MO-9485_40926_CA_IAR_20190619_Initial Action Abatement Report

CESONCa
June 19, 2019
Trudy Beverly
NCDEQ / DWM / UST Section
610 East Center Avenue, Suite 300
Mooresville, North Carolina 28115
RE: Initial Abatement Action Report
Circle K No. 2708383
873 Old Charlotte Road Southwest
Concord, Cabarrus County, North Carolina
NCDEQ UST Facility No. 4527
CES Project No. 6.0005
Dear Mx. Beverly:
CES of NC, PLLC
301 McCullough Drive, Suite 400
Charlotte, North Carolina 28262
704.909.2911 [office]
540.343.6259 [facsimile]
Crawford Environmental Services of North Carolina, PLLC (CES) on behalf of Circle K Stores Inc.
(Circle K) is pleased to submit the enclosed "Initial Abatement Action Report" for the above -
referenced site for your review and approval. This report summarizes UST closure and initial
abatement action activities conducted by CES in May of 2019 following a release from the former
UST system reported on May 23, 2019.
If you have any questions or comments pertaining to this project please feel free to contact me at
[phone] or by email at aaron.williamson(a)crawfordenvironmental.com.
Sincerely,
CRAWFORD ENVIRONMENTAL SERVICES OF NORTH CAROLINA, PLLC
Aaron Williamson
Project Manager
cc: Mrs. Debrah B. Carl - Circle K, Charlotte -NC (electronic)

CESONC..
INITIAL ABATEMENT ACTION REPORT
Circle K No. 2708383
873 Old Charlotte Road Southwest
Concord, Cabarrus County, North Carolina
NCDEQ UST Facility No. 4527
CES Project No. 6.0005
Submittal Date:
June 19, 2019
Prepared For:
Mrs. Debrah B. Carl
Environmental Manager
Circle K Stores Inc.
2550 West Tyvola Road, Suite 200
Charlotte, North Carolina 28217
TM
Prepared By:
Crawford Environmental Services of North Carolina, PLLC
301 McCullough Drive, Suite 400
Charlotte, North Carolina 28262
p: [phone] / f: [phone]
www.crawfordenvironmental.com

CES@NC..
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
SITE INFORMATION
SITE IDENTIFICATION
Facility ID: 4527
UST Incident No: Current: Not Assigned — Former: 27671 (NFA)
Site Risk: Current: Not Determined — Former: Low
Agency Contact: Trudy Beverly, NCDEQ, Mooresville Regional Office
Site Name: Circle K No. 2708383
Site Street Address: 873 Old Charlotte Road Southwest
Concord, North Carolina 28027
County: Cabarrus
Latitude / Longitude: 35.3831660 /-80.5975060 (VIA GPS (a) UST Pit)
SITE CONTACT INFORMATION
UST Owner/Operator:
Circle K Stores Inc.
Address:
2550 West Tyvola Road, Suite 200
Charlotte, NC 28217
Contact:
Debrah B. Carl, Environmental Manager
Telephone:
[phone]
Email:
dcarl circlek.com
Property Owner:
Hickory Woods, Inc.
Address:
PO Box 526
Concord, NC 28026
Consultant:
Crawford Environmental Services of NC, PLLC
Address:
301 McCullough Drive, Suite 400
Charlotte, NC 28262
Telephone:
[phone]
NC License No:
C-550
UST Removal Contractor:
Zebra Environmental & Industrial Services, Inc.
Address:
PO Box 357, High Point, NC 27261
Telephone:
[phone]
Analytical Laboratory 1:
Pace Analytical Services, LLC
Address:
9800 Kincey Avenue, Suite 100, Huntersville, NC 28078
Telephone:
[phone]
State Certification No:
12
Analytical Laboratory 2:
Rapid Environmental Diagnostics, LLC
Address:
5598 Marvin K. Moss Lane Suite 2003, Wilmington, NC 28409
Telephone:
[phone]
State Certification No:
N/A
INFORMATION ABOUT THE RELEASE
Date Discovered: May 22, 2019
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Former UST System
UST(s) Size & Contents: (3) 10,000-gallon Gasoline
Page No. i

...,=.� C::
CL
Certification
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
' Brian L. Haves, a L.�-``, employedby Crawford Environmental Services of North
Carolina, PLLC do certifYthis`.``...� ..`,..`',. �~,\�i.�` i. report is correct and accurate tothe best of y knowledge.
OIMMMMMMW
Crawford Environmental Services of North Carolina, PLLC is licensed to practice geology in North
Carolina, The certification number of the company or corporation to practice geology is C�550,,
0410
45
old a
WO
Brian Lie S"AM
License
.2 i"
Sje
North Car 0�'
40A
Page No. ii

CES@NCa
EXECUTIVE SUMMARY
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
As required, the following executive summary provides the most pertinent information for this
assessment. For additional information please refer to subsequent sections of this report.
➢ Crawford Environmental Services of North Carolina, PLLC (CES) was contracted by Circle
K in May of 2019 to complete underground storage tank (UST) closure assessment activities
associated with the removal of three (3) 10,000-gallon gasoline USTs. The services were
provided in general accordance with a proposal dated April 23, 2019;
➢ Following removal of the UST system, five (5) locations of impacted soils in excess of
NCDEQ Action Levels were identified at the site via Ultraviolet Fluorescence analysis;
➢ Based on confirmed soil contamination, a release was reported to the NCDEQ on May 23,
2019.
➢ As part of required initial abatement activities, over -excavation was performed to remove
grossly contaminated soil at the site. Rock was encountered at depths ranging from 13 to
16-feet BGS. Approximately 130-tons of petroleum impacted soil were removed from the
site;
➢ Groundwater was not encountered during the assessment activities completed by CES at
this site during May of 2019;
➢ Results of the over -excavation extent samples revealed multiple constituents in excess of
the NCDEQ Soil -to -Water Maximum Soil Contaminant Concentrations (MSCCs), but no
constituents were reported in excess of the NCDEQ Industrial/Commercial MSCC.
➢ No sensitive environmental receptors were identified within a 1,500-foot radius of the site;
➢ A historical incident identified as NCDEQ Incident No. 27671 was previously assessed and
closed -out at the site. The release was initially discovered in February of 2004 and
subsequently closed -out in July of 2006 through recordation of a "Notice of Residual
Petroleum" perpetually restricting the use of groundwater at the site as a water supply;
➢ At this time, we recommend closure of the incident reported May 23, 2019 via recordation
of a "Notice of Residual Petroleum" with soil restrictions.
Page No. iii

CES@NCa
TABLE OF CONTENTS
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
SITE INFORMATION.....................................................................................................................I
EXECUTIVE SUMMARY.............................................................................................................III
1.0 INTRODUCTION...............................................................................................................1
2.0 SITE HISTORY AND CHARACTERIZATION...............................................................
2.1 General Information
2.2 Project Contacts
2.3 UST Information
2.4 Past Releases
2.5 Current Facility Status
2.6 Subject Site and Surrounding Property Use
2.7 Regional Geology and Site Hydrogeology
3.0 UST CLOSURE ASSESSMENT....................................................................................
3.1 Preparations for Closure
3.2 UST Cleaning and Residual Fluids Disposal
3.3 UST System Removal and Disposal
3.4 Soil Sampling Locations and Collection Procedures
3.5 Groundwater and Surface Water Sampling Procedures
3.6 Quality Control Measures
3.7 Analytical Methods Used
3.8 Site Sensitivity Evaluation
4.0 SOIL EXCAVATION & ASSESSMENT.........................................................................
4.1 Excavation Extent Determination
4.2 Extent of Soil Excavation Activities
4.3 Quantity of Soils Removed, Storage Methods, and Final Disposition
4.4 Soil Analytical Results
4.5 Groundwater Analytical Results
2
2
2
3
3
3
4
4
5
5
5
5
6
6
6
6
7
11i
5.0 CONCLUSIONS AND RECOMMENDATIONS..............................................................11
6.0 LIMITATIONS.................................................................................................................12
7.0 REFERENCES................................................................................................................13
TABLES
Table 1: Site History - UST Owner/Operator & Other Responsible Party Information
Table 2: UST System & Other Release Information
Table 3: Summary of UST Closure Soil Samples
Table 4: Summary of Over -Excavation Soil Samples
Figure 1:
Site Location Map
Figure 2:
Site Map
Figure 3:
UST Closure Sample Locations
Figure 4:
Over Excavation Sample Locations
Figure 5:
Excavation Extent Sample Locations
Page No. iv

CES@NCa
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
TABLE OF CONTENTS (CONTINUED)
APPENDICES
Appendix A:
UST-3 Form
Appendix B
Waste Disposal Manifest(s)
Appendix C
Site Photographs
Appendix D:
UST-2A Form
Appendix E:
Laboratory Analytical Report & Chain -of -Custody Form(s)
Appendix F:
UST-61 Form
Page No. v

C �� a Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
1.0 Introduction
The purpose of this "Initial Abatement Action Report" is to provide a details of underground
storage tank closure activities and associated initial response and abatement actions associated
with a release discovered during the UST closure activities. The release was reported during UST
removal activities at the Circle K 2708383 facility located at 873 Old Charlotte Road SW in
Concord, North Carolina (Site). A topographic map illustrating the Site vicinity is included as
Figure 1. As required, this report incorporates the elements of a UST Closure Report and Post -
Excavation Soil Contamination Assessment Report.
In May of 2019 three 10,000-gallon petroleum USTs and associated piping and dispensers were
removed from the site by Zebra Environmental and Industrial Services, Inc. (Zebra) with activity
monitoring and assessment provided by Crawford Environmental Services of North Carolina,
PLLC (CES) personnel. A discussion of procedures used during the UST closure activities is
provided in subsequent sections of this report. Upon removal of the UST system, petroleum
contaminated soil was discovered. Over excavation efforts were performed to remove grossly
contaminated soils from the Site.
The Site is currently vacant under lease by Circle K Stores, Inc. (Circle K). The removal of the
former UST system was prompted by permanent closure of the Site facility by Circle K.
Page No. 1

CES@NCa
2.0 Site History and Characterization
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
The site has operated a UST system since at least 1987. Historical UST owner/operator and other
responsible party information is provided in Table 1. As required, the following provides
information relevant to site history and characterization.
2.1 General Information
Facility Name: Circle K No. 2708383
Facility ID Number: 4527
Facility Address: 873 Old Charlotte Road Southwest
Concord, North Carolina 28027
Cabarrus County
2.2 Project Contacts
UST Owner:
Property Owner:
UST Removal Contractor:
Environmental Consultant
Analyzing Laboratory 1
Analyzing Laboratory 2:
Circle K Stores, Inc.
2550 West Tyvola Road, Suite 800
Charlotte, North Carolina 28217
[phone]
Hickory Woods, Inc.
PO Box 526
Concord, North Carolina
Zebra Environmental & Industrial Services, Inc.
PO Box 357
High Point, North Carolina 27261
[phone]
CES
301 McCullough Drive, Suite 400
Charlotte, North Carolina 28262
[phone]
Pace Analytical Services, LLC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
[phone]
NC Certification Number: 12
Rapid Environmental Diagnostics, LLC
5598 Marvin K. Moss Lane, Suite 2003
Wilmington, North Carolina 28409
[phone]
NC Certification Number: N/A
Page No. 2

CES@NCa
2.3 UST Information
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
The former UST system included three single -wall fiberglass tanks containing various
grades of gasoline, two dispenser islands, and associated fiberglass piping. The three
USTs were oriented in a northeast -southwest direction located on the perimeter of the
property in the vicinity of the southwestern property corner as illustrated on Figure 2.
Product piping exited the central northeast side of the UST pit and supplied product to two
double -sided dispensers. UST system and other release information is summarized in
Table 2. No ASTs were present on the site.
2.4 Past Releases
In January and February of 2004, a due diligence investigation involving collection of soil
and groundwater samples at the Site was conducted in response to the sale of Circle K
by ConocoPhillips to Alimentation Couche-Tard. Results of the investigation determined
that soil and groundwater at the Site was impacted with petroleum hydrocarbons.
As a result of the due diligence investigation, the North Carolina Department of
Environment and Natural Resources (now known as the North Carolina Department of
Environmental Quality [NCDEQ]) assigned Incident Number 27671 under responsible
party ConocoPhillips and issued a Notice of Regulatory Requirements (NORR) requesting
the completion of a Site Check at the facility.
On March 23, 2004, a Site Check was completed at the facility by advancing eleven soil
borings in the vicinity of the UST system based on previous soil boring locations and site
check requirements. Results of the site check indicated that releases may have occurred
from the eastern -most UST and from the dispensers.
On April 29, 2004, a NORR requesting the preparation of a Limited Site Assessment (LSA)
was issued by the NCDEQ. Results of the LSA were documented in a report dated
September 15, 2004 prepared by ATC Associates of North Carolina, P.C. (ATC). Based
on the findings of the report, the incident was classified as "low" risk and no further action
was requested.
On June 12, 2006, the NCDEQ issued a "Notice of No Further Action". Incident Number
27671 received closure through recordation of a "Notice of Residual Petroleum" (NRP)
with the Cabarrus County Register of Deeds perpetually restricting groundwater at the site
from use as a water supply. The notice was signed by ConocoPhillips and recorded in
Deed Book 6870, Page 168 on July 11, 2006.
No other information was obtained or reviewed for the completion of this report.
2.5 Current Facility Status
At the time of this assessment the facility was vacant and permanently closed. According
to Circle K, the UST system was last used on May 8, 2019. During the May 2019
assessment activities, improvements observed onsite included a one-story convenience
Page No. 3

CES@NC..
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
store building and the associated paved parking areas. Pertinent site features are
illustrated on Figure 2.
2.6 Subject Site and Surrounding Property Use
The Site facility formerly operated as Circle K 2708383, a convenience store with Shell
branded petroleum retail. The Site was utilized for commercial purposes with adjacent
properties to the northwest and southwest also utilized as commercial properties. Adjacent
properties to the northeast and southeast were utilized for residential purposes. Municipal
water is supplied to the Site and vicinity by the City of Concord.
Surface cover at the site consists primarily with asphalt. Portions of the pavement which
were removed to access the UST system were resurfaced with concrete. Sparse
vegetation is present along the perimeter of the Site.
2.7 Regional Geology and Site Hydrogeology
According to the 1985 "Geologic Map of North Carolina", the site is located within the
Charlotte Belt of the Inner Piedmont Physiographic Province. This area is characterized
by intrusive igneous rocks identified as metamorphosed quartz diorite described as
foliated to massive. The general vicinity also contains metamorphic rocks identified as
biotite gneiss and schist. The metamorphic rocks are described as interangular and
megacrystic with abundant potassic feldspar and garnet interlayered and gradational with
calc-silicate rock, sill imanite-mica schist, mica schist, and amphibolite. Rocks of the
Syenite of Concord Plutonic Suite and Gabbro of Concord Plutonic Suite have also been
identified in the area.
The primary soil type observed during UST closure activities was sandy silt with lean clay.
Weathered rock was encountered at depths ranging from 13 to 16-feet BGS. Groundwater
was not encountered during excavation activities which reached a maximum depth of
approximately 16-feet below ground surface (BGS). Based on previous site assessment,
depth to groundwater at the site ranges from approximately 18 to 20-feet below ground
surface (BGS). Groundwater flow direction, as determined by historical assessments, was
to the east-southeast and generally appears to follow the dip of rock observed in the tank
pit.
Page No. 4

CES@NCa
3.0 UST Closure Assessment
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
In conducting UST removal and assessment activities at the site, the most recent revision of the
NCDEQ "Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases" dated February 1, 2019 was utilized for guidance. The following offers further details
and provides required information pertaining to the UST removal activities conducted at the Site.
3.1 Preparations for Closure
A "Notice of Intent: UST Permanent Closure or Change -In -Service" form (UST-3) was
completed and submitted to the NCDEQ on April 18, 2019 (refer to Appendix A for a copy
of the UST-3 Form). Prior to removal of the UST system, the existing canopy at the site
was demolished beginning May 20, 2019. UST removal and demolition permits were
acquired from the City of Concord and Cabarrus County, as applicable, by the UST
removal contractor. Prior to demolition of the fuel dispenser canopy structure, an asbestos
containing materials survey was also performed.
3.2 UST Cleaning and Residual Fluids Disposal
On May 21, 2019, the USTs and piping were cleaned and evacuated by Zebra utilizing a
pressure washer and vacuum truck in tandem. A total of approximately 595-gallons of a
product/water mixture, consisting primarily of rinsate, was removed from the USTs. Refer
to Appendix B for copies of the disposal manifest. The storage, sampling and disposal of
residual fluids recovered/generated during the UST closure activities were conducted by
Zebra at their High Point, NC facility.
In addition, subsequent to cleaning and prior to removal, the atmosphere within the USTs
was verified inert through the use of an explosive limit meter under direct supervision of a
representative of the City of Concord Fire Department.
3.3 UST System Removal and Disposal
Product dispensers were removed from the two (2) dispenser islands at the Site through
the course of canopy demolition procedures commencing on May 21, 2019. On May 21,
2019, the dispenser sumps and product piping were exposed for visual assessment. The
sumps and piping were observed to be in good condition. Product piping was constructed
of a fiberglass reinforced plastic (FRP). Following inspection, the product piping was
removed from the ground.
USTs were exposed for inspection on May 22, 2019 and appeared to be in good condition.
Following inspection, the USTs were removed from the ground on May 22, 2019 by Zebra.
The cleaned, evacuated, and inert fiberglass USTs were mechanically crushed by Zebra
prior to removal from the excavation. The crushed tank and product piping material was
loaded and transported off -site by Zebra. Certification of tank disposal by Zebra is included
in Appendix B. Photographic documentation of the removal is included in Appendix C.
A copy of the "Site Investigation Report for Permanent Closure or Change -in -Service of
Registered UST' form (UST-2A) is included as required in Appendix D.
Page No. 5

CES@NCa
3.4 Soil Sampling Locations and Collection Procedures
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
Soil samples were collected as required from directly beneath the former UST system
components concurrent with removal of the system. The number of soil samples collected
was based on the specific dimensions of the UST system, as applicable. Soil sample
collection was conducted as follows:
• One sample per 10-linear feet under each UST (12 samples);
• One sample beneath each dispenser (2 samples);
• One sample per 10-linear feet under product lines and every joint (5 samples)
The locations of UST closure soil samples collected from the site is illustrated on Figure
3. Soil samples collected for UST closure assessment were submitted to the Rapid
Environmental Diagnostics, LLC (RED Lab) on -site representative for analysis by "Typing"
UVF. The UVF laboratory report is included in Appendix E.
3.5 Groundwater and Surface Water Sampling Procedures
Groundwater was not encountered in the excavation and no surface water bodies were
observed within 1,500-feet of the site; therefore, no groundwater or surface water samples
were collected during UST closure activities conducted as part of this assessment.
3.6 Quality Control Measures
Sample handling procedures consisted of placing soil samples into sterilized, laboratory -
provided containers. Each sample was labeled with a unique specific identification number
using an indelible marker including at a minimum the collection date and time and then
transported and submitted to the laboratory for analysis under chain -of -custody protocol.
As previously discussed, no field sampling equipment (hand -auger, split -spoon sampler,
etc.) was utilized to collect soil samples; therefore, no decontamination procedures were
necessary to complete soil sampling. All soil samples collected were taken directly from
the bucket of earth excavating equipment utilizing new disposable nitrile gloves during
each sample collection to reduce the overall risk of cross contamination. Care was taken
to collect soil samples not in direct contact with the excavation equipment
Soil samples were collected on May 22, 2019 and were subsequently logged into the
laboratory on the same day. All samples were received by the laboratory within method
specified holding times and temperatures (<6°C). No duplicates or trip blanks were utilized
for this assessment. A copy of the chain -of -custody form(s) is located in Appendix E.
3.7 Analytical Methods Used
Soil samples collected beneath the former UST system were analyzed on -site by RED
Lab using UVF Typing reporting Gasoline Range Organics (GRO), Diesel Range Organics
(DRO), and total benzene, toluene, ethylbenzene, and xylenes (collectively referred to as
"BTEX").
Page No. 6

CES@NCa
3.8 Site Sensitivity Evaluation
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
The site vicinity appears to be serviced by municipal water supply. No suspect water
supply wells, basements, or surface water bodies were observed within a 1,500-foot radius
of the site. Several underground utilities were observed on and adjacent to the site as
shown on Figure 2.
According to the USGS Topographical Map (Figure 1), an intermittent stream is located
approximately 1,200-feet northeast of the site. An additional intermittent stream is located
approximately 1,500-feet south of the site. Both of these intermittent streams form upper
tributaries of Irish Buffalo Creek which is located approximately 5,000-feet northeast of the
site.
Page No. 7

C �� a Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
4.0 Soil Excavation & Assessment
CES referred to the NCDEQ "Guidelines for Site Checks, Tank Closure, and Initial Response and
Abatement for UST Releases" dated February 1, 2019 for guidance in completing initial response
and abatement activities. Due to a confirmed release via soil analytical data from the UST closure
sampling, initial abatement actions commenced including submission of a "24-Hour Release and
UST Leak Reporting Form" (UST-61) to the NCDEQ Mooresville Regional Office on May 23, 2019
via email correspondence. A copy of the UST-61 form is included as Appendix F. The amount
and exact cause of the release are unknown.
As requested by the NCDEQ Incident Manager Trudy Beverly in email correspondence dated
May 29, 2019, a "20-Day Report" was completed and submitted to the NCDEQ on June 10, 2019.
This IAA report incorporates the 20-day requirements previously submitted. The following offers
further details and provides required information pertaining to the initial abatement actions
conducted at the Site.
4.1 Excavation Extent Determination
Following removal of the UST system, soils were visually inspected for staining or other
signs of petroleum contamination. Free product was not observed. During the removal of
the UST system, no materials located beyond 5-feet of the UST system components were
removed. Required UST closure samples were collected directly from the open excavation
at the locations illustrated on Figure 3 and analyzed on -site by UVF analysis performed
by RED Lab.
A photo -ionization detector (PID) calibrated to 1 00-parts-per-mill ion (ppm) Isobutylene
was also utilized in the field to directly screen soils in an effort to help determine the overall
extent of impact and guide any necessary soil excavation/sampling activities. As part of
CES standard operating procedures, field screening equipment is calibrated according to
the manufacturer's specification prior to each use and recorded in a dedicated calibration
log included with the unit. Soils within the excavation were also visually assessed for the
presence of staining.
Soil samples were placed into sealable Zip-loc° bags after preserving the required volume
in laboratory provided bottle -ware, as applicable. The bagged sample was allowed time to
equilibrate and volatilize at ambient air temperature of at least 68-degrees Fahrenheit at
which point the headspace was screened for the presence of volatile organic vapors
utilizing the PID.
4.2 Extent of Soil Excavation Activities
Based on the results of UVF analysis, soils at the locations of SS-6, SS-8, SS-11, SS-1 3,
and SS-16 (Figure 3) were impacted above the NCDEQ Action Limits for GRO and/or
DRO of 50-milligrams per kilogram (mg/kg) and 100-mg/kg, respectively. Over excavation
commenced via spot digging at the locations of GRO and DRO exceedances focusing in
the vertical direction and presumed downgradient locations.
Page No. 8

CES@NCn
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
Rock was encountered in the excavation at depths ranging from 13 to 16-feet BGS which
prevented additional vertical soil excavation where encountered. Depth to rock appeared
to be shallowest at 13-feet BGS on the northwestern side of the UST pit and dipped
towards the southeastern side of the UST pit to a depth of approximately 16-feet BGS.
Excavation base soil samples were collected directly above the soil/rock interface.
Groundwater was not encountered in the excavation; therefore, groundwater samples
were not collected. Sidewall samples were collected and screened to determine the lateral
extent of contamination and direct additional required excavation. Over excavation sample
locations and the final limits of excavation are illustrated on Figure 4. A summary of UST
closure samples and analytical data is provided in Table 3.
Following completion of over excavation activities, extent sidewall and base samples were
collected and submitted to Pace Analytical Services, LLC (Pace) for traditional laboratory
analysis for volatile organic compounds by EPA Method 8260 and volatile petroleum
hydrocarbons by MADEP VPH. On -site UVF analytical results and PID screening
indicated that sidewalls were not impacted, therefore lateral excavation was not
performed.
4.3 Quantity of Soils Removed, Storage Methods, and Final Disposition
During tank removal, a total of approximately 200-cubic yards (yd3) of overburden pea
gravel and 100 yd3 of over burden soil was generated. The overburden material was
initially stockpiled, analyzed via UVF, determined to be clean, and subsequently returned
to the tank basin to be used as backfill material. Results of the stockpile samples are
included in Table 3 and Appendix E.
Soils generated during over -excavation efforts were loaded directly into trucks,
manifested, and transported off -site for disposal at the AES facility located in Thomasville,
NC. Soil samples were collected from the waste stream for disposal characterization
purposes and submitted to RED Lab for UVF screening at regular intervals. Approximately
130-tons of petroleum impacted soil were removed from the site. Certified disposal
manifests are included in Appendix B.
4.4 Soil Analytical Results
After review of the laboratory analytical report for over -excavation soil samples, the
following detections in excess of regulatory limits were reported:
• Sidewall NE (Northeast sidewall of the UST pit)
o Benzene was reported at a concentration of 0.043 milligrams per kilogram
(mg/kg) which is in excess of the NCDEQ Soil -to -Groundwater Maximum
Soil Contaminant Concentration (STW MSCC) of 0.0056 mg/kg;
• Base (Deepest point of base of UST pit on top of rock)
o Aliphatics C5-C8 was reported at a concentration of 205 mg/kg which is in
excess of the NCDEQ STW MSCC of 68 mg/kg;
o Aliphatics C9-C12 was reported at a concentration of 789 mg/kg which is
in excess of the NCDEQ STW MSCC of 540 mg/kg;
Page No. 9

CES@NCa
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
• L Base (Base of lines over -excavation on top of rock)
o Ethylbenzene was reported at a concentration of 9.1 mg/kg which is in
excess of the NCDEQ STW MSCC of 4.9 ug/kg;
o Xylenes were reported at a concentration of 21.7 mg/kg which is in excess
of the NCDEQ STW MSCC of 4.6 mg/kg;
o Naphthalene was reported at a concentration of 16.2 mg/kg which is in
excess of the NCDEQ STW MSCC of 0.16 mg/kg
o Aliphatics C5-C8 was reported at a concentration of 393 mg/kg which is in
excess of the NCDEQ STW MSCC of 68 mg/kg;
o Aliphatics C9-C12 was reported at a concentration of 1,550 mg/kg which is
in excess of both the NCDEQ STW MSCC and Residential Soil Cleanup
Levels MSCC of 540 mg/kg and 1,500 mg/kg, respectively.
Additionally, laboratory reporting limits exceeded the NCDEQ STW MSCCs in soil
samples Sidewall NW, Base, and L Base for Benzene and/or other constituents.
Remaining soil samples were found to be either below NCDEQ regulatory limits or below
the laboratory reporting limit.
A summary of the over -excavation analytical data is provided in Table 4 and illustrated on
Figure 5. A copy of the laboratory report is included in Appendix E.
4.5 Groundwater Analytical Results
No groundwater was encountered during the assessment activities completed by CES at
this site during May of 2019.
Page No. 10

CES@NCa
5.0 Conclusions and Recommendations
Based on the results of this assessment, CES concludes the following:
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
➢ Following the removal of three (3) 10,000-gallon USTs and associated system components,
five (5) locations of impacted soils in excess of NCDEQ Action Levels were identified at the
site via UVF analysis;
➢ Based on confirmed soil contamination, a release was reported to the NCDEQ on May 23,
2019.
➢ Over -excavation was performed to remove grossly contaminated soil at the site. Rock was
encountered at depths ranging from 13 to 16-feet BGS. Approximately 130-tons of
petroleum impacted soil were removed from the site;
➢ Groundwater was not encountered during the assessment activities completed by CES at
this site during May of 2019;
➢ Results of the excavation extent samples revealed multiple constituents in excess of the
NCDEQ STW MSCCs from one sidewall and both base excavation samples (on top of rock).
Only Aliphatics C9-C12 was reported in excess of the NCDEQ Residential Soil Cleanup
Level MSCC. No constituents were reported in excess of the NCDEQ Industrial/Commercial
MSCC.
➢ A historical incident identified as NCDEQ Incident No. 27671was previously assessed and
closed -out at the site. The release was initially discovered in February of 2004 and
subsequently closed -out in July of 2006 through recordation of a "Notice of Residual
Petroleum" perpetually restricting the use of groundwater at the site as a water supply;
➢ No sensitive environmental receptors were identified within a 1,500-foot radius of the site;
➢ At this time, we recommend closure of the incident reported May 23, 2019 via recordation
of a "Notice of Residual Petroleum" with soil restrictions.
Page No. 11

C �� a Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
6.0 Limitations
This report has been prepared for the exclusive use of Circle K Stores Inc. for specific application
to the referenced site in Concord, North Carolina. The assessment was conducted based on the
scope -of -work and level of effort requested by the NCDEQ and with resources adequate only for
that scope -of -work. Our findings have been developed in accordance with generally accepted
standards of geology and hydrogeology practices in the State of North Carolina, available
information, and our professional judgment. No other warranty is expressed or implied.
The data that are presented in this report are indicative of conditions that existed at the precise
locations sampled and at the time the samples were collected. Additionally, the data obtained
from samples would be interpreted as being meaningful with respect to parameters indicated in
the laboratory report. No additional information can be logically be inferred from these data.
Conclusions and recommendations set forth herein are applicable only to the facts and conditions
described at the time of this report
Page No. 12

CES@NCa
7.0 REFERENCES
Initial Abatement Action Report
Circle K 2708383
Concord, North Carolina
"Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases" completed by the UST Section of the NCDEQ, Division of Waste Management (DWM)
dated March 1, 2007, Change 9.
"Guidelines for Assessment and Corrective Action for UST Releases" completed by the UST
Section of the NCDEQ, DWM dated July 15, 2008, Change 3.
"Guidelines for Sampling" completed by the UST Section of the NCDEQ, DWM dated July 15,
2008, Change 2.
"24-Hour Release Report" Completed by ATC dated February 23, 2004.
"Site Check Report" completed by ATC dated April 12, 2004.
"Phase II Limited Site Assessment Report" completed by ATC dated September 15, 2004.
"Notice of No Further Action" completed by ATC dated September 15, 2004.
"20-Day Report" completed by CES dated June 10, 2019.
Page No. 13

TABLES

TABLE I
SITE HISTORY - UST OWNER / OPERATOR OTHER RESPONSIBLE PARTY INFORMATION
Circle K No. 2708383
873 Old Charlotte Road SW
Concord, North Carolina 28027
NCDEQ UST Facility ID: 4527
UST ID Number
1 through 3
Facility ID Number
1 4527
Name of Owner
Dates of Operation (MM/DD/YY to MM/DD/YY)
Circle K Stores, Inc.
2004 to Present
Street Address
2550 West Tyvola Road, Suite 200
City
I State
Zip
ITelephone Number
Charlotte
INC
28217
704-583-5762
Name of Operator
Dates of Operation (MM/DD/YY to MM/DD/YY)
Circle K Stores, Inc.
2004 to Present
Street Address
2550 West Tyvola Road, Suite 200
City
I State
Izip
ITelephone Number
Charlotte
INC
128217
704-583-5762
UST ID Number
1 through 3
Facility ID Number
1 4527
Name of Owner
Dates of Operation (MM/DD/YY to MM/DD/YY)
Conoco Phillips Company
1987 to 2004
Street Address
600 North Dairy Ashford
City
I State
Zip
ITelephone Number
Houston
JTX
77079-1175
832-379-6135
Name of Operator
Dates of Operation (MM/DD/YY to MM/DD/YY)
Conoco Phillips Company
1987 to 2004
Street Address
600 North Dairy Ashford
City
I State
Izip
ITelephone Number
Houston
JTX
77079-1175
832-379-6135
Other Incidents Onsite or Commingled/In Close Proximity
Incident Number
27671
Date Incident Occurred
2/22/2004
Name of Other Responsible Party
Date Incident Report
2/23/2004
Conoco Phillips Company
Date Incident Closed
7/11/2006
Street Address
600 North Dairy Ashford
City
State
Zip
Telephone Number
Houston
TX
77079-1175
1 832-379-6135

TABLE 2
UST SYSTEM AND OTHER RELEASE INFORMATION
Circle K No. 2708383
873 Old Charlotte Road SW
Concord, North Carolina 28027
NCDEQ UST Facility ID: 4527
UST ID Number
Current/Last
Contents
Previous Contents
Capacity
I (gallons)
Construction
Details
Tank
Dimensions
(feet)
Description of
Associated Piping and
Pumps
Date Tank
Installed
Status of
UST
Was Release
Associated with
the UST System?
1
Gasoline
Gasoline
10,000
Fiberglass
8 x 32
Fiberglass/Pressure
1987
Removed
Yes
2
Gasoline
Gasoline
10,000
Fiberglass
8 x 32
Fiberglass/Pressure
1987
Removed
Yes
3
Gasoline
Gasoline
10,000
Fiberglass
8 x 32
Fiberglass/Pressure
1987
Removed
Yes
Description of
Was Release
Current/Last
Capacity
Construction
Tank
Associated Piping and
Date Tank
Status of
Associated with
AST ID Number
Contents
Previous Contents
(gallons)
Details
Dimensions
Pumps
Installed
AST
the AST System?
None
Incident
Number
Material Released
Date of Release
Descrtiption of Release
27671
Gasoline
2/23/2004
1 Petroleum soil contamination discovered during due diligence for property transaction.

TABLE 3
SUMMARY OF UST CLOSURE SOIL SAMPLES
CIRCLE K 2708383
Circle K No. 2708383
873 Old Charlotte Road SW
Concord, North Carolina 28027
NCDEQ UST Facility ID: 4527
Analytical Method (e.g. VOC by EPA 8260)
UVF (mg/kg)
Contaminant of Concern
x
m
70
�
0
0
p
E
Q
_
a
Sample ID
Date
Collected
Source Area
Sample
Depth
(ft BGS)
Incident
Phase
Stockpile
5/22/2019
UST System
N/A
IAA
<0.68
1.9
6.9
8.8
2
<0.22
Stockpile 2
5/22/2019
UST System
N/A
IAA
<0.52
<0.52
<0.52
<0.52
<0.1
<0.17
SS-1
5/22/2019
Dispenser
5
IAA
<0.63
2.2
<0.63
2.2
<0.13
<0.2
SS-2
5/22/2019
Lines
5
IAA
<0.63
<0.63
<0.63
<0.63
<0.13
<0.2
SS-3
5/22/2019
Lines
5
IAA
<0.65
3.4
10.5
13.90
4.10
<0.21
SS-4
5/22/2019
Lines
5
IAA
11.9
22.5
41.3
63.8
52.7
2.00
SS-5
5/22/2019
Dispenser
5
IAA
<0.28
<0.28
<0.28
<0.28
<0.06
<0.09
SS-6
5/22/2019
Lines
5
IAA
20.3
44
186.2
230.2
41.5
1.50
SS-7
5/22/2019
Lines
5
IAA
<0.32
<0.32
0.32
0.32
0.190
<0.1
SS-8
5/22/2019
UST Pit
13
IAA
353.1
2,435
244.5
2679.5
1229
47.4
SS-9
5/22/2019
UST Pit
13
IAA
<0.56
4.5
0.56
5.1
0.3
<0.18
SS-10
5/22/2019
UST Pit
13
IAA
<1.2
4
24.1
28.1
0.8
<0.2
SS-11
5/22/2019
UST Pit
13
IAA
26.2
150.2
32.1
182.3
10.5
0.4
SS-12
5/22/2019
UST Pit
13
IAA
2.2
4.4
5.4
9.8
0.4
<0.16
SS-13
5/22/2019
UST Pit
13
IAA
375.6
2,935
185.2
3,120.2
117.7
4.7
SS-14
5/22/2019
UST Pit
13
IAA
<0.76
<0.76
<0.76
<0.76
<0.15
<0.24
SS-15
5/22/2019
UST Pit
13
IAA
<0.56
2.9
0.56
3.5
0.5
<0.18
SS-16
5/22/2019
UST Pit
13
IAA
24.4
118.1
20.5
138.6
0.7
<0.18
SS-17
5/22/2019
UST Pit
13
IAA
<0.48
2
7
9
0.5
<0.15
SS-18
5/22/2019
UST Pit
13
IAA
<0.37
<0.37
0.37
0.3700
0.2
<0.12
SS-19
5/22/2019
UST Pit
13
IAA
<0.45
<0.45
<0.45
<0.45
<0.09
<0.14
SS-6A
5/22/2019
Lines
6
IAA
<0.77
564.6
336.7
901.3
1,796.0
69.9
SS-613
5/22/2019
Lines
11
IAA
<0.51
309.5
297.2
606.7
186.1
7.2
SS-8A
5/22/2019
UST Pit
16
IAA
286.8
2,135
150.4
2,285.4
582.0
22.7
SS-11A
5/22/2019
UST Pit
16
IAA
<0.55
347.7
278.9
626.6
164.3
6.5
SS-13A
5/22/2019
UST Pit
14
IAA
<0.64
>232.7
>124.1
>356.8
>333.2
>13
Sidewall SE
5/22/2019
UST Pit
10
IAA
<0.7
<0.7
0.7
0.7
0.4
<0.22
Sidewall NE
5/22/2019
UST Pit
10
IAA
<0.36
<0.36
<0.36
<0.36
<0.07
<0.11
Sidewall SW
5/22/2019
UST Pit
10
IAA
<0.64
<0.64
<0.64
<0.64
<0.13
<0.21
Sidewall NW
5/22/2019
UST Pit
10
IAA
<0.45
<0.45
<0.45
<0.45
<0.09
<0.15
L Sidewall NE
5/22/2019
UST Pit
8
IAA
<0.61
10.2
11.4
21.6
7.2
0.3
L Sidewall SE
5/22/2019
UST Pit
8
IAA
5.6
9.9
13.2
23.1
12.7
0.5
L Sidewall NW
5/22/2019
UST Pit
8
IAA
<0.3
<0.3
0.3
0.3
0.3
<0.09
Load 2
5/22/2019
UST Pit
N/A
IAA
3.9
415.7
411.5
827.2
1,280.0
47.7
Load 3
5/22/2019
UST Pit
N/A
IAA
<0.66
406.9
308.4
715.3
181.7
7.2000
Action Level (mg/kg)
N/A
50
100
N/A
N/A
N/A
ft BGS = feet below ground surface
Results in mg/kg

TABLE 4
SUMMARY OF OVER -EXCAVATION SOIL SAMPLES
CIRCLE K 2708383
Circle K No. 2708383
873 Old Charlotte Road SW
Concord, North Carolina 28027
NCDEQ UST Facility ID: 4527
Analytical Method (e.g. VOC by EPA 8260)
EPA 8260D/5035A
MADEP VPH
Contaminant of Concern
c
N
I m
a,
N
_
W
a,
x
L L
GJ �
r
w
s
4
m
a,
C
�
s
a
1 z
Vf
s u
a
a
Vf
s u
a
a
Vf
s u
a
a
Sample ID
Date
Collected
Source Area
Sample
Depth
(ft BGS)
Incident
Phase
Sidewall SE
5/22/2019
UST Pit
10
IAA
0.0024.1
0.0026.1
<0.0058
0.0023.1
<0.0058
0.0047.1
<4.1
<4.1
<4.1
Sidewall NE
5/22/2019
UST Pit
10
IAA
0.043
0.0079
0.0029.1
0.0071.1
0.0028.1
<0.0062
<4.2
<4.2
<4.2
Sidewall SW
5/22/2019
UST Pit
10
IAA
<0.0062
<0.0062
<0.0062
<0.012
<0.0062
<0.0062
<4.2
<4.2
<4.2
Sidewall NW
5/22/2019
UST Pit
10
IAA
<0.17
<0.17
<0.17
<0.33
<0.17
0.041.1
<4.4
<4.4
<4.4
Base
5/22/2019
UST Pit
16
IAA
<0.17
<0.17
<0.17
<0.33
<0.17
<0.17
205
789
366
L Sidewall NE
5/22/2019
Lines
8
IAA
0.0035.1
0.0041J
0.0090
0.0084J
0.0021J
<0.0043
5.5
22.6
14.9
L Sidewall SE
5/22/2019
Lines
8
IAA
<0.0054
<0.0054
<0.0054
<0.011
<0.0054
0.0071
<3.3
<3.3
<3.3
L Sidewall NW
5/22/2019
Lines
8
IAA
0.0036.1
0.023
0.0047.1
0.020
<0.0049
0.057
9.9
5.9
4.1
L Base
5/22/2019
Lines
13
IAA
<0.25
0.37
9.1
21.7
<0.25
16.2
393
1,550
752
Soil -to -Groundwater MSCC (mg/kg)
0.0056
4.3
4.9
4.6
0.091
0.16
68
540
NSE
Residential Soil Cleanup Levels MSCC (mg/kg)
18
1,200
1,560
3,129
350
313
939
1,500
31,000
Industrial/Commercial MSCC (mg/kg)
164
32,000
40,000
81,760
3,100
8,176
24,528
40,000
810,000
MSCC = maximum soil contaminant concentration
ft BGS = feet below ground surface
Results in mg/kg
MSCC = maximum soil contaminant concentration referenced from NCDEQ "Guidelines for Site Checks, Tank Closure, and Initial Response and
Abatement" Table 1 (Version 1 - 2016_11_03)
NSE = No Standard Established
Concentrations Italicized were reported below the laboratory reporting limit, but the reporting limit exceeds the MSCC
Concentrations in Bold exceeded the Soil -to -Groundwater MSCC
Concentrations Underlined exceeded the Residential Soil Cleanup Levels MSCC
J = Estimated value between the method detection limit and laboratory reporting limit.

FIGURES

Legend
\ / \
OF \
Approximate Property Line
Fence
/
\
Former Dispenser
— — — — — — Former UST System
\
E Underground Electric Line
Overhead Electric Line
Underground Natural Gas Line
Underground Communication Line
OF\
W Underground Water Line
ss— Underground Sanitary Sewer Line
\
Underground Storm Sewer Line
0 / ,
%sw—
)! / CO \
Ij?et \
® Storm Sewer Inlet
y/40d
\
YX Light Pole
/ r� l\ �
�j
OF \
`a> Utility Pole
General Notes:
All locations, dimensions, and property lines depicted on
this plan are approximate. This plan should not be used
i . \
UST
Circle K
\
for construction or land conveyance purposes.
Basin ' %
2708383
/
\
Map adapted from Google Earth aerial imagery.
k
\
/ \
0 20' 40' 80'
\
1 inch equals 40 feet
CESOIINCEI
\
/
CLIENT: Circle K Stores, Inc.
Figure 2
873 Old Charlotte Highway
LOCATION:
Concord, North Carolina
Circle K 2708383
Site Map
Adapted from GoogleEarth aerial imagery / /
\ \
Initial Abatement Action Report

Legend
\ / �
\
Approximate Property Line
SS-1
SS-3
\
5
5 �
�
—.—°—x— Fence
\
SS-6
5 5/22/2019
5/22/2019
\
\
Former Dispenser
5/22/2019 2.2
3.4
— — — — — — Former UST System
\ 44 <0.63
186.2
10.5
• Soil Sample Location
SS-16
\
1 3
\
SS-1 Sample Identification
5/22I
SS-4
\
SS-12
5 Sample Depth
5/22/2019 Sample Date
118.1
5
13
SS-17
20.5
5/22/2019 \ 5/22/2019
2.2 Gasoline Rnlcs (/kg)
\
Diesel Raged
Oranaed ganics (mg/kg)
<0.63 g 9
13
/
22.5
\ 4.4
/
5/22/2019
/ � j � �
\ 41.3 �
5.4
/
(ND) Not Detected
2
Gj SS-1/On
CO
7
�. s8-2
\
ate
ryRo
SS-5 //(ND)
/
/—
v�/
\
SS-8 \
SS-6 4/SS-4
!/
13
\
General Notes:
All locations, dimensions, and property lines depicted on
/ ASS-16� \ \
/ SS-17 �� *SS-7 (ND)
�i
5/22/2019
\
this plan are approximate. This plan should not be used
for land
SS-12�
SAS-180�// , _
Circle K
2,435
construction or conveyance purposes.
SS-19 (ND) / ASS-13�SS-8
�S\4 ( �� //. '
2708383
/
244.5
Map adapted from Google Earth aerial imagery.
SS-18
<,i // /ss-9
/
13
/ FSS- �. SS-10
SS-9
5/22/2019
/ \� -11
13
5/22/2019
\
\
<0.37
0.37
4.5
/
/
SS-15
13
\
0.56
0 20' 40' 80'
5/22I2019 SS-13 \
� /
SS-10
13
1 inch equals 40 feet
/
2.9 13
5/22/2019
0.56 2,935
/
5/22/2019
/
4
CF.S@ NCa
185.2
\
24.1
CLIENT: Circle K Stores, Inc.
Figure 3
/ \ SS-11
/
873 Old Charlotte Highway
/
13
LOCATION:
Concord, North Carolina
\ 5/22/2019
/
Circle K 2708383
150.2
UST Closure Sample Locations
Adapted from Goo IeEarth aerial imagery /
p g g Y /
\ \
32.1
/
Initial Abatement Action Report

Legend
------ Approximate Property Line
— ° — — Fence
Cff) Former Dispenser
— — — — — — Former UST System
• Soil Sample Location
SS-1
Sample Identification
5
Sample Depth
5/22/2019
Sample Date
2.2
Gasoline Ranged Organics (mg/kg)
<0.63
Diesel Ranged Organics (mg/kg)
(ND)
Not Detected
General Notes:
All locations, dimensions, and property lines depicted on
this plan are approximate. This plan should not be used
for construction or land conveyance purposes.
Map adapted from Google Earth aerial imagery.
0 20' 40' 80'
1 inch equals 40 feet
CF.S@NC-CJL
CLIENT: Circle K Stores, Inc.
873 Old Charlotte Highway Figure 4
LOCATION: Concord, North Carolina
Circle K 2708383
Over Excavation Sample Locations
Initial Abatement Action Report

Legend
Approximate Property Line
-.-°-r-
Fence
Former Dispenser
— — — — — —
Former UST System
•
Soil Sample Location
Sidewall SE
Sample Identification
10
Sample Depth
5/22/2019
Sample Date
0.0024J
Benzene
0.0026J
Toluene
<0.0058
Ethylbenzene
0.0023J
Xylenes
<0.0058
Methyl-tert Butyl Ether
0.0047J
Naphthalene
<4.1
Aliphatics (C5-C8)
<4.1
Aliphatics (C9-C12)
<4.1
Aliphatics (C9-C10)
General Notes:
Results in mg/kg
Concentrations Italicized were reported below the
laboratory reporting limit, but the reporting limit exceeds
the MSCC
Concentrations in Bold exceeded the Soil -to -Groundwater
MSCC
Concentrations Underlined exceeded the Residential
Soil Cleanup Levels MSCC
J=Estimated value between the method detection limit
and the laboratory reporting limit
0 20' 40' 80'
1 inch equals 40 feet
CES@NC-CJL
CLIENT: Circle K Stores, Inc.
873 Old Charlotte Highway Figure 5
LOCATION: Concord, North Carolina
Circle K 2708383
Excavation Extent Sample Locations
Initial Abatement Action Report

APPENDIX A
UST-3 FORM

UST.3 Notice of Intent: UST Permanent Closure or Change -in -Service
Return completed form to:
STATE USE ONLY
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
i o #
Date Received
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
INSTRUCTIONS (READ THIS FIRST)
Complete and return at least thirty (30) days prior to closure or change -in-service activities. If a Professional Engineer (P.E.) or a Licensed Geologist (L.G.)
provides supervision for closure or change -in-service site assessment activities and signs and seals all closure reports then at least a five (5) working
days notice is acceptable.
Completed UST closure or change -in-service site assessment reports, along with a copy of the UST-2 form, should be submitted to the appropriate Division
of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be submitted to the Central
Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out. Note: Tank fees may
be due on unregistered tanks.
UST closure and change -in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response. The guidelines can be obtained at http://www.wastenotnc.org/. Note: To close tanks in place you must obtain prior approval
from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS
II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
Facility Name or Company
Circle K Stores, Inc.
Circle K 2708383
Street Address
Facility ID # (If known)
1100 Situs Court, Suite 100
00-0-0000004527
City County
Street Address
Raleigh Wake
873 Old Charlotte Road SW
State Zip Code
City County Zip Code
NC 27606
Concord Cabarrus 28027
Phone Number
Email
Phone Number
7041-583-5762
[e-mail]
N/A
III. CONTACT PERSONNEL
Name:
Company Name:
Job Title:
Phone Number:
Debrah Carl
Circle K Stores, Inc.
Environmental Manager
704-583-5762
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE -IN SERVICE
1. Contact local fire marshal. 5. Provide a sketch locating piping, tanks and a P.E. or L.G., with all closure site
2. Plan entire closure event. soil sampling locations. assessment reports bearing the signature
6. Submit a closure report in the format of and seal of the P.E. or L.G. If a release has
3. Conduct Site Soil Assessment. UST-12 (including the form UST-2) within not occurred, the supervision, signature or
4. If removing tanks or closing in place, refer to thirty (30) days following the site seal of a P.E. or L.G. is not required.
API Publication 2015 Cleaning Petroleum investigation. 8. Keep closure records for three (3) years.
Storage Tanks and 1604 Removal and
7. If a release from the tanks has occurred, the
Disposal of Used Underground Petroleum
site assessment portion of the tank closure
Storage Tanks.
must be conducted under the supervision of
V. WORK TO BE PERFORMED BY
Contractor Name:
Contractor Company Name:
Jerry Stanley
Zebra Environmental & Industrial Services, Inc.
Address:
State:
Zip Code:
Phone No:
P.O. Box 357, High Point
NC
27261
336-841-5276
Primary Consultant Name:
Primary Consultant Company Name:
Consultant Phone No:
Aaron Williamson
Crawford Environmental Services, Inc.
704-909-2911
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE -IN-SERVICE
Proposed Activit
Closure
Change -in -Service
Removal
Abandonment in Place *
New Contents Stored
Tank ID No.
Size in Gallons
Last Contents
1
10000
Gasoline, Gas Mix
2
10000
Gasoline, Gas Mix
3
10000
Gasoline, Gas Mix
®
❑
❑
❑
❑
❑
* Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER'S AUTHORIZED REPRESENTATIVE
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title: Aaron Williamson, Agent for Circle K Stores, Inc.
Signature
Date Signed
SCHEDULED REMOVAL DATE
Notify your DWM Regional Office
5/20/19
48 hours before this date if
AVt1*1_
4/18/19
scheduled removal date changes
UST-3 Rev 1/2019

APPENDIX B
WASTE DISPOSAL MANIFEST

SITE BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
CUSTOMER
ZEBRA ENVIR.OMENTAL & IIdD SERV
PO BOX 35*7
HIGH POINT, NC 27261.
Contract:50101220694
Generator:ZEBRA ENVIRONMENTAL SERVTCES, INC
'SITE Y6
TICKETS 1641358
CELL
WEIGHMASTER Quanta S.
DATEITIME IN/22/19 10:10 amDATE/TIME50yJ
? C) 10:36 aT
VEHICLE ZEBD-3
CONTAINER
REFERENCE 573193
BILL OF LADING
SCALE IN GROSS WEIGHT 45,200 NET TONS 6.83
SCALE OUT TARE WIiI:CGIiT 31,540 NET WEIGHT 13,660
INBOUND
INVOICE
OTY.
UNIT
- DESCRIPTION
RATE
EXTENSION
TAX
TOTAL
0.00
tD
Tracking 4TY '
6.83
to
SW -EMPTY CONT/TANK/VES Origin:MECKLENBURG 100%
1..00
ENVIRONMENTAI, FEE 1
IAR
HATS
ND-SAEELY--/ESIARE REO-UIRED- WkiEN-EXITING_YODUR-VEHICLE _
• e
1NHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
TENDERED
The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions
CHANGE
on the reverse side and that he or she has the authority to sign this document on behalf of the customer.
CHFCIG t
RS-F04211PR 107YI21 SIGNATHRF

REPUBLIC
SERVICES, INC.
. . . . . . . . . . . . . NON
7' DO WASTE MANIFEST
NON
. . -HAZARDOUS
-HAZ�R
1 Generator. US EPA ID Number
2 P. g e 1 of
3. Generator's Name and Mailing Address
5. Generating Location (if different)
�°.w.a*t{Z 0 4, 4".
JN"
4. Phone �Z,7 J
6. Phone
7. Transporter #1 Company Name f
8. US EPA ID Number
9. Transporter #I's Phone
11. US EPA ID Number
12. Transporter #2's Phone
10. Transporter #2 Company Name
13. Designated T/S/D Facility Name and Site Address
14. US EPA ID Number
15. Facility's Phone
61,e,
d Description
17 Allied Waste p. Date 118.
Approval #and Ex
Containers
C
Total
19.-
20. Unit
16. Waite Shipping Name an
I
Quantity
WtIvol
6YNo.
Type
I
JT9
b.
C.
1777�
d.
21. Additional Descriptions for Materials Listed Above
22. Special Handling instructions and Additional Information
manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste.
23. GENERATOR'S CERTIFICATION: I certify the materials described on this rn
A T 0
NERATOR'S
E N -
GE
2 3 G
Signature
Month
Day
Year
d
p.d me
e d/ T N
Printed/
P ri. t Typed Name
y YP
Ji
+
i2 J'
IX
24. Transporter #1: Acknowledgement of Receipt of Materials
LLI
Signature,' 7
Month
Year
t [T
Printed/ Typed Name
..Day
CL
U)
25. Transporter k: Acknowledgement of Receipt of Materials
T I
Z
Signature
Month
Day
Year
I/T
Printed/Typed Name
,"T__F2_6. Discrepancy Indication Space
27. Facility Owner or operator: Certification of receipt of waste materials covered by this manifest (except as noted in Item 19)
X Month
Printed/Typed Name
Signature
RTER #2

B-FI/CMS LANDFILL 704-782-2004 28025
5105 MOREHEAD RD CONCORD,
Nc
i CUSTUNn-K
ZEBRA ENVIRONIENTAL 5 IND SERV
po Bid`: 357
HIGH POINT, NC 27261
Coat, act:501,01,"20E94
Gene__at:or:ZEBRA ENVIRONMENTAL SERVICES, IN
SCALE IN GROSS WEIGHT 44,900
SCALE OUT TARE WEIGHT 28,200
aTEyy ncI<eT If 1641361
VEIGHMASTER ()Uant a S .
DATE(TIME,Uy)1; 2/ 19 1 0: 4 4
)ATEMME IN 5 / 2 / ;l 10 : 2 4 art .
CONTAINER
JEHICLE Zh,BD-6
REFERENCE 5-7 31. 91.
BILL OF LADING
NET TONS 8,35
NET WEIGHT 16,�00
QTY. �
--- 00� yp Tr.a kind QTY
8,31 to Sw-EMPTY CONT/TANK/VES Origin:CARARRUS 100"
1 0 ENVIRCNMEN TAT, FEE 1
INBOUND
INVOICE:
'� �IHNf2�AF_ET_Y�LE.SZ6RF RFOUIREQ�H�i i
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW TENDERED
A SET FROM THE SCALE HOUSE. THANK YOU. CHANGE
CHECKtt
The undersigned side and thatai vidu; in she has the aant on ufhority t g this documaliot gn thistdo ument on ibel9alf otthe custon ehas read and widerstands the terms and conditions
on the revers —
SIGNATURE --
RS-F042UPR (07112)
i

ta,REPUBLIC
SERVICES, INC.
,
7
01 NON -HAZARDOUS WASTE MANIFEST
JL
0
1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 o -K,
A
3. Generator's Name and Mailing Address 5. Generating Location (if different)
4. Phone Cl. 1,1,i;,.) :i, 6. Phone
7. Transporter #1 Company Name 8. US EPA ID Number 9. Transporter #1's Phone
10. Transporter #2 Company Name 11. US EPA ID, Number 12. Transporter #2's Phone
13. Designated T/S/D Facility Name and Site Address 14. US EPA ID Number 15. Facility's Phone
16. Waste Shipping Name and Description A?�Allied Waste Approval # and Exp. Date 18. Containers 19.
aI
Total �0. unit
fZ Quant.tyWtVoI
�f No. Type
a.
P
b.
C.FF
d.
21. Additional Descriptions for Materials Listed Above
22. Special Handling Instructions and Additional Information
23. GENERATOR'S CERTIFICATION: I certify the materials described on this manifest are not subject to federal regulations for reporting proper disposal of Hazardous Waste.
Signature
Month
Day
Year
Printed/Typed Name
4
24. Transporterpi: Acknowledgement of Receipt of Materials
Print6ffNpecl fame
Signatd—re",
Month
Day
Year
25. Transporter #2: ,Acknowledgement of Rebe'Ript of Materials
-
Signature
Month
Day
Year
Printed/Typed Name
I
26. Discrepancy Indication Space

Name
Street Address
813 0 1 P
Ca (-' ��
Mailing Address
Phone 34 �;_A
Conta-cTT-
-
DESCRIPTION OF MATERIALS
USDOT Proper Shipping Name
HMI (Complete All Items for Hazardous Materials)
Hazard
Class or Div
UN I NA
ID No.
Packing
Group
Containers
Qty. Type
Total Unit
Quantity Wt./Vol.
a.
1-1,40nrXys 1�9,&q-o(
,T1,(q-jV1111
ly
/
65
RMATION
V0
This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in
proper condition for transportation according to the applicable regulations of the Department of Transportation. I further certify that
none of the materials described above are a hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law, and
unless specifically identified above, the na ss-1 tain less than 1,000 ppm total halogens and do not contain quantifiable levels
(2 ppm) of PCBs as defined by EPW4 CFR Paits 279nd 761.
Printed I TypedName Signature Mo. I Day
TMNSPORTER INFORMATION `
Transporter Zebra EnVlronm ustrial Services Inc 1 hereby acknowledge receipt of the above -described materials for transport
from the generator site listed above.
Address J
901 East Springfield Road S C
High Point, NC 27263 Signature hipmen Date
I hereby acknowledge recei of the above -described materials were received
Transporter or NC0991302669 Unit No. from the generator site and were transported to the facility listed below.
EPA ID No
i
Phone [phone] SiCSn�ture ��,1_� —f� � Abe i� v G D t e
FACILITY INFORMATION
Facility Zebra Environmental & Industrial Services, Inc. I hereby acknowfed ceipt of the materials covered by this manifest
except for any d rep ncy noted below.
Address
901 East Springfield Road
High Point, NC 27263 Signature ec ' t Date
or EPA ID NCO991302669
EPA 1D No.
Phone [phone]
Contact David Tedder
ORIGINAL - Facility Retain COPY 2 - Return to Generator COPY 3 - Transporter Retain COPY 4 - Generator Retain

t
� p
k: ` NORTH CAROLING
$s,
PUBLIC V11'EI�H�iIASTER
,s xA ao3r 3 ,:, .,. LICENSE E. t JUNE 3D, Z01
.13ford, T,Tt' 2.7v 3 1 JOHN GODF E 42.673
vAiID LESS SIGNED
_Y%T."9t-ai_M3e7,'_A:1?I-K11TQ_:aa'L,A:NIT�1'. fAANTR36°.9T
- fit i T
T Am' d N t = - '--
-10
.._—t{—n.
Mono. f
Te.p .. , 6�
'd✓�' to it : '4P, � `a r t '"' ,�'
Dc,s alatia : ATES o !\T(',LLC —
contact: Scott Ytfler 1 virkie 11oldeff
'2841 '.m-4ryj h.%. a RC.:.t-1.t(},pim Ville, NC 27360
Pa1One:
��i�•.
Eck"x�.�;�;��.`�..3�➢'��i'�L,"�,��°�? �G'1�_. ,��_
� �s�
aj
3 A mrq Nveinht
l
L� Wt ?!Y -*��
slab f k t ot rlea 7 sep latiotr for eporting 0,roper di sal of F APMOUS � ASTIE.
t
i5�.7 s f*�A
�rt�x�:� :dew,;
X
1:S
t -
,,

i
6� ttiV3L0� �VEI 9, MASTE
�< Mr-',
, F LICENSE �X �� �5 JU a9 E 3� 42673
�'�ES gay I� ,1,.�i�� JOIN GO�AU,
��
Post .1. C7s LESS SIC1IV
im
PhC A'.tO t ';.31 X"i-77in-4517
N0P-T4ffiVZAPZlOUS WASTE
Load Numbcx: J--f ell_
Contact L �
i
Contact:'
Phone: - 70
3 41 'Momasville, NTG 27360
Contact: 13tc2G$: Scott 4,0 lG;Ti +" 'dY1 <_�.0 IC?lder�
��y
Pildfle: =?lam "'744518m7 D, Sirc
GOO Weight:
Weight:
iy r R"
�sE 1vr �yT fi i ?rfi1 9:G�At �Sa: GE aij Ti�di Z41� ii� T%'r2�li�i CiG' Grl it <1t7t�; OR LU15 zx3_tira 103t,�l9
mi�ject tq tedenai rpFdat" for reporting proper disposed of T,-DkZ +R-0T. S W:<!,` TF—
Drivers Sipature. DaW
Notecl
Ins -peeled SL Acccptld (cx C',�,lxla6#cd above by:.��,S ref NC. ,
s

NCRtWSGjjmAsrsR 4
pUBI.IC fs jtjNE 30y:30't
LICENSE E �tR 426
JOHN GOa REj
pov � ifir : Rik O l f 'In-�` SS 810N1"Ct�;,
Fax rit
L-ura%Nusabe 7z— _•� ..
a'
i�_'3_ ,,�rr;�•ta� f(_�J _ °�'s1a.�'s- t(M,)3'' .D /�`p"5�`qg� 5+,� a� .a..,.._..._..__...,.._. �
(� cY;'� �n{. ��, Fyi-,.t..�� �. Ff' ._............._.»_......._._�•..._....�.M....5 �.- ar�J �.ii.. • f/ �N' � � C p� �L.. �. '��
Mil. Cimnir 4-tom Road
3 iirs.rissrfYfl�, 11C., ZT— • _•,._ �_•••• 1�: B0.,_ 4 T €� r 1 i e ��
13
J V
��`�`��' N � .its ;•� rkf �% ,� f �
'.si;: say �'�'-�.,.,,.._.._....•.e.., .....�._....__.....• "rY't5:i'it.{•_.,-__...r..<�w.....__.,... 1
�a y 1 e� i a ` Y �
F.
i
e
ICr?A f-fj ffii�aT.. til s�?�Q.'f'�3 bk:35i ������:�•m"" a�'+$bwe cal L: is �i��#.ffes" i3C�
a>.i¢`,�"!•tr.°LY4Z.�.£°i::;k3'�i�i.k�}iY�3aa�aP3S':t�"e??�.3�ii,`���fi���t �45�'y����§��.�.1���''+��a'-r`� S�.c`n.:v��. -
1.�.sk-3LT a ktRi tz? ;:r;s.a
dl�. 7i tiY a� �.__. �_.. _ _ w rr �• _
- �� �s?'3L;.� C�i . �'A k�l��ry',.E. � i£ � �e %5'a`�' � k�•'�.e'f. 3'i4'�..�x `a i3•'iR�.'�,�5; aiFia..
�� 4J,

NugTH CAROfi NA u r
PUBLIC WlEIGH ASTER209�
LICENSe EXPIRI J NE 3042019
JOHN GO�FREY
LID
Fist LXfh arlw3l � SS SIGNED
INV ID UN
11;au* "-ate'
- z er-a a;r ? r" i .Fite& pq CA- L.
MRRU
1
y
Fi t, �1 y,�c? � cg%i�k<=Trf— � 0
f s.a i .
Net Weiwit
L7....
are mop:
v aS iN STE.
s'ai7. ,r:,?r::ic 9x3r3''.e%'$R.ne - .,` �' .-g"✓i,�F .r.,_�. C

NORTH CAROLING
PUBLIC WEI HMASTER
LICENSE EXPREk§ JUNE 30, 2019
JOHN GO DFR Y ` 42673
Rcst Off �: 72,aa 0 INVALID ��1LESS SIGNED
sonf
Fax
<-i'4It'7 'ST dM21 .._.. ..
a
3 3 ` � w"'
Lehi,
S2,
�.'.p�..._.._a..._.. �•� _..�. __. _ .._..._._..r._...._._ �• ¢� {� ,{ Wig• 61 i
j,tf �l�d.�T:ii{'+`r._'Lt.�.d. .f�. �a:{i� �q�� _ c��J _..�_.�... P4.•M1();ii'?n'in�w, .._ �..._._. �T�...•'4.a'��.il S'<vl.'_.E.a.�.�,$.:�e.��.ff: +t.�V� F.E j ..
{3�69'.� j�p'}�,��c �'y �p� rn• �ry (�� y i "ty,
23 £'�N' 3'•:'ll�i ii+`�, NCuse s 36zl a�i� /�w71i��{
"Zz
g
pet weleilt
_Ubjectt T d . t s , s ASYT.
rjat(;,
.z „z r i r e�," 1 �' t L•( i' Eye � E,�, r c t ? f?
Drivers Siulstu're -Pate.
a?;..a�?�44<�s�Au _- ``' Sf �n2�3� � ld � a� �� � 8...:.....__.��....,r....r_ �......' ______._._ ' .��.:.....'C"`C•:;�..�
-E-xqlscied 4t Ac"n.. j' r.t h 'G . e st i`ik". £ :L' Inc,,

l
®1�TN AB®LIKA
El
PUBL C W GHNIAST10
A�s JUNE 30, �Q1�
ok Off Rtr: � 1i) LICENSE p1X b2613
a{ _ y� �1 JOIN �0 �3
J ord— M ' ,
} `� �s ��-2'k-O%p IAIVALID UNLESS SIGNE®
R .
YE c
S C MT T X t ..1',T SZi. I iAz,7 KEK
3yt£ is, ..ram 77(l
4-773
i
. lC :3'u that, +filFkk �ddi'��2?3�'7:a'$e�ks ? 3{�'e¢�s�1'
;.C1r ptw- er4n Osal Ls 18'rs! "' i :_
TP
_�,lr..,2�!►eit�r'��<�Gut �i rr�..+:Y�.4z s� �:li...x'��x`�.�?: 'tom _ L 2"` r¢"J ____._. - - �-_.__ _.___.� _.
sigmaure
_i&, a'W Jee .z .fi' 5 2u.,^7 3 lr.'i}
_0,
!!(epp{{ ,�

APPENDIX C
SITE PHOTOGRAPHS

PHOTOGRAPHIC LOG
Crawford Environmental Services, Inc.
1701 Shenandoah Avenue NW
Roanoke, VA 24017
CRAWFORDCNVIRONMENTAL
SERVICES
Site Location: Circle K 2708383
Client Name: CES Project #:
Circle K Stores, Inc. 873 Old Charlotte Road Southwest 6.0005
Concord, NC

PHOTOGRAPHIC LOG
Crawford Environmental Services, Inc. 1^`1_1��
1701 Shenandoah Avenue NW CRAWFORDCNVIRONMENTAL
Roanoke, VA 24017 SERVICES
Site Location: Circle K 2708383
Client Name: CES Project #:
Circle K Stores, Inc. 873 Old Charlotte Road Southwest 6.0005
Concord, NC
Photograph #4
Photo taken looking:
Southwest
Description:
View of UST pit
following removal of
tanks. Note pea gravel
fill material.

PHOTOGRAPHICLOG Crawford Environmental Services, Inc. .nn��-�
1701 Shenandoah Avenue NW CRAWFORDCNVIRONMENTAL
Roanoke, VA 24017 SERVICES
Site Location: Circle K 2708383
Client Name: CES Project #:
Circle K Stores, Inc. 873 Old Charlotte Road Southwest 6.0005
Concord, NC
Photograph #5
Photo taken looking:
West
Description:
Typical view of
product line area over -
excavation efforts.

PHOTOGRAPHIC LOG
Crawford Environmental Services, Inc.
1701 Shenandoah Avenue NW
Roanoke, VA 24017
CRAWFORDCNVIRONMENTAL
SERVICES
Site Location: Circle K 2708383
Client Name: CES Project #:
Circle K Stores, Inc. 873 Old Charlotte Road Southwest 6.0005
Concord, NC

APPENDIX D
UST-2A FORM

UST'2A
Site Investigation Report for Permanent Closure or Change -in -
PC.
Service of
REGISTERED UST `"'�
Return completed form to:
STATE USE ONLY:
NC DEQ / DWM / UST SECTION
Facility ID #
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING
Date Received
phone [phone] fax [phone] http://www.wastenotnc.org/
INSTRUCTIONS READ THIS FIRST
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deg.nc.gov/gbout/divisions/waste-management/waste-
management-permit-quidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change -in-service: Where a UST system will be converted from storing a regulated substance to a non -regulated substance, complete sections I, ll,
III, IV, and VI
4. For more than 5 registered UST systems, attach additional forms as needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-26
I. OWNERSHIP OF TANKS
II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
Facility Name or Company
Circle K Stores, Inc.
Former Circle K 2708383
Street Address
Facility ID # (If known)
2550 West Tyvola Road, Suite 200
4527
City County
Street Address
Charlotte Mecklenburg
873 Old Charlotte Road Southwest
State Zip Code
City County Zip Code
NC 28217
Concord Cabarrus 28027
Phone Number
Phone Number
704-583-5762
N/A
III. CONTACT PERSONNEL
Contact for Facility:
Job Title:
Phone #:
Debrah Carl
Environmental Mgr
704-583-5762
Closure Contractor Name:
Closure Contractor Company:
Address: Po sox 357
Phone #
Barry Ward
Zebra Environmental & Ind. Sry
High Point, NC 27261
336-841-5276
Primary Consultant Name:
Primary Consultant Company:
Address:1701 Shenandoah Ave
N wPhone #
Aaron Williamson
Crawford Environmental Srvs.
Roanoke, VA 24017
540-343-6259
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
V. EXCAVATION CONDITION
UNREGISTERED USTs use Form UST-213
Tank ID
Size in
Last
Last
Permanent
Method of Permanent Closure:
Change -in-
Notable
No.
Gallons
Contents
Use
Close Date
Indicate REMOVED or enter fill
Service
Water in
Free product
odoror
visible soil
Date
material, such as foam/
Date
excavation
contaminatio
concrete/ sand
n
Yes
No
Yes
No
Yes
No
1
10000
Gasoline, C
5/8/19
5/22/19
REMOVED
N/A
❑
®
❑
®
®
❑
2
10000
Gasoline,
5/8/19
5/22/19
REMOVED
N/A
❑
®
❑
®
®
❑
3
10000
Gasoline,
5/8/19
5/22/19
REMOVED
N/A
❑
®
❑
®
®
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate
and complete.
Print name and official title of owner or owner's authorized representative
Aaron R. Williamson
Signature
Date Signed
6/18/19
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] htt ://www.wastenotnc.or / 1/2016

APPENDIX E
LABORATORY ANALYTICAL REPORT & CHAIN -OF -CUSTODY FORM(S)

B'M
REDL
A(DRcY5
_
,
RAPID ENVIRONMENTAL DIAGNOSTICS
suits
Client: CRAWFORD ENVIRONMENTAL
Samples taken
Wednesday, May 22, 2019
Address:
Samples extracted
Wednesday, May 22, 2019
Samples analysed
Wednesday, May 22, 2019
Contact: AARON WILLIAMSON
Operator
CAROLINE STEVENS
Project: CIRCLE K 2708383
U04049
Matrix
Sample ID
Dilution
BTEX
GRO
DRO
TPH
Total
Aromatics
16 EPA
BaP
Ratios
HC Fingerprint Match
used
(C6 - C9)
(C5
- C10)
(C10 - C35)
(C5 - C35)
(C10-C35)
PAHs
%light
%mid
%
AL
heavy
s
STOCKPILE
27.4
<0.68
1.9
6.9
8.8
2
<0.22
<0.027
77.9
14.6
7.5
Deg.Fuel81%,(FCM)
s
SS-1
25.0
<0.63
2.2
<0.63
2.2
<0.13
<0.2
<0.025
99.2
0.8
0
Deg.Gas,(FCM)
s
SS-2
25.0
<0.63
<0.63
<0.63
<0.63
<0.13
<0.2
<0.025
0
100
0
Residual HC,(P)
s
SS-3
26.0
<0.65
3.4
10.5
13.9
4.1
<0.21
<0.026
78.3
15.8
5.8
V.Deg.Diesel 82.6%,(FCM)
s
SS-4
21.7
11.9
22.5
41.3
63.8
52.7
2
<0.022
94.8
4
1.3
Deg.Fuel67.1%,(FCM)
s
SS-5
11.2
<0.28
<0.28
<0.28
<0.28
<0.06
<0.09
<0.011
0
36.2
63.8
Residual HC,(BO)
s
SS-6
33.8
20.3
44
186.2
230.2
41.5
1.5
<0.034
96.6
1.6
1.8
Deg.Diesel 58.6%,(FCM)
s
SS-7
12.8
<0.32
<0.32
0.32
0.32
0.19
<0.1
<0.013
0
52.5
47.5
V.Deg.PHC 62.8%,(FCM),(P)
s SS-8
23.9
353.1
2435 244.5 2679.5 1229
47.4
<0.024 - -
- Deg.Gas,(FCM),(OCR)
s SS-9
1 22.4
<0.56
4.5 0.56 5.06 0.3
<0.18
<0.022 98.8 0.4
0.8 Deg.Gas,(FCM)
Initial
No
O 100.8 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations
are:-
FCM = Results calculated using Fundamental Calibration
Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result
: (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present

QED Hydrocarbon Fingerprints
Project: CIRCLE K 2708383 5/22/2019
' STOCKPILE: Deg.Fuel 81%,(FCM)
SS Dl eg aGaG s,(FCM)
SS-3 : V.Deg.Diesel 82,61/o,(FCM)
SS-4 : Deg.Fuel 67.10/o,(FCM) 1
OEp
8833
SS-7 : V.Deg.PHC 62.8%,(FCM),(P)
I SS-8 : Deg.Gas,(FCM),(OCR) I
0,E0
63952
7001
QED
3438
OE
981
OEE:)I
700

B'M
REDL
A(DRcY5
_
,
RAPID ENVIRONMENTAL DIAGNOSTICS
suits
Client: CRAWFORD ENVIRONMENTAL
Samples taken
Wednesday, May 22, 2019
Address:
Samples extracted
Wednesday, May 22, 2019
Samples analysed
Wednesday, May 22, 2019
Contact: AARON WILLIAMSON
Operator
CAROLINE STEVENS
Project: CIRCLE K 2708383
U04049
Matrix
Sample ID
Dilution
BTEX
GRO
DRO
TPH
Total
Aromatics
16 EPA
BaP
Ratios
HC Fingerprint Match
used
(C6 - C9)
(C5
- C10)
(C10 - C35)
(C5 - C35)
(C10-C35)
PAHs
%light
%mid
%
im
heavy
S
SS-10
24.5
<1.2
4
24.1
28.1
0.83
<0.2
<0.025
99.5
0.3
0.2
Deg.Kerosene 80.8%,(FCM)
S
SS-11
21.7
26.2
150.2
32.1
182.3
10.5
0.38
<0.022
99.5
0.2
0.3
Deg Gas 69.3%,(FCM)
S
SS-12
20.2
2.2
4.4
5.4
9.8
0.37
<0.16
<0.02
99.5
0.4
0.1
Deg.Diesel57.5%,(FCM)
S
SS-13
28.3
375.6
2935
185.2
3120.2
117.7
4.7
<0.028
99.8
0.1
0.1
Deg.Gas 83.9%,(FCM),(OCR)
S
SS-14
30.2
<0.76
<0.76
<0.76
<0.76
<0.15
<0.24
<0.03
0
0
0
PHC not detected
S
SS-15
22.2
<0.56
2.9
0.56
3.46
0.47
<0.18
<0.022
89.8
4.7
5.6
V.Deg.PHC 73.8%,(FCM)
S
SS-16
22.4
24.4
118.1
20.5
138.6
0.66
<0.18
<0.022
99.7
0.1
0.2
Undeg.Gas + Waste Oil 71.9%,(FCM)
S SS-17
19.3
<0.48
2 7 9 0.46
<0.15
<0.019 94.5 5.5
0 Degraded Oil 63.6%,(FCM)
S SS-18
14.8
<0.37
<0.37 0.37 0.37 0.24
<0.12
<0.015 0 47.6
52.4 V.Deg.PHC 59.6%,(FCM)
s SS-19
1 17.9
<0.45
<0.45 <0.45 <0.45 <0.09
<0.14
<0.018 0 30.91
69.1 lResidual HC,(BO)
Initial VcMMul
LAIL, MM
~ FCIVI QC CheLK
97.5
O q El
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations
are:-
FCM = Results calculated using Fundamental Calibration
Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result
: (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present

QED Hydrocarbon Fingerprints
Project: CIRCLE K 2708383 5/22/2019
SS-10 : Deg.Kerosene 80.8%,(FCM) I
SS-12 : Deg.Diesel 57.5%,(FCM)
SS-14 : PHC not detected
OE
7111
7001
(DE
700
SS-16 : Undeg.Gas+ Waste Oil 71.9%,(FCM)
n OE Q
/ 1n 2743
SS-17 : Degraded Oil 63.6%,(FCM)
SS-19 : Residual HC,(BO)
CEO
1947
C C
7001

_ REDL , B'M
RAPID ENVIRONMENTAL DIAGNOSTICS A(DRcY5
Client: CRAWFORD ENVIRONMENTAL Samples taken Wednesday, May 22, 2019
Address: Samples extracted Wednesday, May 22, 2019
Samples analysed Wednesday, May 22, 2019
Contact: AARON WILLIAMSON Operator CAROLINE STEVENS
Project: CIRCLE K 2708383
U04049
Dilution BTEX GRO DRO TPH Total 16 EPA
Matrix Sample ID used (C6 - C9) (C5 - C10) (C10 - C35) (C5 - C35) Aromatics PAHs BaP Ratios HC Fingerprint Match
(C10-C35) I I _
s
STOCKPILE 2
21.0
<0.52
<0.52
<0.52
<0.52
s
SS-6A
31.0
<0.77
564.6
336.7
901.3
s
LOAD 2
53.4
3.9
415.7
411.5
827.2
s
SS-613
20.5
<0.51
309.5
297.2
606.7
s
SS-13A
25.5
<0.64
>232.7
>124.1
>356.8
s
SS-8A
23.2
286.8
2135
150.4
2285.4
Initial MlbratoTZ1C check OK
light
% mid
heavy
<0.1
<0.17
<0.021
0
100
C
1796
69.9
<0.031
99
0.6
0.4
1280
47.7
<0.053
90.3
8.3
1.4
186.1
7.2
<0.02
-
-
>333.2
>13
<0.025
98.7
0.7
O.E
582
22.7
<0.0231
99.7
0.1
0.2
nal FCM QCTie fr O
not detected,(P)
Gas 85.5%,(FCM)
Fuel 62.4%,(FCM)
Gas, (FCM),(PFM),(OCR)
Gas 63.7%,(FCM)
Gas 82.8%,(FCM),(OCR)
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present

Project: CIRCLE K 2708383
LOAD 2 : Deg.Fuel 62.4%,(FCM)
55-13A : Deg.Gas 63.7%,(FCM)
QED Hydrocarbon Fingerprints
OE Q
31280
OE
240851
SS-6A : Deg.Gas 85.5%,(FCM)
55-6B : Deg Gas, (FCM),(PFM),(OCR)
SS-8A : Deg.Gas 82.8%,(FCM),(OCR)
5/22/2019
E ED
480,) I
OE Q
60167
406611

_
REDL , B'M
RAPID ENVIRONMENTAL DIAGNOSTICS
A(DRcY5
suits
Client: CRAWFORD ENVIRONMENT
Address:
Contact: AARON WILLIAMSON
Project: CIRCLE K 2708383
Samples taken
Samples extracted
Samples analysed
Operator
Wednesday, May 22, 2019
Wednesday, May 22, 2019
Wednesday, May 22, 2019
CAROLINE STEVENS
U04049
Matrix
im
Sample ID
Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs
BaP
Ratios
HC Fingerp
%light
% mid
heavy
s
SS-11A
21.8
<0.55
347.7
278.9
626.6
164.3
6.5
<0.022
99
0.7
0.3
Deg Gas 90.1%,(FCM),(PFM),(BO)
s
LOAD 3
26.3
<0.66
406.9
308.4
715.3
181.7
7.2
<0.026
99.1
0.7
0.3
Deg.Gas 90.1 %,(FCM),(PFM),(OCR)
s
SIDEWALL SE
28.0
<0.7
<0.7
0.7
0.7
0.39
<0.22
<0.028
91.1
3.9
5
Residual HC,(OCR)
s
L SIDEWALL NE
24.3
<0.61
10.2
11.4
21.6
7.2
0.3
<0.024
76.5
17.8
5.7
Deg Fuel 77.1%,(FCM)
s
L SIDEWALL SE
18.7
5.6
9.9
13.2
23.1
12.7
0.5
<0.019
92.5
5.4
2.1
Deg.Fuel 77.7%,(FCM)
s
L SIDEWALL NW
11.9
<0.3
<0.3
0.3
0.3
0.29
<0.09
<0.012
0
53.8
46.2
V.Deg.PHC 63.8%,(FCM),(P)
s
SIDEWALL NW
18.2
<0.45
<0.45
<0.45
<0.45
<0.09
<0.15
<0.018
0
0
0
PHC not detected
s
SIDEWALL NE
14.3
<0.36
<0.36
<0.36
<0.36
<0.07
<0.11
<0.014
0
0
0
,(FCM),(P)
s
SIDEWALL SW
25.7
<0.64
<0.64
<0.64
<0.64
<0.13
<0.21
<0.026
0
0
0
PHC not detected
Initial
O
99.1 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present

QED Hydrocarbon Fingerprints
Project: CIRCLE K 2708383 5/22/2019
SS-11A : Deg Gas 90.1%,(FCM),(PFM),(BO) I
SIDEWALL SE: Residual HC,(OCR)
LSIDEWALL SE: Deg.Fuel77.7%,(FCM)
0E )
54123
OE
7001
OE
42591
SIDEWALL NW: PHC not detected I
SIDEWALL SW: PHC not detected
OE
700
07
700
LOAD 3 : Deg.Gas 90.1%,(FCM),(PFM),(OCR)
QED
50215
L SIDEWALL NE : Deg Fuel 77.1%,(FCM)
(DE Q
8619
L SIDEWALL NW: V.Deg. PHC 63.8%,(FCM),(P)
17521

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 04, 2019
Aaron Williamson
Crawford Environmental
301 McCullough Dr
Suite 400
Charlotte, NC 28262
RE: Project: Circle K 2708383
Pace Project No.: 92430462
Dear Aaron Williamson:
Enclosed are the analytical results for sample(s) received by the laboratory on May 23, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, p
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Circle K 2708383
Pace Project No.: 92430462
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 43

aceAnalytical
—pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Circle K 2708383
Pace Project No.: 92430462
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92430462001
Sidewall SE
Solid
05/22/19 13:35
05/23/19 11:36
92430462002
Sidewall NE
Solid
05/22/19 13:55
05/23/19 13:41
92430462003
Sidewall SW
Solid
05/22/19 14:02
05/23/19 13:41
92430462004
Sidewall NW
Solid
05/22/19 14:00
05/23/19 13:41
92430462005
Base
Solid
05/22/1914:15
05/23/19 13:41
92430462006
L Sidewall SE
Solid
05/22/19 13:37
05/23/19 13:41
92430462007
L Sidewall NE
Solid
05/22/19 13:38
05/23/19 13:41
92430462008
L Sidewall NW
Solid
05/22/19 13:40
05/23/19 13:41
92430462009
L Base
Solid
05/22/19 00:00
05/23/19 13:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Circle K 2708383
92430462
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92430462001
Sidewall SE
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462002
Sidewall NE
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462003
Sidewall SW
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462004
Sidewall NW
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462005
Base
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462006
L Sidewall SE
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462007
L Sidewall NE
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462008
L Sidewall NW
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430462009
L Base
MADEP VPH
LMB
6
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall SE
Lab ID:
92430462001
Collected:
05/22/19
13:35
Received: 05/23/19 11:36 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND
mg/kg
4.1
4.1
1
05/24/19 09:21
05/24/19 12:00
N2
Aliphatic (C09-C12)
ND
mg/kg
4.1
4.1
1
05/24/19 09:21
05/24/19 12:00
N2
Aliphatic(C09-C12) Adjusted
ND
mg/kg
4.1
4.1
1
05/24/19 09:21
05/24/19 12:00
N2
Aromatic (C09-C10)
ND
mg/kg
4.1
4.1
1
05/24/19 09:21
05/24/19 12:00
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
93
%
70-130
1
05/24/19 09:21
05/24/19 12:00
460-00-4
4-Bromofluorobenzene (PID) (S)
93
%
70-130
1
05/24/19 09:21
05/24/19 12:00
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
0.22
mg/kg
0.12
0.012
1
06/03/19 13:55
06/03/19 20:03
67-64-1
Benzene
0.0024J
mg/kg
0.0058
0.0019
1
06/03/19 13:55
06/03/19 20:03
71-43-2
Bromobenzene
ND
mg/kg
0.0058
0.0023
1
06/03/19 13:55
06/03/19 20:03
108-86-1
Bromochloromethane
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
74-97-5
Bromodichloromethane
ND
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
75-27-4
Bromoform
ND
mg/kg
0.0058
0.0027
1
06/03/19 13:55
06/03/19 20:03
75-25-2
Bromomethane
ND
mg/kg
0.012
0.0029
1
06/03/19 13:55
06/03/19 20:03
74-83-9
2-Butanone (MEK)
0.073J
mg/kg
0.12
0.0034
1
06/03/19 13:55
06/03/19 20:03
78-93-3
n-Butylbenzene
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0058
0.0019
1
06/03/19 13:55
06/03/19 20:03
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0058
0.0023
1
06/03/19 13:55
06/03/19 20:03
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0058
0.0030
1
06/03/19 13:55
06/03/19 20:03
56-23-5
Chlorobenzene
ND
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
108-90-7
Chloroethane
ND
mg/kg
0.012
0.0028
1
06/03/19 13:55
06/03/19 20:03
75-00-3
Chloroform
ND
mg/kg
0.0058
0.0019
1
06/03/19 13:55
06/03/19 20:03
67-66-3
Chloromethane
ND
mg/kg
0.012
0.0028
1
06/03/19 13:55
06/03/19 20:03
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0058
0.0042
1
06/03/19 13:55
06/03/19 20:03
96-12-8
Dibromochloromethane
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
106-93-4
Dibromomethane
ND
mg/kg
0.0058
0.0029
1
06/03/19 13:55
06/03/19 20:03
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0058
0.0023
1
06/03/19 13:55
06/03/19 20:03
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
0.0042
1
06/03/19 13:55
06/03/19 20:03
75-71-8
L1
1,1-Dichloroethane
ND
mg/kg
0.0058
0.0017
1
06/03/19 13:55
06/03/19 20:03
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0058
0.0026
1
06/03/19 13:55
06/03/19 20:03
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0058
0.0016
1
06/03/19 13:55
06/03/19 20:03
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0058
0.0017
1
06/03/19 13:55
06/03/19 20:03
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall SE Lab ID: 92430462001 Collected: 05/22/19 13:35 Received: 05/23/19 11:36 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
trans- 1,3-Dichloropropene
ND
mg/kg
0.0058
0.0017
1
06/03/19 13:55
06/03/19 20:03
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
108-20-3
Ethylbenzene
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0058
0.0023
1
06/03/19 13:55
06/03/19 20:03
87-68-3
2-Hexanone
ND
mg/kg
0.058
0.0045
1
06/03/19 13:55
06/03/19 20:03
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
99-87-6
Methylene Chloride
ND
mg/kg
0.023
0.0035
1
06/03/19 13:55
06/03/19 20:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.058
0.0043
1
06/03/19 13:55
06/03/19 20:03
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0058
0.0017
1
06/03/19 13:55
06/03/19 20:03
1634-04-4
Naphthalene
0.0047J
mg/kg
0.0058
0.0014
1
06/03/19 13:55
06/03/19 20:03
91-20-3
n-Propylbenzene
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
103-65-1
Styrene
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0058
0.0024
1
06/03/19 13:55
06/03/19 20:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
79-34-5
Tetrachloroethene
ND
mg/kg
0.0058
0.0020
1
06/03/19 13:55
06/03/19 20:03
127-18-4
Toluene
0.0026J
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0058
0.0026
1
06/03/19 13:55
06/03/19 20:03
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0058
0.0019
1
06/03/19 13:55
06/03/19 20:03
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0058
0.0024
1
06/03/19 13:55
06/03/19 20:03
79-00-5
Trichloroethene
ND
mg/kg
0.0058
0.0024
1
06/03/19 13:55
06/03/19 20:03
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0058
0.0026
1
06/03/19 13:55
06/03/19 20:03
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0058
0.0019
1
06/03/19 13:55
06/03/19 20:03
96-18-4
1,2,4-Trimethylbenzene
0.0070
mg/kg
0.0058
0.0023
1
06/03/19 13:55
06/03/19 20:03
95-63-6
1,3,5-Trimethylbenzene
0.0023J
mg/kg
0.0058
0.0021
1
06/03/19 13:55
06/03/19 20:03
108-67-8
Vinyl acetate
ND
mg/kg
0.058
0.010
1
06/03/19 13:55
06/03/19 20:03
108-05-4
Vinyl chloride
ND
mg/kg
0.012
0.0021
1
06/03/19 13:55
06/03/19 20:03
75-01-4
Xylene (Total)
ND
mg/kg
0.012
0.0042
1
06/03/19 13:55
06/03/19 20:03
1330-20-7
m&p-Xylene
ND
mg/kg
0.012
0.0042
1
06/03/19 13:55
06/03/19 20:03
179601-23-1
o-Xylene
0.0023J
mg/kg
0.0058
0.0022
1
06/03/19 13:55
06/03/19 20:03
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
06/03/19 13:55
06/03/19 20:03
2037-26-5
4-Bromofluorobenzene (S)
100
%
70-130
1
06/03/19 13:55
06/03/19 20:03
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-132
1
06/03/19 13:55
06/03/19 20:03
17060-07-0
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
22.7
%
0.10
0.10
1
05/23/19 17:43
REPORT OF LABORATORY ANALYSIS
L1
L1,v1
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall NE
Lab ID:
92430462002
Collected:
05/22/19
13:55
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:29
N2
Aliphatic (C09-C12)
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:29
N2
Aliphatic(C09-C12) Adjusted
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:29
N2
Aromatic (C09-C10)
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:29
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
96
%
70-130
1
05/24/19 09:21
05/24/19 12:29
460-00-4
4-Bromofluorobenzene (PID) (S)
96
%
70-130
1
05/24/19 09:21
05/24/19 12:29
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
0.13
mg/kg
0.12
0.012
1
06/03/19 13:55
06/03/19 18:23
67-64-1
Benzene
0.043
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:23
71-43-2
Bromobenzene
ND
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:23
108-86-1
Bromochloromethane
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
74-97-5
Bromodichloromethane
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
75-27-4
Bromoform
ND
mg/kg
0.0062
0.0028
1
06/03/19 13:55
06/03/19 18:23
75-25-2
Bromomethane
ND
mg/kg
0.012
0.0031
1
06/03/19 13:55
06/03/19 18:23
74-83-9
2-Butanone (MEK)
0.037J
mg/kg
0.12
0.0036
1
06/03/19 13:55
06/03/19 18:23
78-93-3
n-Butylbenzene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:23
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:23
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0062
0.0032
1
06/03/19 13:55
06/03/19 18:23
56-23-5
Chlorobenzene
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
108-90-7
Chloroethane
ND
mg/kg
0.012
0.0030
1
06/03/19 13:55
06/03/19 18:23
75-00-3
Chloroform
ND
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:23
67-66-3
Chloromethane
ND
mg/kg
0.012
0.0030
1
06/03/19 13:55
06/03/19 18:23
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0062
0.0045
1
06/03/19 13:55
06/03/19 18:23
96-12-8
Dibromochloromethane
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
106-93-4
Dibromomethane
ND
mg/kg
0.0062
0.0031
1
06/03/19 13:55
06/03/19 18:23
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:23
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
0.0045
1
06/03/19 13:55
06/03/19 18:23
75-71-8
L1
1,1-Dichloroethane
ND
mg/kg
0.0062
0.0019
1
06/03/19 13:55
06/03/19 18:23
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0062
0.0027
1
06/03/19 13:55
06/03/19 18:23
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0062
0.0017
1
06/03/19 13:55
06/03/19 18:23
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0062
0.0019
1
06/03/19 13:55
06/03/19 18:23
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall NE Lab ID: 92430462002 Collected: 05/22/19 13:55 Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
trans- 1,3-Dichloropropene
ND
mg/kg
0.0062
0.0019
1
06/03/19 13:55
06/03/19 18:23
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
108-20-3
Ethylbenzene
0.0029J
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:23
87-68-3
2-Hexanone
ND
mg/kg
0.062
0.0048
1
06/03/19 13:55
06/03/19 18:23
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
99-87-6
Methylene Chloride
ND
mg/kg
0.025
0.0037
1
06/03/19 13:55
06/03/19 18:23
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.062
0.0046
1
06/03/19 13:55
06/03/19 18:23
108-10-1
Methyl-tert-butyl ether
0.0028J
mg/kg
0.0062
0.0019
1
06/03/19 13:55
06/03/19 18:23
1634-04-4
Naphthalene
ND
mg/kg
0.0062
0.0015
1
06/03/19 13:55
06/03/19 18:23
91-20-3
n-Propylbenzene
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
103-65-1
Styrene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0062
0.0026
1
06/03/19 13:55
06/03/19 18:23
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
79-34-5
Tetrachloroethene
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:23
127-18-4
Toluene
0.0079
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0062
0.0027
1
06/03/19 13:55
06/03/19 18:23
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:23
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0062
0.0026
1
06/03/19 13:55
06/03/19 18:23
79-00-5
Trichloroethene
ND
mg/kg
0.0062
0.0026
1
06/03/19 13:55
06/03/19 18:23
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0062
0.0027
1
06/03/19 13:55
06/03/19 18:23
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:23
96-18-4
1,2,4-Trimethylbenzene
0.0025J
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:23
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:23
108-67-8
Vinyl acetate
ND
mg/kg
0.062
0.011
1
06/03/19 13:55
06/03/19 18:23
108-05-4
Vinyl chloride
ND
mg/kg
0.012
0.0022
1
06/03/19 13:55
06/03/19 18:23
75-01-4
Xylene (Total)
0.0071J
mg/kg
0.012
0.0045
1
06/03/19 13:55
06/03/19 18:23
1330-20-7
m&p-Xylene
0.0066J
mg/kg
0.012
0.0045
1
06/03/19 13:55
06/03/19 18:23
179601-23-1
o-Xylene
0.0071
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:23
95-47-6
Surrogates
Toluene-d8 (S)
102
%
70-130
1
06/03/19 13:55
06/03/19 18:23
2037-26-5
4-Bromofluorobenzene (S)
99
%
70-130
1
06/03/19 13:55
06/03/19 18:23
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-132
1
06/03/19 13:55
06/03/19 18:23
17060-07-0
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
23.7
%
0.10
0.10
1
05/23/19 17:43
REPORT OF LABORATORY ANALYSIS
L1
L1,v1
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall SW
Lab ID:
92430462003
Collected:
05/22/19
14:02
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:59
N2
Aliphatic (C09-C12)
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:59
N2
Aliphatic(C09-C12) Adjusted
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:59
N2
Aromatic (C09-C10)
ND
mg/kg
4.2
4.2
1
05/24/19 09:21
05/24/19 12:59
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
96
%
70-130
1
05/24/19 09:21
05/24/19 12:59
460-00-4
4-Bromofluorobenzene (PID) (S)
96
%
70-130
1
05/24/19 09:21
05/24/19 12:59
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
ND
mg/kg
0.12
0.012
1
06/03/19 13:55
06/03/19 18:48
67-64-1
Benzene
ND
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:48
71-43-2
Bromobenzene
ND
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:48
108-86-1
Bromochloromethane
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:48
74-97-5
Bromodichloromethane
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:48
75-27-4
Bromoform
ND
mg/kg
0.0062
0.0028
1
06/03/19 13:55
06/03/19 18:48
75-25-2
Bromomethane
ND
mg/kg
0.012
0.0031
1
06/03/19 13:55
06/03/19 18:48
74-83-9
2-Butanone (MEK)
0.0050J
mg/kg
0.12
0.0036
1
06/03/19 13:55
06/03/19 18:48
78-93-3
n-Butylbenzene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:48
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:48
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:48
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0062
0.0032
1
06/03/19 13:55
06/03/19 18:48
56-23-5
Chlorobenzene
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:48
108-90-7
Chloroethane
ND
mg/kg
0.012
0.0030
1
06/03/19 13:55
06/03/19 18:48
75-00-3
Chloroform
ND
mg/kg
0.0062
0.0020
1
06/03/19 13:55
06/03/19 18:48
67-66-3
Chloromethane
ND
mg/kg
0.012
0.0030
1
06/03/19 13:55
06/03/19 18:48
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:48
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:48
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0062
0.0044
1
06/03/19 13:55
06/03/19 18:48
96-12-8
Dibromochloromethane
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:48
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:48
106-93-4
Dibromomethane
ND
mg/kg
0.0062
0.0031
1
06/03/19 13:55
06/03/19 18:48
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:48
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0062
0.0025
1
06/03/19 13:55
06/03/19 18:48
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:48
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.012
0.0044
1
06/03/19 13:55
06/03/19 18:48
75-71-8
L1
1,1-Dichloroethane
ND
mg/kg
0.0062
0.0018
1
06/03/19 13:55
06/03/19 18:48
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0062
0.0027
1
06/03/19 13:55
06/03/19 18:48
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:48
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0062
0.0017
1
06/03/19 13:55
06/03/19 18:48
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:48
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:48
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0062
0.0023
1
06/03/19 13:55
06/03/19 18:48
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0062
0.0021
1
06/03/19 13:55
06/03/19 18:48
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0062
0.0018
1
06/03/19 13:55
06/03/19 18:48
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0062
0.0022
1
06/03/19 13:55
06/03/19 18:48
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall SW Lab ID: 92430462003 Collected: 05/22/19 14:02 Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
mg/kg
0.0062
0.0018
1
06/03/1913:55
06/03/1918:48
10061-02-6
ND
mg/kg
0.0062
0.0021
1
06/03/1913:55
06/03/1918:48
108-20-3
ND
mg/kg
0.0062
0.0022
1
06/03/1913:55
06/03/1918:48
100-41-4
ND
mg/kg
0.0062
0.0025
1
06/03/1913:55
06/03/1918:48
87-68-3
ND
mg/kg
0.062
0.0048
1
06/03/1913:55
06/03/1918:48
591-78-6
ND
mg/kg
0.0062
0.0023
1
06/03/1913:55
06/03/1918:48
98-82-8
ND
mg/kg
0.0062
0.0021
1
06/03/1913:55
06/03/1918:48
99-87-6
ND
mg/kg
0.025
0.0037
1
06/03/1913:55
06/03/1918:48
75-09-2
ND
mg/kg
0.062
0.0046
1
06/03/1913:55
06/03/1918:48
108-10-1
ND
mg/kg
0.0062
0.0018
1
06/03/1913:55
06/03/1918:48
1634-04-4
ND
mg/kg
0.0062
0.0015
1
06/03/1913:55
06/03/1918:48
91-20-3
ND
mg/kg
0.0062
0.0021
1
06/03/1913:55
06/03/1918:48
103-65-1
ND
mg/kg
0.0062
0.0022
1
06/03/1913:55
06/03/1918:48
100-42-5
ND
mg/kg
0.0062
0.0026
1
06/03/1913:55
06/03/1918:48
630-20-6
ND
mg/kg
0.0062
0.0023
1
06/03/1913:55
06/03/1918:48
79-34-5
ND
mg/kg
0.0062
0.0021
1
06/03/1913:55
06/03/1918:48
127-18-4
ND
mg/kg
0.0062
0.0022
1
06/03/1913:55
06/03/1918:48
108-88-3
ND
mg/kg
0.0062
0.0027
1
06/03/1913:55
06/03/1918:48
87-61-6
ND
mg/kg
0.0062
0.0020
1
06/03/1913:55
06/03/1918:48
120-82-1
ND
mg/kg
0.0062
0.0022
1
06/03/1913:55
06/03/1918:48
71-55-6
ND
mg/kg
0.0062
0.0026
1
06/03/1913:55
06/03/1918:48
79-00-5
ND
mg/kg
0.0062
0.0026
1
06/03/1913:55
06/03/1918:48
79-01-6
ND
mg/kg
0.0062
0.0027
1
06/03/1913:55
06/03/1918:48
75-69-4
ND
mg/kg
0.0062
0.0020
1
06/03/1913:55
06/03/1918:48
96-18-4
ND
mg/kg
0.0062
0.0025
1
06/03/1913:55
06/03/1918:48
95-63-6
ND
mg/kg
0.0062
0.0022
1
06/03/1913:55
06/03/1918:48
108-67-8
ND
mg/kg
0.062
0.011
1
06/03/1913:55
06/03/1918:48
108-05-4
ND
mg/kg
0.012
0.0022
1
06/03/1913:55
06/03/1918:48
75-01-4
ND
mg/kg
0.012
0.0044
1
06/03/1913:55
06/03/1918:48
1330-20-7
ND
mg/kg
0.012
0.0044
1
06/03/1913:55
06/03/1918:48
179601-23-1
ND
mg/kg
0.0062
0.0023
1
06/03/1913:55
06/03/1918:48
95-47-6
99
%
70-130
1
06/03/1913:55
06/03/1918:48
2037-26-5
103
%
70-130
1
06/03/1913:55
06/03/1918:48
460-00-4
97
%
70-132
1
06/03/1913:55
06/03/1918:48
17060-07-0
Analytical Method: ASTM D2974-87
23.3 % 0.10 0.10 1
REPORT OF LABORATORY ANALYSIS
05/23/19 17:44
L1
L1,v1
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall NW
Lab ID:
92430462004
Collected:
05/22/19
14:00
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND
mg/kg
4.4
4.4
1
05/24/19 09:21
05/24/19 13:28
N2
Aliphatic (C09-C12)
ND
mg/kg
4.4
4.4
1
05/24/19 09:21
05/24/19 13:28
N2
Aliphatic(C09-C12) Adjusted
ND
mg/kg
4.4
4.4
1
05/24/19 09:21
05/24/19 13:28
N2
Aromatic (C09-C10)
ND
mg/kg
4.4
4.4
1
05/24/19 09:21
05/24/19 13:28
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
97
%
70-130
1
05/24/19 09:21
05/24/19 13:28
460-00-4
4-Bromofluorobenzene (PID) (S)
97
%
70-130
1
05/24/19 09:21
05/24/19 13:28
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
ND
mg/kg
3.3
0.33
25
06/04/19 11:40
06/04/19 12:31
67-64-1
Benzene
ND
mg/kg
0.17
0.053
25
06/04/19 11:40
06/04/19 12:31
71-43-2
Bromobenzene
ND
mg/kg
0.17
0.066
25
06/04/19 11:40
06/04/19 12:31
108-86-1
Bromochloromethane
ND
mg/kg
0.17
0.056
25
06/04/19 11:40
06/04/19 12:31
74-97-5
Bromodichloromethane
ND
mg/kg
0.17
0.063
25
06/04/19 11:40
06/04/19 12:31
75-27-4
Bromoform
ND
mg/kg
0.17
0.076
25
06/04/19 11:40
06/04/19 12:31
75-25-2
Bromomethane
ND
mg/kg
0.33
0.083
25
06/04/19 11:40
06/04/19 12:31
74-83-9
2-Butanone (MEK)
ND
mg/kg
3.3
0.096
25
06/04/19 11:40
06/04/19 12:31
78-93-3
n-Butylbenzene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:31
104-51-8
sec-Butylbenzene
ND
mg/kg
0.17
0.053
25
06/04/19 11:40
06/04/19 12:31
135-98-8
tert-Butyl benzene
ND
mg/kg
0.17
0.066
25
06/04/19 11:40
06/04/19 12:31
98-06-6
Carbon tetrachloride
ND
mg/kg
0.17
0.086
25
06/04/19 11:40
06/04/19 12:31
56-23-5
Chlorobenzene
ND
mg/kg
0.17
0.063
25
06/04/19 11:40
06/04/19 12:31
108-90-7
Chloroethane
ND
mg/kg
0.33
0.079
25
06/04/19 11:40
06/04/19 12:31
75-00-3
Chloroform
ND
mg/kg
0.17
0.053
25
06/04/19 11:40
06/04/19 12:31
67-66-3
Chloromethane
ND
mg/kg
0.33
0.079
25
06/04/19 11:40
06/04/19 12:31
74-87-3
2-Chlorotoluene
ND
mg/kg
0.17
0.056
25
06/04/19 11:40
06/04/19 12:31
95-49-8
4-Chlorotoluene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:31
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.17
0.12
25
06/04/19 11:40
06/04/19 12:31
96-12-8
Dibromochloromethane
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:31
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:31
106-93-4
Dibromomethane
ND
mg/kg
0.17
0.083
25
06/04/19 11:40
06/04/19 12:31
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.17
0.063
25
06/04/19 11:40
06/04/19 12:31
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.17
0.066
25
06/04/19 11:40
06/04/19 12:31
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.17
0.056
25
06/04/19 11:40
06/04/19 12:31
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.33
0.12
25
06/04/19 11:40
06/04/19 12:31
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.17
0.050
25
06/04/19 11:40
06/04/19 12:31
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.17
0.073
25
06/04/19 11:40
06/04/19 12:31
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:31
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.17
0.046
25
06/04/19 11:40
06/04/19 12:31
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.17
0.063
25
06/04/19 11:40
06/04/19 12:31
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.17
0.056
25
06/04/19 11:40
06/04/19 12:31
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.17
0.063
25
06/04/19 11:40
06/04/19 12:31
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.17
0.056
25
06/04/19 11:40
06/04/19 12:31
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.17
0.050
25
06/04/19 11:40
06/04/19 12:31
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:31
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Sidewall NW Lab ID: 92430462004 Collected: 05/22/19 14:00 Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
mg/kg
0.17
0.050
25
06/04/1911:40
06/04/1912:31
10061-02-6
ND
mg/kg
0.17
0.056
25
06/04/1911:40
06/04/1912:31
108-20-3
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:31
100-41-4
ND
mg/kg
0.17
0.066
25
06/04/1911:40
06/04/1912:31
87-68-3
ND
mg/kg
1.7
0.13
25
06/04/1911:40
06/04/1912:31
591-78-6
ND
mg/kg
0.17
0.063
25
06/04/1911:40
06/04/1912:31
98-82-8
ND
mg/kg
0.17
0.056
25
06/04/1911:40
06/04/1912:31
99-87-6
ND
mg/kg
0.66
0.099
25
06/04/1911:40
06/04/1912:31
75-09-2
ND
mg/kg
1.7
0.12
25
06/04/1911:40
06/04/1912:31
108-10-1
ND
mg/kg
0.17
0.050
25
06/04/1911:40
06/04/1912:31
1634-04-4
0.041J
mg/kg
0.17
0.040
25
06/04/1911:40
06/04/1912:31
91-20-3
ND
mg/kg
0.17
0.056
25
06/04/1911:40
06/04/1912:31
103-65-1
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:31
100-42-5
ND
mg/kg
0.17
0.069
25
06/04/1911:40
06/04/1912:31
630-20-6
ND
mg/kg
0.17
0.063
25
06/04/1911:40
06/04/1912:31
79-34-5
ND
mg/kg
0.17
0.056
25
06/04/1911:40
06/04/1912:31
127-18-4
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:31
108-88-3
ND
mg/kg
0.17
0.073
25
06/04/1911:40
06/04/1912:31
87-61-6
ND
mg/kg
0.17
0.053
25
06/04/1911:40
06/04/1912:31
120-82-1
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:31
71-55-6
ND
mg/kg
0.17
0.069
25
06/04/1911:40
06/04/1912:31
79-00-5
ND
mg/kg
0.17
0.069
25
06/04/1911:40
06/04/1912:31
79-01-6
ND
mg/kg
0.17
0.073
25
06/04/1911:40
06/04/1912:31
75-69-4
ND
mg/kg
0.17
0.053
25
06/04/1911:40
06/04/1912:31
96-18-4
0.069J
mg/kg
0.17
0.066
25
06/04/1911:40
06/04/1912:31
95-63-6
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:31
108-67-8
ND
mg/kg
1.7
0.29
25
06/04/1911:40
06/04/1912:31
108-05-4
ND
mg/kg
0.33
0.060
25
06/04/1911:40
06/04/1912:31
75-01-4
ND
mg/kg
0.33
0.12
25
06/04/1911:40
06/04/1912:31
1330-20-7
ND
mg/kg
0.33
0.12
25
06/04/1911:40
06/04/1912:31
179601-23-1
ND
mg/kg
0.17
0.063
25
06/04/1911:40
06/04/1912:31
95-47-6
106 % 70-130
103 % 70-130
97 % 70-132
Analytical Method: ASTM D2974-87
25 06/04/1911:40 06/04/1912:31
25 06/04/1911:40 06/04/1912:31
25 06/04/1911:40 06/04/1912:31
24.9 % 0.10 0.10 1
REPORT OF LABORATORY ANALYSIS
05/23/19 17:44
2037-26-5 P2
460-00-4
17060-07-0
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Base
Lab ID:
92430462005
Collected:
05/22/19
14:15
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
205
mg/kg
7.2
7.2
2
05/24/19 09:21
05/26/19 15:41
N2
Aliphatic (C09-C12)
789
mg/kg
7.2
7.2
2
05/24/19 09:21
05/26/19 15:41
N2
Aliphatic(C09-C12) Adjusted
366
mg/kg
7.2
7.2
2
05/24/19 09:21
05/26/19 15:41
N2
Aromatic (C09-C10)
423
mg/kg
7.2
7.2
2
05/24/19 09:21
05/26/19 15:41
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
178
%
70-130
2
05/24/19 09:21
05/26/19 15:41
460-00-4
S2
4-Bromofluorobenzene (PID) (S)
114
%
70-130
2
05/24/19 09:21
05/26/19 15:41
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
ND
mg/kg
3.3
0.33
25
06/04/19 11:40
06/04/19 12:55
67-64-1
Benzene
ND
mg/kg
0.17
0.054
25
06/04/19 11:40
06/04/19 12:55
71-43-2
Bromobenzene
ND
mg/kg
0.17
0.067
25
06/04/19 11:40
06/04/19 12:55
108-86-1
Bromochloromethane
ND
mg/kg
0.17
0.057
25
06/04/19 11:40
06/04/19 12:55
74-97-5
Bromodichloromethane
ND
mg/kg
0.17
0.064
25
06/04/19 11:40
06/04/19 12:55
75-27-4
Bromoform
ND
mg/kg
0.17
0.077
25
06/04/19 11:40
06/04/19 12:55
75-25-2
Bromomethane
ND
mg/kg
0.33
0.084
25
06/04/19 11:40
06/04/19 12:55
74-83-9
2-Butanone (MEK)
ND
mg/kg
3.3
0.097
25
06/04/19 11:40
06/04/19 12:55
78-93-3
n-Butylbenzene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:55
104-51-8
sec-Butylbenzene
ND
mg/kg
0.17
0.054
25
06/04/19 11:40
06/04/19 12:55
135-98-8
tert-Butyl benzene
ND
mg/kg
0.17
0.067
25
06/04/19 11:40
06/04/19 12:55
98-06-6
Carbon tetrachloride
ND
mg/kg
0.17
0.087
25
06/04/19 11:40
06/04/19 12:55
56-23-5
Chlorobenzene
ND
mg/kg
0.17
0.064
25
06/04/19 11:40
06/04/19 12:55
108-90-7
Chloroethane
ND
mg/kg
0.33
0.080
25
06/04/19 11:40
06/04/19 12:55
75-00-3
Chloroform
ND
mg/kg
0.17
0.054
25
06/04/19 11:40
06/04/19 12:55
67-66-3
Chloromethane
ND
mg/kg
0.33
0.080
25
06/04/19 11:40
06/04/19 12:55
74-87-3
2-Chlorotoluene
ND
mg/kg
0.17
0.057
25
06/04/19 11:40
06/04/19 12:55
95-49-8
4-Chlorotoluene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:55
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.17
0.12
25
06/04/19 11:40
06/04/19 12:55
96-12-8
Dibromochloromethane
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:55
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:55
106-93-4
Dibromomethane
ND
mg/kg
0.17
0.084
25
06/04/19 11:40
06/04/19 12:55
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.17
0.064
25
06/04/19 11:40
06/04/19 12:55
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.17
0.067
25
06/04/19 11:40
06/04/19 12:55
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.17
0.057
25
06/04/19 11:40
06/04/19 12:55
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.33
0.12
25
06/04/19 11:40
06/04/19 12:55
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.17
0.050
25
06/04/19 11:40
06/04/19 12:55
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.17
0.074
25
06/04/19 11:40
06/04/19 12:55
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:55
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.17
0.047
25
06/04/19 11:40
06/04/19 12:55
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.17
0.064
25
06/04/19 11:40
06/04/19 12:55
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.17
0.057
25
06/04/19 11:40
06/04/19 12:55
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.17
0.064
25
06/04/19 11:40
06/04/19 12:55
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.17
0.057
25
06/04/19 11:40
06/04/19 12:55
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.17
0.050
25
06/04/19 11:40
06/04/19 12:55
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.17
0.060
25
06/04/19 11:40
06/04/19 12:55
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: Base Lab ID: 92430462005 Collected: 05/22/19 14:15 Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
mg/kg
0.17
0.050
25
06/04/1911:40
06/04/1912:55
10061-02-6
ND
mg/kg
0.17
0.057
25
06/04/1911:40
06/04/1912:55
108-20-3
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:55
100-41-4
ND
mg/kg
0.17
0.067
25
06/04/1911:40
06/04/1912:55
87-68-3
ND
mg/kg
1.7
0.13
25
06/04/1911:40
06/04/1912:55
591-78-6
ND
mg/kg
0.17
0.064
25
06/04/1911:40
06/04/1912:55
98-82-8
ND
mg/kg
0.17
0.057
25
06/04/1911:40
06/04/1912:55
99-87-6
ND
mg/kg
0.67
0.10
25
06/04/1911:40
06/04/1912:55
75-09-2
ND
mg/kg
1.7
0.12
25
06/04/1911:40
06/04/1912:55
108-10-1
ND
mg/kg
0.17
0.050
25
06/04/1911:40
06/04/1912:55
1634-04-4
ND
mg/kg
0.17
0.040
25
06/04/1911:40
06/04/1912:55
91-20-3
ND
mg/kg
0.17
0.057
25
06/04/1911:40
06/04/1912:55
103-65-1
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:55
100-42-5
ND
mg/kg
0.17
0.070
25
06/04/1911:40
06/04/1912:55
630-20-6
ND
mg/kg
0.17
0.064
25
06/04/1911:40
06/04/1912:55
79-34-5
ND
mg/kg
0.17
0.057
25
06/04/1911:40
06/04/1912:55
127-18-4
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:55
108-88-3
ND
mg/kg
0.17
0.074
25
06/04/1911:40
06/04/1912:55
87-61-6
ND
mg/kg
0.17
0.054
25
06/04/1911:40
06/04/1912:55
120-82-1
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:55
71-55-6
ND
mg/kg
0.17
0.070
25
06/04/1911:40
06/04/1912:55
79-00-5
ND
mg/kg
0.17
0.070
25
06/04/1911:40
06/04/1912:55
79-01-6
ND
mg/kg
0.17
0.074
25
06/04/1911:40
06/04/1912:55
75-69-4
ND
mg/kg
0.17
0.054
25
06/04/1911:40
06/04/1912:55
96-18-4
ND
mg/kg
0.17
0.067
25
06/04/1911:40
06/04/1912:55
95-63-6
ND
mg/kg
0.17
0.060
25
06/04/1911:40
06/04/1912:55
108-67-8
ND
mg/kg
1.7
0.29
25
06/04/1911:40
06/04/1912:55
108-05-4
ND
mg/kg
0.33
0.060
25
06/04/1911:40
06/04/1912:55
75-01-4
ND
mg/kg
0.33
0.12
25
06/04/1911:40
06/04/1912:55
1330-20-7
ND
mg/kg
0.33
0.12
25
06/04/1911:40
06/04/1912:55
179601-23-1
ND
mg/kg
0.17
0.064
25
06/04/1911:40
06/04/1912:55
95-47-6
107
%
70-130
25
06/04/1911:40
06/04/1912:55
2037-26-5 P2
101
%
70-130
25
06/04/1911:40
06/04/1912:55
460-00-4
96
%
70-132
25
06/04/1911:40
06/04/1912:55
17060-07-0
Analytical Method: ASTM D2974-87
23.9 % 0.10 0.10 1
REPORT OF LABORATORY ANALYSIS
05/23/19 17:44
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Sidewall SE
Lab ID:
92430462006
Collected:
05/22/19
13:37
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND
mg/kg
3.3
3.3
1
05/24/19 09:21
05/24/19 13:58
N2
Aliphatic (C09-C12)
ND
mg/kg
3.3
3.3
1
05/24/19 09:21
05/24/19 13:58
N2
Aliphatic(C09-C12) Adjusted
ND
mg/kg
3.3
3.3
1
05/24/19 09:21
05/24/19 13:58
N2
Aromatic (C09-C10)
ND
mg/kg
3.3
3.3
1
05/24/19 09:21
05/24/19 13:58
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
94
%
70-130
1
05/24/19 09:21
05/24/19 13:58
460-00-4
4-Bromofluorobenzene (PID) (S)
93
%
70-130
1
05/24/19 09:21
05/24/19 13:58
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
0.16
mg/kg
0.11
0.011
1
06/03/19 13:55
06/03/19 19:13
67-64-1
Benzene
ND
mg/kg
0.0054
0.0017
1
06/03/19 13:55
06/03/19 19:13
71-43-2
Bromobenzene
ND
mg/kg
0.0054
0.0022
1
06/03/19 13:55
06/03/19 19:13
108-86-1
Bromochloromethane
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
74-97-5
Bromodichloromethane
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
75-27-4
Bromoform
ND
mg/kg
0.0054
0.0025
1
06/03/19 13:55
06/03/19 19:13
75-25-2
Bromomethane
ND
mg/kg
0.011
0.0027
1
06/03/19 13:55
06/03/19 19:13
74-83-9
2-Butanone (MEK)
0.021J
mg/kg
0.11
0.0031
1
06/03/19 13:55
06/03/19 19:13
78-93-3
n-Butylbenzene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0054
0.0017
1
06/03/19 13:55
06/03/19 19:13
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0054
0.0022
1
06/03/19 13:55
06/03/19 19:13
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0054
0.0028
1
06/03/19 13:55
06/03/19 19:13
56-23-5
Chlorobenzene
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
108-90-7
Chloroethane
ND
mg/kg
0.011
0.0026
1
06/03/19 13:55
06/03/19 19:13
75-00-3
Chloroform
ND
mg/kg
0.0054
0.0017
1
06/03/19 13:55
06/03/19 19:13
67-66-3
Chloromethane
ND
mg/kg
0.011
0.0026
1
06/03/19 13:55
06/03/19 19:13
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0054
0.0039
1
06/03/19 13:55
06/03/19 19:13
96-12-8
Dibromochloromethane
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
106-93-4
Dibromomethane
ND
mg/kg
0.0054
0.0027
1
06/03/19 13:55
06/03/19 19:13
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0054
0.0022
1
06/03/19 13:55
06/03/19 19:13
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.011
0.0039
1
06/03/19 13:55
06/03/19 19:13
75-71-8
L1
1,1-Dichloroethane
ND
mg/kg
0.0054
0.0016
1
06/03/19 13:55
06/03/19 19:13
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0054
0.0024
1
06/03/19 13:55
06/03/19 19:13
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0054
0.0015
1
06/03/19 13:55
06/03/19 19:13
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0054
0.0016
1
06/03/19 13:55
06/03/19 19:13
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Sidewall SE Lab ID: 92430462006 Collected: 05/22/19 13:37 Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
trans- 1,3-Dichloropropene
ND
mg/kg
0.0054
0.0016
1
06/03/19 13:55
06/03/19 19:13
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
108-20-3
Ethylbenzene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0054
0.0022
1
06/03/19 13:55
06/03/19 19:13
87-68-3
2-Hexanone
ND
mg/kg
0.054
0.0042
1
06/03/19 13:55
06/03/19 19:13
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
99-87-6
Methylene Chloride
ND
mg/kg
0.022
0.0033
1
06/03/19 13:55
06/03/19 19:13
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.054
0.0040
1
06/03/19 13:55
06/03/19 19:13
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0054
0.0016
1
06/03/19 13:55
06/03/19 19:13
1634-04-4
Naphthalene
0.0071
mg/kg
0.0054
0.0013
1
06/03/19 13:55
06/03/19 19:13
91-20-3
n-Propylbenzene
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
103-65-1
Styrene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0054
0.0023
1
06/03/19 13:55
06/03/19 19:13
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
79-34-5
Tetrachloroethene
ND
mg/kg
0.0054
0.0018
1
06/03/19 13:55
06/03/19 19:13
127-18-4
Toluene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0054
0.0024
1
06/03/19 13:55
06/03/19 19:13
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0054
0.0017
1
06/03/19 13:55
06/03/19 19:13
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0054
0.0023
1
06/03/19 13:55
06/03/19 19:13
79-00-5
Trichloroethene
ND
mg/kg
0.0054
0.0023
1
06/03/19 13:55
06/03/19 19:13
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0054
0.0024
1
06/03/19 13:55
06/03/19 19:13
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0054
0.0017
1
06/03/19 13:55
06/03/19 19:13
96-18-4
1,2,4-Trimethylbenzene
0.0034J
mg/kg
0.0054
0.0022
1
06/03/19 13:55
06/03/19 19:13
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0054
0.0020
1
06/03/19 13:55
06/03/19 19:13
108-67-8
Vinyl acetate
ND
mg/kg
0.054
0.0095
1
06/03/19 13:55
06/03/19 19:13
108-05-4
Vinyl chloride
ND
mg/kg
0.011
0.0020
1
06/03/19 13:55
06/03/19 19:13
75-01-4
Xylene (Total)
ND
mg/kg
0.011
0.0039
1
06/03/19 13:55
06/03/19 19:13
1330-20-7
m&p-Xylene
ND
mg/kg
0.011
0.0039
1
06/03/19 13:55
06/03/19 19:13
179601-23-1
o-Xylene
ND
mg/kg
0.0054
0.0021
1
06/03/19 13:55
06/03/19 19:13
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
1
06/03/19 13:55
06/03/19 19:13
2037-26-5
4-Bromofluorobenzene (S)
101
%
70-130
1
06/03/19 13:55
06/03/19 19:13
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-132
1
06/03/19 13:55
06/03/19 19:13
17060-07-0
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
21.2
%
0.10
0.10
1
05/24/19 13:34
REPORT OF LABORATORY ANALYSIS
L1
L1,v1
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Sidewall NE
Lab ID:
92430462007
Collected:
05/22/19
13:38
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
5.5
mg/kg
2.7
2.7
1
05/24/19 09:21
05/24/19 14:27
N2
Aliphatic (C09-C12)
22.6
mg/kg
2.7
2.7
1
05/24/19 09:21
05/24/19 14:27
N2
Aliphatic(C09-C12) Adjusted
14.9
mg/kg
2.7
2.7
1
05/24/19 09:21
05/24/19 14:27
N2
Aromatic (C09-C10)
7.7
mg/kg
2.7
2.7
1
05/24/19 09:21
05/24/19 14:27
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
125
%
70-130
1
05/24/19 09:21
05/24/19 14:27
460-00-4
4-Bromofluorobenzene (PID) (S)
94
%
70-130
1
05/24/19 09:21
05/24/19 14:27
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
0.12
mg/kg
0.086
0.0086
1
06/03/19 13:55
06/03/19 19:38
67-64-1
Benzene
0.0035J
mg/kg
0.0043
0.0014
1
06/03/19 13:55
06/03/19 19:38
71-43-2
Bromobenzene
ND
mg/kg
0.0043
0.0017
1
06/03/19 13:55
06/03/19 19:38
108-86-1
Bromochloromethane
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
74-97-5
Bromodichloromethane
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
75-27-4
Bromoform
ND
mg/kg
0.0043
0.0020
1
06/03/19 13:55
06/03/19 19:38
75-25-2
Bromomethane
ND
mg/kg
0.0086
0.0022
1
06/03/19 13:55
06/03/19 19:38
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.086
0.0025
1
06/03/19 13:55
06/03/19 19:38
78-93-3
n-Butylbenzene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
104-51-8
sec-Butylbenzene
0.0058
mg/kg
0.0043
0.0014
1
06/03/19 13:55
06/03/19 19:38
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0043
0.0017
1
06/03/19 13:55
06/03/19 19:38
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0043
0.0022
1
06/03/19 13:55
06/03/19 19:38
56-23-5
Chlorobenzene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
108-90-7
Chloroethane
ND
mg/kg
0.0086
0.0021
1
06/03/19 13:55
06/03/19 19:38
75-00-3
Chloroform
ND
mg/kg
0.0043
0.0014
1
06/03/19 13:55
06/03/19 19:38
67-66-3
Chloromethane
ND
mg/kg
0.0086
0.0021
1
06/03/19 13:55
06/03/19 19:38
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0043
0.0031
1
06/03/19 13:55
06/03/19 19:38
96-12-8
Dibromochloromethane
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
106-93-4
Dibromomethane
ND
mg/kg
0.0043
0.0022
1
06/03/19 13:55
06/03/19 19:38
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0043
0.0017
1
06/03/19 13:55
06/03/19 19:38
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.0086
0.0031
1
06/03/19 13:55
06/03/19 19:38
75-71-8
L1
1,1-Dichloroethane
ND
mg/kg
0.0043
0.0013
1
06/03/19 13:55
06/03/19 19:38
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0043
0.0019
1
06/03/19 13:55
06/03/19 19:38
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0043
0.0012
1
06/03/19 13:55
06/03/19 19:38
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0043
0.0013
1
06/03/19 13:55
06/03/19 19:38
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Sidewall NE Lab ID: 92430462007 Collected: 05/22/19 13:38 Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
trans- 1,3-Dichloropropene
ND
mg/kg
0.0043
0.0013
1
06/03/19 13:55
06/03/19 19:38
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
108-20-3
Ethylbenzene
0.0090
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0043
0.0017
1
06/03/19 13:55
06/03/19 19:38
87-68-3
2-Hexanone
ND
mg/kg
0.043
0.0034
1
06/03/19 13:55
06/03/19 19:38
591-78-6
Isopropylbenzene (Cumene)
0.0043J
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
99-87-6
Methylene Chloride
ND
mg/kg
0.017
0.0026
1
06/03/19 13:55
06/03/19 19:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.043
0.0032
1
06/03/19 13:55
06/03/19 19:38
108-10-1
Methyl-tert-butyl ether
0.0021J
mg/kg
0.0043
0.0013
1
06/03/19 13:55
06/03/19 19:38
1634-04-4
Naphthalene
ND
mg/kg
0.0043
0.0010
1
06/03/19 13:55
06/03/19 19:38
91-20-3
n-Propylbenzene
0.018
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
103-65-1
Styrene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0043
0.0018
1
06/03/19 13:55
06/03/19 19:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
79-34-5
Tetrachloroethene
ND
mg/kg
0.0043
0.0015
1
06/03/19 13:55
06/03/19 19:38
127-18-4
Toluene
0.0041J
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0043
0.0019
1
06/03/19 13:55
06/03/19 19:38
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0043
0.0014
1
06/03/19 13:55
06/03/19 19:38
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0043
0.0018
1
06/03/19 13:55
06/03/19 19:38
79-00-5
Trichloroethene
ND
mg/kg
0.0043
0.0018
1
06/03/19 13:55
06/03/19 19:38
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0043
0.0019
1
06/03/19 13:55
06/03/19 19:38
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0043
0.0014
1
06/03/19 13:55
06/03/19 19:38
96-18-4
1,2,4-Trimethylbenzene
0.0054
mg/kg
0.0043
0.0017
1
06/03/19 13:55
06/03/19 19:38
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
108-67-8
Vinyl acetate
ND
mg/kg
0.043
0.0076
1
06/03/19 13:55
06/03/19 19:38
108-05-4
Vinyl chloride
ND
mg/kg
0.0086
0.0016
1
06/03/19 13:55
06/03/19 19:38
75-01-4
Xylene (Total)
ND
mg/kg
0.0086
0.0031
1
06/03/19 13:55
06/03/19 19:38
1330-20-7
m&p-Xylene
0.0051J
mg/kg
0.0086
0.0031
1
06/03/19 13:55
06/03/19 19:38
179601-23-1
o-Xylene
0.0033J
mg/kg
0.0043
0.0016
1
06/03/19 13:55
06/03/19 19:38
95-47-6
Surrogates
Toluene-d8 (S)
98
%
70-130
1
06/03/19 13:55
06/03/19 19:38
2037-26-5
4-Bromofluorobenzene (S)
104
%
70-130
1
06/03/19 13:55
06/03/19 19:38
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-132
1
06/03/19 13:55
06/03/19 19:38
17060-07-0
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
18.1
%
0.10
0.10
1
05/24/19 13:34
REPORT OF LABORATORY ANALYSIS
L1
L1,v1
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Sidewall NW
Lab ID:
92430462008
Collected:
05/22/19
13:40
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
9.9
mg/kg
3.0
3.0
1
05/24/19 09:21
05/24/19 14:57
N2
Aliphatic (C09-C12)
5.9
mg/kg
3.0
3.0
1
05/24/19 09:21
05/24/19 14:57
N2
Aliphatic(C09-C12) Adjusted
4.1
mg/kg
3.0
3.0
1
05/24/19 09:21
05/24/19 14:57
N2
Aromatic (C09-C10)
ND
mg/kg
3.0
3.0
1
05/24/19 09:21
05/24/19 14:57
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
106
%
70-130
1
05/24/19 09:21
05/24/19 14:57
460-00-4
4-Bromofluorobenzene (PID) (S)
90
%
70-130
1
05/24/19 09:21
05/24/19 14:57
460-00-4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
0.16
mg/kg
0.098
0.0098
1
06/04/19 10:15
06/04/19 13:00
67-64-1
Benzene
0.0036J
mg/kg
0.0049
0.0016
1
06/04/19 10:15
06/04/19 13:00
71-43-2
Bromobenzene
ND
mg/kg
0.0049
0.0020
1
06/04/19 10:15
06/04/19 13:00
108-86-1
Bromochloromethane
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
74-97-5
Bromodichloromethane
ND
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
75-27-4
Bromoform
ND
mg/kg
0.0049
0.0023
1
06/04/19 10:15
06/04/19 13:00
75-25-2
Bromomethane
ND
mg/kg
0.0098
0.0024
1
06/04/19 10:15
06/04/19 13:00
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.098
0.0028
1
06/04/19 10:15
06/04/19 13:00
78-93-3
n-Butylbenzene
0.0056
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
104-51-8
sec-Butylbenzene
ND
mg/kg
0.0049
0.0016
1
06/04/19 10:15
06/04/19 13:00
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0049
0.0020
1
06/04/19 10:15
06/04/19 13:00
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0049
0.0025
1
06/04/19 10:15
06/04/19 13:00
56-23-5
Chlorobenzene
ND
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
108-90-7
Chloroethane
ND
mg/kg
0.0098
0.0023
1
06/04/19 10:15
06/04/19 13:00
75-00-3
Chloroform
ND
mg/kg
0.0049
0.0016
1
06/04/19 10:15
06/04/19 13:00
67-66-3
Chloromethane
ND
mg/kg
0.0098
0.0023
1
06/04/19 10:15
06/04/19 13:00
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0049
0.0035
1
06/04/19 10:15
06/04/19 13:00
96-12-8
Dibromochloromethane
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
106-93-4
Dibromomethane
ND
mg/kg
0.0049
0.0024
1
06/04/19 10:15
06/04/19 13:00
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0049
0.0020
1
06/04/19 10:15
06/04/19 13:00
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.0098
0.0035
1
06/04/19 10:15
06/04/19 13:00
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0049
0.0015
1
06/04/19 10:15
06/04/19 13:00
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.0049
0.0022
1
06/04/19 10:15
06/04/19 13:00
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0049
0.0014
1
06/04/19 10:15
06/04/19 13:00
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0049
0.0015
1
06/04/19 10:15
06/04/19 13:00
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Sidewall NW
Lab ID:
92430462008
Collected:
05/22/19 13:40
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D
Preparation Method: EPA 5035A
trans- 1,3-Dichloropropene
ND
mg/kg
0.0049
0.0015
1
06/04/19 10:15
06/04/19 13:00
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
108-20-3
Ethylbenzene
0.0047J
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0049
0.0020
1
06/04/19 10:15
06/04/19 13:00
87-68-3
2-Hexanone
ND
mg/kg
0.049
0.0038
1
06/04/19 10:15
06/04/19 13:00
591-78-6
Isopropylbenzene (Cumene)
ND
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
99-87-6
Methylene Chloride
ND
mg/kg
0.020
0.0029
1
06/04/19 10:15
06/04/19 13:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
mg/kg
0.049
0.0036
1
06/04/19 10:15
06/04/19 13:00
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0049
0.0015
1
06/04/19 10:15
06/04/19 13:00
1634-04-4
Naphthalene
0.057
mg/kg
0.0049
0.0012
1
06/04/19 10:15
06/04/19 13:00
91-20-3
n-Propylbenzene
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
103-65-1
Styrene
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0049
0.0021
1
06/04/19 10:15
06/04/19 13:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
79-34-5
Tetrachloroethene
ND
mg/kg
0.0049
0.0017
1
06/04/19 10:15
06/04/19 13:00
127-18-4
Toluene
0.023
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0049
0.0022
1
06/04/19 10:15
06/04/19 13:00
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0049
0.0016
1
06/04/19 10:15
06/04/19 13:00
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0049
0.0021
1
06/04/19 10:15
06/04/19 13:00
79-00-5
Trichloroethene
ND
mg/kg
0.0049
0.0021
1
06/04/19 10:15
06/04/19 13:00
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0049
0.0022
1
06/04/19 10:15
06/04/19 13:00
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.0049
0.0016
1
06/04/19 10:15
06/04/19 13:00
96-18-4
1,2,4-Trimethylbenzene
0.050
mg/kg
0.0049
0.0020
1
06/04/19 10:15
06/04/19 13:00
95-63-6
1,3,5-Trimethylbenzene
ND
mg/kg
0.0049
0.0018
1
06/04/19 10:15
06/04/19 13:00
108-67-8
Vinyl acetate
ND
mg/kg
0.049
0.0086
1
06/04/19 10:15
06/04/19 13:00
108-05-4 v1
Vinyl chloride
ND
mg/kg
0.0098
0.0018
1
06/04/19 10:15
06/04/19 13:00
75-01-4
Xylene (Total)
0.020
mg/kg
0.0098
0.0035
1
06/04/19 10:15
06/04/19 13:00
1330-20-7
m&p-Xylene
0.014
mg/kg
0.0098
0.0035
1
06/04/19 10:15
06/04/19 13:00
179601-23-1
o-Xylene
0.0055
mg/kg
0.0049
0.0019
1
06/04/19 10:15
06/04/19 13:00
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
06/04/19 10:15
06/04/19 13:00
2037-26-5
4-Bromofluorobenzene (S)
101
%
70-130
1
06/04/19 10:15
06/04/19 13:00
460-00-4
1,2-Dichloroethane-d4 (S)
108
%
70-132
1
06/04/19 10:15
06/04/19 13:00
17060-07-0
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
18.2
%
0.10
0.10
1
05/24/19 13:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Base
Lab ID:
92430462009
Collected:
05/22/19 00:00
Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL DF
Prepared
Analyzed CAS No.
Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
393
mg/kg
12.6
12.6 4
05/24/19 09:21
05/26/19 15:11
N2
Aliphatic (C09-C12)
1550
mg/kg
12.6
12.6 4
05/24/19 09:21
05/26/19 15:11
N2
Aliphatic(C09-C12) Adjusted
752
mg/kg
12.6
12.6 4
05/24/19 09:21
05/26/19 15:11
N2
Aromatic (C09-C10)
800
mg/kg
12.6
12.6 4
05/24/19 09:21
05/26/19 15:11
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
232
%
70-130
4
05/24/19 09:21
05/26/19 15:11 460-00-4
S2
4-Bromofluorobenzene (PID) (S)
135
%
70-130
4
05/24/19 09:21
05/26/19 15:11 460-00-4
S2
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Acetone
ND
mg/kg
4.9
0.49
50
06/04/19 11:40
06/04/19 13:20
67-64-1
Benzene
ND
mg/kg
0.25
0.079
50
06/04/19 11:40
06/04/19 13:20
71-43-2
Bromobenzene
ND
mg/kg
0.25
0.098
50
06/04/19 11:40
06/04/19 13:20
108-86-1
Bromochloromethane
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
74-97-5
Bromodichloromethane
ND
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
75-27-4
Bromoform
ND
mg/kg
0.25
0.11
50
06/04/19 11:40
06/04/19 13:20
75-25-2
Bromomethane
ND
mg/kg
0.49
0.12
50
06/04/19 11:40
06/04/19 13:20
74-83-9
2-Butanone (MEK)
ND
mg/kg
4.9
0.14
50
06/04/19 11:40
06/04/19 13:20
78-93-3
n-Butylbenzene
9.8
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
104-51-8
sec-Butylbenzene
ND
mg/kg
0.25
0.079
50
06/04/19 11:40
06/04/19 13:20
135-98-8
tert-Butyl benzene
ND
mg/kg
0.25
0.098
50
06/04/19 11:40
06/04/19 13:20
98-06-6
Carbon tetrachloride
ND
mg/kg
0.25
0.13
50
06/04/19 11:40
06/04/19 13:20
56-23-5
Chlorobenzene
ND
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
108-90-7
Chloroethane
ND
mg/kg
0.49
0.12
50
06/04/19 11:40
06/04/19 13:20
75-00-3
Chloroform
ND
mg/kg
0.25
0.079
50
06/04/19 11:40
06/04/19 13:20
67-66-3
Chloromethane
ND
mg/kg
0.49
0.12
50
06/04/19 11:40
06/04/19 13:20
74-87-3
2-Chlorotoluene
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
95-49-8
4-Chlorotoluene
ND
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.25
0.18
50
06/04/19 11:40
06/04/19 13:20
96-12-8
Dibromochloromethane
ND
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
106-93-4
Dibromomethane
ND
mg/kg
0.25
0.12
50
06/04/19 11:40
06/04/19 13:20
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.25
0.098
50
06/04/19 11:40
06/04/19 13:20
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.49
0.18
50
06/04/19 11:40
06/04/19 13:20
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.25
0.074
50
06/04/19 11:40
06/04/19 13:20
75-34-3
1,2-Dichloroethane
ND
mg/kg
0.25
0.11
50
06/04/19 11:40
06/04/19 13:20
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.25
0.069
50
06/04/19 11:40
06/04/19 13:20
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.25
0.074
50
06/04/19 11:40
06/04/19 13:20
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Circle K 2708383
Pace Project No.: 92430462
Sample: L Base Lab ID: 92430462009 Collected: 05/22/19 00:00 Received: 05/23/19 13:41 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
trans- 1,3-Dichloropropene
ND
mg/kg
0.25
0.074
50
06/04/19 11:40
06/04/19 13:20
10061-02-6
Diisopropyl ether
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
108-20-3
Ethylbenzene
9.1
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.25
0.098
50
06/04/19 11:40
06/04/19 13:20
87-68-3
2-Hexanone
ND
mg/kg
2.5
0.19
50
06/04/19 11:40
06/04/19 13:20
591-78-6
Isopropylbenzene (Cumene)
3.7
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
98-82-8
p-Isopropyltoluene
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
99-87-6
Methylene Chloride
ND
mg/kg
0.98
0.15
50
06/04/19 11:40
06/04/19 13:20
75-09-2
4-Methyl-2-pentanone (MIBK)
6.1
mg/kg
2.5
0.18
50
06/04/19 11:40
06/04/19 13:20
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.25
0.074
50
06/04/19 11:40
06/04/19 13:20
1634-04-4
Naphthalene
16.2
mg/kg
4.9
1.2
1000
06/04/19 11:40
06/04/1916:34
91-20-3
n-Propylbenzene
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
103-65-1
Styrene
ND
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.25
0.10
50
06/04/19 11:40
06/04/19 13:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
79-34-5
Tetrachloroethene
ND
mg/kg
0.25
0.083
50
06/04/19 11:40
06/04/19 13:20
127-18-4
Toluene
0.37
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.25
0.11
50
06/04/19 11:40
06/04/19 13:20
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.25
0.079
50
06/04/19 11:40
06/04/19 13:20
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.25
0.088
50
06/04/19 11:40
06/04/19 13:20
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.25
0.10
50
06/04/19 11:40
06/04/19 13:20
79-00-5
Trichloroethene
ND
mg/kg
0.25
0.10
50
06/04/19 11:40
06/04/19 13:20
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.25
0.11
50
06/04/19 11:40
06/04/19 13:20
75-69-4
1,2,3-Trichloropropane
ND
mg/kg
0.25
0.079
50
06/04/19 11:40
06/04/19 13:20
96-18-4
1,2,4-Trimethylbenzene
75.5
mg/kg
4.9
2.0
1000
06/04/19 11:40
06/04/1916:34
95-63-6
1,3,5-Trimethylbenzene
20.9
mg/kg
4.9
1.8
1000
06/04/19 11:40
06/04/1916:34
108-67-8
Vinyl acetate
ND
mg/kg
2.5
0.43
50
06/04/19 11:40
06/04/19 13:20
108-05-4
Vinyl chloride
ND
mg/kg
0.49
0.088
50
06/04/19 11:40
06/04/19 13:20
75-01-4
Xylene (Total)
21.7
mg/kg
0.49
0.18
50
06/04/19 11:40
06/04/19 13:20
1330-20-7
m&p-Xylene
17.9
mg/kg
0.49
0.18
50
06/04/19 11:40
06/04/19 13:20
179601-23-1
o-Xylene
3.8
mg/kg
0.25
0.093
50
06/04/19 11:40
06/04/19 13:20
95-47-6
Surrogates
Toluene-d8 (S)
101
%
70-130
50
06/04/19 11:40
06/04/19 13:20
2037-26-5
4-Bromofluorobenzene (S)
115
%
70-130
50
06/04/19 11:40
06/04/19 13:20
460-00-4
1,2-Dichloroethane-d4 (S)
92
%
70-132
50
06/04/19 11:40
06/04/19 13:20
17060-07-0
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
21.7
%
0.10
0.10
1
05/24/19 13:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
QC Batch: 477322 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Associated Lab Samples: 92430462001, 92430462002, 92430462003, 92430462004, 92430462005, 92430462006, 92430462007,
92430462008,92430462009
METHOD BLANK: 2584901
Matrix:
Solid
Associated Lab Samples: 92430462001, 92430462002, 92430462003,
92430462004, 92430462005, 92430462006, 92430462007,
92430462008,92430462009
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C05-CO8)
mg/kg
ND
2.5
2.5 05/24/19 10:31 N2
Aliphatic (C09-C12)
mg/kg
ND
2.5
2.5 05/24/19 10:31 N2
Aromatic (C09-C10)
mg/kg
ND
2.5
2.5 05/24/19 10:31 N2
4-Bromofluorobenzene (FID) (S)
%
96
70-130
05/24/19 10:31
4-Bromofluorobenzene (PID) (S)
%
96
70-130
05/24/19 10:31
LABORATORY CONTROL SAMPLE & LCSD:
2584902
2584903
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
14.9
13.1 13.1
88
88
70-130 0 25 N2
Aliphatic (C09-C12)
mg/kg
14.9
14.8 15.0
99
101
30-130 2 25 N2
Aromatic (C09-C10)
mg/kg
5
4.8 4.9
98
99
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
102
104
70-130
4-Bromofluorobenzene (PID) (S)
%
102
104
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
QC Batch: 478737 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92430462001, 92430462002, 92430462003, 92430462006, 92430462007
METHOD BLANK: 2591404 Matrix: Solid
Associated Lab Samples: 92430462001, 92430462002, 92430462003, 92430462006, 92430462007
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0021
06/03/19 11:41
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0021
06/03/19 11:41
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0015
06/03/19 11:41
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0015
06/03/19 11:41
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0022
06/03/19 11:41
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0016
06/03/19 11:41
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0016
06/03/19 11:41
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0020
06/03/19 11:41
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0036
06/03/19 11:41
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0022
06/03/19 11:41
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0020
06/03/19 11:41
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
2-Butanone (MEK)
mg/kg
ND
0.10
0.0029
06/03/19 11:41
2-Chlorotoluene
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
2-Hexanone
mg/kg
ND
0.050
0.0039
06/03/19 11:41
4-Chlorotoluene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0037
06/03/19 11:41
Acetone
mg/kg
ND
0.10
0.010
06/03/19 11:41
Benzene
mg/kg
ND
0.0050
0.0016
06/03/19 11:41
Bromobenzene
mg/kg
ND
0.0050
0.0020
06/03/19 11:41
Bromochloromethane
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
Bromoform
mg/kg
ND
0.0050
0.0023
06/03/19 11:41
Bromomethane
mg/kg
ND
0.010
0.0025
06/03/19 11:41
Carbon tetrachloride
mg/kg
ND
0.0050
0.0026
06/03/19 11:41
Chlorobenzene
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
Chloroethane
mg/kg
ND
0.010
0.0024
06/03/19 11:41
Chloroform
mg/kg
ND
0.0050
0.0016
06/03/19 11:41
Chloromethane
mg/kg
ND
0.010
0.0024
06/03/19 11:41
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0014
06/03/19 11:41
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
Dibromochloromethane
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
METHOD BLANK: 2591404
Matrix: Solid
Associated Lab Samples: 92430462001, 92430462002,
92430462003,
92430462006, 92430462007
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Qualifiers
Dibromomethane
mg/kg
ND
0.0050
0.0025
06/03/19 11:41
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0036
06/03/19 11:41
Diisopropyl ether
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
Ethylbenzene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
Hexachloro-1,3-butadiene
mg/kg
ND
0.0050
0.0020
06/03/19 11:41
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
m&p-Xylene
mg/kg
ND
0.010
0.0036
06/03/19 11:41
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0015
06/03/19 11:41
Methylene Chloride
mg/kg
ND
0.020
0.0030
06/03/19 11:41
n-Butylbenzene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
n-Propylbenzene
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
Naphthalene
mg/kg
ND
0.0050
0.0012
06/03/19 11:41
o-Xylene
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
sec-Butylbenzene
mg/kg
ND
0.0050
0.0016
06/03/19 11:41
Styrene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
tert-Butyl benzene
mg/kg
ND
0.0050
0.0020
06/03/19 11:41
Tetrachloroethene
mg/kg
ND
0.0050
0.0017
06/03/19 11:41
Toluene
mg/kg
ND
0.0050
0.0018
06/03/19 11:41
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0019
06/03/19 11:41
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0015
06/03/19 11:41
Trichloroethene
mg/kg
ND
0.0050
0.0021
06/03/19 11:41
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0022
06/03/19 11:41
Vinyl acetate
mg/kg
ND
0.050
0.0088
06/03/19 11:41
v1
Vinyl chloride
mg/kg
ND
0.010
0.0018
06/03/19 11:41
Xylene (Total)
mg/kg
ND
0.010
0.0036
06/03/19 11:41
1,2-Dichloroethane-d4 (S)
%
99
70-132
06/03/19 11:41
4-Bromofluorobenzene (S)
%
100
70-130
06/03/19 11:41
Toluene-d8 (S)
%
99
70-130
06/03/19 11:41
LABORATORY CONTROL SAMPLE & LCSD:
2591405
2591406
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
0.05
0.067
0.062
133
123
70-130
8 30 L1
1,1,1-Trichloroethane
mg/kg
0.05
0.059
0.056
118
112
70-130
5 30
1,1,2,2-Tetrachloroethane
mg/kg
0.05
0.059
0.056
119
111
55-130
7 30
1,1,2-Trichloroethane
mg/kg
0.05
0.060
0.057
120
115
70-130
4 30
1,1-Dichloroethane
mg/kg
0.05
0.062
0.060
124
120
68-130
4 30
1,1-Dichloroethene
mg/kg
0.05
0.063
0.059
125
117
70-130
6 30
1,1-Dichloropropene
mg/kg
0.05
0.057
0.055
114
109
70-130
5 30
1,2,3-Trichlorobenzene
mg/kg
0.05
0.062
0.059
124
118
70-130
5 30
1,2,3-Trichloropropane
mg/kg
0.05
0.058
0.057
117
114
70-130
2 30
1,2,4-Trichlorobenzene
mg/kg
0.05
0.064
0.058
127
117
70-130
9 30
1,2,4-Trimethylbenzene
mg/kg
0.05
0.060
0.055
120
111
69-130
8 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
LABORATORY CONTROL SAMPLE & LCSD:
2591405
2591406
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
1,2-Dibromo-3-chloropropane
mg/kg
0.05
0.065
0.061
129
122
57-141
6
30
1,2-Dibromoethane (EDB)
mg/kg
0.05
0.061
0.057
122
114
70-130
7
30
1,2-Dichlorobenzene
mg/kg
0.05
0.059
0.055
119
110
70-130
8
30
1,2-Dichloroethane
mg/kg
0.05
0.054
0.053
109
107
70-130
2
30
1,2-Dichloropropane
mg/kg
0.05
0.061
0.057
121
113
70-130
7
30
1,3,5-Trimethylbenzene
mg/kg
0.05
0.059
0.055
118
110
70-130
6
30
1,3-Dichlorobenzene
mg/kg
0.05
0.059
0.055
117
110
70-130
7
30
1,3-Dichloropropane
mg/kg
0.05
0.060
0.057
120
114
70-130
5
30
1,4-Dichlorobenzene
mg/kg
0.05
0.059
0.055
119
110
70-130
7
30
2,2-Dichloropropane
mg/kg
0.05
0.063
0.058
125
116
70-130
8
30
2-Butanone (MEK)
mg/kg
0.1
0.12
0.12
116
120
60-130
3
30
2-Chlorotoluene
mg/kg
0.05
0.060
0.055
119
111
70-130
7
30
2-Hexanone
mg/kg
0.1
0.12
0.11
118
111
70-132
6
30
4-Chlorotoluene
mg/kg
0.05
0.059
0.055
118
110
70-130
7
30
4-Methyl-2-pentanone (MIBK)
mg/kg
0.1
0.12
0.11
116
111
69-130
5
30
Acetone
mg/kg
0.1
0.12
0.11
120
115
49-148
4
30
Benzene
mg/kg
0.05
0.061
0.057
121
114
70-130
6
30
Bromobenzene
mg/kg
0.05
0.060
0.056
121
113
70-130
7
30
Bromochloromethane
mg/kg
0.05
0.061
0.058
122
117
70-130
4
30
Bromodichloromethane
mg/kg
0.05
0.061
0.058
122
116
70-130
5
30
Bromoform
mg/kg
0.05
0.066
0.061
131
121
68-136
8
30
Bromomethane
mg/kg
0.05
0.059
0.055
117
110
60-140
7
30
Carbon tetrachloride
mg/kg
0.05
0.061
0.056
122
112
70-130
9
30
Chlorobenzene
mg/kg
0.05
0.060
0.056
121
113
70-130
7
30
Chloroethane
mg/kg
0.05
0.063
0.062
126
124
51-147
1
30
Chloroform
mg/kg
0.05
0.060
0.056
120
112
70-130
7
30
Chloromethane
mg/kg
0.05
0.063
0.060
126
119
48-130
5
30
cis-1,2-Dichloroethene
mg/kg
0.05
0.061
0.058
122
116
70-130
5
30
cis-1,3-Dichloropropene
mg/kg
0.05
0.062
0.058
124
116
70-130
6
30
Dibromochloromethane
mg/kg
0.05
0.063
0.059
127
119
70-130
7
30
Dibromomethane
mg/kg
0.05
0.061
0.056
122
113
70-130
8
30
Dichlorodifluoromethane
mg/kg
0.05
0.066
0.061
132
122
49-130
8
30 L1
Diisopropyl ether
mg/kg
0.05
0.061
0.059
121
118
66-130
3
30
Ethylbenzene
mg/kg
0.05
0.061
0.057
122
114
70-130
7
30
Hexachloro-1,3-butadiene
mg/kg
0.05
0.061
0.056
123
112
70-130
9
30
Isopropylbenzene (Cumene)
mg/kg
0.05
0.061
0.057
123
113
70-130
8
30
m&p-Xylene
mg/kg
0.1
0.12
0.11
122
114
70-130
7
30
Methyl-tert-butyl ether
mg/kg
0.05
0.060
0.054
120
109
70-130
10
30
Methylene Chloride
mg/kg
0.05
0.056
0.054
112
108
50-137
4
30
n-Butylbenzene
mg/kg
0.05
0.060
0.055
120
110
70-130
8
30
n-Propylbenzene
mg/kg
0.05
0.061
0.056
122
112
70-130
9
30
Naphthalene
mg/kg
0.05
0.061
0.058
122
117
70-131
5
30
o-Xylene
mg/kg
0.05
0.062
0.057
124
115
70-130
7
30
p-Isopropyltoluene
mg/kg
0.05
0.061
0.056
122
113
70-130
8
30
sec-Butylbenzene
mg/kg
0.05
0.061
0.057
123
115
70-130
7
30
Styrene
mg/kg
0.05
0.060
0.056
120
112
70-130
7
30
tert-Butyl benzene
mg/kg
0.05
0.055
0.052
111
103
69-130
7
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
LABORATORY CONTROL SAMPLE & LCSD:
2591405
2591406
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Tetrachloroethene
mg/kg
0.05
0.061
0.057
122
114
56-130
7
30
Toluene
mg/kg
0.05
0.059
0.054
117
108
70-130
9
30
trans-1,2-Dichloroethene
mg/kg
0.05
0.062
0.057
124
115
70-130
8
30
trans- 1,3-Dichloropropene
mg/kg
0.05
0.060
0.056
121
113
70-130
7
30
Trichloroethene
mg/kg
0.05
0.060
0.057
120
113
70-141
6
30
Trichlorofluoromethane
mg/kg
0.05
0.056
0.053
113
106
67-130
6
30
Vinyl acetate
mg/kg
0.1
0.14
0.13
143
127
10-136
12
30 L1,v1
Vinyl chloride
mg/kg
0.05
0.065
0.062
129
123
67-130
5
30
Xylene (Total)
mg/kg
0.15
0.18
0.17
123
114
70-130
7
30
1,2-Dichloroethane-d4 (S)
%
93
93
70-132
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
QC Batch: 478888 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92430462008
METHOD BLANK: 2591942
Associated Lab Samples: 92430462008
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0021
06/04/19 10:30
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0021
06/04/19 10:30
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0015
06/04/19 10:30
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0015
06/04/19 10:30
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0022
06/04/19 10:30
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0016
06/04/19 10:30
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0016
06/04/19 10:30
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0020
06/04/19 10:30
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0036
06/04/19 10:30
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0022
06/04/19 10:30
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0020
06/04/19 10:30
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
2-Butanone (MEK)
mg/kg
ND
0.10
0.0029
06/04/19 10:30
2-Chlorotoluene
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
2-Hexanone
mg/kg
ND
0.050
0.0039
06/04/19 10:30
4-Chlorotoluene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0037
06/04/19 10:30
Acetone
mg/kg
ND
0.10
0.010
06/04/19 10:30
Benzene
mg/kg
ND
0.0050
0.0016
06/04/19 10:30
Bromobenzene
mg/kg
ND
0.0050
0.0020
06/04/19 10:30
Bromochloromethane
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
Bromoform
mg/kg
ND
0.0050
0.0023
06/04/19 10:30
Bromomethane
mg/kg
ND
0.010
0.0025
06/04/19 10:30
Carbon tetrachloride
mg/kg
ND
0.0050
0.0026
06/04/19 10:30
Chlorobenzene
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
Chloroethane
mg/kg
ND
0.010
0.0024
06/04/19 10:30
Chloroform
mg/kg
ND
0.0050
0.0016
06/04/19 10:30
Chloromethane
mg/kg
ND
0.010
0.0024
06/04/19 10:30
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0014
06/04/19 10:30
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
Dibromochloromethane
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
METHOD BLANK: 2591942
Matrix: Solid
Associated Lab Samples: 92430462008
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Qualifiers
Dibromomethane
mg/kg
ND
0.0050
0.0025
06/04/19 10:30
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0036
06/04/19 10:30
Diisopropyl ether
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
Ethylbenzene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
Hexachloro-1,3-butadiene
mg/kg
ND
0.0050
0.0020
06/04/19 10:30
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
m&p-Xylene
mg/kg
ND
0.010
0.0036
06/04/19 10:30
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0015
06/04/19 10:30
Methylene Chloride
mg/kg
ND
0.020
0.0030
06/04/19 10:30
n-Butylbenzene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
n-Propylbenzene
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
Naphthalene
mg/kg
ND
0.0050
0.0012
06/04/19 10:30
o-Xylene
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
sec-Butylbenzene
mg/kg
ND
0.0050
0.0016
06/04/19 10:30
Styrene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
tert-Butyl benzene
mg/kg
ND
0.0050
0.0020
06/04/19 10:30
Tetrachloroethene
mg/kg
ND
0.0050
0.0017
06/04/19 10:30
Toluene
mg/kg
ND
0.0050
0.0018
06/04/19 10:30
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0019
06/04/19 10:30
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0015
06/04/19 10:30
Trichloroethene
mg/kg
ND
0.0050
0.0021
06/04/19 10:30
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0022
06/04/19 10:30
Vinyl acetate
mg/kg
ND
0.050
0.0088
06/04/19 10:30
v1
Vinyl chloride
mg/kg
ND
0.010
0.0018
06/04/19 10:30
Xylene (Total)
mg/kg
ND
0.010
0.0036
06/04/19 10:30
1,2-Dichloroethane-d4 (S)
%
101
70-132
06/04/19 10:30
4-Bromofluorobenzene (S)
%
100
70-130
06/04/19 10:30
Toluene-d8 (S)
%
99
70-130
06/04/19 10:30
LABORATORY CONTROL SAMPLE & LCSD:
2591943
2591944
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
0.05
0.059
0.058
117
115
70-130
2 30
1,1,1-Trichloroethane
mg/kg
0.05
0.053
0.053
106
107
70-130
0 30
1,1,2,2-Tetrachloroethane
mg/kg
0.05
0.052
0.051
104
102
55-130
2 30
1,1,2-Trichloroethane
mg/kg
0.05
0.054
0.054
107
107
70-130
0 30
1,1-Dichloroethane
mg/kg
0.05
0.053
0.056
106
112
68-130
5 30
1,1-Dichloroethene
mg/kg
0.05
0.056
0.057
112
114
70-130
1 30
1,1-Dichloropropene
mg/kg
0.05
0.052
0.052
104
104
70-130
0 30
1,2,3-Trichlorobenzene
mg/kg
0.05
0.057
0.056
113
111
70-130
2 30
1,2,3-Trichloropropane
mg/kg
0.05
0.053
0.052
106
105
70-130
1 30
1,2,4-Trichlorobenzene
mg/kg
0.05
0.055
0.056
111
111
70-130
0 30
1,2,4-Trimethylbenzene
mg/kg
0.05
0.052
0.053
104
107
69-130
2 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
LABORATORY CONTROL SAMPLE & LCSD:
2591943
2591944
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
1,2-Dibromo-3-chloropropane
mg/kg
0.05
0.056
0.059
113
117
57-141
4
30
1,2-Dibromoethane (EDB)
mg/kg
0.05
0.055
0.054
110
107
70-130
2
30
1,2-Dichlorobenzene
mg/kg
0.05
0.053
0.052
105
105
70-130
0
30
1,2-Dichloroethane
mg/kg
0.05
0.051
0.051
102
103
70-130
1
30
1,2-Dichloropropane
mg/kg
0.05
0.055
0.053
110
106
70-130
4
30
1,3,5-Trimethylbenzene
mg/kg
0.05
0.053
0.053
107
107
70-130
0
30
1,3-Dichlorobenzene
mg/kg
0.05
0.053
0.053
106
106
70-130
0
30
1,3-Dichloropropane
mg/kg
0.05
0.054
0.053
108
107
70-130
2
30
1,4-Dichlorobenzene
mg/kg
0.05
0.052
0.052
105
104
70-130
1
30
2,2-Dichloropropane
mg/kg
0.05
0.055
0.055
110
110
70-130
0
30
2-Butanone (MEK)
mg/kg
0.1
0.11
0.11
110
109
60-130
1
30
2-Chlorotoluene
mg/kg
0.05
0.053
0.053
106
106
70-130
0
30
2-Hexanone
mg/kg
0.1
0.11
0.11
108
109
70-132
1
30
4-Chlorotoluene
mg/kg
0.05
0.053
0.053
107
106
70-130
1
30
4-Methyl-2-pentanone (MIBK)
mg/kg
0.1
0.11
0.11
110
109
69-130
1
30
Acetone
mg/kg
0.1
0.11
0.11
113
107
49-148
6
30
Benzene
mg/kg
0.05
0.054
0.053
108
106
70-130
2
30
Bromobenzene
mg/kg
0.05
0.055
0.054
110
109
70-130
1
30
Bromochloromethane
mg/kg
0.05
0.055
0.056
110
113
70-130
2
30
Bromodichloromethane
mg/kg
0.05
0.056
0.055
112
109
70-130
3
30
Bromoform
mg/kg
0.05
0.058
0.057
116
113
68-136
3
30
Bromomethane
mg/kg
0.05
0.054
0.055
108
109
60-140
1
30
Carbon tetrachloride
mg/kg
0.05
0.053
0.053
107
107
70-130
0
30
Chlorobenzene
mg/kg
0.05
0.054
0.053
108
106
70-130
2
30
Chloroethane
mg/kg
0.05
0.058
0.058
117
116
51-147
1
30
Chloroform
mg/kg
0.05
0.053
0.054
106
108
70-130
2
30
Chloromethane
mg/kg
0.05
0.054
0.054
108
109
48-130
1
30
cis-1,2-Dichloroethene
mg/kg
0.05
0.054
0.056
109
112
70-130
2
30
cis-1,3-Dichloropropene
mg/kg
0.05
0.055
0.054
111
108
70-130
2
30
Dibromochloromethane
mg/kg
0.05
0.057
0.055
114
110
70-130
3
30
Dibromomethane
mg/kg
0.05
0.053
0.054
106
107
70-130
1
30
Dichlorodifluoromethane
mg/kg
0.05
0.055
0.055
109
110
49-130
0
30
Diisopropyl ether
mg/kg
0.05
0.058
0.059
116
117
66-130
1
30
Ethylbenzene
mg/kg
0.05
0.054
0.053
108
106
70-130
2
30
Hexachloro-1,3-butadiene
mg/kg
0.05
0.053
0.053
106
106
70-130
1
30
Isopropylbenzene (Cumene)
mg/kg
0.05
0.055
0.053
110
106
70-130
3
30
m&p-Xylene
mg/kg
0.1
0.11
0.11
109
107
70-130
1
30
Methyl-tert-butyl ether
mg/kg
0.05
0.055
0.058
110
115
70-130
5
30
Methylene Chloride
mg/kg
0.05
0.050
0.052
101
103
50-137
2
30
n-Butylbenzene
mg/kg
0.05
0.053
0.054
106
109
70-130
2
30
n-Propylbenzene
mg/kg
0.05
0.054
0.054
108
108
70-130
0
30
Naphthalene
mg/kg
0.05
0.056
0.054
112
109
70-131
3
30
o-Xylene
mg/kg
0.05
0.055
0.054
110
108
70-130
1
30
p-Isopropyltoluene
mg/kg
0.05
0.054
0.054
108
108
70-130
0
30
sec-Butylbenzene
mg/kg
0.05
0.055
0.055
110
110
70-130
0
30
Styrene
mg/kg
0.05
0.053
0.053
106
105
70-130
1
30
tert-Butyl benzene
mg/kg
0.05
0.049
0.049
98
97
69-130
1
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
LABORATORY CONTROL SAMPLE & LCSD:
2591943
2591944
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Tetrachloroethene
mg/kg
0.05
0.053
0.052
107
104
56-130
3
30
Toluene
mg/kg
0.05
0.052
0.051
104
102
70-130
3
30
trans-1,2-Dichloroethene
mg/kg
0.05
0.055
0.056
110
112
70-130
2
30
trans- 1,3-Dichloropropene
mg/kg
0.05
0.054
0.054
107
109
70-130
2
30
Trichloroethene
mg/kg
0.05
0.054
0.053
108
106
70-141
2
30
Trichlorofluoromethane
mg/kg
0.05
0.051
0.052
101
103
67-130
2
30
Vinyl acetate
mg/kg
0.1
0.13
0.13
128
127
10-136
1
30 v1
Vinyl chloride
mg/kg
0.05
0.056
0.056
111
111
67-130
0
30
Xylene (Total)
mg/kg
0.15
0.16
0.16
109
108
70-130
1
30
1,2-Dichloroethane-d4 (S)
%
97
94
70-132
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8(S)
%
100
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
QC Batch: 478914 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92430462004, 92430462005, 92430462009
METHOD BLANK: 2592061 Matrix:
Associated Lab Samples: 92430462004, 92430462005, 92430462009
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0021
06/04/19 09:41
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0021
06/04/19 09:41
1,1-Dichloroethane
mg/kg
ND
0.0050
0.0015
06/04/19 09:41
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0015
06/04/19 09:41
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0022
06/04/19 09:41
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0016
06/04/19 09:41
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0016
06/04/19 09:41
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0020
06/04/19 09:41
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0036
06/04/19 09:41
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0022
06/04/19 09:41
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0020
06/04/19 09:41
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
2,2-Dichloropropane
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
2-Butanone (MEK)
mg/kg
ND
0.10
0.0029
06/04/19 09:41
2-Chlorotoluene
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
2-Hexanone
mg/kg
ND
0.050
0.0039
06/04/19 09:41
4-Chlorotoluene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0037
06/04/19 09:41
Acetone
mg/kg
ND
0.10
0.010
06/04/19 09:41
Benzene
mg/kg
ND
0.0050
0.0016
06/04/19 09:41
Bromobenzene
mg/kg
ND
0.0050
0.0020
06/04/19 09:41
Bromochloromethane
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
Bromodichloromethane
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
Bromoform
mg/kg
ND
0.0050
0.0023
06/04/19 09:41
Bromomethane
mg/kg
ND
0.010
0.0025
06/04/19 09:41
Carbon tetrachloride
mg/kg
ND
0.0050
0.0026
06/04/19 09:41
Chlorobenzene
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
Chloroethane
mg/kg
ND
0.010
0.0024
06/04/19 09:41
Chloroform
mg/kg
ND
0.0050
0.0016
06/04/19 09:41
Chloromethane
mg/kg
ND
0.010
0.0024
06/04/19 09:41
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0014
06/04/19 09:41
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
Dibromochloromethane
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
METHOD BLANK: 2592061 Matrix:
Associated Lab Samples: 92430462004, 92430462005, 92430462009
Blank
Parameter Units Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromomethane
mg/kg
ND
0.0050
0.0025
06/04/19 09:41
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0036
06/04/19 09:41
Diisopropyl ether
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
Ethylbenzene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
Hexachloro-1,3-butadiene
mg/kg
ND
0.0050
0.0020
06/04/19 09:41
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
m&p-Xylene
mg/kg
ND
0.010
0.0036
06/04/19 09:41
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0015
06/04/19 09:41
Methylene Chloride
mg/kg
ND
0.020
0.0030
06/04/19 09:41
n-Butylbenzene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
n-Propylbenzene
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
Naphthalene
mg/kg
ND
0.0050
0.0012
06/04/19 09:41
o-Xylene
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
sec-Butylbenzene
mg/kg
ND
0.0050
0.0016
06/04/19 09:41
Styrene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
tert-Butyl benzene
mg/kg
ND
0.0050
0.0020
06/04/19 09:41
Tetrachloroethene
mg/kg
ND
0.0050
0.0017
06/04/19 09:41
Toluene
mg/kg
ND
0.0050
0.0018
06/04/19 09:41
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.0019
06/04/19 09:41
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.0015
06/04/19 09:41
Trichloroethene
mg/kg
ND
0.0050
0.0021
06/04/19 09:41
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0022
06/04/19 09:41
Vinyl acetate
mg/kg
ND
0.050
0.0088
06/04/19 09:41
Vinyl chloride
mg/kg
ND
0.010
0.0018
06/04/19 09:41
Xylene (Total)
mg/kg
ND
0.010
0.0036
06/04/19 09:41
1,2-Dichloroethane-d4 (S)
%
82
70-132
06/04/19 09:41
4-Bromofluorobenzene (S)
%
101
70-130
06/04/19 09:41
Toluene-d8 (S)
%
109
70-130
06/04/19 09:41
Qualifiers
LABORATORY CONTROL SAMPLE:
2592062
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
0.05
0.054
108
70-130
1,1,1-Trichloroethane
mg/kg
0.05
0.052
105
70-130
1,1,2,2-Tetrachloroethane
mg/kg
0.05
0.049
98
55-130
1,1,2-Trichloroethane
mg/kg
0.05
0.053
107
70-130
1,1-Dichloroethane
mg/kg
0.05
0.051
102
68-130
1,1-Dichloroethene
mg/kg
0.05
0.053
106
70-130
1,1-Dichloropropene
mg/kg
0.05
0.054
107
70-130
1,2,3-Trichlorobenzene
mg/kg
0.05
0.050
100
70-130
1,2,3-Trichloropropane
mg/kg
0.05
0.051
102
70-130
1,2,4-Trichlorobenzene
mg/kg
0.05
0.050
100
70-130
1,2,4-Trimethylbenzene
mg/kg
0.05
0.048
96
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
LABORATORY CONTROL SAMPLE:
Parameter
2592062
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
mg/kg
0.05
0.049
98
57-141
1,2-Dibromoethane (EDB)
mg/kg
0.05
0.052
105
70-130
1,2-Dichlorobenzene
mg/kg
0.05
0.048
97
70-130
1,2-Dichloroethane
mg/kg
0.05
0.048
96
70-130
1,2-Dichloropropane
mg/kg
0.05
0.054
108
70-130
1,3,5-Trimethylbenzene
mg/kg
0.05
0.050
100
70-130
1,3-Dichlorobenzene
mg/kg
0.05
0.049
98
70-130
1,3-Dichloropropane
mg/kg
0.05
0.053
106
70-130
1,4-Dichlorobenzene
mg/kg
0.05
0.049
98
70-130
2,2-Dichloropropane
mg/kg
0.05
0.053
106
70-130
2-Butanone (MEK)
mg/kg
0.1
0.11
110
60-130
2-Chlorotoluene
mg/kg
0.05
0.050
99
70-130
2-Hexanone
mg/kg
0.1
0.11
106
70-132
4-Chlorotoluene
mg/kg
0.05
0.049
99
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
0.1
0.10
105
69-130
Acetone
mg/kg
0.1
0.11
105
49-148
Benzene
mg/kg
0.05
0.054
109
70-130
Bromobenzene
mg/kg
0.05
0.049
99
70-130
Bromochloromethane
mg/kg
0.05
0.051
102
70-130
Bromodichloromethane
mg/kg
0.05
0.054
108
70-130
Bromoform
mg/kg
0.05
0.052
104
68-136
Bromomethane
mg/kg
0.05
0.054
108
60-140
Carbon tetrachloride
mg/kg
0.05
0.053
106
70-130
Chlorobenzene
mg/kg
0.05
0.049
98
70-130
Chloroethane
mg/kg
0.05
0.053
105
51-147
Chloroform
mg/kg
0.05
0.048
96
70-130
Chloromethane
mg/kg
0.05
0.050
99
48-130
cis-1,2-Dichloroethene
mg/kg
0.05
0.051
102
70-130
cis-1,3-Dichloropropene
mg/kg
0.05
0.056
113
70-130
Dibromochloromethane
mg/kg
0.05
0.053
107
70-130
Dibromomethane
mg/kg
0.05
0.052
105
70-130
Dichlorodifluoromethane
mg/kg
0.05
0.052
104
49-130
Diisopropyl ether
mg/kg
0.05
0.054
108
66-130
Ethylbenzene
mg/kg
0.05
0.051
102
70-130
Hexachloro-1,3-butadiene
mg/kg
0.05
0.049
99
70-130
Isopropylbenzene (Cumene)
mg/kg
0.05
0.052
104
70-130
m&p-Xylene
mg/kg
0.1
0.10
104
70-130
Methyl-tert-butyl ether
mg/kg
0.05
0.049
98
70-130
Methylene Chloride
mg/kg
0.05
0.048
95
50-137
n-Butylbenzene
mg/kg
0.05
0.049
98
70-130
n-Propylbenzene
mg/kg
0.05
0.051
102
70-130
Naphthalene
mg/kg
0.05
0.048
96
70-131
o-Xylene
mg/kg
0.05
0.052
103
70-130
p-Isopropyltoluene
mg/kg
0.05
0.050
101
70-130
sec-Butylbenzene
mg/kg
0.05
0.051
103
70-130
Styrene
mg/kg
0.05
0.051
102
70-130
tert-Butyl benzene
mg/kg
0.05
0.045
91
69-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
LABORATORY CONTROL SAMPLE:
Parameter
2592062
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Tetrachloroethene
mg/kg
0.05
0.051
103
56-130
Toluene
mg/kg
0.05
0.049
98
70-130
trans-1,2-Dichloroethene
mg/kg
0.05
0.053
106
70-130
trans- 1,3-Dichloropropene
mg/kg
0.05
0.054
108
70-130
Trichloroethene
mg/kg
0.05
0.056
111
70-141
Trichlorofluoromethane
mg/kg
0.05
0.048
96
67-130
Vinyl acetate
mg/kg
0.1
0.086
86
10-136
Vinyl chloride
mg/kg
0.05
0.051
103
67-130
Xylene (Total)
mg/kg
0.15
0.16
104
70-130
1,2-Dichloroethane-d4 (S)
%
98
70-132
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
97
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2592063
MS
92430462004 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2592064
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.69
0.69
0.63
0.58
92
84
52-133
9
30
1,1,1-Trichloroethane
mg/kg
ND
0.69
0.69
0.61
0.58
88
85
49-137
4
30
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.69
0.69
0.60
0.55
87
79
39-150
10
30
1,1,2-Trichloroethane
mg/kg
ND
0.69
0.69
0.61
0.60
89
88
48-140
1
30
1,1-Dichloroethane
mg/kg
ND
0.69
0.69
0.60
0.60
88
88
46-135
0
30
1,1-Dichloroethene
mg/kg
ND
0.69
0.69
0.59
0.58
86
84
38-149
2
30
1,1-Dichloropropene
mg/kg
ND
0.69
0.69
0.58
0.56
85
82
41-140
4
30
1,2,3-Trichlorobenzene
mg/kg
ND
0.69
0.69
0.65
0.64
94
93
10-158
1
30
1,2,3-Trichooropropane
mg/kg
ND
0.69
0.69
0.59
0.58
86
84
33-157
2
30
1,2,4-Trichlorobenzene
mg/kg
ND
0.69
0.69
0.63
0.60
86
83
10-155
4
30
1,2,4-Trimethyl benzene
mg/kg
0.069J
0.69
0.69
0.79
0.68
105
88
24-154
15
30
1,2-Dibromo-3-
mg/kg
ND
0.69
0.69
0.54
0.50
79
73
33-158
7
30
chloropropane
1,2-Dibromoethane (EDB)
mg/kg
ND
0.69
0.69
0.59
0.55
85
80
40-136
7
30
1,2-Dichlorobenzene
mg/kg
ND
0.69
0.69
0.62
0.60
89
88
27-146
2
30
1,2-Dichloroethane
mg/kg
ND
0.69
0.69
0.60
0.59
88
86
49-140
2
30
1,2-Dichloropropane
mg/kg
ND
0.69
0.69
0.65
0.62
95
90
44-143
5
30
1,3,5-Trimethyl benzene
mg/kg
ND
0.69
0.69
0.65
0.61
90
84
40-144
6
30
1,3-Dichlorobenzene
mg/kg
ND
0.69
0.69
0.61
0.58
88
84
33-140
4
30
1,3-Dichloropropane
mg/kg
ND
0.69
0.69
0.63
0.58
92
84
47-147
9
30
1,4-Dichlorobenzene
mg/kg
ND
0.69
0.69
0.61
0.58
88
84
35-139
4
30
2,2-Dichloropropane
mg/kg
ND
0.69
0.69
0.61
0.60
89
87
41-140
2
30
2-Butanone (MEK)
mg/kg
ND
1.3
1.3
1.11
1.01
78
75
10-181
30
2-Chlorotoluene
mg/kg
ND
0.69
0.69
0.62
0.62
90
90
38-147
0
30
2-Hexanone
mg/kg
ND
1.3
1.3
1.11
1.01
80
74
18-169
30
4-Chlorotoluene
mg/kg
ND
0.69
0.69
0.61
0.59
89
86
36-145
4
30
4-Methyl-2-pentanone
mg/kg
ND
1.3
1.3
1.11
1.11
81
77
16-175
30
(MIBK)
Acetone
mg/kg
ND
1.3
1.3
0.991
1.11
72
77
10-200
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
Date: 06/04/2019 05:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 35 of 43

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2592063
MS
92430462004 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2592064
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
Benzene
mg/kg
ND
0.69
0.69
0.66
0.63
96
92
46-136
4
30
Bromobenzene
mg/kg
ND
0.69
0.69
0.64
0.62
93
89
38-149
4
30
Bromochloromethane
mg/kg
ND
0.69
0.69
0.61
0.61
89
88
44-142
1
30
Bromodichloromethane
mg/kg
ND
0.69
0.69
0.62
0.61
90
88
41-140
2
30
Bromoform
mg/kg
ND
0.69
0.69
0.54
0.51
79
74
34-145
7
30
Bromomethane
mg/kg
ND
0.69
0.69
0.50
0.52
73
75
14-162
3
30
Carbon tetrachloride
mg/kg
ND
0.69
0.69
0.60
0.61
87
89
44-141
2
30
Chlorobenzene
mg/kg
ND
0.69
0.69
0.62
0.59
90
85
39-141
5
30
Chloroethane
mg/kg
ND
0.69
0.69
0.33J
0.32J
47
47
10-182
30
Chloroform
mg/kg
ND
0.69
0.69
0.57
0.56
83
82
45-140
2
30
Chloromethane
mg/kg
ND
0.69
0.69
0.59
0.60
86
88
19-149
2
30
cis-1,2-Dichloroethene
mg/kg
ND
0.69
0.69
0.62
0.61
90
88
38-150
2
30
cis-1,3-Dichloropropene
mg/kg
ND
0.69
0.69
0.63
0.60
92
87
30-144
5
30
Dibromochloromethane
mg/kg
ND
0.69
0.69
0.57
0.51
83
74
36-145
11
30
Dibromomethane
mg/kg
ND
0.69
0.69
0.64
0.61
94
89
41-145
5
30
Dichlorodifluoromethane
mg/kg
ND
0.69
0.69
0.59
0.59
85
85
16-146
0
30
Diisopropyl ether
mg/kg
ND
0.69
0.69
0.57
0.53
83
78
41-143
7
30
Ethylbenzene
mg/kg
ND
0.69
0.69
0.67
0.62
97
90
35-144
7
30
Hexachloro-1,3-butadiene
mg/kg
ND
0.69
0.69
0.60
0.58
87
84
10-160
4
30
Isopropylbenzene
mg/kg
ND
0.69
0.69
0.66
0.61
96
89
30-152
7
30
(Cumene)
m&p-Xylene
mg/kg
ND
1.3
1.3
1.4
1.2
100
90
33-145
10
30
Methyl-tert-butyl ether
mg/kg
ND
0.69
0.69
0.58
0.56
85
81
49-140
5
30
Methylene Chloride
mg/kg
ND
0.69
0.69
0.66J
0.63J
96
91
10-174
30
n-Butylbenzene
mg/kg
ND
0.69
0.69
0.62
0.59
90
85
10-160
6
30
n-Propylbenzene
mg/kg
ND
0.69
0.69
0.65
0.62
94
90
24-159
5
30
Naphthalene
mg/kg
0.041J
0.69
0.69
0.64
0.60
87
81
10-171
6
30
o-Xylene
mg/kg
ND
0.69
0.69
0.68
0.62
99
91
31-150
9
30
p-Isopropyltoluene
mg/kg
ND
0.69
0.69
0.64
0.60
93
87
21-154
7
30
sec-Butylbenzene
mg/kg
ND
0.69
0.69
0.63
0.61
92
89
19-159
3
30
Styrene
mg/kg
ND
0.69
0.69
0.64
0.60
93
87
15-152
6
30
tert-Butylbenzene
mg/kg
ND
0.69
0.69
0.55
0.54
80
79
31-141
2
30
Tetrachloroethene
mg/kg
ND
0.69
0.69
0.61
0.56
89
81
19-141
9
30
Toluene
mg/kg
ND
0.69
0.69
0.64
0.64
92
92
31-146
0
30
trans-1,2-Dichloroethene
mg/kg
ND
0.69
0.69
0.62
0.59
90
86
28-157
5
30
trans-1,3-Dichloropropene
mg/kg
ND
0.69
0.69
0.62
0.59
90
85
25-146
6
30
Trichloroethene
mg/kg
ND
0.69
0.69
0.64
0.62
94
90
34-149
4
30
Trichlorofluoromethane
mg/kg
ND
0.69
0.69
0.34
0.33
49
48
10-167
2
30
Vinyl acetate
mg/kg
ND
1.3
1.3
0.93J
0.88J
68
64
10-200
30
Vinyl chloride
mg/kg
ND
0.69
0.69
0.61
0.58
89
85
36-155
5
30
Xylene (Total)
mg/kg
ND
2.1
2.1
2.1
1.9
100
90
29-148
10
30
1,2-Dichloroethane-d4 (S)
%
97
94
70-132
4-Bromofluorobenzene (S)
%
102
100
70-130
Toluene-d8 (S)
%
100
102
70-130
P2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
QC Batch: 477227 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92430462001, 92430462002, 92430462003, 92430462004, 92430462005
SAMPLE DUPLICATE: 2584621
92430425001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 15.8 16.4 4 25 H1
SAMPLE DUPLICATE: 2584622
92430427001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 26.6 26.2 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Circle K 2708383
Pace Project No.: 92430462
QC Batch: 477407 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92430462006, 92430462007, 92430462008, 92430462009
SAMPLE DUPLICATE: 2585360
92430341001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 96.5 96.4 0 25
SAMPLE DUPLICATE: 2585361
92430462009 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 21.7 21.8 0 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Circle K 2708383
Pace Project No.: 92430462
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
H1 Analysis conducted outside the EPA method holding time.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
P2 Re -extraction or re -analysis could not be performed due to insufficient sample amount.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/04/2019 05:38 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 43

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Circle K 2708383
92430462
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92430462001
Sidewall SE
MADEP VPH
477322
MADEP VPH
477707
92430462002
Sidewall NE
MADEP VPH
477322
MADEP VPH
477707
92430462003
Sidewall SW
MADEP VPH
477322
MADEP VPH
477707
92430462004
Sidewall NW
MADEP VPH
477322
MADEP VPH
477707
92430462005
Base
MADEP VPH
477322
MADEP VPH
477707
92430462006
L Sidewall SE
MADEP VPH
477322
MADEP VPH
477707
92430462007
L Sidewall NE
MADEP VPH
477322
MADEP VPH
477707
92430462008
L Sidewall NW
MADEP VPH
477322
MADEP VPH
477707
92430462009
L Base
MADEP VPH
477322
MADEP VPH
477707
92430462001
Sidewall SE
EPA 5035A
478737
EPA 8260D
478749
92430462002
Sidewall NE
EPA 5035A
478737
EPA 8260D
478749
92430462003
Sidewall SW
EPA 5035A
478737
EPA 8260D
478749
92430462004
Sidewall NW
EPA 5035A
478914
EPA 8260D
478927
92430462005
Base
EPA 5035A
478914
EPA 8260D
478927
92430462006
L Sidewall SE
EPA 5035A
478737
EPA 8260D
478749
92430462007
L Sidewall NE
EPA 5035A
478737
EPA 8260D
478749
92430462008
L Sidewall NW
EPA 5035A
478888
EPA 8260D
478907
92430462009
L Base
EPA 5035A
478914
EPA 8260D
478927
92430462001
Sidewall SE
ASTM D2974-87
477227
92430462002
Sidewall NE
ASTM D2974-87
477227
92430462003
Sidewall SW
ASTM D2974-87
477227
92430462004
Sidewall NW
ASTM D2974-87
477227
92430462005
Base
ASTM D2974-87
477227
92430462006
L Sidewall SE
ASTM D2974-87
477407
92430462007
L Sidewall NE
ASTM D2974-87
477407
92430462008
L Sidewall NW
ASTM D2974-87
477407
92430462009
L Base
ASTM D2974-87
477407
Date: 06/04/2019 05:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 40 of 43

m
c3CEAflaijflCdl"
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
?age 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvlllp ❑ Raleigh[] Mechanicsville❑
Sampleo Client Name: � W,: 92430462
Upon ReceiptProject!
Courier: []Fed Ex ❑UPS ❑USPS ,]Client 13111111
❑ Commercial []Pace []Other:to1111111—
0452
Custody Seal Present? ❑Yes
0A
❑No Seals Intact? ❑Yes ❑No
Date/Initials Person Examining Contents: I
Packing Material: []Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
❑Yes ❑Na []N/A
Thermometers" ❑fR Gun i0: 92TO48 Type of Ice: ❑Wet ❑Blue ❑None
�l-"
Eoaler Temp (°C): } Correctlon Factor: Add/Subtract ('C) p,p
Temp should be above freezing to 6°C
Cooler Temp Corrected ('C): []Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (4 "N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign soutce (internationally,
M1 _ r—I.._ anti Puertn Rlrol? nYes FlNo
Comments/Discrepancy:
Chain of Custody Present?
[]Yes
❑No
❑N/A
1.
Samples Arrived within Hold Time? .
❑res
❑No
❑NIA
2.
Short Hold, Time Analysis (02 hr.)?
❑Yes
❑No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
[]NO
❑N/A
4.
Sufficient Volume?
. Dyes
On
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Des
❑Yes
ONO
❑No
❑N/A
❑NIA
6.
Containers Intact?
❑Yes
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
❑N/A
3.
$ample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:... i---1`
[]yes
�
❑No
[]N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑yes
[]No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
[:]No
[]No
❑N/A
❑NIA
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ONO
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Tlme:
ID of split containers:
Date: S%24
Date:
Page 41 of 43

Document Name:
document Revised: February 7, 2018
e
aceAnalyucal
Sample Condition Upon Receipt(SCUR)
Page I of 2
Document No.:
Issuing Authority,
F-CAR-Cs-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRD/8015 (water) OOC, LLHg
**Bottom half of box is to list number of bottle
Project #i
WO#:92430462
PM: PTE Due Date: 06/04/19
CLIENT: 92—CRAWFORD
E
v
$
a
CL
C
V
M
Ln
n
M
Q
a
m
w
w
CL
V
v
a
Ln
N
7
m
a
rp
a2i
v
C
U
o
a
l�A
N
a
M
2
G
C
a
.••i
a
m
0.
a
=
V
ro
°•
a
m
n
M
Z
Z
V
n
Q
N
a
m
Z
a
N
U
°-
N
a
m
H
a
a
Z
V
_�
a
M
a
m
C
ro
ro
[7
a
O/
E
3
Z
v
C
a`
¢
ti
l7
a
=
n
U
S
`a
a
C
ry
C7
a
a
a
7
W
n
E
N
l7
a
n
$
VI
N
2
`v
m
ar
.••i
l'7
a
N
n
O
LA
N
2
6
E
¢
N
L7
a
V
Z
o
E
¢
J
E
a
n
a
t9
a
-Z.
U
x
Q
>
EJE
l7
n
.z_..
m
N
N
A
z
q
>
E
l7
>
Q
Z
4
L
D
Q
O
l7
>
=
?
d
rry
x
4
O
q
a
at
Q
o
m
N
Y
u
a
m.EEE
Y
¢
0
>
Z
x
7
y
r
a
Y
t7
>
Z
`-'
�9
d
m
y
,n
v
rNi
,n
a
Ln
Zap
M
a
y
=
`a
J
N
F"
ea
a
v,
T
e�
Z
u
m
J
E
N
a
m
a
y
E
EEEEbEEEEvwaE`E
O
r�
L7
a
O
ip
c
ve
E
O
N
v�i
y
M
}
d
C
a
4
E
C
C�7
o
i
f
z
3
I
'
4
5
j
I
6
j
i
7
8
I
I
to
a.z
pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
bate preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot b
Note: Whenever there is a discrepancy affecting North Carolina compiiance samples, a copy of this form will he Pent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 42 of 43

i.
m
m
U
2
Q
EO
G a
E
E
N
d m
r C
d �
c0
U
a, z
W
C
ao
ow
O�
cn
N
Ua0
LL
U
0 4
Z C
helul
sa�dweg
z
NIJ.
�
Ie�ooO
D
z
Palea3
0
10
z
-
uo PaA!aaaa
{Nu,) auuolgo lenp!saa
--- -
m
N
N
0 u! d"li
Li
y�
w 'S
U.
a r-,
,1,
a
�
� {
N
�
rs
QC
t
J
V
�
q
N
�
O
ti
y
3
c
o
- --
to
4
HdA
i�1,
�
�
o
09Z9 ,(q OOA
pC
m
L
LL
NIA
lsal sasdIeuV
C
a
la4lO
K
1
o �
. C
o
!oueglapy
1
a
w
G
EOZSZeN
3
2
a)
y
C
HOeN
L
m
-•
E
to
!
r
m
m
�
N
IOH
s-
3a
CONH
OOSZH
C
U r!Lu
paivaselduO
c u
s
0
.
J ay
ayy`
C
U U
U
sb3NivlNoa doa
m
`a
�¢
a a-
a
M�
IT
Q
W
W
N0110311001V dV131 3ldWVS--
on�
Zry
a
a
1
N
Z
u
Q
LijE
O
O
LLI
L
Z �,
z
z
LU
Lo
p
INI
a
0)
-E2
m I
(dW00=0 BV2f:i=D) 3dA13ldWVS
y
°
ti
z
(gBl ai sapm pgan aasp 3400 7(IiJiVW
�a
n y
lay
a
p E
°u553a
7
tr
0
N
�.
a
L d
d
in0¢O�
d
00:
ff
U
a a`
o
a
so33a' in0 dOi=
c
6Y
E
0
c
y
Z
76
C
J
Q
U
.>
.-
W y`
a -
/\
t
v
u E
0 4'
Q„ o
N
W—
L L Q
o
U
U
Q N a
N Z
m
0AD
c�m�
�Z�
0
°
°
Page 43 c
3
n
J�-
rsV
M
VW31�
f 43

APPENDIX F
UST-61 FORM

UST-61
24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
in NC suspected release
(DWM USE ONLY)
Suspected Contamination? (Y/N) _Y
Facility ID Number _4527
Incident # Risk (H,I,L,U)
Confirmed GW Contamination? (Y/N) _N
Date Leak Discovered _5/22/19
Received On Received By
Confirmed Soil Contamination ?(Y/N) _Y
Comm/Non-Commercial? _Comm_
Reported by (circle one): Phone, Fax or Report
Samples Taken?(Y/N) _Y
Reg/Non-regulated? _Reg
Region
Free Product? (Y/N) _N If Yes, State
Greatest Thickness
INCIDENT DESCRIPTION
Incident Name: Circle K 2708383
Address: 873 Old Charlotte Road SW
County: Cabarrus
City/Town: Concord
Zip Code: 28262
Regional Office (circle one): Ashe ' e, Mooresville, etteville,
Raleigh, Washington, Wilmington, Wins on- a em
Latitude (decimal degrees): 35.4088 Longitude (decimal degrees) :-80.5795
Obtained by:
X❑GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)
❑Topographic map
❑GIs Address matching
❑Other
❑Unknown
Describe location:
Soil contamination discovered during closure of UST system. All tanks/piping/dispensers removed.
Soil laboratory analytical results within pit and line trench 5/22/19 indicated elevated TPH-GRO.
Over -excavation performed to top of rock 12-16 ft BGS, groundwater not observed.
Removed approximately 100-tons soil. Amount of release unknown, no free product observed.
No sensitive receptors identified.
UST Pit
HOW RELEASE WAS DISCOVERED (Release code)
(Check one)
❑Release Detection Equipment or Methods ❑Visual/Odor ❑Groundwater Contamination
®During UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination
❑Property Transfer ❑Water Supply Well Contamination ❑Other (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Tvpe of Release Product Type Released
(Check primary source) (Check primary cause) (Check one) (Check primary product type released)
® Tank ❑ Spill X❑ Petroleum X❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil
❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend
Heating Oil ❑ Vegetable Oil 100%
❑❑ Dispenser Corrosion Both
❑❑
❑ ❑
Other Petroleum E10 — E20Physical/Mechanical
❑ Submersible Turbine Pump ❑
Products
Damage Location ❑ E21 — E84
❑ Delivery Problem (Check one) Metals
❑
❑ Install Problem ❑ E85 — E99
❑ Spill Bucket ❑ Other Inorganics
❑ Other X❑Facility ❑Ethanol 100%
❑ Other ❑ Other Organics
X❑ Unknown ❑Residence ❑ E01 — E09
El Unknown
❑Other
Definitions presented on reverse
Definitions presented on reverse
Ownership
1. Municipal 2. Military 3. Unkno 4. Private 5. deral 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial [ Commercial . Mining
UST Form 61 (02/19) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Circle K Stores, Inc.
Point of Contact
Address
Debrah Carl
2550 West Tyvola Road, Suite 200
City Charlotte
State
Zip Code
Telephone Number
NC
28217
704-583-5762
I
UST SYSTEM OPERATOR I
UST Operator/Company
Address
Circle K Stores, Inc.
2550 West Tyvola Road, Suite 200
City Charlotte
State
Zip Code
Telephone Number
NC
28217
704-583-5700
LANDOWNER AT LOCATION OF UST INCIDENT I
Landowner
Address
Hickory Woods, Inc.
PO Box 526
City
State
Zip Code
Telephone Number
Concord
NC
28026
N/A
I
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Aaron Williamson
Company Crawford Environmental Services, Inc.
Telephone Number704-909-2911
Title Project Manager
Address 301 McCullough Drive, Suite 400, Charlotte, NC 28262
Date 5/23/19
UST Form 61 (02/19)
Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

'",q Body Shopwe
.0ad outhwes `yRps
kv •r �
6
oo le
•S: .,tit,. It - L