MO-9473_40915_CA_IAR_20190702_ Initial Action Abatement Report & Email Discussion

INITIAL ABATEMENT ACTION REPORT
LINDA LAKE DRIVE UST
7609 LINDA LAKE DRIVE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
INCIDENT NO.: PENDING
FACILITY I.D. NO.: N/A
MID -ATLANTIC JOB NO. OOOH1378.00
Risk Classification: Unassigned
Land Use: Unassigned
Latitude: 35.245861 ° N
Longitude: 80.733052' W
Date Discovered: March, 2019
Estimated Quantity of Release: Unknown
Cause/Source of Release: Heating Oil UST
Prepared For:
Lifespan Inc.
1511 Shopton Road, Suite A
Charlotte, North Carolina 28127
Prepared By:
Mid -Atlantic Associates, Inc.
1125 East Morehead Street, Suite 104
Charlotte, North Carolina 28204
July 2, 2019
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Initial Abatement Action Report
In addition to reporting initial response and abatement actions and assessment actions and presenting initial site characterization, this
newly -created Initial Abatement Action Report must fulfill the requirements, when a release has been discovered, for the following individual
reports:
❑ Site Check Report (Section C)
0 UST Closure Report (UST-12) with UST-2 Form (Section D)
0 Post -Excavation Soil Contamination Assessment Report (Section H)
❑ Free Product Recovery Report (Section E)
Check the applicable report(s). Complete Section A-L, as required, including the sections specifically designated for the reports you have
indicated. The Initial Abatement Action Report must be submitted to the appropriate regional office within 90 days following discovery of
release.
A. Site Information
1. Site Identification
➢ Date of Report: July 1, 2019
➢ Facility I.D.: N/A UST Incident Number (if known): Unassigned
➢ Site Name: Linda Lake Drive UST
➢ Site Street Address: 7609 Linda Lake Drive
➢ City/Town: Charlotte Zip Code: 28215 County: Mecklenburg County
➢ Description of Geographical Data Point (e.g. diesel fill port): Home Heating Oil Tank
➢ Location method (GPS, topographical map, other): Google Earth Software
➢ Latitude (decimal degrees): 35.245903' N Longitude (decimal degrees): 80.733063' W
2. Information about Contacts Associated with the Release (Addresses must include street, city, state, zip code and mailing
address, if different).
➢ UST Owner: Kenneth_Fuquay/ CEO
➢ Address: 1511 Shopton Road, Suite A, Charlotte, North Carolina 28127 Phone: [phone]
➢ UST Operator: Kenneth Fuquay/ CEO
➢ Address: 1511 Shopton Road, Suite A Charlotte North Carolina 28127 Phone: [phone]
➢ Property Owner: Same as UST Owner
➢ Address: Same as UST Owner Phone: Same
➢ Property Occupant: Unoccupied
➢ Address: Phone:
➢ Consultant/Contractor: Mid -Atlantic Associates, Inc.
➢ Address: 1125 East Morehead Street, Suite 104, Charlotte, North Carolina 28204 Phone: [phone]
➢ Analytical Laboratory: Shealy Environmental Services, Inc. State Certification No. 329
➢ Address: 106 Vantage Point Drive, West Columbia South Columbia 29172 Phone: [phone]
3. Information about Release:
➢ Date Discovered: March 29, 2019
➢ Estimated Quantity of Release: Unknown
➢ Cause of Release: Corrosion of UST system.
➢ Source of Release (e.g. Dispenser/Piping/UST): UST
➢ Sizes and Contents of UST(s) (or other containment from which the release occurred): One 550-gallon heating oil UST
4. Certification (The title page must display the seal and signature of the certifying P.E. or L.G. and the name and
certification number of the company or corporation, if applicable [See 15A NCAC 2L.0103(e)].)
I, Patrick R. Kelly , a Professional Engineer/ Licensed Geologist] (circle one) for
Mid -Atlantic Associates, Inc. (firm or company of employment), do certify that the information contained in this report is
correct and accurate to the best of my knowledge.
(Please Affix Seal and Signature)
Mid -Atlantic Associates, Inc. (Name of Company or Corporation) is licensed to practice geology/engineering (circle one or both) in North
Carolina. The certification number of the company or corporation is C-186 and F-0967
atlantic
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M id Atlantic
Engineering & Environmental Solutions
1 125 E. Morehnad Street, Suite
104
?;harictir, NC 28204-28�1-9
MAAONLINE.COM
July 2, 2019
Ms. Trudy Beverly
NCDEQ-DWM
UST Section -Mooresville Regional Office
610 East Center Avenue
Mooresville, North Carolina 82115
Subject: INITIAL ABATEMENT ACTION REPORT
LINDA LAKE DRIVE UST
7609 LINDA LAKE DRIVE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
INCIDENT NO.: PENDING
MID -ATLANTIC JOB NO. 00OH1378.00
Dear Ms. Trudy Beverly:
On behalf of Lifespan Inc. (Lifespan), Mid -Atlantic Associates, Inc. (Mid -Atlantic) submits
the enclosed Initial Abatement Action Report for the above -referenced site. If you have
any questions, please contact us at [phone].
Sincerely,
MID-ATLANT C A CIA
r
P®rick elly, P.G.
Project Geologist
cc: Kenneth Fuquay/ CEO
Lifespan, Inc.
00OH1378.00 Initial Abatement Action Report
, INC.
Greg D. Icenhour, P.G.
Vice President
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

o�
Atlantic
Engineering & Environmental Solutions
y
MAAONLINE.COM
INITIAL ABATEMENT ACTION REPORT
550-GALLON HEATING OIL UST
LINDA LAKE DRIVE UST
7609 LINDA LAKE DRIVE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
INCIDENT NO.: PENDING
July 2, 2019
Mid -Atlantic Job No. 0001­11378.00
Prepared For:
Lifespan, Inc.
1511 Shopton Road, Suite A
Charlotte, North Carolina 28127
Prepared By:
Patrick R. Kelly,4F:G.
Project Geologist
Greg D. Icenhour, P.G.
Principal Geologist
T.yE�, fNC.
2 rr, n ,,. _
3(" r
'7- 2-rY
i r
EXPERIENCED CUSTOMER FOCUSED INNOVATIVE

TABLE OF CONTENTS
1.0 SITE HISTORY AND CHARACTERIZATION............................................................................................1
1.1 INTRODUCTION.....................................................................................................1
1.2 OWNER/OPERATOR OF THE UST..........................................................................1
1.3 PROPERTY OWNER.............................................................................................. 1
1.5 CONTACTS..........................................................................................................2
1.6 UST INFORMATION...............................................................................................2
1.7 SITE CHARACTERISTICS........................................................................................2
1.8 SUMMARY OF ACTIVITIES PERFORMED TO DATE.....................................................3
2.0 UST CLOSURE PROCEDURES.....................................................................................................................3
2.1
PRE -CLOSURE PROCEDURES...............................................................................3
2.2
EXCAVATION PROCEDURES..................................................................................3
2.3
EXCAVATED SOIL.................................................................................................3
2.4
SAMPLING PROCEDURES......................................................................................4
2.5
QUALITY CONTROL MEASURES..............................................................................4
2.6
INVESTIGATIVE RESULTS......................................................................................4
3.0
INITIAL RESPONSE'AND ABATEMENT ACTION...................................................................................4
4.0 EXCAVATION OF CONTAMINATED SOIL...............................................................................................5
4.1 OVER -EXCAVATION AND SAMPLING ACTIVITIES.......................................................5
4.2 BACKFILLING PROCEDURES..................................................................................5
4.3 QUALITY CONTROL MEASURES.............................................................................5
4.4 INVESTIGATIVE RESULTS......................................................................................5
5.0 REGULATORY STATUS.................................................................................................................................6
6.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS....................................................................6
IT:T-11TA1►CeT�
Drawing 1 Topographic Site Map
Drawing 2 Soil Sample Location Map
TABLES
Table 1 UST System Information
Table 2 Soil Sampling Results
�_TJ»►1_�1C�LX+�
Appendix A UST-61 Form
Appendix B UST, Soil, and Sludge Disposal Documentation.
Appendix C Laboratory Analytical Report and Chain -of -Custody Record for
Soil Samples
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1.0 SITE HISTORY AND CHARACTERIZATION
1.1 Introduction
The subject site is a single family home, and is located at 7609 Linda Lake Drive, in
Charlotte, Mecklenburg County, North Carolina (Drawing 1). During soil sampling as
part of real estate due diligence activities on March 29, 2019, Carolina Environmental
Response discovered a release from a 550-gallon capacity heating oil underground
storage tank (UST) at the above referenced property. The location of the former UST is
shown on Drawing 2.
This report presents background information; a summary of the UST removal and closure
assessment procedures; documentation of the over -excavation of contaminated soil; the
laboratory analytical results; and our findings, conclusions and recommendations. The
opinions included herein are based on our experience and the information obtained
during the study. This report is based on limited observations made on the dates noted
using the procedures described herein. If additional information becomes available, we
request the opportunity to review the information, reassess the potential environmental
concerns and modify our conclusions and recommendations, if appropriate.
1.2 Owner/Operator of the UST
Lifespan, Inc.
Mr. Kenneth Fuquay/ CEO
1511 Shopton Road, Suite A
Charlotte, North Carolina 28127
[phone]
1.3 Property Owner
Lifespan, Inc.
Mr. Kenneth Fuquay/ CEO
1511 Shopton Road, Suite A
Charlotte, North Carolina 28127
[phone]
1.4 Facility Information.
7609 Linda Lake Dr.
Charlotte, North Carolina 28215
Facility I.D. #: TBD
Latitude: 35.245861 ° N
Longitude: 80.733052' W
Atlantic
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Initial Abatement Action Report
Linda Lake Drive UST, 7609 Linda Lake Drive
Charlotte, North Carolina
1.5 Contacts
Primary Contact: Lifespan, Inc.
Mr. Kenneth Fuquay/ CEO
1511 Shopton Road, Suite A
Charlotte, North Carolina 28127
[phone]
Closure Contractor: EHC Environmental
P. O. Box 902
Red Springs, North Carolina 28377
[phone]
Consultant: Mid -Atlantic Associates, Inc.
1125 East Morehead Street
Charlotte, North Carolina 28204
[phone]
Mr. Patrick R. Kelly
Laboratory: Shealy Environmental Services, Inc.
106 Vantage Point Drive
West Columbia, South Columbia 29172
[phone]
Ms. Kelly Nance
I9**l vb�2rel • u 5 1 t • �
July 1, 2019
Page 2
One 550-gallon capacity heating oil UST was used at the subject site to provide fuel for
the associated residence. According to information provided by Lifespan, ground
contamination from a heating oil UST on the subject site was discovered during a real
estate due diligence activities. See Drawing 2 for the former location of the tank and
Table 1 for UST Information.
1.7 Site Characteristics
The subject site is currently a residential property. The area surrounding the subject site
is residential. Surface drainage is generally to the southeast. An unnamed drainage
feature is approximately 20 feet to the east of the subject site and runs into an unnamed
pond approximately 200 feet southeast of the subject site. According to the North
Carolina Department of Environmental Quality (NCDEQ), NC Surface Water webpage,
the associated pond is a Class C waterbody. Based on a visual reconnaissance of the
adjacent properties and the Mecklenburg County Well information system, the subject site
and surrounding properties appear to be serviced by the municipal water system.
Atlantic
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Initial Abatement Action Report July 1, 2019
Linda Lake Drive UST, 7609 Linda Lake Drive Page 3
Charlotte, North Carolina
1.8 Summary of Activities Performed To Date
The subject parcel has no known previous releases. The subject UST was excavated on
May 29, 2019.
2.0 UST CLOSURE PROCEDURES
2.1 Pre -Closure Procedures
On March 29, 2019, prior to the removal of the heating oil UST, Carolina Environmental
Response personnel had sampled the soil next to the UST. The analysis identified
elevated levels of gasoline range organics (GRO) and diesel range organics (DRO)
indicating a suspected underground heating oil leak. On April 18, 2019, Mid -Atlantic
associates prepared and submitted a UST-61 24-Hour Release and UST Leak Reporting
Form to the NDEEQ. A copy of the UST-61 is included in Appendix A. On May 29, 2019,
approximately 350 gallons of heating oil and water was removed by EHC Environmental
(EHC) and transported to EHC's facility in Red Springs, North Carolina for disposal.
Following removal of the residual product from the UST, EHC removed the heating oil
UST on May 29, 2019. The disposal certificates for UST sludge are included in
Appendix B.
2.2 Excavation Procedures
The top of the UST was located approximately 2 feet below land surface (BLS). Soil was
initially removed from the top and three sides of the UST so that it could be removed from
the excavation. Upon removal of the tank, a leak from a seam on the south end of the
UST was noted. Free product was encountered in the subsurface adjacent to the UST
system. Groundwater was not encountered during excavation activities. EHC removed
the UST from the excavation, loaded it onto a trailer and transported the UST to their
facility in Red Springs, North Carolina for cleaning and disposal. As of the date of this
report, a UST Disposal certificate has not been received by Mid -Atlantic. A copy of the
UST Disposal certificate will be provided as soon as it is received.
2.3 Excavated Soil
Following removal of the UST, free product impacted soil was removed from the
excavation and direct loaded onto a dump truck for transportation and disposal.
Additional soil removed from the excavation was screened for evidence of volatile
organic vapors with a Mini Rae 3000 Photo Ionization Detector (PID). During removal
activities, the PID was used to determine the presence of potentially contaminated
soils. Over -excavation procedures were limited due to the proximity of the building
foundation. Approximately 4.14 tons of contaminated soil was transported off -site and
Atlantic
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Initial Abatement Action Report July 1, 2019
Linda Lake Drive UST, 7609 Linda Lake Drive Page 4
Charlotte, North Carolina
disposed at GTA Farms, LLC in Shannon, North Carolina. Copies of the waste
manifests and weight tickets are included in Appendix B.
2.4 Sampling Procedures
Upon UST removal, one closure soil sample (HO-1) was collected according to
procedures outlined in the NCDEQs Underground Storage Tank Section Guidelines for
Site Checks, Tank Closure, and Initial Response and Abatement. The closure sample
was collected from the native soil below the former UST at an approximate depth of 6 feet
BLS. The approximate location at which the soil sample was collected is shown on
Drawing 2. Samples were placed into pre -labeled, laboratory -supplied glassware, placed
into an ice -filled coolers and transported under chain -of -custody to Shealy Environmental
Services, Inc. (Shealy) in West Columbia, South Carolina for analysis of total petroleum
hydrocarbons gasoline range organics (TPH-GRO) and diesel range organics (TPH-DRO)
by EPA Methods 5035 and 3550, respectively.
2.5 Quality Control Measures
The UST closure soil samples were collected from the track hoe bucket. New nitrile
gloves were worn during the collection and handling of the soil. Each sample was placed
into pre -labeled, laboratory -supplied glassware, placed into an ice -filled cooler and
shipped under chain -of -custody control to Prism for analysis.
2.6 Investigative Results
A laboratory analytical report for the UST closure soil sample is provided in Appendix C
and summarized in Table 2. As summarized, the closure samples (HO-1) exhibited TPH-
GRO and DRO concentrations exceeding the NCDEQ UST Section's action level of 50
milligrams per kilogram (mg/Kg) for GRO and 100 mg/Kg for DRO.
3.0 INITIAL RESPONSE AND ABATEMENT ACTION
During UST removal, indications of petroleum impacted soil were observed. According to
procedures outlined in the NCDEQ's Underground Storage Tank Section Guidelines for
Site Checks, Tank Closure, and Initial Response and Abatement, over -excavation of
contaminated soil was performed, and is described below.
Atlantic
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Initial Abatement Action Report July 1, 2019
Linda Lake Drive UST, 7609 Linda Lake Drive Page 5
Charlotte, North Carolina
4.0 EXCAVATION OF CONTAMINATED SOIL
4.1 Over -Excavation and Samplina Activities
Immediately following the removal of the UST, soils were excavated to remove the visible
free product in the excavation. Following the removal of the free product contaminated
soils, Mid -Atlantic directed EHC to excavate additional soil for post excavation sampling.
The excavated soils were direct loaded onto a dump truck for transportation and disposal.
Samples were periodically collected from the floor and sidewalls of the excavated area
and scanned with the PID to monitor cleanup progress. Excavation activities were
terminated due to concerns of undermining the foundation of the building. Following the
completion of excavation activities, confirmatory soil samples (SW-N, SW-E, SW-S, SW-
W, and BOTTOM) were collected and prepared for laboratory analysis. The five over -
excavation samples were submitted for analysis for volatile organic compounds (VOCs)
using EPA Method 5035/8260, semi -volatile organic compounds (SVOCs) using EPA
Method 8270, and volatile petroleum hydrocarbons (VPH) and extractable petroleum
hydrocarbons (EPH) using the Massachusetts Department of Environmental Protection
(MADEP) methods, in accordance with NCDEQ UST Section guidelines. The locations of
the confirmatory samples and the limits of the excavation are shown on Drawing 2.
Copies of the laboratory analytical reports for this project are provided in Appendix C.
Excavated soils were placed into a dump truck for disposal. A total of 4.14 tons of soil
was disposed by EHC. Soil disposal manifests and weight tickets are included in
Appendix B.
4.2 Backfilling Procedures.
Upon removal of the UST, collection of closure samples, and over -excavation activities,
the excavation was backfilled. Backfill material was clean imported fill provided by
EHC.
4.3 Quality Control Measures
The over -excavation soil samples were retrieved using the excavator bucket. Samples
were collected so that sampled soils did not have contact with the bucket. New nitrile
gloves were worn during the collection and handling of each soil sample. The samples
were placed into pre -labeled, laboratory -supplied glassware, placed into an ice -filled
cooler and shipped under chain -of -custody to Shealy for analysis.
4.4 Investigative Results
According to laboratory analytical results of the over -excavation samples collected,
constituents of concern (COC) were detected in the over -excavation confirmation
samples. COCs were detected above the NCDEQ soil -to -groundwater Maximum Soil
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Initial Abatement Action Report
Linda Lake Drive UST, 7609 Linda Lake Drive
Charlotte, North Carolina
July 1, 2019
Page 6
Contaminant Concentrations (MSCCs) and Residential MSCCs in soil samples SW-N,
SW-W, SW-S, and SW-E. Please refer to Table 2 and Appendix C for a complete list
of detected constituents.
5.0 REGULATORY STATUS
UST closure soil sampling indicated that a release had occurred from the UST. Post
excavation soil samples indicates that soil concentrations above the soil -to -groundwater
MSCCS and residential MSCCs were detected in the sidewall samples. No exceedances
of the MSCCs were detected in sample collected from the excavation bottom. No water
supply wells were identified within 150 feet of the source area. As such, the subject site is
considered low risk.
6.0 SUMMARY, CONCLUSIONS AND RECOMMENDATIONS
UST closure and initial abatement activities are summarized as follows:
• One UST; a 550 .gallon capacity heating oil UST was removed during closure
activities;
• Petroleum -contaminated soil (4.14 tons) were excavated and transported off -site
for disposal, and
• Based on the laboratory results for post -excavation confirmatory soil samples,
petroleum impacted soils in excess of the Residential MSCCs remains in the
subsurface.
• The site is considered low risk according to the NCDEQ Guidelines for Site
Checks, Tank Closure, and Initial Response and Abatement for UST Releases.
Mid -Atlantic recommends that this incident be closed with a Conditional NFA
designation pending the completion of a Notice of Residual Petroleum (NORP) and
public notification.
-a Atlantic
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DRAWINGS
=� Atlantic
Engineer;mg & Environmental So!ut on<_

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CONTOUR
INTERVAL = 10 FEET
REFERENCES:
1. USGS TOPOGRAPHIC QUADRANGLES: MINT HILL, NC;
CHARLOTTE EAST, INC; DERITA, INC; HARRISBURG, INC - 2016 0
2. PROPERTY BOUNDARY FROM MECKLENBURG COUNTY 1
Ift Mid Atlantic
Engineering & Environmental Solutions
FIGURE 1 - SITE LOCATION MAP
LINDA LAKE DRIVE UST
7609 LINDA LAKE DRIVE
CHARLOTTE, NORTH CAROLINA
SCALE:1:24,000
1,000 2,000
DRAWN
BY:
DRAFT
CHECK:
JLS
ENG.
CHECK:
PRK
4,000
= Feet
DATE:
JUNE 2019
JOB NO:
H1378.00 Task 10000
05G-H 1378.00-01
FIG NO: 1

a
SW-W
�� V�_ _-�6-
i NOTE: ALL LOCATIONS ARE APPROXIMATE
41
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sm dr
4
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v ■
Legend
SAMPLE LOCATION
0 UST LOCATION (APPROXIMATE)
® EXCAVATION EXTENT (APPROXIMATE)
0 SITE BOUNDARY
REFERENCES:
SCALE:1:120
1. 2019 AERIAL IMAGERY AND COUNTY DATA FROM
MECKLENBURG COUNTY GIS. 0
5 10
20
2. MID -ATLANTIC FIELD NOTES.
Feet
DRAWN
DATE:
FIGURE 2 - SITE MAP
BY:
JUNE 2019
LINDA LAKE DRIVE UST
Mid Atlantic
DRAFT JLS
CHECK:
JOB 8.0
H1378.00 Task 10000
Engineering& Environmental Solutions 7609 LINDA LAKE DRIVE
CHARLOTTE, NORTH CAROLINA
ENG.
CHECK: PRK
APPROVAL: GDI
GIS NO:
05G-H1378.00-02
FIG NO: 2

TABLES
17
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TABLE 1
UST SYSTEM INFORMATION
7609 Linda Lakes Drive
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
MID -ATLANTIC JOB NO: OOO1-11378.00
Release
UST ID Number
Current/Last Contents
Previous Contents
Capacity (Gallons)
Tank Dimensions
Fonion
Date Installed
Status of
Associated with
UST
System? i'i
F -0001
Heating Oil
Same
550
46"-D X 74"-L
Single -walled steel
Unkown
Removed
Yes
6/2015

TABLE 2
SOIL SAMPLING RESULTS
7609 Linda Lakes Drive
CHARLOTTE, NORTH CAROLINA
FACILITY ID #: TBD
MID -ATLANTIC PROJECT NO.:
0001-11378.00
Method
TPH
Volitile Organic Compounds
Semi-Volitile Organic Compounds
MADEP
Action Level
10
10
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Soil -to -groundwater MSCC
NA
NA
0.0056
NE
4.9
1.7
NE
NE
4.3
4.6
NE
3.6
8.2
940
4.7
290
47
0.16
56
270
68
540
#
31
Residential MSCC
NA
NA
18
NE
1,560
1,564
NE
NE
1,200
3,129
NE
63
940
4,600
62
620
620
313
469
469
939
1,500
31,000
469
Industrial/Commercial MSCC
NA
NA
164
NE
40,000
40,880
NE
NE
3,200
81,760
NE
1,635
24,000
122,000
1,635
16,400
16,400
8,176
12,264
12,264
24,528
40,000
810,000
12,264
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>1 v
~ V
;a �.
O
....
L
4) v
v
v
O
LL ""
Q_
R
v
�
V
U
U
R
.0 L
U"
U
N
V v
E
N
M
d
U
W
O
rL
H
d
Q
Q
0
LL
Z
L
Q
u)
EL
o
H
d
N
U
U
U
U0 Q
U
U
�j
Q
HO-1
05/29/19
NA
357.0
220
1,200
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
SW-N
05/29/19
7
501.7
NA
NA
ND
0.76J
6.6
4.5
NA
4.9
ND
28
16
130
ND
6.6
4.6
1.1
8.0
31
28
4.2
93
1,100
6,000
7,100
1,200
790
4,500
5,290
SW-W
05/29/19
7
399.3
NA
NA
ND
NO
NO
ND
0.27 J
NO
NO
ND
NO
ND
960
2.3
NO
0.28
0.99
ND
4.0
2.0
5.6 J
200
2,300
2,500
740
160
1,500
1 1,660
SW-S
05/29/19
7.5
347.0
NA
NA
ND
ND
ND
ND
NO
NO
NO
ND
NO
4.5
NO
0.75 J
NO
ND
ND
1.4
2.1
0.49 J
24
210
550
760
130
180
330
510
SW-E
05/29/19
8
365.0
NA
NA
ND
ND
0.21 J
ND
NO
NO
NO
0.62 J
NO
2.3
NO
0.4 J
NO
ND
NO
0.85 J
0.58 J
0.32 J
6.0 J
120
2,000
2,120
500
140
660
800
BOTTOM
05/29/19
8
365.0
NA
NA
ND
ND
ND
NO
ND
NO
NO
ND
NO
2.7
NO
0.54 J
NO
ND
0.33 J
0.56 J
1.3
0.35 J
1.5 J
59
480
539
130
43
290
333
Notes:
mg/kg - milligrams per kilogram
NA - Not Analyzed
ND - Not detected at or above laboratory quantation limits
NE - Not established value
J - Estimated value above the laboratory quanitation limit but below
the reporting
limit
Bold values exceed the NCDEQ Action Level and/or the
Soil -to -groundwater MSCC
Shaded Vlaues exceed the NDEQ Residential MSCC
MSCC - Maximum Soil Contaminant Concentration
# - Health based level > 100

APPENDIX A
UST-61 FORM
w _ Atlantic
Evigine-ering & Environmental Solutions

UST-61
24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
in NC suspected release
(DWM USE ONLY)
Suspected Contamination? (Y/N) Yes
Facility ID Number
Incident # Risk (H,I,L,U)
Confirmed GW Contamination? (Y/N) NO
Date Leak Discovered March 29, 2019
Received On Received By
Confirmed Soil Contamination ?(Y/N) Yes
Comm/Non-Commercial? NON
Reported by (circle one): Phone, Fax or Report
Samples Taken?(Y/N) Yes - Lab Data Attached
Reg/Non-regulated? NON
Region
Free Product? (Y/N) If Yes, State Greatest
Thickness
INCIDENT DESCRIPTION
Incident Name: 7609 Linda Lake Drive
Address: 7609 Linda Lake Drive
County: Mecklenburg
City/Town: Charlotte
Zip Code: 28215
Regional Office (circle one): Asheville Mooresville, ayetteviIle,
Raleigh, Washington, Wilmington, Wins on- a em
Latitude (decimal degrees): 35.245964 Longitude (decimal degrees) : 80.733156
Obtained by:
❑GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)
❑Topographic map
❑GIS Address matching
®Other Google Earth
❑unknown
Describe location:
One soil sample collected on March 29, 2019 as part of real estate due diligence
indicated TPH GRO concentrations of 45.2 mg/kg and DRO concentrations of
3,770 mg/kg. UST system was not in use at the time of discovery. No known sensitive
receptors are believed to be impacted. UST remains in place.
Single-family residential
neighborhood.
HOW RELEASE WAS DISCOVERED (Release code)
(Check one)
❑Release Detection Equipment or Methods ❑Visual/Odor ❑Groundwater Contamination
❑During UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination
x]Property Transfer ❑Water Supply Well Contamination ❑Other (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check primary source) (Check primary cause) (Check one) (Check primary product type released)
❑X Tank ❑ Spill X❑ Petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil
❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend
❑X ❑
❑ Dispenser ❑X Corrosion (Suspected) ❑Both Heating Oil Vegetable Oil 100%
❑ Other Petroleum ❑ E10 - E20
❑ Submersible Turbine Pump ❑Physical/Mechanical
Location Products
❑ (Check one) Metals Delivery Problem Damage ❑ E21 - E84
❑
❑ Install Problem ❑ E85 - E99
❑ Spill Bucket ❑ Other Inorganics
❑ Other [-]Facility ❑Ethanol 100%
❑ Other ❑ Other Organics
❑ Unknown ❑X Residence ❑ E01 - E09
❑ Unknown
❑Other
Definitions presented on reverse
Definitions presented on reverse
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes
2. No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company Unknown
Point of Contact
Address
City
State
Zip Code
Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company
Address
Unknown
City
State
Zip Code
Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner
Lifespan Inc.
Address
1511 Shopton Road, Suite A
City Charlotte
State NC
Zip Code 28217
Telephone Number
[phone]
Draw Sketch of Area (showing two major road intersections) or Attach Map
Map Attached
_77Person Reporting Incident Greg D. Icenhour
Company Mid -Atlantic Associates, Inc.
Telephone Number [phone]
Title Principal Geologist
Address 1125 E. Morehead Street, Ste. 104, Charlotte, NC 28204
Date April 18, 2019
UST Form 61 (02/19)
Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

LO 0\so VP
qO
.O 0
7609 Linda Lake Drive
0 40
ds
� J
Date Printed: 4/18/2019 9:04:38 AM
0 0.005)'01 0.02 Miles E
This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, surveys, planimetric maps, and other public records and data.
Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification. Mecklenburg County and its mapping contractors assume no legal
responsibility for the information contained herein.

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 05, 2019
Lee Shank
Carolina Environmental Respons
5648 Daphne Drive
Charlotte, NC 28269
RE: Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
Dear Lee Shank:
Enclosed are the analytical results for sample(s) received by the laboratory on March 29, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
f&ro- l
Amanda Payne
[e-mail]
[phone]
Project Manager
Enclosures
cc: Steve Hamilton, Carolina Environmental Response Team
Cassandra Kisiah, Carolina Environmental Response
Team
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 1 of 14

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Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
Charlotte Certification IDs
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
7609 Linda Lake Dr
92423343
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92423343001
Tank #1
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
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Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
Lab Sample ID
Method
92423343001
EPA 8015C Modified
EPA 8015C Modified
ASTM D2974-87
SUMMARY OF DETECTION
Client Sample ID
Parameters
Tank #1
Diesel Range Organics(C10-C28)
Gas Range Organics (C6-C10)
Percent Moisture
Result
Units
3770
mg/kg
45.2
mg/kg
24.8
%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Report Limit
Analyzed
66.3
04/04/1915:42
7.1
03/31 /19 19:06
0.10
03/29/1916:22
Qualifiers
Page 4 of 14

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PROJECT NARRATIVE
Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Carolina Environmental Response Team
Date: April 05, 2019
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 8015C Modified. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 466960
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
• Tank #1 (Lab ID: 92423343001)
• n-Pentacosane (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
Method: EPA 8015C Modified
Description: Gasoline Range Organics
Client: Carolina Environmental Response Team
Date: April 05, 2019
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 8015C Modified. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 466516
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
• Tank #1 (Lab ID: 92423343001)
• 4-Bromofluorobenzene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
Sample: Tank #1
Lab ID: 92423343001 Collected: 03/29/19 13:10 Received: 03/29/19 14:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
3770 mg/kg 66.3 10 04/03/19 15:53 04/04/19 15:42
Surrogates
n-Pentacosane (S)
0 % 33-129 10 04/03/19 15:53 04/04/19 15:42 629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
45.2 mg/kg 7.1 1 03/31/19 14:46 03/31/19 19:06
Surrogates
4-Bromofluorobenzene (S)
161 % 63-130 1 03/31/19 14:46 03/31/19 19:06 460-00-4 S5
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
24.8 % 0.10 1 03/29/19 16:22
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
QC Batch: 466516
Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E
Analysis Description: Gasoline
Range Organics
Associated Lab Samples: 92423343001
METHOD BLANK: 2535606
Matrix: Solid
Associated Lab Samples: 92423343001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 6.0
03/31/19 13:20
4-Bromofluorobenzene (S)
%
93 63-130
03/31/19 13:20
LABORATORY CONTROL SAMPLE: 2535607
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50.4 51.6
102 70-130
4-Bromofluorobenzene (S)
%
117 63-130
MATRIX SPIKE SAMPLE: 2535609
92423362004 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 58.9
73.0 114
40-155
4-Bromofluorobenzene (S)
%
123
63-130
SAMPLE DUPLICATE: 2535608
92423362001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Gas Range Organics (C6-C10)
mg/kg
10.9 13.8
24
4-Bromofluorobenzene (S)
%
110 129
16
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
QC Batch: 466960 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92423343001
METHOD BLANK: 2537732 Matrix: Solid
Associated Lab Samples: 92423343001
Blank Reporting
Parameter Units Result Limit Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 04/03/19 12:50
n-Pentacosane(S) % 74 33-129 04/03/1912:50
LABORATORY CONTROL SAMPLE:
2537733
Parameter
Units
Diesel Range Organics(C10-C28)
mg/kg
n-Pentacosane(S)
%
MATRIX SPIKE SAMPLE:
2537734
Parameter
Units
Diesel Range Organics(C10-C28)
mg/kg
n-Pentacosane(S)
%
SAMPLE DUPLICATE: 2537735
Parameter
Diesel Range Organics(C10-C28)
n-Pentacosane(S)
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
67.1 61.8 92 43-130
79 33-129
92423331003 Spike MS
Result Conc. Result
ND 98.6 88.8
92423331004 Dup
Units Result Result
mg/kg ND ND
% 67 66
MS % Rec
% Rec Limits Qualifiers
90 10-130
80 33-129
RPD Qualifiers
N
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
QC Batch: 466378 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92423343001
SAMPLE DUPLICATE: 2535004
92423163001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 11.9 14.0 16
SAMPLE DUPLICATE: 2535005
92423197001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 81.1 82.8 2
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: 7609 Linda Lake Dr
Pace Project No.: 92423343
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
7609 Linda Lake Dr
92423343
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92423343001
Tank #1
EPA 3546
466960 EPA 8015C Modified
467087
92423343001
Tank #1
EPA 5030B
466516 EPA 8015C Modified
466519
92423343001
Tank #1
ASTM D2974-87
466378
REPORT OF LABORATORY ANALYSIS
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Page 13 of 1

Document Name:
Sample Condition Upon Recei
Document No.:
F-CAR-05-033-Rev.06
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform,TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # rWo# ; g2423343
PM: AP Due Date: 04/05/19
CLIENT: 92—CERT
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
tot k
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certiftcation Office [I,e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 14 of 14

APPENDIX B
UST, SOIL, AND SLUDGE DISPOSAL
DOCUMENTATION.
Atlantic
�::gireer:ng & Environmental Solutions

y SOWHAZARDOUS
WASTE
MANIFEST
EMERGENCY PHONE NO.
[phone]
GTA. Farms. LLC
1295 McNeill Lake Road
Shannon, NC 28386
[phone]
SRU 600072
Name
re I ds �h / aMailing Address
lyy e+r aC � Ir
0'
DESCRIPTION OF MATERIALS (Additional Information on Back►
Manifest Document No
Generator GPS Location Pa e
of
US EPA ID No.
Phone No.
Contact
HM
USDOT Proper Shipping Name
Hazard
Class or Div.
UN/NA,
ID No.
Packing
Group
Containers.
Qty Type
Total
Quantity
Unit
Wt/Vol
a.
Petroleum Contaminated Soil
b
re e ; "J tep<
�----
d
c
MAQTG
I NOTE: SEE SOIL ANALYTICAL REQUIREMENTS ON BACK OF THIS FORM
GENERATOR'S CERTIFICATION
This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in proper condition for
transportation according to the applicable regulations of the Department of Transportation. I further certify that none of the materials described above are
a hazardous waster as defined by EPA 40 CPR Part 261 or any applicable state law, and unless specifically identified above; the materials contain less
than 1, 000 ppm total halogens and do not contain quantifiable levers (2 ppm) of PCBs as.defined b EPA 40 CFR Parts 279'and 761.
c�nntedFryped N me o (L 0�s 114 SiMOF,)O�
Mo/Day/Yr.
C-as
I hereby acknowledge receipt of the above -described materials for'transport
from the generator site listed above.
Address
Transporter or Unit No.
Signature Mo/Day/Yr.
I hereby acknowledge that the above-describedmaterials were received from
EPA ID No.
the generator site and were transported to the facility listed below.
Phone
Signature f
���^(AJ► /
o/Day/Yr:
FACILITY
INFORMATION
Facility GTA Farms, LLC.
I hereby acknowledge receipt of the materials covered by this manifest
Mailing Address Post
except for
any dis r
pancy noted below'.
Office Box 547
Red Springs, NC 23877
nature Receipt Date
Facility Permit No. SRU 600072
Discrepancies / Routing Codes / Handling Methods
Phone [phone] or 910 850-4299
Contact: Thomas Ammons
GPS LOCATION:
WHITE: Generator CANARY: Transporter #1 PINK: Transporter #2 GOLD: Generator

NON -HAZARDOUS 1. Generator ID Number 2. Pa e 1 of 3. Emergency Response Phone 4. Waste Tracking Number
WASTE MANIFEST 2- l/ qr r� / �,�✓
6
5. Generator's Name and Mailing Address Generato s Sit A` ss (' di �m rent tha ailinngladdress)
y �� P7
d:tw,
Generator's Phone:6.
rTransporter 1C mpany Name U.S. EPA ID Number
�i ///,jj
�ransporxer2_Company Name U.S. EPA ID Number
8. Designated Facility Name and Site Address U.S. EPA ID Number
Facili 's Phone:
9. Waste Shipping Name and Description
10. Containers
11. Total
12. Unit
No.
Type
„Lu
Quantity
Wt.Nol.
o[
1'
Q
2.
3.
4.
13. Special Handling Instructions and Additional Information
14. GENERATOR'S/OFFEROR'S CERTIFICATION: I hereby declare that the contents of this consignment are fully and accurately described above by the proper shipping name, and are classified, packaged,
marked and labeled/placarded, and are in all respects in proper condition for transport according to applicable' ternational
tional governmental regulations.
Gen rator's/Offeroes Pri�J d/Typed Name ig atue Month Day Year
-.r
F—
15. International Shipments
❑ Import to U.S. ❑
z
Export from U.S. of entry/exit:
Transporter Signature for exports only): ate leavin U.S.:
w
16. Transporter Acknowledgment of Receipt of Materials
r—
IL
Tr orter 1 Printed/T ad Name
tSigna Month Day Year
�5
N
Tr nsporter 2 Printed/Typed Name Signature Month Day Year
17. Discrepancy
17a. Discrepancy Indication Space
❑ Quantity ❑ Type ❑ Residue ❑ Partial Rejection ❑ Full Rejection
17b. Alternate Facility (or Generator) Manifest Reference Number:
3
U.S. EPA ID Number
U
rai
Facility's Phone:
w
17c. Signature of Alternate Facility (or Generator)
a
Month Day Year
z
w
0
18. Designated Facility Owner or Operator: Certification of receipt of materials covered by the manifest except as noted in Item 17a
Printedlfyped Name Signature
\ Month Dayy� Year
Un
icn o� c• n `� 1
aa,ncv. a1VV) V DESIGNATED FACILITY TO GENERATOR

APPENDIX C
LABORATORY ANALYTICAL REPORT
AND CHAIN -OF -CUSTODY RECORD
FOR SOIL SAMPLES
Atlantic
Engineering & Environmental Solutions

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Mid -Atlantic Associates, Inc.
1125 East Morehead Street
Suite # 104
Charlotte, NC 28204
Attention: Patrick Kelly
Project Name: 7609 Linda Lake Drive UST
Lot Number:UE31010
Date Completed:06/12/2019
06/12/2019 4:03 PM
Approved and released by:
Project Manager: Kelly M. Nance
PCCRFp d
AM
AC CF ED I T E D
qB
11900 ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 88

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Mid -Atlantic Associates, Inc.
Lot Number: UE31010
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
TPH-GRO
12 - The hydrocarbon pattern resembles #2 diesel fuel.
Volatiles
The continuing calibration verification (CCV) associated with samples -002, -003, -004, -005, and -006
had 2-hexanone and methyl acetate recovered above the acceptance limits. This could potentially result
in a high bias on analytical results. There were no detections above the LOQ for these compounds in the
associated samples; therefore, data quality is not impacted.
Samples -003, -004, -005, and -006 were analyzed via high level analysis due to the sample matrix. The
reporting limits have been raised accordingly.
Semivolatiles
The matrix spike/matrix spike duplicate (MS/MSD) associated with sample -003 had multiple compounds
recovered outside of the acceptance limits. Additionally, a number of RPDs exceeded the acceptance
limit. The laboratory control sample (LCS) was recovered within the required acceptance limits; therefore,
this likely demonstrates a matrix effect.
MA EPH
Sample -002 was diluted 10X due to high concentrations of target compounds. As a result, the associated
surrogates were recovered outside of the acceptance limits. No corrective action was required, as
dilutions of 5X and greater impact recovery accuracy.
Sample -003 had surrogates recovered outside of the acceptance limits due to objective evidence of
matrix interference.
MADEP VPH
Samples -002, -003, -004, and -005 had surrogates recovered outside of the acceptance limits due to
objective evidence of matrix interference.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 88

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 88

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Mid -Atlantic Associates, Inc.
Lot Number: UE31010
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
HO-1
Solid
05/29/20191150
05/30/2019
002
SW-N
Solid
05/29/20191215
05/30/2019
003
SW-W
Solid
05/29/20191220
05/30/2019
004
SW-S
Solid
05/29/20191240
05/30/2019
005
SW-E
Solid
05/29/20191235
05/30/2019
006
BOTTOM
Solid
05/29/20191245
05/30/2019
(6 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 88

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Mid -Atlantic Associates, Inc.
Lot Number: UE31010
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001
HO-1
Solid
TPH-DRO
8015C
1200000
12
ug/kg
7
001
HO-1
Solid
TPH-GRO
8015C
220000
ug/kg
8
002
SW-N
Solid
Cyclohexane
8260D
760
J
ug/kg
9
002
SW-N
Solid
Ethylbenzene
8260D
6600
ug/kg
9
002
SW-N
Solid
Isopropylbenzene
8260D
4500
ug/kg
9
002
SW-N
Solid
Methylcyclohexane
8260D
4900
ug/kg
9
002
SW-N
Solid
Xylenes (total)
8260D
28000
ug/kg
10
002
SW-N
Solid
Anthracene
8270E
6600
ug/kg
11
002
SW-N
Solid
1,1'-Biphenyl
8270E
16000
ug/kg
11
002
SW-N
Solid
Dibenzofuran
8270E
4600
ug/kg
11
002
SW-N
Solid
Fluoranthene
8270E
1100
ug/kg
11
002
SW-N
Solid
Fluorene
8270E
8000
ug/kg
11
002
SW-N
Solid
2-Methylnaphthalene
8270E
130000
ug/kg
12
002
SW-N
Solid
Naphthalene
8270E
31000
ug/kg
12
002
SW-N
Solid
Phenanthrene
8270E
28000
ug/kg
12
002
SW-N
Solid
Pyrene
8270E
4200
ug/kg
12
002
SW-N
Solid
C11 - C22 Aromatics
MADEP-EPH-
4500
mg/kg
13
002
SW-N
Solid
C9 - C18 Aliphatics
MADEP-EPH-
6000
mg/kg
14
002
SW-N
Solid
C19 - C36 Aliphatics
MADEP-EPH-
1200
mg/kg
14
002
SW-N
Solid
C5 - C8 Aliphatics
MADEP-VPH-
93
mg/kg
15
002
SW-N
Solid
C9 - C12 Aliphatics
MADEP-VPH-
1100
mg/kg
15
002
SW-N
Solid
C9 - C10 Aromatics
MADEP-VPH-
790
mg/kg
16
003
SW-W
Solid
Methyl acetate
8260D
270
J
ug/kg
17
003
SW-W
Solid
Acenaphthene
8270E
960
ug/kg
19
003
SW-W
Solid
Anthracene
8270E
2300
ug/kg
19
003
SW-W
Solid
Fluoranthene
8270E
280
ug/kg
19
003
SW-W
Solid
Fluorene
8270E
990
ug/kg
19
003
SW-W
Solid
Phenanthrene
8270E
4000
ug/kg
20
003
SW-W
Solid
Pyrene
8270E
2000
ug/kg
20
003
SW-W
Solid
C11 - C22 Aromatics
MADEP-EPH-
1500
mg/kg
21
003
SW-W
Solid
C9 - C18 Aliphatics
MADEP-EPH-
2300
mg/kg
22
003
SW-W
Solid
C19 - C36 Aliphatics
MADEP-EPH-
740
mg/kg
22
003
SW-W
Solid
C5 - C8 Aliphatics
MADEP-VPH-
5.6
J
mg/kg
23
003
SW-W
Solid
C9 - C12 Aliphatics
MADEP-VPH-
200
mg/kg
23
003
SW-W
Solid
C9 - C10 Aromatics
MADEP-VPH-
160
mg/kg
24
004
SW-S
Solid
Anthracene
8270E
750
J
ug/kg
27
004
SW-S
Solid
2-Methylnaphthalene
8270E
4500
ug/kg
28
004
SW-S
Solid
Naphthalene
8270E
1400
ug/kg
28
004
SW-S
Solid
Phenanthrene
8270E
2100
ug/kg
28
004
SW-S
Solid
Pyrene
8270E
490
J
ug/kg
28
004
SW-S
Solid
C11 - C22 Aromatics
MADEP-EPH-
330
mg/kg
29
004
SW-S
Solid
C9 - C18 Aliphatics
MADEP-EPH-
550
mg/kg
30
004
SW-S
Solid
C19 - C36 Aliphatics
MADEP-EPH-
130
mg/kg
30
004
SW-S
Solid
C5 - C8 Aliphatics
MADEP-VPH-
24
mg/kg
31
004
SW-S
Solid
C9 - C12 Aliphatics
MADEP-VPH-
210
mg/kg
31
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 88

Detection Summary (Continued)
Lot Number: UE31010
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
004
SW-S
Solid
C9 - C10 Aromatics
MADEP-VPH-
180
mg/kg
32
005
SW-E
Solid
Ethylbenzene
8260D
210
J
ug/kg
33
005
SW-E
Solid
Xylenes (total)
8260D
620
J
ug/kg
34
005
SW-E
Solid
Anthracene
8270E
400
J
ug/kg
35
005
SW-E
Solid
2-Methylnaphthalene
8270E
2300
ug/kg
36
005
SW-E
Solid
Naphthalene
8270E
850
J
ug/kg
36
005
SW-E
Solid
Phenanthrene
8270E
580
J
ug/kg
36
005
SW-E
Solid
Pyrene
8270E
320
J
ug/kg
36
005
SW-E
Solid
C11 - C22 Aromatics
MADEP-EPH-
660
mg/kg
37
005
SW-E
Solid
C9 - C18 Aliphatics
MADEP-EPH-
2000
mg/kg
38
005
SW-E
Solid
C19 - C36 Aliphatics
MADEP-EPH-
500
mg/kg
38
005
SW-E
Solid
C5 - C8 Aliphatics
MADEP-VPH-
6.0
J
mg/kg
39
005
SW-E
Solid
C9 - C12 Aliphatics
MADEP-VPH-
120
mg/kg
39
005
SW-E
Solid
C9 - C10 Aromatics
MADEP-VPH-
140
mg/kg
40
006
BOTTOM
Solid
Anthracene
8270E
540
J
ug/kg
43
006
BOTTOM
Solid
Fluorene
8270E
330
J
ug/kg
43
006
BOTTOM
Solid
2-Methylnaphthalene
8270E
2700
ug/kg
44
006
BOTTOM
Solid
Naphthalene
8270E
560
J
ug/kg
44
006
BOTTOM
Solid
Phenanthrene
8270E
1300
ug/kg
44
006
BOTTOM
Solid
Pyrene
8270E
350
J
ug/kg
44
006
BOTTOM
Solid
C11 - C22 Aromatics
MADEP-EPH-
290
mg/kg
45
006
BOTTOM
Solid
C9 - C18 Aliphatics
MADEP-EPH-
480
mg/kg
46
006
BOTTOM
Solid
C19 - C36 Aliphatics
MADEP-EPH-
130
mg/kg
46
006
BOTTOM
Solid
C5 - C8 Aliphatics
MADEP-VPH-
1.5
J
mg/kg
47
006
BOTTOM
Solid
C9 - C12 Aliphatics
MADEP-VPH-
59
mg/kg
47
006
BOTTOM
Solid
C9 - C10 Aromatics
MADEP-VPH-
43
mg/kg
48
(71 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 88

TPH - DRO
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-001
Description: HO-1 Matrix: Solid
Date Sampled:05/29/2019 1150 % Solids: 76.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 06/05/2019 2101 CHG 05/31/2019 2314 18378
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TPH-DRO 8015C 1200000 12 8800 4200 ug/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl
98 55-120
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 88

TPH - GRID
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-001
Description: HO-1 Matrix: Solid
Date Sampled:05/29/2019 1150 % Solids: 76.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8015C 10 05/31/20191815 JJG 18370
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TPH-GRO 8015C 220000 69000 35000 ug/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene
98 23-179
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035 High 8260D
4 06/03/2019 1848 JM1
18534
6.25
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
5600
2200
ug/kg
1
Benzene
71-43-2
8260D
ND
1400
560
ug/kg
1
Bromodichloromethane
75-27-4
8260D
ND
1400
560
ug/kg
1
Bromoform
75-25-2
8260D
ND
1400
560
ug/kg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
1400
840
ug/kg
1
2-Butanone (MEK)
78-93-3
8260D
ND
5600
1100
ug/kg
1
Carbon disulfide
75-15-0
8260D
ND
1400
560
ug/kg
1
Carbon tetrachloride
56-23-5
8260D
ND
1400
560
ug/kg
1
Chlorobenzene
108-90-7
8260D
ND
1400
560
ug/kg
1
Chloroethane
75-00-3
8260D
ND
1400
560
ug/kg
1
Chloroform
67-66-3
8260D
ND
1400
560
ug/kg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
1400
840
ug/kg
1
Cyclohexane
110-82-7
8260D
760 J
1400
560
ug/kg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
1400
560
ug/kg
1
Dibromochloromethane
124-48-1
8260D
ND
1400
560
ug/kg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
1400
560
ug/kg
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
1400
560
ug/kg
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
1400
560
ug/kg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
1400
560
ug/kg
1
Dichlorodifluoromethane
75-71-8
8260D
ND
1400
840
ug/kg
1
1,1-Dichloroethane
75-34-3
8260D
ND
1400
560
ug/kg
1
1,2-Dichloroethane
107-06-2
8260D
ND
1400
560
ug/kg
1
1,1-Dichloroethene
75-35-4
8260D
ND
1400
560
ug/kg
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
1400
560
ug/kg
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
1400
560
ug/kg
1
1,2-Dichloropropane
78-87-5
8260D
ND
1400
560
ug/kg
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
1400
560
ug/kg
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
1400
560
ug/kg
1
Ethylbenzene
100-41-4
8260D
6600
1400
560
ug/kg
1
2-Hexanone
591-78-6
8260D
ND
2800
1100
ug/kg
1
Isopropylbenzene
98-82-8
8260D
4500
1400
560
ug/kg
1
Methyl acetate
79-20-9
8260D
ND
1400
560
ug/kg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
1400
560
ug/kg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
2800
1100
ug/kg
1
Methylcyclohexane
108-87-2
8260D
4900
1400
560
ug/kg
1
Methylene chloride
75-09-2
8260D
ND
1400
560
ug/kg
1
Styrene
100-42-5
8260D
ND
1400
560
ug/kg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
1400
560
ug/kg
1
Tetrachloroethene
127-18-4
8260D
ND
1400
560
ug/kg
1
Toluene
108-88-3
8260D
ND
1400
560
ug/kg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1400
560
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
1400
560
ug/kg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
1400
560
ug/kg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
1400
560
ug/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 High 8260D 4 06/03/2019 1848 JM1 18534 6.25
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
1400
560
ug/kg
1
Trichlorofluoromethane
75-69-4
8260D
ND
1400
560
ug/kg
1
Vinyl chloride
75-01-4
8260D
ND
1400
840
ug/kg
1
Xylenes (total)
1330-20-7
8260D
28000
2800
1100
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
111 47-138
97 53-142
111 68-124
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
5 06/11/2019
2107 SCD
06/01/2019 2311 18379
2 3546
8270E
50 06/12/2019 1332 SCD
06/01/2019 2311 18379
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
85
32
ug/kg
1
Acenaphthylene
208-96-8
8270E
ND
85
20
ug/kg
1
Acetophenone
98-86-2
8270E
ND
430
44
ug/kg
1
Anthracene
120-12-7
8270E
6600
85
16
ug/kg
1
Atrazine
1912-24-9
8270E
ND
430
32
ug/kg
1
Benzaldehyde
100-52-7
8270E
ND
430
32
ug/kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
85
13
ug/kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
85
11
ug/kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
85
12
ug/kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
85
24
ug/kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
85
14
ug/kg
1
1,1'-Biphenyl
92-52-4
8270E
16000
4300
320
ug/kg
2
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
430
32
ug/kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
430
32
ug/kg
1
Caprolactam
105-60-2
8270E
ND
430
75
ug/kg
1
Carbazole
86-74-8
8270E
ND
430
32
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
430
43
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
430
36
ug/kg
1
4-Chloroaniline
106-47-8
8270E
ND
430
37
ug/kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
430
32
ug/kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
430
35
ug/kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
430
80
ug/kg
1
2-Chlorophenol
95-57-8
8270E
ND
430
68
ug/kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
430
32
ug/kg
1
Chrysene
218-01-9
8270E
ND
85
20
ug/kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
85
19
ug/kg
1
Dibenzofuran
132-64-9
8270E
4600
430
32
ug/kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
430
64
ug/kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
430
42
ug/kg
1
Diethylphthalate
84-66-2
8270E
ND
430
32
ug/kg
1
Dimethyl phthalate
131-11-3
8270E
ND
430
32
ug/kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
430
69
ug/kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
430
62
ug/kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
2100
160
ug/kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
2100
160
ug/kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
830
78
ug/kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
830
68
ug/kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
430
32
ug/kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
430
160
ug/kg
1
Fluoranthene
206-44-0
8270E
1100
85
14
ug/kg
1
Fluorene
86-73-7
8270E
8000
85
12
ug/kg
1
Hexachlorobenzene
118-74-1
8270E
ND
430
32
ug/kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
430
54
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 5 06/11/2019 2107 SCD 06/01/2019 2311 18379
2 3546 8270E 50 06/12/2019 1332 SCD 06/01/2019 2311 18379
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachlorocyclopentadiene
77-47-4
8270E
ND
2100
160
ug/kg
Hexachloroethane
67-72-1
8270E
ND
430
35
ug/kg
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
85
17
ug/kg
Isophorone
78-59-1
8270E
ND
430
40
ug/kg
2-Methylnaphthalene
91-57-6
8270E
130000
850
370
ug/kg
2-Methylphenol
95-48-7
8270E
ND
430
110
ug/kg
3+4-Methylphenol
106-44-5
8270E
ND
830
110
ug/kg
Naphthalene
91-20-3
8270E
31000
850
300
ug/kg
2-Nitroaniline
88-74-4
8270E
ND
830
120
ug/kg
3-Nitroaniline
99-09-2
8270E
ND
830
120
ug/kg
4-Nitroaniline
100-01-6
8270E
ND
830
130
ug/kg
Nitrobenzene
98-95-3
8270E
ND
430
50
ug/kg
2-Nitrophenol
88-75-5
8270E
ND
830
64
ug/kg
4-Nitrophenol
100-02-7
8270E
ND
2100
660
ug/kg
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
430
37
ug/kg
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
430
32
ug/kg
Pentachlorophenol
87-86-5
8270E
ND
2100
170
ug/kg
Phenanthrene
85-01-8
8270E
28000
850
140
ug/kg
Phenol
108-95-2
8270E
ND
430
40
ug/kg
Pyrene
129-00-0
8270E
4200
85
18
ug/kg
2,4,5-Trichlorophenol
95-95-4
8270E
ND
430
32
ug/kg
2,4,6-Trichlorophenol
88-06-2
8270E
ND
430
32
ug/kg
Run 1
Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery
Limits Q
% Recovery
Limits
2-Fluorobiphenyl
130
24-137
82
24-137
2-Fluorophenol
54
16-136
32
16-136
Nitrobenzene-d5
115
12-144
68
12-144
Phenol-d5
45
26-148
37
26-148
Terphenyl-d14
102
20-127
116
20-127
2,4,6-Tribromophenol
101
27-128
75
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 88

MA EPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 10 06/06/2019 1721 CHG 06/02/2019 2016 18432
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH- 4500 130 130 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) N 226 40-140
2-Fluorobiphenyl (fractionation 1) N 435 40-140
o - Terphenyl (aromatic) 46 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 13 of 88

MA EPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 20 06/06/2019 1651 CHG 06/02/2019 2016 18431
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 6000 260 260 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH- 1200 260 260 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
50 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 14 of 88

MADEP VPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date
Batch
1
VPH
MADEP-VPH-18-2.1
4
06/07/20191631 JJG
19104
2
VPH
MADEP-VPH-18-2.1
10
06/10/20191506 JJG
19250
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- 93 25 5.1 mg/kg 1
C9 - C12 Aliphatics MADEP-VPH- 1100 63 13 mg/kg 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
2,5-Dibromotoluene (FID)
N 0.00 70-130 N 0.00 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 15 of 88

MADEP VPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-002
Description: SW-N Matrix: Solid
Date Sampled:05/29/2019 1215 % Solids: 74.9 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 4 06/07/20191631 JJG 19103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 790 8.4 3.4 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
N 0.00 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 16 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035 High 8260D
1 06/03/2019 1910 JM1
18534
4.31
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
1900
770
ug/kg
1
Benzene
71-43-2
8260D
ND
480
190
ug/kg
1
Bromodichloromethane
75-27-4
8260D
ND
480
190
ug/kg
1
Bromoform
75-25-2
8260D
ND
480
190
ug/kg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
480
290
ug/kg
1
2-Butanone (MEK)
78-93-3
8260D
ND
1900
380
ug/kg
1
Carbon disulfide
75-15-0
8260D
ND
480
190
ug/kg
1
Carbon tetrachloride
56-23-5
8260D
ND
480
190
ug/kg
1
Chlorobenzene
108-90-7
8260D
ND
480
190
ug/kg
1
Chloroethane
75-00-3
8260D
ND
480
190
ug/kg
1
Chloroform
67-66-3
8260D
ND
480
190
ug/kg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
480
290
ug/kg
1
Cyclohexane
110-82-7
8260D
ND
480
190
ug/kg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
480
190
ug/kg
1
Dibromochloromethane
124-48-1
8260D
ND
480
190
ug/kg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
480
190
ug/kg
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
480
190
ug/kg
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
480
190
ug/kg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
480
190
ug/kg
1
Dichlorodifluoromethane
75-71-8
8260D
ND
480
290
ug/kg
1
1,1-Dichloroethane
75-34-3
8260D
ND
480
190
ug/kg
1
1,2-Dichloroethane
107-06-2
8260D
ND
480
190
ug/kg
1
1,1-Dichloroethene
75-35-4
8260D
ND
480
190
ug/kg
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
480
190
ug/kg
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
480
190
ug/kg
1
1,2-Dichloropropane
78-87-5
8260D
ND
480
190
ug/kg
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
480
190
ug/kg
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
480
190
ug/kg
1
Ethylbenzene
100-41-4
8260D
ND
480
190
ug/kg
1
2-Hexanone
591-78-6
8260D
ND
960
380
ug/kg
1
Isopropylbenzene
98-82-8
8260D
ND
480
190
ug/kg
1
Methyl acetate
79-20-9
8260D
270 J
480
190
ug/kg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
480
190
ug/kg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
960
380
ug/kg
1
Methylcyclohexane
108-87-2
8260D
ND
480
190
ug/kg
1
Methylene chloride
75-09-2
8260D
ND
480
190
ug/kg
1
Styrene
100-42-5
8260D
ND
480
190
ug/kg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
480
190
ug/kg
1
Tetrachloroethene
127-18-4
8260D
ND
480
190
ug/kg
1
Toluene
108-88-3
8260D
ND
480
190
ug/kg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
480
190
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
480
190
ug/kg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
480
190
ug/kg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
480
190
ug/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 17 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 High 8260D 1 06/03/2019 1910 JM1 18534 4.31
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
480
190
ug/kg
1
Trichlorofluoromethane
75-69-4
8260D
ND
480
190
ug/kg
1
Vinyl chloride
75-01-4
8260D
ND
480
290
ug/kg
1
Xylenes (total)
1330-20-7
8260D
ND
960
380
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
111 47-138
100 53-142
104 68-124
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 18 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
10 06/11/2019 2132 SCD
06/01/2019 2311 18379
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
960
170
66
ug/kg
1
Acenaphthylene
208-96-8
8270E
ND
170
42
ug/kg
1
Acetophenone
98-86-2
8270E
ND
880
91
ug/kg
1
Anthracene
120-12-7
8270E
2300
170
34
ug/kg
1
Atrazine
1912-24-9
8270E
ND
880
66
ug/kg
1
Benzaldehyde
100-52-7
8270E
ND
880
65
ug/kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
170
26
ug/kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
170
22
ug/kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
170
25
ug/kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
170
49
ug/kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
170
28
ug/kg
1
1,1'-Biphenyl
92-52-4
8270E
ND
880
65
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
880
65
ug/kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
880
65
ug/kg
1
Caprolactam
105-60-2
8270E
ND
880
150
ug/kg
1
Carbazole
86-74-8
8270E
ND
880
65
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
880
88
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
880
73
ug/kg
1
4-Chloroaniline
106-47-8
8270E
ND
880
76
ug/kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
880
65
ug/kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
880
71
ug/kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
880
160
ug/kg
1
2-Chlorophenol
95-57-8
8270E
ND
880
140
ug/kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
880
65
ug/kg
1
Chrysene
218-01-9
8270E
ND
170
41
ug/kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
170
39
ug/kg
1
Dibenzofuran
132-64-9
8270E
ND
880
66
ug/kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
880
130
ug/kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
880
86
ug/kg
1
Diethylphthalate
84-66-2
8270E
ND
880
65
ug/kg
1
Dimethyl phthalate
131-11-3
8270E
ND
880
65
ug/kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
880
140
ug/kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
880
130
ug/kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
4300
330
ug/kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
4300
330
ug/kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
1700
160
ug/kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
1700
140
ug/kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
880
65
ug/kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
880
330
ug/kg
1
Fluoranthene
206-44-0
8270E
280
170
28
ug/kg
1
Fluorene
86-73-7
8270E
990
170
25
ug/kg
1
Hexachlorobenzene
118-74-1
8270E
ND
880
65
ug/kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
880
110
ug/kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
4300
330
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 19 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 10 06/11/2019 2132 SCD 06/01/2019 2311 18379
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
880
71
ug/kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
170
35
ug/kg
1
Isophorone
78-59-1
8270E
ND
880
81
ug/kg
1
2-Methylnaphthalene
91-57-6
8270E
ND
170
77
ug/kg
1
2-Methylphenol
95-48-7
8270E
ND
880
230
ug/kg
1
3+4-Methylphenol
106-44-5
8270E
ND
1700
220
ug/kg
1
Naphthalene
91-20-3
8270E
ND
170
61
ug/kg
1
2-Nitroaniline
88-74-4
8270E
ND
1700
240
ug/kg
1
3-Nitroaniline
99-09-2
8270E
ND
1700
240
ug/kg
1
4-Nitroaniline
100-01-6
8270E
ND
1700
260
ug/kg
1
Nitrobenzene
98-95-3
8270E
ND
880
100
ug/kg
1
2-Nitrophenol
88-75-5
8270E
ND
1700
130
ug/kg
1
4-Nitrophenol
100-02-7
8270E
ND
4300
1400
ug/kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
880
75
ug/kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
880
67
ug/kg
1
Pentachlorophenol
87-86-5
8270E
ND
4300
350
ug/kg
1
Phenanthrene
85-01-8
8270E
4000
170
29
ug/kg
1
Phenol
108-95-2
8270E
ND
880
82
ug/kg
1
Pyrene
129-00-0
8270E
2000
170
37
ug/kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
880
65
ug/kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
880
65
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
87 24-137
2-Fluorophenol
60 16-136
Nitrobenzene-d5
37 12-144
Phenol-d5
63 26-148
Terphenyl-d14
102 20-127
2,4,6-Tribromophenol
113 27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 20 of 88

MA EPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/05/2019 0234 CHG 06/02/2019 2016 18432
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH- 1500 13 13 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) 140 40-140
2-Fluorobiphenyl (fractionation 1) N 200 40-140
o - Terphenyl (aromatic) 64 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 21 of 88

MA EPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/04/2019 2112 CHG 06/02/2019 2016 18431
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 2300 13 13 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH- 740 13 13 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
57 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 22 of 88

MADEP VPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 2 06/07/20191659 JJG 19104
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- 5.6 J 12 2.3 mg/kg 1
C9 - C12 Aliphatics MADEP-VPH- 200 12 2.3 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
N 0.00 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 23 of 88

MADEP VPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-003
Description: SW-W Matrix: Solid
Date Sampled:05/29/2019 1220 % Solids: 74.0 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 2 06/07/20191659 JJG 19103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 160 3.9 1.5 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
N 153 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 24 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035 High 8260D
1 06/03/2019 1931 JM1
18534
5.80
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
1400
570
ug/kg
1
Benzene
71-43-2
8260D
ND
360
140
ug/kg
1
Bromodichloromethane
75-27-4
8260D
ND
360
140
ug/kg
1
Bromoform
75-25-2
8260D
ND
360
140
ug/kg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
360
210
ug/kg
1
2-Butanone (MEK)
78-93-3
8260D
ND
1400
290
ug/kg
1
Carbon disulfide
75-15-0
8260D
ND
360
140
ug/kg
1
Carbon tetrachloride
56-23-5
8260D
ND
360
140
ug/kg
1
Chlorobenzene
108-90-7
8260D
ND
360
140
ug/kg
1
Chloroethane
75-00-3
8260D
ND
360
140
ug/kg
1
Chloroform
67-66-3
8260D
ND
360
140
ug/kg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
360
210
ug/kg
1
Cyclohexane
110-82-7
8260D
ND
360
140
ug/kg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
360
140
ug/kg
1
Dibromochloromethane
124-48-1
8260D
ND
360
140
ug/kg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
360
140
ug/kg
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
360
140
ug/kg
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
360
140
ug/kg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
360
140
ug/kg
1
Dichlorodifluoromethane
75-71-8
8260D
ND
360
210
ug/kg
1
1,1-Dichloroethane
75-34-3
8260D
ND
360
140
ug/kg
1
1,2-Dichloroethane
107-06-2
8260D
ND
360
140
ug/kg
1
1,1-Dichloroethene
75-35-4
8260D
ND
360
140
ug/kg
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
360
140
ug/kg
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
360
140
ug/kg
1
1,2-Dichloropropane
78-87-5
8260D
ND
360
140
ug/kg
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
360
140
ug/kg
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
360
140
ug/kg
1
Ethylbenzene
100-41-4
8260D
ND
360
140
ug/kg
1
2-Hexanone
591-78-6
8260D
ND
710
290
ug/kg
1
Isopropylbenzene
98-82-8
8260D
ND
360
140
ug/kg
1
Methyl acetate
79-20-9
8260D
ND
360
140
ug/kg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
360
140
ug/kg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
710
290
ug/kg
1
Methylcyclohexane
108-87-2
8260D
ND
360
140
ug/kg
1
Methylene chloride
75-09-2
8260D
ND
360
140
ug/kg
1
Styrene
100-42-5
8260D
ND
360
140
ug/kg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
360
140
ug/kg
1
Tetrachloroethene
127-18-4
8260D
ND
360
140
ug/kg
1
Toluene
108-88-3
8260D
ND
360
140
ug/kg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
360
140
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
360
140
ug/kg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
360
140
ug/kg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
360
140
ug/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 25 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 High 8260D 1 06/03/2019 1931 JM1 18534 5.80
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
360
140
ug/kg
1
Trichlorofluoromethane
75-69-4
8260D
ND
360
140
ug/kg
1
Vinyl chloride
75-01-4
8260D
ND
360
210
ug/kg
1
Xylenes (total)
1330-20-7
8260D
ND
710
290
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
117 47-138
102 53-142
110 68-124
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 26 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
50 06/08/20191625 SCD
06/06/20191705 18849
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
860
320
ug/kg
1
Acenaphthylene
208-96-8
8270E
ND
860
210
ug/kg
1
Acetophenone
98-86-2
8270E
ND
4300
450
ug/kg
1
Anthracene
120-12-7
8270E
750 J
860
170
ug/kg
1
Atrazine
1912-24-9
8270E
ND
4300
320
ug/kg
1
Benzaldehyde
100-52-7
8270E
ND
4300
320
ug/kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
860
130
ug/kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
860
110
ug/kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
860
120
ug/kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
860
240
ug/kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
860
140
ug/kg
1
1,1'-Biphenyl
92-52-4
8270E
ND
4300
320
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4300
320
ug/kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4300
320
ug/kg
1
Caprolactam
105-60-2
8270E
ND
4300
760
ug/kg
1
Carbazole
86-74-8
8270E
ND
4300
320
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4300
430
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4300
360
ug/kg
1
4-Chloroaniline
106-47-8
8270E
ND
4300
370
ug/kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4300
320
ug/kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4300
350
ug/kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
4300
810
ug/kg
1
2-Chlorophenol
95-57-8
8270E
ND
4300
680
ug/kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4300
320
ug/kg
1
Chrysene
218-01-9
8270E
ND
860
200
ug/kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
860
190
ug/kg
1
Dibenzofuran
132-64-9
8270E
ND
4300
320
ug/kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4300
650
ug/kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
4300
420
ug/kg
1
Diethylphthalate
84-66-2
8270E
ND
4300
320
ug/kg
1
Dimethyl phthalate
131-11-3
8270E
ND
4300
320
ug/kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4300
690
ug/kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4300
630
ug/kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
21000
1600
ug/kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
21000
1600
ug/kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8400
790
ug/kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8400
690
ug/kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
4300
320
ug/kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4300
1600
ug/kg
1
Fluoranthene
206-44-0
8270E
ND
860
140
ug/kg
1
Fluorene
86-73-7
8270E
ND
860
120
ug/kg
1
Hexachlorobenzene
118-74-1
8270E
ND
4300
320
ug/kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
4300
550
ug/kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
21000
1600
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 27 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 50 06/08/20191625 SCD 06/06/20191705 18849
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4300
350
ug/kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
860
170
ug/kg
1
Isophorone
78-59-1
8270E
ND
4300
400
ug/kg
1
2-Methylnaphthalene
91-57-6
8270E
4500
860
380
ug/kg
1
2-Methylphenol
95-48-7
8270E
ND
4300
1100
ug/kg
1
3+4-Methylphenol
106-44-5
8270E
ND
8400
1100
ug/kg
1
Naphthalene
91-20-3
8270E
1400
860
300
ug/kg
1
2-Nitroaniline
88-74-4
8270E
ND
8400
1200
ug/kg
1
3-Nitroaniline
99-09-2
8270E
ND
8400
1200
ug/kg
1
4-Nitroaniline
100-01-6
8270E
ND
8400
1300
ug/kg
1
Nitrobenzene
98-95-3
8270E
ND
4300
500
ug/kg
1
2-Nitrophenol
88-75-5
8270E
ND
8400
640
ug/kg
1
4-Nitrophenol
100-02-7
8270E
ND
21000
6700
ug/kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4300
370
ug/kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4300
330
ug/kg
1
Pentachlorophenol
87-86-5
8270E
ND
21000
1700
ug/kg
1
Phenanthrene
85-01-8
8270E
2100
860
140
ug/kg
1
Phenol
108-95-2
8270E
ND
4300
400
ug/kg
1
Pyrene
129-00-0
8270E
490 J
860
180
ug/kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4300
320
ug/kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4300
320
ug/kg
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
87
24-137
2-Fluorophenol
40
16-136
Nitrobenzene-d5
69
12-144
Phenol-d5
29
26-148
Terphenyl-d14
88
20-127
2,4,6-Tribromophenol
71
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 28 of 88

MA EPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/05/2019 0304 CHG 06/02/2019 2016 18432
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH- 330 13 13 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1)
o - Terphenyl (aromatic)
103 40-140
131 40-140
72 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 29 of 88

MA EPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/04/2019 2141 CHG 06/02/2019 2016 18431
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 550 13 13 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH- 130 13 13 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
61 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 30 of 88

MADEP VPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 06/07/20191727 JJG 19104
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- 24 5.0 0.99 mg/kg 1
C9 - C12 Aliphatics MADEP-VPH- 210 5.0 0.99 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
N 0.00 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 31 of 88

MADEP VPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-004
Description: SW-S Matrix: Solid
Date Sampled:05/29/2019 1240 % Solids: 76.6 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 06/07/20191727 JJG 19103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 180 1.7 0.66 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
N 0.00 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 32 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035 High 8260D
1 06/03/2019 1953 JM1
18534
4.64
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
1700
680
ug/kg
1
Benzene
71-43-2
8260D
ND
420
170
ug/kg
1
Bromodichloromethane
75-27-4
8260D
ND
420
170
ug/kg
1
Bromoform
75-25-2
8260D
ND
420
170
ug/kg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
420
250
ug/kg
1
2-Butanone (MEK)
78-93-3
8260D
ND
1700
340
ug/kg
1
Carbon disulfide
75-15-0
8260D
ND
420
170
ug/kg
1
Carbon tetrachloride
56-23-5
8260D
ND
420
170
ug/kg
1
Chlorobenzene
108-90-7
8260D
ND
420
170
ug/kg
1
Chloroethane
75-00-3
8260D
ND
420
170
ug/kg
1
Chloroform
67-66-3
8260D
ND
420
170
ug/kg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
420
250
ug/kg
1
Cyclohexane
110-82-7
8260D
ND
420
170
ug/kg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
420
170
ug/kg
1
Dibromochloromethane
124-48-1
8260D
ND
420
170
ug/kg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
420
170
ug/kg
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
420
170
ug/kg
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
420
170
ug/kg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
420
170
ug/kg
1
Dichlorodifluoromethane
75-71-8
8260D
ND
420
250
ug/kg
1
1,1-Dichloroethane
75-34-3
8260D
ND
420
170
ug/kg
1
1,2-Dichloroethane
107-06-2
8260D
ND
420
170
ug/kg
1
1,1-Dichloroethene
75-35-4
8260D
ND
420
170
ug/kg
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
420
170
ug/kg
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
420
170
ug/kg
1
1,2-Dichloropropane
78-87-5
8260D
ND
420
170
ug/kg
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
420
170
ug/kg
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
420
170
ug/kg
1
Ethylbenzene
100-41-4
8260D
210 J
420
170
ug/kg
1
2-Hexanone
591-78-6
8260D
ND
840
340
ug/kg
1
Isopropylbenzene
98-82-8
8260D
ND
420
170
ug/kg
1
Methyl acetate
79-20-9
8260D
ND
420
170
ug/kg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
420
170
ug/kg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
840
340
ug/kg
1
Methylcyclohexane
108-87-2
8260D
ND
420
170
ug/kg
1
Methylene chloride
75-09-2
8260D
ND
420
170
ug/kg
1
Styrene
100-42-5
8260D
ND
420
170
ug/kg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
420
170
ug/kg
1
Tetrachloroethene
127-18-4
8260D
ND
420
170
ug/kg
1
Toluene
108-88-3
8260D
ND
420
170
ug/kg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
420
170
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
420
170
ug/kg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
420
170
ug/kg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
420
170
ug/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 33 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 High 8260D 1 06/03/2019 1953 JM1 18534 4.64
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
420
170
ug/kg
1
Trichlorofluoromethane
75-69-4
8260D
ND
420
170
ug/kg
1
Vinyl chloride
75-01-4
8260D
ND
420
250
ug/kg
1
Xylenes (total)
1330-20-7
8260D
620 J
840
340
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
112 47-138
101 53-142
107 68-124
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 34 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
50 06/08/20191650 SCD
06/06/20191705 18849
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
860
320
ug/kg
1
Acenaphthylene
208-96-8
8270E
ND
860
210
ug/kg
1
Acetophenone
98-86-2
8270E
ND
4300
450
ug/kg
1
Anthracene
120-12-7
8270E
400 J
860
170
ug/kg
1
Atrazine
1912-24-9
8270E
ND
4300
320
ug/kg
1
Benzaldehyde
100-52-7
8270E
ND
4300
320
ug/kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
860
130
ug/kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
860
110
ug/kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
860
120
ug/kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
860
240
ug/kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
860
140
ug/kg
1
1,1'-Biphenyl
92-52-4
8270E
ND
4300
320
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4300
320
ug/kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4300
320
ug/kg
1
Caprolactam
105-60-2
8270E
ND
4300
760
ug/kg
1
Carbazole
86-74-8
8270E
ND
4300
320
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4300
430
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4300
360
ug/kg
1
4-Chloroaniline
106-47-8
8270E
ND
4300
370
ug/kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4300
320
ug/kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4300
350
ug/kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
4300
810
ug/kg
1
2-Chlorophenol
95-57-8
8270E
ND
4300
680
ug/kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4300
320
ug/kg
1
Chrysene
218-01-9
8270E
ND
860
200
ug/kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
860
190
ug/kg
1
Dibenzofuran
132-64-9
8270E
ND
4300
320
ug/kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4300
650
ug/kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
4300
420
ug/kg
1
Diethylphthalate
84-66-2
8270E
ND
4300
320
ug/kg
1
Dimethyl phthalate
131-11-3
8270E
ND
4300
320
ug/kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4300
690
ug/kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4300
630
ug/kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
21000
1600
ug/kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
21000
1600
ug/kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8400
790
ug/kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8400
690
ug/kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
4300
320
ug/kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4300
1600
ug/kg
1
Fluoranthene
206-44-0
8270E
ND
860
140
ug/kg
1
Fluorene
86-73-7
8270E
ND
860
120
ug/kg
1
Hexachlorobenzene
118-74-1
8270E
ND
4300
320
ug/kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
4300
550
ug/kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
21000
1600
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 35 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 50 06/08/20191650 SCD 06/06/20191705 18849
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4300
350
ug/kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
860
170
ug/kg
1
Isophorone
78-59-1
8270E
ND
4300
400
ug/kg
1
2-Methylnaphthalene
91-57-6
8270E
2300
860
380
ug/kg
1
2-Methylphenol
95-48-7
8270E
ND
4300
1100
ug/kg
1
3+4-Methylphenol
106-44-5
8270E
ND
8400
1100
ug/kg
1
Naphthalene
91-20-3
8270E
850 J
860
300
ug/kg
1
2-Nitroaniline
88-74-4
8270E
ND
8400
1200
ug/kg
1
3-Nitroaniline
99-09-2
8270E
ND
8400
1200
ug/kg
1
4-Nitroaniline
100-01-6
8270E
ND
8400
1300
ug/kg
1
Nitrobenzene
98-95-3
8270E
ND
4300
500
ug/kg
1
2-Nitrophenol
88-75-5
8270E
ND
8400
640
ug/kg
1
4-Nitrophenol
100-02-7
8270E
ND
21000
6600
ug/kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4300
370
ug/kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4300
330
ug/kg
1
Pentachlorophenol
87-86-5
8270E
ND
21000
1700
ug/kg
1
Phenanthrene
85-01-8
8270E
580 J
860
140
ug/kg
1
Phenol
108-95-2
8270E
ND
4300
400
ug/kg
1
Pyrene
129-00-0
8270E
320 J
860
180
ug/kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4300
320
ug/kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4300
320
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
78 24-137
2-Fluorophenol
35 16-136
Nitrobenzene-d5
81 12-144
Phenol-d5
30 26-148
Terphenyl-d14
103 20-127
2,4,6-Tribromophenol
52 27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 36 of 88

MA EPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/05/2019 0333 CHG 06/02/2019 2016 18432
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH- 660 12 12 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1)
o - Terphenyl (aromatic)
99 40-140
126 40-140
80 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 37 of 88

MA EPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/04/2019 2210 CHG 06/02/2019 2016 18431
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 2000 12 12 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH- 500 12 12 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
58 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 38 of 88

MADEP VPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 06/07/20191755 JJG 19104
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- 6.0 J 6.2 1.2 mg/kg 1
C9 - C12 Aliphatics MADEP-VPH- 120 6.2 1.2 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
70 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 39 of 88

MADEP VPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-005
Description: SW-E Matrix: Solid
Date Sampled:05/29/2019 1235 % Solids: 77.2 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 06/07/20191755 JJG 19103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 140 2.1 0.83 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
N 65 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 40 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
Sample Wt.(g)
1 5035 High 8260D
1 06/03/2019 2015 JM1
18534
4.59
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
1700
680
ug/kg
1
Benzene
71-43-2
8260D
ND
430
170
ug/kg
1
Bromodichloromethane
75-27-4
8260D
ND
430
170
ug/kg
1
Bromoform
75-25-2
8260D
ND
430
170
ug/kg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
430
260
ug/kg
1
2-Butanone (MEK)
78-93-3
8260D
ND
1700
340
ug/kg
1
Carbon disulfide
75-15-0
8260D
ND
430
170
ug/kg
1
Carbon tetrachloride
56-23-5
8260D
ND
430
170
ug/kg
1
Chlorobenzene
108-90-7
8260D
ND
430
170
ug/kg
1
Chloroethane
75-00-3
8260D
ND
430
170
ug/kg
1
Chloroform
67-66-3
8260D
ND
430
170
ug/kg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
430
260
ug/kg
1
Cyclohexane
110-82-7
8260D
ND
430
170
ug/kg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
430
170
ug/kg
1
Dibromochloromethane
124-48-1
8260D
ND
430
170
ug/kg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
430
170
ug/kg
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
430
170
ug/kg
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
430
170
ug/kg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
430
170
ug/kg
1
Dichlorodifluoromethane
75-71-8
8260D
ND
430
260
ug/kg
1
1,1-Dichloroethane
75-34-3
8260D
ND
430
170
ug/kg
1
1,2-Dichloroethane
107-06-2
8260D
ND
430
170
ug/kg
1
1,1-Dichloroethene
75-35-4
8260D
ND
430
170
ug/kg
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
430
170
ug/kg
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
430
170
ug/kg
1
1,2-Dichloropropane
78-87-5
8260D
ND
430
170
ug/kg
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
430
170
ug/kg
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
430
170
ug/kg
1
Ethylbenzene
100-41-4
8260D
ND
430
170
ug/kg
1
2-Hexanone
591-78-6
8260D
ND
860
340
ug/kg
1
Isopropylbenzene
98-82-8
8260D
ND
430
170
ug/kg
1
Methyl acetate
79-20-9
8260D
ND
430
170
ug/kg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
430
170
ug/kg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
860
340
ug/kg
1
Methylcyclohexane
108-87-2
8260D
ND
430
170
ug/kg
1
Methylene chloride
75-09-2
8260D
ND
430
170
ug/kg
1
Styrene
100-42-5
8260D
ND
430
170
ug/kg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
430
170
ug/kg
1
Tetrachloroethene
127-18-4
8260D
ND
430
170
ug/kg
1
Toluene
108-88-3
8260D
ND
430
170
ug/kg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
430
170
ug/kg
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
430
170
ug/kg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
430
170
ug/kg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
430
170
ug/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 41 of 88

Volatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 High 8260D 1 06/03/2019 2015 JM1 18534 4.59
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
430
170
ug/kg
1
Trichlorofluoromethane
75-69-4
8260D
ND
430
170
ug/kg
1
Vinyl chloride
75-01-4
8260D
ND
430
260
ug/kg
1
Xylenes (total)
1330-20-7
8260D
ND
860
340
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
112 47-138
104 53-142
111 68-124
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 42 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
50 06/08/20191715 SCD
06/06/20191705 18849
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
840
320
ug/kg
1
Acenaphthylene
208-96-8
8270E
ND
840
200
ug/kg
1
Acetophenone
98-86-2
8270E
ND
4200
440
ug/kg
1
Anthracene
120-12-7
8270E
540 J
840
160
ug/kg
1
Atrazine
1912-24-9
8270E
ND
4200
320
ug/kg
1
Benzaldehyde
100-52-7
8270E
ND
4200
320
ug/kg
1
Benzo(a)anthracene
56-55-3
8270E
ND
840
130
ug/kg
1
Benzo(a)pyrene
50-32-8
8270E
ND
840
110
ug/kg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
840
120
ug/kg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
840
240
ug/kg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
840
130
ug/kg
1
1,1'-Biphenyl
92-52-4
8270E
ND
4200
320
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4200
320
ug/kg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4200
320
ug/kg
1
Caprolactam
105-60-2
8270E
ND
4200
750
ug/kg
1
Carbazole
86-74-8
8270E
ND
4200
320
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4200
420
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4200
350
ug/kg
1
4-Chloroaniline
106-47-8
8270E
ND
4200
370
ug/kg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4200
320
ug/kg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4200
340
ug/kg
1
2-Chloronaphthalene
91-58-7
8270E
ND
4200
790
ug/kg
1
2-Chlorophenol
95-57-8
8270E
ND
4200
670
ug/kg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4200
320
ug/kg
1
Chrysene
218-01-9
8270E
ND
840
200
ug/kg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
840
190
ug/kg
1
Dibenzofuran
132-64-9
8270E
ND
4200
320
ug/kg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4200
630
ug/kg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
4200
420
ug/kg
1
Diethylphthalate
84-66-2
8270E
ND
4200
320
ug/kg
1
Dimethyl phthalate
131-11-3
8270E
ND
4200
320
ug/kg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4200
680
ug/kg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4200
620
ug/kg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
21000
1600
ug/kg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
21000
1600
ug/kg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8200
770
ug/kg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8200
680
ug/kg
1
Di-n-octylphthalate
117-84-0
8270E
ND
4200
320
ug/kg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4200
1600
ug/kg
1
Fluoranthene
206-44-0
8270E
ND
840
140
ug/kg
1
Fluorene
86-73-7
8270E
330 J
840
120
ug/kg
1
Hexachlorobenzene
118-74-1
8270E
ND
4200
320
ug/kg
1
Hexachlorobutadiene
87-68-3
8270E
ND
4200
540
ug/kg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
21000
1600
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result < LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 43 of 88

Semivolatile Organic Compounds by GC/MS
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 50 06/08/20191715 SCD 06/06/20191705 18849
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4200
340
ug/kg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
840
170
ug/kg
1
Isophorone
78-59-1
8270E
ND
4200
390
ug/kg
1
2-Methylnaphthalene
91-57-6
8270E
2700
840
370
ug/kg
1
2-Methylphenol
95-48-7
8270E
ND
4200
1100
ug/kg
1
3+4-Methylphenol
106-44-5
8270E
ND
8200
1000
ug/kg
1
Naphthalene
91-20-3
8270E
560 J
840
300
ug/kg
1
2-Nitroaniline
88-74-4
8270E
ND
8200
1200
ug/kg
1
3-Nitroaniline
99-09-2
8270E
ND
8200
1200
ug/kg
1
4-Nitroaniline
100-01-6
8270E
ND
8200
1300
ug/kg
1
Nitrobenzene
98-95-3
8270E
ND
4200
490
ug/kg
1
2-Nitrophenol
88-75-5
8270E
ND
8200
630
ug/kg
1
4-Nitrophenol
100-02-7
8270E
ND
21000
6500
ug/kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4200
360
ug/kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4200
320
ug/kg
1
Pentachlorophenol
87-86-5
8270E
ND
21000
1700
ug/kg
1
Phenanthrene
85-01-8
8270E
1300
840
140
ug/kg
1
Phenol
108-95-2
8270E
ND
4200
390
ug/kg
1
Pyrene
129-00-0
8270E
350 J
840
180
ug/kg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4200
320
ug/kg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4200
320
ug/kg
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
79
24-137
2-Fluorophenol
32
16-136
Nitrobenzene-d5
72
12-144
Phenol-d5
30
26-148
Terphenyl-d14
81
20-127
2,4,6-Tribromophenol
46
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 44 of 88

MA EPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/05/2019 0402 CHG 06/02/2019 2016 18432
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH- 290 12 12 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1)
o - Terphenyl (aromatic)
101 40-140
126 40-140
78 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 45 of 88

MA EPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 06/04/2019 2240 CHG 06/02/2019 2016 18431
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 480 12 12 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH- 130 12 12 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
67 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 46 of 88

MADEP VPH (aliphatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 06/07/20191823 JJG 19104
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- 1.5 J 5.5 1.1 mg/kg 1
C9 - C12 Aliphatics MADEP-VPH- 59 5.5 1.1 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
99 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 47 of 88

MADEP VPH (aromatics)
Client: Mid -Atlantic Associates, Inc. Laboratory ID: UE31010-006
Description: BOTTOM Matrix: Solid
Date Sampled:05/29/2019 1245 % Solids: 77.1 06/05/2019 0126
Date Received:05/30/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 06/07/20191823 JJG 19103
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 43 1.8 0.73 mg/kg 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
121 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 48 of 88

QC Summary
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 49 of 88

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ18534-001 Matrix: Solid
Batch: 18534 Prep Method: 5035 High
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
1000
400
ug/kg
06/03/2019 1826
Benzene
ND
1
250
100
ug/kg
06/03/2019 1826
Bromodichloromethane
ND
1
250
100
ug/kg
06/03/2019 1826
Bromoform
ND
1
250
100
ug/kg
06/03/2019 1826
Bromomethane (Methyl bromide)
ND
1
250
150
ug/kg
06/03/2019 1826
2-Butanone (MEK)
ND
1
1000
200
ug/kg
06/03/2019 1826
Carbon disulfide
ND
1
250
100
ug/kg
06/03/2019 1826
Carbon tetrachloride
ND
1
250
100
ug/kg
06/03/2019 1826
Chlorobenzene
ND
1
250
100
ug/kg
06/03/2019 1826
Chloroethane
ND
1
250
100
ug/kg
06/03/2019 1826
Chloroform
ND
1
250
100
ug/kg
06/03/2019 1826
Chloromethane (Methyl chloride)
ND
1
250
150
ug/kg
06/03/2019 1826
Cyclohexane
ND
1
250
100
ug/kg
06/03/2019 1826
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
250
100
ug/kg
06/03/2019 1826
Dibromochloromethane
ND
1
250
100
ug/kg
06/03/2019 1826
1,2-Dibromoethane (EDB)
ND
1
250
100
ug/kg
06/03/2019 1826
1,2-Dichlorobenzene
ND
1
250
100
ug/kg
06/03/2019 1826
1,3-Dichlorobenzene
ND
1
250
100
ug/kg
06/03/2019 1826
1,4-Dichlorobenzene
ND
1
250
100
ug/kg
06/03/2019 1826
Dichlorodifluoromethane
ND
1
250
150
ug/kg
06/03/2019 1826
1,1-Dichloroethane
ND
1
250
100
ug/kg
06/03/2019 1826
1,2-Dichloroethane
ND
1
250
100
ug/kg
06/03/2019 1826
1,1-Dichloroethene
ND
1
250
100
ug/kg
06/03/2019 1826
cis- 1,2-Dichloroethene
ND
1
250
100
ug/kg
06/03/2019 1826
trans- 1,2-Dichloroethene
ND
1
250
100
ug/kg
06/03/2019 1826
1,2-Dichloropropane
ND
1
250
100
ug/kg
06/03/2019 1826
cis- 1,3-Dichloropropene
ND
1
250
100
ug/kg
06/03/2019 1826
trans- 1,3-Dichloropropene
ND
1
250
100
ug/kg
06/03/2019 1826
Ethylbenzene
ND
1
250
100
ug/kg
06/03/2019 1826
2-Hexanone
ND
1
500
200
ug/kg
06/03/2019 1826
Isopropylbenzene
ND
1
250
100
ug/kg
06/03/2019 1826
Methyl acetate
ND
1
250
100
ug/kg
06/03/2019 1826
Methyl tertiary butyl ether (MTBE)
ND
1
250
100
ug/kg
06/03/2019 1826
4-Methyl-2-pentanone
ND
1
500
200
ug/kg
06/03/2019 1826
Methylcyclohexane
ND
1
250
100
ug/kg
06/03/2019 1826
Methylene chloride
ND
1
250
100
ug/kg
06/03/2019 1826
Styrene
ND
1
250
100
ug/kg
06/03/2019 1826
1,1,2,2-Tetrachloroethane
ND
1
250
100
ug/kg
06/03/2019 1826
Tetrachloroethene
ND
1
250
100
ug/kg
06/03/2019 1826
Toluene
ND
1
250
100
ug/kg
06/03/2019 1826
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
250
100
ug/kg
06/03/2019 1826
1,2,4-Trichlorobenzene
ND
1
250
100
ug/kg
06/03/2019 1826
1,1,1-Trichloroethane
ND
1
250
100
ug/kg
06/03/2019 1826
1,1,2-Trichloroethane
ND
1
250
100
ug/kg
06/03/2019 1826
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 50 of 88

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ18534-001 Matrix: Solid
Batch: 18534 Prep Method: 5035 High
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
250
100
ug/kg
06/03/2019 1826
Trichlorofluoromethane
ND
1
250
100
ug/kg
06/03/2019 1826
Vinyl chloride
ND
1
250
150
ug/kg
06/03/2019 1826
Xylenes (total)
ND
1
500
200
ug/kg
06/03/2019 1826
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 97 47-138
1,2-Dichloroethane-d4 86 53-142
Toluene-d8 93 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 51 of 88

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ18534-002
Matrix:
Solid
Batch: 18534
Prep Method:
5035 High
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Acetone
5000
4500
1
91
60-140
06/03/2019 1803
Benzene
2500
2600
1
105
70-130
06/03/2019 1803
Bromodichloromethane
2500
2500
1
101
70-130
06/03/2019 1803
Bromoform
2500
2300
1
92
70-130
06/03/2019 1803
Bromomethane (Methyl bromide)
2500
2200
1
89
70-130
06/03/2019 1803
2-Butanone (MEK)
5000
4900
1
97
60-140
06/03/2019 1803
Carbon disulfide
2500
2300
1
92
70-130
06/03/2019 1803
Carbon tetrachloride
2500
2600
1
105
70-130
06/03/2019 1803
Chlorobenzene
2500
2600
1
105
70-130
06/03/2019 1803
Chloroethane
2500
2500
1
101
70-130
06/03/2019 1803
Chloroform
2500
2500
1
100
70-130
06/03/2019 1803
Chloromethane (Methyl chloride)
2500
2200
1
90
60-140
06/03/2019 1803
Cyclohexane
2500
3000
1
119
70-130
06/03/2019 1803
1,2-Dibromo-3-chloropropane (DBCP)
2500
2200
1
87
70-130
06/03/2019 1803
Dibromochloromethane
2500
2500
1
101
70-130
06/03/2019 1803
1,2-Dibromoethane (EDB)
2500
2700
1
107
70-130
06/03/2019 1803
1,2-Dichlorobenzene
2500
2600
1
102
70-130
06/03/2019 1803
1,3-Dichlorobenzene
2500
2600
1
105
70-130
06/03/2019 1803
1,4-Dichlorobenzene
2500
2600
1
104
70-130
06/03/2019 1803
Dichlorodifluoromethane
2500
1800
1
73
60-140
06/03/2019 1803
1,1-Dichloroethane
2500
2500
1
102
70-130
06/03/2019 1803
1,2-Dichloroethane
2500
2600
1
103
70-130
06/03/2019 1803
1,1-Dichloroethene
2500
2400
1
97
70-130
06/03/2019 1803
cis- 1,2-Dichloroethene
2500
2600
1
104
70-130
06/03/2019 1803
trans- 1,2-Dichloroethene
2500
2600
1
106
70-130
06/03/2019 1803
1,2-Dichloropropane
2500
2600
1
104
70-130
06/03/2019 1803
cis- 1,3-Dichloropropene
2500
2600
1
103
70-130
06/03/2019 1803
trans- 1,3-Dichloropropene
2500
2600
1
103
70-130
06/03/2019 1803
Ethylbenzene
2500
2700
1
110
70-130
06/03/2019 1803
2-Hexanone
5000
4900
1
98
70-130
06/03/2019 1803
Isopropylbenzene
2500
2800
1
110
70-130
06/03/2019 1803
Methyl acetate
2500
2500
1
98
70-130
06/03/2019 1803
Methyl tertiary butyl ether (MTBE)
2500
2400
1
98
70-130
06/03/2019 1803
4-Methyl-2-pentanone
5000
4800
1
96
70-130
06/03/2019 1803
Methylcyclohexane
2500
3000
1
121
70-130
06/03/2019 1803
Methylene chloride
2500
2300
1
92
70-130
06/03/2019 1803
Styrene
2500
2700
1
107
70-130
06/03/2019 1803
1,1,2,2-Tetrachloroethane
2500
2500
1
101
70-130
06/03/2019 1803
Tetrachloroethene
2500
2800
1
111
70-130
06/03/2019 1803
Toluene
2500
2700
1
107
70-130
06/03/2019 1803
1,1,2-Trichloro-1,2,2-Trifluoroethane
2500
2700
1
108
70-130
06/03/2019 1803
1,2,4-Trichlorobenzene
2500
2600
1
102
70-130
06/03/2019 1803
1,1,1-Trichloroethane
2500
2500
1
102
70-130
06/03/2019 1803
1,1,2-Trichloroethane
2500
2600
1
106
70-130
06/03/2019 1803
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 52 of 88

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ18534-002
Matrix:
Solid
Batch: 18534
Prep Method:
5035 High
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
2500
2800
1
112
70-130
06/03/2019 1803
Trichlorofluoromethane
2500
2600
1
104
70-130
06/03/2019 1803
Vinyl chloride
2500
2400
1
98
70-130
06/03/2019 1803
Xylenes (total)
5000
5400
1
109
70-130
06/03/2019 1803
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene 100 47-138
1,2-Dichloroethane-d4 87 53-142
Toluene-d8 97 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 53 of 88

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ18379-001 Matrix: Solid
Batch: 18379 Prep Method: 3546
Analytical Method: 8270E Prep Date: 06/01/2019 2311
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
13
5.0
ug/kg
06/11/2019 1301
Acenaphthylene
ND
1
13
3.2
ug/kg
06/11/2019 1301
Acetophenone
ND
1
67
6.9
ug/kg
06/11/2019 1301
Anthracene
ND
1
13
2.6
ug/kg
06/11/2019 1301
Atrazine
ND
1
67
5.0
ug/kg
06/11/2019 1301
Benzaldehyde
ND
1
67
5.0
ug/kg
06/11/2019 1301
Benzo(a)anthracene
ND
1
13
2.0
ug/kg
06/11/2019 1301
Benzo(a)pyrene
ND
1
13
1.7
ug/kg
06/11/2019 1301
Benzo(k)fluoranthene
ND
1
13
1.9
ug/kg
06/11/2019 1301
Benzo(g,h,i)perylene
ND
1
13
3.8
ug/kg
06/11/2019 1301
Benzo(k)fluoranthene
ND
1
13
2.1
ug/kg
06/11/2019 1301
1,1'-Biphenyl
ND
1
67
5.0
ug/kg
06/11/2019 1301
4-Bromophenyl phenyl ether
ND
1
67
5.0
ug/kg
06/11/2019 1301
Butyl benzyl phthalate
ND
1
67
5.0
ug/kg
06/11/2019 1301
Caprolactam
ND
1
67
12
ug/kg
06/11/2019 1301
Carbazole
ND
1
67
5.0
ug/kg
06/11/2019 1301
bis (2-Chloro-1-methylethyl) ether
ND
1
67
6.7
ug/kg
06/11/2019 1301
4-Chloro-3-methyl phenol
ND
1
67
5.6
ug/kg
06/11/2019 1301
4-Chloroaniline
ND
1
67
5.8
ug/kg
06/11/2019 1301
bis(2-Chloroethoxy)methane
ND
1
67
5.0
ug/kg
06/11/2019 1301
bis(2-Chloroethyl)ether
ND
1
67
5.5
ug/kg
06/11/2019 1301
2-Chloronaphthalene
ND
1
67
13
ug/kg
06/11/2019 1301
2-Chlorophenol
ND
1
67
11
ug/kg
06/11/2019 1301
4-Chlorophenyl phenyl ether
ND
1
67
5.0
ug/kg
06/11/2019 1301
Chrysene
ND
1
13
3.1
ug/kg
06/11/2019 1301
Dibenzo(a,h)anthracene
ND
1
13
3.0
ug/kg
06/11/2019 1301
Dibenzofuran
ND
1
67
5.0
ug/kg
06/11/2019 1301
3,3'-Dichlorobenzidine
ND
1
67
10
ug/kg
06/11/2019 1301
2,4-Dichlorophenol
ND
1
67
6.6
ug/kg
06/11/2019 1301
Diethylphthalate
ND
1
67
5.0
ug/kg
06/11/2019 1301
Dimethyl phthalate
ND
1
67
5.0
ug/kg
06/11/2019 1301
2,4-Dimethylphenol
ND
1
67
11
ug/kg
06/11/2019 1301
Di-n-butyl phthalate
ND
1
67
9.8
ug/kg
06/11/2019 1301
4,6-Dinitro-2-methyl phenol
ND
1
330
25
ug/kg
06/11/2019 1301
2,4-Dinitrophenol
ND
1
330
25
ug/kg
06/11/2019 1301
2,4-Dinitrotoluene
ND
1
130
12
ug/kg
06/11/2019 1301
2,6-Dinitrotoluene
ND
1
130
11
ug/kg
06/11/2019 1301
Di-n-octylphthalate
ND
1
67
5.0
ug/kg
06/11/2019 1301
bis(2-Ethylhexyl)phthalate
ND
1
67
25
ug/kg
06/11/2019 1301
Fluoranthene
ND
1
13
2.2
ug/kg
06/11/2019 1301
Fluorene
ND
1
13
1.9
ug/kg
06/11/2019 1301
Hexachlorobenzene
ND
1
67
5.0
ug/kg
06/11/2019 1301
Hexachlorobutadiene
ND
1
67
8.5
ug/kg
06/11/2019 1301
Hexachlorocyclopentadiene
ND
1
330
25
ug/kg
06/11/2019 1301
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 54 of 88

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ18379-001 Matrix: Solid
Batch: 18379 Prep Method: 3546
Analytical Method: 8270E Prep Date: 06/01/2019 2311
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
67
5.5
ug/kg
06/11/20191301
Indeno(1,2,3-c,d)pyrene
ND
1
13
2.7
ug/kg
06/11/20191301
Isophorone
ND
1
67
6.2
ug/kg
06/11/20191301
2-Methyl naphthalene
ND
1
13
5.9
ug/kg
06/11/20191301
2-Methylphenol
ND
1
67
18
ug/kg
06/11/20191301
3+4-Methylphenol
ND
1
130
17
ug/kg
06/11/20191301
Naphthalene
ND
1
13
4.7
ug/kg
06/11/20191301
2-Nitroaniline
ND
1
130
19
ug/kg
06/11/20191301
3-Nitroaniline
ND
1
130
18
ug/kg
06/11/20191301
4-Nitroaniline
ND
1
130
20
ug/kg
06/11/20191301
Nitrobenzene
ND
1
67
7.8
ug/kg
06/11/20191301
2-Nitrophenol
ND
1
130
10
ug/kg
06/11/20191301
4-Nitrophenol
ND
1
330
100
ug/kg
06/11/20191301
N-Nitrosodi-n-propylamine
ND
1
67
5.7
ug/kg
06/11/20191301
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
67
5.1
ug/kg
06/11/2019 1301
Pentachlorophenol
ND
1
330
27
ug/kg
06/11/20191301
Phenanthrene
ND
1
13
2.3
ug/kg
06/11/20191301
Phenol
ND
1
67
6.2
ug/kg
06/11/20191301
Pyrene
ND
1
13
2.8
ug/kg
06/11/20191301
2,4,5-Trichlorophenol
ND
1
67
5.0
ug/kg
06/11/20191301
2,4,6-Trichlorophenol
ND
1
67
5.0
ug/kg
06/11/20191301
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 85 24-137
2-Fluorophenol 69 16-136
Nitrobenzene-d5
88
12-144
Phenol-d5
75
26-148
Terphenyl-d14
110
20-127
2,4,6-Tribromophenol
88
27-128
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 55 of 88

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ18379-002
Matrix:
Solid
Batch: 18379
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 06/01/2019 2311
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
670
590
1
88
12-111
06/11/2019 1325
Acenaphthylene
670
610
1
92
44-122
06/11/2019 1325
Acetophenone
670
460
1
68
48-111
06/11/2019 1325
Anthracene
670
660
1
99
16-122
06/11/2019 1325
Atrazine
670
720
1
107
48-116
06/11/2019 1325
Benzaldehyde
670
550
1
83
10-110
06/11/2019 1325
Benzo(a)anthracene
670
670
1
100
40-121
06/11/2019 1325
Benzo(a)pyrene
670
690
1
103
36-114
06/11/2019 1325
Benzo(k)fluoranthene
670
670
1
101
38-123
06/11/2019 1325
Benzo(g,h,i)perylene
670
680
1
101
43-120
06/11/2019 1325
Benzo(k)fluoranthene
670
670
1
100
40-126
06/11/2019 1325
1,1'-Biphenyl
670
570
1
86
49-110
06/11/2019 1325
4-Bromophenyl phenyl ether
670
620
1
93
46-118
06/11/2019 1325
Butyl benzyl phthalate
670
740
1
111
46-128
06/11/2019 1325
Caprolactam
670
660
1
99
43-121
06/11/2019 1325
Carbazole
670
680
1
102
47-128
06/11/2019 1325
bis (2-Chloro-1-methylethyl) ether
670
510
1
76
31-102
06/11/2019 1325
4-Chloro-3-methyl phenol
670
650
1
97
49-118
06/11/2019 1325
4-Chloroaniline
670
430
1
64
17-106
06/11/2019 1325
bis(2-Chloroethoxy)methane
670
570
1
86
39-108
06/11/2019 1325
bis(2-Chloroethyl)ether
670
520
1
77
32-105
06/11/2019 1325
2-Chloronaphthalene
670
570
1
85
31-127
06/11/2019 1325
2-Chlorophenol
670
510
1
77
37-106
06/11/2019 1325
4-Chlorophenyl phenyl ether
670
610
1
91
47-116
06/11/2019 1325
Chrysene
670
650
1
98
41-124
06/11/2019 1325
Dibenzo(a,h)anthracene
670
680
1
102
38-125
06/11/2019 1325
Dibenzofuran
670
600
1
89
45-112
06/11/2019 1325
3,3'-Dichlorobenzidine
670
680
1
102
10-119
06/11/2019 1325
2,4-Dichlorophenol
670
580
1
88
41-113
06/11/2019 1325
Diethylphthalate
670
660
1
99
49-123
06/11/2019 1325
Dimethyl phthalate
670
650
1
98
48-120
06/11/2019 1325
2,4-Dimethylphenol
670
760
1
114
33-123
06/11/2019 1325
Di-n-butyl phthalate
670
690
1
104
51-129
06/11/2019 1325
4,6-Dinitro-2-methyl phenol
670
400
1
61
40-130
06/11/2019 1325
2,4-Dinitrophenol
1300
530
1
40
10-113
06/11/2019 1325
2,4-Dinitrotoluene
670
690
1
104
48-124
06/11/2019 1325
2,6-Dinitrotoluene
670
670
1
100
47-125
06/11/2019 1325
Di-n-octylphthalate
670
730
1
110
49-142
06/11/2019 1325
bis(2-Ethylhexyl)phthalate
670
730
1
109
45-128
06/11/2019 1325
Fluoranthene
670
680
1
103
26-133
06/11/2019 1325
Fluorene
670
620
1
93
19-108
06/11/2019 1325
Hexachlorobenzene
670
620
1
93
44-122
06/11/2019 1325
Hexachlorobutadiene
670
520
1
78
33-103
06/11/2019 1325
Hexachlorocyclopentadiene
3300
2300
1
68
18-121
06/11/2019 1325
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 56 of 88

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ18379-002
Matrix:
Solid
Batch: 18379
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 06/01/2019 2311
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Hexachloroethane
670
500
1
74
30-96
06/11/20191325
Indeno(1,2,3-c,d)pyrene
670
670
1
100
42-123
06/11/20191325
Isophorone
670
610
1
91
41-113
06/11/20191325
2-Methyl naphthalene
670
580
1
87
10-107
06/11/20191325
2-Methylphenol
670
570
1
85
32-107
06/11/20191325
3+4-Methylphenol
670
570
1
86
39-108
06/11/20191325
Naphthalene
670
580
1
87
10-112
06/11/20191325
2-Nitroaniline
670
710
1
106
45-123
06/11/20191325
3-Nitroaniline
670
630
1
94
24-127
06/11/20191325
4-Nitroaniline
670
730
1
110
48-127
06/11/20191325
Nitrobenzene
670
560
1
84
33-114
06/11/20191325
2-Nitrophenol
670
550
1
82
35-108
06/11/20191325
4-Nitrophenol
1300
1300
1
97
18-154
06/11/20191325
N-Nitrosodi-n-propylamine
670
550
1
82
32-115
06/11/20191325
N-Nitrosodiphenylamine (Diphenylamine)
670
670
1
100
53-150
06/11/2019 1325
Pentachlorophenol
1300
880
1
66
27-138
06/11/20191325
Phenanthrene
670
630
1
94
16-123
06/11/20191325
Phenol
670
550
1
83
36-108
06/11/20191325
Pyrene
670
650
1
97
34-121
06/11/20191325
2,4,5-Trichlorophenol
670
610
1
92
46-122
06/11/20191325
2,4,6-Trichlorophenol
670
600
1
90
38-115
06/11/20191325
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 88 24-137
2-Fluorophenol 80 16-136
Nitrobenzene-d5 90 12-144
Phenol-d5 82 26-148
Terphenyl-d14 112 20-127
2,4,6-Tribromophenol 100 27-128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 57 of 88

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: UE31010-003MS
Matrix:
Solid
Batch: 18379
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 06/01/2019 2311
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
(ug/kg)
Q
Dil
% Rec
Limit
Analysis Date
Acenaphthene
960
880
1600
10
68
12-111
06/11/2019 2156
Acenaphthylene
ND
880
980
10
111
44-122
06/11/2019 2156
Acetophenone
ND
880
1200
N
10
140
30-130
06/11/2019 2156
Anthracene
2300
880
2800
10
57
16-122
06/11/2019 2156
Atrazine
ND
880
2200
N
10
244
30-130
06/11/2019 2156
Benzaldehyde
ND
880
680
10
77
10-110
06/11/2019 2156
Benzo(a)anthracene
ND
880
880
10
99
40-121
06/11/2019 2156
Benzo(a)pyrene
ND
880
820
10
93
36-114
06/11/2019 2156
Benzo(k)fluoranthene
ND
880
780
10
89
38-123
06/11/2019 2156
Benzo(g,h,i)perylene
ND
880
650
10
73
43-120
06/11/2019 2156
Benzo(k)fluoranthene
ND
880
780
10
88
40-126
06/11/2019 2156
1,1'-Biphenyl
ND
880
810
10
92
30-130
06/11/2019 2156
4-Bromophenyl phenyl ether
ND
880
1600
N
10
176
30-130
06/11/2019 2156
Butyl benzyl phthalate
ND
880
920
10
104
30-130
06/11/2019 2156
Caprolactam
ND
880
280
10
32
30-130
06/11/2019 2156
Carbazole
ND
880
1100
10
125
30-130
06/11/2019 2156
bis (2-Chloro-1-methylethyl) ether
ND
880
620
10
71
30-130
06/11/2019 2156
4-Chloro-3-methyl phenol
ND
880
1300
N
10
147
30-130
06/11/2019 2156
4-Chloroaniline
ND
880
420
10
48
17-106
06/11/2019 2156
bis(2-Chloroethoxy)methane
ND
880
680
10
78
30-130
06/11/2019 2156
bis(2-Chloroethyl)ether
ND
880
610
10
69
30-130
06/11/2019 2156
2-Chloronaphthalene
ND
880
780
10
88
30-130
06/11/2019 2156
2-Chlorophenol
ND
880
640
10
72
30-130
06/11/2019 2156
4-Chlorophenyl phenyl ether
ND
880
890
10
100
30-130
06/11/2019 2156
Chrysene
ND
880
840
10
95
41-124
06/11/2019 2156
Dibenzo(a,h)anthracene
ND
880
700
10
80
38-125
06/11/2019 2156
Dibenzofuran
ND
880
930
10
106
30-130
06/11/2019 2156
3,3'-Dichlorobenzidine
ND
880
730
10
83
10-119
06/11/2019 2156
2,4-Dichlorophenol
ND
880
3700
N
10
417
30-130
06/11/2019 2156
Diethylphthalate
ND
880
1100
10
121
30-130
06/11/2019 2156
Dimethyl phthalate
ND
880
1300
N
10
149
30-130
06/11/2019 2156
2,4-Dimethylphenol
ND
880
1700
N
10
194
30-130
06/11/2019 2156
Di-n-butyl phthalate
ND
880
880
10
100
30-130
06/11/2019 2156
4,6-Dinitro-2-methyl phenol
ND
880
1200
N
10
135
30-130
06/11/2019 2156
2,4-Dinitrophenol
ND
1800
3900
N
10
218
30-130
06/11/2019 2156
2,4-Dinitrotoluene
ND
880
3400
N
10
381
30-130
06/11/2019 2156
2,6-Dinitrotoluene
ND
880
900
10
102
30-130
06/11/2019 2156
Di-n-octylphthalate
ND
880
780
10
88
30-130
06/11/2019 2156
bis(2-Ethylhexyl)phthalate
ND
880
880
10
100
30-130
06/11/2019 2156
Fluoranthene
280
880
1000
10
87
26-133
06/11/2019 2156
Fluorene
990
880
1600
10
73
19-108
06/11/2019 2156
Hexachlorobenzene
ND
880
880
10
100
30-130
06/11/2019 2156
Hexachlorobutadiene
ND
880
720
10
81
30-130
06/11/2019 2156
Hexachlorocyclopentadiene
ND
4400
ND
N
10
0.00
30-130
06/11/2019 2156
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 58 of 88

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: UE31010-003MS
Matrix:
Solid
Batch: 18379
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 06/01/2019 2311
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
(ug/kg)
Q
Dil
% Rec
Limit
Analysis Date
Hexachloroethane
ND
880
510
10
58
30-130
06/11/2019 2156
Indeno(1,2,3-c,d)pyrene
ND
880
710
10
80
42-123
06/11/2019 2156
Isophorone
ND
880
1600
N
10
181
30-130
06/11/2019 2156
2-Methyl naphthalene
ND
880
860
10
97
10-107
06/11/2019 2156
2-Methylphenol
ND
880
560
10
63
30-130
06/11/2019 2156
3+4-Methylphenol
ND
880
550
10
62
30-130
06/11/2019 2156
Naphthalene
ND
880
930
10
105
10-112
06/11/2019 2156
2-Nitroaniline
ND
880
1000
10
118
30-130
06/11/2019 2156
3-Nitroaniline
ND
880
2000
N
10
223
30-130
06/11/2019 2156
4-Nitroaniline
ND
880
2600
N
10
291
30-130
06/11/2019 2156
Nitrobenzene
ND
880
1000
10
116
30-130
06/11/2019 2156
2-Nitrophenol
ND
880
1200
N
10
135
30-130
06/11/2019 2156
4-Nitrophenol
ND
1800
3900
N
10
218
30-130
06/11/2019 2156
N-Nitrosodi-n-propylamine
ND
880
730
10
82
30-130
06/11/2019 2156
N-Nitrosodiphenylamine (Diphenylamine)
ND
880
8000
N
10
906
30-130
06/11/2019 2156
Pentachlorophenol
ND
1800
2900
N
10
162
30-130
06/11/2019 2156
Phenanthrene
4000
880
3900
N
10
-6.1
16-123
06/11/2019 2156
Phenol
ND
880
610
10
70
30-130
06/11/2019 2156
Pyrene
2000
880
2500
10
54
34-121
06/11/2019 2156
2,4,5-Trichlorophenol
ND
880
770
10
87
30-130
06/11/2019 2156
2,4,6-Trichlorophenol
ND
880
1600
N
10
182
30-130
06/11/2019 2156
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 87 24-137
2-Fluorophenol 62 16-136
Nitrobenzene-d5 61 12-144
Phenol-d5 66 26-148
Terphenyl-d14 102 20-127
2,4,6-Tribromophenol 115 27-128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 59 of 88

Semivolatile Organic Compounds by GC/MS - MSD
Sample ID: UE31010-003MD
Matrix:
Solid
Batch: 18379
Prep
Method:
3546
Analytical Method: 8270E
Prep Date: 06/01/2019 2311
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/kg)
(ug/kg)
(ug/kg)
Q
Dil
% Rec
% RPD
Limit
Limit
Analysis Date
Acenaphthene
960
880
1900
10
102
17
12-111
30
06/11/2019 2220
Acenaphthylene
ND
880
1000
10
119
6.3
44-122
30
06/11/2019 2220
Acetophenone
ND
880
1600
N
10
181
25
30-130
40
06/11/2019 2220
Anthracene
2300
880
3200
10
100
13
16-122
30
06/11/2019 2220
Atrazine
ND
880
2400
N
10
272
10
30-130
40
06/11/2019 2220
Benzaldehyde
ND
880
710
10
81
4.0
10-110
40
06/11/2019 2220
Benzo(a)anthracene
ND
880
890
10
101
1.2
40-121
30
06/11/2019 2220
Benzo(a)pyrene
ND
880
850
10
96
2.9
36-114
30
06/11/2019 2220
Benzo(k)fluoranthene
ND
880
800
10
91
2.1
38-123
30
06/11/2019 2220
Benzo(g,h,i)perylene
ND
880
690
10
78
6.5
43-120
30
06/11/2019 2220
Benzo(k)fluoranthene
ND
880
820
10
93
5.4
40-126
30
06/11/2019 2220
1,1'-Biphenyl
ND
880
880
10
101
8.4
30-130
40
06/11/2019 2220
4-Bromophenyl phenyl ether
ND
880
1400
N
10
161
9.6
30-130
40
06/11/2019 2220
Butyl benzyl phthalate
ND
880
940
10
108
2.2
30-130
40
06/11/2019 2220
Caprolactam
ND
880
620
+
10
71
75
30-130
40
06/11/2019 2220
Carbazole
ND
880
1200
N
10
136
7.4
30-130
40
06/11/2019 2220
bis (2-Chloro-1-methylethyl) ether
ND
880
650
10
74
3.9
30-130
40
06/11/2019 2220
4-Chloro-3-methyl phenol
ND
880
1400
N
10
159
7.1
30-130
40
06/11/2019 2220
4-Chloroaniline
ND
880
420
10
47
1.7
17-106
40
06/11/2019 2220
bis(2-Chloroethoxy)methane
ND
880
720
10
82
5.1
30-130
40
06/11/2019 2220
bis(2-Chloroethyl)ether
ND
880
640
10
72
4.7
30-130
40
06/11/2019 2220
2-Chloronaphthalene
ND
880
800
10
91
2.8
30-130
40
06/11/2019 2220
2-Chlorophenol
ND
880
670
10
76
4.5
30-130
40
06/11/2019 2220
4-Chlorophenyl phenyl ether
ND
880
1100
10
120
17
30-130
40
06/11/2019 2220
Chrysene
ND
880
880
10
100
4.6
41-124
30
06/11/2019 2220
Dibenzo(a,h)anthracene
ND
880
730
10
83
3.3
38-125
30
06/11/2019 2220
Dibenzofuran
ND
880
1000
10
118
10
30-130
40
06/11/2019 2220
3,3'-Dichlorobenzidine
ND
880
660
10
75
10
10-119
40
06/11/2019 2220
2,4-Dichlorophenol
ND
880
4600
N
10
526
22
30-130
40
06/11/2019 2220
Diethylphthalate
ND
880
1100
10
127
3.9
30-130
40
06/11/2019 2220
Dimethyl phthalate
ND
880
1400
N
10
164
8.9
30-130
40
06/11/2019 2220
2,4-Dimethylphenol
ND
880
1700
N
10
195
0.39
30-130
40
06/11/2019 2220
Di-n-butyl phthalate
ND
880
900
10
102
1.3
30-130
40
06/11/2019 2220
4,6-Dinitro-2-methyl phenol
ND
880
1200
N
10
138
1.2
30-130
40
06/11/2019 2220
2,4-Dinitrophenol
ND
1800
4700
N
10
266
19
30-130
40
06/11/2019 2220
2,4-Dinitrotoluene
ND
880
3800
N
10
437
13
30-130
40
06/11/2019 2220
2,6-Dinitrotoluene
ND
880
430
+
10
48
72
30-130
40
06/11/2019 2220
Di-n-octylphthalate
ND
880
800
10
91
2.8
30-130
40
06/11/2019 2220
bis(2-Ethylhexyl)phthalate
ND
880
900
10
103
2.5
30-130
40
06/11/2019 2220
Fluoranthene
280
880
1100
10
90
2.6
26-133
30
06/11/2019 2220
Fluorene
990
880
2000
N
10
117
21
19-108
30
06/11/2019 2220
Hexachlorobenzene
ND
880
890
10
101
0.72
30-130
40
06/11/2019 2220
Hexachlorobutadiene
ND
880
740
10
84
3.0
30-130
40
06/11/2019 2220
Hexachlorocyclopentadiene
ND
4400
7100
N,+
10
162
200
30-130
40
06/11/2019 2220
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 60 of 88

Semivolatile Organic Compounds by GC/MS - MSD
Sample ID: UE31010-003MD
Matrix:
Solid
Batch: 18379
Prep
Method:
3546
Analytical Method: 8270E
Prep Date: 06/01/2019 2311
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/kg)
(ug/kg)
(ug/kg)
Q
Dil
% Rec
% RPD
Limit
Limit
Analysis Date
Hexachloroethane
ND
880
480
10
54
7.0
30-130
40
06/11/2019 2220
Indeno(1,2,3-c,d)pyrene
ND
880
700
10
80
0.42
42-123
30
06/11/2019 2220
Isophorone
ND
880
1900
N
10
213
16
30-130
40
06/11/2019 2220
2-Methyl naphthalene
ND
880
1100
N
10
124
24
10-107
30
06/11/2019 2220
2-Methylphenol
ND
880
540
10
61
4.0
30-130
40
06/11/2019 2220
3+4-Methylphenol
ND
880
590
10
67
6.0
30-130
40
06/11/2019 2220
Naphthalene
ND
880
1000
N
10
113
7.2
10-112
30
06/11/2019 2220
2-Nitroaniline
ND
880
1300
N
10
147
22
30-130
40
06/11/2019 2220
3-Nitroaniline
ND
880
1200
N,+
10
141
46
30-130
40
06/11/2019 2220
4-Nitroaniline
ND
880
3000
N
10
344
16
30-130
40
06/11/2019 2220
Nitrobenzene
ND
880
1100
10
129
10
30-130
40
06/11/2019 2220
2-Nitrophenol
ND
880
1500
N
10
167
21
30-130
40
06/11/2019 2220
4-Nitrophenol
ND
1800
4200
N
10
241
9.4
30-130
40
06/11/2019 2220
N-Nitrosodi-n-propylamine
ND
880
790
10
90
8.3
30-130
40
06/11/2019 2220
N-Nitrosodiphenylamine (Diphenylamine)
ND
880
9800
N
10
1120
21
30-130
40
06/11/2019 2220
Pentachlorophenol
ND
1800
3200
N
10
184
12
30-130
40
06/11/2019 2220
Phenanthrene
4000
880
5300
N
10
151
30
16-123
30
06/11/2019 2220
Phenol
ND
880
640
10
73
4.4
30-130
40
06/11/2019 2220
Pyrene
2000
880
2900
10
98
14
34-121
30
06/11/2019 2220
2,4,5-Trichlorophenol
ND
880
1100
10
121
32
30-130
40
06/11/2019 2220
2,4,6-Trichlorophenol
ND
880
2000
N
10
230
23
30-130
40
06/11/2019 2220
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 93 24-137
2-Fluorophenol 66 16-136
Nitrobenzene-d5 66 12-144
Phenol-d5 66 26-148
Terphenyl-d14 105 20-127
2,4,6-Tribromophenol 126 27-128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 61 of 88

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ18849-001 Matrix: Solid
Batch: 18849 Prep Method: 3546
Analytical Method: 8270E Prep Date: 06/06/2019 1705
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
13
5.0
ug/kg
06/07/2019 1326
Acenaphthylene
ND
1
13
3.2
ug/kg
06/07/2019 1326
Acetophenone
ND
1
67
6.9
ug/kg
06/07/2019 1326
Anthracene
ND
1
13
2.6
ug/kg
06/07/2019 1326
Atrazine
ND
1
67
5.0
ug/kg
06/07/2019 1326
Benzaldehyde
ND
1
67
5.0
ug/kg
06/07/2019 1326
Benzo(a)anthracene
ND
1
13
2.0
ug/kg
06/07/2019 1326
Benzo(a)pyrene
ND
1
13
1.7
ug/kg
06/07/2019 1326
Benzo(k)fluoranthene
ND
1
13
1.9
ug/kg
06/07/2019 1326
Benzo(g,h,i)perylene
ND
1
13
3.8
ug/kg
06/07/2019 1326
Benzo(k)fluoranthene
ND
1
13
2.1
ug/kg
06/07/2019 1326
1,1'-Biphenyl
ND
1
67
5.0
ug/kg
06/07/2019 1326
4-Bromophenyl phenyl ether
ND
1
67
5.0
ug/kg
06/07/2019 1326
Butyl benzyl phthalate
ND
1
67
5.0
ug/kg
06/07/2019 1326
Caprolactam
ND
1
67
12
ug/kg
06/07/2019 1326
Carbazole
ND
1
67
5.0
ug/kg
06/07/2019 1326
bis (2-Chloro-1-methylethyl) ether
ND
1
67
6.7
ug/kg
06/07/2019 1326
4-Chloro-3-methyl phenol
ND
1
67
5.6
ug/kg
06/07/2019 1326
4-Chloroaniline
ND
1
67
5.8
ug/kg
06/07/2019 1326
bis(2-Chloroethoxy)methane
ND
1
67
5.0
ug/kg
06/07/2019 1326
bis(2-Chloroethyl)ether
ND
1
67
5.5
ug/kg
06/07/2019 1326
2-Chloronaphthalene
ND
1
67
13
ug/kg
06/07/2019 1326
2-Chlorophenol
ND
1
67
11
ug/kg
06/07/2019 1326
4-Chlorophenyl phenyl ether
ND
1
67
5.0
ug/kg
06/07/2019 1326
Chrysene
ND
1
13
3.1
ug/kg
06/07/2019 1326
Dibenzo(a,h)anthracene
ND
1
13
3.0
ug/kg
06/07/2019 1326
Dibenzofuran
ND
1
67
5.0
ug/kg
06/07/2019 1326
3,3'-Dichlorobenzidine
ND
1
67
10
ug/kg
06/07/2019 1326
2,4-Dichlorophenol
ND
1
67
6.6
ug/kg
06/07/2019 1326
Diethylphthalate
ND
1
67
5.0
ug/kg
06/07/2019 1326
Dimethyl phthalate
ND
1
67
5.0
ug/kg
06/07/2019 1326
2,4-Dimethylphenol
ND
1
67
11
ug/kg
06/07/2019 1326
Di-n-butyl phthalate
ND
1
67
9.8
ug/kg
06/07/2019 1326
4,6-Dinitro-2-methyl phenol
ND
1
330
25
ug/kg
06/07/2019 1326
2,4-Dinitrophenol
ND
1
330
25
ug/kg
06/07/2019 1326
2,4-Dinitrotoluene
ND
1
130
12
ug/kg
06/07/2019 1326
2,6-Dinitrotoluene
ND
1
130
11
ug/kg
06/07/2019 1326
Di-n-octylphthalate
ND
1
67
5.0
ug/kg
06/07/2019 1326
bis(2-Ethylhexyl)phthalate
ND
1
67
25
ug/kg
06/07/2019 1326
Fluoranthene
ND
1
13
2.2
ug/kg
06/07/2019 1326
Fluorene
ND
1
13
1.9
ug/kg
06/07/2019 1326
Hexachlorobenzene
ND
1
67
5.0
ug/kg
06/07/2019 1326
Hexachlorobutadiene
ND
1
67
8.5
ug/kg
06/07/2019 1326
Hexachlorocyclopentadiene
ND
1
330
25
ug/kg
06/07/2019 1326
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 62 of 88

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ18849-001 Matrix: Solid
Batch: 18849 Prep Method: 3546
Analytical Method: 8270E Prep Date: 06/06/2019 1705
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
67
5.5
ug/kg
06/07/20191326
Indeno(1,2,3-c,d)pyrene
ND
1
13
2.7
ug/kg
06/07/20191326
Isophorone
ND
1
67
6.2
ug/kg
06/07/20191326
2-Methyl naphthalene
ND
1
13
5.9
ug/kg
06/07/20191326
2-Methylphenol
ND
1
67
18
ug/kg
06/07/20191326
3+4-Methylphenol
ND
1
130
17
ug/kg
06/07/20191326
Naphthalene
ND
1
13
4.7
ug/kg
06/07/20191326
2-Nitroaniline
ND
1
130
19
ug/kg
06/07/20191326
3-Nitroaniline
ND
1
130
18
ug/kg
06/07/20191326
4-Nitroaniline
ND
1
130
20
ug/kg
06/07/20191326
Nitrobenzene
ND
1
67
7.8
ug/kg
06/07/20191326
2-Nitrophenol
ND
1
130
10
ug/kg
06/07/20191326
4-Nitrophenol
ND
1
330
100
ug/kg
06/07/20191326
N-Nitrosodi-n-propylamine
ND
1
67
5.7
ug/kg
06/07/20191326
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
67
5.1
ug/kg
06/07/2019 1326
Pentachlorophenol
ND
1
330
27
ug/kg
06/07/20191326
Phenanthrene
ND
1
13
2.3
ug/kg
06/07/20191326
Phenol
ND
1
67
6.2
ug/kg
06/07/20191326
Pyrene
ND
1
13
2.8
ug/kg
06/07/20191326
2,4,5-Trichlorophenol
ND
1
67
5.0
ug/kg
06/07/20191326
2,4,6-Trichlorophenol
ND
1
67
5.0
ug/kg
06/07/20191326
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 54 24-137
2-Fluorophenol 64 16-136
Nitrobenzene-d5
74
12-144
Phenol-d5
67
26-148
Terphenyl-d14
77
20-127
2,4,6-Tribromophenol
59
27-128
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 63 of 88

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ18849-002
Matrix:
Solid
Batch: 18849
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 06/06/2019 1705
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
670
410
1
61
12-111
06/07/2019 1351
Acenaphthylene
670
370
1
56
44-122
06/07/2019 1351
Acetophenone
670
480
1
72
48-111
06/07/2019 1351
Anthracene
670
410
1
61
16-122
06/07/2019 1351
Atrazine
670
420
1
63
48-116
06/07/2019 1351
Benzaldehyde
670
300
1
45
10-110
06/07/2019 1351
Benzo(a)anthracene
670
420
1
62
40-121
06/07/2019 1351
Benzo(a)pyrene
670
460
1
69
36-114
06/07/2019 1351
Benzo(k)fluoranthene
670
460
1
69
38-123
06/07/2019 1351
Benzo(g,h,i)perylene
670
470
1
71
43-120
06/07/2019 1351
Benzo(k)fluoranthene
670
490
1
74
40-126
06/07/2019 1351
1,1'-Biphenyl
670
380
1
57
49-110
06/07/2019 1351
4-Bromophenyl phenyl ether
670
360
1
54
46-118
06/07/2019 1351
Butyl benzyl phthalate
670
550
1
83
46-128
06/07/2019 1351
Caprolactam
670
420
1
62
43-121
06/07/2019 1351
Carbazole
670
410
1
62
47-128
06/07/2019 1351
bis (2-Chloro-1-methylethyl) ether
670
540
1
81
31-102
06/07/2019 1351
4-Chloro-3-methyl phenol
670
470
1
70
49-118
06/07/2019 1351
4-Chloroaniline
670
390
1
58
17-106
06/07/2019 1351
bis(2-Chloroethoxy)methane
670
440
1
66
39-108
06/07/2019 1351
bis(2-Chloroethyl)ether
670
560
1
84
32-105
06/07/2019 1351
2-Chloronaphthalene
670
350
1
53
31-127
06/07/2019 1351
2-Chlorophenol
670
490
1
73
37-106
06/07/2019 1351
4-Chlorophenyl phenyl ether
670
330
1
49
47-116
06/07/2019 1351
Chrysene
670
430
1
64
41-124
06/07/2019 1351
Dibenzo(a,h)anthracene
670
480
1
72
38-125
06/07/2019 1351
Dibenzofuran
670
350
1
53
45-112
06/07/2019 1351
3,3'-Dichlorobenzidine
670
290
1
44
10-119
06/07/2019 1351
2,4-Dichlorophenol
670
390
1
58
41-113
06/07/2019 1351
Diethylphthalate
670
400
1
60
49-123
06/07/2019 1351
Dimethyl phthalate
670
370
1
55
48-120
06/07/2019 1351
2,4-Dimethylphenol
670
600
1
90
33-123
06/07/2019 1351
Di-n-butyl phthalate
670
440
1
66
51-129
06/07/2019 1351
4,6-Dinitro-2-methyl phenol
670
520
1
79
40-130
06/07/2019 1351
2,4-Dinitrophenol
1300
1000
1
76
10-113
06/07/2019 1351
2,4-Dinitrotoluene
670
420
1
63
48-124
06/07/2019 1351
2,6-Dinitrotoluene
670
390
1
58
47-125
06/07/2019 1351
Di-n-octylphthalate
670
580
1
87
49-142
06/07/2019 1351
bis(2-Ethylhexyl)phthalate
670
500
1
74
45-128
06/07/2019 1351
Fluoranthene
670
390
1
58
26-133
06/07/2019 1351
Fluorene
670
380
1
57
19-108
06/07/2019 1351
Hexachlorobenzene
670
380
1
57
44-122
06/07/2019 1351
Hexachlorobutadiene
670
370
1
56
33-103
06/07/2019 1351
Hexachlorocyclopentadiene
3300
2400
1
72
18-121
06/07/2019 1351
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 64 of 88

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ18849-002
Matrix:
Solid
Batch: 18849
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 06/06/2019 1705
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg)
Q Dil
% Rec
Limit
Analysis Date
Hexachloroethane
670
460
1
69
30-96
06/07/20191351
Indeno(1,2,3-c,d)pyrene
670
470
1
71
42-123
06/07/20191351
Isophorone
670
490
1
73
41-113
06/07/20191351
2-Methyl naphthalene
670
400
1
60
10-107
06/07/20191351
2-Methylphenol
670
610
1
91
32-107
06/07/20191351
3+4-Methylphenol
670
540
1
82
39-108
06/07/20191351
Naphthalene
670
440
1
66
10-112
06/07/20191351
2-Nitroaniline
670
450
1
67
45-123
06/07/20191351
3-Nitroaniline
670
370
1
55
24-127
06/07/20191351
4-Nitroaniline
670
440
1
66
48-127
06/07/20191351
Nitrobenzene
670
540
1
82
33-114
06/07/20191351
2-Nitrophenol
670
440
1
66
35-108
06/07/20191351
4-Nitrophenol
1300
1100
1
82
18-154
06/07/20191351
N-Nitrosodi-n-propylamine
670
600
1
91
32-115
06/07/20191351
N-Nitrosodiphenylamine (Diphenylamine)
670
430
1
64
53-150
06/07/2019 1351
Pentachlorophenol
1300
810
1
60
27-138
06/07/20191351
Phenanthrene
670
420
1
63
16-123
06/07/20191351
Phenol
670
560
1
84
36-108
06/07/20191351
Pyrene
670
450
1
67
34-121
06/07/20191351
2,4,5-Trichlorophenol
670
350
1
52
46-122
06/07/20191351
2,4,6-Trichlorophenol
670
350
1
52
38-115
06/07/20191351
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 58 24-137
2-Fluorophenol 74 16-136
Nitrobenzene-d5 89 12-144
Phenol-d5 84 26-148
Terphenyl-d14 76 20-127
2,4,6-Tribromophenol 64 27-128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 65 of 88

TPH - DRO - MB
Sample ID: UQ18378-001 Matrix: Solid
Batch: 18378 Prep Method: 3550C
Analytical Method: 8015C Prep Date: 05/31/2019 2314
Parameter Result Q Dil LOQ DL Units Analysis Date
TPH-DRO ND 1 6700 3200 ug/kg 06/05/20191926
Surrogate
o - Terphenyl
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
89 55-120
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 66 of 88

TPH - DRO - LCS
Sample ID: UQ18378-002
Matrix: Solid
Batch: 18378
Prep Method: 3550C
Analytical Method: 8015C
Prep Date: 05/31/2019 2314
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil % Rec Limit Analysis Date
TPH-DRO
83000
70000
1 84 70-130 06/05/20191945
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
95 55-120
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 67 of 88

MA EPH (aliphatics) - MB
Sample ID: UQ18431-001 Matrix: Solid
Batch: 18431 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 06/02/2019 2016
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics ND 1 10 10 mg/kg 06/04/2019 1745
C19 - C36 Aliphatics ND 1 10 10 mg/kg 06/04/2019 1745
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 96 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 68 of 88

MA EPH (aliphatics) - LCS
Sample ID: UQ18431-002
Matrix: Solid
Batch: 18431
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 06/02/2019 2016
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg)
Q Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
30
19
1 62
40-140 06/04/2019 1815
C19 - C36 Aliphatics
40
43
1 107
40-140 06/04/2019 1815
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 98 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 69 of 88

MA EPH (aliphatics) - LCSD
Sample ID: UQ18431-003
Matrix: Solid
Batch: 18431
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 06/02/2019 2016
Spike
Amount
Result
% Rec
% RPD
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
30
20
1 68 9.0 40-140
25 06/04/2019 1844
C19 - C36 Aliphatics
40
42
1 104 2.4 40-140
25 06/04/2019 1844
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 99 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 70 of 88

MA EPH (aromatics) - MB
Sample ID: UQ18432-001 Matrix: Solid
Batch: 18432 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 06/02/2019 2016
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 10 10 mg/kg 06/04/2019 2309
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 109 40-140
2-Fluorobiphenyl (fractionation 1) 115 40-140
o - Terphenyl (aromatic) 82 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 71 of 88

MA EPH (aromatics) - LCS
Sample ID: UQ18432-002
Matrix: Solid
Batch: 18432
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 06/02/2019 2016
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
85
68
1 80 40-140 06/04/2019 2338
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2) 98 40-140
2-Fluorobiphenyl (fractionation 1) 109 40-140
o - Terphenyl (aromatic) 86 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 72 of 88

MA EPH (aromatics) - LCSD
Sample ID: UQ18432-003 Matrix: Solid
Batch: 18432 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 06/02/2019 2016
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 85 76 1 90 11 40-140 25 06/05/2019 0008
Surrogate
2-Bromonaphthalene (fractionation 2)
2-Fluorobiphenyl (fractionation 1)
o - Terphenyl (aromatic)
Acceptance
Q % Rec Limit
114
40-140
127
40-140
99
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 73 of 88

TPH- GRO -MB
Sample ID: UQ18370-001 Matrix: Solid
Batch: 18370 Prep Method: 5030E
Analytical Method: 8015C
Parameter Result Q Dil LOQ DL Units Analysis Date
TPH-GRO ND 1 5000 2500 ug/kg 05/31/20191728
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 110 23-179
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 74 of 88

TPH - GRO - LCS
Sample ID: UQ18370-002 Matrix: Solid
Batch: 18370 Prep Method: 5030E
Analytical Method: 8015C
Spike
Amount Result % Rec
Parameter (ug/kg) (ug/kg) Q Dil % Rec Limit Analysis Date
TPH-GRO 50000 52000 1 104 70-130 05/31/20191641
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
107 23-179
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 75 of 88

TPH - GRO - LCSD
Sample ID: UQ18370-003
Matrix: Solid
Batch: 18370
Prep Method: 5030E
Analytical Method: 8015C
Spike
Amount
Result
% Rec % RPD
Parameter
(ug/kg)
(ug/kg) Q
Dil % Rec % RPD Limit Limit Analysis Date
TPH-GRO
50000
52000
1 105 0.58 70-130 20 05/31/20191704
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
106 23-179
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 76 of 88

MADEP VPH (aromatics) - MB
Sample ID: UQ19103-001 Matrix: Solid
Batch: 19103 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 1.3 0.50 mg/kg 06/07/2019 1444
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 82 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 77 of 88

MADEP VPH (aromatics) - LCS
Sample ID: UQ19103-002 Matrix: Solid
Batch: 19103 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 1.3 1.5 1 120 70-130 06/07/2019 1348
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
100 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 78 of 88

MADEP VPH (aromatics) - LCSD
Sample ID: UQ19103-003 Matrix: Solid
Batch: 19103 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 1.3 1.6 1 128 6.5 70-130 25 06/07/2019 1416
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 100 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 79 of 88

MADEP VPH (aliphatics) - MB
Sample ID: UQ19104-001 Matrix: Solid
Batch: 19104 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 3.8 0.75 mg/kg 06/07/2019 1444
C9 - C12 Aliphatics ND 1 3.8 0.75 mg/kg 06/07/2019 1444
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 80 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 80 of 88

MADEP VPH (aliphatics) - LCS
Sample ID: UQ19104-002
Matrix: Solid
Batch: 19104
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter (mg/kg)
(mg/kg) Q
Dil % Rec
Limit Analysis Date
C5 - C8 Aliphatics 7.5
8.5
1 114
70-130 06/07/2019 1348
C9 - C12 Aliphatics 8.8
10
1 114
70-130 06/07/2019 1348
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID) 94 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 81 of 88

MADEP VPH (aliphatics) - LCSD
Sample ID: UQ19104-003
Matrix: Solid
Batch: 19104
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
% RPD
Parameter (mg/kg)
(mg/kg) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics 7.5
9.2
1 122 7.4
70-130
25 06/07/2019 1416
C9 - C12 Aliphatics 8.8
11
1 126 9.5
70-130
25 06/07/2019 1416
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 98 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 82 of 88

MADEP VPH (aliphatics) - MB
Sample ID: UQ19250-001 Matrix: Solid
Batch: 19250 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C12 Aliphatics ND 1 3.8 0.75 mg/kg 06/07/2019 1444
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 80 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 83 of 88

MADEP VPH (aliphatics) - LCS
Sample ID: UQ19250-002 Matrix: Solid
Batch: 19250 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
C9 - C12 Aliphatics 8.8 10 1 114 70-130 06/07/2019 1348
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 94 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 84 of 88

MADEP VPH (aliphatics) - LCSD
Sample ID: UQ19250-003 Matrix: Solid
Batch: 19250 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C12 Aliphatics 8.8 11 1 126 9.5 70-130 25 06/07/2019 1416
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 98 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 85 of 88

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 86 of 88

SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 87 of 88

SHEALY ENVIRONMENTAL SERVICES, INC.
Shwly 6nvi=m tvl F;BmiQ .
Sample Receipt Checklist (SRC)
Client. laid-.4tiantic Cooler Ins cetcd by+date: �xH ! pS;ih+I 9
I Qeent of reccilrr: FSI C;Jient U UPS 0 FedFA Othcr.—
Yus
NO
1, %Mzrc uusludy seals present on the cnoier?
12. If cu.mdy gal s were ont, wore rhay intact and unbroken"
Yes
Nol D NA
PE SG'ip ID' tkTA Chlorine Strip ID, NA Tested by- NA
Original temperature 1 p9ij r ipt Vcrived (Corrected) temperaure uren reeeipi INSolid 511ap-QUP ID: 1MI l
4,3 14,3 -C NA ; NA -C NA INN _°C NA ,MA aC
lvietJhpd: ®xe+mpermu" 131arrk Against BattleF. rR Con TI? _ 5 IR GuL; lr arreciiuu `'C:
+ Faukv: 0
bferhod of,' Jaftt: V Wet Ice ❑ uc; lee PN ❑ r)ry I: r. ❑ None
❑ 'as
❑ No
ONA
1- Tf tempmturr of any cooler excaeded6.4°C, was Project Manager Nmified'�
PM was Notified by phone + ejuaiI f f"L—Lo4mv (circle one).
d. 1s the orunmercial crwr:.&A packing slip attached to this furrO
M No
®NA
Yes
❑ Nn
5. Wcr -ninr custody pnxeaiures ralinquishedrreceiu�xi}liolluxed�
Yes
NU
6, WvN samlpls EDs listed on the. CX)C'7
® Ym
❑ No
7, were swil pie Bs listjA on A samplc containers'?
Yes
❑ No
$, Was collection date & time listed ant the CaC''
Yo
❑ No
$, Was Coll ealien Jwj-- & tim a ILstad rnt all sample contai riimi?
® Ye*
C] No
10. Did all cont0.Eer 141,?el irihurination (ID, dace, time) agree with the CO+C?
Vus
❑ Na
I I, Were tests to toe performed listed on the CQC?
0 Yes
❑ No
13, Did all samples Orr Ive in lbv prop" cwtainera for earh tlett mUor in good condition
(unbroken, Uds nrr. cbc,ln
'�s
❑ N'
11, Was adoquaTe, sample volumo evrulalale7
709
Q No
14. Were elt smnplem rwaiveti within r the ImMilrg limn or 48 hours, whichever crwres Fr8I'
Yer
❑ No
t5- WeVe any soli ks tontniners missin excess eiMlt one) samples Ncrt listed nn C O C,?
❑ Yes
Q No
71 NA
16- Fon'Vi)A and JRSK-175 sair+Plm were bubbles present s" pnLL-sirl:" (V41or 6mm in diameter)
in any *Cbc VUA vials?
❑ Yrri
No
TEA
17, Were all DRalmetalsinuLricut samptea roceived at a PH af<
Ll Yet
0 Na
®Tti A
] 8. Were 01 C
yWLidC sampics rrcei ued al a P14 > 17 and suifide sample.5 reaeivcd ar a pi I �K!
❑ Yrs
❑ No
ONA
J9. 14rcrcal applirableNgj.TKNkyaul e.+ atjoV6;S f<U„3mgfLj sample$ free Of, esidrla.
Ctlhxinc?
❑ ,�s
❑ o
NA
20, Were client rc wkslrequestt (i-e- (e�u�tstad dilutions, msfMST) designations, eoC---)
oa,-r%&Aly transcribed from the COC into the cx)mmcnt section itt LTMS7
❑ Yc
-No
IT,-
W&3 the c uotc lnunber Jisled M the euntaincr label? If yes, Quote# NA
Sample ]Preservation (hduat bo rompketed for (illy Sanaplv(s) inr:orrecdy przsen+ed art. with Juaadspacej
Sarnpla(s) NA were ra�eivcxl iucorreNly preserved and w= adjusted accordi?:kI •
iti saiaipk receiving witli NA mL of circle Due- 1-12SO4, HNM HC1. NOT using Six #IAA
imc ofprescrvaiiorl NA lF more than aLw preservative is noeded, pleaRe note in the camntenrs bel[rw,
Sampie(s) NA were maivDd with bubbles>6 mm iu diatneter-
Sanoplos) NA were received with TRC > 0.5 me/L. (If #I9? is No) andTerc
]l1Ste� eraCDRlin ly in sample. rereil"Jtig with sodium thiosulfate (Na,S�oj with Shea 1D: NA
SR Mrcnrle lrib6L applied by- J5H Dope; 05/31i19
C olnl r Un l:t:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 88 of 88

Beverly, Trudy
From: Greg Icenhour <[e-mail]>
Sent: Tuesday, July 2, 2019 11:11 AM
To: Beverly, Trudy; Patrick Kelly
Cc: Kenneth Fuquay
Subject: RE: [External] FW: 7609 Linda Lakes Drive IAA Report
Importance: High
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to [e-mail]
Thanks Trudy — Patrick, run with this ASAP.
With best regards,
I d Mantic
Enginoonng A Ems nm nW Sclwt o &
Greg D. Icenhour, P.G., MBA
Vice President/Charlotte Branch Manager
MID -ATLANTIC ASSOCIATES, INC.
1125 E. Morehead Street, Suite 104
Charlotte, NC 28204-2849
[phone]— Phone
[phone] — Fax
[phone]— Mobile
Corporate Office:
409 Rogers View Court
Raleigh, NC 27610
Office: [phone]
Facsimile: [phone]
Outstanding service since 1993
http://www.maaonline.com
Confidentiality Notice: The information contained in this e-mail is intended only for the individual or entity to whom it is
addressed. Its contents (including any attachments) may contain confidential and/or privileged information. If you are not an
intended recipient you must not use, disclose, disseminate, copy or print its contents. If you receive this e-mail in error, please
notify the sender by reply e-mail and delete and destroy the message.
From: Beverly, Trudy [mailto:[e-mail]]
Sent: Tuesday, July 02, 2019 11:10 AM
To: Greg Icenhour <[e-mail]>; Patrick Kelly <[e-mail]>

Cc: Kenneth Fuquay <[e-mail]>
Subject: RE: [External] FW: 7609 Linda Lakes Drive IAA Report
Greg and Patrick,
I can issue the conditional no further action letter once the Notice of Residual Petroleum has been received by this
office for review and signature before filing with the Mecklenburg County Register of Deeds. The conditional No
Further Action letter will then direct you to file the UST signed Notice of Residual Petroleum with Mecklenburg
County and conduct public notice. Once copies of the filed Notice of Residual Petroleum and public notice
documentation are received, I will issue a No Further Action letter to close the site.
Instructions and Form for Notice of Residual Petroleum with Alternate Land Use Restriction
https://deg.nc.gov/about/divisions/waste-management/ust/forms
Let me know if you have any questions,
Trudy
From: Greg Icenhour [mailto:[e-mail]]
Sent: Tuesday, July 2, 2019 10:54 AM
To: Beverly, Trudy <[e-mail]>; Patrick Kelly <[e-mail]>
Cc: Kenneth Fuquay <[e-mail]>
Subject: RE: [External] FW: 7609 Linda Lakes Drive IAA Report
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to [e-mail]
Hi Trudy —just an FYI, the owner is a non-profit and would like to get this property on the market as quickly as
feasible. A previous contract fell through due to the UST issues, which hopefully we can put to bed with a NORP.
Thanks for the assistance and have a great 4tnl
With best regards,
Mid cAtlantic
Greg D. Icenhour, P.G., MBA
Vice President/Charlotte Branch Manager
MID -ATLANTIC ASSOCIATES, INC.
1125 E. Morehead Street, Suite 104
Charlotte, NC 28204-2849
[phone]— Phone
[phone] — Fax
[phone]— Mobile
Corporate Office:
409 Rogers View Court
Raleigh, NC 27610
Office: [phone]
Facsimile: [phone]
Outstanding service since 1993

http://www.maaonIine.com
Confidentiality Notice: The information contained in this e-mail is intended only for the individual or entity to whom it is
addressed. Its contents (including any attachments) may contain confidential and/or privileged information. If you are not an
intended recipient you must not use, disclose, disseminate, copy or print its contents. If you receive this e-mail in error, please
notify the sender by reply e-mail and delete and destroy the message.
From: Beverly, Trudy[mailto:[e-mail]]
Sent: Tuesday, July 02, 2019 10:52 AM
To: Patrick Kelly <[e-mail]>
Cc: Greg Icenhour <[e-mail]>; Kenneth Fuquay <[e-mail]>
Subject: RE: [External] FW: 7609 Linda Lakes Drive IAA Report
I appreciate the update.
Thank you,
Trudy
Tle '�, Lam.
D E��
No
r& Orokes D d
N��,NCA��IINA LOT Sc o, Momud : Offilm
Department at Environmental quality Ci" 235-21
82 (OW
Email correspondence to and from this address is subject to ttie
!North Carolina Public Records Law and may be disclosed io third paidos.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.,gov/about/divisions/waste-management/ust/ast-
program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https:Hdeq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-mane eg ment- ig s=maps
File Review Procedures:
https:Hdeq.nc.,gov/about/divisions/waste-management/ust/file-review-procedures#mooresvill e-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https:Hedocs.deg.nc.gov/WasteManagement/Search.aspx
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/Electronic%20Document%20Submittal
%20Memo%20Update.pdf
https:Hfiles.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/UST%20file%20names%20for%20Las
erfiche.docx
From: Patrick Kelly [mailto:[e-mail]]
Sent: Tuesday, July 2, 2019 10:36 AM
To: Beverly, Trudy <[e-mail]>

Cc: Greg Icenhour <[e-mail]>; Kenneth Fuquay <[e-mail]>
Subject: [External] FW: 7609 Linda Lakes Drive IAA Report
Trudy,
I was having trouble burning this PDF to a CD to include with the hard copy of the report. A hard copy of the
report will go out in the mail today. Please do not hesitate to contact me if you have any questions or concerns.
Sincerely,
MidAtlantict'j.4I
Patrick R. Kelly, P.G.
Project Geologist
MID -ATLANTIC ASSOCIATES, INC.
1125 E. Morehead Street, Suite 104, Charlotte, NC 28204
980-585-1271 Office
704-560-0645 Mobile
www.MAAONLINE.com I Outstanding Service Since 1993
Confidentiality Notice: The information contained in this e-mail is intended only for the individual or entity to whom it is addressed.Its
contents (including any attachments) may contain confidential and/or privileged information. If you are not an intended recipient you must
not use, disclose, disseminate, copy or print its contents. If you receive this e-mail in error, please notify the sender by reply e-mail and
delete and destroy the message.