MO-9474_0_C_UST-12_20190329_UST Permanent Closure Report

opm
ENVIRONMENTAL
Risk Well Managed
March 29, 2019
Cookeville, Tennessee
1053 Oak Hill Drive Cookeville, TN 38501
f: 877.884.6775
t: 931.432.5552
Ms. Trudy Beverly
NCDEQ, Division of Waste Management, UST Section
610 East Center Avenue, Suite 301
Mooresville, North Carolina, 28115
Re: UST Permanent Closure Report
830 Dolly Street NW
Concord, Cabarrus County, North Carolina 28027
FAC ID# 00-0-0000025325
PM Project Number 15-4189-0-0001
Dear Ms. Beverly:
Tennessee Locations
Murfreesboro Knoxville
Chattanooga
On behalf of the owner for the subject property, PM Environmental, Inc. (PM) is submitting the
attached UST Permanent Closure Report requesting a no further action (NFA) status.
Please contact me at 865-329-7191 should you have any questions or comments concerning this
submittal.
Sincerely,
PM Environmental, Inc.
Maryse Speckner
Senior Project Consultant
Enclosure
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UNDERGROUND STORAGE TANK
PERMANENT CLOSURE REPORT
830 Dolly Street NW, Concord, North Carolina
PM Project Number 15-4389-0-0001
Prepared for.
Mr. Long Huynh
5868 Crimson Oak Court
Harrisburg, North Carolina 28075
Prepared by:
PM Environmental, Inc.
333 Troy Circle, Suite M
Knoxville, Tennessee 37923
www.pmenv.com

OPM
ENVIRONMENTAL
Risk Well Managep
Corporate Headquarters
Lansing, Michigan
3340 Ranger Road. Lansing. MI 48906
} 877 884 6775
t 517 321 3331
UST CLOSURE REPORT
FOR
Graham Construction Co. Inc.
830 Dolly Street NW
Concord, Cabarrus County, North Carolina 28027
Michigan Locations
Berkley Bay City
Grand Rapids Chesterfield
Lansing
Facility I.D. Number: 00-0-000002532
Latitude: 35.427868 North Longitude:-80.609851 West
March 29, 2019
PREPARED FOR:
Mr. Long Huynh
5868 Crimson Oak Court
Harrisburg, North Carolina
704-661-7078
CONSULTANT:
PM Environmental, Inc.
333 Troy Circle, Suite M
Knoxville, Tennessee
865-329-7191
PM Project No. 15-4389-0-0001
X-�A� ��- 'i "(D
Maryse Speckner John W. Hargraves, P.G.
Sr. Project Consultant Regional Manager/Senior Geologist
ALABAMA I FLORiaA I ILLINOIS I MICHIGAN I MISSISSIPPI 1 NEW JERSEY I NORTH CAROLINA I OHIO I TENNESSEE I WWW.PMENV.COM
QUALITY S E R V I C E SOLUTI 0NS

UST Closure Report for Graham Construction Co.
Located at located at 830 Dolly Street NW, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4389-0-0001; March 29, 2019
TABLE OF CONTENTS
TABLE OF CONTENTS............................................................................................................. 1
A.
Site Information.................................................................................................................... 2
1. Site Identification....................................................................................................... 2
2. Contact Information................................................................................................... 2
3. Release InformationN/A............................................................................................ 2
4. Report Certification.................................................................................................... 2
B.
Site History and Characterization.......................................................................................... 3
C.
Closure Procedures.............................................................................................................. 3
D.
Conclusions and Recommendations..................................................................................... 5
FIGURES
Figure 1 Property Vicinity Map
Figure 2 Generalized Diagram of the Subject Property and Adjoining Properties
Figure 3 Excavation Limit Location Map with Test Pit Sample Locations and Analytical
Results
TABLES
Table 1 Summary of Soil Analytical Results — TPH, VOCs, SVOCs, VPH and EPH
APPENDICES
Appendix A
Copy of Fire Department Permit
Appendix B
UST Certificate of Disposal
Appendix C
Laboratory Report and Chain of Custody for Soil Samples
Appendix D
Photographs of Closure Activities
PM Environmental, Inc.
Page 1

UST Closure Report for Graham Construction Co.
Located at located at 830 Dolly Street NW, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4389-0-0001; March 29, 2019
A. Site Information
1. Site Identification
Date of Report: March 29, 2019
Facility ID#: 00-0-000002532
UST Incident#: N/A
Site Name: Graham Construction Co. Inc.
Site Street Address: 830 Dolly Street NW
Nearest City/Town: Concord, North Carolina
Zip Code: 28027
County: Cabarrus
Latitude: 35.427868 North Longitude:
2. Contact Information
UST Owner:
Address:
Phone:
UST Operator:
Property Owner:
Property Owner Address:
Property Owner Phone:
Property Occupant:
Consultant/Contractor:
Address:
Analytical Laboratory:
Address:
State Certification:
Phone:
3. Release Information
4. Report Certification
-80.609851 West
Mr. Long Huynh
5868 Crimson Oak Court, Harrisburg, NC 28075
704-661-7078
N/A
Mr. Long Huynh
5868 Crimson Oak Court, Harrisburg, NC 28075
704-661-7078
Charlotte Nail Supply (formerly Graham Construction Co.)
PM Environmental, Inc.
333 Troy Circle, Suite M, Knoxville, TN 37923
Waypoint Analytical
2790 Whitten Road, Memphis, TN 38133
#TN02027
901-213-2400
N/A
I, John. W. Hargraves, a Licensed Geologist for PM Environmental, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
G'1 `oSEAL
%4 2242
John W. Hargraves P.G."'•.�Fy°t`��'��'a�`
Regional Manager/Senior Geo0-fJV
PM Environmental, Inc.
Page 2

UST Closure Report for Graham Construction Co.
Located at located at 830 Dolly Street NW, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4389-0-0001; March 29, 2019
B. Site History and Characterization
The subject property consists of one parcel totaling approximately 1.41 acres located at 830
Dolly Street NW, Concord, Cabarrus County, North Carolina (Parcel ID No. 101-112-0046.00).
The subject property is developed with two structures: a single -story commercial building and a
warehouse building. The subject property is currently owned and operated by Charlotte Nail
Supply but was previously occupied by Graham Construction Co, a general contractor. The
property location is illustrated on Figure 1. The subject property layout and adjoining properties
are illustrated on Figure 2.
Underground storage tank (UST) system details:
Was
UST
Capacity
Release
ID#
Product
(gallons)
Date Installed
Date Removed
Assoc. with
UST
System
1
Gasoline
2,000
November 15, 1972
December 31, 1990
No
1A
Gasoline
2,000
January 1, 1991
February 8, 2019
No
As listed above, the subject property contained one 2,000-gallon capacity, single -wall, steel,
gasoline UST. The tank basin and dispenser were located at the southwest corner of the
warehouse building. The dispenser was located directly above the tank and was housed in a
shed enclosure attached to the warehouse. Based on registration records, it appears that the
UST was a replacement for a previous UST installed at the same location. No additional
information is available. The location of the tank is illustrated on Figure 2.
C. Closure Procedures
At the time of closure, the UST had not been used in several years and contained no
measurable amount of gasoline and/or water.
Prior to the commencement of closure activities, North Carolina One -Call Center, a utility
locating service, was contacted to locate utilities on or adjacent to the site and the utilities were
marked by the respective utility companies where they entered or were located adjacent to the
site. Additionally, a permit was obtained from the Concord Department of Fire and Life Safety.
A copy is of the permit is attached in Appendix A.
On February 8, 2019, Elite Environmental Services, Inc. (Elite) conducted the permanent
closure activities of gasoline UST system at the subject property. PM completed the oversight
and sampling activities during the closure activities. The closure activities consisted of
removing the shed housing the dispenser, removing the overburden soil to uncover the tank,
excavating and examining the tank, obtaining confirmation soil samples, and backfilling the
basin with excavated overburden soil and stone.
The top of the tank was encountered approximately one foot below the ground surface. The
UST had the following dimensions:
PM Environmental, Inc.
Page 3

UST Closure Report for Graham Construction Co.
Located at located at 830 Dolly Street NW, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4389-0-0001; March 29, 2019
• Diameter: 5 feet
• Length: 12 feet
• Capacity: 2,000 gallons
• Construction: Steel
The steel tank was removed from the basin, inspected, and no holes or breaches were visibly
identified. The tank was loaded on a flatbed trailer and transported to Foss Recycling located at
4604 York Highway, Gastonia, North Carolina for recycling. A copy of the tank certificate of
disposal is included in Appendix B.
During the sampling activities, soil screening was conducted using a photo ionization detector
(PID). Overburden soil which did not exhibit hydrocarbon odors or photoionization detector
(PID) readings were stockpiled onsite and returned to the excavation following the sampling
activities. Five soil samples (TP-1 through TP-5) were collected from the sidewalls and base of
the UST basin. The soil sample locations are illustrated on Figure 3. Groundwater was not
encountered in the tank pit during the excavation activities.
Soil samples were obtained from the excavated basin sidewalls and basin floor, examined, and
scanned with a PID. The sample identifications, locations, and PID results were as follows:
• TP-1, south sidewall, 4 ft bgs, 0.0 ppm (PID).
• TP-2, west sidewall, 4 ft. bgs, 0.0 ppm (PID).
• TP-3, north sidewall, 4 ft. bgs, 0.0 ppm (PID).
• TP-4, east sidewall, 4 ft. bgs, 0.0 ppm (PID).
• TP-5, basin bottom, 7 ft. bgs, 0.0 ppm (PID).
Reference: ppm refers to parts -per -million; bgs refers to below ground surface
The confirmation soil samples were placed into laboratory -supplied containers, labeled, and
transported to Waypoint Analytical located in Memphis, Tennessee for analysis under chain of
custody procedures. Each of the sidewall confirmation soil samples (TP-1 through TP-4) were
submitted for laboratory analysis of volatile organic compounds (VOCs), semi -volatile organic
compounds (SVOCs), and Massachusetts Department of Environmental Protection Volatile
Petroleum Hydrocarbons and Extractable Petroleum Hydrocarbons (MADEP VPH/EPH).
Additionally, the bottom confirmation sample (TP-5) was analyzed for Total Petroleum
Hydrocarbon (TPH) — Gasoline Range Organics (GRO) and Diesel Range Organics (DRO).
Analytical Results:
The soil analytical results were compared with the North Carolina Department of Environment
and Natural Resources (NCDENR) — Division of Waste Management (DWM), UST Section
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases.
Review of the soil analytical results indicated no target analytes detected above the laboratory
Method Reporting Limit (MRL) and/or applicable criteria.
The analytical results are summarized in Table 1 along with the criteria used by the NCDEQ,
Division of Waste Management, UST Section, and illustrated on Figure 3. The laboratory
analytical report and chain of custody are provided in Appendix C.
PM Environmental, Inc.
Page 4

UST Closure Report for Graham Construction Co.
Located at located at 830 Dolly Street NW, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4389-0-0001; March 29, 2019
Photographic documentation is provided in Appendix D.
D. Conclusions and Recommendations
Based on the analytical results of confirmation samples, there is no evidence of a release and
PM recommends the site granted no further action (NFA) in accordance with the NCDEQ UST
Section guidelines.
If you have any questions related to this document, please contact us at 800-313-2966.
Sincerely,
PM ENVIRONMENTAL, INC.
Maryse Speckner
Sr. Environmental Consultant
V
�ve
J n VII. Hargras, P.G.
Regional Manager/Senior Geologist
PM Environmental, Inc.
Page 5

Figures
Environmental
PM Ca & Engineering
ENVIRONMENTAL Services

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CA BA R R U S COUNTY NORTH CAROUN" COUNTY LOCATIONS
SCALE 1:24,000
1 MILE 1/2 MILE 0 1 MILE
FIGURE 1
PROPERTY VICINITY MAP
USGS, 7.5 MINUTE SERIES
CONCORD, NC QUADRANGLE, 1969. PHOTO REVISED 1987.
PROJ: THIS IS NOT A LEGAL DRN BY: DAT RC E: 3/6/2019
Environmental COMMERCIAL PROPERTY SURVEY
SC
83O DOLLY STREET NW VERIFY SCALE CHKD BY: SCALE: ,
&Engineering 0 2,000. MS 1' = 2-000'
CONCORD, NC IF NOT r' ON THIS
ENVIRONMENTAL Services SHEET BUST FILE NAME:
SCALES ACCORDINGLY. 15-4389-0-001 FOOR00

Tables
Environmental
PM & Engineering
ENVIRONMENTAL Services

TABLE 1
SUMMARY OF SOIL ANALYTICAL RESULTS
ALIPHATICS/AROMATICS, VOCS, SVOCS, TPH-GRO, and TPH-DRO
830 DOLLY STREET NW, CONCORD, NORTH CAROLINA
PM PROJECT # 15-4389-0-0001
ALIPHATICS / AROMATICS,
C.0
N
a)
VOLATILE ORGANIC COMPOUNDS (VOCs),
00
SEMI VOLATILE ORGANIC COMPOUNDS (SVOCs),
U
°'
rn
°'
°'
a)a)
Y
U
U
c
c
N
TOTAL PETROLEUM HYDROCATBONS - GASOLINE RANGE ORGANICS (TPH-GRO), AND
N
°
Y
w w
>
O
N
°'
a
X
�?
TOTAL PETROELUM HYDROCARBONS - DIESEL RANGE ORGANICS (TPH-DRO)
m
Q
w
�
(nn
m
o
0
0_
Q
Q
E
O
w
(mg/kg)
¢
a
Q
o
Q
Chemical Abstract Service Number
(CAS#)
NA
NA
NA
NA
67-64-1
78-93-3
Various
Various
71-43-2
108-88-3
100-41-4
1330-20-7
NA
NA
Sample ID
Sample Date
Sample Depth (bgs)
MADEP VPH and EPH
VOCs
SVOCs
VOCs
TPH
TPH
TP-1
2/8/2019
4
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
TP-2
2/8/2019
4
BRL
BRL
2.86 J
BRL
0.106
BRL
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
TP-3
2/8/2019
4
BRL
BRL
BRL
BRL
0.0114
BRL
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
TP-4
2/8/2019
4
BRL
BRL
BRL
BRL
0.0802
0.0069 J
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
TP-5
2/8/2019
7
BRL
BDL
BRL
BRL
0.0143 J
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
1.36 J
North Carolina Department of Environmental Quality, Division of Waste Management, UST Section (NCDEQ UST) Soil Criteria
TPH
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
50
100
Soil to Groundwater MSCC
68
540
IMMOBILE
31
24
16
Various
Various
0.0056
4.3
4.9
4.6
NA
NA
Residential MSCC
939
1500
31000
469
14000
9385
Various
Various
18
1200
1560
3129
NA
NA
Industrial/Commercial MSCC
24528
40000
810000
12264
360000
245280
Various
Various
164
32000
40000
81760
NA
NA
Applicable Criterion/RBSL Exceeded
BOLD Value Exceeds Applicable Criterion/RBSL
bgs Below Ground Surface (feet)
BRL Below the Laboratory Reporting Limit
J Estimated Value
mg/kg milligrams per kilograms
NA Not Applicable
TPH Total Petroleum Hydrocarbons
MADEP Massechusetts Department of Environmental Protection

Appendix A
Environmental
OPM & Engineering
ENVIRONMENTAL Services

CONCORD DEPARTMENT OF FIRE AND LIFE SAFETY
PERMIT
PO Box 308, Concord, NC 28026-0308
704-920-5517; Fax [phone]
Permit No. 02082019TM001 Valid Dates of Permit: 02/08/2019 03/08/2019
From To
PERMIT INFORMATION
Location: Name: Graham Const. Co - PM Environmental
Address:830 Dolly Ave Nw
Concord, Nc 28027
Phone: Offc 704-786-4181
Issued To: Elite Environmental Services, Inc
Address:322 Clarendon Estates Dr, Clover, SC 29710
Permit Fee:$250.00 Date Paid:02/07/2019
Check No.: 2013 Receipt No.:
Steve Risch
On -Site Contact Name:
PERMIT TYPE:
Permit Type: 105.7.6.2 Flam. & Comb. Liquids (AST,UST) Removal
PERMIT GUIDELINES: IIIIIIIIIIN
1. This permit is issued only for the location or establishement listed, and must be
posted on the premises or in the possession of the permitee.
2. The permit is used for the condition(s) listed.
3. The permits limitations and conditions shall be adhered to at all times.
4. The permit is valid only for the person or business to whom it was issued.
5. Failure to obtain permit before use/installation will result in the fee for the
permit being doubled.
6. Permit fees include one inspection/test, additonal inspections/test will result in
additional fees.
IL PERMIT SPECIFIC PROVISIONS:
Fire Inspections will consist of the following:
1. On -site inspections by CFD-FMO inspectors to witness that the tanks are removed.
2. Witness that soil or water samples are taken at the time of tank removal if
applicable.
3. Document method if inerting or purging of tank(s), if applicable.
4. Approve back filling of excavation if no release is detected.
5. If release is detected, soils must be stored on site and adjacent areas
protected, or soils are to be removed to a proper site for disposal.
6. Tanks are to be marked - "unfit for human consumption."
Notes: SPECIFIC COMMENTS TO THIS PERMIT (If blank, no additional comments):
FAILURE TO FOLLOW THESE GUIDELINES OR MAKING FALSE STATEMENTS OR
MISREPRESENTATIONS TO A MATERIAL FACT IN THE APPLICATION FOR
PERMIT OR PLANS SUBMITTED OR A CONDITION OF THE PERMIT SHALL
RESULT IN IMMEDIATE PERMIT REVOCATION.
02/08/2019 12:25 Page 1 of 2

Permit No. O2O82O19TMOOl
Fire Official Issuing Permit: John T MCGaha Date of Issue: 02/08/2019
02/08/2019 12:25 Page 2 of 2

Appendix B
Environmental
OPM & Engineering
ENVIRONMENTAL Services

■
E L me
Environmental. Services
www e Li,�e.-e vuri crab v�Gaiw i @e t v}�-e w�i.troyvG vw O f f i c , 803. 81 S -528 8 • Mo�w(.e�
704. 914.8 56 8
CERTIFICATE OF DISPOSAL
(UST)
Underground Storage Tank
Be it known the (1) tank located at:
830 Dolly Street
Concord, NC 28025
Of which contained gasoline with the following capacities of Two
thousand (2,000) gallons, the tank contained no residual material and
was removed per API
standards on February 08, 201P
B S�ef a • ' 'u(, ( l,s
Y
Position: vt'o(` A �� I.
Contractor:
Elite Environmental Services
322 Clarendon Estates Drive
Clover, SC 29710
Disposal Facility:
Foss Recycling^
4604 York Hwy
Gastonia, NC 28052
Elite Environmental Services, Inc. Project No. 10161
Original to Customer, copy to file
ff W e • 322 Gl a cre +n ci o w EPhI4-ems D ri vv • G{.ay-,mr, S G 2 g 7 20

Appendix C
Environmental
OPM & Engineering
ENVIRONMENTAL Services

Waypointo
ANALYTICAL
2/19/2019
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN, 37919
Ref: Analytical Testing
Lab Report Number: 19-042-0252
Client Project Description: 830 Dolly St,
Concord, NC
Proj #: 15-4389-0-0001
Project Number: 15-4389-0-0001
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Ms. Maryse Speckner:
Waypoint Analytical, LLC. received sample(s) on 2/9/2019 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
�& 4 t
f
Andrea R Brownfield
Project manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Alabama #40750 Louisiana #04015 VA NELAP #460181 Texas #T104704180-11-6 Arkansas #88-0650
Mississippi California #2904 NC #415 Oklahoma #9311 Virginia #00106
Kentucky #90047 Tennessee #TN02027 EPA #TN00012 Kentucky UST #41
Page 1 of 76

(2)
2790 Whitten Road, Memphis, TN 38133
Waypoint, Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 19-042-0252
Client Project Description: 830 Dolly St,
Concord, NC
Proj #: 15-4389-0-0001
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
93056
TP-1
Solids
02/08/2019
13:00
02/09/2019
93057
TP-2
Solids
02/08/2019
13:15
02/09/2019
93058
TP-3
Solids
02/08/2019
13:30
02/09/2019
93059
TP-4
Solids
02/08/2019
13:45
02/09/2019
93060
TP-5
Solids
02/08/2019
14:00
02/09/2019
93164
TP-1
Solids
02/08/2019
13:00
02/09/2019
MAVPH
93165
TP-2
Solids
02/08/2019
13:15
02/09/2019
MAVPH
93166
TP-3
Solids
02/08/2019
13:30
02/09/2019
MAVPH
93167
TP-4
Solids
02/08/2019
13:45
02/09/2019
MAVPH
93168
TP-5
Solids
02/08/2019
14:00
02/09/2019
MAVPH
Prism Laboratories, Inc., Charlotte, NC
Page 2 of 76

(2)
Waypoeint. 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 °Fax [phone].2440
ANALYTICAL www.waypointanalytical.com
Summary of Detected Analytes
Project:
830 Dolly St,
Report Number:
19-042-0252
Client Sample ID
Lab Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
TP-1
L 93056
SW-DRYWT
% Moisture
17.7
%
02/15/2019 16:43
TP-2
L 93057
8260D
Acetone
0.106
mg/Kg - dry
0.0133
02/13/2019 16:10
MAEPH
Aliphatic C19-06
2.86
mg/Kg - dry
2.53
02/16/2019 08:19
J
SW-DRYWT
% Moisture
24.4
%
02/15/2019 16:43
TP-3
L 93058
8260D
Acetone
0.0114
mg/Kg - dry
0.0103
02/13/2019 16:51
J
SW-DRYWT
% Moisture
13.3
%
02/15/2019 17:05
TP-4
L 93059
8260D
Acetone
0.0802
mg/Kg - dry
0.0103
02/13/2019 17:32
8260D
Methyl Ethyl Ketone (MEK)
0.0069
mg/Kg - dry
0.0060
02/13/2019 17:32
J
SW-DRYWT
% Moisture
13.3
%
02/15/2019 17:05
TP-5
L 93060
8015B DRO
Diesel Range Organics (C10-C28) 1.36
mg/Kg - dry
1.27
02/13/2019 19:09
J
8260D
Acetone
0.0143
mg/Kg - dry
0.0104
02/13/2019 18:13
J
SW-DRYWT
% Moisture
14.1
%
02/15/2019 17:05
Page 3 of 76

Waypointo
ANALYTICAL
Client: PM ENVIRONMENTAL, INC.
Project: 830 Dolly St,
Lab Report Number: 19-042-0252
Date: 2/19/2019
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Volatile Organic Compounds - GC/MS Method 8260D
Sample 93056 (TP-1)
Analyte: 4-Bromofluorobenzene
QC Batch No: 1-422037/1-422031
Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high
recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Semivolatile Organic Compounds - GC/MS Method 8270E
Analyte: 2,4-Dinitrophenol
QC Batch No: 1-422041 /L422038
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
186 pg/Kg which calculates to a recovery of 11.2% which is within the acceptable recovery range.
Analyte: 3,3'-Dimethylbenzidine
QC Batch No: 1-422041/1-422038
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Benzidine
QC Batch No: 1-422041 /L422038
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Analyte: Benzoic Acid
QC Batch No: 1-422041/1-422038
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Data for this
analyte is flagged "M" to indicate that results should be considered minimum concentration due to the potential for
a low bias.
Page 4 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.48 g
1
2/13/2019 15:29:32
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
67-64-1
Acetone
ND
0.0109
0.0486
mg/Kg - dry
75-05-8
Acetonitrile
ND
0.0511
0.243
mg/Kg - dry
107-02-8
Acrolein
ND
0.0030
0.0486
mg/Kg - dry
107-13-1
Acrylonitrile
ND
0.0050
0.0486
mg/Kg - dry
71-43-2
Benzene
ND
0.0020
0.0024
mg/Kg - dry
108-86-1
Bromobenzene
ND
0.0011
0.0024
mg/Kg - dry
74-97-5
Bromochloromethane
ND
0.0019
0.0024
mg/Kg - dry
75-27-4
Bromodichloromethane
ND
0.0011
0.0024
mg/Kg - dry
75-25-2
Bromoform
ND
0.0022
0.0024
mg/Kg - dry
74-83-9
Bromomethane
ND
0.0007
0.0024
mg/Kg - dry
78-93-3
Methyl Ethyl Ketone (MEK)
ND
0.0063
0.0486
mg/Kg - dry
104-51-8
n-Butylbenzene
ND
0.0022
0.0024
mg/Kg - dry
135-98-8
sec -Butyl benzene
ND
0.0016
0.0024
mg/Kg - dry
98-06-6
tert-Butyl benzene
ND
0.0014
0.0024
mg/Kg - dry
75-15-0
Carbon Disulfide
ND
0.0010
0.0024
mg/Kg - dry
56-23-5
Carbon Tetrachloride
ND
0.0016
0.0024
mg/Kg - dry
108-90-7
Chlorobenzene
ND
0.0014
0.0024
mg/Kg - dry
124-48-1
Chlorodibromomethane
ND
0.0017
0.0024
mg/Kg - dry
75-00-3
Chloroethane
ND
0.0021
0.0024
mg/Kg - dry
67-66-3
Chloroform
ND
0.0022
0.0024
mg/Kg - dry
74-87-3
Chloromethane
ND
0.0015
0.0024
mg/Kg - dry
95-49-8
2-Chlorotoluene
ND
0.0022
0.0024
mg/Kg - dry
106-43-4
4-Chlorotoluene
ND
0.0015
0.0024
mg/Kg - dry
96-12-8
1,2-Dibromo-3-Chloropropane
ND
0.0077
0.0121
mg/Kg - dry
106-93-4
1,2-Dibromoethane
ND
0.0016
0.0024
mg/Kg - dry
74-95-3
Dibromomethane
ND
0.0018
0.0024
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.0023
0.0024
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 5 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.48 g
1
2/13/2019 15:29:32
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
541-73-1
1,3-Dichlorobenzene
ND
0.0017
0.0024
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.0022
0.0024
mg/Kg - dry
75-71-8
Dichlorodifluoromethane
ND
0.0022
0.0024
mg/Kg - dry
75-34-3
1,1-Dichloroethane
ND
0.0012
0.0024
mg/Kg - dry
107-06-2
1,2-Dichloroethane
ND
0.0021
0.0024
mg/Kg - dry
75-35-4
1,1-Dichloroethene
ND
0.0011
0.0024
mg/Kg - dry
156-59-2
cis-1,2-Dichloroethene
ND
0.0009
0.0024
mg/Kg - dry
156-60-5
trans-1,2-Dichloroethene
ND
0.0013
0.0024
mg/Kg - dry
540-59-0
1,2-Dichloroethene (Total)
ND
0.0009
0.0024
mg/Kg - dry
78-87-5
1,2-Dichloropropane
ND
0.0011
0.0024
mg/Kg - dry
142-28-9
1,3-Dichloropropane
ND
0.0019
0.0024
mg/Kg - dry
594-20-7
2,2-Dichloropropane
ND
0.0010
0.0024
mg/Kg - dry
563-58-6
1,1-Dichloropropene
ND
0.0007
0.0024
mg/Kg - dry
10061-01-5
cis-1,3-Dichloropropene
ND
0.0010
0.0024
mg/Kg - dry
10061-02-6
trans-1,3-Dichloropropene
ND
0.0011
0.0024
mg/Kg - dry
141-78-6
Ethyl Acetate
ND
0.0051
0.0486
mg/Kg - dry
100-41-4
Ethylbenzene
ND
0.0018
0.0024
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.0017
0.0024
mg/Kg - dry
591-78-6
2-Hexanone
ND
0.0028
0.0121
mg/Kg - dry
74-88-4
Iodomethane
ND
0.0065
0.0121
mg/Kg - dry
98-82-8
Isopropyl benzene
ND
0.0018
0.0024
mg/Kg - dry
99-87-6
4-Isopropyl toluene
ND
0.0019
0.0024
mg/Kg - dry
1634-04-4
Methyl tert-butyl ether (MTBE)
ND
0.0006
0.0024
mg/Kg - dry
108-10-1
4-Methyl -2-Pentanone
ND
0.0041
0.0121
mg/Kg - dry
75-09-2
Methylene Chloride
ND
0.0116
0.0121
mg/Kg - dry
91-20-3
Naphthalene
ND
0.0045
0.0121
mg/Kg - dry
109-60-4
n-Propyl acetate
ND
0.0051
0.0121
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 6 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.48 g
1
2/13/2019 15:29:32
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
103-65-1
n-Propylbenzene
ND
0.0018
0.0024
mg/Kg - dry
100-42-5
Styrene
ND
0.0022
0.0024
mg/Kg - dry
630-20-6
1,1,1,2-Tetrachloroethane
ND
0.0023
0.0024
mg/Kg - dry
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.0020
0.0024
mg/Kg - dry
127-18-4
Tetrachloroethene
ND
0.0020
0.0024
mg/Kg - dry
108-88-3
Toluene
ND
0.0035
0.0048
mg/Kg - dry
87-61-6
1,2,3-Trichlorobenzene
ND
0.0019
0.0024
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.0021
0.0024
mg/Kg - dry
71-55-6
1,1,1-Trichloroethane
ND
0.0011
0.0024
mg/Kg - dry
79-00-5
1,1,2-Trichloroethane
ND
0.0021
0.0024
mg/Kg - dry
79-01-6
Trichloroethene
ND
0.0014
0.0024
mg/Kg - dry
75-69-4
Trichlorofluoromethane
ND
0.0011
0.0024
mg/Kg - dry
96-18-4
1,2,3-Trichloropropane
ND
0.0020
0.0024
mg/Kg - dry
95-63-6
1,2,4-Trimethylbenzene
ND
0.0014
0.0024
mg/Kg - dry
108-67-8
1,3,5-Trimethylbenzene
ND
0.0023
0.0024
mg/Kg - dry
108-05-4
Vinyl Acetate
ND
0.0104
0.0486
mg/Kg - dry
75-01-4
Vinyl Chloride
ND
0.0013
0.0024
mg/Kg - dry
95-47-6
o-Xylene
ND
0.0016
0.0024
mg/Kg - dry
179601-23-1
m,p-Xylene
ND
0.0033
0.0048
mg/Kg - dry
1330-20-7
Xylene (Total)
ND
0.0016
0.0024
mg/Kg - dry
CAS#
Surrogate
% Recovery
Rec. Limits
460-00-4
4-Bromofluorobenzene
140
60-140%
17060-07-0
1,2-Dichloroethane-d4
127
60-140%
2037-26-5
Toluene-d8
136
60-140%
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 7 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 18:59:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
83-32-9
Acenaphthene
ND
0.013
0.081
mg/Kg - dry
208-96-8
Acenaphthylene
ND
0.014
0.081
mg/Kg - dry
98-86-2
Acetophenone
ND
0.018
0.206
mg/Kg - dry
62-53-3
Aniline
ND
0.005
0.206
mg/Kg - dry
120-12-7
Anthracene
ND
0.015
0.081
mg/Kg - dry
92-87-5
Benzidine
ND
M
0.614
0.814
mg/Kg - dry
56-55-3
Benzo(a)anthracene
ND
0.010
0.081
mg/Kg - dry
50-32-8
Benzo(a)pyrene
ND
0.012
0.081
mg/Kg - dry
205-99-2
Benzo(b)fluoranthene
ND
0.010
0.081
mg/Kg - dry
191-24-2
Benzo(g,h,i)perylene
ND
0.016
0.081
mg/Kg - dry
207-08-9
Benzo(k)fluoranthene
ND
0.013
0.081
mg/Kg - dry
65-85-0
Benzoic Acid
ND
M
0.020
0.400
mg/Kg - dry
100-51-6
Benzyl alcohol
ND
0.026
0.400
mg/Kg - dry
111-91-1
Bis(2-Chloroethoxy)methane
ND
0.013
0.206
mg/Kg - dry
111-44-4
Bis(2-Chloroethyl)ether
ND
0.007
0.206
mg/Kg - dry
108-60-1
Bis(2-Chloroisopropyl)ether
ND
0.026
0.206
mg/Kg - dry
117-81-7
Bis(2-ethylhexyl)phthalate
ND
0.018
0.400
mg/Kg - dry
101-55-3
4-Bromophenyl phenyl ether
ND
0.018
0.206
mg/Kg - dry
85-68-7
Butyl benzyl phthalate
ND
0.020
0.206
mg/Kg - dry
86-74-8
Carbazole
ND
0.012
0.206
mg/Kg - dry
59-50-7
4-Chloro-3-methylphenol
ND
0.019
0.206
mg/Kg - dry
106-47-8
4-Chloroaniline
ND
0.015
0.206
mg/Kg - dry
91-58-7
2-Chloronaphthalene
ND
0.011
0.206
mg/Kg - dry
95-57-8
2-Chlorophenol
ND
0.016
0.206
mg/Kg - dry
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.014
0.206
mg/Kg - dry
218-01-9
Chrysene
ND
0.013
0.081
mg/Kg - dry
53-70-3
Dibenz(a,h)anthracene
ND
0.013
0.081
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 8 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 18:59:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
132-64-9
Dibenzofuran
ND
0.017
0.206
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.010
0.206
mg/Kg - dry
541-73-1
1,3-Dichlorobenzene
ND
0.010
0.206
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.011
0.206
mg/Kg - dry
91-94-1
3,3'-Dichlorobenzidine
ND
0.133
0.400
mg/Kg - dry
120-83-2
2,4-Dichlorophenol
ND
0.018
0.206
mg/Kg - dry
87-65-0
2,6-Dichlorophenol
ND
0.016
0.206
mg/Kg - dry
84-66-2
Diethyl phthalate
ND
0.013
0.206
mg/Kg - dry
131-11-3
Dimethyl phthalate
ND
0.017
0.206
mg/Kg - dry
119-93-7
3,3' Dimethylbenzidine
ND M
0.043
0.400
mg/Kg - dry
105-67-9
2,4-Dimethyl phenol
ND
0.026
0.206
mg/Kg - dry
84-74-2
Di-n-butyl phthalate
ND
0.017
0.206
mg/Kg - dry
534-52-1
4,6-Dinitro-2-methyl phenol
ND
0.010
0.400
mg/Kg - dry
51-28-5
2,4-Dinitrophenol
ND
0.011
0.400
mg/Kg - dry
121-14-2
2,4-Dinitrotoluene
ND
0.013
0.206
mg/Kg - dry
606-20-2
2,6-Dinitrotoluene
ND
0.014
0.206
mg/Kg - dry
117-84-0
Di-n-Octyl Phthalate
ND
0.026
0.206
mg/Kg - dry
206-44-0
Fluoranthene
ND
0.012
0.081
mg/Kg - dry
86-73-7
Fluorene
ND
0.019
0.081
mg/Kg - dry
118-74-1
Hexachlorobenzene
ND
0.013
0.206
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.011
0.206
mg/Kg - dry
77-47-4
Hexachlorocyclopentadiene
ND
0.017
0.206
mg/Kg - dry
67-72-1
Hexachloroethane
ND
0.012
0.206
mg/Kg - dry
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.021
0.081
mg/Kg - dry
78-59-1
Isophorone
ND
0.013
0.206
mg/Kg - dry
91-57-6
2-Methyl naphthalene
ND
0.011
0.081
mg/Kg - dry
95-48-7
2-Methylphenol
ND
0.018
0.206
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 9 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 18:59:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
108-39-4
3&4 Methylphenol
ND
0.017
0.206
mg/Kg - dry
91-20-3
Naphthalene
ND
0.013
0.081
mg/Kg - dry
88-74-4
2-Nitroaniline
ND
0.020
0.206
mg/Kg - dry
99-09-2
3-Nitroaniline
ND
0.011
0.400
mg/Kg - dry
100-01-6
4-Nitroaniline
ND
0.014
0.206
mg/Kg - dry
98-95-3
Nitrobenzene
ND
0.007
0.206
mg/Kg - dry
88-75-5
2-Nitrophenol
ND
0.020
0.206
mg/Kg - dry
100-02-7
4-Nitrophenol
ND
0.016
0.206
mg/Kg - dry
62-75-9
N-Nitrosodimethylamine
ND
0.006
0.206
mg/Kg - dry
86-30-6
N-Nitrosodiphenylamine
ND
0.015
0.400
mg/Kg - dry
55-18-5
N-Nitrosodiethylamine
ND
0.024
0.206
mg/Kg - dry
924-16-3
N-Nitroso-di-n-butylamine
ND
0.019
0.206
mg/Kg - dry
621-64-7
N-Nitroso-di-n-propylamine
ND
0.012
0.206
mg/Kg - dry
87-86-5
Pentachlorophenol
ND
0.022
0.400
mg/Kg - dry
85-01-8
Phenanthrene
ND
0.016
0.081
mg/Kg - dry
108-95-2
Phenol
ND
0.024
0.206
mg/Kg - dry
129-00-0
Pyrene
ND
0.015
0.081
mg/Kg - dry
110-86-1
Pyridine
ND
0.018
0.400
mg/Kg - dry
95-94-3
1,2,4,5-Tetrachlorobenzene
ND
0.010
0.206
mg/Kg - dry
58-90-2
2,3,4,6-Tetrachlorophenol
ND
0.018
0.206
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.012
0.206
mg/Kg - dry
95-95-4
2,4,5-Trichlorophenol
ND
0.024
0.206
mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 10 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
C\A/_S277f1F
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 18:59:00
CGC
L422041
CAS#
Parameter
88-06-2
2,4,6-Trichlorophenol
CAS#
Surrogate
321-60-8
2-Fluorobiphenyl
367-12-4
2-Fluorophenol
4165-60-0
Nitrobenzene-d5
13127-88-3
Phenol-d6
1718-51-0
4-Terphenyl-d14
118-79-6
2,4,6-Tribromophenol
Result MDL MQL Units
ND 0.017 0.206 mg/Kg - dry
Recovery
Rec. Limits
25.0
20-79%
26.8
10-85%
26.0
22-72%
29.8
10-96%
31.8
22-104%
33.3
10-112%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.0 g
1
2/16/2019 02:45:54
MMK
L421893
CAS#
Parameter
C11-C22
Aromatic C11-C22
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
MA�Du
Result MDL MQL Units
ND 2.48 10.3 mg/Kg - dry
Recovery Rec. Limits
52.9 40-140%
51.3 40-140%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.0 g
1
2/16/2019 07:46:17
MMK
L421893
CAS# Parameter Result MDL MQL Units
C19-C36 Aliphatic C19-C36 ND 2.32 4.86 mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 11 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-1 Date Collected
02/08/2019 13:00
WPA Lab No
93056
Date Received
02/09/2019
Matrix
Solids
nn A gnu
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.0 g
1
2/16/2019 07:46:17
MMK
L421893
CAS#
Parameter
C9-C18
Aliphatic C9-C18
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
CIA1_r'%Dv1A1T
Result MDL MQL Units
ND 1.86 3.65 mg/Kg - dry
Recovery Rec. Limits
52.9 40-140%
51.3 40-140%
Prep Date
Prep Batch
Prep Method
Dilution
Analysis Date
By
Analytical Batch
NA
NA
NA
1
2/15/201916:43:00
RXC
L421695
CAS# Parameter Result MQL Units
Moisture % Moisture 17.7 %
Qualifiers/ Outside QC limit
Definitions M Minimum value
MQL Method Quantitation Limit
J Estimated value
MDL Method Detection Limit
ND Not Detected
Page 12 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
4.45 g
1
2/13/2019 16:10:32
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
67-64-1
Acetone
0.106
0.0133
0.0593
mg/Kg - dry
75-05-8
Acetonitrile
ND
0.0625
0.298
mg/Kg - dry
107-02-8
Acrolein
ND
0.0036
0.0593
mg/Kg - dry
107-13-1
Acrylonitrile
ND
0.0061
0.0593
mg/Kg - dry
71-43-2
Benzene
ND
0.0025
0.0029
mg/Kg - dry
108-86-1
Bromobenzene
ND
0.0014
0.0029
mg/Kg - dry
74-97-5
Bromochloromethane
ND
0.0023
0.0029
mg/Kg - dry
75-27-4
Bromodichloromethane
ND
0.0013
0.0029
mg/Kg - dry
75-25-2
Bromoform
ND
0.0027
0.0029
mg/Kg - dry
74-83-9
Bromomethane
ND
0.0009
0.0029
mg/Kg - dry
78-93-3
Methyl Ethyl Ketone (MEK)
ND
0.0077
0.0593
mg/Kg - dry
104-51-8
n-Butylbenzene
ND
0.0027
0.0029
mg/Kg - dry
135-98-8
sec -Butyl benzene
ND
0.0019
0.0029
mg/Kg - dry
98-06-6
tert-Butyl benzene
ND
0.0017
0.0029
mg/Kg - dry
75-15-0
Carbon Disulfide
ND
0.0012
0.0029
mg/Kg - dry
56-23-5
Carbon Tetrachloride
ND
0.0019
0.0029
mg/Kg - dry
108-90-7
Chlorobenzene
ND
0.0017
0.0029
mg/Kg - dry
124-48-1
Chlorodibromomethane
ND
0.0020
0.0029
mg/Kg - dry
75-00-3
Chloroethane
ND
0.0025
0.0029
mg/Kg - dry
67-66-3
Chloroform
ND
0.0027
0.0029
mg/Kg - dry
74-87-3
Chloromethane
ND
0.0019
0.0029
mg/Kg - dry
95-49-8
2-Chlorotoluene
ND
0.0027
0.0029
mg/Kg - dry
106-43-4
4-Chlorotoluene
ND
0.0019
0.0029
mg/Kg - dry
96-12-8
1,2-Dibromo-3-Chloropropane
ND
0.0094
0.0148
mg/Kg - dry
106-93-4
1,2-Dibromoethane
ND
0.0019
0.0029
mg/Kg - dry
74-95-3
Dibromomethane
ND
0.0022
0.0029
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.0028
0.0029
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 13 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
4.45 g
1
2/13/2019 16:10:32
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
541-73-1
1,3-Dichlorobenzene
ND
0.0021
0.0029
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.0027
0.0029
mg/Kg - dry
75-71-8
Dichlorodifluoromethane
ND
0.0028
0.0029
mg/Kg - dry
75-34-3
1,1-Dichloroethane
ND
0.0015
0.0029
mg/Kg - dry
107-06-2
1,2-Dichloroethane
ND
0.0026
0.0029
mg/Kg - dry
75-35-4
1,1-Dichloroethene
ND
0.0013
0.0029
mg/Kg - dry
156-59-2
cis-1,2-Dichloroethene
ND
0.0011
0.0029
mg/Kg - dry
156-60-5
trans-1,2-Dichloroethene
ND
0.0016
0.0029
mg/Kg - dry
540-59-0
1,2-Dichloroethene (Total)
ND
0.0011
0.0029
mg/Kg - dry
78-87-5
1,2-Dichloropropane
ND
0.0014
0.0029
mg/Kg - dry
142-28-9
1,3-Dichloropropane
ND
0.0023
0.0029
mg/Kg - dry
594-20-7
2,2-Dichloropropane
ND
0.0013
0.0029
mg/Kg - dry
563-58-6
1,1-Dichloropropene
ND
0.0009
0.0029
mg/Kg - dry
10061-01-5
cis-1,3-Dichloropropene
ND
0.0012
0.0029
mg/Kg - dry
10061-02-6
trans-1,3-Dichloropropene
ND
0.0013
0.0029
mg/Kg - dry
141-78-6
Ethyl Acetate
ND
0.0063
0.0593
mg/Kg - dry
100-41-4
Ethylbenzene
ND
0.0022
0.0029
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.0021
0.0029
mg/Kg - dry
591-78-6
2-Hexanone
ND
0.0035
0.0148
mg/Kg - dry
74-88-4
Iodomethane
ND
0.0080
0.0148
mg/Kg - dry
98-82-8
Isopropyl benzene
ND
0.0023
0.0029
mg/Kg - dry
99-87-6
4-Isopropyl toluene
ND
0.0023
0.0029
mg/Kg - dry
1634-04-4
Methyl tert-butyl ether (MTBE)
ND
0.0007
0.0029
mg/Kg - dry
108-10-1
4-Methyl -2-Pentanone
ND
0.0050
0.0148
mg/Kg - dry
75-09-2
Methylene Chloride
ND
0.0142
0.0148
mg/Kg - dry
91-20-3
Naphthalene
ND
0.0055
0.0148
mg/Kg - dry
109-60-4
n-Propyl acetate
ND
0.0062
0.0148
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 14 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
4.45 g
1
2/13/2019 16:10:32
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
103-65-1
n-Propylbenzene
ND
0.0022
0.0029
mg/Kg - dry
100-42-5
Styrene
ND
0.0027
0.0029
mg/Kg - dry
630-20-6
1,1,1,2-Tetrachloroethane
ND
0.0029
0.0029
mg/Kg - dry
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.0024
0.0029
mg/Kg - dry
127-18-4
Tetrachloroethene
ND
0.0024
0.0029
mg/Kg - dry
108-88-3
Toluene
ND
0.0042
0.0059
mg/Kg - dry
87-61-6
1,2,3-Trichlorobenzene
ND
0.0023
0.0029
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.0026
0.0029
mg/Kg - dry
71-55-6
1,1,1-Trichloroethane
ND
0.0014
0.0029
mg/Kg - dry
79-00-5
1,1,2-Trichloroethane
ND
0.0026
0.0029
mg/Kg - dry
79-01-6
Trichloroethene
ND
0.0017
0.0029
mg/Kg - dry
75-69-4
Trichlorofluoromethane
ND
0.0014
0.0029
mg/Kg - dry
96-18-4
1,2,3-Trichloropropane
ND
0.0024
0.0029
mg/Kg - dry
95-63-6
1,2,4-Trimethylbenzene
ND
0.0017
0.0029
mg/Kg - dry
108-67-8
1,3,5-Trimethylbenzene
ND
0.0028
0.0029
mg/Kg - dry
108-05-4
Vinyl Acetate
ND
0.0127
0.0593
mg/Kg - dry
75-01-4
Vinyl Chloride
ND
0.0017
0.0029
mg/Kg - dry
95-47-6
o-Xylene
ND
0.0020
0.0029
mg/Kg - dry
179601-23-1
m,p-Xylene
ND
0.0040
0.0059
mg/Kg - dry
1330-20-7
Xylene (Total)
ND
0.0020
0.0029
mg/Kg - dry
CAS#
Surrogate
% Recovery
Rec. Limits
460-00-4
4-Bromofluorobenzene
109
60-140%
17060-07-0
1,2-Dichloroethane-d4
122
60-140%
2037-26-5
Toluene-d8
104
60-140%
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 15 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.3 g
1
2/13/2019 19:18:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
83-32-9
Acenaphthene
ND
0.014
0.088
mg/Kg - dry
208-96-8
Acenaphthylene
ND
0.015
0.088
mg/Kg - dry
98-86-2
Acetophenone
ND
0.019
0.224
mg/Kg - dry
62-53-3
Aniline
ND
0.005
0.224
mg/Kg - dry
120-12-7
Anthracene
ND
0.017
0.088
mg/Kg - dry
92-87-5
Benzidine
ND
M
0.669
0.886
mg/Kg - dry
56-55-3
Benzo(a)anthracene
ND
0.011
0.088
mg/Kg - dry
50-32-8
Benzo(a)pyrene
ND
0.013
0.088
mg/Kg - dry
205-99-2
Benzo(b)fluoranthene
ND
0.011
0.088
mg/Kg - dry
191-24-2
Benzo(g,h,i)perylene
ND
0.017
0.088
mg/Kg - dry
207-08-9
Benzo(k)fluoranthene
ND
0.015
0.088
mg/Kg - dry
65-85-0
Benzoic Acid
ND
M
0.022
0.436
mg/Kg - dry
100-51-6
Benzyl alcohol
ND
0.028
0.436
mg/Kg - dry
111-91-1
Bis(2-Chloroethoxy)methane
ND
0.014
0.224
mg/Kg - dry
111-44-4
Bis(2-Chloroethyl)ether
ND
0.008
0.224
mg/Kg - dry
108-60-1
Bis(2-Chloroisopropyl)ether
ND
0.028
0.224
mg/Kg - dry
117-81-7
Bis(2-ethylhexyl)phthalate
ND
0.020
0.436
mg/Kg - dry
101-55-3
4-Bromophenyl phenyl ether
ND
0.019
0.224
mg/Kg - dry
85-68-7
Butyl benzyl phthalate
ND
0.022
0.224
mg/Kg - dry
86-74-8
Carbazole
ND
0.013
0.224
mg/Kg - dry
59-50-7
4-Chloro-3-methylphenol
ND
0.021
0.224
mg/Kg - dry
106-47-8
4-Chloroaniline
ND
0.016
0.224
mg/Kg - dry
91-58-7
2-Chloronaphthalene
ND
0.012
0.224
mg/Kg - dry
95-57-8
2-Chlorophenol
ND
0.017
0.224
mg/Kg - dry
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.015
0.224
mg/Kg - dry
218-01-9
Chrysene
ND
0.014
0.088
mg/Kg - dry
53-70-3
Dibenz(a,h)anthracene
ND
0.015
0.088
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 16 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.3 g
1
2/13/2019 19:18:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
132-64-9
Dibenzofuran
ND
0.019
0.224
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.011
0.224
mg/Kg - dry
541-73-1
1,3-Dichlorobenzene
ND
0.011
0.224
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.012
0.224
mg/Kg - dry
91-94-1
3,3'-Dichlorobenzidine
ND
0.145
0.436
mg/Kg - dry
120-83-2
2,4-Dichlorophenol
ND
0.020
0.224
mg/Kg - dry
87-65-0
2,6-Dichlorophenol
ND
0.017
0.224
mg/Kg - dry
84-66-2
Diethyl phthalate
ND
0.014
0.224
mg/Kg - dry
131-11-3
Dimethyl phthalate
ND
0.018
0.224
mg/Kg - dry
119-93-7
3,3' Dimethylbenzidine
ND M
0.047
0.436
mg/Kg - dry
105-67-9
2,4-Dimethyl phenol
ND
0.028
0.224
mg/Kg - dry
84-74-2
Di-n-butyl phthalate
ND
0.019
0.224
mg/Kg - dry
534-52-1
4,6-Dinitro-2-methyl phenol
ND
0.011
0.436
mg/Kg - dry
51-28-5
2,4-Dinitrophenol
ND
0.012
0.436
mg/Kg - dry
121-14-2
2,4-Dinitrotoluene
ND
0.014
0.224
mg/Kg - dry
606-20-2
2,6-Dinitrotoluene
ND
0.015
0.224
mg/Kg - dry
117-84-0
Di-n-Octyl Phthalate
ND
0.029
0.224
mg/Kg - dry
206-44-0
Fluoranthene
ND
0.013
0.088
mg/Kg - dry
86-73-7
Fluorene
ND
0.020
0.088
mg/Kg - dry
118-74-1
Hexachlorobenzene
ND
0.014
0.224
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.012
0.224
mg/Kg - dry
77-47-4
Hexachlorocyclopentadiene
ND
0.018
0.224
mg/Kg - dry
67-72-1
Hexachloroethane
ND
0.014
0.224
mg/Kg - dry
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.023
0.088
mg/Kg - dry
78-59-1
Isophorone
ND
0.014
0.224
mg/Kg - dry
91-57-6
2-Methyl naphthalene
ND
0.012
0.088
mg/Kg - dry
95-48-7
2-Methylphenol
ND
0.020
0.224
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 17 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.3 g
1
2/13/2019 19:18:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
108-39-4
3&4 Methylphenol
ND
0.019
0.224
mg/Kg - dry
91-20-3
Naphthalene
ND
0.014
0.088
mg/Kg - dry
88-74-4
2-Nitroaniline
ND
0.022
0.224
mg/Kg - dry
99-09-2
3-Nitroaniline
ND
0.012
0.436
mg/Kg - dry
100-01-6
4-Nitroaniline
ND
0.016
0.224
mg/Kg - dry
98-95-3
Nitrobenzene
ND
0.008
0.224
mg/Kg - dry
88-75-5
2-Nitrophenol
ND
0.022
0.224
mg/Kg - dry
100-02-7
4-Nitrophenol
ND
0.018
0.224
mg/Kg - dry
62-75-9
N-Nitrosodimethylamine
ND
0.007
0.224
mg/Kg - dry
86-30-6
N-Nitrosodiphenylamine
ND
0.016
0.436
mg/Kg - dry
55-18-5
N-Nitrosodiethylamine
ND
0.026
0.224
mg/Kg - dry
924-16-3
N-Nitroso-di-n-butylamine
ND
0.020
0.224
mg/Kg - dry
621-64-7
N-Nitroso-di-n-propylamine
ND
0.013
0.224
mg/Kg - dry
87-86-5
Pentachlorophenol
ND
0.024
0.436
mg/Kg - dry
85-01-8
Phenanthrene
ND
0.018
0.088
mg/Kg - dry
108-95-2
Phenol
ND
0.026
0.224
mg/Kg - dry
129-00-0
Pyrene
ND
0.016
0.088
mg/Kg - dry
110-86-1
Pyridine
ND
0.020
0.436
mg/Kg - dry
95-94-3
1,2,4,5-Tetrachlorobenzene
ND
0.011
0.224
mg/Kg - dry
58-90-2
2,3,4,6-Tetrachlorophenol
ND
0.020
0.224
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.013
0.224
mg/Kg - dry
95-95-4
2,4,5-Trichlorophenol
ND
0.026
0.224
mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 18 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
C\A/_S277f1F
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.3 g
1
2/13/2019 19:18:00
CGC
L422041
CAS#
Parameter
88-06-2
2,4,6-Trichlorophenol
CAS#
Surrogate
321-60-8
2-Fluorobiphenyl
367-12-4
2-Fluorophenol
4165-60-0
Nitrobenzene-d5
13127-88-3
Phenol-d6
1718-51-0
4-Terphenyl-d14
118-79-6
2,4,6-Tribromophenol
Result MDL MQL Units
ND 0.019 0.224 mg/Kg - dry
Recovery
Rec. Limits
31.5
20-79%
28.8
10-85%
28.6
22-72%
33.9
10-96%
38.8
22-104%
46.1
10-112%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.7 g
1
2/16/2019 03:19:16
MMK
L421893
CAS#
Parameter
C11-C22
Aromatic C11-C22
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
MA�Du
Result MDL MQL Units
ND 2.70 11.2 mg/Kg - dry
Recovery Rec. Limits
54.1 40-140%
55.2 40-140%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.7 g
1
2/16/2019 08:19:44
MMK
L421893
CAS# Parameter
C19-C36 Aliphatic C19-C36
Qualifiers/ Outside QC limit
Definitions M Minimum value
MQL Method Quantitation Limit
Result
MDL
MQL
Units
2.86 J
2.53
5.29
mg/Kg - dry
J Estimated value
MDL Method Detection Limit
ND Not Detected
Page 19 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-2 Date Collected
02/08/2019 13:15
WPA Lab No
93057
Date Received
02/09/2019
Matrix
Solids
nn A gnu
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.7 g
1
2/16/2019 08:19:44
MMK
L421893
CAS#
Parameter
C9-C18
Aliphatic C9-C18
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
CIA1_r'%Dv1A1T
Result MDL MQL Units
ND 2.02 3.97 mg/Kg - dry
Recovery Rec. Limits
54.1 40-140%
55.2 40-140%
Prep Date
Prep Batch
Prep Method
Dilution
Analysis Date
By
Analytical Batch
NA
NA
NA
1
2/15/201916:43:00
RXC
L421695
CAS# Parameter Result MQL Units
Moisture % Moisture 24.4 %
Qualifiers/ Outside QC limit
Definitions M Minimum value
MQL Method Quantitation Limit
J Estimated value
MDL Method Detection Limit
ND Not Detected
Page 20 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
6.27 g
1
2/13/2019 16:51:30
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
67-64-1
Acetone
0.0114 J
0.0103
0.0461
mg/Kg - dry
75-05-8
Acetonitrile
ND
0.0485
0.231
mg/Kg - dry
107-02-8
Acrolein
ND
0.0028
0.0461
mg/Kg - dry
107-13-1
Acrylonitrile
ND
0.0047
0.0461
mg/Kg - dry
71-43-2
Benzene
ND
0.0019
0.0023
mg/Kg - dry
108-86-1
Bromobenzene
ND
0.0011
0.0023
mg/Kg - dry
74-97-5
Bromochloromethane
ND
0.0018
0.0023
mg/Kg - dry
75-27-4
Bromodichloromethane
ND
0.0010
0.0023
mg/Kg - dry
75-25-2
Bromoform
ND
0.0021
0.0023
mg/Kg - dry
74-83-9
Bromomethane
ND
0.0007
0.0023
mg/Kg - dry
78-93-3
Methyl Ethyl Ketone (MEK)
ND
0.0060
0.0461
mg/Kg - dry
104-51-8
n-Butylbenzene
ND
0.0021
0.0023
mg/Kg - dry
135-98-8
sec -Butyl benzene
ND
0.0015
0.0023
mg/Kg - dry
98-06-6
tert-Butyl benzene
ND
0.0013
0.0023
mg/Kg - dry
75-15-0
Carbon Disulfide
ND
0.0009
0.0023
mg/Kg - dry
56-23-5
Carbon Tetrachloride
ND
0.0015
0.0023
mg/Kg - dry
108-90-7
Chlorobenzene
ND
0.0013
0.0023
mg/Kg - dry
124-48-1
Chlorodibromomethane
ND
0.0016
0.0023
mg/Kg - dry
75-00-3
Chloroethane
ND
0.0020
0.0023
mg/Kg - dry
67-66-3
Chloroform
ND
0.0021
0.0023
mg/Kg - dry
74-87-3
Chloromethane
ND
0.0014
0.0023
mg/Kg - dry
95-49-8
2-Chlorotoluene
ND
0.0021
0.0023
mg/Kg - dry
106-43-4
4-Chlorotoluene
ND
0.0014
0.0023
mg/Kg - dry
96-12-8
1,2-Dibromo-3-Chloropropane
ND
0.0073
0.0115
mg/Kg - dry
106-93-4
1,2-Dibromoethane
ND
0.0015
0.0023
mg/Kg - dry
74-95-3
Dibromomethane
ND
0.0017
0.0023
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.0022
0.0023
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 21 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
6.27 g
1
2/13/2019 16:51:30
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
541-73-1
1,3-Dichlorobenzene
ND
0.0016
0.0023
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.0021
0.0023
mg/Kg - dry
75-71-8
Dichlorodifluoromethane
ND
0.0021
0.0023
mg/Kg - dry
75-34-3
1,1-Dichloroethane
ND
0.0011
0.0023
mg/Kg - dry
107-06-2
1,2-Dichloroethane
ND
0.0020
0.0023
mg/Kg - dry
75-35-4
1,1-Dichloroethene
ND
0.0010
0.0023
mg/Kg - dry
156-59-2
cis-1,2-Dichloroethene
ND
0.0008
0.0023
mg/Kg - dry
156-60-5
trans-1,2-Dichloroethene
ND
0.0012
0.0023
mg/Kg - dry
540-59-0
1,2-Dichloroethene (Total)
ND
0.0008
0.0023
mg/Kg - dry
78-87-5
1,2-Dichloropropane
ND
0.0011
0.0023
mg/Kg - dry
142-28-9
1,3-Dichloropropane
ND
0.0018
0.0023
mg/Kg - dry
594-20-7
2,2-Dichloropropane
ND
0.0010
0.0023
mg/Kg - dry
563-58-6
1,1-Dichloropropene
ND
0.0007
0.0023
mg/Kg - dry
10061-01-5
cis-1,3-Dichloropropene
ND
0.0009
0.0023
mg/Kg - dry
10061-02-6
trans-1,3-Dichloropropene
ND
0.0010
0.0023
mg/Kg - dry
141-78-6
Ethyl Acetate
ND
0.0049
0.0461
mg/Kg - dry
100-41-4
Ethylbenzene
ND
0.0017
0.0023
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.0016
0.0023
mg/Kg - dry
591-78-6
2-Hexanone
ND
0.0027
0.0115
mg/Kg - dry
74-88-4
Iodomethane
ND
0.0062
0.0115
mg/Kg - dry
98-82-8
Isopropyl benzene
ND
0.0017
0.0023
mg/Kg - dry
99-87-6
4-Isopropyl toluene
ND
0.0018
0.0023
mg/Kg - dry
1634-04-4
Methyl tert-butyl ether (MTBE)
ND
0.0006
0.0023
mg/Kg - dry
108-10-1
4-Methyl -2-Pentanone
ND
0.0039
0.0115
mg/Kg - dry
75-09-2
Methylene Chloride
ND
0.0110
0.0115
mg/Kg - dry
91-20-3
Naphthalene
ND
0.0042
0.0115
mg/Kg - dry
109-60-4
n-Propyl acetate
ND
0.0048
0.0115
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 22 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
6.27 g
1
2/13/2019 16:51:30
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
103-65-1
n-Propylbenzene
ND
0.0017
0.0023
mg/Kg - dry
100-42-5
Styrene
ND
0.0021
0.0023
mg/Kg - dry
630-20-6
1,1,1,2-Tetrachloroethane
ND
0.0022
0.0023
mg/Kg - dry
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.0019
0.0023
mg/Kg - dry
127-18-4
Tetrachloroethene
ND
0.0019
0.0023
mg/Kg - dry
108-88-3
Toluene
ND
0.0033
0.0046
mg/Kg - dry
87-61-6
1,2,3-Trichlorobenzene
ND
0.0018
0.0023
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.0020
0.0023
mg/Kg - dry
71-55-6
1,1,1-Trichloroethane
ND
0.0011
0.0023
mg/Kg - dry
79-00-5
1,1,2-Trichloroethane
ND
0.0020
0.0023
mg/Kg - dry
79-01-6
Trichloroethene
ND
0.0013
0.0023
mg/Kg - dry
75-69-4
Trichlorofluoromethane
ND
0.0011
0.0023
mg/Kg - dry
96-18-4
1,2,3-Trichloropropane
ND
0.0019
0.0023
mg/Kg - dry
95-63-6
1,2,4-Trimethylbenzene
ND
0.0013
0.0023
mg/Kg - dry
108-67-8
1,3,5-Trimethylbenzene
ND
0.0022
0.0023
mg/Kg - dry
108-05-4
Vinyl Acetate
ND
0.0099
0.0461
mg/Kg - dry
75-01-4
Vinyl Chloride
ND
0.0013
0.0023
mg/Kg - dry
95-47-6
o-Xylene
ND
0.0015
0.0023
mg/Kg - dry
179601-23-1
m,p-Xylene
ND
0.0031
0.0046
mg/Kg - dry
1330-20-7
Xylene (Total)
ND
0.0015
0.0023
mg/Kg - dry
CAS#
Surrogate
% Recovery
Rec. Limits
460-00-4
4-Bromofluorobenzene
106
60-140%
17060-07-0
1,2-Dichloroethane-d4
115
60-140%
2037-26-5
Toluene-d8
102
60-140%
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 23 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.5 g
1
2/13/2019 19:38:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
83-32-9
Acenaphthene
ND
0.012
0.076
mg/Kg - dry
208-96-8
Acenaphthylene
ND
0.013
0.076
mg/Kg - dry
98-86-2
Acetophenone
ND
0.017
0.196
mg/Kg - dry
62-53-3
Aniline
ND
0.005
0.196
mg/Kg - dry
120-12-7
Anthracene
ND
0.014
0.076
mg/Kg - dry
92-87-5
Benzidine
ND
M
0.583
0.772
mg/Kg - dry
56-55-3
Benzo(a)anthracene
ND
0.009
0.076
mg/Kg - dry
50-32-8
Benzo(a)pyrene
ND
0.011
0.076
mg/Kg - dry
205-99-2
Benzo(b)fluoranthene
ND
0.009
0.076
mg/Kg - dry
191-24-2
Benzo(g,h,i)perylene
ND
0.015
0.076
mg/Kg - dry
207-08-9
Benzo(k)fluoranthene
ND
0.013
0.076
mg/Kg - dry
65-85-0
Benzoic Acid
ND
M
0.019
0.380
mg/Kg - dry
100-51-6
Benzyl alcohol
ND
0.024
0.380
mg/Kg - dry
111-91-1
Bis(2-Chloroethoxy)methane
ND
0.013
0.196
mg/Kg - dry
111-44-4
Bis(2-Chloroethyl)ether
ND
0.007
0.196
mg/Kg - dry
108-60-1
Bis(2-Chloroisopropyl)ether
ND
0.025
0.196
mg/Kg - dry
117-81-7
Bis(2-ethylhexyl)phthalate
ND
0.017
0.380
mg/Kg - dry
101-55-3
4-Bromophenyl phenyl ether
ND
0.017
0.196
mg/Kg - dry
85-68-7
Butyl benzyl phthalate
ND
0.019
0.196
mg/Kg - dry
86-74-8
Carbazole
ND
0.011
0.196
mg/Kg - dry
59-50-7
4-Chloro-3-methylphenol
ND
0.018
0.196
mg/Kg - dry
106-47-8
4-Chloroaniline
ND
0.014
0.196
mg/Kg - dry
91-58-7
2-Chloronaphthalene
ND
0.010
0.196
mg/Kg - dry
95-57-8
2-Chlorophenol
ND
0.015
0.196
mg/Kg - dry
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.013
0.196
mg/Kg - dry
218-01-9
Chrysene
ND
0.012
0.076
mg/Kg - dry
53-70-3
Dibenz(a,h)anthracene
ND
0.013
0.076
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 24 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.5 g
1
2/13/2019 19:38:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
132-64-9
Dibenzofuran
ND
0.016
0.196
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.009
0.196
mg/Kg - dry
541-73-1
1,3-Dichlorobenzene
ND
0.010
0.196
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.011
0.196
mg/Kg - dry
91-94-1
3,3'-Dichlorobenzidine
ND
0.126
0.380
mg/Kg - dry
120-83-2
2,4-Dichlorophenol
ND
0.017
0.196
mg/Kg - dry
87-65-0
2,6-Dichlorophenol
ND
0.015
0.196
mg/Kg - dry
84-66-2
Diethyl phthalate
ND
0.012
0.196
mg/Kg - dry
131-11-3
Dimethyl phthalate
ND
0.016
0.196
mg/Kg - dry
119-93-7
3,3' Dimethylbenzidine
ND M
0.041
0.380
mg/Kg - dry
105-67-9
2,4-Dimethyl phenol
ND
0.025
0.196
mg/Kg - dry
84-74-2
Di-n-butyl phthalate
ND
0.016
0.196
mg/Kg - dry
534-52-1
4,6-Dinitro-2-methyl phenol
ND
0.010
0.380
mg/Kg - dry
51-28-5
2,4-Dinitrophenol
ND
0.011
0.380
mg/Kg - dry
121-14-2
2,4-Dinitrotoluene
ND
0.012
0.196
mg/Kg - dry
606-20-2
2,6-Dinitrotoluene
ND
0.013
0.196
mg/Kg - dry
117-84-0
Di-n-Octyl Phthalate
ND
0.025
0.196
mg/Kg - dry
206-44-0
Fluoranthene
ND
0.011
0.076
mg/Kg - dry
86-73-7
Fluorene
ND
0.018
0.076
mg/Kg - dry
118-74-1
Hexachlorobenzene
ND
0.012
0.196
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.011
0.196
mg/Kg - dry
77-47-4
Hexachlorocyclopentadiene
ND
0.016
0.196
mg/Kg - dry
67-72-1
Hexachloroethane
ND
0.012
0.196
mg/Kg - dry
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.020
0.076
mg/Kg - dry
78-59-1
Isophorone
ND
0.012
0.196
mg/Kg - dry
91-57-6
2-Methyl naphthalene
ND
0.011
0.076
mg/Kg - dry
95-48-7
2-Methylphenol
ND
0.017
0.196
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 25 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.5 g
1
2/13/2019 19:38:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
108-39-4
3&4 Methylphenol
ND
0.016
0.196
mg/Kg - dry
91-20-3
Naphthalene
ND
0.012
0.076
mg/Kg - dry
88-74-4
2-Nitroaniline
ND
0.019
0.196
mg/Kg - dry
99-09-2
3-Nitroaniline
ND
0.011
0.380
mg/Kg - dry
100-01-6
4-Nitroaniline
ND
0.013
0.196
mg/Kg - dry
98-95-3
Nitrobenzene
ND
0.007
0.196
mg/Kg - dry
88-75-5
2-Nitrophenol
ND
0.019
0.196
mg/Kg - dry
100-02-7
4-Nitrophenol
ND
0.015
0.196
mg/Kg - dry
62-75-9
N-Nitrosodimethylamine
ND
0.006
0.196
mg/Kg - dry
86-30-6
N-Nitrosodiphenylamine
ND
0.014
0.380
mg/Kg - dry
55-18-5
N-Nitrosodiethylamine
ND
0.023
0.196
mg/Kg - dry
924-16-3
N-Nitroso-di-n-butylamine
ND
0.018
0.196
mg/Kg - dry
621-64-7
N-Nitroso-di-n-propylamine
ND
0.011
0.196
mg/Kg - dry
87-86-5
Pentachlorophenol
ND
0.021
0.380
mg/Kg - dry
85-01-8
Phenanthrene
ND
0.015
0.076
mg/Kg - dry
108-95-2
Phenol
ND
0.023
0.196
mg/Kg - dry
129-00-0
Pyrene
ND
0.014
0.076
mg/Kg - dry
110-86-1
Pyridine
ND
0.017
0.380
mg/Kg - dry
95-94-3
1,2,4,5-Tetrachlorobenzene
ND
0.010
0.196
mg/Kg - dry
58-90-2
2,3,4,6-Tetrachlorophenol
ND
0.017
0.196
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.011
0.196
mg/Kg - dry
95-95-4
2,4,5-Trichlorophenol
ND
0.023
0.196
mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 26 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
C\A/_S277f1F
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.5 g
1
2/13/2019 19:38:00
CGC
L422041
CAS#
Parameter
88-06-2
2,4,6-Trichlorophenol
CAS#
Surrogate
321-60-8
2-Fluorobiphenyl
367-12-4
2-Fluorophenol
4165-60-0
Nitrobenzene-d5
13127-88-3
Phenol-d6
1718-51-0
4-Terphenyl-d14
118-79-6
2,4,6-Tribromophenol
Result MDL MQL Units
ND 0.017 0.196 mg/Kg - dry
Recovery
Rec. Limits
31.7
20-79%
32.0
10-85%
30.8
22-72%
35.7
10-96%
34.8
22-104%
40.5
10-112%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.2 g
1
2/16/2019 03:52:38
MMK
L421893
CAS#
Parameter
C11-C22
Aromatic C11-C22
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
MA�Du
Result MDL MQL Units
ND 2.35 9.80 mg/Kg - dry
Recovery Rec. Limits
49.1 40-140%
50.7 40-140%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.2 g
1
2/16/2019 08:53:10
MMK
L421893
CAS# Parameter Result MDL MQL Units
C19-C36 Aliphatic C19-C36 ND 2.20 4.61 mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 27 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-3 Date Collected
02/08/2019 13:30
WPA Lab No
93058
Date Received
02/09/2019
Matrix
Solids
nn A gnu
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.2 g
1
2/16/2019 08:53:10
MMK
L421893
CAS#
Parameter
C9-C18
Aliphatic C9-C18
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
CIA1_r'%Dv1A1T
Result MDL MQL Units
ND 1.76 3.46 mg/Kg - dry
Recovery Rec. Limits
49.1 40-140%
50.7 40-140%
Prep Date
Prep Batch
Prep Method
Dilution
Analysis Date
By
Analytical Batch
NA
NA
NA
1
2/15/201917:05:00
RXC
L421696
CAS# Parameter Result MQL Units
Moisture % Moisture 13.3 %
Qualifiers/ Outside QC limit
Definitions M Minimum value
MQL Method Quantitation Limit
J Estimated value
MDL Method Detection Limit
ND Not Detected
Page 28 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.64 g
1
2/13/2019 17:32:29
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
67-64-1
Acetone
0.0802
0.0103
0.0461
mg/Kg - dry
75-05-8
Acetonitrile
ND
0.0485
0.231
mg/Kg - dry
107-02-8
Acrolein
ND
0.0028
0.0461
mg/Kg - dry
107-13-1
Acrylonitrile
ND
0.0047
0.0461
mg/Kg - dry
71-43-2
Benzene
ND
0.0019
0.0023
mg/Kg - dry
108-86-1
Bromobenzene
ND
0.0011
0.0023
mg/Kg - dry
74-97-5
Bromochloromethane
ND
0.0018
0.0023
mg/Kg - dry
75-27-4
Bromodichloromethane
ND
0.0010
0.0023
mg/Kg - dry
75-25-2
Bromoform
ND
0.0021
0.0023
mg/Kg - dry
74-83-9
Bromomethane
ND
0.0007
0.0023
mg/Kg - dry
78-93-3
Methyl Ethyl Ketone (MEK)
0.0069 J
0.0060
0.0461
mg/Kg - dry
104-51-8
n-Butylbenzene
ND
0.0021
0.0023
mg/Kg - dry
135-98-8
sec -Butyl benzene
ND
0.0015
0.0023
mg/Kg - dry
98-06-6
tert-Butyl benzene
ND
0.0013
0.0023
mg/Kg - dry
75-15-0
Carbon Disulfide
ND
0.0009
0.0023
mg/Kg - dry
56-23-5
Carbon Tetrachloride
ND
0.0015
0.0023
mg/Kg - dry
108-90-7
Chlorobenzene
ND
0.0013
0.0023
mg/Kg - dry
124-48-1
Chlorodibromomethane
ND
0.0016
0.0023
mg/Kg - dry
75-00-3
Chloroethane
ND
0.0020
0.0023
mg/Kg - dry
67-66-3
Chloroform
ND
0.0021
0.0023
mg/Kg - dry
74-87-3
Chloromethane
ND
0.0014
0.0023
mg/Kg - dry
95-49-8
2-Chlorotoluene
ND
0.0021
0.0023
mg/Kg - dry
106-43-4
4-Chlorotoluene
ND
0.0014
0.0023
mg/Kg - dry
96-12-8
1,2-Dibromo-3-Chloropropane
ND
0.0073
0.0115
mg/Kg - dry
106-93-4
1,2-Dibromoethane
ND
0.0015
0.0023
mg/Kg - dry
74-95-3
Dibromomethane
ND
0.0017
0.0023
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.0022
0.0023
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 29 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.64 g
1
2/13/2019 17:32:29
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
541-73-1
1,3-Dichlorobenzene
ND
0.0016
0.0023
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.0021
0.0023
mg/Kg - dry
75-71-8
Dichlorodifluoromethane
ND
0.0021
0.0023
mg/Kg - dry
75-34-3
1,1-Dichloroethane
ND
0.0011
0.0023
mg/Kg - dry
107-06-2
1,2-Dichloroethane
ND
0.0020
0.0023
mg/Kg - dry
75-35-4
1,1-Dichloroethene
ND
0.0010
0.0023
mg/Kg - dry
156-59-2
cis-1,2-Dichloroethene
ND
0.0008
0.0023
mg/Kg - dry
156-60-5
trans-1,2-Dichloroethene
ND
0.0012
0.0023
mg/Kg - dry
540-59-0
1,2-Dichloroethene (Total)
ND
0.0008
0.0023
mg/Kg - dry
78-87-5
1,2-Dichloropropane
ND
0.0011
0.0023
mg/Kg - dry
142-28-9
1,3-Dichloropropane
ND
0.0018
0.0023
mg/Kg - dry
594-20-7
2,2-Dichloropropane
ND
0.0010
0.0023
mg/Kg - dry
563-58-6
1,1-Dichloropropene
ND
0.0007
0.0023
mg/Kg - dry
10061-01-5
cis-1,3-Dichloropropene
ND
0.0009
0.0023
mg/Kg - dry
10061-02-6
trans-1,3-Dichloropropene
ND
0.0010
0.0023
mg/Kg - dry
141-78-6
Ethyl Acetate
ND
0.0049
0.0461
mg/Kg - dry
100-41-4
Ethylbenzene
ND
0.0017
0.0023
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.0016
0.0023
mg/Kg - dry
591-78-6
2-Hexanone
ND
0.0027
0.0115
mg/Kg - dry
74-88-4
Iodomethane
ND
0.0062
0.0115
mg/Kg - dry
98-82-8
Isopropyl benzene
ND
0.0017
0.0023
mg/Kg - dry
99-87-6
4-Isopropyl toluene
ND
0.0018
0.0023
mg/Kg - dry
1634-04-4
Methyl tert-butyl ether (MTBE)
ND
0.0006
0.0023
mg/Kg - dry
108-10-1
4-Methyl -2-Pentanone
ND
0.0039
0.0115
mg/Kg - dry
75-09-2
Methylene Chloride
ND
0.0110
0.0115
mg/Kg - dry
91-20-3
Naphthalene
ND
0.0042
0.0115
mg/Kg - dry
109-60-4
n-Propyl acetate
ND
0.0048
0.0115
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 30 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.64 g
1
2/13/2019 17:32:29
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
103-65-1
n-Propylbenzene
ND
0.0017
0.0023
mg/Kg - dry
100-42-5
Styrene
ND
0.0021
0.0023
mg/Kg - dry
630-20-6
1,1,1,2-Tetrachloroethane
ND
0.0022
0.0023
mg/Kg - dry
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.0019
0.0023
mg/Kg - dry
127-18-4
Tetrachloroethene
ND
0.0019
0.0023
mg/Kg - dry
108-88-3
Toluene
ND
0.0033
0.0046
mg/Kg - dry
87-61-6
1,2,3-Trichlorobenzene
ND
0.0018
0.0023
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.0020
0.0023
mg/Kg - dry
71-55-6
1,1,1-Trichloroethane
ND
0.0011
0.0023
mg/Kg - dry
79-00-5
1,1,2-Trichloroethane
ND
0.0020
0.0023
mg/Kg - dry
79-01-6
Trichloroethene
ND
0.0013
0.0023
mg/Kg - dry
75-69-4
Trichlorofluoromethane
ND
0.0011
0.0023
mg/Kg - dry
96-18-4
1,2,3-Trichloropropane
ND
0.0019
0.0023
mg/Kg - dry
95-63-6
1,2,4-Trimethylbenzene
ND
0.0013
0.0023
mg/Kg - dry
108-67-8
1,3,5-Trimethylbenzene
ND
0.0022
0.0023
mg/Kg - dry
108-05-4
Vinyl Acetate
ND
0.0099
0.0461
mg/Kg - dry
75-01-4
Vinyl Chloride
ND
0.0013
0.0023
mg/Kg - dry
95-47-6
o-Xylene
ND
0.0015
0.0023
mg/Kg - dry
179601-23-1
m,p-Xylene
ND
0.0031
0.0046
mg/Kg - dry
1330-20-7
Xylene (Total)
ND
0.0015
0.0023
mg/Kg - dry
CAS#
Surrogate
% Recovery
Rec. Limits
460-00-4
4-Bromofluorobenzene
82.8
60-140%
17060-07-0
1,2-Dichloroethane-d4
112
60-140%
2037-26-5
Toluene-d8
87.4
60-140%
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 31 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.7 g
1
2/13/2019 19:57:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
83-32-9
Acenaphthene
ND
0.012
0.076
mg/Kg - dry
208-96-8
Acenaphthylene
ND
0.013
0.076
mg/Kg - dry
98-86-2
Acetophenone
ND
0.017
0.196
mg/Kg - dry
62-53-3
Aniline
ND
0.005
0.196
mg/Kg - dry
120-12-7
Anthracene
ND
0.014
0.076
mg/Kg - dry
92-87-5
Benzidine
ND
M
0.583
0.772
mg/Kg - dry
56-55-3
Benzo(a)anthracene
ND
0.009
0.076
mg/Kg - dry
50-32-8
Benzo(a)pyrene
ND
0.011
0.076
mg/Kg - dry
205-99-2
Benzo(b)fluoranthene
ND
0.009
0.076
mg/Kg - dry
191-24-2
Benzo(g,h,i)perylene
ND
0.015
0.076
mg/Kg - dry
207-08-9
Benzo(k)fluoranthene
ND
0.013
0.076
mg/Kg - dry
65-85-0
Benzoic Acid
ND
M
0.019
0.380
mg/Kg - dry
100-51-6
Benzyl alcohol
ND
0.024
0.380
mg/Kg - dry
111-91-1
Bis(2-Chloroethoxy)methane
ND
0.013
0.196
mg/Kg - dry
111-44-4
Bis(2-Chloroethyl)ether
ND
0.007
0.196
mg/Kg - dry
108-60-1
Bis(2-Chloroisopropyl)ether
ND
0.025
0.196
mg/Kg - dry
117-81-7
Bis(2-ethylhexyl)phthalate
ND
0.017
0.380
mg/Kg - dry
101-55-3
4-Bromophenyl phenyl ether
ND
0.017
0.196
mg/Kg - dry
85-68-7
Butyl benzyl phthalate
ND
0.019
0.196
mg/Kg - dry
86-74-8
Carbazole
ND
0.011
0.196
mg/Kg - dry
59-50-7
4-Chloro-3-methylphenol
ND
0.018
0.196
mg/Kg - dry
106-47-8
4-Chloroaniline
ND
0.014
0.196
mg/Kg - dry
91-58-7
2-Chloronaphthalene
ND
0.010
0.196
mg/Kg - dry
95-57-8
2-Chlorophenol
ND
0.015
0.196
mg/Kg - dry
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.013
0.196
mg/Kg - dry
218-01-9
Chrysene
ND
0.012
0.076
mg/Kg - dry
53-70-3
Dibenz(a,h)anthracene
ND
0.013
0.076
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 32 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.7 g
1
2/13/2019 19:57:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
132-64-9
Dibenzofuran
ND
0.016
0.196
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.009
0.196
mg/Kg - dry
541-73-1
1,3-Dichlorobenzene
ND
0.010
0.196
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.011
0.196
mg/Kg - dry
91-94-1
3,3'-Dichlorobenzidine
ND
0.126
0.380
mg/Kg - dry
120-83-2
2,4-Dichlorophenol
ND
0.017
0.196
mg/Kg - dry
87-65-0
2,6-Dichlorophenol
ND
0.015
0.196
mg/Kg - dry
84-66-2
Diethyl phthalate
ND
0.012
0.196
mg/Kg - dry
131-11-3
Dimethyl phthalate
ND
0.016
0.196
mg/Kg - dry
119-93-7
3,3' Dimethylbenzidine
ND M
0.041
0.380
mg/Kg - dry
105-67-9
2,4-Dimethyl phenol
ND
0.025
0.196
mg/Kg - dry
84-74-2
Di-n-butyl phthalate
ND
0.016
0.196
mg/Kg - dry
534-52-1
4,6-Dinitro-2-methyl phenol
ND
0.010
0.380
mg/Kg - dry
51-28-5
2,4-Dinitrophenol
ND
0.011
0.380
mg/Kg - dry
121-14-2
2,4-Dinitrotoluene
ND
0.012
0.196
mg/Kg - dry
606-20-2
2,6-Dinitrotoluene
ND
0.013
0.196
mg/Kg - dry
117-84-0
Di-n-Octyl Phthalate
ND
0.025
0.196
mg/Kg - dry
206-44-0
Fluoranthene
ND
0.011
0.076
mg/Kg - dry
86-73-7
Fluorene
ND
0.018
0.076
mg/Kg - dry
118-74-1
Hexachlorobenzene
ND
0.012
0.196
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.011
0.196
mg/Kg - dry
77-47-4
Hexachlorocyclopentadiene
ND
0.016
0.196
mg/Kg - dry
67-72-1
Hexachloroethane
ND
0.012
0.196
mg/Kg - dry
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.020
0.076
mg/Kg - dry
78-59-1
Isophorone
ND
0.012
0.196
mg/Kg - dry
91-57-6
2-Methyl naphthalene
ND
0.011
0.076
mg/Kg - dry
95-48-7
2-Methylphenol
ND
0.017
0.196
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 33 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.7 g
1
2/13/2019 19:57:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
108-39-4
3&4 Methylphenol
ND
0.016
0.196
mg/Kg - dry
91-20-3
Naphthalene
ND
0.012
0.076
mg/Kg - dry
88-74-4
2-Nitroaniline
ND
0.019
0.196
mg/Kg - dry
99-09-2
3-Nitroaniline
ND
0.011
0.380
mg/Kg - dry
100-01-6
4-Nitroaniline
ND
0.013
0.196
mg/Kg - dry
98-95-3
Nitrobenzene
ND
0.007
0.196
mg/Kg - dry
88-75-5
2-Nitrophenol
ND
0.019
0.196
mg/Kg - dry
100-02-7
4-Nitrophenol
ND
0.015
0.196
mg/Kg - dry
62-75-9
N-Nitrosodimethylamine
ND
0.006
0.196
mg/Kg - dry
86-30-6
N-Nitrosodiphenylamine
ND
0.014
0.380
mg/Kg - dry
55-18-5
N-Nitrosodiethylamine
ND
0.023
0.196
mg/Kg - dry
924-16-3
N-Nitroso-di-n-butylamine
ND
0.018
0.196
mg/Kg - dry
621-64-7
N-Nitroso-di-n-propylamine
ND
0.011
0.196
mg/Kg - dry
87-86-5
Pentachlorophenol
ND
0.021
0.380
mg/Kg - dry
85-01-8
Phenanthrene
ND
0.015
0.076
mg/Kg - dry
108-95-2
Phenol
ND
0.023
0.196
mg/Kg - dry
129-00-0
Pyrene
ND
0.014
0.076
mg/Kg - dry
110-86-1
Pyridine
ND
0.017
0.380
mg/Kg - dry
95-94-3
1,2,4,5-Tetrachlorobenzene
ND
0.010
0.196
mg/Kg - dry
58-90-2
2,3,4,6-Tetrachlorophenol
ND
0.017
0.196
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.011
0.196
mg/Kg - dry
95-95-4
2,4,5-Trichlorophenol
ND
0.023
0.196
mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 34 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
C\A/_S277f1F
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.7 g
1
2/13/2019 19:57:00
CGC
L422041
CAS#
Parameter
88-06-2
2,4,6-Trichlorophenol
CAS#
Surrogate
321-60-8
2-Fluorobiphenyl
367-12-4
2-Fluorophenol
4165-60-0
Nitrobenzene-d5
13127-88-3
Phenol-d6
1718-51-0
4-Terphenyl-d14
118-79-6
2,4,6-Tribromophenol
Result MDL MQL Units
ND 0.017 0.196 mg/Kg - dry
Recovery
Rec. Limits
25.0
20-79%
24.0
10-85%
25.0
22-72%
27.3
10-96%
28.3
22-104%
29.7
10-112%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.7 g
1
2/16/2019 04:25:57
MMK
L421893
CAS#
Parameter
C11-C22
Aromatic C11-C22
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
MA�Du
Result MDL MQL Units
ND 2.35 9.80 mg/Kg - dry
Recovery Rec. Limits
50.1 40-140%
53.4 40-140%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.7 g
1
2/16/2019 09:26:34
MMK
L421893
CAS# Parameter Result MDL MQL Units
C19-C36 Aliphatic C19-C36 ND 2.20 4.61 mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 35 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-4 Date Collected
02/08/2019 13:45
WPA Lab No
93059
Date Received
02/09/2019
Matrix
Solids
nn A gnu
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.7 g
1
2/16/2019 09:26:34
MMK
L421893
CAS#
Parameter
C9-C18
Aliphatic C9-C18
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
CIA1_r'%Dv1A1T
Result MDL MQL Units
ND 1.76 3.46 mg/Kg - dry
Recovery Rec. Limits
50.1 40-140%
53.4 40-140%
Prep Date
Prep Batch
Prep Method
Dilution
Analysis Date
By
Analytical Batch
NA
NA
NA
1
2/15/201917:05:00
RXC
L421696
CAS# Parameter Result MQL Units
Moisture % Moisture 13.3 %
Qualifiers/ Outside QC limit
Definitions M Minimum value
MQL Method Quantitation Limit
J Estimated value
MDL Method Detection Limit
ND Not Detected
Page 36 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
CIA/_Q01 rP1nDnl
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 09:50
L421188
3546
30.1 g
1
2/13/2019 19:09:09
BEB
L421403
CAS#
Parameter
TNDIESEL
Diesel Range Organics (C10-C28)
CAS#
Surrogate
84-15-1
o-Terphenyl
C\A/-Qf11 S(Yr
m
Result MDL MQL Units
1.36 J 1.27 3.88 mg/Kg - dry
Recovery Rec. Limits
66.6 50-150%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:42
L421644
5035
5.29 g
50
2/14/2019 20:28:10
SPC
L421650
CAS#
Parameter
C6-C10
Gasoline Range Organics (C6-C10)
CAS#
Surrogate
106-39-8
4-Bromochlorobenzene
C1A/_Q7tifln
(1Z/)2EZ1
Result MDL MQL Units
ND 9.91 11.0 mg/Kg - dry
Recovery Rec. Limits
82.4 50-150%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.91 g
1
2/13/2019 18:13:38
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
67-64-1
Acetone
0.0143 J
0.0104
0.0465
mg/Kg - dry
75-05-8
Acetonitrile
ND
0.0490
0.233
mg/Kg - dry
107-02-8
Acrolein
ND
0.0028
0.0465
mg/Kg - dry
107-13-1
Acrylonitrile
ND
0.0048
0.0465
mg/Kg - dry
71-43-2
Benzene
ND
0.0019
0.0023
mg/Kg - dry
108-86-1
Bromobenzene
ND
0.0011
0.0023
mg/Kg - dry
74-97-5
Bromochloromethane
ND
0.0018
0.0023
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 37 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.91 g
1
2/13/2019 18:13:38
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
75-27-4
Bromodichloromethane
ND
0.0010
0.0023
mg/Kg - dry
75-25-2
Bromoform
ND
0.0021
0.0023
mg/Kg - dry
74-83-9
Bromomethane
ND
0.0007
0.0023
mg/Kg - dry
78-93-3
Methyl Ethyl Ketone (MEK)
ND
0.0060
0.0465
mg/Kg - dry
104-51-8
n-Butylbenzene
ND
0.0021
0.0023
mg/Kg - dry
135-98-8
sec -Butyl benzene
ND
0.0015
0.0023
mg/Kg - dry
98-06-6
tert-Butyl benzene
ND
0.0013
0.0023
mg/Kg - dry
75-15-0
Carbon Disulfide
ND
0.0009
0.0023
mg/Kg - dry
56-23-5
Carbon Tetrachloride
ND
0.0015
0.0023
mg/Kg - dry
108-90-7
Chlorobenzene
ND
0.0013
0.0023
mg/Kg - dry
124-48-1
Chlorodibromomethane
ND
0.0016
0.0023
mg/Kg - dry
75-00-3
Chloroethane
ND
0.0020
0.0023
mg/Kg - dry
67-66-3
Chloroform
ND
0.0021
0.0023
mg/Kg - dry
74-87-3
Chloromethane
ND
0.0015
0.0023
mg/Kg - dry
95-49-8
2-Chlorotoluene
ND
0.0021
0.0023
mg/Kg - dry
106-43-4
4-Chlorotoluene
ND
0.0015
0.0023
mg/Kg - dry
96-12-8
1,2-Dibromo-3-Chloropropane
ND
0.0073
0.0116
mg/Kg - dry
106-93-4
1,2-Dibromoethane
ND
0.0015
0.0023
mg/Kg - dry
74-95-3
Dibromomethane
ND
0.0017
0.0023
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.0022
0.0023
mg/Kg - dry
541-73-1
1,3-Dichlorobenzene
ND
0.0017
0.0023
mg/Kg - dry
106-46-7
1,4-Dichlorobenzene
ND
0.0021
0.0023
mg/Kg - dry
75-71-8
Dichlorodifluoromethane
ND
0.0022
0.0023
mg/Kg - dry
75-34-3
1,1-Dichloroethane
ND
0.0011
0.0023
mg/Kg - dry
107-06-2
1,2-Dichloroethane
ND
0.0020
0.0023
mg/Kg - dry
75-35-4
1,1-Dichloroethene
ND
0.0010
0.0023
mg/Kg - dry
156-59-2
cis-1,2-Dichloroethene
ND
0.0008
0.0023
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 38 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.91 g
1
2/13/2019 18:13:38
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
156-60-5
trans-1,2-Dichloroethene
ND
0.0012
0.0023
mg/Kg - dry
540-59-0
1,2-Dichloroethene (Total)
ND
0.0008
0.0023
mg/Kg - dry
78-87-5
1,2-Dichloropropane
ND
0.0011
0.0023
mg/Kg - dry
142-28-9
1,3-Dichloropropane
ND
0.0018
0.0023
mg/Kg - dry
594-20-7
2,2-Dichloropropane
ND
0.0010
0.0023
mg/Kg - dry
563-58-6
1,1-Dichloropropene
ND
0.0007
0.0023
mg/Kg - dry
10061-01-5
cis-1,3-Dichloropropene
ND
0.0009
0.0023
mg/Kg - dry
10061-02-6
trans-1,3-Dichloropropene
ND
0.0010
0.0023
mg/Kg - dry
141-78-6
Ethyl Acetate
ND
0.0049
0.0465
mg/Kg - dry
100-41-4
Ethylbenzene
ND
0.0017
0.0023
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.0016
0.0023
mg/Kg - dry
591-78-6
2-Hexanone
ND
0.0027
0.0116
mg/Kg - dry
74-88-4
Iodomethane
ND
0.0063
0.0116
mg/Kg - dry
98-82-8
Isopropyl benzene
ND
0.0018
0.0023
mg/Kg - dry
99-87-6
4-Isopropyl toluene
ND
0.0018
0.0023
mg/Kg - dry
1634-04-4
Methyl tert-butyl ether (MTBE)
ND
0.0006
0.0023
mg/Kg - dry
108-10-1
4-Methyl -2-Pentanone
ND
0.0039
0.0116
mg/Kg - dry
75-09-2
Methylene Chloride
ND
0.0111
0.0116
mg/Kg - dry
91-20-3
Naphthalene
ND
0.0043
0.0116
mg/Kg - dry
109-60-4
n-Propyl acetate
ND
0.0049
0.0116
mg/Kg - dry
103-65-1
n-Propylbenzene
ND
0.0017
0.0023
mg/Kg - dry
100-42-5
Styrene
ND
0.0021
0.0023
mg/Kg - dry
630-20-6
1,1,1,2-Tetrachloroethane
ND
0.0022
0.0023
mg/Kg - dry
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.0019
0.0023
mg/Kg - dry
127-18-4
Tetrachloroethene
ND
0.0019
0.0023
mg/Kg - dry
108-88-3
Toluene
ND
0.0033
0.0046
mg/Kg - dry
87-61-6
1,2,3-Trichlorobenzene
ND
0.0018
0.0023
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 39 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
SW-8260D (5035)
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/13/2019 08:44
L422031
5035
5.91 g
1
2/13/2019 18:13:38
SPC
L422037
CAS#
Parameter
Result
MDL
MQL
Units
120-82-1
1,2,4-Trichlorobenzene
ND
0.0020
0.0023
mg/Kg - dry
71-55-6
1,1,1-Trichloroethane
ND
0.0011
0.0023
mg/Kg - dry
79-00-5
1,1,2-Trichloroethane
ND
0.0020
0.0023
mg/Kg - dry
79-01-6
Trichloroethene
ND
0.0013
0.0023
mg/Kg - dry
75-69-4
Trichlorofluoromethane
ND
0.0011
0.0023
mg/Kg - dry
96-18-4
1,2,3-Trichloropropane
ND
0.0019
0.0023
mg/Kg - dry
95-63-6
1,2,4-Trimethylbenzene
ND
0.0013
0.0023
mg/Kg - dry
108-67-8
1,3,5-Trimethylbenzene
ND
0.0022
0.0023
mg/Kg - dry
108-05-4
Vinyl Acetate
ND
0.0100
0.0465
mg/Kg - dry
75-01-4
Vinyl Chloride
ND
0.0013
0.0023
mg/Kg - dry
95-47-6
o-Xylene
ND
0.0015
0.0023
mg/Kg - dry
179601-23-1
m,p-Xylene
ND
0.0032
0.0046
mg/Kg - dry
1330-20-7
Xylene (Total)
ND
0.0015
0.0023
mg/Kg - dry
CAS#
Surrogate
% Recovery
Rec. Limits
460-00-4
4-Bromofluorobenzene
83.0
60-140%
17060-07-0
1,2-Dichloroethane-d4
108
60-140%
2037-26-5
Toluene-d8
92.4
60-140%
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 20:16:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
83-32-9
Acenaphthene
ND
0.012
0.077
mg/Kg - dry
208-96-8
Acenaphthylene
ND
0.013
0.077
mg/Kg - dry
98-86-2
Acetophenone
ND
0.017
0.197
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 40 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 20:16:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
62-53-3
Aniline
ND
0.005
0.197
mg/Kg - dry
120-12-7
Anthracene
ND
0.015
0.077
mg/Kg - dry
92-87-5
Benzidine
ND
M
0.589
0.779
mg/Kg - dry
56-55-3
Benzo(a)anthracene
ND
0.010
0.077
mg/Kg - dry
50-32-8
Benzo(a)pyrene
ND
0.011
0.077
mg/Kg - dry
205-99-2
Benzo(b)fluoranthene
ND
0.009
0.077
mg/Kg - dry
191-24-2
Benzo(g,h,i)perylene
ND
0.015
0.077
mg/Kg - dry
207-08-9
Benzo(k)fluoranthene
ND
0.013
0.077
mg/Kg - dry
65-85-0
Benzoic Acid
ND
M
0.019
0.384
mg/Kg - dry
100-51-6
Benzyl alcohol
ND
0.024
0.384
mg/Kg - dry
111-91-1
Bis(2-Chloroethoxy)methane
ND
0.013
0.197
mg/Kg - dry
111-44-4
Bis(2-Chloroethyl)ether
ND
0.007
0.197
mg/Kg - dry
108-60-1
Bis(2-Chloroisopropyl)ether
ND
0.025
0.197
mg/Kg - dry
117-81-7
Bis(2-ethylhexyl)phthalate
ND
0.017
0.384
mg/Kg - dry
101-55-3
4-Bromophenyl phenyl ether
ND
0.017
0.197
mg/Kg - dry
85-68-7
Butyl benzyl phthalate
ND
0.020
0.197
mg/Kg - dry
86-74-8
Carbazole
ND
0.011
0.197
mg/Kg - dry
59-50-7
4-Chloro-3-methylphenol
ND
0.018
0.197
mg/Kg - dry
106-47-8
4-Chloroaniline
ND
0.014
0.197
mg/Kg - dry
91-58-7
2-Chloronaphthalene
ND
0.010
0.197
mg/Kg - dry
95-57-8
2-Chlorophenol
ND
0.015
0.197
mg/Kg - dry
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.013
0.197
mg/Kg - dry
218-01-9
Chrysene
ND
0.012
0.077
mg/Kg - dry
53-70-3
Dibenz(a,h)anthracene
ND
0.013
0.077
mg/Kg - dry
132-64-9
Dibenzofuran
ND
0.016
0.197
mg/Kg - dry
95-50-1
1,2-Dichlorobenzene
ND
0.010
0.197
mg/Kg - dry
541-73-1
1,3-Dichlorobenzene
ND
0.010
0.197
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 41 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 20:16:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
106-46-7
1,4-Dichlorobenzene
ND
0.011
0.197
mg/Kg - dry
91-94-1
3,3'-Dichlorobenzidine
ND
0.128
0.384
mg/Kg - dry
120-83-2
2,4-Dichlorophenol
ND
0.017
0.197
mg/Kg - dry
87-65-0
2,6-Dichlorophenol
ND
0.015
0.197
mg/Kg - dry
84-66-2
Diethyl phthalate
ND
0.012
0.197
mg/Kg - dry
131-11-3
Dimethyl phthalate
ND
0.016
0.197
mg/Kg - dry
119-93-7
3,3' Dimethylbenzidine
ND M
0.041
0.384
mg/Kg - dry
105-67-9
2,4-Dimethyl phenol
ND
0.025
0.197
mg/Kg - dry
84-74-2
Di-n-butyl phthalate
ND
0.016
0.197
mg/Kg - dry
534-52-1
4,6-Dinitro-2-methyl phenol
ND
0.010
0.384
mg/Kg - dry
51-28-5
2,4-Dinitrophenol
ND
0.011
0.384
mg/Kg - dry
121-14-2
2,4-Dinitrotoluene
ND
0.012
0.197
mg/Kg - dry
606-20-2
2,6-Dinitrotoluene
ND
0.013
0.197
mg/Kg - dry
117-84-0
Di-n-Octyl Phthalate
ND
0.025
0.197
mg/Kg - dry
206-44-0
Fluoranthene
ND
0.011
0.077
mg/Kg - dry
86-73-7
Fluorene
ND
0.018
0.077
mg/Kg - dry
118-74-1
Hexachlorobenzene
ND
0.012
0.197
mg/Kg - dry
87-68-3
Hexachlorobutadiene
ND
0.011
0.197
mg/Kg - dry
77-47-4
Hexachlorocyclopentadiene
ND
0.016
0.197
mg/Kg - dry
67-72-1
Hexachloroethane
ND
0.012
0.197
mg/Kg - dry
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.020
0.077
mg/Kg - dry
78-59-1
Isophorone
ND
0.013
0.197
mg/Kg - dry
91-57-6
2-Methyl naphthalene
ND
0.011
0.077
mg/Kg - dry
95-48-7
2-Methylphenol
ND
0.017
0.197
mg/Kg - dry
108-39-4
3&4 Methylphenol
ND
0.016
0.197
mg/Kg - dry
91-20-3
Naphthalene
ND
0.012
0.077
mg/Kg - dry
88-74-4
2-Nitroaniline
ND
0.019
0.197
mg/Kg - dry
Qualifiers/
Outside QC limit
J
Estimated value
Definitions
M Minimum value
MDL
Method Detection
Limit
MQL Method Quantitation Limit
ND
Not Detected
Page 42 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP_5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
SW-8270E
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 20:16:00
CGC
L422041
CAS#
Parameter
Result
MDL
MQL
Units
99-09-2
3-Nitroaniline
ND
0.011
0.384
mg/Kg - dry
100-01-6
4-Nitroaniline
ND
0.014
0.197
mg/Kg - dry
98-95-3
Nitrobenzene
ND
0.007
0.197
mg/Kg - dry
88-75-5
2-Nitrophenol
ND
0.019
0.197
mg/Kg - dry
100-02-7
4-Nitrophenol
ND
0.015
0.197
mg/Kg - dry
62-75-9
N-Nitrosodimethylamine
ND
0.006
0.197
mg/Kg - dry
86-30-6
N-Nitrosodiphenylamine
ND
0.014
0.384
mg/Kg - dry
55-18-5
N-Nitrosodiethylamine
ND
0.023
0.197
mg/Kg - dry
924-16-3
N-Nitroso-di-n-butylamine
ND
0.018
0.197
mg/Kg - dry
621-64-7
N-Nitroso-di-n-propylamine
ND
0.012
0.197
mg/Kg - dry
87-86-5
Pentachlorophenol
ND
0.021
0.384
mg/Kg - dry
85-01-8
Phenanthrene
ND
0.016
0.077
mg/Kg - dry
108-95-2
Phenol
ND
0.023
0.197
mg/Kg - dry
129-00-0
Pyrene
ND
0.014
0.077
mg/Kg - dry
110-86-1
Pyridine
ND
0.018
0.384
mg/Kg - dry
95-94-3
1,2,4,5-Tetrachlorobenzene
ND
0.010
0.197
mg/Kg - dry
58-90-2
2,3,4,6-Tetrachlorophenol
ND
0.018
0.197
mg/Kg - dry
120-82-1
1,2,4-Trichlorobenzene
ND
0.011
0.197
mg/Kg - dry
95-95-4
2,4,5-Trichlorophenol
ND
0.023
0.197
mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 43 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
C\A/_S277f1F
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/12/2019 10:26
L422038
3546
30.6 g
1
2/13/2019 20:16:00
CGC
L422041
CAS#
Parameter
88-06-2
2,4,6-Trichlorophenol
CAS#
Surrogate
321-60-8
2-Fluorobiphenyl
367-12-4
2-Fluorophenol
4165-60-0
Nitrobenzene-d5
13127-88-3
Phenol-d6
1718-51-0
4-Terphenyl-d14
118-79-6
2,4,6-Tribromophenol
Result MDL MQL Units
ND 0.017 0.197 mg/Kg - dry
Recovery
Rec. Limits
22.5
20-79%
20.3
10-85%
22.0
22-72%
23.1
10-96%
31.5
22-104%
25.3
10-112%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.6 g
1
2/16/2019 04:59:18
MMK
L421893
CAS#
Parameter
C11-C22
Aromatic C11-C22
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
MA�Du
Result MDL MQL Units
ND 2.37 9.90 mg/Kg - dry
Recovery Rec. Limits
56.3 40-140%
46.1 40-140%
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.6 g
1
2/16/2019 10:00:02
MMK
L421893
CAS# Parameter Result MDL MQL Units
C19-C36 Aliphatic C19-C36 ND 2.22 4.66 mg/Kg - dry
Qualifiers/ Outside QC limit J Estimated value
Definitions M Minimum value MDL Method Detection Limit
MQL Method Quantitation Limit ND Not Detected
Page 44 of 76

Waypoint.M
ANALYTICAL
Project ID: 15-4389-0-0001
Project 830 Dolly St,
Information: Concord, NC
Proj #: 15-4389-0-0001
PM ENVIRONMENTAL, INC.
Ms. Maryse Speckner
333 Troy Circle, Suite M
Knoxville, TN 37919
Report Number: 19-042-0252
Report Date: 2/19/2019
Sample Results
TP-5 Date Collected
02/08/2019 14:00
WPA Lab No
93060
Date Received
02/09/2019
Matrix
Solids
nn A gnu
Prep Date
Prep Batch
Prep Method
Sample
Dilution
Analysis Date
By
Analytical Batch
02/14/2019 09:29
L421390
MAEPH (Soil)
30.6 g
1
2/16/2019 10:00:02
MMK
L421893
CAS#
Parameter
C9-C18
Aliphatic C9-C18
CAS#
Surrogate
3386-33-2
Chlorooctadecane
84-15-1
o-Terphenyl
CIA1_r'%Dv1A1T
Result MDL MQL Units
ND 1.78 3.49 mg/Kg - dry
Recovery Rec. Limits
56.3 40-140%
46.1 40-140%
Prep Date
Prep Batch
Prep Method
Dilution
Analysis Date
By
Analytical Batch
NA
NA
NA
1
2/15/201917:05:00
RXC
L421696
CAS# Parameter Result MQL Units
Moisture % Moisture 14.1 %
Qualifiers/ Outside QC limit
Definitions M Minimum value
MQL Method Quantitation Limit
J Estimated value
MDL Method Detection Limit
ND Not Detected
Page 45 of 76

Case Narrative
PRISM
.. LABORATORIES, INC.
Waypoint Analytical, LLC
Ashley Morris
2790 Whitten Road
Memphis, TN 38133
NC Certification No. 402
Full -Service Analytical & NC Drinking Water Cert No. 37735
Environmental Solutions SC Certification No. 99012
Project: 19-042-0252
Lab Submittal Date: 02/13/2019
Prism Work Order: 9020200
02/18/2019
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a,j
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
Reviewed By Terri W. Cole For Angela D. Overcash
Project Manager
A Analysis performed at Waypoint Analytical.
Aa Result < 1/2 RL. No further action taken.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 11
Page 46 of 76

Sample Receipt Summary
S
Full -Service Analytical &
/rP R I M
Environmental Solutions
02/18/2019
LABORATORIES INC.
Prism Work Order: 9020200
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
TP-1
9020200-01
Solid
02/08/19 13:00 02/13/19 10:00
TP-2
9020200-02
Solid
02/08/19 13:15 02/13/19 10:00
TP-3
9020200-03
Solid
02/08/19 13:30 02/13/19 10:00
TP-4
9020200-04
Solid
02/08/19 13:45 02/13/19 10:00
TP-5
9020200-05
Solid
02/08/19 14:00 02/13/19 10:00
Samples were received in good condition at 3.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 11
Page 47 of 76

�P R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Prism ID Client ID
There were no detections reported.
Parameter
Summary of Detections
Method
02/18/2019
Prism Work Order: 9020200
Result
Units
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 48 of 76
Page 3 of 11

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Waypoint Analytical, LLC Project: 19-042-0252
Attn: Ashley Morris
2790 Whitten Road
Memphis, TN 38133 Sample Matrix: Solid
Laboratory Report
02/18/2019
Client Sample ID: TP-1
Prism Sample ID: 9020200-01
Prism Work Order: 9020200
Time Collected: 02/08/19 13:00
Time Submitted: 02/13/19 10:00
Parameter
Result
Units
Report MDL Dilution
Method Analysis Analyst
Batch
Limit Factor
Date/Time
ID
General Chemistry Parameters
% Solids
82.3 A
% by
0.100 0.100 1
SM2540 G 2115/19 16:43
ADO
P9130308
Weight
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
18 0.58 100
MADEP VPH 2/14/19 15:39
TBL
P9130242
C9-Cl2 Aliphatics
BRL
mg/kg dry
18 0.94 100
MADEP VPH 2/14/19 15:39
TBL
P9130242
C9-Cl0 Aromatics
BRL
mg/kg dry
18 0.20 100
MADEP VPH 2/14/19 15:39
TBL
P9130242
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
107 %
70-130
2,5-Dibromotoluene (FID)
110 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 11
Page 49 of 76

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Waypoint Analytical, LLC Project: 19-042-0252
Attn: Ashley Morris
2790 Whitten Road
Memphis, TN 38133 Sample Matrix: Solid
Laboratory Report
02/18/2019
Client Sample ID: TP-2
Prism Sample ID: 9020200-02
Prism Work Order: 9020200
Time Collected: 02/08/19 13:15
Time Submitted: 02/13/19 10:00
Parameter
Result
Units
Report MDL Dilution
Method Analysis Analyst
Batch
Limit Factor
Date/Time
ID
General Chemistry Parameters
% Solids
75.6 A
% by
0.100 0.100 1
SM2540 G 2115/19 16:43
ADO
P9130308
Weight
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
17 0.56 100
MADEP VPH 2/14/19 16:07
TBL
P9130242
C9-Cl2 Aliphatics
BRL
mg/kg dry
17 0.90 100
MADEP VPH 2/14/19 16:07
TBL
P9130242
C9-Cl0 Aromatics
BRL
mg/kg dry
17 0.19 100
MADEP VPH 2/14/19 16:07
TBL
P9130242
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
108 %
70-130
2,5-Dibromotoluene (FID)
112 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 11
Page 50 of 76

PR I S M Fun -Service Analytical Environmental Solutions
LABORATORIES INC.
Waypoint Analytical, LLC Project: 19-042-0252
Attn: Ashley Morris
2790 Whitten Road
Memphis, TN 38133 Sample Matrix: Solid
Laboratory Report
02/18/2019
Client Sample ID: TP-3
Prism Sample ID: 9020200-03
Prism Work Order: 9020200
Time Collected: 02/08/19 13:30
Time Submitted: 02/13/19 10:00
Parameter
Result
Units
Report MDL Dilution
Method Analysis
Analyst
Batch
Limit Factor
Date/Time
ID
General Chemistry Parameters
% Solids
86.7 A
% by
0.100 0.100 1
SM2540 G 2115/19 17:05
ADO
P9130308
Weight
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
14 0.47 100
MADEP VPH 2/14/19 17:03
TBL
P9130242
C9-Cl2 Aliphatics
BRL
mg/kg dry
14 0.76 100
MADEP VPH 2/14/19 17:03
TBL
P9130242
C9-Cl0 Aromatics
BRL
mg/kg dry
14 0.16 100
MADEP VPH 2/14/19 17:03
TBL
P9130242
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
103 %
70-130
2,5-Dibromotoluene (FID)
106 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 11
Page 51 of 76

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Waypoint Analytical, LLC Project: 19-042-0252
Attn: Ashley Morris
2790 Whitten Road
Memphis, TN 38133 Sample Matrix: Solid
Laboratory Report
02/18/2019
Client Sample ID: TP-4
Prism Sample ID: 9020200-04
Prism Work Order: 9020200
Time Collected: 02/08/19 13:45
Time Submitted: 02/13/19 10:00
Parameter
Result
Units
Report MDL Dilution
Method Analysis Analyst
Batch
Limit Factor
Date/Time
ID
General Chemistry Parameters
% Solids
86.7 A
% by
0.100 0.100 1
SM2540 G 2115/19 17:05
ADO
P9130308
Weight
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
17 0.55 100
MADEP VPH 2/14/19 16:35
TBL
P9130242
C9-Cl2 Aliphatics
BRL
mg/kg dry
17 0.89 100
MADEP VPH 2/14/19 16:35
TBL
P9130242
C9-Cl0 Aromatics
BRL
mg/kg dry
17 0.19 100
MADEP VPH 2/14/19 16:35
TBL
P9130242
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
111 %
70-130
2,5-Dibromotoluene (FID)
114 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 11
Page 52 of 76

PR I S M Fun -Service Analytical Environmental Solutions
LABORATORIES INC.
Waypoint Analytical, LLC Project: 19-042-0252
Attn: Ashley Morris
2790 Whitten Road
Memphis, TN 38133 Sample Matrix: Solid
Laboratory Report
02/18/2019
Client Sample ID: TP-5
Prism Sample ID: 9020200-05
Prism Work Order: 9020200
Time Collected: 02/08/19 14:00
Time Submitted: 02/13/19 10:00
Parameter
Result
Units
Report MDL Dilution
Method Analysis
Analyst
Batch
Limit Factor
Date/Time
ID
General Chemistry Parameters
% Solids
85.9 A
% by
0.100 0.100 1
SM2540 G 2115/19 17:05
ADO
P9130308
Weight
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
16 0.50 100
MADEP VPH 2/14/19 15:10
TBL
P9130242
C9-Cl2 Aliphatics
BRL
mg/kg dry
16 0.81 100
MADEP VPH 2/14/19 15:10
TBL
P9130242
C9-Cl0 Aromatics
BRL
mg/kg dry
16 0.17 100
MADEP VPH 2/14/19 15:10
TBL
P9130242
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
115 %
70-130
2,5-Dibromotoluene (FID)
118 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 11
Page 53 of 76

/r Full -Service Analytical s
P R I IS M
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
2/18/19
Waypoint Analytical, LLC Project: 19-042-0252 Prism Work Order: 9020200
Attn: Ashley Morris Time Submitted: 2/13/2019 10:00:OOAM
2790 Whitten Road
Memphis, TN 38133
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9BO242 - MADEP VPH (S)
Blank (P9B0242-BLK1)
Prepared & Analyzed: 02/14/19
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl2 Aliphatics
2.26
5.0
mg/kg wet
Aa, J
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
10500
ug/L
10000 105
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10900
ug/L
10000 109
70-130
LCS (P9130242-13S7)
Prepared & Analyzed: 02/14/19
C5-C8 Aliphatics
38.3
5.0
mg/kg wet
32.00 120
70-130
C9-Cl0 Aromatics
11.3
5.0
mg/kg wet
10.67 106
70-130
C9-Cl2 Aliphatic
35.5
5.0
mg/kg wet
32.00 ill
70-130
Surrogate: 2,5-Dibromotoluene (PID)
10400
ug/L
10000 104
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10700
ug/L
10000 107
70-130
LCS Dup (P9B0242-BSD1)
Prepared & Analyzed: 02/14/19
C5-C8 Aliphatics
38.7
5.0
mg/kg wet
32.00 121
70-130 1 50
C9-Cl0 Aromatics
11.3
5.0
mg/kg wet
10.67 106
70-130 0.1 50
C9-Cl2 Aliphatic
36.0
5.0
mg/kg wet
32.00 113
70-130 1 50
Surrogate: 2,5-Dibromotoluene (PID)
10000
ug/L
10000 100
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10600
ug/L
10000 106
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 11
Page 54 of 76

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Waypoint Analytical, LLC
Attn: Ashley Morris
2790 Whitten Road
Memphis, TN 38133
General Chemistry Parameters - Quality Control
Analyte
Project: 19-042-0252
Level II QC Report
2/18/19
Prism Work Order: 9020200
Time Submitted: 2/13/2019 10:00:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9130308 - Solids, Dry Weight
Duplicate (P9130308-DUP1) Source: 9020200-01 Prepared: 02/18/19 Analyzed: 02/15/19
% Solids Complete 0.100 % by Weight 82.3 0 20 A
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch
Initial
Final
Date/Time
9020200-01 P9130308
30 g
30 g
02/18/19 14:21
9020200-02 P9130308
30 g
30 g
02/18/19 14:21
9020200-03 P9130308
30 g
30 g
02/18/19 14:21
9020200-04 P960308
30 g
30 g
02/18/19 14:21
9020200-05 P9130308
30 g
30 g
02/18/19 14:21
Prep Method: MADEP VPH (S)
Lab Number Batch
Initial
Final
Date/Time
9020200-01
P9130242
5.05
g 16
mL
02/14/19
12:04
9020200-02
P960242
5.75
g 16
mL
02/14/19
12:04
9020200-03
P9130242
5.98
g 16
mL
02/14/19
12:04
9020200-04
P9130242
5.05
g 16
mL
02/14/19
12:04
9020200-05
P9130242
5.61
g 16
mL
02/14/19
12:04
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 11
Page 55 of 76

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Page 11 of 11

0
Waypoint. 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Quality Control Data
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Prep: L421188 QC Analytical Batch(es): L421403
QC Prep Batch Method: 3546 Analysis Method: 8015B DRO
Analysis Description: Total Petroleum Hydrocarbons - Extractable
Lab Reagent Blank LRB-1-421188 Matrix: SOL
Associated Lab Samples: 93060
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Diesel Range Organics (C10-C28) mg/Kg <1.09 1.09 3.33 02/13/19 18:07
OTP Surrogate (S) 02/13/19 18:07 94.4 50-150
Laboratory Control Sample LCS-1-421188
Spike LCS LCS %Rec % Rec
Parameter Units Conc. Result Limits
Diesel Range Organics (C10-C28) mg/Kg 33.3 17.4 52.2 50-150
OTP Surrogate (S) 73.3 50-150
Matrix Spike & Matrix Spike Duplicate L 93060-MS-1-421188 L 93060-MSD-L421188
MS Spike MSD MS Result MSD MS MSD %Rec Max
Parameter Units Result Conc. Spike Result %Rec %Rec Limits RPD RPD
Conc.
Diesel Range Organics (C10-C28) mg/Kg 1.17 32.6 33.1 18.3 23.6 56.1 71.2 50-150 25.2 30
OTP Surrogate (S) 67.7 73.1 50-150
Date: 02/19/2019 04:33 PM Page 1 of 18
Page 57 of 76

0 Waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Quality Control Data
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Prep: L421644
QC Analytical Batch(es): L421650
QC Prep Batch Method: 5035
Analysis Method:
8015C GRO
Analysis Description:
Total Petroleum Hydrocarbons - Volatile
Lab Reagent Blank
LRB-1-421644
Matrix: SOL
Associated Lab Samples: 93060
Blank MDL
MQL
Analyzed
%
% Rec
Parameter Units
Result
Recovery
Limits
Gasoline Range Organics (C6-C10) mg/Kg
<9.00 9.00
10.0
02/14/19 13:17
4-Bromochlorobenzene (S)
02/14/19 13:17
98.6
50-150
Laboratory Control Sample & LCSD
LCS-1-421644 LCSD-L421644
Spike
LCS LCSD
LCS LCSD
% Rec
Parameter Units
Conc.
Result Result
%Rec a/o Rec
Limits
RPD Max
RPD
Gasoline Range Organics (C6-CIO) mg/Kg
200
208 210
104 105
50-150
0.9 30
4-Bromochlorobenzene (S)
115 108
50-150
Date: 02/19/2019 04:33 PM Page 2 of 18
Page 58 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422031 QC Analytical Batch(es): L422037
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-L422031 Matrix: SOL
Associated Lab Samples: 93056, 93057, 93058, 93059, 93060
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acetone
mg/Kg
<0.0089
0.0089
0.0400
02/13/19 11:23
Acetonitrile
mg/Kg
<0.0421
0.0421
0.200
02/13/19 11:23
Acrolein
mg/Kg
<0.0024
0.0024
0.0400
02/13/19 11:23
Acrylonitrile
mg/Kg
<0.0041
0.0041
0.0400
02/13/19 11:23
Benzene
mg/Kg
<0.0016
0.0016
0.0020
02/13/19 11:23
Bromobenzene
mg/Kg
<0.0009
0.0009
0.0020
02/13/19 11:23
Bromochloromethane
mg/Kg
<0.0015
0.0015
0.0020
02/13/19 11:23
Bromodichloromethane
mg/Kg
<0.0009
0.0009
0.0020
02/13/19 11:23
Bromoform
mg/Kg
<0.0018
0.0018
0.0020
02/13/19 11:23
Bromomethane
mg/Kg
<0.0006
0.0006
0.0020
02/13/19 11:23
Methyl Ethyl Ketone (MEK)
mg/Kg
<0.0052
0.0052
0.0400
02/13/19 11:23
n-Butylbenzene
mg/Kg
<0.0018
0.0018
0.0020
02/13/19 11:23
sec -Butyl benzene
mg/Kg
<0.0013
0.0013
0.0020
02/13/19 11:23
tert-Butyl benzene
mg/Kg
<0.0011
0.0011
0.0020
02/13/19 11:23
Carbon Disulfide
mg/Kg
<0.0008
0.0008
0.0020
02/13/19 11:23
Carbon Tetrachloride
mg/Kg
<0.0013
0.0013
0.0020
02/13/19 11:23
Chlorobenzene
mg/Kg
<0.0011
0.0011
0.0020
02/13/19 11:23
Chlorodibromomethane
mg/Kg
<0.0014
0.0014
0.0020
02/13/19 11:23
Chloroethane
mg/Kg
<0.0017
0.0017
0.0020
02/13/19 11:23
Chloroform
mg/Kg
<0.0018
0.0018
0.0020
02/13/19 11:23
Chloromethane
mg/Kg
<0.0013
0.0013
0.0020
02/13/19 11:23
2-Chlorotoluene
mg/Kg
<0.0018
0.0018
0.0020
02/13/19 11:23
4-Chlorotoluene
mg/Kg
<0.0013
0.0013
0.0020
02/13/19 11:23
1,2-Dibromo-3-Chloropropane
mg/Kg
<0.0063
0.0063
0.0100
02/13/19 11:23
1,2-Dibromoethane
mg/Kg
<0.0013
0.0013
0.0020
02/13/19 11:23
Dibromomethane
mg/Kg
<0.0015
0.0015
0.0020
02/13/19 11:23
1,2-Dichlorobenzene
mg/Kg
<0.0019
0.0019
0.0020
02/13/19 11:23
Date: 02/19/2019 04:33 PM Page 3 of 18
Page 59 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422031 QC Analytical Batch(es): L422037
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-L422031 Matrix: SOL
Associated Lab Samples: 93056, 93057, 93058, 93059, 93060
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
1,3-Dichlorobenzene
mg/Kg
<0.0014
0.0014
0.0020
02/13/19 11:23
1,4-Dichlorobenzene
mg/Kg
<0.0018
0.0018
0.0020
02/13/19 11:23
Dichlorodifluoromethane
mg/Kg
<0.0018
0.0018
0.0020
02/13/19 11:23
1,1-Dichloroethane
mg/Kg
<0.0010
0.0010
0.0020
02/13/19 11:23
1,2-Dichloroethane
mg/Kg
<0.0017
0.0017
0.0020
02/13/19 11:23
1,1-Dichloroethene
mg/Kg
<0.0009
0.0009
0.0020
02/13/19 11:23
cis-1,2-Dichloroethene
mg/Kg
<0.0007
0.0007
0.0020
02/13/19 11:23
trans-1,2-Dichloroethene
mg/Kg
<0.0010
0.0010
0.0020
02/13/19 11:23
1,2-Dichloropropane
mg/Kg
<0.0009
0.0009
0.0020
02/13/19 11:23
1,3-Dichloropropane
mg/Kg
<0.0016
0.0016
0.0020
02/13/19 11:23
2,2-Dichloropropane
mg/Kg
<0.0009
0.0009
0.0020
02/13/19 11:23
1,1-Dichloropropene
mg/Kg
<0.0006
0.0006
0.0020
02/13/19 11:23
cis-1,3-Dichloropropene
mg/Kg
<0.0008
0.0008
0.0020
02/13/19 11:23
trans-1,3-Dichloropropene
mg/Kg
<0.0009
0.0009
0.0020
02/13/19 11:23
Ethyl Acetate
mg/Kg
<0.0042
0.0042
0.0400
02/13/19 11:23
Ethylbenzene
mg/Kg
<0.0015
0.0015
0.0020
02/13/19 11:23
Hexachlorobutadiene
mg/Kg
<0.0014
0.0014
0.0020
02/13/19 11:23
2-Hexanone
mg/Kg
<0.0023
0.0023
0.0100
02/13/19 11:23
Iodomethane
mg/Kg
<0.0054
0.0054
0.0100
02/13/19 11:23
Isopropyl benzene
mg/Kg
<0.0015
0.0015
0.0020
02/13/19 11:23
4-Isopropyl toluene
mg/Kg
<0.0015
0.0015
0.0020
02/13/19 11:23
Methyl tert-butyl ether (MTBE)
mg/Kg
<0.0005
0.0005
0.0020
02/13/19 11:23
4-Methyl-2-Pentanone
mg/Kg
<0.0034
0.0034
0.0100
02/13/19 11:23
Methylene Chloride
mg/Kg
<0.0095
0.0095
0.0100
02/13/19 11:23
Naphthalene
mg/Kg
<0.0037
0.0037
0.0100
02/13/19 11:23
n-Propyl acetate
mg/Kg
<0.0042
0.0042
0.0100
02/13/19 11:23
n-Propylbenzene
mg/Kg
<0.0014
0.0014
0.0020
02/13/19 11:23
Date: 02/19/2019 04:33 PM Page 4 of 18
Page 60 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Prep: L422031
QC Prep Batch Method: 5035
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank
Associated Lab Samples:
Parameter
LRB-L422031
93056, 93057, 93058, 93059, 93060
Blank MDL
Units Result
Styrene
mg/Kg
<0.0018
0.0018
1,1,1,2-Tetrachloroethane
mg/Kg
<0.0019
0.0019
1,1,2,2-Tetrachloroethane
mg/Kg
<0.0016
0.0016
Tetrachloroethene
mg/Kg
<0.0016
0.0016
Toluene
mg/Kg
<0.0028
0.0028
1,2,3-Trichlorobenzene
mg/Kg
<0.0015
0.0015
1,2,4-Trichlorobenzene
mg/Kg
<0.0017
0.0017
1,1,1-Trichloroethane
mg/Kg
<0.0009
0.0009
1,1,2-Trichloroethane
mg/Kg
<0.0017
0.0017
Trichloroethene
mg/Kg
<0.0011
0.0011
Trichlorofluoromethane
mg/Kg
<0.0009
0.0009
1,2,3-Trichloropropane
mg/Kg
<0.0016
0.0016
1,2,4-Trimethyl benzene
mg/Kg
<0.0011
0.0011
1,3,5-Trimethyl benzene
mg/Kg
<0.0019
0.0019
Vinyl Acetate
mg/Kg
<0.0085
0.0085
Vinyl Chloride
mg/Kg
<0.0011
0.0011
o-Xylene
mg/Kg
<0.0013
0.0013
m,p-Xylene
mg/Kg
<0.0027
0.0027
4-Bromofluorobenzene (S)
1,2-Dichloroethane - d4 (S)
Toluene-d8 (S)
QC Analytical Batch(es): L422037
Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Matrix: SOL
MQL Analyzed % % Rec
Recovery Limits
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0040
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0400
02/13/19
11:23
0.0020
02/13/19
11:23
0.0020
02/13/19
11:23
0.0040
02/13/19
11:23
02/13/19
11:23 131 60-140
02/13/19
11:23 122 60-140
02/13/19
11:23 112 60-140
Laboratory Control Sample & LCSD LCS-L422031 LCSD-L422031
Spike
Parameter Units Conc.
Acetone mg/Kg 0.100
LCS
LCSD
LCS
LCSD
% Rec
Result
Result
%Rec
% Rec
Limits
0.0925
0.112
92.5
112
60-140
RPD Max
RPD
19.0 20
Date: 02/19/2019 04:33 PM Page 5 of 18
Page 61 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422031 QC Analytical Batch(es): L422037
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-1-422031 LCSD-L422031
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
Acetonitrile
mg/Kg
1.00
0.900
0.966
90.0
96.6
60-140
7.0
20
Acrolein
mg/Kg
0.100
0.110
0.112
110
112
40-160
1.8
20
Acrylonitrile
mg/Kg
0.100
0.0866
0.0911
86.6
91.1
50-150
5.0
20
Benzene
mg/Kg
0.100
0.102
0.111
102
111
60-140
8.4
20
Bromobenzene
mg/Kg
0.100
0.114
0.0912
114
91.2
60-140
22.2*
20
Bromochloromethane
mg/Kg
0.100
0.106
0.122
106
122
60-140
14.0
20
Bromodichloromethane
mg/Kg
0.100
0.0999
0.114
99.9
114
60-140
13.1
20
Bromoform
mg/Kg
0.100
0.108
0.108
108
108
60-140
0.0
20
Bromomethane
mg/Kg
0.100
0.0744
0.0652
74.4
65.2
40-160
13.1
20
Methyl Ethyl Ketone (MEK)
mg/Kg
0.100
0.0907
0.0941
90.7
94.1
60-140
3.6
20
n-Butylbenzene
mg/Kg
0.100
0.112
0.113
112
113
60-140
0.8
20
sec -Butyl benzene
mg/Kg
0.100
0.121
0.119
121
119
60-140
1.6
20
tert-Butyl benzene
mg/Kg
0.100
0.104
0.113
104
113
60-140
8.2
20
Carbon Disulfide
mg/Kg
0.100
0.0908
0.102
90.8
102
40-140
11.6
20
Carbon Tetrachloride
mg/Kg
0.100
0.108
0.120
108
120
60-140
10.5
20
Chlorobenzene
mg/Kg
0.100
0.110
0.104
110
104
60-140
5.6
20
Chlorodibromomethane
mg/Kg
0.100
0.0999
0.110
99.9
110
60-140
9.6
20
Chloroethane
mg/Kg
0.100
0.115
0.115
115
115
40-160
0.0
20
Chloroform
mg/Kg
0.100
0.0979
0.116
97.9
116
60-140
16.9
20
Chloromethane
mg/Kg
0.100
0.0796
0.0791
79.6
79.1
60-140
0.6
20
2-Chlorotoluene
mg/Kg
0.100
0.113
0.121
113
121
60-140
6.8
20
4-Chlorotoluene
mg/Kg
0.100
0.118
0.119
118
119
60-140
0.8
20
1,2-Dibromo-3-Chloropropane
mg/Kg
0.100
0.0980
0.0947
98.0
94.7
60-140
3.4
20
1,2-Dibromoethane
mg/Kg
0.100
0.101
0.106
101
106
60-140
4.8
20
Dibromomethane
mg/Kg
0.100
0.0988
0.111
98.8
111
60-140
11.6
20
1,2-Dichlorobenzene
mg/Kg
0.100
0.0941
0.0940
94.1
94.0
60-140
0.1
20
* QC Fail Date: 02/19/2019 04:33 PM Page 6 of 18
Page 62 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422031 QC Analytical Batch(es): L422037
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-1-422031 LCSD-L422031
Parameter
Units
Spike
Conc.
LCS
Result
LCSD
Result
LCS
%Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD
1,3-Dichlorobenzene
mg/Kg
0.100
0.110
0.118
110
118
60-140
7.0
20
1,4-Dichlorobenzene
mg/Kg
0.100
0.101
0.110
101
110
60-140
8.5
20
Dichlorodifluoromethane
mg/Kg
0.100
0.0604
0.0591
60.4
59.1
40-140
2.1
20
1,1-Dichloroethane
mg/Kg
0.100
0.103
0.116
103
116
60-140
11.8
20
1,2-Dichloroethane
mg/Kg
0.100
0.101
0.108
101
108
60-140
6.6
20
1,1-Dichloroethene
mg/Kg
0.100
0.102
0.117
102
117
60-140
13.6
20
cis-1,2-Dichloroethene
mg/Kg
0.100
0.105
0.118
105
118
60-140
11.6
20
trans-1,2-Dichloroethene
mg/Kg
0.100
0.0979
0.113
97.9
113
60-140
14.3
20
1,2-Dichloropropane
mg/Kg
0.100
0.0906
0.102
90.6
102
60-140
11.8
20
1,3-Dichloropropane
mg/Kg
0.100
0.103
0.115
103
115
60-140
11.0
20
2,2-Dichloropropane
mg/Kg
0.100
0.107
0.118
107
118
60-140
9.7
20
1,1-Dichloropropene
mg/Kg
0.100
0.111
0.120
111
120
60-140
7.7
20
cis-1,3-Dichloropropene
mg/Kg
0.100
0.0996
0.116
99.6
116
60-140
15.2
20
trans-1,3-Dichloropropene
mg/Kg
0.100
0.102
0.111
102
111
60-140
8.4
20
Ethyl Acetate
mg/Kg
0.100
0.126
0.140
126
140
60-140
10.5
20
Ethylbenzene
mg/Kg
0.100
0.104
0.109
104
109
60-140
4.6
20
Hexachlorobutadiene
mg/Kg
0.100
0.125
0.122
125
122
40-160
2.4
20
2-Hexanone
mg/Kg
0.100
0.0922
0.0958
92.2
95.8
60-140
3.8
20
Iodomethane
mg/Kg
0.100
0.0865
0.104
86.5
104
40-160
18.3
20
Isopropyl benzene
mg/Kg
0.100
0.110
0.109
110
109
60-140
0.9
20
4-Isopropyl toluene
mg/Kg
0.100
0.116
0.118
116
118
60-140
1.7
20
Methyl tert-butyl ether (MTBE)
mg/Kg
0.100
0.0951
0.108
95.1
108
60-140
12.7
20
4-Methyl-2-Pentanone
mg/Kg
0.100
0.0943
0.106
94.3
106
60-140
11.6
20
Methylene Chloride
mg/Kg
0.100
0.0857
0.0973
85.7
97.3
60-140
12.6
20
Naphthalene
mg/Kg
0.100
0.0996
0.0904
99.6
90.4
60-140
9.6
20
n-Propyl acetate
mg/Kg
0.100
0.107
0.111
107
111
40-160
3.6
20
Date: 02/19/2019 04:33 PM Page 7 of 18
Page 63 of 76

Waypointo
ANALYTICAL
Client ID:
Project Description:
Report No:
PM ENVIRONMENTAL, INC.
830 Dolly St,
19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422031 QC Analytical Batch(es): L422037
QC Prep Batch Method: 5035 Analysis Method: 8260D
Analysis Description: Volatile Organic Compounds - GC/MS
Laboratory Control Sample & LCSD LCS-1-422031 LCSD-L422031
Spike LCS LCSD LCS LCSD % Rec
Parameter Units Conc. Result Result %Rec % Rec Limits RPD
n-Propylbenzene
mg/Kg
0.100
0.107
0.120
107
120
60-140
11.4
Styrene
mg/Kg
0.100
0.116
0.106
116
106
60-140
9.0
1,1,1,2-Tetrachloroethane
mg/Kg
0.100
0.104
0.108
104
108
60-140
3.7
1,1,2,2-Tetrachloroethane
mg/Kg
0.100
0.102
0.0977
102
97.7
60-140
4.3
Tetrachloroethene
mg/Kg
0.100
0.109
0.130
109
130
60-140
17.5
Toluene
mg/Kg
0.100
0.0974
0.109
97.4
109
60-140
11.2
1,2,3-Trichlorobenzene
mg/Kg
0.100
0.128
0.126
128
126
60-140
1.5
1,2,4-Trichlorobenzene
mg/Kg
0.100
0.129
0.135
129
135
60-140
4.5
1,1,1-Trichloroethane
mg/Kg
0.100
0.103
0.118
103
118
60-140
13.5
1,1,2-Trichloroethane
mg/Kg
0.100
0.0957
0.107
95.7
107
60-140
11.1
Trichloroethene
mg/Kg
0.100
0.106
0.122
106
122
60-140
14.0
Trichlorofluoromethane
mg/Kg
0.100
0.119
0.112
119
112
60-140
6.0
1,2,3-Trichloropropane
mg/Kg
0.100
0.106
0.101
106
101
60-140
4.8
1,2,4-Trimethyl benzene
mg/Kg
0.100
0.117
0.116
117
116
60-140
0.8
1,3,5-Trimethylbenzene
mg/Kg
0.100
0.120
0.117
120
117
60-140
2.5
Vinyl Acetate
mg/Kg
0.100
0.112
0.124
112
124
40-160
10.1
Vinyl Chloride
mg/Kg
0.100
0.0866
0.0802
86.6
80.2
60-140
7.6
o-Xylene
mg/Kg
0.100
0.115
0.119
115
119
60-140
3.4
m,p-Xylene
mg/Kg
0.200
0.225
0.250
113
125
60-140
10.5
4-Bromofluorobenzene (S)
114
115
60-140
1,2-Dichloroethane - d4 (S)
109
124
60-140
Toluene-d8(S)
98.5
115
60-140
Max
RPD
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Date: 02/19/2019 04:33 PM Page 8 of 18
Page 64 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Prep: L422038
QC Prep Batch Method: 3546
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
Lab Reagent Blank LRB-L422038
Associated Lab Samples: 93056, 93057, 93058, 93059, 93060
QC Analytical Batch(es): L422041
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Matrix: SOL
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
Acenaphthene
mg/Kg
<0.010
0.010
0.066
02/13/19 13:34
Acenaphthylene
mg/Kg
<0.011
0.011
0.066
02/13/19 13:34
Acetophenone
mg/Kg
<0.015
0.015
0.170
02/13/19 13:34
Aniline
mg/Kg
<0.004
0.004
0.170
02/13/19 13:34
Anthracene
mg/Kg
<0.013
0.013
0.066
02/13/19 13:34
Benzidine
mg/Kg
<0.506
0.506
0.670
02/13/19 13:34
Benzo(a)anthracene
mg/Kg
<0.008
0.008
0.066
02/13/19 13:34
Benzo(a)pyrene
mg/Kg
<0.010
0.010
0.066
02/13/19 13:34
Benzo(b)fluoranthene
mg/Kg
<0.008
0.008
0.066
02/13/19 13:34
Benzo(g,h,i)perylene
mg/Kg
<0.013
0.013
0.066
02/13/19 13:34
Benzo(k)fluoranthene
mg/Kg
<0.011
0.011
0.066
02/13/19 13:34
Benzoic Acid
mg/Kg
<0.016
0.016
0.330
02/13/19 13:34
Benzyl alcohol
mg/Kg
<0.021
0.021
0.330
02/13/19 13:34
Bis(2-Chloroethoxy)methane
mg/Kg
<0.011
0.011
0.170
02/13/19 13:34
Bis(2-Chloroethyl)ether
mg/Kg
<0.006
0.006
0.170
02/13/19 13:34
Bis(2-Chloroisopropyl)ether
mg/Kg
<0.021
0.021
0.170
02/13/19 13:34
Bis(2-ethyl hexyl)phthalate
mg/Kg
<0.015
0.015
0.330
02/13/19 13:34
4-Bromophenyl phenyl ether
mg/Kg
<0.015
0.015
0.170
02/13/19 13:34
Butyl benzyl phthalate
mg/Kg
<0.017
0.017
0.170
02/13/19 13:34
Carbazole
mg/Kg
<0.009
0.009
0.170
02/13/19 13:34
4-Chloro-3-methylphenol
mg/Kg
<0.016
0.016
0.170
02/13/19 13:34
4-Chloroaniline
mg/Kg
<0.012
0.012
0.170
02/13/19 13:34
2-Chloronaphthalene
mg/Kg
<0.009
0.009
0.170
02/13/19 13:34
2-Chlorophenol
mg/Kg
<0.013
0.013
0.170
02/13/19 13:34
4-Chlorophenyl phenyl ether
mg/Kg
<0.011
0.011
0.170
02/13/19 13:34
Chrysene
mg/Kg
<0.011
0.011
0.066
02/13/19 13:34
Dibenz(a,h)anthracene
mg/Kg
0.011
0.011
0.066
02/13/19 13:34
Date:
02/19/2019 04:33 PM
Page 9 of 18
Page 65 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Prep: L422038
QC Prep Batch Method: 3546
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Analytical Batch(es): L422041
Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-L422038 Matrix: SOL
Associated Lab Samples: 93056, 93057, 93058, 93059, 93060
Parameter
Units
Blank
Result
MDL
MQL
Analyzed
Dibenzofuran
mg/Kg
<0.014
0.014
0.170
02/13/19 13:34
1,2-Dichlorobenzene
mg/Kg
<0.008
0.008
0.170
02/13/19 13:34
1,3-Dichlorobenzene
mg/Kg
<0.008
0.008
0.170
02/13/19 13:34
1,4-Dichlorobenzene
mg/Kg
<0.009
0.009
0.170
02/13/19 13:34
3,3'-Dichlorobenzidine
mg/Kg
<0.110
0.110
0.330
02/13/19 13:34
2,4-Dichlorophenol
mg/Kg
<0.015
0.015
0.170
02/13/19 13:34
2,6-Dichlorophenol
mg/Kg
<0.013
0.013
0.170
02/13/19 13:34
Diethyl phthalate
mg/Kg
<0.010
0.010
0.170
02/13/19 13:34
Dimethyl phthalate
mg/Kg
<0.014
0.014
0.170
02/13/19 13:34
3,3' Dimethylbenzidine
mg/Kg
<0.035
0.035
0.330
02/13/19 13:34
2,4-Dimethylphenol
mg/Kg
<0.021
0.021
0.170
02/13/19 13:34
Di-n-butyl phthalate
mg/Kg
<0.014
0.014
0.170
02/13/19 13:34
4,6- Din itro-2-methylphenol
mg/Kg
<0.008
0.008
0.330
02/13/19 13:34
2,4-Dinitrophenol
mg/Kg
<0.009
0.009
0.330
02/13/19 13:34
2,4-Dinitrotoluene
mg/Kg
<0.011
0.011
0.170
02/13/19 13:34
2,6-Dinitrotoluene
mg/Kg
<0.011
0.011
0.170
02/13/19 13:34
Di-n-Octyl Phthalate
mg/Kg
<0.022
0.022
0.170
02/13/19 13:34
Fluoranthene
mg/Kg
<0.010
0.010
0.066
02/13/19 13:34
Fluorene
mg/Kg
<0.015
0.015
0.066
02/13/19 13:34
Hexachlorobenzene
mg/Kg
<0.010
0.010
0.170
02/13/19 13:34
Hexachlorobutadiene
mg/Kg
<0.009
0.009
0.170
02/13/19 13:34
Hexachlorocyclopentadiene
mg/Kg
<0.014
0.014
0.170
02/13/19 13:34
Hexachloroethane
mg/Kg
<0.010
0.010
0.170
02/13/19 13:34
Indeno(1,2,3-cd)pyrene
mg/Kg
<0.017
0.017
0.066
02/13/19 13:34
Isophorone
mg/Kg
<0.011
0.011
0.170
02/13/19 13:34
2-Methylnaphthalene
mg/Kg
<0.009
0.009
0.066
02/13/19 13:34
2-Methylphenol
mg/Kg
<0.015
0.015
0.170
02/13/19 13:34
% % Rec
Recovery Limits
Date: 02/19/2019 04:33 PM
Page 66 of 76
Page 10 of 18

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422038 QC Analytical Batch(es): L422041
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-L422038 Matrix: SOL
Associated Lab Samples: 93056, 93057, 93058, 93059, 93060
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
3&4 Methylphenol
mg/Kg
<0.014
0.014
0.170
02/13/19 13:34
Naphthalene
mg/Kg
<0.010
0.010
0.066
02/13/19 13:34
2-Nitroaniline
mg/Kg
<0.017
0.017
0.170
02/13/19 13:34
3-Nitroaniline
mg/Kg
<0.009
0.009
0.330
02/13/19 13:34
4-Nitroaniline
mg/Kg
<0.012
0.012
0.170
02/13/19 13:34
Nitrobenzene
mg/Kg
<0.006
0.006
0.170
02/13/19 13:34
2-Nitrophenol
mg/Kg
<0.016
0.016
0.170
02/13/19 13:34
4-Nitrophenol
mg/Kg
<0.013
0.013
0.170
02/13/19 13:34
N-Nitrosodimethylamine
mg/Kg
<0.005
0.005
0.170
02/13/19 13:34
N-Nitrosodiphenylamine
mg/Kg
<0.012
0.012
0.330
02/13/19 13:34
N-Nitrosodiethylamine
mg/Kg
<0.020
0.020
0.170
02/13/19 13:34
N-Nitroso-di-n-butylamine
mg/Kg
<0.015
0.015
0.170
02/13/19 13:34
N-Nitroso-di-n-propylamine
mg/Kg
<0.010
0.010
0.170
02/13/19 13:34
Pentachlorophenol
mg/Kg
<0.018
0.018
0.330
02/13/19 13:34
Phenanthrene
mg/Kg
<0.013
0.013
0.066
02/13/19 13:34
Phenol
mg/Kg
<0.020
0.020
0.170
02/13/19 13:34
Pyrene
mg/Kg
<0.012
0.012
0.066
02/13/19 13:34
Pyridine
mg/Kg
<0.015
0.015
0.330
02/13/19 13:34
1,2,4,5-Tetrachlorobenzene
mg/Kg
<0.008
0.008
0.170
02/13/19 13:34
2,3,4,6-Tetrachlorophenol
mg/Kg
<0.015
0.015
0.170
02/13/19 13:34
1,2,4-Trichlorobenzene
mg/Kg
<0.010
0.010
0.170
02/13/19 13:34
2,4,5-Trichlorophenol
mg/Kg
<0.020
0.020
0.170
02/13/19 13:34
2,4,6-Trichlorophenol
mg/Kg
<0.014
0.014
0.170
02/13/19 13:34
2-Fluorobiphenyl (S)
02/13/19 13:34
2-Fluorophenol (S)
02/13/19 13:34
Nitrobenzene-d5 (S)
02/13/19 13:34
Phenol-d6 (S)
02/13/19 13:34
39.9
20-79
35.4
10-85
38.1
22-72
39.9
10-96
Date: 02/19/2019 04:33 PM
Page 67 of 76
Page 11 of 18

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422038 QC Analytical Batch(es): L422041
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Lab Reagent Blank LRB-L422038 Matrix: SOL
Associated Lab Samples: 93056, 93057, 93058, 93059, 93060
Blank MDL MQL Analyzed % % Rec
Parameter Units Result Recovery Limits
4-Terphenyl-d14 (S) 02/13/19 13:34 48.9 22-104
2,4,6-Tribromophenol(S) 02/13/19 13:34 45.6 10-112
Laboratory Control Sample LCS-L422038
Spike
Parameter Units Conc.
LCS LCS %Rec % Rec
Result Limits
Acenaphthene
mg/Kg
1.67
1.01
60.4
10-146
Acenaphthylene
mg/Kg
1.67
0.904
54.1
10-146
Acetophenone
mg/Kg
1.67
0.728
43.5
10-146
Aniline
mg/Kg
1.67
0.553
33.1
10-146
Anthracene
mg/Kg
1.67
1.03
61.6
10-146
Benzidine
mg/Kg
1.67
<0.506
0.0*
1-146
Benzo(a)anthracene
mg/Kg
1.67
1.01
60.4
10-146
Benzo(a)pyrene
mg/Kg
1.67
0.982
58.8
10-146
Benzo(b)fluoranthene
mg/Kg
1.67
1.08
64.6
10-146
Benzo(g,h,i)perylene
mg/Kg
1.67
0.880
52.6
10-146
Benzo(k)fluoranthene
mg/Kg
1.67
1.13
67.6
10-146
Benzoic Acid
mg/Kg
1.67
<0.016
0.0*
10-146
Benzyl alcohol
mg/Kg
1.67
0.862
51.6
10-146
Bis(2-Chloroethoxy)methane
mg/Kg
1.67
0.801
47.9
10-146
Bis(2-Chloroethyl)ether
mg/Kg
1.67
0.695
41.6
10-146
Bis(2-Chloroisopropyl)ether
mg/Kg
1.67
0.831
49.7
10-146
Bis(2-ethyl hexyl)phthalate
mg/Kg
1.67
0.972
58.2
10-146
4-Bromophenyl phenyl ether
mg/Kg
1.67
0.976
58.4
10-146
Butyl benzyl phthalate
mg/Kg
1.67
0.963
57.6
10-146
Carbazole
mg/Kg
1.67
0.973
58.2
10-146
4-Chloro-3-methylphenol
mg/Kg
1.67
0.967
57.9
10-146
* QC Fail Date: 02/19/2019 04:33 PM Page 12 of 18
Page 68 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422038 QC Analytical Batch(es): L422041
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-1-422038
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
4-Chloroaniline
mg/Kg
1.67
0.683
40.8
10-146
2-Chloronaphthalene
mg/Kg
1.67
0.812
48.6
10-146
2-Chlorophenol
mg/Kg
1.67
0.762
45.6
10-146
4-Chlorophenyl phenyl ether
mg/Kg
1.67
1.06
63.4
10-146
Chrysene
mg/Kg
1.67
1.02
61.0
10-146
Dibenz(a,h)anthracene
mg/Kg
1.67
0.940
56.2
10-146
Dibenzofuran
mg/Kg
1.67
0.946
56.6
10-146
1,2-Dichlorobenzene
mg/Kg
1.67
0.732
43.8
14-137
1,3-Dichlorobenzene
mg/Kg
1.67
0.709
42.4
14-134
1,4-Dichlorobenzene
mg/Kg
1.67
0.712
42.6
10-141
3,3'-Dichlorobenzidine
mg/Kg
1.67
0.609
36.4
10-146
2,4-Dichlorophenol
mg/Kg
1.67
0.624
37.3
10-146
2,6-Dichlorophenol
mg/Kg
1.67
0.992
59.4
10-146
Diethyl phthalate
mg/Kg
1.67
1.04
62.2
10-146
Dimethyl phthalate
mg/Kg
1.67
0.994
59.5
10-146
3,3' Dimethylbenzidine
mg/Kg
1.67
<0.035
0.0*
1-146
2,4-Dimethylphenol
mg/Kg
1.67
0.750
44.9
10-146
Di-n-butyl phthalate
mg/Kg
1.67
1.07
64.0
10-146
4,6- Din itro-2-methylphenol
mg/Kg
1.67
0.474
28.3
10-146
2,4-Dinitrophenol
mg/Kg
1.67
0.186
0.0*
10-146
2,4-Dinitrotoluene
mg/Kg
1.67
1.12
67.0
10-146
2,6-Dinitrotoluene
mg/Kg
1.67
0.951
56.9
10-146
Di-n-Octyl Phthalate
mg/Kg
1.67
1.09
65.2
10-146
Fluoranthene
mg/Kg
1.67
1.17
70.0
10-146
Fluorene
mg/Kg
1.67
1.00
59.8
10-146
Hexachlorobenzene
mg/Kg
1.67
0.874
52.3
10-146
Hexachlorobutadiene
mg/Kg
1.67
0.805
48.2
33-151
* QC Fail Date: 02/19/2019 04:33 PM Page 13 of 18
Page 69 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
QC Prep: L422038 QC Analytical Batch(es): L422041
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-1-422038
Parameter
Units
Spike
Conc.
LCS
Result
LCS %Rec
% Rec
Limits
Hexachlorocyclopentadiene
mg/Kg
1.67
0.498
29.8
10-146
Hexachloroethane
mg/Kg
1.67
0.693
41.4
10-146
Indeno(1,2,3-cd)pyrene
mg/Kg
1.67
0.855
51.1
10-146
Isophorone
mg/Kg
1.67
0.573
34.3
10-146
2-Methylnaphthalene
mg/Kg
1.67
0.840
50.2
10-146
2-Methylphenol
mg/Kg
1.67
0.785
47.0
10-146
3&4 Methylphenol
mg/Kg
1.67
0.930
55.6
10-146
Naphthalene
mg/Kg
1.67
0.764
45.7
37-148
2-Nitroaniline
mg/Kg
1.67
0.945
56.5
10-146
3-Nitroaniline
mg/Kg
1.67
1.05
62.8
10-146
4-Nitroaniline
mg/Kg
1.67
1.59
95.2
10-146
Nitrobenzene
mg/Kg
1.67
0.825
49.4
10-146
2-Nitrophenol
mg/Kg
1.67
0.683
40.8
10-146
4-Nitrophenol
mg/Kg
1.67
0.959
57.4
10-146
N-Nitrosodimethylamine
mg/Kg
1.67
0.722
43.2
10-146
N-Nitrosodiphenylamine
mg/Kg
1.67
0.739
44.2
10-146
N-Nitrosodiethylamine
mg/Kg
1.67
0.768
45.9
10-146
N-Nitroso-di-n-butylamine
mg/Kg
1.67
1.02
61.0
10-146
N-Nitroso-di-n-propylamine
mg/Kg
1.67
0.830
49.7
10-146
Pentachlorophenol
mg/Kg
1.67
0.748
44.7
10-146
Phenanthrene
mg/Kg
1.67
0.979
58.6
10-146
Phenol
mg/Kg
1.67
0.817
48.9
10-146
Pyrene
mg/Kg
1.67
0.996
59.6
10-146
Pyridine
mg/Kg
1.67
0.444
26.5
10-146
1,2,4,5-Tetrachlorobenzene
mg/Kg
1.67
0.891
53.3
21-136
2,3,4,6-Tetrachlorophenol
mg/Kg
1.67
0.899
53.8
10-146
1,2,4-Trichlorobenzene
mg/Kg
1.67
0.801
47.9
10-146
Date: 02/19/2019 04:33 PM Page 14 of 18
Page 70 of 76

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Prep: L422038 QC Analytical Batch(es): L422041
QC Prep Batch Method: 3546 Analysis Method: 8270E
Analysis Description: Semivolatile Organic Compounds - GC/MS
Laboratory Control Sample LCS-L422038
Parameter
Spike
Units Conc.
LCS
Result
LCS %Rec
% Rec
Limits
2,4,5-Trichlorophenol
mg/Kg 1.67
0.885
52.9
10-146
2,4,6-Trichlorophenol
mg/Kg 1.67
0.877
52.5
10-146
2-Fluorobiphenyl (S)
39.6
20-79
2-Fluorophenol (S)
43.8
10-85
Nitrobenzene-d5 (S)
42.0
22-72
Phenol-d6 (S)
49.8
10-96
4-Terphenyl-d14 (S)
41.1
22-104
2,4,6-Tribromophenol (S)
42.0
10-112
Date: 02/19/2019 04:33 PM Page 15 of 18
Page 71 of 76

0 Waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Quality Control Data
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Prep:
L421390
QC Analytical Batch(es): L421893
QC Prep Batch Method:
MAEPH (Soil)
Analysis Method:
MAEPH
Analysis Description:
Massachussetts EPH
Lab Reagent Blank
LRB-L421390
Matrix: SOL
Associated Lab Samples:
93056, 93057, 93058, 93059, 93060
Blank MDL
MQL
Analyzed
%
% Rec
Parameter
Units
Result
Recovery
Limits
Chlorooctadecane (S)
02/16/19 05:32
66.4
40-140
OTP Surrogate (S)
02/16/19 00:32
66.0
40-140
Laboratory Control Sample
LCS-1-421390
Spike
LCS
LCS %Rec
% Rec
Parameter
Units
Conc.
Result
Limits
Aliphatic C19-06
mg/Kg
15.0
8.21
54.7
40-140
Aliphatic C9-C18
mg/Kg
10.0
4.91
49.1
40-140
Aromatic C11-C22
mg/Kg
25.0
16.8
67.2
40-140
Chlorooctadecane (S)
62.4
40-140
OTP Surrogate (S)
59.2
40-140
Matrix Spike & Matrix Spike Duplicate
L 93058-MS-L421390 L 93058-MSD-L421390
MS Spike
MSD MS Result
MSD MS
MSD
%Rec
Max
Parameter
Units
Result Conc.
Spike
Result %Rec
%Rec
Limits
RPD
RPD
Conc.
Aliphatic C19-06
mg/Kg
<1.91 9.80
10.0 4.74
5.75 48.3
57.5
40-140
19.2
25
Aliphatic C9-C18
mg/Kg
<1.53 6.54
6.67 2.90
2.79 0.0*
0.0*
40-140
0.0
25
Aromatic C11-C22
mg/Kg
<2.04 16.3
16.7 11.9
10.6 73.0
63.4
40-140
11.5
25
Chlorooctadecane (S)
40.4
57.7
40-140
OTP Surrogate (S)
62.5
56.6
40-140
* QC Fail
Date:
02/19/2019 04:33 PM
Page 16 of 18
Page 72 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Analytical Batch:
Analysis Method:
Analysis Description:
Duplicate
Parameter
% Moisture
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
L421695
SW-DRYWT
Dry Weight Determination
L 92910-DUP
Result DUP
Units Result
% 13.5 13.3
RPD Max RPD Analyzed
1.4 20.0 02/15/19 16:43
Date: 02/19/2019 04:33 PM Page 17 of 18
Page 73 of 76

Waypointo
ANALYTICAL
Client ID: PM ENVIRONMENTAL, INC.
Project Description: 830 Dolly St,
Report No: 19-042-0252
QC Analytical Batch:
Analysis Method:
Analysis Description:
Duplicate
Parameter
% Moisture
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Quality Control Data
L421696
SW-DRYWT
Dry Weight Determination
L 93058-DUP
Result DUP
Units Result
% 13.3 12.6
RPD Max RPD Analyzed
5.4 20.0 02/15/19 17:05
Date: 02/19/2019 04:33 PM Page 18 of 18
Page 74 of 76

0
2790 Whitten Road, Memphis,
Waypoint.
Main 901.213.2400 °Fax [phone].2440
ANALYTICAL www.waypointanalytical.com
Cooler Receipt Form
Customer Number: 24376
Customer Name: PM ENVIRONMENTAL, INC.
Report Number: 19-042-0252
Shipping Method
0 Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: 39
Shipping container/cooler uncompromised?
0 Yes
0 No
Number of coolers received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Required
Custody seals intact on sample bottles?
0 Yes
0 No
Not Required
Chain of Custody (COC) present?
0 Yes
0 No
COC agrees with sample label(s)?
0 Yes
0 No
COC properly completed
0 Yes
0 No
Samples in proper containers?
0 Yes
0 No
Sample containers intact?
® Yes
0 No
Sufficient sample volume for indicated test(s)?
0 Yes
0 No
All samples received within holding time?
0 Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F High concentration container (48 hr) F_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) ✓ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
Comments: F
0 Yes
0 No
Signature: ory Phillips Date & Time: 02/11/2019 12:00:46
Page 75 of 76

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Page 76 of 76

Appendix D
Environmental
OPM & Engineering
ENVIRONMENTAL Services

PARPhotographs
from Permanent UST Closure Activities
PM Project No. 15-4389-0-0001
ENVIRONMENTAL
Location: 830 Dolly Street NW, Concord, NC
Photograph 1
View of the subject property depicting location
'
of UST basin and dispenser shed.
t.
Photograph 2
k
View of the UST fill port adjacent to the shed.

P Photographs from Permanent UST Closure Activities
PM Project No. 15-4389-0-0001
ENVIRONMENTAL Location: 830 Dolly Street NW, Concord, NC
Photograph 3
Photograph 4
View of the UST being exposed.
View of UST being uncovered.

P
Photographs from Permanent UST Closure Activities
0PM
Project No. 15-4389-0-0001
ENVIRONMENTAL
Location: 830 Dolly Street NW, Concord, NC
Photograph 5
sl
j
View of excavated UST.
r
Y
Photograph 6
I:
a
t —
View of excavation following removal of UST.

4010IN
PM
Photographs from Permanent UST Closure Activities
PM Project No. 15-4389-0-0001
ENVIRONMENTAL
Location: 830 Dolly Street NW, Concord, NC
Photograph 7
t� 1
View of UST prior to loading on flatbed truck for
transportation.
...
Photograph 8
_
View of former UST basin following backfilling
and site restoration activities.

UST=3 Notice of Intent: UST Permanent Closure or Change -in -Service
Return completed form to:
STATE Use ONLY
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
I.D. #
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES,
Date Received
INSTRUCTIONS (READ THIS FIRST)
Complete and return at least thirty (30) days prior to closure or change -in-service activities. If a Professional Engineer (P.E.) or a Licensed Geologist (L.G.)
provides supervision for closure or change -in-service site assessment activities and signs and seals all closure reports then at least a five (5) working
days notice is acceptable.
Completed UST closure or change -in-service site assessment reports, along with a copy of the UST-2 form, should be submitted to the appropriate Division
of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form should also be submitted to the Central
Office in Raleigh so that the status of the tanks may be changed to permanently closed and your tank fee account can be closed out. Note: Tank fees may
be due on unregistered tanks.
UST closure and change -in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response. The guidelines can be obtained at http://www.wastenotnc.org/. Note: To close tanks in place you must obtain prior approval
from the DWM Regional office located in the region where the facility is located.
You must make sure that LISTS removed from your property are disposed of properly. When choosing a closure contractor, ask where the tank(s) will be
taken for disposal. Usually, LISTS are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS
11. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
Facility Name or Companyy
Mr. Lonq Hu nh
Graham Construction Co
Street Address
Facility ID # (If known)
5868 Crimson Oak Court
00-0-0000025325
City County
Street Address
Harrisburg Cabarrus
830 Dolly Street NW
State Zip Code
City County Zi Code
NC 28075
Concord Cabarrus 28g27
Phone Number
Email
Phone Number
[phone]
lanile naliamc mail.com
III. CONTACT PERSONNEL
Name:
Company Name:
Job Title:
Phone Number:
Mr. Long Hu nh I
Owner
[phone]
IV, TANK REMOVAL, CLOSURE IN PLACE, CHANGE -IN SERVICE
1. Contact local fire marshal. 5. Provide a sketch locating piping, tanks and a P.E. or L.G., with all closure site
2. Plan entire closure event, soil sampling locations. assessment reports bearing the signature
3. Conduct Site Soil Assessment. 6. Submit a closure report in the format of and seal of the P.E. or L.G. If a release has
UST-12 (including the form UST-2) within not occurred, the supervision, signature or
4. If removing tanks or closing in place, refer to thirty (30) days following the site seal of a P.E. or L.G. is not required.
API Publication 2015 Cleaning Petroleum investigation. 8. Keep closure records for three (3) years.
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum 7.If a release from the tanks has occurred, the
Storage Tanks. site assessment portion of the tank closure
must be conducted under the supervision of
V. WORK TO BE PERFORMED BY
Contractor Name:
Contractor Company Name:
Steve Risch
Elite Environmental Services
Address:
State:
Zip Code:
Phone No:
322 Clarendon Estates Dr., Clover
SC
29710
[phone]
Primary Consultant Name:
Primary Consultant Company Name:
Consultant Phone No:
Maryse Speckner
PM Environmental, Inc.
[phone]
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE -IN-SERVICE
Proposed Activit
Closure
Change -in -Service
Tank ID No.
Size in Gallons
Last Contents
Removal
Abandonment in Place
New Contents Stored
001
2000
gasoline
■❑
❑
❑
❑
Li
* Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII. OWNER OR OWNER'S AUTHORIZED REPRESENTATIVE
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title: Maryse Speckner / Sr. Project Consultant
Signature
D to Signed i
SCHEDULED REMOVAL DATE
Notify your DWM Regional Office
1 q
2/8/2019
48 hours before this date if
date
scheduled removal changes
UST-3 Rev 1/2019

U ST'2A
Site Investigation Report
for Permanent Closure or
Change -IN
in -
KC
REGISTERED
Service of
UST
`"'VQ"r °' „o
Return completed form to:
NC DEQ / DWM / UST SECTION
STATE USE ONLY:
Facility ID #
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING
Date Received
phone [phone] fax [phone] http://www.wastenotnc.orq/
INSTRUCTIONS
READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can
be obtained at http://deg.nc.goy/about/divisions/waste-management/waste-
management-permit-guidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change -in-service: Where a UST system will be converted from storing
III, IV, and VI
a regulated substance to a non -regulated substance, complete sections I, Il,
4. For more than 5 registered UST systems, attach additional forms as
needed
5. Tank Fee Refund: An annual tank fee may be refunded for a tank for which a tank fee was not required. An owner or operator must submit
a written request and include: (1) contact information, (2) federal identification # or SSN, and (3) a
copy of UST-2 form. The annual tank
fee will be prorated based on the date of permanent closure.
6. UNREGISTERED USTs use Form UST-26
I. OWNERSHIP OF TANKS
II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
Facility Name or Company
Mr. Long Hu nh
Graham Construction Co. Inc
Street Address
Facility ID # (If known)
5868 Crimson Oak Ct,
00-0-0000025325
City County
Street Address
Harrisburg Cabarrus
830 Dolly Street NW
State Zip Code
City
County Zip Code
NC 28075
Concord
Cabarrus 28027
Phone Number
Phone Number
[phone]
III. CONTACT PERSONNEL
Contact for Facility:
Job Title:
Phone #:
Mr. Long Huynh
Owner
[phone]
Closure Contractor Name:
Closure Contractor Company:
Address:
Phone #
Steve Risch
Elite Environmental Services
Clover, SC
[phone]
Primary Consultant Name:
Primary Consultant Company:
Address:
Phone #
Ma se S eckner
PM Environmental, Inc.
Knoxville, TN
[phone]
IV. UST INFORMATION FOR REGISTERED UST SYSTEMS
V. EXCAVATION CONDITION
UNREGISTERED USTs use Form UST-213
Tank ID
No.
Size in
Gallons
Last
Contents
Last
Use
Date
Permanent
Close Date
Method of Permanent Closure:
Indicate REMOVED or enter fill
material, such as foam/
Change -in-
Service
Date
Water in
excavation
Free product
Notable
odor or
visible soil
contaminatio
concrete/ sand
n
Yes
No
Yes
No
Yes
No
001
2000
Gasoline,
unk
2/8/2019
REMOVED
NA
❑
®
❑
®
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar
with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining
the information, I believe that the
submitted information is true accurate
and complete.
Print name and official title of owner or owner's authorized representative
Maryse Speckner / Sr. Project Consultant
Signature
4 k
Date Signed
3/6/2019
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE (919)
707-8171 FAX [phone] httR.//www.wastenotnc.org/
1/2016

Beverly, Trudy
From: Maryse Speckner <[e-mail]>
Sent: Monday, April 1, 2019 11:29 AM
To: Beverly, Trudy
Subject: RE: [External] 830 Dolly Street NW, Concord, NC - FAC ID#00-0-0000025325
Permanent Closure Report
not click links or open attachments unless you verify. Send all suspicious email as an
[e-mail]
Very helpful. Thanks Trudy!
/41a7ee
Maryse D. Speckner I Senior Project Consultant
PM ENVIRONMENTAL, INC
p:865-329-7191 1 f:877-884-6775 1 c:865-323-1587 1 [e-mail]
From: Beverly, Trudy <[e-mail]>
Sent: Monday, April 1, 2019 11:16 AM
To: Maryse Speckner <[e-mail]>
Subject: RE: [External] 830 Dolly Street NW, Concord, NC - FAC ID#00-0-0000025325 Permanent Closure Report
Good Morning Maryse,
Thanks for touching base about the closure report. No worries, I'll be here to assist with questions. The UST
Section requires electronic and paper copies. Links to the policies are below.
Document Submittal St UST File Names for Laserfiche Policies:
httns:Hfiles.nc. izov/ncdea/Waste%2OMana,2ement/DWMIUST/Corrective%2OAction/Electronic%2ODocument%2OSubmittal
%20Memo%2OUpdate.pdf
https://files.nc. eov/ncdea/Waste%2OManaeement/DWMIUST/Corrective%2OAction/UST%20file%20names%20for%2OLas
erfiche.docx
Have a wonderful day,
Trudy
e:,e- DEc1le,
NORTH CAROLINA
Department of Environmental quality
Tl ,pL.
Noah Offohns Elopmunm uEEmiumumd Qudky
UST g[ 4 liounvik Rgaml O
(1"235,2182 (4
Tt W am
Finail cone spondenre. to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties,
Office Mailing Address:

610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: h!Ws:Hdeq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-mana,gement/ust/ast-
program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-mana e� ig's-maps
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https:Hedocs.deq.nc.aov/WasteManagement/Search.asp
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/Electronic%20Document%20Submittal
%20Memo%20Update.pdf
https:Hfiles.nc. gov/ncdeq/Waste%20Management/DWM/TJST/Corrective%20Action/LIST%20file%20names%20for%20Las
erfiche.docx
From: Maryse Speckner [mailto:[e-mail]]
Sent: Monday, April 1, 2019 10:55 AM
To: Beverly, Trudy <[e-mail]>
Subject: [External] 830 Dolly Street NW, Concord, NC - FAC ID#00-0-0000025325 Permanent Closure Report
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
achment to [e-mail]
Good morning Trudy,
This is Maryse Speckner with PM Environmental.
We spoke on the phone a couple months ago regarding this project. As I mentioned, Don Warren is no longer
with PM and I have been assigned this project.
I am not familiar with the 'ins & outs' of NCDENR, so I need a little guidance.
The UST closure activities were completed on 2/8/19 and the permanent closure report is attached along with
completed UST-2A and UST-3 forms.
Will the electronic copy be sufficient, or do we also need to send you a hard copy? If so, we will send one right
away.
The UST-2A and UST 3 forms have been mailed to the Central and Regional offices.
Thanks so much!
/lla,�-gse

Maryse D. Speckner I Senior Project Consultant
PM ENVIRONMENTAL, INC.
333 Troy Circle I Suite M I Knoxville, TN 37919 1 www.pmenv.com
p: 865-329-71911 f:877-884-6775 1 c:865-323-1587 1 [e-mail]
Environmental & Engineering Services Nationwide