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3412_Forsyth_OldSalisburyRoad_CDLF_GW_FID1336847_20190726
I pENR USE ONLY ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No) Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records' as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): HDR Engineering, Inc. of the Carolinas Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Eric A. Wright Phone: 704-338-6719 E-mail: eric.wright@hdrinc.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Old Salisbury Road landfill 3336 Old Salisbury Road 34-12 .0500 May 7-10, 2019 and Winston-Salem, NC 27127 May 29-31, 2019 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring �X Detection Monitoring �X Assessment Monitoring Corrective Action T e of data submitted: (Check all that apply) X Groundwater monitoring data from monitoring wells Fx Methane gas monitoring data Groundwater monitoring data from private water supply wells ❑ Corrective action data (specify) Leachate monitoring data Other(specify) X Surface water monitoring data Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Eric A. Wright A . Project Engineer 704-338-6719 Facility Representative Na Title 7/16/2019 Date 440 South Church Street Suite 1000 Charlotte NC 28202 Facility Representative Address F-0116 NC PE Firm License Number (if applicable effective May 1, 2009) (Area Code) Te ♦♦� ;` r v11 -�� L 01 027 •'•FNGiNE�Q.0 0 /I ••••..•.•• N / I., �A Nt Engineer Seal oo.A-4 910nna F)I Winston-Salem • Forsyth County City/County Utilities Water • Sewer • So€id Waste Disposal HDR Project No. 10125427 Wn', Assessment Monitorina Report Groundwater and Surface Water Sampling Event — May 2019 Old Salisbury Road Landfill NCDEQ Permit NO. 34-12 Forsyth County, North Carolina July 2019 This page intentionally left blank. Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report Contents Contents 1 General...............................................................................................................................1 1.1 Facility Background...................................................................................................... 1 1.2 Regulatory Authority.................................................................................................... 1 1.3 Assessment Monitoring................................................................................................ 1 1.4 Geologic Characteristics.............................................................................................. 3 1.4.1 Regional Geologic and Hydrogeologic Setting ...................................................... 3 1.4.2 Site Specific Topography and Drainage................................................................ 3 1.4.3 Site Specific Hydrogeology................................................................................... 3 2 Monitoring Network.............................................................................................................4 3 Data Collection................................................................................................................... 5 3.1 Water Level Measurements......................................................................................... 5 3.2 Groundwater Flow........................................................................................................ 6 3.3 Sample Collection and Analysis................................................................................... 7 4 Analytical Results................................................................................................................ 8 4.1 Groundwater................................................................................................................8 4.2 Surface Water.............................................................................................................. 9 4.3 Landfill Gas.................................................................................................................12 5 Summary & Conclusions....................................................................................................12 Tables Table 1 Existing groundwater monitoring well details................................................................. 4 Table 2 Sampling parameters and schedule.............................................................................. 5 Table 3 Groundwater elevations................................................................................................ 6 Table 4 Hydraulic gradient and flow velocity.............................................................................. 7 Table 5 Lab detections — May 2019..........................................................................................10 Table 6 Field parameters — May 2019.......................................................................................11 Table7 Gas Readings..............................................................................................................12 Figures Figure 1 Groundwater contours and sample locations................................................................ 2 Figure 2 Historical groundwater elevations................................................................................. 6 Figure 3 MW-2R groundwater detections................................................................................... 9 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Contents Appendices Appendix A — Summary of Monitoring Results Appendix B — Laboratory Reports Appendix C — Field Data Appendix D — Electronic Files Acronyms 213 15A NCAC Subchapter 02B — Surface Water and Wetlands Standards 2L 15A NCAC Subchapter 02L - Groundwater Classification and Standards pg/L micrograms per liter EPA United States Environmental Protection Agency MCL Maximum Contaminant Level MDL method detection limit NC DENR North Carolina Department of Environment and Natural Resources' NCDEQ North Carolina Department of Environmental Quality' ND not detected in sample NE standard not established NS not sampled NTU Nephelometric turbidity units PCB polychlorinated biphenyl PCE tetrachloroethene PRL practical reporting limit PVC polyvinyl chloride SVOC semi -volatile organic compound VOC volatile organic compound USGS U.S. Geological Survey Prior to September 18, 2015, the NCDEQ was referred to as the NC DENR. Both naming conventions are used in this report, as appropriate. Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� General 1 General HDR Engineering, Inc. of the Carolinas (HDR), on behalf of the Winston-Salem City/County Utility Commission (the City), is submitting this Assessment Monitoring Report for the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North Carolina. 1.1 Facility Background OSR covers approximately 56 acres within a 140-acre tract north of Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The Forsyth/Davidson County line borders the site to the south (Figure 1). The facility was issued a permit to operate on July 3, 1996 and opened in August of the same year. 1.2 Regulatory Authority OSR is currently operating under North Carolina Department of Environmental and Natural Resources (NC DENR) facility permit number 34-12 dated April 6, 2015 (DIN 23258). Groundwater monitoring and reporting requirements are outlined in items 36 to 45 of the permit. NC Solid Waste Management (SWM) Rules 15A NCAC 13B .0544(b) and .0544(c) define the requirements applicable to groundwater and surface water monitoring plans for OSR, respectively. The groundwater monitoring plan was approved by NC DENR on March 5, 2015 (DIN 23910). 1.3 Assessment Monitoring OSR is in assessment monitoring due to exceedances of Groundwater Quality Standards, as specified in 15 NCAC 02L .0202 (2L Standards), for benzene and tetrachloroethene (PCE) detected in well MW-2R during 2011. On December 9, 2011, an Assessment Monitoring Plan for MW-2R was submitted in accordance with 15A NCAC 1313. This plan was approved with two exceptions on January 17, 2012. The first exception required the location of MW-15 to be in the same flow path as MW-2R; the second required all wells to be sampled for 40 CFR Part 258 — "Appendix II List of Hazardous Inorganic and Organic Constituents" (Appendix II) constituents. In February 2014, the City requested, and NC DENR approved, the following modifications to the facility's Assessment Monitoring Plan. • Groundwater monitoring wells MW-1 R, MW-2R, MW-4R and MW-15 will be sampled semi-annually for Appendix I and the previously detected Appendix II constituents; • All fourteen groundwater monitoring wells (including MW-1 R, MW-2R, MW-4R and MW- 15) will be sampled during every other Fall event (odd years) for the entire Appendix II constituent list. • Additional Appendix II constituents detected during these events will be added to the sampling program for subsequent semiannual events. In January 2016, HDR recommended changes to the semi-annual sampling schedule. North Carolina Department of Environmental Quality (NCDEQ) approved sampling for additional detected parameters. The request to remove selected parameters from the sampling schedule was denied. On May 29, 2018, NCDEQ added 1,4-Dioxane (p-Dioxane) to the sampling plan for all wells on a semi-annual basis with a 2L Standard of 3 pg/L. SURVEY BOUNDARY �`1 �-'�iILNI I1II . �!�IIIII� 7 LEGEND EXISTING CONTOURS - - - - PROPERTY BOUNDARY PERMIT/PHASE BOUNDARY 735 GROUNDWATER CONTOURS SURVEY BOUNDARY EXISNNG ABANDONED MONITORING WELLS (MW & OW) 00 METHANE PROBES (MM) SW-1 SURFACE WATER APPROXIMATE GROUNDWATER FLOW - NOTES 1. SITE TOPOGRAPHIC INFORMATION FOR A PORTION OF I & II AND ALL OF PHASES III -VI & SURROUNDING AREA PROVIDED BY CARTOGRAPHIC AERIAL MAPPING, INC. FOR THE • MM-10 BRADY SURVEYING COMPANY DATED JAN. 3, 41. SW-2 2014. THE REMAINING SITE TOPOGRAPHIC INFORMATION PROVIDED BY CARTOGRAPHIC AERIAL MAPPING INC. FOR BRADY SURVEYING COMPANY DATED JAN. 3 2011. 2. PROPERTY BOUNDARY TAKEN FROM DATA SUPPLIED BY BRADY SURVEYING, INC. DATED MARCH 14, 1994. 728.96 3. GROUNDWATER ELEVATIONS ARE IN MEAN SEA MW-11 LEVEL, MEASURED ON MAY 29, 2019 (SHOWN NEXT TO WELL LABEL). 4. MW-15 IS NOT USED TO DEVELOP THE GROUNDWATER SURFACE SHOWN DUE TO IT BEING INSTALLED IN BEDROCK. MM-11 SCALE IN FEET \ \ 734.13 200 100 0 200 400 MW-12 1 "=400' LANDFILL PERMIT BOUNDARY � - 7\ x MM 12 \ \ 743.15 I PROPERTY LINE -765� MW-13I � 7 SW-4 - - 765.11 j/ 1 `- F�2 , .. PROJECT TITLE OLD SALISBURY ROAD C & D LANDFILL SHEET TITLE GROUNDWATER CONTOURS AND SAMPLE LOCATIONS SPRING 2019 PROJECT NUMBER 10125427 PROJECT MANAGER M. PLUMMER, P.E. DATE MAY 2019 REFERENCE SHEET LAYOUT 2 REFERENCE DOCUMENT 00D-03 EXHIBIT NUMBER FIGURE 1 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� General 1.4 Geologic Characteristics This section paraphrases the descriptions in the original July 2003 Ground Water Monitoring Plan and the 2003 Design Hydrogeologic Investigation Report. 1.4.1 Regional Geologic and Hydrogeologic Setting Per the 1985 Geologic Map of North Carolina, OSR is located in the Charlotte belt of the Piedmont Physiographic Province. This province is characterized by metamorphic and igneous plutonic rocks, which have been extensively weathered and eroded, forming an undulating topography. Subsurface conditions generally consist of topsoil underlain by residual soils, saprolite, partially weathered rock (PWR), and fractured rock. There is generally a gradual transition between material types with varying thickness. Bedrock is typically fractured granodiorite overlain by PWR, overlain by highly weathered bedrock (saprolite). Saprolite varies in thickness from a few feet to over 100 feet. Saprolite retains some of the original (relict) structural features of the parent rock. The near surface residual soils are formed by physical and chemical weathering of the saprolite and usually do not retain the relict structural features. Groundwater is present within fractures and joints in the bedrock and within the pore spaces of the overlying-saprolite and residual soils. Groundwater is primarily recharged by precipitation and commonly located within the saprolite layer. Groundwater moves laterally toward streams and surface water bodies and generally follows the surface topography. 1.4.2 Site Specific Topography and Drainage Surface drainage at OSR is primarily controlled by a north -northwestern trending ridge within the property. This ridge directs runoff northeast, west and southwest into tributaries of South Fork Muddy Creek. The majority of surface runoff is directed to South Fork Muddy Creek to the north. A small area on the southeast portion of the site drains south into Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow to the west where they converge with Muddy Creek and eventually discharge to the Yadkin River. 1.4.3 Site Specific Hydrogeology As documented in the Design Hydrogeological Investigation Report submitted by HDR on December 2, 2003, the uppermost aquifer underlying the facility is comprised of three stratigraphic units. The stratigraphic downward progression of the three units is saprolite transitioning into PWR, then bedrock. Groundwater flows through the pore space of the saprolite and PWR, while groundwater flow through the bedrock is primarily through fractures. OSR was constructed within the unconsolidated micaceous silty sands and sandy silts produced by the in -situ weathering of the granodioritic parent rock. There is no evidence of discrete flow patterns resulting from relict quartz veins, dikes, healed fractures, or strong preferential alignment of minerals (i.e., foliation). In general, groundwater flows from areas of higher elevation to areas of lower elevation. As such, the water table generally mimics the topography. Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Monitoring Network 2 Monitoring Network The monitoring network consists of fourteen groundwater wells and four surface water sampling points. Sampling of site monitoring wells and surface water monitoring locations is conducted on a semi-annual basis. Details of monitoring wells are provided in Table 1. Groundwater monitoring well MW-1 R is located hydraulically upgradient of the landfill and is considered as the background well for the site. Upstream surface water (SW-1) and downstream surface water (SW-2) samples are obtained from the adjacent stream to the east. Two surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity of MW- 2R. SW-3 is located south of the entrance road near MW-2R; while SW-4 is located on the north side of the entrance road, downstream of SW-3. Table 1 Existing groundwater monitoring well details Depth: Top Of NC Sate NC Sate Well Well Depth Ground to Screened Screened Casing Ground OSR LF Plane Plane Diameter (below Top of Interval Interval Elevation Elevation WELL Installed Northing Easting (inches) ground) Screen (ft) Geology (ft MSL) (ft MSL) MW-1R 12/27/1995 820,411 1,622,983 2 60.0 45 15 Granitic saprolite 836.42 833.40 MW-2R 12/29/1995 820,974 1,622,722 2 23.0 8 15 Granitic saprolite 785.22 781.81 MW-3R 7/7/1999 821,237 1,621,463 2 27.0 12 15 Granitic saprolite 776.60 772.90 MW-4R 12/28/1995 820,435 1,621,428 2 20.0 5 15 Granitic saprolite 767.96 765.70 MW-5R 12/29/1995 820,137 1,622,130 2 32.0 17 15 Granitic saprolite 784.36 782.30 MW-7 12/28/1995 820,886 1,621,424 2 48.0 33 15 Granitic saprolite 803.66 802.10 MW-8 7/7/1999 821,930 1,621,485 2 27.0 12 15 Granitic saprolite 762.50 759.80 MW-9 8/11/2004 822,311 1,621,986 2 60.0 45 15 Sand 790.28 788.04 MW-10 8/10/2004 822,626 1,622,699 2 21.0 6 15 Sand 738.21 735.70 MW-11 8/10/2004 822,307 1,622,838 2 20.0 5 15 Sand 732.59 730.35 MW-12 8/9/2004 821,844 1,622,955 2 16.0 6 10 Silt 739.07 736.41 MW-13 8/9/2004 821,500 1,622,915 2 20.0 5 15 Sand 751.23 749.19 MW-14 8/11/2004 822,420 1,622,260 2 60.0 45 15 Sand 783.88 781.44 MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58 MW-6R 7/8/1999 821,079 1,622,430 2 60.0 45 15 PWR 820.40 817.80 The sampling plan for OSR is provided in Table 2. This plan requires full Appendix II sampling for all wells every two years, and sampling for Appendix I and detected Appendix II constituents during the other events. Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report Data Collection FN Table 2 Sampling parameters and schedule Method Parameter(s) Frequency Monitoring Surface Wells Water EPA 300.0 Sulfate 2x/year 2x/ ear All All All All EPA 6010 Trace Metals Mercury Pesticides: All EPA 7470 2x/ ear All All Fall of odd years 2019 All None Pesticides recently detected: EPA 8081 4,4'-DDD, 4,4'-DDT, Aldrin, alpha-BHC, MW-1 R, MW-2R, delta-BHC, Endosulfan I, Endosulfan 11, 2x/year MW-4, MW-7, None Endrin, Endrin aldehyde, Heptachlor, MW-10 & MW-15 Heptachlor epoxide & Methox chlor EPA 8082 PCBs: All Fall of odd years 2019 All None Herbicides: All Fall of odd years 2019 All None Herbicides previously detected: 2x/year MW-1 R, MW-2R, None EPA 8151 2,4,5-TP (Silvex), 2,4-D MW-4R & MW-15 App I VOCs + Tetrah drofuran 2x/ ear All All Appendix 11 VOCs Fall of odd years 2019 All None EPA 8260 Apendix II VOCs recently detected: Dichlorodifluoromethane 2x/year All None 1,4-Dioxane 2x/ ear All All SVOCs: All Fall of odd years 2019 All None SVOCs recently detected: EPA 8270 Benzo(a)anthracene, Bis(2- MW-1 R, MW-2R, ethyl hexyl)phthalate, Chrysene 2x/year MW-4R , MW-3R SW-2 Dibenz(a,h)anth race ne, & Indeno(1,2,3- & MW-15 cd)pyrene SM 2320B Alkalinity 2x/year All All SM 2540C Total Dissolved Solids 2x/year All All SM 4500 Chloride, Cyanide, Sulfide 2x/ ear All All Field Temperature, Specific conductance, 2x/year All All Dissolved Oxygen, Redox, Turbidity, pH Field Total well depth, static water level 2x/ ear All NA 3 Data Collection 3.1 Water Level Measurements On May 7, 2019, static groundwater level measurements were obtained from groundwater monitoring wells MW-1 R through MW-5R and MW-7 through MW-15. Groundwater depths were measured from the top of the PVC casing. Groundwater is measured to the nearest 0.01 foot prior to purging each well. Depth to water data is used to calculate static groundwater elevations. Groundwater elevations from this event are presented in Table 3. Historic groundwater elevations are depicted on Figure 2. 5 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection Table 3 Groundwater elevations Well ID Top of Ground Well Screen Depth to Groundwater Casing Elevation Depth Length Water Elevation Elevation (ft MSL) (ft bgs) (ft) (ft) (ft MSL) (ft MSL) MW-1 R 836.42 833.40 60 15 33.87 802.55 MW-2R 785.22 781.81 23 15 6.75 778.47 MW-3R 776.60 772.90 27 15 14.11 762.49 MW-4R 767.96 765.70 20 15 5.64 762.32 MW-5R 784.36 782.30 32 15 9.41 774.95 MW-7 803.66 802.10 48 15 34.25 769.41 MW-8 762.50 759.80 27 15 10.43 752.07 MW-9 790.28 788.04 60 15 51.63 738.65 MW-10 738.21 735.70 21 15 10.23 727.98 MW-11 732.59 730.35 20 15 3.63 728.96 MW-12 739.07 736.41 16 10 4.94 734.13 MW-13 751.23 749.19 20 15 8.08 743.15 MW-14 783.88 781.44 60 15 50.49 733.39 MW-15 802.85 800.58 48.2 15 37.74 765.11 ID - identification ft - feet MSL - mean sea level bgs - below ground surface �l���l��r������r7"Ir�lr�" �� �II"r„ ■"I pTw-w M. s�.a����e�9� ■�"iiiiri��ii�iiiiiiiiiiiiiii�iiiiiiiiiii�ii■ Figure 2 Historical groundwater elevations 3.2 Groundwater Flow Hydraulic gradients were calculated between representative well pairs. The flow velocities have been calculated based on the values for historic hydraulic conductivity (0.466 ft./day) and effective porosity (25 percent), as presented in Table 2-9 of the December 2003 OSR Design Hydrogeologic Investigation Report for the landfill. Hydraulic gradients and flow velocities are presented in Table 4. 6 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection The minimum and maximum values are based on the historic data collected from the site beginning in May 2003. HDR estimates a travel time of about four years between MW-2R and MW-15, based on the estimated flow rate of 49 ft/yr and a distance of 195 feet. Table 4 Hydraulic gradient and flow velocity Hydraulic Based on Historic Gradient Record Flow Velocity MinimumLMaximum Nov 2016 May 2017 Nov 2017 May 2018 Nov 2018 May 2019 (ft./yr.) MW-1 R to 0.026 - ' 0.028 0.027, 0.027 - 0.027 - 0.027 '� 0.026/ MW-4R i 19 19 18 18 MW-1 R to 0.038 0.040 0.04 0.03 0.04 0.03 0.03 MW-2R / 26 27 27 2627 26 26 7�%6 MW-2R to 0.063 0.0 0.06 0.06 0.06 MW-13 1742 43 42 42 43 MW-13 to 0.013 0.015 0.01 0.01 0.01 0.01 0.01 0.01 MW-10 9 10 9 9 10 10 10 9 MW-2R to 0. 0.068 MW-15 47 3.3 Sample Collection and Analysis HDR collected samples from the fourteen wells and four surface water locations between May 7 and May 31, 2019, during two sampling events. The first event occurred over the four -day period (May 7-10, 2019) and the second over a three-day period (May 29-31, 2019). The first event included collection of sulfate, trace metals, mercury, semi -volatile organic compounds, alkalinity, TDS, chloride, cyanide and sulfide samples. In addition, the synoptic groundwater elevations were measured on May 7, 2019. Pesticides, herbicides and VOCs samples were collected during the second event. Samples were sent to Pace Analytical Laboratories, Inc. (Pace) of Huntersville, North Carolina (NC Cert. # 5342) for analysis. Low -flow sampling techniques were used to purge groundwater from each well until stabilization of field parameters (pH, conductivity, redox, temperature, turbidity, and dissolved oxygen) occurred. Samples were collected from each of the groundwater wells using the dedicated QED TM MicroPurge® pumps that were installed in August 2004, except MW-15, which is sampled with a variable speed submersible pump. Field parameters were recorded and are presented in Appendix B. Groundwater samples were labeled with the project name, sample ID, date, and time the sample was collected. This same information was recorded on a chain -of -custody form. The samples were placed in a cooler chilled with ice, then transported under chain -of -custody procedures to Pace. 7 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report Analytical Results 4 Analytical Results 1.1 Groundwater During this sampling event, 33 detections exceeded the 2L Standards. These exceedances consisted of ten parameters at ten well locations. The constituents detected above 2L Standards for this event are: • Cobalt in MW-2R, MW-3R, MW-4R, MW-10, MW-11, and MW-12 • Iron in MW-2R, MW-3R, MW-4R, MW-10, MW-11, MW-12, and MW-15 • Manganese in MW-2R, MW-3R, MW-4R, MW-7, MW-10, MW-11, MW-12, and MW-15 • Vanadium in MW-5R • Mercury in MW-1 R • Benzene in MW-2R • Methylene Chloride in MW-7 • Tetrachloroethene in MW-2R • 1,4-Dioxane in MW-4R, MW-10, and MW-12 • Total dissolved solids in MW-2R, MW-3, MW-10 and MW-12 Detections during this sampling event are presented in Table 5. Field parameters are presented in Table 6. Historical detections are presented in Appendix A. A copy of the laboratory report is provided in Appendix B. The field data sheets are provided in Appendix C. A Microsoft Excel file containing the analytical data in NCDEQ electronic data deliverable format is included as part of Appendix D. In 2011, MW-2R analytical detections of benzene and PCE above groundwater standards triggered assessment monitoring. The trends of constituents that have detections in MW-2R are shown on Figure 3. 8 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Analytical Results MW-211 Groundwater Detections OSRConstruction & Demolition Landfill Permit 34-12 loououuo 10000DO 100000 10000 J e 1000 e m c 0 100 7o 7 0.1 .0 N-N Date Collected Figure 3 MW-2R groundwater detections 4.2 Surface Water —f- Total Dissolved Solids Alkalinity. Total as CaCO3 —if5odium Manganese me —Iron +Barium " Tetrahydrofuran --X—C o ba It —#—Benzene 1.4-Dioxane (p-Dioxane) Tetrachloroethene Vinyl chloride —4--Methyiene Chloride Surface water analytical results were compared to 15A NCAC 02B (213 Standards). The 213 Standards do not provide criteria for alkalinity or iron, so the EPA's Nationally Recommended Water Quality Criteria for Class C freshwater was applied. There were no 213 exceedances, however all locations exceeded the Class C standard for alkalinity and all locations except for SW-1 exceeded the Class C standard for iron. Detections during this sampling event are presented in Table 5. Field parameters are presented in Table 6. Historical detections are presented in Appendix A. A copy of the laboratory report is provided in Appendix B. The field data sheets are provided in Appendix C. A Microsoft Excel file containing the analytical data in NCDEQ electronic data deliverable format is included as part of Appendix D. 9 This page intentionally left blank. Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report Analytical Results Table 5 Lab detections - May 2019 2B 250000 250000 Wg/L 21000 700 Wg/L 6.5 4 Wg/L 11 10 Wg/L NE 1 pg/L NE 1000 pg/L 1DDD 300 pg/L NE 50 pg/L 25 100 pg/L NE NE pg/L NE 0.3 pg/L NE 1000 pg/L EPA 3DD_D Sulfate EPA 6D1 DID Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Sodium Vanadium Zinc EPA 7470A Mercury EPA 8260D 1 95100 1210 163000 9620 12800 6560 295 260 320 216 55.9 169 47.9 217 0.61 5.4 3.5 235000 22300 149000 1 5910 65.6 100 200 138 234 0.6 0.61 Ab 45900 7970 13500 43600 1 273 29.8 109 95.6 1 12.61 11.6 9.6 , M 63.5 148 MI 42.3 362 ® 889370 13000 38i0� 19.5 3.3 7.1 ®i 5.2 39.3 ®i 48.5 680 7990 7710 13.4 8.4 7.2 6.2 4.4 6.9 4.4 15800 57300 2540 71200 13000 17500 9620 14100 136000 12900 20700 9940 17400 23000 19400 12300 34000 22000 4.5 5.2 18 5.9 5.1 90.1 NE 6 pg/L 1,1-Dichloroethane 2000 6000 pg/L Acetone 1.19 1 pg/L Benzene NE 70 pg/L cis-1,2-Dichloroethene 0.9 NE 1000 pg/L Dichlorodifluoromethane 670 500 pg/L m&p-Xylene 11000 3 pg/L Methylene Chloride NE 500 pg/L o-Xylene 0.7 D_7 pg/L Tetrachloroethene 0.43 1.3 0.68 0.67 1.5 1 0.68 0.33 0.33 DA 1.4 3 029 0.52 0.73 110DD0 NE pg/L Tetrahydrofuran 51.3 11.4 80.4 113 9-21 1 6.1 2.5 3 pg/L Trichlorcethene I 0.97 2 NE 2000 Wg/L Trichloroflucromethane EPA 8260B Mod_ 1.7 0.81 0.92 NE 3 Wg/L 1,4-Diaxane(p-Dicxane) 2.3 ffffffff, _� � ® 1.3 1.3 SM 232OB �� i 200DD NE pg/L Alkalinity, Total as CaC0�3 83800 j7000 488000 12900i] 29200 5 _A500 29700 506000 154000 176000 52800 64900 74200 22300 54900 413000 26 SM 2540C NE 500000 pg/L Total Dissolved Solids 202000 1 i i 1 1 i i 11 167000 175000 192000 170000 190000 I 236000 i 11 i 115000 163000 448000 174000 182000 668000 4-0 SM 45O[)LCI-E 6470 4290 230000 250000 pg/L Chloride 9770 42300 44604 1 2220 15600 6930 1 65100 12300 34000 6290 3870 115000 55400 19400 28000 1 SM 45DD-CN-E 5 70 Wg/L Cyanide 7.2 SM 45DaS2D _ NE NE Wg/L Suffide Note - To distinguish non detections (ND) from not sampled (NS), refer to complete laboratory analysis. This table represents both ND and NS as blanks. 347 1 56.8 13. 10 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report Analytical Results Table 6 Field parameters - May 2019 pmhos/cm Field Specific Conductance 232 1262 427.7 1304 mg/L Oxygen, Dissolved 1.72 1.16 2.06 0.98 my REDOX -34.4 -80.4 -103.9 -50.1 NTU Turbidity 2.9 9.9 53.2 13.8 Std. Units Field pH 5.3 6.1 6.3 6.0 feet Static Water Level 33.87 6.75 14.11 5.64 60 21 27 20 Total Well Depth deg C Field Temperature 18.9 15.9 15.7 14.9 184.1 234 1 85.5 1 1167.21 1648 1 375.9 780 142 199.2 611 226.3 213.2 1172 735 6.04 0.58 7.51 6.01 3.32 6.01 4.30 4.26 1.82 1.90 4.49 7.32 1.85 5.35 2.9 53.5 6.5 -3.6 -280 -299 -217 -80.6 -47.1 -35.2 173.3 -63.5 -52.7 -43.2 6.5 0.6 1.7 6.3 17.2 10.0 1.5 2.5 1.7 14.3 18.8 40.5 34.5 30.5 5.9 5.3 5.2 5.2 6.3 5.8 5.8 5.3 5.2 6.1 6.7 7.4 6.4 6.9 9.41 34.25 10.43 51.63 10.23 3.63 4.94 8.08 50.49 37.74 30 48 27 60 21 20 15.7 20 60 48 16.4 16.3 15.3 17.4 19.8 15.8 1 16.1 15.6 1 17.4 1 18.81 17.5 1 23.4 1 14.91 19.3 11 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Summary & Conclusions 4.3 Landfill Gas Landfill gas is measured at MW-2R and wells in the vicinity of MM-1 during each groundwater sampling event. The results indicate the presence of carbon dioxide above ambient levels in MM-1. The City is responsible for quarterly sampling of all methane monitoring wells and the related reporting, which is not included in this document. Gas readings taken during this event are presented in Table 7. Table 7 Gas Readings Date ID # CH4 (%) CO2 (%) 02 (%) Balance 21-May-18 MM-1 0.0% 40' , 16.3% 79.7% 21-May-18 MW-13 0.0% 0.1% 20.0% 79.9% 21-May-18 MW-15 0.0% 0.3% 20.0% 79.7% 21-May-18 MW-1R 0.0% 0.0% 20.4% 79.6% 21-May-18 MW-2R 0.0% 0.0% 20.3% 79.7% 26-Nov-18 MM-1 0.0% 4' . 18.0% 77.6% 26-Nov-18 MW-13 0.0% 0.2% 19.9% 79.9% 26-Nov-18 MW-15 0.0% 0.2% 19.8% 79.8% 26-Nov-18 MW-1 R 0.0% 0.1 % 20.2% 79.7% 26-Nov-18 MW-2R 0.0% 0.6% 22.6% 76.8% 6-May-19 MM-1 0.0% 4.6% 14.5% 80.9% 6-May-19 MW-13 0.0% 0.0% 20.1 % 79.9% 6-May-19 MW-15 0.0% 0.3% ' . 80.3% 6-May-19 MW-1 R 0.0% 0.0% 20.0% 80.0% 6-May-19 MW-2R 0.0% 0.0% 19.7% 80.3% Highlighted cells are outside of normal atmospheric ranges 5 Summary & Conclusions Three wells exceeded the 2L Standard for 1,4-Dioxane for this event. The Appendix 11 pesticides (heptachlor and heptachlor epoxide) were not detected during the May 2019 event. They were last detected during the November 2016 sampling event. Other detections from this event are generally consistent with previous events. No changes to the current plan are recommended at this time. 12 Winston-Salem City/County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Summary & Conclusions This page intentionally left blank. 14 Winston-Salem City/County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report Appendix A — Summary of Monitoring Results A AppendixA— Summary of Monitoring Results Appendix II Detections Detections by Well Location Detections by Date Surface Water Detections Winston-Salem City/County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. Al 50 pg/L 50 pg/L 70 pg/L 70 pg/L 70 pg/L 0.3 pg/L 0.3 pg/L 40 pg/L 40 pg/L 40 pg/L 0.008 pg/L 0.008 pg/L 0.004 pg/L 0.004 pg/L NE Pg/L NE Ng/L NE Pg/L NE Ng/L 40 pg/L 40 pg/L 200 pg/L 200 pg/L 1000 pg/L 1000 pg/L 0.005 pg/L 0.005 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Column Labels 0 ti Row Labels 2 o z a)i '' ao o 0 o z z z Herbicides ' '_IIIMEMMEIM �mm mm ' . MENNEN EMENEEMEMEMENIN '- ..• - . Equipment sticides •. Heptachlor 0.21 OM12MEMEN M 0.09 0.17 emi CsMENEM MEMENIN . • • .. • - _ MENNEN MENIMMEME _• - • - . : • - . MEMEMEMEMMEME Benzo(g,h,i)perylen-.■■■■■■■■■■■■®■ MW-4R Dibenz(a,h)anthracene MEMEMEMEMEMEME -_________ 1 ___MM W-S GW Revised.xlsb 1 of 7 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard IVICIL•-abels .• 100 pg/L 100 pg/L 100 pg/L 0.05 pg/L 0.05 pg/L 6 pg/L 6 pg/L 6 pg/L 0.4 pg/L 0.4 pg/L 6 pg/L 6 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 40 pg/L 40 pg/L 40 pg/L 40 pg/L 40 pg/L Row Labels 7. Di-n-octylphthalate MW-8 5.6 MW-12 5.6 Indeno(1,2,3-cd)pyrene MW-3R • 1,1-Dichloroethane 0.53 MW-2R 0.43 0.39 0.54 0.48 0.48 0.49 1.1 0.83 1.3 1.2 MW-7 1.3 1.3 1.1 1.6 1.4 1.3 1.5 1.2 0.91 1.1 1.3 0.81 0.9 0.8 1,2-Dichloroethane MW-2R 1 0.24 1,4-Dichlorobenzene MW-2R 1 0.41 0.37 0.46 0.39 0.38 0.4 1,4-Dioxane p-Dioxane MW-2R 2.3 2.1 M W-4 R 2.4 M W-7 2 MW-10 MW-12 SW-2 1.3 SW-3 1.3 2-Hexanone 0.5 MW-2R MW-10 0.72 0.69 0.96 SW-2 1.8 SW-4 3.1 W-S GW Revised.xlsb 2 of 7 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard NE pg/L 4-Methyl-2-pentanone (MIBK) 0.65 2.8 NE pg/L MW-10 1.7 1.1 2.5 2.6 5.6 2.2 6000 pg/L Acetone 10.2 18.3 6000 pg/L Equipment 6000 pg/L MW-2R 10.3 6000 pg/L MW-3R 21.4 6000 pg/L MW-4R 11 6000 pg/L MW-5R 18.4 6000 pg/L MW-7 15.7 6000 pg/L MW-8 15.8 6000 pg/L MW-10 16.4 13.7 12.1 22.5 14.1 11.8 6000 pg/L MW-11 21.1 6000 pg/L MW-12 12.1 6000 pg/L MW-13 17.3 6000 pg/L MW-14 14.7 6000 pg/L MW-15 13.2 6000 pg/L SW-1 11.2 6000 pg/L SW-2 12.9 6000 pg/L SW-3 16.2 6000 pg/L SW-4 16 1 pg/L Benzene 1 pg/L MW-2R • 1 pg/L MW-4R 0.38 0.42 0.28 0.3 1 pg/L MW-7 0.68 0.37 0.41 0.39 0.38 0.43 0.42 0.26 0.29 1 pg/L MW-10 0.33 0.55 0.55 0.57 0.52 0.83 0.46 0.44 1 pg/L MW-12 0.33 1 pg/L SW-3 0.731 0.42 0.541 0.32 0.9 20 W-S GW Revised.xlsb 3 of 7 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard 700 pg/L Disulfide 700 pg/L _Carbon MW-10 T 3000 pg/L Chloroethane 3000 pg/L MW-2R 70 pg/L Chloroform 70 pg/L MW-15 3 pg/L Chloromethane 3 pg/L MW-2R 3 pg/L MW-7 3 pg/L MW-11 3 pg/L SW-2 70 pg/L cis- 1,2-DichloroethenE 70 pg/L MW-1 R 0.9 70 pg/L MW-2R 0.67 70 pg/L MW-7 1.5 70 pg/L MW-10 70 pg/L MW-12 0.4 70 pg/L SW-2 70 pg/L SW-3 1000 pg/L Dichlorodifluorometha 1000 pg/L MW-2R 1000 pg/L MW-7 1000 pg/L MW-9 1.4 1000 pg/L MW-12 1000 pg/L MW-14 3 600 pg/L Ethylbenzene 600 pg/L MW-1 R 600 pg/L MW-10 .abets 00 T 00 T r- T r- T r- ti T CO T (p (.0 T U-) T L T T 't T M T M T 1 O z 1 M 1 N 0 1 O z T 1 M 2 1 O z _______-- T > 1 M 2 1 O z 1 M 2 1 O z 1 cu 2 1 O z 1 cu 2 rEMENEENEENEENEms MENEENEEN MEMEMENESEN 1 �• 1 1. 1 1 0.23 1 0.85 1 : 1 1 • 16 1 0.38 0.55 0.66 16 0.51 0.47 1 • 1 1 1 1 1:6 1: 1 0.8 1 0.73 1 1 1 0.23 0.27 0.23 0.2 0.33 0.35 0.23 0.33 1 .26 ie .26 1• 0.99 1 :: 1 • 1 0.23 2.4 3.6 2.1 mi W-S GW Revised.xlsb 4 of 7 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard 500 pg/L m&p-Xylene 500 pg/L MW-7 1 500 pg/L MW-10 3 pg/L Methylene Chloride 3 pg/L Equipment Blank 3 pg/L MW-1 R 3 pg/L MW-2R 3 pg/L MW-3R 3 pg/L MW-4R 3 pg/L MW-5R 3 pg/L MW-7 3 pg/L MW-8 3 pg/L MW-10 3 pg/L MW-11 3 pg/L MW-12 3 pg/L MW-14 3 pg/L MW-15 3 pg/L SW-1 3 pg/L SW-2 3 pg/L SW-3 3 pg/L SW-4 6 pg/L Naphthalene 6 pg/L MW-2R 500 pg/L o-Xylene 500 pg/L MW-2R 1.1 1.7 1.6 1.4 0.68 1.3 1.1 2.4 1.7 1.1 500 pg/L MW-7 0.681 0.591 0.651 0.621 0.68 500 pg/L MW-10 0.28 0.53 0.78 1.1 0.97 1.2 2.2 1.2 2.1 0.46 0.63 1 2.1 1.81 1.1 0.68I 1.2I 1.1 1.1 1.8LM 2.3 1.3 2.3 2.3 2.9 2.11 2.9 1.1 2.8 1.2 1.4 2 2 1.6 2.4 2 1 1.2 1 0.9 1.3 0.33 0.31 0.5 0.5 0.47 0.27 0.4 0.36 0.3 0.43 0.85 0.65 W-S GW Revised.xlsb 5 of 7 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard 0.7 pg/L Tetrachloroethene 0.7 pg/L MW-2R 0.7 pg/L MW-7 0.48 0.7 pg/L MW-14 0.52 0.61 NE pg/L Tetrahydrofuran NE pg/L Equipment Blank 3.2 NE pg/L MW-2R 51.3 45.4 46 59.1 28 36.3 39.1 49.6 35.8 34.6 79.2 72.6 100 111 NE pg/L MW-4R 11.4 9.3 13.6 3.5 7 5.8 15.9 11.8 12 8.5 NE pg/L MW-7 80.4 50.5 24.9 20.1 32 21.7 13.5 17.7 14.1 8.8 5.2 14 24 NE pg/L MW-10 113 169 192 135 131 182 237 6.1 120 145 106 18.6 5 NE pg/L MW-11 4.5 NE pg/L MW-12 5.9 11.4 26.8 12.4 NE pg/L MW-15 9.2 14.8 12 16.8 27.3 19.8 16.9 15.5 21.4 15 7.4 NE pg/L SW-2 61.3 18.4 NE pg/L SW-3 6.1 3.4 6.3 3.3 10.2 9.7 19 5.1 NE pg/L SW-4 13.7 5.7 3.5 3.6 4.1 4.4 600 pg/L Toluene 0.27 600 pg/L MW-2R 600 pg/L MW-10 0.26 0.35 0.27 0.63 600 pg/L SW-2 0.52 3 pg/L Trichloroethene 3 pg/L MW-1 R 0.65 3 pg/L MW-2R 0.97 0.9 0.93 1.3 0.93 1 1.2 0.71 0.66 0.79 0.85 0.71 0.9 0.7 3 pg/L MW-7 0.58 W-S GW Revised.xlsb 6 of 7 Al 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 2000 pg/L 88 pg/L 88 pg/L 0.03 pg/L 0.03 pg/L 500 pg/L 500 pg/L 500 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Trichlorofluoromethane MW-2R MW-7 2 MW-9 1.7 MW-10 MW-12 0.81 MW-14 0.92 MW-15 SW-4 Vinyl acetate MW-2R Vinyl chloride MW-2R Xylenes (Total M W-7 MW-10 1.5 0.71 1 1.5 2.4 3.7 12 12 1.2 1.2 1.6 1.6 0.91 1.5 0.92 1.4 0.79 1.2 0.62 0.5 0.3 1.3 1.3 1.4 1.2 1.4 1 1.3 1.1 0.98 0.96 0.47 0.7 0.4 0.2 0.3 0.4 1 0.89 1.4 0.52 1 2.8 1.4 0.82 0.22 0.32 0.86 0.79 0.8 0.87 0.75 0.58 1.1 0.54 0.59 0.57 0.34 0.21 0.42 0.22 0.71 2.1 4.4 5.1 4.8 4.4 3.9 5.3 7.6 4.3 0.32 0.27 0.3 2 1.1 1.2 W-S GW Revised.xlsb 7 of 7 A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 3 pg/L 700 pg/L 250000 Ng/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300 pg/L 15 pg/L 50.0 pg/L 1 pg/L 3 pg/L 20 pg/L 20 pg/L NE pg/L 250000 Ng/L 600 pg/L 500000 Ng/L 3 pg/L 1000 Ng/L 6 pg/L 350 ug/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 Ng/L 40 pg/L 0.1 pg/L 6000 Ng/L 0.002 Ng/L NE pg/L 0.006 Ng/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 Ng/L 3000 Ng/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 Ng/L 70 pg/L 0.019 pg/L 1000 Ng/L 2 pg/L 2 pg/L 0.008 pg/L 300 pg/L 15 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value -. Column Labels Historical detections by 40 710 well location •MW-1 R 64300 Alkalinity, Total as CaCO3 83800 84100 76100 68600 54900 48100 39600 Arsenic Barium 285 284 263 260 272 241 228 207 164 Benzo(a)anthracene B i s(2-ethyl h exyl )phtha late Carbon Disulfide Chloride 9770 8920 9040 9290 8860 9630 9000 8510 7640 Chromium 4 Chrysene cis-1,2-Dichloroethene 0.9 0.85 0.71 0.8 0.62 0.38 0.2 Cyanide Ethylbenzene 0.38 Iron 111 43.1 54.8 96.2 78.8 82.8 Lead Manganese 19.5 16.7 17.6 11.8 12.5 7.3 7.2 2.8 Mercury 0.57 0.34 0.23 Methylene Chloride 2.3 Selenium Silver Sodium 15800 16500 15500 15200 15800 14600 13300 13200 11600 Sulfate 1380 1080 1070 1700 Toluene Total Dissolved Solids 202000 164000 166000 153000 165000 154000 138000 78000 133000 Trichloroethene 0.7 Zinc 5.2 5.1 5 5.5 5.7 5.6 MW-2R 1,1-Dichloroethane 0.43 0.39 0.5 0.48 0.48 653 0.49 1,1-Dichloroethene 1,2-Dichloroethane 0.24 1,4-Dichlorobenzene 0.41 0.4 0.46 0.39 0.38 1,4-Dioxane (p-Dioxane) 2.3 2.1 2,4,5-TP (Silvex) 0.072 0.14 2,4-D 0.43 2,4-Dinitrotoluene 5.9 2,6-Dinitrotoluene 8.1 2-Butanone (MEK) 2-Hexanone 4,4'-DDT Acetone 10.3 Aldrin Alkalinity, Total as CaCO3 577000 573000 663000 670000 587000 571000 482000 440000 358000 alpha-BHC Antimony Arsenic Barium 1 260 258 289 323 323 272 ;324 279 287 Benzene B i s(2-ethyl h exyl )phtha late Cadmium Chloride 42300 34500 42200 47600 50400 47600 47700 48700 44200 Chloroethane Chloroform Chloromethane 0.25 Chromium 3.3 2.7 2.8 2.6 cis-1,2-Dichloroethene 0.67 0.38 0.55 0.7 0.6 0.51 0.47 0.26 Cobalt . Copper 9.6 2.6 6.3 Cyanide 4.1 5 5.1 7.5 delta-BHC Dichlorodifluoromethane 0.26 Endrin Endrin aldehyde Heptachlor Iron .t Lead 3.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 1 of 36 A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 3 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300 pg/L 15 pg/L 50.0 pg/L 1 pg/L 3 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L 300 pg/L 15 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value -. Historical detections by well location MWA R Alkalinity, Total as CaCO3 37600 30000 28100 29800 26300 27100 27500 Arsenic Barium 142 124 106 109 91.7 93.8 82.6 Benzo(a)anthracene Bis(2-ethylhexyl)phthalate 2.4 Carbon Disulfide Chloride 7090 5600 5880 5910 5320 5350 Chromium Chrysene 1.5 cis-1,2-Dichloroethene Cyanide 4.4 Ethylbenzene Iron 85.8 52.9 Lead Manganese 2.9 Mercury Methylene Chloride Selenium Silver Sodium 10600 10800 9940 9080 9180 9440 7670 Sulfate 1720 Toluene Total Dissolved Solids 120000 91000 103000 84000 95000 93000 95000 Trichloroethene Zinc MW-2R 1.1 1.3 1.2 1.2 1,1-Dichloroethane 0.83 1.2 1.1 1,1-Dichloroethene 36.6 38.7 1,2-Dichloroethane 1,4-Dichlorobenzene 0.4 1,4-Dioxane (p-Dioxane) 2,4,5-TP (Silvex) 0.23 2,4-D 1.1 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Butanone (MEK) 2-Hexanone 0.48 4,4'-DDT Acetone 20.3 3.7 Aldrin Alkalinity, Total as CaCO3 453000 344000 349000 363000 277000 196000 219000 alpha-BHC Antimony Arsenic Barium 339 324 311 324 335 366 351 Benzene Bis(2-ethylhexyl)phthalate 1.1 Cadmium Chloride 49800 50500 56700 50000 64000 61500 62400 Chloroethane 2.1 Chloroform 0.16 0.26 Chloromethane Chromium 3.4 cis-1,2-Dichloroethene 0.5 0.38 0.41 0.26 0.25 0.33 0.46 Cobalt Copper 9.6 Cyanide 4.2 delta-BHC Dich lorodifluoromethane Endrin 0.27 Endrin aldehyde 0.23 0.28 Heptachlor Iron :� •� •:� Lead Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 2 of 36 A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 3 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300 pg/L 15 pg/L 50.0 pg/L 1 pg/L 3 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L 300 pg/L 15 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location -. MW-1 R Alkalinity, Total as CaCO3 Arsenic 5.8 Barium 92.8 74 85 90 105 81 94 82 78 48 95 96 460 120 100 130 280 87 Benzo(a)anthracene Bis(2-ethylhexyl)phthalate Carbon Disulfide Chloride Chromium 2 0.9 0.6 0.5 2 3.5 4.3 2.3 5 = 6.6 Chrysene cis-1,2-Dichloroethene Cyanide Ethylbenzene Iron Lead 10 Manganese Mercury Methylene Chloride Selenium 5.5 Silver 0.48 0.6 0.4 Sodium Sulfate Toluene 21 Total Dissolved Solids Trichloroethene Zinc MW-2R 1,1-Dichloroethane 1,1-Dichloroethene 1,2-Dichloroethane II A-Dichlorobenzene 1,4-Dioxane (p-Dioxane) 2,4,5-TP (Silvex) 2,4-D 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Butanone (MEK) 2-Hexanone 4,4'-DDT Acetone Aldrin Alkalinity, Total as CaCO3 alpha-BHC Antimony Arsenic Barium 80.7 89 99 102 107 79 90 52 62 43 52 55 60 56 140 100 160 280 Benzene Bis(2-ethylhexyl)phthalate Cadmium 1.9 Chloride Chloroethane Chloroform 3.4 Chloromethane Chromium 1.6 0.5 0.8 2.2 2.1 cis-1,2-Dichloroethene Cobalt Copper Cyanide delta-BHC Dich lorodifluoromethane Endrin Endrin aldehyde Heptachlor Iron Lead 7 8.9 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 3 of 36 A2 Facility Permit MWA R NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.05 pg/L Benzo(a)anthracene 3 pg/L Bis(2-ethylhexyl)phthalate 700 pg/L Carbon Disulfide 250000 pg/L Chloride 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 600 pg/L Ethylbenzene 300 pg/L Iron 15 pg/L Lead 50.0 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichooroethene 1000 pg/L Zinc MW-2R 6 pg/L 1,1-Dichloroethane 350 pg/L 1,1-Dichloroethene 0.4 pg/L 1,2-Dichloroethane 6 pg/L 1,4-Dichlorobenzene 3 pg/L 1,4-Dioxane (p-Dioxane) 50 pg/L 2,4,5-TP (Silvex) 70 pg/L 2,4-D NE pg/L 2,4-Dinitrotoluene NE pg/L 2,6-Dinitrotoluene 4000 pg/L 2-Butanone (MEK) 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 0.002 pg/L Aldrin NE pg/L Alkalinity, Total as CaCO3 0.006 pg/L alpha-BHC 1 pg/L Antimony 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 3 pg/L Bis(2-ethylhexyl)phthalate 2 pg/L Cadmium 250000 pg/L Chloride 3000 pg/L Chloroethane 70 pg/L Chloroform 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron 15 pg/L Lead Old Salisbury Road Landfill (C&D) His 150 6.6 61 3.9 torical detections by well locati 110 130 150 160 100 290 100 180 224 28 23 5.2 7.8 3 6 12 6 0.2 86 180 120 150 190 340 200 160 350 3 = 7.8 === 4 9 6.5 6.9 WMWMWW 14 8 im on Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 4 of 36 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 500 pg/L m&p-Xylene 50 pg/L Manganese 1 f M 1 pg/L Mercury NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 1.1 6 pg/L Naphthalene 100 pg/L Nickel 13.4 16.1 16.8 NS pg/L Nitrogen, Ammonia 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 57300 64400 73200 250000 pg/L Sulfate 85100 95900 105000 1 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 51.3 45.4 46 59 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids I 20.3 17 18.51 71779 18 3 pg/L Trichloroethene 0.97 0.9 0.93 1.3 0.93 2000 pg/L Trichlorofluoromethane 1.5 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 2 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone 18 NE pg/L Alkalinity, Total as CaCO3 488000 192000 115000 10 pg/L Arsenic 5.7 700 pg/L Barium 320 275 234 200 pg/L Benzo(g,h,i)perylene 3 pg/L Bis(2-ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 44600 2660 2180 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 5 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 11:61 of 15 pg/L Lead 4.9 50 pg/L Manganese of 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver 72400 70200 61500 61400 51400 110000 121000 115000 115000 98400 �• 36.3 39.1 49.6 35.8 34.6 796000 831000 769000 806000 632000 M ® m ®m 5.8 8.7 21.4 114000 133000 87800 102000 107000 5.5 3.9 3.3 309 297 278 271 214 1 2650 2520 2050 �mP!7 2990 2990 4.4 4.7 3.4 NE pg/L Sodium 2540 2770 2680 2380 250000 pg/L Sulfate 1210 1300 691 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 213000 177000 164000 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 5.1 2.4 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 129000 291000 101000 10 pg/L Arsenic 700 pg/L Barium 216 222 270 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 2220 25200 12500 3.4 3.51 1 3.81 2. 2.3 5 5.5 2240 2450 2310 2590 1530 1800 2200 300 33000 168000 188000 137000 18200 8.7 11 461000 315000 454000 99000 144000 117000 198 343 255 210 184 306 0.38 1.7 49200 35800 58400 13800 16900 22200 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND W-S GW Revised.xlsb 5of36 A2 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L 100 pg/L NS pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 3 pg/L 2000 pg/L 0.3 pg/L 88 pg/L 0.03 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 200 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 1000 pg/L 2 pg/L 250000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location Row Labels m&p-Xylene I 1 66 0.7 Manganese 9880 7950 8710 7880 8400:� Mercury Methane 1280 Methoxychlor 0.83 Methylene Chloride Naphthalene 0.86 1.3 1.6 1.9 Nickel 25.9 20.6 27.1 20.7 21.8 22.3 20.9 Nitrogen, Ammonia 0.12 o-Xylene 0.33 0.31 0.54 0.54 0.63 1 1.2 0.8 Selenium 16.5 Silver 5.2 5 2.5 0.9 0.7 Sodium 58300 59700 46200 45700 43400 38400 31800 27200 Sulfate 1117000 136000 128000 115000 79500 950001 96300 Tetrachloroethene 79.2 72.6 99.6 111 93.2 152 Tetrahydrofuran 197 274 226 Thallium Toluene Total Dissolved Solids 498000 • • : • 0.85 0.71 0.89 0.68 0.77 0.82 Trichloroethene 0.88 0.7 Trichlorofluoromethane 2.4 3.7 12 12.1 16.9 20.9 20.1 32 36 22 22 Vanadium Vinyl acetate Vinyl chloride Xylenes (Total) 0.98 1.6 Zinc 16.8 12.2 21.1 24.5 35.2 33.3 MW-3R Acetone Alkalinity, Total as CaCO3 177000 155000 155000 175000 142000 150000 155000 Arsenic 8.9 4 Barium 221 205 201 216 173 228 237 301 302 314 Benzo(g,h,i)perylene Bis(2-ethylhexyl)phthalate Cadmium 0.8 Carbon Disulfide Chloride 2940 3260 3620 3860 3920 Chromium Cobalt Copper Cyanide 10.4 7.1 8.1 9.1 6.5 Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron I of ll Lead 2.7 Manganese :� •� ••� •�� Mercury Methylene Chloride Selenium Silver 0.6 0.5 Sodium 2770 Sulfate 3740 4230 3400 5070 5420 6860 Tin 5.8 Total Dissolved Solids 191000 187000 193000 175000 172000 168000 180000 Vanadium Zinc 10.5 MW-4R 1,4-Dioxane (p-Dioxane) 4,4'-DDT Acetone Alkalinity, Total as CaCO3 286000 222000 224000 203000 174000 64300 143000 Arsenic Barium 305 264 296 375 400 407 328 126 335 56 Benzene 0.42 0.28 0.27 Butylbenzylphthalate Cadmium Chloride 50500 29700 36500 33700 34500 33200 29200 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 6 of 36 A2 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L 100 pg/L NS pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 3 pg/L 2000 pg/L 0.3 pg/L 88 pg/L 0.03 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 200 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 1000 pg/L 2 pg/L 250000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections -. m&p-Xylene Manganese Mercury Methane Methoxychlor Methylene Chloride Naphthalene Nickel Nitrogen, Ammonia o-Xylene Selenium Silver 0.68 0.6 1.2 0.9 Sodium Sulfate Tetrachloroethene Tetrahydrofuran Thallium Toluene Total Dissolved Solids Trichloroethene Trich I orofluo rom eth a ne Vanadium Vinyl acetate Vinyl chloride Xylenes (Total) Zinc MW-3R Acetone Alkalinity, Total as CaCO3 Arsenic Barium 289 252 231 293 273 Benzo(g,h,i)perylene Bis(2-ethyl hexyl )phthalate Cadmium Carbon Disulfide 26.1 3.3 Chloride Chromium 0.6 Cobalt Copper Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron Lead Manganese Mercury Methylene Chloride Selenium 12 4.9 18.1 Silver 1 0.3 1.5 0.9 Sodium Sulfate Tin Total Dissolved Solids Vanadium Zinc MW-4R 1,4-Dioxane (p-Dioxane) 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Arsenic Barium 334 58 263 172 287 Benzene Butylbenzylphthalate Cadmium Chloride Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 7 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 0.4 NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 6 pg/L Naphthalene 100 pg/L Nickel NS pg/L Nitrogen, Ammonia 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver 6 NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone _ NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 5.9 700 pg/L Barium 300 52 &UjK*-U1j 620 200 pg/L Benzo(g,h,i)perylene 3 pg/L Bis(2-ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 10 pg/L Chromium 9 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 0.2 0.7 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 7.5 700 pg/L Barium 350 650 280 595 570 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 7 2 pg/L Cadmium 250000 pg/L Chloride Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 8 of 36 A2 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 20 pg/L NE pg/L 250000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 200 pg/L 6 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 0.019 pg/L 700 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Labels Historical detections by well -. Chloromethane Chromium 6.4 3.2 Cobalt Copper 5 Cyanide delta-BHC Endosulfan II Iron Lead Manganese Mercury Methylene Chloride Nickel 8A 5 4.1 7.5 5.8 Selenium Silver Sodium 71200 42600 17800 65500 42100 Sulfate 163000 104000 50300 179000 125000 Sulfide 105 Tetrahydrofuran 11.4 9.3 Thallium 0.029 Total Dissolved Solids 167000 496000 250000 : • o i l Vanadium Zinc 5.9 5.2 ��l 9.9 5.8 8.6 MW-5R Acetone Alkalinity, Total as CaCO3 29200 35600 33600 33500 Arsenic Barium 55.8 59.8 52.5 53.2 B i s(2-ethyl h exyl )phtha late Cadmium Carbon Disulfide Chloride 15600 15100 15200 16200 Chloromethane Chromium 5.4 5.5 5.3 Cobalt Cyanide 7.2 Iron 63.5 88.2 37.9 Lead Manganese 4.2 Mercury Methylene Chloride Silver Sodium 13000 14600 12800 13500 Sulfate 8620 8090 8220 7830 Total Dissolved Solids 175000 156000 164000 144000 Vanadium Zinc MW-6R Arsenic Barium Chromium Lead Mercury MW-7 1,1,1-Trichloroethane 1,1-Dichloroethane 1.3 1.3 1.1 1.6 1.4 1,4-Dioxane (p-Dioxane) 2 4,4'-DDD Acetone Alkalinity, Total as CaCO3 54200 78500 75900 80400 Arsenic Barium 168 161 158 152 Benzene 0.68 0.37 0.41 0.4 0.38 Beryllium 0.61 0.62 2.1 beta-BHC Carbon Disulfide ocation 3.2 2.8 4.2 214 292 2.9 8 3.2 3.7 2.8 71000 14500 23800 23000 193000 48700 70300 72700 13.6 3.5 7 5.8 IM 241000 161000 304000 8.4 17.8 5.9 7.5 18.4 32300 32700 30800 32300 28600 57.1 55.9 55.9 92.7 54 15100 16400 15300 16200 15700 4.6 5.8 5.1 4.8 4.4 68.4 87.85 113 13900 14200 13100 11300 13100 7740 8450 7620 7430 8000 56000 145000 154000 104000 166000 7.3 1.2 0.91 1.1 1.3 1.5 15.7 85000 80100 71700 67300 64100 163 140 129 140 122 0.43 0.42 0.26 0.29 0.58 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 9 of 36 A2 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 20 pg/L NE pg/L 250000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 200 pg/L 6 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 0.019 pg/L 700 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location Row Labels Chloromethane Chromium Cobalt Copper Cyanide 4.3 5.9 delta-BHC Endosulfan II 0.12 Iron 126 89.5 158 145 Lead Manganese Mercury Methylene Chloride Nickel 7.2 5.3 Selenium 11.5 Silver Sodium 55400 39700 42600 42600 43600 40400 35300 Sulfate 143000 85200 113000 97600 73600 98700 61800 Sulfide Tetrahydrofuran 15.9 11.8 11.7 8.5 13.5 8.8 Thallium Total Dissolved Solids • • 1 445000 496000 413000 435000 374000 345000 Vanadium Zinc 7.2 13.6 MW-5R Acetone Alkalinity, Total as CaCO3 24000 31900 31700 34800 31200 134000 32800 Arsenic Barium 58.2 54.4 53.9 57.7 53.4 57.5 85.2 Bis(2-ethylhexyl)phthalate 1 Cadmium Carbon Disulfide Chloride 15500 13900 15200 16200 16100 16100 16400 Chloromethane Chromium 4.8 5.6 5.2 Cobalt Cyanide 5.1 ;43. Iron 221 123 126 102 209 Lead Manganese 2.6 6.1 Mercury Methylene Chloride Silver Sodium 13700 13600 13800 13000 14500 14200 13300 Sulfate 8180 8060 8310 11200 8400 7910 7020 Total Dissolved Solids 163000 167000 154000 131000 157000 149000 139000 Vanadium Zinc 11.4 15.3 MW-6R Arsenic Barium Chromium Lead Mercury MW-7 1,1,1-Trichloroethane 1,1-Dichloroethane 1.3 0.81 0.9 0.84 1.2 1.2 1,4-Dioxane (p-Dioxane) 4,4'-DDD Acetone Alkalinity, Total as CaCO3 62400 51900 51600 63500 51900 50200 47 Arsenic Barium 111 90.8 98.8 115 95.1 100 Benzene Beryllium beta-BHC Carbon Disulfide Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 10 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 3 pg/L Chloromethane 10 pg/L Chromium 5.4 1.2 0.6 0.4 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 4.8 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver 2.4 2.6 0.9 NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 66.8 53 56 58 70.6 58 3 pg/L Bis(2-ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 8.6 5.2 5.3 5.6 8.4 6.4 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver 0.6 0.3 0.8 0.6 NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1,1,1-Trichloroethane 6 pg/L 1,1-Dichloroethane 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 104 87 99 96 101 89 1 pg/L Benzene 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon Disulfide 12.5 58 6.2 5.51 5 NIMM 36 M 57 54 531 80 761 65 721 6511501 6101 270 3.5 5.6 0.4 7.3 8.7 9.5 7.4 7 5.1 281 251 24 2.2 2.4 131 7.6 4111801 5301 62 3.2 4.1 7.6 761 741 601 531 631 1 180�13012101 84 p Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND W-S GW Revised.xlsb 11 of 36 A2 Facility Permit 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 3 pg/L Bis(2-ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1,1,1-Trichloroethane 6 pg/L 1,1-Dichloroethane 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon Disulfide Old Salisbury Road Landfill (C&D) Historical detections by well location 8.1 1 9.5 0.4 0.3 ' © 1 820 ### 82 29 38 96 170 16 70 43 96 11111111 16 29 69 3120 19 .■■■N. . 411 82 59 2.6 2.8 5.8 9 390 9 3601 260 300 590 IM 141 141 11 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 12 of 36 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 250000 pg/L Chloride 6470 6580 6490 7390 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1.5 0.86 0.85 1.1 1.1 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 35 25 15 pg/L Lead 500 pg/L m&p-Xylene 1 1.1 1.7 1.6 1.4 50 pg/L Manganese 44 43.8 43 1 pg/L Mercury 3 pg/L Methylene Chloride 1.7 500 pg/L o-Xylene 0.68 0.59 0.65 0.6 0.68 20 pg/L Silver NE pg/L Sodium 17500 17700 16600 15300 250000 pg/L Sulfate 12800 12700 14200 13400 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 80.4 50.5 24.9 20.1 500000 pg/L Total Dissolved Solids 192000 171000 181000 175000 3 pg/L Trichloroethene 0.6 2000 pg/L Trichlorofluoromethane 2 1.2 1.2 1.6 1.6 500 pg/L Xylenes (Total) 1000 pg/L Zinc 6 9 5 M W-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 26600 24200 27000 10 pg/L Arsenic 700 pg/L Barium 47.8 36 41.2 250000 pg/L Chloride 4290 3110 3660 10 pg/L Chromium 3.5 2.6 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 42.4 39.3 15 pg/L Lead 50 pg/L Manganese 3.3 4 4.4 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 9620 8300 8810 250000 pg/L Sulfate 6560 1060 2980 500000 pg/L Total Dissolved Solids 170000 68000 75000 1000 pg/L Zinc M W-9 NE pg/L Alkalinity, Total as CaCO3 29700 33500 31800 10 pg/L Arsenic 700 pg/L Barium 217 215 193 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 6830 5330 4830 10 pg/L Chromium 4.2 70 pg/L Cyanide 46. 386 4. 37. 3. 1000 pg/L Dichlorodifluoromethane 1.4 0.99 1.2 1.7 300 pg/L Iron 148 250 35.3 15 pg/L Lead 50 pg/L Manganese 7.1 10.7 4.2 1 20 pg/L Silver NE pg/L Sodium 14100 15700 14300 14< 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 190000 139000 133000 136( 2000 pg/L Trichlorofluoromethane 1.7 1.3 1.3 1.4 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) 6.41 8.5 5. 7 1 5290 4820 4430 6050 4340 0.13 1.1 1.1 0.77 0.8 0.73 0.62 1 0.15 25.2 1.2 2.2 1.8 0.84 1.5 35.6 28.8 33.6 27.1 2.1 0.46 0.63 0.47 0.27 0.4 17800 16200 16400 15700 16300 6720 3800 2930 10100 1850 0.48 32 21.7 13.5 17.7 14.1 75000 153000 137000 78000 145000 0.91 1.5 0.92 1.4 0.79 8.9 5.7 5.2 6.8 20800 25800 24800 23200 20000 42.9 44 38.3 34.4 30 3060 2670 1960 2040 1960 4.1 9.9 4.3 5.1 5.6 48.6 54 3 2.7 2.9 3.3 3.4 1.1 9240 9700 8280 7940 6940 2700 4090 1630 1350 1860 67000 67000 87000 79000 61000 7.1 25400 23300 21200 23400 18900 207 195 197 186 182 4610 4360 6850 4710 4290 4.7 1.5 0.88 0.76 149 128 4.6 8.5 6.3 4 3.5 15400 15700 14200 14500 14500 960 3440 1110 2030 141000 135000 103000 142000 134000 1.4 1 1.3 1.1 0.98 5.1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 13 of 36 A2 Facility Permit 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 500 pg/L o-Xylene 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) Old Salisbury Road Landfill (C&D) Historical detections by well location 4300 3600 5160 5340 3810 1.3 0.6 0.73 0.37 0.54 0.72 0.62 0.5 0.67 0.7 5 76.5 1.1 0.96 1.4 22.9 15.5 19.4 24.9 17.4 10.2 12.7 2.9 0.36 0.27 0.4 0.8 0.2 0.6 16600 14200 13000 14300 13900 13700 12000 1360 2090 8.8 5.2 13.7 24.2 26 18.9 138000 126000 116000 108000 111000 109000 124000 1.2 0.62 0.47 0.25 0.29 0.34 0.5 1.2 0.79 3.8 22800 21300 19700 22800 19500 20100 19600 2.6 38 30.7 25.4 28.5 26.9 27.5 24.4 27 27 29 1350 1800 1510 2070 1860 1 0.6 1.4 136 61.5 60.8 57.8 151 19.9 6.8 7 0.1 7810 6160 5580 6120 6980 6250 5410 2100 64000 50000 61000 51000 58000 52000 81000 15.2 45.4 18300 18300 18400 21700 17200 20100 17400 3.5 193 168 170 174 142 142 141 153 157 134 3610 3610 3950 4300 3560 0.28 0.28 55.9 136 7.6 6.9 16.6 0.4 0.3 14600 12400 13500 12900 13100 12600 11900 2100 3200 141000 107000 124000 100000 118000 123000 128000 0.96 0.47 0.69 0.36 0.49 0.42 0.3 5.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 14 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 0.65 0.9 7.3 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 500 pg/L o-Xylene 20 pg/L Silver 0.88 0.4 1 0.7 NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 27.2 25 33 24 250000 pg/L Chloride 10 pg/L Chromium 0.8 1 0.4 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 5.31 6 0.2 6.8 2.6 6 26.6 30 29 29 26 25 30 480 52 77 48150 2.4 3.2 3.8 2 6.7 1 pg/L Mercury 0.1 3 pg/L Methylene Chloride 20 pg/L Silver 0.16 0.2 0.1 0.16 NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 128 173 124 124 117 140 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 7.6 0.5 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver 0.32 0.2 0.4 0.2 NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 0.3 140 100 100 85 95 240 14 15 of 36 A2 Facility Permit 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 500 pg/L o-Xylene 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) Old Salisbury Road Landfill (C&D) Historical detections by well location 2.5 8.71 12 0.21 10.4 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 16 of 36 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 40 Ng/L 2-Hexanone 0.72 0.69 0.96 NE pg/L 4-Methyl-2-pentanone (MIBK) 0.65 1.7 1.1 2.8 2.5 2.6 5.6 6000 Ng/L Acetone 16.4 14 12.1 22.5 14.1 11.8 NE pg/L Alkalinity, Total as CaCO3 506000 652000 506000 520000 446000 626000 29000 48200 47300 10 pg/L Arsenic 2.6 5.2 700 pg/L Barium 65.6 83.1 94.7 106 221 148 292 241 660 1 pg/L Benzene 0.33 0.55 0.55 0.6 0.52 0.83 0.46 4 pg/L Beryllium 3.2 1.9 2.8 700 pg/L Carbon Disulfide 2.1 2 5.2 250000 Ng/L Chloride 65100 88500 158000 163000 Wjd.1111 202000 9640 47400 51800 10 pg/L Chromium 5.6 4.1 4.6 4.2 6.4 9.1 3.5 6.7 70 pg/L cis-1,2-Dichloroethene 0.23 0.3 0.23 0.2 0.33 1 pg/L Cobalt 1000 Ng/L Copper 16.4 6.3 3.8 70 pg/L Cyanide 4.3 4.8 5.4 4.1 9.8 40 pg/L Endosulfan 1 0.17 600 pg/L Ethylbenzene 0.4 0.53 0.55 0.4 1 0.008 pg/L Heptachlor 1 1 0.004 pg/L Heptachlor epoxide I W 300 pg/L Iron I :91 vi 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 2.6 3.9 0.68 1.3 1.1 4.1 1.2 I I so, of •0 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 7.2 11.1 8.5 7.6 6.9 500 pg/L o-Xylene 0.28 0.53 0.78 1.1 0.97 1 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 136000 151000 157000 138000 123000 250000 Ng/L Sulfate 235000 64100 Egff 0r'1 W2U1j1U1 NE pg/L Sulfide 347 240 127 NE pg/L Tetrahydrofuran 113 169 192 135 131 182 0.2 pg/L Thallium 0.043 2000 Ng/L Tin 600 pg/L Toluene 0.26 0.4 0.27 500000 Ng/L Total Dissolved Solids 2000 Ng/L Trichlorofluoromethane 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-11 0.1 pg/L 4,4'-DDT 1 . Immeallif 6000 Ng/L Acetone NE pg/L Alkalinity, Total as CaCO3 154000 161000 130000 700 pg/L Barium 100 95.8 82.8 200 pg/L Benzo(g,h,i)perylene 250000 Ng/L Chloride 12300 11800 12500 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 Ng/L Copper 70 pg/L Cyanide 4 4.4 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 12800 13600 12000 250000 Ng/L Sulfate 22300 20700 15300 NE pg/L Sulfide 56.8 53.8 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 Ng/L Total Dissolved Solids 236000 237000 232000 0.3 pg/L Vanadium Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb Il 2.6 8.5 11. 2.1 0.68 1. me 0.12 0.12 0.2 2.8 1.2 10.7 4.7 3.9 5. 2.1 0.43 0.8 184000 10300 198001 1410 15800 63600 877 237 6.1 120 14 0.6 M� 131100103000127900 5.41 1 5.11 1 341 27.21 21 21.1 130000I 1350001 107000 I1040000 127�000 132�03 0 89.8 102 93.1 130001 135001 14500 114500 149001 14400 0.23 2.8 4.1 4.2 1.4 5.6 12300 11700 12000 11200 12000 9460 16200 14100 17100 15200 19100 15300 4.5 218000 226000 189000 236000 =239000 17 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MIBV 2.2 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 42200 31400 26700 32100 25500 413000 10 pg/L Arsenic 700 pg/L Barium 262 132 112 115 101 96.5 1 pg/L Benzene 0.44 4 pg/L Beryllium 1.4 700 pg/L Carbon Disulfide 250000 pg/L Chloride 2220 1820 1790 2040 1800 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 0.35 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan 1 600 pg/L Ethylbenzene 0.73 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron .1 84.3 92.8 218 55.1 15 pg/L Lead 4.1 500 pg/L m&p-Xylene 1.1 50 pg/L Manganese 1 10.9 7.9 5.1 1 pg/L Mercury 0.33 0.51 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene 0.65 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 6860 5280 250000 pg/L Sulfate NE pg/L Sulfide 260 NE pg/L Tetrahydrofuran 106 18.6 5 0.2 pg/L Thallium 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 86000 63000 66000 46000 63000 2000 pg/L Trichlorofluoromethane 0.2 0.33 0.38 0.49 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc 6.2 MWA1 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 143000 175000 161000 189000 153000 700 pg/L Barium 96.8 94.3 87.8 87 76.8 200 pg/L Benzo(g,h,i)perylene 250000 pg/L Chloride 15000 12400 14000 14200 12900 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron Y.11011 I I 1 .11 � 15 pg/L Lead 3.6 50 pg/L Manganese '•� :'� 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE ug/L Sodium 10000 8490 9070 8290 8770 250000 pg/L Sulfate 12800 10700 10400 11000 10400 NE pg/L Sulfide 130 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 228000 207000 236000 228000 220000 0.3 pg/L Vanadium WiW Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 21700 91.3 81 39 47 0.6 6 490001 1 89000 0.05 120000 122000 70.3 57.5 1.3 10800 8480 7460 6480 9700 7590 4.4 161000 165000 0.1 0.5 56 1.2 12 38 0.5 18 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MIB 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 39.1 39 42 42 1 pg/L Benzene 4 pg/L Beryllium 700 pg/L Carbon Disulfide 13 250000 pg/L Chloride 10 pg/L Chromium 0.7 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan 1 600 pg/L Ethylbenzene 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver 0.19 NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MWA1 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 31.8 28 29 29 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 20 pg/L Selenium 8.7 20 pg/L Silver 0.5 0.8 0.4 NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 40.81 521 71 461 821 551 98 0.2 6.8 6.2 23.1 25 24 26 27 24 28 47 3.9 3.3 19 of 36 A2 1000 Ng/L 3 pg/L 6000 Ng/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 Ng/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 Ng/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 Ng/L NE pg/L 0.2 pg/L 500000 Ng/L 2000 Ng/L 1000 Ng/L 350 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 4 pg/L 250000 Ng/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 250000 Ng/L NE pg/L NE pg/L 2000 Ng/L 500000 Ng/L 2000 Ng/L 0.3 pg/L 1000 ug/L 6000 Ng/L NE pg/L 10 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections b well location Value Column Labels Y -. Zinc MW-12 1,4-Dioxane (p-Dioxane) 5.3 Acetone Alkalinity, Total as CaCO3 176000 117000 65800 73800 Arsenic Barium 200 132 82.8 84.2 Benzene 0.33 Benzo(g,h,i)perylene Beryllium 0.88 Chloride 34000 14400 11100 10400 Chloromethane Chromium cis-1,2-Dichloroethene 0.4 0.2 Cobalt 5.5 Cyanide 4.8 Dichlorod ifl uoromethane Di-n-octylphthalate Indeno(1,2,3-cd)pyrene Iron 19 • 175 125 Manganese 2260 Methylene Chloride Nickel 6.2 3.3 Silver Sodium 20700 17600 13400 13200 Sulfate 149000 91700 64300 62400 Tetrahydrofuran 5.9 Thallium Total Dissolved Solids 301000 218000 219000 Trichlorofluoromethane 0.81 1 0.89 1.4 0.52 Zinc MW-13 1,1-Dichloroethene Acetone Alkalinity, Total as CaCO3 52800 52800 47200 44600 Arsenic Barium 138 124 114 116 Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Beryllium 0.6 0.69 0.63 0.52 Chloride 6290 5120 4790 4770 Chromium 3.8 Cobalt Copper Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron 42.3 71.8 108 193 Lead Manganese 5.2 9.8 7.4 17.9 Nickel Silver Sodium 9940 10900 9540 9740 Sulfate 5910 5650 4510 4960 Sulfide Tetrahydrofuran Tin Total Dissolved Solids 115000 111000 107000 90000 Trich lorofluoromethane Vanadium Zinc MW-14 Acetone Alkalinity, Total as CaCO3 64900 67100 61800 63500 Arsenic 12.1 64500 72900 55900 41000 192C 113 144 1901 95.7 60 1197001 233001 1 260001 9000 5.3 0.23 5.6 274 • 49.6 9. 2 2 4.4 6.2 5.5 3.2 16200 19200 1920C 13700 1120 86100 129000 169000 70800 7360 11.4 26.8 12.4 0.021 288000 286000 382000 234000 16300 1 2.8 1.4 0.82 0.2 17.3 42400 42300 41000 37100 2.6 120 91.6 210 71.5 2.2 0.68 0.6 4310 4100 4590 3270 376 2. 8.5 5 58 1111116SII�E'L§ 8 2. 9.7 26.7 41. 6.4 10000 9380 9420 12200 1070 5670 5390 7280 10100 933 89000 79000 145000 110000 107000 5.7 12.8 40.5 8.6 7.9 14.7 55300 59700 50400 5150 445200 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 21 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 1000 pg/L Zinc 92 MW-12 3 pg/L 1,4-Dioxane (p-Dioxane) 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 40500 45500 39300 29600 40200 37200 10 pg/L Arsenic 700 pg/L Barium 59.2 61.1 47.6 50.1 50.5 46.9 1 pg/L Benzene 200 pg/L Benzo(g,h,i)perylene 1.2 4 pg/L Beryllium 250000 pg/L Chloride 8240 6180 6230 5820 4900 8200 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 100 pg/L Di-n-octylphthalate 0.05 pg/L Indeno(1,2,3-cd)pyrene WEE 300 pg/L Iron 253 50 pg/L Manganese 14.6 13.2 33.6 15.7 3 pg/L Methylene Chloride 100 pg/L Nickel 4.1 20 pg/L Silver NE pg/L Sodium 12800 11000 10500 11100 11000 11600 250000 pg/L Sulfate 32800 48000 27400 51800 24200 20500 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 135000 149000 126000 138000 127000 130000 2000 pg/L Trichlorofluoromethane 0.32 1000 pg/L Zinc 30.8 MW-13 350 pg/L 1,1-Dichloroethene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 36200 46400 43200 58700 43900 52200 10 pg/L Arsenic 700 pg/L Barium 130 77.1 106 176 279 144 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 1.5 4 pg/L Beryllium 1.2 2.4 3.5 1.4 250000 pg/L Chloride 5870 3880 5700 3820 6150 5380 10 pg/L Chromium 3 7.1 1 pg/L Cobalt 1000 pg/L Copper 3.8 7.6 6.9 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 232 0 0 :. 15 pg/L Lead 5.4 6.5 7.5 50 pg/L Manganese 34.1 48.8 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 10700 11200 11700 19100 14600 16700 250000 pg/L Sulfate 8660 8680 9360 7820 9770 9420 NE pg/L Sulfide 151 106 178 NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 119000 113000 114000 87000 144000 110000 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc 13.7 17.2 37.3 51 20 MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 42300 37400 32800 35600 28900 30100 10 pg/L Arsenic Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 40200 2.7 60.1 39 45 41 8030 0.2 2.6 1.1 2.4 0.7 0.2 9980 15300 124000 44500 139 164 176 126 2.3 5.5 3.9 4 1.7 6.1 .1 6.4 4.3 .e 0.7 0.4 20200 9460 19 159000 31.6 30400 22 of 36 A2 1000 pg/L 3 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 pg/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 1000 pg/L 350 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 4 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 2000 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location -. Zinc MW-12 1,4-Dioxane (p-Dioxane) Acetone Alkalinity, Total as CaCO3 Arsenic Barium 38 35 58 61 47.3 31 66 55 77 50 77 74 Benzene Benzo(g,h,i)perylene Beryllium Chloride Chloromethane Chromium 2 1.8 4 2.1 cis-1,2-Dichloroethene Cobalt Cyanide Dich lorodifluoromethane Di-n-octylphthalate Indeno(1,2,3-cd)pyrene Iron Manganese Methylene Chloride Nickel Silver 0.39 0.4 0.2 0.26 Sodium Sulfate Tetrahydrofuran Thallium Total Dissolved Solids Trich I orofluo rom eth a ne Zinc MW-13 1,1-Dichloroethene 19.8 Acetone Alkalinity, Total as CaCO3 Arsenic Barium 117 79 89 65 85.6 79 62 65 59 46 57160 Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Beryllium Chloride Chromium 0.8 1.6 2.2 1.1 2 4.8 9.2 Cobalt Copper Cyanide Dibenz(a,h)anthracene Indeno(1,2,3-cd)pyrene Iron Lead 11 Manganese Nickel Silver 0.41 0.4 0.2 Sodium Sulfate Sulfide Tetrahydrofuran Tin Total Dissolved Solids Trichlorofluoromethane 18.6 Vanadium Zinc MW-14 Acetone Alkalinity, Total as CaCO3 Arsenic 7.3 8.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 23 of 36 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 700 pg/L Barium 234 246 212 214 221 188 188 183 179 4 pg/L Beryllium 0.61 0.83 0.59 0.54 0.6 0.57 0.83 0.63 0.54 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 3870 3840 3930 3620 3260 3410 3470 3930 3510 3 pg/L Chloromethane 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 4.3 5.3 1000 pg/L Dichlorodifluoromethane 3 2.4 3 3.6 3.9 3.6 2.3 3.6 2.1 300 pg/L Iron 36.2 124 93.9 134 123 15 pg/L Lead 50 pg/L Manganese 38.3 17.4 18.4 18.1 13.7 21.6 25.7 1 pg/L Mercury 3 pg/L Methylene Chloride 1.6 100 pg/L Nickel 4.4 6.3 2.6 2.7 2.8 2.8 20 pg/L Silver NE pg/L Sodium 17400 18600 16900 17100 16900 16200 15400 15800 14500 250000 pg/L Sulfate 663 1400 1080 1790 0.7 pg/L Tetrachloroethene 0.52 0.61 0.2 pg/L Thallium 0.048 500000 pg/L Total Dissolved Solids 163000 154000 152000 142000 130000 118000 85000 135000 131000 2000 pg/L Trichlorofluoromethane 0.92 0.86 0.79 0.8 0.87 0.75 0.58 1.1 0.54 0.59 0.3 pg/L Vanadium 1000 pg/L Zinc 5.3 6.3 MW-15 350 pg/L 1,1-Dichloroethene 70 pg/L 2,4-D 0.27 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone 13.2 NE pg/L Alkalinity, Total as CaCO3 74200 89900 112000 110000 98100 101000 104000 103000 91500 10 pg/L Arsenic 4.5 700 pg/L Barium 29.8 24.4 11.4 17.1 22.7 14 11 74 105 250000 pg/L Chloride 115000 128000 89700 89800 104000 98000 94000 113000 98200 70 pg/L Chloroform 0.45 0.4 0.44 0.4 0.44 0.7 0.44 0.26 10 pg/L Chromium 5.4 7.6 1000 pg/L Copper 3 2.6 7.1 8.8 70 pg/L Cyanide 4.2 300 pg/L Iron D 227 :i 15 pg/L Lead 1 61 6.8 50 pg/L Manganese 3 pg/L Methylene Chloride 2.4 100 pg/L Nickel 2.7 3.9 4.3 NE pg/L Sodium 23000 26100 20500 19800 21600 20200 20100 21800 20300 250000 pg/L Sulfate 45900 49900 54600 59600 58300 58700 63700 70000 65400 NE pg/L Sulfide NE pg/L Tetrahydrofuran 9.2 14.8 12 16.8 27.3 19.8 16.9 0.2 pg/L Thallium 0.049 500000 pg/L Total Dissolved Solids 448000 395000 369000 370000 410000 371000 418000 362000 360000 2000 pg/L Trichlorofluoromethane 0.21 0.42 0.2 0.71 2.1 4.4 5.1 4.8 4.4 0.3 pg/L Vanadium 1000 pg/L Zinc 5.1 5.8 6.6 7.1 16.2 6.3 5.9 35.4 49 SW-1 6000 pg/L Acetone 11.2 NE pg/L Alkalinity, Total as CaCO3 22300 27400 49200 43600 33200 57400 27700 35100 44500 10 pg/L Arsenic 3.6 700 pg/L Barium 109 47 68.2 47.5 86.8 65.9 69.5 65 72.2 4 pg/L Beryllium 2 pg/L Cadmium 250000 pg/L Chloride 55400 18300 29700 35700 49200 26800 26000 21600 31500 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 8.6 3.9 70 pg/L Cyanide 4.4 4.7 2 pg/L Endrin 300 pg/L Iron onn" f� 15 pg/L Lead Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 25 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 700 pg/L Barium 193 163 140 254 160 122 4 pg/L Beryllium 0.6 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 3720 3630 4100 4290 4790 3 pg/L Chloromethane 10 pg/L Chromium 4.5 6.6 6 1000 pg/L Copper 4.8 9.5 5.8 70 pg/L Cyanide 6 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 1 142 t' 1 15 pg/L Lead 50 pg/L Manganese 1 40.2 0 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 5.3 8.6 13.7 12.5 20 pg/L Silver NE pg/L Sodium 14400 12800 12300 13500 15000 14300 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 119000 124000 123000 102000 127000 145000 2000 pg/L Trichlorofluoromethane 0.57 0.34 0.3 pg/L Vanadium 1000 pg/L Zinc 13.3 11.7 27.4 23 MW-15 350 pg/L 1,1-Dichloroethene 3.1 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 0.062 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 54700 96600 64300 78900 77600 75300 10 pg/L Arsenic 7.1 5.7 700 pg/L Barium 41.5 8.6 23.8 59.6 143 115 250000 pg/L Chloride 146000 83400 124000 124000 143000 60600 70 pg/L Chloroform 0.49 0.77 0.63 0.49 1.4 10 pg/L Chromium 6.7 7.2 1000 pg/L Copper 10.5 70 pg/L Cyanide 5.2 300 pg/L Iron 233 292 239 E6 VAA91111=11111111 15 pg/L Lead 9.5 7.6 50 pg/L Manganese 33 34.7 14 .1 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 24000 24200 25300 26700 21200 16300 250000 pg/L Sulfate 43800 59500 53200 41200 35600 25800 NE pg/L Sulfide 100 NE pg/L Tetrahydrofuran 15.5 21.4 14.7 7.4 6.3 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 464000 373000 410000 442000 298000 260000 2000 pg/L Trichlorofluoromethane 3.9 5.3 7.6 4.3 8.1 7.3 0.3 pg/L Vanadium 1000 pg/L Zinc 5.3 17.1 22.7 45.6 51.1 SW-1 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 63700 45200 72700 58000 79700 47200 10 pg/L Arsenic 5.9 700 pg/L Barium 276 65.8 71.1 58.9 63.3 70.4 4 pg/L Beryllium 1.1 2 pg/L Cadmium 0.7 250000 pg/L Chloride 19500 23700 18100 20600 19700 25300 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 16A 70 pg/L Cyanide 2 pg/L Endrin 0.08 300 pg/L Iron .01 .•�� �� �� 15 pg/L Lead Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 1431 1 1251 1291 1 130 0.2 1.8 2.3 1 3 0.7 0.4 12700 138000 12 2.2 19600 42.5 19100 70 3.7 93 26 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 700 pg/L Barium 242 98 583 186 130 210 460 250 120 69 66 170 4 pg/L Beryllium 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 0.4 = 4.1 1.7 6.6 3.9 3.2 1000 pg/L Copper 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 7.2 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Silver 0.54 0.5 0.6 NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-15 350 pg/L 1,1-Dichloroethene 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc SW-1 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 77.7 46 78 80 4 pg/L Beryllium 2 pg/L Cadmium 250000 pg/L Chloride 5.2 22.7 70.3 88 54 10 pg/L Chromium 0.6 0.7 1.2 0.61 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 2 pg/L Endrin 300 pg/L Iron 15 pg/L Lead Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 5.9 8 0.4 11201 73EM 531500 4.21 27 of 36 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 50 Ng/L Manganese 48.5 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 19400 250000 Ng/L Sulfate 7970 500000 Ng/L Total Dissolved Solids 174000 0.3 pg/L Vanadium 1000 Ng/L Zinc SW-2 3 pg/L 1,4-Dioxane (p-Dioxane) 1.3 11800 4140 106000 15600 2060 131000 5.2 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone 13 NE pg/L Alkalinity, Total as CaCO3 54900 62600 56000 10 pg/L Arsenic 700 pg/L Barium 85.6 78.8 74.2 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3 pg/L Bis(2-ethylhexyl)phthalate 250000 Ng/L Chloride 19400 12800 13500 3 pg/L Chloromethane 10 pg/L Chromium 2.8 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 0.3 1 pg/L Cobalt 1000 Ng/L Copper 4.1 70 pg/L Cyanide 4.2 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron NEW U 15 pg/L Lead 50 pg/L Manganese Me 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 12300 11900 11300 250000 Ng/L Sulfate 13500 20000 11100 NE pg/L Sulfide NE pg/L Tetrahydrofuran 61 600 pg/L Toluene 500000 Ng/L Total Dissolved Solids 182000 144000 135000 0.3 pg/L Vanadium 1000 Ng/L Zinc SW-3 3 pg/L 1,4-Dioxane (p-Dioxane) 1.3 40 pg/L 3&4-Methylphenol(m&p Cresol) 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 473000 181000 356000 700 pg/L Barium 273 122 223 1 pg/L Benzene 0.73 250000 Ng/L Chloride 28000 12000 22300 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb F, 30001 42001 16000 12730 22530 134110 111130001 4320 114460I 143000 116000140000 123000 10.1 7.2 7.5 1.8 57600 46200 58800 1 32300 43200 32= 3.7 65.4 77.5 108 73.1 70WI 152001 13800 6190 I 9720 12500 0.12 3.8 3. 81 300 1510 2070 22601 ® mm 160 317 291 10: 11MEN 116001 11600 10200 118420 11300 9920 10900 6270 0.52 1250001 1129000 106000 11300011050001125000 16.2 477000 251000 520000 161000 210000 118000 217 173 270 114 152 105 0.42 33800 18400 34000 10500 16300 27000 3.4 MW 0.26 29 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 8.7 20 pg/L Selenium 7 20 pg/L Silver NE pg/L Sodium 12500 14500 13000 12400 1E 250000 pg/L Sulfate 3130 2820 2190 2700 2 500000 pg/L Total Dissolved Solids 122000 126000 125000 104000 131 0.3 pg/L Vanadium 1000 pg/L Zinc 69.8 SW-2 3 pg/L 1,4-Dioxane (p-Dioxane) _ 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 2390 41300 48900 48600 44 10 pg/L Arsenic 6.2 700 pg/L Barium 171 59.7 50.1 51.7 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 0.64 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 28200 10700 11600 10800 1C 3 pg/L Chloromethane 10 pg/L Chromium 3.2 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 3.2 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 7.4 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 3.1 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 17600 9840 10300 9160 £ 250000 pg/L Sulfate 5620 12700 5490 5090 4 NE pg/L Sulfide 142 NE pg/L Tetrahydrofuran 18.4 600 pg/L Toluene 143001 9390 98000 �140000 3.6 2.9 4 44200 26100 53.41 1 81 1.8 1.1 11300 10900 W 9890 8650 6180 1 38300 500000 pg/L Total Dissolved Solids 117000 120000 114000 91000 101000 101000 1189000 0.3 pg/L Vanadium �=218 1000 pg/L Zinc SW-3 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 3&4-Methylphenol(m&p Cre 3.6 0.1 pg/L 4,4'-DDD 0.079 0.1 pg/L 4,4'-DDT 0.09 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 389000 259000 516000 293000 317000 221000 160000 700 pg/L Barium 206 181 348 185 315 179 123 1 pg/L Benzene 0.54 0.32 0.88 0.34 0.25 250000 pg/L Chloride 27000 16900 34800 20000 24300 22800 20900 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 0.4 49 0.2 0.3 59 0.2 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 30 of 36 A2 Facility Permit 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-2 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3 pg/L Bis(2-ethylhexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-3 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 3&4-Methylphenol(m&p Cre: 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 1 pg/L Benzene 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt Old Salisbury Road Landfill (C&D) Historical detections by well location 0.621 1 0.41 0.41 0.51 52.1 461 511 511 49.4 300 44 0.4 150 51 471 65 63 4.7 11 7.6 0.081 0.36 0.5 0.3 0.26 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 31 of 36 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 1000 pg/L Copper 4.4 70 pg/L Cyanide 4.6 6 42 pg/L Endosulfan II 300 pg/L Iron •1 1111141 1' "41111 15 pg/L Lead 2.7 50 pg/L Manganese - f 3 pg/L Methylene Chloride 1 100 pg/L Nickel 6.9 3.9 5.5 3.6 6.8 2.8 2.8 NE pg/L Sodium 34000 16900 27000 35500 24600 38400 14700 20900 18200 250000 pg/L Sulfate 43600 16000 18500 33800 15200 18500 11400 27000 17000 NE pg/L Tetrahydrofuran 6.1 3.4 6.3 3.3 2000 pg/L Tin 2.8 500000 pg/L Total Dissolved Solids • • : 241000 413000 321000 a e l 231000 300000 233000 0.3 pg/L Vanadium 1000 pg/L Zinc 7.1 9.6 13.6 SW-4 350 pg/L 1,1-Dichloroethene 40 pg/L 2-Hexanone 3.1 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 16 NE pg/L Alkalinity, Total as CaCO3 265000 145000 211000 192000 187000 240000 148000 187000 242000 700 pg/L Barium 382 124 138 110 121 128 113 115 187 250000 pg/L Chloride 18700 24800 29800 36800 27400 27900 20300 19800 19000 70 pg/L Chloroform 10 pg/L Chromium 4.7 1 pg/L Cobalt 70 pg/L Cyanide 4.1 5.6 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron :1 of 1 1 50 pg/L Manganese 1 :0 1 1 1 3 pg/L Methylene Chloride 1.2 100 pg/L Nickel 4.4 2.6 2.5 3.6 NE pg/L Sodium 22000 20000 23400 25600 23400 26000 16900 20200 23800 250000 pg/L Sulfate 17400 27500 24400 26700 18200 28600 16600 24900 23500 NE pg/L Tetrahydrofuran 13.7 5.7 3.5 3.6 4.1 500000 pg/L Total Dissolved Solids 444000 236000 327000 317000 289000 325000 229000 267000 371000 2000 pg/L Trichlorofluoromethane 0.32 0.3 pg/L Vanadium "90 1000 pg/L Zinc 6.9 8.3 7.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 33 of 36 A2 Facility Permit Old Salisbury Road Landfill (C&D) 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-4 350 pg/L 1,1-Dichloroethene 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc Historical detections by well location 0.071 0.085 4.8 12 29900 29900 41100 25000 33800 21300 18500 16800 26300 62500 20100 36400 26400 19800 10.2 9.7 18.9 5.1 4.8 4.5 473000 319000 327000 432000 329000 237000 10.8 0.58 0.062 0.054 140000 158000 152000 147000 220000 158000 131000 82.8 126 101 106 151 136 105 24300 30800 31000 26900 28800 30900 23600 0.97 0=1 0.066 0.061 •0 4180 1640 2140 1060 •0 17800 24400 20100 18200 29000 20000 17900 17600 23500 23000 13200 32300 23600 19500 4.4 222000 257000 270000 255000 349000 272000 234000 0.27 0.25 1.4 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 34 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 250000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 3 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L Concentration Row Labels Column Labels 3w May-19 EPA 300.0 pg/L Sulfate SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C NgIL Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide SM 4500-S2D pg/L Sulfide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance deg C Field Temperature EPA 8260B Mod. pg/L 1,4-Dioxane (p-Dioxane) EPA 601 OD pg/L Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Sodium Vanadium Zinc EPA 7470A pg/L Mercury 85100 1210 163000 8620 12800 6560 235000 22300 149000 5910 45900 838001 577000 4880001 129000 292001 542001 266001 29700 5060001 154000 1760001 52800 649001 74200 202000 ���� ���� 167000 175000 192000 170000 190000 ���� 236000 ���� 115000 163000 448000 9770 42300 44600 2220 15600 6470 4290 6830 65100 12300 34000 6290 3870 115000 7.2 347 56.8 100.3 20.5 43.18 16.43 28.22 102.35 32.3 154.41 31.02 11.22 15.15 24.42 151.2 113.25 120 42 54 40 60 96 54 120 42 40 31.28 40 120 96 2.31 1.78 3.85 1.58 11.68 0.94 12.52 11.94 4.17 6.8 4.97 8.11 3.07 3.65 3.37 11.71 59.87 19.46 7.55 0.94 3.05 9.06 23.79 12.98 2.42 4.17 3 24.7 10.46 12.09 12.43 12 11.42 10.47 10.24 10.26 12.49 11.57 11.53 10.45 10.25 12.15 193 333.4 293.4 297.8 81.6 165.9 65.1 -47.7 603.7 608.2 469.8 402.2 219.3 111.2 441.8 2352 812.9 2471 348 447.1 162.3 1317.2 3029 706.5 1452 268.3 377.7 1185.4 35.3 31 30.6 28.5 30.9 32.2 30.1 34.3 35.2 30.9 31.2 31.1 33.6 36.4 2.3 2 285 260 320 216 55.8 168 47.8 217 65.6 100 200 138 234 29.8 0.61 0.6 0.61 5.4 3.5 9.6 19.5 .. 4 0 13.4 • • .01 8.4 63.5 3.3 148 7.1 r 7.2 r e a 1 .1 6.2 42.3 5.2 36.2 38.3 4A 0 15800 57300 2540 71200 13000 17500 9620 14100 136000 12800 20700 9940 17400 23000 5.2 18 5.9 5.1 7/15/2019 1 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units r r 0 . 0r00 w/L �0r0�TotalDissolved l pg/L Concentration Row Labels Column Labels MW-1R MW-2R MW-31R MW-4R MW-51R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 EPA 8260D : • Chloride . • ." - Field Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance deg C Field Temperature Sulfate EPA 8151 Solids Chloride Sulfide Field --------------- 2.3 ----®r "" ---�--- -------------- ------ 4.3 -------- ------------- 1.4feet -----------�- --------------- --------------- --------------- ���■ i������������� .o� 1111111111111MIE 1•1Ir 357000 " .. --------------- --------------- --------------- --------------- --------------- .•��� 726000 ��� ••.:�� .��� - ��� .:��r •��� 1370000 --------------- =,$I NKOMO wr Mie --------------- --------------NE - --------------- 7/15/2019 2 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 6 pg/L NE pg/L 1 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 600 pg/L 3 pg/L 2000 pg/L 88 pg/L 3 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L Ng/L pg/L Concentration Row Labels Column Labels Teel Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance deg C Field Temperature EPA 8260B pg/L 1,1-Dichloroethane 4-Methyl-2-pentanone (MIBK) Benzene cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl acetate EPA 8260B Mod. pg/L 1,4-Dioxane (p-Dioxane) EPA 6010D pg/L Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese 70.39 14.9 33.24 16.3 21.77 73 29.54 106.96 23.01 6.6 8.95 15.79 103.89 77.51 60 21 27 20 30 48 27 60 21 20 15.7 20 60 48 0.4 1.6 1.5 0.8 5.5 2.5 4.9 6.7 0.4 0.5 1 3.6 3.5 4.2 2.8 6.8 3.5 7.1 0.55 0.8 1.1 9.4 7.1 6.6 3.4 3.3 5.7 3.2 5.4 6.3 6.3 6.3 6.2 5.6 5.7 5.7 6.5 5.9 5.9 5.5 5.7 6.1 -135.3 -43.2 -69.5 48 198.2 30.8 145 158.8 175.7 55.8 39.6 27.7 163.8 -59.7 218.7 1145 426 671 170.1 238.2 54.1 152.3 1866 346.4 426 124.8 178 699 13.5 14 14.9 14.7 13.8 7.3 14.6 14.5 13 13.4 14.8 14.2 13.6 15.5 1.3 0.65 0.37 0.55 0.85 0.38 0.86 0.99 2.4 1.1 0.59 0.53 45.4 50.5 169 0.26 0.9 1.2 1.3 1 0.86 0.21 2 2.1 2.4 284 258 275 222 59.8 161 36 215 83.1 95.8 132 124 246 24.4 0.62 0.88 0.69 0.83 3.3 5.5 4.2 5.6 2.6 • 1:01 42.4E250 2.650 c 71.8 ..:15 16.7 : • 4 44 4.7 r 0 9.8 r 7/15/2019 3 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 6 pg/L 6 pg/L 40 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L Concentration Row Labels Column Labels 16.1 5 w qff Iff 11.1 3.3 6.3 Nickel Sodium Vanadium Zinc EPA 7470A pg/L Mercury May-18 EPA 300.0 NgIL Sulfate EPA 6010 pg/L Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470 pg/L Mercury EPA 8260 pg/L 1,1-Dichloroethane 1,4-Dichlorobenzene 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C NgIL Total Dissolved Solids SM 4500-CI-E 16500 64400 2770 42600 14600 17700 8300 15700 151000 13600 17600 10900 18600 26100 5.1 5.2 6 5.3 5.8 0.57 105000 691 50300 8220 14200 2980 ��� 15300 64300 4510 54600 5.7 263 289 234 270 52.5 158 41.2 193 94.7 82.8 82.8 114 212 11.4 2.1 0.63 0.59 6.4 5.3 2.6 4.1 5 3 111 4.9 •: 88.2 35 39.3 35.3 18 3.9 175 108 124 17.6 8 16.8 is 4.1 43.8 4.4 4.2 8.5 .1 7.4 17.4 2.6 1 15500 73200 2680 17800 12800 16600 8810 14300 157000 12000 13400 9540 16900 20500 5 19.9 9 6.6 0.34 0.39 1.1 0.41 0.72 1.7 16.4 0.41 0.55 0.45 0.71 0.55 0.85 0.23 1.2 3 1.7 0.68 1.7 0.65 0.78 46 24.9 192 5.9 14.8 0.93 1.2 1.3 0.89 0.79 0.42 76100 663000 115000 101000 33600 75900 27000 31800 506000 130000 65800 47200 61800 112000 166000 ��� 177000 250000 164000 181000 75000 133000 .swei 232000 218000 107000 152000 369000 7/15/2019 4 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 250000 pg/L 70 pg/L NE pg/L 0.2 pg/L 6 pg/L 6 pg/L 6000 pg/L 1 pg/L 700 pg/L 70 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 600 pg/L 3 pg/L 2000 pg/L Concentration Row Labels Column Labels pg/L Chloride SM 4500-CN-E pg/L Cyanide SM 4500-S2D pg/L Sulfide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH my REDOX pmhos/cm Field Specific Conductance °C Field Temperature EPA 6020B pg/L Thallium December-17 EPA 8260 pg/L 1,1-Dichloroethane 1,4-Dichlorobenzene Acetone Benzene Carbon Disulfide Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane 9040 42200 2180 12500 15200 6490 3660 4830 158000 12500 11100 4790 3930 89700 5 4.8 4.4 4.8 4.2 105 240 71.02 15.65 38.14 16.68 21.98 74.1 31.8 106.92 23.28 7.57 9.22 16.97 104.4 78.28 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1.09 0.71 1.1 0.21 5.49 1.2 5.49 6.55 0.13 1.53 0.36 4.06 5.48 2.01 0.8 1.34 5.46 60.65 1.08 0.57 0.78 2.67 8.15 4.77 1.61 1.55 2.9 5.13 5.5 6.2 6.3 6 5.9 5.5 5.4 5.6 6.3 6 5.9 5.6 5.5 6.2 199.4 4.1 52.1 1988. 194.1 2034. 237.7 185 -105.9 5.1 1962. 256.7 2004. 68 221.7 1391 423.5 343.9 176.7 234.9 70.7 155.8 1840 349.9 304.2 121.8 183.9 641 22 17.2 18.7 18.2 17.3 17.8 16.5 18.9 17.4 17.9 17 16.2 19.1 16.9 0.029 0.54 1.6 0.37 13.7 0.39 0.57 2.1 0.44 0.76 0.66 1.1 0.27 0.23 1.7 3.6 0.41 1.6 1.3 1.1 0.62 1.1 59.1 135 0.35 0.65 1.3 0.58 1.6 1.4 1.4 0.81 0.22 7/15/2019 5 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) I Historical detections by date 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature November-17 EPA 300.0 pg/L 250000 pg/L Sulfate EPA 6010 pg/L 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 10 pg/L Chromium 1 pg/L Cobalt 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 100 pg/L Nickel NE pg/L Sodium 0.3 pg/L Vanadium 1000 pg/L Zinc EPA 7470 pg/L 1 pg/L Mercury EPA 8151 pg/L 50 pg/L 2,4,5-TP (Silvex) 70 pg/L 2,4-D 0.3 pg/L Pentachlorophenol EPA 8260 pg/L 6 pg/L 1,1-Dichloroethane 6 pg/L 1,4-Dichlorobenzene NE pg/L 4-Methyl-2-pentanone (MIBK) 6000 pg/L Acetone 1 pg/L Benzene 70 pg/L Chloroform 70 pg/L cis-1,2-Dichloroethene 1000 pg/L Dichlorodifluoromethane Column Labels MW-1R MW-2R 1.4 MW-3R MW-4R MW-5R MW-61R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 --------------- --------------- --------------- ®-® 10.2 --®�--�-- 23.5 3010 9.41 78700 93 365 ----- 22.5 3270 ----- 29300 1050 10600 5440 1050 13800 1590 169 317 r .r � r r - r � ..r :rr rr r � •:rr ---- 4.9 --------- 3.6 --------------- --------------- 2.6 ----------- 7/15/2019 6 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L 1000 pg/L NE pg/L 500000 pg/L 250000 pg/L NE pg/L 250000 pg/L 700 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.2 pg/L Concentration Row Labels Column Labels 1.4 1.1 m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 pg/L Butylbenzylphthalate SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-S2D pg/L Sulfide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature June-17 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Barium Chromium Cobalt Iron Lead Manganese Nickel Sodium Thallium 0.68 0.97 28 20.1 131 0.93 1.5 1.61 1.2 0.521 0.871 0.71 1.7 71400 670000 78900 461000 33500 80400 28200 27900 520000 130000 73800 44600 63500 110000 15300ONEIRIJIUs 164000 11@ 144000 175000 82000 136000 veil 218000 219000 90000 142000 370000 9290 47600 2650 49200 16200 7390 3860 4430 163000 13000 10400 4770 3620 89800 127 69.55 16.44 40.74 8.92 11.42 73.26 35.28 105.72 24.24 8.7 10.61 18 103.92 39.37 60 21 27 20 30 48 27 60 21 20 15.7 20 60 50.85 0.6 2.09 0.3 0.23 5.95 0.5 4.2 6.3 0.1 0.1 0.34 4.3 3.3 4.36 1.1 11.87 7.6 8.94 0.92 0.1 0.4 7.9 9.3 8.9 1.61 2.8 2.4 98.53 5.6 6.3 6.4 6.2 6.1 5.6 5.6 5.5 6.3 6.1 6.1 5.6 5.5 6.4 158.6 -10.1 -109.6 48.5 70.4 135.5 166.3 206.8 44.7 -43 60.9 182.2 215.5 65.2 208.3 1393 394.2 1209 176.8 288.4 77.4 160 1989 348.3 299.8 111.4 172.7 624 17.2 13.1 15.5 16.2 16.5 16.31 16.3 15.3 16.3 16.4 16.5 17.2 16.1 16 110000 125000 oil 14100 323 343 221 102 4.2 . 9 17 .� 5.8 4.1 •1 • 6.9 72400 42100 123000 11700 0.043 7/15/2019 7 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) I Historical detections by date 0.3 pg/L Vanadium 1000 pg/L Zinc EPA 8260 pg/L 6 pg/L 1,1-Dichloroethane 0.4 pg/L 1,2-Dichloroethane NE pg/L 4-Methyl-2-pentanone (MIBK) 6000 pg/L Acetone 1 pg/L Benzene 700 pg/L Carbon Disulfide 3 pg/L Chloromethane 70 pg/L cis-1,2-Dichloroethene 600 pg/L Ethylbenzene 500 pg/L m&p-Xylene 500 pg/L o-Xylene NE pg/L Tetrahydrofuran 600 pg/L Toluene 3 pg/L Trichloroethene SM 2320B pg/L NE pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L 500000 pg/L Total Dissolved Solids SM 4500-CI-E pg/L 250000 pg/L Chloride Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance 'C Field Temperature May-17 EPA 300.0 pg/L 250000 pg/L Sulfate EPA 6010 pg/L 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 10 pg/L Chromium 1 pg/L Cobalt Column Labels MWAR MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 2.1 -_-_-_-_-_-_-_-_-_-_-_-_-_ --------------- --------------- --------------- -_ 796000 -_ 552000 -_-_ - 1150000 •rrr -_-_-_-_ --------------- r 318000 NEW i —_-- --------------- -- 11.5 ------------ 7/15/2019 8 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) Historical detections by date 2L Units 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.2 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6 pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L Concentration Row Labels Copper Iron Lead Manganese Nickel Sodium Thallium Tin Vanadium Zinc EPA 8260 pg/L 1,1-Dichloroethane Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichlorofluoromethane SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide Field feet Static Water Level Total Well Depth Column Labels 54.8 : • 0 3.4 7 68.4 25.2 12.5 .1 3 4.6 15800 2240 13900 17800 9240 15400 5.5 8.9 5.1 1.3 21.4 18.4 15.7 15.8 0.43 0.38 1.1 1.5 1.2 0.46 32 0.91 1.4 68600 114000 32300 85000 20800 25400 165000 133000 156000 175000 67000 141000 8860 2520 15100 5290 3060 4610 4.4 4.4 9.9 70.19 7.83 36.9 8.21 21.4 73.38 30.33 105.64 11.55 60 27 50 48 27 60 7/15/2019 9 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 0.3 pg/L 1000 pg/L 0.008 pg/L 0.004 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 700 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L Row Labels mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance 'C Field Temperature November-16 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Arsenic Barium Beryllium Chromium Cobalt Iron Lead Manganese Nickel Selenium Sodium Vanadium Zinc EPA 8081 pg/L Heptachlor Heptachlor epoxide EPA 8260 pg/L 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Carbon Disulfide Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene 1.3 0.5 5.4 0.4 5.4 6.51 0.3 4.03 3.28 3.06 3.5 5.3 3.1 4.2 1.16 0.4 9.26 1.75 5.42 23.24 5.5 6.3 5.9 5.5 5.6 5.5 5.9 5.6 5.5 6.3 179.6 -601 182.6 210.21 195 178.8 107.5 138.8 147 121 209.7 392.9 175.5 2207. 68.1 159 367.4 116.5 173.7 690 20.3 20.4 21.2 19.7 17 19.8 17.4 16.9 18.4 17.6 1380 121000 1530 193000 8450 3800 4090 3440 EbM118al 17100 129000 5390 1400 58700 3.9 2.6 241 272 297 255 55.9 140 44 195 148 93.1 144 91.6 188 14 0.58 0.57 2.8 5.8 4.1 6.4 96.2 •: :. is 3.5 214 149 r 2.6 is 274 123 7.3 18.5 • 1 8 8 35.6 2.7 8.5 10.7 1 6.2 26.7 13.7 5 14600 70200 2450 71000 14200 16200 9700 15700 184000 12000 19200 9380 16200 20200 5.7 8.4 7.3 5.7 5.1 12.8 6.3 n ]i 0.53 1.5 0.39 2.5 14.1 0.38 0.42 0.83 5.2 0.44 0.2 0.47 1.1 0.33 0.62 0.88 2.3 0.38 0.55 2.2 2.1 0.63 2.1 0.48 39.1 13.6 21.7 237 26.8 16.8 1.2 7/15/2019 10 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 3 pg/L Concentration Row Labels Column Labels 1.bI 1 2.8 0.58 4.4 I richlorofluoromethane Vinyl chloride SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX Nmhos/cm Field Specific Conductance °C Field Temperature June-16 EPA 8260 pg/L Methylene Chloride Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX Nmhos/cm 64300 571000 133000 454000 32700 80100 25800 23300 626000 107000 72900 42300 59700 101000 154000 Iff M3000 ' Iff 145000 153000 67000 135000 ffd11r'8 189000 286000 79000 118000 371000 9630 47600 2050 58400 16400 4820 2670 4360 202000 14500 23300 4100 3410 98000 5.4 68.82 16.64 2047. 17.87 22.26 36.41 34.35 104.13 24.2 8.77 10.74 18.41 103.03 39.3 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1.52 1.18 2.9 3.5 5.73 1.2 7.7 8.26 1.16 4.39 1.34 4.6 4 3.19 0.72 1.51 5.3 7.03 0.31 0.25 0.31 4.61 6.38 5.81 2.97 7.23 1.95 44.5 5.6 6.2 6.3 6.1 5.9 5.6 5.7 5.5 6.2 6 5.9 5.7 5.6 6.4 137.2 24.1 -61.4 176.7 242.9 152 217.5 272 62.3 16.7 175.1 241.4 270.5 177.6 202.8 1262 380.4 1204 176 203.1 73.7 167.8 2535 355 463.1 106.2 158.6 609.9 16.6 15.9 15 16 16.3 15.3 16.5 17.11 17.2 16.1 16.7 16.4 17.1 15.2 34.65 7.68 36.15 60 20 48 1.7 0.2 0.3 1.4 4.26 0.42 5.4 6 5.6 242.6 212.4 257.5 7/15/2019 11 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 250000 pg/L 1 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 1 pg/L 40 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L Concentration Row Labels Column Labels 194.3 981 198.4 Field Specific Conductance .0 Field Temperature May-16 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Antimony Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Sodium Tin Vanadium Zinc EPA 7470 pg/L Mercury EPA 8081 pg/L Endosulfan 1 EPA 8260 pg/L 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L 22 15.9 17 1080 115000 1800 48700 7620 2930 1630 15800 15200 169000 7280 63700 3.3 5.2 228 324 278 210 55.9 129 38.3 197 292 103 190 210 188 11 3.2 2.2 0.83 2.6 1 3.21 5.1 9.1 2.8 16.4 8.5 78.8 .0 1 87.8 128 1 1 1 8 227 7.2 1.1 8 17.9 .: 3.2 28.8 2.9 6.3 4.7 5.5 6.4 21.6 2.7 5.5 13300 61500 2310 14500 13100 16400 8280 14200 10300 11200 19200 9420 15400 20100 1 3.1 1 2.5 17.8 5.2 34 40.5 5.9 0.12 0.15 1.2 0.26 0.7 0.77 3.6 1.8 2.3 2.9 0.47 1.1 2.8 1.4 2 1.6 2.4 49.6 3.5 13.5 6.1 12.4 27.3 0.71 0.71 0.92 1.3 1.4 1.1 5.1 54900 482000 87800 99000 30800 71700 24800 21200 29000 104000 55900 41000 50400 104000 138000� 241000 154000 137000 87000 103000 311000 236000 382000 145000 85000 418000 7/15/2019 12 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 1111 • 1 • I 1111 • 1 • 1 •/L 10 .Copper 11 . 1 . 11 . 1 . pg/L 1 111 . 13 pg/L 10 . ' 1 . ./L 0.004 ./L Concentration W. •Chloride Column Labels MW-1R •111 MW-2R 11 MW-3R � MW-4R :11 MW-5R 11 MW-6R MW-7 MW-8 MW-9 " 1 MW-10 MW-11 11 MW-12 MW-13 MW-14 MW-15 I SM I I Cyanidefeet Field Static Water Level Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature Novem ' , I I I EPA 6010 Chromium--- ... . SodiumNE Vanadium EPA 7470 • 8081 •Enclosulfan I0.008 Heptachlor Heptachlor epoxide --------------- --------------- -®��---®-®®---- --------------- --------------- --------------- --------------- --------------- --------------- --------------- 1 1 111 11 1 11 �- 1 11 �� . .11 11 1:11 MR 11 1:1 1111 --------------- --------------- ------------®-® ----®----® -�' 17.4 3080 9010 9.1 68200 7100 -®------®-�� 28.3 312 407 2.5 32600 1890 ---- --�- 3.1 3690 587 2.9 34600 2020 ---- 523 790 62.1 466 69.3 8180 297 ----------®' ---- 11 •11 :11 11 - 11 "I,•:11 111Effm11 11off:11 :11 ---------- 8.8 ---- ---------®' ----- 11.9 9.9- 3.7---- 5.6 3.5- 2.6- 18.9 --------------- --------------- 0.12 --------- 0.093 ----- 7/15/2019 13 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 6 pg/L 6 pg/L 40 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L NE pg/L 200 pg/L 0.005 pg/L 100 pg/L 0.05 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L Row Labels EPA 8260 pg/L 1,1-Dichloroethane 1,4-Dichlorobenzene 2-Hexanone 4-Methyl-2-pentanone (MIBK Acetone Benzene Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 pg/L 2,4-Dinitrotoluene 2,6-Dinitrotoluene Benzo(g,h,i)perylene Dibenz(a,h)anthracene Di-n-octylphthalate Indeno(1,2,3-cd)pyrene SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide Field feet 7 0.91 0.38 0.69 2.6 11.8 0.44 0.25 0.26 0.8 0.26 1 0.76 0.23 2.1 0.4 0.84 0.68 1.3 2.3 1.2 2 0.27 0.43 35.8 7 17.7 120 19.8 0.27 0.66 1 1.4 1.1 0.82 0.54 4.8 5.9 8.1 1 5.6 5.6 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000 41000 37100 51500 103000 78000 - .III 137000 161000 104000 78000 79000 142000 403000 281000 234000 110000 135000 362000 8510 48700 2990 16900 16200 6050 2040 4710 47400 14900 9000 3270 3930 113000 7.5 5.1 4.7 9.8 4.2 5.3 5 5.3 7/15/2019 14 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 NgIL 15 NgIL 50 pg/L 100 pg/L NE pg/L 0.2 pg/L 0.3 pg/L 1000 pg/L 1 pg/L 50 pg/L 70 pg/L 6 pg/L 40 pg/L NE pg/L 1 pg/L 70 pg/L 3 pg/L 70 pg/L 600 pg/L 500 pg/L Row Labels 72.25 16.3 43.76 20.31 23.2 76.9 36.73 107.71 24.15 7.17 9.51 17.47 104.89 78.88 Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature May-15 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Thallium Vanadium Zinc EPA 7470 pg/L Mercury EPA 8151 pg/L 2,4,5-TP (Silvex) 2,4-D EPA 8260 pg/L 1,1-Dichloroethane 2-Hexanone 4-Methyl-2-pentanone (MIBK) Benzene Chloroform Chloromethane cis-1,2-Dichloroethene Ethylbenzene m&p-Xylene 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 2.2 2 0.2 3.3 5.9 0.7 4.4 6.3 0.2 0.1 3.4 1.2 4.8 2.8 1 5.6 3 9.6 1 1 1.6 2.6 295 9.3 8.9 51.6 5.9 154.9 5.4 6.1 6.3 5.8 5.8 5.51 5.4 5.31 5.4 5.9 5.81 5.5 5.41 6.2 34.8 -35.2 -91.6 48.8 52.6 30.9 4 54.3 -77.7 -38.7 -23.3 5.2 49.6 34.8 163.2 1044 211.4 395.9 164.5 196.6 58.4 151.5 365.1 400.8 281.5 108.9 152.1 596.2 16 15.9 15.2 15.5 15.91 15.3 15.6 15.9 16.5 15.8 16.2 16.2 16.3 15.6 1700 98400 3000 72700 8000 1850 1860 2030 8770 15300 73600 9330 1790 65400 164 287 214 306 54 122 30 182 660 93.7 60.9 89.3 179 105 2.8 0.66 0.54 4.8 6.7 2.9 7.6 6.3 3.8 8.8 .� 3.3 .��� 2.7 292 113 54 11.6 00 2.9 �� 2.9 0.�� 6.8 17 •: 2.8 27.1 3.4 3.5 5.9 •• 9.7 41.2 25.7 2.8 4.3 11600 5140C 23000 13100 16300 6940 14500 14100 9460 11200 10700 14500 20300 8.7 7.5 6.8 21.2 7.9 49 0.29 0.14 0.43 0.49 1.1 0.96 5.6 0.29 0.46 0.26 0.13 0.73 1 1.5 1.2 7/15/2019 15 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L Concentration Row Labels Column Labels 2.3 2.1 Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C Ng/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature November-14 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc 0.4 0.85 34.6 5.8 14.1 145 16.9 0.63 0.79 1.5 0.79 0.98 0.22 0.59 4.4 39600 358000 107000 117000 28600 64100 20000 18900 47300 132000 19200 36900 45200 91500 133000 ��U9 182000 304000 166000 145000 61000 134000 279000 239000 163000 107000 131000 360000 7640 44200 2990 22200 15700 4340 1960 4290 51800 14400 8070 3760 3510 98200 71.44 16.32 42.18 18.28 21.85 75.46 16.85 53.36 23.35 8.07 9.8 8.98 52.23 39.21 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 4.5 1.6 2 2.5 6.8 0.4 5.7 6.3 1.5 0.3 5.4 2.7 5.2 2 1.2 8.8 6.2 12.2 2.2 1.2 2.3 1.4 246.4 8 7.7 32.7 26.1 81.7 5.5 6.1 6.1 5.9 5.9 5.6 5.7 5.5 5.2 6 6 5.7 5.6 6.2 265.1 15.4 1.1 262.8 244.4 228.8 255.2 2068. 244.7 34.3 230.6 218.9 221.2 176 153.1 985 363.4 422 175.1 194.8 50.9 148.3 297.2 407.8 234.3 115 150.1 611 18 13.7 15 13.3 14.7 16.7 16.1 17.5 17.1 13.4 14.9 18.71 17.1 17.3 1720 117000 3740 143000 8180 1360 2100 12800 32800 8660 43800 2.6 3.5 142 339 221 305 58.2 111 38 193 262 96.8 59.2 130 193 41.5 1.4 1.21 0.6 3.4 4.8 3 4.5 9.6 3.8 4.8 85.8 .1 25.9 of 2.7 1261 7.2 221 1 2.6 76.5 22.9 19.9 55.9 7.6 1 4.1 3.6 1 5.4 233 33 10600 58300 27701 554001 13700 16600 7810 14600 6860 10000 12800 10700 14400 24000 16.8 7.2 5.3 6.2 13.7 13.3 5.3 7/15/2019 16 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 1 pg/L 6 pg/L 6 pg/L NE pg/L 1 pg/L 3000 pg/L 70 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L Row Labels EPA 7470 pg/L Mercury EPA 8260 pg/L 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBI< Benzene Chloroethane cis-1,2-Dichloroethene Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide SM 4500-S211) pg/L Sulfide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature May-14 EPA 300.0 pg/L 7 0.33 1.1 1.3 0.4 2.2 0.42 0.44 2.1 0.5 0.73 0.35 0.73 1.1 1.1 0.33 2.9 0.36 0.65 79.21 15.9 8.8 106 15.5 0.85 2.4 1.2 0.96 0.57 3.9 37600 453000 177000 286000 24000 62400 22800 18300 42200 143000 40500 36200 42300 54700 120000EFLGAIIIIU 191000 . sls 163000 138000 64000 141000 86000 228000 135000 119000 119000 464000 7090 49800 2940 50500 15500 4300 1350 3610 2220 15000 8240 5870 3720 146000 4.4 4.2 10.4 4.3 5.1 260 130 151 69.7 17.18 21.87 18.4 22.36 36.9 37.58 104.74 24.68 5.4 10.76 18.48 103.8 79 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1 0.5 6.3 0.5 5 0.5 2.3 8.3 0.5 0.5 0.5 3.8 1.25 1.7 3.53 5.2 10 3.6 1.2 9.1 2 98 9.9 5.2 152 7.8 20.1 5.6 6.1 6 5.9 6 5.6 5.7 5.5 5.1 5.9 5.9 5.6 5.6 6.2 194 38 13 158 198 184 224 252 198 -61 101 232 242 182 138 1150 363 971 184 186 59 161 106 440 203 120 159 647 14.8 13.2 13.2 13.7 12.9 13.7 13 12.4 15.3 15.4 15.4 13.8 11.9 16.7 7/15/2019 17 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 250000 pg/L 1 pg/L 10 pg/L 700 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 1000 pg/L 1 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L Concentration Row Labels Column Labels 136000 4230 85200 8060 1 10700 48000 8680 59500 Sulfate EPA 6010 pg/L Antimony Arsenic Barium Chromium Cobalt Iron Manganese Nickel Selenium Sodium Zinc EPA 7470 pg/L Mercury EPA 8260 pg/L 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units 8.9 124 324 205 264 54.4 90.8 30.7 168 132 94.3 61.1 77.1 163 8.6 5.6 52.9 20.6 123 6.1 15.5 10.9 11 •.1 14.6 232 34.1 142 40.2 292 34.7 16.5 11.5 10800 59700 39700 13600 14200 6160 12400 849C 11000 11200 12800 24200 11.4 17.2 11.7 0.51 0.831 0.81 0.28 0.49 0.38 0.37 0.31 72.6 11.8 5.2 18.6 21.4 0.71 3.7 0.62 0.47 0.2 0.32 0.34 5.3 30000 344000 155000 222000 31900 51900 21300 18300 31400 175000 45500 46400 37400 96600 91000 ��� 187000 445000 167000 126000 50000 107000 63000 207000 149000 113000 124000 373000 5600 50500 3260 29700 13900 3600 1800 3610 1820 12400 6180 3880 3630 83400 70.78 14.24 37.86 14.47 20.22 74.12 26.82 52.72 11.34 8.55 9.77 17.91 103.61 76.95 60 21 27 20 30 37.05 27 60 21 20 15.58 20 60 50.85 5.3 4.8 6.3 6.2 8.6 3.8 8.4 8.7 8.3 7.5 8.4 6.8 8.1 5.4 3 11 6 17 10 6 8 5 4 22 15 147 118 50 7/15/2019 18 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 250000 pg/L 700 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 50 pg/L 70 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L Row Labels 5.6 5.8 6 5.7 5.7 5.3 5 5.2 5 6 5.9 5.6 5.5 6.3 Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature November-13 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Barium Cobalt Iron Manganese Nickel Sodium Vanadium _ Zinc EPA 8151 pg/L 2,4,5-TP (Silver 2,4-D _ EPA 8260 pg/L 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C NgIL Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide Field feet 411 243 146 374 389 363 389 436 436 27 315 367 437 406 137 1040 367 715 194 171 64 155 86 430 243 149 156 623 18.41 19.6 18.7 14.8 14.7 17.2 16 17.7 15 14.4 15 16.6 17.7 17.8 128000 3400 113000 8310 10400 27400 9360 53200 106 311 201 296 53.9 98.8 25.4 170 112 87.8 47.6 106 140 23.8 89.5 136 136 84.3 Is 253 W 8 239 27.1 • • • 5.3 19.4 6.8 6.9 7.9 8 48.8 14 9940 46200 42600 13800 13000 5580 13500 9070 10500 11700 12300 25300 12.2 17.1 0.23 1.1 1.3 0.9 0.27 0.77 0.41 0.54 0.28 0.86 0.54 99.6 11.7 13.7 5 14.7 0.89 12 0.47 0.69 0.33 7.6 28100 349000 155000 224000 31700 51600 19700 18400 26700 161000 39300 43200 32800 64300 103000 ��� 193000 496000 154000 116000 61000 124000 66000 236000 126000 114000 123000 410000 5880 56700 3620 36500 15200 5160 1510 3950 1790 14000 6230 5700 4100 124000 7.1 5.9 6 5.2 7/15/2019 19 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6 pg/L 40 pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 500 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 500 pg/L NE pg/L Row Labels 71.87 16.65 45.08 18.63 22.73 76.44 36.08 106.03 24.77 9.1 10.56 18.83 104.66 79.28 Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Sid. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature May-13 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Tin Vanadium Zinc EPA 8260 pg/L 1,1-Dichloroethane 2-Hexanone Acetone Benzene Chloroform cis-1,2-Dichloroethene m&p-Xylene Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Xylenes (Total) SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 8.7 0.9 0.7 7.5 5.6 0.5 10.2 9.2 2.2 0.5 6.5 1.3 6.5 2.8 1 3 1 12 3 2 5 11 4 8 9 123 250 21 5.6 5.6 5.9 5.8 5.9 5.51 5.4 5.2 5.2 5.91 5.8 5.4 5.41 6.2 228 68 -8 207 239 200 357 363 327 -66 189 280 355 241 104 840 316 678 168 144 48 138 63 385 153 115 123 614 18.3 13.8 15.9 17.2 17.4 16.5 15.1 16.31 16.7 16.7 17.1 14.8 16.7 17 115000 5070 97600 11200 2100 3200 11000 51800 7820 41200 109 324 216 375 57.7 115 28.5 174 115 87 50.1 176 254 59.6 2.4 1 7.11 6.6 7.6 9.5 158 126 61.5 92.8 0 . I 13.2 6.5 � 8.6 .1 :: •. 20.7 24.9 16.6 9080 45700 42600 13000 14300 6120 12900 829C 11100 19100 13500 26700 5.8 21.1 10.5 13.6 37.3 27.4 22.7 1.2 0.84 0.48 20.3 0.63 0.26 0.72 0.96 1.3 0.54 0.27 111 8.5 24.2 7.4 0.68 12.1 0.25 0.36 0.38 4.3 1.2 29800 363000 175000 203000 34800 63500 22800 21700 32100 189000 29600 58700 35600 78900 7/15/2019 20 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 0.1 pg/L 0.002 pg/L 42 pg/L 2 pg/L 2 pg/L 0.004 pg/L 6 pg/L Concentration Row Labels Column Labels pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature November-12 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 8081 pg/L 4,4'-DDD Dieldrin Endosulfan II Endrin Endrin aldehyde Heptachlor epoxide EPA 8260 pg/L 1,1-Dichloroethane 84000 :•1IP v6006 413000 131000 108000 51000 100000 46000 228000 138000 87000 102000 442000 5910 50000 3860 33700 16200 5340 2070 4300 2040 14200 5820 3820 4290 124000 8.1 5 73 15.54 21.94 17.53 21.44 38.62 31.43 106.24 23.65 8.13 9.59 17.62 104.48 78.61 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 8.3 1.9 6 2.7 7.1 0.9 7.2 7.4 3.1 6.4 9.3 1.3 6.4 2.5 1 1 1 36 1 1 1 44 1 6 5 587 446 190 5.6 5.8 5.8 5.6 6 5.3 5.5 5 5.2 6.2 5.8 5.6 5.5 6.1 263 10 21 246 274 211 260 282 267 -22 185 204 254 224 68 802 217 382 116 106 31 88 43 400 197 136 81 403 20.9 19.7 15.71 15.6 15.21 16.3 17.5 18.1 16.31 14.71 14.7 16.51 18.2 17.9 79500 5420 73600 8400 2090 10400 24200 9770 35600 7.1 91.7 335 173 400 53.4 95.1 26.9 142 101 76.8 50.5 279 160 143 3.5 6 6.7 6.9 5.8 10.5 �� 102 60.8 218 •��� 1 �� 7.5 1 1 9.5 21.8 17.4 5.1 33.6 8 13.7 9180 43400 43600 14500 13900 6980 13100 5280 8770 11000 14600 15000 21200 24.5 15.2 92 30.8 51 23 45.6 0.062 0.12 0.27 0.23 1.2 1.2 7/15/2019 21 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 1 pg/L 3000 pg/L 70 pg/L 70 Ng/L 1000 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 500 pg/L 0.05 pg/L 3 pg/L 5 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L Row Labels Benzene Chloroethane Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Xylenes (Total) EPA 8270 pg/L Benzo(a)anthracene Bis(2-ethylhexyl)phthalate Chrysene SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide SM 4500-S2D pg/L Sulfide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH my REDOX 1.3 0.16 0.49 l 0.62 0.28 1.6 0.63 93.2 13.5 26 6.3 0.77 16.9 0.29 0.49 0.49 8.1 0.98 0.79 2.4 1.5 1.1 1 26300 277000 142000 174000 31200 51900 19500 17200 25500 153000 40200 43900 28900 77600 95000 MkIN 11r' 172000 435000 157000 111000 58000 118000 63000 220000 127000 144000 127000 298000 5320 64000 3920 34500 16100 3810 1860 3560 1800 12900 4900 6150 4790 143000 9.1 106 100 72.24 17.78 45.36 1926. 22.81 77.49 37.56 105.53 25.13 8.94 10.71 18.71 104.68 79.91 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 5.5 1.5 1.2 2.3 6.4 1.8 9.8 7.3 4.4 0.9 3 2.3 6.4 2.3 1 1 25 14 14 7 1 1 1 25 1 605 329 456 5.7 5.8 5.6 5.7 5.8 5.4 5.7 5.5 5 6.1 5.9 5.5 5.5 6.5 236 77 16 181 245 197 260 352 366 -61 150 246 365 160 7/15/2019 22 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 1111 • 1 • 1 •/L 11 • 1 • 11 . 1 . NE pg/L 13 pg/L 1000 . 1 11 pg/L 0.006 . 0.019 . 0.019 . 0.002 . 1008 . 0.004 ./L 1 ./L 1 ./L 11 . 1 . 10 • 11 • Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Field Specific Conductance Field Temperature EPA 1 i i EPA 6010 Chromium-®---------® Cobalt14.8 .n Sodium:•11 Vanad EPA 8081 ■ ■ ■ 4,4'-DDT .. . . - . . - Dieldrin Heptachlor Heptachlor epoxide Methoxychlor------------- • 8260 Chloroform--------------® • - o-Xylene------------- • . " - " . . . . - -s (Total)-®------------- --------------- --------------- --------------- 111 ®" '1 •: 11----- 11 1 11 �- :11 --------------- --------------- --------------® 16.4 21.5 ----------- 26300, 5391, 3760 1140 10000 -®�------ 8280 9310 370 --®- 91.5 170 327 -® - '1.11 11 - 11 .11 -� .11 . 11 11 . 11 ------------ 7.2 - 23.4 -®----------�-® --------------- --------------- ------ 0.13 -------- �0. 0.54 - ------------- ---- 0.14 ------ 0.1 1 1 ---- 0.18 - 0.069 0.081 -------- 0.48------------- ------ 0.066 -------- --------------- --------------- 1.5 ------------- 3.2 ------------- 1.7 ------------- ------------® 7/15/2019 23 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 0.005 pg/L 0.05 pg/L 200 pg/L 3 pg/L 0.005 pg/L 0.05 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 250000 pg/L 700 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L Concentration Row Labels Column Labels EPA 8270 pg/L Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Bis(2-ethylhexyl)phthalate Dibenz(a,h)anth racene Indeno(1,2,3-cd)pyrene SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide SM 4500-S2D pg/L Sulfide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature December-11 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Barium Chromium Cobalt Iron Manganese 1.3 1.2 1.5 27100 196000 150000 64300 134000 50200 20100 20100 413000 120000 37200 52200 30100 75300 93000 119 168000 374000 149000 109000 52000 123000 49000 161000 130000 110000 145000 260000 5350 61500 33200 16100 10800 8200 5380 60600 6.5 178 36.43 7.99 21.01 8.24 10.55 38.23 15.03 52.4 11.92 4.13 5.04 8.92 52.03 39.39 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 5 2.9 0.8 0.7 8.7 0.8 6.7 7.2 4.8 0.5 5.4 1.6 6.9 2.5 1 4 3 7 2 1 7 2 2 14 8 150 32 112 5.2 5.8 5.8 5.5 5.4 5.5 5.5 5.2 5.2 5.5 6.1 5.9 5.8 6.4 166 43 -24 156 189 185 176 180 196 -78 166 189 177 121 102 809 329 568 182 149 52 140 66 325 176 144 150 404 16.7 15.2 13.8 13 13.9 14.71 14.4 16 14.5 14.21 15.1 15 16.4 16.7 61800 7020 82.6 328 85.2 4 43.5 F1 7/15/2019 24 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units NE pg/L 0.3 pg/L 1000 NE pg/L ■r000TotalDissolved 250000 250000 1000 rr pg/L 0 100 NE pg/L 0 ■ r 6000 Concentration Column Labels MW-1R MW-21R MW-3R MW-4R MW-5R m9wono MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Sodium Vanadium Alkalinity, Total as CaCO3 . . . . feet Field Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature Novem EPA • 1 1 EPA 6010 Copper Iron Sodium . EPA 8260 . 13 ----®---------- --------------- --------------- r■ -- r •r ---------- --- r ---------- --------------- --------------- --------------- --------------- --------------- --------------- ' . --------� r-- --------------- 11.8 ------------ 2980 40300 ----®- 4241 230001 30301 1250 58.3 6140 140 2050 71 - -_ -_ 7920 7310 -_-_-_®_�_-_ -©--------- ------------ 10.8 -- -®-----®----�®- --------------- -®------------- 7/15/2019 25 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 1 •/L 11 • 11 . 1 . 111 ./L pg/L 11111 . NS pg/L NE pg/L 1 . NE pg/L Concentration Column Labels MW-1R MW-21R 2 MW-3R -_-_---__---- MW-4R MW-5R MW-61R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Chloroform------------- : • - Chloride o-Xylene-®------------- .. - - - TrichlorofluoromethaneNE Alkalinity, Total as CaCO3'111 •Total. -. SolidsChloride Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 350.1 Nitrogen, Ammonia EPA 6010 •SodiumEPA 8260 • . - - - Alkalinity, Total as CaCO3------------- 3.5 ------------- 1.8 ------------- ----�-�®1 "" ----- --------------- 111 --- 11 •.11 •11 11 1111 11 •11 1. 11 --------------- ••:111 :1111 --- '111 111 :111 :•111 . 111 •111 •111 :111 --------------- --------------- --------------- --------------- --------------- --------------- --------------- 11 ------------- --------------- 1.6 ------------- 1.6 ------------- --------------- --------------- --------------- 7/15/2019 26 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 250000 •Chloridefeet r pg/L r 500 11 . r . Concentration LabelsRow SM ' I • Field Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature May-1 1 EPA 6010 EPA 8260 Chloroform------------- . .. :. Chloride o-Xylene------------ .. - Field Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Column Labels MWAR ---_-_---__---- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 --------------- • • ------------- --------------- --------------- --------------- --------------- �r 1.3 ------------- 4.1 ------------- 1.4feet ------------- --------------- --------------- --------------- --------------- 7/15/2019 27 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 11 pg/L 1 • 111 •/L Concentration Column Labels MW-1R MW-21R MW-3R MW-4R MW-5R MW-61R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Field Specific Conductance Field Temperature EPA 6010 Barium • 8260 Chloride Field Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature 1 • 8260 Field Trichlorofluoromethanefeet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 6010 --------------- --------------- --------------- -®�-®-------- 4.2feet ------------- --------------- --------------- --------------- --------------- --------------- ------------- --------------- --------------- -®------------- --------------- --------------- --------------- --------------- --------------- --------------- 7/15/2019 28 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 1 . 11 . 1 . 111 •/L 11 1pg/L 1 . Concentration Column Labels MW-1R MW-21R MW-3R MW-4R MW-5R MW-61R MW-7 MW-8 MW-9 ---®--- MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 • 8260 Field Trichlorofluoromethanefeet Static Water Level TotalDepth g/L Oxygen,Dissolved NTU Turbidity • Field • mv - ■. pmhos/cm-11■1■1■1■1■1■1■1■11■1�1■}T�1■1■y}�1■1■ - • Specific Conductance�Illll�llll�lllllmlllllml■IIIIIm11111m11111m11111:iiJ11111r.•.Illllmlllll�...11lllml■ Field TemperatureField feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 6010 Silver EPA 8260 • ■ .. - - - �11111�1111�1111�111�1■1111�1111•..w..11lll�llll®• ' ' 1111�' 1111�Illllm' 11111�1■ �IIIII.w...1111:Gii:J1■Illl.�a.•1■1111....1■1111'w��ll■1111.�a..11111�111111:Gai1111.��.1■ -11■1■1■1■1■1■1■1■11■1■1■1■1■1■ -11■ 1■ 1■ 1■ 1■ 1■ 1■ 1■ 11■ 1■ 1■ 1■ 1■ 1■ -®1■1■1■1■1■1■1■11■1■1■1■1■1■ -11■ 1■ 1■ 1■ 1■ 1■ 1■ 1■ 11■ 1■ 1■ 1■ 1■ 1■ -11■ 1■ 1■ 1■ 1■ 1■ 1■ 1■ 11■ 1■ 1■ 1■ 1■ 1■ ®' ' 11111' 111•. w,.' 111®' 1111T1■111.. w..' ®®111®' ®111r1�111�®1■ ®IIIIImlllllm111111111■Illllm®Illllm®Illllmlll•n�. .' Illllmlllllml■ -11■ 1■ 1■T 1■ 1■ 1■ 1■ 1■ 11■ 1■ 1■ 1■ 1■T 1■ �_IIIII:iIIJ®IIIIIiLiilllll�' 1■®_®_IIIII•SJ' 11111�11111�11111�' ' IIII�IIIIIICJI■ ©111111101111110' Illllm©1■©11111101111110' ©®®1■Illllml■ -11■1■1■1■1■1■1■1■11■1■1■1■1■1■ �_®_III®' 1111�' 111�1■®_®_®_IIII®' 1111��®_®_®_I■ ®' 11111�®1111®' 1111�1■®1111�1111� Illlla....11lllm®1111�1■ -11■ 1■ 1■ 1■ 1■ 1■ 1■ 1■ 11■ 1■ 1■ 1■ 1■ 1■ �IIIIIIli3:illll�lllllli3:i1111�1■1111�®1111�®IIIIIC�i7®1111•nw.•1111�1■ ■ ��i ■■ 1� �11111 .•w.11ll�llllmllll�" 1■Illllm®Illllmllll�llll..w..11lllli.i' ®1111�1■ 11111•w•.'.1■111113i11111r6J1■1111'w'.•.IIII.w...1111.��.1111�11111:SJ1111.��.1111rQiL1111'��al■ --------------- -11■1■1■1■1■1■1■1■11■1■1■1111�' 1■1■ 7/15/2019 29 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) I Historical detections by date 700 pg/L Carbon Disulfide 3 pg/L Methylene Chloride 2000 pg/L Trichlorofluoromethane Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved NTU Turbidity Std. Units Field pH my REDOX Nmhos/cm Field Specific Conductance °C Field Temperature March-09 EPA 6010 pg/L 700 pg/L Barium 10 pg/L Chromium 20 pg/L Silver EPA 8260 pg/L 700 pg/L Carbon Disulfide Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved Std. Units Field pH my REDOX Nmhos/cm Field Specific Conductance 'C Field Temperature December-08 EPA 6010 pg/L 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 20 pg/L Selenium 20 pg/L Silver EPA 8260 pg/L 70 pg/L Chloroform Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 --------------- --------------- --------------- --------------- --------------- --------------- --------------- 40.2 - ------------- 26.2 - --------------- 7/15/2019 30 of 36 A3 700 pg/L 10 pg/L 20 pg/L 20 pg/L 1 pg/L 4000 pg/L 6000 pg/L 700 pg/L 10 pg/L 1 pg/L 20 pg/L 20 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) I Historical detections by date Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved Std. Units Field pH my REDOX Nmhos/cm Field Specific Conductance °C Field Temperature March-08 EPA 6010 pg/L Barium Chromium Selenium Silver EPA 7470 pg/L Mercury EPA 8260 pg/L 2-Butanone (MEK) Acetone Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved Std. Units Field pH my REDOX Nmhos/cm Field Specific Conductance 'C Field Temperature November-07 (blank) pg/L Barium Chromium Mercury Selenium Silver Field feet Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 --------------- --------------- --------------- --------------- --------------- --------------- --------------- --------------- --------------- 7/15/2019 31 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 4000 pg/L 700 pg/L 10 pg/L 15 pg/L 20 pg/L 10 pg/L 700 pg/L 2 pg/L 10 pg/L 15 pg/L Row Labels 38.12 9.32 22.72 10.65 11.65 40.4 16.78 50.38 12.34 4.33 4.95 9.27 50.78 Static Water Level Total Well Depth mg/L Oxygen, Dissolved Std. Units Field pH my REDOX Nmhos/cm Field Specific Conductance 'C Field Temperature April-07 (blank) pg/L 2-Butanone (MEK) Barium Chromium Lead Selenium Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved Std. Units Field pH my REDOX Nmhos/cm Field Specific Conductance 'C Field Temperature November-06 (blank) pg/L Arsenic Barium Cadmium Chromium Lead Field feet Static Water Level Total Well Depth mg/L Oxygen, Dissolved Std. Units Field pH my REDOX Nmhos/cm 60 21 27 20 30 48 27 60 21 20 15.58 20 60 5.08 0.72 1.69 1.32 6.5 0.85 7.12 7.32 6.59 1.02 2.01 5.16 7.33 6.52 6.67 6.21 6.35 7 6.07 6.27 5.73 5.95 6.67 6.48 6.83 5.82 59 61 66 43 61 53 66 56 73 -801 21 73 58 85 176 217 394 161 126 51 121 36 121 114 65 140 15.42 14.08 13.221 16.04 14.9 14.16 15.48 15.75 16.38 16.33 16.3 15.32 15.75 11 81 79 310 200 58 89 30 140 52 25 31 79 210 6.4 6.6 5.2 37.43 8.58 20.12 8.71 10.33 39.81 14.14 49.98 11.43 2.66 4.21 8.67 49.43 60 21 27 20 30 48 27 60 21 20 15.7 20 60 3.82 0.48 290 1.07 5.55 0.67 5.14 5.35 5.53 280 6.57 4.59 5.7 5.86 5.59 5.81 6 6.17 5.66 5.03 5.86 5.62 5.96 6.02 5.72 5.79 58 50 -3 -8 36 30 48 90 124 -114 87 110 99 91 151 324 333 171 139 52 115 39 125 105 72 140 15.4 12.4 14.2 12.1 13.5 15.41 14.3 15.5 14 13.9 13.5 12.9 15.4 8.3 94 90 2301 220 58 76 29 140 71 24 66 62 460 6.2 38.17 8.74 22.3 9.81 11.17 40.13 16.19 49.85 11.94 3.41 4.65 8.92 40.93 60 21 27 20 30 48 27 60 21 20 15.6 20 60 4.28 0.31 1.15 0.42 5.88 1.21 6.2 5.44 5.67 0.31 0.85 4.54 6.41 6.29 5.97 5.94 6.16 6.49 5.94 6.15 5.94 5.84 6.64 6.24 5.84 6 -13 114 160 59 59 95 35 90 221 67 132 235 171 7/15/2019 32 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 11 • 1 '/L 11 • 1 •/L 11 • 1 •/L 1 • 1 • 11pg/L 1 '/L 11 • 1 'Chromium--wwwwww 1 • 1 • 11 . 1 ./L 1 . 11 ./L Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Field Specific Conductance�®wwww®wwww®w®w FieldTemperature . 1 Barium Chromium-�wwwwwww�ww© November-05 ' EPA 6010 Barium Chromium--ww®wwwwwlwww®w . • 1 ' EPA 8260 •Chloromethane-wlww June-05�a Barium Chromium--ww®wwww-wwwww November-04 Barium Chromium©wl®w August-14��www Barium ' May-14��wwwwwww�wwww�■w Barium Chromium ' November-03���� Barium ��wwwwwww�wwwww wwwwwwwww ��wwwwwww��wwww ��wwwwwww�wwwww ��wwwwwww�wwwww 15 w ��wwwwwww�www®w ��wwwwwww�wwwww ��wwwwwww�wwwww 11 wwwww 11®wwww ��wwwwwww�www®w --wwwwwww-wwwww ��wwwwwww�wwwww ®ww®w®®w®www®w --wwwwwww-wwwww ��wwwwwww�wwwww 5.4 wwwwwlwwwww �w�wwww�wwwww ��wwwwwww�wwwww ��wwwwwww�wwwww 11 w®w®®wwwwwww ®-wwwwwww-wwwww --ww- .wwww-wwwww ��wwwwwww�wwwww ��wwwwwww�wwwww --ww®wwww-wwwww 14 wwwww®www �wwww�ww�ww ��wwwwwww�wwwww ��wwwwwww�wwwww --wwwwwww wwwww 14 13 ®w®®w ��wwwwwww�wwwww --wwwwwww®' wwwww ��wwwwwww�wwwww ��wwwwwww�wwwww ��ww©wwww wwwww wwwww 14 ®® 26 28 wwlwwwww 18 ®ww 41 wwlwwwww �wwwww�wwwww ��wwwwwww�wwwww ��wwwwwww�wwwww ��wwwwwww�wwwww 820 ®w-wwwww 7/15/2019 33 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 1 ./L 1 ./L 1 . 11 . 1 ./L 1 • 1pg/L 11 . 1 ./L 600 ./L 1 . 11 . 1 ./L 1 . 11 1 .Chromium 11 • Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 150 MW-8 ®------- MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 ChromIum Cadmium---- Chromium • " Chromium November-0111 Arsenic Chromium Toluene Chromium i June-00 22 ----- 24 -------- �� 2.7 ---------- 17------- --------------- --------------- --®------------ ����------- 23 26 23 ------- -- 21 ----------- ------®' .----------- --------------- --------------- 16 17 36------- ®.1 22 ®----- 16 11 19 35 900 95 36® � 140 95 38 1300 270 36 2700 94 150 ------- ------ ------ --------------- --------------- -- �®.1 16 18 950 50 53 1 38 -- ®i 49 16 46 =------ 1300 2600 210 92------- 26 210------- ------ --------------- 1 ®� 31 1500 1 ®�� 11 45 2600 89�------ 4200 -- 100 80 �r--------- 28 82 580 240 65 400 ------- --------------- --------------- ®'-------- --------------- 7/15/2019 34 of 36 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date 2L Units 1 . r 10 pg/L 10 pg/L r 10 pg/L 6000 10 pg/L ;; 10 pg/L 10 pg/L 00 pg/L 10 pg/L r 10 pg/L 00 10 pg/L pg/L r0 10 pg/L Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Chromium Arsenic Chromium Chloride - . Arsenic Carbon Disulfide :u Chromium Arsenic Barium Chromium Chromium Ill .mium ' Silver . .. Chromium --®®----------- ®i ® 14 860 ��-------- 24 60 29 Mlff� 40 40-®-------- 62 -------- -- ----------- -- ----------- ®i ME11E1EEl� -- 13 ®i 13 950 EEEE 110 38 MINE190 50 16 - 10 10 960 30 10 -------- -------- -------- -- ---------- - �---------- 11 1100 1400 2000 � 1300 ------- 12 - 210 68 77 300 39 76 96 29 12 - 350 36May-98 -------- ------- NINE -- ---------- -- ----------- 49 - 34 19 860 25 32 850 130 43 820 170 69 33 20 1200 430 38 ------- ------- ------- --------------- --------------- 11 ® 43 31 16 26 55 29 16 31 14 EEE[l� 1800 410 53 -------- -------- -------- MEN -ow---------- --------------- � � 3 800 ------------- 750 -------- 28 27 - 70 21 180 2320 -------- -------- MEE 01 M■ M■ --------------- --------------- MEEE�lME� -MEE� MEE� 790 20 15 720 47 16 43 20 10 ��-------- 970 21 -------- -------- 7/15/2019 35 of 36 A3 4000 pg/L 700 pg/L 2 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Historical detections by date Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Barium Cadmium .. e . • --------------- 1230 � 1000 1400 1930-------- 7 12 21 f96 12 28Lead 26 15 17 18 17Mercury 1.8 � 1.7 1.4I 1.4-------- 7/15/2019 36 of 36 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Surface water detections of concern within the last 6 years Max of Result Column Labels 79- SW-1 EPA 300.0 250000 pg/L Sulfate 7970 4140 2060 2730 2530 3410 4320 4460 3690 3130 2820 2190 2700 EPA 6010 150 pg/L Arsenic 3.6 5.9 21000 pg/L Barium 68.2 47.5 86.8 65.9 69.5 65 72.2 276 65.8 71.1 58.9 6.5 pg/L Beryllium 1.1 NE pg/L Cadmium 0.7 11 pg/L Chromium 13 NE pg/L Cobalt 9 14.6 NE pg/L Copper 8.6 3.9 16.4 1000 pg/L Iron 6560 4900 5040 5660 5520 9830 8870 155000 8210 22800 6900 NE pg/L Lead 18.3 NE pg/L Manganese 926 461 804 1050 465 688 1160 1760 749 1530 855 25 pg/L Nickel 8.7 NE pg/L Selenium 7 NE pg/L Sodium 15600 17000 23000 14200 13000 12800 16000 12500 14500 13000 12400 NE pg/L Vanadium 4.3 37 NE pg/L Zinc 5.2 10.1 7.2 7.5 69.8 EPA 601OD 21000 pg/L Barium 109 47 1000 pg/L Iron 889 1840 NE pg/L Manganese 48.5 135 NE pg/L Sodium 19400 11800 EPA 8260 2000 pg/L Acetone 11.2 11000 pg/L Methylene Chloride 2 Field Field pH 6.7 6 6.5 7.4 6.5 6.4 6.7 6.3 6.1 6.4 6.2 6.4 Field Specific Conductance 226.3 125.1 211.3 211 250.9 208.3 92.6 228.7 247 205 246 208 Field Temperature 17.5 11 22.8 8 21 17.2 9.4 20.4 10.8 21.2 13.7 22.4 Oxygen, Dissolved 4.49 6.2 4.34 6.6 4.7 3.25 5.5 4.5 0.5 5.5 3 5 REDOX 173.3 44.2 6.6 -121.9 -7.1 14.7 -78.3 11 7 284 -31 -13 Static Water Level Total Well Depth 0 Turbidity 18.8 15.3 25.06 4.96 15.12 19.33 48.7 26.5 363.9 51 35 45 SM 2320B 20000 pg/L Alkalinity, Total as CaCO3 22300 27400 49200 43600 33200 57400 27700 35100 44500 63700 45200 72700 58000 SM 2540C NE pg/L Total Dissolved Solids 174000 106000 131000 123000 143000 116000 118000 113000 140000 122000 126000 125000 104000 SM 4500-CI-E 230000 pg/L Chloride 55400 18300 29700 35700 49200 26800 26000 21600 31500 19500 23700 18100 20600 SM 4500-CN-E 5 pg/L Cyanide 4.4 4.7 SW-2 EPA 300.0 7/15/2019 1 of 5 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Surface water detections of concern within the last 6 years Max of Result Column Labels 26 250000 pg/L Sulfate 13500 20000 11100 9920 10900 6270 17100 11600 7280 5620 12700 5490 5090 EPA 6010 150 pg/L Arsenic 3.7 17 6.2 21000 pg/L Barium 74.2 65.4 77.5 108 73.1 70 700 171 59.7 50.1 51.7 6.5 pg/L Beryllium 3.7 0.64 11 pg/L Chromium 2.8 3.8 40.3 3.2 NE pg/L Cobalt 5.9 4.4 NE pg/L Copper 81.6 3.2 1000 pg/L Iron 2540 1740 1790 29900 1510 2070 226000 75000 2130 3360 1400 NE pg/L Lead 2.7 75 7.4 NE pg/L Manganese 397 196 304 1160 317 291 1020 1010 219 152 153 25 pg/L Nickel 16.4 3.1 NE pg/L Sodium 11300 11600 11600 10200 8420 11300 8390 17600 9840 10300 9160 NE pg/L Vanadium 3.2 127 11.6 NE pg/L Zinc 249 28 EPA 601 OD 21000 pg/L Barium 85.6 78.8 NE pg/L Copper 4.1 1000 pg/L Iron 4370 4140 NE pg/L Manganese 680 615 NE pg/L Sodium 12300 11900 EPA 7470 0.012 pg/L Mercury 0.2 EPA 8260 NE pg/L 2-Hexanone 1.8 2000 pg/L Acetone 12.9 NE pg/L Chloromethane 0.12 NE pg/L cis-1,2-Dichloroethene 0.33 11000 pg/L Methylene Chloride 3.1 110000 pg/L Tetrahydrofuran 61.3 18.4 11 pg/L Toluene 0.52 EPA 8260E Mod. NE pg/L 1,4-Dioxane (p-Dioxane) 1.3 Field Field pH 7.42 6.6 6.5 6.8 7.1 6.8 6.5 6.6 6.5 6.3 6.8 6.7 7 Field Specific Conductance 213.2 203.7 179.4 783.6 181 172 208.7 88.6 185.9 324 183 134 144 Field Temperature 23.4 11.1 19 3.2 10.3 21 21.5 11.9 19.7 11.2 19.7 12.7 23 Oxygen, Dissolved 7.32 7.2 6.82 2.4 7.8 6.3 1.91 3.5 0.2 2.11 7.3 4 9.5 REDOX -63.5 -21.1 -4.8 -68.9 -50.3 -15.2 -57 -84.6 -79.4 -36 252 -12 -10 Static Water Level Total Well Depth 0 Turbidity 40.5 15.7 19.24 554.5 8.66 14.72 34.84 20.5 385.5 136.9 23 2 11 SM 2320B 20000 pg/L Alkalinity, Total as CaCO3 54900 62600 56000 57600 46200 58800 32300 43200 33200 2390 41300 48900 48600 SM 2540C NE pg/L Total Dissolved Solids 182000 144000 135000 125000 129000 106000 113000 105000 125000 117000 120000 114000 91000 7/15/2019 2 of 5 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Surface water detections of concern within the last 6 years Max of Result Column Labels I 79- SM 4500-CI-E 230000 pg/L Chloride 19400 12800 13500 15200 13800 6190 9720 12500 4050 28200 10700 11600 10800 SM 4500-CN-E 5 pg/L Cyanide 4.2 SM 4500-S2D NE pg/L Sulfide 142 SW-3 EPA 300.0 250000 pg/L Sulfate 43600 16000 18500 33800 15200 18500 11400 27000 17000 16800 26300 62500 20100 EPA 6010 21000 fag/L Barium 223 217 173 270 114 152 105 206 181 348 185 11 lag/L Chromium 3.4 NE pg/L Cobalt 5.3 7.2 3 6.8 3.4 14.8 14.4 25.3 NE pg/L Copper 4.4 1000 fag/L Iron 13100 1720 8240 10500 3390 4160 4940 5270 8890 11700 9560 NE lag/L Lead 2.7 NE pg/L Manganese 6310 7340 4750 8350 2310 3860 1420 5080 4320 8930 3990 25 pg/L Nickel 3.9 5.5 3.6 6.8 2.8 2.8 4.8 12 NE pg/L Sodium 27000 35500 24600 38400 14700 20900 18200 29900 29900 41100 25000 NE fag/L Tin 2.8 NE pg/L Vanadium 2.5 5.6 9.7 9.8 NE pg/L Zinc 9.6 13.6 10.8 EPA 601 OD 21000 fag/L Barium 273 122 NE pg/L Cobalt 12.6 1000 pg/L Iron 13000 2500 NE pg/L Manganese 7890 2130 25 pg/L Nickel 6.9 NE pg/L Sodium 34000 16900 NE pg/L Zinc 7.1 EPA 8260 2000 pg/L Acetone 16.2 1.19 pg/L Benzene 0.42 0.54 0.32 0.88 NE pg/L cis-1,2-Dichloroethene 0.26 11000 fag/L Methylene Chloride 1 110000 pg/L Tetrahydrofuran 3.4 6.3 3.3 10.2 9.7 18.9 5.1 EPA 8260B Mod. NE pg/L 1,4-Dioxane (p-Dioxane) 1.3 EPA 8270 NE lag/L 3&4-Methylphenol(m&p Cresol) 3.6 Field Field pH 6.35 6.5 6.5 6.7 6.6 6.5 6.4 6.9 6.6 6.5 6.2 6.3 Field Specific Conductance 1172 376 702 959 549 1006 274.8 364.2 885 649 899 575 Field Temperature 14.9 11 21.5 7.9 21.2 15.6 8.2 17.5 12.5 18.9 15.1 22.4 Oxygen, Dissolved 1.85 6.2 1.34 3 4.3 2.81 3.2 6.9 4.5 2.9 2.5 1.9 REDOX -52.7 -5.9 -33.2 -19 -49.6 -23.6 -90 -15.8 -45 127 -15 -53 Static Water Level Total Well Depth 0 Turbidity 34.5 10.9 45.87 14.79 7.94 13.52 9.1 42.7 16.6 14 57 13 7/15/2019 3 of 5 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Surface water detections of concern within the last 6 years Max of Result Column Labels 2B SM 2320B 20000 pg/L Alkalinity, Total as CaCO3 473000 181000 356000 477000 251000 520000 161000 210000 118000 389000 259000 516000 293000 SM 2540C NE pg/L Total Dissolved Solids 668000 241000 413000 600000 321000 623000 231000 300000 233000 473000 319000 705000 327000 SM 4500-CI-E 230000 pg/L Chloride 28000 12000 22300 33800 18400 34000 10500 16300 27000 27000 16900 34800 20000 SM 4500-CN-E 5 pg/L Cyanide 4.6 6 EPA 8260D 1.19 pg/L Benzene 0.73 110000 pg/L Tetrahydrofuran 6.1 SW-4 EPA 300.0 250000 pg/L Sulfate 17400 27500 24400 26700 18200 28600 16600 24900 23500 17600 23500 23000 13200 EPA 6010 21000 pg/L Barium 138 110 121 128 113 115 187 82.8 126 101 106 11 pg/L Chromium 4.7 NE pg/L Cobalt 5.9 10.4 1000 pg/L Iron 3020 802 1480 1520 1520 2240 9220 638 2520 1790 4180 NE pg/L Manganese 3580 1020 2900 2930 1930 2550 5050 739 2250 1080 1650 25 pg/L Nickel 2.6 2.5 3.6 NE pg/L Sodium 23400 25600 23400 26000 16900 20200 23800 17800 24400 20100 18200 NE pg/L Vanadium 3.5 5.9 NE pg/L Zinc 8.3 7.3 EPA 601 OD 21000 pg/L Barium 382 124 NE pg/L Cobalt 11.6 1000 pg/L Iron 38700 3890 NE pg/L Manganese 7710 1470 25 pg/L Nickel 4.4 NE pg/L Sodium 22000 20000 NE pg/L Vanadium 4.5 NE pg/L Zinc 90.1 6.9 EPA 8260 NE pg/L 2-Hexanone 3.1 2000 pg/L Acetone 16 11000 pg/L Methylene Chloride 1.2 110000 pg/L Tetrahydrofuran 5.7 3.5 3.6 4.1 4.4 NE pg/L TrichIorofluoromethane 0.32 0.27 0.25 Field Field pH 6.87 6.7 7 7.1 7.3 7.2 7 6.5 6.7 6.8 6.8 6.9 Field Specific Conductance 735 374.7 530 509.1 461 549.9 247.9 603 344 478 369 367 Field Temperature 19.3 11.7 22.3 8.1 20.4 17 9 18.2 10 19.3 12.8 23.3 Oxygen, Dissolved 5.35 7.5 7.12 7.5 6 6.33 7.6 3.5 8.18 7 4.3 5.8 REDOX -43.2 -40.1 -42.6 -2.7 -38.5 -72.6 -87.1 -25.5 27 262 61 -31 Static Water Level Total Well Depth 0 Turbidity 30.5 8.4 9.89 3.5 7.13 6.16 3.2 18.6 28.3 33 4 15 SM 2320B 7/15/2019 4 of 5 A4 Facility Permit Qualifier Max of 26-units Row .• 20000 pg/L Alkalinity, Total as CaCO3 SM 2540C NE pg/L Total Dissolved Solids SM 4500-CI-E 230000 pg/L Chloride SM 4500-CN-E 5 pg/L Cyanide EPA 8260D 110000 pg/L Tetrahydrofuran 34-12 Old Salisbury Road Landfill (C&D) (Multiple Items) Surface water detections of concern within the last 6 years 265000 145000 211000 192000 187000 240000 148000 187000 242000 140000 158000 152000 147000 444000 236000 327000 317000 289000 325000 229000 267000 371000 222000 257000 270000 255000 18700 24800 29800 36800 27400 27900 20300 19800 19000 24300 30800 31000 26900 4.1 5.6 13.7 7/15/2019 5 of 5 Winston-Salem City/County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports Appendix Laboratory Winston-Salem City/County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports This page intentionally left blank. aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 03, 2019 Mark Filardi HDR 440 S. Church St Suite 900 Charlotte, NC 28202 RE: Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Dear Mark Filardi: Enclosed are the analytical results for sample(s) received by the laboratory on May 10, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Eden Certification IDs 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 VirginiaNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LF GW SAMPLING 92428830 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92428830001 MW-1R SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270E BPJ 8 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830002 MW-2R SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270E BPJ 8 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830003 MW-3R SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270E BPJ 8 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830004 MW-4R SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270E BPJ 8 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830005 MW-15 SM 2540C-2011 NMH 1 PASI-E REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270E BPJ 8 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830006 SW-2 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270E BPJ 8 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830007 EQUIPMENT BLANK SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270E BPJ 8 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830008 MW-5R SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830009 MW-7 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830010 MW-8 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 NAL 1 PASI-A 92428830011 MW-9 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 NAL 1 PASI-A 92428830012 MW-10 SM 2540C-2011 NMH 1 PASI-E EPA 601OD IDS, SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830013 MW-11 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LF GW SAMPLING 92428830 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92428830014 MW-12 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830015 MW-13 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830016 MW-14 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830017 SW-1 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830018 SW-3 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A 92428830019 SW-4 SM 2540C-2011 NMH 1 PASI-E EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A SM 2320B-2011 ECH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 GC 1 PASI-A SM 4500-CN-E-2011 CJH1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MWAR Lab ID: 92428830001 Collected: 05/08/19 15:16 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 202 mg/L 25.0 1 05/14/19 10:53 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:10 7440-38-2 Barium 285 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:10 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:10 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-50-8 Iron ND ug/L 50.0 1 06/01/19 00:51 06/01/19 12:10 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7439-92-1 Manganese 19.5 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:10 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-22-4 Sodium 15800 ug/L 5000 1 06/01/19 00:51 06/01/19 12:10 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:10 7440-62-2 Zinc 5.2J ug/L 10.0 1 06/01/19 00:51 06/01/19 12:10 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury 1.2 ug/L 0.20 1 05/30/19 09:58 05/30/19 20:02 7439-97-6 M1 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 16:54 56-55-3 Chrysene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 16:54 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 16:54 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 05/13/19 18:17 05/14/19 16:54 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 16:54 193-39-5 Surrogates Nitrobenzene-d5 (S) 77 % 13-130 1 05/13/19 18:17 05/14/19 16:54 4165-60-0 2-Fluorobiphenyl (S) 85 % 13-130 1 05/13/19 18:17 05/14/19 16:54 321-60-8 Terphenyl-d14 (S) 104 % 25-130 1 05/13/19 18:17 05/14/19 16:54 1718-51-0 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 83800 ug/L 5000 1 05/17/19 17:25 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:30 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate ND ug/L 1000 1 05/28/1916:37 14808-79-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MWAR Lab ID: 92428830001 Collected: 05/08/19 15:16 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 9770 ug/L 1000 1 05/13/1919:19 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:10 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-211 Lab ID: 92428830002 Collected: 05/09/19 15:07 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 1150 mg/L 167 1 05/15/19 14:01 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:28 7440-38-2 Barium 260 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:28 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:28 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-47-3 Cobalt 19.8 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-48-4 Copper 9.6 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-50-8 Iron 4690 ug/L 50.0 1 06/01/19 00:51 06/01/19 12:28 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7439-92-1 Manganese 8240 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7439-96-5 Nickel 13.4 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:28 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-22-4 Sodium 57300 ug/L 5000 1 06/01/19 00:51 06/01/19 12:28 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:28 7440-62-2 Zinc 18.0 ug/L 10.0 1 06/01/19 00:51 06/01/19 12:28 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:09 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 17:56 56-55-3 Chrysene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 17:56 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 17:56 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 05/13/19 18:17 05/14/19 17:56 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 17:56 193-39-5 Surrogates Nitrobenzene-d5 (S) 85 % 13-130 1 05/13/19 18:17 05/14/19 17:56 4165-60-0 2-Fluorobiphenyl (S) 88 % 13-130 1 05/13/19 18:17 05/14/19 17:56 321-60-8 Terphenyl-d14 (S) 90 % 25-130 1 05/13/19 18:17 05/14/19 17:56 1718-51-0 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 577000 ug/L 5000 1 05/17/19 20:23 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:49 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 85100 ug/L 1000 1 05/28/1917:20 14808-79-8 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. oil Page 10 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-211 Lab ID: 92428830002 Collected: 05/09/19 15:07 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 06/03/2019 07:05 AM Analytical Method: SM 4500-CI-E-2011 42300 ug/L 2000 2 05/13/1919:56 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 05/18/1912:00 05/19/1912:22 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-311 Lab ID: 92428830003 Collected: 05/09/19 12:54 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 1040 mg/L 167 1 05/15/19 14:00 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:31 7440-38-2 Barium 320 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:31 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:31 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-47-3 Cobalt 16.1 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-50-8 Iron 91800 ug/L 50.0 1 06/01/19 00:51 06/01/19 12:31 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7439-92-1 Manganese 6850 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:31 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-22-4 Sodium 2540J ug/L 5000 1 06/01/19 00:51 06/01/19 12:31 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:31 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:31 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:16 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 18:58 56-55-3 Chrysene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 18:58 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 18:58 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 05/13/19 18:17 05/14/19 18:58 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 18:58 193-39-5 Surrogates Nitrobenzene-d5 (S) 83 % 13-130 1 05/13/19 18:17 05/14/19 18:58 4165-60-0 2-Fluorobiphenyl (S) 88 % 13-130 1 05/13/19 18:17 05/14/19 18:58 321-60-8 Terphenyl-d14 (S) 84 % 25-130 1 05/13/19 18:17 05/14/19 18:58 1718-51-0 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 488000 ug/L 5000 1 05/20/19 14:41 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:49 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 1210 ug/L 1000 1 05/28/1917:35 14808-79-8 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-311 Lab ID: 92428830003 Collected: 05/09/19 12:54 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 06/03/2019 07:05 AM Analytical Method: SM 4500-CI-E-2011 44600 ug/L 2000 2 05/13/1919:57 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 05/18/1912:00 05/19/1912:23 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-411 Lab ID: 92428830004 Collected: 05/09/19 09:37 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 167 mg/L 25.0 1 05/15/19 14:00 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:34 7440-38-2 Barium 216 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:34 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:34 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-47-3 Cobalt 103 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-50-8 Iron 476 ug/L 50.0 1 06/01/19 00:51 06/01/19 12:34 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7439-92-1 Manganese 1130 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7439-96-5 Nickel 8.4 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:34 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-22-4 Sodium 71200 ug/L 5000 1 06/01/19 00:51 06/01/19 12:34 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:34 7440-62-2 Zinc 5.91 ug/L 10.0 1 06/01/19 00:51 06/01/19 12:34 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:18 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:29 56-55-3 Chrysene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:29 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:29 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 05/13/19 18:17 05/14/19 19:29 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:29 193-39-5 Surrogates Nitrobenzene-d5 (S) 75 % 13-130 1 05/13/19 18:17 05/14/19 19:29 4165-60-0 2-Fluorobiphenyl (S) 79 % 13-130 1 05/13/19 18:17 05/14/19 19:29 321-60-8 Terphenyl-d14 (S) 85 % 25-130 1 05/13/19 18:17 05/14/19 19:29 1718-51-0 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 129000 ug/L 5000 1 05/20/19 15:15 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:50 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 163000 ug/L 4000 4 05/28/19 23:09 14808-79-8 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 811 Page 14 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-411 Lab ID: 92428830004 Collected: 05/09/19 09:37 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 06/03/2019 07:05 AM Analytical Method: SM 4500-CI-E-2011 2220 ug/L 1000 1 05/13/1919:22 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 05/18/1912:00 05/19/1912:26 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-15 Lab ID: 92428830005 Collected: 05/10/19 08:35 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 448 mg/L 100 1 05/15/19 13:59 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:37 7440-38-2 Barium 29.8 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:37 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:37 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-50-8 Iron 374 ug/L 50.0 1 06/01/19 00:51 06/01/19 12:37 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7439-92-1 Manganese 110 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:37 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-22-4 Sodium 23000 ug/L 5000 1 06/01/19 00:51 06/01/19 12:37 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:37 7440-62-2 Zinc 5.11 ug/L 10.0 1 06/01/19 00:51 06/01/19 12:37 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:20 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:59 56-55-3 Chrysene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:59 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:59 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 05/13/19 18:17 05/14/19 19:59 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 19:59 193-39-5 Surrogates Nitrobenzene-d5 (S) 76 % 13-130 1 05/13/19 18:17 05/14/19 19:59 4165-60-0 2-Fluorobiphenyl (S) 80 % 13-130 1 05/13/19 18:17 05/14/19 19:59 321-60-8 Terphenyl-d14 (S) 98 % 25-130 1 05/13/19 18:17 05/14/19 19:59 1718-51-0 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 74200 ug/L 5000 1 05/20/19 15:42 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 23:02 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 45900 ug/L 1000 1 05/28/1918:03 14808-79-8 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-15 Lab ID: 92428830005 Collected: 05/10/19 08:35 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 06/03/2019 07:05 AM Analytical Method: SM 4500-CI-E-2011 115000 ug/L 10000 10 05/13/1919:23 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 05/18/1912:00 05/19/1912:30 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: SW-2 Lab ID: 92428830006 Collected: 05/10/19 09:45 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 182 mg/L 25.0 1 05/15/19 13:59 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:40 7440-38-2 Barium 85.6 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:40 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:40 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-50-8 Iron 4370 ug/L 50.0 1 06/01/19 00:51 06/01/19 12:40 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7439-92-1 Manganese 680 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:40 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-22-4 Sodium 12300 ug/L 5000 1 06/01/19 00:51 06/01/19 12:40 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:40 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:40 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:23 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 20:30 56-55-3 Chrysene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 20:30 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 20:30 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 05/13/19 18:17 05/14/19 20:30 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 20:30 193-39-5 Surrogates Nitrobenzene-d5 (S) 71 % 13-130 1 05/13/19 18:17 05/14/19 20:30 4165-60-0 2-Fluorobiphenyl (S) 77 % 13-130 1 05/13/19 18:17 05/14/19 20:30 321-60-8 Terphenyl-d14 (S) 88 % 25-130 1 05/13/19 18:17 05/14/19 20:30 1718-51-0 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 54900 ug/L 5000 1 05/20/19 15:52 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 23:02 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 13500 ug/L 1000 1 05/28/1918:18 14808-79-8 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: SW-2 Lab ID: 92428830006 Collected: 05/10/19 09:45 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 06/03/2019 07:05 AM Analytical Method: SM 4500-CI-E-2011 19400 ug/L 1000 1 05/13/1919:24 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 05/18/1912:00 05/19/1912:31 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 19 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: EQUIPMENT BLANK Lab ID: 92428830007 Collected: 05/10/19 10:35 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 30.0 mg/L 25.0 1 05/15/19 13:58 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:43 7440-38-2 Barium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:43 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:43 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-50-8 Iron ND ug/L 50.0 1 06/01/19 00:51 06/01/19 12:43 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7439-92-1 Manganese ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:43 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-22-4 Sodium ND ug/L 5000 1 06/01/19 00:51 06/01/19 12:43 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:43 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:43 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:25 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 21:00 56-55-3 Chrysene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 21:00 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 21:00 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 05/13/19 18:17 05/14/19 21:00 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 05/13/19 18:17 05/14/19 21:00 193-39-5 Surrogates Nitrobenzene-d5 (S) 78 % 13-130 1 05/13/19 18:17 05/14/19 21:00 4165-60-0 2-Fluorobiphenyl (S) 89 % 13-130 1 05/13/19 18:17 05/14/19 21:00 321-60-8 Terphenyl-d14 (S) 119 % 25-130 1 05/13/19 18:17 05/14/19 21:00 1718-51-0 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 ND ug/L 5000 1 05/20/19 15:59 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 23:03 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate ND ug/L 1000 1 05/28/1919:02 14808-79-8 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: EQUIPMENT BLANK Lab ID: 92428830007 Collected: 05/10/19 10:35 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 06/03/2019 07:05 AM Analytical Method: SM 4500-CI-E-2011 ND ug/L 1000 1 05/13/1919:27 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 05/18/1912:00 05/19/1912:32 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-511 Lab ID: 92428830008 Collected: 05/09/19 08:26 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 175 mg/L 25.0 1 05/15/19 14:00 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:46 7440-38-2 Barium 55.8 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:46 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:46 7440-43-9 Chromium 5.4 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-50-8 Iron 63.5 ug/L 50.0 1 06/01/19 00:51 06/01/19 12:46 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7439-92-1 Manganese ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:46 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-22-4 Sodium 13000 ug/L 5000 1 06/01/19 00:51 06/01/19 12:46 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-31-5 Vanadium 4.3J ug/L 5.0 1 06/01/19 00:51 06/01/19 12:46 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:46 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:28 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 29200 ug/L 5000 1 05/20/19 16:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 22:57 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 8620 ug/L 1000 1 05/28/1919:16 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 15600 ug/L 1000 1 05/13/1919:28 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide 7.2J ug/L 8.0 1 05/18/1912:00 05/19/1912:33 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 22 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-7 Lab ID: 92428830009 Collected: 05/09/19 10:46 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 192 mg/L 25.0 1 05/15/19 14:00 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:49 7440-38-2 Barium 168 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-39-3 Beryllium 0.61J ug/L 1.0 1 06/01/19 00:51 06/01/19 12:49 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:49 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-50-8 Iron ND ug/L 50.0 1 06/01/19 00:51 06/01/19 12:49 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7439-92-1 Manganese 57.7 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:49 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-22-4 Sodium 17500 ug/L 5000 1 06/01/19 00:51 06/01/19 12:49 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:49 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:49 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:30 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 54200 ug/L 5000 1 05/20/19 16:08 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 22:59 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 12800 ug/L 1000 1 05/28/1919:31 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 6470 ug/L 1000 1 05/13/1919:30 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:34 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-8 Lab ID: 92428830010 Collected: 05/07/19 13:50 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 170 mg/L 25.0 1 05/13/19 14:02 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:52 7440-38-2 Barium 47.8 ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:52 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 12:52 7440-43-9 Chromium 3.5J ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-50-8 Iron ND ug/L 50.0 1 06/01/19 00:51 06/01/19 12:52 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7439-92-1 Manganese 3.3J ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:52 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-22-4 Sodium 9620 ug/L 5000 1 06/01/19 00:51 06/01/19 12:52 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 12:52 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 12:52 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:32 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 26600 ug/L 5000 1 05/16/19 17:16 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:21 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 6560 ug/L 1000 1 05/28/1919:45 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 4290 ug/L 1000 1 05/13/1919:33 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/15/1914:26 05/16/1911:36 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. oil Page 24 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-9 Lab ID: 92428830011 Collected: 05/07/19 14:45 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 190 mg/L 25.0 1 05/13/19 14:01 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:01 7440-38-2 Barium 217 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:01 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:01 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-50-8 Iron 148 ug/L 50.0 1 06/01/19 00:51 06/01/19 13:01 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7439-92-1 Manganese 7.1 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:01 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-22-4 Sodium 14100 ug/L 5000 1 06/01/19 00:51 06/01/19 13:01 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:01 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:01 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:35 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 29700 ug/L 5000 1 05/16/19 17:21 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:21 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate ND ug/L 1000 1 05/28/19 20:00 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 6830 ug/L 1000 1 05/13/1919:34 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/15/1914:26 05/16/1911:37 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. oil Page 25 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-10 Lab ID: 92428830012 Collected: 05/08/19 10:04 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 1110 mg/L 25.0 1 05/14/19 10:52 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:04 7440-38-2 Barium 65.6 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:04 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:04 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-47-3 Cobalt 15.1 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-50-8 Iron 2320 ug/L 50.0 1 06/01/19 00:51 06/01/19 13:04 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7439-92-1 Manganese 20500 ug/L 25.0 5 06/01/19 00:51 06/01/19 16:03 7439-96-5 Nickel 7.2 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:04 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-22-4 Sodium 136000 ug/L 25000 5 06/01/19 00:51 06/01/19 16:03 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:04 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:04 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:37 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 506000 ug/L 5000 1 05/17/19 17:36 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide 347 ug/L 100 1 05/14/19 00:30 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 235000 ug/L 5000 5 05/28/19 23:24 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 65100 ug/L 10000 10 05/13/1919:35 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:11 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 26 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-11 Lab ID: 92428830013 Collected: 05/08/19 11:10 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 236 mg/L 33.3 1 05/15/19 10:38 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:07 7440-38-2 Barium 100 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:07 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:07 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-47-3 Cobalt 4.8J ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-50-8 Iron 27500 ug/L 50.0 1 06/01/19 00:51 06/01/19 13:07 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7439-92-1 Manganese 1740 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:07 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-22-4 Sodium 12800 ug/L 5000 1 06/01/19 00:51 06/01/19 13:07 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:07 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:07 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:44 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 154000 ug/L 5000 1 05/17/19 17:45 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide 56.8J ug/L 100 1 05/14/19 00:31 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 22300 ug/L 1000 1 05/28/19 20:58 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 12300 ug/L 1000 1 05/13/1919:38 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:12 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. D6,H1 Page 27 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-12 Lab ID: 92428830014 Collected: 05/08/19 12:35 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 1710 mg/L 100 1 05/15/19 10:37 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:10 7440-38-2 Barium 200 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:10 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:10 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-47-3 Cobalt 5.5 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-50-8 Iron 1990 ug/L 50.0 1 06/01/19 00:51 06/01/19 13:10 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7439-92-1 Manganese 2260 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7439-96-5 Nickel 6.2 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:10 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-22-4 Sodium 20700 ug/L 5000 1 06/01/19 00:51 06/01/19 13:10 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:10 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:10 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:47 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 176000 ug/L 5000 1 05/17/19 17:58 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:31 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 149000 ug/L 3000 3 05/28/19 23:39 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 34000 ug/L 1000 1 05/13/1919:39 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:14 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. oil Page 28 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-13 Lab ID: 92428830015 Collected: 05/08/19 14:04 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 115 mg/L 25.0 1 05/15/19 10:37 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:13 7440-38-2 Barium 138 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-39-3 Beryllium 0.60J ug/L 1.0 1 06/01/19 00:51 06/01/19 13:13 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:13 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-50-8 Iron 42.3J ug/L 50.0 1 06/01/19 00:51 06/01/19 13:13 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7439-92-1 Manganese 5.2 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:13 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-22-4 Sodium 9940 ug/L 5000 1 06/01/19 00:51 06/01/19 13:13 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:13 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:13 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:49 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 52800 ug/L 5000 1 05/17/19 18:12 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:32 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 5910 ug/L 1000 1 05/28/19 21:56 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 6290 ug/L 1000 1 05/13/1919:40 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:15 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: MW-14 Lab ID: 92428830016 Collected: 05/08/19 08:36 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 163 mg/L 25.0 1 05/15/19 10:36 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:16 7440-38-2 Barium 234 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-39-3 Beryllium 0.61J ug/L 1.0 1 06/01/19 00:51 06/01/19 13:16 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:16 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-50-8 Iron 36.2J ug/L 50.0 1 06/01/19 00:51 06/01/19 13:16 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7439-92-1 Manganese 38.3 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7439-96-5 Nickel 4AJ ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:16 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-22-4 Sodium 17400 ug/L 5000 1 06/01/19 00:51 06/01/19 13:16 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:16 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:16 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:51 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 64900 ug/L 5000 1 05/17/19 18:20 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/14/19 00:32 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate ND ug/L 1000 1 05/28/19 22:10 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 3870 ug/L 1000 1 05/13/1919:41 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:16 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: SW-1 Lab ID: 92428830017 Collected: 05/10/19 10:05 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 174 mg/L 25.0 1 05/15/19 13:57 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:19 7440-38-2 Barium 109 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:19 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:19 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-47-3 Cobalt ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-50-8 Iron 889 ug/L 50.0 1 06/01/19 00:51 06/01/19 13:19 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7439-92-1 Manganese 48.5 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7439-96-5 Nickel ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:19 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-22-4 Sodium 19400 ug/L 5000 1 06/01/19 00:51 06/01/19 13:19 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:19 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:19 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:54 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 22300 ug/L 5000 1 05/20/19 16:34 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 23:04 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 7970 ug/L 1000 1 05/28/19 22:25 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 55400 ug/L 5000 5 05/13/19 20:00 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:35 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: SW-3 Lab ID: 92428830018 Collected: 05/10/19 09:10 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 668 mg/L 100 1 05/15/19 13:57 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:22 7440-38-2 Barium 273 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:22 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:22 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-47-3 Cobalt 12.6 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-50-8 Iron 13000 ug/L 50.0 1 06/01/19 00:51 06/01/19 13:22 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7439-92-1 Manganese 7890 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7439-96-5 Nickel 6.9 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:22 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-22-4 Sodium 34000 ug/L 5000 1 06/01/19 00:51 06/01/19 13:22 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-31-5 Vanadium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:22 7440-62-2 Zinc ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:22 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:56 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 473000 ug/L 5000 1 05/20/19 16:39 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 23:04 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 43600 ug/L 1000 1 05/28/19 22:39 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 28000 ug/L 1000 1 05/13/1919:42 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:36 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Sample: SW-4 Lab ID: 92428830019 Collected: 05/10/19 09:25 Received: 05/10/19 12:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 444 mg/L 100 1 05/15/19 13:57 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-36-0 Arsenic ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:25 7440-38-2 Barium 382 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-39-3 Beryllium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:25 7440-41-7 Cadmium ND ug/L 1.0 1 06/01/19 00:51 06/01/19 13:25 7440-43-9 Chromium ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-47-3 Cobalt 11.6 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-48-4 Copper ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-50-8 Iron 38700 ug/L 50.0 1 06/01/19 00:51 06/01/19 13:25 7439-89-6 Lead ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7439-92-1 Manganese 7710 ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7439-96-5 Nickel 4AJ ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-02-0 Selenium ND ug/L 10.0 1 06/01/19 00:51 06/01/19 13:25 7782-49-2 Silver ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-22-4 Sodium 22000 ug/L 5000 1 06/01/19 00:51 06/01/19 13:25 7440-23-5 Tin ND ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-31-5 Vanadium 4.5J ug/L 5.0 1 06/01/19 00:51 06/01/19 13:25 7440-62-2 Zinc 90.1 ug/L 10.0 1 06/01/19 00:51 06/01/19 13:25 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 05/30/19 09:58 05/30/19 20:58 7439-97-6 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 265000 ug/L 5000 1 05/22/19 12:11 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 05/15/19 23:05 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 17400 ug/L 1000 1 05/28/19 22:54 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 18700 ug/L 1000 1 05/13/1919:43 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 05/18/1912:00 05/19/1912:36 57-12-5 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 33 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 474933 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92428830010, 92428830011 METHOD BLANK: 2574556 Matrix: Water Associated Lab Samples: 92428830010, 92428830011 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 05/13/19 13:53 LABORATORY CONTROL SAMPLE: 2574557 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 234 94 90-110 SAMPLE DUPLICATE: 2574558 92428830010 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 170 80.0 72 D6 SAMPLE DUPLICATE: 2574559 92428830011 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 190 136 33 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 34 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475125 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92428830001, 92428830012 METHOD BLANK: 2575233 Matrix: Water Associated Lab Samples: 92428830001, 92428830012 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 05/14/19 10:48 LABORATORY CONTROL SAMPLE: 2575234 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 274 110 90-110 SAMPLE DUPLICATE: 2575235 92428041067 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 268 310 15 D6 SAMPLE DUPLICATE: 2575236 92428041068 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 194 400 69 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 35 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475393 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92428830013, 92428830014, 92428830015, 92428830016 METHOD BLANK: 2576464 Matrix: Water Associated Lab Samples: 92428830013, 92428830014, 92428830015, 92428830016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 05/15/19 10:38 LABORATORY CONTROL SAMPLE: 2576465 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 228 91 90-110 SAMPLE DUPLICATE: 2576466 92428830013 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 236 215 9 D6,H1 SAMPLE DUPLICATE: 2576467 92428830014 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 1710 568 100 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 36 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475439 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008, 92428830009,92428830017,92428830018,92428830019 METHOD BLANK: 2576682 Matrix: Water Associated Lab Samples: 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008, 92428830009,92428830017,92428830018,92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 05/15/19 14:02 LABORATORY CONTROL SAMPLE: 2576683 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 264 106 90-110 SAMPLE DUPLICATE: 2576684 92428041090 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 237 295 22 D6 SAMPLE DUPLICATE: 2576685 92428830002 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 1150 807 35 D6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 478119 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008,92428830009,92428830010,92428830011,92428830012,92428830013,92428830014, 92428830015,92428830016,92428830017,92428830018,92428830019 METHOD BLANK: 2588417 Matrix: Water Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008,92428830009,92428830010,92428830011,92428830012,92428830013,92428830014, 92428830015,92428830016,92428830017,92428830018,92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 05/30/1919:57 LABORATORY CONTROL SAMPLE: 2588418 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.4 95 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2588419 2588420 MS MSD 92428830001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L 1.2 2.5 2.5 3.3 3.0 85 71 75-125 11 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 477758 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008,92428830009,92428830010,92428830011,92428830012,92428830013,92428830014, 92428830015,92428830016,92428830017,92428830018,92428830019 METHOD BLANK: 2586880 Matrix: Water Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008,92428830009,92428830010,92428830011,92428830012,92428830013,92428830014, 92428830015,92428830016,92428830017,92428830018,92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Antimony ug/L ND 5.0 06/01/1912:04 Arsenic ug/L ND 10.0 06/01/1912:04 Barium ug/L ND 5.0 06/01/1912:04 Beryllium ug/L ND 1.0 06/01/1912:04 Cadmium ug/L ND 1.0 06/01/1912:04 Chromium ug/L ND 5.0 06/01/1912:04 Cobalt ug/L ND 5.0 06/01/1912:04 Copper ug/L ND 5.0 06/01/1912:04 Iron ug/L ND 50.0 06/01/1912:04 Lead ug/L ND 5.0 06/01/1912:04 Manganese ug/L ND 5.0 06/01/1912:04 Nickel ug/L ND 5.0 06/01/1912:04 Selenium ug/L ND 10.0 06/01/1912:04 Silver ug/L ND 5.0 06/01/1912:04 Sodium ug/L ND 5000 06/01/1912:04 Tin ug/L ND 5.0 06/01/1912:04 Vanadium ug/L ND 5.0 06/01/1912:04 Zinc ug/L ND 10.0 06/01/1912:04 LABORATORY CONTROL SAMPLE: Parameter 2586881 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 500 503 101 80-120 Arsenic ug/L 500 472 94 80-120 Barium ug/L 500 504 101 80-120 Beryllium ug/L 500 499 100 80-120 Cadmium ug/L 500 500 100 80-120 Chromium ug/L 500 504 101 80-120 Cobalt ug/L 500 497 99 80-120 Copper ug/L 500 511 102 80-120 Iron ug/L 5000 5050 101 80-120 Lead ug/L 500 495 99 80-120 Manganese ug/L 500 500 100 80-120 Nickel ug/L 500 494 99 80-120 Selenium ug/L 500 498 100 80-120 Silver ug/L 250 257 103 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 LABORATORY CONTROL SAMPLE: 2586881 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Sodium ug/L 5000 5040 101 80-120 Tin ug/L 500 507 101 80-120 Vanadium ug/L 500 503 101 80-120 Zinc ug/L 500 496 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2586882 MS 92428830001 Spike Parameter Units Result Conc. Antimony ug/L ND 500 Arsenic ug/L ND 500 Barium ug/L 285 500 Beryllium ug/L ND 500 Cadmium ug/L ND 500 Chromium ug/L ND 500 Cobalt ug/L ND 500 Copper ug/L ND 500 Iron ug/L ND 5000 Lead ug/L ND 500 Manganese ug/L 19.5 500 Nickel ug/L ND 500 Selenium ug/L ND 500 Silver ug/L ND 250 Sodium ug/L 15800 5000 Tin ug/L ND 500 Vanadium ug/L ND 500 Zinc ug/L 5.2J 500 Qualifiers 2586883 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 500 505 100 101 75-125 1 500 494 498 99 99 75-125 1 500 805 808 104 105 75-125 0 500 519 528 104 106 75-125 2 500 508 512 102 102 75-125 1 500 511 515 102 103 75-125 1 500 499 504 100 101 75-125 1 500 518 523 104 105 75-125 1 5000 5170 5210 103 104 75-125 1 500 496 501 99 100 75-125 1 500 523 527 101 101 75-125 1 500 493 499 98 100 75-125 1 500 546 552 109 110 75-125 1 250 253 255 101 102 75-125 1 5000 21600 21500 117 114 75-125 1 500 508 514 101 102 75-125 1 500 513 518 102 103 75-125 1 500 509 516 101 102 75-125 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Qual Page 40 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 474895 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007 METHOD BLANK: 2574362 Matrix: Water Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 05/14/19 15:52 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 05/14/19 15:52 Chrysene ug/L ND 10.0 05/14/19 15:52 Dibenz(a,h)anthracene ug/L ND 10.0 05/14/19 15:52 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 05/14/19 15:52 2-Fluorobiphenyl (S) % 84 13-130 05/14/19 15:52 Nitrobenzene-d5 (S) % 72 13-130 05/14/19 15:52 Terphenyl-d14 (S) % 102 25-130 05/14/19 15:52 LABORATORY CONTROL SAMPLE: 2574363 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 54.4 109 50-130 bis(2-Ethylhexyl)phthalate ug/L 50 55.0 110 50-130 Chrysene ug/L 50 54.4 109 50-130 Dibenz(a,h)anthracene ug/L 50 54.9 110 40-130 Indeno(1,2,3-cd)pyrene ug/L 50 55.6 111 40-130 2-Fluorobiphenyl (S) % 91 13-130 Nitrobenzene-d5 (S) % 87 13-130 Terphenyl-d14 (S) % 104 25-130 MATRIX SPIKE SAMPLE: Parameter 2574364 Units 92428830001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Benzo(a)anthracene ug/L ND 50 52.8 106 50-130 bis(2-Ethylhexyl)phthalate ug/L ND 50 54.6 107 50-130 Chrysene ug/L ND 50 52.8 106 50-130 Dibenz(a,h)anthracene ug/L ND 50 53.3 107 40-130 Indeno(1,2,3-cd)pyrene ug/L ND 50 54.5 109 40-130 2-Fluorobiphenyl (S) % 79 13-130 Nitrobenzene-d5 (S) % 77 13-130 Terphenyl-d14 (S) % 96 25-130 SAMPLE DUPLICATE: 2574365 92428830002 Dup Parameter Units Result Result RPD Qualifiers Benzo(a)anthracene ug/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 41 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 SAMPLE DUPLICATE: 2574365 Parameter Units 92428830002 Result Dup Result RPD Qualifiers bis(2-Ethylhexyl)phthalate ug/L ND ND Chrysene ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Indeno(1,2,3-cd)pyrene ug/L ND ND 2-Fluorobiphenyl (S) % 88 85 Nitrobenzene-d5 (S) % 85 80 Terphenyl-d14 (S) % 90 71 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 42 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475680 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Associated Lab Samples: 92428830010, 92428830011 METHOD BLANK: 2577867 Matrix: Water Associated Lab Samples: 92428830010, 92428830011 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 05/16/19 16:18 LABORATORY CONTROL SAMPLE: 2577868 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 49300 99 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2577869 2577870 MS MSD 92428041048 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 261 50000 50000 296000 301000 70 81 80-120 2 M1 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2577871 2577872 MS MSD 92428642004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 13300 50000 50000 64800 64900 103 103 80-120 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 43 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475950 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830012, 92428830013, 92428830014, 92428830015, 92428830016 METHOD BLANK: 2578864 Matrix: Water Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830012, 92428830013, 92428830014, 92428830015, 92428830016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 05/17/19 16:49 LABORATORY CONTROL SAMPLE: 2578865 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 51500 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2578866 2578867 MS MSD 92428041072 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 7.8 50000 50000 62300 62300 109 109 80-120 0 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2578868 2578869 MS MSD 92429191003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 26.5 50000 50000 77600 77700 102 103 80-120 0 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 476289 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Associated Lab Samples: 92428830004, 92428830005, 92428830006, 92428830007, 92428830008, 92428830009, 92428830017, 92428830018,92428830019 METHOD BLANK: 2580319 Matrix: Water Associated Lab Samples: 92428830004, 92428830005, 92428830006, 92428830007, 92428830008, 92428830009, 92428830017, 92428830018,92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 05/20/19 15:01 LABORATORY CONTROL SAMPLE: 2580320 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 49200 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2580321 2580322 MS MSD 92428830004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 129000 50000 50000 163000 156000 68 56 80-120 4 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2580323 2580324 MS MSD 92428041075 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 58.6 50000 50000 109000 109000 101 101 80-120 0 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475036 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92428830010, 92428830011 METHOD BLANK: 2574888 Matrix: Water Associated Lab Samples: 92428830010, 92428830011 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 100 05/14/19 00:11 LABORATORY CONTROL SAMPLE: 2574889 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 536 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574890 2574891 MS MSD 92428245006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 516 524 103 105 80-120 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574892 2574893 MS MSD 92428413003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 535 542 107 108 80-120 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475037 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92428830001,92428830002,92428830003,92428830004,92428830012,92428830013,92428830014, 92428830015,92428830016 METHOD BLANK: 2574894 Matrix: Water Associated Lab Samples: 92428830001,92428830002,92428830003,92428830004,92428830012,92428830013,92428830014, 92428830015,92428830016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 100 05/14/19 00:26 LABORATORY CONTROL SAMPLE: 2574895 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 526 105 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574896 2574897 MS MSD 92428715001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 330 332 66 66 80-120 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574898 2574899 MS MSD 92428698001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L 0.67 500 500 1060 1020 79 69 80-120 4 M1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475554 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92428830005, 92428830006, 92428830007, 92428830008, 92428830009, 92428830017, 92428830018, 92428830019 METHOD BLANK: 2577476 Matrix: Water Associated Lab Samples: 92428830005, 92428830006, 92428830007, 92428830008, 92428830009, 92428830017, 92428830018, 92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 100 05/15/19 22:54 LABORATORY CONTROL SAMPLE: 2577477 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 522 104 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2577478 2577479 MS MSD 92428830008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 527 520 105 104 80-120 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2577480 2577481 MS MSD 92428830007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 566 564 113 113 80-120 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 48 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 477718 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008,92428830009,92428830010,92428830011,92428830012,92428830013,92428830014, 92428830015,92428830016,92428830017,92428830018,92428830019 METHOD BLANK: 2586751 Matrix: Water Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008,92428830009,92428830010,92428830011,92428830012,92428830013,92428830014, 92428830015,92428830016,92428830017,92428830018,92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 1000 05/28/1916:07 LABORATORY CONTROL SAMPLE: 2586752 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 48800 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2586753 2586754 MS MSD 92428830001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate ug/L ND 50000 50000 50200 50800 100 101 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2586755 2586756 MS MSD 92428830011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate ug/L ND 50000 50000 52500 51700 104 103 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 474983 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008 METHOD BLANK: 2574683 Matrix: Water Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830004, 92428830005, 92428830006, 92428830007, 92428830008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 05/13/1918:59 LABORATORY CONTROL SAMPLE: 2574684 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20200 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574685 2574686 MS MSD 92428642003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 2340 10000 10000 12300 12200 100 99 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574687 2574688 MS MSD 92428734006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 730J 10000 10000 10700 10600 100 99 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 474986 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Associated Lab Samples: 92428830009,92428830010,92428830011,92428830012,92428830013,92428830014,92428830015, 92428830016,92428830017,92428830018,92428830019 METHOD BLANK: 2574689 Matrix: Water Associated Lab Samples: 92428830009,92428830010,92428830011,92428830012,92428830013,92428830014,92428830015, 92428830016,92428830017,92428830018,92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 05/13/1919:29 LABORATORY CONTROL SAMPLE: 2574690 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20400 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574691 2574692 MS MSD 92428830009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 6470 10000 10000 16100 16100 96 96 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2574693 2574694 MS MSD 92428830019 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 18700 10000 10000 28400 28700 97 100 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 475355 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92428830010, 92428830011 METHOD BLANK: 2576299 Matrix: Water Associated Lab Samples: 92428830010, 92428830011 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 8.0 05/16/1911:10 LABORATORY CONTROL SAMPLE: 2576300 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 102 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2576301 2576302 MS MSD 92428151004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L ND 100 100 84.9 88.5 84 88 80-120 4 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2576303 2576304 MS MSD 92428587001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L 0.088 100 100 151 154 63 66 80-120 2 M1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 52 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 476151 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830012, 92428830013, 92428830014, 92428830015, 92428830016 METHOD BLANK: 2579914 Matrix: Water Associated Lab Samples: 92428830001, 92428830002, 92428830003, 92428830012, 92428830013, 92428830014, 92428830015, 92428830016 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 8.0 05/19/1911:58 LABORATORY CONTROL SAMPLE: 2579915 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 101 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2579916 2579917 MS MSD 92428952001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L ND 100 100 106 105 102 101 80-120 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2579918 2579919 MS MSD 92428830013 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L ND 100 100 99.2 95.7 96 92 80-120 4 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 53 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LF GW SAMPLING Pace Project No.: 92428830 QC Batch: 476152 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92428830004, 92428830005, 92428830006, 92428830007, 92428830008, 92428830009, 92428830017, 92428830018,92428830019 METHOD BLANK: 2579920 Matrix: Water Associated Lab Samples: 92428830004, 92428830005, 92428830006, 92428830007, 92428830008, 92428830009, 92428830017, 92428830018,92428830019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 8.0 05/19/1912:24 LABORATORY CONTROL SAMPLE: 2579921 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 105 105 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2579922 2579923 MS MSD 92428830004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L ND 100 100 94.6 99.5 89 94 80-120 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2579924 2579925 MS MSD 92429365002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L ND 100 100 106 101 106 100 80-120 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: OSR LF GW SAMPLING Pace Project No.: 92428830 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-E Pace Analytical Services - Eden ANALYTE QUALIFIERS D6 The precision between the sample and sample duplicate exceeded laboratory control limits. H1 Analysis conducted outside the EPA method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 55 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LF GW SAMPLING 92428830 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92428830001 MWA R SM 2540C-2011 475125 92428830002 MW-2R SM 254OC-2011 475439 92428830003 MW-3R SM 254OC-2011 475439 92428830004 MW-4R SM 254OC-2011 475439 92428830005 MW-15 SM 254OC-2011 475439 92428830006 SW-2 SM 254OC-2011 475439 92428830007 EQUIPMENT BLANK SM 254OC-2011 475439 92428830008 MW-5R SM 254OC-2011 475439 92428830009 MW-7 SM 254OC-2011 475439 92428830010 MW-8 SM 2540C-2011 474933 92428830011 MW-9 SM 2540C-2011 474933 92428830012 MW-10 SM 254OC-2011 475125 92428830013 MW-11 SM 2540C-2011 475393 92428830014 MW-12 SM 2540C-2011 475393 92428830015 MW-13 SM 2540C-2011 475393 92428830016 MW-14 SM 2540C-2011 475393 92428830017 SW-1 SM 254OC-2011 475439 92428830018 SW-3 SM 254OC-2011 475439 92428830019 SW-4 SM 254OC-2011 475439 92428830001 MWA R EPA 3010A 477758 EPA 6010D 478566 92428830002 MW-211 EPA 3010A 477758 EPA 6010D 478566 92428830003 MW-311 EPA 3010A 477758 EPA 6010D 478566 92428830004 MW-411 EPA 3010A 477758 EPA 6010D 478566 92428830005 MW-15 EPA 3010A 477758 EPA 6010D 478566 92428830006 SW-2 EPA 3010A 477758 EPA 6010D 478566 92428830007 EQUIPMENT BLANK EPA 3010A 477758 EPA6010D 478566 92428830008 MW-511 EPA 3010A 477758 EPA 6010D 478566 92428830009 MW-7 EPA 3010A 477758 EPA 6010D 478566 92428830010 MW-8 EPA 3010A 477758 EPA 6010D 478566 92428830011 MW-9 EPA 3010A 477758 EPA 6010D 478566 92428830012 MW-10 EPA 3010A 477758 EPA 6010D 478566 92428830013 MW-11 EPA 3010A 477758 EPA 6010D 478566 92428830014 MW-12 EPA 3010A 477758 EPA 6010D 478566 92428830015 MW-13 EPA 3010A 477758 EPA 6010D 478566 92428830016 MW-14 EPA 3010A 477758 EPA 6010D 478566 92428830017 SW-1 EPA 3010A 477758 EPA 6010D 478566 92428830018 SW-3 EPA 3010A 477758 EPA 6010D 478566 92428830019 SW-4 EPA 3010A 477758 EPA 6010D 478566 92428830001 MWA R EPA 7470A 478119 EPA 7470A 478159 92428830002 MW-2R EPA 7470A 478119 EPA 7470A 478159 92428830003 MW-3R EPA 7470A 478119 EPA 7470A 478159 92428830004 MW-4R EPA 7470A 478119 EPA 7470A 478159 92428830005 MW-15 EPA 7470A 478119 EPA 7470A 478159 92428830006 SW-2 EPA 7470A 478119 EPA 7470A 478159 92428830007 EQUIPMENT BLANK EPA 7470A 478119 EPA 7470A 478159 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 56 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LF GW SAMPLING 92428830 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92428830008 MW-511 EPA 7470A 478119 EPA 7470A 478159 92428830009 MW-7 EPA 7470A 478119 EPA 7470A 478159 92428830010 MW-8 EPA 7470A 478119 EPA 7470A 478159 92428830011 MW-9 EPA 7470A 478119 EPA 7470A 478159 92428830012 MW-10 EPA 7470A 478119 EPA 7470A 478159 92428830013 MW-11 EPA 7470A 478119 EPA 7470A 478159 92428830014 MW-12 EPA 7470A 478119 EPA 7470A 478159 92428830015 MW-13 EPA 7470A 478119 EPA 7470A 478159 92428830016 MW-14 EPA 7470A 478119 EPA 7470A 478159 92428830017 SW-1 EPA 7470A 478119 EPA 7470A 478159 92428830018 SW-3 EPA 7470A 478119 EPA 7470A 478159 92428830019 SW-4 EPA 7470A 478119 EPA 7470A 478159 92428830001 MWA R EPA 3510C 474895 EPA 8270E 475228 92428830002 MW-2R EPA 3510C 474895 EPA 8270E 475228 92428830003 MW-3R EPA 3510C 474895 EPA 8270E 475228 92428830004 MW-4R EPA 3510C 474895 EPA 8270E 475228 92428830005 MW-15 EPA 3510C 474895 EPA 8270E 475228 92428830006 SW-2 EPA 3510C 474895 EPA 8270E 475228 92428830007 EQUIPMENT BLANK EPA 3510C 474895 EPA 8270E 475228 92428830001 MWA R SM 2320E-2011 475950 92428830002 MW-211 SM 2320B-2011 475950 92428830003 MW-311 SM 2320B-2011 475950 92428830004 MW-4R SM 2320B-2011 476289 92428830005 MW-15 SM 2320B-2011 476289 92428830006 SW-2 SM 2320E-2011 476289 92428830007 EQUIPMENT BLANK SM 2320B-2011 476289 92428830008 MW-5R SM 2320B-2011 476289 92428830009 MW-7 SM 2320B-2011 476289 92428830010 MW-8 SM 2320B-2011 475680 92428830011 MW-9 SM 2320B-2011 475680 92428830012 MW-10 SM 2320B-2011 475950 92428830013 MW-11 SM 2320B-2011 475950 92428830014 MW-12 SM 2320B-2011 475950 92428830015 MW-13 SM 2320B-2011 475950 92428830016 MW-14 SM 2320B-2011 475950 92428830017 SW-1 SM 2320E-2011 476289 92428830018 SW-3 SM 2320E-2011 476289 92428830019 SW-4 SM 2320E-2011 476289 92428830001 MWA R SM 4500-S2D-2011 475037 92428830002 MW-2R SM 4500-S2D-2011 475037 92428830003 MW-3R SM 4500-S2D-2011 475037 92428830004 MW-4R SM 4500-S2D-2011 475037 92428830005 MW-15 SM 4500-S2D-2011 475554 92428830006 SW-2 SM 4500-S2D-2011 475554 92428830007 EQUIPMENT BLANK SM 4500-S2D-2011 475554 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 57 of 64 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LF GW SAMPLING Pace Project No.: 92428830 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92428830008 MW-511 SM 4500-S2D-2011 475554 92428830009 MW-7 SM 4500-S2D-2011 475554 92428830010 MW-8 SM 4500-S2D-2011 475036 92428830011 MW-9 SM 4500-S2D-2011 475036 92428830012 MW-10 SM 4500-S2D-2011 475037 92428830013 MW-11 SM 4500-S2D-2011 475037 92428830014 MW-12 SM 4500-S2D-2011 475037 92428830015 MW-13 SM 4500-S2D-2011 475037 92428830016 MW-14 SM 4500-S2D-2011 475037 92428830017 SW-1 SM 4500-S2D-2011 475554 92428830018 SW-3 SM 4500-S2D-2011 475554 92428830019 SW-4 SM 4500-S2D-2011 475554 92428830001 MWA R EPA 300.0 Rev 2.1 1993 477718 92428830002 MW-211 EPA 300.0 Rev 2.1 1993 477718 92428830003 MW-311 EPA 300.0 Rev 2.1 1993 477718 92428830004 MW-411 EPA 300.0 Rev 2.1 1993 477718 92428830005 MW-15 EPA 300.0 Rev 2.1 1993 477718 92428830006 SW-2 EPA 300.0 Rev 2.1 1993 477718 92428830007 EQUIPMENT BLANK EPA 300.0 Rev 2.1 1993 477718 92428830008 MW-5R EPA 300.0 Rev 2.1 1993 477718 92428830009 MW-7 EPA 300.0 Rev 2.1 1993 477718 92428830010 MW-8 EPA 300.0 Rev 2.1 1993 477718 92428830011 MW-9 EPA 300.0 Rev 2.1 1993 477718 92428830012 MW-10 EPA 300.0 Rev 2.1 1993 477718 92428830013 MW-11 EPA 300.0 Rev 2.1 1993 477718 92428830014 MW-12 EPA 300.0 Rev 2.1 1993 477718 92428830015 MW-13 EPA 300.0 Rev 2.1 1993 477718 92428830016 MW-14 EPA 300.0 Rev 2.1 1993 477718 92428830017 SW-1 EPA 300.0 Rev 2.1 1993 477718 92428830018 SW-3 EPA 300.0 Rev 2.1 1993 477718 92428830019 SW-4 EPA 300.0 Rev 2.1 1993 477718 92428830001 MWA R SM 4500-CI-E-2011 474983 92428830002 MW-2R SM 4500-CI-E-2011 474983 92428830003 MW-3R SM 4500-CI-E-2011 474983 92428830004 MW-4R SM 4500-CI-E-2011 474983 92428830005 MW-15 SM 4500-CI-E-2011 474983 92428830006 SW-2 SM 4500-CI-E-2011 474983 92428830007 EQUIPMENT BLANK SM 4500-CI-E-2011 474983 92428830008 MW-5R SM 4500-CI-E-2011 474983 92428830009 MW-7 SM 4500-CI-E-2011 474986 92428830010 MW-8 SM 4500-CI-E-2011 474986 92428830011 MW-9 SM 4500-CI-E-2011 474986 92428830012 MW-10 SM 4500-CI-E-2011 474986 92428830013 MW-11 SM 4500-CI-E-2011 474986 92428830014 MW-12 SM 4500-CI-E-2011 474986 92428830015 MW-13 SM 4500-CI-E-2011 474986 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/03/2019 07:05 AM without the written consent of Pace Analytical Services, LLC. Page 58 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LF GW SAMPLING 92428830 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92428830016 MW-14 SM 4500-CI-E-2011 474986 92428830017 SW-1 SM 4500-CI-E-2011 474986 92428830018 SW-3 SM 4500-CI-E-2011 474986 92428830019 SW-4 SM 4500-CI-E-2011 474986 92428830001 MWA R SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830002 MW-2R SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830003 MW-3R SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830004 MW-411 SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830005 MWA 5 SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830006 SW-2 SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830007 EQUIPMENT BLANK SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830008 MW-5R SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830009 MW-7 SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830010 MW-8 SM 4500-CN-E-2011 475355 SM 4500-CN-E-2011 475535 92428830011 MW-9 SM 4500-CN-E-2011 475355 SM 4500-CN-E-2011 475535 92428830012 MW-10 SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830013 MW-11 SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830014 MW-12 SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830015 MW-13 SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830016 MW-14 SM 4500-CN-E-2011 476151 SM 4500-CN-E-2011 476216 92428830017 SW-1 SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830018 SW-3 SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 92428830019 SW-4 SM 4500-CN-E-2011 476152 SM 4500-CN-E-2011 476218 Date: 06/03/2019 07:05 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 59 of 64 Document Name: Document Revised: February 7, 2018 r i3Cef�IlailCc�� Sample Condition Upon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: r F-CAA-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden Greenwood Huntersville C21, Raleigh[] Mechanicsville[] Client Nanie:Upon ReceiptW O# : 92428830 � � Projec#! Courier: []Fed Ex ❑UPS ❑USPS Client ❑ Commercial ❑Pace ❑Other; 92428830 III i1 Custody Seal Present? ❑Yes 9 o Seals intact? [:]YesQ1,411 I / Bate/Initials Person Examining Cankenti ;k—n- Racking Material: ❑Bubble Wrap I� bbie Bags [:]None ❑ Other Biological TisSU '" n? Thermo 'I ❑Yes [:]No N/A rR cur, ID, 92TO48 Type of ice: DWet ❑Blue ❑None Cooler Temp ('Cl: ?�' Correction Factor: Add/Subtract ('Cl 0.0 Temp should be above freezing to VC Cooler Temp Corrected ['Cj: ❑Samples out of temp criteria. Samples on ice, coaling process has begun USDA Regulated Soil VNJIA, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, including Hawaii and Puerto Rico)? Des ONO Comments/Discreaanev: Chain of Custody Present? es ❑No ❑N/A 1. Samples Arrived within Hold Time? Yes []No []N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes a ❑N/A 3. Rush Turn Around Time Requested? Elves li a []N/A 4. 5ufficient Volume?PfYes ❑No []N/A S. Correct Containers Used? es [:]No ❑N/A G. -Pace Containers Used? s ❑ND ❑N/A Containers Intact? 2 e5 ❑No [:]WA 7. Dissolved analysis: Samples Field Filtered? ❑y ❑No QdI'A g. Sample Labels Match COC? , es [)No ❑N/A 9. -Includes Date/Time/ID/Analys Headspace in VOA Vials f>5-6mm Trip Blank Present? Trip Blank Custody Seals Present? COMMENTS/SAMPLE DISCREPANCY IJYes ❑No LJa/A 1 10. []Yes ❑No QWl 11. Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Project Manager SRF Review: Date: Date: Field Data Required? [:]Yes ❑No Page 60 of 64 Document Name: Document Revised: February 7, 2018 aceAr2alytical - Sample Condition Upon Receipt(SCUR) Pagel of 2 Document No.: Issuing Authority: F•CAR-CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLH8 "Bottom half of box is to list number of bottle t 5- 1 Project is WO# : 92428830 PM: KLI{1 Duo Darr 03/24/19 CLIENT: 92-NDR at E a Y Z 2 a c a u a eN-i 7 Q a m Z 2 W a. c u a N 6 /�'1 a an Z 2 a) a c v 0. 7 N 0. m Q 2 m a c °' .y eel a m _ U V O in N a E .r _ R a m v p Z T u E N 2 nl a m x Z ;a 4 4 Z a E N .. N ? a m ry - A a v z p 10 a E ry .r V Q a m v a m U a w q E v ? u. a` ? Z W 2 °� y x v a a _ C c U O D x n E E E a ¢ Q a` w of .a .--I N = = : e1 rl RI l7 [7 l7 Q G Q N v N a E Q y rl yr N 4 a V U a z v v D a in E S Q 1 E a Q r`"v , E ,¢ N of Q ni T l7 U a a d E v Q O 7 E O -7 = d1 +.77 O z m ¢ vryi 2 N c Q 4 O 0 y E E P O 0 r � O+ QI �7 t7 > > 4 Z tl D m Q O 7 E O q a in W O r$yi z Y « m in O = vi j y a a a '° .2 y m Y 3.f O > > z m a ,^ E v7 .N-1 a �n 10 a z in '9 a v E O N a w ci N 2 A o. E ,� N a m ? N V a a E E O rl l7 .9 = w zn c q c N O N ,n 7 z > r 2 a c a E Q O Q i7 C 2?J � 2 V z 3 � I N \\N Z 4N r N\\ 1 L Z 1 1 6 2 7 'J 8 � � L I 9 � � f fX N\ N 1 \\\iA N N\- 11 Ndi 12 N I F\�\ X N, � NIq NNI pH Adjustment Log for Preserved Samples Sample 1D Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot d Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will besent to the North Carolina DEHNR Certification Office (Ee. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 61 of 64 Name: Doc9C5033-Rev.06 Document Revised: February 7, 2018 �—�aceAndlytdal Sample Conditon Receipt(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination Is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform,TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project I W0# ; 92428830 PM: KLH1 Due Date; 05/24/19 CLIENT: 92-HDR z z z a z U n A, o LJ y z N r z 2 N Z Z b N n ? R7 z -- ? N =1 y R tr 2 W V C ^ a 2 V T a _ 2 Q Z2t a 5 v a ti G u pl a O 0 H = rn 2 u 4 Y ^D Z O N Z tea! C =d Y a VI = N 2 E a \ Z y M N Q Z a ? 0 4 rn m « _ a y U tJ 4 N Z Z V G C n 4 a E vi • a E o V a E o V ro `a e 'P o a E Ln ; o E o - N u tg ° rc o a a E J E E ® 0 E ¢ v v 0 E a `i a J E a E E a v a E ¢ E E Ln ry a rn 2 O a J E Z ¢ D > J E 7 O E O > E Y m a 1' m y ffi a N a� m E 9 n J E a J E c a G J N Q E J E ! d 7 a N m a Ul rOv a r+ H 7 a ry MQV a v, w M .N-1 .� H = .i N M — rl � o N rn o.4 r la 0 G M M 0 L 0 N of N IL c O O O N 7 O 17 � 0 n c7 m an m m m m m m 3 4 a a a a ¢ o > > 0 > vi ,n m a > o 1 `` i \X'1\4 N' 2 _l I 3 � NN ✓ K 4 [. I 1 s (-"I u fi -\';++ 1 NN 7 7 L- ^^ U ✓ B \\\�s 9 10 11 12 171 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot 4 Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. out of hold, incorrect preservative, out of temp, incorrect containers. Page 62 of 64 3 3 C a 0 a c» J N ..► o m co ti m rr A (aro .a ITEM # n N H 4 - ` c2 m En O �n 3 tYi D 2' C y P o �O �1 f!� in70 70 3 3 3 N m N N X c W cp n�D n� 3 c ^ .� N ; r o N m C P v = xA T to s F x R 3 0 m a m O W a O v A m s MATRIXCOOE (see valid codes la left) o n Q SAMPLETYPE (G=GRAB C=COMP) _ O re A v o n � m O a 0 z i �f J �L111 yi Ste_ - D rn N W rt m m o 3 Z C7 D O Q Sy1 _ �1`r G '� Q [may S (�! �. -4 m Z tl `n 6_ tl Z C�� E tip' cn r(�ii J O SAMPLE TEMP AT COLLECTION N 77 LA ` k ] _i _j --J I OF CONTAINERS w m m a o D= rNi Q m if 'r VJ ,l'(J'f " 1 ail `� 4 �.P� UnpreServed o ^ — H2SO4 2 m v, 0 m Q HNO3 'U # v m n C � HCI 'Ibn o m O n � NaOH m h n C � n Na25203 L m Q1 Methanol rn Z cV 77 Other NL�� Ci L �. 1O D fl1 — Analyses Test YIN rn C x x X x x x x 8270 ^° oar a ? x X X X X X x x x x x X Alkalinity z 8 (p X x x x x x x x x X X X T0S by 254OC 3 C a � - x x x x x X X x x X X x Chloride � a m 3 v � j X X x x x x x x X x x X Cyanide a Y 'b_ �i d (D Cj " ti,� x x x x x x x x x X X x Sulfide C n O 4 3 eh CL � W ..-J re m C of v m LID N Residual Chlorine (M) b A b O c O V Sc o ` jam' O C o CQ Ij Page 63 of 64 X v rn rn D n m [n m - 00 ji: ITEM # A m N o w a> cn w N p a a Ch en En CL p 3 m a n n n z N C N m [3 1 r N N C N fD H_ r a c o % m A n » _ n 0 v m ��v Crro20 n G m # v a 3 O v m � C MAiRIXCCOE (see valid codes to lefi) o SAMPLE TYPE (G=GRAB C=CGMp) ro - O > > C O n 0 IT, � a -I A C-) O m r- 17 r� O -nl S IT O m N .e a' m rn 3 a C� [� +l1 _ �It z 0 m 7 z 6 r O UI m `n SAMPLE TEMP AT COLLECTION y `i 1 � U\ �� Cn " Y # OF CONTAINERS �� -annr m m m n o m n a /4 .J`t \d l,S't Unproserved ,(} N y p' 5 O N y/ {� 4n O O C W .0 H2SO4 m e m z C o � O m HNO3 w 2L FY y C7 HCI 2 m O D C � y m -'� Methanol m z h� OtherA),0 iJLi4L � Analyses Test YIN B270 ? D x x x x X X x Alkalinity X X X x x x x TH by2540C a m X x x x x X X Chloride m w c (. x x x x x x x Cyanide ' A 0 0 1 C 1, ! n I x x x x x x X Sulfide w y @ ~ y n (V rh n � a w z rnl 'N W m c or tu tu c Residual Chlorine (YIN) N m ID s 0 ma's c o ; o n {�f N Page 64 of 64 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 11, 2019 Mark Filardi HDR 440 S. Church St Suite 900 Charlotte, NC 28202 RE: Project: OSR Pace Project No.: 92431068 Dear Mark Filardi: Enclosed are the analytical results for sample(s) received by the laboratory between May 30, 2019 and May 31, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR Pace Project No.: 92431068 Atlanta Certification IDs 110 Technology Parkway Peachtree Corners, GA 30092 Florida DOH Certification #: E87315 Georgia DW Inorganics Certification #: 812 Georgia DW Microbiology Certification #: 812 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 CERTIFICATIONS North Carolina Certification #: 381 South Carolina Certification #: 98011001 Virginia Certification #: 460204 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR 92431068 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92431068001 MW-8 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068002 MW-9 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068003 MW-10 EPA 8081 B SEM 14 PASI-C EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068004 MW-11 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068005 MW-12 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068006 MW-14 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068007 TRIP BLANK EPA 8260D CL 53 PASI-C 92431068008 MW-1 R EPA 8081 B SEM 14 PASI-C EPA8151A MZP 11 PASI-GA EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068009 MW-2R EPA 8081 B SEM 14 PASI-C EPA8151A MZP 11 PASI-GA EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068010 MW-3R EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068011 MW-4R EPA 8081 B SEM 14 PASI-C EPA8151A MZP 11 PASI-GA EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068012 MW-5R EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068013 MW-7 EPA 8081 B SEM 14 PASI-C EPA 8260B Mod. SAS 3 PASI-C EPA 8260D CL 53 PASI-C 92431068014 MW-13 EPA 8260B Mod. SAS 3 PASI-C EPA 8260D CL 53 PASI-C 92431068015 MW-15 EPA 8081 B SEM 14 PASI-C EPA8151A MZP 11 PASI-GA REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR Pace Project No.: 92431068 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 8260B Mod. SAS 3 PASI-C EPA 8260D CL 53 PASI-C 92431068016 SW-1 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068017 SW-2 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068018 SW-3 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068019 SW-4 EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C 92431068020 EQUIPMENT BLANK EPA 8260B Mod. LMB 3 PASI-C EPA 8260D CL 53 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-8 Lab ID: 92431068001 Collected: 05/29/19 08:14 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 17:43 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 17:43 17060-07-0 Toluene-d8 (S) 106 % 50-150 1 06/05/19 17:43 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 05:30 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 05:30 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 05:30 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 05:30 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 05:30 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 05:30 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 05:30 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 05:30 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 05:30 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 05:30 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 05:30 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 05:30 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 05:30 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 05:30 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 05:30 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 05:30 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 05:30 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 05:30 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 05:30 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 05:30 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 05:30 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 05:30 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 05:30 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 05:30 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 05:30 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 05:30 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 05:30 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 05:30 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 05:30 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 05:30 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 05:30 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 05:30 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 05:30 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 05:30 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 05:30 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 05:30 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 05:30 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 05:30 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 05:30 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 05:30 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 05:30 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-8 Lab ID: 92431068001 Collected: 05/29/19 08:14 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 05:30 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 05:30 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 05:30 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 05:30 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 05:30 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 05:30 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 05:30 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 05:30 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 05:30 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 06/11/19 05:30 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/11/19 05:30 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/11/19 05:30 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-9 Lab ID: 92431068002 Collected: 05/29/19 09:10 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 18:02 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 18:02 17060-07-0 Toluene-d8 (S) 106 % 50-150 1 06/05/19 18:02 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 05:47 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 05:47 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 05:47 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 05:47 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 05:47 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 05:47 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 05:47 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 05:47 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 05:47 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 05:47 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 05:47 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 05:47 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 05:47 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 05:47 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 05:47 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 05:47 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 05:47 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 05:47 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 05:47 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 05:47 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 05:47 110-57-6 Dichlorodifluoromethane 1.4 ug/L 1.0 1 06/11/19 05:47 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 05:47 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 05:47 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 05:47 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 05:47 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 05:47 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 05:47 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 05:47 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 05:47 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 05:47 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 05:47 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 05:47 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 05:47 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 05:47 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 05:47 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 05:47 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 05:47 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 05:47 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 05:47 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 05:47 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-9 Lab ID: 92431068002 Collected: 05/29/19 09:10 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 05:47 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 05:47 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 05:47 79-01-6 Trichlorofluoromethane 1.7 ug/L 1.0 1 06/11/19 05:47 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 05:47 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 05:47 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 05:47 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 05:47 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 05:47 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 06/11/19 05:47 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/11/19 05:47 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 06/11/19 05:47 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-10 Lab ID: 92431068003 Collected: 05/29/19 12:39 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV Low Level Landfill Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 309-00-2 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 319-84-6 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 319-86-8 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 72-54-8 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 50-29-3 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 959-98-8 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 33213-65-9 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 72-20-8 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 7421-93-4 L1 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 76-44-8 ND ug/L 0.050 1 06/04/19 09:19 06/07/19 23:03 1024-57-3 ND ug/L 0.15 1 06/04/19 09:19 06/07/19 23:03 72-43-5 42 % 92 % Analytical Method: EPA 8260E Mod. 6.4 ug/L 99 % 108 % Analytical Method: EPA 8260D 10-130 1 06/04/19 09:19 06/07/19 23:03 877-09-8 10-130 1 06/04/19 09:19 06/07/19 23:03 2051-24-3 2.0 1 06/05/19 18:21 123-91-1 50-150 1 06/05/19 18:21 17060-07-0 50-150 1 06/05/19 18:21 2037-26-5 Acetone ND ug/L 25.0 1 06/11/19 06:05 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 06:05 107-13-1 Benzene 0.33J ug/L 1.0 1 06/11/19 06:05 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 06:05 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 06:05 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 06:05 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 06:05 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 06:05 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 06:05 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 06:05 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 06:05 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 06:05 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 06:05 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 06:05 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 06:05 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 06:05 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 06:05 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 06:05 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:05 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:05 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 06:05 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 06:05 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 06:05 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 06:05 107-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-10 Lab ID: 92431068003 Collected: 05/29/19 12:39 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 06/11/2019 04:30 PM Analytical Method: EPA 8260D ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 113 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 0.28J ug/L 98 % 101 % 99 % 1.0 1 06/11/19 06:05 75-35-4 1.0 1 06/11/19 06:05 156-59-2 1.0 1 06/11/19 06:05 156-60-5 1.0 1 06/11/19 06:05 78-87-5 1.0 1 06/11/19 06:05 10061-01-5 1.0 1 06/11/19 06:05 10061-02-6 1.0 1 06/11/19 06:05 100-41-4 5.0 1 06/11/19 06:05 591-78-6 20.0 1 06/11/19 06:05 74-88-4 5.0 1 06/11/19 06:05 75-09-2 5.0 1 06/11/19 06:05 108-10-1 1.0 1 06/11/19 06:05 100-42-5 1.0 1 06/11/19 06:05 630-20-6 1.0 1 06/11/19 06:05 79-34-5 1.0 1 06/11/19 06:05 127-18-4 10.0 1 06/11/19 06:05 109-99-9 1.0 1 06/11/19 06:05 108-88-3 1.0 1 06/11/19 06:05 71-55-6 1.0 1 06/11/19 06:05 79-00-5 1.0 1 06/11/19 06:05 79-01-6 1.0 1 06/11/19 06:05 75-69-4 1.0 1 06/11/19 06:05 96-18-4 2.0 1 06/11/19 06:05 108-05-4 1.0 1 06/11/19 06:05 75-01-4 2.0 1 06/11/19 06:05 179601-23-1 1.0 1 06/11/19 06:05 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06/11/19 06:05 460-00-4 06/11/19 06:05 17060-07-0 06/11/19 06:05 2037-26-5 Page 10 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-11 Lab ID: 92431068004 Collected: 05/29/19 13:53 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 18:41 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 99 % 50-150 1 06/05/19 18:41 17060-07-0 Toluene-d8 (S) 106 % 50-150 1 06/05/19 18:41 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 06:22 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 06:22 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 06:22 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 06:22 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 06:22 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 06:22 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 06:22 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 06:22 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 06:22 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 06:22 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 06:22 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 06:22 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 06:22 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 06:22 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 06:22 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 06:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 06:22 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 06:22 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:22 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:22 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 06:22 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 06:22 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 06:22 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 06:22 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 06:22 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 06:22 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 06:22 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 06:22 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 06:22 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 06:22 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 06:22 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 06:22 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 06:22 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 06:22 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 06:22 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 06:22 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 06:22 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 06:22 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 06:22 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 06:22 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 06:22 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-11 Lab ID: 92431068004 Collected: 05/29/19 13:53 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 06:22 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 06:22 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 06:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 06:22 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 06:22 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 06:22 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 06:22 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 06:22 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 06:22 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 06/11/19 06:22 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/11/19 06:22 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 06/11/19 06:22 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-12 Lab ID: 92431068005 Collected: 05/29/19 14:46 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) 5.3 ug/L 2.0 1 06/05/19 19:00 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 19:00 17060-07-0 Toluene-d8 (S) 105 % 50-150 1 06/05/19 19:00 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 06:40 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 06:40 107-13-1 Benzene 0.33J ug/L 1.0 1 06/11/19 06:40 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 06:40 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 06:40 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 06:40 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 06:40 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 06:40 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 06:40 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 06:40 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 06:40 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 06:40 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 06:40 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 06:40 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 06:40 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 06:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 06:40 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 06:40 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:40 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:40 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 06:40 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 06:40 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 06:40 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 06:40 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 06:40 75-35-4 cis-1,2-Dichloroethene 0.40J ug/L 1.0 1 06/11/19 06:40 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 06:40 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 06:40 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 06:40 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 06:40 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 06:40 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 06:40 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 06:40 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 06:40 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 06:40 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 06:40 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 06:40 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 06:40 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 06:40 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 06:40 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 06:40 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-12 Lab ID: 92431068005 Collected: 05/29/19 14:46 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 06:40 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 06:40 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 06:40 79-01-6 Trichlorofluoromethane 0.811 ug/L 1.0 1 06/11/19 06:40 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 06:40 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 06:40 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 06:40 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 06:40 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 06:40 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 06/11/19 06:40 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/11/19 06:40 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/11/19 06:40 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-14 Lab ID: 92431068006 Collected: 05/29/19 10:20 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/07/19 11:35 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 99 % 50-150 1 06/07/19 11:35 17060-07-0 Toluene-d8 (S) 109 % 50-150 1 06/07/19 11:35 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 06:57 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 06:57 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 06:57 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 06:57 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 06:57 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 06:57 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 06:57 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 06:57 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 06:57 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 06:57 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 06:57 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 06:57 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 06:57 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 06:57 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 06:57 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 06:57 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 06:57 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 06:57 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:57 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 06:57 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 06:57 110-57-6 Dichlorodifluoromethane 3.0 ug/L 1.0 1 06/11/19 06:57 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 06:57 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 06:57 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 06:57 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 06:57 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 06:57 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 06:57 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 06:57 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 06:57 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 06:57 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 06:57 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 06:57 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 06:57 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 06:57 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 06:57 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 06:57 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 06:57 79-34-5 Tetrachloroethene 0.52J ug/L 1.0 1 06/11/19 06:57 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 06:57 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 06:57 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-14 Lab ID: 92431068006 Collected: 05/29/19 10:20 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 06:57 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 06:57 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 06:57 79-01-6 Trichlorofluoromethane 0.92J ug/L 1.0 1 06/11/19 06:57 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 06:57 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 06:57 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 06:57 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 06:57 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 06:57 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 06/11/19 06:57 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/11/19 06:57 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 06/11/19 06:57 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: TRIP BLANK Lab ID: 92431068007 Collected: 05/30/19 00:00 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 04:55 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 04:55 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 04:55 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 04:55 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 04:55 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 04:55 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 04:55 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 04:55 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 04:55 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 04:55 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 04:55 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 04:55 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 04:55 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 04:55 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 04:55 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 04:55 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 04:55 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 04:55 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 04:55 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 04:55 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 04:55 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 04:55 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 04:55 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 04:55 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 04:55 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 04:55 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 04:55 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 04:55 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 04:55 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 04:55 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 04:55 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 04:55 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 04:55 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 04:55 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 04:55 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 04:55 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 04:55 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 04:55 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 04:55 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 04:55 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 04:55 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 04:55 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 04:55 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 04:55 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 04:55 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 04:55 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 04:55 108-05-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: TRIP BLANK Lab ID: 92431068007 Collected: 05/30/19 00:00 Received: 05/30/19 07:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Vinyl chloride ND ug/L 1.0 1 06/11/19 04:55 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 04:55 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 04:55 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 06/11/19 04:55 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/11/19 04:55 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/11/19 04:55 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MWAR Lab ID: 92431068008 Collected: 05/31/19 14:45 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Aldrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 309-00-2 alpha-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 319-84-6 delta-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 319-86-8 4,4'-DDD ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 72-54-8 4,4'-DDT ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 50-29-3 Endosulfan I ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 959-98-8 Endosulfan 11 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 33213-65-9 Endrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 72-20-8 Endrin aldehyde ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 7421-93-4 Heptachlor ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 06/05/19 20:42 06/07/19 17:44 1024-57-3 Methoxychlor ND ug/L 0.15 1 06/05/19 20:42 06/07/19 17:44 72-43-5 Surrogates Tetrachloro-m-xylene (S) 55 % 10-130 1 06/05/19 20:42 06/07/19 17:44 877-09-8 Decachlorobiphenyl (S) 144 % 10-130 1 06/05/19 20:42 06/07/19 17:44 2051-24-3 8151A Cl Acid Herbicide Waters Analytical Method: EPA 8151A Preparation Method: EPA 8151A 2,4-D ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:08 94-75-7 Dalapon ND ug/L 10.0 1 06/06/19 11:10 06/10/19 21:08 75-99-0 2,4-DB ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:08 94-82-6 Dicamba ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:08 1918-00-9 Dichloroprop ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:08 120-36-5 Dinoseb ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:08 88-85-7 MCPA ND ug/L 1000 1 06/06/19 11:10 06/10/19 21:08 94-74-6 MCPP ND ug/L 1000 1 06/06/19 11:10 06/10/19 21:08 7085-19-0 2,4,5-T ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:08 93-76-5 2,4,5-TP (Silvex) ND ug/L 10.0 1 06/06/19 11:10 06/10/19 21:08 93-72-1 Surrogates 2,4-DCAA (S) 135 %. 10-155 1 06/06/19 11:10 06/10/19 21:08 19719-28-9 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 13:33 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 100 % 50-150 1 06/05/19 13:33 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 06/05/19 13:33 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 07:15 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 07:15 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 07:15 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 07:15 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 07:15 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 07:15 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 07:15 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 07:15 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 07:15 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 07:15 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. M1 M1 S3 Page 19 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MWAR Lab ID: 92431068008 Collected: 05/31/19 14:45 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 06/11/2019 04:30 PM Analytical Method: EPA 8260D ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 0.901 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 98 % 103 % 100 % 1.0 1 06/11/19 07:15 108-90-7 1.0 1 06/11/19 07:15 75-00-3 5.0 1 06/11/19 07:15 67-66-3 1.0 1 06/11/19 07:15 74-87-3 5.0 1 06/11/19 07:15 96-12-8 1.0 1 06/11/19 07:15 124-48-1 1.0 1 06/11/19 07:15 106-93-4 1.0 1 06/11/19 07:15 74-95-3 1.0 1 06/11/19 07:15 95-50-1 1.0 1 06/11/19 07:15 106-46-7 1.0 1 06/11/19 07:15 110-57-6 1.0 1 06/11/19 07:15 75-71-8 1.0 1 06/11/19 07:15 75-34-3 1.0 1 06/11/19 07:15 107-06-2 1.0 1 06/11/19 07:15 75-35-4 1.0 1 06/11/19 07:15 156-59-2 1.0 1 06/11/19 07:15 156-60-5 1.0 1 06/11/19 07:15 78-87-5 1.0 1 06/11/19 07:15 10061-01-5 1.0 1 06/11/19 07:15 10061-02-6 1.0 1 06/11/19 07:15 100-41-4 5.0 1 06/11/19 07:15 591-78-6 20.0 1 06/11/19 07:15 74-88-4 5.0 1 06/11/19 07:15 75-09-2 5.0 1 06/11/19 07:15 108-10-1 1.0 1 06/11/19 07:15 100-42-5 1.0 1 06/11/19 07:15 630-20-6 1.0 1 06/11/19 07:15 79-34-5 1.0 1 06/11/19 07:15 127-18-4 10.0 1 06/11/19 07:15 109-99-9 1.0 1 06/11/19 07:15 108-88-3 1.0 1 06/11/19 07:15 71-55-6 1.0 1 06/11/19 07:15 79-00-5 1.0 1 06/11/19 07:15 79-01-6 1.0 1 06/11/19 07:15 75-69-4 1.0 1 06/11/19 07:15 96-18-4 2.0 1 06/11/19 07:15 108-05-4 1.0 1 06/11/19 07:15 75-01-4 2.0 1 06/11/19 07:15 179601-23-1 1.0 1 06/11/19 07:15 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06/11/19 07:15 460-00-4 06/11/19 07:15 17060-07-0 06/11/19 07:15 2037-26-5 Page 20 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-2R Lab ID: 92431068009 Collected: 05/31/19 12:15 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Aldrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 309-00-2 alpha-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 319-84-6 delta-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 319-86-8 4,4'-DDD ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 72-54-8 4,4'-DDT ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 50-29-3 Endosulfan I ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 959-98-8 Endosulfan 11 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 33213-65-9 Endrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 72-20-8 Endrin aldehyde ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 7421-93-4 Heptachlor ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:10 1024-57-3 Methoxychlor ND ug/L 0.15 1 06/05/19 20:42 06/07/19 18:10 72-43-5 Surrogates Tetrachloro-m-xylene (S) 78 % 10-130 1 06/05/19 20:42 06/07/19 18:10 877-09-8 Decachlorobiphenyl (S) 110 % 10-130 1 06/05/19 20:42 06/07/19 18:10 2051-24-3 8151A Cl Acid Herbicide Waters Analytical Method: EPA 8151A Preparation Method: EPA 8151A 2,4-D ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:30 94-75-7 Dalapon ND ug/L 10.0 1 06/06/19 11:10 06/10/19 21:30 75-99-0 2,4-DB ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:30 94-82-6 Dicamba ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:30 1918-00-9 Dichloroprop ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:30 120-36-5 Dinoseb ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:30 88-85-7 MCPA ND ug/L 1000 1 06/06/19 11:10 06/10/19 21:30 94-74-6 MCPP ND ug/L 1000 1 06/06/19 11:10 06/10/19 21:30 7085-19-0 2,4,5-T ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:30 93-76-5 2,4,5-TP (Silvex) ND ug/L 10.0 1 06/06/19 11:10 06/10/19 21:30 93-72-1 Surrogates 2,4-DCAA (S) 116 %. 10-155 1 06/06/19 11:10 06/10/19 21:30 19719-28-9 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) 2.3 ug/L 2.0 1 06/05/19 13:52 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 101 % 50-150 1 06/05/19 13:52 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 06/05/19 13:52 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 07:32 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 07:32 107-13-1 Benzene 2.3 ug/L 1.0 1 06/11/19 07:32 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 07:32 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 07:32 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 07:32 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 07:32 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 07:32 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 07:32 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 07:32 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-2R Lab ID: 92431068009 Collected: 05/31/19 12:15 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 06/11/2019 04:30 PM Analytical Method: EPA 8260D ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 0.43J ug/L ND ug/L ND ug/L 0.67J ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 1.4 ug/L 51.3 ug/L ND ug/L ND ug/L ND ug/L 0.97J ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 98 % 102 % 100 % 1.0 1 06/11/19 07:32 108-90-7 1.0 1 06/11/19 07:32 75-00-3 5.0 1 06/11/19 07:32 67-66-3 1.0 1 06/11/19 07:32 74-87-3 5.0 1 06/11/19 07:32 96-12-8 1.0 1 06/11/19 07:32 124-48-1 1.0 1 06/11/19 07:32 106-93-4 1.0 1 06/11/19 07:32 74-95-3 1.0 1 06/11/19 07:32 95-50-1 1.0 1 06/11/19 07:32 106-46-7 1.0 1 06/11/19 07:32 110-57-6 1.0 1 06/11/19 07:32 75-71-8 1.0 1 06/11/19 07:32 75-34-3 1.0 1 06/11/19 07:32 107-06-2 1.0 1 06/11/19 07:32 75-35-4 1.0 1 06/11/19 07:32 156-59-2 1.0 1 06/11/19 07:32 156-60-5 1.0 1 06/11/19 07:32 78-87-5 1.0 1 06/11/19 07:32 10061-01-5 1.0 1 06/11/19 07:32 10061-02-6 1.0 1 06/11/19 07:32 100-41-4 5.0 1 06/11/19 07:32 591-78-6 20.0 1 06/11/19 07:32 74-88-4 5.0 1 06/11/19 07:32 75-09-2 5.0 1 06/11/19 07:32 108-10-1 1.0 1 06/11/19 07:32 100-42-5 1.0 1 06/11/19 07:32 630-20-6 1.0 1 06/11/19 07:32 79-34-5 1.0 1 06/11/19 07:32 127-18-4 10.0 1 06/11/19 07:32 109-99-9 1.0 1 06/11/19 07:32 108-88-3 1.0 1 06/11/19 07:32 71-55-6 1.0 1 06/11/19 07:32 79-00-5 1.0 1 06/11/19 07:32 79-01-6 1.0 1 06/11/19 07:32 75-69-4 1.0 1 06/11/19 07:32 96-18-4 2.0 1 06/11/19 07:32 108-05-4 1.0 1 06/11/19 07:32 75-01-4 2.0 1 06/11/19 07:32 179601-23-1 1.0 1 06/11/19 07:32 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06/11/19 07:32 460-00-4 06/11/19 07:32 17060-07-0 06/11/19 07:32 2037-26-5 Page 22 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-3R Lab ID: 92431068010 Collected: 05/31/19 07:58 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 14:11 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 100 % 50-150 1 06/05/19 14:11 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 06/05/19 14:11 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 07:50 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 07:50 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 07:50 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 07:50 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 07:50 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 07:50 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 07:50 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 07:50 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 07:50 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 07:50 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 07:50 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 07:50 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 07:50 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 07:50 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 07:50 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 07:50 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 07:50 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 07:50 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 07:50 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 07:50 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 07:50 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 07:50 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 07:50 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 07:50 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 07:50 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 07:50 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 07:50 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 07:50 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 07:50 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 07:50 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 07:50 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 07:50 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 07:50 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 07:50 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 07:50 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 07:50 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 07:50 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 07:50 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 07:50 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 07:50 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 07:50 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-3R Lab ID: 92431068010 Collected: 05/31/19 07:58 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 07:50 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 07:50 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 07:50 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 07:50 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 07:50 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 07:50 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 07:50 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 07:50 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 07:50 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 06/11/19 07:50 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/11/19 07:50 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/11/19 07:50 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 24 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-4R Lab ID: 92431068011 Collected: 05/31/19 10:11 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Aldrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 309-00-2 alpha-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 319-84-6 delta-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 319-86-8 4,4'-DDD ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 72-54-8 4,4'-DDT ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 50-29-3 Endosulfan I ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 959-98-8 Endosulfan 11 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 33213-65-9 Endrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 72-20-8 Endrin aldehyde ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 7421-93-4 Heptachlor ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:35 1024-57-3 Methoxychlor ND ug/L 0.15 1 06/05/19 20:42 06/07/19 18:35 72-43-5 Surrogates Tetrachloro-m-xylene (S) 116 % 10-130 1 06/05/19 20:42 06/07/19 18:35 877-09-8 Decachlorobiphenyl (S) 120 % 10-130 1 06/05/19 20:42 06/07/19 18:35 2051-24-3 8151A Cl Acid Herbicide Waters Analytical Method: EPA 8151A Preparation Method: EPA 8151A 2,4-D ND ug/L 5.0 1 06/06/19 11:10 06/10/19 20:46 94-75-7 Dalapon ND ug/L 10.0 1 06/06/19 11:10 06/10/19 20:46 75-99-0 2,4-DB ND ug/L 5.0 1 06/06/19 11:10 06/10/19 20:46 94-82-6 Dicamba ND ug/L 5.0 1 06/06/19 11:10 06/10/19 20:46 1918-00-9 Dichloroprop ND ug/L 5.0 1 06/06/19 11:10 06/10/19 20:46 120-36-5 Dinoseb ND ug/L 5.0 1 06/06/19 11:10 06/10/19 20:46 88-85-7 MCPA ND ug/L 1000 1 06/06/19 11:10 06/10/19 20:46 94-74-6 MCPP ND ug/L 1000 1 06/06/19 11:10 06/10/19 20:46 7085-19-0 2,4,5-T ND ug/L 5.0 1 06/06/19 11:10 06/10/19 20:46 93-76-5 2,4,5-TP (Silvex) ND ug/L 10.0 1 06/06/19 11:10 06/10/19 20:46 93-72-1 Surrogates 2,4-DCAA (S) 74 %. 10-155 1 06/06/19 11:10 06/10/19 20:46 19719-28-9 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) 5.1 ug/L 2.0 1 06/05/19 14:30 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 100 % 50-150 1 06/05/19 14:30 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 06/05/19 14:30 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 08:07 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 08:07 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 08:07 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 08:07 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 08:07 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 08:07 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 08:07 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 08:07 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 08:07 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 08:07 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-4R Lab ID: 92431068011 Collected: 05/31/19 10:11 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 06/11/2019 04:30 PM Analytical Method: EPA 8260D ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 11.4 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 98 % 100 % 100 % 1.0 1 06/11/19 08:07 108-90-7 1.0 1 06/11/19 08:07 75-00-3 5.0 1 06/11/19 08:07 67-66-3 1.0 1 06/11/19 08:07 74-87-3 5.0 1 06/11/19 08:07 96-12-8 1.0 1 06/11/19 08:07 124-48-1 1.0 1 06/11/19 08:07 106-93-4 1.0 1 06/11/19 08:07 74-95-3 1.0 1 06/11/19 08:07 95-50-1 1.0 1 06/11/19 08:07 106-46-7 1.0 1 06/11/19 08:07 110-57-6 1.0 1 06/11/19 08:07 75-71-8 1.0 1 06/11/19 08:07 75-34-3 1.0 1 06/11/19 08:07 107-06-2 1.0 1 06/11/19 08:07 75-35-4 1.0 1 06/11/19 08:07 156-59-2 1.0 1 06/11/19 08:07 156-60-5 1.0 1 06/11/19 08:07 78-87-5 1.0 1 06/11/19 08:07 10061-01-5 1.0 1 06/11/19 08:07 10061-02-6 1.0 1 06/11/19 08:07 100-41-4 5.0 1 06/11/19 08:07 591-78-6 20.0 1 06/11/19 08:07 74-88-4 5.0 1 06/11/19 08:07 75-09-2 5.0 1 06/11/19 08:07 108-10-1 1.0 1 06/11/19 08:07 100-42-5 1.0 1 06/11/19 08:07 630-20-6 1.0 1 06/11/19 08:07 79-34-5 1.0 1 06/11/19 08:07 127-18-4 10.0 1 06/11/19 08:07 109-99-9 1.0 1 06/11/19 08:07 108-88-3 1.0 1 06/11/19 08:07 71-55-6 1.0 1 06/11/19 08:07 79-00-5 1.0 1 06/11/19 08:07 79-01-6 1.0 1 06/11/19 08:07 75-69-4 1.0 1 06/11/19 08:07 96-18-4 2.0 1 06/11/19 08:07 108-05-4 1.0 1 06/11/19 08:07 75-01-4 2.0 1 06/11/19 08:07 179601-23-1 1.0 1 06/11/19 08:07 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06/11/19 08:07 460-00-4 06/11/19 08:07 17060-07-0 06/11/19 08:07 2037-26-5 Page 26 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-5R Lab ID: 92431068012 Collected: 05/31/19 11:28 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 14:50 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 96 % 50-150 1 06/05/19 14:50 17060-07-0 Toluene-d8 (S) 105 % 50-150 1 06/05/19 14:50 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 08:25 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 08:25 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 08:25 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 08:25 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 08:25 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 08:25 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 08:25 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 08:25 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 08:25 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 08:25 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 08:25 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 08:25 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 08:25 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 08:25 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 08:25 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 08:25 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 08:25 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 08:25 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 08:25 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 08:25 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 08:25 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 08:25 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 08:25 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 08:25 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 08:25 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 08:25 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 08:25 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 08:25 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 08:25 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 08:25 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 08:25 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 08:25 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 08:25 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 08:25 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 08:25 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 08:25 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 08:25 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 08:25 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 08:25 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 08:25 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 08:25 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-5R Lab ID: 92431068012 Collected: 05/31/19 11:28 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 08:25 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 08:25 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 08:25 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 08:25 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 08:25 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 08:25 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 08:25 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 08:25 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 08:25 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 06/11/19 08:25 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/11/19 08:25 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 06/11/19 08:25 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-7 Lab ID: 92431068013 Collected: 05/31/19 08:52 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV Low Level Landfill Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 309-00-2 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 319-84-6 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 319-86-8 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 72-54-8 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 50-29-3 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 959-98-8 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 33213-65-9 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 72-20-8 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 7421-93-4 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 76-44-8 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 18:48 1024-57-3 ND ug/L 0.15 1 06/05/19 20:42 06/07/19 18:48 72-43-5 37 % 118 % Analytical Method: EPA 8260E Mod. 2.OJ ug/L 100 % 108 % Analytical Method: EPA 8260D 10-130 1 06/05/19 20:42 06/07/19 18:48 877-09-8 10-130 1 06/05/19 20:42 06/07/19 18:48 2051-24-3 2.0 1 06/05/19 15:09 123-91-1 50-150 1 06/05/19 15:09 17060-07-0 50-150 1 06/05/19 15:09 2037-26-5 Acetone ND ug/L 25.0 1 06/11/19 08:42 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 08:42 107-13-1 Benzene 0.68J ug/L 1.0 1 06/11/19 08:42 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 08:42 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 08:42 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 08:42 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 08:42 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 08:42 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 08:42 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 08:42 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 08:42 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 08:42 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 08:42 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 08:42 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 08:42 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 08:42 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 08:42 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 08:42 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 08:42 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 08:42 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 08:42 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 08:42 75-71-8 1,1-Dichloroethane 1.3 ug/L 1.0 1 06/11/19 08:42 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 08:42 107-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-7 Lab ID: 92431068013 Collected: 05/31/19 08:52 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 06/11/2019 04:30 PM Analytical Method: EPA 8260D ND ug/L 1.5 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 4.3J ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 80.4 ug/L ND ug/L ND ug/L ND ug/L ND ug/L 2.0 ug/L ND ug/L ND ug/L ND ug/L 1.0J ug/L 0.68J ug/L 97 % 101 % 99 % 1.0 1 06/11/19 08:42 75-35-4 1.0 1 06/11/19 08:42 156-59-2 1.0 1 06/11/19 08:42 156-60-5 1.0 1 06/11/19 08:42 78-87-5 1.0 1 06/11/19 08:42 10061-01-5 1.0 1 06/11/19 08:42 10061-02-6 1.0 1 06/11/19 08:42 100-41-4 5.0 1 06/11/19 08:42 591-78-6 20.0 1 06/11/19 08:42 74-88-4 5.0 1 06/11/19 08:42 75-09-2 5.0 1 06/11/19 08:42 108-10-1 1.0 1 06/11/19 08:42 100-42-5 1.0 1 06/11/19 08:42 630-20-6 1.0 1 06/11/19 08:42 79-34-5 1.0 1 06/11/19 08:42 127-18-4 10.0 1 06/11/19 08:42 109-99-9 1.0 1 06/11/19 08:42 108-88-3 1.0 1 06/11/19 08:42 71-55-6 1.0 1 06/11/19 08:42 79-00-5 1.0 1 06/11/19 08:42 79-01-6 1.0 1 06/11/19 08:42 75-69-4 1.0 1 06/11/19 08:42 96-18-4 2.0 1 06/11/19 08:42 108-05-4 1.0 1 06/11/19 08:42 75-01-4 2.0 1 06/11/19 08:42 179601-23-1 1.0 1 06/11/19 08:42 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06/11/19 08:42 460-00-4 06/11/19 08:42 17060-07-0 06/11/19 08:42 2037-26-5 Page 30 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-13 Lab ID: 92431068014 Collected: 05/31/19 08:28 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 15:28 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 95 % 50-150 1 06/05/19 15:28 17060-07-0 Toluene-d8 (S) 106 % 50-150 1 06/05/19 15:28 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 08:59 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 08:59 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 08:59 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 08:59 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 08:59 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 08:59 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 08:59 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 08:59 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 08:59 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 08:59 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 08:59 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 08:59 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 08:59 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 08:59 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 08:59 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 08:59 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 08:59 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 08:59 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 08:59 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 08:59 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 08:59 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 08:59 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 08:59 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 08:59 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 08:59 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 08:59 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 08:59 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 08:59 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 08:59 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 08:59 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 08:59 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 08:59 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 08:59 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 08:59 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 08:59 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 08:59 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 08:59 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 08:59 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 08:59 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 08:59 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 08:59 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-13 Lab ID: 92431068014 Collected: 05/31/19 08:28 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 08:59 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 08:59 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 08:59 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 08:59 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 08:59 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 08:59 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 08:59 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 08:59 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 08:59 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 06/11/19 08:59 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/11/19 08:59 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/11/19 08:59 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-15 Lab ID: 92431068015 Collected: 05/31/19 13:42 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Aldrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 309-00-2 alpha-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 319-84-6 delta-BHC ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 319-86-8 4,4'-DDD ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 72-54-8 4,4'-DDT ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 50-29-3 Endosulfan I ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 959-98-8 Endosulfan 11 ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 33213-65-9 Endrin ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 72-20-8 Endrin aldehyde ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 7421-93-4 Heptachlor ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 76-44-8 Heptachlor epoxide ND ug/L 0.050 1 06/05/19 20:42 06/07/19 19:01 1024-57-3 Methoxychlor ND ug/L 0.15 1 06/05/19 20:42 06/07/19 19:01 72-43-5 Surrogates Tetrachloro-m-xylene (S) 77 % 10-130 1 06/05/19 20:42 06/07/19 19:01 877-09-8 Decachlorobiphenyl (S) 108 % 10-130 1 06/05/19 20:42 06/07/19 19:01 2051-24-3 8151A Cl Acid Herbicide Waters Analytical Method: EPA 8151A Preparation Method: EPA 8151A 2,4-D ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:52 94-75-7 Dalapon ND ug/L 10.0 1 06/06/19 11:10 06/10/19 21:52 75-99-0 2,4-DB ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:52 94-82-6 Dicamba ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:52 1918-00-9 Dichloroprop ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:52 120-36-5 Dinoseb ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:52 88-85-7 MCPA ND ug/L 1000 1 06/06/19 11:10 06/10/19 21:52 94-74-6 MCPP ND ug/L 1000 1 06/06/19 11:10 06/10/19 21:52 7085-19-0 2,4,5-T ND ug/L 5.0 1 06/06/19 11:10 06/10/19 21:52 93-76-5 2,4,5-TP (Silvex) ND ug/L 10.0 1 06/06/19 11:10 06/10/19 21:52 93-72-1 Surrogates 2,4-DCAA (S) 106 %. 10-155 1 06/06/19 11:10 06/10/19 21:52 19719-28-9 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 15:48 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 15:48 17060-07-0 Toluene-d8 (S) 106 % 50-150 1 06/05/19 15:48 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 09:17 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 09:17 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 09:17 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 09:17 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 09:17 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 09:17 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 09:17 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 09:17 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 09:17 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 09:17 56-23-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: MW-15 Lab ID: 92431068015 Collected: 05/31/19 13:42 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Date: 06/11/2019 04:30 PM Analytical Method: EPA 8260D ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 9.2J ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 96 % 103 % 99 % 1.0 1 06/11/19 09:17 108-90-7 1.0 1 06/11/19 09:17 75-00-3 5.0 1 06/11/19 09:17 67-66-3 1.0 1 06/11/19 09:17 74-87-3 5.0 1 06/11/19 09:17 96-12-8 1.0 1 06/11/19 09:17 124-48-1 1.0 1 06/11/19 09:17 106-93-4 1.0 1 06/11/19 09:17 74-95-3 1.0 1 06/11/19 09:17 95-50-1 1.0 1 06/11/19 09:17 106-46-7 1.0 1 06/11/19 09:17 110-57-6 1.0 1 06/11/19 09:17 75-71-8 1.0 1 06/11/19 09:17 75-34-3 1.0 1 06/11/19 09:17 107-06-2 1.0 1 06/11/19 09:17 75-35-4 1.0 1 06/11/19 09:17 156-59-2 1.0 1 06/11/19 09:17 156-60-5 1.0 1 06/11/19 09:17 78-87-5 1.0 1 06/11/19 09:17 10061-01-5 1.0 1 06/11/19 09:17 10061-02-6 1.0 1 06/11/19 09:17 100-41-4 5.0 1 06/11/19 09:17 591-78-6 20.0 1 06/11/19 09:17 74-88-4 5.0 1 06/11/19 09:17 75-09-2 5.0 1 06/11/19 09:17 108-10-1 1.0 1 06/11/19 09:17 100-42-5 1.0 1 06/11/19 09:17 630-20-6 1.0 1 06/11/19 09:17 79-34-5 1.0 1 06/11/19 09:17 127-18-4 10.0 1 06/11/19 09:17 109-99-9 1.0 1 06/11/19 09:17 108-88-3 1.0 1 06/11/19 09:17 71-55-6 1.0 1 06/11/19 09:17 79-00-5 1.0 1 06/11/19 09:17 79-01-6 1.0 1 06/11/19 09:17 75-69-4 1.0 1 06/11/19 09:17 96-18-4 2.0 1 06/11/19 09:17 108-05-4 1.0 1 06/11/19 09:17 75-01-4 2.0 1 06/11/19 09:17 179601-23-1 1.0 1 06/11/19 09:17 95-47-6 70-130 1 70-130 1 70-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 06/11/19 09:17 460-00-4 06/11/19 09:17 17060-07-0 06/11/19 09:17 2037-26-5 Page 34 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-1 Lab ID: 92431068016 Collected: 05/30/19 15:45 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 16:07 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 16:07 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 06/05/19 16:07 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 09:34 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 09:34 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 09:34 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 09:34 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 09:34 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 09:34 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 09:34 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 09:34 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 09:34 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 09:34 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 09:34 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 09:34 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 09:34 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 09:34 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 09:34 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 09:34 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 09:34 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 09:34 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 09:34 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 09:34 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 09:34 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 09:34 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 09:34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 09:34 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 09:34 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 09:34 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 09:34 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 09:34 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 09:34 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 09:34 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 09:34 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 09:34 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 09:34 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 09:34 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 09:34 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 09:34 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 09:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 09:34 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 09:34 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 09:34 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 09:34 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-1 Lab ID: 92431068016 Collected: 05/30/19 15:45 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 09:34 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 09:34 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 09:34 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 09:34 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 09:34 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 09:34 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 09:34 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 09:34 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 09:34 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 06/11/19 09:34 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/11/19 09:34 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 06/11/19 09:34 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-2 Lab ID: 92431068017 Collected: 05/30/19 14:35 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) 1.3J ug/L 2.0 1 06/05/19 16:26 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 16:26 17060-07-0 Toluene-d8 (S) 106 % 50-150 1 06/05/19 16:26 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 09:52 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 09:52 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 09:52 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 09:52 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 09:52 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 09:52 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 09:52 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 09:52 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 09:52 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 09:52 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 09:52 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 09:52 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 09:52 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 09:52 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 09:52 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 09:52 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 09:52 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 09:52 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 09:52 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 09:52 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 09:52 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 09:52 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 09:52 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 09:52 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 09:52 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 09:52 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 09:52 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 09:52 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 09:52 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 09:52 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 09:52 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 09:52 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 09:52 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 09:52 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 09:52 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 09:52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 09:52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 09:52 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 09:52 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 09:52 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 09:52 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-2 Lab ID: 92431068017 Collected: 05/30/19 14:35 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 09:52 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 09:52 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 09:52 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 09:52 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 09:52 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 09:52 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 09:52 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 09:52 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 09:52 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 06/11/19 09:52 460-00-4 1,2-Dichloroethane-d4 (S) 101 % 70-130 1 06/11/19 09:52 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/11/19 09:52 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 38 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-3 Lab ID: 92431068018 Collected: 05/30/19 15:25 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) 1.3J ug/L 2.0 1 06/05/19 16:45 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 100 % 50-150 1 06/05/19 16:45 17060-07-0 Toluene-d8 (S) 108 % 50-150 1 06/05/19 16:45 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 10:09 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 10:09 107-13-1 Benzene 0.73J ug/L 1.0 1 06/11/19 10:09 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 10:09 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 10:09 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 10:09 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 10:09 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 10:09 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 10:09 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 10:09 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 10:09 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 10:09 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 10:09 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 10:09 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 10:09 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 10:09 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 10:09 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 10:09 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 10:09 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 10:09 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 10:09 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 10:09 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 10:09 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 10:09 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 10:09 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 10:09 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 10:09 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 10:09 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 10:09 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 10:09 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 10:09 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 10:09 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 10:09 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 10:09 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 10:09 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 10:09 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 10:09 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 10:09 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 10:09 127-18-4 Tetrahydrofuran 6.1J ug/L 10.0 1 06/11/19 10:09 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 10:09 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-3 Lab ID: 92431068018 Collected: 05/30/19 15:25 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 10:09 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 10:09 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 10:09 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 10:09 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 10:09 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 10:09 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 10:09 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 10:09 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 10:09 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 06/11/19 10:09 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/11/19 10:09 17060-07-0 Toluene-d8 (S) 101 % 70-130 1 06/11/19 10:09 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 40 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-4 Lab ID: 92431068019 Collected: 05/30/19 14:56 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 17:04 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 17:04 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 06/05/19 17:04 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone ND ug/L 25.0 1 06/11/19 10:44 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 10:44 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 10:44 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 10:44 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 10:44 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 10:44 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 10:44 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 10:44 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 10:44 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 10:44 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 10:44 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 10:44 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 10:44 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 10:44 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 10:44 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 10:44 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 10:44 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 10:44 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 10:44 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 10:44 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 10:44 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 10:44 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 10:44 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 10:44 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 10:44 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 10:44 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 10:44 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 10:44 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 10:44 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 10:44 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 10:44 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 10:44 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 10:44 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 10:44 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 10:44 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 10:44 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 10:44 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 10:44 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 10:44 127-18-4 Tetrahydrofuran 13.7 ug/L 10.0 1 06/11/19 10:44 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 10:44 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: SW-4 Lab ID: 92431068019 Collected: 05/30/19 14:56 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 10:44 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 10:44 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 10:44 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 10:44 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 10:44 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 10:44 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 10:44 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 10:44 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 10:44 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 06/11/19 10:44 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 06/11/19 10:44 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 06/11/19 10:44 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 42 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: EQUIPMENT BLANK Lab ID: 92431068020 Collected: 05/31/19 17:45 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Analytical Method: EPA 8260E Mod 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 06/05/19 17:24 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 06/05/19 17:24 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 06/05/19 17:24 2037-26-5 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Acetone 10.2J ug/L 25.0 1 06/11/19 05:13 67-64-1 Acrylonitrile ND ug/L 10.0 1 06/11/19 05:13 107-13-1 Benzene ND ug/L 1.0 1 06/11/19 05:13 71-43-2 Bromochloromethane ND ug/L 1.0 1 06/11/19 05:13 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/11/19 05:13 75-27-4 Bromoform ND ug/L 1.0 1 06/11/19 05:13 75-25-2 Bromomethane ND ug/L 2.0 1 06/11/19 05:13 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 06/11/19 05:13 78-93-3 Carbon disulfide ND ug/L 2.0 1 06/11/19 05:13 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 06/11/19 05:13 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/11/19 05:13 108-90-7 Chloroethane ND ug/L 1.0 1 06/11/19 05:13 75-00-3 Chloroform ND ug/L 5.0 1 06/11/19 05:13 67-66-3 Chloromethane ND ug/L 1.0 1 06/11/19 05:13 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 1 06/11/19 05:13 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/11/19 05:13 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 06/11/19 05:13 106-93-4 Dibromomethane ND ug/L 1.0 1 06/11/19 05:13 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/11/19 05:13 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/11/19 05:13 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 06/11/19 05:13 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 06/11/19 05:13 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/11/19 05:13 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/11/19 05:13 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/11/19 05:13 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 05:13 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/11/19 05:13 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/11/19 05:13 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 05:13 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 06/11/19 05:13 10061-02-6 Ethylbenzene ND ug/L 1.0 1 06/11/19 05:13 100-41-4 2-Hexanone ND ug/L 5.0 1 06/11/19 05:13 591-78-6 lodomethane ND ug/L 20.0 1 06/11/19 05:13 74-88-4 Methylene Chloride ND ug/L 5.0 1 06/11/19 05:13 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 06/11/19 05:13 108-10-1 Styrene ND ug/L 1.0 1 06/11/19 05:13 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 05:13 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/11/19 05:13 79-34-5 Tetrachloroethene ND ug/L 1.0 1 06/11/19 05:13 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 06/11/19 05:13 109-99-9 Toluene ND ug/L 1.0 1 06/11/19 05:13 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92431068 Sample: EQUIPMENT BLANK Lab ID: 92431068020 Collected: 05/31/19 17:45 Received: 05/31/19 17:51 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D 1,1,1-Trichloroethane ND ug/L 1.0 1 06/11/19 05:13 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/11/19 05:13 79-00-5 Trichloroethene ND ug/L 1.0 1 06/11/19 05:13 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/11/19 05:13 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/11/19 05:13 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/11/19 05:13 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/11/19 05:13 75-01-4 m&p-Xylene ND ug/L 2.0 1 06/11/19 05:13 179601-23-1 o-Xylene ND ug/L 1.0 1 06/11/19 05:13 95-47-6 Surrogates 4-Bromofluorobenzene (S) 98 % 70-130 1 06/11/19 05:13 460-00-4 1,2-Dichloroethane-d4 (S) 99 % 70-130 1 06/11/19 05:13 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 06/11/19 05:13 2037-26-5 Date: 06/11/2019 04:30 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 44 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 QC Batch: 479013 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 92431068001, 92431068002, 92431068003, 92431068004, 92431068005, 92431068008, 92431068009, 92431068010,92431068011,92431068012,92431068013,92431068014,92431068015,92431068016, 92431068017,92431068018,92431068019,92431068020 METHOD BLANK: 2592584 Matrix: Water Associated Lab Samples: 92431068001, 92431068002, 92431068003, 92431068004, 92431068005, 92431068008, 92431068009, 92431068010,92431068011,92431068012,92431068013,92431068014,92431068015,92431068016, 92431068017,92431068018,92431068019,92431068020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 06/05/19 12:15 1,2-Dichloroethane-d4 (S) % 98 50-150 06/05/19 12:15 Toluene-d8 (S) % 105 50-150 06/05/19 12:15 LABORATORY CONTROL SAMPLE: 2592585 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 18.8 94 70-130 1,2-Dichloroethane-d4 (S) % 98 50-150 Toluene-d8(S) % 105 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2592586 2592587 MS MSD 92431068019 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 21.2 19.5 101 92 50-150 8 1,2-Dichloroethane-d4 (S) % 103 102 50-150 Toluene-d8(S) % 108 108 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 QC Batch: 479727 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 92431068006 METHOD BLANK: 2596094 Associated Lab Samples: 92431068006 Parameter Units 1,4-Dioxane (p-Dioxane) ug/L 1,2-Dichloroethane-d4 (S) % Toluene-d8 (S) % Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 06/07/1910:57 96 50-150 06/07/1910:57 107 50-150 06/07/1910:57 LABORATORY CONTROL SAMPLE: 2596095 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.0 95 70-130 1,2-Dichloroethane-d4 (S) % 100 50-150 Toluene-d8(S) % 107 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2596158 2596159 MS MSD 92431892010 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane(p-Dioxane) ug/L 2.5 20 20 19.5 20.0 85 87 50-150 2 1,2-Dichloroethane-d4 (S) % 100 98 50-150 Toluene-d8(S) % 112 109 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 QC Batch: 480198 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Associated Lab Samples: 92431068001, 92431068002, 92431068003, 92431068004, 92431068005, 92431068006, 92431068007, 92431068008,92431068009,92431068010,92431068011,92431068012,92431068013,92431068014, 92431068015,92431068016,92431068017,92431068018,92431068019,92431068020 METHOD BLANK: 2598328 Matrix: Water Associated Lab Samples: 92431068001, 92431068002, 92431068003, 92431068004, 92431068005, 92431068006, 92431068007, 92431068008,92431068009,92431068010,92431068011,92431068012,92431068013,92431068014, 92431068015,92431068016,92431068017,92431068018,92431068019,92431068020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/11/19 04:38 1,1,1-Trichloroethane ug/L ND 1.0 06/11/19 04:38 1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/11/19 04:38 1,1,2-Trichloroethane ug/L ND 1.0 06/11/19 04:38 1,1-Dichloroethane ug/L ND 1.0 06/11/19 04:38 1,1-Dichloroethene ug/L ND 1.0 06/11/19 04:38 1,2,3-Trichloropropane ug/L ND 1.0 06/11/19 04:38 1,2-Dibromo-3-chloropropane ug/L ND 5.0 06/11/19 04:38 1,2-Dibromoethane (EDB) ug/L ND 1.0 06/11/19 04:38 1,2-Dichlorobenzene ug/L ND 1.0 06/11/19 04:38 1,2-Dichloroethane ug/L ND 1.0 06/11/19 04:38 1,2-Dichloropropane ug/L ND 1.0 06/11/19 04:38 1,4-Dichlorobenzene ug/L ND 1.0 06/11/19 04:38 2-Butanone (MEK) ug/L ND 5.0 06/11/19 04:38 2-Hexanone ug/L ND 5.0 06/11/19 04:38 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 06/11/19 04:38 Acetone ug/L ND 25.0 06/11/19 04:38 Acrylonitrile ug/L ND 10.0 06/11/19 04:38 Benzene ug/L ND 1.0 06/11/19 04:38 Bromochloromethane ug/L ND 1.0 06/11/19 04:38 Bromodichloromethane ug/L ND 1.0 06/11/19 04:38 Bromoform ug/L ND 1.0 06/11/19 04:38 Bromomethane ug/L ND 2.0 06/11/19 04:38 Carbon disulfide ug/L ND 2.0 06/11/19 04:38 Carbon tetrachloride ug/L ND 1.0 06/11/19 04:38 Chlorobenzene ug/L ND 1.0 06/11/19 04:38 Chloroethane ug/L ND 1.0 06/11/19 04:38 Chloroform ug/L ND 5.0 06/11/19 04:38 Chloromethane ug/L ND 1.0 06/11/19 04:38 cis-1,2-Dichloroethene ug/L ND 1.0 06/11/19 04:38 cis-1,3-Dichloropropene ug/L ND 1.0 06/11/19 04:38 Dibromochloromethane ug/L ND 1.0 06/11/19 04:38 Dibromomethane ug/L ND 1.0 06/11/19 04:38 Dichlorodifluoromethane ug/L ND 1.0 06/11/19 04:38 Ethylbenzene ug/L ND 1.0 06/11/19 04:38 lodomethane ug/L ND 20.0 06/11/19 04:38 m&p-Xylene ug/L ND 2.0 06/11/19 04:38 Methylene Chloride ug/L ND 5.0 06/11/19 04:38 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 METHOD BLANK: 2598328 Matrix: Water Associated Lab Samples: 92431068001, 92431068002, 92431068003, 92431068004, 92431068005, 92431068006, 92431068007, 92431068008,92431068009,92431068010,92431068011,92431068012,92431068013,92431068014, 92431068015,92431068016,92431068017,92431068018,92431068019,92431068020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers o-Xylene ug/L ND 1.0 06/11/19 04:38 Styrene ug/L ND 1.0 06/11/19 04:38 Tetrachloroethene ug/L ND 1.0 06/11/19 04:38 Tetrahydrofuran ug/L ND 10.0 06/11/19 04:38 Toluene ug/L ND 1.0 06/11/19 04:38 trans-1,2-Dichloroethene ug/L ND 1.0 06/11/19 04:38 trans- 1,3-Dichloropropene ug/L ND 1.0 06/11/19 04:38 trans-1,4-Dichloro-2-butene ug/L ND 1.0 06/11/19 04:38 Trichloroethene ug/L ND 1.0 06/11/19 04:38 Trichlorofluoromethane ug/L ND 1.0 06/11/19 04:38 Vinyl acetate ug/L ND 2.0 06/11/19 04:38 Vinyl chloride ug/L ND 1.0 06/11/19 04:38 1,2-Dichloroethane-d4 (S) % 101 70-130 06/11/19 04:38 4-Bromofluorobenzene (S) % 97 70-130 06/11/19 04:38 Toluene-d8 (S) % 98 70-130 06/11/19 04:38 LABORATORY CONTROL SAMPLE: Parameter 2598329 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 50.8 102 70-130 1,1,1-Trichloroethane ug/L 50 47.1 94 70-130 1,1,2,2-Tetrachloroethane ug/L 50 47.4 95 70-130 1,1,2-Trichloroethane ug/L 50 48.7 97 70-130 1,1-Dichloroethane ug/L 50 46.9 94 70-130 1,1-Dichloroethene ug/L 50 48.5 97 70-130 1,2,3-Trichloropropane ug/L 50 47.3 95 70-130 1,2-Dibromo-3-chloropropane ug/L 50 50.9 102 70-130 1,2-Dibromoethane (EDB) ug/L 50 47.5 95 70-130 1,2-Dichlorobenzene ug/L 50 46.6 93 70-130 1,2-Dichloroethane ug/L 50 46.0 92 70-130 1,2-Dichloropropane ug/L 50 46.3 93 70-130 1,4-Dichlorobenzene ug/L 50 46.0 92 70-130 2-Butanone (MEK) ug/L 100 103 103 64-135 2-Hexanone ug/L 100 100 100 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 96.8 97 70-130 Acetone ug/L 100 111 111 61-157 Acrylonitrile ug/L 250 238 95 61-143 Benzene ug/L 50 46.2 92 70-130 Bromochloromethane ug/L 50 48.0 96 70-130 Bromodichloromethane ug/L 50 48.9 98 70-130 Bromoform ug/L 50 51.4 103 70-130 Bromomethane ug/L 50 51.6 103 38-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 LABORATORY CONTROL SAMPLE: Parameter 2598329 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Carbon disulfide ug/L 50 46.4 93 68-130 Carbon tetrachloride ug/L 50 45.8 92 70-130 Chlorobenzene ug/L 50 45.5 91 70-130 Chloroethane ug/L 50 54.1 108 37-142 Chloroform ug/L 50 47.0 94 70-130 Chloromethane ug/L 50 44.6 89 48-130 cis-1,2-Dichloroethene ug/L 50 47.2 94 70-130 cis-1,3-Dichloropropene ug/L 50 47.9 96 70-130 Dibromochloromethane ug/L 50 51.4 103 70-130 Dibromomethane ug/L 50 49.0 98 70-130 Dichlorodifluoromethane ug/L 50 42.6 85 53-134 Ethylbenzene ug/L 50 47.0 94 70-130 lodomethane ug/L 100 100 100 40-130 m&p-Xylene ug/L 100 94.0 94 70-130 Methylene Chloride ug/L 50 47.4 95 67-132 o-Xylene ug/L 50 47.0 94 70-131 Styrene ug/L 50 47.7 95 70-130 Tetrachloroethene ug/L 50 45.7 91 69-130 Tetrahydrofuran ug/L 500 490 98 62-130 Toluene ug/L 50 45.7 91 70-130 trans-1,2-Dichloroethene ug/L 50 47.2 94 70-130 trans- 1,3-Dichloropropene ug/L 50 46.9 94 70-130 trans-1,4-Dichloro-2-butene ug/L 50 71.7 143 35-189 Trichloroethene ug/L 50 45.7 91 70-130 Trichlorofluoromethane ug/L 50 47.9 96 63-130 Vinyl acetate ug/L 100 99.4 99 55-143 Vinyl chloride ug/L 50 45.9 92 70-131 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 98 70-130 Qualifiers MATRIX SPIKE SAMPLE: Parameter 2598331 Units 92431068019 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 20.2 101 73-134 1,1,1-Trichloroethane ug/L ND 20 20.7 104 82-143 1,1,2,2-Tetrachloroethane ug/L ND 20 19.9 99 70-136 1,1,2-Trichloroethane ug/L ND 20 20.2 101 70-135 1,1-Dichloroethane ug/L ND 20 20.8 104 70-139 1,1-Dichloroethene ug/L ND 20 21.5 108 70-154 1,2,3-Trichloropropane ug/L ND 20 19.4 97 71-137 1,2-Dibromo-3-chloropropane ug/L ND 20 18.4 92 65-134 1,2-Dibromoethane (EDB) ug/L ND 20 19.8 99 70-137 1,2-Dichlorobenzene ug/L ND 20 18.9 94 70-133 1,2-Dichloroethane ug/L ND 20 19.1 96 70-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 68 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 MATRIX SPIKE SAMPLE: 2598331 92431068019 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2-Dichloropropane ug/L ND 20 19.5 98 70-140 1,4-Dichlorobenzene ug/L ND 20 18.8 94 70-133 2-Butanone (MEK) ug/L ND 40 43.9 110 60-139 2-Hexanone ug/L ND 40 39.4 99 65-138 4-Methyl-2-pentanone (MIBK) ug/L ND 40 39.0 97 65-135 Acetone ug/L ND 40 50.0 125 60-148 Acrylonitrile ug/L ND 100 100 100 64-147 Benzene ug/L ND 20 20.0 100 70-151 Bromochloromethane ug/L ND 20 20.9 104 70-141 Bromodichloromethane ug/L ND 20 19.2 96 70-138 Bromoform ug/L ND 20 17.4 87 63-130 Bromomethane ug/L ND 20 11.8 59 15-152 Carbon disulfide ug/L ND 20 20.5 102 69-149 Carbon tetrachloride ug/L ND 20 19.6 98 70-143 Chlorobenzene ug/L ND 20 19.1 95 70-138 Chloroethane ug/L ND 20 22.6 113 52-163 Chloroform ug/L ND 20 20.5 102 70-139 Chloromethane ug/L ND 20 20.4 102 41-139 cis-1,2-Dichloroethene ug/L ND 20 20.7 104 70-141 cis-1,3-Dichloropropene ug/L ND 20 18.6 93 70-137 Dibromochloromethane ug/L ND 20 18.8 94 70-134 Dibromomethane ug/L ND 20 20.0 100 70-138 Dichlorodifluoromethane ug/L ND 20 19.9 100 47-155 Ethylbenzene ug/L ND 20 19.8 99 66-153 lodomethane ug/L ND 40 35.0 88 20-138 m&p-Xylene ug/L ND 40 39.2 98 69-152 Methylene Chloride ug/L ND 20 19.3 96 42-159 o-Xylene ug/L ND 20 19.9 99 70-148 Styrene ug/L ND 20 19.4 97 70-135 Tetrachloroethene ug/L ND 20 19.6 98 59-143 Tetrahydrofuran ug/L 13.7 200 216 101 70-133 Toluene ug/L ND 20 19.2 96 59-148 trans-1,2-Dichloroethene ug/L ND 20 20.7 103 70-146 trans- 1,3-Dichloropropene ug/L ND 20 17.5 87 70-135 trans-1,4-Dichloro-2-butene ug/L ND 20 14.2 71 47-135 Trichloroethene ug/L ND 20 20.0 100 70-147 Trichlorofluoromethane ug/L ND 20 20.7 103 70-148 Vinyl acetate ug/L ND 40 28.8 72 49-151 Vinyl chloride ug/L ND 20 21.1 106 70-156 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 100 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 SAMPLE DUPLICATE: 2598330 Parameter Units 92431068018 Result Dup Result 1,1,1,2-Tetrachloroethane ug/L ND ND 1,1,1-Trichloroethane ug/L ND ND 1,1,2,2-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,2,3-Trichloropropane ug/L ND ND 1,2-Dibromo-3-chloropropane ug/L ND ND 1,2-Dibromoethane (EDB) ug/L ND ND 1,2-Dichlorobenzene ug/L ND ND 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND ND 1,4-Dichlorobenzene ug/L ND ND 2-Butanone (MEK) ug/L ND ND 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L 0.73J 0.66J Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Dichlorodifluoromethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND m&p-Xylene ug/L ND ND Methylene Chloride ug/L ND ND o-Xylene ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Tetrahydrofuran ug/L 6.1 J 5.6J Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 SAMPLE DUPLICATE: 2598330 92431068018 Dup Parameter Units Result Result RPD Qualifiers Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND 1,2-Dichloroethane-d4 (S) % 102 103 4-Bromofluorobenzene (S) % 98 98 Toluene-d8(S) % 101 99 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 QC Batch: 478862 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Associated Lab Samples: 92431068003 METHOD BLANK: 2591861 Associated Lab Samples: 92431068003 Parameter Units 4,4'-DDD ug/L 4,4'-DDT ug/L Aldrin ug/L alpha-BHC ug/L delta-BHC ug/L Endosulfan I ug/L Endosulfan 11 ug/L Endrin ug/L Endrin aldehyde ug/L Heptachlor ug/L Heptachlor epoxide ug/L Methoxychlor ug/L Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % Matrix: Water Blank Result Reporting Limit Analyzed ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.050 06/07/19 23:29 ND 0.15 06/07/19 23:29 96 10-130 06/07/19 23:29 70 10-130 06/07/19 23:29 LABORATORY CONTROL SAMPLE: Parameter 2591862 Units Spike Conc. LCS Result 4,4'-DDD ug/L 0.25 0.20 4,4'-DDT ug/L 0.25 0.22 Aldrin ug/L 0.25 0.18 alpha-BHC ug/L 0.25 0.20 delta-BHC ug/L 0.25 0.20 Endosulfan I ug/L 0.25 0.21 Endosulfan II ug/L 0.25 0.22 Endrin ug/L 0.25 0.21 Endrin aldehyde ug/L 0.25 0.42 Heptachlor ug/L 0.25 0.20 Heptachlor epoxide ug/L 0.25 0.19 Methoxychlor ug/L 0.74 0.80 Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % Qualifiers LCS % Rec % Rec Limits Qualifiers 81 49-130 89 45-130 73 25-130 81 53-130 82 54-130 85 43-130 88 64-130 84 56-130 171 59-130 L1 81 37-130 76 56-130 108 46-130 97 10-130 76 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 QC Batch: 479295 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Associated Lab Samples: 92431068008, 92431068009, 92431068011, 92431068013, 92431068015 METHOD BLANK: 2593946 Matrix: Water Associated Lab Samples: 92431068008, 92431068009, 92431068011, 92431068013, 92431068015 Blank Reporting Parameter Units Result Limit Analyzed 4,4'-DDD ug/L ND 0.050 06/07/19 21:21 4,4'-DDT ug/L ND 0.050 06/07/19 21:21 Aldrin ug/L ND 0.050 06/07/19 21:21 alpha-BHC ug/L ND 0.050 06/07/19 21:21 delta-BHC ug/L ND 0.050 06/07/19 21:21 Endosulfan I ug/L ND 0.050 06/07/19 21:21 Endosulfan 11 ug/L ND 0.050 06/07/19 21:21 Endrin ug/L ND 0.050 06/07/19 21:21 Endrin aldehyde ug/L ND 0.050 06/07/19 21:21 Heptachlor ug/L ND 0.050 06/07/19 21:21 Heptachlor epoxide ug/L ND 0.050 06/07/19 21:21 Methoxychlor ug/L ND 0.15 06/07/19 21:21 Decachlorobiphenyl (S) % 85 10-130 06/07/19 21:21 Tetrachloro-m-xylene (S) % 87 10-130 06/07/19 21:21 LABORATORY CONTROL SAMPLE: Parameter 2593947 Units Spike Conc. LCS LCS Result % Rec 4,4'-DDD ug/L 0.25 0.28 4,4'-DDT ug/L 0.25 0.25 Aldrin ug/L 0.25 0.095 alpha-BHC ug/L 0.25 0.24 delta-BHC ug/L 0.25 0.23 Endosulfan I ug/L 0.25 0.24 Endosulfan II ug/L 0.25 0.25 Endrin ug/L 0.25 0.24 Endrin aldehyde ug/L 0.25 0.23 Heptachlor ug/L 0.25 0.16 Heptachlor epoxide ug/L 0.25 0.22 Methoxychlor ug/L 0.75 0.84 Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % Qualifiers % Rec Limits 114 49-130 102 45-130 38 25-130 94 53-130 93 54-130 97 43-130 101 64-130 94 56-130 93 59-130 62 37-130 89 56-130 112 46-130 114 10-130 90 10-130 Qualifiers 92431068008 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L ND 0.25 0.32 128 28-130 4,4'-DDT ug/L ND 0.25 0.33 131 11-130 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 MATRIX SPIKE SAMPLE: 2593948 92431068008 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Aldrin ug/L ND 0.25 0.14 56 10-130 alpha-BHC ug/L ND 0.25 0.25 100 27-130 delta-BHC ug/L ND 0.25 0.15 58 44-130 Endosulfan I ug/L ND 0.25 0.23 90 10-139 Endosulfan II ug/L ND 0.25 0.27 108 36-130 Endrin ug/L ND 0.25 0.25 98 26-130 Endrin aldehyde ug/L ND 0.25 0.34 134 19-160 Heptachlor ug/L ND 0.25 0.45 181 25-130 M1 Heptachlor epoxide ug/L ND 0.25 0.37 149 18-130 M1 Methoxychlor ug/L ND 0.75 0.89 119 10-130 Decachlorobiphenyl (S) % 117 10-130 Tetrachloro-m-xylene (S) % 36 10-130 SAMPLE DUPLICATE: 2593949 92431068009 Dup Parameter Units Result Result RPD Qualifiers 4,4'-DDD ug/L ND ND 4,4'-DDT ug/L ND ND Aldrin ug/L ND ND alpha-BHC ug/L ND ND delta-BHC ug/L ND ND Endosulfan I ug/L ND ND Endosulfan II ug/L ND ND Endrin ug/L ND ND Endrin aldehyde ug/L ND ND Heptachlor ug/L ND ND Heptachlor epoxide ug/L ND ND Methoxychlor ug/L ND ND Decachlorobiphenyl (S) % 110 102 Tetrachloro-m-xylene (S) % 78 81 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 QC Batch: 29728 Analysis Method: EPA 8151A QC Batch Method: EPA8151A Analysis Description: 8151AGCS Herbicides Associated Lab Samples: 92431068008, 92431068009, 92431068011, 92431068015 METHOD BLANK: 133791 Associated Lab Samples: Parameter Matrix: Water 92431068008, 92431068009, 92431068011, 92431068015 Blank Reporting Units Result Limit Analyzed Qualifiers 2,4,5-T ug/L ND 5.0 06/10/19 19:19 2,4,5-TP (Silvex) ug/L ND 10.0 06/10/19 19:19 2,4-D ug/L ND 5.0 06/10/19 19:19 2,4-DB ug/L ND 5.0 06/10/19 19:19 Dalapon ug/L ND 10.0 06/10/19 19:19 Dicamba ug/L ND 5.0 06/10/19 19:19 Dichloroprop ug/L ND 5.0 06/10/19 19:19 Dinoseb ug/L ND 5.0 06/10/19 19:19 MCPA ug/L ND 1000 06/10/19 19:19 MCPP ug/L ND 1000 06/10/19 19:19 2,4-DCAA (S) %. 123 10-155 06/10/19 19:19 LABORATORY CONTROL SAMPLE: Parameter 133792 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4,5-T ug/L 10 9.2 92 31-150 2,4,5-TP (Silvex) ug/L 10 9.11 91 35-138 2,4-D ug/L 10 8.9 89 29-145 2,4-DB ug/L 10 10.1 101 24-145 Dalapon ug/L 10 9.3J 93 31-120 Dicamba ug/L 10 8.5 85 45-139 Dichloroprop ug/L 10 8.8 88 54-139 Dinoseb ug/L 10 3.6J 36 10-182 MCPA ug/L 1000 1160 116 25-147 MCPP ug/L 1000 963J 96 10-169 2,4-DCAA (S) %. 123 10-155 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 133793 133794 MS MSD 92431068011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 2,4,5-T ug/L ND 10 10 7.9 11.1 79 111 10-158 34 2,4,5-TP (Silvex) ug/L ND 10 10 8.1J 11.6 81 116 10-156 2,4-D ug/L ND 10 10 8.0 10 80 100 10-156 21 2,4-DB ug/L ND 10 10 10.1 14.3 101 143 24-145 34 Dalapon ug/L ND 10 10 9.6J 11.9 96 119 31-120 Dicamba ug/L ND 10 10 8.1 10.9 81 109 45-139 30 Dichloroprop ug/L ND 10 10 7.9 11.0 79 110 54-139 32 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92431068 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 133793 133794 MS MSD 92431068011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Dinoseb ug/L ND 10 10 3.7J 11.9 37 119 10-174 MCPA ug/L ND 1000 1000 1270 976J 127 98 25-147 MCPP ug/L ND 1000 1000 877J 1020 88 102 10-169 2,4-DCAA (S) %. 114 142 10-155 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 68 Pace Analytical Services, LLC ceAnalX cal ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: OSR Pace Project No.: 92431068 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte PASI-GA Pace Analytical Services - Atlanta, GA ANALYTE QUALIFIERS L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 68 acmnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR 92431068 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92431068003 MW-10 EPA 3510C 478862 EPA 8081B 479808 92431068008 MW-1R EPA 3510C 479295 EPA 8081B 479804 92431068009 MW-2R EPA 3510C 479295 EPA 8081B 479804 92431068011 MW-4R EPA 3510C 479295 EPA 8081B 479804 92431068013 MW-7 EPA 3510C 479295 EPA 8081B 479804 92431068015 MW-15 EPA 3510C 479295 EPA 8081B 479804 92431068008 MW-1R EPA 8151A 29728 EPA 8151A 29909 92431068009 MW-2R EPA 8151A 29728 EPA 8151A 29909 92431068011 MW-4R EPA 8151A 29728 EPA 8151A 29909 92431068015 MW-15 EPA 8151A 29728 EPA 8151A 29909 92431068001 MW-8 EPA 8260B Mod. 479013 92431068002 MW-9 EPA 8260B Mod. 479013 92431068003 MW-10 EPA 8260B Mod. 479013 92431068004 MW-11 EPA 8260B Mod. 479013 92431068005 MW-12 EPA 8260B Mod. 479013 92431068006 MW-14 EPA 8260B Mod. 479727 92431068008 MW-1 R EPA 8260B Mod. 479013 92431068009 MW-2R EPA 8260B Mod. 479013 92431068010 MW-3R EPA 8260B Mod. 479013 92431068011 MW-4R EPA 8260B Mod. 479013 92431068012 MW-5R EPA 8260B Mod. 479013 92431068013 MW-7 EPA 8260B Mod. 479013 92431068014 MW-13 EPA 8260B Mod. 479013 92431068015 MW-15 EPA 8260B Mod. 479013 92431068016 SW-1 EPA 8260B Mod. 479013 92431068017 SW-2 EPA 8260B Mod. 479013 92431068018 SW-3 EPA 8260B Mod. 479013 92431068019 SW-4 EPA 8260B Mod. 479013 92431068020 EQUIPMENT BLANK EPA 8260B Mod. 479013 92431068001 MW-8 EPA 8260D 480198 92431068002 MW-9 EPA 8260D 480198 92431068003 MW-10 EPA 8260D 480198 92431068004 MW-11 EPA 8260D 480198 92431068005 MW-12 EPA 8260D 480198 92431068006 MW-14 EPA 8260D 480198 92431068007 TRIP BLANK EPA 8260D 480198 92431068008 MW-1R EPA 8260D 480198 92431068009 MW-2R EPA 8260D 480198 92431068010 MW-3R EPA 8260D 480198 92431068011 MW-4R EPA 8260D 480198 92431068012 MW-5R EPA 8260D 480198 92431068013 MW-7 EPA 8260D 480198 92431068014 MW-13 EPA 8260D 480198 92431068015 MW-15 EPA 8260D 480198 92431068016 SW-1 EPA 8260D 480198 92431068017 SW-2 EPA 8260D 480198 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11/2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Page 59 of 68 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR Pace Project No.: 92431068 Lab ID Sample ID QC Batch Method QC Batch 92431068018 SW-3 EPA 8260D 480198 92431068019 SW-4 EPA 8260D 480198 92431068020 EQUIPMENT BLANK EPA 8260D 480198 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/11 /2019 04:30 PM without the written consent of Pace Analytical Services, LLC. Analytical Analytical Method Batch Page 60 of 68 Document Name: Document Revised: February 7, 2018 m Sample Condition Upon Receipt(SCUR) Pa e 1 of 2 xeAnd"Gal Document No.: Issuing Authority: r F•CAR-CS-033-Rev.06 Pace Carolinas quality Office 3 Laboratory receiving samples: Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[] SampleCondition Client No Wp# : 92431D68 --Upon Receiptt� Project 1 Courier: ❑Fed Ex ❑UPS ❑USPS []Client ❑ Commercial ❑Pace ❑Other: 92431058 Custody Seal Present? []Yes ❑No Seats Intact? []Yes QNo Date/Initials Person Examining Contents:='Lt_�= Packing Material: [I Bubble Wrap ❑Bubble Bags ❑None ❑ Other Biological Tissue Frozen? Thermometer; ❑Yes ONo ❑N/A �y g2TQ4g Typeotice: .©wet ❑Blue ❑None nR Gun 10; Cooler Temp ('C): %�.. L _ Correction Factor: Add/Subtract (°C) 0.0 L. Temp should be above freezing to VC Cooler Temp Corrected ('C): ❑Samples out of temp criteria. Samples on ice, cooling process hasbegun USDA Hegulated5oil (© NIA, water sample) Did sarriples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source ('internationally, 111__ Chi_ inrhidinaHawaii and Puerto Rico)? ❑Yes ONO Cam ments/Discrepancy: Chain of Custody Present? ,,� [JYes [:]No ❑N/A 1, Samples Arrived within Bold Time? Mes []NO []N/A 2. Short Hold Time Anaiysls (<72 hr.)? DYes ONO ❑N/A 3, Rush Turn Around Time Requested? ❑Yes []No [IN/A 4. Sufficient Volume? C]Yes []No ❑N/A S. Correct Containers Used? -Pace Containers Used? ❑Yes ❑Yes ❑No [:]No ❑N/A ❑NIA 6. Containers Intact? QYes [:]No []N/A 7. analysis: Samples Field Filtered? ❑Yes []No ❑N/A 8. —Dissolved Sample Labels Match COC? -Includes Date/Time/1D/Analysis Matrix: I [:]Yes []No. []N/A 9. Headspace in VOA Vials (>5-Gmm)? (-]Yes ❑1 ❑N/A 10. Trip Blank Present? Trip Blank Custody Seals present? 04es (2fes []No [:]No ❑N/A ❑NIA 11. COMMENTS/SAMPLE DISCREPANCY _ f i + Lot ID ofiplit containers: CLIENT NOTIFICATION/RESOLLMON Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? []Yes ❑No Page 61 of 68 Document Name: Sample Condition Upon Rec Document No.: Document Revised: February 7, 2018 Page 1 of 2 Issuing Authority: Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions- VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project # W0# : 92431068 Phi: KLH1 Due Date: 06/13/19 CLIENT: 92-HDR m N a 0. 7 V E to N a m v n V m d E O N rn M a m d m cl V a E O -A 7 N a m Z N `! a N a v *' rl � •i 0. m ._. 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N @ ` be l7 � > U to ftl y`y ,� J E to N •~ F= tit 0 � ¢ Y 2 U v J E In 14 ry F N a kA m S Z u m J E N N 4 an d m � c y E a o O lJ a Z M 5 c O � J E O 7 4J W > 10 a 8 a C 9 4 E V 7 Q1 l7 o 1 \1V 2 4 -7 5 \\N7\\N 6 � p I 1 7 -) t_ \N 9 I \d\N\ N\\J 10 N I 11 12 I Nlls PH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon recelpt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot rr Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy at this Corm will be sent to the North Laronna ueHNlt certincauon Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 62 of 68 Sample Conditian an Receipt(SCUR} Page 1 of 2 ,�tiiG2�lCla+Y°r�� Document No.: IssvingAuthority: F-CAR-M033•Rev.06 Pace Carolinas Quality + Laboratory receiving samples: Asheville ❑ Eden[]Greenwood ❑ Huntersville Raleigh[] Merhanit ville❑ .'. Upon . , Client Name: � I Project � WO# : 92431068 Courier: [-]Fed Ex ❑UPS USPS lient PM; KLH1 Due Date: 06/13,19 ❑ Commercial ❑Pace ❑other: CLIENT: 92—HDR Custody Seal Present? ❑Yes Seals Intact? ❑Yes No Bate/InitialSFersan Examining[antsnis�(" Paelsing Material: []Bubble Wrap Bubble Bags ❑None ❑ other Biological Tissue F fen? Oyes ❑No N/A Thermometer'R 92TQ48 Type of Ice; ❑Wet ❑Blue []None In It]; Gun 7/_�Correction Factor: Add/Subtract('C} CoolerTerrlp ('Cj: i LL J T 0,0 Temps Id be abase freezing to 6°C ice, Cooler Temp Corrected ('C): L �. samples out of temp criteria. Samples cn cooling process hasbeoun USDA Regulate@ soil Did samples origi a in N/A, water sample) a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samp'es originate from a foreign source (intern ❑Yes LJNo incluoiigmawa+i a,m rue,tu ni—P L_J u Comments/Discrepancy: Chain of Custbdy Present? �� LAves ❑Nv ❑N/A 1. Samples Arrived within Hold Time? es []No ❑NIA 2. Short Hold "Time Analysis (572 hr.)? -[-]Yes +o ❑N/A 3. Rush Turn Around Time Requested? ❑Yes Otfa ❑NIA 4, Sufficient Volume? es ❑ND [INIA 5. Correct Containers Used? es ❑No [:]N/A 6. pace Containers used? L�fYes ❑Nv ❑NIA Containers Intact? Yes ❑Nv ❑NIA 7. Dissolved analysis_ Samples Field Filtered? ❑Yes ❑No ❑ A 8" Sample Laheis Match COC? Iny. ❑No ❑NIA 9. -IncludesDate/Time/II]/Analysis Matrix: Headspace in VDA Vials (>S-6mm)? ❑Yes D ❑NIA 10. Trip Blank Present? ❑Yes o ❑NIA 11" . Trip Blank Custody Seals Present? ❑Yes ❑ND ❑ COMMENTS/SAMPLE DISCREPANCY Lot ID of Iplit containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date; Date: Field Data Required? ❑Yes ❑No Page 63 of 68 /� m Sample Condition Upon Re / CDAnNydCaj Document No.: *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TCC, Off and Grease, DRO/8015 (water) DOC, LLHg *'"Bottom half of box is to list number of bottle t(SCURI Page 1 of 2 Issuing Authority: Pace Carolinas Quality Office Project# W—Q—#-@ 92431068 PM: KLH1 Due Del,e: 06/13/19 CLIENT: 92—NDR u Q 2 C 7 u A a f: N 7 Qa m a al C u F+ N a E Ln Vl a ii Co ¢ d) C u '� itl a E o O 7 a m Z C C N °1 & m N ¢ T A in N _ �%7 a ® ry V a Z u f0 Q E o Ln Z a to =o z M S�u� Q N V N rn N 1J 3 m u N A CL 2 0 Z t0 a M_ IV U a In CL C �. N �. a E� w �? 1=f- $ Z Z `1 C E :: r� L7 4 y Y _ U 2 9 E :: = 2 r1 l7 ¢ = ai G O. y ¢ �n M 77 ¢ N V G N 2 d E V] rl l7 ¢ N Z a N I E ¢ E VI N m l7 ¢ U i Z b Q -� E O rev a T Q M l7 a Z .... u 2 Q 6 o S QI l7 o a m 2 q p > 1 E P F CI C7 > a Z G e 7 q O > o 7 G1 t7 > fl 4 m 2 Q O o d Oi C7 JM z nl 0 « Y y n m Y 0 O > ¢ x Y a y .1C Y o, Y Y C7 > Q u R V1 ^ N' r- V1 4 v sr _ H e9 C. y 41 in E o M F a a V�NN aFZ $ N S Z u A 0. E ,� Ln a nl d m ? 2 a C y a E ¢ L o rl O l9 4 y C O C E a N 17 w N 2 a C a q is o V 7 01 l7 o 1 z G 3 4 5 6 Z\ I \N 7 8 9 N \N\ 11 �z �sA\�\ I N �` PH Adjustment Log for Preserved Samples Sample 10 Type of Preservative pH upon recelpt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot p Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will oe sent to the Norm Laronna utnrvn ceruocanon u11 ice fr.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 64 of 68 m Sample Condition Upon Receipt(SCUR) Page 1 of 2 ceAnalytfcal Document No.: issuing Authority: f-CAR-CS-033-Rev.06 t Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TCC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle Project # WO,#:92431068 PM: KLNJ CLIENT: 92_HCp Du* Daf..: 06/13/19 QF z u z v yl a e 7 J E h eel a m z a ✓, a e M u J Ei V) N 7 a m z_ d N C `o. r D u �v J E O N a m z a a c � d `w — rY a m u N v O „u} � E oti N ri a m _ N v p z 2 � J E 0 N'I rV Y li m ^' z ay u C z u ro J E ui N �1 N a m u N v 0 OM 2 q J E en N rl U a m ?FZ v a A I7 -0 W r C o y ? ti 3 a d a C 7 n Q ; — — ri .i l7 a V a = E a = — r-I 2 .i 6� a ? 2 d a a E ¢ J of N of i7 a v G V ul N E a v W H L7 a V x O eev T y E q J E o lid N u, en a ? V Q 0 N M Q M a a Z `� ¢ 0 J E O Y .2 a+ 17 a a ? Rl '� q 0 ' 0 I 0 l7 > Q r 2 a r d C J E Q � l7 > _ O a 2 ¢ 0 J E co t7 o z N M v�i mi y a ? :a. < d > z i± " \ y > l+ a Y! R r m t7 > I a a v, J E n. 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Ir Appendix C — Field Data Winston-Salem City/County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix C — Field Data This page intentionally left blank. 14 Location Project / Client n■ MESA rSI2 1TLA�) lrA FF 11w c II � Location V .-. _ 7.� IL, n/( `` 17 Date �r project / Client QS L'O f, Octkr` L- lc' uU k�.f� �1 Location _Utl�,. "�rF.K�ji.� U7te R71t Project 1 Client I MW I3 J,og. 07445' M O - lZ �tA` 07 56 075 7 �7,1 rxlr �+j'�% Og VO �y IO,��• Y" 10-3r, 1 q. j l' V Io7. mw •-� 39 ,-r s' ass1 mw' q �_ 5' G LI I opll k'W-i[- 3347' 0$31. Y'' o-59, 9.-ii► 094D 75'' O i Location �,k� Sc,t ��` Date _R proiect I Client -- �7, 01 /7 052 ✓'i 5 t! J �Y. Y'+7 �'r(,.t fJ.�v r w� f'� `G I C'O ri;.�j . Lj -R zo _ ��,�. Location , ��" "�'� ✓ �. �. Date � I� Project / Client -77 LIZ 1 30 •gp_ oY, e Location Date project / Client p770 MIA) - r_[z I - I •r r 22 Location I I •• / • Project / Client 05 6Z " P I= p71e -- 07 Zo - 5e-4 L f Cam, PAW � v� �G � 3 ws - �� St�7 � L-( CO�tz d 1 "Xil- SAAD - � i Location Date -• �. project / Client j__51(i C.ev,e Nl� . rlu.,Jnq- l,.7 !MV L r 24 Location Date L10 Project Chent Ai r4 6, C� 17) Version: Sheet of ERGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: _Winston-Salem, NC Sampling Personnel: Robert Mull Date: Weather: i-1, L 'r MO-9 Well Information Well Diameter (in): 2 Purge Equipment: Screened Interval (ft): Pump Type: Well Depth (ft): Pump Depth (ft-bTOC): Z L' Depth -to -Water (ft-bTOC): In- qN' Tubing Diameter (in): Water Column Thickness (ft): 1(9 -�Sb Well Volume (ft^3): Z6Ir 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CQ COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 0 5- 0 1't•-7 7`7 c' SGo -go s 3. l 35 s z� 5� Sal J+7 77.0 5-vi -7 1. Z.S7 ry L4 3 s' 2- z 0 0.2-7 '7 s. a l 1 7 L-Z 5-- l (o . -71, 9 Z- ZLv 3�-1°l 135 Li,0 0•-0 9.0 1 f.GG l(�owc Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative �00 e , /u L1 0VO Sampled By: f6o 77 Sample Time: 5� Date Sampled: Zo1 Sampler Signature: Dotes: � . -tier ; 0 • Z•? SGiV A"'-- T� Version: Sheet _ of FNGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: f M 10I Weather: Qc,- J_� Well Information Well Diameter (in): Purge Equipment: C-060 Co.4,01 Screened Interval (ft): Pump Type: Well Depth (ft): Pump Depth (ft-bTOC): - Depth -to -Water (ft-bTOC): - fil-Ss ` Tubing Diameter (in): Water Column Thickness (ft): &LAS� Well Volume (ft^3): 3� 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Oro—v 5 TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. o (C) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) I � 0 0.0 51.E 6 --A 17 • I/ I S7 4 0-6, I q 1,5- 0.4 0.09 49 _ . l l I S5-0.9 90, -5-'2- 3 J LH -0 0 0•0 1 5,Ol 17 I Y0. Lo Z -uS .-79 IKL(5 0• 0,09. ?Z 0 174 1.5TO To ` 3Ci 00'N . Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative _ W iHus Soo ,I A.J L') I'LSw�� of ►J4aN ' �,� C w: I1 ..l^ 40I �.: o J-1 Sampled By: Sample Time: 1Ku5 Date Sampled: s f -)11 Sampler Signature: y LI I Notes: f V W r-k = ) 00 Version Sheet of 11111111111111IN Groundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: _ Winston-Salem, NC Sampling Personnel: Robert Mull Date: �_/ � 1 Z o m Weather: ' • s" - w-10 u Well Information Well Diameter (in): 2 Purge Equipment: Cv �tw_jv- Screened Interval (ft): Pump Type: Well Depth (ft): [00 � Pump Depth (ft-bTOC): ^ S S Depth -to -Water (ft-bTOC): 5b.yukk Tubing Diameter (in): Water Column Thickness (ft): q•lc;(v Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO d S WATER (ft-bTOC) Wp PHO i p (standard units) TEMP. o (C) COND. (µS/cm) DISSOLVED OXYGEN (mg/Q /. ° % � ORP (mV) !V TURBIDITY (NTUs) COLOR/ ODOR (describe) 0 $off 91 0 '01; S.3`1 ) s �.� �-� ► �N �. got 0 3s 0 7 < D.0 "-.Dn( �s.� ��•I Z Z.°I _IyLi� Z „�� ( D 0. u% 0 70 S,a'7 c5 6 I &.0 lgy._S i,ZS 1L)0 ._ 081 o-o-7 i\ i 1.71 -IS�.� 1-v rU OW a. .7S I _1 V. I I&"9 I.qg I7" q i.101 00'-C- 0m o Z•I .v 0•`7 "�.12 ]v i$,2 D it,K.•z I -2S IvvY—c., 3 0.0-2 S`•Io -Z 111,9 I. 5 —I-)-L•Z i. -z,1 &)O%' _ Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative f6l -0 19�C1U w`% oAJIA al tiLDL Sampled By: t�,.f1 ('�'1v11 Sample Time: Date Sampled: I °k Sampler Signature: Notes: T4wCI-MA- -L -L 7 6- r^%, �0.0'7 ��%" • Version: Sheet _ of FNGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: E 19 / 16) Weather: S U n MO -I0 Well Information Well Diameter (in): '1 Purge Equipment: 0 ^� Screened Interval (ft): Pump Type: 'D't Well Depth (ft): IN • Go _ Pump Depth (ft-bTOC): '4 - (o' Depth -to -Water (ft-bTOC): l0 • ZN' Tubing Diameter (in): Water Column Thickness (ft): I d, -7V Well Volume (ft^3): _ -7 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): ` 5r TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. (°C) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 093q ff ff 0,01 r0" y)( c, 15'5 It4gQ 3-30 -7RL4-Z n-3� c%U'-'_ �g1Y1 0- 5 0•1S I0. )S (4 1-7 - 7 -0 'l7•0 Kh'_<. D�N4 0,� 0--70 .off Jf9.,57 .-0 UVoi,-� 09H9 0.5'� Go5 0•Vi ,tip 1.6.q ILLI 11 I.-U(e -3►'-S.1 /-.lq PovLf- ".5 01 )uo_� 1•0_5 1u--7 Vov� 51 D 3S -7S <7 ,5 ro im I5 I'S"il 'L ` �Tw rS• Z,O ioo,-Z 102 ;S 0 0-� 0.9 -37"3 )vow_ Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative \ `U 00L( 50�7 I 4 )'A Iti o.— 7-5,r> lin L Mv LA 2Sv df 4 r4 I ZSw, IAA O N S'l Pot Sampled By: u {.' ••ll Sample Time: Ivor Date Sampled: Sampler Signature: [Notes: �',�w,p,-��k = Zlv S ��/w .� - V-0 1 Version: Sheet of ERGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: Sz R / I `1 Weather: zP l v c4, /, � rl- MWA Well Information rr Well Diameter (in): Z` Purge Equipment: tU-0✓���7� Screened Interval (ft): Pump Type: Well Depth (ft): TO Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 3•(QO� Tubing Diameter (in): Water Column Thickness (ft): 110,14, Well Volume (ft^3): Z • &7- 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): c, TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 105 •0 Wn 3` 7?L 5,90 1.5 3Z(�•l - �� ..� 3 7� ►V�.� 05 `7 0.11A tI. lA 0. o 12L, 3,73 3• 79 !.s • i 1319, 0 '. Z-1 - Zti S• 1 3s rv� .I0 0•-( D"Ivt O'au 4 5i5 151 0•11i-7 -Zqi Z 3 11 I%S •Z r .0 %_ .9.71- IS• 1 310.0 o.N -3o9-9 1105 Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative ] 1110 2.so P Pp Sampled By: _ .' nit,.-\ ILA "o Sample Time: 1110 Date Sampled: Sampler Signature: Notes: '�v✓y�rctk ='L'�U w��w - U•Cl(ou 5NJj,,ti. "Au--L')L Version: Sheet `of ERGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: Winston-Salem, NC Sampling Perso nel: Robert Mull _ Date: q / f Gl Weather: vG �) , Z K' T 6MIJ._IZ- Well Information Well Diameter (in): 2 Purge Equipment: c,,� o� Screened Interval (ft): Pump Type: L�� .' c c rr~ Well Depth (ft): �$ r�1 Pump Depth (ft-bTOC): I(q .7 Depth -to -Water (ft-bTOC): ctit Tubing Diameter (in): Water Column Thickness (ft): 10' 7 ,-1 \ Well Volume (ft^3): 1, r 7ti 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; T = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP- o (C) COND. ([Is/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 17.Zv ill _0. [ �,2`i !! ((S Z � 5� -8Z IS8. �T� [ s J 04 � Lc).-?l .1 b ( �l W00 (l✓ Vdd�� I LLL -1 Ll 5•-7rl 1 S• S6 I I - Ib� K 1 ..,� l 7'-1 3 0 0 - I•.?7 1 7,2 V� 0rl �r�� /� /(o. IP�O 0, � (D 1 -o it3s' • 0.1 5, 1 5.'7tl I 77- Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative tAO.12 pS 5-00 poty lu/fq v 14 O i Vl as'L 9t 7/ Sampled By: 160 !l-e, M,H Sample Time: LZ '_'x- Date Sampled: Sampler Signature: IL (Notes: ,.�Prkkt = 3v3r2 Mgr_J,,� Version: Sheet of 111111111INN Groundwater Sampling Form Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: s% ( q Weather: Er" uy, am, +7V Sample ID: Mw_)3 Well Information Well Diameter (in): ��1 Purge Equipment: , �9 c0��-�` Screened Interval (ft): Pump Type: Well Depth (ft): zc7� Pump Depth (ft-bTOC): i Depth -to -Water (ft-bTOC): o-7 Tubing Diameter (in): Water Column Thickness (ft): \` • 5'�; Well Volume (ft^3): Ci 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): �• nn« ' `7� TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) i D-ol 5- 17-7.1 5.oS 1•2 Z-os w �35 . o .'-?Z 5_. I 15- � 1'7--7 ,1 4 - () Ll ti — 5.1 Le Ifl f -[, 4.oLA a3�0•L � � U�,,.� 1 L4L2Z , -L vS .q.1 S U /5. I • LP Wa3l7v Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative I q0 (-I 00 L o ZM of Su WC ') #V0 � (� Sampled By: c. 1 Sample Time: i v Date Sampled: Sampler Signature: JNotes: H,Mrd hkt, = fo.oks CAA" k Version: Sheet of F)� Groundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: r Weather: �.- a"" o MQ-1Y--- Well Information Well Diameter (in): `Z 1 ( Purge Equipment: %yeo ('tilr� Screened Interval (ft): Pump Type: h cc•. �-�L �G��� ,,.p Well Depth (ft): 60 Pump Depth (ft-bTOC): wS� Depth -to -Water (ft-bTOC): 37' 3� Tubing Diameter (in): Water Column Thickness (ft): Zb • 7/] Well Volume (ft^3): Li • Z 0 1 Well Volume = (Total Depth - Static Water Level) # Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter lnstrument(s): i lrf Ari.t TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. o (C) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) usU Pl Q,L (A31;; 5. �g 1' [2.0 3-2 -/O, .0 i.o5 � 500 00% 0. 'L 3 3LA z SZS ,? V1-0 2- 59 IZ . 0.G-5- a 0 LA z 0 1 It -A o °3 31 5 . �1 ZI n53 p. -f. Q .310 D -o Z , [ 19,& 7101 1,5te -lt{ - b 0 47 nlowc. BIZ I •L& 0.0'--s .3 -10 Zfl1-1 0 SS A-�b"- 5 U ti D. ' o S-W I Id-q Zo5• 1 77- -189.4 Q. U9 vL- Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative y AV II l S lL' 1 b� so v ,mot- a l f0& Z-'10 7-loori>,' , '' 1U yk I ZS w"L- f0i 0 S L' I % AA_ IZS ft"— pol oit� Sampled By: �w r►^ v Sample Time: Iv Date Sampled: I 1 Sampler Signature: <� et- JNote4s: l Version: Sheet of KRGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert _Mull Date: M I I GI Weather: Well Information Well Diameter (in): Z Purge Equipment: GU C'0' Screened Interval (ft): Pump Type: 71)t CAi�z Well Depth (ft): 22�2 Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 3U' Tubing Diameter (in): Water Column Thickness (ft): _ ?c�•h` Well Volume (ft^3): 31 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. o (C) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) wo 0.0-75 ( -70 flat(• 2 —J.b •IX AA�--t_ 09 ILA 0.o75 5•t;l LI.0 �� 7 `� `iS ���1•5 0-0 D It 0.075 119,01, S • S I I!LL I bLf-q : . q 0' 0715' 10.0 5 Z A. s 0.0-7 10,OZ !:5. ILI-S 1 s. bL1- u 5 1,05 0� Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative + Iv '� 0M 5vo WL- to l 10//4 Os•`k (s50 n.L l lL)1A wl�.a) tiSJ n't- tol )U M I7is VvL a1 /(%n0 Fatempled By: ti•,.I- v1._A Sample Time: Sampled:? Sampler Signature: - JNotes: Pu,,-ertik -- - O*U—J5 Version: 94111� Sheet of KRGroundwater Sampling Form Sample ID: dl' W-t4iL Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: S /-I /I G( Weather: �Lz' F t �+ Well Information Well Diameter (in): Purge Equipment: cv'- - -y� Screened interval (ft): Pump Type: Well Depth (ft): Zi�� Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): ZS. SUO Tubing Diameter (in): Water Column Thickness (ft): _ m-40 Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): C" TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) I� or0-kk Z &'O 1_. (0! -7. l70•� pp d v� %\ ,LA 0- W-1 t7 S-,)1 )?,.(p 111g 1,1,3-M.-? o.� VUvw 5 uLl_t 0.11 © 56 � � Al,Q 1 - T lP .1 Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative SU of M *I � (- � ' n l A Qd'�W Obi 0 i"'t 14 Yong t 7_ l w� � I PVw Jf-( Qx :---4 �, w,L o L 17� Sampled By: ab77 M71 I Sample Time: i 3 Date Sampled: el Sampler Signature: LLA- 1 (Notes: Puwpro.�z '(►�w�C'w.y 0•l\ 501"_ Version: Sheet of KRGroundwater Sampling Form Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: `Winston-Salem, NC Sampling Personnel: Robert Mull Date: Weather: Sample ID: /tl�J- -7 Well Information rr Well Diameter (in): Purge Equipment: eocuCiJ4ro 4 Screened Interval (ft): f l Pump Type: `• .c� I fc�� +N+ Well Depth (ft): "t • Vol Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 3 L< < Tubing Diameter (in): 'Water Column Thickness (ft): Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): 0t,", , `ter TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CQ COND. (µ5/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 9 0• Q1,3� -,!;. 0 0 � _tip . a ,( - u 5,2Z lb,o 0 -'N - z sS.2 0, H S IU),�_ )OQZ o.L M 1If•0 0 . �� 1 0 13q p', •0 a D)S• 3. U S� -ZI�1.`f iVvwC Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative i0riAJ (0 I S Sa7wL al�'� Rff��n 1!,_, 1. 5- 1 .•.• v o'.. v H Lz ITS WL I ti4 o Vz Sampled By: _ �1 Sample Time: Utp Date Sampled: 7 A Sampler Signature: zzli6L A AllI j Notes: `vv P r t, L 1,H' , iw•� IM, ^ = 0.0( 5• 1 /,_,-, ?fix Version Sheet of FNGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: Winston-Salem, NC Sampling Personnel: Robert Mull Date: r f l' i Weather: C-� I` ` o U �• vt Well Information Well Diameter (in): Purge Equipment: �n-e oG� •�_�-a� Screened Interval (ft): Pump Type: C.��,�•1� Well Depth (ft): 'C-! Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): ly _ Tubing Diameter (in): Water Column Thickness (ft): i -f. � v' Well Volume (ft^3): '... ()7. 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): ai ..� TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 11,1d o 0� 14•35 �•} 3�' •S `� c77 `l(o�, [`� a ILLI o. 7 4 v• oL [O 1-5, oz.1 I U ZZS 0 .1--1 Z .0& iU-SS_ b •I .[v 37 -`A .0 J,0 V9 Q,-&A- 0 .� .o i�i 35 (�, Is. 3 0=� Z 11 -la 1 2 . r">3 V -.T'A 1 o- 12> 15.7 2-1 3 1 ff-7 o L I IZ5-7 p T4 J ,Lfl( U. I1-I IS,-7 b J 177- 400 (L LLS U • Lid l 1 q -__�.S [S 15, 3 's-:L I. 71 ` NI-1-5 153 z- 6vo', Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative A so rn V f,,1, OG`f Z�" `Raly, Joc.OIq Sampled By: Nlvll Sample Time: 17, Date Sampled:____6j A hci Sampler Signature: - - Notes: I{` P��k - iAo 010V IUOf-( Version:n6111111011b Sheet `6f Purging Information (Page 2) TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) TURBIDITY (NTUs) (✓ � �l _-QOAR r {�1�e) � � ODOR (describe) I-zqi 0,19 1. 0'o '� � l� IS� ��S.Z �'� SS.1 �Z(0•�� L:�Lv� izsl pry .-L o. ,�g b -t-. IS • -59 0 60. 1- 705, L � S`l r . 0 l �! S� f �- � � `� 7 � 5-0 ` 7�7`'(� LSE' C-._ . Version: Sheet — of IIIIIIIIIIIIII)M4 Groundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location:_ Winston-Salem, NC Sampling Personnel: Robert Mull Date: s?'q I 1 cq Weather: S Ll^'-, =-7�` r- MW -Z,�- i� Well Information Well Diameter (in): Z Purge Equipment:��^�'�� Screened Interval (ft): Pump Type: Well Depth (ft): �.1� Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): &;, % Tubing Diameter (in): Water Column Thickness (ft): M-175* Well Volume (ft^3): Z- 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): a,f, - y { TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP, o ( C) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 1�35 0.0 .4S S 1 y�h 0•2,-L •o S-LA D.0 LA 1 low 0.91 -ztit.�1 ll 9 Iv�� `iy 0•_Sz .,L1 D•o 6 I .61 IOU 0 --7I 1A 1 1-�),0 f(i� ' 0 1b `i 1JON D -7 ut1, 1 51 0 e ,o(D 10 L)L 5 S! 119 N (9 . "7(D -IAU.5 ZL . � I(iU 55 Q Uk 0,G 05 I ,O 10 -5 `TS- C)-i () (V w _J ' ( I Ci�� V ` (U� �1 — 7�"1 S • I p, , CIL Q.Qfe 10-19• 0 15.0 logi U- C7 1 0'-] J0'-ttLLL1U D.a(. io lue-k Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative ✓v� I�c+.tt,s sc7 �- oI �� vw©h� %-10 1-4 Sampled By: Sample Time: 1 a -7 Date Sampled: ! Sampler Signature: - . [Notes: Prr - 310 w��,� - V-O(� 1 Alt - 'L35 ANLJ.1t. c 111)a.ok( Version Sheet of FNGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: 40, 0 h1 Weather: J b-1 u- _A2V%W _(o 5 1 tk Well Information r� Well Diameter (in): Z Purge Equipment: Screened Interval (ft): Pump Type: i.t}� ESP Well Depth (ft): LW Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 37. �oS� Tubing Diameter (in): Water Column Thickness (ft): i0 !Pi' Well Volume (ft^3): 1, 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): , r.. � TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. ('C) COND. (µs/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 0�?tg 0 ff Q.-it 9 7.35 I (u30 4`7 --7D,0 I4• o •-L 7, 8. 0 17=12 12 •1- Z5 1,22 - V7.0 I-). L Idv .•Z 38•`iZ .19 n. t)o Zeta - 17 •l V(_ QWeDr i 0.09 30,0o Le.I 1 L F 7,09 -�2, 70. � Il)a, 0 o,09 , 01 S 7. yuotc z 0 . I lP • It -7K • 1 PJ0 e, 3` .7, q: I 57 --A - 7� f Li Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative -15 PZ J7nt 0(7 /� l l t �• t,v mL at, 1I04 & soy / - UD P" -ti {v V 0 (( 50t ,` A, (Zsw.c of c%dN lyL Sampled By: 1. v &A Sample Time: Date Sampled: r u Sampler Signature: ! Notes: au�-Qrr650 ""4'_.-r o.Z �4t � 6w' 74 Locat [oil-- Projec.t / Client uate Locaholl Date t5, NwIlt 07�0 T— T-1 197/0 o7lo - A.SC,) 7 S,(_ /V'7 ,f) 10114, kv cvs A�,' So Oil is Ve 1LI10 V_r w - ro- 6-1 -S- - /6 L, - � '.') IG Location 0'- I/e— _ Dalry4,� PI'oject / client 017 .- - - r%%-�d9� � �� If O,x a�lo'• J� ��� �- - - � � f'`a .•�,. ��,� sty •-�l� - tJ 11 LI o c") � I �Vv -41 Lo cat lo I I v-J.9 L Date Proj(_)cr/Cliwn� Llo, Z, 177, -L I 4AS/t, - Li - i AYL LIN) mv OCT SLJI__� y"t CO- 6X7 m7 ,,,catioll_� Date CL o6sl 19 Ci r .51 Version: 04/30/2019 Sheet ^ of F)M�l Groundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: 4fL`' 1 `i Weather: llW ._ 9 Well Information Well Diameter (in): Z- Purge Equipment: Screened Interval (ft): /2' - ZJ7 Pump Type: 'Well Depth (ft): L7 ` Pump Depth (ft-bTC1Q Depth -to -Water (ft-bTOC): 1• H1.' Tubing Diameter (in): 'Water Column Thickness (ft): ? `r.`;-7 ' Well Volume (ft^3): T. L41 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s):Ho Y51-" TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. o (C) COND. (VS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 0,07 1 ro 6- c-f z S• yi 9 2 7se 1 0•1� 0`0 1.T5 s"-K7- IS' �: z �l y 4 2 -3 �> u t-I .& U-07 11•3V yZ, 1 -� 7•I ?.3� �`'`! Z-7� OY01 .'LI • . P- 47 • o 7 I i . 5 S 910 - -Lz V.v7 j I- Z-q L) '7,1 1,4,9 of 0 "ZI r . Z U . a � S z � K•S � ' _5 1 3 11:c".` Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative �n l� A v 7v � Sampled By: W I f Sample Time: _3'1�1 Date Sampled: r/Sampler Signature: L� lNotes: fV-PrAk -170 r.Z. 0•0 ) S..I/--- Version: 04/30/2019 Sheet of� KRGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: )yi Weather: �2 .. ,,, n * -7J'' '- mid-1 Well Information Well Diameter (in): z" Purge Equipment: (� G�:•Yv f Screened Interval (ft): q _�; I - 110 Pump Type: L INd i pvv__ Well Depth (ft): urn° Pump Depth (ft-bTOC): 5? •S" Depth -to -Water (ft-bTOC): 5- 'L 3 Tubing Diameter (in): Water Column Thickness (ft): t IT Well Volume (ft^3): 1 'AC) 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Y u%AL, Y51 TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. ('C) COND. (VS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) ;! COLOR/ ODOR (describe) of S , 45 0 5 a - vs D o V -u 'I 5 7. 2.. -5 - 3 !v 7. 7 Z- Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify Sample Information Sample Number Collection Time Parameter Container Preservative ,7 Ltig Sampled By: 7r (4rk- kA-Sample Time: ITS Date Sampled: Sampler Signature: rt-1 INotes: a((, Z v �,...�N - O-V'!� '�"I/— Version: 04/30/2019 Sheet of F)� Groundwater Sampling Form Sample ID Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: _7st_I_r`l Weather: 5 7 f` �11w ` 1 `/ Well Information Well Diameter (in): Z Purge Equipment: cc.,1-,� � Screened Interval (ft): ysl - 4 Pump Type: L Well Depth (ft): k v ( Pump Depth (ft-bTOC): S Z --5- Depth-to-Water (ft-bTOC): SO • Z7 ` Tubing Diameter (in): Water Column Thickness (ft): If. 'I--� Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; T = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): P4--- r ysi- TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CQ COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 01.5 7 0.19 0.1 e o. OL, -�-o. q!�- Si i6 1-7•1, 1 e1 .3 Z' - 3� V c; nob, .1 2 U of� S0 S 1� )7 5 I5 v .Sr -37. Z•�7 (}vr-c_ uv, p, v cite Su.SI '.1 to 17. q %17 .L -t,7 -qt. I .Gz v V1Z. loji I.ot q.o1a So, te 7S 1'7S• 1•07- -1zo1 Si k2bxv- 0 t 5 n.1% 1, zte n UL, s U 5• 1 Le 1 'I 19'J. Z 5 Z 4 o 'L Z. Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative L'S'o"L Aw NCi Sampled By: I- n^ ,iI Sample Time: /07-0 Date Sampled: 1/'r b 9 Sampler Signature: L.[ (Notes: PL v4r.,lf, ;, -z►v ti /�.,. = 0. 06 Version: 04/30/2019 Sheet of 11MY4 Groundwater Sampling Form sample ID: MO-10 Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: _ Winston-Salem, NC Sampling Personnel: Robert Mull Date: < j 7-1) L i `) Weather: Well Information Well Diameter (in): Z Purge Equipment: _ _GyL'� '( Screened Interval (ft): 0 Z I n � Pump Type: Lug t LA (A i3lu AAzi 7v-.-F Well Depth (ft): Pump Depth (ft-bTOC): 1 s -S Depth -to -Water (ft-bTOC): �0 SV _ Tubing Diameter (in): Water Column Thickness (ft): 10•HS Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 1 /SZ — oa �q U `1 L ) S'e -21 - 29.E 7v--S t we .y a sal d- or91,, 6-z-5- 6-00 -T-5z-2 37 / ,,s V7 •1► D • 10. S Z-S 4-7 1S5 q qi • l"�l- oLl -1-7 v-L 10•9 b2-1- 14 -S ISS 51 ' - MI. 3, 5--4 17,01 0 uS 1,5-S 10.,111 lv-5S 7-3 b.'_2 5- Z y-GL - 311.E 1,I 114j D-`(S y 9 0.v1 0. 4, L'Z, )10s 1_.E;y7 .50 Z7. 7 III L) L(.S Z - y 0.9b " Zt 1b- 1 y L .5. -311- U 'l s- L UV- 17.7- -L 2 4, 0-UL-1 -74e zz l5 5 ls4N 3 729 0--1- 1 2-f"3 v.oq 10,70 .V7 1S i 1fW 1 3-3v -Zgo-v 17•�- Uv�� Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative z3 (� L- A:�-- Mom► v f0 0 �Pfl NUJ^ Sampled By: ham[ MI/11 Sample Time: t_'! Date Sampled: 1 Sampler Signature: f [Notes: rt-rr-.k 0.0 3•r��.� 11 19 �Q—'Pr'4 4- D.v&I Version: 04/30/2019 Sheet of Purging Information (Page 2) TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. (*C) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) TURBIDITY (NTUs) �V � (411�) Cv�'� O R (describe) I'Z3 0,'z �,v3 0,0t, U�L,$ 6-td •7 &S -5•0s? YS•0( vo-5 Vo"- O-vq , Li 11, IU04 Version: 04/30/2019 Sheet of KRGroundwater Sampling Form Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: Winston-Salem, NC Sampling Personnel: Robert Mull Date: r 0 / i `'l Weather: Sample ID: PI W1 Well Information 'Well Diameter (in): 2 Purge Equipment: Screened Interval (ft): S� , TO � Pump Type: �c.� 7C �n �+� 3�nr� � i��•�. {' 'Well Depth (ft): TO Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 3 , `lq k Tubing Diameter (in): Water Column Thickness (ft): / i, u ( Well Volume (ft^3): Z• ��%, 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): ys i TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. (°C) COND. (µs/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 0.1 9-Ito X. yU /5- -W.'3 7. Oct i N32 d •3 U 'S v 19 S 11 1.5 , a� 37/ 0 6 S� r z6/. -K �- 0.1, 19 zJ S. 9 -1 '.!7-,7-.s 6-,47 z?e4-e 1),3 p. o. L 7,2 , S?L S, 7 3-7-9 (a , 0 - Z7`7. . 2,? Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = specify Sample Information Sample Number Collection Time Parameter Container Preservative �nW A\ Sampled By: rn Sample Time: 1 �T Date Sampled: VvI /I I Sampler Signature: Notes:,�vw��a� ; 3d5 ,,��1,,; ^ . 0 0 l Version: 04/30/2019 Sheet of� IMN Groundwater Sampling Form Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: S[ Z qI, I Weather: Sample ID: Mtl) - I z Well Information Well Diameter (in): Z Purge Equipment: 6c- o e-�,n) , I Screened Interval (ft): -51, 7" `._Si_ rump Type: D��%�,I 131 a)-b-- ��...� Well Depth (ft): I 7" f 5r59` Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 5Z-5-' Tubing Diameter (in): Water Column Thickness (ft): i(0 , 33 Well Volume (ft^3): , be 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; T = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): krrnw V S ` TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. o (C) COND. (VS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) y z1 — --- -5,6 —; ��,.. �, t 52 I 's-t o- 1 0-1 G- 6K S, Zv 21 �. �� s 1 ►� 11-lu t -,l 4, 7 5.7 / /a-Z 7`2 35 -T `Z7s L I "414 U•-�. l U-1 �y6 � $, e /6 3 1l; 3•XK 6o. i,i4lo O^A- ruZIN •3 S • I ,' c�ti -7 Cy, ?xv 9' 32 — LSD 122� Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify Sample Information Sample Number Collection Time Parameter Container Preservative yL14, VOL, Xu'o 7(2 Sampled By: -1 Sample Time: ly Date Sampled: 2q % Sampler Signature: Notes: Ii;vLfrc%e=395n�rt/,.)- = APU Version: 04/30/2019 Sheet of 1111111111111IN Groundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: SI3411 Weather: n.. Well Information 'Well Diameter (in): Z7� Purge Equipment: .Screened Interval (ft): % - 'Zoe Pump Type: Well Depth (ft): 70` Pump Depth (ft-bTOC): _ ) Z • S _ Depth -to -Water (ft-bTOC): 7' Tubing Diameter (in): Water Column Thickness (ft): l l "1 Well Volume (ft^3): . 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameterinstrument(s): qa TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft•bTOC) pH (standard units) TEMP. CC) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 09) z I- T p. , `1 •t S • i-I U)?f K- 0 TL U. -L 0 IJ 6.-761 57. -�,'3 i _q- 7 i 14 _S-Z, -75--1 Iq 0 .17_ O.2q v,0E1 g-L 5 Lts' IS.S lH3" L4a✓.c -7 Z, s �% A \ 0•1L 0, U•OLI DYZLI IZLi 1 0-0 9-94- q• yg g, i eql -211-7 .I V v 1r 16 fv 1 LIZ"J Ci`'Z& — FO-4, Z-Tqh�vwL Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative . U c) K 7C2 ,6.L_ Coli Sampled By: >'.- v Sample Time: U- Date Sampled: Sampler Signature: a (Notes: flan.., pin J_ - /I,,) =. 0, 014 Version: 04/30/2019 Sheet of W%RN Groundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: _ Winston-Salem, NC Sampling Personnel: Robert Mull Date: ; N f A Weather: Mrj-3z_ Well Information Well Diameter (in): `z Purge Equipment: Screened Interval (ft): I Z` - Z7 ` Pump Type: N.A)criAt 9Wa _ P ^-• - Well Depth (ft): -t7 ' Pump Depth (ft-bTOC): 1 S� Depth -to -Water (ft-bTOC): 4,7Tubing Diameter (in): Water Column Thickness (ft): I Z�'3 Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): ZI TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) n7z '' -- v try 1 �)' y /Lsr.s u �37 r� v 'Z. �7z[,0.1 x 0� -2�a` ,1--7 --"-0 ,S u�(-�f y),'7,"I c3gv.':5 3,-9Z —79-'N 7v.'7 �51 • C ] �f( y� 7S -I V-LAJ I S, ( Z 7 9 Zg. v l y �. '7 4— Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative f� VN.. 1� I f L- /� Sampled By: ..{ Sample Time: t} 7S Date Sampled: sam Sampler Signature: Notes: �ur>1� _ ) �(✓ 1^-�.�a� ��� ���+�"^ ` Version: 04/30/2019 Sheet � of KRGroundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date:%3t / )i Weather: mlIj-7 Well Information Well Diameter (in): Z Purge Equipment: e') C.r" Screened Interval (ft): -� -� Pump Type: D �'�1•,���•' Well Depth (ft): 4 Pump Depth (ft-bTOC): 40 Depth -to -Water (ft-bTOC): 3 . 9 Tubing Diameter (in): Water Column Thickness (ft): Well Volume (ft^3): I,•'1A 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; V = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameterinstrument(s): HGnnK. I y� TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. (�C) COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) on' - 0 . u 3 N * �LL'- 0,0L, 3 b - 7-0 1L.,.3 L3-7- (' • S•U 7, 5- 1 - 06 M c .17, V,Isux J7 5,L% JL 5 Z3i4 A 0,.s"7 _C,5,7— 0, 514 0, Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative fv��j --7 �.1 Llol_ z'60 Lev Ltv.K A—_,— J c . 0 77 �v '�S.,.L o1 �V L Ate.. Sampled By: _r{, I- �N)�l ( Sample Time: /d�- Date Sampled: — _ , ..)'/ S Sampler Signature: Notes: ��w���r,� _ Version: 04/30/2019 Sheet of F)M� Groundwater Sampling Form Sample ID: Mw- `fir` Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: Winston-Salem, NC Sampling Personnel: Robert Mull Date: > 1 ,L) Weather: 1, Well Information Well Diameter (in): 2 Purge Equipment.. � G .-. f Screened Interval (ft): S o Pump Type: ��- Well Depth (ft): � Pump Depth (ft-bTOC): 1 t Depth -to -Water (ft-bTOC): 5 - 7 Tubing Diameter (in): Water Column Thickness (ft): , 2 _S ' Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): klvttick, ` Sr — TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. o (C) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) V91M — 01 � S,7• _s.I� /s'o 1' us iL iLJ V J 71 0-1 le - 3 - c4 - V Il l :30,T" 1001 v-Z_,-4 v Kolr S..7 3 / q- I l ,_� /y• vr,S U-2-`t 1>2G 0-06 ..7LI 6 Ic4-e /30Cv l".Q 3- Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative (�f 1 1 v l l ✓oc izL.0 ��, u0 M �- ,q:" f'� �, L s �S'� r L A 6� ,0o -7 u 70 v „� f 1►t% Sampled By: 4 t Sample Time: 0/1 Date Sampled: S 3l Sampler Signature: [Notes: f (,,n -,r,, W_ r. z z;� —W -,rv% 61. 470 �, r� Version: 04/30/2019 Sheet of F)� Groundwater Sampling Form Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: I Weather: 07110 tio`i- ! r— Sample ID: /V- - IN Weil Information Well Diameter (in): ZPurge Equipment: cOrk,A Screened Interval (ft): 15i - 30Pump Type: Well Depth (ft): So Pump Depth (ft-bTOC): r17-15 � Depth -to -Water (ft-bTOC): ff', 14 Tubing Diameter (in): Water Column Thickness (ft): 10 .5_1-� Well Volume (ft^3): 3, 7 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Gnnk TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (PS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 0501 0-0 '-0 L !;,'1& . z9 3_ - ) c) o.j e 0,01, 7 53 1 -io �1 LIm 0-01 - -C)� 5,12 1&'5 J 9+7- i T- 6p-,-Z- 1tio (? 0 - v 5 0--110 y - o'T 7 -7 S 164.1 Q - U cd &-50 e� Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative �� SZ I Neu fuu? Sampled By: 16= M71 I Sample Time: 1 Date Sampled: Sampler Signature: Notes: �'�►^ {'�d� >ti ; �lv... y/w�,s. U- v1 ?=�!/ Version: 04/30/2019 Sheet of KRGroundwater Sampling Form Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: ,5131_b', Weather: Sample ID: L Well Information 0 'Well Diameter (in): Purge Equipment: (»oCGn4^11 Screened Interval (ft): �i' Pump Type: Well Depth (ft): �_ )� Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): G� 9?�' Tubing Diameter (in): Water Column Thickness (ft): . 0'10 Well Volume (ft^3): Z. ZtA 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): ra 4 nst 5 7 TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC) pH (standard units) TEMP. CC) COND. (VS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) Lc 12-3 6"O t l5 - "Z-7 0 c, - o .5Z 6,03 /.5 , 6,"I 0 - V ^ 77,) Y, (iv , z - '" ? • ,k z, -v' l t , 5- 7 .- � r �s� 7 �7 'v� V r (7r / 4 ` �p7 V ' f% . 1 1/5� `Y r i L5. / J - �2 Vi. / r E%y-, '� DV Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify 4-t, F�"Sample Information Sample Number Collection Time Parameter Container Preservative Z IS L) _7N 1: I'L, . ^tnE- 031 94 OL q U 40n-L- 14 Sampled By: 7-LL41 Sample Time: i Date Sampled: I3+I/`t SamplerSignature: w� Notes: Pw k = qZ0 t^�%-`� �• 1 Sel�w� 120A (,—,er-qCL 315 ^^ z lw3%� O bQ�w �� s• Version: 04/30/2019 Sheet ^ of HPGroundwater Sampling Form Site Information Site Name: OSR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: ri 1 ?, % 1 I I Weather: Sample ID: /5( i, Well Information Well Diameter (in): Z Purge Equipment: Screened Interval (ft): 33� - L4I' Pump Type:,, c, i' v-, sC' C' Well Depth (ft): --� �` Pump Depth (ft-bTOC): `fV S Depth -to -Water (ft-bTOC): 57- Tubing Diameter (in): Water Column Thickness (ft): 10.14 Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): J(q%4_, y s_S TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (ft-bTOC)C pH (standard units) TEMP. CQ COND. (µS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) 690 J y G ;� 0, � �I 5 i c2 & Z -_ �7 1I 7 94, 1 'W / fi t• Ss xq o( 9 5 E '76- L 1 FO 0 6 ' z % -7 Z . z:� 32� 1 3'1 -�; 0- Ls Z ®K-L' CU _ 9 - -0 � O !r Jz-q 4,117,K-` "T_ /v - /.tom Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time r) Parameter Container Preservative VOL p Sampled By: t'S"r WlSample Time: �- Date Sampled: 5 ' r Sampler Signature: l I/ Notes:' 13- r,1 � , -'(' _ ]6g h- I-/J--- S J I-, ;.)--V V I Version: 04/30/2019 Sheet of K)OZ Groundwater Sampling Form Site Information Site Name: CISR Landfill Project Number: 10125427 Site Location: —Winston-Salem, NC Sampling Personnel: Robert Mull Date: . V -M J L� Weather: Sample ID: M I.) r 1 IZ- Well Information Well Diameter (in): ZPurge Equipment: e,cvn {- I Screened Interval (ft): �l�i- �� Pump Type: , I4sI, Well Depth (ft): Pump Depth (ft-bTOC): S Z S Depth -to -Water (ft-bTOC): 2 7tubing Diameter (in): Water Column Thickness (ft): IL`1." i Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameterinstrument(s): TIME VOLUME PURGED (gallons) CUMULATIVE VOLUME PURGED (gallons) PURGE RATE (GPM) DEPTH TO WATER (f[•bTOC) pH (standard units) TEMP. ('C) COND. (VS/cm) DISSOLVED OXYGEN (mg/L) ORP (mV) TURBIDITY (NTUs) COLOR/ ODOR (describe) M7 i( J Z�`z. 0, 7 Ll W if • 14, Vic• ,"� ,� G•IJ 3�2`i %l�.y 73"z o.�� 5� L9 - U j r3-S,R" 5- )L 7 237-" ' e)• G v ZS -S- .L47- lU `i U c�. r Z7 %G•'-I Z3'Z.Z &_ I �32" 'Z -Z l y4T 0• s 0.) z32" .5-9 ,p 7 JAJC;�'_ Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative U 5 k/0 7N '7v Zv,Y� %�l MUuu 40 ,. L Sampled By: Sample Time: i q`(_57 Date Sampled: ���L J'� Sampler Signature: --J` ! Notes: Puv�.r icik j'7 •. •�/ — ejc7 5 w l/ram. Winston-Salem City/County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files i ..ip rip I. _T Appendix D — Electronic Files rtable Document Format (PDF) of this Report ectronic Data Deliverable (EDD) of Groundwater asults Winston-Salem City/County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files This page intentionally left blank. HDR Engineering, Inc. of the Carolinas 440 S Church Street, Suite 1000 Charlotte, NC 28202-2075 704.338.6700 NC License F0116 hdrinc.com © 2019 HDR, Inc., all rights reserved