HomeMy WebLinkAbout9208_Wake_NCFairgrounds_MSWLF_AnnualGW_FID1343027_20190819ENR USE ONLY: fil L]PaiperR.port ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reoortina Form
Notice: This form and any information attached to it are "Pubfio Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6),
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or ox000d the reporting limito
Attach a notification table of any methane gas values that attain or exceed explosive gas levels This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
WithersRavenel, Inc (Consultant)
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Matthew James, PG Phone: 919-469-3340
E-mail: mjames@withersravenel.com
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
rcl
sed NC Fairgrounds Landfill Nowell Road, Raleigh, Wake County
) g(Northwest of Intersection with NC 54) �92-08 .1600 GW: July 18, 2019
i
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring Assessment Monitoring U Corrective Action
T e of data submitted: (Check all that apply)
X Groundwater monitoring data from monitoring wells ❑ Methane gas monitoring data
Groundwater monitoring data from private water supply wells ❑ Corrective action data (specify)
_ Leachate monitoring data
X' Surface water monitoring data ❑ Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration
❑ Yes, a Patifircation of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. 1 am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Matthew James, PG Project Geolgist 919-469-3340
Title
115 MacKenan Drive, Cary, NC 27511
Facility Representative Address
C-0832
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
(Area Code) Telephone Number �gEtHnirf�yr�r
Affix NC LlcensSeal
sZ
_ SEAL =
2310 s
` CO
�"+" ' JH i
■■ WithersRavenel
,. Our People. Your Success.
August 19, 2019
Jaclynne Drummond, Hydrogeologist
Environmental Compliance - Solid Waste Section
NC DEQ, Division of Waste Management
1646 Mail Service Center
Raleigh, NC 27699-1646
Subject: Summer 2019 Annual Groundwater and Surface Water Monitoring Report
Closed NC Fairgrounds Landfill, Permit #92-08,
NC Dept of Agriculture and Consumer Services
WR Project No. 02000082.20
Ms. Drummond:
WithersRavenel (WR) has completed the Summer 2019 Annual Groundwater and Surface Water
monitoring event at the above referenced facility. The scope of work performed by WR included
groundwater sample collection from existing groundwater monitoring wells and surface water sample
collection along Richland Creek in accordance with the North Carolina Department of Environment
Quality (NCDEQ) approved Water Quality and Landfill Gas Monitoring Plan dated September 2008, which
will be referenced as "The Plan" throughout this report.
The closed NC Fairgrounds Landfill is located approximately four miles west of downtown Raleigh and
approximately 1,600 feet northeast of the intersection of NC Highway 54 (Chapel Hill Road) and Nowell
Road (Figure 1). The facility was permitted as a sanitary landfill on August 9, 1982 (Permit #92-08).
According to documentation reviewed by WR, the closed landfill was operated between approximately
1982 and 1988. Samples from five groundwater monitoring wells and two surface water collection points
are intended to be collected and tested on annual basis in accordance with The Plan and correspondence
received from the Department of Waste Management.
The following paragraphs summarize the event which took place on July 18, 2019.
Cordially,
WithersRavenel
Austin Pote G. Matthew James, P.G.
Staff Engineer Senior Geologist
115 MacKenan Drive I Cary, NC 275111 tel.: 919.469.3340 1 fax: 919.467-6008 1 www.withersravenel.com I License No. C-0832
1410 Commonwealth Drive Suite 1011 Wilmington, NC 28403 1 tel: 910.256.9277 1 fax: 910.256.2584
416 Gallimore Dairy Road Suite D I Greensboro, NC 27409 1 tel: 336.605.3009 1 fax: 919.467.6008
Closed NC Fairgrounds Landfill
Annual Groundwater and Surface Water Monitoring Report
WR Project No.: 02000082.20
August 2019
1.0 WATER QUALITY SAMPLING METHODOLOGY
1.1 Groundwater Sampling
Five groundwater monitoring wells, MW-1, MW-2, MW-3, MW-4, and MW-5, were installed at the site in
November 2000 at locations proximal to two waste areas. Figure 2 illustrates the locations of the waste
boundary and monitoring wells. Monitoring well construction details are summarized in Table 1 and
copies of the boring logs and well completion reports for the monitoring wells are included as Appendix A.
Groundwater sampling activities were performed on July 18, 2019 in accordance with protocols detailed
in The Plan. Prior to monitoring well gauging, each monitoring well was opened to allow water levels to
equilibrate to atmospheric pressure. Water levels within each monitoring well were then measured using a
decontaminated electronic water level meter. Groundwater elevation measurements were referenced to
the top of the well casing. The groundwater elevations were calculated to range from 411.90 to 437.54
feet above mean sea level (MSL) for this sampling event. The July 18, 2019 groundwater elevation data is
summarized in Table 1 and a Groundwater Potentiometric Map is included as Figure 2.
Each monitoring well was purged using the low -flow technique. During the purging process, turbidity was
monitored until a clarity less than 10 Nephelometric Turbidity Units (NTU) was achieved. Final turbidity
measurements were recorded in the field notes. Copies of the field notes are included as Appendix B.
Following purging activities, groundwater samples were collected using the same polyethylene tubing used
to purge the wells. Groundwater samples were decanted into laboratory provided bottleware and
immediately placed into an ice -chilled cooler. Collected samples were shipped under proper chain -of -
custody to ENCO Labs in Cary, NC for analysis of volatile organic compounds (VOCs) by EPA Method
8260B, the eight RCRA metals by EPA Method 6010D and 7470A, and 1,4-Dioxane by EPA Method
8260B SIM.
1.2 Surface Water Sampling
Surface water samples were also collected on July 18, 2019 from monitoring points designated as SA-1
and SA-2, located along Richland Creek. SA-1 is considered the upstream sampling location
(approximately 35' 47' 28" North and 78' 43' 43" West) and SA-2 is considered the downstream sampling
location (approximately 35' 47' 31" North and 78' 43' 37" West). To preserve the integrity of the
preservatives within the sample containers, a properly decontaminated Teflon' ladle was used to collect
the surface water samples. The contents of the ladle were immediately decanted into laboratory provided
bottleware. The samples were then placed into ice -chilled coolers and shipped under proper chain -of -
custody to ENCO Labs in Cary, NC for analysis of volatile organic compounds (VOCs) by EPA Method
8260B, the eight RCRA metals by EPA Method 6010D and 7470A, and 1,4-Dioxane by EPA Method
8260B SIM.
Page 2
Closed NC Fairgrounds Landfill
Annual Groundwater and Surface Water Monitoring Report
WR Project No.: 02000082.20
August 2019
2.0 LABORATORY ANALYTICAL RESULTS
Julv 2019 - Groundwater and Surface Water SamalinR Event
The following analytical results exceeded the North Carolina 2L Standard.
• MW-3: Selenium - 76.4 µg/L
Laboratory results for the analytes identified in the July 2019 samples are summarized in Table 2. Copies
of the laboratory analytical reports are included as Appendix C.
Page 3
Closed NC Fairgrounds Landfill
Annual Groundwater and Surface Water Monitoring Report
WR Project No.: 02000082.20
August 2019
3.0 SUMMARY OF REGULATORY EXCEEDANCES AND CONCLUSIONS
Groundwater and Surface Water Monitoring:
• No targeted VOC compounds were detected at concentrations that exceeded their NC 2L
Standard.
• MW-3 had a detection Selenium above NC 2L Standards.
If you have any questions or require additional information concerning this Report and the request to
pursue incident closure, please do not hesitate to contact us at (919) 469-3340.
The next annual groundwater and surface water monitoring event for the Closed NC Fairgrounds Landfill
is planned to occur in Summer 2020.
Sincerely,
WithersRavenel
Austin Pote G. Matthew James, P.G.
Staff Engineer Senior Geologist
cc: Mr. Richard Clark, richard.clark@ncagr.gov, NCDACS
Page 4
TABLES
Table 1
Monitoring Well and Groundwater Data
Closed NC Fairgrounds Landfill
Wake County, North Carolina
WithersRavenel Project # 2000082.20
GW
Monitoring
Ground Surface
TOC
Depth to Water in
Elevation in
Well Depth
Screen
Well
Northing
Easting
Elevation
Elevation in
Feet Below TOC
Feet MSL
in Feet Bls
Interval in
in Feet MSL
Feet MSL
Feet BLS
7/18/2019
7/18/2019
MW-1
743884.26
2079242.17
450.9
453.47
15.93
437.54
19
9 t019
MW-2
744085.55
2079482.30
432.1
435.08
5.56
429.52
15
2 to 14
MW-3
743914.97
2080239.77
429.6
432.89
20.99
411.90
25
10 to 25
MW-4
743570.71
2080213.13
433.3
436.21
20.45
415.76
30
11 to 26
MW-5
j 744186.3297
j 2079598.90
j 431.8
j 433.59
j 15.80
j 417.79
j 25
j 8 to 23
Notes:
BLS = Below the Land Surface
MSL = Mean See Level
TOC = Top of Casing
All wells constructed of two (2)-inch PVC
Page 1 of 1
TABLE 2
Summary of Detected Parameters in Groundwater and Surface
Water
Closed NC Fairgrounds Landfill
Wake County, North Carolina
WithersRavenel Project # 2000082.20
ORGANIC
MW-1
MW-2
MW-3
MW-4
MW-5
SA-1
SA-2
NC 2L Limit
CONSTITUENTS
(µg/L)
Sample Date
7/18/2019
7/18/2019
7/18/2019
7/18/2019
7/18/2019
7/18/2019
7/18/2019
VOCS
All Non -Detect
NA
INORGANIC
CONSTITUENTS
Arsenic
<7.60
<7.60
<7.60
<7.60
<7.60
<7.60
<7.60
10
Barium
16.7
152
195
35.8
35.2
39.5
23.7
700
Cadmium
<0.360
0.69
<0.360
0.586
<0.360
<0.360
<0.360
2
Chromium
<1.40
<1.40
2.35
<1.40
<1.40
<1.40
<1.40
10
Lead
<3.10
<3.10
<3.10
<3.10
<3.10
<3.10
<3.10
15
Selenium
<6.20
<6.20
76.4
<6.20
<6.20
<6.20
<6.20
20
Silver
<1.90
<1.90
<1.90
<1.90
<1.90
<1.90
<1.90
20
Mercury
<0.150
<0.150
<0.150
<0.150
<0.150
<0.150
<0.150
1
Notes:
Qualifiers: J - The identification of the analyte is acceptable; the reported value is an estimate.
B - The same analyte is found in the associated blank.
NIL = Not Listed
All Concentrations reported in tag/L (Parts per Billion)
Concentrations in BOLD Exceed the Labortory Detection Limit
Concentrations in BOLD and Shaded Exceed the NC 2L Standard
MW = Monitoring Well Designation
SA = Surface Water Designation
Page 1 of 1
TABLE 3
LANDFILL GAS PROBE DATA
Closed NC Fairgrounds Landfill
Wake County, North Carolina
WithersRavenel Project # 2000082.20
Ground Surface
Screen
Methane
Probe Depth in
Northing
Easting
Elevation in Feet
Interval in
Probe
feet BLS
MSL
Feet BLS
LFG-1
743753.92
2079430.96
460.3
10
3 to 10
LFG-2
743748.48
2079583.23
456.0
10
3 to 10
LFG-3
743746.98
2079796.58
449.7
10
3 to 10
LFG-4
743697.32
2079878.36
441.1
10
2.5 to 9.5
LFG-5
743581.77
2079872.59
436.0
10
3 to 9
LFG-6
743440.17
2079870.99
445.0
10
3 to 10
LFG-7
ND
ND
ND
10
3 to 10
LFG-8
ND
ND
ND
12
2 to 12
LFG-9
ND
ND
ND
10
3 to 10
Notes:
BLS = Below the Land Surface
MSL = Mean See
Level
ND = Not Defined
All Probes are constructed of 1.25-inch PVC
Page 1 of 1
FIGURES
I
u
r
f Jr
Mount
Ve`r\no\n
FllttSBO(.
rN
- w U
4 � �
LU
TRWI T-Y_--Rp
r
WESTCf �i
.Western
� om jti62? u
t k-ja
GRAPHIC SCALE
r— . r
0 500 1000 Q00
1 inch =1000 ft.
1/ CLOSED NC FAIRGROUNDS DRAWN BY: SCALE: FIGURENO.:
WithersRavenel LANDFILL AP 1"=1000' 1
I / Engineers I Planners I Surveyors RALEIGH, WAKE COUNTY, NORTH CAROLINA
APPROVED BY: DATE: PROJECTNO.:
1.-1-1, ,NC,,,11 1-1,1-1:-GENERAL LOCATION MAP mi 07/24/2017 0200082.20
k\00\00-080\0008222-9a1e !y w4a Mo Qo6"\Praj\2016 9a A Y Eaa1\6d1 YM R wt - i\uSOS -1:14 �w"- JJ7 24, 2017 - PO7E, AUSM
PROPERTY TINE
---------------
04
sit
00
^-I b o N ° O a
w G o td
- 0 O O
Ol
O N Z3
h
r
� 1 N N e�-r
oo
oo
I 6 4 m
rLLLZ Q o Y
o a $
PROPERTY LINE
MW-5
'" 420 0
425 417.79
430^ MW-2
7\ 42952
435
440 \
\0 M W`
437.54 L F G - 8
LFG-7 y� `LFG-9 —LFG-E
LFG-1 \ \
�VLD E fEF"
YONF11 Po
Q H
ems'
41O i
_ M W - 3
415 411.90
\ '
JLFG-3
r SA-2
u
LEGEND
GROUNDWATER ELEVATION CONTOUR
LANDFILL PROPERTY BOUNDARY
PROPERTY LINES FOR
ADJACENT PARCELS
CENTERLINE OF DRAINAGE FEATURE
FEATURE (ROAD
0 (ROADS,, STRUCTURES, ETC.)
W
0
W
F
d Q
W
�
j
9
0
J
J
LL
LFG-4
OBSERVED U
OF BURIED WASTE
inz
O
MW-1 EXISTING
(A u
_
�pLFG-5
101 GROUNDWATER MONITORING WELL
in =
•,rr--,;
$ MW-4
Z o
EXISTING LANDFILL GAS (METHANE)
z O
415.76
LFG-1 9 MONITORING PROBE
0 z
\
Ov
SA-1 0 SURFACE WATER
MONITORING LOCATION
LFG-G
°
Q Y
LL Q
l7
NOTE.
N
P
1. TOPOGRAPHIC, PLANIMETRIC, AND PROPERTY UNE INFORMATION
0
FURNISHED 13Y CITY OF RALEIGH GIS.
V
2. PROPERTY LINE TAKEN FROM CITY OF RALEIGH GIS.
3. GROUNDWATER MONITORING WELLS AND LANDFILL GAS
MONITORING PROBE LOCATIONS SURVEYED BY WITHERSRAVENEL.
4. 2013 AERIAL OBTAINED FROM LOCAL GIS SOURCES.
^ ,
0
^C
W
SA-1
pro S
L.L v
EXISTING
EDWARDS MILL
ROAD RIGHT-OF-WAY
W �
41 �
� u
w 6
GRAPHIC SCALE
200
0 100 200
400
ft.
,
APT
1 inch = 200
APPENDIXA
MONITORING WELL
INSTALLATION RECORDS
rvrraEns& RA L
LOG OF BORING MWA
urve
Engineering & Surveying, Inc
ill MacKanan Drive -Cary. N.C. Z7511
w.uxE+S���
(Page 1 of 1)
Dept. of Agriculture/State Fair
Date Started
: 11/6/2000 Drilling Company
: GeoTechnologies, Inc.
Nowell Road
Date Completed
: 11110/2000 Northing Coord.
: NIA
Raleigh, NC
Hole Diameter
: 8.5 in. Easting Coord.
: NIA
Project # 200082.0
Dolling Method
: H.SA_ Survey By
: WRES
Sampling Method
: Split Spoon Logged By
: Ty Colwell
U
Depth =
in o) 9 Feet OUT
0
S
10 M
1 20
DESCRIPTION
Stiff to very stiff Micaceous CLAYEY
SANDY SILT, Red, Pink, Gray and Gold
Layers
Boring terminated at 19.0 feet. Installed
groundwater monitoring well.
= Well: MW-1
H o - Elev.:450.85
U FID
CL E o iPPm) Cover
cf6n m o t fl
5
1 6
7
.I [�—Casing
Bentonite
pack
Well Construction
Information
WELL CONSTRUCTION
Date Compl. :11/10/2000
Hole Dia. : 8.5 in.
Drill. Method : HSA
Company Rep.
WELL CASING
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
WELLSCREEN
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
Opening :.010 slot
SAND PACK: medium
SEAL : bentonite
NOTES
Groundwater is approx.
11.6 feet below ground
surface. Top of casing is
2.62 feet above ground
surface. Elevation shown is
ground surface elevation.
North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 276941636-Phone (919) 733.3221
WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc.
WELL CONSTRUCTION CERTIFICATION #: 2504
MW-1 STATE WELL CONSTRUCTION PERMIT #: 2504
1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Raleigh County:
Nowell Road
(Road Name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER: Department of Aadculture/ State Fair
Address: 1025 Blue Ridge Road
Raleigh NC 27607
(City or Town) (State) (Zip Code)
4. DATE DRILLED 11/6/2000
5. TOTAL DEPTH 19.0
6. CUTTINGS COLLECTED YES❑ NO®
7. DOES WELL REPLACE EXISTING WELL? YES❑ NO®
8. STATIC WATER LEVEL Below Top of Casing) 11.6 R.
(Use "+" 9 Above Top of Casing)
9. TOP OF CASING IS +2.62 Ft above Land Surface*
Top orcasing lertninated attor below land surface requires a variance In Accordance YAM 15A NCAV ZC.0778
10. YIELD (gpm) N/A METHOD OF TEST N/A
11. WATER ZONES (depth) N/A
12. CLORINATION:
Type N/A
Amount N/A
13. CASING
Depth.
Diameter
Wall Thickness
Material
Or Weight/Ft.
From 9.0 To +2.62
Ft. 2"
Sch.40
PVC
From To
Ft.
From To
Ft.
14. GROUT
Depth
Material
Method
From 5.0 To 0.0
Ft. Neat Cement
Pump & Trim
From To
Ft.
15. SCREEN
Depth
Diameter
Slot Size
Material
From 19.0 To 9.0
Ft. 2 In
0.010
In
PVC
From To
Ft. In
In
From To
Ft. In
In
16. SAND/GRAVEL PACK:
Depth
Size
Material
From 19.0 To 7.0
FL #2
Sand
From To
Ft.
17. REMARKS: Bentonite Plug
from 7.0 feet to 5.0
feet.
Wake
DRILLING LOG
From To
DEPTH
Formation Description
0.0 3"
Topsoil
3" 19.0
Micaceous clayey
sandy silt, red, pink,
gray; and gold
layers
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY 0 THI` S/RECORDV N PROVIDED TO THE WELL OWNER.
FOR OFFICE USE ONLY (S NATUR OF PERSO CONSTRUCTING THE WELL) (DATE)
Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days.
Serial No.
o- WITHERS & RAVENEL
LOG OF BORING M W-2
Engineering & Sarveyiag, Ine
111 MacKenan Drive • Cary, N.C. 27511
wmrExs� (Page 1 of 1)
Dept. of AgricultureiState Fair Date Started : 111712000 . Drilling Company : GeoTechnologhes, Inc.
Nowell Road Date Completed : 1111012000 Northing Coord. : N/A
Raleigh, NC Hole Diameter : 8.5 in. Easting Coord. : N/A
Project # 200082.0 Drilling Method : H.S.A. Survey By : WRES
Sampling Method : Split Spoon Lagged By : Ty Colwell
U
Depth z
in m Q
Feet aj OC
a �
0
2
3]
SM
5
7
SM
9
10 SM
11
12
13 SM
Cr Iw
0
m
3 15
N
m
O
O 16
0
0
rr
d
17
CD
z
w 18
S 19
N
N
�n
DESCRIPTION
Soft Micaceous CLAYEY
Red, Light Gray and White
Stiff Micaceous CLAYEY SANDY SILT,
Dark, Medium and Light Brown Layers
Stiff Micaceous SANDY SILT,
Gold and Light Brown
SILT, Gold, Gray, Brown and White
Layers
Boring terminated at 15.0 feet. Installed
groundwater monitoring well.
Well: MW-2
y 0 FID Elev.:432.06
E o (PPIM) �— Cover
ca m m D 1
Cash
Grout
10i=1
4
2 7
6
3
3 7
12
Bentonite
Screen
Sand pack
Well Construction
Information
WELL CONSTRUCTION
Date Compl.: 11/10/2000
Hole Dia. : 8.5 in.
Drill. Method : HSA
Company Rep.
WELL CASING
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
WELL SCREEN
Material : Sch 40 PVC
Diameter : 2 in.
Joints . threaded
Opening :.010 slot
SAND PACK: medium
SEAL : bentonite
NOTES
Groundwater is approx.
1.8 feet below ground
surface. Top of casing is
3.02 feet above ground
surface. Elevation shown is
ground surface elevation.
North Carol ina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636-Phone (919) 733-3221
WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc.
WELL CONSTRUCTION CERTIFICATION #: 2504
'-2 STATE WELL CONSTRUCTION PERMIT #: 2504
1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery 0 Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Raleigh County: Wake
Nowell Road
(Road Name and Numbers, Community, or Subdivision and Lot No.) M]%V-2
3. OWNER: Department of Aadculture/ State Fair
Address: 1025 Blue Ridge Road
Raleigh NC 27607
(City or Town) (State) (Zip Code)
4. DATE DRILLED 11M2000
5. TOTAL DEPTH 15.0
6. CUTTINGS COLLECTED YES❑ NON
7. DOES WELL REPLACE EXISTING WELL? YES❑ - NO®
8. STATIC WATER LEVEL Below Top of Casing) 1.8 Ft.
(Use "V if Above Top of Casing)
9. TOP OF CASING IS +3.02 Ft above Land Surface*
'Top olcaft lemAnated atlor below land surface requires a variance In Accordance Wilb 15A NCAV 2C.0118
10. YIELD (gpm) N/A METHOD OF TEST
11. WATER ZONES (depth) N/A
12. CLORINATION:
13. CASING
Depth
From 2.0 To +3.02
From To
From To
14. GROUT
Depth
From 5.0 To 0.0
From To
15. SCREEN
Depth
From 14.0 To 2.0
From To _
From To
ype WA Amount
WA
N/A
DRILLING LOG
From To
DEPTH
Formation Description
0.0
3"
Topsoil
3"
7.0
Mic cl. sandy silt,
red, It. gry., & white
7.0
9.5
Mic. cl. sandy silt,
dark, med. and light
brown layers
9.5
11.0
Mic. sd . silt, white,
gold & light brown
layers
11.0
15.0
Mic. cl. sandy silt,
gold, gray, brown
and white layers
If additional space is needed use back of form.
Diameter Wall Thickness Material LOCATION SKETCH
Or Weight/Ft (Show direction and distance from at least two State
Ft. 2" Sch. 40 PVC Roads, or other map reference points)
FL
Ft.
Material Method
Ft. Neat Cement Pump & Trim
FL
Diameter Slot Size
Ft. 2 In 0.010
Ft. In
R. In
16. SAND/GRAVEL PACK:
Depth
From 15.0 To 1.5 FL
From To FL
Size
#2 Sand
17. REMARKS: Bentonite Plug from 1.5 feet to 1.25 feet.
Material
In PVC
In
In
Material
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY S I CORD S PROVIDED TO THE WELL OWNER.
FOR OFFICE USE ONLY (S19NATURE OF PERSO CONSTRUCTING THE WELL) (DATE)
Quad no: Submit original to Division of WaterQuality, Groundwater Section within 30 days.
Serial No.
RURERS & RAVENEL
LOG OF BORING MW 3
Engineering&Surveying,Inc
111 MacKenan Orive . Cary, N.C. 27511
irmreRr�
(Page 1 of 1)
Dept. of Agriculture/State Fair
Date Started
: 11/8/2000 Drilling Company
: GeoTechnologies, Inc.
Nowell Road
Date Completed
: 11/10/2000 Northing Coord.
: N/A
Raleigh, NC
Hole Diameter
Drilling Method
Sampling Method
: 8.5 in. Easting Coord.
: H.SA. Survey By
: Split Spoon Logged By
: N/A
: WRES
: Ty Colwell
Project # 200082.0
U
Depth =
in U
Feet j
0 _ .
1
1 20
SM
SM
SM
SM
DESCRIPTION
SANDY SILT, Brown
Very Stiff to stiff Micaceous SANDY
SILT with traces of PARTIALLY
WEATHERED ROCK, Red, Gold, Gray
and Light Brown Layers
SILT, Brown, Gold, Gray and Light
Brown Layers
traces of PARTIALLY WEATHERED
ROCK, Gray and Brown
Boring terminated at 25.0 feet. Installed
groundwater monitoring well_
Well: MW-3
y o' Elev.:429.63
U FID
E o (ppm) Cover
rn in 0 1
5
5
6
3
4
5
5 II 5
k
Well Construction
Information
WELL CONSTRUCTION
Date Compl.: 11/10/2000
Hole Dia. : 8.5 in.
Drill. Method . HSA
Company Rep.
WELL CASING
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
WELL SCREEN
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
Opening :.010 slot
SAND PACK: medium
SEAL : bentonite
NOTES
Groundwater is approx_
19.9 feet below ground
surface. Top of casing is
3.26 feet above ground
surface. Elevation shown is
ground surface elevation.
North Carolina- Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C_ 27699-1636-Phone (919) 733-3" 1
WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc.
WELL CONSTRUCTION CERTIFICATION #: 2504
MW-3 STATE WELL CONSTRUCTION PERMIT #: 2504
1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injectibn ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Raleigh County: Wake
Nowell Road
(Road Name and Numbers, Community, or Subdivision and Lot No.) MW-3
3. OWNER: Department of Agriculture/ State Fair
Address: 1025 Blue Ridge Road
Raleigh NC 27607
(City or Town) (State) (Zip Code)
4. DATE DRILLED 11/8/2000
5. TOTAL DEPTH 25.0 .
6. CUTTINGS COLLECTED YES[:] NO®
7. DOES WELL REPLACE EXISTING WELL? YES[:] NO®
8. STATIC WATER LEVEL Below Top of Casing) 19.9 Ft.
(Use "+' if Above Top of Casing)
9. TOP OF CASING 1S +3.26 Ft above Land Surface"
'rop of rasing term nated allar below land surface requires a variance In Accordance Wdh 15A NCAV 2C.0118
10. YIELD (gpm) N/A METHOD OF TEST
11. WATER ZONES (depth) N/A
N/A
12. CLORINATION:
Type N/A
Amount N/A
13. CASING
Depth
Diameter
Wall Thickness
Material
Or Weighl/Ft.
From 10.0 To +3.26
Ft 2"
Sch.40
PVC
From To
Ft
From To
Ft
14. GROUT
Depth
Material
Method
From 6.5 To 0.0
Ft. Neat Cement
Pump & Trim
From To
Ft.
15. SCREEN
Depth
Diameter
Slot Size
Material
From 25.0 To 10.0
R. 2 In
0.010
In
PVC
From To
Ft. In
In
From To
Ft In
In
16. SAND/GRAVEL PACK:
Depth
Size
Material
From 25.0 To 8.5
FL #2
Sand
From To
Ft.
17. REMARKS: Bentonite Plug
from 8.5 feet to 6.5
feet.
DRILLING LOG
From To
DEPTH
Formation Description
0.0
3"
Topsoil
3"
3.0
Mic. sandy silt, br.
3.0
13.5
Mic. sandy silt with
traces of P.W.R,
red, gold, gray and
light brown layers
13.5
23.5
Mic. sandy silt, br.,
gld., gry. & It. br.
23.5
25.0
Mic. sandy silt with
traces of P.W.R,
gray and brown
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
I DO HEREBY CERTIFY THATTHIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY R CORD H B PROVIDED TO THE WELL OWNER.
/Z /j 2oao
FOR OFFICE USE ONLY (SIdNATURff OF PERSON dONSTRUCTING THE WELL) (DATE)
Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days.
c ,.;. t h l
P
WITHERS & RA MVEL
Engineering &Surveying, Inc
LOG OF BORING MW-4
WIdiPRSkRAYFYHl 711 MacKenm Drive - Cary, N.C.27511
(Page 1 of 1)
Dept of Agriculture/State Fair
Date Started
: 11/7/2000 Drilling Company
: GeoTechnologies, Inc.
Nowell Road
Date Completed
:11/1012000 Northing Coord.
: NIA
Raleigh, NC
Hole Diameter
: 8.5 in. Easting Coord.
: N/A
Project # 200082.0
Drilling Method
: H.SA Survey By
: WRES
Sampling Method
: Split Spoon Logged By
: Ty Colwell
U
Depth
in m Q
Feet � rC
0
5
10
ML
15
z 0 25
m
N
m
oO_
O
O
z
a
30
Q
z
w
N
N 35
SM
DESCRIPTION
and Light Brown Layers ~ V
Well: MW-4
0 FID Elev.:433.33
E o (ppm) Cover
CU co m o 1 fl
F2]1
66 91
❑ 6 I
7
❑I 8
Stiff Micaceous SANDY SILT with ❑ 4
traces of PARTIALLY WEATHERED 5 s
8
ROCK, Red, Gray, Gold and Light
Brown Layers
Boring terminated at 30.0 feet. Installed
groundwater monitoring well.
Grout
Casing
Bentonite
Screen
Sand pack
Well Construction
Information
WELL CONSTRUCTION
Date Compl.: 11/1012000
Hole Dia. : 8.5 in.
Drill. Method : HSA
Company Rep.
WELL CASING
Material : Sch 40 PVC
Diameter :2 in.
Joints :threaded
WELL SCREEN
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
Opening :.010 slot
SAND PACK: medium
SEAL : bentonite
NOTES
Groundwater is approx.
18.5 feet below ground
surface. Top of casing is
2.88 feet above ground
surface. Elevation shown is
ground surface elevation.
North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 27699-1636-Phone (919) 733-3221
` WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnolociees, Inc.
WELL CONSTRUCTION CERTIFICATION #: 2504
MW-4 STATE WELL CONSTRUCTION PERMIT #: 2504
1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCATION: (Show sketch of the location below)
Nearest Town: Raleigh County: Wake
Nowell Road
(Road Name and Numbers, Community, or Subdivision and Lot No.) MW-4
3. OWNER: Department of Aariculturel State Fair
Address:. 1025 Blue Ridge Road
Raleigh NC 27607
(City or town) (State) (Zip Code)
4. DATE DRILLED 11I712000
5. TOTAL DEPTH 30.0
6. CUTTINGS COLLECTED YES[!] NO®
7. DOES WELL REPLACE EXISTING WELL? YES[:] NO®
8. STATIC WATER LEVEL Below Top.of Casing) 18.5 Ft.
(Use'+"d Above Top of Casing)
9. TOP OF CASING IS +2.88 Ft above Land Surface*
'Top of rasing tordnated atror bebw land surface requires a variance In Accordance WAh 15A NCAV 2C.0118
10. YIELD (gpm) NIA METHOD OF TEST
11. WATER ZONES (depth) NIA
WA
12. CLORINATION:
Type NIA
Amount NIA
13. CASING
Depth
Diameter
Wall Thickness
Material
Or WeightiFt
From 11.0 To +2.88
Ft. 2"
Sch.40
PVC
From To
Ft.
From To
FL
14. GROUT
Depth
Material
Method
From 7.0 To 0.0
Ft. Neat Cement
Pump & Trim
From To
Ft
15. SCREEN
Depth
Diameter
Slot Size
Material
From 26.0 To 11.0
FL 2 In
0.010
In
PVC
From To
Ft In
In
From To
Ft In
In
16. SAND/GRAVEL PACK:
Depth
Size
Material
From 30.0 To 9.0
Ft. #2
Sand
From To
FL
17. REMARKS: Bentonite Pluq
from 9.0 feet to 7.0
feet.
DRILLING LOG
From To
DEPTH
Formation Description
0.0
3"
Topsoil
3"
23.5
Micaceous silt,
purple, gold, red
and light brown
layers
23.5
30.0
Micaceous sandy
silt with traces of
partially weathered
rock, red, gray, gold
and light brown
layers
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY OF THIS RECORD HAS-BEEN.PROVIDED TO THE WELL OWNER.
/2 /3 2000
FOR OFFICE USE ONLY (SIGNATURE OV PERSON C NSTRUCTING THE WELL) (DATE)
Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days.
WITHERS & RAYENEL
Engineering & Surveying, fne-
LOG OF BORING M W-5
111 MacKsnan Drive - Cary, N.C. 27511
wrffreRsrr��
(Page 1 of 1)
Dept. of Agricutture/State Fair
Date Started
: 11f7/2000 Drilling Company
: Geo-rechnologies, Inc.
Nowell Road
Date Completed
: 11/1012000 Northing Coord.
: N/A
Raleigh, NC
Hole Diameter
: &5 in. Easting Ccord.
: N/A
Project # 200082.0
Drilling Method
: H-SA Survey By
: WRES
Sampling Method
: Sprit Spoon Logged By
: Ty Colwell
U
Depth r
in o7 a
Feet �
� U
0
ALI
5
SM
10
DESCRIPTION
Stiff Micaceous SILT, Brown
Stiff to very stiff Micaceous SAND
SILT, Gray, Gold and Light Brown
Layers
c Well: MW-5
F!D Elev.:431.77
E U o
c(PPm) Cover
`o m o 1 F I
3
3 4
15 Medium Stiff Micaceous SANDY SILT 5
with traces of PARTIALLY WEATHERED
ROCK, Red, Gray, Gold and Light
Brown Layers
20� SM
Boring terminated at 25.0 feet. Installed
groundwater monitoring well.
El
3
Screen
Sand Pack
Well Construction
Information
WELL CONSTRUCTION
Date Compl. :1111012000
Hole Dia. : 8.5 in.
Drill. Method : HSA
Company Rep.
WELL CASING
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
WELL SCREEN
Material : Sch 40 PVC
Diameter : 2 in.
Joints : threaded
Opening :.010 slot
SAND PACK: medium
SEAL : bentonite
NOTES
Groundwater is approx.
12.9 feet below ground
surface. Top of casing is
1.82 feet above ground
surface. Elevation shown is
ground surface elevation.
V
Ngrth Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section
1636 Mail Service Center - Raleigh, N.C. 276991636-Phone (919) 733-3221
WELL CONSTRUCTION RECORD WELL CONTRACTOR: GeoTechnologies, Inc.
WELL CONSTRUCTION CERTIFICATION #: 2504
MW-S STATE WELL CONSTRUCTION PERMIT #: 2504
1. WELL USE (Check Applicable Box): Municipal ❑ Industrial ❑ Agricultural ❑ Monitoring
Recovery ❑ Heat Pump Water Injection ❑ Other ❑ If Other, List Use:
2. WELL LOCH 1-ION: (Show sketch of the location below)
Nearest Town: Raleigh County: Wake
Nowell Road
(Road Name and Numbers, Community, or Subdivision and Lot No.)
3. OWNER: Department of AQ6cultur/ State Fair
Address: 1025 Blue Ridge Road
Raleigh NC 27607
(City or Town) (State) (zip Code)
4. DATE DRILLED 11[7/2000
5. TOTAL DEPTH 25.0
6. CUTTINGS COLLECTED YES[:] NO®
7. DOES WELL REPLACE EXISTING WELL? YES[:] NON
8. STATIC WATER LEVEL Below Top of Casing) 12.9 Ft.
(Use "+" if Above Top of casing)
9. TOP OF CASING IS +1.82 Ft above Land Surface*
'Top of casing terminated atlor below land surface requires a variance In Accordance Wilh 15A NCAV 2CD118
10. YIELD (gpm) N/A METHOD OF TEST N/A
11. WATER ZONES (depth) N/A
12. CLORINATION:
Type N/A
Amount N/A
13. CASING
Depth
Diameter
Wall Thickness
Material
Or WeighttFt.
From 8.0 To +1.82
Ft. 2"
Sch.40
PVC
From To
Ft.
From To
Ft.
14. GROUT
Depth
Material
Method
From 4.0 To 0.0
Ft. Neat Cement
Pump & Trim
From To
Ft.
15. SCREEN
Depth
Diameter
Slot Size
Material
From 23.0 To 8.0
Ft. 2 In
0.010
In
PVC
From To
Ft. In
In
From To
Ft. In
In
16. SAND/GRAVEL PACK:
Depth
Size
Material
From 25.0 To 6.0
Ft. #2
Sand
From To
Ft.
17. REMARKS: Bentonite Plug from 6.0 feet to 4.0
feet.
DRILLING LOG
From To
DEPTH
Formation Description
0.0
3n
Topsoil
3"
2.0
Mic. silt, brown
2.0
14.5
Mic. sandy silt,
gray, gold and light
brown layers
14.5
25.0
Micaceous sandy
silt with traces of
partially weathered
rock, red, gray, gold
and light brown
layers
If additional space is needed use back of form.
LOCATION SKETCH
(Show direction and distance from at least two State
Roads, or other map reference points)
I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION
STANDARDS, AND THAT A COPY OFITIJJS RECORD S B PROVIDED TO THE WELL OWNER.
/2 /3/C»o
FOR OFFICE USE ONLY (SI ATURE OF PERSON(CONSTRUCTING THE WELL) (DATE)
Quad no: Submit original to Division of Water Quality, Groundwater Section within 30 days.
APPENDIX B
FIELD NOTES
Page of
Job Number
Groundwater Sampling Form State ID
Well ID I.
Site Name t., f r I 4...Jf!Date
Well Depth Depth to Water . `r Well Diameter
Casing Material Screen Length Well Water Volume
Sampling Crew
Pump Type Tubing Type Intake set at
Weather Conditions Notes (eg odor or color)
Time Water Level Volume Purged DO Temp EC pH ORP Turbidity
KUM
Other Parameters
Sampled at l rJ Parameters taken with
Samples delivered to by at
.Analysis
VOCs
Preservative
HCL
Bottle ware
40 ml VOAs glass
Number of Bottles Hold Time
14 Days
SVOCs
None
1 Liter glass
7 Days
Metals
Nitric Acid
250 ml plastic
180 Days
NO3+NO2
Sulfuric Acid
125 ml plastic
28 Days
Herbicides
None
1 Liter glass
7 days
Pesticides
None
1 Liter glass
7 Days
Other
Well Volume Ualculat[on
1" well [well depth -depth to water] x 0.0408 gallons/ft. x 3 = 0.124/ft. _
2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft =
4" well [well depth -depth to water] x 0.653 gallons/ft. x 3 = 1.959/ft =
C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016
Page of
i! - Your Succe--
Job Number
Groundwater Sampling Form State ID
]] � Well ID W 1
Site Name `fGf� ;,("r �,� Date t
Well Depth Depth to Water 5,56 Well Diameter
Casing Material Screen Length Well Water Volume
Sampling Crew
Pump Type Tubing Type Intake set at
Weather Conditions _ Notes (eg. odor or color)
Time Water Level Volume Purged DO Temp EC pH ORP Turbidity
124 Hr.) (from TOM IGals 1 Imnll 1 toM h iC/rm% kfnnHnrr % !m\/1 WTI 1)
Other Parameters
Sampled at Parameters taken with
Samples delivered to rby at
Analysis
Preservative
Bottle ware
Number of Bottles Hold Time
VOCs
HCL
40 ml VOAs glass
14 Days
SVOCs
None
1 Liter glass
7 Days
Metals
Nitric Acid
250 ml plastic
180 Days
NO3+NO2
Sulfuric Acid
125 ml plastic
28 Days
Herbicides
None
1 Liter glass
7 days
Pesticides
None
1 Liter glass
7 Days
Other
Well Volume Calculation
1 " well [well depth -depth to water] x 0.0408 gallons/ft. x 3 = 0.124/ft. _
2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft =
4" well [well depth -depth to water] x 0.653 gallons/ft. x 3 = 1.959/ft =
C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016
Page of
Job Number
Groundwater Sampling Form State ID
Well ID f-A�_j _
Site Name Date
Well Depth _ Depth to Watery '• Well Diameter
Casing Material Screen Length Well Water Volume
Sampling Crew
Pump Type Tubing Type Intake set at
Weather Conditions Notes (eg. odor or color)
Time Water Level Volume Purged DO Temp EC pH ORP Turbidity
(94 Hr )i lfrnm Tnr.7 ft;alc ) tmnll 1 (Cry (Wqh-m) 1&nnrinrrl) IMM W71 i%
rl
MdM
EN
utner rarameters
Sampled at
Samples delivered to
Parameters taken with
by
at
Analysis
Preservative
Bottle ware
Number of Bottles Hold Time
VOCs
HCL
40 ml VOAs glass
14 Days
SVOCs
None
1 Liter glass
7 Days
Metals
Nitric Acid
250 ml plastic
180 Days
NO3+NO2
Sulfuric Acid
125 ml plastic
28 Days
Herbicides
None
1 Liter glass
7 days
Pesticides
None
1 Liter glass
7 Days
Other
vven volume ua[cu[anon
1 n well [well depth -depth to water] x
2" well [well depth -depth to water] x
4° well [well depth -depth to water] x
0.0408 gallons/ft. x 3 = 0.124/ft. _
0.163 gallons/ft. x 3 = 0.489/ft =
0.653 gallons/ft. x 3 = 1.959/ft =
C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016
% 0 V f i1 � -n r s R v -, 1 Page of
Our Per3ple, Your Success
Job Number
Groundwater Sampling Form State ID
Qp r Well ID Ul 1 JLd
Site Name r,,,-l` Date
Well Depth d Depth to Water Well Diameter
Casing Material Screen Length Well Water Volume
Sampling Crew
Pump Type Tubing Type Intake set at
Weather Conditions Notes (eg. odor or color)
Time Water Level Volume Purged DO Temp EC pH ORP Turbidity
(24 Hr 1 (frnm TC)('. (("aIQ ) lmnll 1 !or`l e Q/..—I i-4--.,A. ,A) r—%M /KiTi I%
outer rararneters
Sampled at L(5 Parameters taken with
Samples delivered to by at
Analysis
Preservative
Bottle ware
Number of Bottles Hold Time
VOCs
SVOCs
Metals
NO3+NO2
Herbicides
Pesticides
Other
HCL
None
Nitric Acid
Sulfuric Acid
None
None
40 ml VOAs glass
1 Liter glass
250 ml plastic
125 ml plastic
1 Liter glass
1 Liter glass
14 Days
7 Days
180 Days
28 Days
7 days
7 Days
• vn V v U1 I lu oar UlQ Llul I
1" well [well depth -depth to water] x 0.0408 gallonslft. x 3 = 0.124/ft. _
2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft =
4" well [well depth -depth to water] x 0.653 gallons/ft. x 3 = 1.959/ft =
C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016
Page of
NO Our neopl.,
Job Number
Groundwater Sampling Form State ID
Well ID
Site Namer �ct �}c�'� Date
Well Depth .� Depth to Well Diameter
Casing Material Screen Length Well Water Volume
Sampling Crew
Pump Type Tubing Type Intake set at
Weather Conditions Notes (eg. odor or color)
Time Water Level Volume Purged DO Temp EC pH ORP Turbidity
(24 Hr.l rfrnm T(-)r..) (talc 1 fmr/I ) lot,% I'.C/--%
vU IGI f-OI QI1 ICLCI J
Sampled at Parameters taken with
Samples delivered to by at
Analysis
Preservative
Bottle ware
Number of Bottles Hold Time
VOCs
SVOCs
Metals
NO3+NO2
Herbicides
Pesticides
Other
HCL
None
Nitric Acid
Sulfuric Acid
None
None
40 ml VOAs glass
1 Liter glass
250 ml plastic
125 ml plastic
1 Liter glass
1 Liter glass
14 Days
7 Days
180 Days
28 Days
7 days
7 Days
vv Gu vv U11 IC. Va UUIQIRAI
1"well [well depth -depth to water] x 0.0408 gallons/ft. x 3 = 0.124/ft. _
2" well [well depth -depth to water] x 0.163 gallons/ft. x 3 = 0.489/ft =
4" well [well depth -depth to water] x 0.653gallons/ft. x 3 = 1.959/ft =
C:\Users\jgarrett\Desktop\Revised GW Sampling Form 2016
APPENDIX C
ANALYTICAL REPORT
2�SQ ENCO Laboratories
9g
Accurate. Timely. Respousive. luuavative.
102-A Woodwinds Industrial Court
Cary NC, 27511
Phone: 919.467.3090 FAX: 919.467.3515
Tuesday, July 30, 2019
Withers & Ravenel Environmental (WI009)
Attn: Matt James
115 MacKenan Drive
Cary, NC 27511
RE: Laboratory Results for
Project Number: 02000082.20, Project Name/Desc: Closed State Fairgrounds Landfill
ENCO Workorder(s): CC11273
Dear Matt James,
Enclosed is a copy of your laboratory report for test samples received by our laboratory on
Friday, July 19, 2019.
Unless otherwise noted in an attached project narrative, all samples were received in
acceptable condition and processed in accordance with the referenced methods/procedures.
Results for these procedures apply only to the samples as submitted.
The analytical results contained in this report are in compliance with NELAC standards, except
as noted in the project narrative if applicable. This report shall not be reproduced except in
full, without the written approval of the Laboratory.
This report contains only those analyses performed by Environmental Conservation
Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from
outside organizations will be reported under separate cover.
If you have any questions or require further information, please do not hesitate to contact me.
Sincerely,
OUCLC'=-:�CA
Chuck Smith
Project Manager
Enclosure(s)
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 28
(� �Eo
www.encolabs.com
SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: MW-1
Lab ID: CC11273-01
Sampled: 07/18/19 11:30
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
O1/14/20
07/25/19 06:36
07/26/19 11:27
EPA 6010D
EPA 3005A
O1/14/20
07/25/19 09:34
07/29/19 13:21
EPA 7470A
EPA 7470A
08/15/19
07/29/19 13:02
07/30/19 10:51
EPA 8260D
EPA 503013_MS
08/01/19
07/24/19 00:00
07/24/19 16:24
EPA 8260D
EPA 503013_MS
08/01/19
07/25/19 15:06
07/25/19 21:17
Client ID: MW-2
Lab ID: CC11273-02
Sampled: 07/18/19 12:55
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
O1/14/20
07/25/19 09:34
07/29/19 14:40
EPA 7470A
EPA 7470A
08/15/19
07/29/19 13:02
07/30/19 11:04
EPA 8260D
EPA 503013_MS
08/01/19
07/24/19 00:00
07/24/19 17:01
EPA 8260D
EPA 503013_MS
08/01/19
07/25/19 15:06
07/25/19 21:49
Client ID: MW-3
Lab ID: CC11273-03
Sampled: 07/18/19 14:15
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
01/14/20
07/25/19 09:34
07/29/19 13:36
EPA 7470A
EPA 7470A
08/15/19
07/29/19 13:02
07/30/19 11:06
EPA 8260D
EPA 5030B_MS
08/01/19
07/24/19 00:00
07/24/19 17:37
EPA 8260D
EPA 5030B_MIS
08/01/19
07/25/19 15:06
07/25/19 22:20
Client ID: MW-3
Lab ID: CC11273-03RE1
Sampled: 07/18/19 14:15
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
O1/14/20
07/25/19 09:34
07/29/19 15:29
Client ID: MW-4
Lab ID: CC11273-04
Sampled: 07/18/19 14:55
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
01/14/20
07/25/19 09:34
07/29/19 13:39
EPA 7470A
EPA 7470A
08/15/19
07/29/19 13:02
07/30/19 11:08
EPA 8260D
EPA 503013_MS
08/01/19
07/24/19 00:00
07/24/19 18:14
EPA 8260D
EPA 5030B_MS
08/01/19
07/25/19 15:06
07/25/19 22:51
Client ID: MW-5
Lab ID: CC11273-05
Sampled: 07/18/19 13:35
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
O1/14/20
07/25/19 09:34
07/29/19 13:41
EPA 7470A
EPA 7470A
08/15/19
07/29/19 13:02
07/30/19 11:15
EPA 8260D
EPA 503013_MS
08/01/19
07/24/19 00:00
07/24/19 18:50
EPA 8260D
EPA 503013_MS
08/01/19
07/25/19 15:06
07/25/19 23:23
Client ID: SA-1
Lab ID: CC11273-06
Sampled: 07/18/19 15:30
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
O1/14/20
07/25/19 09:34
07/29/19 13:44
EPA 7470A
EPA 7470A
08/15/19
07/29/19 13:02
07/30/19 11:17
EPA 8260D
EPA 5030B_MIS
08/01/19
07/24/19 00:00
07/24/19 19:27
EPA 8260D
EPA 503013_MS
08/01/19
07/25/19 15:06
07/25/19 23:54
Client ID: SA-2
Lab ID: CC11273-07
Sampled: 07/18/19 16:00
Received: 07/19/19 14:20
Parameter
Preparation
Hold Date/Time(s)
Prep Date/Time(s)
Analysis Date/Time(s)
EPA 6010D
EPA 3005A
O1/14/20
07/25/19 09:34
07/29/19 13:55
EPA 7470A
EPA 7470A
08/15/19
07/29/19 13:02
07/30/19 11:20
EPA 8260D
EPA 50306_MS
08/01/19
07/24/19 00:00
07/24/19 20:04
EPA 8260D
EPA 503013_MS
08/01/19
07/25/19 15:06
07/26/19 00:25
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 28
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SAMPLE SUMMARY/LABORATORY CHRONICLE
Client ID: Trip Blank Lab ID: CC11273-08 Sampled: 07/18/19 11:30 Received: 07/19/19 14:20
Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s)
EPA 8260D EPA 503013_MS 08/01/19
EPA 8260D EPA 5030B_MS 08/01/19
07/24/19 00:00 07/24/19 20:41
07/25/19 15:06 07/26/19 00:57
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 28
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SAMPLE DETECTION SUMMARY
Client ID: MW-1 Lab ID: CC11273-01
Anala Results Flag MDL POLL Units Method Notes
Barium - Total
16.7 1.10 10.0
EPA 6010D
Client ID: MW-2 Lab ID: CC11273-02
Anala Results Flag MDL POLL Units Method Notes
Barium - Total 152 1.10 10.0 ug/L EPA 6010D
Cadmium - Total
0.690
1
0.360
1.00
ug/L
EPA 6010D
Client ID: MW-3
Lab ID:
CC11273-03
Anala
Barium - Total
Chromium - Total
Results
195
2.35
Flag
1
MDL
1.10
1.40
POLL
10.0
10.0
Units
ug/L
ug/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID: MW-3
Lab ID:
CC11273-03RE3
Anala
Selenium - Total
Results
76.4
Flag
ID
MDL
62.0
POLL
100
Units
ug/L
Method
EPA 6010D
Notes
R-05
Client ID: MW-4
Lab ID:
CC11273-04
Anala
Barium - Total
Cadmium - Total
Results
35.8
0.586
Flag
1
MDL
1.10
0.360
POLL
10.0
1.00
Units
ug/L
ug/L
Method
EPA 6010D
EPA 6010D
Notes
Client ID: MW-5
Lab ID:
CC11273-05
Anala
Barium - Total
Results
35.2
Flag
MDL
1.10
POLL
10.0
Units
ug/L
Method
EPA 6010D
Notes
Client ID: SA-1
Lab ID:
CC11273-06
Anala
Barium - Total
Results
39.5
Flag
MDL
1.10
POLL
10.0
Units
ug/L
Method
EPA 6010D
Notes
Client ID: SA-2
Lab ID:
CC11273-07
Anala
Barium - Total
Results
23.7
Flag
MDL
1.10
POLL
10.0
Units
ug/L
Method
EPA 6010D
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 28
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ANALYTICAL RESULTS
Description: MW-1 Lab Sample ID: CC11273-01 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 11:30 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flao
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/25/19 21:17
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/25/19 21:17
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/25/19 21:17
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/25/19 21:17
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/25/19 21:17
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/25/19 21:17
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1 1.5
5.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Chloroethane [75-00-31^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1 0.18
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1 0.20
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1 0.27
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1 1.7
5.0
9G25033
EPA 8260D
07/25/19
21:17
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1 0.17
2.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1 0.065
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Styrene[100-42-5]^
0.11
u
ug/L
1 0.11
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Toluene [108-88-3]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1 0.21
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1 0.70
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1 0.24
1.0
9G25033
EPA 8260D
07/25/19
21:17
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1 0.95
5.0
9G25033
EPA 8260D
07/25/19
21:17
REF
FINAL
This report relates only
to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 5 of 28
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www.encolabs.com
ANALYTICAL RESULTS
Description: MW-1 Lab Sample ID: CC11273-01 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 11:30 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 21:17 REF
Xylenes(Total)[1330-20-7]^ 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 21:17 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
55
1
50.0
110 %
53-136
9G25033
EPA 8260D
07125119 21:17
REF
Dlbromofluoromethane
51
1
50.0
102 %
67-129
9G25033
EPA 8260D
07125119 21:17
REF
Toluene-d8
48
1
50.0
96 %
59-134
9G25033
EPA 8260D
07125119 21:17
REF
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
u
ug/L
1
0.150 0.200
9G29038
EPA 7470A
07/30/19 10:51
RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60 10.0
9G25003
EPA 6010D
07/26/19 11:27
JDH
Barium [7440-39-3]^
16.7
ug/L
1
1.10 10.0
9G25003
EPA 6010D
07/26/19 11:27
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360 1.00
9G25003
EPA 6010D
07/26/19 11:27
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40 10.0
9G25003
EPA 6010D
07/26/19 11:27
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10 10.0
9G25003
EPA 6010D
07/26/19 11:27
JDH
Selenium [7782-49-2]^
6.20
u
ug/L
1
6.20 10.0
9G25013
EPA 6010D
07/29/19 13:21
JDH
Silver [7440-22-4]^
1.90
u
ug/L
1
1.90 10.0
9G25003
EPA 6010D
07/26/19 11:27
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.2
u
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 16:24
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
5.3
1
5.00
107 %
75-125
9G24024
EPA 8260D
0712411916:24
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 28
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ANALYTICAL RESULTS
Description: MW-2 Lab Sample ID: CC11273-02 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 12:55 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flao
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/25/19 21:49
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/25/19 21:49
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/25/19 21:49
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/25/19 21:49
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1
1.5
5.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Chloroethane [75-00-31^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1
0.18
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1
0.20
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1
0.27
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1
1.7
5.0
9G25033
EPA 8260D
07/25/19 21:49
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1
0.17
2.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1
0.065
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Styrene[100-42-5]^
0.11
u
ug/L
1
0.11
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Toluene [108-88-3]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1
0.70
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1
0.24
1.0
9G25033
EPA 8260D
07/25/19 21:49
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1
0.95
5.0
9G25033
EPA 8260D
07/25/19 21:49
REF
FINAL
This report relates only
to the sample as received by the laboratory,
and may only be reproduced in full.
Page 7 of 28
(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-2 Lab Sample ID: CC1 1273-02 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 12:55 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 21:49 REF
Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 21:49 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
54
1
50.0
109 %
53-136
9G25033
EPA 8260D
07125119 21:49
REF
Dlbromofluoromethane
52
1
50.0
105 %
67-129
9G25033
EPA 8260D
07125119 21:49
REF
Toluene-d8
49
1
50.0
97 %
59-134
9G25033
EPA 8260D
07125119 21:49
REF
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
u
ug/L
1
0.150 0.200
9G29038
EPA 7470A
07/30/19 11:04
RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60 10.0
9G25013
EPA 6010D
07/29/19 14:40
JDH
Barium [7440-39-3]^
152
ug/L
1
1.10 10.0
9G25013
EPA 6010D
07/29/19 14:40
JDH
Cadmium [7440-43-9]^
0.690
J
ug/L
1
0.360 1.00
9G25013
EPA 6010D
07/29/19 14:40
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40 10.0
9G25013
EPA 6010D
07/29/19 14:40
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10 10.0
9G25013
EPA 6010D
07/29/19 14:40
JDH
Selenium [7782-49-2]^
6.20
u
ug/L
1
6.20 10.0
9G25013
EPA 6010D
07/29/19 14:40
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90 10.0
9G25013
EPA 6010D
07/29/19 14:40
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
1,4-Dioxane [123-91-1]^
1.2
u
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 17:01
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
5.4
1
5.00
109 %
75-125
9G24024
EPA 8260D
0712411917:01
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 28
00�
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-3 Lab Sample ID: CC11273-03 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 14:15 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flao
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/25/19
22:20
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/25/19
22:20
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/25/19
22:20
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/25/19
22:20
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1 1.5
5.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Chloroethane [75-00-31^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1 0.18
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1 0.20
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1 0.27
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1 1.7
5.0
9G25033
EPA 8260D
07/25/19
22:20
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1 0.17
2.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1 0.065
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Styrene[100-42-5]^
0.11
u
ug/L
1 0.11
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Toluene [108-88-3]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1 0.21
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1 0.70
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1 0.24
1.0
9G25033
EPA 8260D
07/25/19
22:20
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1 0.95
5.0
9G25033
EPA 8260D
07/25/19
22:20
REF
FINAL
This report relates only
to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 9 of 28
(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-3 Lab Sample ID: CC1 1273-03 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 14:15 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 22:20 REF
Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 22:20 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
56
1
50.0
ill %
53-136
9G25033
EPA 8260D
07125119 22:20
REF
Dlbromofluoromethane
50
1
50.0
99 %
67-129
9G25033
EPA 8260D
07125119 22:20
REF
Toluene-d8
48
1
50.0
97 %
59-134
9G25033
EPA 6260D
07125119 22:20
REF
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
Mercury [7439-97-6]^
0.150
u
ug/L
1
0.150 0.200
9G29038
EPA 7470A
07/30/19 11:06
RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60 10.0
9G25013
EPA 6010D
07/29/19 13:36
JDH
Barium [7440-39-3]^
195
ug/L
1
1.10 10.0
9G25013
EPA 6010D
07/29/19 13:36
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360 1.00
9G25013
EPA 6010D
07/29/19 13:36
JDH
Chromium [7440-47-3]^
2.35
J
ug/L
1
1.40 10.0
9G25013
EPA 6010D
07/29/19 13:36
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10 10.0
9G25013
EPA 6010D
07/29/19 13:36
JDH
Selenium [7782-49-2]^
76.4
JD
ug/L
10
62.0 100
9G25013
EPA 6010D
07/29/19 15:29
JDH
R-05
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90 10.0
9G25013
EPA 6010D
07/29/19 13:36
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte fCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.2
u
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 17:37
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-&
5.5
1
5.00
110 %
75-125
9G24024
EPA 8260D
071241191737
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 28
00�
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-4 Lab Sample ID: CC11273-04 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 14:55 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flao
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/25/19 22:51
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/25/19 22:51
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/25/19 22:51
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/25/19 22:51
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/25/19 22:51
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/25/19 22:51
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1 1.5
5.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Chloroethane [75-00-31^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1 0.18
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1 0.20
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1 0.27
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1 1.7
5.0
9G25033
EPA 8260D
07/25/19
22:51
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1 0.17
2.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1 0.065
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Styrene[100-42-5]^
0.11
u
ug/L
1 0.11
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Toluene [108-88-3]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1 0.21
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1 0.70
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1 0.24
1.0
9G25033
EPA 8260D
07/25/19
22:51
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1 0.95
5.0
9G25033
EPA 8260D
07/25/19
22:51
REF
FINAL
This report relates only
to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 11 of 28
(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-4 Lab Sample ID: CC1 1273-04 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 14:55 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 22:51 REF
Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 22:51 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
57
1
50.0
115 %
53-136
9G25033
EPA 8260D
07125119 22:51
REF
Dlbromofluoromethane
51
1
50.0
102 %
67-129
9G25033
EPA 8260D
07125119 22:51
REF
Toluene-d8
49
1
50.0
98 %
59-134
9G25033
EPA 8260D
07125119 22:51
REF
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
Mercury [7439-97-6]^
0.150
u
ug/L
1
0.150 0.200
9G29038
EPA 7470A
07/30/19 11:08
RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60 10.0
9G25013
EPA 6010D
07/29/19 13:39
JDH
Barium [7440-39-3]^
35.8
ug/L
1
1.10 10.0
9G25013
EPA 6010D
07/29/19 13:39
JDH
Cadmium [7440-43-9]^
0.586
J
ug/L
1
0.360 1.00
9G25013
EPA 6010D
07/29/19 13:39
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40 10.0
9G25013
EPA 6010D
07/29/19 13:39
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10 10.0
9G25013
EPA 6010D
07/29/19 13:39
JDH
Selenium [7782-49-2]^
6.20
u
ug/L
1
6.20 10.0
9G25013
EPA 6010D
07/29/19 13:39
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90 10.0
9G25013
EPA 6010D
07/29/19 13:39
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.2
u
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 18:14
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
5.5
1
5.00
109 %
75-125
9G24024
EPA 8260D
0712411918:14
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 28
00�
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-5 Lab Sample ID: CC11273-05 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 13:35 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flao
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/25/19
23:23
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/25/19
23:23
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/25/19
23:23
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/25/19
23:23
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1 1.5
5.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Chloroethane [75-00-3]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1 0.18
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1 0.20
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1 0.27
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1 1.7
5.0
9G25033
EPA 8260D
07/25/19
23:23
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1 0.17
2.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1 0.065
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Styrene[100-42-5]^
0.11
u
ug/L
1 0.11
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Toluene [108-88-3]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1 0.21
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1 0.70
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1 0.24
1.0
9G25033
EPA 8260D
07/25/19
23:23
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1 0.95
5.0
9G25033
EPA 8260D
07/25/19
23:23
REF
FINAL
This report relates only
to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 13 of 28
(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: MW-5 Lab Sample ID: CC11273-05 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 13:35 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 23:23 REF
Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 23:23 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
56
1
50.0
113 %
53-136
9G25033
EPA 8260D
07125119 23:23
REF
Dlbromofluoromethane
50
1
50.0
100 %
67-129
9G25033
EPA 8260D
07125119 23:23
REF
Toluene-d8
50
1
50.0
99 %
59-134
9G25033
EPA 8260D
07125119 23:23
REF
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
u
ug/L
1
0.150 0.200
9G29038
EPA 7470A
07/30/19 11:15
RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60 10.0
9G25013
EPA 6010D
07/29/19 13:41
JDH
Barium [7440-39-3]^
35.2
ug/L
1
1.10 10.0
9G25013
EPA 6010D
07/29/19 13:41
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360 1.00
9G25013
EPA 6010D
07/29/19 13:41
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40 10.0
9G25013
EPA 6010D
07/29/19 13:41
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10 10.0
9G25013
EPA 6010D
07/29/19 13:41
JDH
Selenium [7782-49-2]^
6.20
u
ug/L
1
6.20 10.0
9G25013
EPA 6010D
07/29/19 13:41
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90 10.0
9G25013
EPA 6010D
07/29/19 13:41
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.2
u
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 18:50
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
5.0
1
5.00
99 %
75-125
9G24024
EPA 8260D
0712411918:50
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 28
00�
www.encolabs.com
ANALYTICAL RESULTS
Description: SA-1 Lab Sample ID: CC11273-06 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 15:30 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flag
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/25/19
23:54
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/25/19
23:54
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/25/19
23:54
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/25/19
23:54
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1 1.5
5.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Chloroethane [75-00-31^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1 0.18
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1 0.20
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1 0.27
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1 1.7
5.0
9G25033
EPA 8260D
07/25/19
23:54
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1 0.17
2.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1 0.065
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Styrene[100-42-5]^
0.11
u
ug/L
1 0.11
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Toluene [108-88-3]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1 0.21
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1 0.70
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1 0.24
1.0
9G25033
EPA 8260D
07/25/19
23:54
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1 0.95
5.0
9G25033
EPA 8260D
07/25/19
23:54
REF
FINAL
This report relates only
to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 15 of 28
(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: SA-1 Lab Sample ID: CC1 1273-06 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 15:30 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/25/19 23:54 REF
Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/25/19 23:54 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
56
1
50.0
112 %
53-136
9G25033
EPA 8260D
07125119 23:54
REF
Dlbromofluoromethane
50
1
50.0
100 %
67-129
9G25033
EPA 8260D
07125119 23:54
REF
Toluene-d8
48
1
50.0
96 %
59-134
9G25033
EPA 8260D
07125119 23:54
REF
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
u
ug/L
1
0.150 0.200
9G29038
EPA 7470A
07/30/19 11:17
RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60 10.0
9G25013
EPA 6010D
07/29/19 13:44
JDH
Barium [7440-39-3]^
39.5
ug/L
1
1.10 10.0
9G25013
EPA 6010D
07/29/19 13:44
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360 1.00
9G25013
EPA 6010D
07/29/19 13:44
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40 10.0
9G25013
EPA 6010D
07/29/19 13:44
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10 10.0
9G25013
EPA 6010D
07/29/19 13:44
JDH
Selenium [7782-49-2]^
6.20
u
ug/L
1
6.20 10.0
9G25013
EPA 6010D
07/29/19 13:44
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90 10.0
9G25013
EPA 6010D
07/29/19 13:44
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.2
u
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 19:27
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-d8
5.4
1
5.00
107 %
75-125
9G24024
EPA 8260D
0712411919:27
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 28
00�
www.encolabs.com
ANALYTICAL RESULTS
Description: SA-2 Lab Sample ID: CC11273-07 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 16:00 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flag
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/26/19
00:25
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/26/19
00:25
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/26/19
00:25
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/26/19
00:25
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1 1.5
5.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Chloroethane [75-00-31^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1 0.18
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1 0.20
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1 0.27
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1 1.7
5.0
9G25033
EPA 8260D
07/26/19
00:25
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1 0.17
2.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1 0.065
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Styrene[100-42-5]^
0.11
u
ug/L
1 0.11
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Toluene [108-88-3]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1 0.21
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1 0.70
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1 0.24
1.0
9G25033
EPA 8260D
07/26/19
00:25
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1 0.95
5.0
9G25033
EPA 8260D
07/26/19
00:25
REF
FINAL
This report relates only
to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 17 of 28
(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: SA-2 Lab Sample ID: CC1 1273-07 Received: 07/19/19 14:20
Matrix: Ground Water Sampled:07/18/19 16:00 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By:J.Garrett
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 u ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/26/19 00:25 REF
Xylenes (Total) [1330-20-7]1 0.45 u ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/26/19 00:25 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy
Notes
4-Bromofluorobenzene
55
1
50.0
ill %
53-136
9G25033
EPA 8260D
07126119 00:25
REF
Dlbromofluoromethane
49
1
50.0
97 %
67-129
9G25033
EPA 8260D
07126119 00:25
REF
Toluene-d8
48
1
50.0
97 %
59-134
9G25033
EPA 6260D
07126119 00:25
REF
Metals by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Mercury [7439-97-6]^
0.150
u
ug/L
1
0.150 0.200
9G29038
EPA 7470A
07/30/19 11:20
RLF
Metals (total recoverable) by EPA 6000/7000 Series Methods
^ - ENCO Cary certified analyte [NC 591]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
By
Notes
Arsenic[7440-38-2]^
7.60
u
ug/L
1
7.60 10.0
9G25013
EPA 6010D
07/29/19 13:55
JDH
Barium [7440-39-3]^
23.7
ug/L
1
1.10 10.0
9G25013
EPA 6010D
07/29/19 13:55
JDH
Cadmium [7440-43-9]^
0.360
u
ug/L
1
0.360 1.00
9G25013
EPA 6010D
07/29/19 13:55
JDH
Chromium [7440-47-3]^
1.40
u
ug/L
1
1.40 10.0
9G25013
EPA 6010D
07/29/19 13:55
JDH
Lead [7439-92-1]^
3.10
u
ug/L
1
3.10 10.0
9G25013
EPA 6010D
07/29/19 13:55
JDH
Selenium [7782-49-2]^
6.20
u
ug/L
1
6.20 10.0
9G25013
EPA 6010D
07/29/19 13:55
JDH
Silver[7440-22-4]^
1.90
u
ug/L
1
1.90 10.0
9G25013
EPA 6010D
07/29/19 13:55
JDH
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL PQL
Batch
Method
Analyzed
Ay
Notes
1,4-Dioxane [123-91-1]^
1.2
u
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 20:04
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By
Notes
Toluene-&
5.4
1
5.00
108 %
75-125
9G24024
EPA 8260D
07124119 20:04
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 28
00�
www.encolabs.com
ANALYTICAL RESULTS
Description: Trip Blank Lab Sample ID: CC11273-08 Received: 07/19/19 14:20
Matrix: Water Sampled:07/18/19 11:30 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By: ENCO
Volatile Organic Compounds
by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte fCAS Numberl
Results
Flao
Units
DF
MDL
Q
Batch
Method
Analyzed
By
Notes
1,1,1,2-Tetrachloroethane [630-20-6]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,1,1-Trichloroethane [71-55-6]^
0.12
u
ug/L
1
0.12
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,1,2,2-Tetrachloroethane [79-34-5]^
0.28
u
ug/L
1
0.28
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,1,2-Trichloroethane [79-00-5]^
0.14
u
ug/L
1
0.14
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,1-Dichloroethane [75-34-3]^
0.13
u
ug/L
1
0.13
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,1-Dichloroethene [75-35-4]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,2,3-Trichloropropane [96-18-4]^
0.23
u
ug/L
1
0.23
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,2-Dibromo-3-chloropropane [96-12-8]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,2-Dibromoethane [106-93-4]^
0.66
u
ug/L
1
0.66
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,2-Dichlorobenzene [95-50-1]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,2-Dichloroethane [107-06-2]^
0.21
u
ug/L
1
0.21
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
QV-01
1,2-Dichloropropane [78-87-5]^
0.10
u
ug/L
1
0.10
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
1,4-Dichlorobenzene [106-46-7]^
0.19
u
ug/L
1
0.19
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
2-Butanone [78-93-3]^
1.3
u
ug/L
1
1.3
5.0
9G25033
EPA 8260D
07/26/19
00:57
REF
2-Hexanone [591-78-6]^
0.88
u
ug/L
1
0.88
5.0
9G25033
EPA 8260D
07/26/19
00:57
REF
4-Methyl-2-pentanone [108-10-1]^
1.1
u
ug/L
1
1.1
5.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Acetone [67-64-1]^
10
u
ug/L
1
10
20
9G25033
EPA 8260D
07/26/19
00:57
REF
Acrylonitrile [107-13-1]^
3.5
u
ug/L
1
3.5
10
9G25033
EPA 8260D
07/26/19
00:57
REF
Benzene[71-43-2]^
0.15
u
ug/L
1
0.15
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Bromochloromethane [74-97-5]^
0.48
u
ug/L
1
0.48
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Bromodichloromethane [75-27-4]^
0.17
u
ug/L
1
0.17
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
QV-01
Bromoform [75-25-2]^
0.22
u
ug/L
1
0.22
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
QL-02,
QV-01
Bromomethane [74-83-9]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Carbon disulfide [75-15-0]^
1.5
u
ug/L
1 1.5
5.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Carbon tetrachloride [56-23-5]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
QV-01
Chlorobenzene[108-90-7]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Chloroethane [75-00-31^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Chloroform [67-66-3]^
0.18
u
ug/L
1 0.18
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Chloromethane [74-87-3]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
cis-1,2-Dichloroethene [156-59-2]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
cis-1,3-Dichloropropene [10061-01-5]^
0.20
u
ug/L
1 0.20
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Dibromochloromethane [124-48-1]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Dibromomethane [74-95-3]^
0.27
u
ug/L
1 0.27
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Ethylbenzene[100-41-4]^
0.13
u
ug/L
1 0.13
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Iodomethane [74-88-4]^
1.7
u
ug/L
1 1.7
5.0
9G25033
EPA 8260D
07/26/19
00:57
REF
m,p-Xylenes[108-38-3/106-42-3]^
0.17
u
ug/L
1 0.17
2.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Methylene chloride [75-09-2]^
0.23
u
ug/L
1 0.23
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
o-Xylene [95-47-6]^
0.065
u
ug/L
1 0.065
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Styrene[100-42-5]^
0.11
u
ug/L
1 0.11
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Tetrachloroethene [127-18-4]^
0.17
u
ug/L
1 0.17
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Toluene [108-88-3]^
0.14
u
ug/L
1 0.14
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
trans-1,2-Dichloroethene [156-60-5]^
0.21
u
ug/L
1 0.21
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
trans-1,3-Dichloropropene [10061-02-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
trans-1,4-Dichloro-2-butene [110-57-6]^
0.70
u
ug/L
1 0.70
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
QV-01
Trichloroethene [79-01-6]^
0.15
u
ug/L
1 0.15
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
Trichlorofluoromethane [75-69-4]^
0.24
u
ug/L
1 0.24
1.0
9G25033
EPA 8260D
07/26/19
00:57
REF
QV-01
Vinyl acetate [108-05-4]^
0.95
u
ug/L
1 0.95
5.0
9G25033
EPA 8260D
07/26/19
00:57
REF
FINAL
This report relates only
to the sample as received
by the laboratory,
and may only be reproduced in full.
Page 19 of 28
(� �Eo
www.encolabs.com
ANALYTICAL RESULTS
Description: Trip Blank Lab Sample ID: CC1 1273-08 Received: 07/19/19 14:20
Matrix: Water Sampled:07/18/19 11:30 Work Order: CC11273
Project: Closed State Fairgrounds Landfill Sampled By: ENCO
Volatile Organic Compounds by GCMS
^ - ENCO Cary certified analyte [NC 591]
Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes
Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9G25033 EPA 8260D 07/26/19 00:57 REF
Xylenes (Total) [1330-20-7]1 0.45 U ug/L 1 0.45 3.0 9G25033 EPA 8260D 07/26/19 00:57 REF
Surrogates
Results
DF
Soike Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
ffy Notes
4-Bromofluorobenzene
56
1
50.0
112 %
53-136
9G25033
EPA 8260D
07126119 00:57
REF
Dlbromofluoromethane
49
1
50.0
98 %
67-129
9G25033
EPA 8260D
07126119 00:57
REF
Toluene-d8
49
1
50.0
99 %
59-134
9G25033
EPA 6260D
07126119 00:57
REF
Volatile Organic Compounds by GCMS SIM Isotope Dilution
^ - ENCO Orlando certified analyte [NC 424]
Analyte rCAS Numberl
Results
Flag
Units
DF
MDL POLL
Batch
Method
Analyzed
Ay Notes
1,4-Dioxane [123-91-1]^
1.2
U
ug/L
1
1.2 2.0
9G24024
EPA 8260D
07/24/19 20:41
KKW
Surrogates
Results
DF
So/ke Lv/
% Rec
% Rec Limits
Batch
Method
Ana/vzed
By Notes
Toluene-&
5.2
1
5.00
104 %
75-125
9G24024
EPA 8260D
07124119 20:41
KKW
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 28
(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9G25033 - EPA 5030E MS
Blank (9G25033-BLK3) Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 20:46
Analvte
Result
Flaa
POL
Units
1, 1, 1,2-Tetrachloroethane
0.17
U
1.0
ug/L
1,1,1-Trichloroethane
0.12
U
1.0
ug/L
1,1,2,2-Tetrachloroethane
0.28
U
1.0
ug/L
1,1,2-Trichloroethane
0.14
U
1.0
ug/L
1,1-Dichloroethane
0.13
U
1.0
ug/L
1,1-Dichloroethene
0.21
U
1.0
ug/L
1,2,3-Trichloropropane
0.23
U
1.0
ug/L
1,2-Dibromo-3-chloropropane
0.48
U
1.0
ug/L
1,2-Dibromoethane
0.66
U
1.0
ug/L
1,2-Dichlorobenzene
0.19
U
1.0
ug/L
1,2-Dichloroethane
0.21
U
1.0
ug/L
1,2-Dichloropropane
0.10
U
1.0
ug/L
1,4-Dichlorobenzene
0.19
U
1.0
ug/L
2-Butanone
1.3
U
5.0
ug/L
2-Hexanone
0.88
U
5.0
ug/L
4-Methyl-2-pentanone
1.1
U
5.0
ug/L
Acetone
10
U
20
ug/L
Acrylonitrile
3.5
U
10
ug/L
Benzene
0.15
U
1.0
ug/L
Bromochloromethane
0.48
U
1.0
ug/L
Bromodichloromethane
0.17
U
1.0
ug/L
Bromoform
0.22
U
1.0
ug/L
Bromomethane
0.14
U
1.0
ug/L
Carbon disulfide
1.5
U
5.0
ug/L
Carbon tetrachloride
0.17
U
1.0
ug/L
Chlorobenzene
0.17
U
1.0
ug/L
Chloroethane
0.23
U
1.0
ug/L
Chloroform
0.18
U
1.0
ug/L
Chloromethane
0.13
U
1.0
ug/L
cis- 1,2-Dichloroethene
0.15
U
1.0
ug/L
cis- 1,3-Dichloropropene
0.20
U
1.0
ug/L
Dibromochloromethane
0.17
U
1.0
ug/L
Dibromomethane
0.27
U
1.0
ug/L
Ethylbenzene
0.13
U
1.0
ug/L
Iodomethane
1.7
U
5.0
ug/L
m,p-Xylenes
0.17
U
2.0
ug/L
Methylene chloride
0.23
U
1.0
ug/L
o-Xylene
0.065
U
1.0
ug/L
Styrene
0.11
U
1.0
ug/L
Tetrachloroethene
0.17
U
1.0
ug/L
Toluene
0.14
U
1.0
ug/L
trans-1,2-Dichloroethene
0.21
U
1.0
ug/L
trans-1,3-Dichloropropene
0.15
U
1.0
ug/L
trans-1,4-Dichloro-2-butene
0.70
U
1.0
ug/L
Trichloroethene
0.15
U
1.0
ug/L
Trichlorofluoromethane
0.24
U
1.0
ug/L
Vinyl acetate
0.95
U
5.0
ug/L
Vinyl chloride
0.32
U
1.0
ug/L
Xylenes (Total)
0.45
U
3.0
ug/L
Spike Source %REC RPD
Level Result %REC Limits RPD Limit
Notes
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 28
(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Volatile Organic Compounds by GCMS - Quality Control
Batch 9G25033 - EPA 5030E MS - Continued
Blank (9G25033-BLK3) Continued Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 20:46
Spike Source %REC RPD
Analvte
Result Flaq POL
Units
Level Result %REC Limits RPD Limit Notes
4-Bromofluorobenzene
55
u9/L
50.0 111 53-136
Dibromofluoromethane
51
u9/L
50.0 102 67-129
Toluene-d8
50
u9/L
50.0 100 59-134
LCS (9G25033-BS1)
Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 18:39
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
105
75-133
Benzene
20
1.0
ug/L
20.0
98
80-134
Chlorobenzene
18
1.0
ug/L
20.0
92
80-120
Toluene
18
1.0
ug/L
20.0
88
71-120
Trichloroethene
22
1.0
ug/L
20.0
111
74-120
4-Bromofluorobenzene
56
u9/L
50.0
115
53-136
Dibromofluoromethane
52
u9/L
50.0
103
67-129
Toluene-d8
56
u9/L
50.0
111
59-134
Matrix Spike (9G25033-M81)
Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 19:11
Source: CC12372-09
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
1,1-Dichloroethene
21
1.0
ug/L
20.0
0.21 U
103
75-133
Benzene
20
1.0
ug/L
20.0
0.15 U
99
80-134
Chlorobenzene
18
1.0
ug/L
20.0
0.17 U
90
80-120
Toluene
17
1.0
ug/L
20.0
0.14 U
85
71-120
Trichloroethene
22
1.0
ug/L
20.0
0.15 U
109
74-120
4-Bromofluorobenzene
58
u9/L
50.0
116
53-136
Dibromofluoromethane
51
u9/L
50.0
101
67-129
Toluene-d8
51
u9/L
50.0
101
59-134
Matrix Spike Dup (9G25033-MSD1)
Prepared: 07/25/2019 15:06 Analyzed: 07/25/2019 19:43
Source: CC12372-09
Spike
Source
%REC
RPD
Analvte Result Flaq POL
Units
Level
Result
%REC
Limits
RPD
Limit Notes
1,1-Dichloroethene 21 1.0
ug/L
20.0
0.21 U
106
75-133
2
20
Benzene 19 1.0
ug/L
20.0
0.15 U
93
80-134
5
17
Chlorobenzene 17 1.0
ug/L
20.0
0.17 U
84
80-120
7
16
Toluene 16 1.0
ug/L
20.0
0.14 U
82
71-120
3
17
Trichloroethene 21 1.0
ug/L
20.0
0.15 U
103
74-120
6
22
4-Bromofluorobenzene 55
u9/L
50.0
111
53-136
Dibromofluoromethane 51
u9/L
50.0
103
67-129
Toluene-d8 50
u9/L
50.0
99
59-134
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 9G29038 - EPA 7470A
Blank (9G29038-BLK3) Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:47
Spike Source %REC RPD
Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes
Mercury 0.150 U 0.200 ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 28
(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals by EPA 6000/7000 Series Methods - Quality Control
Batch 9G29038 - EPA 7470A - Continued
LCS (9G29038-BS3) Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:49
Spike
Source
%REC
RPD
Analvte
Result
Flaq
Q
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.18
0.200
ug/L
5.00
104
80-120
Matrix Spike (9G29038-MS1)
Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:54
Source: CC11273-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
4.96
0.200
ug/L
5.00
0.150 U
99
75-125
Matrix Spike Dup (9G29038-MSD1)
Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:56
Source: CC11273-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
4.97
0.200
ug/L
5.00
0.150 U
99
75-125 0.2
25
Post Spike (9G29038-PSI)
Prepared: 07/29/2019 13:02 Analyzed: 07/30/2019 10:59
Source: CC11273-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit
Notes
Mercury
5.75
0.200
ug/L
4.76
0.0343
120
75-125
Metals (total recoverable) by EPA 6000/7000
Series Methods -
Quality Control
Batch 9G25003 - EPA 3005A
Blank (9G25003-BLK3) Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 10:53
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
Blank (9G25003-BLK2)
Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 10:57
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
LCS (9G25003-BS1)
Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 11:02
Spike
Source
%REC RPD
Analvte
Result Flaq
POL
Units
Level
Result %REC
Limits RPD Limit Notes
Arsenic
192
10.0
ug/L
200
96
80-120
Barium
200
10.0
ug/L
200
100
80-120
Cadmium
19.3
1.00
ug/L
20.0
97
80-120
Chromium
193
10.0
ug/L
200
96
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be reproduced in
full. Page 23 of 28
(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9G25003 - EPA 3005A - Continued
LCS (9G25003-BS1) Continued Prepared: 07/25/2019 06:36 Analyzed: 07/26/2019 11:02
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Lead
191
10.0
ug/L
200
95 80-120
Silver
201
10.0
ug/L
200
101 80-120
Matrix Spike (9G25003-MSS)
Prepared:
07/25/2019
06:36 Analyzed: 07/26/2019 11:04
Source: CC09034-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
191
10.0
ug/L
200
7.60 U
95 75-125
Barium
209
10.0
ug/L
200
11.8
98 75-125
Cadmium
19.5
1.00
ug/L
20.0
0.360 U
97 75-125
Chromium
199
10.0
ug/L
200
1.40 U
99 75-125
Lead
198
10.0
ug/L
200
3.10 U
99 75-125
Silver
206
10.0
ug/L
200
1.90 U
103 75-125
Matrix Spike Dup (9G25003-MSDI)
Prepared:
07/25/2019
06:36 Analyzed: 07/26/2019 11:07
Source: CC09034-01
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
192
10.0
ug/L
200
7.60 U
96 75-125 0.8
20
Barium
215
10.0
ug/L
200
11.8
102 75-125 3
20
Cadmium
19.5
1.00
ug/L
20.0
0.360 U
97 75-125 0.07
20
Chromium
197
10.0
ug/L
200
1.40 U
98 75-125 1
20
Lead
194
10.0
ug/L
200
3.10 U
97 75-125 2
20
Silver
204
10.0
ug/L
200
1.90 U
102 75-125 0.9
20
Post Spike (9G25003-PSI)
Prepared:
07/25/2019
06:36 Analyzed: 07/26/2019 11:10
Source: CC09034-01
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Arsenic
0.191
0.0100
mg/L
0.200
-0.00811
96
80-120
Barium
0.208
0.0100
mg/L
0.200
0.0118
98
80-120
Cadmium
0.0195
0.00100
mg/L
0.0200
4.46E-5
97
80-120
Chromium
0.198
0.0100
mg/L
0.200
0.000455
99
80-120
Lead
0.196
0.0100
mg/L
0.200
0.00139
97
80-120
Silver
0.209
0.0100
mg/L
0.200
-0.000309
105
80-120
Batch 9G25013 - EPA 3005A
Blank (9G25013-BLK1)
Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 12:52
Spike
Source
%REC
RPD
Analvte
Result
Flaq
POL
Units
Level
Result
%REC
Limits RPD
Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Selenium
6.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 28
(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9G25013 - EPA 3005A - Continued
Blank (9G25013-BLK2) Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 12:55
Spike Source %REC RPD
Analvte
Result
Flaq
POL
Units
Level Result %REC Limits RPD Limit Notes
Arsenic
7.60
U
10.0
ug/L
Barium
1.10
U
10.0
ug/L
Cadmium
0.360
U
1.00
ug/L
Chromium
1.40
U
10.0
ug/L
Lead
3.10
U
10.0
ug/L
Selenium
6.20
U
10.0
ug/L
Silver
1.90
U
10.0
ug/L
LCS (9G25013-BSI)
Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 13:08
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
197
10.0
ug/L
200
98 80-120
Barium
195
10.0
ug/L
200
98 80-120
Cadmium
20.2
1.00
ug/L
20.0
101 80-120
Chromium
196
10.0
ug/L
200
98 80-120
Lead
193
10.0
ug/L
200
96 80-120
Selenium
209
10.0
ug/L
200
105 80-120
Silver
203
10.0
ug/L
200
101 80-120
Matrix Spike (9G25013-MSS)
Prepared:
07/25/2019
09:34 Analyzed: 07/29/2019 13:11
Source: CC11273-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
POL
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
204
10.0
ug/L
200
7.60 U
102 75-125
Barium
351
10.0
ug/L
200
152
99 75-125
Cadmium
21.5
1.00
ug/L
20.0
0.690
104 75-125
Chromium
207
10.0
ug/L
200
1.40 U
103 75-125
Lead
197
10.0
ug/L
200
3.10 U
98 75-125
Selenium
213
10.0
ug/L
200
6.20 U
107 75-125
Silver
214
10.0
ug/L
200
1.90 U
107 75-125
Matrix Spike Dup (9G25013-MSD3)
Prepared:
07/25/2019
09:34 Analyzed: 07/29/2019 13:14
Source: CC11273-02
Spike
Source
%REC
RPD
Analvte
Result Flaq
Q
Units
Level
Result
%REC Limits RPD
Limit Notes
Arsenic
207
10.0
ug/L
200
7.60 U
103 75-125 2
20
Barium
354
10.0
ug/L
200
152
101 75-125 0.7
20
Cadmium
21.7
1.00
ug/L
20.0
0.690
105 75-125 0.8
20
Chromium
207
10.0
ug/L
200
1.40 U
104 75-125 0.2
20
Lead
202
10.0
ug/L
200
3.10 U
101 75-125 2
20
Selenium
222
10.0
ug/L
200
6.20 U
111 75-125 4
20
Silver
216
10.0
ug/L
200
1.90 U
108 75-125 0.9
20
Post Spike (9G25013-PSI)
Prepared:
07/25/2019
09:34 Analyzed: 07/29/2019 13:16
Source: CC11273-02
Spike
Source
%REC RPD
Analvte
Result
Flaq POL
Units
Level
Result
%REC
Limits RPD Limit Notes
Arsenic
0.202
0.0100
mg/L
0.200
0.00178
100
80-120
Barium
0.352
0.0100
mg/L
0.200
0.152
100
80-120
Cadmium
0.0216
0.00100
mg/L
0.0200
0.000690
105
80-120
Chromium
0.207
0.0100
mg/L
0.200
0.000376
103
80-120
FINAL
This report relates only to the sample as received by the
laboratory, and
may only be
reproduced in
full. Page 25 of 28
(� �Eo
www.encolabs.com
QUALITY CONTROL DATA
Metals (total recoverable) by EPA 6000/7000 Series Methods - Quality Control
Batch 9G25013 - EPA 3005A - Continued
Post Spike (9G25013-PSI) Continued
Prepared: 07/25/2019 09:34 Analyzed: 07/29/2019 13:16
Source: CC11273-02
Spike
Source
%REC
RPD
Analvte Result Flaq
POL Units
Level
Result
%REC Limits RPD
Limit Notes
Lead 0.194
0.0100 mg/L
0.200
-0.00286
97 80-120
Selenium 0.217
0.0100 mg/L
0.200
-0.00534
108 80-120
Silver 0.220
0.0100 mg/L
0.200
-0.00101
110 80-120
Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control
Batch 9G24024 - EPA 5030E MS
Blank (9G24024-BLK1)
Prepared: 07/24/2019 00:00 Analyzed: 07/24/2019 11:47
Spike
Source
%REC
RPD
Analvte Result Flaq
POL Units
Level
Result
%REC Limits RPD
Limit Notes
1,4-Dioxane 1.2 U
2.0 ug/L
Toluene-d8 5.4 u91L 5.00 108 75-125
LCS (9G24024-BSI) Prepared: 07/24/2019 00:00 Analyzed: 07/24/2019 10:40
Spike Source %REC RPD
Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 24 2.0 ug/L 25.0 95 80-133
Toluene-d8 5.0 u91L 5.00 99 75-125
LCS Dup (9G24024-BSD1) Prepared: 07/24/2019 00:00 Analyzed: 07/24/2019 11:13
Spike Source %REC RPD
Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes
1,4-Dioxane 26 2.0 ug/L 25.0 103 80-133 8 19 QM-10
Toluene-& 5.1 u9/L 5.00 103 75-125 QM-10
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 28
(� �Eo
www.encolabs.com
FLAGS/NOTES AND DEFINITIONS
B The analyte was detected in the associated method blank.
D The sample was analyzed at dilution.
J The reported value is between the laboratory method detection limit (MDL) and the laboratory method
reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable.
U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation
data and moisture content, where applicable.
E The concentration indicated for this analyte is an estimated value above the calibration range of the
instrument. This value is considered an estimate.
MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is
based on the low point of the calibration curve, when applicable, sample preparation factor, dilution
factor, and, in the case of soil samples, moisture content.
PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL.
N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater
confidence) to make a "tentative identification".
P Greater than 25% concentration difference was observed between the primary and secondary GC column.
The lower concentration is reported.
[CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses.
QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact.
QM-10 LCS/LCSD were analyzed in place of MS/MSD.
QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there
is no impact.
R-05 The sample was diluted due to the presence of high levels of non -target analytes resulting in elevated
reporting limits.
FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 28
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Sample Preservation Verification
ENCO Cary
C1
,,a
.Om= N6, CG$
Iml
Work Order: CC11273 Project: Closed State Fairgrounds Landfill
Client: Withers & Ravenel Environmental (W1009) Project #: 02000082.20
Logged In: 19-Jul-19 14:23 Logged By: John C King
Preservation Check Performed By: Date/Time: �. ��% /
CC11273-01
Cont
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y7/ N / NA
Y /'N_,/ NA
CC11273-02
Cont
Type
Pres (pH)
Requirement
pH Checked /
Control,
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
( / N / NA
Y / / NA
CC11273-03
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
Y- / N / NA
Y / N ,/ NA
CC11273-04
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted DateTme
Reagent Used/Comments
Requirement
In Control
Adjusted
A
250mLP+HNO3
<2
()/ N / NA
Y / / NA
CC11273-05
Cant
Type
Pres (pH)
Requirement
pH Checked /
In Control
pH Adjusted DateMme
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
& / N / NA
Y / NA
CC11273-06
Cont
Type
Pres (pH)
pH Checked /
pH Adjusted Date/Time
Reagent Used/Comments
Requirement
In Control
Adiusted
A
250mLP+HNO3
<2
Y;/ N / NA
Y / N / NA
CC11273-07
Cont
Type
Pres (pH)
Requirement
IpH Checked /
I In Control
pH Adjusted Date/Time
Adjusted
Reagent Used/Comments
A
250mLP+HNO3
<2
Y / N / NA
Y / N '4 NA
Reagent Name ID
1
2 /}
pH Strip ID: < D. -/
C:\ELM NT\Print\wko_PreservationCheck. rpt
Rea ent Name ID Rea ent Name ID
3 5
4 6
Page 1 c