HomeMy WebLinkAboutMO-9331_40792_CA_LSA_20190726_Limited Site AssessmentI 'AW-14
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Civil-Geotechnical-Surveying
July 26, 2019
Trudy Beverly, L.G.
Hydrogeologist
North Carolina Department of Environment and Natural Resources
601 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Re: Limited Site Assessment Transmittal Letter
Byrum Property
5628 Closeburn Road
Charlotte, Mecklenburg County, North Carolina 28210
UST Incident Number 40792
Dear Ms. Beverly:
On behalf of our client, Parkstone South, LLC, owner of the property at 5628 Closeburn
Road (former Byrum Property), Charlotte, North Carolina (Property), Concord
Engineering and Surveying, Inc. (CESI) is submitting the attached Limited Site
Assessment for your review.
CESI appreciates your assistance on this project. Should you have any questions, please
do not hesitate to contact me at (704) 795-1585.
Sincerely,
Az� �— e--,—
Steven E. Irminger, P.E.
Senior Engineer
45 Spring Street, SW P.O. Box 268 Concord, NC 28026-0268 704-786-5404
www.cesicgs.com NC License Number C-0263
Limited Site Assessment Report
A. Site Information
1. Site Identification
-Date of Report: July 26, 2019
Facility I.D.: Unknown UST Incident Number (if known): 40792
Site Name: Byrum Property (MO-9331)
Site Street Address: 5628 Closeburn Road
City/Town: Charlotte Zip Code: 28210 County: Mecklenburg
Description of Geographical Data Point (e.g., diesel fill port): Center of tank farm.
Location Method (GPS, topographical map, other): GIS Address matching
Latitude (decimal degrees): 35.149821 Longitude (decimal degrees):-80.845903
2. Information about Contacts Associated with the Leaking UST System
BUST Owner: Parkstone South, LLC
Address: Tel:704-701-9099
BUST Operator: N/A
Address: Tel
Property Owner: Parkstone South, LLC
Address: 568 Jetton Street, Suite 200; Davidson, NC 28036
'Property Occupant: None (Vacant lot)
Address: Tel
Consultant/Contractor: Concord Engineering and Surveying, Inc. (CESI)
Address: 46 Spring Street, Concord, NC 28026 Tel: (704) 701-9099
Analytical Laboratory: Pace Analytical, Inc. State Certification No. 37712
Address: 9800 Kincey Avenue, Huntersville, North Carolina Tel: (704) 875-9092
3. Information about Release
Date Discovered: January 22, 2018
Estimated Quantity of Release: Unknown
Cause of Release: Corrosion
Source of Release (Dispenser/Piping/UST): UST
Sizes and contents of UST system(s) from which the release occurred):
(1) 550 gallon UST
Approximately 67 gallons of heating oil was encountered in the tank and removed prior to
removal of the UST. The dates of operation are not known.
4. Certification (The title page must display the seal and signature of the certifying P.E. or
L.G. and the name and certification number of the company or corporation [See 15A NCAC
2L . 0103(e).])
I, Steven Irminger, a Professional Engineer, do certify that the information contained in this report is
correct and accurate to the best of my knowledge.
Steven E. Irminger, P.E. #21005 _` .'z ti9 SEAL =
021005 -
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 2
B. Site History and Characterization
1. Details regarding the ownership of the former UST is provided in Table B-2.
2. Details regarding information of the former UST are provided in Table B-1.
Based on our review of the available information, the property was undeveloped and
wooded land from at least 1940 until construction of a residential dwelling in 1955. On
January 22, 2018, Summit Engineering, Laboratory, Testing (Summit) advanced two soil
borings on either end of a heating oil UST at the property. The borings were conducted
to assess soil conditions in the vicinity of the tank prior to a sale of the property.
Analytical results of a soil sample from one end of the UST were reported with
concentrations exceeding the Maximum Soil Cleanup Concentrations (MSCCs) for
residential sites. Summit submitted form UST-61, on behalf of the owner, on April 22,
2018.
A Notice of Regulatory Requirements (NORR) was issued for this site by DEQ on
August 29, 2018. A copy of the NORR is attached in Appendix 1.
In February and March 2019, the building was razed. On March 22, 2019, a 550 gallon
heating oil UST was removed from the property. A closure assessment report for the
tank removed March 22, 2019, was completed by ECS Southeast, LLP (ECS) and
prepared in a report dated May 8, 2019. According to the ECS report, following removal
of the UST, a total of 314.35 tons of petroleum impacted soil was removed from the site
for treatment at Environmental Soil, Inc., of Shelby, North Carolina. In addition, 6,756
gallons of contact water was pumped from the excavation following heavy rain. The
contact water was removed for offsite disposal.
Analyses of confirmatory soil samples collected during the tank closure assessment
revealed that none of the parameters tested exceeded the MSCCs for residential sites.
Soil samples collected from the excavation bottom, east, and west walls, exceeded the
soil -to -groundwater MSCC for 1-Methylnaphthalene and Extractable Aromatic (C11-
C22) hydrocarbons. In addition, the sample collected from the bottom of the excavation
exceeded the Volatile Aromatic (C09-C10) hydrocarbons soil -to -groundwater MSCC.
Analysis of a groundwater sample collected during performance of this Limited Site
Assessment (LSA) reported dissolved naphthalene at a concentration of 1.0 ug/L and
total Chromium at a concentration of 6.3 ug/L. All other tested parameters were reported
to be below the sample detection limit.
A street atlas showing the property location is provided as Figure 1. The property
location on a portion of a USGS topographic map is provided as Figure 2.
3. Provide non -UST information:
a. The tank of this report was underground. No evidence of aboveground storage
tanks were observed or reported.
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 3
b. No spills have been reported for the facility other than the discovery January
22, 2018.
4. Provide a comprehensive description of the release, including date discovered,
cause and source (including tank identification number and contents), and the
relationship of historical UST releases, non -UST releases, and off -site releases
(indicate incident number) to contamination from current release.
The precise source and timing of contamination is not known. No historical UST
releases, non -UST releases, or off -site releases have been reported.
5. Provide a brief description of site characteristics (including status of facility (active
or inactive), land use of site and surrounding area, water supply, topography,
vegetation, surface water, wells, buildings, surface cover, soil type, depth to and
nature of bedrock, depth to groundwater, direction of groundwater flow, etc.)
Site Characteristics: The property is identified as Assessor Parcel Number (APN)
17125221 and is assigned the numerical street address 5628 Closeburn Road by
Mecklenburg County. The property is currently vacant land. The property location is
shown on a Street Atlas as Figure 1. A copy of the Mecklenburg County GIS
assessor information and tax card is included in Appendix 2.
Site Vicinity Characteristics: The property vicinity is residential. A site vicinity map
is provided as Figure 3.
DIRECTION
ADDRESS/OCCUPIED
TOPOGRAPHIC
BY/USE
POSITION RELATIVE
TO PROPERTY
North
5605, 5617, 5621, 5629, Closeburn
Up gradient
Road/ single family residences
East
5700 Closeburn Road/single family
Cross gradient
residence
West
5615 Glenkirk Road/single family
Up gradient
residence
South
5640, 5700, 5728 Glenkirk Road/single
Down gradient
family residence
Water Supply: The subject property and vicinity is provided water from the City of
Charlotte. No potable or irrigation wells were observed on the subject property or
nearby the property. Adjoining properties are provided potable water by municipal
water from a main located along Closeburn Road and Glenkirk Road.
Topographer CESI obtained a copy of the USGS 7.5-minute topographic map,
Charlotte, North Carolina Quadrangle, dated 1993. A copy of a portion of the
topographic map showing the property location is provided on Figure 2. The
elevation of the property is approximately 660 feet above mean sea level (msl). Based
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 4
upon the topographic contours observed on the USGS topographic contour map, the
property slope is generally downward toward the south.
Vegetation: The property surface cover is turf and wooded land along its southern
boundary.
Surface Water: A tributary of Sugar Creek flows along the southern boundary of the
Property.
Wells: No wells were observed at the property.
Buildings: The property is not improved with structures. The Property Layout is
shown as Figure 3.
Surface Cover: The majority of the property surface is covered by turf.
Soil Type: According to the USDA web -based soil survey of Mecklenburg County,
approximately 17 percent of the surficial soil at the property is comprised of Cecil -
Urban Land Complex. The Cecil series consists of very deep, well drained,
moderately permeable soils on ridges and side slopes of the Piedmont uplands. They
are deep to saprolite and very deep to bedrock. They formed in residuum weathered
from felsic, igneous and high-grade metamorphic rocks of the Piedmont uplands.
Slopes range from 0 to 25 percent. Depth to bedrock ranges from 6 to 10 feet or more.
Approximately 59 percent of the surficial soil at the Property is comprised of the
Enon Series. The Enon series consists of very deep, well drained, slowly permeable
soils on ridgetops and side slopes in the Piedmont. They have formed in residuum
weathered from mafic or intermediate igneous and high-grade metamorphic rocks
such as diorite, gabbro, diabase, or hornblende gneiss or schist. Slope ranges from 2
to 45 percent. The solum thickness ranges from 20 to 50 inches. Depth to bedrock is
more than 60 inches. Urban soil is material that has been manipulated or disturbed.
The urban soils typically consist of asphalt and concrete from construction sites.
Approximately 23 percent of the surficial soils at the Property are of the Helena soil
series. The Helena soil series is a very deep, moderately well -drained, with slow
permeability sandy loam, that is usually found on a four percent slop in a cultivated
field.
Depth to and Nature of Bedrock: According to the Geologic Map of North Carolina
1985, the property is located in the Piedmont Physiographic Province. The dominant
rocks in this region are composed mainly of metamorphic and igneous rocks ranging
in age from Precambrian to Paleozoic. Bedrock was not observed at the surface in
the vicinity of the Property. Onsite drilling encountered fine grained sand and silts to
approximately 12-feet below ground. Competent bedrock was encountered from 12
feet to 45-feet (the maximum depth penetrated) below grade.
Depth to groundwater: Drilling at the site revealed depth to water approximately 31-
feet below grade.
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 5
6. Summarize initial abatement actions, assessment activities, and corrective actions
performed to date and list all reports previously submitted.
A closure assessment report for the tank removed March 22, 2019, was completed by
ECS Southeast, LLP (ECS) and prepared in a report dated May 8, 2019.
According to the ECS report, following removal of the UST, a total of 314.35 tons of
petroleum impacted soil was removed from the site for treatment at Environmental
Soil, Inc., of Shelby, North Carolina. In addition, 6,756 gallons of contact water was
pumped from the excavation following heavy rain. The contact water was removed
for offsite disposal.
Analyses of confirmatory soil samples collected during the tank closure assessment
revealed that none of the parameters tested exceeded the Maximum Soil Cleanup
Concentrations (MSCCs) for residential sites. Soil samples collected from the
excavation bottom, east, and west walls, exceeded the soil -to -groundwater MSCC for
1-Methylnaphthalene and Extractable Aromatic (C 11-C22) hydrocarbons. In
addition, the sample collected from the bottom of the excavation exceeded the
Volatile Aromatic (C09-C10) hydrocarbons soil -to -groundwater MSCC. The
analytical results of soil samples collected during the tank closure are summarized in
Table B-3.
Analysis of a groundwater sample collected during the Limited Site Assessment
revealed naphthalene at a concentration of 1.0 micrograms per Liter (ug/L) and Total
Chromium at a concentration of 6.3 ug/L. The LSA sampling and analytical results
are discussed in Section G of this report.
C. Risk Characterization
Submit the following questionnaire in its entirety. Answer all questions completely. Attach
additional pages as needed to fully explain answers. Base answers/explanations on information
obtained (or updated from preceding reports) during the current investigation. Note: Source
area means point of release from a UST system.
Limited Site Assessment Risk Classification and Land Use Form
Part I — Groundwater/Surface WaterNapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non -drinking purposes?YES
2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release?YES O
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water,
filling swimming pools) located within 250 feet of the source area of the release? YES/i@)
4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there
no other source of water supply other than the groundwater)? YES9G
5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined
space or pose any other serious threat to public health, public safety or the environment? YE
6. Are there any other factors that would cause the release to pose an imminent danger to public health, pu is
safety, or the environment? YES/ �
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 6
If yes, describe.
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release?
E /NO
If YES, does the maximum groundwater contaminant concentration exceed the surface water quality
standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? YES®
8. Is the source area of the release located within a approved or planned wellhead protection area as defined in
42 USC 300h-7(e)? YES®
If yes, describe.
9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled "Geolog of
North Carolina" published by the Department in 1985 YES N
If YES, is the source area of the release located in an area in which there is recharge to an unconfined or
semi -confined deeper aquifer that is being used or may be used as a source of drinking water? YES®
If YES, describe.
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels
(see Table 9) established by the Department? YES(9
Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or temporary)?YES N&
Describe. _The property is being redeveloped for residential use
2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church,
nursing home, or other place of public assembly? YES T�
Describe.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial
(e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.
enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? YE
Describe.
4. Do children visit the property? E NO
Explain. Children and adults will visit the property once redevelopment is complete.
Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or
both)? YES/�T)
Explain.
The property is currently not provided with a fence or security system.
5. Do pavement, buildings, or other structures cap the contaminated soil? ENO
Describe.
Contaminated soil encountered during the tank closure was removed for offsite disposal in April 2019. A
total of 314.35 tons were removed. The parcel is currently being redeveloped for residential use. The
source area is within the footprint of the proposed building and driveway.
6. What is the zoning status of the property? The property is currently zoned Residential (R-3).
7. Is the use of the property likely to change in the next 20 years? YES/0
Explain. The use is unlikely to change.
Limited Site Assessment July 26, 2019
5628 Closeburn Road, Charlotte, NC Page No. 7
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release
(excludes property containing source area of the release):
1. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)? A permanent residence will be placed
above the former storage tank location.
2. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home or other
place of public assembly? The Ivey Memory Wellness Day Center is located 250 feet
east of the source area.
3. What is the zoning status of properties in the surrounding area? The site and adjoining
areas are zoned Residential (R-3). The land use of neighboring properties is summarized
in Table B-10 and shown in Figure 9.
4. Briefly characterize the use and activities of the land in the surrounding area. The
properties surrounding the Property are primarily residential.
D. Receptor Information
Determine and describe all potential receptors, including those in the categories listed below.
Compile this information in a table entitled Public and Private Water Supply Well and Other
Receptor Information (Complete Table B-5 from the Guidelines, Appendix B.) in which an
identification code is assigned to each potential receptor. Indicate the locations of each
potential receptor, using the identification code, on a potential receptor map. Use information
from all available sources and from site investigations.
An unnamed tributary of Sugar Creek borders the property to the south. The Ivey Memory wellness
Day Center is located 460 feet east of the source area.
1. Water Supply Wells
Determine and describe the location, use, and ownership of public and private water
supply wells in the area within 1,500 feet of the source of the release. Compile this
information in Table B-5 and indicate the well locations on the potential receptor map.
Note whether well users are also served by a municipal water supply. Refer to the
instructions for a water supply well survey in Section 2.3 of the Guidelines.
Properties within 500-feet of the release were walked. Properties between 500 and 1,500 feet
from the site were observed from the public road. No water supply wells were observed
within 1,500 feet of the release. All of the adjoining properties appear to be connected to the
municipal water supply. The adjoining properties are numbered on the Sensitive Receptor
Map (Figure 4). The key to the numbered locations is provided in Table B-5.
2. Public Water Supplies
Determine the existence and availability of public water supplies within 1,500 feet of the
source area of the release. Compile this information in Table B-5 and indicate the
locations of the nearest public water lines and the source(s) of the public water supply on
the potential receptor map.
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 8
The City of Charlotte receives drinking water from the Catawba River and Lake Norman
which are in excess of five miles from the Property.
A water main is located along Closeburn Road which borders the property.
3. Surface Water
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) located within 1,500
feet of the source area of the release and indicate distance from source of release in Table
B-5 and indicate locations on the potential receptor map.
The distance to surface water is summarized on Table B-5 and shown on the potential
receptor map (Figure 7).
4. Wellhead Protection Areas
Indicate whether or not the UST release source area is located within an approved
wellhead protection area. Refer to Section 2.3 of the Guidelines for instructions on how to
access the list of currently approved wellhead protection plans and generate a map of UST
and wellhead protection area locations. List any identified wellhead protection area in
Table B-5 by PWS ID number and PWS system name and show the wellhead protection
area on the potential receptor map. To document performance of the wellhead protection
area investigation append to the potential receptor map a copy of the map generated using
ArcIMS Viewer to show 1) the UST location, 2) the wellhead protection area, and 3)
community wells.
The area of the UST release is not located within a wellhead protection area.
5. Deep Aquifers in the Coastal Plain Physiographic Re, -ion
Indicate if the source area of the release is located in an area in which there is recharge to
an unconfined or semi -confined deeper aquifer and indicate if that aquifer is being used
or may be used as a source of drinking water, referring to Section 2.3 of the Guidelines.
Based on a review of scientific literature on the regional hydrogeology and well
construction records and lithologic logs for deeper wells in the area, identify and describe
the deep aquifers underlying the release. Include information on the depth of the deep
aquifer in relation to the surficial saturated zone, the lithology and hydraulic conductivity
of the strata between the surficial aquifer and the deeper aquifer, and the difference in
groundwater head between the surficial aquifer and the deeper aquifer. Discuss the local
and regional usage of the deep aquifer and the draw down from major pumping
influences. Also, specify the distance from the source area of the release to major
discharge areas, such as streams and rivers. Cite all sources and references used for this
discussion.
NOTE: This requirement only pertains to releases in the Coastal Plain physiographic
region as designated on a map entitled "Geology of North Carolina" published by the
Department in 1985. This map can be obtained for a fee from the North Carolina Geologic
Survey,1612 MSC, Raleigh, NC 27699-1612.
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 9
Groundwater in the vicinity of the release is not used as a municipal source of potable water.
6. Subsurface Structures
Describe subsurface features, including sewers, utility lines, conduits, basements, vaults,
septic tanks, drainfields, etc., referring to Section 2.3 of the Guidelines. Compile this
information in Table B-5 and indicate the locations on the potential receptor map.
Discuss the risk of explosion due to the accumulation of vapors in confined space and
the threat to public health, public safety or the environment posed by vapors in the
subsurface features.
No basements were observed on the property or adjoining properties. Underground utilities
are located along Spring Street. Based on the lack of free product observed at the site, the
risk of an explosion hazard at this site is considered low.
E. Land Use
1. Property Owners and Occupants
Determine the names and addresses of property owners and occupants within or
contiguous to the area containing contamination and all property owners and occupants
within or contiguous to the area where the contamination is expected to migrate. Compile
this information in Table B-6 from the Guidelines, Appendix B, and indicate the property
locations on the land use map.
Please refer to Table B-6 and Figure 7.
2. Sensitive Land Use Features
List features sensitive to impact from the release (schools, daycare centers, nursing homes,
hospitals, playgrounds, parks and recreation areas, churches, camps and other places of
assembly) and show the zoning status of the area within 1500' of the source of the release
Compile this information in Table B-10 from the Guidelines, Appendix B, and indicate the
feature locations on the land use map.
Sensitive receptors were identified within 1,500 feet of the property and are listed in Table B-
10. The approximate locations of the sensitive receptors are shown on Figure 5.
F. Site Geology and Hydrogeology
Describe the soil and geology encountered at the site. Discuss the effects of soil and geological
characteristics on the migration and attenuation of contaminants. Include information
obtained during assessment activities (e.g., lithologic descriptions made during drilling, probe
surveys, tank closure, etc). If a Phase II investigation is required include a discussion of
groundwater flow direction and hydraulic gradient (vertical and horizontal).
The site is underlain by Saprolite consisting of an orange and red sequence of silts and sands
from approximately grade to 12 feet below grade. Crystalline bedrock is present from
approximately 12 feet below grade to the maximum depth penetrated of 45 feet below grade.
Limited Site Assessment
5628 Closeburn Road, Charlotte, NC
July 26, 2019
Page No. 10
G. Sampling Results
Phase IInvestigation
Responsible parties must perform a Phase I investigation for all releases.
A Phase I investigation includes the installation of one monitoring well in the source area of a
release. Soil samples are to be collected every five feet in the unsaturated zone and should be
analyzed in accordance with the methods specified in Table S of the Guidelines, Analytical
Methods for Petroleum Contaminated Soil. If the water table is encountered at 25 feet or
greater from the land surface, samples for laboratory analysis should be collected every 10 feet
in the unsaturated zone.
On May 30, 2019, CESI supervised the installation of one monitoring well in the location of the
former UST. The boring of the well was conducted by South Atlantic Environmental Drilling
and Construction Company (SAEDACCO) of Fort Mill, South Carolina. The boring of well
MW-1 was advanced in the middle of the former excavation. The boring was advanced using the
hollow stem auger drilling method. The approximate location of the boring is shown on a layout
of the property as Figure 4. The first 12-feet of drilling encountered clean imported soil which
had been backfilled to the excavation conducted by ECS in May 2019. During the drilling, a 2-
foot long, washed, stainless steel spoon was advanced at five-foot intervals. An undisturbed core
was retrieved from each of the spoons for observation and field screening by CESI personnel.
The boring encountered orange silty sand and fine grained fill from grade to approximately 11-
feet below grade. Auger refusal was encountered at 12-feet below grade and no returns were
retrieved in the split spoon sampler. CESI directed SAEDACCO switch to air rotary drilling to
continue the boring to a depth of 45-feet below grade. No undisturbed soil samples were
retrieved during drilling through the rock. For this reason, no soil samples were collected.
Suspect minor fractures were observed at approximately 36-feet and 43-feet below grade. No
water was indicated during drilling or immediately following drilling. CESI instructed
SAEDACCO to install a temporary well consisting of 2-inch diameter PVC. The well was
constructed with 15-feet of 0.010-inch machine slotted PVC. A Number 2 filter sand was placed
around the screen from the bottom of the well to two -feet above the top of the screen. The well
head was covered with plastic and allowed to rest for two days. CESI returned to the site on
June 3, 2019, and measured water in the well at a depth of approximately 31-feet from grade.
Following purge of the well, CESI personnel collected a water sample intro laboratory provided
sample jars. The water samples were immediately placed on ice. The samples were transported
using chain -of -custody protocol to Pace Analytical, Inc. (Pace) of Huntersville, North Carolina.
CESI requested that the samples be analyzed for Volatile Organic Compounds (VOCs) by EPA
Method 8260, Semi-VOCs (SVOCs) by EPA Method 625, and Massachusetts Department of
Environmental Protection (MADEP) Volatile Petroleum Hydrocarbons (VPH) and Extractable
Petroleum Hydrocarbons (EPH), and Total Chromium and Lead. A summary of the analytical
results is provided in Table B-4. Copies of laboratory reports and chain of custody records are
provided in Appendix 5.
Limited Site Assessment July 26, 2019
5628 Closeburn Road, Charlotte, NC Page No. 11
Phase II Investigation (if required)
A Phase H investigation should only be conducted if the release is from a high risk
commercial UST and the levels of groundwater contamination detected in the source area
monitoring well exceed the groundwater standards or interim standards by a factor of 10.
Based on the analytical results, a Phase II investigation is not required.
H. Conclusions and Recommendations
Discuss the risk criteria that apply to the release and identify any other site -specific factors
related to the release that may pose a risk to human health and the environment. Also, discuss
any site -specific conditions or possible actions that could result in lowering the level of risk
posed by the release.
The reported concentration of dissolved naphthalene (1.0 ug/L) and Chromium (6.3 ug/L), in the
water sample collected from well MW-1 do not exceed the North Carolina Groundwater Quality
2L Standards. Based on the lack of dissolved parameters exceeding the 2L standards and the
lack of adsorbed parameters exceeding the residential use MSCC, No Further Action is
recommended.
As this site is in the process of being redeveloped and a pending real estate transaction, CESI, on
behalf of our client would appreciate a speedy review and return letter approving No Further
Action for this incident.
I. Free Product Investigation and Recovery (if applicable)
No free product was observed at the site.
LIST OF FIGURES
FIGURE 1 Street Atlas
FIGURE 2 Topographic Location Map
FIGURE 3 Site Vicinity Map
FIGURE 4 Site Layout
FIGURE 5 Sensitive Receptor Map
FIGURE 6 Adjoining Property Key
FIGURE 7 Land Use Map
LIST OF TABLES
B-1
Site History — UST/AST Information
B-2
Site History — Owner/Operator Information
B-3
Soil Sample Analytical Results
B-4
Groundwater Sample Analytical Results
B-5
Receptor Information
B-6
Adjoining Parcel Ownership
B-7
Well Construction Information
Limited Site Assessment July 26, 2019
5628 Closeburn Road, Charlotte, NC Page No. 12
B-8 NOT USED
B-9 Groundwater Elevations
B-10 Land Use
LIST OF APPENDICES
APPENDIX 1 DEQ Correspondence
APPENDIX 2 Deed and GIS Information
APPENDIX 3 Soil and Groundwater Laboratory Report and Chain -of -Custody Record
FIGURES
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Site Name: Byrum Property
CONCORD ENGINEERING 5628 Closeburn Rd
AND SURVEYING, INC. Charlotte, North Carolina 28210
Project Number: 180453.000
Subject Property
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Site Name: Byrum Property
CONCORD ENGINEERING 5628 Closeburn Rd
AND SURVEYING, INC. Charlotte, North Carolina 28210
Project Number: 180453.000
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Subject Property
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FIGURE 3 SITE VICINITY Not to Scale N T
Site Name: Byrum Property
CONCORD ENGINEERING 5628 Closeburn Rd
AND SURVEYING, INC. Charlotte, North Carolina 28210
Project Number: 180453.000
Subject Property
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FIGURE 4 SITE LAYOUT Not to Scale N T
Site Name: Byrum Property
CONCORD ENGINEERING 5628 Closeburn Rd
AND SURVEYING, INC. Charlotte, North Carolina 28210
Project Number: 180453.000
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FIGURE 5 SENSITIVE Not to Scale N t
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Site Name: Byrum Property
CONCORD ENGINEERING 5628 Closeburn Rd
AND SURVEYING, INC. Charlotte, North Carolina 28210
Project Number: 180453.000
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Site Name: Byrum Property
CONCORD ENGINEERING 5628 Closeburn Rd
AND SURVEYING, INC. Charlotte, North Carolina 28210
Project Number: 180453.000
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Site Name: Byrum Property
CONCORD ENGINEERING 5628 Closeburn Rd
AND SURVEYING, INC. Charlotte, North Carolina 28210
Project Number: 180453.000
TABLES
Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
S stem?
1
Heating oil
None
550
Single wall
4' diameter
Single wall
1955
Removed
Yes
steel
6' long
steel
2019
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
FIncident
Material
Date of
Description of Release
Number
Released
Release
40792
Heating oil
1/22/18
Soil impacted with heating oil was reported in a boring advanced alongside the heating oil
UST as part of a due diligence assessment.
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
* * * Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)
Change 2
Appendix B
Reporting Tables
Table B-2: Site History - UST/AST Owner/Operator and Other Responsible Party Information
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property
UST ID Number
1
Facility ID Number
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/yy)
Parkstone South LLC
Current DID NOT OPERATE UST
Street Address
568 Jetton Street, Suite 200
City
State
Zip
Telephone Number
Davidson
NC
28036
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
Street Address
City
State
Zip
lephone Number
Incident Number
Name of Other Responsible Party
Dates of Release(s)
mm/dd/ to mm/dd/
Byrum Land & Timber Inc. (Prior owner)
January 22, 2018
Street Address
P.O. Box 11795
City
State
Zip
Telephone Number
Charlotte
NC
128220
Add additional records for all owners, operators and responsible parties as necessary.
Change 2
Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results (FROM CLOSURE REPORT)
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property Facility ID#:
Analytical Method (e.g., VOC by EPA 8260)
�
8270D
8270D
8270D
8270D
8270D
8260B
8260B
82608
8260B
8260B
Contaminant of Concern 4
.y
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
p
p
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
I)
LSA,
o
4
etc.)
4-
Excavat
0.191
B-1
03/22/19
ion
10
Closure
0.28J
0.181
0.48
<0.37
0.0035j
0.0073
0.0089
0.028J
0.0024
bottom
J
North
<0.39
<0.39
<0.39
<0.39
<0.39
<0.005
<0.005
<0.005
<0.051
<0.005
N-1
03/22/19
wall
8
Closure
1
1
I
1
East
0.55
E-1
03/22/19
wall
8
Closure
1.2
0.35J
0.93
0.111
0.012
0.034
0.027
<0.060
0.0060
West
0.34J
<0.005
0.0033
0.0044
<0.005
<0.005
W 1
03/22/19
wall
8
Closure
0.87
0.28J
0.80
0.101
2
J
J
2
2
Minimum Reporting Limit (mg/kg)
0.39
0.39
0.39
0.39
0.39
0.0051
0.0051
0.0051
0.051
0.0051
Soil to groundwater MSCC (mg/kg)
0.004
3.6
47
56
270
8.5
8.3
0.12
24
1.7
Residential MSCC (mg/kg)
20
63
620
469
469
782
782
100
14000
1564
Industrial/Commercial MSCC (mg/kg)
100
1635
16400
12264
12264
20440
20440
4000
360000
40880
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2
Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results (FROM CLOSURE REPORT)
Revision Date: 12/19/2017 Incident Number and Name: Campus Gas Station Facility ID#:
Analytical Method (e.g., VOC by EPA 8260)
�
8260B
8260B
8260B
8260B
8260B
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
N
Z
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
Y
1)
LSA,71
a
°
a
etc.)
Z
a1
rn
F�
Excavat
B-1
03/22/19
ion
10
Closure
0.033
0.013
<0.005
0.025J
0.0027
bottom
6
J
North
0.0028
<0.005
<0.005
<0.005
<0.005
N-1
03/22/19
wall
8
Closure
J
1
1
1
1
East
0.073
0.038
0.0036
E-1
03/22/19
wall
8
Closure
0.0076
0.039
J
West
0.0047
<0.005
<0.005
W-1
03/22/19
wall
8
Closure
0.020
J
2
0.0077
2
Minimum Reporting Limit (mg/kg)
0.0051
0.0051
0.0051
0.0051
0.0051
Soil to groundwater MSCC (mg/kg)
0.16
4.3
1.7
3.3
3.4
Residential MSCC (mg/kg)
313
626
626
626
626
Industrial/Commercial MSCC (mg/kg)
8176
16350
16350
16350
16350
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2
Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results (FROM CLOSURE REPORT)
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property Facility ID#:
Analytical Method (e.g., VOC by EPA 8260)
8270D
8270D
8270D
8270D
8270D
8260B
8260B
8260B
8260B
8260B
Contaminant of Concern 4
y
y
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
Q
p
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
20Day,
1
LSA,
4
o
0
0
etc.
C—'�
-
o
South
<0.40
<0.40
<0.40
<0.40
<0.40
<0.006
<0.006
<0.006
<0.063
<0.006
S-1
03/22/19
wall
8
Closure
3
3
3
3
Minimum Reporting Limit (mg/kg)
0.39
0.39
0.39
0.39
0.39
0.0051
0.0051
0.0051
0.051
0.0051
Soil to groundwater MSCC (mg/kg)
0.004
3.6
47
56
270
8.5
8.3
0.12
24
1.7
Residential MSCC (mg/kg)
20
63
620
469
469
782
782
100
14000
1564
Industrial/Commercial MSCC (mg/kg)
100
1635
16400
12264
1 12264
1 20440
1 20440
1 4000
1 360000
40880
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2
Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results (FROM CLOSURE REPORT)
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property Facility ID#:
Analytical Method (e.g., VOC by EPA 8260)
�
8260B
8260B
8260B
8260B
8260B
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Q
Tank pit
20Day,
y
1)
LSA,
P�
etc.
F�
South
<0.006
<0.006
<0.006
<0.006
<0.006
S-1
03/22/19
wall
8
Closure
3
3
3
3
3
Minimum Reporting Limit (mg/kg)
0.0051
0.0051
0.0051
0.0051
0.0051
Soil to groundwater MSCC (mg/kg)
0.16
4.3
1.7
3.3
3.4
Residential MSCC (mg/kg)
313
626
626
626
626
Industrial/Commercial MSCC (mg/kg)
8176
16350
16350
16350
16350
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2
Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results (FROM CLOSURE REPORT)
Revision Date: 12/19/2017 Incident Number and Name: Campus Gas Station Facility ID#:
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
o,
U
a
o,
U
a
N
U
a
o
U
U
a
U
U
a
o
U
U
a
Sample
ID
Date
Collected
(m/dd/yy)
Source
Area
(eg.
Tank pit
1)
Sample
Depth
(ft BGS)
Incident
Phase
(Closure
, 20Day,
LSA,
etc.
S-1
03/22/19
South
wall
8
Closure
<30
<30
<12
<22
<22
<22
Minimum Reporting Limit (mg/kg)
29
29
11
20
19
19
Soil to groundwater MSCC (mg/kg)
540
31
68
540
31
Residential MSCC (mg/kg)
1500
31000
469
939
1500
469
Industrial/Commercial MSCC (mg/kg)
40000
810000
12264
24528
40000
12264
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2
Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results (FROM CLOSURE REPORT)
Revision Date: 12/19/2017 Incident Number and Name: Campus Gas Station Facility ID#:
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
N
o
o
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
U
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
o,
o,
Tank pit
, 20Day,
U
U
U
U
U
U
1)
LSA,
a
a
a
a
a
a
etc.
Excavat
B-1
03/22/19
ion
10
Closure
270
70
200
<20
36
36
bottom
North
<29
<29
<11
<19
<19
N-1
03/22/19
wall
8
Closure
<19
East
160
50
E-1
03/22/19
wall
8
Closure
140
<20
43
21
West
W-1
03/22/19
wall
8
Closure
220
75
170
<20
17J
9.81
Minimum Reporting Limit (mg/kg)
29
29
11
20
19
19
Soil to groundwater MSCC (mg/kg)
540
31
68
540
31
Residential MSCC (mg/kg)
1500
31000
469
939
1500
469
Industrial/Commercial MSCC (mg/kg)
40000
810000
12264
24528
40000
12264
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2
Appendix B
Reporting Tables
Table B-4: Summary of Groundwater and Surface Water Sampling Results
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property Facility ID#:
Analytical Method (e.g., VOC by SM600013) or
EPA
Field Measurement (FM)->
8260n
6oioD
Contaminant of Concern/ Field Measurement4
Well or
Date
Sample
Incident
,
SW ID
Collected
ID
Phase
(Closure,
y
2013ay,
o
LSA, etc.
HU
MW-1
06/03/2019
Water
LSA
1.0
6.3
Minimum Reporting Limit (ug/1)
1.0
5.0
2L Standard (ug/1)
6
10
GCL (ug/1)
6000
10000
NC 2B Standard or EPA National Criteria
(ug/1)
Field measurement parameters include temperature, pH, dissolved oxygen, specific conductivity, Eh, and alkalinity
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
Results for contaminants must be reported in ug/l
µg/1=micrograms per liter GCL = gross contamination level Yellow shading indicates exceedance of NCAC 2L. Red
shading indicates exceedance of GCL
Change 2
Appendix B
Reporting Tables
Table B-5: Public and Private Water Supply Well and Other Receptor Information
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property
Public and Private Water Supply Wells
Facility ID#:
Latitude/
Distance
Longitude *
Well
Well
Well
from
Well Owner/ User
(decimal
Well
Depth
Type
Casing
Screen
source
s. a
o
Well #
(indicate which)
Address
Phone Number
degrees)
Use
(ft
of
Depth (ft.
Interval
area of
p �
BGS)
Well
BGS)
`x to y ft.
release
**
BGS)
(ft.)
Other Receptors
(Other public water supplies reservoirs, supply lines surface water bodies, wellhead protection areas recharge areas for deep aquifers subsurface structures)
Latitude/ Longitude of
Up or
Distance from
Receptor
Description
Location
*
any significant point(s)
Contact
Phone
Usage
down-
source area of
ID
(describe to left)
Number
(decimal degrees)
gradient
release (ft.)
1
Stream (in pipe)
South of release
35.149089/-80.845363
None
Down
205
2
Park Road Park
West of release
35.174884/-80.848570
Puab is
Cross
1150
pk
3
Lake
West of release
35.149427/-80.849556
None
Cross
1186
4
Ivey Memory Day
East of Release
35.149656/-80.843813
704-909-
Senior
Cross
380
Center
2070
Center
35.150122/-80.843016
Assiste
5
Brighton Gardens
Northeast of Release
704-643-
d
Up
649
1400
Living
* The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells or replication of sampling points.
** Ft BGS = feet below ground surface
10 Change 2
Appendix B
Reporting Tables
Table B-6: Property Owners/ Occupants
Revision Date: 7/26/2019 Incident Number and Name: 40792 Byrum Property Facility ID#:
Tax Parcel
Owner/ Occupant Name
Number/
Address
(Last, First MI)
Map ID
Cooper, Donnell and Karen B
17125222 /1
5615 Glenkirk Road, Charlotte, NC 28210
Copper Builders LLC
17125207 /2
1235 E Blvd Unit 155, Charlotte, NC 28203
Marrongelie, Kevin
17125155/3
5617 Closeburn Road, Charlotte, NC 28210
Bramley, Thomas J
17125156/4
5621 Closeburn Road, Charlotte, NC 28210
Travis, Van B
17125113 /5
5629 Closeburn Road, Charlotte, NC 28210
Lippard, John B
17125219 /6
5700 Closeburn Road, Charlotte, NC 28210
Green, Ned F
17125226 /7
5728 Glenkirk Road, Charlotte, NC 28210
Borachok, Gregg
17125227 /8
5700 Glenkirk Road, Charlotte, NC 28210
Sass, Daniel A
17125228 /9
5460 Glenkirk Road, Charlotte, NC 28210
Anderson, William M
17125229 /10
5634 Glenkirk Road, Charlotte, NC 28210
11 Change 2
Appendix B
Reporting Tables
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property Facility ID#:
Well
ID
Date
Installed
(m/dd/yy)
Date
Water
Level
Measured
(m/dd/yy)
Well
Casing
Diameter
(in.)
Well
Casing
Depth
(ft.
BGS
Screened
Interval
(x to y
ft. BGS)
Depth
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Depth to
Water
from Top
of Casing
ft.
Free
Product
Thickness
** (ft.)
Groundwater
Elevation*
(ft.)
Latitude/
Longitude
(decimal
degrees)***
MW-1
05/31/19
06/03/19
2
458
30-45
45
NM
31
None
NM
35.149821/
-80.845903
ft BGS = feet below ground
* Reference Point for Elevation Measurements , Assumed Elevation: ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
*** The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
12 Change 2
Appendix G
Contaminant Sources Other than USTs
Table B-9: Current and Historical Groundwater Elevations and Free Product Thickness
Revision Date: 7/26/2019_ Incident Number and Name: 40792 Byrum Property
Facility ID#:
Well ID
#
Date
Screened Interval
(top of screen,
bottom of screen)
Depth to Water*
Uncorrected
(feet)
Free
Product
Thickness
feet
Depth to Water*
Corrected
for Free Product
Thickness feet)
Top of
Casing
Elevation
(MSL)
Groundwater
Surface
Elevation
(MSL
MW-1
06/03/19
30-45
31
NA
31
NM
NM
*Depth to Water is measured from Top of Casing
14 Change 2
Appendix G
Contaminant Sources Other than USTs
Table B-10: Land Use
Revision Date: 17/26/2019 Incident Number and Name: 40792 Byrum Property Facility ID#:
Map ID #
Date
Determined
Land Use Feature
(include zoning)
Location
(complete street address if applicable)
Distance and
Direction from
Source Area
N,S,E,W of
property
07/26/2019
Residential (R-3)
Subject Property and adjoining properties
250 feet radial
(except southeast
SE of
property
7/26/2019
Residential (R-
8MF)
250 feet southeast of property
250 feet southeast of
pproperty
15 Change 2
APPENDIX I
ROY COOPER
Governor
MICHAEL S. REGAN
Secrerary
MICHAEL SCOTT
Director
Sandra Gravely, President
Byrum Land & Timber, Inc.
P.O. Box 11795
Charlotte, NC 28220
(via email)
Dear Ms. Gravely:
NORTH CAROLINA
Environmental Quality
August 29, 2018
Re: Notice of Regulatory Requirements
15A NCAC 2L .0404 and 2L .0405
Risk -based Assessment and Corrective Action for
Petroleum Underground Storage Tanks
Byrum Property
5628 Closeburn Road, Charlotte
Mecklenburg County
Incident Number:40792
Risk Classification: Unknown
Information received by this office of the UST Section, Division of Waste Management, on January 29,
2018 confirms a release or discharge from a petroleum underground storage tank (UST) system at the
above -referenced location. Records indicate that you are the owner or operator of this UST system.
Therefore, as a responsible party, you must comply with the initial response and abatement action
requirements of Title 15A NCAC 2L .0404 and, if applicable, the assessment and reporting requirements of
Title 15A NCAC 2L .0405, within the timeframes specified in the attached rules. (Be aware that if the latter
rule is applicable, you must comply with its requirements even if you do not receive formal notification from
the UST Section.)
Initial abatement action requirements include the preparation and submittal of an Initial Abatement
Action (IAA) Report, in accordance with Title 15A NCAC 2L .0404 and the most recent version of the
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases, within 90 days
of discovery of the release.
Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department of Environmental Quality in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b).
NORTH C+4RpL D E Q
u�prmwry of EmlmmYeHsl 9�
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville. North Carolina 28115
704.663.1699
Please note that before you sell, transfer, or request a "No Further Action" determination for a property that
has not been remediated to below "unrestricted use" standards, you must file a Notice of Residual Petroleum
("Notice") with the Register of Deeds in the county where the property is located (NCGS 14313-279.9 and 14313-
279.11).
Failure to comply with the State's rules in the manner and time specified may result in the assessment of
civil penalties and/or the use of other enforcement mechanisms.
If you have any questions regarding the actions that must be taken or the rules mentioned in this letter,
please contact me by phone at (704) 235-2182 or by email at Trudy.Beverlynncdenr.gov.
Sincerely,
a-1Y1- Zevad�,
Trudy Beverly, L.G.
Hydrogeologist
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
cc: Shawna Caldwell, Mecklenburg County Groundwater & Wastewater Services
Patrick Lowery, Summit Engineering (via email)
NORTH C.4R0.'+1A�E Q�
un of En- r,nn H-, 9Nor
North Carolina Department of Environmental Quality I Division of Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville. North Carolina 28115
704.663.1699
Beverly, Trudy
From: Beverly, Trudy
Sent: Wednesday, August 29, 2018 2:49 PM
To: sgravely2016@gmail.com'
Cc: plowery@summit-companies.com'
Subject: Byrum Property #40792 — Notice of Regulatory Requirements Letter
Attachments: MO-9331_40792_G_NORR_20180829_NORR for Initial Assessment.pdf
Ms. Gravely,
It was lovely speaking with you this afternoon. As we discussed by phone, the Notice of Regulatory Requirements letter
for the Byrum Property (UST incident number 40792) is attached to this email.
Electronic files for this site can be found on Laserfiche at the following link for viewing and downloading,
https://edocs.deg.nc.gov/WasteManagement/Search.aspx?dbid=0&searchcommand=%7B%SBWM%5D%3A%SBProgra
m ID%5D%3D%22%2AMO-9331%2A%22%7D&cr=1.
Below you will find some general information about home heating oil underground storage tanks:
Home heating oil underground storage tanks are not and haven't been regulated in the state of North Carolina. The UST
section only has records of those that have been reported to our agency. These reports a generally result from
notifications of contamination or tank removals at properties where parties are seeing "no further action" status. Home
heating oil tanks are non -regulated, non-commercial underground storage tanks (USTs) that are exempt from the
"technical regulations" (e.g., leak detection monitoring, corrosion protection, spill and overfill control) that apply to
regulated USTs. Even though home heating oil tanks are exempt from these technical regulations, sampling and cleanup
regulations may apply if there is a leak or spill from your tank. If there is no evidence of a release, then there is no need
to report to the UST Section. The links below provide additional information.
If a leak is discovered under the current ownership of the property, the current property owner is considered the
responsible party for clean-up. Many companies do environmental work related to underground storage tanks.
Typically, they can be found in the yellow pages of a telephone book under "Environmental Consultants." The DWM UST
Section provides a list where companies that do environmental work can provide their information. This list is called the
"UST Service Provider Listing" it is located at http://deg.nc.gov/about/divisions/waste-management/ust/service-
provider-listing. When choosing a company, we recommend getting several estimates and references. Site assessments
and cleanup work must be conducted under the responsible charge of a licensed geologist or professional engineer.
Please note that before you sell, transfer, or request a "No Further Action" determination for a property that has
not been remediated to below "unrestricted use" standards, you must file a Notice of Residual Petroleum
("Notice") with the Register of Deeds in the county where the property is located (NCGS 143B-279.9 and 14313-
279.11).
Underground — Heating Oil Tanks
Non -Regulated Underground Storage Tanks — Frequently Asked Questions
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Brochures-FAQs/Brochure-NonReg%20UST.Of
Home Heating Oil Underground Storage Tanks — General Guidance
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Brochures-FAQs/FAQ-Home%20Heating%20UST.Of
Non -Regulated Noncommercial Petroleum UST Systems (Underground Heating Oil Tanks) Flowchart
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Brochures-
FAQs/H HO%20Tank%20Flowchart%20070717.odf
Guidelines for Site Checks, Tank Closure and Initial Response (text and figures)
"Portions that are Non -Regulated and Non -Regulated and Non -Commercial
https://deg.nc.gov/about/divisions/waste-management/ust/guidance-documents
Have a wonderful day,
Trudy
D�E
NC RTH C;AR01. INA
Department of Environmental quality
Trudy Beverly, LG.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environment Quality
Underground Storage Tanks Section
Corrective Action Branch
Mooresville Regional Office
(704) 235-2182 (Office)
Trudy.Beverly@ncdenr.gov
Er7k d C0fMSPQrxjL5,nC0 to and Yom this swans of wbjeCt to the
Wh C rdire P. :; Regards Law aW may be dis� to third parries.
Branch's Underground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-
management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deg.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps
File Review Procedures:
https://deg.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://edocs.deg.nc.gov/WasteManagement/Search.aspx
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.gov/ncdeg/Waste%20Management/DWM/UST/Corrective%2OAction/Electronic%2ODocument%2OSubmi
ttal%20Memo%2OUpdate.pdf
https://files.nc.gov/ncdeg/Waste%20Management/DWM/UST/Corrective%2OAction/UST%2Ofile%20names%20for%20
Laserfiche.docx
APPENDIX 2
MECKLENBURG COUNTY — PROPERTY RECORD CARD PROPERTY SEARCH
PARCEL ID: 17125220
PARKSTONE SOUTH LLC
Total Appraised Value
5628 CLOSEBURN RD
568 JETTON ST STE 200
$1,046,000
CHARLOTTE NC
DAVIDSON NC 28036
KEY INFORMATION
Land Use Code
R100
Neighborhood
R120
Land Use Desc
SINGLE FAMILY RESIDENTIAL Land
2.761 ACRE
Exemption/Deferment
-
Municipality
CHARLOTTE
Last Sale Date
12/21/2018
Fire District
CITY OF CHARLOTTE
Last Sale Price
$990,000
Special District
NA
Legal Description
L11 M64-490
ASSESSMENT DETAILS
Notice of 2019 Real Estate Assessed Value
Land Value
$1,043,700
Building Value
$2,300
Features
$0
Total
$1,046,000
BUILDING (1)
Finished Area 1,832 Year Built 1955 Built Use / Style SINGLE FAMILY
RESIDENTIAL
Story 1 STORY Heat FORCED AIR - Fuel GAS
DUCTED
Foundation CRAWL SPACE External Wall FACE BRICK Fireplace(s) 1
Full Bath(s) 2 Half Bath(s) Bedroom(s) 3
Total (SgFt) 3,045
LAND
Use Units Type Neighborhood Assessment
R100 2.761 ACRE R120 $1,043,700
RECENT SALES HISTORY
The sales history includes only qualified sales made since January 1, 2016. A sale is qualified when it has been verified, by the
appraiser, as an arm's length transaction for fair market value. Only qualified sales are considered in the appraisal process. For a
complete history of sales and other transfers, please visit Polaris. The Register of Deeds records, indexes, and stores all real estate
related documents that are presented for registration.
Sale Date Sale Price LUC at Sale Legal Reference Deed Type Sold as Vacant Grantor Grantee
12/21/2018 $990,000 R100 33190-610 SPECIAL WARRANTY DEED No BYRUM LAND & TIMBER INC PARKSTONE SOUTH LLC
VALUE CHANGES
The value change history shows only changes in appraised value; it does not show exemptions, exclusions or deferrals that could
reduce a property's taxable value. If any of these are in effect for a particular tax year, it will be shown on the property tax bill for
that year. It is also possible that some previous value changes might be missing from this list or listed in the wrong order. If you
have any questions, please call the County Assessor's Office at 704-336-7600.
Date of Value Change
Effective for Tax Year
Reason for Change
New Value
01/15/2019
2019
COUNTYWIDE REVALUATION
$1,046,000
11 /09/2014
2011
REVALUATION REVIEW - PEARSON
$676,400
02/04/2011
2011
COUNTYWIDE REVALUATION
$800,700
01/02/2003
2003
COUNTYWIDE REVALUATION
$373,100
I
I,
�5
200 ft
Disclaimer
Mecklenburg County makes every effort to produce the most accurate information possible. No warranties, expressed or implied, are provided for the data
herein, its use or interpretation.
https://property.spatialest.com/nc/mecklenburg/#/property/177855/print 2/2
APPENDIX 3
aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
June 06, 2019
Mr. Steve Irminger
Irminger Consulting
7015 Erinbrook Road
Concord, NC 28025
RE: Project: Water
Pace Project No.: 92431399
Dear Mr. Irminger:
Enclosed are the analytical results for sample(s) received by the laboratory on June 03, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
tyriek.hooks@pacelabs.com
(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 26
acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Water
Pace Project No.: 92431399
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDS
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 26
aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Water
92431399
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92431399001
MW-1
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 6010D
IDS
2
PASI-A
EPA 625.1
PKS
58
PASI-C
EPA 8260D
DLK
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 26
aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Water
Pace Project No.: 92431399
Sample: MWA Lab ID: 92431399001 Collected: 06/03/19 09:00 Received: 06/03/19 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
ug/L
98.0
1
06/03/19 18:38
06/05/19 16:35
N2
Aliphatic (C19-C36)
ND
ug/L
98.0
1
06/03/19 18:38
06/05/19 16:35
N2
Aromatic (C11-C22)
ND
ug/L
98.0
1
06/03/19 18:38
06/05/19 16:35
N2
Surrogates
Nonatriacontane (S)
55
%
40-140
1
06/03/19 18:38
06/05/19 16:35
7194-86-7
o-Terphenyl (S)
84
%
40-140
1
06/03/19 18:38
06/05/19 16:35
84-15-1
2-Fluorobiphenyl (S)
88
%
40-140
1
06/03/19 18:38
06/05/19 16:35
321-60-8
2-Bromonaphthalene (S)
85
%
40-140
1
06/03/19 18:38
06/05/19 16:35
580-13-2
VPH NC Water
Analytical Method:
MADEP VPH
Aliphatic (C05-008)
ND
ug/L
50.0
1
06/04/19 13:45
N2
Aliphatic (C09-C12)
ND
ug/L
50.0
1
06/04/19 13:45
N2
Aliphatic(C09-C12) Adjusted
ND
ug/L
50.0
1
06/04/19 13:45
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
06/04/19 13:45
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
93
%
70-130
1
06/04/19 13:45
460-00-4
4-Bromofluorobenzene (PID) (S)
91
%
70-130
1
06/04/19 13:45
460-00-4
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Chromium
6.3
ug/L
5.0
1
06/04/19 00:45
06/04/19 20:25
7440-47-3
Lead
ND
ug/L
5.0
1
06/04/19 00:45
06/04/19 20:25
7439-92-1
625 RVE
Analytical Method: EPA 625.1
Preparation Method:
EPA
625.1
Acenaphthene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
208-96-8
Anthracene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
06/05/19 14:47
06/05/19 21:33
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
7005-72-3
Chrysene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
06/05/19 14:47
06/05/19 21:33
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
06/05/19 14:47
06/05/19 21:33
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
131-11-3
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 06/06/2019 05:02 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 4 of 26
aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Water
Pace Project No.: 92431399
Sample: MW-1
Parameters
ANALYTICAL RESULTS
Lab ID: 92431399001 Collected: 06/03/19 09:00 Received: 06/03/19 14:35 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Di-n-butylphthalate
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
06/05/19 14:47
06/05/19 21:33
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
06/05/19 14:47
06/05/19 21:33
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
117-81-7
Fluoranthene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
206-44-0
Fluorene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
06/05/19 14:47
06/05/19 21:33
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
193-39-5
Isophorone
ND
ug/L
10.0
1
06/05/19 14:47
06/05/19 21:33
78-59-1
Naphthalene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
06/05/19 14:47
06/05/19 21:33
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
06/05/19 14:47
06/05/19 21:33
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
06/05/19 14:47
06/05/19 21:33
87-86-5
Phenanthrene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
85-01-8
Phenol
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
108-95-2
Pyrene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
06/05/19 14:47
06/05/19 21:33
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
06/05/19 14:47
06/05/19 21:33
88-06-2
Surrogates
Nitrobenzene-d5 (S)
73
%
10-120
1
06/05/19 14:47
06/05/19 21:33
4165-60-0
2-Fluorobiphenyl (S)
65
%
15-120
1
06/05/19 14:47
06/05/19 21:33
321-60-8
Terphenyl-d14 (S)
94
%
11-131
1
06/05/19 14:47
06/05/19 21:33
1718-51-0
Phenol-d6 (S)
42
%
10-120
1
06/05/19 14:47
06/05/19 21:33
13127-88-3
2-Fluorophenol (S)
59
%
10-120
1
06/05/19 14:47
06/05/19 21:33
367-12-4
2,4,6-Tribromophenol (S)
83
%
10-137
1
06/05/19 14:47
06/05/19 21:33
118-79-6
8260D MSV Low Level
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
06/05/19 19:34
67-64-1
Benzene
ND
ug/L
1.0
1
06/05/19 19:34
71-43-2
Bromobenzene
ND
ug/L
1.0
1
06/05/19 19:34
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
06/05/19 19:34
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
06/05/19 19:34
75-27-4
Bromoform
ND
ug/L
1.0
1
06/05/19 19:34
75-25-2
Bromomethane
ND
ug/L
2.0
1
06/05/19 19:34
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
06/05/19 19:34
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
06/05/19 19:34
56-23-5
REPORT OF LABORATORY ANALYSIS
M
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Water
Pace Project No.: 92431399
Sample: MW-1 Lab ID: 92431399001 Collected: 06/03/19 09:00 Received: 06/03/19 14:35 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method: EPA 8260D
Chlorobenzene
ND
ug/L
1.0
1
06/05/19 19:34
108-90-7
Chloroethane
ND
ug/L
1.0
1
06/05/19 19:34
75-00-3
Chloroform
ND
ug/L
5.0
1
06/05/19 19:34
67-66-3
Chloromethane
ND
ug/L
1.0
1
06/05/19 19:34
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
06/05/19 19:34
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
06/05/19 19:34
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
06/05/19 19:34
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
06/05/19 19:34
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
06/05/19 19:34
106-93-4
Dibromomethane
ND
ug/L
1.0
1
06/05/19 19:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
06/05/19 19:34
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
06/05/19 19:34
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
06/05/19 19:34
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
06/05/19 19:34
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
1
06/05/19 19:34
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
06/05/19 19:34
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
06/05/19 19:34
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
06/05/19 19:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
06/05/19 19:34
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
06/05/19 19:34
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
1
06/05/19 19:34
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
1
06/05/19 19:34
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
1
06/05/19 19:34
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
06/05/19 19:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
06/05/19 19:34
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
06/05/19 19:34
108-20-3
Ethylbenzene
ND
ug/L
1.0
1
06/05/19 19:34
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
1.0
1
06/05/19 19:34
87-68-3
2-Hexanone
ND
ug/L
5.0
1
06/05/19 19:34
591-78-6
p-Isopropyltoluene
ND
ug/L
1.0
1
06/05/19 19:34
99-87-6
Methylene Chloride
ND
ug/L
5.0
1
06/05/19 19:34
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
06/05/19 19:34
108-10-1
Methyl-tert-butyl ether
ND
ug/L
1.0
1
06/05/19 19:34
1634-04-4
Naphthalene
1.0
ug/L
1.0
1
06/05/19 19:34
91-20-3
Styrene
ND
ug/L
1.0
1
06/05/19 19:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
06/05/19 19:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
06/05/19 19:34
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
06/05/19 19:34
127-18-4
Toluene
ND
ug/L
1.0
1
06/05/19 19:34
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
1.0
1
06/05/19 19:34
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
1.0
1
06/05/19 19:34
120-82-1
1,1,1-Trichloroethane
ND
ug/L
1.0
1
06/05/19 19:34
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
06/05/19 19:34
79-00-5
Trichloroethene
ND
ug/L
1.0
1
06/05/19 19:34
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
06/05/19 19:34
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
06/05/19 19:34
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
06/05/19 19:34
108-05-4
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except in full,
Date: 06/06/2019 05:02 PM
without
the written consent
of Pace Analytical Services, LLC.
Page 6 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Water
Pace Project No.: 92431399
Sample: MW-1
Lab ID: 92431399001 Collected: 06/03/19 09:00
Received: 06/03/19 14:35 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level
Analytical Method:
EPA 8260D
Vinyl chloride
ND
ug/L
1.0
1
06/05/19 19:34
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
06/05/19 19:34
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
06/05/19 19:34
179601-23-1
o-Xylene
ND
ug/L
1.0
1
06/05/19 19:34
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
06/05/19 19:34
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
06/05/19 19:34
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
06/05/19 19:34
2037-26-5
Date: 06/06/2019 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
QC Batch: 478940 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92431399001
METHOD BLANK: 2592184
Associated Lab Samples: 92431399001
Parameter
Units
Aliphatic (C05-008)
ug/L
Aliphatic (C09-C12)
ug/L
Aromatic (C09-C10)
ug/L
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
Matrix: Water
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
50.0
06/04/1913:16 N2
ND
50.0
06/04/1913:16 N2
ND
50.0
06/04/1913:16 N2
98
70-130
06/04/1913:16
96
70-130
06/04/1913:16
LABORATORY CONTROL SAMPLE & LCSD:
2592185
2592186
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
244
234
81
78
70-130 4 25 N2
Aliphatic (C09-C12)
ug/L
300
297
292
99
97
30-130 2 25 N2
Aromatic (C09-C10)
ug/L
100
95.3
94.0
95
94
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
105
98
70-130
4-Bromofluorobenzene (PID) (S)
%
102
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
QC Batch: 478810 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92431399001
METHOD BLANK: 2591738 Matrix: Water
Associated Lab Samples: 92431399001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chromium ug/L ND 5.0 06/04/1919:15
Lead ug/L ND 5.0 06/04/1919:15
LABORATORY CONTROL SAMPLE: 2591739
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chromium ug/L 500 441 88 80-120
Lead ug/L 500 442 88 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2591740
2591741
MS
MSD
92430283001
Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units
Result
Conc.
Conc.
Result
Result % Rec
% Rec Limits RPD Qual
Chromium ug/L
ND
500
500
521
507 104
101 75-125 3
Lead ug/L
ND
500
500
507
495 101
99 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
QC Batch: 479106 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Associated Lab Samples: 92431399001
METHOD BLANK: 2592936
Associated Lab Samples: 92431399001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/05/19 13:22
1,1,1-Trichloroethane
ug/L
ND
1.0
06/05/19 13:22
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/05/19 13:22
1,1,2-Trichloroethane
ug/L
ND
1.0
06/05/19 13:22
1,1-Dichloroethane
ug/L
ND
1.0
06/05/19 13:22
1,1-Dichloroethene
ug/L
ND
1.0
06/05/19 13:22
1,1-Dichloropropene
ug/L
ND
1.0
06/05/19 13:22
1,2,3-Trichlorobenzene
ug/L
ND
1.0
06/05/19 13:22
1,2,3-Trichloropropane
ug/L
ND
1.0
06/05/19 13:22
1,2,4-Trichlorobenzene
ug/L
ND
1.0
06/05/19 13:22
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
06/05/19 13:22
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/05/19 13:22
1,2-Dichlorobenzene
ug/L
ND
1.0
06/05/19 13:22
1,2-Dichloroethane
ug/L
ND
1.0
06/05/19 13:22
1,2-Dichloropropane
ug/L
ND
1.0
06/05/19 13:22
1,3-Dichlorobenzene
ug/L
ND
1.0
06/05/19 13:22
1,3-Dichloropropane
ug/L
ND
1.0
06/05/19 13:22
1,4-Dichlorobenzene
ug/L
ND
1.0
06/05/19 13:22
2,2-Dichloropropane
ug/L
ND
1.0
06/05/19 13:22
2-Butanone (MEK)
ug/L
ND
5.0
06/05/19 13:22
2-Chlorotoluene
ug/L
ND
1.0
06/05/19 13:22
2-Hexanone
ug/L
ND
5.0
06/05/19 13:22
4-Chlorotoluene
ug/L
ND
1.0
06/05/19 13:22
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/05/19 13:22
Acetone
ug/L
ND
25.0
06/05/19 13:22
Benzene
ug/L
ND
1.0
06/05/19 13:22
Bromobenzene
ug/L
ND
1.0
06/05/19 13:22
Bromochloromethane
ug/L
ND
1.0
06/05/19 13:22
Bromodichloromethane
ug/L
ND
1.0
06/05/19 13:22
Bromoform
ug/L
ND
1.0
06/05/19 13:22
Bromomethane
ug/L
ND
2.0
06/05/19 13:22 IK
Carbon tetrachloride
ug/L
ND
1.0
06/05/19 13:22
Chlorobenzene
ug/L
ND
1.0
06/05/19 13:22
Chloroethane
ug/L
ND
1.0
06/05/19 13:22
Chloroform
ug/L
ND
5.0
06/05/19 13:22
Chloromethane
ug/L
ND
1.0
06/05/19 13:22
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/05/19 13:22
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/05/19 13:22
Dibromochloromethane
ug/L
ND
1.0
06/05/19 13:22
Dibromomethane
ug/L
ND
1.0
06/05/19 13:22
Dichlorodifluoromethane
ug/L
ND
1.0
06/05/19 13:22
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
METHOD BLANK: 2592936
Associated Lab Samples: 92431399001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
06/05/19 13:22
Ethylbenzene
ug/L
ND
1.0
06/05/19 13:22
Hexachloro-1,3-butadiene
ug/L
ND
1.0
06/05/19 13:22
m&p-Xylene
ug/L
ND
2.0
06/05/19 13:22
Methyl-tert-butyl ether
ug/L
ND
1.0
06/05/19 13:22
Methylene Chloride
ug/L
ND
5.0
06/05/19 13:22
Naphthalene
ug/L
ND
1.0
06/05/19 13:22
o-Xylene
ug/L
ND
1.0
06/05/19 13:22
p-Isopropyltoluene
ug/L
ND
1.0
06/05/19 13:22
Styrene
ug/L
ND
1.0
06/05/19 13:22
Tetrachloroethene
ug/L
ND
1.0
06/05/19 13:22
Toluene
ug/L
ND
1.0
06/05/19 13:22
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/05/19 13:22
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/05/19 13:22
Trichloroethene
ug/L
ND
1.0
06/05/19 13:22
Trichlorofluoromethane
ug/L
ND
1.0
06/05/19 13:22
Vinyl acetate
ug/L
ND
2.0
06/05/19 13:22
Vinyl chloride
ug/L
ND
1.0
06/05/19 13:22
Xylene (Total)
ug/L
ND
1.0
06/05/19 13:22
1,2-Dichloroethane-d4 (S)
%
93
70-130
06/05/19 13:22
4-Bromofluorobenzene (S)
%
96
70-130
06/05/19 13:22
Toluene-d8 (S)
%
99
70-130
06/05/19 13:22
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2592937
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.9
104
70-130
1,1,1-Trichloroethane
ug/L
50
50.7
101
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,2-Trichloroethane
ug/L
50
51.1
102
70-130
1,1-Dichloroethane
ug/L
50
52.6
105
70-130
1,1-Dichloroethene
ug/L
50
54.7
109
70-130
1,1-Dichloropropene
ug/L
50
50.6
101
70-130
1,2,3-Trichlorobenzene
ug/L
50
55.9
112
70-130
1,2,3-Trichloropropane
ug/L
50
54.1
108
70-130
1,2,4-Trichlorobenzene
ug/L
50
55.8
112
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.9
102
70-130
1,2-Dibromoethane (EDB)
ug/L
50
51.6
103
70-130
1,2-Dichlorobenzene
ug/L
50
50.7
101
70-130
1,2-Dichloroethane
ug/L
50
45.8
92
70-130
1,2-Dichloropropane
ug/L
50
52.1
104
70-130
1,3-Dichlorobenzene
ug/L
50
50.5
101
70-130
1,3-Dichloropropane
ug/L
50
51.7
103
70-131
1,4-Dichlorobenzene
ug/L
50
50.3
101
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
LABORATORY CONTROL SAMPLE:
Parameter
2592937
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,2-Dichloropropane
ug/L
50
53.5
107
69-130
2-Butanone (MEK)
ug/L
100
101
101
64-135
2-Chlorotoluene
ug/L
50
50.1
100
70-130
2-Hexanone
ug/L
100
104
104
66-135
4-Chlorotoluene
ug/L
50
51.2
102
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
103
103
70-130
Acetone
ug/L
100
116
116
61-157
Benzene
ug/L
50
51.4
103
70-130
Bromobenzene
ug/L
50
51.5
103
70-130
Bromochloromethane
ug/L
50
51.5
103
70-130
Bromodichloromethane
ug/L
50
51.9
104
70-130
Bromoform
ug/L
50
53.0
106
70-130
Bromomethane
ug/L
50
59.5
119
38-130IK
Carbon tetrachloride
ug/L
50
50.1
100
70-130
Chlorobenzene
ug/L
50
49.8
100
70-130
Chloroethane
ug/L
50
54.5
109
37-142
Chloroform
ug/L
50
51.2
102
70-130
Chloromethane
ug/L
50
54.6
109
48-130
cis-1,2-Dichloroethene
ug/L
50
51.9
104
70-130
cis-1,3-Dichloropropene
ug/L
50
52.5
105
70-130
Dibromochloromethane
ug/L
50
52.0
104
70-130
Dibromomethane
ug/L
50
52.2
104
70-130
Dichlorodifluoromethane
ug/L
50
62.9
126
53-134
Diisopropyl ether
ug/L
50
53.4
107
70-135
Ethylbenzene
ug/L
50
51.4
103
70-130
Hexachloro-1,3-butadiene
ug/L
50
56.0
112
68-132
m&p-Xylene
ug/L
100
102
102
70-130
Methyl-tert-butyl ether
ug/L
50
52.4
105
70-130
Methylene Chloride
ug/L
50
46.2
92
67-132
Naphthalene
ug/L
50
54.1
108
70-130
o-Xylene
ug/L
50
53.5
107
70-131
p-Isopropyltoluene
ug/L
50
53.4
107
70-130
Styrene
ug/L
50
51.5
103
70-130
Tetrachloroethene
ug/L
50
49.0
98
69-130
Toluene
ug/L
50
50.4
101
70-130
trans-1,2-Dichloroethene
ug/L
50
54.1
108
70-130
trans- 1,3-Dichloropropene
ug/L
50
53.2
106
70-130
Trichloroethene
ug/L
50
50.5
101
70-130
Trichlorofluoromethane
ug/L
50
53.0
106
63-130
Vinyl acetate
ug/L
100
111
111
55-143
Vinyl chloride
ug/L
50
58.3
117
70-131
Xylene (Total)
ug/L
150
156
104
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 26
aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2592938
2592939
MS
MSD
92431212005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
500
500
615
579
123
116
73-134
6
1,1,1-Trichloroethane
ug/L
ND
500
500
637
591
127
118
82-143
7
1,1,2,2-Tetrachloroethane
ug/L
ND
500
500
608
547
122
109
70-136
11
1,1,2-Trichloroethane
ug/L
ND
500
500
590
551
118
110
70-135
7
1,1-Dichloroethane
ug/L
ND
500
500
649
611
130
122
70-139
6
1,1-Dichloroethene
ug/L
ND
500
500
684
604
137
121
70-154
13
1,1-Dichloropropene
ug/L
ND
500
500
622
587
124
117
70-149
6
1,2,3-Trichlorobenzene
ug/L
ND
500
500
609
511
122
102
70-135
18
1,2,3-Trichloropropane
ug/L
ND
500
500
557
581
111
116
71-137
4
1,2,4-Trichlorobenzene
ug/L
ND
500
500
613
559
123
112
73-140
9
1,2-Dibromo-3-chloropropane
ug/L
ND
500
500
587
552
117
110
65-134
6
1,2-Dibromoethane (EDB)
ug/L
ND
500
500
608
537
122
107
70-137
12
1,2-Dichlorobenzene
ug/L
ND
500
500
590
535
118
107
70-133
10
1,2-Dichloroethane
ug/L
ND
500
500
571
505
113
100
70-137
12
1,2-Dichloropropane
ug/L
ND
500
500
630
576
126
115
70-140
9
1,3-Dichlorobenzene
ug/L
ND
500
500
597
565
119
113
70-135
6
1,3-Dichloropropane
ug/L
ND
500
500
611
563
122
113
70-143
8
1,4-Dichlorobenzene
ug/L
ND
500
500
579
532
116
106
70-133
9
2,2-Dichloropropane
ug/L
ND
500
500
674
643
135
129
61-148
5
2-Butanone (MEK)
ug/L
ND
1000
1000
1260
1220
118
114
60-139
4
2-Chlorotoluene
ug/L
ND
500
500
657
630
131
126
70-144
4
2-Hexanone
ug/L
ND
1000
1000
1240
1160
124
116
65-138
6
4-Chlorotoluene
ug/L
ND
500
500
615
574
123
115
70-137
7
4-Methyl-2-pentanone (MIBK)
ug/L
ND
1000
1000
1230
1170
123
117
65-135
5
Acetone
ug/L
ND
1000
1000
1260
1210
126
121
60-148
5
Benzene
ug/L
ND
500
500
645
606
129
121
70-151
6
Bromobenzene
ug/L
ND
500
500
619
574
124
115
70-136
8
Bromochloromethane
ug/L
ND
500
500
623
607
125
121
70-141
3
Bromodichloromethane
ug/L
ND
500
500
627
571
125
114
70-138
9
Bromoform
ug/L
ND
500
500
574
535
115
107
63-130
7
Bromomethane
ug/L
ND
500
500
782
705
156
141
15-152
101K,M1
Carbon tetrachloride
ug/L
ND
500
500
606
574
121
115
70-143
6
Chlorobenzene
ug/L
ND
500
500
596
567
119
113
70-138
5
Chloroethane
ug/L
ND
500
500
819
508
164
102
52-163
47 M1,R1
Chloroform
ug/L
ND
500
500
612
599
122
120
70-139
2
Chloromethane
ug/L
ND
500
500
658
602
132
120
41-139
9
cis-1,2-Dichloroethene
ug/L
ND
500
500
640
581
128
116
70-141
10
cis-1,3-Dichloropropene
ug/L
ND
500
500
625
605
125
121
70-137
3
Dibromochloromethane
ug/L
ND
500
500
608
584
122
117
70-134
4
Dibromomethane
ug/L
ND
500
500
605
584
121
117
70-138
4
Dichlorodifluoromethane
ug/L
ND
500
500
716
650
143
130
47-155
10
Diisopropyl ether
ug/L
ND
500
500
671
613
134
123
63-144
9
Ethylbenzene
ug/L
1270
500
500
1860
1710
116
87
66-153
8
Hexachloro-1,3-butadiene
ug/L
ND
500
500
599
531
120
106
65-149
12
m&p-Xylene
ug/L
8040
1000
1000
8930
8230
89
19
69-152
8 M1
Methyl-tert-butyl ether
ug/L
ND
500
500
666
594
133
119
54-156
11
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 26
aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2592938
2592939
MS
MSD
92431212005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Methylene Chloride
ug/L
ND
500
500
589
542
111
102
42-159
8
Naphthalene
ug/L
935
500
500
1480
1460
110
105
61-148
1
o-Xylene
ug/L
4460
500
500
4930
4590
94
25
70-148
7 M1
p-Isopropyltoluene
ug/L
ND
500
500
636
595
123
115
70-146
7
Styrene
ug/L
ND
500
500
668
616
134
123
70-135
8
Tetrachloroethene
ug/L
ND
500
500
593
578
119
116
59-143
3
Toluene
ug/L
2020
500
500
2610
2400
118
77
59-148
8
trans-1,2-Dichloroethene
ug/L
ND
500
500
686
615
137
123
70-146
11
trans- 1,3-Dichloropropene
ug/L
ND
500
500
606
576
121
115
70-135
5
Trichloroethene
ug/L
ND
500
500
621
569
124
114
70-147
9
Trichlorofluoromethane
ug/L
ND
500
500
640
609
128
122
70-148
5
Vinyl acetate
ug/L
ND
1000
1000
1330
1220
133
122
49-151
9
Vinyl chloride
ug/L
ND
500
500
734
663
147
133
70-156
10
Xylene (Total)
ug/L
12500
1500
1500
13900
12800
91
21
63-158
8 MS
1,2-Dichloroethane-d4 (S)
%
94
91
70-130
4-Bromofluorobenzene (S)
%
96
96
70-130
Toluene-d8(S)
%
100
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 26
aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
QC Batch: 479101 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92431399001
METHOD BLANK: 2592913
Associated Lab Samples: 92431399001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
06/05/19 17:20
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
06/05/19 17:20
2,4,6-Trichlorophenol
ug/L
ND
10.0
06/05/19 17:20
2,4-Dichlorophenol
ug/L
ND
5.0
06/05/19 17:20
2,4-Dimethylphenol
ug/L
ND
10.0
06/05/19 17:20
2,4-Dinitrophenol
ug/L
ND
50.0
06/05/19 17:20
2,4-Dinitrotoluene
ug/L
ND
5.0
06/05/19 17:20
2,6-Dinitrotoluene
ug/L
ND
5.0
06/05/19 17:20
2-Chloronaphthalene
ug/L
ND
5.0
06/05/19 17:20
2-Chlorophenol
ug/L
ND
5.0
06/05/19 17:20
2-Nitrophenol
ug/L
ND
5.0
06/05/19 17:20
3,3'-Dichlorobenzidine
ug/L
ND
25.0
06/05/19 17:20
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
06/05/19 17:20
4-Bromophenylphenyl ether
ug/L
ND
5.0
06/05/19 17:20
4-Chloro-3-methylphenol
ug/L
ND
5.0
06/05/19 17:20
4-Chlorophenylphenyl ether
ug/L
ND
5.0
06/05/19 17:20
4-Nitrophenol
ug/L
ND
50.0
06/05/19 17:20
Acenaphthene
ug/L
ND
5.0
06/05/19 17:20
Acenaphthylene
ug/L
ND
5.0
06/05/19 17:20
Anthracene
ug/L
ND
5.0
06/05/19 17:20
Benzo(a)anthracene
ug/L
ND
5.0
06/05/19 17:20
Benzo(a)pyrene
ug/L
ND
5.0
06/05/19 17:20
Benzo(b)fluoranthene
ug/L
ND
5.0
06/05/19 17:20
Benzo(g,h,i)perylene
ug/L
ND
5.0
06/05/19 17:20
Benzo(k)fluoranthene
ug/L
ND
5.0
06/05/19 17:20
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
06/05/19 17:20
bis(2-Chloroethyl) ether
ug/L
ND
5.0
06/05/19 17:20
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
06/05/19 17:20
Butylbenzylphthalate
ug/L
ND
5.0
06/05/19 17:20
Chrysene
ug/L
ND
5.0
06/05/19 17:20
Di-n-butylphthalate
ug/L
ND
5.0
06/05/19 17:20
Di-n-octylphthalate
ug/L
ND
5.0
06/05/19 17:20
Dibenz(a,h)anthracene
ug/L
ND
5.0
06/05/19 17:20
Diethylphthalate
ug/L
ND
5.0
06/05/19 17:20
Dimethylphthalate
ug/L
ND
5.0
06/05/19 17:20
Fluoranthene
ug/L
ND
5.0
06/05/19 17:20
Fluorene
ug/L
ND
5.0
06/05/19 17:20
Hexachloro-1,3-butadiene
ug/L
ND
5.0
06/05/19 17:20
Hexachlorobenzene
ug/L
ND
5.0
06/05/19 17:20
Hexachlorocyclopentadiene
ug/L
ND
10.0
06/05/19 17:20
Hexachloroethane
ug/L
ND
5.0
06/05/19 17:20
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 26
aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
METHOD BLANK: 2592913
Associated Lab Samples: 92431399001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
06/05/19 17:20
Isophorone
ug/L
ND
10.0
06/05/19 17:20
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
06/05/19 17:20
N-Nitrosodimethylamine
ug/L
ND
5.0
06/05/19 17:20
N-Nitrosodiphenylamine
ug/L
ND
10.0
06/05/19 17:20
Naphthalene
ug/L
ND
5.0
06/05/19 17:20
Nitrobenzene
ug/L
ND
5.0
06/05/19 17:20
Pentachlorophenol
ug/L
ND
10.0
06/05/19 17:20
Phenanthrene
ug/L
ND
5.0
06/05/19 17:20
Phenol
ug/L
ND
5.0
06/05/19 17:20
Pyrene
ug/L
ND
5.0
06/05/19 17:20
2,4,6-Tribromophenol (S)
%
98
10-137
06/05/19 17:20
2-Fluorobiphenyl (S)
%
84
15-120
06/05/19 17:20
2-Fluorophenol (S)
%
86
10-120
06/05/19 17:20
Nitrobenzene-d5 (S)
%
95
10-120
06/05/19 17:20
Phenol-d6 (S)
%
61
10-120
06/05/19 17:20
Terphenyl-d14 (S)
%
106
11-131
06/05/19 17:20
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2592914
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
25.5
51
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
33.1
66
36-166
2,4,6-Trichlorophenol
ug/L
50
39.0
78
37-144
2,4-Dichlorophenol
ug/L
50
38.0
76
1-191
2,4-Dimethylphenol
ug/L
50
36.5
73
32-119
2,4-Dinitrophenol
ug/L
250
217
87
1-181
2,4-Dinitrotoluene
ug/L
50
38.5
77
39-139
2,6-Dinitrotoluene
ug/L
50
37.2
74
50-158
2-Chloronaphthalene
ug/L
50
33.9
68
60-118
2-Chlorophenol
ug/L
50
35.1
70
23-134
2-Nitrophenol
ug/L
50
35.4
71
29-182
3,3'-Dichlorobenzidine
ug/L
100
84.3
84
1-262
4,6-Dinitro-2-methyl phenol
ug/L
100
94.1
94
1-181
4-Bromophenylphenyl ether
ug/L
50
37.0
74
53-127
4-ChIoro-3-methyl phenol
ug/L
100
80.7
81
22-147
4-Chlorophenylphenyl ether
ug/L
50
36.1
72
25-158
4-Nitrophenol
ug/L
250
171
68
1-132
Acenaphthene
ug/L
50
33.6
67
47-145
Acenaphthylene
ug/L
50
34.2
68
33-145
Anthracene
ug/L
50
39.0
78
1-166
Benzo(a)anthracene
ug/L
50
42.2
84
33-143
Benzo(a)pyrene
ug/L
50
41.0
82
17-163
Benzo(b)fluoranthene
ug/L
50
47.1
94
24-159
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 26
aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
LABORATORY CONTROL SAMPLE:
2592914
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(g,h,i)perylene
ug/L
50
42.4
85
1-219
Benzo(k)fluoranthene
ug/L
50
41.6
83
11-162
bis(2-Chloroethoxy)methane
ug/L
50
35.3
71
33-184
bis(2-Chloroethyl) ether
ug/L
50
34.5
69
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
39.0
78
8-158
Butylbenzylphthalate
ug/L
50
39.0
78
1-152
Chrysene
ug/L
50
37.4
75
17-168
Di-n-butylphthalate
ug/L
50
36.7
73
1-118
Di-n-octylphthalate
ug/L
50
38.8
78
4-146
Dibenz(a,h)anthracene
ug/L
50
43.7
87
1-227
Diethylphthalate
ug/L
50
36.0
72
1-114
Dimethylphthalate
ug/L
50
36.1
72
1-112
Fluoranthene
ug/L
50
40.5
81
26-137
Fluorene
ug/L
50
36.7
73
59-121
Hexachloro-1,3-butadiene
ug/L
50
23.3
47
24-116
Hexachlorobenzene
ug/L
50
34.1
68
1-152
Hexachlorocyclopentadiene
ug/L
50
23.2
46
25-150
Hexachloroethane
ug/L
50
22.2
44
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
42.8
86
1-171
Isophorone
ug/L
50
31.3
63
21-196
N-Nitroso-di-n-propylamine
ug/L
50
34.2
68
1-230
N-Nitrosodimethylamine
ug/L
50
28.5
57
25-150
N-Nitrosodiphenylamine
ug/L
50
37.1
74
25-150
Naphthalene
ug/L
50
31.6
63
21-133
Nitrobenzene
ug/L
50
31.4
63
35-180
Pentachlorophenol
ug/L
100
89.4
89
14-176
Phenanthrene
ug/L
50
38.3
77
54-120
Phenol
ug/L
50
26.5
53
5-112
Pyrene
ug/L
50
39.8
80
52-115
2,4,6-Tribromophenol (S)
%
82
10-137
2-Fluorobiphenyl (S)
%
66
15-120
2-Fluorophenol (S)
%
63
10-120
Nitrobenzene-d5(S)
%
71
10-120
Phenol-d6 (S)
%
51
10-120
Terphenyl-d14 (S)
%
80
11-131
MATRIX SPIKE SAMPLE:
2594284
92430410005
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
50
22.0
44
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
ND
50
21.1
42
36-166
2,4,6-Trichlorophenol
ug/L
ND
50
30.7
61
37-144
2,4-Dichlorophenol
ug/L
ND
50
29.1
58
1-191
2,4-Dimethylphenol
ug/L
ND
50
28.8
58
32-119
2,4-Dinitrophenol
ug/L
ND
250
218
87
1-181
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 26
aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
MATRIX SPIKE SAMPLE:
2594284
92430410005
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
ND
50
39.3
79
39-139
2,6-Dinitrotoluene
ug/L
ND
50
34.6
69
50-158
2-Chloronaphthalene
ug/L
ND
50
29.5
59
60-118 M1
2-Chlorophenol
ug/L
ND
50
28.6
57
23-134
2-Nitrophenol
ug/L
ND
50
28.1
56
29-182
3,3'-Dichlorobenzidine
ug/L
ND
100
82.5
83
1-262
4,6-Dinitro-2-methyl phenol
ug/L
ND
100
98.9
99
1-181
4-Bromophenylphenyl ether
ug/L
ND
50
34.5
69
53-127
4-Chloro-3-methylphenol
ug/L
ND
100
56.1
56
22-147
4-Chlorophenylphenyl ether
ug/L
ND
50
29.2
58
25-158
4-Nitrophenol
ug/L
ND
250
126
50
1-132
Acenaphthene
ug/L
ND
50
29.3
59
47-145
Acenaphthylene
ug/L
ND
50
30.1
60
33-145
Anthracene
ug/L
ND
50
43.6
87
1-166
Benzo(a)anthracene
ug/L
ND
50
46.9
94
33-143
Benzo(a)pyrene
ug/L
ND
50
46.9
94
17-163
Benzo(b)fluoranthene
ug/L
ND
50
50.0
100
24-159
Benzo(g,h,i)perylene
ug/L
ND
50
45.8
92
1-219
Benzo(k)fluoranthene
ug/L
ND
50
48.1
96
11-162
bis(2-Chloroethoxy)methane
ug/L
ND
50
26.0
52
33-184
bis(2-Chloroethyl) ether
ug/L
ND
50
27.6
55
12-158
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
42.7
85
8-158
Butylbenzylphthalate
ug/L
ND
50
40.3
81
1-152
Chrysene
ug/L
ND
50
42.2
84
17-168
Di-n-butylphthalate
ug/L
ND
50
41.4
83
1-118
Di-n-octylphthalate
ug/L
ND
50
41.1
82
4-146
Dibenz(a,h)anthracene
ug/L
ND
50
45.4
91
1-227
Diethylphthalate
ug/L
ND
50
38.7
77
1-114
Dimethylphthalate
ug/L
ND
50
34.1
68
1-112
Fluoranthene
ug/L
ND
50
47.1
94
26-137
Fluorene
ug/L
ND
50
32.6
65
59-121
Hexachloro-1,3-butadiene
ug/L
ND
50
19.6
39
24-116
Hexachlorobenzene
ug/L
ND
50
34.8
70
1-152
Hexachlorocyclopentadiene
ug/L
ND
50
20.5
41
25-150
Hexachloroethane
ug/L
ND
50
19.6
39
40-113 M1
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
47.2
94
1-171
Isophorone
ug/L
ND
50
25.5
51
21-196
N-Nitroso-di-n-propylamine
ug/L
ND
50
26.0
52
1-230
N-Nitrosodimethylamine
ug/L
ND
50
21.9
44
25-150
N-Nitrosodiphenylamine
ug/L
ND
50
37.4
75
25-150
Naphthalene
ug/L
ND
50
27.7
55
21-133
Nitrobenzene
ug/L
ND
50
25.9
52
35-180
Pentachlorophenol
ug/L
ND
100
81.5
81
14-176
Phenanthrene
ug/L
ND
50
42.7
85
54-120
Phenol
ug/L
ND
50
16.8
34
5-112
Pyrene
ug/L
ND
50
46.7
93
52-115
2,4,6-Tribromophenol (S)
%
86
10-137
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 26
aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
MATRIX SPIKE SAMPLE:
2594284
92430410005 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
2-Fluorobiphenyl (S)
%
56
15-120
2-Fluorophenol(S)
%
44
10-120
Nitrobenzene-d5 (S)
%
58
10-120
Phenol-d6 (S)
%
33
10-120
Terphenyl-d14 (S)
%
89
11-131
SAMPLE DUPLICATE: 2594285
Parameter
Units
92430410006
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/L
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/L
ND
ND
2,4,6-Trichlorophenol
ug/L
ND
ND
2,4-Dichlorophenol
ug/L
ND
ND
2,4-Dimethylphenol
ug/L
ND
ND
2,4-Dinitrophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
ND
2,6-Dinitrotoluene
ug/L
ND
ND
2-Chloronaphthalene
ug/L
ND
ND
2-Chlorophenol
ug/L
ND
ND
2-Nitrophenol
ug/L
ND
ND
3,3'-Dichlorobenzidine
ug/L
ND
ND
4,6-Dinitro-2-methyl phenol
ug/L
ND
ND
4-Bromophenylphenyl ether
ug/L
ND
ND
4-Chloro-3-methylphenol
ug/L
ND
ND
4-Chlorophenylphenyl ether
ug/L
ND
ND
4-Nitrophenol
ug/L
ND
ND
Acenaphthene
ug/L
ND
ND
Acenaphthylene
ug/L
ND
ND
Anthracene
ug/L
ND
ND
Benzo(a)anthracene
ug/L
ND
ND
Benzo(a)pyrene
ug/L
ND
ND
Benzo(b)fluoranthene
ug/L
ND
ND
Benzo(g,h,i)perylene
ug/L
ND
ND
Benzo(k)fluoranthene
ug/L
ND
ND
bis(2-Chloroethoxy)methane
ug/L
ND
ND
bis(2-Chloroethyl) ether
ug/L
ND
ND
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
Butylbenzylphthalate
ug/L
ND
ND
Chrysene
ug/L
ND
ND
Di-n-butylphthalate
ug/L
ND
ND
Di-n-octylphthalate
ug/L
ND
ND
Dibenz(a,h)anthracene
ug/L
ND
ND
Diethylphthalate
ug/L
ND
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 26
aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
SAMPLE DUPLICATE: 2594285
Parameter
Units
92430410006
Result
Dup
Result
Fluorene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitroso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tribromophenol (S)
%
79
51
2-Fluorobiphenyl (S)
%
66
54
2-Fluorophenol (S)
%
58
43
Nitrobenzene-d5 (S)
%
67
54
Phenol-d6 (S)
%
46
31
Terphenyl-d14 (S)
%
103
57
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 26
aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Water
Pace Project No.: 92431399
QC Batch: 478758 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Associated Lab Samples: 92431399001
METHOD BLANK: 2591455
Matrix:
Water
Associated Lab Samples: 92431399001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
ug/L
ND
100
06/05/19 06:50 N2
Aliphatic (C19-C36)
ug/L
ND
100
06/05/19 06:50 N2
Aromatic (C11-C22)
ug/L
ND
100
06/05/19 06:50 N2
2-Bromonaphthalene (S)
%
85
40-140
06/05/19 06:50
2-Fluorobiphenyl (S)
%
82
40-140
06/05/19 06:50
Nonatriacontane (S)
%
55
40-140
06/05/19 06:50
o-Terphenyl (S)
%
68
40-140
06/05/19 06:50
LABORATORY CONTROL SAMPLE & LCSD:
2591456
2591457
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
ug/L
300
147
171
49
57
40-140 15 50 N2
Aliphatic (C19-C36)
ug/L
400
232
270
58
67
40-140 15 50 N2
Aromatic (C11-C22)
ug/L
850
508
596
60
70
40-140 16 50 N2
2-Bromonaphthalene (S)
%
82
85
40-140
2-Fluorobiphenyl (S)
%
82
83
40-140
Nonatriacontane (S)
%
60
61
40-140
o-Terphenyl(S)
%
70
82
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 26
Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: Water
Pace Project No.: 92431399
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MS Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 05:02 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 26
aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Water
92431399
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92431399001
MW-1
MADEP EPH
478758
MADEP EPH
479069
92431399001
MW-1
MADEP VPH
478940
92431399001
MW-1
EPA 3010A
478810
EPA 6010D
478829
92431399001
MW-1
EPA 625.1
479101
EPA 625.1
479360
92431399001
MW-1
EPA 8260D
479106
Date: 06/06/2019 05:02 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 26
+ Sample Condition U on Retei C(SCUR Page 1 of 2
:aCi;Rnao--ca Document No.: Issuing Authority:
F-CAR-CS-033-Rew06 Pace Carolinas Quality I
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvilf Raleigh❑ Mechanicsville(]
SarrIple . . Client Name: �0#92431399
Upon ReceiptProjectA
Courser: ❑.Fed Ex ❑UPS ❑USl'S Eclient
❑ Commercial r ❑Pace ❑Other, 92431399
Custody Sea! Present? Oyes 101NO Seals Intact? []Yeso
Date/Initials Person Examining Contents:
Packing Material: []Bubble Wrap Bubble Bags ❑None ❑ other Biological Tissue F,�zen?
Thermometer ❑Yes ❑No N/A
92TO48 Type of Ice: Ljy / t ❑Blue []None
R Gun 10: -�---
[ooler Terrip (°L): �-� ° Correction Factor: Add/Subtract ('Q 0.0
Tempshould be above freezing to VC
Cooler Temp Corrected (°C). ❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated SoN N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? Did samples originate from a foreign source (Internatlanally,..
ram.. - F-1-1 _ i—iE„rdauawaii and Puerto Rlcol? nYes []No -
Comments/Discrepancy:
Chain of Custody Present?
a
esEINO
❑N/A
1.
Satno kn Arrived within Hold rime?
Yes
ONO
❑NIA
2.
Short Hcld,Time Anal sls (<72 hr.)?
❑Yes
r1do,
❑N A
3.
Rush ruin Around Tune Requested?
es
NIA
Sufficlentvolume?
es
EIN.
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
ess
QNo
EJNo
❑N/A
N/A
6.
Containers Intact?
es
❑No
NIA
7.
Dissolved analysis: Samples Field R8ered?—
❑Yes
❑Na
ONIA
6.
Sample Labels Match COO
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
Yes
❑Na
o
[]N/A
❑N A
9.
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
[]No
QNo
/A
IA
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes [:]No
Lot ID of split containers:
CLIENT NOT1FKATION/RESC]LUrION
Person contacted: Date/Time:
Project Manager SCURF Review: a1W Date:
Project Manager SRF Review: Date:
Page 24 of 26
Document Name:
Condition upon Rec
Document No.:
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
WQ#:92431399
PM: TIH Due Date. 06/05/19
CLIENT: 92-Irminger
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preseryation
adjusted
Amount of Preservative
added
Lot N
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will nesent to the North Carolina ULHNK certmcation UrnCe tr.e.
Out of hold, incorrect preservative, out of temp, Incorrect containers.
Page 25 of 26
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A
Section B Section C .
Required Clie
Irformaton: Required Project Information: Invoice Information: Pa e - 1 Of 1
mingerConsulting Inc Report To: Steve Irminger Attention:
015 Erinhrook Road Copy To: Company Name: 70
Company: !
Address:
Concord, NC 2E
D25
Address:
4� fit"
Email: stEvei
finger gmail.00m
Purchase Order#:
Pace Quote:
Phone:
04)795-1585 Fax
Project Name: Water
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Beverly, Trudy
From: Beverly, Trudy
Sent: Wednesday, July 31, 2019 11:25 AM
To: Steven Irminger
Subject: RE: [External] LSA Byrum Property Incident 40792
Good Morning Steve,
No need to mail a hard copy of this report.
Thank you,
Trudy
Trudy Eev erly . L.G.
�i•a�roggoTo :st, Divirio�: of F�:asra .Fa�:agement
D E Forth Carolina Department ofEnNironmental
nRTF nRrn vn
n.p-m—t 0 Environmental quality Quality
UST Section: MooresAle Regional Office
(7Cl4) 23i-21 R2 (nffiir�l
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hlWs:Hdeq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-
program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deu.nc. cov/about/divisions/waste-manacement/waste-management-rules-data/waste-management-cis-maps
File Review Procedures:
hM2s:Hdeq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
httDs:Hedocs.dea.nc. cov/WasteManacement/Search.asnx
Document Submittal & UST File Names for Laserfiche Policies:
httDs:Hfiles.nc. cov/ncdea/Waste%20Manaeement/DWM/UST/Corrective%20Action/Electronic%20Document%20Submittal
%20Memo%20Update.pdf
https://files.nc.cov/ncdea/Waste%20Manaeement/DWM/ JST/Corrective%20Action/UST%20file%20names%20for%20Las
erfiche.docx
From: Steven Irminger [mailto:steveirminger@gmail.com]
Sent: Wednesday, July 31, 2019 9:20 AM
To: Beverly, Trudy <trudy.beverly@ncdenr.gov>
Subject: [External] LSA Byrum Property Incident 40792
ernal email. Do not click links or open attachments unless you verify. Send all suspicious email as an
�chm�o report.spam@nc.gov
Good Morning Trudy,
Hope you are having a good summer. Please find attached an LSA for the Byrum Property located at
5628 Closeburn Road, Charlotte, NC(Incident 40792).
Soil contamination was discovered in 2018 during due diligence assessment of a heating oil UST. The
UST was closed by removal this spring and impacted soil was removed. However, confirmation soil
sampling revealed concentrations exceeding soil -to -groundwater. The LSA did not encounter
groundwater above bedrock. Using air rotary methods, a well was installed to 45-feet below
grade. This well produced water which was sampled for the LSA. Naphthalene was reported at 1.0
ug/L and chromium at 6.3 ug/L. No other parameters reported above the sample detection limit.
This incident should qualify for closure with no land use restrictions.
Hopefully, an easy review on your part. The owner is trying to complete a real estate deal so your
speedy review would be much appreciated. Please call me with any questions.
Do you need a hard copy?
Steve Irminger
704-701-9099