Acetate 121 20 µg/L 100 121 70-130 1.81 25 Vinyl Chloride 8.98 0.50 µg/L 10.0 89.8 60-140 3.39 25 t m+p Xylene 17.6 1.0 µg/L 20.0 88.2 70-130 3.78 25 o-Xylene 8.84 0.50 µg/L 10.0 88.4 70-130 1.68 25 Surrogate:l,2-Dichloroethane-d4 22.4 µg/L 25.0 89.8 70-130 Surrogate: Toluene-d8 26.1 µg/L 25.0 104 70-130 Surrogate:4-Bromofluorobenzene 26.9 µg/L 25.0 107 70-130 Page 12 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235707 - MA VPH Blank (B235707-BLK1) Prepared & Analyzed: 07/17/19 Unadjusted C5-C8 Aliphatics ND 100 µg/L C5-C8 Aliphatics ND 100 µg/L Unadjusted C9-C12 Aliphatics ND 100 µg/L C9-C 12 Aliphatics ND 100 µg/L C9-C10Aromatics ND 100 µg/L Benzene ND 1.0 µg/L Butylcyclohexane ND 1.0 µg/L Decane ND 1.0 µg/L Ethylbenzene ND 1.0 µg/L Methyl tert-Butyl Ether (MTBE) ND 1.0 µg/L 2-Methylpentane ND 1.0 µg/L Naphthalene ND 5.0 µg/L Nonane ND 1.0 µg/L Pentane ND 1.0 µg/L Toluene ND 1.0 µg/L 1,2,4-Trimethylbenzene ND 1.0 µg/L 2,2,4-Trimethylpentane ND 1.0 µg/L m+p Xylene ND 2.0 µg/L o-Xylene ND 1.0 µg/L Surrogate:2,5-Dibromotoluene (FID) 38.6 µg/L 40.0 96.4 70-130 Surrogate: 2,5-Dibromotoluene (PID) 36.5 µg/L 40.0 91.2 70-130 LCS (B235707-BS1) Prepared & Analyzed: 07/17/19 Benzene 45.2 1.0 µg/L 50.0 90.5 70-130 Butylcyclohexane 57.5 1.0 µg/L 50.0 115 70-130 Decane 45.7 1.0 µg/L 50.0 91.4 70-130 Ethylbenzene 45.8 1.0 µg/L 50.0 91.6 70-130 Methyl tert-Butyl Ether (MTBE) 43.2 1.0 µg/L 50.0 86.4 70-130 2-Methylpentane 41.0 1.0 µg/L 50.0 82.1 70-130 Naphthalene 45.7 5.0 µg/L 50.0 91.5 70-130 Nonane 54.3 1•0 µg/L 50.0 109 70-130 Pentane 36.1 1.0 µg/L 50.0 72.1 70-130 Toluene 45.4 1.0 µg/L 50.0 90.9 70-130 1,2,4-Trimethylbenzene 46.1 1•0 µg/L 50.0 92.3 70-130 2,2,4-Trimethylpentane 41.8 1.0 µg/L 50.0 83.6 70-130 m+p Xylene 92.4 2.0 µg/L 100 92.4 70-130 o-Xylene 46.3 1•0 µg/L 50.0 92.6 70-130 Surrogate:2,5-Dibromotoluene (FID) 40.5 µg/L 40.0 101 70-130 Surrogate:2,5-Dibromotoluene (PID) 40.9 µg/L 40.0 102 70-130 LCS Dup (B235707-BSD1) Prepared & Analyzed: 07/17/19 Benzene 45.1 1.0 µg/L 50.0 90.3 70-130 0.219 Butylcyclohexane 562 1.0 µg/L 50.0 112 70-130 2.40 Decane 44.4 1.0 µg/L 50.0 88.9 70-130 2.74 Ethylbenzene 46.3 1.0 µg/L 50.0 92.5 70-130 1.00 Methyl tert-Butyl Ether (MTBE) 43.4 1.0 µg/L 50.0 86.8 70-130 0.416 2-Methylpentane 41.7 1.0 µg/L 50.0 83.5 70-130 1.69 Naphthalene 46.3 5.0 µg/L 50.0 92.5 70-130 1.14 Nonane 53.8 1.0 µg/L 50.0 108 70-130 1.01 Pentane 37.0 1.0 µg/L 50.0 74.0 70-130 2.60 Toluene 45.7 1.0 µg/L 50.0 91.5 70-130 0.654 1,2,4-Trimethylbenzene 46.4 1.0 µg/L 50.0 92.8 70-130 0.551 25 25 25 25 25 25 25 25 25 25 25 Page 13 of 21 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B235707 - MA VPH LCS Dup (B235707-BSD1) Prepared & Analyzed: 07/17/19 2,2,4-Trimethylpentane 41.6 1.0 µg/L 50.0 83.3 70-130 0.388 25 m+p Xylene 93.1 2.0 µg/L 100 93.1 70-130 0.755 25 o-Xylene 46.5 1.0 µg/L 50.0 93.0 70-130 0.416 25 Surrogate:2,5-Dibromotoluene (FID) 39.8 µg/L 40.0 99.6 70-130 Surrogate: 2,5-Dibromotoluene (PID) 37.9 µg/L 40.0 94.7 70-130 Page 14 of 21 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 * FAX 413/525-6405 " TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Page 15 of 21 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications MADEP-VPH-Feb 2018 Rev 2.1 in Water Unadjusted C5-C8 Aliphatics CT,NC,ME,NH-P C5-C8 Aliphatics CT,NC,ME,NH-P Unadjusted C9-C12 Aliphatics CT,NC,ME,NH-P C9-C12 Aliphatics CT,NC,ME,NH-P C9-C10 Aromatics CT,NC,ME,NH-P Benzene CT,NC,ME,NH-P Ethylbenzene CT,NC,ME,NH-P Methyl tert-Butyl Ether (MTBE) CT,NC,ME,NH-P Naphthalene CT,NC,ME,NH-P Toluene CT,NC,ME,NH-P m+p Xylene CT,NC,ME,NH-P o-Xylene CT,NC,ME,NH-P SM21-22 6200B in Water Acetone NC Benzene NC Bromobenzene NC Bromochloromethane NC Bromodichloromethane NC Bromoform NC Bromomethane NC 2-Butanone (MEK) NC n-Butylbenzene NC sec-Butylbenzene NC tert-Butylbenzene NC Carbon Tetrachloride NC Chlorobenzene NC Ethanol NC Chlorodibromomethane NC Chloroethane NC Chloroform NC Chloromethane NC 2-Chlorotoluene NC 4-Chlorotoluene NC 1,2-Dibromoethane (EDB) NC 1,2-Dichlorobenzene NC 1,3-Dichlorobenzene NC 1,4-Dichlorobenzene NC Dichlorodifluoromethane (Freon 12) NC 1,1-Dichloroethane NC 1,2-Dichloroethane NC 1,1-Dichloroethylene NC cis-1,2-Dichloroethylene NC trans-1,2-Dichloroethylene NC 1,2-Dichloropropane NC 1,3-Dichloropropane NC 2,2-Dichloropropane NC Page 16 of 21 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SM21-22 6200B in Water 1,1-Dichloropropene NC cis-1,3-Dichloropropene NC trans-1,3-Dichloropropene NC Diisopropyl Ether (DIPE) NC Ethylbenzene NC 2-Hexanone (MBK) NC Isopropylbenzene (Cumene) NC p-Isopropyltoluene (p-Cymene) NC Methyl tert-Butyl Ether (MTBE) NC Methylene Chloride NC 4-Methyl-2-pentanone (MIBK) NC Naphthalene NC n-Propylbenzene NC Styrene NC 1,1,2,2-Tetrachloroethane NC Tetrachloroethylene NC Toluene NC 1,2,3-Trichlorobenzene NC 1,2,4-Trichlorobenzene NC 1, 1, 1 -Trichloroethane NC 1,1,2-Trichloroethane NC Trichloroethylene NC Trichlorofluoromethane (Freon 11) NC 1,2,3-Trichloropropane NC 1,2,4-Trimethylbenzene NC 1,3,5-Trimethylbenzene NC Vinyl Acetate NC Vinyl Chloride NC m+p Xylene NC o-Xylene NC Page 17 of 21 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/1/2020 MA Massachusetts DEP M-MA100 06/30/2020 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2020 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2020 RI Rhode Island Department of Health LAO00112 12/30/2019 NC North Carolina Div. of Water Quality 652 12/31/2019 NJ New Jersey DEP MA007 NELAP 06/30/2020 FL Florida Department of Health E871027 NELAP 06/30/2020 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2020 ME State of Maine 2011028 06/9/2021 VA Commonwealth of Virginia 460217 12/14/2019 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2020 NC-DW North Carolina Department of Health 25703 07/31/2019 PA Commonwealth of Pennsylvania DEP 68-05812 06/30/2020 Page 18 of 21 Table of Contents a o d¢ m T U U ou a L7 m o O o �n U '✓3 Gl W ..�''. 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I M C U xW C p 'E N 0 ti �' [} li U El El ff] E] W El 0 EJ L A E E E E�E E 7/16/2019 Track your package or shipment with FedEx Tracking Bw '� 775744934432� Delivered Tuesday/ 7/ 16/2019 at 9:33 am FROM Raleigh, Nc Lis Shipment Facts TRACKING NUMBER 775?4493��r32 DIMENSIONS 18x11x16 in TOTALSHIPMENT WEIGHT 15 lhs / &S kgs PACKAGING Yourr P,-,ckaging SHIP DATE Mcn 7/15/2019 Travel History DELIVERED Signed for by: B.BECCA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY SERVICE edEx Priority ovemiaht To EAST LMA US WEIGHT 16 bs / 6,8 kgs DELIVERED TO "TOTAL PIECES Shipping!Receivi,g 1 TERMS SHIPPER REFERENCE l hird Party 190 SPECIAL HANDLING SECTION STANDARD TRANSIT Deliver Weekday, Additional Handling 0 Stiirchaige //16/20 i 9 by 1030 am ACTUAL DELIVERY T ue 7/1 61/2011() 932 any Tuesday,7/16/2019 9:33 am EAST LONG MEADOW, MA Delivered T49 am WINDSOR LOCKS, CT On Fed EX vehicle for delivery 7.4p am WIN DSCR LOCKS, CT Al local FedEx facility https://www.fedex.com/apps/fedextraokl?action=track&tracknu mbers=775744934432&locale=en_US&cntry_code=us Table of Contents `i"If E_. Locai Scan Time IN/ Page 20 of 21 Table of Contents Client Received By Date How were the samples In Cooler + No Cooler received? Direct from Sampling Were samples within By Gun # n O -..... ! r1 Time 01'3 . On Ice i No Ice Ambient Melted Ice Actual Temp - ,-( i Temperature . 2-6 C l By Blank # Actual Temp - Was Custody Seal Intact? Were Samples Tampered with? fV Was COC Relinquished ? Does Chain Agree With Samples? Are there broken/leaking/loose caps on any samples? Is COC in ink/ Legible? Did COC include all Client T pertinent Information? ProjectAre Sample labels filled out and legible? Are there Lab to Alters? if Are there Rushes? Are there Short Holds? Is there enough Volume? Is there Headspace where applicable? Proper Media/Containers Used? Were trip blanks received? Do all samples have the proper pH? Were samples received within holding time? Analysis `17 _ Sampler Name T - ID's -- — Collection Dates/Times T r TW Acid Who was notified? Who was notified? Who was notified? MS/MSD?�� Is splitting sampts required? On COC? Base 11