21007_Hoke Street _BAR_20180531

Aptus Management, PLLC
Environmental Management Solutions

Aptus Management, PLLC 109 Amber Court Carrboro, NC 27510
May 31, 2018 Sarah Hardison Young VIA EMAIL: [e-mail] Brownfields Project Manager NC Division of Waste Management
217 W Jones St. Raleigh, NC 27603-6100 SUBJECT: SURFICIAL SOIL TESTING REPORT PASSAGE HOME SITE – RALEIGH, NORTH CAROLINA BROWNFIELDS PROJECT NUMBER: 21007-17-092
Dear Ms. Young: Provided below is a summary of the surficial soil testing conducted at the Passage Home site in Raleigh. As indicated, we found no contamination by VOCs, SVOCs, RCRA metals, herbicides or pesticides which would pose an unacceptable risk, or which were measured above the IHSB Preliminary Soil Remediation Goals (PSRGs)1. BACKGROUND INFORMATION The intent of this assessment was to evaluate surficial soil conditions to allow urban gardening
consisting of a green house, urban ag building and a series of hoop houses. Gardening or produce production would not occur in native soil – instead it will be done in raised planting beds.
The sampling focused on the 0.8-acre central portion of the 1412 Garner Road parcel (No. 1703920658) where the urban gardening will occur, and the 0.54-acre lot with street address 506 Hoke Street (No. 1703920846) located to the north of the gardening area that will be used to enter
and exit the gardening area. The western third of the 1412 Garner Road parcel will be improved with a parking lot and the eastern third will, for the time being, remain vacant – so no soil sampling was conducted at this time in these areas. The earlier Phase II assessment of the Hoke Street site (Limited Phase II ESA, PES, Nov. 1, 2016) showed no soil contamination at the western edge of the urban garden area (MW-3S, S-4, S-5 and S-6) near where we will construct the greenhouse and urban ag building. SAMPLING On March 27, 2018, Aptus collected ten (10) surficial soil samples, B-1 through B-10, as shown in
the attached figure over the 1.3-acre area. Two samples were collected where the greenhouse and urban ag building will be constructed, four were collected to the east where we will have raised planting beds, and four samples were collected from the 506 Hoke Street parcel, including where
containers of some type were noted in a 2005 aerial photo (Wake County iMaps) and where an area of possible vegetative stress (2010 iMaps) was noted – although this turned out to be a small concrete pad possibly used as a street light base. We also collected a background soil sample for
RCRA metals at an adjacent vacant lot to the northeast.

1 Background levels of arsenic were measured above the residential PSRG.

Soil Testing Report May 31, 2018 Passage Home Site - Raleigh, NC
Aptus Management, PLLC Page 2
Discrete soil samples were collected with a hand auger at the 0.5’ to 1’ interval for analysis of SVOCs by EPA Method 8270 and RCRA Metals by EPA Method 6010, and at the 1’ to 2’
interval for analysis of VOCs by EPA Method 8260. All samples were collected using a field-decontaminated hand auger. The upper six inches of
soil/gravel/vegetative roots from each auger boring location was removed and discarded. The SVOC and metals samples were collected from the auger bucket and placed directly into laboratory-provided glassware. Samples for VOC analysis were collected directly from the hand-
auger bucket using a laboratory-provided discrete VOC sampling device. There were no visual and olfactory observations indicating possible contamination.
Samples were packed on ice and shipped under proper chain-of-custody to Prism Laboratories in Charlotte, NC for analyses.
On May 18, 2018, follow-up sampling was conducted for herbicides and pesticides by EPA Methods 8115 and 8081, respectively. Aptus collected discrete samples from the same ten locations and prepared three (3) composites for analysis (B 1-4C, B 5,6,8C and B 7,9,10C). All
samples were collected using a field-decontaminated hand auger. The upper six inches of soil/gravel/vegetative roots from each auger boring location was removed and discarded. The samples were collected from the auger bucket, composited and placed directly into laboratory-provided glassware. RESULTS As summarized in Table 1, acetone, a common lab anomaly, was measured low levels in all samples. 1,1,1-Trichloroethane, tetrachloroethylene and trichloroethylene were measured at low concentrations below their respective PSRGs in one sample, B-8, collected from the southeastern portion of the site. RCRA metals, as expected, were detected in the soil samples.
Except for arsenic, all metals were below their respective IHSB PSRGs. Arsenic was measured above its residential PSRG (0.68 mg/kg) at concentrations ranging from 0.93 mg/kg to 5 mg/kg, which is within expected background levels. Two pesticides, beta-BHC and 4,4-DDD were
measured at low concentrations below their respective PSRGs. No SVOCs or herbicides were measured above the lab’s reporting limits, reported as BRL (below reporting limits).
Provided as attachments are the full laboratory reports and a summary of the data in Excel format is provided along with this report. If you have questions regarding this submittal or associated documentation, please feel free to contact me at [phone]. Sincerely, APTUS MANAGEMENT, PLLC
John Gallagher, PE Engineer of Record
Soil Testing Report May 31, 2018 Passage Home Site - Raleigh, NC
Aptus Management, PLLC Page 3

Attachments

Aptus Management, PLLC
SOIL SAMPLING LOCATIONS
Urban Garden Area
o o
ooo
o
o - Soil Sampling - 1412 Garner Rd
o
o
o o
o - Soil Sampling - 506 Hoke St
DisclaimeriMaps makes every effort to produce and publish the most current and accurate information possible.However, the maps are produced for information purposes,and are NOT surveys. No warranties, expressed or implied,are provided for the data therein, its use,or its interpretation.
Passage Home Soil Sampling 0 50 10025 ft
1 inch = 50 feet±

Aptus Management, PLLC
Soil Test Summary Table
B-1 B-2 B-3 B-4 B-5 B-6 B-7 B-8 B-9 B-10 Background
VOCs (mg/Kg)------
Acetone 12,000 140,000 25 0.028 0.057 0.047 0.085 0.046 0.045 0.025 0.030 0.032 0.039 NA
1,1,1-Trichloroethane 1,700 7,600 1.4 BRL BRL BRL BRL BRL BRL BRL 0.0022 BRL BRL NA
Tetrachloroethylene 17 82 0.063 BRL BRL BRL BRL BRL BRL BRL 0.015 BRL BRL NA
Trichloroethylene 0.87 4.0 0.021 BRL BRL BRL BRL BRL BRL BRL 0.011 BRL BRL NA
SVOCs (mg/Kg)------BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NA
RCRA Metals, Total (mg/Kg)------
Mercury 1.9 3.1 1.0 0.1 0.094 0.070 0.077 0.085 0.068 0.10 0.080 0.096 0.092 0.11
Arsenic 0.68 3.0 5.8 3.0 1.7 2.5 2.1 3.5 5.0 3.6 1.1 2.1 3.8 0.93
Barium 3,000 44,000 580 59 45 33 49 37 52 31 22 31 32 18
Cadmium 14 200 3.0 0.19 0.14 0.044 0.33 BRL BRL BRL 0.078 0.056 BRL BRL
Chromium 23,000 350,000 360,000 20 32 31 16 23 33 22 9.0 13 36 9.3
Lead 400 800 270 120 170 27 62 19 15 21 26 44 30 21
Selenium 78 1,200 2.1 0.82 0.77 1.3 1.3 0.74 1.1 0.93 0.49 0.47 0.96 0.53
Silver 78 1,200 3.4 0.038 0.044 0.029 0.044 0.037 0.024 BRL 0.026 0.025 BRL 0.025
Pesticides B 1-4C B 5, 6, 8C B 7, 9, 10C
beta-BHC 0.3 1.3 0.0023 0.0019 BRL BRL
4,4-DDD 0.38 4.9 0.47 BRL 0.0019 BRL
Herbicides ---------BRL BRL BRL
NOTES:* Preliminary Soil Remediation Goals (PSRG) per Inactive Hazardous Sites Branch
BRL - Below Laboratory Reporting Limit. See Laboratory Report
NA - Not AnalyzedBolded and Shaded concentrations exceed one or more IHSB PSRG health-based soil remediation goals
IHSB PSRG -
Residential *
(mg/kg)
IHSB PSRG -
Industrial*
(mg/kg)
IHSB PSRG Protection of
Groundwater*
(mg/kg)
Table 1Soil Sample Analytical Results
Hoke St Redevelopment SiteRaleigh, North Carolina
Constituent
Sample ID

Aptus Management, PLLC
Prism Lab Report
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This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
05/24/2018
Proctor Environmental Services, Inc.
Tom Proctor
5113 Yachtsman Ct.
Raleigh, NC 27615
Project: Hoke St Raleigh
Lab Submittal Date: 05/18/2018
Prism Work Order: 8050339
Method 8151analysis was subcontracted to Analytical Environmental Services. Laboratory report is
attached.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 19
Sample Receipt Summary
05/24/2018
Prism Work Order: 8050339
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
8050339-01 05/17/18B 1-4C 05/18/18Solid
8050339-02 05/17/18B 5-8C 05/18/18Solid
8050339-03 05/17/18B 7,9-10C 05/18/18Solid
Samples were received in good condition at 3.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 19
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8050339
05/24/2018
Summary of Detections
0.0019 J mg/kg dry8050339-01 B 1-4C beta-BHC 8081B
0.0019 J mg/kg dry8050339-02 B 5-8C 4,4’-DDD 8081B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 19
Laboratory Report
05/24/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Hoke St RaleighProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: B 1-4C
Prism Sample ID: 8050339-01
Prism Work Order: 8050339
Time Collected: 05/17/18 15:30
Time Submitted: 05/18/18 12:12
General Chemistry Parameters
89.2 *SM2540 G P8E046310.100 5/22/18 9:45 TJY% by
Weight
0.100% Solids
Organochlorine Pesticides by GC/ECD
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.000264,4’-DDD
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.000394,4’-DDE
BRL 8081B P8E042410.0034 5/23/18 16:21 JMVmg/kg dry 0.000924,4’-DDT
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00058Aldrin
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00066alpha-BHC
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00050cis-Chlordane
0.0019 8081B P8E042410.0022 5/23/18 16:21 JMVJmg/kg dry 0.00048beta-BHC
BRL 8081B P8E042410.056 5/22/18 18:23 JMVmg/kg dry 0.011Chlordane
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00036delta-BHC
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00035Dieldrin
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00041Endosulfan I
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00031Endosulfan II
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00026Endosulfan Sulfate
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00032Endrin
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00049Endrin Aldehyde
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00061Endrin Ketone
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00061gamma-BHC
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00046trans-Chlordane
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00056Heptachlor
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.00043Heptachlor Epoxide
BRL 8081B P8E042410.0022 5/23/18 16:21 JMVmg/kg dry 0.0012Methoxychlor
BRL 8081B P8E042410.056 5/23/18 16:21 JMVmg/kg dry 0.011Toxaphene
Surrogate Recovery Control Limits
26-20464 %Decachlorobiphenyl
40-16262 %Tetrachloro-m-xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 19
Laboratory Report
05/24/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Hoke St RaleighProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: B 5-8C
Prism Sample ID: 8050339-02
Prism Work Order: 8050339
Time Collected: 05/17/18 15:45
Time Submitted: 05/18/18 12:12
General Chemistry Parameters
83.0 *SM2540 G P8E046310.100 5/22/18 9:45 TJY% by
Weight
0.100% Solids
Organochlorine Pesticides by GC/ECD
0.0019 8081B P8E042410.0024 5/23/18 16:33 JMVJmg/kg dry 0.000284,4’-DDD
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.000424,4’-DDE
BRL 8081B P8E042410.0036 5/23/18 16:33 JMVmg/kg dry 0.000994,4’-DDT
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00062Aldrin
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00071alpha-BHC
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00054cis-Chlordane
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00052beta-BHC
BRL 8081B P8E042410.060 5/22/18 18:35 JMVmg/kg dry 0.012Chlordane
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00039delta-BHC
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00038Dieldrin
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00044Endosulfan I
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00033Endosulfan II
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00028Endosulfan Sulfate
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00034Endrin
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00053Endrin Aldehyde
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00065Endrin Ketone
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00066gamma-BHC
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00050trans-Chlordane
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00060Heptachlor
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.00046Heptachlor Epoxide
BRL 8081B P8E042410.0024 5/23/18 16:33 JMVmg/kg dry 0.0013Methoxychlor
BRL 8081B P8E042410.060 5/23/18 16:33 JMVmg/kg dry 0.012Toxaphene
Surrogate Recovery Control Limits
26-20458 %Decachlorobiphenyl
40-16257 %Tetrachloro-m-xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 19
Laboratory Report
05/24/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
5113 Yachtsman Ct.
Project: Hoke St RaleighProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Sample Matrix: Solid
Client Sample ID: B 7,9-10C
Prism Sample ID: 8050339-03
Prism Work Order: 8050339
Time Collected: 05/17/18 16:00
Time Submitted: 05/18/18 12:12
General Chemistry Parameters
80.3 *SM2540 G P8E046310.100 5/22/18 9:45 TJY% by
Weight
0.100% Solids
Organochlorine Pesticides by GC/ECD
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.000294,4’-DDD
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.000444,4’-DDE
BRL 8081B P8E042410.0037 5/23/18 16:45 JMVmg/kg dry 0.00104,4’-DDT
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00064Aldrin
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00073alpha-BHC
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00056cis-Chlordane
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00054beta-BHC
BRL 8081B P8E042410.062 5/22/18 18:46 JMVmg/kg dry 0.012Chlordane
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00040delta-BHC
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00039Dieldrin
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00046Endosulfan I
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00034Endosulfan II
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00029Endosulfan Sulfate
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00036Endrin
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00054Endrin Aldehyde
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00067Endrin Ketone
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00068gamma-BHC
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00051trans-Chlordane
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00062Heptachlor
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.00048Heptachlor Epoxide
BRL 8081B P8E042410.0025 5/23/18 16:45 JMVmg/kg dry 0.0014Methoxychlor
BRL 8081B P8E042410.062 5/23/18 16:45 JMVmg/kg dry 0.012Toxaphene
Surrogate Recovery Control Limits
26-20426 %Decachlorobiphenyl
40-16252 %Tetrachloro-m-xylene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 19
5/24/18
Level II QC Report
5113 Yachtsman Ct.
Project: Hoke St RaleighProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8050339
Time Submitted: 5/18/2018 12:12:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Organochlorine Pesticides by GC/ECD - Quality Control
Batch P8E0424 - 3546
Blank (P8E0424-BLK1)Prepared: 05/21/18 Analyzed: 05/23/18
4,4’-DDD mg/kg wetBRL0.0020
4,4’-DDE mg/kg wetBRL0.0020
4,4’-DDT mg/kg wetBRL0.0030
Aldrin mg/kg wetBRL0.0020
alpha-BHC mg/kg wetBRL0.0020
cis-Chlordane mg/kg wetBRL0.0020
beta-BHC mg/kg wetBRL0.0020
Chlordane mg/kg wetBRL0.050
delta-BHC mg/kg wetBRL0.0020
Dieldrin mg/kg wetBRL0.0020
Endosulfan I mg/kg wetBRL0.0020
Endosulfan II mg/kg wetBRL0.0020
Endosulfan Sulfate mg/kg wetBRL0.0020
Endrin mg/kg wetBRL0.0020
Endrin Aldehyde mg/kg wetBRL0.0020
Endrin Ketone mg/kg wetBRL0.0020
gamma-BHC mg/kg wetBRL0.0020
trans-Chlordane mg/kg wetBRL0.0020
Heptachlor mg/kg wetBRL0.0020
Heptachlor Epoxide mg/kg wetBRL0.0020
Methoxychlor mg/kg wetBRL0.0020
Toxaphene mg/kg wetBRL0.050
mg/kg wet 0.03333 26-204Surrogate: Decachlorobiphenyl 620.0207
mg/kg wet 0.03333 40-162Surrogate: Tetrachloro-m-xylene 720.0239
LCS (P8E0424-BS1)Prepared: 05/21/18 Analyzed: 05/23/18
4,4’-DDD mg/kg wet0.0255 0.0020 0.03333 56-13977
4,4’-DDE mg/kg wet0.0297 0.0020 0.03333 56-13489
4,4’-DDT mg/kg wet0.0260 0.0030 0.03333 50-14578
Aldrin mg/kg wet0.0301 0.0020 0.03333 45-13690
alpha-BHC mg/kg wet0.0328 0.0020 0.03333 45-13798
cis-Chlordane mg/kg wet0.0286 0.0020 0.03333 54-13386
beta-BHC mg/kg wet0.0298 0.0020 0.03333 50-13689
delta-BHC mg/kg wet0.0282 0.0020 0.03333 47-13984
Dieldrin mg/kg wet0.0288 0.0020 0.03333 56-13686
Endosulfan I mg/kg wet0.0267 0.0020 0.03333 53-13280
Endosulfan II mg/kg wet0.0270 0.0020 0.03333 53-13481
Endosulfan Sulfate mg/kg wet0.0270 0.0020 0.03333 55-13681
Endrin mg/kg wet0.0301 0.0020 0.03333 57-14090
Endrin Aldehyde mg/kg wet0.0291 0.0020 0.03333 35-13787
Endrin Ketone mg/kg wet0.0257 0.0020 0.03333 55-13677
gamma-BHC mg/kg wet0.0311 0.0020 0.03333 49-13593
trans-Chlordane mg/kg wet0.0275 0.0020 0.03333 53-13582
Heptachlor mg/kg wet0.0276 0.0020 0.03333 47-13683
Heptachlor Epoxide mg/kg wet0.0292 0.0020 0.03333 52-13688
Methoxychlor mg/kg wet0.0264 0.0020 0.03333 52-14379
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 19
5/24/18
Level II QC Report
5113 Yachtsman Ct.
Project: Hoke St RaleighProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8050339
Time Submitted: 5/18/2018 12:12:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Organochlorine Pesticides by GC/ECD - Quality Control
Batch P8E0424 - 3546
LCS (P8E0424-BS1)Prepared: 05/21/18 Analyzed: 05/23/18
mg/kg wet 0.03333 26-204Surrogate: Decachlorobiphenyl 630.0209
mg/kg wet 0.03333 40-162Surrogate: Tetrachloro-m-xylene 710.0235
LCS (P8E0424-BS2)Prepared: 05/21/18 Analyzed: 05/22/18
Chlordane mg/kg wet0.381 0.050 0.3333 43-149114
mg/kg wet 0.03333 26-204Surrogate: Decachlorobiphenyl 620.0207
mg/kg wet 0.03333 40-162Surrogate: Tetrachloro-m-xylene 720.0241
LCS (P8E0424-BS3)Prepared: 05/21/18 Analyzed: 05/23/18
Toxaphene mg/kg wet0.335 0.050 0.3333 33-141100
mg/kg wet 0.03333 26-204Surrogate: Decachlorobiphenyl 580.0193
mg/kg wet 0.03333 40-162Surrogate: Tetrachloro-m-xylene 670.0224
LCS Dup (P8E0424-BSD1)Prepared: 05/21/18 Analyzed: 05/23/18
4,4’-DDD mg/kg wet0.0293 0.0020 0.03333 2056-13988 14
4,4’-DDE mg/kg wet0.0331 0.0020 0.03333 2056-13499 11
4,4’-DDT mg/kg wet0.0313 0.0030 0.03333 2050-14594 18
Aldrin mg/kg wet0.0317 0.0020 0.03333 2045-13695 5
alpha-BHC mg/kg wet0.0342 0.0020 0.03333 2045-137103 4
cis-Chlordane mg/kg wet0.0308 0.0020 0.03333 2054-13392 7
beta-BHC mg/kg wet0.0303 0.0020 0.03333 2050-13691 2
delta-BHC mg/kg wet0.0291 0.0020 0.03333 2047-13987 3
Dieldrin mg/kg wet0.0318 0.0020 0.03333 2056-13695 10
Endosulfan I mg/kg wet0.0292 0.0020 0.03333 2053-13287 9
Endosulfan II mg/kg wet0.0284 0.0020 0.03333 2053-13485 5
Endosulfan Sulfate mg/kg wet0.0309 0.0020 0.03333 2055-13693 13
Endrin mg/kg wet0.0334 0.0020 0.03333 2057-140100 10
Endrin Aldehyde mg/kg wet0.0326 0.0020 0.03333 2035-13798 11
Endrin Ketone mg/kg wet0.0304 0.0020 0.03333 2055-13691 17
gamma-BHC mg/kg wet0.0324 0.0020 0.03333 2049-13597 4
trans-Chlordane mg/kg wet0.0289 0.0020 0.03333 2053-13587 5
Heptachlor mg/kg wet0.0302 0.0020 0.03333 2047-13691 9
Heptachlor Epoxide mg/kg wet0.0313 0.0020 0.03333 2052-13694 7
Methoxychlor mg/kg wet0.0331 0.0020 0.03333 20 D52-14399 22
mg/kg wet 0.03333 26-204Surrogate: Decachlorobiphenyl 800.0267
mg/kg wet 0.03333 40-162Surrogate: Tetrachloro-m-xylene 730.0242
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 19
5/24/18
Level II QC Report
5113 Yachtsman Ct.
Project: Hoke St RaleighProctor Environmental Services, Inc.
Raleigh, NC 27615
Attn: Tom Proctor
Prism Work Order: 8050339
Time Submitted: 5/18/2018 12:12:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P8E0463 - Solids, Dry Weight
Duplicate (P8E0463-DUP2)Prepared & Analyzed: 05/22/18 Source: 8050339-01
% Solids % by Weight89.9 0.100 89.2 200.9
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P8E04638050339-01 05/22/18 9:4530 30g g
P8E04638050339-02 05/22/18 9:4530 30g g
P8E04638050339-03 05/22/18 9:4530 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P8E04248050339-01 05/21/18 10:3030.05 10g mL
P8E04248050339-01 05/21/18 10:3030.05 10g mL
P8E04248050339-02 05/21/18 10:3030.02 10g mL
P8E04248050339-02 05/21/18 10:3030.02 10g mL
P8E04248050339-03 05/21/18 10:3030.08 10g mL
P8E04248050339-03 05/21/18 10:3030.08 10g mL
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Analysis
8050339-01 Herbicides (Sub)
8050339-02 Herbicides (Sub)
8050339-03 Herbicides (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 19
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May 23, 2018
LABORATORY REPORT NUMBER
PROJECT ID
Primary Data Review By
Project Manager, AES
1805L16
Terri W. Cole
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
8050339
Chris Pafford Project Manager, Access Analytical
[e-mail]
Ashley Amick
PLEASE NOTE:
-Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
-AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
-Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Secondary Data Review By
ATTENTION
DATE
CLIENT
ANALYTICAL REPORT
Page 1 of 8
Page 2 of 8
1805L16-001A
23-May-18Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Solid
5/17/2018 3:30:00 PM
B1-4C
Matrix:
Collection Date:
Client Sample ID:
8050339
Prism Laboratories
Lab ID:
Project Name:
AnalystMDL
Lab Order Tag Number:8050339-011805L16
(SW3550C)CHLORINATED HERBICIDES SW8151A
2,4,5-T BRL 37 ug/Kg-dry 261001 1 05/22/2018 14:39 UH6.7
2,4,5-TP (Silvex)BRL 37 ug/Kg-dry 261001 1 05/22/2018 14:39 UH6.1
2,4-D BRL 37 ug/Kg-dry 261001 1 05/22/2018 14:39 UH11
2,4-DB BRL 190 ug/Kg-dry 261001 1 05/22/2018 14:39 UH6.4
Dalapon BRL 370 ug/Kg-dry 261001 1 05/22/2018 14:39 UH6.3
Dicamba BRL 37 ug/Kg-dry 261001 1 05/22/2018 14:39 UH6.0
Dichlorprop BRL 37 ug/Kg-dry 261001 1 05/22/2018 14:39 UH7.8
Dinoseb BRL 95 ug/Kg-dry 261001 1 05/22/2018 14:39 UH59
MCPA BRL 3700 ug/Kg-dry 261001 1 05/22/2018 14:39 UH880
MCPP BRL 3700 ug/Kg-dry 261001 1 05/22/2018 14:39 UH2300
Surr: DCAA 70.2 44.3-132 %REC 261001 1 05/22/2018 14:39 UH0
PERCENT MOISTURE D2216
Percent Moisture 10.3 0 wt%R370856 1 05/21/2018 17:00 AK0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not Detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
Page 3 of 8
1805L16-002A
23-May-18Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Solid
5/17/2018 3:45:00 PM
B5-8C
Matrix:
Collection Date:
Client Sample ID:
8050339
Prism Laboratories
Lab ID:
Project Name:
AnalystMDL
Lab Order Tag Number:8050339-021805L16
(SW3550C)CHLORINATED HERBICIDES SW8151A
2,4,5-T BRL 40 ug/Kg-dry 261001 1 05/22/2018 15:43 UH7.3
2,4,5-TP (Silvex)BRL 40 ug/Kg-dry 261001 1 05/22/2018 15:43 UH6.7
2,4-D BRL 40 ug/Kg-dry 261001 1 05/22/2018 15:43 UH12
2,4-DB BRL 210 ug/Kg-dry 261001 1 05/22/2018 15:43 UH7.1
Dalapon BRL 400 ug/Kg-dry 261001 1 05/22/2018 15:43 UH6.9
Dicamba BRL 40 ug/Kg-dry 261001 1 05/22/2018 15:43 UH6.6
Dichlorprop BRL 40 ug/Kg-dry 261001 1 05/22/2018 15:43 UH8.6
Dinoseb BRL 100 ug/Kg-dry 261001 1 05/22/2018 15:43 UH65
MCPA BRL 4000 ug/Kg-dry 261001 1 05/22/2018 15:43 UH970
MCPP BRL 4000 ug/Kg-dry 261001 1 05/22/2018 15:43 UH2500
Surr: DCAA 78.3 44.3-132 %REC 261001 1 05/22/2018 15:43 UH0
PERCENT MOISTURE D2216
Percent Moisture 18.5 0 wt%R370856 1 05/21/2018 17:00 AK0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not Detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
Page 4 of 8
1805L16-003A
23-May-18Date:Analytical Environmental Services, Inc
Analyses Date AnalyzedDFBatchIDUnitsQualReporting
LimitResult
Client:
Solid
5/17/2018 4:00:00 PM
B7,9-10C
Matrix:
Collection Date:
Client Sample ID:
8050339
Prism Laboratories
Lab ID:
Project Name:
AnalystMDL
Lab Order Tag Number:8050339-031805L16
(SW3550C)CHLORINATED HERBICIDES SW8151A
2,4,5-T BRL 42 ug/Kg-dry 261001 1 05/22/2018 16:04 UH7.6
2,4,5-TP (Silvex)BRL 42 ug/Kg-dry 261001 1 05/22/2018 16:04 UH6.9
2,4-D BRL 42 ug/Kg-dry 261001 1 05/22/2018 16:04 UH12
2,4-DB BRL 220 ug/Kg-dry 261001 1 05/22/2018 16:04 UH7.3
Dalapon BRL 420 ug/Kg-dry 261001 1 05/22/2018 16:04 UH7.2
Dicamba BRL 42 ug/Kg-dry 261001 1 05/22/2018 16:04 UH6.8
Dichlorprop BRL 42 ug/Kg-dry 261001 1 05/22/2018 16:04 UH8.8
Dinoseb BRL 110 ug/Kg-dry 261001 1 05/22/2018 16:04 UH67
MCPA BRL 4200 ug/Kg-dry 261001 1 05/22/2018 16:04 UH1000
MCPP BRL 4200 ug/Kg-dry 261001 1 05/22/2018 16:04 UH2600
Surr: DCAA 89 44.3-132 %REC 261001 1 05/22/2018 16:04 UH0
PERCENT MOISTURE D2216
Percent Moisture 21.0 0 wt%R370856 1 05/21/2018 17:00 AK0
Qualifiers: * Value exceeds maximum contaminant level
BRL Not Detected at MDL
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
< Less than Result value
> Greater than Result value
J Estimated value detected below Reporting Limit
Page 5 of 8
SAMPLE/COOLERRECEIPTCHECKLIST1. ClientName:AESWorkOrderNumber:2.Carrier:FedExUPSUSPSClientCourierOtherYes No N/A DetailsComments3.Shippingcontainer/coolerreceivedingoodcondition?damagedleakingother4.Custodysealspresentonshippingcontainer?5.Custodysealsintactonshippingcontainer?6.Temperatureblankspresent?7.Coolertemperature(s)withinlimitsof0Ͳ6϶C?[Seeitem13 and 14fortemperature recordings.]Coolinginitiatedforrecentlycollectedsamples/icepresent8.ChainofCustody(COC)present?9.ChainofCustodysigned,dated,andtimedwhenrelinquishedandreceived?10.Samplernameand/orsignatureonCOC?11.Wereallsamplesreceivedwithinholdingtime?12.TATmarkedontheCOC?IfnoTATindicated,proceededwithstandardTATperTerms&Conditions.13.Cooler1Temperature϶CCooler2Temperature϶CCooler3Temperature϶CCooler4Temperature϶CCooler5Temperature϶CCooler6Temperature϶CCooler7Temperature϶CCooler8Temperature϶C15.Comments:IcertifythatIhavecompletedsections1Ͳ1ϱ(datedinitials).Yes No N/A DetailsComments16.Weresamplecontainersintactuponreceipt?17.Custodysealspresentonsamplecontainers?18.Custodysealsintactonsamplecontainers?19. DosamplecontainerlabelsmatchtheCOC?incompleteinfoillegiblenolabelother20.AreanalysesrequestedindicatedontheCOC?21. WereallofthesampleslistedontheCOCreceived?samplesreceivedbutnotlistedonCOCsampleslistedonCOCnotreceived22.Wasthesamplecollectiondate/timenoted?23.Didwereceivesufficientsamplevolumeforindicatedanalyses?24.Weresamplesreceivedinappropriatecontainers?25.WereVOAsamplesreceivedwithoutheadspace(<1/4"bubble)?26.Weretripblankssubmitted?listedonCOCnotlistedonCOC27.Comments:IcertifythatIhavecompletedsections1ϲͲ27(datedinitials).Yes No N/ADetailsComments28.Havecontainersneedingchemicalpreservationbeenchecked? *29.Containersmeetpreservationguidelines?30.WaspHadjusted at Sample Receipt?IcertifythatIhavecompletedsections28Ͳ30(datedinitials).ClearSave asAccess Analytical, Inc.1805L16■0.914.KR 5/19/18This section only applies to samples where pH can bechecked at Sample Receipt.KR 5/19/18* Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.KR 5/19/18Checklist 6.9.17 Rev 2LockedPage 6 of 8
23-May-18Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT8050339
1805L16
Prism Laboratories
261001
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:261001MBLK 05/22/2018CHLORINATED HERBICIDES SW8151A
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 05/21/2018 371045MB-261001
8228721
2,4,5-T 33BRL
2,4,5-TP (Silvex)33BRL
2,4-D 33BRL
2,4-DB 170BRL
Dalapon 330BRL
Dicamba 33BRL
Dichlorprop 33BRL
Dinoseb 85BRL
MCPA 3300BRL
MCPP 3300BRL
Surr: DCAA 0131.6 166.7 78.9 44.3 132
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:261001LCS 05/22/2018CHLORINATED HERBICIDES SW8151A
Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg 05/21/2018 371045LCS-261001
8228723
2,4,5-T 33144.9 166.7 86.9 51.4 125
2,4,5-TP (Silvex)33133.7 166.7 80.2 52.1 120
2,4-D 33143.4 166.7 86.0 41.9 124
Dicamba 33142.6 166.7 85.6 50.4 120
Dichlorprop 33139.0 166.7 83.4 50.6 121
Surr: DCAA 0131.2 166.7 78.7 44.3 132
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:261001MS 05/22/2018CHLORINATED HERBICIDES SW8151A
B1-4C Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg-dry 05/21/2018 3710451805L16-001AMS
8228733
2,4,5-T 37141.5 185.8 76.1 43 124
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 7 of 8
23-May-18Date:Analytical Environmental Services, Inc
Client:
BatchID:Workorder:
Project Name:ANALYTICAL QC SUMMARY REPORT8050339
1805L16
Prism Laboratories
261001
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:261001MS 05/22/2018CHLORINATED HERBICIDES SW8151A
B1-4C Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg-dry 05/21/2018 3710451805L16-001AMS
8228733
2,4,5-TP (Silvex)37139.7 185.8 75.2 49.3 121
2,4-D 37147.2 185.8 79.2 40.9 129
Dicamba 37144.4 185.8 77.7 47 128
Dichlorprop 37153.0 185.8 82.4 41.3 125
Surr: DCAA 0147.1 185.8 79.2 44.3 132
RPT Limit QualAnalyteResultSPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit
SampleType:BatchID:Analysis Date:Seq No:TestCode:261001MSD 05/22/2018CHLORINATED HERBICIDES SW8151A
B1-4C Units:Prep Date:Sample ID:Client ID:Run No:ug/Kg-dry 05/21/2018 3710451805L16-001AMSD
8228735
2,4,5-T 37134.9 32.1185.5 72.7 43 124 141.5 4.79
2,4,5-TP (Silvex)37133.2 30.9185.5 71.8 49.3 121 139.7 4.74
2,4-D 37148.1 39.4185.5 79.8 40.9 129 147.2 0.610
Dicamba 37143.8 28.7185.5 77.5 47 128 144.4 0.378
Dichlorprop 37149.4 52.5185.5 80.5 41.3 125 153.0 2.41
Surr: DCAA 0135.9 0185.5 73.3 44.3 132 147.1 0
Qualifiers:
J Estimated value detected below Reporting Limit
BRL Below reporting limit H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
< Less than Result value> Greater than Result value
R RPD outside limits due to matrix
Rpt Lim Reporting Limit
Page 8 of 8