1203_Burke_JohnsRiver_CDLF_GWBaseline_Permit_FID1323365_20190627

�R USE ONLY ❑Paper Report [:]Electronic Data - Email CD (data loaded: Yes / No) Doc/Event #:
IIII PP'NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Joyce Engineerin
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: G. Van Ness Burbach. Ph.D.. P.G.
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Johns River Feb. 21, 2018; May 16, 2018;
C&D Landfill Expansion 2500 Marsh Trail 12-03 .0500 Aug. 29, 2018; Dec. 5, 2018;
(Phase 1A) Morganton, NC Feb. 7, 2019.
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data
Surface water monitoring data ❑
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
G. Van Ness Burbach, Ph.D., PG Sr. Technical Consultant
Facili M
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Signatu e a
2211 W. Meadowview Rd., Ste. 101 Greensboro, NC 27407
Facility Representative Address
C-0782
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
[phone]
(Area Code) Telephone Number
Affix NC Licensed/ Professional Geologist Seal
40,
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June 27, 2019
Ms. Jackie Drummond
North Carolina Department of Environment and Natural Resources
Division of Waste Management, Solid Waste Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Via Email: [e-mail]
RE: Phase 1A Background Sampling Report
Burke County - Johns River Landfill, Permit No. 12-03
Project No. 2181871, Tasks No. 04
Dear Ms. Drummond:
On behalf of Burke County, La Bella Associates (LaBella - formerly known as Joyce Engineering)
presents this report on the background sampling of monitoring wells MW-23S, MW-24S, MW-30, and
MW-35 at the Johns River Waste Management Facility (Permit No. 12-03) in accordance with North
Carolina Solid Waste Management Regulations (NCSWMR). Background sampling events were
conducted in February, May, August, and December 2018. A North Carolina Environmental
Monitoring Reporting Form (EMRF) for the four sampling events is attached.
INTRODUCTION:
Burke County recently completed construction of Phase 2A and Phase 4 of the C&D landfill
expansion. In accordance with the approved Water Quality Monitoring Plan (WQMP) for the facility
(dated November 2018), there are four additional groundwater monitoring wells designated as
compliance wells for Phases 2A and 4: MW-23S, MW-24S, MW-30, and MW-35. An amendment to
the Phase 1A Permit to Operate, dated February 7, 2018, allowed construction of Phase 2A and
Phase 4; and a modification to the Phase 1A Permit to Operate, dated November 7, 2018, permitted
operation of Phases 2A and 4.
Monitoring well MW-30 was installed in 2015 during hydrogeologic investigations for the new cells
and is located southeast of Phase 4. Several PZs were converted to monitoring wells in February
2018 (see Well Installation and Abandonment Report dated March 16, 2018), including the
following: MW-35 (formerly PZ-35), located upgradient along the NW corner of proposed Phase 2A,
between the closed C&D-over-MSW landfill and Phase 2A; MW 23S (formerly PZ-16S), located SE of
MW-35, downgradient of the boundary between Phase 2A and Phase 4; and MW-24S (discussed
below). Well construction data for these wells are summarized in Table 1(Attachment 1). The well
locations are shown on the attached Drawing 1(Attachment 2) and the
According to the Water Quality Monitoring Plan for the facility, monitoring wells MW-24S and
MW-24D, were supposed to have been converted from piezometers PZ-8S and PZ-8D, respectively,
which were approximately 200 feet downgradient of Phase 4; however, PZ-8S and PZ-8D could not
2211 W. Meadowview Road #1o1 i Greensboro. NC 27407 p [phone]
www.LabeLLapc.com

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be found and are believed to have been destroyed. As a result, the wrong piezometer (PZ-18) was
converted to MW-24S so MW-24S is actually the former PZ-18, and is located approximately 600
feet downgradient of Phase 4. The error was not discovered until later, when samplers reported that
the well was not located where it was shown on the site plan. MW-24S will be discussed further in
the conclusions.
SAMPLING EVENTS:
Background sampling events for MW-23S, MW-24S, MW-30, and MW-35 were conducted on
February 20-21, 2018, May 16, 2018, August 29-30, 2018, and December 5-6, 2018. Wells were
purged and sampled using either a portable 12-volt pump or disposable bailers in accordance with
standard sampling protocols. All sampling equipment was properly decontaminated prior to use and
between wells. Depth -to -water measurements were obtained to the nearest 0.01 foot using an
electronic water level indicator for all monitoring wells in the compliance network prior to purging.
Measurements of temperature, pH, specific conductivity, and turbidity were recorded in the site log
book as well as on field data logs prior to purging, after each purge volume, and during sampling.
Field data logs for the four sampling events are provided in Attachment 3.
Laboratory -supplied containers were prepared and labeled (either by the laboratory or in the field, as
indicated) with the following information:
• Monitoring well number (completed by field personnel);
• Date and time of sample collection (completed by field personnel);
• Initials of sampling personnel (completed by field personnel);
• Project name and number (completed by the laboratory);
• Chemical preservative (completed by the laboratory); and
• Requested chemical analysis (completed by the laboratory).
Groundwater samples from each monitoring well were dispensed directly from the disposable bailers
or 12-volt pumps into the provided laboratory containers, either immediately after purging or within
24 hours of the final purge volume. Immediately after collection, the samples were placed in a
laboratory -provided cooler and chilled with ice.
In addition, resampling events for vanadium in MW-30 and vanadium and iron in MW-35 were
conducted on February 7, 2019, due to initial exceedances. The same sampling protocols were
followed.
LABORATORY ANALYSES:
The groundwater samples were submitted to Pace Analytical Services, Inc. of Huntersville, North
Carolina under chain -of -custody control for analysis. The samples were analyzed for the NC Appendix
I volatile organic compounds (VOCs) and Appendix I metals, plus additional required C&D
parameters. LaBella requested Level II data reports. The samples were received by the laboratory in
good condition, properly preserved, and within required hold times.
In addition to samples collected for compliance monitoring at the Johns River Waste Management
Facility, a Field Blank was collected by LaBella personnel for each sampling event. Also, a Trip Blank
prepared by the laboratory accompanied the VOC sampling containers from and back to the
laboratory. The Field Blank was analyzed for the NC Appendix I VOCs and metals plus additional
required C&D parameters, and the Trip Blank was analyzed for Appendix I VOCs plus tetrahydrofuran
only.

0=1
Upon receipt of the laboratory data packages, LaBella personnel reviewed the data packages for
quality assurance/quality control (QA/QC) purposes and for possible regulatory issues. If any QA/QC
or regulatory issues were found, the laboratory would be contacted to resolve the issue, and a
resampling event might be scheduled, if needed. The laboratory analytical packages can be found in
Appendix B of this report. The data package was reviewed for the following:
• General typographical errors;
• Correct analyses performed and within method specified hold times;
• Biased data results based on Surrogate Recoveries, Matrix Spike, Matrix Spike Duplicate,
and Laboratory Control Samples;
• Blank -qualified data (B-flags);
• Detections exceeding the North Carolina 15A NCAC 2L Groundwater Standards (NC 2L),
NC Interim Maximum Allowable Concentrations (IMACs), or NCDEQ Groundwater Water
Protection Standards (GWPS); and
• Detections that are above historical levels.
ANALYTICAL RESULTS:
The detected constituents in these four wells for the four sampling events are summarized in Table 2
(Attachment 1). The complete laboratory certificates -of -analysis and chains -of -custody are included
in Attachment 4 of this report.
The inorganic constituents detected above the Method Reporting Limit (MRL) or Practical
Quantitation Limit (PQL) in one or more of these wells in one or more of the sampling events were
arsenic, barium, chromium, cobalt, copper, iron, lead, manganese, nickel, thallium, vanadium, zinc,
chloride, alkalinity, sulfate, and total dissolved solids (TDS). Chromium was detected in exceedance
of the NC 2L in one out of four events in MW-35, Iron was detected in exceedance of the NC 2L in all
four wells. Manganese was detected in exceedance of the NC 2L in one of the four events in
MW-23S and in two events MW-30. Vanadium was detected in exceedance of the GWPS in one of
the four primary events in MW-30 and in two events in MW-35. The February 2019 resampling event
found no detectable vanadium in either MW-30 or MW-35; however, iron above the NC 2L was
detected in MW-35.
Two NC Appendix I organic constituents (ethylbenzene and toluene) were detected above the MRL in
one of the new monitoring wells (MW-23S) during one of the four sampling event, but these
constituents were not detected in the other three events. No organic constituents were detected
above their NC2L or GWPS in any of the four sampling events.
CONCLUSIONS:
The data collected for the four background sampling events from wells MW-23S, MW-24S, MW-30,
and MW-35 in February, May, August, and December 2018 fulfill the background sampling
requirements of the NCSWMR.
An ASD demonstrating that iron and manganese are naturally -occurring was approved for the facility
by NCDEQ on April 12, 2012. The exceedances for chromium, manganese, and vanadium were
inconsistent, appearing in only one or two of the four sampling events in each well that had an
exceedance. In addition, the December 2018 vanadium exceedances in MW-30 and MW-35 were
refuted by the February 2019 resampling event. We recommend continuing to monitor these
constituents in these wells, and if the exceedances persist, an ASD may be required.

023
Monitoring well MW-24S was converted from the wrong piezometer, so its location is actually too far
(about 600 feet) from the waste unit to be an effective monitoring well; therefore, we request that
MW-24S be removed from the monitoring network. Well MW-24S (both the intended location and
the errant location) is between MW-23S and MW-30 in the downgradient direction from Phase 4.
Since wells MW-23S and MW-30 are only about 575 feet apart, we believe they are adequate to
monitor groundwater downgradient from Phases 2A and 4; therefore, we do not propose a
replacement for MW-24S.
If you wish to have a hard copy of the report, drawings, or appendices, we will be happy to provide it
upon your request. Please feel free to contact me or Miguel Vazquez at [phone] if you have
any questions regarding this report.
Respectfully submitted,
LaBella Associates
Van Burbach, Ph.D., P.G
Sr. Technical Consultant
Attachments:
EMRF
Attachment 1
- Tables 1&2
Attachment 2
- Drawing 1
Attachment 3
-Sampling Field Logs
Attachment 4
- Laboratory Reports
Cc: Miles Champion - Burke County

ATTACHMENT 1: Tables 1 & 2

TABLE 1: New Monitoring Wells for Phases 2A and 4
Date
GS
TOC
Date
Top
Bottom
Lithology of
ID (Former ID)
Coverted
Total Depth
Elevation
Elevation
Installed
Screen
Screen
Screened Interval
to MW
(Ft-AMSL)
(Ft-AMSL)
(Ft.-BGS)
(Ft.-BGS)
(Ft.-BGS)
MW-23S (PZ-16S)
1037.66
1040.23
June 1996
Feb. 2018
20
3
20
Saprolite
MW-23D (PZ-16D)
1037.77
1040.18
June 1996
Feb. 2018
68
63
68
Bedrock
MW-24S (PZ-18)
1054.11
1056.68
June 1996
Feb. 2018
55
40
55
Saprolite
MW-30
1052.00
1054.60
Dec.2016
Dec.2016
50
35
50
Bedrock
MW-35 (PZ-35)
1060.64
1063.39
May 2011
Feb. 2018
57.5
15
35
Saprolite
Ft-BGS = Feet below ground surface.
Ft-AMSL = Feet above mean sea level.
Johns River Landfill, Permit # 12-03
Burke County LaBella Associates

TABLE 2: Phase 2A/4 Background Sampling Results
PARAMETER
SAMPLE DATE
METHOD
DL
RL
MW-23S
MW-24S
MW-30
MW-35
Blanks
Arsenic
2/21/2018
EPA 6010
5
10
6.6 J
ND
ND
ND
ND
NC 2L = 1 pg/L
5/16/2018
EPA 6010
5
10
ND
ND
ND
ND
ND
8/29/2018
EPA 6010
5
10
ND
ND
ND
ND
ND
12/5/2018
EPA 6010
5
10
ND
ND
ND
ND
ND
Barium
2/21/2018
EPA 6010
2.5
100
7.4 J
37.9 J
105.0
29.2 J
ND
NC 2L = 700 pg/L
5/16/2018
EPA 6010
2.5
100
10.8 J
42.4 J
44.9 J
22.1 J
ND
8/29/2018
EPA 6010
2.5
100
13.0 J
31.6 J
40.8 J
146
ND
12/5/2018
EPA 6010
2.5
100
5.5
32.6
58.4
42.8
ND
Beryllium
2/21/2018
EPA 8260
0.5
1
ND
ND
ND
ND
ND
NC 2L = 4 pg/L
5/16/2018
EPA 8260
0.5
1
ND
ND
ND
ND
ND
8/29/2018
EPA 8260
0.5
1
ND
ND
ND
0.81 J
ND
12/5/2018
EPA 8260
0.5
1
ND
ND
ND
ND
ND
Chromium
2/21/2018
EPA 8260
2.5
10
ND
ND
7.8 J
ND
ND
NC 2L = 10 pg/L
5/16/2018
EPA 8260
2.5
10
ND
ND
3.1 J
ND
ND
8/29/2018
EPA 8260
2.5
10
3.6 J
ND
2.9 J
22.0
ND
12/5/2018
EPA 8260
2.5
10
ND
ND
4.1 J
3.8 J
ND
Cobalt
2/21/2018
EPA 6010
2.5
10
ND
ND
6.2 J
ND
ND
GWPS = 1 pg/L
5/16/2018
EPA 6010
2.5
10
ND
ND
3.6 J
ND
ND
8/29/2018
EPA 6010
2.5
10
6.2 J
ND
ND
5.6 J
ND
12/5/2018
EPA 6010
2.5
5
3.1 J
ND
3.7 J
ND
ND
Copper
2/21/2018
EPA 8260
2.5
10
ND
ND
2.8 J
ND
ND
NC 2L = 1000 pg/L
5/16/2018
EPA 8260
2.5
10
ND
ND
ND
ND
ND
8/29/2018
EPA 8260
2.5
10
ND
ND
ND
26.9
ND
12/5/2018
EPA 8260
2.5
5
ND
ND
ND
4.1 J
ND
Lead
2/21/2018
EPA 8260
2.5
10
ND
ND
6.4 J
ND
ND
NC 2L =15 pg/L
5/16/2018
EPA 8260
2.5
10
ND
ND
2.8 J
ND
ND
8/29/2018
EPA 8260
2.5
10
3.7 J
ND
ND
9.6 J
ND
12/5/2018
EPA 8260
2.5
10
ND
ND
ND
ND
ND
Iron
2/21/2018
EPA 6010
25
300
NA
NA
NA
NA
ND
NC 2L = 300 pg/L
5/16/2018
EPA 6010
25
300
75.6 J
1,570
3,140
110
ND
8/29/2018
EPA 6010
25
300
NA
NA
NA
NA
ND
12/5/2018
EPA 6010
25
300
323
1,550
5,440
3,410
ND
Resample>
2/7/2019
EPA 6010
25
50
---
---
532.0
---
---
Manganese
2/21/2018
EPA 6010
2.5
50
NA
NA
NA
NA
ND
NC 2L = 50 pVL
5/16/2018
EPA 6010
2.5
50
17 J
29.5 J
762
ND
ND
8/29/2018
EPA 6010
2.5
50
NA
NA
NA
NA
ND
12/5/2018
EPA 6010
2.5
5
73.7
29.5
477
41.2
ND
Burke Co., John's River Landfill LaBella Associates
Permit No. 12-03 Page 1 of 3

TABLE 2: Phase 2A/4 Background Sampling Results
PARAMETER
SAMPLE DATE
METHOD
DL
RL
MW-23S
MW-24S
MW-30
MW-35
Blanks
Nickel
2/21/2018
EPA 6010
2.5
50
ND
ND
5.5 J
ND
ND
NC 2L = 100 pg/L
5/16/2018
EPA 6008
2.5
50
ND
ND
3.4 J
ND
ND
8/29/2018
EPA 6009
2.5
50
ND
ND
ND
8.6 J
ND
12/5/2018
EPA 6010
2.5
5
ND
ND
3.4 J
ND
ND
Thallium
2/21/2018
EPA 6010
0.02
5.5
ND
ND
ND
ND
ND
GWPS = 0.28 pVL
5/16/2018
EPA 6010
0.02
5.5
ND
ND
ND
ND
ND
8/29/2018
EPA 6010
0.02
5.5
0.046 J
0.074 J
0.061 J
0.31 J
ND
12/5/2018
EPA 6010
0.06
0.1
ND
0.081 J
0.13
0.062 J
ND
Vanadium
2/21/2018
EPA 6010
2.5
25
ND
ND
13.0 J
ND
ND
GWPS = 0.3 pVL
5/16/2018
EPA 6010
2.5
25
ND
ND
4.7 J
ND
ND
8/29/2018
EPA 6010
2.5
5
4.1 J
ND
2.9 J
39.1
ND
12/5/2018
EPA 6010
2.5
5
ND
ND
6.6
6.2
ND
Resample>
2/7/2019
EPA 6010
2.5
5
---
---
ND
ND
---
Zinc
2/21/2018
EPA 6010
5
10
ND
6.5 J
28.9
ND
ND
NC 2L = 1,000 pg/L
5/16/2018
EPA 6010
5
10
5.7 J
7.0 J
9.0 J
ND
ND
8/29/2018
EPA 6010
5
10
6.5 J
8.9 J
11.0
44.4
ND
12/5/2018
EPA 6010
5
10
ND
8.7 J
15.5
7.4 J
ND
Ethylbenzene
2/21/2018
EPA 8260
0.3
1
ND
ND
ND
ND
ND
NC 2L = 600 pVL
5/16/2018
EPA 8260
0.3
1
ND
ND
ND
ND
ND
8/29/2018
EPA 8260
0.3
1
1.9
ND
ND
ND
ND
12/5/2018
EPA 8260
0.3
1
ND
ND
ND
ND
ND
Methylene Chloride
2/21/2018
EPA 8260
0.97
1
ND
ND
ND
ND
ND
NC 2L = 5 pg/L
5/16/2018
EPA 8260
0.97
1
ND
ND
ND
ND
ND
8/29/2018
EPA 8260
0.97
1
ND
ND
ND
ND
4.3 J
12/5/2018
EPA 8260
0.97
1
ND
ND
ND
ND
ND
Toluene
2/21/2018
EPA 8260
0.26
1
ND
ND
ND
ND
ND
NC 2L = 600 pg/L
5/16/2018
EPA 8260
0.26
1
ND
ND
ND
ND
ND
8/29/2018
EPA 8260
0.26
1
6.7
ND
ND
ND
ND
12/5/2018
EPA 8260
0.26
1
ND
ND
ND
ND
ND
Sulfate
2/21/2018
s EPA 300.0
2,000
250,000
NO
NO
NO
ND
ND
NC 2L = 250,000 pVL
5/16/2018
s EPA 300.0
2,000
250,000
2,890 J
ND
ND
561 J
ND
8/29/2018
s EPA 300.0
2,000
250,000
ND
NO
NO
NO
NO
12/5/2018
s EPA 300.0
1,000
250,000
1,030
NO
ND
541 J
ND
Burke Co., John's River Landfill LaBella Associates
Permit No. 12-03 Page 2 of 3

TABLE 2: Phase 2A/4 Background Sampling Results
PARAMETER
SAMPLE DATE
METHOD
DL
RL
MW-23S
MW-24S
MW-30
MW-35
Blanks
Chloride
2/21/2018
SM 4500-CI-E
1,000
1,000
NO
NO
ND
ND
ND
INC 2L = 250,000 pg/L
5/16/2018
SM 4500-CI-E
1,000
1,000
1,340
2,680
1,480
1,320
ND
8/29/2018
SM 4500-CI-E
1,000
1,000
NO
NO
NO
ND
ND
12/5/2018
SM 4500-CI-E
500
1,000
2,710
2,760
1,310
1,200
ND
Alkalinity, Total as CaCO3
2/21/2018
SM 2320B
1,000
5,000
NO
ND
ND
ND
ND
INC 2L/ GWPS = NE
5/16/2018
SM 2320B
1,000
5,000
24,600
5,010
25,000
8,870
ND
8/29/2018
SM 2320B
1,000
5,000
NO
NO
NO
NO
ND
12/5/2018
SM 2320B
1,000
5,000
2,980 J
3,580 J
16,200
8,340
ND
Total Dissolved Solids (TDS)
2/21/2018
SM 2540C
25,000
25,000
NO
NO
ND
ND
ND
INC 2L = 500,000 pg/L
5/16/2018
SM 2540C
25,000
25,000
59,000
31,000
56,000
27,000
ND
8/29/2018
SM 2540C
25,000
25,000
ND
NO
NO
NO
ND
12/5/2018
1 SM 2540C
1 25,000
1 25,000
1 25,000
1 26,000
1 55,000
1 37,000
1 ND
NOTES:
All concentrations in miocrograms per liter (pg,/L).
DL = Method Detection Limit.
RL = Reporting Limit.
NC 2L = NC Groundwater Standard established by 15 A NCAC 2L.0202.
GWPS = Groundwater protection standard established by the Solid Waste Section for constituents with no listed NC 2L.
NE = Not Established.
NA = Not analyzed for this parameter.
ND = Not detected above the DL.
J = Estimated concentration below the SWSL or RL.
B = Blank -qualified detection (parameter was detected in a field, trip, or method blank at a similar concentration).
Bold = Result in exceedance of the NC 2L or GWPS (J-flagged and B-flagged data are not considered exceedances).
Burke Co., John's River Landfill LaBella Associates
Permit No. 12-03 Page 3 of 3

ATTACHMENT 2: Drawing 1

PROTECTED AREA �\
\ \� 1 EXISTING TRAIL
TT —
SHOOTING
_ / -
,\ RANGETRANS
TRANSFER FACILI
CURRENT BACKGROUND WELL T)—
\vv� \
\LAND
,OG, 1 (FORIUERL -11 \\\ \� Js \� ✓ ,.. \
/J T \
41U2ENT PHASE IALIIv�T A
� P~�� MUL(:F'FING\
/ABANDONED DO // A,\C \ \
°° Q°��
�//
/
`z // AND
-36 1 �. ll' /V�/ P 61.3
I IIIIII IIY T ' (NM
W_
IIU 'I � l ,.\� PZ-�
,G-35 PNM,�,
191I
/lv
APPROX. LIMeITOOFo )/ ;\ dvi 1 9'%J,/���)\\�\
\ EXISTING WASTE 1 \\\\\\ �f/.%4° l I �� / � \\\
\\ BOUNDARY \ ) /
\ % llll �1\�\ \ /
\�
.,
\ \ \\ \ / ` M)4(N�\
v �\ V \�\ III III
v`AVNI\vvy`�V\\�\��y\ \I�IIIIII NIIII I �� "
1 070
\ \ \ \\V A\
gmSvv
\\\ \\
�
EXISTING hO / i
\ SEDIMENT---'-,,, �� X \ II II I IIII \\ - / / - _
_
BASIN // I\\\==C---9�.-r�4g �\/5 / ' 100 / / / / / ,
\�= MW-16S / \ /
✓ � -16D �99�3
SMP-5 O 995.
� �D,,"sue
/ - 8 MW-19 / 994.23
PP�BP�1NgP
GRAPHIC SCALE V \
0 i W 200 400 \ \I
(FEET)
LEGEND
1050 EXISTING 25' TOPOGRAPHIC CONTOUR
1080 EXISTING 10' TOPOGRAPHIC CONTOUR
EXISTING 5' TOPOGRAPHIC CONTOUR
EXISTING 2' TOPOGRAPHIC CONTOUR
,O GROUNDWATER SURFACE CONTOUR [FEET
ABOVE MEAN SEA LEVEL (AMSL)]
— — — PROPERTY LINE
GROUNDWATER FLOW PATHWAY USED TO
CALCULATE HYDRAULIC GRADIENT
EXISTING ROAD
APPROXIMATE LIMITS OF WASTE
CENTERLINE OF STREAM
- MW 13 COMPLIANCE WELL LOCATION AND IDENTIFICATION WITH STATIC
1010.70 WATER LEVEL ELEVATION (FEET AMSL)
MW-18 SENTINEL WELL LOCATION AND IDENTIFICATION WITH STATIC
WATER LEVEL ELEVATION (FEET AMSL)
O MW-9 ABANDONED OR UNUSED MONITORING WELL
PZ-9D PIEZOMETER LOCATION AND IDENTIFICATION
GMP-3 GAS PROBE LOCATION AND IDENTIFICATION
Q SMP-5 SURFACE MONITORING POINT LOCATION AND IDENTIFICATION
O T1 TEMPORARY WELL
(NM) NOT MEASURED
APPROXIMATE LOCATION OF SPRING HEAD
JEA020 CONTROL POINT LOCATION AND IDENTIFICATION
OSEGMENT USED FOR GRADIENT CALCULATION
FLOW PATH LENGTH
11 767 LF
22 1,142 LF
13 766 LF
NOTES
1. TOPOGRAPHIC CONTOUR INTERVAL =2 AND 10 FEET
2. GROUNDWATER SURFACE CONTOUR INTERVAL = 10 FEET.
3. STATIC WATER LEVELS WERE MEASURED ON DECEMBER 4, 2018.
4. GROUNDWATER CONTOURS BASED ON LINEAR INTERPOLATION BETWEEN AND
EXTRAPOLATION FROM KNOWN DATA, TOPOGRAPHIC CONTOURS, AND KNOWN
FIELD CONDITIONS.
5. MW-16D GROUNDWATER ELEVATION WAS NOT USED IN CALCULATING
GROUNDWATER CONTOURS.
LaBella
Powered by partnership.
2211 W. MEADOWVIEW ROAD
GREENSBORO, NC 27407
PHONE: [phone]
labellapc.com
F-
T
T
L—
F-
T
T
L-
1
C 2019 LaBelle Associates
JOHNS RIVER WASTE
MANAGEMENT FACILITY
BURKE COUNTY. NORTH CAROLINA
N0: DATE'. DESCRIPTION:
Rev s ons
PROJECT NUMBER
2180009
DRAWN BY
RWH
REVIEWED BY:
VB
ISSUED FOR:
GROUNDWATER REPORT
DATE:
JUNE 26, 2019
DRAWING NAME:
GROUNDWATER
POTENTIOMETRIC SURFACE
MAP DECEMBER 4, 2018
PERMIT NO. 12-03
DRAWING NUMBER:
A
it

ATTACHMENT 3: Sampling Field Logs

DATE: 2/20/2018
&'u i `C
ENGINEER/NG GROUND WATER SAMPLING1 LOG
Project Name: Burke County- Johns River Project No. /Task No.: 2180009.07
Well ID: MW-23S Sampler(s): H. Seaton
Well Location: downhill from MW-35 and sed. pond
Well Diameter:
2
inches
Initial Depth to Water (DTW):
8.85
feet
Depth to Bottom (DTB):
20.00
feet
Water Column Thickness (WCT):
11.15
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
1.8
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
5.4
gallons
Actual Amount Purged/Bailed:
5.4
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 10.05
feet
Gallons
Time
Temp(°C)
pH (s.u.)
Cond.
(Ps/cm)
Turb.
(NTU)
Initials
0
0934
11.3
6.53
72
26.83
HS
1.8
0936
11.0
5.15
103
275
HS
Dry @ 2.8 gal
HS
Before Sampling
1325
12.6
5.10
31
20.15
HS
Comments (weather conditions, odor, color, silt, etc.): The weather was partly cloudy with
temperatures in the 60s on 2/20/18. The well was purged and sampled on 2/20/18.
Signature: GAG''"� Date:
QA/QC Sign Off: Date: 19

DATE: 2/20-21/2018
4'u i `r
ENGINEERING GROUND WATER SAMPLINGI LOG
Project Name: Burke County- Johns River Project No. /Task No.: 2180009.07
Well ID: MW-24S Sampler(s): H. Seaton
Well Location:
Well Diameter:
2
inches
Initial Depth to Water (DTW):
48.80
feet
Depth to Bottom (DTB):
55.00
feet
Water Column Thickness (WCT):
6.20
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
1.0
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
3.0
gallons
Actual Amount Purged/Bailed:
3.0
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 48.95
feet
Gallons
Time
Temp(°C)
pH (s.u.)
Cond.
(µS/cm)
Turb.
(NTU)
Initials
0
1104
14.5
6.32
44
125
HS
1.0
1109
14.4
5.65
32
>1000
HS
2.0
1112
14.3
5.50
31
>1000
HS
3.0
1116
14.3
5.48
30
>1000
HS
Before Sampling
0815
14.3
6.25
35
21.75
HS
Comments (weather conditions, odor, color, silt, etc.): The weather was partly cloudy with
temperatures in the 60s on 2/20/18 and 2/21/18. The well was purged on 2/20/18 and
sampled on 2/21/18. Field blank was taken (d) 0835 on 2/21/18.
Signature: Date:j
QA/QC Sign Off: i, Date: V'!P if) g� 2C�1G'j

DATE: 2/20-21 /2018
&'u i `rMff
ENG/NEERING GROUND WATER SAMPLINGI LOG
Project Name: Burke County- Johns River. Project No. /Task No.: 2180009.07
Well ID: MW-30 Sampler(s): H. Seaton
Well Location:
Well Diameter:
2
inches
Initial Depth to Water (DTW):
21.10
feet
Depth to Bottom (DTB):
50.00
feet
Water Column Thickness (WCT):
21.00
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
3.4
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
10.2
gallons
Actual Amount Purged/Bailed:
10.2
gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling: 35.75
feet
Gallons
Time
Temp(°C)
pH (s.u.)
Cond.
(µS/cm)
Turb.
(NTII)
Initials
0
1018
14.5
6.43
104
33.16
HS
3.4
1025
14.5
6.72
94
>1000
HS
6.8
1029
14.5
6.73
105
>1000
HS
Dry @ 7.8 gal
2/21/18
Before Sampling
0800
14.8
6.54
109
174.5
HS
Comments (weather conditions, odor, color, silt, etc.): The weather was partly cloud
temperatures in the 60s on 2/20/ 18 and on 2/21/18. The well was purged on 2/20/ 18 and
sampled on 2/21/18.
Signature:' Date:
QA/QC Sign Off:L�,,,,� Date:

DATE: 05/15-16/18
A`u i `c
ENGINEERING Development and GROUND WATER SAMPLING LOG
Project Name: John's River, Burke Co Project No./Task No.:
2180009.03
Well ID: MW-23S Sampler(s): R. Mesubed / M. Anderson
Well Location:
Well Diameter:
2
inches
Initial Depth to Water (DTW):
4.04
feet
Depth to Bottom (DTB):
20.00
feet
Water Column Thickness (WCT):
15.96
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
2.6
gallons
For 4" Well: WCT X 0.653 =
Rallons
For THREE Well Volumes: WV X 3 =
7.8
gallons
Actual Amount Purged/Bailed:
7.8
gallons
Purged with: Disposable bailer
Sampled with: Disposable bailer
Depth to Water before Sampling: 4.41
feet
Gallons
Time
Temp(°C)
pH
(s.u.)
Cond.
(µS/cm)
Turb.
(NTU)
Initials
0
1501
19.8
6.34
49.8
23.72
RM
2.6
1505
14.2
6.56
43.6
49.47
RM
5.2
1510
14.9
6.60
43.7
66.95
RM
7.8
1512
15.4
6.56
44.1
142.8
RM
05/16/18
Before Sampling
1405
17.4
5.87
46.5
5.02
RM
Comments (weather conditions, odor, color, silt, etc.): The weather was clear, sunny
with temperatures in the 60s on 05/15/2018 and lightly rainy with temperatures in the
60's on 05/16/2018. The well was purged on 05/15/2018 and sampled on 05/16/2018.
Signature: Date: Q.Srllp is
QA/QC Sign O __ Date: __ 0-4 - OGl -t9-�

DATE: 05/15-16/18
&JLJ 1 �G
ENGINEERING Development and GROUND WATER SAMPLING LOG
Project Name: John's River, Burke Co Project No./Task No.: 2180009.03
Well ID: MW-24S Sampler(s): R. Mesubed / M. Anderson
Well Location:
Well Diameter:
2
inches
Initial Depth to Water (DTW):
46.40
feet
Depth to Bottom (DTB):
55.00
feet
Water Column Thickness (WCT):
8.60
feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163 =
1.4
gallons
For 4" Well: WCT X 0.653 =
gallons
For THREE Well Volumes: WV X 3 =
4.2
gallons
Actual Amount Purged/Bailed:
4.2
gallons
Purged with: Disposable bailer
Sampled with: Disposable bailer
Depth to Water before Sampling: 44.33
feet
Gallons
Time
Temp(°C)
pH
(s.u.)
Cond.
(0/cm)
Turb.
(NTU)
Initials
0
1553
15.6
5.45
21.9
256.2
RM
1.4
1555
15.1
5.29
14.6
>1000
RM
2.8
1557
15.1
5.23
21.8
>1000
RM
4.2
1600
15.2
5.15
21.2
>1000
RM
05/16/18
Before Sampling
1315
15.8
6.64
23.5
7.97
RM
Comments (weather conditions, odor, color, silt, etc.): The weather was clear, sunny
with temperatures in the 60s on 05/15/2018 and lightly rainy with temperatures in the
60's on 05/16/2018. The well was purged on 05/15/2018 and sampled on 05/16/2018.
Signature: �' Date:
QA/QC Sign Off: Date: ©A -l`-l21

_ DATE: 05/ 15-16/ 18
ENGINEERING GROUND WATER SAMPLING LOG
Project Name: Burke County- Johns River Project No. /Task No.: 2180009.03
Well ID: MW-30 Sampler(s): R. Mesubed / M. Anderson
Well Location: in the field on left between shop and road to C&D entrance
Well Diameter:
2 inches
Initial Depth to Water (DTW):
27.90 feet
Depth to Bottom (DTB):
50.00 feet
Water Column Thickness (WCT):
22.10 feet [DTB-DTW]
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163
= 3.6 gallons
For 4" Well: WCT X 0.653
= gallons
For THREE Well Volumes: WV X 3
= 10.8 gallons
Actual Amount Purged/Bailed:
10.8 gallons
Purged with: Disposable Bailer
Sampled with: Disposable Bailer
Depth to Water before Sampling:
29.88 feet
Gallons
Time
Temp ff)
DO (mg/L)
Cond.
(PS/cm)
pH
(s.u.)
ORP (mV)
Turb.
(NTU)
Initials
0
1430
16.6
6.26
42.2
5.88
100.7
12.14
RM
3.6
1434
15.2
5.80
42.2
5.64
106.8
> 1100
RM
7.2
1439
15.1
4.77
43.9
5.68
112.1
>1100
RM
Dry @ 9.0 gal
RM
05/16/18
LBefore Sample
1255
18.2
8.20
45.6
6.22
97.3
51.59
RM
Comments (weather conditions, odor, color, silt, etc.):
The weather was clear, sunny with temperatures in the 60s on 05/15/2018 and lightly
rainy with temperatures in the 60's on 05/16/2018. The well was purged on 05/15/2018
and sampled on 05/16/2018.
Signature: X'0" ' Date: OY-1,16M
QA/QC Sign Off- Date: _Q�N -004 - 1b
Revised 12/30/05

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I LaBella
2211W. Meadowview Rd Suite 101
Greensboro, NC 27407
Telephone: [phone]
Facsimile: [phone]
WELL I.D.:
WELL SAMPLING INFORMATION
Well Diameter: _
2 J)
Depth of Well:
Measuring Point:
Pump Type:
Project Name:
Location:
Project No.:
Sampled By:
Date: g/-zq / zolz
Weather: 750 'S ASV Y1+�11
Static Water Level: q,'So
Length of Well Screen: 1-7'
Depth to Top of Pump: --
Tubing Type: k, n -- �"
Time
515
Pump Rate
DO r`+� ;
Gallons
Purged
-
pH
Temp
°C
Conductivity
(mS/cm)
Turbidity
(NTU)
Dissolved 0, Redox
(m ) (mV)
Alkalinity
-
1 Iron (11) Comments
-
+/- 0.1
.o0
ZI.$
+/- 3%
J -O
y 1100
+ 10%
Z. O
+/- 10 mV
— . 3
Szv
-
.O-1
2-D-Z
A 53. H
>I100
i4 . -7.2
g,�
—
-
IS2s
——fo,
O7
ZO. 14
3 (o. 3
S--
S3o
S35
-
-
(o . 0'1
("QI
Zo, 0
ZO. 3
1 1 s • -I
22,1
2 35. -1
2C>ce,&
7S, ► H
3 . ZO
0 . $
IZ•(.o
-
-
-
-
1Syc�
,p
20.-I
IO8,-7
180-3
,IS
1 19•)
-
-
S�S
-
.o
ZO.S
Its.
i(oK•7
3,S2-
1 I(o,'
-
SSD
ss
-
to.ao
�s
Zl . D
Zo- q
11. 5
103,7
jqq, 5
1 C), '.5
.-
41.,19
-
-
5-19s
ZI.Z
S.tS
0(o.Co
3.IS-
S
-
1 zo
-
�,0
yl. Z
S.t7
769.02
I. 3
Z.�.
-
-
l(oz5
cA
ZC.7 1
-78.
5 .1
, 7(
zg. s
-
-
vyuuua rulgcu , U. v D 7, o 1 G• y -.Sb - - -
15 irp35 — oo Z 71,(o SIo.gq Z.IR 38-0
(o,—
Purge Time Purge Time End: Final Static Water Level:
Start:
Notes:

LaBella Project Name: s U r-
p
Location: .) ohn
21g
2211W. Meadowview Rd Suite 101 Project No.: t$ 7
Greensboro NC 27407 Sampled By•
` �11 I
oY1y1 S i ver Lx oan a)1
Telephone: [phone]
Facsimile: [phone] Date: g/ j ©/ ZO1
WELL I.D.: Mw — ' O Weather: ' C
Well Diameter: 2 " Static Water Level: 77. e, S-
Depth of Well: 5z, pp
Measuring Point:
Pump Type:
Length of Well Screen:
Depth to Top of Pump:
Tubing Type:
-7— _ ,—
__s�2k—� ;7 - ] m r, In a 4-u h, nn
�.I r.. _
-Gallons
Purged
TubiUdi)Vy
(NT
OMIM
Alkalinity Iron(II) Comments
I vUILUIw r ul Scu 1 -1 . 5 `15,-P "7,7. '-1-1 %Pi /7 11111-I>
II53 5.qo 14,Z LM 2- 72 1 59, 3
Purge Time Purge Time End: 1, s 3 Final Static Water Level:
Start:
T
ER; ..��§ E
Notes:
WA 5WYIOC� on 3 / 30/ 20 t � (:�P 1153

Project Name:
LaBella
&r C,oVn�`y -
�Y1n�
����
C-x r�SiO✓1
Location:
'o\(\'s
Project No.: Z) g ig-11 pj�Q� Oy
2211W. Meadowview Rd Suite 101
Greensboro, NC 27407 Sampled By: S , S)e60'4, 1 L
Telephone: [phone] Facsimile: [phone] Date: e/ Zq / ZD 113
WELL I.D.: >Mw - 'j `j Weather: gU S -4— �5 v n ✓�
WELL .SAMPLING INFORMATION
Well Diameter: 2 /' Static Water Level:
Depth of Well: 39.0S' Length of Well Screen:
Measuring Point: Depth to Top of Pump:
Pump Type: k P1. Icily Tubing Type:
FIELD-P-k, 1fFft-IUI A T-4-VA m
22. 57
201
G-al—lons
Purged
=(nductmivity
MSIC
Comments
Purge Time , 2 O� i Purge Time End: 1
Start: �7 q
Notes: weJI SaYnp' A On '�3/ 30/ 201 q 2 oq q3
Final Static Water Level:

0. LaBella
2211W. Meadowview Rd Suite 101
Greensboro, NC 27407
Telephone: [phone]
Facsimile: [phone]
WELL I.D.:
Project Name:
Location:
Project No.:
Sampled By:
Date:
Weather:
8 `7 l rJho.�e _ 0
LL SAMPLING IN)H'ORMATION
Well Diameter: 2 Static Water Level:
Depth of Well: 5- 7, dp Length of Well Screen: 1 S'
Measuring Point: — Depth to Top of Pump:
Pump Type: c Tubing Type: i
F1ELD.. ,t�1R° �TI�R M ;�Cir •F1VTTi}N'1` . --- --.. __ - --- _ ..,_. , _._...,,. _ . . ,. .. ... , . - - ... � _...�....---
Gallons
Purged
-----------
-----------
-----------
-----------
-----------
-----------
-----------
-----------
-----------
. ,..... ............. ....6"
Purge Time , 2 S Purge Time End: Final Static Water Level:
Start:
LIZ
Notes:
ih� lvClk Wd"S 5aYY#e.'A cvt

DATE:_1
A LaBella Company GROUND WATER SAMPLING LOG
Project Name: SVK� Co. - T h n s P i %xvi Project No. /Task No.: Z1818 7 1 /'o hA se- 02-
Well ID: MVV ^ 2- S S Sampler(s): M P_5 U Ls. Sl ebc&
Well Location: 6+u-,em M W - 3 S Q„ d_ 'MW -ZqS ,
Well Diameter: 2
Initial Depth to Water (DTW)
Depth to Bottom (DTB):
Water Column Thickness (WCT):
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163
e -S
inches
9. Z6 feet
�U . AQ feet
��. feet [DTB-DTW]
),IF gallons
For 4" Well: WCT X 0.653 = gallons
For THREE Well Volumes: WV X 3 = �. '�/ gallons
Actual Amount Purged/Bailed: S `7 gallons
Purged with: Bailer Pump Other:
Sampled with: Bailer Pump Otther:
Depth to Water before Sampling: %. 7 7 feet
Gallons
Time
Temp('
C)
pH
Cond.
(µS/cm)
DO
(mg/L)
ORP
(mV)
Turb.(ntu)
Initials
W Z
/ -/. 5
36: 3
2• 5-2
�. 9
(� M
/ • �'
� �
� s 3
5. 7y
36,
2. 2 9
77
957/
R M
3.6,,
>1Jo0
9,M
`J' �
`
(0• 1
S.
2S3
o
op
Z M
Date of sample:
12�Sr
Before Sampling
15-L40
12.7
5S 7g
//
92.6 1
2.
100.
Z/. y
P-M
Comments (weather conditions, odor, color, silt, etc.):
MA-23S ark MW-ZID lo,6M V (_ wo,s
funny w LIDS, orn 12-1q Glnci SLiny)\1
Signature: ���_ Date: lVs/20/S
QA/QC Sign Off: ___ �/�� Date: /

�.iL./ w< `►�. DATE: Z-6/ ? 0 !
A LaBella Company GROUND WATER SAMPLING LOG
Project Name: gunk Co. —Jo�ns ;ver Project No. /Task No.: ZF51871 / �cti d Z
Well ID: Z y s Sampler(s):
Well Location: L-ocaAel`,n '1.0R'«-�h _ ��-s� M\b,]_ZZ
Well Diameter:
Initial Depth to Water (DTW):
Depth to Bottom (DTB):
Water Column Thickness (WCT)
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163
For 4" Well: WCT X 0.653
For THREE Well Volumes: WV X 3
Actual Amount Purged/Bailed:
Purged with:
Sampled with
2 inches
25- feet
00 feet
97Z
feet [DTB-DTW]
!- '-/ gallons
gallons
2 gallons
2 Qallons
Depth to Water before Sampling: feet
Gallons
Time
Temp('
C)
pH
Cond.
(µS/cm)
DO
(mg/L)
ORP
(mV)
Turb.(ntu)
Initials
1(0
I Z -9
S 90
1q,
-S 05'
8�1, G
3 .q
A
1 . 7
/l!o 90
I� O
5 6'S
c>
�p, D
2_g(o
10,�. Cp
>/Ooo
RM
Z-
1(0 3z
13- Co
5
Z0, 7
2.$5
j�. ?>
>/oo�
2
d%3q
�5.53
00,
Z-gq
11'55
>IDW
M
Date of sample:
)Z&/18
Before Sampling
jyZO
i3-Q
(oo
Zj, 3
I.90
loz.
Comments (weather conditions, odor, color, silt, etc.):
1 Z /ld
�j
Signature:f�C�,y Date: 6/010 15
QA/QC Sign Off: Date: Z

DATE: 2/-/2olB
L, A LaBella Company GROUND WATER SAMPLING LOG
Project Name: � & -:Yo} n S R) �- V r Project No. /Task No.:
Well ID: /" l UV — —?o Sampler(s):
Well Location:
Well Diameter:
Initial Depth to Water (DTW):
Depth to Bottom (DTB):
Water Column Thickness (WCT)
Calculation for One Well Volume (WV):
For 2" Well:
For 4" Well:
For THREE Well Volumes:
Actual Amount Purg
Purged with:
WCT X 0.163
WCT X 0.653
WVX3
ed/Bailed:
Bail Pumn
y)' r/qad �o eq-D e-'7 ct„ 6,
2 inches
fS, feet
�� • d feet
feet [DTB-DTW]
�• gallons
gallons
10,T gallons
gallons
Sampled with: Bailer Pump Other:
Depth to Water before Sampling: .GB; OE feet
Gallons
Time
Temp('
C)
pH
Cond.
(WS/cm)
DO
(mg/L)
ORP
(mV)
Turb.(ntu)
Initials
Q
i COs4,,
741
s
2. 7
i Dy. b
19, 1-1
1,
3•C�
1-n
I .0
�s51
3G.(0
> WOD
�
7. 2-
I-7N
IS,S
s "61
S7.'�;
2d6-7
>JMD
A r
9.2 callo
Date of sample:
IZ/5-1116
Before Sampling
D-7
(D'2
Q
Comments (weather conditions, odor, color, silt, etc.):
on JZ IZ/ S
V 1 i.. v,,J) W oLS L)raejOa 17 I Clad Sot "2A 6✓1 � Z
Signature: ����Date: ZIS�ZD I
QA/QC Sign Off: Date:

DATE:
A LaBella Company GROUND WATER SAMPLING LOG
Project Name: (..o. ^ J ok1t S We-` Project No. /Task No.: 2i S 18 71 1p lea. St Dz
Well ID: M W — 3 Sampler(s):_ R. ge Sl>1-d /S. S-leba H % k
Well Location: JRono.7- A e-y.0-n✓ts; 0o are t , JD w,n �� �, � 3�1-�- s�L �n r►d
Well Diameter:
Initial Depth to Water (DTW):
Depth to Bottom (DTB):
Water Column Thickness (WCT):
Calculation for One Well Volume (WV):
For 2" Well: WCT X 0.163
For 4" Well: WCT X 0.653
For THREE Well Volumes: WV X 3
2 inches
Z-13 feet
. QS feet
. / feet [DTB-DTW]
Z. �o gallons
gallons
7• S' gallons
Actual Amount Purged/Bailed: 7.19 gallons
Purged with: it Pump Other:
Sampled with: ailer Pump Other:
Depth to Water before Sampling: 2�-9(o feet
Gallons
Time
Temp('
C)
pH
Cond.
(µS/cm)
DO
(mg/L)
ORP
(mV)
Turb.(ntu)
Initials
U
Ilo 30
15
Shy
M. 9
2- y3
6G .0
57. 15-
s
Z.<,
I1,35
1S, s'
S.7(
I .2
�3�'
BZ.s
>l000
�SS
s, Z
1640
1 /.s 3
5. 73
/94
Z. y
S! y
> loao
SS
78
1(A3
Is
5:8�
19.
2.y/
87. a
>i000
�S
Date of sample:
1215 !$
Before Sampling
] sq9
/ y s 140.0yZO
D
3. 7s
L� f�
/0 Z/
ss
Comments (weather conditions, odor, color, silt, etc.):
51, hi a«I well. T wG4 )V-&.- was sv��► � � �+'
and -!r1"1 v 4- , O' o l Z/,S
Signature: Date: %�!Z,j /Zo ! $
QA/QC Sign Off: Date: 2-1l
i'
3

Q, LaBeLLa
2211W. Meadowview Rd Suite 101
Greensboro, NC 27407
Telephone: [phone]
Facsimile: [phone]
WELL I.D.: W- 3 p
WELL SAMPLING INFORMATION
Project Name: SV-L Cour 'Ii -/ ` Totn 5 1�i\�u P)e-sa qp �e-
Location:
Project No.: 21 S ($7 ► k,,,,- 0 1
Sampled By: -TI-HI'tl5011 s• S1e61014nikL
Date: 217 % ZO 1 q
Weather: 7D 's -�- Sv✓fh
Well Diameter: ;2 Static Water Level: 2&, 2 Z
Depth of Well: �©. 00 Length of Well Screen:
Measuring Point: - Depth to Top of Pump: —
Pump Type: kr• l' blcadA, r-n Tubing Type: _ f� k ;b�, ► i n
I� i'15''PARAME11t][VO A4iTR7+`.WWRAIT
-----------
-----------
-----------
-----------
-----------
-----------
-----------
Purge Time I
Start:
Purge Time End: ) q 5-6
Notes: 1 U I l� ��Gw►iiA� �Z� (2 I q Qo
Final Static Water Level:

LaBella Project Name: EorL CogrA -T,-V Ws
Location: --J_oV,,n 's LoiAlj
Project No.: 'Q S 1 87_I �7MG1�2 L 1
2211W. Meadowview Rd Suite 101
Greensboro, NC 27407 Sampled By: T I l Ud Son �S- S� �pG1 ✓i IL
Telephone: [phone]
Facsimile: [phone] Date: 2/7 / Zv 1 q
WELL I.D.. )Ar 3 Weather: 0 '
s vrii\!
Well Diameter: Static Water Level:
Depth of Well: 3�% US Length of Well Screen: -,
V- e.scLmo\
Measuring Pont: — Depth to Top of Pump:
Pump Type: 9�-'O ec11 6.1adA-L- L,rr,f Tubing Type: Sk; bore +-b n
FIELD pARAME�F;'A►,4'�[mF1�rr1r.N� _ - - - .. _..._�� ,-,
Time
Pump Rate
Gallons
Purged
pH
Temp
"C
Conductivity
(MS/CM)
Turbidity
(NTU)
Dissolved Oz
(m L)
Redox
(mV)
Alkalinity
Iron (11)
Comments
+/- 0.1
+/- 3%
+ 10%
+/- 10 mV
1 310
S_ T(7
Z 1 , Co
'L 3. !o
f l o
0 "?z
1 SZ7, 1
--
—
1 315
-
5-, 7
21/. q
2. -72
170. 5
—
—
1320
-
7-7
2N. z
Zil, 7
Z-190
IS2.5-
-
-
3zs
—
5.7y
zy.r
ZS
S.zs
-
-
T,....1
r
Purge Time Purge Time End: Final Static Water Level:
Start: f 3 1 C) 1 330
-
..........
r.,A.
Notes:
1 bo4le 50,VYI A L 13 30

ATTACHMENT 4: Laboratory Reports

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
March 06, 2018
Mr. Van Burbach
Joyce Engineering -Greensboro
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Burke Co LF
Pace Project No.: 92374491
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on February 22, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
trey. [e-mail]
[phone]
Project Manager
Enclosures
cc: Gretta Eller, LaBella Associates, D.P.C.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 30

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Burke Co LF
Pace Project No.: 92374491
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cart 0074
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 2 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Burke Co LF
Pace Project No.: 92374491
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92374491001
MW-24S
Water
02/21/18 08:15
02/22/18 13:43
92374491002
MW-23S
Water
02/20/1813:25
02/22/18 13:43
92374491003
MW-30
Water
02/21/18 08:00
02/22/18 13:43
92374491004
MW-35
Water
02/20/1813:21
02/22/18 13:43
92374491005
Field Blank
Water
02/21/18 08:35
02/22/18 13:43
92374491006
Trip Blank
Water
02/19/18 08:00
02/22/18 13:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Burke Co LF
92374491
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92374491001
MW-24S
EPA 6010
SER
14
PASI-A
EPA 6020
CRT
1
PASI-O
EPA 8260
GAW
50
PASI-C
92374491002
MW-23S
EPA 6010
SER
14
PASI-A
EPA 6020
CRT
1
PASI-O
EPA 8260
GAW
50
PASI-C
92374491003
MW-30
EPA 6010
SER
14
PASI-A
EPA 6020
CRT
1
PASI-O
EPA 8260
GAW
50
PASI-C
92374491004
MW-35
EPA 6010
SER
14
PASI-A
EPA 6020
CRT
1
PASI-O
EPA 8260
GAW
50
PASI-C
92374491005
Field Blank
EPA 6010
SER
14
PASI-A
EPA 6020
CRT
1
PASI-O
EPA 8260
GAW
50
PASI-C
92374491006
Trip Blank
EPA 8260
GAW
50
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
Burke Co LF
92374491
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92374491001
MW-24S
EPA 6010
Barium
37.9J
ug/L
100
03/01/18 04:26
EPA 6010
Zinc
6.5J
ug/L
10.0
03/01/18 04:26
92374491002
MW-23S
EPA 6010
Arsenic
6.6J
ug/L
10.0
03/01/18 04:29
EPA 6010
Barium
7AJ
ug/L
100
03/01/18 04:29
92374491003
MW-30
EPA 6010
Barium
105
ug/L
100
03/01/18 04:33
EPA 6010
Chromium
7.8J
ug/L
10.0
03/01/18 04:33
EPA 6010
Cobalt
6.2J
ug/L
10.0
03/01/18 04:33
EPA 6010
Copper
2.8J
ug/L
10.0
03/01/18 04:33
EPA 6010
Lead
6AJ
ug/L
10.0
03/01/18 04:33
EPA 6010
Nickel
5.5J
ug/L
50.0
03/01/18 04:33
EPA 6010
Vanadium
13.OJ
ug/L
25.0
03/01/18 04:33
EPA 6010
Zinc
28.9
ug/L
10.0
03/01/18 04:33
92374491004
MW-35
EPA 6010
Barium
29.2J
ug/L
100
03/01/18 04:36
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 30

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-24S Lab ID: 92374491001 Collected: 02/21/18 08:15 Received: 02/22/18 13:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
02/24/18 14:20
03/01/18 04:26
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:26
7440-38-2
Barium
37.9J
ug/L
100
2.5
1
02/24/18 14:20
03/01/18 04:26
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:26
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:26
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:26
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:26
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:26
7440-50-8
Lead
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:26
7439-92-1
Nickel
ND
ug/L
50.0
2.5
1
02/24/18 14:20
03/01/18 04:26
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:26
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:26
7440-22-4
Vanadium
ND
ug/L
25.0
2.5
1
02/24/18 14:20
03/01/18 04:26
7440-62-2
Zinc
6.5J
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:26
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020
Preparation
Method: EPA 3010
Thallium
ND
ug/L
5.5
0.50
1
03/06/18 00:54
03/06/18 16:24
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
ND
ug/L
100
10.0
1
02/23/18 10:41
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
02/23/18 10:41
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
02/23/18 10:41
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
02/23/18 10:41
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
02/23/18 10:41
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
02/23/18 10:41
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
02/23/18 10:41
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
02/23/18 10:41
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
02/23/18 10:41
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
02/23/18 10:41
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
02/23/18 10:41
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
02/23/18 10:41
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
02/23/18 10:41
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
02/23/18 10:41
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
02/23/18 10:41
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
02/23/18 10:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
02/23/18 10:41
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
02/23/18 10:41
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
02/23/18 10:41
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
02/23/18 10:41
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
02/23/18 10:41
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
02/23/18 10:41
75-34-3 L2
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
02/23/18 10:41
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
02/23/18 10:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
02/23/18 10:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
02/23/18 10:41
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
02/23/18 10:41
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 30

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-24S
Lab ID:
92374491001
Collected:
02/21/18 08:15
Received: 02/22/18 13:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
02/23/18 10:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
02/23/18 10:41
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
02/23/18 10:41
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
02/23/18 10:41
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
02/23/18 10:41
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
02/23/18 10:41
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
02/23/18 10:41
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
02/23/18 10:41
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
02/23/18 10:41
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
02/23/18 10:41
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
02/23/18 10:41
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
02/23/18 10:41
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
02/23/18 10:41
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
02/23/18 10:41
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
02/23/18 10:41
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
02/23/18 10:41
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
02/23/18 10:41
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
02/23/18 10:41
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
02/23/18 10:41
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
02/23/18 10:41
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
02/23/18 10:41
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
02/23/18 10:41
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
02/23/18 10:41
2037-26-5
Date: 03/06/2018 09:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 30

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ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-23S Lab ID: 92374491002 Collected: 02/20/18 13:25 Received: 02/22/18 13:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
02/24/18 14:20
03/01/18 04:29
7440-36-0
Arsenic
6.6J
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:29
7440-38-2
Barium
7.4J
ug/L
100
2.5
1
02/24/18 14:20
03/01/18 04:29
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:29
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:29
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:29
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:29
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:29
7440-50-8
Lead
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:29
7439-92-1
Nickel
ND
ug/L
50.0
2.5
1
02/24/18 14:20
03/01/18 04:29
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:29
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:29
7440-22-4
Vanadium
ND
ug/L
25.0
2.5
1
02/24/18 14:20
03/01/18 04:29
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:29
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020
Preparation
Method: EPA 3010
Thallium
ND
ug/L
5.5
0.50
1
03/06/18 00:54
03/06/18 16:31
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
ND
ug/L
100
10.0
1
02/23/18 10:58
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
02/23/18 10:58
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
02/23/18 10:58
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
02/23/18 10:58
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
02/23/18 10:58
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
02/23/18 10:58
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
02/23/18 10:58
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
02/23/18 10:58
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
02/23/18 10:58
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
02/23/18 10:58
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
02/23/18 10:58
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
02/23/18 10:58
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
02/23/18 10:58
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
02/23/18 10:58
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
02/23/18 10:58
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
02/23/18 10:58
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
02/23/18 10:58
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
02/23/18 10:58
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
02/23/18 10:58
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
02/23/18 10:58
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
02/23/18 10:58
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
02/23/18 10:58
75-34-3 L2
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
02/23/18 10:58
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
02/23/18 10:58
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
02/23/18 10:58
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
02/23/18 10:58
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
02/23/18 10:58
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 30

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ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-23S
Lab ID:
92374491002
Collected:
02/20/18 13:25
Received: 02/22/18 13:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
02/23/18 10:58
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
02/23/18 10:58
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
02/23/18 10:58
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
02/23/18 10:58
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
02/23/18 10:58
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
02/23/18 10:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
02/23/18 10:58
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
02/23/18 10:58
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
02/23/18 10:58
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
02/23/18 10:58
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
02/23/18 10:58
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
02/23/18 10:58
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
02/23/18 10:58
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
02/23/18 10:58
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
02/23/18 10:58
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
02/23/18 10:58
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
02/23/18 10:58
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
02/23/18 10:58
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
02/23/18 10:58
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
02/23/18 10:58
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
02/23/18 10:58
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
02/23/18 10:58
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
02/23/18 10:58
2037-26-5
Date: 03/06/2018 09:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 30

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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-30 Lab ID: 92374491003 Collected: 02/21/18 08:00 Received: 02/22/18 13:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 03/06/2018 09:48 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
02/24/18 14:20
03/01/18 04:33
7440-36-0
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:33
7440-38-2
105
ug/L
100
2.5
1
02/24/18 14:20
03/01/18 04:33
7440-39-3
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:33
7440-41-7
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:33
7440-43-9
7.8J
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:33
7440-47-3
6.2J
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:33
7440-48-4
2.8J
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:33
7440-50-8
6.4J
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:33
7439-92-1
5.5J
ug/L
50.0
2.5
1
02/24/18 14:20
03/01/18 04:33
7440-02-0
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:33
7782-49-2
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:33
7440-22-4
13.OJ
ug/L
25.0
2.5
1
02/24/18 14:20
03/01/18 04:33
7440-62-2
28.9
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:33
7440-66-6
Analytical Method: EPA 6020 Preparation Method: EPA 3010
ND ug/L 5.5 0.50 1 03/06/18 00:54 03/06/18 16:32 7440-28-0
Analytical Method: EPA 8260
ND
ug/L
100
10.0
1
02/23/1811:14
67-64-1
ND
ug/L
200
1.9
1
02/23/1811:14
107-13-1
ND
ug/L
1.0
0.25
1
02/23/1811:14
71-43-2
ND
ug/L
3.0
0.17
1
02/23/1811:14
74-97-5
ND
ug/L
1.0
0.18
1
02/23/1811:14
75-27-4
ND
ug/L
3.0
0.26
1
02/23/1811:14
75-25-2
ND
ug/L
10.0
0.29
1
02/23/1811:14
74-83-9
ND
ug/L
100
0.96
1
02/23/1811:14
78-93-3
ND
ug/L
100
1.2
1
02/23/1811:14
75-15-0
ND
ug/L
1.0
0.25
1
02/23/1811:14
56-23-5
ND
ug/L
3.0
0.23
1
02/23/1811:14
108-90-7
ND
ug/L
10.0
0.54
1
02/23/1811:14
75-00-3
ND
ug/L
5.0
0.14
1
02/23/1811:14
67-66-3
ND
ug/L
1.0
0.11
1
02/23/1811:14
74-87-3
ND
ug/L
13.0
2.0
1
02/23/1811:14
96-12-8
ND
ug/L
3.0
0.21
1
02/23/1811:14
124-48-1
ND
ug/L
1.0
0.27
1
02/23/1811:14
106-93-4
ND
ug/L
10.0
0.21
1
02/23/1811:14
74-95-3
ND
ug/L
5.0
0.30
1
02/23/1811:14
95-50-1
ND
ug/L
1.0
0.33
1
02/23/1811:14
106-46-7
ND
ug/L
100
1.0
1
02/23/1811:14
110-57-6
ND
ug/L
5.0
0.32
1
02/23/1811:14
75-34-3
ND
ug/L
1.0
0.24
1
02/23/1811:14
107-06-2
ND
ug/L
5.0
0.56
1
02/23/1811:14
75-35-4
ND
ug/L
5.0
0.19
1
02/23/1811:14
156-59-2
ND
ug/L
5.0
0.49
1
02/23/1811:14
156-60-5
ND
ug/L
1.0
0.27
1
02/23/1811:14
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L2
Page 10 of 30

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-30
Lab ID:
92374491003
Collected:
02/21/18 08:00
Received: 02/22/18 13:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
02/23/18 11:14
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
02/23/18 11:14
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
02/23/18 11:14
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
02/23/18 11:14
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
02/23/18 11:14
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
02/23/18 11:14
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
02/23/18 11:14
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
02/23/18 11:14
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
02/23/18 11:14
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
02/23/18 11:14
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
02/23/18 11:14
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
02/23/18 11:14
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
02/23/18 11:14
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
02/23/18 11:14
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
02/23/18 11:14
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
02/23/18 11:14
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
02/23/18 11:14
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
02/23/18 11:14
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
02/23/18 11:14
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
02/23/18 11:14
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
02/23/18 11:14
460-00-4
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
02/23/18 11:14
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
02/23/18 11:14
2037-26-5
Date: 03/06/2018 09:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 30

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-35 Lab ID: 92374491004 Collected: 02/20/18 13:21 Received: 02/22/18 13:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 03/06/2018 09:48 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
02/24/18 14:20
03/01/18 04:36
7440-36-0
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:36
7440-38-2
29.2J
ug/L
100
2.5
1
02/24/18 14:20
03/01/18 04:36
7440-39-3
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:36
7440-41-7
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:36
7440-43-9
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:36
7440-47-3
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:36
7440-48-4
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:36
7440-50-8
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:36
7439-92-1
ND
ug/L
50.0
2.5
1
02/24/18 14:20
03/01/18 04:36
7440-02-0
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:36
7782-49-2
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:36
7440-22-4
ND
ug/L
25.0
2.5
1
02/24/18 14:20
03/01/18 04:36
7440-62-2
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:36
7440-66-6
Analytical Method: EPA 6020 Preparation Method: EPA 3010
ND ug/L 5.5 0.50 1 03/06/18 00:54 03/06/18 16:38 7440-28-0
Analytical Method: EPA 8260
ND
ug/L
100
10.0
1
02/23/1811:31
67-64-1
ND
ug/L
200
1.9
1
02/23/1811:31
107-13-1
ND
ug/L
1.0
0.25
1
02/23/1811:31
71-43-2
ND
ug/L
3.0
0.17
1
02/23/1811:31
74-97-5
ND
ug/L
1.0
0.18
1
02/23/1811:31
75-27-4
ND
ug/L
3.0
0.26
1
02/23/1811:31
75-25-2
ND
ug/L
10.0
0.29
1
02/23/1811:31
74-83-9
ND
ug/L
100
0.96
1
02/23/1811:31
78-93-3
ND
ug/L
100
1.2
1
02/23/1811:31
75-15-0
ND
ug/L
1.0
0.25
1
02/23/1811:31
56-23-5
ND
ug/L
3.0
0.23
1
02/23/1811:31
108-90-7
ND
ug/L
10.0
0.54
1
02/23/1811:31
75-00-3
ND
ug/L
5.0
0.14
1
02/23/1811:31
67-66-3
ND
ug/L
1.0
0.11
1
02/23/1811:31
74-87-3
ND
ug/L
13.0
2.0
1
02/23/1811:31
96-12-8
ND
ug/L
3.0
0.21
1
02/23/1811:31
124-48-1
ND
ug/L
1.0
0.27
1
02/23/1811:31
106-93-4
ND
ug/L
10.0
0.21
1
02/23/1811:31
74-95-3
ND
ug/L
5.0
0.30
1
02/23/1811:31
95-50-1
ND
ug/L
1.0
0.33
1
02/23/1811:31
106-46-7
ND
ug/L
100
1.0
1
02/23/1811:31
110-57-6
ND
ug/L
5.0
0.32
1
02/23/1811:31
75-34-3
ND
ug/L
1.0
0.24
1
02/23/1811:31
107-06-2
ND
ug/L
5.0
0.56
1
02/23/1811:31
75-35-4
ND
ug/L
5.0
0.19
1
02/23/1811:31
156-59-2
ND
ug/L
5.0
0.49
1
02/23/1811:31
156-60-5
ND
ug/L
1.0
0.27
1
02/23/1811:31
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L2
Page 12 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: MW-35
Lab ID:
92374491004
Collected:
02/20/18 13:21
Received: 02/22/18 13:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
02/23/18 11:31
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
02/23/18 11:31
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
02/23/18 11:31
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
02/23/18 11:31
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
02/23/18 11:31
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
02/23/18 11:31
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
02/23/18 11:31
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
02/23/18 11:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
02/23/18 11:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
02/23/18 11:31
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
02/23/18 11:31
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
02/23/18 11:31
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
02/23/18 11:31
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
02/23/18 11:31
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
02/23/18 11:31
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
02/23/18 11:31
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
02/23/18 11:31
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
02/23/18 11:31
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
02/23/18 11:31
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
02/23/18 11:31
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
02/23/18 11:31
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
02/23/18 11:31
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
02/23/18 11:31
2037-26-5
Date: 03/06/2018 09:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 30

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: Field Blank Lab ID: 92374491005 Collected: 02/21/18 08:35 Received: 02/22/18 13:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 03/06/2018 09:48 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
02/24/18 14:20
03/01/18 04:39
7440-36-0
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:39
7440-38-2
ND
ug/L
100
2.5
1
02/24/18 14:20
03/01/18 04:39
7440-39-3
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:39
7440-41-7
ND
ug/L
1.0
0.50
1
02/24/18 14:20
03/01/18 04:39
7440-43-9
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:39
7440-47-3
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:39
7440-48-4
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:39
7440-50-8
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:39
7439-92-1
ND
ug/L
50.0
2.5
1
02/24/18 14:20
03/01/18 04:39
7440-02-0
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:39
7782-49-2
ND
ug/L
10.0
2.5
1
02/24/18 14:20
03/01/18 04:39
7440-22-4
ND
ug/L
25.0
2.5
1
02/24/18 14:20
03/01/18 04:39
7440-62-2
ND
ug/L
10.0
5.0
1
02/24/18 14:20
03/01/18 04:39
7440-66-6
Analytical Method: EPA 6020 Preparation Method: EPA 3010
ND ug/L 5.5 0.50 1 03/06/18 00:54 03/06/18 16:39 7440-28-0
Analytical Method: EPA 8260
ND
ug/L
100
10.0
1
02/23/1811:48
67-64-1
ND
ug/L
200
1.9
1
02/23/1811:48
107-13-1
ND
ug/L
1.0
0.25
1
02/23/1811:48
71-43-2
ND
ug/L
3.0
0.17
1
02/23/1811:48
74-97-5
ND
ug/L
1.0
0.18
1
02/23/1811:48
75-27-4
ND
ug/L
3.0
0.26
1
02/23/1811:48
75-25-2
ND
ug/L
10.0
0.29
1
02/23/1811:48
74-83-9
ND
ug/L
100
0.96
1
02/23/1811:48
78-93-3
ND
ug/L
100
1.2
1
02/23/1811:48
75-15-0
ND
ug/L
1.0
0.25
1
02/23/1811:48
56-23-5
ND
ug/L
3.0
0.23
1
02/23/1811:48
108-90-7
ND
ug/L
10.0
0.54
1
02/23/1811:48
75-00-3
ND
ug/L
5.0
0.14
1
02/23/1811:48
67-66-3
ND
ug/L
1.0
0.11
1
02/23/1811:48
74-87-3
ND
ug/L
13.0
2.0
1
02/23/1811:48
96-12-8
ND
ug/L
3.0
0.21
1
02/23/1811:48
124-48-1
ND
ug/L
1.0
0.27
1
02/23/1811:48
106-93-4
ND
ug/L
10.0
0.21
1
02/23/1811:48
74-95-3
ND
ug/L
5.0
0.30
1
02/23/1811:48
95-50-1
ND
ug/L
1.0
0.33
1
02/23/1811:48
106-46-7
ND
ug/L
100
1.0
1
02/23/1811:48
110-57-6
ND
ug/L
5.0
0.32
1
02/23/1811:48
75-34-3
ND
ug/L
1.0
0.24
1
02/23/1811:48
107-06-2
ND
ug/L
5.0
0.56
1
02/23/1811:48
75-35-4
ND
ug/L
5.0
0.19
1
02/23/1811:48
156-59-2
ND
ug/L
5.0
0.49
1
02/23/1811:48
156-60-5
ND
ug/L
1.0
0.27
1
02/23/1811:48
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L2
Page 14 of 30

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: Field Blank
Lab ID:
92374491005
Collected:
02/21/18 08:35
Received: 02/22/18 13:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
02/23/18 11:48
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
02/23/18 11:48
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
02/23/18 11:48
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
02/23/18 11:48
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
02/23/18 11:48
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
02/23/18 11:48
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
02/23/18 11:48
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
02/23/18 11:48
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
02/23/18 11:48
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
02/23/18 11:48
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
02/23/18 11:48
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
02/23/18 11:48
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
02/23/18 11:48
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
02/23/18 11:48
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
02/23/18 11:48
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
02/23/18 11:48
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
02/23/18 11:48
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
02/23/18 11:48
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
02/23/18 11:48
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
02/23/18 11:48
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
02/23/18 11:48
460-00-4
1,2-Dichloroethane-d4 (S)
94
%
70-130
1
02/23/18 11:48
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
02/23/18 11:48
2037-26-5
Date: 03/06/2018 09:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: Trip Blank Lab ID: 92374491006 Collected: 02/19/18 08:00 Received: 02/22/18 13:43 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Date: 03/06/2018 09:48 PM
Analytical Method: EPA 8260
ND
ug/L
100
10.0
1
02/23/1812:05
67-64-1
ND
ug/L
200
1.9
1
02/23/1812:05
107-13-1
ND
ug/L
1.0
0.25
1
02/23/1812:05
71-43-2
ND
ug/L
3.0
0.17
1
02/23/1812:05
74-97-5
ND
ug/L
1.0
0.18
1
02/23/1812:05
75-27-4
ND
ug/L
3.0
0.26
1
02/23/1812:05
75-25-2
ND
ug/L
10.0
0.29
1
02/23/1812:05
74-83-9
ND
ug/L
100
0.96
1
02/23/1812:05
78-93-3
ND
ug/L
100
1.2
1
02/23/1812:05
75-15-0
ND
ug/L
1.0
0.25
1
02/23/1812:05
56-23-5
ND
ug/L
3.0
0.23
1
02/23/1812:05
108-90-7
ND
ug/L
10.0
0.54
1
02/23/1812:05
75-00-3
ND
ug/L
5.0
0.14
1
02/23/1812:05
67-66-3
ND
ug/L
1.0
0.11
1
02/23/1812:05
74-87-3
ND
ug/L
13.0
2.0
1
02/23/1812:05
96-12-8
ND
ug/L
3.0
0.21
1
02/23/1812:05
124-48-1
ND
ug/L
1.0
0.27
1
02/23/1812:05
106-93-4
ND
ug/L
10.0
0.21
1
02/23/1812:05
74-95-3
ND
ug/L
5.0
0.30
1
02/23/1812:05
95-50-1
ND
ug/L
1.0
0.33
1
02/23/1812:05
106-46-7
ND
ug/L
100
1.0
1
02/23/1812:05
110-57-6
ND
ug/L
5.0
0.32
1
02/23/1812:05
75-34-3
ND
ug/L
1.0
0.24
1
02/23/1812:05
107-06-2
ND
ug/L
5.0
0.56
1
02/23/1812:05
75-35-4
ND
ug/L
5.0
0.19
1
02/23/1812:05
156-59-2
ND
ug/L
5.0
0.49
1
02/23/1812:05
156-60-5
ND
ug/L
1.0
0.27
1
02/23/1812:05
78-87-5
ND
ug/L
1.0
0.13
1
02/23/1812:05
10061-01-5
ND
ug/L
1.0
0.26
1
02/23/1812:05
10061-02-6
ND
ug/L
1.0
0.30
1
02/23/1812:05
100-41-4
ND
ug/L
50.0
0.46
1
02/23/1812:05
591-78-6
ND
ug/L
10.0
0.32
1
02/23/1812:05
74-88-4
ND
ug/L
1.0
0.97
1
02/23/1812:05
75-09-2
ND
ug/L
100
0.33
1
02/23/1812:05
108-10-1
ND
ug/L
1.0
0.26
1
02/23/1812:05
100-42-5
ND
ug/L
5.0
0.33
1
02/23/1812:05
630-20-6
ND
ug/L
3.0
0.40
1
02/23/1812:05
79-34-5
ND
ug/L
1.0
0.46
1
02/23/1812:05
127-18-4
ND
ug/L
1.0
0.26
1
02/23/1812:05
108-88-3
ND
ug/L
1.0
0.48
1
02/23/1812:05
71-55-6
ND
ug/L
1.0
0.29
1
02/23/1812:05
79-00-5
ND
ug/L
1.0
0.47
1
02/23/1812:05
79-01-6
ND
ug/L
1.0
0.20
1
02/23/1812:05
75-69-4
ND
ug/L
1.0
0.41
1
02/23/1812:05
96-18-4
ND
ug/L
50.0
0.35
1
02/23/1812:05
108-05-4
ND
ug/L
1.0
0.62
1
02/23/1812:05
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
L2
Page 16 of 30

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ANALYTICAL RESULTS
Project: Burke Co LF
Pace Project No.: 92374491
Sample: Trip Blank
Lab ID:
92374491006
Collected:
02/19/18 08:00
Received: 02/22/18 13:43 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260
Xylene (Total)
ND
ug/L
5.0
0.66 1
02/23/18 12:05
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
93
%
70-130
1
02/23/18 12:05
460-00-4
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
02/23/18 12:05
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
02/23/18 12:05
2037-26-5
Date: 03/06/2018 09:48 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 30

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QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
QC Batch: 399439 Analysis Method: EPA 6010
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92374491001, 92374491002, 92374491003, 92374491004, 92374491005
METHOD BLANK: 2215480 Matrix: Water
Associated Lab Samples: 92374491001, 92374491002, 92374491003, 92374491004, 92374491005
Blank Reporting
Parameter Units Result Limit MDL
Antimony
ug/L
ND
6.0
Arsenic
ug/L
ND
10.0
Barium
ug/L
ND
100
Beryllium
ug/L
ND
1.0
Cadmium
ug/L
ND
1.0
Chromium
ug/L
ND
10.0
Cobalt
ug/L
ND
10.0
Copper
ug/L
ND
10.0
Lead
ug/L
ND
10.0
Nickel
ug/L
ND
50.0
Selenium
ug/L
ND
10.0
Silver
ug/L
ND
10.0
Vanadium
ug/L
ND
25.0
Zinc
ug/L
ND
10.0
Analyzed
3.9
03/01 /18 03:18
5.0
03/01 /18 03:18
2.5
03/01 /18 03:18
0.50
03/01 /18 03:18
0.50
03/01 /18 03:18
2.5
03/01 /18 03:18
2.5
03/01 /18 03:18
2.5
03/01 /18 03:18
2.5
03/01 /18 03:18
2.5
03/01 /18 03:18
5.0
03/01 /18 03:18
2.5
03/01 /18 03:18
2.5
03/01 /18 03:18
5.0
03/01 /18 03:18
LABORATORY CONTROL SAMPLE:
Parameter
2215481
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
513
103
80-120
Arsenic
ug/L
500
501
100
80-120
Barium
ug/L
500
521
104
80-120
Beryllium
ug/L
500
514
103
80-120
Cadmium
ug/L
500
510
102
80-120
Chromium
ug/L
500
506
101
80-120
Cobalt
ug/L
500
499
100
80-120
Copper
ug/L
500
531
106
80-120
Lead
ug/L
500
492
98
80-120
Nickel
ug/L
500
505
101
80-120
Selenium
ug/L
500
507
101
80-120
Silver
ug/L
250
258
103
80-120
Vanadium
ug/L
500
512
102
80-120
Zinc
ug/L
500
490
98
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2215482 2215483
MS MSD
92374504003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 526 505 105 101 75-125 4 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2215482
2215483
MS
MSD
92374504003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
517
499
103
99
75-125
4
20
Barium
ug/L
73.6
500
500
610
578
107
101
75-125
5
20
Beryllium
ug/L
ND
500
500
531
505
106
101
75-125
5
20
Cadmium
ug/L
ND
500
500
527
504
105
101
75-125
5
20
Chromium
ug/L
ND
500
500
517
493
103
98
75-125
5
20
Cobalt
ug/L
ND
500
500
503
489
101
98
75-125
3
20
Copper
ug/L
ND
500
500
544
519
109
104
75-125
5
20
Lead
ug/L
ND
500
500
502
479
100
96
75-125
5
20
Nickel
ug/L
ND
500
500
510
487
102
97
75-125
5
20
Selenium
ug/L
ND
500
500
540
517
108
103
75-125
4
20
Silver
ug/L
ND
250
250
267
254
107
102
75-125
5
20
Vanadium
ug/L
ND
500
500
530
505
106
101
75-125
5
20
Zinc
ug/L
ND
500
500
514
492
101
97
75-125
4
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
QC Batch: 430666 Analysis Method: EPA 6020
QC Batch Method: EPA 3010 Analysis Description: 6020 MET
Associated Lab Samples: 92374491001, 92374491002, 92374491003, 92374491004, 92374491005
METHOD BLANK: 2341371 Matrix: Water
Associated Lab Samples: 92374491001, 92374491002, 92374491003, 92374491004, 92374491005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 5.5 0.50 03/06/1815:59
LABORATORY CONTROL SAMPLE: 2341372
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 50 48.7 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2341373 2341374
MS MSD
92374491001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 50 50 49.4 50.2 99 100 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
QC Batch: 399482 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92374491001, 92374491002, 92374491003, 92374491004, 92374491005, 92374491006
METHOD BLANK: 2215649 Matrix: Water
Associated Lab Samples: 92374491001, 92374491002, 92374491003, 92374491004, 92374491005, 92374491006
Blank Reporting
Parameter Units Result Limit MDL Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
0.33
02/23/18 10:07
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
02/23/18 10:07
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
0.40
02/23/18 10:07
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
02/23/18 10:07
1,1-Dichloroethane
ug/L
ND
5.0
0.32
02/23/18 10:07
1,1-Dichloroethene
ug/L
ND
5.0
0.56
02/23/18 10:07
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
02/23/18 10:07
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
2.0
02/23/18 10:07
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
02/23/18 10:07
1,2-Dichlorobenzene
ug/L
ND
5.0
0.30
02/23/18 10:07
1,2-Dichloroethane
ug/L
ND
1.0
0.24
02/23/18 10:07
1,2-Dichloropropane
ug/L
ND
1.0
0.27
02/23/18 10:07
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
02/23/18 10:07
2-Butanone (MEK)
ug/L
ND
100
0.96
02/23/18 10:07
2-Hexanone
ug/L
ND
50.0
0.46
02/23/18 10:07
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
0.33
02/23/18 10:07
Acetone
ug/L
ND
100
10.0
02/23/18 10:07
Acrylonitrile
ug/L
ND
200
1.9
02/23/18 10:07
Benzene
ug/L
ND
1.0
0.25
02/23/18 10:07
Bromochloromethane
ug/L
ND
3.0
0.17
02/23/18 10:07
Bromodichloromethane
ug/L
ND
1.0
0.18
02/23/18 10:07
Bromoform
ug/L
ND
3.0
0.26
02/23/18 10:07
Bromomethane
ug/L
ND
10.0
0.29
02/23/18 10:07
Carbon disulfide
ug/L
ND
100
1.2
02/23/18 10:07
Carbon tetrachloride
ug/L
ND
1.0
0.25
02/23/18 10:07
Chlorobenzene
ug/L
ND
3.0
0.23
02/23/18 10:07
Chloroethane
ug/L
ND
10.0
0.54
02/23/18 10:07
Chloroform
ug/L
ND
5.0
0.14
02/23/18 10:07
Chloromethane
ug/L
ND
1.0
0.11
02/23/18 10:07
cis-1,2-Dichloroethene
ug/L
ND
5.0
0.19
02/23/18 10:07
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
02/23/18 10:07
Dibromochloromethane
ug/L
ND
3.0
0.21
02/23/18 10:07
Dibromomethane
ug/L
ND
10.0
0.21
02/23/18 10:07
Ethylbenzene
ug/L
ND
1.0
0.30
02/23/18 10:07
lodomethane
ug/L
ND
10.0
0.32
02/23/18 10:07
Methylene Chloride
ug/L
ND
1.0
0.97
02/23/18 10:07
Styrene
ug/L
ND
1.0
0.26
02/23/18 10:07
Tetrachloroethene
ug/L
ND
1.0
0.46
02/23/18 10:07
Toluene
ug/L
ND
1.0
0.26
02/23/18 10:07
trans-1,2-Dichloroethene
ug/L
ND
5.0
0.49
02/23/18 10:07
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
02/23/18 10:07
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 30

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[phone]
QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
METHOD BLANK: 2215649
Matrix:
Water
Associated Lab Samples:
92374491001, 92374491002, 92374491003, 92374491004, 92374491005, 92374491006
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
trans-1,4-Dichloro-2-butene
ug/L
ND
100
1.0
02/23/18 10:07
Trichloroethene
ug/L
ND
1.0
0.47
02/23/18 10:07
Trichlorofluoromethane
ug/L
ND
1.0
0.20
02/23/18 10:07
Vinyl acetate
ug/L
ND
50.0
0.35
02/23/18 10:07
Vinyl chloride
ug/L
ND
1.0
0.62
02/23/18 10:07
Xylene (Total)
ug/L
ND
5.0
0.66
02/23/18 10:07
1,2-Dichloroethane-d4 (S)
%
92
70-130
02/23/18 10:07
4-Bromofluorobenzene (S)
%
98
70-130
02/23/18 10:07
Toluene-d8 (S)
%
106
70-130
02/23/18 10:07
LABORATORY CONTROL SAMPLE:
Parameter
2215650
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.0
102
80-125
1,1,1-Trichloroethane
ug/L
50
48.5
97
71-129
1,1,2,2-Tetrachloroethane
ug/L
50
56.8
114
79-124
1,1,2-Trichloroethane
ug/L
50
55.5
111
85-125
1,1-Dichloroethane
ug/L
50
31.9
64
73-126 L2
1,1-Dichloroethene
ug/L
50
41.7
83
66-135
1,2,3-Trichloropropane
ug/L
50
56.5
113
75-130
1,2-Dibromo-3-chloropropane
ug/L
50
56.9
114
71-133
1,2-Dibromoethane (EDB)
ug/L
50
56.9
114
83-124
1,2-Dichlorobenzene
ug/L
50
55.5
111
80-133
1,2-Dichloroethane
ug/L
50
43.0
86
67-128
1,2-Dichloropropane
ug/L
50
53.3
107
75-132
1,4-Dichlorobenzene
ug/L
50
53.6
107
78-130
2-Butanone (MEK)
ug/L
100
89.9J
90
61-144
2-Hexanone
ug/L
100
100
100
68-143
4-Methyl-2-pentanone (MIBK)
ug/L
100
103
103
72-135
Acetone
ug/L
100
90.1 J
90
48-146
Acrylonitrile
ug/L
250
215
86
40-160
Benzene
ug/L
50
54.7
109
80-125
Bromochloromethane
ug/L
50
49.8
100
71-125
Bromodichloromethane
ug/L
50
54.6
109
78-124
Bromoform
ug/L
50
52.1
104
71-128
Bromomethane
ug/L
50
48.9
98
40-160
Carbon disulfide
ug/L
50
41.1J
82
50-160
Carbon tetrachloride
ug/L
50
50.9
102
69-131
Chlorobenzene
ug/L
50
54.4
109
81-122
Chloroethane
ug/L
50
40.4
81
39-148
Chloroform
ug/L
50
45.9
92
73-127
Chloromethane
ug/L
50
39.8
80
44-146
cis-1,2-Dichloroethene
ug/L
50
46.2
92
74-124
cis-1,3-Dichloropropene
ug/L
50
56.4
113
72-132
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
LABORATORY CONTROL SAMPLE:
2215650
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Dibromochloromethane
ug/L
50
58.4
117
78-125
Dibromomethane
ug/L
50
49.6
99
82-120
Ethylbenzene
ug/L
50
54.2
108
79-121
lodomethane
ug/L
100
89.3
89
39-154
Methylene Chloride
ug/L
50
39.8
80
64-133
Styrene
ug/L
50
54.8
110
84-126
Tetrachloroethene
ug/L
50
52.8
106
78-122
Toluene
ug/L
50
49.8
100
80-121
trans-1,2-Dichloroethene
ug/L
50
41.1
82
71-127
trans- 1,3-Dichloropropene
ug/L
50
49.2
98
69-141
trans-1,4-Dichloro-2-butene
ug/L
50
50.1J
100
40-160
Trichloroethene
ug/L
50
53.4
107
78-122
Trichlorofluoromethane
ug/L
50
39.8
80
53-137
Vinyl acetate
ug/L
100
88.2
88
40-160
Vinyl chloride
ug/L
50
51.2
102
58-137
Xylene (Total)
ug/L
150
167
111
81-126
1,2-Dichloroethane-d4 (S)
%
83
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
2215652
92374533002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.6
103
70-130
1,1,1-Trichloroethane
ug/L
ND
20
21.7
109
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20.8
104
70-130
1,1,2-Trichloroethane
ug/L
ND
20
20.5
102
70-130
1,1-Dichloroethane
ug/L
ND
20
19.8
99
70-130
1,1-Dichloroethene
ug/L
ND
20
20.7
103
70-166
1,2,3-Trichloropropane
ug/L
ND
20
20.7
103
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
20
19.9
100
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
20
21.5
107
70-130
1,2-Dichlorobenzene
ug/L
ND
20
22.4
112
70-130
1,2-Dichloroethane
ug/L
ND
20
20.3
101
70-130
1,2-Dichloropropane
ug/L
ND
20
21.9
110
70-130
1,4-Dichlorobenzene
ug/L
ND
20
21.8
109
70-130
2-Butanone (MEK)
ug/L
ND
40
31.0J
78
70-130
2-Hexanone
ug/L
ND
40
34.OJ
85
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
35.3J
88
70-130
Acetone
ug/L
ND
40
34.3J
86
70-130
Acrylonitrile
ug/L
ND
100
95AJ
95
70-130
Benzene
ug/L
0.40J
20
23.3
114
70-148
Bromochloromethane
ug/L
ND
20
22.4
112
70-130
Bromodichloromethane
ug/L
ND
20
21.7
109
70-130
Bromoform
ug/L
ND
20
19.9
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
MATRIX SPIKE SAMPLE:
Parameter
2215652
Units
92374533002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Bromomethane
ug/L
ND
20
16.8
84
70-130
Carbon disulfide
ug/L
ND
20
19.7J
99
70-130
Carbon tetrachloride
ug/L
ND
20
22.5
113
70-130
Chlorobenzene
ug/L
ND
20
23.1
115
70-146
Chloroethane
ug/L
ND
20
22.7
114
70-130
Chloroform
ug/L
ND
20
21.3
107
70-130
Chloromethane
ug/L
ND
20
16.9
84
70-130
cis-1,2-Dichloroethene
ug/L
ND
20
21.1
105
70-130
cis-1,3-Dichloropropene
ug/L
ND
20
21.0
105
70-130
Dibromochloromethane
ug/L
ND
20
21.3
106
70-130
Dibromomethane
ug/L
ND
20
21.1
105
70-130
Ethylbenzene
ug/L
ND
20
22.9
114
70-130
lodomethane
ug/L
ND
40
29.0
73
70-130
Methylene Chloride
ug/L
ND
20
17.8
89
70-130
Styrene
ug/L
ND
20
23.1
115
70-130
Tetrachloroethene
ug/L
ND
20
21.2
106
70-130
Toluene
ug/L
ND
20
21.2
106
70-155
trans-1,2-Dichloroethene
ug/L
ND
20
19.5
97
70-130
trans- 1,3-Dichloropropene
ug/L
ND
20
19.8
99
70-130
trans-1,4-Dichloro-2-butene
ug/L
ND
20
17.2J
86
70-130
Trichloroethene
ug/L
ND
20
24.1
120
69-151
Trichlorofluoromethane
ug/L
ND
20
20.1
101
70-130
Vinyl acetate
ug/L
ND
40
32AJ
81
70-130
Vinyl chloride
ug/L
ND
20
22.5
112
70-130
Xylene (Total)
ug/L
ND
60
68.4
114
70-130
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 2215651
Parameter
Units
92374533001
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co LF
Pace Project No.: 92374491
SAMPLE DUPLICATE: 2215651
Parameter
Units
92374533001
Result
Dup
Result
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
0.38J
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
0.34J
0.37J
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
94
94
4-Bromofluorobenzene (S)
%
96
97
Toluene-d8 (S)
%
103
103
Max
RPD RPD Qualifiers
is
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 30

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Burke Co LF
Pace Project No.: 92374491
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Burke Co LF
92374491
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92374491001
MW-24S
EPA 3010A
399439
EPA 6010
399621
92374491002
MW-23S
EPA 3010A
399439
EPA 6010
399621
92374491003
MW-30
EPA 3010A
399439
EPA 6010
399621
92374491004
MW-35
EPA 3010A
399439
EPA 6010
399621
92374491005
Field Blank
EPA 3010A
399439
EPA 6010
399621
92374491001
MW-24S
EPA 3010
430666
EPA 6020
430678
92374491002
MW-23S
EPA 3010
430666
EPA 6020
430678
92374491003
MW-30
EPA 3010
430666
EPA 6020
430678
92374491004
MW-35
EPA 3010
430666
EPA 6020
430678
92374491005
Field Blank
EPA 3010
430666
EPA 6020
430678
92374491001
MW-24S
EPA 8260
399482
92374491002
MW-23S
EPA 8260
399482
92374491003
MW-30
EPA 8260
399482
92374491004
MW-35
EPA 8260
399482
92374491005
Field Blank
EPA 8260
399482
92374491006
Trip Blank
EPA 8260
399482
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/06/2018 09:48 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 30

Document Name:
Document Revised: February 7, 2018
aceAnalytical y
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville El_' Ralelgh❑ Mechanicsville❑
Sample Condition Client Name: WO# : 92374491
Project
Courier: []Fed Ex [-]UPS CUSPS ❑Client IIIIII 1111111111111111
❑ Commercial ❑1�ce ❑ether 92-374491
Custody Seal Present? ❑Yes QNo Seals Intact? []Yes -QNo
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other
Thermometer:
❑ IR Gun ID: 92TO36 Type of lee: IOW ❑Blue
ZI
Cooler Temp ('C): Correction Factor: Add/Subtract (°C) +0.1
Cooler Temp Corrected (°C): - L Z
USDA Regulated Soil (.fN/A, water sample)
Did samples ote in a quararitine zone within the United States: CA, NY, or SC (check mapsl?
I�Yes 110
Date/lnitlals Person Examining Contents: L�5 `} _'4 '
Biological Tissue F en?
[]Nonee
[:]Yeses [:]No N/A
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Old samples originate from a foreign source (intern nally,
includlna Hawaii and Puerto Rico)? MYes I—IMb
Comments/Dlscrepancy:
Chain of Custody Present?
es
ON.
❑N/a
I.
Samples Arrived within Hold Time?
es
❑No
N/A
2.
Short Hold Time Analysis (<72 h►.)?
❑Yes
No
❑N/A
9.
Rush Turn Around Time Requested?
❑Yes
CaKo
❑N/A
A.
Sufficient Volume?
2K.1
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Y
Yes
[]No
[]No
[]NIA
❑N/A
6.
Containers intact?
E fYes
QNo
N/A
7.
Dissolved analysis: Samples Field Filtered? ❑Yes
EfN.
❑N/A
a.
Sample Labels Match COC?
-Includes Date/Time/IQ/Analysis
E]Ves
Matrix:
❑No
[]N/A
9.
In VOA Vials (>5-6mm)?
❑Yes
o
N/A
10.
nHeadspace
lank Present?
lank Custody Seals Present?
Pes
04s
❑No
[]NO
❑N/A
❑PI/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Date Required? []Yes [:]NO
Lot ID of split containers;
CLIENT NOTIFICATION/FRESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review: �L
Date/Time:
Date: z /2z/ e
Date: Z /2 Z61-&
Page 28 of 30

Document Name:
0ocument Revised: February 7, 2018
y
aceAnaWical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water] DOC, LLHg
**Bottom half of box is to list number of bottle
Project # Wp# : 92374491
PM: RWC Due Dale: 03/08/18
CLIENT: 92-Joyce Eng
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pH Adjustment Log for Preserved Samples
Sample 10
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
tot k
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this torn will be seat to the Norrn Carouna ur:nrvn LeruaLeuuu V, uCC k X.
Out of hold, irmrrect preservative, out of temp, incorrect containers.
Page 29 of 30

PaceMalylical
Section A
Required Client lnfonnation:
Section B
Required Project Information:
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section C
Invoice Information:
Pacle - 1 Of 1
Company: La6ella Associates. D, P,C. - NC I
Report TO: Haley Seaton
Attention:
Address: 2211 W. Meadowview Rd.
Copy To-,
Company Name:
Greensboro, NC 27407
Address:
Regulatory Agency
Email: hseaton labellapccorn
Purchase Order#
Pace Quote
Phone: [phone] Fax
Project Name'. Burke Cc LF
Pace Project Manager: trey _carter pacelabs,core
State 1 Location
Requested Due Date:
Project #:
Pace Profile #: 2327-5
NC
Requested
Anal
sis
Filtered
Y!N
MATRIX CODE
COLLECTED
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 01, 2018
Mr. Van Burbach
Joyce Engineering -Greensboro
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Johns River - Expansion GW
Pace Project No.: 92385350
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on May 18, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Trey Carter
trey. [e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Van Burbach, Joyce Engineering -NC
Gretta Eller, LaBella Associates, D.P.C.
Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 42

acmnalytical
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Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Montana Certification #: Cert 0074
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL022
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
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SAMPLE SUMMARY
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92385350001
1203-MW-20
Water
05/16/1814:25
05/18/1812:12
92385350002
1203-MW-38
Water
05/16/1810:00
05/18/1812:12
92385350003
MW-23S
Water
05/16/1814:05
05/18/1812:12
92385350004
MW-24S
Water
05/16/1813:15
05/18/1812:12
92385350005
MW-30
Water
05/16/1812:55
05/18/1812:12
92385350006
MW-35
Water
05/16/1811:40
05/18/1812:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 42

aceAnalytical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Johns River - Expansion GW
92385350
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92385350001
1203-MW-20
EPA 6010
SER
17
PASI-A
EPA 6020
CRT
1
PASI-O
EPA7470
JMW1
1
PASI-A
EPA 8260
CAH
52
PASI-C
SM 2320B
KDF1
1
PASI-A
SM 2540C
NAL
1
PASI-A
EPA 300.0
BRJ
1
PASI-A
SM 4500-CI-E
BRJ
1
PASI-A
92385350002
1203-MW-38
EPA 6010
SER
17
PASI-A
EPA 6020
CRT
1
PASI-O
EPA7470
JMW1
1
PASI-A
EPA 8260
CAH
52
PASI-C
SM 2320B
KDF1
1
PASI-A
SM 2540C
NAL
1
PASI-A
EPA 300.0
BRJ
1
PASI-A
SM 4500-CI-E
BRJ
1
PASI-A
92385350003
MW-23S
EPA 6010
SER
17
PASI-A
EPA 6020
CRT
1
PASI-O
EPA7470
JMW1
1
PASI-A
EPA 8260
CAH
52
PASI-C
SM 2320B
KDF1
1
PASI-A
SM 2540C
NAL
1
PASI-A
EPA 300.0
BRJ
1
PASI-A
SM 4500-CI-E
BRJ
1
PASI-A
92385350004
MW-24S
EPA 6010
SER
17
PASI-A
EPA 6020
CRT
1
PASI-O
EPA7470
JMW1
1
PASI-A
EPA 8260
CAH
52
PASI-C
SM 2320B
KDF1
1
PASI-A
SM 2540C
NAL
1
PASI-A
EPA 300.0
BRJ
1
PASI-A
SM 4500-CI-E
BRJ
1
PASI-A
92385350005
MW-30
EPA 6010
SER
17
PASI-A
EPA 6020
CRT
1
PASI-O
EPA7470
JMW1
1
PASI-A
EPA 8260
CAH
52
PASI-C
SM 2320B
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 4 of 42

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
SM 2540C
NAL
1
PASI-A
EPA 300.0
BRJ
1
PASI-A
SM 4500-CI-E
BRJ
1
PASI-A
92385350006 MW-35 EPA 6010
SER
17
PASI-A
EPA 6020
CRT
1
PASI-O
EPA7470
JMW1
1
PASI-A
EPA 8260
CAH
52
PASI-C
SM 2320B
KDF1
1
PASI-A
SM 2540C
NAL
1
PASI-A
EPA 300.0
CDC
1
PASI-A
SM 4500-CI-E
BRJ
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 42

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Johns River - Expansion GW
Pace Project No.:
92385350
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92385350001
1203-MW-20
EPA 6010
Barium
54.1 J
ug/L
100
06/01/18 01:42
EPA 6010
Iron
1920
ug/L
300
06/01/18 01:42
EPA 6010
Manganese
35.3J
ug/L
50.0
06/01/18 01:42
EPA 6010
Vanadium
3.2J
ug/L
25.0
06/01/18 01:42
EPA 6010
Zinc
5.5J
ug/L
10.0
06/01/18 01:42
SM 2320B
Alkalinity, Total as CaCO3
7860
ug/L
5000
05/24/18 20:23
SM 2540C
Total Dissolved Solids
34000
ug/L
25000
05/23/18 12:30
SM 4500-CI-E
Chloride
1590
ug/L
1000
05/30/18 15:16
92385350002
1203-MW-38
EPA 6010
Barium
117
ug/L
100
06/01/18 01:51
EPA 6010
Cobalt
15.7
ug/L
10.0
06/01/18 01:51
EPA 6010
Iron
19900
ug/L
300
06/01/18 01:51
EPA 6010
Lead
65.8
ug/L
10.0
06/01/18 01:51
EPA 6010
Manganese
4260
ug/L
50.0
06/01/18 01:51
EPA 6010
Nickel
4AJ
ug/L
50.0
06/01/18 01:51
EPA 8260
Benzene
4.6
ug/L
1.0
05/30/18 08:54
EPA 8260
Chlorobenzene
0.70J
ug/L
3.0
05/30/18 08:54
EPA 8260
1,2-Dichlorobenzene
0.34J
ug/L
5.0
05/30/18 08:54
EPA 8260
1,4-Dichlorobenzene
15.1
ug/L
1.0
05/30/18 08:54
EPA 8260
1,1-Dichloroethane
4.1J
ug/L
5.0
05/30/18 08:54
EPA 8260
1,2-Dichloroethane
0.64J
ug/L
1.0
05/30/18 08:54
EPA 8260
cis-1,2-Dichloroethene
7.1
ug/L
5.0
05/30/18 08:54
EPA 8260
Ethylbenzene
0.70J
ug/L
1.0
05/30/18 08:54
EPA 8260
Tetrahydrofuran
314
ug/L
10.0
05/30/18 08:54
EPA 8260
Toluene
0.54J
ug/L
1.0
05/30/18 08:54
EPA 8260
Trichloroethene
1.2
ug/L
1.0
05/30/18 08:54
EPA 8260
Vinyl chloride
3.1
ug/L
1.0
05/30/18 08:54
EPA 8260
Xylene (Total)
9.8
ug/L
5.0
05/30/18 08:54
SM 2320B
Alkalinity, Total as CaCO3
253000
ug/L
5000
05/24/18 20:33
SM 2540C
Total Dissolved Solids
282000
ug/L
25000
05/23/18 12:30
EPA 300.0
Sulfate
983J
ug/L
250000
05/23/18 07:55
SM 4500-CI-E
Chloride
6570
ug/L
2000
05/30/18 15:17
92385350003
MW-23S
EPA 6010
Barium
10.8J
ug/L
100
06/01/18 01:54
EPA 6010
Iron
75.6J
ug/L
300
06/01/18 01:54
EPA 6010
Manganese
17.OJ
ug/L
50.0
06/01/18 01:54
EPA 6010
Zinc
5.7J
ug/L
10.0
06/01/18 01:54
SM 2320B
Alkalinity, Total as CaCO3
24600
ug/L
5000
05/24/18 20:41
SM 2540C
Total Dissolved Solids
59000
ug/L
25000
05/23/18 12:30
EPA 300.0
Sulfate
2890J
ug/L
250000
05/23/18 08:12
SM 4500-CI-E
Chloride
1340
ug/L
1000
05/30/18 15:18
92385350004
MW-24S
EPA 6010
Barium
42AJ
ug/L
100
06/01/18 01:57
EPA 6010
Iron
1570
ug/L
300
06/01/18 01:57
EPA 6010
Manganese
29.5J
ug/L
50.0
06/01/18 01:57
EPA 6010
Zinc
7.OJ
ug/L
10.0
06/01/18 01:57
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 6 of 42

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
Johns River - Expansion GW
92385350
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92385350004
MW-24S
SM 2320B
Alkalinity, Total as CaCO3
5010
ug/L
5000
05/24/18 20:52
SM 2540C
Total Dissolved Solids
31000
ug/L
25000
05/23/18 12:30
SM 4500-CI-E
Chloride
2680
ug/L
1000
05/30/18 15:19
92385350005
MW-30
EPA 6010
Barium
44.9J
ug/L
100
05/31/1816:16
EPA 6010
Chromium
3.1J
ug/L
10.0
05/31/1816:16
EPA 6010
Cobalt
3.6J
ug/L
10.0
05/31/1816:16
EPA 6010
Iron
3140
ug/L
300
05/31/1816:16
EPA 6010
Lead
2.8J
ug/L
10.0
05/31/1816:16
EPA 6010
Manganese
762
ug/L
50.0
05/31/1816:16
EPA 6010
Nickel
3AJ
ug/L
50.0
05/31/1816:16
EPA 6010
Vanadium
4.7J
ug/L
25.0
05/31/1816:16
EPA 6010
Zinc
9.01
ug/L
10.0
05/31/1816:16
SM 2320B
Alkalinity, Total as CaCO3
25000
ug/L
5000
05/24/18 21:01
SM 2540C
Total Dissolved Solids
56000
ug/L
25000
05/23/18 12:30
SM 4500-CI-E
Chloride
1480
ug/L
1000
05/30/18 15:23
92385350006
MW-35
EPA 6010
Barium
22.1 J
ug/L
100
05/31/18 22:00
EPA 6010
Iron
110J
ug/L
300
05/31/18 22:00
SM 2320B
Alkalinity, Total as CaCO3
8870
ug/L
5000
05/24/18 21:12
SM 2540C
Total Dissolved Solids
27000
ug/L
25000
05/23/18 12:51 D6
EPA 300.0
Sulfate
561 J
ug/L
250000
05/26/18 03:43
SM 4500-CI-E
Chloride
1320
ug/L
1000
05/30/18 15:24
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: 1203-MW-20 Lab ID: 92385350001 Collected: 05/16/18 14:25 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
05/29/18 16:05
06/01/18 01:42
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:42
7440-38-2
Barium
54.1J
ug/L
100
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:42
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:42
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-50-8
Iron
1920
ug/L
300
25.0
1
05/29/18 16:05
06/01/18 01:42
7439-89-6
Lead
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7439-92-1
Manganese
35.3J
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7439-96-5
Nickel
ND
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:42
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-22-4
Tin
ND
ug/L
5.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-31-5
Vanadium
3.2J
ug/L
25.0
2.5
1
05/29/18 16:05
06/01/18 01:42
7440-62-2
Zinc
5.5J
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:42
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020
Preparation
Method: EPA 3010
Thallium
ND
ug/L
27.5
2.5
5
05/24/18 20:15
05/25/18 04:23
7440-28-0 D3
7470 Mercury
Analytical Method: EPA 7470
Preparation
Method: EPA 7470
Mercury
ND
ug/L
0.20
0.10
1
05/31/1810:00
05/31/1819:23
7439-97-6
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
ND
ug/L
100
10.0
1
05/30/18 08:38
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
05/30/18 08:38
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
05/30/18 08:38
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
05/30/18 08:38
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
05/30/18 08:38
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
05/30/18 08:38
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
05/30/18 08:38
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
05/30/18 08:38
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
05/30/18 08:38
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
05/30/18 08:38
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
05/30/18 08:38
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
05/30/18 08:38
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
05/30/18 08:38
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
05/30/18 08:38
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
05/30/18 08:38
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
05/30/18 08:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
05/30/18 08:38
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
05/30/18 08:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
05/30/18 08:38
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
05/30/18 08:38
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
05/30/18 08:38
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM
without the written consent of Pace Analytical Services, LLC.
Page 8 of 42

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ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: 1203-MW-20 Lab ID: 92385350001 Collected: 05/16/18 14:25 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
05/30/18 08:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
05/30/18 08:38
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
05/30/18 08:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
05/30/18 08:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
05/30/18 08:38
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
05/30/18 08:38
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
05/30/18 08:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
05/30/18 08:38
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
05/30/18 08:38
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
05/30/18 08:38
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
05/30/18 08:38
74-88-4
Isobutanol
ND
ug/L
100
35.0
1
05/30/18 08:38
78-83-1
Methylene Chloride
ND
ug/L
1.0
0.97
1
05/30/18 08:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
05/30/18 08:38
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
05/30/18 08:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
05/30/18 08:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
05/30/18 08:38
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
05/30/18 08:38
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
05/30/18 08:38
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
05/30/18 08:38
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
05/30/18 08:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
05/30/18 08:38
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
05/30/18 08:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
05/30/18 08:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
05/30/18 08:38
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
05/30/18 08:38
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
05/30/18 08:38
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
05/30/18 08:38
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
05/30/18 08:38
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
05/30/18 08:38
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
05/30/18 08:38
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B
Alkalinity, Total as CaCO3
7860
ug/L
5000
1000
1
05/24/18 20:23
2540C Total Dissolved Solids
Analytical Method: SM
2540C
Total Dissolved Solids
34000
ug/L
25000
25000
1
05/23/18 12:30
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
ND
ug/L
250000
500
1
05/23/18 07:38
14808-79-8
4500 Chloride
Analytical Method: SM
4500-CI-E
Chloride
1590
ug/L
1000
500
1
05/30/1815:16
16887-00-6
Date: 06/01 /2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: 1203-MW-38 Lab ID: 92385350002 Collected: 05/16/18 10:00 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
05/29/18 16:05
06/01/18 01:51
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:51
7440-38-2
Barium
117
ug/L
100
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:51
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:51
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-47-3
Cobalt
15.7
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-50-8
Iron
19900
ug/L
300
25.0
1
05/29/18 16:05
06/01/18 01:51
7439-89-6
Lead
65.8
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7439-92-1
Manganese
4260
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7439-96-5
Nickel
4.4J
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:51
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-22-4
Tin
ND
ug/L
5.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-31-5
Vanadium
ND
ug/L
25.0
2.5
1
05/29/18 16:05
06/01/18 01:51
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:51
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020
Preparation
Method: EPA 3010
Thallium
ND
ug/L
27.5
2.5
5
05/24/18 20:15
05/25/18 04:25
7440-28-0 D3
7470 Mercury
Analytical Method: EPA 7470
Preparation
Method: EPA 7470
Mercury
ND
ug/L
0.20
0.10
1
05/31/1810:00
05/31/1819:25
7439-97-6
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
ND
ug/L
100
10.0
1
05/30/18 08:54
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
05/30/18 08:54
107-13-1
Benzene
4.6
ug/L
1.0
0.25
1
05/30/18 08:54
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
05/30/18 08:54
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
05/30/18 08:54
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
05/30/18 08:54
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
05/30/18 08:54
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
05/30/18 08:54
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
05/30/18 08:54
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
05/30/18 08:54
56-23-5
Chlorobenzene
0.70J
ug/L
3.0
0.23
1
05/30/18 08:54
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
05/30/18 08:54
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
05/30/18 08:54
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
05/30/18 08:54
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
05/30/18 08:54
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
05/30/18 08:54
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
05/30/18 08:54
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
05/30/18 08:54
74-95-3
1,2-Dichlorobenzene
0.34J
ug/L
5.0
0.30
1
05/30/18 08:54
95-50-1
1,4-Dichlorobenzene
15.1
ug/L
1.0
0.33
1
05/30/18 08:54
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
05/30/18 08:54
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: 1203-MW-38 Lab ID: 92385350002 Collected: 05/16/18 10:00 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloroethane
4.1J
ug/L
5.0
0.32
1
05/30/18 08:54
75-34-3
1,2-Dichloroethane
0.64J
ug/L
1.0
0.24
1
05/30/18 08:54
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
05/30/18 08:54
75-35-4
cis-1,2-Dichloroethene
7.1
ug/L
5.0
0.19
1
05/30/18 08:54
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
05/30/18 08:54
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
05/30/18 08:54
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
05/30/18 08:54
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
05/30/18 08:54
10061-02-6
Ethylbenzene
0.70J
ug/L
1.0
0.30
1
05/30/18 08:54
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
05/30/18 08:54
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
05/30/18 08:54
74-88-4
Isobutanol
ND
ug/L
100
35.0
1
05/30/18 08:54
78-83-1
Methylene Chloride
ND
ug/L
1.0
0.97
1
05/30/18 08:54
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
05/30/18 08:54
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
05/30/18 08:54
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
05/30/18 08:54
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
05/30/18 08:54
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
05/30/18 08:54
127-18-4
Tetrahydrofuran
314
ug/L
10.0
3.1
1
05/30/18 08:54
109-99-9
Toluene
0.54J
ug/L
1.0
0.26
1
05/30/18 08:54
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
05/30/18 08:54
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
05/30/18 08:54
79-00-5
Trichloroethene
1.2
ug/L
1.0
0.47
1
05/30/18 08:54
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
05/30/18 08:54
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
05/30/18 08:54
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
05/30/18 08:54
108-05-4
Vinyl chloride
3.1
ug/L
1.0
0.62
1
05/30/18 08:54
75-01-4
Xylene (Total)
9.8
ug/L
5.0
0.66
1
05/30/18 08:54
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
05/30/18 08:54
460-00-4
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
05/30/18 08:54
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
05/30/18 08:54
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B
Alkalinity, Total as CaCO3
253000
ug/L
5000
1000
1
05/24/18 20:33
2540C Total Dissolved Solids
Analytical Method: SM
2540C
Total Dissolved Solids
282000
ug/L
25000
25000
1
05/23/18 12:30
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
983J
ug/L
250000
500
1
05/23/18 07:55
14808-79-8
4500 Chloride
Analytical Method: SM
4500-CI-E
Chloride
6570
ug/L
2000
1000
2
05/30/1815:17
16887-00-6
Date: 06/01 /2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-23S Lab ID: 92385350003 Collected: 05/16/18 14:05 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 301 OA
Antimony
ND
ug/L
6.0
3.9
1
05/29/18 16:05
06/01/18 01:54
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:54
7440-38-2
Barium
10.8J
ug/L
100
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:54
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:54
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-50-8
Iron
75.6J
ug/L
300
25.0
1
05/29/18 16:05
06/01/18 01:54
7439-89-6
Lead
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7439-92-1
Manganese
17.OJ
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7439-96-5
Nickel
ND
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:54
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-22-4
Tin
ND
ug/L
5.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-31-5
Vanadium
ND
ug/L
25.0
2.5
1
05/29/18 16:05
06/01/18 01:54
7440-62-2
Zinc
5.7J
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:54
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020
Preparation
Method: EPA 3010
Thallium
ND
ug/L
27.5
2.5
5
05/24/18 20:15
05/25/18 04:27
7440-28-0 D3
7470 Mercury
Analytical Method: EPA 7470
Preparation
Method: EPA 7470
Mercury
ND
ug/L
0.20
0.10
1
05/31/1810:00
05/31/1819:28
7439-97-6
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
ND
ug/L
100
10.0
1
05/30/18 09:10
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
05/30/18 09:10
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
05/30/18 09:10
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
05/30/18 09:10
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
05/30/18 09:10
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
05/30/18 09:10
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
05/30/18 09:10
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
05/30/18 09:10
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
05/30/18 09:10
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
05/30/18 09:10
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
05/30/18 09:10
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
05/30/18 09:10
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
05/30/18 09:10
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
05/30/18 09:10
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
05/30/18 09:10
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
05/30/18 09:10
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
05/30/18 09:10
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
05/30/18 09:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
05/30/18 09:10
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
05/30/18 09:10
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
05/30/18 09:10
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-23S Lab ID: 92385350003 Collected: 05/16/18 14:05 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
05/30/18 09:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
05/30/18 09:10
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
05/30/18 09:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
05/30/18 09:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
05/30/18 09:10
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
05/30/18 09:10
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
05/30/18 09:10
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
05/30/18 09:10
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
05/30/18 09:10
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
05/30/18 09:10
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
05/30/18 09:10
74-88-4
Isobutanol
ND
ug/L
100
35.0
1
05/30/18 09:10
78-83-1
Methylene Chloride
ND
ug/L
1.0
0.97
1
05/30/18 09:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
05/30/18 09:10
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
05/30/18 09:10
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
05/30/18 09:10
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
05/30/18 09:10
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
05/30/18 09:10
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
05/30/18 09:10
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
05/30/18 09:10
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
05/30/18 09:10
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
05/30/18 09:10
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
05/30/18 09:10
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
05/30/18 09:10
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
05/30/18 09:10
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
05/30/18 09:10
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
05/30/18 09:10
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
05/30/18 09:10
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
05/30/18 09:10
460-00-4
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
05/30/18 09:10
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
05/30/18 09:10
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B
Alkalinity, Total as CaCO3
24600
ug/L
5000
1000
1
05/24/18 20:41
2540C Total Dissolved Solids
Analytical Method: SM
2540C
Total Dissolved Solids
59000
ug/L
25000
25000
1
05/23/18 12:30
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
2890J
ug/L
250000
500
1
05/23/18 08:12
14808-79-8
4500 Chloride
Analytical Method: SM
4500-CI-E
Chloride
1340
ug/L
1000
500
1
05/30/1815:18
16887-00-6
Date: 06/01 /2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-24S Lab ID: 92385350004 Collected: 05/16/18 13:15 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
05/29/18 16:05
06/01/18 01:57
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:57
7440-38-2
Barium
42.4J
ug/L
100
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:57
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/29/18 16:05
06/01/18 01:57
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-50-8
Iron
1570
ug/L
300
25.0
1
05/29/18 16:05
06/01/18 01:57
7439-89-6
Lead
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7439-92-1
Manganese
29.5J
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7439-96-5
Nickel
ND
ug/L
50.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:57
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-22-4
Tin
ND
ug/L
5.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-31-5
Vanadium
ND
ug/L
25.0
2.5
1
05/29/18 16:05
06/01/18 01:57
7440-62-2
Zinc
7.OJ
ug/L
10.0
5.0
1
05/29/18 16:05
06/01/18 01:57
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020
Preparation
Method: EPA 3010
Thallium
ND
ug/L
27.5
2.5
5
05/24/18 20:15
05/25/18 04:29
7440-28-0 D3
7470 Mercury
Analytical Method: EPA 7470
Preparation
Method: EPA 7470
Mercury
ND
ug/L
0.20
0.10
1
05/31/1810:00
05/31/1819:35
7439-97-6
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
ND
ug/L
100
10.0
1
05/30/18 07:33
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
05/30/18 07:33
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
05/30/18 07:33
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
05/30/18 07:33
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
05/30/18 07:33
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
05/30/18 07:33
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
05/30/18 07:33
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
05/30/18 07:33
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
05/30/18 07:33
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
05/30/18 07:33
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
05/30/18 07:33
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
05/30/18 07:33
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
05/30/18 07:33
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
05/30/18 07:33
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
05/30/18 07:33
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
05/30/18 07:33
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
05/30/18 07:33
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
05/30/18 07:33
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
05/30/18 07:33
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
05/30/18 07:33
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
05/30/18 07:33
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 42

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-24S Lab ID: 92385350004 Collected: 05/16/18 13:15 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
05/30/18 07:33
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
05/30/18 07:33
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
05/30/18 07:33
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
05/30/18 07:33
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
05/30/18 07:33
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
05/30/18 07:33
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
05/30/18 07:33
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
05/30/18 07:33
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
05/30/18 07:33
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
05/30/18 07:33
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
05/30/18 07:33
74-88-4
Isobutanol
ND
ug/L
100
35.0
1
05/30/18 07:33
78-83-1
Methylene Chloride
ND
ug/L
1.0
0.97
1
05/30/18 07:33
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
05/30/18 07:33
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
05/30/18 07:33
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
05/30/18 07:33
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
05/30/18 07:33
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
05/30/18 07:33
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
05/30/18 07:33
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
05/30/18 07:33
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
05/30/18 07:33
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
05/30/18 07:33
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
05/30/18 07:33
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
05/30/18 07:33
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
05/30/18 07:33
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
05/30/18 07:33
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
05/30/18 07:33
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
05/30/18 07:33
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
05/30/18 07:33
460-00-4
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
05/30/18 07:33
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
05/30/18 07:33
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B
Alkalinity, Total as CaCO3
5010
ug/L
5000
1000
1
05/24/18 20:52
2540C Total Dissolved Solids
Analytical Method: SM
2540C
Total Dissolved Solids
31000
ug/L
25000
25000
1
05/23/18 12:30
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
ND
ug/L
250000
500
1
05/23/18 09:45
14808-79-8
4500 Chloride
Analytical Method: SM
4500-CI-E
Chloride
2680
ug/L
1000
500
1
05/30/1815:19
16887-00-6
Date: 06/01 /2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-30 Lab ID: 92385350005 Collected: 05/16/18 12:55 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
05/29/1816:05
05/31/1816:16
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
05/29/1816:05
05/31/1816:16
7440-38-2
Barium
44.9J
ug/L
100
2.5
1
05/29/1816:05
05/31/1816:16
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
05/29/1816:05
05/31/1816:16
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
05/29/1816:05
05/31/1816:16
7440-43-9
Chromium
3.1J
ug/L
10.0
2.5
1
05/29/1816:05
05/31/1816:16
7440-47-3
Cobalt
3.6J
ug/L
10.0
2.5
1
05/29/1816:05
05/31/1816:16
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
05/29/1816:05
05/31/1816:16
7440-50-8
Iron
3140
ug/L
300
25.0
1
05/29/1816:05
05/31/1816:16
7439-89-6
Lead
2.8J
ug/L
10.0
2.5
1
05/29/1816:05
05/31/1816:16
7439-92-1
Manganese
762
ug/L
50.0
2.5
1
05/29/1816:05
05/31/1816:16
7439-96-5
Nickel
3.4J
ug/L
50.0
2.5
1
05/29/1816:05
05/31/1816:16
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
05/29/1816:05
05/31/1816:16
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
05/29/1816:05
05/31/1816:16
7440-22-4
Tin
ND
ug/L
5.0
2.5
1
05/29/1816:05
05/31/1816:16
7440-31-5
Vanadium
4.7J
ug/L
25.0
2.5
1
05/29/1816:05
05/31/1816:16
7440-62-2
Zinc
9.01
ug/L
10.0
5.0
1
05/29/1816:05
05/31/1816:16
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020
Preparation
Method: EPA 3010
Thallium
ND
ug/L
27.5
2.5
5
05/24/18 20:15
05/25/18 04:31
7440-28-0 D3
7470 Mercury
Analytical Method: EPA 7470
Preparation
Method: EPA 7470
Mercury
ND
ug/L
0.20
0.10
1
05/31/1810:00
05/31/1819:37
7439-97-6
8260 MSV Low Level Landfill
Analytical Method: EPA 8260
Acetone
ND
ug/L
100
10.0
1
05/30/18 07:49
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
05/30/18 07:49
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
05/30/18 07:49
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
05/30/18 07:49
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
05/30/18 07:49
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
05/30/18 07:49
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
05/30/18 07:49
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
05/30/18 07:49
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
05/30/18 07:49
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
05/30/18 07:49
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
05/30/18 07:49
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
05/30/18 07:49
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
05/30/18 07:49
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
05/30/18 07:49
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
05/30/18 07:49
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
05/30/18 07:49
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
05/30/18 07:49
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
05/30/18 07:49
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
05/30/18 07:49
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
05/30/18 07:49
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
05/30/18 07:49
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 42

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ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-30 Lab ID: 92385350005 Collected: 05/16/18 12:55 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
05/30/18 07:49
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
05/30/18 07:49
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
05/30/18 07:49
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
05/30/18 07:49
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
05/30/18 07:49
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
05/30/18 07:49
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
05/30/18 07:49
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
05/30/18 07:49
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
05/30/18 07:49
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
05/30/18 07:49
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
05/30/18 07:49
74-88-4
Isobutanol
ND
ug/L
100
35.0
1
05/30/18 07:49
78-83-1
Methylene Chloride
ND
ug/L
1.0
0.97
1
05/30/18 07:49
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
05/30/18 07:49
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
05/30/18 07:49
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
05/30/18 07:49
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
05/30/18 07:49
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
05/30/18 07:49
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
05/30/18 07:49
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
05/30/18 07:49
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
05/30/18 07:49
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
05/30/18 07:49
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
05/30/18 07:49
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
05/30/18 07:49
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
05/30/18 07:49
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
05/30/18 07:49
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
05/30/18 07:49
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
05/30/18 07:49
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
05/30/18 07:49
460-00-4
1,2-Dichloroethane-d4 (S)
95
%
70-130
1
05/30/18 07:49
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
05/30/18 07:49
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B
Alkalinity, Total as CaCO3
25000
ug/L
5000
1000
1
05/24/18 21:01
2540C Total Dissolved Solids
Analytical Method: SM
2540C
Total Dissolved Solids
56000
ug/L
25000
25000
1
05/23/18 12:30
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
ND
ug/L
250000
500
1
05/23/1810:02
14808-79-8
4500 Chloride
Analytical Method: SM
4500-CI-E
Chloride
1480
ug/L
1000
500
1
05/30/1815:23
16887-00-6
Date: 06/01 /2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 42

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ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-35 Lab ID: 92385350006 Collected: 05/16/18 11:40 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Tin
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Date: 06/01 /2018 03:42 PM
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
05/30/18 12:00
05/31/18 22:00
7440-36-0
ND
ug/L
10.0
5.0
1
05/30/18 12:00
05/31/18 22:00
7440-38-2
22.1J
ug/L
100
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-39-3
ND
ug/L
1.0
0.50
1
05/30/18 12:00
05/31/18 22:00
7440-41-7
ND
ug/L
1.0
0.50
1
05/30/18 12:00
05/31/18 22:00
7440-43-9
ND
ug/L
10.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-47-3
ND
ug/L
10.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-48-4
ND
ug/L
10.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-50-8
110J
ug/L
300
25.0
1
05/30/18 12:00
05/31/18 22:00
7439-89-6
ND
ug/L
10.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7439-92-1
ND
ug/L
50.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7439-96-5
ND
ug/L
50.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-02-0
ND
ug/L
10.0
5.0
1
05/30/18 12:00
05/31/18 22:00
7782-49-2
ND
ug/L
10.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-22-4
ND
ug/L
5.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-31-5
ND
ug/L
25.0
2.5
1
05/30/18 12:00
05/31/18 22:00
7440-62-2
ND
ug/L
10.0
5.0
1
05/30/18 12:00
05/31/18 22:00
7440-66-6
Analytical Method: EPA 6020 Preparation Method: EPA 3010
ND ug/L 27.5 2.5 5 05/24/18 20:15 05/25/18 04:32 7440-28-0 D3
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.10 1 05/31/18 10:00 05/31/18 19:39 7439-97-6
Analytical Method: EPA 8260
ND
ug/L
100
10.0
1
05/30/18 08:05
67-64-1
ND
ug/L
200
1.9
1
05/30/18 08:05
107-13-1
ND
ug/L
1.0
0.25
1
05/30/18 08:05
71-43-2
ND
ug/L
3.0
0.17
1
05/30/18 08:05
74-97-5
ND
ug/L
1.0
0.18
1
05/30/18 08:05
75-27-4
ND
ug/L
3.0
0.26
1
05/30/18 08:05
75-25-2
ND
ug/L
10.0
0.29
1
05/30/18 08:05
74-83-9
ND
ug/L
100
0.96
1
05/30/18 08:05
78-93-3
ND
ug/L
100
1.2
1
05/30/18 08:05
75-15-0
ND
ug/L
1.0
0.25
1
05/30/18 08:05
56-23-5
ND
ug/L
3.0
0.23
1
05/30/18 08:05
108-90-7
ND
ug/L
10.0
0.54
1
05/30/18 08:05
75-00-3
ND
ug/L
5.0
0.14
1
05/30/18 08:05
67-66-3
ND
ug/L
1.0
0.11
1
05/30/18 08:05
74-87-3
ND
ug/L
13.0
2.0
1
05/30/18 08:05
96-12-8
ND
ug/L
3.0
0.21
1
05/30/18 08:05
124-48-1
ND
ug/L
1.0
0.27
1
05/30/18 08:05
106-93-4
ND
ug/L
10.0
0.21
1
05/30/18 08:05
74-95-3
ND
ug/L
5.0
0.30
1
05/30/18 08:05
95-50-1
ND
ug/L
1.0
0.33
1
05/30/18 08:05
106-46-7
ND
ug/L
100
1.0
1
05/30/18 08:05
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 42

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ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Sample: MW-35 Lab ID: 92385350006 Collected: 05/16/18 11:40 Received: 05/18/18 12:12 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Isobutanol
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
2540C Total Dissolved Solids
Total Dissolved Solids
300.0 IC Anions 28 Days
Sulfate
4500 Chloride
Chloride
Date: 06/01 /2018 03:42 PM
Analytical Method: EPA 8260
ND
ug/L
5.0
0.32
1
05/30/18 08:05
75-34-3
ND
ug/L
1.0
0.24
1
05/30/18 08:05
107-06-2
ND
ug/L
5.0
0.56
1
05/30/18 08:05
75-35-4
ND
ug/L
5.0
0.19
1
05/30/18 08:05
156-59-2
ND
ug/L
5.0
0.49
1
05/30/18 08:05
156-60-5
ND
ug/L
1.0
0.27
1
05/30/18 08:05
78-87-5
ND
ug/L
1.0
0.13
1
05/30/18 08:05
10061-01-5
ND
ug/L
1.0
0.26
1
05/30/18 08:05
10061-02-6
ND
ug/L
1.0
0.30
1
05/30/18 08:05
100-41-4
ND
ug/L
50.0
0.46
1
05/30/18 08:05
591-78-6
ND
ug/L
10.0
0.32
1
05/30/18 08:05
74-88-4
ND
ug/L
100
35.0
1
05/30/18 08:05
78-83-1
ND
ug/L
1.0
0.97
1
05/30/18 08:05
75-09-2
ND
ug/L
100
0.33
1
05/30/18 08:05
108-10-1
ND
ug/L
1.0
0.26
1
05/30/18 08:05
100-42-5
ND
ug/L
5.0
0.33
1
05/30/18 08:05
630-20-6
ND
ug/L
3.0
0.40
1
05/30/18 08:05
79-34-5
ND
ug/L
1.0
0.46
1
05/30/18 08:05
127-18-4
ND
ug/L
10.0
3.1
1
05/30/18 08:05
109-99-9
ND
ug/L
1.0
0.26
1
05/30/18 08:05
108-88-3
ND
ug/L
1.0
0.48
1
05/30/18 08:05
71-55-6
ND
ug/L
1.0
0.29
1
05/30/18 08:05
79-00-5
ND
ug/L
1.0
0.47
1
05/30/18 08:05
79-01-6
ND
ug/L
1.0
0.20
1
05/30/18 08:05
75-69-4
ND
ug/L
1.0
0.41
1
05/30/18 08:05
96-18-4
ND
ug/L
50.0
0.35
1
05/30/18 08:05
108-05-4
ND
ug/L
1.0
0.62
1
05/30/18 08:05
75-01-4
ND
ug/L
5.0
0.66
1
05/30/18 08:05
1330-20-7
96
%
70-130
1
05/30/18 08:05
460-00-4
94
%
70-130
1
05/30/18 08:05
17060-07-0
102
%
70-130
1
05/30/18 08:05
2037-26-5
Analytical Method: SM
2320B
8870
ug/L
5000
1000
1
05/24/18 21:12
Analytical Method: SM
2540C
27000
ug/L
25000
25000
1
05/23/1812:51
Analytical Method: EPA 300.0
561J
ug/L
250000
500
1
05/26/18 03:43
14808-79-8
Analytical Method: SM
4500-CI-E
1320
ug/L
1000
500
1
05/30/1815:24
16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
W
Page 19 of 42

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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 412925
Analysis Method: EPA 7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury
Associated Lab Samples: 92385350001, 92385350002,
92385350003, 92385350004, 92385350005, 92385350006
METHOD BLANK: 2290327
Matrix: Water
Associated Lab Samples: 92385350001, 92385350002,
92385350003, 92385350004, 92385350005, 92385350006
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Mercury ug/L
ND 0.20 0.10 05/31/1819:09
LABORATORY CONTROL SAMPLE: 2290328
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury ug/L
2.5 2.4 95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2290329 2290330
MS MSD
92385346001
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Mercury ug/L ND
2.5 2.5 2.4 2.4 94 94
75-125 0 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 42

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[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 412695 Analysis Method: EPA 6010
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005
METHOD BLANK: 2289297 Matrix: Water
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005
Blank Reporting
Parameter Units Result Limit MDL
Analyzed
Antimony
ug/L
ND
6.0
3.9
06/01/18 01:23
Arsenic
ug/L
ND
10.0
5.0
06/01/18 01:23
Barium
ug/L
ND
100
2.5
06/01/18 01:23
Beryllium
ug/L
ND
1.0
0.50
06/01/18 01:23
Cadmium
ug/L
ND
1.0
0.50
06/01/18 01:23
Chromium
ug/L
ND
10.0
2.5
06/01/18 01:23
Cobalt
ug/L
ND
10.0
2.5
06/01/18 01:23
Copper
ug/L
ND
10.0
2.5
06/01/18 01:23
Iron
ug/L
ND
300
25.0
06/01/18 01:23
Lead
ug/L
ND
10.0
2.5
06/01/18 01:23
Manganese
ug/L
ND
50.0
2.5
06/01/18 01:23
Nickel
ug/L
ND
50.0
2.5
06/01/18 01:23
Selenium
ug/L
ND
10.0
5.0
06/01/18 01:23
Silver
ug/L
ND
10.0
2.5
06/01/18 01:23
Tin
ug/L
ND
5.0
2.5
06/01/18 01:23
Vanadium
ug/L
ND
25.0
2.5
06/01/18 01:23
Zinc
ug/L
ND
10.0
5.0
06/01/18 01:23
LABORATORY CONTROL SAMPLE:
Parameter
2289298
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
482
96
80-120
Arsenic
ug/L
500
462
92
80-120
Barium
ug/L
500
530
106
80-120
Beryllium
ug/L
500
526
105
80-120
Cadmium
ug/L
500
490
98
80-120
Chromium
ug/L
500
500
100
80-120
Cobalt
ug/L
500
478
96
80-120
Copper
ug/L
500
509
102
80-120
Iron
ug/L
5000
5260
105
80-120
Lead
ug/L
500
472
94
80-120
Manganese
ug/L
500
485
97
80-120
Nickel
ug/L
500
488
98
80-120
Selenium
ug/L
500
461
92
80-120
Silver
ug/L
250
247
99
80-120
Tin
ug/L
500
480
96
80-120
Vanadium
ug/L
500
500
100
80-120
Zinc
ug/L
500
458
92
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 42

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
2289299
2289300
MS
MSD
92385346001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
483
472
96
94
75-125
2
20
Arsenic
ug/L
ND
500
500
461
451
92
90
75-125
2
20
Barium
ug/L
ND
500
500
528
518
106
104
75-125
2
20
Beryllium
ug/L
ND
500
500
523
514
105
103
75-125
2
20
Cadmium
ug/L
ND
500
500
488
479
98
96
75-125
2
20
Chromium
ug/L
ND
500
500
494
487
99
97
75-125
2
20
Cobalt
ug/L
ND
500
500
476
467
95
93
75-125
2
20
Copper
ug/L
ND
500
500
506
494
101
99
75-125
2
20
Iron
ug/L
ND
5000
5000
5240
5160
105
103
75-125
2
20
Lead
ug/L
ND
500
500
471
462
94
92
75-125
2
20
Manganese
ug/L
ND
500
500
482
472
96
94
75-125
2
20
Nickel
ug/L
ND
500
500
486
479
97
96
75-125
1
20
Selenium
ug/L
ND
500
500
462
452
92
90
75-125
2
20
Silver
ug/L
ND
250
250
247
240
99
96
75-125
3
20
Tin
ug/L
ND
500
500
478
468
96
94
75-125
2
20
Vanadium
ug/L
ND
500
500
496
486
99
97
75-125
2
20
Zinc
ug/L
ND
500
500
453
443
91
89
75-125
2
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 42

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 412778 Analysis Method: EPA 6010
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92385350006
METHOD BLANK: 2289725
Associated Lab Samples: 92385350006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
6.0
3.9
05/31/18 21:54
Arsenic
ug/L
ND
10.0
5.0
05/31/18 21:54
Barium
ug/L
ND
100
2.5
05/31/18 21:54
Beryllium
ug/L
ND
1.0
0.50
05/31/18 21:54
Cadmium
ug/L
ND
1.0
0.50
05/31/18 21:54
Chromium
ug/L
ND
10.0
2.5
05/31/18 21:54
Cobalt
ug/L
ND
10.0
2.5
05/31/18 21:54
Copper
ug/L
ND
10.0
2.5
05/31/18 21:54
Iron
ug/L
ND
300
25.0
05/31/18 21:54
Lead
ug/L
ND
10.0
2.5
05/31/18 21:54
Manganese
ug/L
ND
50.0
2.5
05/31/18 21:54
Nickel
ug/L
ND
50.0
2.5
05/31/18 21:54
Selenium
ug/L
ND
10.0
5.0
05/31/18 21:54
Silver
ug/L
ND
10.0
2.5
05/31/18 21:54
Tin
ug/L
ND
5.0
2.5
05/31/18 21:54
Vanadium
ug/L
ND
25.0
2.5
05/31/18 21:54
Zinc
ug/L
ND
10.0
5.0
05/31/18 21:54
LABORATORY CONTROL SAMPLE:
2289726
Parameter
Units
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Iron
ug/L
Lead
ug/L
Manganese
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Tin
ug/L
Vanadium
ug/L
Zinc
ug/L
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
500
487
97
80-120
500
472
94
80-120
500
498
100
80-120
500
497
99
80-120
500
486
97
80-120
500
484
97
80-120
500
479
96
80-120
500
500
100
80-120
5000
4920
98
80-120
500
473
95
80-120
500
468
94
80-120
500
482
96
80-120
500
473
95
80-120
250
243
97
80-120
500
480
96
80-120
500
481
96
80-120
500
462
92
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 42

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
2289727
2289728
MS
MSD
92385350006
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
497
491
99
98
75-125
1
20
Arsenic
ug/L
ND
500
500
485
478
97
96
75-125
1
20
Barium
ug/L
22.1J
500
500
534
527
102
101
75-125
1
20
Beryllium
ug/L
ND
500
500
511
505
102
101
75-125
1
20
Cadmium
ug/L
ND
500
500
495
492
99
98
75-125
1
20
Chromium
ug/L
ND
500
500
496
489
99
98
75-125
1
20
Cobalt
ug/L
ND
500
500
489
485
98
97
75-125
1
20
Copper
ug/L
ND
500
500
515
507
103
101
75-125
2
20
Iron
ug/L
1101
5000
5000
5150
5110
101
100
75-125
1
20
Lead
ug/L
ND
500
500
482
477
96
95
75-125
1
20
Manganese
ug/L
ND
500
500
482
480
96
95
75-125
1
20
Nickel
ug/L
ND
500
500
492
488
98
97
75-125
1
20
Selenium
ug/L
ND
500
500
480
477
96
95
75-125
1
20
Silver
ug/L
ND
250
250
249
245
100
98
75-125
2
20
Tin
ug/L
ND
500
500
492
489
98
97
75-125
1
20
Vanadium
ug/L
ND
500
500
495
490
99
98
75-125
1
20
Zinc
ug/L
ND
500
500
472
470
94
94
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 42

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 450041
Analysis Method: EPA 6020
QC Batch Method: EPA 3010
Analysis Description: 6020 MET
Associated Lab Samples: 92385350001, 92385350002,
92385350003, 92385350004, 92385350005, 92385350006
METHOD BLANK: 2438657
Matrix: Water
Associated Lab Samples: 92385350001, 92385350002,
92385350003, 92385350004, 92385350005, 92385350006
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Thallium ug/L
ND 5.5
0.50 05/25/18 04:01
LABORATORY CONTROL SAMPLE: 2438658
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
50 50.3 101
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2438659 2438660
MS MSD
92384698001
Spike Spike MS MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec
Limits RPD RPD Qual
Thallium ug/L ND
50 50 49.9 50.4
99 100
75-125 1 20 D3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 412680 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005, 92385350006
METHOD BLANK: 2289194 Matrix: Water
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005, 92385350006
Blank Reporting
Parameter Units Result Limit MDL Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
0.33
05/30/18 04:19
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
05/30/18 04:19
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
0.40
05/30/18 04:19
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
05/30/18 04:19
1,1-Dichloroethane
ug/L
ND
5.0
0.32
05/30/18 04:19
1,1-Dichloroethene
ug/L
ND
5.0
0.56
05/30/18 04:19
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
05/30/18 04:19
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
2.0
05/30/18 04:19
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
05/30/18 04:19
1,2-Dichlorobenzene
ug/L
ND
5.0
0.30
05/30/18 04:19
1,2-Dichloroethane
ug/L
ND
1.0
0.24
05/30/18 04:19
1,2-Dichloropropane
ug/L
ND
1.0
0.27
05/30/18 04:19
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
05/30/18 04:19
2-Butanone (MEK)
ug/L
ND
100
0.96
05/30/18 04:19
2-Hexanone
ug/L
ND
50.0
0.46
05/30/18 04:19
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
0.33
05/30/18 04:19
Acetone
ug/L
ND
100
10.0
05/30/18 04:19
Acrylonitrile
ug/L
ND
200
1.9
05/30/18 04:19
Benzene
ug/L
ND
1.0
0.25
05/30/18 04:19
Bromochloromethane
ug/L
ND
3.0
0.17
05/30/18 04:19
Bromodichloromethane
ug/L
ND
1.0
0.18
05/30/18 04:19
Bromoform
ug/L
ND
3.0
0.26
05/30/18 04:19
Bromomethane
ug/L
ND
10.0
0.29
05/30/18 04:19
Carbon disulfide
ug/L
ND
100
1.2
05/30/18 04:19
Carbon tetrachloride
ug/L
ND
1.0
0.25
05/30/18 04:19
Chlorobenzene
ug/L
ND
3.0
0.23
05/30/18 04:19
Chloroethane
ug/L
ND
10.0
0.54
05/30/18 04:19
Chloroform
ug/L
ND
5.0
0.14
05/30/18 04:19
Chloromethane
ug/L
ND
1.0
0.11
05/30/18 04:19
cis-1,2-Dichloroethene
ug/L
ND
5.0
0.19
05/30/18 04:19
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
05/30/18 04:19
Dibromochloromethane
ug/L
ND
3.0
0.21
05/30/18 04:19
Dibromomethane
ug/L
ND
10.0
0.21
05/30/18 04:19
Ethylbenzene
ug/L
ND
1.0
0.30
05/30/18 04:19
lodomethane
ug/L
ND
10.0
0.32
05/30/18 04:19
Isobutanol
ug/L
ND
100
35.0
05/30/18 04:19
Methylene Chloride
ug/L
ND
1.0
0.97
05/30/18 04:19
Styrene
ug/L
ND
1.0
0.26
05/30/18 04:19
Tetrachloroethene
ug/L
ND
1.0
0.46
05/30/18 04:19
Tetrahydrofuran
ug/L
ND
10.0
3.1
05/30/18 04:19
Toluene
ug/L
ND
1.0
0.26
05/30/18 04:19
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
METHOD BLANK: 2289194 Matrix: Water
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005, 92385350006
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
5.0
0.49
05/30/18 04:19
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
05/30/18 04:19
trans-1,4-Dichloro-2-butene
ug/L
ND
100
1.0
05/30/18 04:19
Trichloroethene
ug/L
ND
1.0
0.47
05/30/18 04:19
Trichlorofluoromethane
ug/L
ND
1.0
0.20
05/30/18 04:19
Vinyl acetate
ug/L
ND
50.0
0.35
05/30/18 04:19
Vinyl chloride
ug/L
ND
1.0
0.62
05/30/18 04:19
Xylene (Total)
ug/L
ND
5.0
0.66
05/30/18 04:19
1,2-Dichloroethane-d4 (S)
%
92
70-130
05/30/18 04:19
4-Bromofluorobenzene (S)
%
98
70-130
05/30/18 04:19
Toluene-d8 (S)
%
100
70-130
05/30/18 04:19
LABORATORY CONTROL SAMPLE:
2289195
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
52.7
105
80-125
1,1,1-Trichloroethane
ug/L
50
49.9
100
71-129
1,1,2,2-Tetrachloroethane
ug/L
50
52.8
106
79-124
1,1,2-Trichloroethane
ug/L
50
51.6
103
85-125
1,1-Dichloroethane
ug/L
50
47.1
94
73-126
1,1-Dichloroethene
ug/L
50
48.6
97
66-135
1,2,3-Trichloropropane
ug/L
50
51.0
102
75-130
1,2-Dibromo-3-chloropropane
ug/L
50
56.5
113
71-133
1,2-Dibromoethane (EDB)
ug/L
50
52.6
105
83-124
1,2-Dichlorobenzene
ug/L
50
50.5
101
80-133
1,2-Dichloroethane
ug/L
50
45.6
91
67-128
1,2-Dichloropropane
ug/L
50
50.9
102
75-132
1,4-Dichlorobenzene
ug/L
50
48.8
98
78-130
2-Butanone (MEK)
ug/L
100
91.6J
92
61-144
2-Hexanone
ug/L
100
97.6
98
68-143
4-Methyl-2-pentanone (MIBK)
ug/L
100
93.5J
93
72-135
Acetone
ug/L
100
90.1 J
90
48-146
Acrylonitrile
ug/L
250
256
102
40-160
Benzene
ug/L
50
50.9
102
80-125
Bromochloromethane
ug/L
50
51.2
102
71-125
Bromodichloromethane
ug/L
50
52.8
106
78-124
Bromoform
ug/L
50
56.2
112
71-128
Bromomethane
ug/L
50
37.4
75
40-160
Carbon disulfide
ug/L
50
49.1J
98
50-160
Carbon tetrachloride
ug/L
50
50.8
102
69-131
Chlorobenzene
ug/L
50
51.1
102
81-122
Chloroethane
ug/L
50
33.2
66
39-148
Chloroform
ug/L
50
49.9
100
73-127
Chloromethane
ug/L
50
36.7
73
44-146
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 42

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
LABORATORY CONTROL SAMPLE:
2289195
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
49.1
98
74-124
cis-1,3-Dichloropropene
ug/L
50
51.8
104
72-132
Dibromochloromethane
ug/L
50
55.6
111
78-125
Dibromomethane
ug/L
50
53.2
106
82-120
Ethylbenzene
ug/L
50
51.0
102
79-121
lodomethane
ug/L
100
78.8
79
39-154
Isobutanol
ug/L
1000
1020
102
34-160
Methylene Chloride
ug/L
50
46.0
92
64-133
Styrene
ug/L
50
52.5
105
84-126
Tetrachloroethene
ug/L
50
43.8
88
78-122
Tetrahydrofuran
ug/L
500
466
93
69-148
Toluene
ug/L
50
49.7
99
80-121
trans-1,2-Dichloroethene
ug/L
50
49.3
99
71-127
trans- 1,3-Dichloropropene
ug/L
50
51.9
104
69-141
trans-1,4-Dichloro-2-butene
ug/L
50
50.5J
101
40-160
Trichloroethene
ug/L
50
50.0
100
78-122
Trichlorofluoromethane
ug/L
50
47.6
95
53-137
Vinyl acetate
ug/L
100
109
109
40-160
Vinyl chloride
ug/L
50
47.1
94
58-137
Xylene (Total)
ug/L
150
154
103
81-126
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
2289196
92385968005
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
21.3
107
70-130
1,1,1-Trichloroethane
ug/L
ND
20
21.0
105
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
20
21.4
107
70-130
1,1,2-Trichloroethane
ug/L
ND
20
21.4
107
70-130
1,1-Dichloroethane
ug/L
ND
20
19.6
98
70-130
1,1-Dichloroethene
ug/L
ND
20
21.5
108
70-166
1,2,3-Trichloropropane
ug/L
ND
20
21.4
107
70-130
1,2-Dibromo-3-chloropropane
ug/L
ND
20
21.2
106
70-130
1,2-Dibromoethane (EDB)
ug/L
ND
20
21.1
106
70-130
1,2-Dichlorobenzene
ug/L
ND
20
20.6
103
70-130
1,2-Dichloroethane
ug/L
ND
20
19.7
98
70-130
1,2-Dichloropropene
ug/L
ND
20
21.6
108
70-130
1,4-Dichlorobenzene
ug/L
ND
20
20.3
102
70-130
2-Butanone (MEK)
ug/L
ND
40
37.7J
94
70-130
2-Hexanone
ug/L
ND
40
39.3J
98
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
38.2J
95
70-130
Acetone
ug/L
ND
40
37AJ
94
70-130
Acrylonitrile
ug/L
ND
100
1011
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
MATRIX SPIKE SAMPLE:
Parameter
2289196
Units
92385968005
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
22.0
110
70-148
Bromochloromethane
ug/L
ND
20
21.4
107
70-130
Bromodichloromethane
ug/L
ND
20
21.2
106
70-130
Bromoform
ug/L
ND
20
20.1
100
70-130
Bromomethane
ug/L
ND
20
11.0
55
70-130 M1
Carbon disulfide
ug/L
ND
20
21.1J
105
70-130
Carbon tetrachloride
ug/L
ND
20
22.1
110
70-130
Chlorobenzene
ug/L
ND
20
21.6
108
70-146
Chloroethane
ug/L
ND
20
17.6
88
70-130
Chloroform
ug/L
ND
20
20.2
101
70-130
Chloromethane
ug/L
ND
20
16.5
83
70-130
cis-1,2-Dichloroethene
ug/L
ND
20
20.8
104
70-130
cis-1,3-Dichloropropene
ug/L
ND
20
21.5
108
70-130
Dibromochloromethane
ug/L
ND
20
21.1
106
70-130
Dibromomethane
ug/L
ND
20
21.9
109
70-130
Ethylbenzene
ug/L
ND
20
21.8
109
70-130
lodomethane
ug/L
ND
40
28.5
71
70-130
Isobutanol
ug/L
ND
400
393
98
70-130
Methylene Chloride
ug/L
ND
20
14.8
74
70-130
Styrene
ug/L
ND
20
21.4
107
70-130
Tetrachloroethene
ug/L
ND
20
18.9
95
70-130
Tetrahydrofuran
ug/L
ND
200
189
94
70-130
Toluene
ug/L
ND
20
21.2
106
70-155
trans-1,2-Dichloroethene
ug/L
ND
20
21.2
106
70-130
trans- 1,3-Dichloropropene
ug/L
ND
20
21.2
106
70-130
trans-1,4-Dichloro-2-butene
ug/L
ND
20
18.7J
93
70-130
Trichloroethene
ug/L
ND
20
21.8
109
69-151
Trichlorofluoromethane
ug/L
ND
20
22.3
111
70-130
Vinyl acetate
ug/L
ND
40
43.5J
109
70-130
Vinyl chloride
ug/L
ND
20
21.9
109
70-130
Xylene (Total)
ug/L
ND
60
66.1
110
70-130
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE: 2289197
92385968006
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
SAMPLE DUPLICATE: 2289197
Parameter
Units
92385968006
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
Isobutanol
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Tetrahydrofuran
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
92
93
4-Bromofluorobenzene (S)
%
96
98
Toluene-d8(S)
%
100
101
Max
RPD RPD Qualifiers
1
2
1
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 412060 Analysis Method: SM 2320B
QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005, 92385350006
METHOD BLANK: 2285867 Matrix: Water
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005, 92385350006
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Alkalinity, Total as CaCO3 ug/L ND 5000 1000 05/24/18 16:22
LABORATORY CONTROL SAMPLE: 2285868
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L 50000 51800 104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2285869 2285870
MS MSD
92385024001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 20.5 mg/L 50000 50000 70700 72100 101 103 80-120 2 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2285871 2285872
MS MSD
92385049013 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 668 mg/L 50000 50000 713000 716000 90 96 80-120 0 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 31 of 42

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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 411996
Analysis Method: SM 2540C
QC Batch Method: SM 2540C
Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005
METHOD BLANK: 2285346
Matrix: Water
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005
Blank Reporting
Parameter
Units
Result Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND 25000 25000 05/23/18 12:30
LABORATORY CONTROL SAMPLE:
2285347
Spike LCS LCS
% Rec
Parameter
Units
Conc. Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
250000 260000 104
90-110
SAMPLE DUPLICATE: 2285348
92385053009 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
100 mg/L 97000
3 5
SAMPLE DUPLICATE: 2285349
92385163001 Dup
Max
Parameter
Units
Result Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
ND 26000
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 411997
Analysis Method: SM 2540C
QC Batch Method: SM 2540C
Analysis Description:
2540C Total Dissolved Solids
Associated Lab Samples: 92385350006
METHOD BLANK: 2285355
Matrix:
Water
Associated Lab Samples: 92385350006
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND
25000 25000
05/23/18 12:51
LABORATORY CONTROL SAMPLE: 2285356
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
250000
250000 100
90-110
SAMPLE DUPLICATE: 2285357
92385350006
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
27000
29000 7
5 D6
SAMPLE DUPLICATE: 2285358
92385230002
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
62.0 mg/L
62000 0
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 411763
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92385350001, 92385350002,
92385350003, 92385350004, 92385350005
METHOD BLANK: 2284255
Matrix: Water
Associated Lab Samples: 92385350001, 92385350002,
92385350003, 92385350004, 92385350005
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Sulfate ug/L
ND 250000 500 05/23/18 00:25
LABORATORY CONTROL SAMPLE: 2284256
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Sulfate ug/L
50000 47900J 96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2284257 2284258
MS MSD
92385228002
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Sulfate ug/L 15.7 mg/L
50000 50000 66800J 69400J 102 107
90-110 4 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2284259 2284260
MS MSD
92385049011 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfate ug/L 4.7 mg/L 50000 50000 57200J 57800J 105 106 90-110 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 34 of 42

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 412158
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92385350006
METHOD BLANK: 2286340
Matrix: Water
Associated Lab Samples: 92385350006
Blank Reporting
Parameter Units
Result Limit
MDL
Analyzed
Qualifiers
Sulfate ug/L
ND 250000
500 05/25/18 21:46
LABORATORY CONTROL SAMPLE: 2286341
Spike LCS
LCS
% Rec
Parameter Units
Conc. Result
% Rec
Limits Qualifiers
Sulfate ug/L
50000 49600J
99
90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2286342 2286343
MS MSD
92385712002
Spike Spike MS
MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result
Result
% Rec % Rec
Limits RPD RPD Qual
Sulfate ug/L 28.8 mg/L
50000 50000 78200J
81300J
99 105
90-110 4 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2286344 2286345
MS MSD
92385656005 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfate ug/L ND 50000 50000 52800J 50800J 105 101 90-110 4 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92385350
QC Batch: 412774 Analysis Method: SM 4500-CI-E
QC Batch Method: SM 4500-CI-E Analysis Description: 4500 Chloride
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005, 92385350006
METHOD BLANK: 2289695 Matrix: Water
Associated Lab Samples: 92385350001, 92385350002, 92385350003, 92385350004, 92385350005, 92385350006
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Chloride ug/L ND 1000 500 05/30/1814:59
LABORATORY CONTROL SAMPLE: 2289696
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride ug/L 20000 20400 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2289697 2289698
MS MSD
92385656003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chloride ug/L 3.0 mg/L 10000 10000 12700 13000 97 100 90-110 2 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2289699 2289700
MS MSD
92385350004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chloride ug/L 2680 10000 10000 12100 12100 94 94 90-110 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/01 /2018 03:42 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 42

aceAnalytical
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[phone]
QUALIFIERS
Project: Johns River - Expansion GW
Pace Project No.: 92385350
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-O Pace Analytical Services - Ormond Beach
BATCH QUALIFIERS
Batch: 450065
Ill Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Johns River - Expansion GW
92385350
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92385350001
1203-MW-20
EPA 3010A
412695
EPA 6010
412972
92385350002
1203-MW-38
EPA 3010A
412695
EPA 6010
412972
92385350003
MW-23S
EPA 3010A
412695
EPA 6010
412972
92385350004
MW-24S
EPA 3010A
412695
EPA 6010
412972
92385350005
MW-30
EPA 3010A
412695
EPA 6010
412972
92385350006
MW-35
EPA 3010A
412778
EPA 6010
412956
92385350001
1203-MW-20
EPA 3010
450041
EPA 6020
450065
92385350002
1203-MW-38
EPA 3010
450041
EPA 6020
450065
92385350003
MW-23S
EPA 3010
450041
EPA 6020
450065
92385350004
MW-24S
EPA 3010
450041
EPA 6020
450065
92385350005
MW-30
EPA 3010
450041
EPA 6020
450065
92385350006
MW-35
EPA 3010
450041
EPA 6020
450065
92385350001
1203-MW-20
EPA 7470
412925
EPA 7470
413217
92385350002
1203-MW-38
EPA 7470
412925
EPA 7470
413217
92385350003
MW-23S
EPA 7470
412925
EPA 7470
413217
92385350004
MW-24S
EPA 7470
412925
EPA 7470
413217
92385350005
MW-30
EPA 7470
412925
EPA 7470
413217
92385350006
MW-35
EPA 7470
412925
EPA 7470
413217
92385350001
1203-MW-20
EPA 8260
412680
92385350002
1203-MW-38
EPA 8260
412680
92385350003
MW-23S
EPA 8260
412680
92385350004
MW-24S
EPA 8260
412680
92385350005
MW-30
EPA 8260
412680
92385350006
MW-35
EPA 8260
412680
92385350001
1203-MW-20
SM 2320B
412060
92385350002
1203-MW-38
SM 2320B
412060
92385350003
MW-23S
SM 2320B
412060
92385350004
MW-24S
SM 2320B
412060
92385350005
MW-30
SM 2320B
412060
92385350006
MW-35
SM 2320B
412060
92385350001
1203-MW-20
SM 2540C
411996
92385350002
1203-MW-38
SM 2540C
411996
92385350003
MW-23S
SM 2540C
411996
92385350004
MW-24S
SM 2540C
411996
92385350005
MW-30
SM 2540C
411996
92385350006
MW-35
SM 2540C
411997
92385350001
1203-MW-20
EPA 300.0
411763
92385350002
1203-MW-38
EPA 300.0
411763
92385350003
MW-23S
EPA 300.0
411763
92385350004
MW-24S
EPA 300.0
411763
92385350005
MW-30
EPA 300.0
411763
92385350006
MW-35
EPA 300.0
412158
92385350001
1203-MW-20
SM 4500-CI-E
412774
92385350002
1203-MW-38
SM 4500-CI-E
412774
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 06/01 /2018 03:42 PM
without the written consent of Pace Analytical Services, LLC.
Page 38 of 42

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Johns River - Expansion GW
Pace Project No.: 92385350
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92385350003
MW-23S
SM 4500-CI-E
412774
92385350004
MW-24S
SM 4500-CI-E
412774
92385350005
MW-30
SM 4500-CI-E
412774
92385350006
MW-35
SM 4500-CI-E
412774
Date: 06/01 /2018 03:42 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 39 of 42

uocument Name:
b Sample Condition Upon Receil
Document No.:
F-CAR-CS-033-Rev.05
VV�u y Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville�' Raleigh❑ Mechanicsville[]
SampleClient Name: WO# : 92385350
Upon•, .. 1.1 C)e 1 (% Proiec•
Courier: []Fed Ex ❑UPS ❑LISPS ❑Client
❑ Commercial '2Pace ❑Other: 92385350
Custody Seal Present? ❑Yes ❑01d-- Seals Intact? Dyes ❑I�e C,�j
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap rBubble Bags ❑None ❑ Other Biological TissueFrozen?
Thermometer: Type of Ice: �h12�❑8iue,'Jane
❑Yes r]No EVA
❑iR Gun io: 92TO40
Cooler Temp (°C): Correction Factor: Add/Subtract (^Cj +0.4 Temp .
should be above freezing to 6-C
�
Cooler Temp Corrected (•C): , q ' ? I]Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil.12-J/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
.,.;_nY 71y.a F—Nc
IJyes IJNO—
Comments/Discrepancy:
Chain of Custody Present?
[]No
❑N/A
i.
Samples Arrived within Hold Time?
#fie
[-]No
❑N/A
?.
Short Hold Time Analysis (<72 hr.)?
❑Yes
21,
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
o
❑NIA
4.
Sufficient Volume?
es
❑Na
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
g?g-
Elyjw
❑No
[:]No
❑NIA
❑N/A
6.
Containers 4ntact?
es
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC?
-Includes Date/'Time/ID/Analysis 4latrix:
Headspace in V0A Viais (>5-Gmm)?
❑Yes
❑Peso
❑Yes .
Z'No
o
❑N/A
❑N/A
❑N/A
S.
9-
10.
TripBlankPresent?
Trip Blank Custody Seals Present?
[]Yes
❑Yes
o
❑ a
❑N/A
❑N/A
1-1.
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESCOL4ITION
Person contacted:
Lot IDofspiit
iZ 1 S5
1�,crc�
patejTime:
containers:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: Date:
Project Manager SRF Review: (G Date:
Page 40 of 42

1�cmAna fyf aS
>ampie Wnamon upon teeter
Document No,:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechjorination is
verified and within the acceptance range for preservation
samples.
Exceptions; VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project W0# : 92385350
PM: RWC Due Date: 06/04/18
CLIENT: 92-Joyce Eng
E
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
'40te: Whenever tPere is a discrepancy airecting North Carolina compElance samples, a cupy u< <nts I I wni oe Set < <u _ G .� w •••• -• •• Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 41 of 42

102 CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
becuon A Section B Section C
Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1
Company. LaBella Associates, D.P.C. - NC Report To: Haley Seaton Altentbn:
Address 2211 W. Meadowview Rd. Copy To: Company Name:
Greensboro, NC 274D7
Address
Regulatory Agency
Email: hseaton labellapc_com
Purchase Order #:
Pace Quote.
Phone: [phone] Fax
Project Name. Johns River - Expansion GW
Pace Project Manager: trey, carter pacelabs_com,
State I Location
Requested Due Dale:
Project #:
Pace Profile #: 2327-4
NC
Requested
Anal
sis
Filtered
YIN
�
2
MATRIX CODE
—
COLLECTED
Z
Preservatives
>'
D—k,ng W.I., DW
Water WT
m
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Waste Water WW
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SAMPLE ID S..VS.I.d SL
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START
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w
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II.I
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DATE
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DATE
TIME
_
=
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WT
X
X
X
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WT
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3
MW-235
WT
-
x
x
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WT
X
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7
8
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11
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ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION
A
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
!z--
SAMPLER NAME AND SIGNATURE
PRINT Name of SAMPLER: p ` }n
�'YLt t9` l l ck't ff-1'>'"u :rL
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SIGNATURE of SA_ MPLER: f n • DATE Signed-
:
m
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LJ iT 1
N
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IL
r—

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 14, 2018
Mr. Van Burbach
Joyce Engineering -Greensboro
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Johns River - Expansion GW
Pace Project No.: 92398011
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on August 31, 2018. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
��i Flo _ _.1I , .�:
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr. Van Burbach, Joyce Engineering -NC
Gretta Eller, LaBella Associates, D.P.C.
Mr. Daniel Girdner, LaBella Associates, D.P.C.
Miguel Vazquez, Joyce Engineering
Rochelle mesubed, Joyce Engineering
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 35

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 35

aceAnalytical
—pacelabsxom
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92398011001
MW-23S
Water
08/29/1816:45
08/31/18 13:37
92398011002
MW-24S
Water
08/30/1813:35
08/31/18 13:37
92398011003
MW-30
Water
08/30/1811:53
08/31/18 13:37
92398011004
MW-35
Water
08/30/18 09:43
08/31/18 13:37
92398011005
Field Blank
Water
08/30/18 13:40
08/31/18 13:37
92398011006
Trip Blank
Water
08/29/18 08:00
08/31/18 13:37
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 35

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Johns River - Expansion GW
92398011
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92398011001
MW-23S
EPA 6010D
IDS
14
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
GAW
50
PASI-C
92398011002
MW-24S
EPA 6010D
DS
14
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
GAW
50
PASI-C
92398011003
MW-30
EPA 6010D
SER
14
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
GAW
50
PASI-C
92398011004
MW-35
EPA 6010D
SER
14
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
GAW
50
PASI-C
92398011005
Field Blank
EPA 6010D
IDS
14
PASI-A
EPA6020B
JMW1
1
PASI-A
EPA 8260E
GAW
50
PASI-C
92398011006
Trip Blank
EPA 8260E
GAW
50
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
Johns River - Expansion GW
92398011
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92398011001
MW-23S
EPA 6010D
Barium
13.OJ
ug/L
100
09/12/18 20:10
EPA 6010D
Chromium
3.6J
ug/L
10.0
09/12/18 20:10
EPA 6010D
Cobalt
6.2J
ug/L
10.0
09/12/18 20:10
EPA 6010D
Lead
3.7J
ug/L
10.0
09/12/18 20:10
EPA 6010D
Vanadium
4.1 J
ug/L
25.0
09/12/18 20:10
EPA 6010D
Zinc
6.5J
ug/L
10.0
09/12/18 20:10
EPA 6020B
Thallium
0.046J
ug/L
5.5
09/07/18 18:43
EPA8260B
Ethylbenzene
1.9
ug/L
1.0
09/11/1817:51
EPA8260B
Toluene
6.7
ug/L
1.0
09/11/1817:51
92398011002
MW-24S
EPA 6010D
Barium
31.6J
ug/L
100
09/12/18 20:22
EPA 6010D
Zinc
8.9J
ug/L
10.0
09/12/18 20:22
EPA 6020B
Thallium
0.074J
ug/L
5.5
09/07/18 18:53
92398011003
MW-30
EPA 6010D
Barium
40.8J
ug/L
100
09/12/18 22:45
EPA 6010D
Chromium
2.9J
ug/L
10.0
09/12/18 22:45
EPA 6010D
Vanadium
2.9J
ug/L
25.0
09/12/18 22:45
EPA 6010D
Zinc
11.0
ug/L
10.0
09/12/18 22:45
EPA 6020B
Thallium
0.061 J
ug/L
5.5
09/07/18 18:56
92398011004
MW-35
EPA 6010D
Barium
146
ug/L
100
09/13/18 20:33
EPA 6010D
Beryllium
0.81 J
ug/L
1.0
09/13/18 20:33
EPA 6010D
Chromium
22.0
ug/L
10.0
09/13/18 20:33
EPA 6010D
Cobalt
5.6J
ug/L
10.0
09/13/18 20:33
EPA 6010D
Copper
26.9
ug/L
10.0
09/13/18 20:33
EPA 6010D
Lead
9.6J
ug/L
10.0
09/13/18 20:33
EPA 6010D
Nickel
8.6J
ug/L
50.0
09/13/18 20:33
EPA 6010D
Vanadium
39.1
ug/L
25.0
09/13/18 20:33
EPA 6010D
Zinc
44.4
ug/L
10.0
09/13/18 20:33
EPA 6020B
Thallium
0.31 J
ug/L
5.5
09/07/18 18:59
92398011005
Field Blank
EPA8260B
Methylene Chloride
4.3
ug/L
1.0
09/11/1814:57 C9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-23S Lab ID: 92398011001 Collected: 08/29/18 16:45 Received: 08/31/18 13:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
Antimony
ND
ug/L
6.0
3.9
1
09/11/18 16:06
09/12/18 20:10
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:10
7440-38-2
Barium
13.OJ
ug/L
100
2.5
1
09/11/18 16:06
09/12/18 20:10
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 20:10
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 20:10
7440-43-9
Chromium
3.6J
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:10
7440-47-3
Cobalt
6.2J
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:10
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:10
7440-50-8
Lead
3.7J
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:10
7439-92-1
Nickel
ND
ug/L
50.0
2.5
1
09/11/18 16:06
09/12/18 20:10
7440-02-0 P8
Selenium
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:10
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:10
7440-22-4
Vanadium
4.1J
ug/L
25.0
2.5
1
09/11/18 16:06
09/12/18 20:10
7440-62-2
Zinc
6.5J
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:10
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.046J
ug/L
5.5
0.020
1
09/06/18 08:24
09/07/18 18:43
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
09/11/18 17:51
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
09/11/18 17:51
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
09/11/18 17:51
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
09/11/18 17:51
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
09/11/18 17:51
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
09/11/18 17:51
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
09/11/18 17:51
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
09/11/18 17:51
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
09/11/18 17:51
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
09/11/18 17:51
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
09/11/18 17:51
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
09/11/18 17:51
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
09/11/18 17:51
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
09/11/18 17:51
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
09/11/18 17:51
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
09/11/18 17:51
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
09/11/18 17:51
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
09/11/18 17:51
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
09/11/18 17:51
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
09/11/18 17:51
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
09/11/18 17:51
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
09/11/18 17:51
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
09/11/18 17:51
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
09/11/18 17:51
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
09/11/18 17:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
09/11/18 17:51
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
09/11/18 17:51
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 35

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-23S
Lab ID:
92398011001
Collected:
08/29/18 16:45
Received: 08/31/18 13:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
09/11/18 17:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
09/11/18 17:51
10061-02-6
Ethylbenzene
1.9
ug/L
1.0
0.30
1
09/11/18 17:51
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
09/11/18 17:51
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
09/11/18 17:51
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
09/11/18 17:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
09/11/18 17:51
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
09/11/18 17:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
09/11/18 17:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
09/11/18 17:51
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
09/11/18 17:51
127-18-4
Toluene
6.7
ug/L
1.0
0.26
1
09/11/18 17:51
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
09/11/18 17:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
09/11/18 17:51
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
09/11/18 17:51
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
09/11/18 17:51
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
09/11/18 17:51
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
09/11/18 17:51
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
09/11/18 17:51
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
09/11/18 17:51
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/11/18 17:51
460-00-4
1,2-Dichloroethane-d4 (S)
86
%
70-130
1
09/11/18 17:51
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
09/11/18 17:51
2037-26-5
Date: 09/14/2018 11:12 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-24S Lab ID: 92398011002 Collected: 08/30/18 13:35 Received: 08/31/18 13:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
09/11/18 16:06
09/12/18 20:22
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:22
7440-38-2
Barium
31.6J
ug/L
100
2.5
1
09/11/18 16:06
09/12/18 20:22
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 20:22
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 20:22
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:22
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:22
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:22
7440-50-8
Lead
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:22
7439-92-1
Nickel
ND
ug/L
50.0
2.5
1
09/11/18 16:06
09/12/18 20:22
7440-02-0 P8
Selenium
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:22
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:22
7440-22-4
Vanadium
ND
ug/L
25.0
2.5
1
09/11/18 16:06
09/12/18 20:22
7440-62-2
Zinc
8.91
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:22
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.074J
ug/L
5.5
0.020
1
09/06/18 08:24
09/07/18 18:53
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
09/11/18 18:08
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
09/11/18 18:08
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
09/11/18 18:08
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
09/11/18 18:08
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
09/11/18 18:08
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
09/11/18 18:08
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
09/11/18 18:08
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
09/11/18 18:08
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
09/11/18 18:08
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
09/11/18 18:08
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
09/11/18 18:08
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
09/11/18 18:08
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
09/11/18 18:08
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
09/11/18 18:08
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
09/11/18 18:08
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
09/11/18 18:08
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
09/11/18 18:08
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
09/11/18 18:08
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
09/11/18 18:08
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
09/11/18 18:08
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
09/11/18 18:08
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
09/11/18 18:08
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
09/11/18 18:08
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
09/11/18 18:08
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
09/11/18 18:08
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
09/11/18 18:08
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
09/11/18 18:08
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-24S
Lab ID:
92398011002
Collected:
08/30/18 13:35
Received: 08/31/18 13:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
09/11/18 18:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
09/11/18 18:08
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
09/11/18 18:08
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
09/11/18 18:08
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
09/11/18 18:08
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
09/11/18 18:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
09/11/18 18:08
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
09/11/18 18:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
09/11/18 18:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
09/11/18 18:08
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
09/11/18 18:08
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
09/11/18 18:08
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
09/11/18 18:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
09/11/18 18:08
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
09/11/18 18:08
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
09/11/18 18:08
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
09/11/18 18:08
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
09/11/18 18:08
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
09/11/18 18:08
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
09/11/18 18:08
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/11/18 18:08
460-00-4
1,2-Dichloroethane-d4 (S)
88
%
70-130
1
09/11/18 18:08
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
09/11/18 18:08
2037-26-5
Date: 09/14/2018 11:12 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-30 Lab ID: 92398011003 Collected: 08/30/18 11:53 Received: 08/31/18 13:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 09/14/2018 11:12 AM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
6.0
3.9
1
09/11/18 16:06
09/12/18 22:45
7440-36-0
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 22:45
7440-38-2
40.8J
ug/L
100
2.5
1
09/11/18 16:06
09/12/18 22:45
7440-39-3
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 22:45
7440-41-7
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 22:45
7440-43-9
2.9J
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 22:45
7440-47-3
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 22:45
7440-48-4
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 22:45
7440-50-8
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 22:45
7439-92-1
ND
ug/L
50.0
2.5
1
09/11/18 16:06
09/12/18 22:45
7440-02-0 P8
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 22:45
7782-49-2
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 22:45
7440-22-4
2.9J
ug/L
25.0
2.5
1
09/11/18 16:06
09/12/18 22:45
7440-62-2
11.0
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 22:45
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.061J ug/L 5.5 0.020 1 09/06/18 08:24 09/07/18 18:56 7440-28-0
Analytical Method: EPA 8260E
ND
ug/L
100
10.0
1
09/11/1818:25
67-64-1
ND
ug/L
200
1.9
1
09/11/1818:25
107-13-1
ND
ug/L
1.0
0.25
1
09/11/1818:25
71-43-2
ND
ug/L
3.0
0.17
1
09/11/1818:25
74-97-5
ND
ug/L
1.0
0.18
1
09/11/1818:25
75-27-4
ND
ug/L
3.0
0.26
1
09/11/1818:25
75-25-2
ND
ug/L
10.0
0.29
1
09/11/1818:25
74-83-9
ND
ug/L
100
0.96
1
09/11/1818:25
78-93-3
ND
ug/L
100
1.2
1
09/11/1818:25
75-15-0
ND
ug/L
1.0
0.25
1
09/11/1818:25
56-23-5
ND
ug/L
3.0
0.23
1
09/11/1818:25
108-90-7
ND
ug/L
10.0
0.54
1
09/11/1818:25
75-00-3
ND
ug/L
5.0
0.14
1
09/11/1818:25
67-66-3
ND
ug/L
1.0
0.11
1
09/11/1818:25
74-87-3
ND
ug/L
13.0
2.0
1
09/11/1818:25
96-12-8
ND
ug/L
3.0
0.21
1
09/11/1818:25
124-48-1
ND
ug/L
1.0
0.27
1
09/11/1818:25
106-93-4
ND
ug/L
10.0
0.21
1
09/11/1818:25
74-95-3
ND
ug/L
5.0
0.30
1
09/11/1818:25
95-50-1
ND
ug/L
1.0
0.33
1
09/11/1818:25
106-46-7
ND
ug/L
100
1.0
1
09/11/1818:25
110-57-6
ND
ug/L
5.0
0.32
1
09/11/1818:25
75-34-3
ND
ug/L
1.0
0.24
1
09/11/1818:25
107-06-2
ND
ug/L
5.0
0.56
1
09/11/1818:25
75-35-4
ND
ug/L
5.0
0.19
1
09/11/1818:25
156-59-2
ND
ug/L
5.0
0.49
1
09/11/1818:25
156-60-5
ND
ug/L
1.0
0.27
1
09/11/1818:25
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-30
Lab ID:
92398011003
Collected:
08/30/18 11:53
Received: 08/31/18 13:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
09/11/18 18:25
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
09/11/18 18:25
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
09/11/18 18:25
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
09/11/18 18:25
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
09/11/18 18:25
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
09/11/18 18:25
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
09/11/18 18:25
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
09/11/18 18:25
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
09/11/18 18:25
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
09/11/18 18:25
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
09/11/18 18:25
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
09/11/18 18:25
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
09/11/18 18:25
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
09/11/18 18:25
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
09/11/18 18:25
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
09/11/18 18:25
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
09/11/18 18:25
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
09/11/18 18:25
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
09/11/18 18:25
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
09/11/18 18:25
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
09/11/18 18:25
460-00-4
1,2-Dichloroethane-d4 (S)
84
%
70-130
1
09/11/18 18:25
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
09/11/18 18:25
2037-26-5
Date: 09/14/2018 11:12 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-35 Lab ID: 92398011004 Collected: 08/30/18 09:43 Received: 08/31/18 13:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
09/13/18 13:36
09/13/18 20:33
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
09/13/18 13:36
09/13/18 20:33
7440-38-2
Barium
146
ug/L
100
2.5
1
09/13/18 13:36
09/13/18 20:33
7440-39-3
Beryllium
0.811
ug/L
1.0
0.50
1
09/13/18 13:36
09/13/18 20:33
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
09/13/18 13:36
09/13/18 20:33
7440-43-9
Chromium
22.0
ug/L
10.0
2.5
1
09/13/18 13:36
09/13/18 20:33
7440-47-3
Cobalt
5.6J
ug/L
10.0
2.5
1
09/13/18 13:36
09/13/18 20:33
7440-48-4
Copper
26.9
ug/L
10.0
2.5
1
09/13/18 13:36
09/13/18 20:33
7440-50-8
Lead
9.6J
ug/L
10.0
2.5
1
09/13/18 13:36
09/13/18 20:33
7439-92-1
Nickel
8.6J
ug/L
50.0
2.5
1
09/13/18 13:36
09/13/18 20:33
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
09/13/18 13:36
09/13/18 20:33
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
09/13/18 13:36
09/13/18 20:33
7440-22-4
Vanadium
39.1
ug/L
25.0
2.5
1
09/13/18 13:36
09/13/18 20:33
7440-62-2
Zinc
44.4
ug/L
10.0
5.0
1
09/13/18 13:36
09/13/18 20:33
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
0.31J
ug/L
5.5
0.020
1
09/06/18 08:24
09/07/18 18:59
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
09/11/18 22:36
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
09/11/18 22:36
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
09/11/18 22:36
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
09/11/18 22:36
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
09/11/18 22:36
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
09/11/18 22:36
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
09/11/18 22:36
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
09/11/18 22:36
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
09/11/18 22:36
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
09/11/18 22:36
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
09/11/18 22:36
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
09/11/18 22:36
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
09/11/18 22:36
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
09/11/18 22:36
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
09/11/18 22:36
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
09/11/18 22:36
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
09/11/18 22:36
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
09/11/18 22:36
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
09/11/18 22:36
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
09/11/18 22:36
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
09/11/18 22:36
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
09/11/18 22:36
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
09/11/18 22:36
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
09/11/18 22:36
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
09/11/18 22:36
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
09/11/18 22:36
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
09/11/18 22:36
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: MW-35
Lab ID:
92398011004
Collected:
08/30/18 09:43
Received: 08/31/18 13:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
09/11/18 22:36
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
09/11/18 22:36
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
09/11/18 22:36
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
09/11/18 22:36
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
09/11/18 22:36
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
09/11/18 22:36
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
09/11/18 22:36
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
09/11/18 22:36
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
09/11/18 22:36
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
09/11/18 22:36
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
09/11/18 22:36
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
09/11/18 22:36
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
09/11/18 22:36
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
09/11/18 22:36
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
09/11/18 22:36
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
09/11/18 22:36
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
09/11/18 22:36
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
09/11/18 22:36
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
09/11/18 22:36
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
09/11/18 22:36
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
09/11/18 22:36
460-00-4
1,2-Dichloroethane-d4 (S)
83
%
70-130
1
09/11/18 22:36
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
09/11/18 22:36
2037-26-5
Date: 09/14/2018 11:12 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: Field Blank Lab ID: 92398011005 Collected: 08/30/18 13:40 Received: 08/31/18 13:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
6.0
3.9
1
09/11/18 16:06
09/12/18 20:34
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:34
7440-38-2
Barium
ND
ug/L
100
2.5
1
09/11/18 16:06
09/12/18 20:34
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 20:34
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
09/11/18 16:06
09/12/18 20:34
7440-43-9
Chromium
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:34
7440-47-3
Cobalt
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:34
7440-48-4
Copper
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:34
7440-50-8
Lead
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:34
7439-92-1
Nickel
ND
ug/L
50.0
2.5
1
09/11/18 16:06
09/12/18 20:34
7440-02-0 P8
Selenium
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:34
7782-49-2
Silver
ND
ug/L
10.0
2.5
1
09/11/18 16:06
09/12/18 20:34
7440-22-4
Vanadium
ND
ug/L
25.0
2.5
1
09/11/18 16:06
09/12/18 20:34
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
09/11/18 16:06
09/12/18 20:34
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
5.5
0.020
1
09/06/18 08:24
09/07/18 19:01
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
09/11/18 14:57
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
09/11/18 14:57
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
09/11/18 14:57
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
09/11/18 14:57
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
09/11/18 14:57
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
09/11/18 14:57
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
09/11/18 14:57
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
09/11/18 14:57
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
09/11/18 14:57
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
09/11/18 14:57
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
09/11/18 14:57
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
09/11/18 14:57
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
09/11/18 14:57
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
09/11/18 14:57
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
09/11/18 14:57
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
09/11/18 14:57
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
09/11/18 14:57
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
09/11/18 14:57
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
09/11/18 14:57
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
09/11/18 14:57
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
09/11/18 14:57
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
09/11/18 14:57
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
09/11/18 14:57
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
09/11/18 14:57
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
09/11/18 14:57
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
09/11/18 14:57
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
09/11/18 14:57
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: Field Blank
Lab ID:
92398011005
Collected:
08/30/18 13:40
Received: 08/31/18 13:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
09/11/18 14:57
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
09/11/18 14:57
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
09/11/18 14:57
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
09/11/18 14:57
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
09/11/18 14:57
74-88-4
Methylene Chloride
4.3
ug/L
1.0
0.97
1
09/11/18 14:57
75-09-2 C9
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
09/11/18 14:57
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
09/11/18 14:57
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
09/11/18 14:57
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
09/11/18 14:57
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
09/11/18 14:57
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
09/11/18 14:57
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
09/11/18 14:57
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
09/11/18 14:57
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
09/11/18 14:57
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
09/11/18 14:57
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
09/11/18 14:57
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
09/11/18 14:57
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
09/11/18 14:57
75-01-4
Xylene (Total)
ND
ug/L
5.0
0.66
1
09/11/18 14:57
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
09/11/18 14:57
460-00-4
1,2-Dichloroethane-d4 (S)
84
%
70-130
1
09/11/18 14:57
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
09/11/18 14:57
2037-26-5
Date: 09/14/2018 11:12 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 35

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ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: Trip Blank Lab ID: 92398011006 Collected: 08/29/18 08:00 Received: 08/31/18 13:37 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
Acetone
ND
ug/L
100
10.0
1
09/11/18 22:03
67-64-1
Acrylonitrile
ND
ug/L
200
1.9
1
09/11/18 22:03
107-13-1
Benzene
ND
ug/L
1.0
0.25
1
09/11/18 22:03
71-43-2
Bromochloromethane
ND
ug/L
3.0
0.17
1
09/11/18 22:03
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.18
1
09/11/18 22:03
75-27-4
Bromoform
ND
ug/L
3.0
0.26
1
09/11/18 22:03
75-25-2
Bromomethane
ND
ug/L
10.0
0.29
1
09/11/18 22:03
74-83-9
2-Butanone (MEK)
ND
ug/L
100
0.96
1
09/11/18 22:03
78-93-3
Carbon disulfide
ND
ug/L
100
1.2
1
09/11/18 22:03
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.25
1
09/11/18 22:03
56-23-5
Chlorobenzene
ND
ug/L
3.0
0.23
1
09/11/18 22:03
108-90-7
Chloroethane
ND
ug/L
10.0
0.54
1
09/11/18 22:03
75-00-3
Chloroform
ND
ug/L
5.0
0.14
1
09/11/18 22:03
67-66-3
Chloromethane
ND
ug/L
1.0
0.11
1
09/11/18 22:03
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
13.0
2.0
1
09/11/18 22:03
96-12-8
Dibromochloromethane
ND
ug/L
3.0
0.21
1
09/11/18 22:03
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.27
1
09/11/18 22:03
106-93-4
Dibromomethane
ND
ug/L
10.0
0.21
1
09/11/18 22:03
74-95-3
1,2-Dichlorobenzene
ND
ug/L
5.0
0.30
1
09/11/18 22:03
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
09/11/18 22:03
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
100
1.0
1
09/11/18 22:03
110-57-6
1,1-Dichloroethane
ND
ug/L
5.0
0.32
1
09/11/18 22:03
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
09/11/18 22:03
107-06-2
1,1-Dichloroethene
ND
ug/L
5.0
0.56
1
09/11/18 22:03
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
5.0
0.19
1
09/11/18 22:03
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
5.0
0.49
1
09/11/18 22:03
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
09/11/18 22:03
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
09/11/18 22:03
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
09/11/18 22:03
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
09/11/18 22:03
100-41-4
2-Hexanone
ND
ug/L
50.0
0.46
1
09/11/18 22:03
591-78-6
lodomethane
ND
ug/L
10.0
0.32
1
09/11/18 22:03
74-88-4
Methylene Chloride
ND
ug/L
1.0
0.97
1
09/11/18 22:03
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
100
0.33
1
09/11/18 22:03
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
09/11/18 22:03
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
5.0
0.33
1
09/11/18 22:03
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
3.0
0.40
1
09/11/18 22:03
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
09/11/18 22:03
127-18-4
Toluene
ND
ug/L
1.0
0.26
1
09/11/18 22:03
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
09/11/18 22:03
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
09/11/18 22:03
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
09/11/18 22:03
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
09/11/18 22:03
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
09/11/18 22:03
96-18-4
Vinyl acetate
ND
ug/L
50.0
0.35
1
09/11/18 22:03
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
09/11/18 22:03
75-01-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 35

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ANALYTICAL RESULTS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
Sample: Trip Blank
Lab ID:
92398011006
Collected:
08/29/18 08:00
Received: 08/31/18 13:37 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical
Method: EPA 8260E
Xylene (Total)
ND
ug/L
5.0
0.66 1
09/11/18 22:03
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
09/11/18 22:03
460-00-4
1,2-Dichloroethane-d4 (S)
84
%
70-130
1
09/11/18 22:03
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
09/11/18 22:03
2037-26-5
Date: 09/14/2018 11:12 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 35

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Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
QC Batch: 430066 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92398011001, 92398011002, 92398011003, 92398011005
METHOD BLANK: 2373355
Matrix:
Water
Associated Lab Samples:
92398011001, 92398011002,
92398011003, 92398011005
Blank
Reporting
Parameter
Units
Result
Limit
Antimony
ug/L
ND
6.0
Arsenic
ug/L
ND
10.0
Barium
ug/L
ND
100
Beryllium
ug/L
ND
1.0
Cadmium
ug/L
ND
1.0
Chromium
ug/L
ND
10.0
Cobalt
ug/L
ND
10.0
Copper
ug/L
ND
10.0
Lead
ug/L
ND
10.0
Nickel
ug/L
2.8J
50.0
Selenium
ug/L
ND
10.0
Silver
ug/L
ND
10.0
Vanadium
ug/L
ND
25.0
Zinc
ug/L
ND
10.0
MDL Analyzed
3.9
09/13/18 00:08
5.0
09/13/18 00:08
2.5
09/13/18 00:08
0.50
09/13/18 00:08
0.50
09/13/18 00:08
2.5
09/13/18 00:08
2.5
09/13/18 00:08
2.5
09/13/18 00:08
2.5
09/13/18 00:08
2.5
09/13/18 00:08
5.0
09/13/18 00:08
2.5
09/13/18 00:08
2.5
09/13/18 00:08
5.0
09/13/18 00:08
LABORATORY CONTROL SAMPLE:
Parameter
2373356
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
493
99
80-120
Arsenic
ug/L
500
470
94
80-120
Barium
ug/L
500
513
103
80-120
Beryllium
ug/L
500
516
103
80-120
Cadmium
ug/L
500
486
97
80-120
Chromium
ug/L
500
495
99
80-120
Cobalt
ug/L
500
482
96
80-120
Copper
ug/L
500
510
102
80-120
Lead
ug/L
500
474
95
80-120
Nickel
ug/L
500
485
97
80-120
Selenium
ug/L
500
473
95
80-120
Silver
ug/L
250
250
100
80-120
Vanadium
ug/L
500
495
99
80-120
Zinc
ug/L
500
468
94
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2373357 2373358
MS MSD
92398011001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 489 485 98 97 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
2373357
2373358
MS
MSD
92398011001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
470
467
94
93
75-125
1
20
Barium
ug/L
13.OJ
500
500
516
512
101
100
75-125
1
20
Beryllium
ug/L
ND
500
500
508
505
102
101
75-125
1
20
Cadmium
ug/L
ND
500
500
486
485
97
97
75-125
0
20
Chromium
ug/L
3.6J
500
500
490
491
97
97
75-125
0
20
Cobalt
ug/L
6.2J
500
500
483
481
95
95
75-125
0
20
Copper
ug/L
ND
500
500
505
503
101
100
75-125
0
20
Lead
ug/L
3.7J
500
500
473
471
94
93
75-125
0
20
Nickel
ug/L
ND
500
500
481
479
96
95
75-125
0
20
Selenium
ug/L
ND
500
500
478
476
95
95
75-125
0
20
Silver
ug/L
ND
250
250
246
247
99
99
75-125
0
20
Vanadium
ug/L
4.1J
500
500
493
494
98
98
75-125
0
20
Zinc
ug/L
6.5J
500
500
475
474
94
93
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
QC Batch: 430587 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92398011004
METHOD BLANK: 2375576
Associated Lab Samples: 92398011004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
6.0
3.9
09/13/18 20:27
Arsenic
ug/L
ND
10.0
5.0
09/13/18 20:27
Barium
ug/L
ND
100
2.5
09/13/18 20:27
Beryllium
ug/L
ND
1.0
0.50
09/13/18 20:27
Cadmium
ug/L
ND
1.0
0.50
09/13/18 20:27
Chromium
ug/L
ND
10.0
2.5
09/13/18 20:27
Cobalt
ug/L
ND
10.0
2.5
09/13/18 20:27
Copper
ug/L
ND
10.0
2.5
09/13/18 20:27
Lead
ug/L
ND
10.0
2.5
09/13/18 20:27
Nickel
ug/L
ND
50.0
2.5
09/13/18 20:27
Selenium
ug/L
ND
10.0
5.0
09/13/18 20:27
Silver
ug/L
ND
10.0
2.5
09/13/18 20:27
Vanadium
ug/L
ND
25.0
2.5
09/13/18 20:27
Zinc
ug/L
ND
10.0
5.0
09/13/18 20:27
LABORATORY CONTROL SAMPLE:
Parameter
2375577
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
474
95
80-120
Arsenic
ug/L
500
449
90
80-120
Barium
ug/L
500
512
102
80-120
Beryllium
ug/L
500
516
103
80-120
Cadmium
ug/L
500
479
96
80-120
Chromium
ug/L
500
487
97
80-120
Cobalt
ug/L
500
461
92
80-120
Copper
ug/L
500
493
99
80-120
Lead
ug/L
500
459
92
80-120
Nickel
ug/L
500
470
94
80-120
Selenium
ug/L
500
463
93
80-120
Silver
ug/L
250
247
99
80-120
Vanadium
ug/L
500
475
95
80-120
Zinc
ug/L
500
448
90
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2375578 2375580
MS MSD
92398011004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 449 451 90 90 75-125 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
2375578
2375580
MS
MSD
92398011004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
450
451
90
90
75-125
0
20
Barium
ug/L
146
500
500
652
654
101
101
75-125
0
20
Beryllium
ug/L
0.81J
500
500
519
519
104
104
75-125
0
20
Cadmium
ug/L
ND
500
500
488
490
98
98
75-125
0
20
Chromium
ug/L
22.0
500
500
512
514
98
98
75-125
1
20
Cobalt
ug/L
5.6J
500
500
466
467
92
92
75-125
0
20
Copper
ug/L
26.9
500
500
523
528
99
100
75-125
1
20
Lead
ug/L
9.6J
500
500
466
465
91
91
75-125
0
20
Nickel
ug/L
8.6J
500
500
479
480
94
94
75-125
0
20
Selenium
ug/L
ND
500
500
482
487
96
97
75-125
1
20
Silver
ug/L
ND
250
250
249
250
100
100
75-125
1
20
Vanadium
ug/L
39.1
500
500
518
524
96
97
75-125
1
20
Zinc
ug/L
44.4
500
500
497
500
91
91
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 21 of 35

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
QC Batch: 429067
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92398011001, 92398011002,
92398011003, 92398011004, 92398011005
METHOD BLANK: 2369054
Matrix: Water
Associated Lab Samples: 92398011001, 92398011002,
92398011003, 92398011004, 92398011005
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed Qualifiers
Thallium ug/L
ND 5.5 0.020
09/07/1818:32
LABORATORY CONTROL SAMPLE: 2369055
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 9.0 90
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2369056 2369057
MS MSD
92398011001
Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
Thallium ug/L 0.046J
10 10 9.2 9.3
91 93 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
QC Batch: 429886 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92398011001, 92398011002, 92398011003, 92398011005
METHOD BLANK: 2372590 Matrix: Water
Associated Lab Samples: 92398011001, 92398011002, 92398011003, 92398011005
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
0.33
09/11/18 08:47
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
09/11/18 08:47
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
0.40
09/11/18 08:47
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
09/11/18 08:47
1,1-Dichloroethane
ug/L
ND
5.0
0.32
09/11/18 08:47
1,1-Dichloroethene
ug/L
ND
5.0
0.56
09/11/18 08:47
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
09/11/18 08:47
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
2.0
09/11/18 08:47
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
09/11/18 08:47
1,2-Dichlorobenzene
ug/L
ND
5.0
0.30
09/11/18 08:47
1,2-Dichloroethane
ug/L
ND
1.0
0.24
09/11/18 08:47
1,2-Dichloropropane
ug/L
ND
1.0
0.27
09/11/18 08:47
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
09/11/18 08:47
2-Butanone (MEK)
ug/L
ND
100
0.96
09/11/18 08:47
2-Hexanone
ug/L
ND
50.0
0.46
09/11/18 08:47
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
0.33
09/11/18 08:47
Acetone
ug/L
ND
100
10.0
09/11/18 08:47
Acrylonitrile
ug/L
ND
200
1.9
09/11/18 08:47
Benzene
ug/L
ND
1.0
0.25
09/11/18 08:47
Bromochloromethane
ug/L
ND
3.0
0.17
09/11/18 08:47
Bromodichloromethane
ug/L
ND
1.0
0.18
09/11/18 08:47
Bromoform
ug/L
ND
3.0
0.26
09/11/18 08:47
Bromomethane
ug/L
ND
10.0
0.29
09/11/18 08:47
Carbon disulfide
ug/L
ND
100
1.2
09/11/18 08:47
Carbon tetrachloride
ug/L
ND
1.0
0.25
09/11/18 08:47
Chlorobenzene
ug/L
ND
3.0
0.23
09/11/18 08:47
Chloroethane
ug/L
ND
10.0
0.54
09/11/18 08:47
Chloroform
ug/L
ND
5.0
0.14
09/11/18 08:47
Chloromethane
ug/L
ND
1.0
0.11
09/11/18 08:47
cis-1,2-Dichloroethene
ug/L
ND
5.0
0.19
09/11/18 08:47
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
09/11/18 08:47
Dibromochloromethane
ug/L
ND
3.0
0.21
09/11/18 08:47
Dibromomethane
ug/L
ND
10.0
0.21
09/11/18 08:47
Ethylbenzene
ug/L
ND
1.0
0.30
09/11/18 08:47
lodomethane
ug/L
ND
10.0
0.32
09/11/18 08:47
Methylene Chloride
ug/L
ND
1.0
0.97
09/11/18 08:47
Styrene
ug/L
ND
1.0
0.26
09/11/18 08:47
Tetrachloroethene
ug/L
ND
1.0
0.46
09/11/18 08:47
Toluene
ug/L
ND
1.0
0.26
09/11/18 08:47
trans-1,2-Dichloroethene
ug/L
ND
5.0
0.49
09/11/18 08:47
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
09/11/18 08:47
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
METHOD BLANK: 2372590
Matrix:
Water
Associated Lab Samples:
92398011001, 92398011002,
92398011003, 92398011005
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
trans-1,4-Dichloro-2-butene
ug/L
ND
100
1.0
09/11/18 08:47
Trichloroethene
ug/L
ND
1.0
0.47
09/11/18 08:47
Trichlorofluoromethane
ug/L
ND
1.0
0.20
09/11/18 08:47
Vinyl acetate
ug/L
ND
50.0
0.35
09/11/18 08:47
Vinyl chloride
ug/L
ND
1.0
0.62
09/11/18 08:47
Xylene (Total)
ug/L
ND
5.0
0.66
09/11/18 08:47
1,2-Dichloroethane-d4 (S)
%
83
70-130
09/11/18 08:47
4-Bromofluorobenzene (S)
%
106
70-130
09/11/18 08:47
Toluene-d8 (S)
%
105
70-130
09/11/18 08:47
LABORATORY CONTROL SAMPLE:
Parameter
2372591
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
56.1
112
80-125
1,1,1-Trichloroethane
ug/L
50
50.3
101
71-129
1,1,2,2-Tetrachloroethane
ug/L
50
47.9
96
79-124
1,1,2-Trichloroethane
ug/L
50
52.0
104
85-125
1,1-Dichloroethane
ug/L
50
48.5
97
73-126
1,1-Dichloroethene
ug/L
50
52.1
104
66-135
1,2,3-Trichloropropane
ug/L
50
50.6
101
75-130
1,2-Dibromo-3-chloropropane
ug/L
50
46.7
93
71-133
1,2-Dibromoethane (EDB)
ug/L
50
51.9
104
83-124
1,2-Dichlorobenzene
ug/L
50
50.4
101
80-133
1,2-Dichloroethane
ug/L
50
48.3
97
67-128
1,2-Dichloropropane
ug/L
50
58.5
117
75-132
1,4-Dichlorobenzene
ug/L
50
50.1
100
78-130
2-Butanone (MEK)
ug/L
100
87.8J
88
61-144
2-Hexanone
ug/L
100
88.4
88
68-143
4-Methyl-2-pentanone (MIBK)
ug/L
100
82.7J
83
72-135
Acetone
ug/L
100
89.2J
89
48-146
Acrylonitrile
ug/L
250
250
100
40-160
Benzene
ug/L
50
55.8
112
80-125
Bromochloromethane
ug/L
50
53.4
107
71-125
Bromodichloromethane
ug/L
50
50.2
100
78-124
Bromoform
ug/L
50
47.7
95
71-128
Bromomethane
ug/L
50
28.2
56
40-160
Carbon disulfide
ug/L
50
51.9J
104
50-160
Carbon tetrachloride
ug/L
50
53.5
107
69-131
Chlorobenzene
ug/L
50
54.6
109
81-122
Chloroethane
ug/L
50
35.1
70
39-148
Chloroform
ug/L
50
49.7
99
73-127
Chloromethane
ug/L
50
34.4
69
44-146
cis-1,2-Dichloroethene
ug/L
50
50.3
101
74-124
cis-1,3-Dichloropropene
ug/L
50
55.7
111
72-132
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
LABORATORY CONTROL SAMPLE: 2372591
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Dibromochloromethane
ug/L
50
49.6
99
78-125
Dibromomethane
ug/L
50
55.5
111
82-120
Ethylbenzene
ug/L
50
51.8
104
79-121
lodomethane
ug/L
100
97.6
98
39-154
Methylene Chloride
ug/L
50
48.3
97
64-133
Styrene
ug/L
50
51.0
102
84-126
Tetrachloroethene
ug/L
50
55.4
111
78-122
Toluene
ug/L
50
52.9
106
80-121
trans-1,2-Dichloroethene
ug/L
50
52.6
105
71-127
trans- 1,3-Dichloropropene
ug/L
50
52.5
105
69-141
trans-1,4-Dichloro-2-butene
ug/L
50
37.8J
76
40-160
Trichloroethene
ug/L
50
57.5
115
78-122
Trichlorofluoromethane
ug/L
50
46.4
93
53-137
Vinyl acetate
ug/L
100
85.0
85
40-160
Vinyl chloride
ug/L
50
55.1
110
58-137
Xylene (Total)
ug/L
150
158
105
81-126
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
94
70-130
Toluene-d8 (S)
%
93
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2372592
2372593
MS
MSD
92397359008
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.2
21.5
101
107
70-130
6
30
1,1,1-Trichloroethane
ug/L
ND
20
20
18.5
20.8
93
104
70-130
12
30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
18.3
19.3
92
96
70-130
5
30
1,1,2-Trichloroethane
ug/L
ND
20
20
19.6
20.6
98
103
70-130
5
30
1,1-Dichloroethane
ug/L
ND
20
20
17.6
19.2
88
96
70-130
9
30
1,1-Dichloroethene
ug/L
ND
20
20
18.9
21.4
94
107
70-166
13
30
1,2,3-Trichloropropane
ug/L
ND
20
20
19.2
20.8
96
104
70-130
8
30
1,2-Dibromo-3-
ug/L
ND
20
20
17.7
18.0
89
90
70-130
2
30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
18.9
19.7
94
99
70-130
5
30
1,2-Dichlorobenzene
ug/L
ND
20
20
19.7
20.8
98
104
70-130
5
30
1,2-Dichloroethane
ug/L
ND
20
20
17.8
19.8
89
99
70-130
11
30
1,2-Dichloropropane
ug/L
ND
20
20
22.2
24.1
111
120
70-130
8
30
1,4-Dichlorobenzene
ug/L
ND
20
20
19.9
20.7
100
103
70-130
4
30
2-Butanone (MEK)
ug/L
ND
40
40
31.9J
36AJ
80
91
70-130
13
30
2-Hexanone
ug/L
ND
40
40
33.7J
35.2J
84
88
70-130
5
30
4-Methyl-2-pentanone
ug/L
ND
40
40
33.6J
34.7J
84
87
70-130
3
30
(MIBK)
Acetone
ug/L
ND
40
40
33.7J
37.9J
84
95
70-130
12
30
Acrylonitrile
ug/L
ND
100
100
93.6J
99.3J
94
99
70-130
6
30
Benzene
ug/L
ND
20
20
22.0
22.9
110
114
70-148
4
30
Bromochloromethane
ug/L
ND
20
20
19.9
21.8
100
109
70-130
9
30
Results presented
on this page are in the
units indicated by the "Units" column except where
an alternate unit is presented to
the right
of the result.
REPORT OF LABORATORY ANALYSIS
This
report shall
not be reproduced,
except
in full,
Date: 09/14/2018 11:12 AM
without
the written consent
of Pace
Analytical
Services, LLC.
Page 25 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2372592
2372593
MS
MSD
92397359008
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Bromodichloromethane
ug/L
ND
20
20
19.5
20.4
98
102
70-130
4
30
Bromoform
ug/L
ND
20
20
16.1
17.5
80
87
70-130
8
30
Bromomethane
ug/L
ND
20
20
5.5J
7.2J
27
36
70-130
28
30 M1
Carbon disulfide
ug/L
ND
20
20
15.9J
19.8J
80
99
70-130
22
30
Carbon tetrachloride
ug/L
ND
20
20
21.5
22.5
107
113
70-130
5
30
Chlorobenzene
ug/L
ND
20
20
21.8
23.5
109
117
70-146
8
30
Chloroethane
ug/L
ND
20
20
15.5
17.8
77
89
70-130
14
30
Chloroform
ug/L
ND
20
20
17.9
19.6
89
98
70-130
9
30
Chloromethane
ug/L
ND
20
20
9.1
9.9
45
50
70-130
9
30 M1
cis-1,2-Dichloroethene
ug/L
ND
20
20
18.9
20.8
95
104
70-130
9
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
18.4
19.4
92
97
70-130
5
30
Dibromochloromethane
ug/L
ND
20
20
17.7
19.0
88
95
70-130
7
30
Dibromomethane
ug/L
ND
20
20
22.6
23.4
113
117
70-130
3
30
Ethylbenzene
ug/L
ND
20
20
20.4
21.9
102
110
70-130
7
30
lodomethane
ug/L
ND
40
40
22.4
33.6
56
84
70-130
40
30 M1,R1
Methylene Chloride
ug/L
ND
20
20
16.5
18.6
83
93
70-130
12
30
Styrene
ug/L
ND
20
20
19.7
21.0
99
105
70-130
6
30
Tetrachloroethene
ug/L
ND
20
20
21.3
23.4
107
117
70-130
9
30
Toluene
ug/L
ND
20
20
21.3
23.4
106
117
70-155
10
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.9
22.7
100
114
70-130
13
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
18.0
18.9
90
95
70-130
5
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
8.5J
9.01
43
45
70-130
6
30 M1
Trichloroethene
ug/L
ND
20
20
21.3
22.7
107
114
69-151
6
30
Trichlorofluoromethane
ug/L
ND
20
20
17.0
19.3
85
97
70-130
13
30
Vinyl acetate
ug/L
ND
40
40
21.3J
23.1J
53
58
70-130
8
30 M1
Vinyl chloride
ug/L
ND
20
20
17.3
19.3
86
97
70-130
11
30
Xylene (Total)
ug/L
ND
60
60
62.1
66.9
103
111
70-130
7
30
1,2-Dichloroethane-d4 (S)
%
86
85
70-130
4-Bromofluorobenzene (S)
%
96
94
70-130
Toluene-d8 (S)
%
96
96
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 26 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
QC Batch: 430085 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92398011004, 92398011006
METHOD BLANK: 2373437
Associated Lab Samples: 92398011004, 92398011006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
5.0
0.33
09/11/18 21:46
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
09/11/18 21:46
1,1,2,2-Tetrachloroethane
ug/L
ND
3.0
0.40
09/11/18 21:46
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
09/11/18 21:46
1,1-Dichloroethane
ug/L
ND
5.0
0.32
09/11/18 21:46
1,1-Dichloroethene
ug/L
ND
5.0
0.56
09/11/18 21:46
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
09/11/18 21:46
1,2-Dibromo-3-chloropropane
ug/L
ND
13.0
2.0
09/11/18 21:46
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
09/11/18 21:46
1,2-Dichlorobenzene
ug/L
ND
5.0
0.30
09/11/18 21:46
1,2-Dichloroethane
ug/L
ND
1.0
0.24
09/11/18 21:46
1,2-Dichloropropane
ug/L
ND
1.0
0.27
09/11/18 21:46
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
09/11/18 21:46
2-Butanone (MEK)
ug/L
ND
100
0.96
09/11/18 21:46
2-Hexanone
ug/L
ND
50.0
0.46
09/11/18 21:46
4-Methyl-2-pentanone (MIBK)
ug/L
ND
100
0.33
09/11/18 21:46
Acetone
ug/L
ND
100
10.0
09/11/18 21:46
Acrylonitrile
ug/L
ND
200
1.9
09/11/18 21:46
Benzene
ug/L
ND
1.0
0.25
09/11/18 21:46
Bromochloromethane
ug/L
ND
3.0
0.17
09/11/18 21:46
Bromodichloromethane
ug/L
ND
1.0
0.18
09/11/18 21:46
Bromoform
ug/L
ND
3.0
0.26
09/11/18 21:46
Bromomethane
ug/L
ND
10.0
0.29
09/11/18 21:46
Carbon disulfide
ug/L
ND
100
1.2
09/11/18 21:46
Carbon tetrachloride
ug/L
ND
1.0
0.25
09/11/18 21:46
Chlorobenzene
ug/L
ND
3.0
0.23
09/11/18 21:46
Chloroethane
ug/L
ND
10.0
0.54
09/11/18 21:46
Chloroform
ug/L
ND
5.0
0.14
09/11/18 21:46
Chloromethane
ug/L
ND
1.0
0.11
09/11/18 21:46
cis-1,2-Dichloroethene
ug/L
ND
5.0
0.19
09/11/18 21:46
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
09/11/18 21:46
Dibromochloromethane
ug/L
ND
3.0
0.21
09/11/18 21:46
Dibromomethane
ug/L
ND
10.0
0.21
09/11/18 21:46
Ethylbenzene
ug/L
ND
1.0
0.30
09/11/18 21:46
lodomethane
ug/L
ND
10.0
0.32
09/11/18 21:46
Methylene Chloride
ug/L
ND
1.0
0.97
09/11/18 21:46
Styrene
ug/L
ND
1.0
0.26
09/11/18 21:46
Tetrachloroethene
ug/L
ND
1.0
0.46
09/11/18 21:46
Toluene
ug/L
ND
1.0
0.26
09/11/18 21:46
trans-1,2-Dichloroethene
ug/L
ND
5.0
0.49
09/11/18 21:46
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
09/11/18 21:46
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
METHOD BLANK: 2373437
Matrix:
Water
Associated Lab Samples:
92398011004, 92398011006
Blank
Reporting
Parameter
Units
Result
Limit MDL
trans-1,4-Dichloro-2-butene
ug/L
ND
100
Trichloroethene
ug/L
ND
1.0
Trichlorofluoromethane
ug/L
ND
1.0
Vinyl acetate
ug/L
ND
50.0
Vinyl chloride
ug/L
ND
1.0
Xylene (Total)
ug/L
ND
5.0
1,2-Dichloroethane-d4 (S)
%
85
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
106
70-130
Analyzed
1.0
09/11/18 21:46
0.47
09/11/18 21:46
0.20
09/11/18 21:46
0.35
09/11/18 21:46
0.62
09/11/18 21:46
0.66
09/11/18 21:46
09/11/18 21:46
09/11/18 21:46
09/11/18 21:46
LABORATORY CONTROL SAMPLE:
Parameter
2373438
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
54.7
109
80-125
1,1,1-Trichloroethane
ug/L
50
48.0
96
71-129
1,1,2,2-Tetrachloroethane
ug/L
50
47.2
94
79-124
1,1,2-Trichloroethane
ug/L
50
51.7
103
85-125
1,1-Dichloroethane
ug/L
50
45.3
91
73-126
1,1-Dichloroethene
ug/L
50
48.8
98
66-135
1,2,3-Trichloropropane
ug/L
50
50.0
100
75-130
1,2-Dibromo-3-chloropropane
ug/L
50
47.2
94
71-133
1,2-Dibromoethane (EDB)
ug/L
50
50.7
101
83-124
1,2-Dichlorobenzene
ug/L
50
49.5
99
80-133
1,2-Dichloroethane
ug/L
50
46.2
92
67-128
1,2-Dichloropropane
ug/L
50
56.4
113
75-132
1,4-Dichlorobenzene
ug/L
50
49.6
99
78-130
2-Butanone (MEK)
ug/L
100
86.2J
86
61-144
2-Hexanone
ug/L
100
88.9
89
68-143
4-Methyl-2-pentanone (MIBK)
ug/L
100
84.OJ
84
72-135
Acetone
ug/L
100
89.6J
90
48-146
Acrylonitrile
ug/L
250
244
98
40-160
Benzene
ug/L
50
54.1
108
80-125
Bromochloromethane
ug/L
50
50.0
100
71-125
Bromodichloromethane
ug/L
50
48.5
97
78-124
Bromoform
ug/L
50
46.9
94
71-128
Bromomethane
ug/L
50
22.0
44
40-160
Carbon disulfide
ug/L
50
49.5J
99
50-160
Carbon tetrachloride
ug/L
50
51.5
103
69-131
Chlorobenzene
ug/L
50
52.9
106
81-122
Chloroethane
ug/L
50
31.4
63
39-148
Chloroform
ug/L
50
47.1
94
73-127
Chloromethane
ug/L
50
29.5
59
44-146
cis-1,2-Dichloroethene
ug/L
50
46.9
94
74-124
cis-1,3-Dichloropropene
ug/L
50
53.4
107
72-132
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
LABORATORY CONTROL SAMPLE: 2373438
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Dibromochloromethane
ug/L
50
48.7
97
78-125
Dibromomethane
ug/L
50
53.5
107
82-120
Ethylbenzene
ug/L
50
49.9
100
79-121
lodomethane
ug/L
100
90.7
91
39-154
Methylene Chloride
ug/L
50
46.5
93
64-133
Styrene
ug/L
50
47.9
96
84-126
Tetrachloroethene
ug/L
50
55.0
110
78-122
Toluene
ug/L
50
52.2
104
80-121
trans-1,2-Dichloroethene
ug/L
50
49.0
98
71-127
trans- 1,3-Dichloropropene
ug/L
50
50.3
101
69-141
trans-1,4-Dichloro-2-butene
ug/L
50
31.9J
64
40-160
Trichloroethene
ug/L
50
56.2
112
78-122
Trichlorofluoromethane
ug/L
50
43.9
88
53-137
Vinyl acetate
ug/L
100
82.5
83
40-160
Vinyl chloride
ug/L
50
51.5
103
58-137
Xylene (Total)
ug/L
150
150
100
81-126
1,2-Dichloroethane-d4 (S)
%
88
70-130
4-Bromofluorobenzene (S)
%
92
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2373439
2373440
MS
MSD
92398653004
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
21.5
22.4
107
112
70-130
4 30
1,1,1-Trichloroethane
ug/L
ND
20
20
20.5
21.8
102
109
70-130
6 30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.1
20.0
96
100
70-130
5 30
1,1,2-Trichloroethane
ug/L
ND
20
20
20.0
21.5
100
108
70-130
8 30
1,1-Dichloroethane
ug/L
ND
20
20
19.6
20.4
98
102
70-130
4 30
1,1-Dichloroethene
ug/L
ND
20
20
19.6
20.3
98
102
70-166
4 30
1,2,3-Trichloropropane
ug/L
ND
20
20
20.7
21.2
104
106
70-130
2 30
1,2-Dibromo-3-
ug/L
ND
20
20
19.6
19.8
98
99
70-130
1 30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
19.8
20.6
99
103
70-130
4 30
1,2-Dichlorobenzene
ug/L
ND
20
20
21.3
22.0
106
110
70-130
3 30
1,2-Dichloroethane
ug/L
ND
20
20
18.9
19.8
94
99
70-130
5 30
1,2-Dichloropropane
ug/L
ND
20
20
24.7
25.3
124
126
70-130
2 30
1,4-Dichlorobenzene
ug/L
ND
20
20
21.6
22.5
108
112
70-130
4 30
2-Butanone (MEK)
ug/L
ND
40
40
33.2J
34.2J
83
86
70-130
3 30
2-Hexanone
ug/L
ND
40
40
35.1J
35.6J
88
89
70-130
1 30
4-Methyl-2-pentanone
ug/L
ND
40
40
34.OJ
35.9J
85
90
70-130
5 30
(MIBK)
Acetone
ug/L
ND
40
40
34.9J
34.7J
87
87
70-130
1 30
Acrylonitrile
ug/L
ND
100
100
98AJ
103J
98
103
70-130
5 30
Benzene
ug/L
ND
20
20
23.0
23.8
115
119
70-148
3 30
Bromochloromethane
ug/L
ND
20
20
21.1
22.5
106
112
70-130
6 30
Results presented
on this page are in the
units indicated by the "Units" column except where
an alternate unit is presented to
the right
of the result.
REPORT OF LABORATORY ANALYSIS
This
report shall
not be reproduced,
except
in full,
Date: 09/14/2018 11:12 AM
without
the written consent
of Pace
Analytical
Services, LLC.
Page 29 of 35

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Johns River - Expansion GW
Pace Project No.: 92398011
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2373439
2373440
MS
MSD
92398653004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Bromodichloromethane
ug/L
ND
20
20
21.2
22.4
106
112
70-130
6
30
Bromoform
ug/L
ND
20
20
18.3
19.1
91
95
70-130
4
30
Bromomethane
ug/L
ND
20
20
11.8
12.1
59
61
70-130
3
30 M1
Carbon disulfide
ug/L
ND
20
20
16AJ
16.3J
82
81
70-130
1
30
Carbon tetrachloride
ug/L
ND
20
20
23.6
24.1
118
120
70-130
2
30
Chlorobenzene
ug/L
ND
20
20
23.1
24.1
115
121
70-146
5
30
Chloroethane
ug/L
ND
20
20
12.8
13.9
64
70
70-130
9
30 M1
Chloroform
ug/L
ND
20
20
18.6
20.3
93
101
70-130
8
30
Chloromethane
ug/L
ND
20
20
7.4
8.0
37
40
70-130
7
30 M1
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
21.3
101
107
70-130
6
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.3
22.1
106
111
70-130
4
30
Dibromochloromethane
ug/L
ND
20
20
19.2
20.0
96
100
70-130
4
30
Dibromomethane
ug/L
ND
20
20
23.4
24.7
117
123
70-130
6
30
Ethylbenzene
ug/L
ND
20
20
22.3
23.5
111
118
70-130
5
30
lodomethane
ug/L
ND
40
40
26.9
29.6
67
74
70-130
10
30 M1
Methylene Chloride
ug/L
ND
20
20
16.3
17.3
82
86
70-130
5
30
Styrene
ug/L
ND
20
20
21.3
22.9
107
114
70-130
7
30
Tetrachloroethene
ug/L
ND
20
20
23.6
24.8
118
124
70-130
5
30
Toluene
ug/L
ND
20
20
23.4
24.4
117
122
70-155
4
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.1
23.3
105
116
70-130
10
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
20.7
21.3
104
107
70-130
3
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
14.3J
14.6J
71
73
70-130
2
30
Trichloroethene
ug/L
ND
20
20
23.5
24.7
118
124
69-151
5
30
Trichlorofluoromethane
ug/L
ND
20
20
17.3
18.1
86
91
70-130
5
30
Vinyl acetate
ug/L
ND
40
40
30.2J
31.5J
76
79
70-130
4
30
Vinyl chloride
ug/L
ND
20
20
13.7
14.7
69
73
70-130
7
30 M1
Xylene (Total)
ug/L
ND
60
60
67.7
70.9
113
118
70-130
5
30
1,2-Dichloroethane-d4 (S)
%
85
86
70-130
4-Bromofluorobenzene (S)
%
93
94
70-130
Toluene-d8 (S)
%
97
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC.
Page 30 of 35

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: Johns River - Expansion GW
Pace Project No.: 92398011
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than
the blank or were below the reporting limit.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 35

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Johns River - Expansion GW
Pace Project No.:
92398011
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92398011001
MW-23S
EPA 3010A
430066
EPA 6010D
430125
92398011002
MW-24S
EPA 3010A
430066
EPA 6010D
430125
92398011003
MW-30
EPA 3010A
430066
EPA 6010D
430125
92398011004
MW-35
EPA 3010A
430587
EPA 6010D
430687
92398011005
Field Blank
EPA 3010A
430066
EPA6010D
430125
92398011001
MW-23S
EPA 3010A
429067
EPA 6020B
429223
92398011002
MW-24S
EPA 3010A
429067
EPA 6020B
429223
92398011003
MW-30
EPA 3010A
429067
EPA 6020B
429223
92398011004
MW-35
EPA 3010A
429067
EPA 6020B
429223
92398011005
Field Blank
EPA 3010A
429067
EPA 6020B
429223
92398011001
MW-23S
EPA 8260B
429886
92398011002
MW-24S
EPA 8260B
429886
92398011003
MW-30
EPA 8260B
429886
92398011004
MW-35
EPA 8260B
430085
92398011005
Field Blank
EPA 8260B
429886
92398011006
Trip Blank
EPA 8260B
430085
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/14/2018 11:12 AM without the written consent of Pace Analytical Services, LLC. Page 32 of 35

Document Name:
Document Revised: February 7, 2018
aCeAnafXica(
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [f Raleigh❑ Mechanicsville❑
Sample Conditian Client Name:
Upon Rerpipt Project #:
Courier: Fed Ex
❑ ❑UPS ❑U5P5 ❑Client
❑ Commercial []Pace ❑Other;
Custody Seal Present? Dyes E]NO Seals Intact? ❑Yes QNo L
WOk:92358011
1111111111111111111111
Oil
Date/Initials Person Examining Contents: AO 0 16
Packing Material: ❑Bubble wrap ❑bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer,, Dyes QNo ❑N/A
_0iR Gun ID: 92T045 Type of Ice: QWet ❑81ue []None
Cooler Temp ('CJ: 1 -1 Correction Factor: Add/Subtract IT) ^
Temp should be above freezing to 6°C
Cooler Temp Corrected (°C):
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Sail (❑'N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
I 1Yes FINo inriudhL7 Hawaii and Puprtn Rirnl? MYpt FINn
Cam ments/ Discrepancy:
Chain of Custody Present?
3res
❑No
❑N/A
1,
Samples Arrived within Hold Time?
Qyes
❑No
❑N/A
2.
Short Hold TlmeAnalysis (<72 hr.)?
❑yes
QNo
❑N/A
I
Rush Turn Around Time Requested?
Dyes
EfNo
❑N/A
4.
Sufficient Volume?
Yes
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
[[nYes
Yes
❑N❑
❑No
❑N/A
❑N/A
6.
Containers Intact?
Q` yes
ONO
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]No
[N/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Dyes
W
[]No
❑N/A
9.
Headspace in VCA Vials (>5-6mml?
❑Yes
BNo
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
QYes
❑yes
❑No
❑No
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? ❑Yes ❑No
Person contacted: Date/Time:
Project Manager SCURF Review: Date: Vt
Project Manager SRF Review: 1� Date:
Page 33 of 35

a
_. 8ceAnalylieal
Document Name:
Sample Condition Upon Recelpt(SCUR)
Document Revised: February 7, 2018
Page I of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHE
"Bottom half of box is to list number of battle
WO#.92398011
PM: NMG Due Date: 09/13/18
CLIENT: 92-Jos,ce Eng
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pH Adjustment Log for Preserved Samples
Sample 1D
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will besent to the North Carolina DEHNR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 34 of 35

1"Analytical
Section A
Required Client Information:
Company: Joyce Engini
Address, 2211 West h
Greensboro, NC 27407
Emu!! To:yburbach2i(
Phone: [phone]
Requested Due Date/TAT. 1
SAMPLE ID
One Character per box.
tA-Z. 0-9 1. -)
Sample Ids must be unique
W
F
1
MW-23S
2
MW-24S
3
M W-30
4
MW-35
5
Field Blank
6
Trip Blank
7
8
9
10
11
12
LO
tm
5
CHAIN -OF -CUSTODY / Analytical Request Document
LO
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
d
Section B
Section G
Required Project Information:
Invoice Information:
Pa e . 1
Of 1
Repon To, Van Burbach
Attention: Lecia Jones
Rd. Copy To: Samantha Slebodik, Miguel Vazquez company Name: Joyce Engineering
Address: 1604 Ownby Ln., Richmond, VA 23220
Regulatory Agency
rin .Coal
Purchase Order No. 2180009.02
Pace Quote Reference:
Client Project ID: Johns River - Expansion GW
Pace Project Manager GasiorowSki, Nicole
State ! Location
Ult
Container Order Number
Pace Profile #: 2327
North Carolina
ADDITIONAL COMMENTS
MAT", cone
p'i11Z Water Dw
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m
a
°
u
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COLLECTED
z
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Preservatives
Z
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wale' W7
$
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SOL
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START
END
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RELINQUISHED BY I AFFILIATION DATE I E A ACCEPTEDB f
w-- Itawla W31118 i r JW71
TIME SAMPLE CONDITIONS
z5 N
02
SAMPLER NAME AND SIGNATURE
n m
PRINT Name of SAMPLER: , j _ y1 ) a o m z E
jl'1K (1� ii ii' v }
C
SIGNATURE of MPLE DATE Signed:
z > o `m
�{y i'�l II6 m m o m 4 w
t77 ! liy F C: U V rn

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 27, 2018
Mr. Van Burbach
Joyce Engineering -Greensboro
2211 West Meadowview Rd
Boone Bldg, Suite 101
Greensboro, NC 27407
RE: Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Dear Mr. Burbach:
Enclosed are the analytical results for sample(s) received by the laboratory on December 07, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Van Burbach, Joyce Engineering -NC
Gretta Eller, LaBella Associates, D.P.C.
Daniel Girdner, LaBella Associates, D.P.C.
Rochelle Mesubed, Joyce Engineering
Miguel Vazquez, Joyce Engineering
�pQ ACrfFO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
9e0 without the written consent of Pace Analytical Services, LLC.
Page 1 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92410048001
1203-MW-20
Water
12/05/1815:22
12/07/1810:20
92410048002
1203-MW-23S
Water
12/05/1815:40
12/07/1810:20
92410048003
1203-MW-24S
Water
12/06/1814:20
12/07/1810:20
92410048004
1203-MW-30
Water
12/05/1816:09
12/07/1810:20
92410048005
1203-MW-38
Water
12/06/1813:00
12/07/1810:20
92410048006
1203-MW-35
Water
12/05/1815:49
12/07/1810:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Burke Co. Johns R C&D Exp.
92410048
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92410048001
1203-MW-20
EPA 6010D
IDS
17
PASI-A
EPA 6020E
SER
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CRV
1
PASI-A
EPA 300.0 Rev 2.1 1993
BRJ
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
92410048002
1203-MW-23S
EPA 6010D
DS
17
PASI-A
EPA 6020E
SER
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CRV
1
PASI-A
EPA 300.0 Rev 2.1 1993
BRJ
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
92410048003
1203-MW-24S
EPA 6010D
IDS
17
PASI-A
EPA 6020E
SER
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
NSCQ
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CRV
1
PASI-A
EPA 300.0 Rev 2.1 1993
BRJ
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
92410048004
1203-MW-30
EPA 6010D
IDS
17
PASI-A
EPA 6020E
SER
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CRV
1
PASI-A
EPA 300.0 Rev 2.1 1993
BRJ
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
92410048005
1203-MW-38
RSK 175 Modified
LMB
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
EPA 6010D
IDS
17
PASI-A
EPA 6020E
SER
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
NSCQ
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CRV
1
PASI-A
EPA 300.0 Rev 2.1 1993
BRJ
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
92410048006 1203-MW-35 RSK 175 Modified
LMB
1
PASI-C
EPA 6010D
IDS
17
PASI-A
EPA 6020E
SER
1
PASI-A
EPA7470A
JMW1
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
SM 2320B-2011
ECH
1
PASI-A
SM 2540C-2011
CRV
1
PASI-A
EPA 300.0 Rev 2.1 1993
BRJ
1
PASI-A
SM 4500-CI-E-2011
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Burke Co. Johns R C&D Exp.
Pace Project No.:
92410048
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92410048001
1203-MW-20
EPA 601 OD
Barium
179
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Chromium
13.5
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Cobalt
5.1
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Copper
14.6
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Iron
13600
ug/L
50.0
12/17/18 22:02
EPA 601 OD
Lead
6.5
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Manganese
235
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Nickel
7.4
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Vanadium
20.7
ug/L
5.0
12/17/18 22:02
EPA 601 OD
Zinc
32.8
ug/L
10.0
12/17/18 22:02
EPA 6020B
Thallium
0.26
ug/L
0.10
12/15/18 01:36
SM 2320B-2011
Alkalinity, Total as CaCO3
5290
ug/L
5000
12/17/18 16:40
SM 2540C-2011
Total Dissolved Solids
82000
ug/L
25000
12/11/18 17:30
SM 4500-CI-E-2011
Chloride
2230
ug/L
1000
12/17/18 10:22
92410048002
1203-MW-23S
EPA 601 OD
Barium
5.5
ug/L
5.0
12/17/18 22:05
EPA 601 OD
Cobalt
3.1 J
ug/L
5.0
12/17/18 22:05
EPA 601 OD
Iron
323
ug/L
50.0
12/17/18 22:05
EPA 601 OD
Manganese
73.7
ug/L
5.0
12/17/18 22:05
SM 2320B-2011
Alkalinity, Total as CaCO3
2980J
ug/L
5000
12/17/18 16:45
SM 2540C-2011
Total Dissolved Solids
25000
ug/L
25000
12/11/18 17:30
EPA 300.0 Rev 2.1 1993 Sulfate
1030
ug/L
1000
12/20/18 04:50
SM 4500-CI-E-2011
Chloride
2710
ug/L
1000
12/17/18 10:23
92410048003
1203-MW-24S
EPA 601 OD
Barium
32.6
ug/L
5.0
12/17/18 22:08
EPA 601 OD
Iron
1550
ug/L
50.0
12/17/18 22:08
EPA 601 OD
Manganese
29.5
ug/L
5.0
12/17/18 22:08
EPA 601 OD
Zinc
8.7J
ug/L
10.0
12/17/18 22:08
EPA 6020B
Thallium
0.081 J
ug/L
0.10
12/15/18 01:40
SM 2320B-2011
Alkalinity, Total as CaCO3
3580J
ug/L
5000
12/18/18 22:10
SM 2540C-2011
Total Dissolved Solids
26000
ug/L
25000
12/11/18 21:12
SM 4500-CI-E-2011
Chloride
2760
ug/L
1000
12/17/18 10:24
92410048004
1203-MW-30
EPA 601 OD
Barium
58.4
ug/L
5.0
12/17/18 22:11
EPA 601 OD
Chromium
4.1 J
ug/L
5.0
12/17/18 22:11
EPA 601 OD
Cobalt
3.7J
ug/L
5.0
12/17/18 22:11
EPA 601 OD
Iron
5440
ug/L
50.0
12/17/18 22:11
EPA 601 OD
Manganese
477
ug/L
5.0
12/17/18 22:11
EPA 601 OD
Nickel
3AJ
ug/L
5.0
12/17/18 22:11
EPA 601 OD
Vanadium
6.6
ug/L
5.0
12/17/18 22:11
EPA 601 OD
Zinc
15.5
ug/L
10.0
12/17/18 22:11
EPA 6020B
Thallium
0.13
ug/L
0.10
12/15/18 03:27
SM 2320B-2011
Alkalinity, Total as CaCO3
16200
ug/L
5000
12/17/18 16:49
SM 2540C-2011
Total Dissolved Solids
55000
ug/L
25000
12/11/18 17:30
SM 4500-CI-E-2011
Chloride
1310
ug/L
1000
12/17/18 10:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Lab Sample ID Client Sample ID
Method Parameters
92410048005
RSK 175 Modified
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B Mod.
SM 2320B-2011
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
SM 4500-CI-E-2011
92410048006
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 6020B
SM 2320B-2011
SM 2540C-2011
EPA 300.0 Rev 2.1 1993
SM 4500-CI-E-2011
1203-MW-38
Methane
Barium
Cobalt
Iron
Manganese
Nickel
Benzene
Chlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
cis-1,2-Dichloroethene
Ethylbenzene
Tetrahydrofuran
Vinyl chloride
Xylene (Total)
1,4-Dioxane (p-Dioxane)
Alkalinity, Total as CaCO3
Total Dissolved Solids
Sulfate
Chloride
1203-MW-35
Barium
Chromium
Copper
Iron
Manganese
Vanadium
Zinc
Thallium
Alkalinity, Total as CaCO3
Total Dissolved Solids
Sulfate
Chloride
SUMMARY OF DETECTION
Result
Units
Report Limit
Analyzed Qualifiers
12300
ug/L
10.0
12/12/1812:06
106
ug/L
5.0
12/17/18 22:14
17.5
ug/L
5.0
12/17/18 22:14
17600
ug/L
50.0
12/17/18 22:14
4870
ug/L
5.0
12/17/18 22:14
4.9J
ug/L
5.0
12/17/18 22:14
5.6
ug/L
1.0
12/19/18 21:28
0.83J
ug/L
1.0
12/19/18 21:28
16.9
ug/L
1.0
12/19/18 21:28
5.2
ug/L
1.0
12/19/18 21:28
6.9
ug/L
1.0
12/19/18 21:28
0.86J
ug/L
1.0
12/19/18 21:28
447
ug/L
10.0
12/19/18 21:28
4.3
ug/L
1.0
12/19/18 21:28
14.7
ug/L
1.0
12/19/18 21:28
2.4
ug/L
2.0
12/14/18 23:01
263000
ug/L
5000
12/18/18 22:15
277000
ug/L
25000
12/11 /18 21:12
716J
ug/L
1000
12/20/18 05:35
7280
ug/L
1000
12/17/1810:30
42.8
ug/L
5.0
12/17/18 22:17
3.8J
ug/L
5.0
12/17/18 22:17
4.1 J
ug/L
5.0
12/17/18 22:17
3410
ug/L
50.0
12/17/18 22:17
41.2
ug/L
5.0
12/17/18 22:17
6.2
ug/L
5.0
12/17/18 22:17
7AJ
ug/L
10.0
12/17/18 22:17
0.062J
ug/L
0.10
12/15/18 03:42
8340
ug/L
5000
12/17/1817:04
37000
ug/L
25000
12/11 /18 21:02
541J
ug/L
1000
12/20/18 06:35
1200
ug/L
1000
12/17/1810:31
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-20 Lab ID: 92410048001 Collected: 12/05/18 15:22 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Tin
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.9
1
12/08/18 06:50
12/17/18 22:02
7440-36-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:02
7440-38-2
179
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-39-3
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:02
7440-41-7
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:02
7440-43-9
13.5
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-47-3
5.1
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-48-4
14.6
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-50-8
13600
ug/L
50.0
25.0
1
12/08/18 06:50
12/17/18 22:02
7439-89-6
6.5
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7439-92-1
235
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7439-96-5
7.4
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-02-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:02
7782-49-2
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-22-4
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-31-5
20.7
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:02
7440-62-2
32.8
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:02
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.26 ug/L 0.10 0.060 1 12/12/18 15:31 12/15/18 01:36 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 12/11/1818:33 12/12/1816:20 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
25.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
10.0
1
12/16/18 06:04
67-64-1
1.9
1
12/16/18 06:04
107-13-1
0.25
1
12/16/18 06:04
71-43-2
0.17
1
12/16/18 06:04
74-97-5
0.18
1
12/16/18 06:04
75-27-4
0.26
1
12/16/18 06:04
75-25-2
0.29
1
12/16/18 06:04
74-83-9
0.96
1
12/16/18 06:04
78-93-3
1.2
1
12/16/18 06:04
75-15-0
0.25
1
12/16/18 06:04
56-23-5
0.23
1
12/16/18 06:04
108-90-7
0.54
1
12/16/18 06:04
75-00-3
0.14
1
12/16/18 06:04
67-66-3
0.11
1
12/16/18 06:04
74-87-3
2.0
1
12/16/18 06:04
96-12-8
0.21
1
12/16/18 06:04
124-48-1
0.27
1
12/16/18 06:04
106-93-4
0.21
1
12/16/18 06:04
74-95-3
0.30
1
12/16/18 06:04
95-50-1
0.33
1
12/16/18 06:04
106-46-7
1.0
1
12/16/18 06:04
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-20 Lab ID: 92410048001 Collected: 12/05/18 15:22 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Isobutanol
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
2540C Total Dissolved Solids
Total Dissolved Solids
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 8260E
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
5.0
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
102
%
70-130
93
%
70-130
100
%
70-130
Analytical Method: EPA 8260E Mod.
ND
ug/L
2.0
89
%
50-150
77
%
50-150
Analytical Method: SM
2320B-2011
5290
ug/L
5000
Analytical Method: SM
2540C-2011
82000
ug/L
25000
0.32
1
12/16/18 06:04
75-34-3
0.24
1
12/16/18 06:04
107-06-2
0.56
1
12/16/18 06:04
75-35-4
0.19
1
12/16/18 06:04
156-59-2
0.49
1
12/16/18 06:04
156-60-5
0.27
1
12/16/18 06:04
78-87-5
0.13
1
12/16/18 06:04
10061-01-5
0.26
1
12/16/18 06:04
10061-02-6
0.30
1
12/16/18 06:04
100-41-4
0.46
1
12/16/18 06:04
591-78-6
0.32
1
12/16/18 06:04
74-88-4
35.0
1
12/16/18 06:04
78-83-1
0.97
1
12/16/18 06:04
75-09-2
0.33
1
12/16/18 06:04
108-10-1
0.26
1
12/16/18 06:04
100-42-5
0.33
1
12/16/18 06:04
630-20-6
0.40
1
12/16/18 06:04
79-34-5
0.46
1
12/16/18 06:04
127-18-4
3.1
1
12/16/18 06:04
109-99-9
0.26
1
12/16/18 06:04
108-88-3
0.48
1
12/16/18 06:04
71-55-6
0.29
1
12/16/18 06:04
79-00-5
0.47
1
12/16/18 06:04
79-01-6
0.20
1
12/16/18 06:04
75-69-4
0.41
1
12/16/18 06:04
96-18-4
0.35
1
12/16/18 06:04
108-05-4
0.62
1
12/16/18 06:04
75-01-4
0.66
1
12/16/18 06:04
1330-20-7
1 12/16/18 06:04 460-00-4
1 12/16/18 06:04 17060-07-0
1 12/16/18 06:04 2037-26-5
1.9 1 12/14/18 16:54 123-91-1
1 12/14/18 16:54 17060-07-0
1 12/14/18 16:54 2037-26-5
1000 1 12/17/18 16:40
25000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/11/18 17:30
Page 9 of 72

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-20
Lab ID: 92410048001 Collected: 12/05/18 15:22
Received: 12/07/18 10:20 Matrix: Water
Report
Parameters
Results Units Limit MDL DF
Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Sulfate
ND ug/L 1000 500 1
12/20/18 04:05 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Chloride
2230 ug/L 1000 500 1
12/17/1810:22 16887-00-6
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 72

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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-23S Lab ID: 92410048002 Collected: 12/05/18 15:40 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Tin
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.9
1
12/08/18 06:50
12/17/18 22:05
7440-36-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:05
7440-38-2
5.5
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-39-3
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:05
7440-41-7
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:05
7440-43-9
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-47-3
3.1J
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-48-4
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-50-8
323
ug/L
50.0
25.0
1
12/08/18 06:50
12/17/18 22:05
7439-89-6
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7439-92-1
73.7
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7439-96-5
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-02-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:05
7782-49-2
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-22-4
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-31-5
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:05
7440-62-2
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:05
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/12/18 15:31 12/15/18 01:38 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 12/11/1818:33 12/12/1816:22 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
25.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
10.0
1
12/16/18 06:21
67-64-1
1.9
1
12/16/18 06:21
107-13-1
0.25
1
12/16/18 06:21
71-43-2
0.17
1
12/16/18 06:21
74-97-5
0.18
1
12/16/18 06:21
75-27-4
0.26
1
12/16/18 06:21
75-25-2
0.29
1
12/16/18 06:21
74-83-9
0.96
1
12/16/18 06:21
78-93-3
1.2
1
12/16/18 06:21
75-15-0
0.25
1
12/16/18 06:21
56-23-5
0.23
1
12/16/18 06:21
108-90-7
0.54
1
12/16/18 06:21
75-00-3
0.14
1
12/16/18 06:21
67-66-3
0.11
1
12/16/18 06:21
74-87-3
2.0
1
12/16/18 06:21
96-12-8
0.21
1
12/16/18 06:21
124-48-1
0.27
1
12/16/18 06:21
106-93-4
0.21
1
12/16/18 06:21
74-95-3
0.30
1
12/16/18 06:21
95-50-1
0.33
1
12/16/18 06:21
106-46-7
1.0
1
12/16/18 06:21
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 72

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9800 Kincey Ave. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-23S Lab ID: 92410048002 Collected: 12/05/18 15:40 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Isobutanol
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
2540C Total Dissolved Solids
Total Dissolved Solids
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 8260E
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
5.0
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
97
%
70-130
92
%
70-130
99
%
70-130
Analytical Method: EPA 8260E Mod.
ND
ug/L
2.0
89
%
50-150
77
%
50-150
Analytical Method: SM
2320B-2011
2980J
ug/L
5000
Analytical Method: SM
2540C-2011
25000
ug/L
25000
0.32
1
12/16/18 06:21
75-34-3
0.24
1
12/16/18 06:21
107-06-2
0.56
1
12/16/18 06:21
75-35-4
0.19
1
12/16/18 06:21
156-59-2
0.49
1
12/16/18 06:21
156-60-5
0.27
1
12/16/18 06:21
78-87-5
0.13
1
12/16/18 06:21
10061-01-5
0.26
1
12/16/18 06:21
10061-02-6
0.30
1
12/16/18 06:21
100-41-4
0.46
1
12/16/18 06:21
591-78-6
0.32
1
12/16/18 06:21
74-88-4
35.0
1
12/16/18 06:21
78-83-1
0.97
1
12/16/18 06:21
75-09-2
0.33
1
12/16/18 06:21
108-10-1
0.26
1
12/16/18 06:21
100-42-5
0.33
1
12/16/18 06:21
630-20-6
0.40
1
12/16/18 06:21
79-34-5
0.46
1
12/16/18 06:21
127-18-4
3.1
1
12/16/18 06:21
109-99-9
0.26
1
12/16/18 06:21
108-88-3
0.48
1
12/16/18 06:21
71-55-6
0.29
1
12/16/18 06:21
79-00-5
0.47
1
12/16/18 06:21
79-01-6
0.20
1
12/16/18 06:21
75-69-4
0.41
1
12/16/18 06:21
96-18-4
0.35
1
12/16/18 06:21
108-05-4
0.62
1
12/16/18 06:21
75-01-4
0.66
1
12/16/18 06:21
1330-20-7
1 12/16/18 06:21 460-00-4
1 12/16/18 06:21 17060-07-0
1 12/16/18 06:21 2037-26-5
1.9 1 12/14/18 17:13 123-91-1
1 12/14/18 17:13 17060-07-0
1 12/14/18 17:13 2037-26-5
1000 1 12/17/18 16:45
25000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/11/18 17:30
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-23S Lab ID: 92410048002 Collected: 12/05/18 15:40 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993
Sulfate 1030 ug/L 1000 500 1 12/20/18 04:50 14808-79-8
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Chloride 2710 ug/L 1000 500 1 12/17/1810:23 16887-00-6
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 72

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[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-24S Lab ID: 92410048003 Collected: 12/06/18 14:20 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Tin
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.9
1
12/08/18 06:50
12/17/18 22:08
7440-36-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:08
7440-38-2
32.6
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-39-3
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:08
7440-41-7
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:08
7440-43-9
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-47-3
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-48-4
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-50-8
1550
ug/L
50.0
25.0
1
12/08/18 06:50
12/17/18 22:08
7439-89-6
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7439-92-1
29.5
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7439-96-5
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-02-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:08
7782-49-2
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-22-4
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-31-5
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:08
7440-62-2
8.7J
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:08
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.081J ug/L 0.10 0.060 1 12/12/18 15:31 12/15/18 01:40 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 12/11/1818:33 12/12/1816:25 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
25.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
10.0
1
12/19/18 21:10
67-64-1
1.9
1
12/19/18 21:10
107-13-1
0.25
1
12/19/18 21:10
71-43-2
0.17
1
12/19/18 21:10
74-97-5
0.18
1
12/19/18 21:10
75-27-4
0.26
1
12/19/18 21:10
75-25-2
0.29
1
12/19/18 21:10
74-83-9
0.96
1
12/19/18 21:10
78-93-3
1.2
1
12/19/18 21:10
75-15-0
0.25
1
12/19/18 21:10
56-23-5
0.23
1
12/19/18 21:10
108-90-7
0.54
1
12/19/18 21:10
75-00-3
0.14
1
12/19/18 21:10
67-66-3
0.11
1
12/19/18 21:10
74-87-3
2.0
1
12/19/18 21:10
96-12-8
0.21
1
12/19/18 21:10
124-48-1
0.27
1
12/19/18 21:10
106-93-4
0.21
1
12/19/18 21:10
74-95-3
0.30
1
12/19/18 21:10
95-50-1
0.33
1
12/19/18 21:10
106-46-7
1.0
1
12/19/18 21:10
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-24S Lab ID: 92410048003 Collected: 12/06/18 14:20 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Isobutanol
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
2540C Total Dissolved Solids
Total Dissolved Solids
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 8260E
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
5.0
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
94
%
70-130
103
%
70-130
106
%
70-130
Analytical Method: EPA 8260E Mod.
ND
ug/L
2.0
87
%
50-150
75
%
50-150
Analytical Method: SM
2320B-2011
3580J
ug/L
5000
Analytical Method: SM
2540C-2011
26000
ug/L
25000
0.32
1
12/19/18 21:10
75-34-3
0.24
1
12/19/18 21:10
107-06-2
0.56
1
12/19/18 21:10
75-35-4
0.19
1
12/19/18 21:10
156-59-2
0.49
1
12/19/18 21:10
156-60-5
0.27
1
12/19/18 21:10
78-87-5
0.13
1
12/19/18 21:10
10061-01-5
0.26
1
12/19/18 21:10
10061-02-6
0.30
1
12/19/18 21:10
100-41-4
0.46
1
12/19/18 21:10
591-78-6
0.32
1
12/19/18 21:10
74-88-4
35.0
1
12/19/18 21:10
78-83-1
0.97
1
12/19/18 21:10
75-09-2
0.33
1
12/19/18 21:10
108-10-1
0.26
1
12/19/18 21:10
100-42-5
0.33
1
12/19/18 21:10
630-20-6
0.40
1
12/19/18 21:10
79-34-5
0.46
1
12/19/18 21:10
127-18-4
3.1
1
12/19/18 21:10
109-99-9
0.26
1
12/19/18 21:10
108-88-3
0.48
1
12/19/18 21:10
71-55-6
0.29
1
12/19/18 21:10
79-00-5
0.47
1
12/19/18 21:10
79-01-6
0.20
1
12/19/18 21:10
75-69-4
0.41
1
12/19/18 21:10
96-18-4
0.35
1
12/19/18 21:10
108-05-4
0.62
1
12/19/18 21:10
75-01-4
0.66
1
12/19/18 21:10
1330-20-7
1 12/19/18 21:10 460-00-4
1 12/19/18 21:10 17060-07-0
1 12/19/18 21:10 2037-26-5
1.9 1 12/14/18 22:42 123-91-1
1 12/14/18 22:42 17060-07-0
1 12/14/18 22:42 2037-26-5
1000 1 12/18/18 22:10
25000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/11/18 21:12
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-24S Lab ID: 92410048003 Collected: 12/06/18 14:20 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993
Sulfate ND ug/L 1000 500 1 12/20/18 05:05 14808-79-8
4500 Chloride Analytical Method: SM 4500-CI-E-2011
Chloride 2760 ug/L 1000 500 1 12/17/1810:24 16887-00-6
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 72

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-30 Lab ID: 92410048004 Collected: 12/05/18 16:09 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Manganese
Nickel
Selenium
Silver
Tin
Vanadium
Zinc
6020 MET ICPMS
Thallium
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.9
1
12/08/18 06:50
12/17/18 22:11
7440-36-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:11
7440-38-2
58.4
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-39-3
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:11
7440-41-7
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:11
7440-43-9
4.1J
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-47-3
3.7J
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-48-4
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-50-8
5440
ug/L
50.0
25.0
1
12/08/18 06:50
12/17/18 22:11
7439-89-6
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7439-92-1
477
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7439-96-5
3.4J
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-02-0
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:11
7782-49-2
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-22-4
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-31-5
6.6
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:11
7440-62-2
15.5
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:11
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.13 ug/L 0.10 0.060 1 12/12/18 15:31 12/15/18 03:27 7440-28-0
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 12/11/1818:33 12/12/1816:27 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
25.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
10.0
1
12/16/18 06:38
67-64-1
1.9
1
12/16/18 06:38
107-13-1
0.25
1
12/16/18 06:38
71-43-2
0.17
1
12/16/18 06:38
74-97-5
0.18
1
12/16/18 06:38
75-27-4
0.26
1
12/16/18 06:38
75-25-2
0.29
1
12/16/18 06:38
74-83-9
0.96
1
12/16/18 06:38
78-93-3
1.2
1
12/16/18 06:38
75-15-0
0.25
1
12/16/18 06:38
56-23-5
0.23
1
12/16/18 06:38
108-90-7
0.54
1
12/16/18 06:38
75-00-3
0.14
1
12/16/18 06:38
67-66-3
0.11
1
12/16/18 06:38
74-87-3
2.0
1
12/16/18 06:38
96-12-8
0.21
1
12/16/18 06:38
124-48-1
0.27
1
12/16/18 06:38
106-93-4
0.21
1
12/16/18 06:38
74-95-3
0.30
1
12/16/18 06:38
95-50-1
0.33
1
12/16/18 06:38
106-46-7
1.0
1
12/16/18 06:38
110-57-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-30 Lab ID: 92410048004 Collected: 12/05/18 16:09 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Isobutanol
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Tetrahydrofuran
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
2320B Alkalinity
Alkalinity, Total as CaCO3
2540C Total Dissolved Solids
Total Dissolved Solids
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 8260E
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
5.0
ND
ug/L
100
ND
ug/L
1.0
ND
ug/L
5.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
101
%
70-130
89
%
70-130
100
%
70-130
Analytical Method: EPA 8260E Mod.
ND
ug/L
2.0
88
%
50-150
76
%
50-150
Analytical Method: SM
2320B-2011
16200
ug/L
5000
Analytical Method: SM
2540C-2011
55000
ug/L
25000
0.32
1
12/16/18 06:38
75-34-3
0.24
1
12/16/18 06:38
107-06-2
0.56
1
12/16/18 06:38
75-35-4
0.19
1
12/16/18 06:38
156-59-2
0.49
1
12/16/18 06:38
156-60-5
0.27
1
12/16/18 06:38
78-87-5
0.13
1
12/16/18 06:38
10061-01-5
0.26
1
12/16/18 06:38
10061-02-6
0.30
1
12/16/18 06:38
100-41-4
0.46
1
12/16/18 06:38
591-78-6
0.32
1
12/16/18 06:38
74-88-4
35.0
1
12/16/18 06:38
78-83-1
0.97
1
12/16/18 06:38
75-09-2
0.33
1
12/16/18 06:38
108-10-1
0.26
1
12/16/18 06:38
100-42-5
0.33
1
12/16/18 06:38
630-20-6
0.40
1
12/16/18 06:38
79-34-5
0.46
1
12/16/18 06:38
127-18-4
3.1
1
12/16/18 06:38
109-99-9
0.26
1
12/16/18 06:38
108-88-3
0.48
1
12/16/18 06:38
71-55-6
0.29
1
12/16/18 06:38
79-00-5
0.47
1
12/16/18 06:38
79-01-6
0.20
1
12/16/18 06:38
75-69-4
0.41
1
12/16/18 06:38
96-18-4
0.35
1
12/16/18 06:38
108-05-4
0.62
1
12/16/18 06:38
75-01-4
0.66
1
12/16/18 06:38
1330-20-7
1 12/16/18 06:38 460-00-4
1 12/16/18 06:38 17060-07-0
1 12/16/18 06:38 2037-26-5
1.9 1 12/14/18 17:33 123-91-1
1 12/14/18 17:33 17060-07-0
1 12/14/18 17:33 2037-26-5
1000 1 12/17/18 16:49
25000 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/11/18 17:30
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-30
Lab ID: 92410048004 Collected: 12/05/18 16:09
Received: 12/07/18 10:20 Matrix: Water
Report
Parameters
Results Units Limit MDL DF
Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Sulfate
ND ug/L 1000 500 1
12/20/18 05:20 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Chloride
1310 ug/L 1000 500 1
12/17/1810:29 16887-00-6
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 19 of 72

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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-38 Lab ID: 92410048005 Collected: 12/06/18 13:00 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
RSK 175 Headspace Analytical Method: RSK 175 Modified
Methane 12300 ug/L 10.0 10.0 1 12/12/1812:06 74-82-8
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
12/08/18 06:50
12/17/18 22:14
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:14
7440-38-2
Barium
106
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:14
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:14
7440-43-9
Chromium
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-47-3
Cobalt
17.5
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-48-4
Copper
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-50-8
Iron
17600
ug/L
50.0
25.0
1
12/08/18 06:50
12/17/18 22:14
7439-89-6
Lead
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7439-92-1
Manganese
4870
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7439-96-5
Nickel
4.9J
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:14
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-22-4
Tin
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-31-5
Vanadium
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:14
7440-62-2
Zinc
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:14
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
12/12/18 15:31
12/15/18 03:40
7440-28-0
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 12/11/1818:33 12/12/1816:29 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
25.0
ND
ug/L
10.0
5.6
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
0.83J
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
10.0
1
12/19/18 21:28
67-64-1
1.9
1
12/19/18 21:28
107-13-1
0.25
1
12/19/18 21:28
71-43-2
0.17
1
12/19/18 21:28
74-97-5
0.18
1
12/19/18 21:28
75-27-4
0.26
1
12/19/18 21:28
75-25-2
0.29
1
12/19/18 21:28
74-83-9
0.96
1
12/19/18 21:28
78-93-3
1.2
1
12/19/18 21:28
75-15-0
0.25
1
12/19/18 21:28
56-23-5
0.23
1
12/19/18 21:28
108-90-7
0.54
1
12/19/18 21:28
75-00-3
0.14
1
12/19/18 21:28
67-66-3
0.11
1
12/19/18 21:28
74-87-3
2.0
1
12/19/18 21:28
96-12-8
0.21
1
12/19/18 21:28
124-48-1
0.27
1
12/19/18 21:28
106-93-4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 20 of 72

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-38 Lab ID: 92410048005 Collected: 12/06/18 13:00 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
Dibromomethane
ND
ug/L
1.0
0.21
1
12/19/18 21:28
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.30
1
12/19/18 21:28
95-50-1
1,4-Dichlorobenzene
16.9
ug/L
1.0
0.33
1
12/19/18 21:28
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1.0
1
12/19/18 21:28
110-57-6
1,1-Dichloroethane
5.2
ug/L
1.0
0.32
1
12/19/18 21:28
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
12/19/18 21:28
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.56
1
12/19/18 21:28
75-35-4
cis-1,2-Dichloroethene
6.9
ug/L
1.0
0.19
1
12/19/18 21:28
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.49
1
12/19/18 21:28
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
12/19/18 21:28
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
12/19/18 21:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
12/19/18 21:28
10061-02-6
Ethylbenzene
0.86J
ug/L
1.0
0.30
1
12/19/18 21:28
100-41-4
2-Hexanone
ND
ug/L
5.0
0.46
1
12/19/18 21:28
591-78-6
lodomethane
ND
ug/L
5.0
0.32
1
12/19/18 21:28
74-88-4
Isobutanol
ND
ug/L
100
35.0
1
12/19/18 21:28
78-83-1
Methylene Chloride
ND
ug/L
1.0
0.97
1
12/19/18 21:28
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
0.33
1
12/19/18 21:28
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
12/19/18 21:28
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.33
1
12/19/18 21:28
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.40
1
12/19/18 21:28
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
12/19/18 21:28
127-18-4
Tetrahydrofuran
447
ug/L
10.0
3.1
1
12/19/18 21:28
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
12/19/18 21:28
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
12/19/18 21:28
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
12/19/18 21:28
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
12/19/18 21:28
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
12/19/18 21:28
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
12/19/18 21:28
96-18-4
Vinyl acetate
ND
ug/L
2.0
0.35
1
12/19/18 21:28
108-05-4
Vinyl chloride
4.3
ug/L
1.0
0.62
1
12/19/18 21:28
75-01-4
Xylene (Total)
14.7
ug/L
1.0
0.66
1
12/19/18 21:28
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/19/18 21:28
460-00-4
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
12/19/18 21:28
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
12/19/18 21:28
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
2.4
ug/L
2.0
1.9
1
12/14/18 23:01
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
87
%
50-150
1
12/14/18 23:01
17060-07-0
Toluene-d8 (S)
75
%
50-150
1
12/14/18 23:01
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
263000
ug/L
5000
1000
1
12/18/18 22:15
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-38
Lab ID: 92410048005 Collected:
12/06/18 13:00
Received: 12/07/18 10:20 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Total Dissolved Solids
277000 ug/L 25000
25000
1
12/11/18 21:12
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Sulfate
716J ug/L 1000
500
1
12/20/18 05:35 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Chloride
7280 ug/L 1000
500
1
12/17/1810:30 16887-00-6
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 22 of 72

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-35 Lab ID: 92410048006 Collected: 12/05/18 15:49 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
RSK 175 Headspace Analytical Method: RSK 175 Modified
Methane ND ug/L 10.0 10.0 1 12/12/1817:59 74-82-8
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.9
1
12/08/18 06:50
12/17/18 22:17
7440-36-0
Arsenic
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:17
7440-38-2
Barium
42.8
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-39-3
Beryllium
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:17
7440-41-7
Cadmium
ND
ug/L
1.0
0.50
1
12/08/18 06:50
12/17/18 22:17
7440-43-9
Chromium
3.8J
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-47-3
Cobalt
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-48-4
Copper
4.1J
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-50-8
Iron
3410
ug/L
50.0
25.0
1
12/08/18 06:50
12/17/18 22:17
7439-89-6
Lead
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7439-92-1
Manganese
41.2
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7439-96-5
Nickel
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-02-0
Selenium
ND
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:17
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-22-4
Tin
ND
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-31-5
Vanadium
6.2
ug/L
5.0
2.5
1
12/08/18 06:50
12/17/18 22:17
7440-62-2
Zinc
7.4J
ug/L
10.0
5.0
1
12/08/18 06:50
12/17/18 22:17
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA
3010A
Thallium
0.062J
ug/L
0.10
0.060
1
12/12/18 15:31
12/15/18 03:42
7440-28-0
7470 Mercury
Mercury
8260 MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Date: 12/27/2018 04:11 PM
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
ND ug/L 0.20 0.10 1 12/11/1818:33 12/12/1816:32 7439-97-6
Analytical Method: EPA 8260E
ND
ug/L
25.0
ND
ug/L
10.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
5.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
1.0
ND
ug/L
2.0
ND
ug/L
1.0
ND
ug/L
1.0
10.0
1
12/16/18 06:55
67-64-1
1.9
1
12/16/18 06:55
107-13-1
0.25
1
12/16/18 06:55
71-43-2
0.17
1
12/16/18 06:55
74-97-5
0.18
1
12/16/18 06:55
75-27-4
0.26
1
12/16/18 06:55
75-25-2
0.29
1
12/16/18 06:55
74-83-9
0.96
1
12/16/18 06:55
78-93-3
1.2
1
12/16/18 06:55
75-15-0
0.25
1
12/16/18 06:55
56-23-5
0.23
1
12/16/18 06:55
108-90-7
0.54
1
12/16/18 06:55
75-00-3
0.14
1
12/16/18 06:55
67-66-3
0.11
1
12/16/18 06:55
74-87-3
2.0
1
12/16/18 06:55
96-12-8
0.21
1
12/16/18 06:55
124-48-1
0.27
1
12/16/18 06:55
106-93-4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-35 Lab ID: 92410048006 Collected: 12/05/18 15:49 Received: 12/07/18 10:20 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
Dibromomethane
ND
ug/L
1.0
0.21
1
12/16/18 06:55
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.30
1
12/16/18 06:55
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.33
1
12/16/18 06:55
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1.0
1
12/16/18 06:55
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.32
1
12/16/18 06:55
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.24
1
12/16/18 06:55
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.56
1
12/16/18 06:55
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.19
1
12/16/18 06:55
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.49
1
12/16/18 06:55
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.27
1
12/16/18 06:55
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.13
1
12/16/18 06:55
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.26
1
12/16/18 06:55
10061-02-6
Ethylbenzene
ND
ug/L
1.0
0.30
1
12/16/18 06:55
100-41-4
2-Hexanone
ND
ug/L
5.0
0.46
1
12/16/18 06:55
591-78-6
lodomethane
ND
ug/L
5.0
0.32
1
12/16/18 06:55
74-88-4
Isobutanol
ND
ug/L
100
35.0
1
12/16/18 06:55
78-83-1
Methylene Chloride
ND
ug/L
1.0
0.97
1
12/16/18 06:55
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
0.33
1
12/16/18 06:55
108-10-1
Styrene
ND
ug/L
1.0
0.26
1
12/16/18 06:55
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.33
1
12/16/18 06:55
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.40
1
12/16/18 06:55
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.46
1
12/16/18 06:55
127-18-4
Tetrahydrofuran
ND
ug/L
10.0
3.1
1
12/16/18 06:55
109-99-9
Toluene
ND
ug/L
1.0
0.26
1
12/16/18 06:55
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.48
1
12/16/18 06:55
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.29
1
12/16/18 06:55
79-00-5
Trichloroethene
ND
ug/L
1.0
0.47
1
12/16/18 06:55
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.20
1
12/16/18 06:55
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.41
1
12/16/18 06:55
96-18-4
Vinyl acetate
ND
ug/L
2.0
0.35
1
12/16/18 06:55
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.62
1
12/16/18 06:55
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.66
1
12/16/18 06:55
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/16/18 06:55
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
12/16/18 06:55
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
12/16/18 06:55
2037-26-5
8260 MSV SIM
Analytical Method: EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1.9
1
12/14/18 17:52
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92
%
50-150
1
12/14/18 17:52
17060-07-0
Toluene-d8 (S)
77
%
50-150
1
12/14/18 17:52
2037-26-5
2320B Alkalinity
Analytical Method: SM
2320B-2011
Alkalinity, Total as CaCO3
8340
ug/L
5000
1000
1
12/17/18 17:04
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Sample: 1203-MW-35
Lab ID: 92410048006 Collected:
12/05/18 15:49
Received: 12/07/18 10:20 Matrix: Water
Report
Parameters
Results Units Limit
MDL
DF
Prepared Analyzed CAS No. Qual
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2011
Total Dissolved Solids
37000 ug/L 25000
25000
1
12/11/18 21:02
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1
1993
Sulfate
541J ug/L 1000
500
1
12/20/18 06:35 14808-79-8
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Chloride
1200 ug/L 1000
500
1
12/17/1810:31 16887-00-6
Date: 12/27/2018 04:11 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 25 of 72

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QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 446939
Analysis Method: RSK 175 Modified
QC Batch Method: RSK 175 Modified
Analysis Description: RSK
175 HEADSPACE
Associated Lab Samples: 92410048005
METHOD BLANK: 2449332
Matrix: Water
Associated Lab Samples: 92410048005
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Methane
ug/L
ND 10.0
10.0
12/12/1810:04
LABORATORY CONTROL SAMPLE: 2449333
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Methane
ug/L
396 460
116
70-130
MATRIX SPIKE SAMPLE: 2449642
92410041004 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Methane
ug/L
17.4 396
480
117
70-130
SAMPLE DUPLICATE: 2449846
92410258004 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Methane
ug/L
3120 3360
8
20
SAMPLE DUPLICATE: 2452734
92410258009 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Methane
ug/L
ND ND
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 72

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447111
Analysis Method: RSK 175 Modified
QC Batch Method: RSK 175 Modified
Analysis Description: RSK
175 HEADSPACE
Associated Lab Samples: 92410048006
METHOD BLANK: 2450241
Matrix: Water
Associated Lab Samples: 92410048006
Blank Reporting
Parameter
Units
Result Limit
MDL
Analyzed
Qualifiers
Methane
ug/L
ND 10.0
10.0
12/12/1816:58
LABORATORY CONTROL SAMPLE: 2450242
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Methane
ug/L
396 464
117
70-130
MATRIX SPIKE SAMPLE: 2450244
92410041003 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Methane
ug/L
ND 396
432
109
70-130
SAMPLE DUPLICATE: 2450243
92409899006 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Methane
ug/L
ND ND
20
SAMPLE DUPLICATE: 2450245
92410258019 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Methane
ug/L
ND ND
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 446706
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury
Associated Lab Samples: 92410048001, 92410048002,
92410048003, 92410048004, 92410048005, 92410048006
METHOD BLANK: 2448241
Matrix: Water
Associated Lab Samples: 92410048001, 92410048002,
92410048003, 92410048004, 92410048005, 92410048006
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Mercury ug/L
ND 0.20 0.10 12/12/1815:44
LABORATORY CONTROL SAMPLE: 2448242
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mercury ug/L
2.5 2.7 108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2448243 2448244
MS MSD
92410015001
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Mercury ug/L ND
2.5 2.5 2.6 2.7 105 107
75-125 2 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 446531 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92410048001, 92410048002, 92410048003, 92410048004, 92410048005, 92410048006
METHOD BLANK: 2447415 Matrix: Water
Associated Lab Samples: 92410048001, 92410048002, 92410048003, 92410048004, 92410048005, 92410048006
Blank Reporting
Parameter Units Result Limit MDL Analyzed
Antimony
ug/L
ND
5.0
3.9
12/17/18 21:23
Arsenic
ug/L
ND
10.0
5.0
12/17/18 21:23
Barium
ug/L
ND
5.0
2.5
12/17/18 21:23
Beryllium
ug/L
ND
1.0
0.50
12/17/18 21:23
Cadmium
ug/L
ND
1.0
0.50
12/17/18 21:23
Chromium
ug/L
ND
5.0
2.5
12/17/18 21:23
Cobalt
ug/L
ND
5.0
2.5
12/17/18 21:23
Copper
ug/L
ND
5.0
2.5
12/17/18 21:23
Iron
ug/L
ND
50.0
25.0
12/17/18 21:23
Lead
ug/L
ND
5.0
2.5
12/17/18 21:23
Manganese
ug/L
ND
5.0
2.5
12/17/18 21:23
Nickel
ug/L
ND
5.0
2.5
12/17/18 21:23
Selenium
ug/L
ND
10.0
5.0
12/17/18 21:23
Silver
ug/L
ND
5.0
2.5
12/17/18 21:23
Tin
ug/L
ND
5.0
2.5
12/17/18 21:23
Vanadium
ug/L
ND
5.0
2.5
12/17/18 21:23
Zinc
ug/L
ND
10.0
5.0
12/17/18 21:23
LABORATORY CONTROL SAMPLE:
Parameter
2447416
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
524
105
80-120
Arsenic
ug/L
500
496
99
80-120
Barium
ug/L
500
522
104
80-120
Beryllium
ug/L
500
524
105
80-120
Cadmium
ug/L
500
520
104
80-120
Chromium
ug/L
500
525
105
80-120
Cobalt
ug/L
500
517
103
80-120
Copper
ug/L
500
538
108
80-120
Iron
ug/L
5000
5390
108
80-120
Lead
ug/L
500
503
101
80-120
Manganese
ug/L
500
525
105
80-120
Nickel
ug/L
500
521
104
80-120
Selenium
ug/L
500
512
102
80-120
Silver
ug/L
250
273
109
80-120
Tin
ug/L
500
527
105
80-120
Vanadium
ug/L
500
527
105
80-120
Zinc
ug/L
500
517
103
80-120
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 72

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE:
2447417
2447418
MS
MSD
92410015001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
494
479
99
96
75-125
3
20
Arsenic
ug/L
ND
500
500
464
452
93
90
75-125
3
20
Barium
ug/L
9.9
500
500
506
492
99
96
75-125
3
20
Beryllium
ug/L
ND
500
500
495
482
99
96
75-125
3
20
Cadmium
ug/L
ND
500
500
494
480
99
96
75-125
3
20
Chromium
ug/L
ND
500
500
497
483
99
97
75-125
3
20
Cobalt
ug/L
ND
500
500
487
475
97
95
75-125
3
20
Copper
ug/L
5.8
500
500
500
484
99
96
75-125
3
20
Iron
ug/L
167
5000
5000
5250
5110
102
99
75-125
3
20
Lead
ug/L
ND
500
500
477
464
95
93
75-125
3
20
Manganese
ug/L
10
500
500
507
490
99
96
75-125
3
20
Nickel
ug/L
ND
500
500
492
480
98
96
75-125
3
20
Selenium
ug/L
ND
500
500
482
470
96
94
75-125
2
20
Silver
ug/L
ND
250
250
251
243
100
97
75-125
3
20
Tin
ug/L
ND
500
500
499
485
100
97
75-125
3
20
Vanadium
ug/L
ND
500
500
500
487
100
97
75-125
3
20
Zinc
ug/L
51.4
500
500
539
525
97
95
75-125
3
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 72

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 446925
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92410048004, 92410048005,
92410048006
METHOD BLANK: 2449254
Matrix: Water
Associated Lab Samples: 92410048004, 92410048005,
92410048006
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Thallium ug/L
ND 0.10 0.060
12/15/18 03:23
LABORATORY CONTROL SAMPLE: 2449255
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 9.4 94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449256 2449257
MS MSD
92410048004
Spike Spike MS MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec
Limits RPD RPD Qual
Thallium ug/L 0.13
10 10 9.6 9.9
94 97
75-125 3 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449258 2449259
MS MSD
92410090003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 9.7 9.7 96 97 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447050
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92410048001, 92410048002,
92410048003
METHOD BLANK: 2449871
Matrix: Water
Associated Lab Samples: 92410048001, 92410048002,
92410048003
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed
Qualifiers
Thallium ug/L
ND 0.10 0.060
12/15/18 00:49
LABORATORY CONTROL SAMPLE: 2449872
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 9.4 94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449873 2449874
MS MSD
92409256011
Spike Spike MS MSD
MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec
Limits RPD RPD Qual
Thallium ug/L ND
10 10 9.5 9.5
95 95
75-125 0 20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449875 2449876
MS MSD
92410040003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 8.9 9.8 89 97 75-125 9 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447864 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92410048001, 92410048002, 92410048004, 92410048006
METHOD BLANK: 2453789 Matrix: Water
Associated Lab Samples: 92410048001, 92410048002, 92410048004, 92410048006
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.33
12/16/18 00:56
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
12/16/18 00:56
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.40
12/16/18 00:56
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
12/16/18 00:56
1,1-Dichloroethane
ug/L
ND
1.0
0.32
12/16/18 00:56
1,1-Dichloroethene
ug/L
ND
1.0
0.56
12/16/18 00:56
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
12/16/18 00:56
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
2.0
12/16/18 00:56
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
12/16/18 00:56
1,2-Dichlorobenzene
ug/L
ND
1.0
0.30
12/16/18 00:56
1,2-Dichloroethane
ug/L
ND
1.0
0.24
12/16/18 00:56
1,2-Dichloropropane
ug/L
ND
1.0
0.27
12/16/18 00:56
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
12/16/18 00:56
2-Butanone (MEK)
ug/L
ND
5.0
0.96
12/16/18 00:56
2-Hexanone
ug/L
ND
5.0
0.46
12/16/18 00:56
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
0.33
12/16/18 00:56
Acetone
ug/L
ND
25.0
10.0
12/16/18 00:56
Acrylonitrile
ug/L
ND
10.0
1.9
12/16/18 00:56
Benzene
ug/L
ND
1.0
0.25
12/16/18 00:56
Bromochloromethane
ug/L
ND
1.0
0.17
12/16/18 00:56
Bromodichloromethane
ug/L
ND
1.0
0.18
12/16/18 00:56
Bromoform
ug/L
ND
1.0
0.26
12/16/18 00:56
Bromomethane
ug/L
ND
2.0
0.29
12/16/18 00:56
Carbon disulfide
ug/L
ND
2.0
1.2
12/16/18 00:56
Carbon tetrachloride
ug/L
ND
1.0
0.25
12/16/18 00:56
Chlorobenzene
ug/L
ND
1.0
0.23
12/16/18 00:56
Chloroethane
ug/L
ND
1.0
0.54
12/16/18 00:56
Chloroform
ug/L
ND
1.0
0.14
12/16/18 00:56
Chloromethane
ug/L
ND
1.0
0.11
12/16/18 00:56
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.19
12/16/18 00:56
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
12/16/18 00:56
Dibromochloromethane
ug/L
ND
1.0
0.21
12/16/18 00:56
Dibromomethane
ug/L
ND
1.0
0.21
12/16/18 00:56
Ethylbenzene
ug/L
ND
1.0
0.30
12/16/18 00:56
lodomethane
ug/L
ND
5.0
0.32
12/16/18 00:56
Isobutanol
ug/L
ND
100
35.0
12/16/18 00:56
Methylene Chloride
ug/L
ND
1.0
0.97
12/16/18 00:56
Styrene
ug/L
ND
1.0
0.26
12/16/18 00:56
Tetrachloroethene
ug/L
ND
1.0
0.46
12/16/18 00:56
Tetrahydrofuran
ug/L
ND
10.0
3.1
12/16/18 00:56
Toluene
ug/L
ND
1.0
0.26
12/16/18 00:56
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
METHOD BLANK: 2453789 Matrix: Water
Associated Lab Samples: 92410048001, 92410048002, 92410048004, 92410048006
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.49
12/16/18 00:56
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
12/16/18 00:56
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
1.0
12/16/18 00:56
Trichloroethene
ug/L
ND
1.0
0.47
12/16/18 00:56
Trichlorofluoromethane
ug/L
ND
1.0
0.20
12/16/18 00:56
Vinyl acetate
ug/L
ND
2.0
0.35
12/16/18 00:56
Vinyl chloride
ug/L
ND
1.0
0.62
12/16/18 00:56
Xylene (Total)
ug/L
ND
1.0
0.66
12/16/18 00:56
1,2-Dichloroethane-d4 (S)
%
84
70-130
12/16/18 00:56
4-Bromofluorobenzene (S)
%
100
70-130
12/16/18 00:56
Toluene-d8 (S)
%
100
70-130
12/16/18 00:56
LABORATORY CONTROL SAMPLE:
2453790
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
70-130
1,1,1-Trichloroethane
ug/L
50
49.1
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.7
105
70-130
1,1,2-Trichloroethane
ug/L
50
54.8
110
70-130
1,1-Dichloroethane
ug/L
50
50.8
102
70-130
1,1-Dichloroethene
ug/L
50
52.2
104
70-130
1,2,3-Trichloropropane
ug/L
50
45.9
92
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.0
106
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.3
101
70-130
1,2-Dichlorobenzene
ug/L
50
48.6
97
70-130
1,2-Dichloroethane
ug/L
50
48.2
96
70-130
1,2-Dichloropropane
ug/L
50
50.0
100
70-130
1,4-Dichlorobenzene
ug/L
50
47.9
96
70-130
2-Butanone (MEK)
ug/L
100
96.4
96
64-135
2-Hexanone
ug/L
100
97.2
97
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
97.8
98
70-130
Acetone
ug/L
100
96.3
96
61-157
Acrylonitrile
ug/L
250
246
98
61-143
Benzene
ug/L
50
53.8
108
70-130
Bromochloromethane
ug/L
50
56.8
114
70-130
Bromodichloromethane
ug/L
50
52.8
106
70-130
Bromoform
ug/L
50
49.1
98
70-130
Bromomethane
ug/L
50
40.7
81
38-130
Carbon disulfide
ug/L
50
53.8
108
68-130
Carbon tetrachloride
ug/L
50
51.3
103
70-130
Chlorobenzene
ug/L
50
51.0
102
70-130
Chloroethane
ug/L
50
48.4
97
37-142
Chloroform
ug/L
50
49.2
98
70-130
Chloromethane
ug/L
50
45.6
91
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
LABORATORY CONTROL SAMPLE: 2453790
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
51.2
102
70-130
cis-1,3-Dichloropropene
ug/L
50
53.8
108
70-130
Dibromochloromethane
ug/L
50
51.5
103
70-130
Dibromomethane
ug/L
50
56.9
114
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
lodomethane
ug/L
100
90.0
90
40-130
Isobutanol
ug/L
1000
947
95
44-144
Methylene Chloride
ug/L
50
44.4
89
67-132
Styrene
ug/L
50
52.6
105
70-130
Tetrachloroethene
ug/L
50
50.8
102
69-130
Tetrahydrofuran
ug/L
500
470
94
62-130
Toluene
ug/L
50
51.3
103
70-130
trans-1,2-Dichloroethene
ug/L
50
51.5
103
70-130
trans- 1,3-Dichloropropene
ug/L
50
54.3
109
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
47.9
96
35-189
Trichloroethene
ug/L
50
54.4
109
70-130
Trichlorofluoromethane
ug/L
50
51.0
102
63-130
Vinyl acetate
ug/L
100
99.9
100
55-143
Vinyl chloride
ug/L
50
51.7
103
70-131
Xylene (Total)
ug/L
150
158
105
70-130
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2453791
2453792
MS
MSD
92410469002
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
23.0
23.0
115
115
73-134
0 30
1,1,1-Trichloroethane
ug/L
ND
20
20
21.1
21.3
106
107
82-143
1 30
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.9
22.0
109
110
70-136
0 30
1,1,2-Trichloroethane
ug/L
ND
20
20
23.1
23.2
115
116
70-135
1 30
1,1-Dichloroethane
ug/L
ND
20
20
21.3
21.6
107
108
70-139
1 30
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.7
107
108
70-154
1 30
1,2,3-Trichloropropane
ug/L
ND
20
20
21.8
23.7
109
118
71-137
8 30
1,2-Dibromo-3-
ug/L
ND
20
20
21.6
21.0
108
105
65-134
3 30
chloropropane
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.9
21.1
109
106
70-137
3 30
1,2-Dichlorobenzene
ug/L
ND
20
20
19.9
19.2
100
96
70-133
4 30
1,2-Dichloroethane
ug/L
ND
20
20
21.1
20.7
106
104
70-137
2 30
1,2-Dichloropropane
ug/L
ND
20
20
20.8
21.0
104
105
70-140
1 30
1,4-Dichlorobenzene
ug/L
ND
20
20
19.6
20.0
98
100
70-133
2 30
2-Butanone (MEK)
ug/L
ND
40
40
40.8
39.7
102
99
60-139
3 30
2-Hexanone
ug/L
ND
40
40
41.9
40.9
105
102
65-138
2 30
4-Methyl-2-pentanone
ug/L
ND
40
40
40.8
42.0
102
105
65-135
3 30
(MIBK)
Results presented on this page are in the
units indicated by the "Units" column
except where
an alternate unit is presented to
the right
of the result.
REPORT OF LABORATORY ANALYSIS
This
report shall
not be reproduced, except
in full,
Date: 12/27/2018 04:11 PM
without
the written consent
of Pace Analytical
Services, LLC.
Page 35 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2453791
2453792
MS
MSD
92410469002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Acetone
ug/L
ND
40
40
43.4
43.8
108
110
60-148
1
30
Acrylonitrile
ug/L
ND
100
100
96.9
97.0
97
97
64-147
0
30
Benzene
ug/L
ND
20
20
23.3
22.9
116
115
70-151
2
30
Bromochloromethane
ug/L
ND
20
20
23.6
23.6
118
118
70-141
0
30
Bromodichloromethane
ug/L
ND
20
20
21.8
22.3
109
112
70-138
2
30
Bromoform
ug/L
ND
20
20
19.7
18.8
98
94
63-130
5
30
Bromomethane
ug/L
ND
20
20
15.3
16.7
76
84
15-152
9
30
Carbon disulfide
ug/L
ND
20
20
21.5
20.4
108
102
69-149
5
30
Carbon tetrachloride
ug/L
ND
20
20
23.1
23.2
115
116
70-143
0
30
Chlorobenzene
ug/L
ND
20
20
22.0
21.5
110
107
70-138
2
30
Chloroethane
ug/L
ND
20
20
21.3
20.5
106
103
52-163
4
30
Chloroform
ug/L
ND
20
20
20.9
20.8
104
104
70-139
0
30
Chloromethane
ug/L
ND
20
20
16.8
16.8
84
84
41-139
0
30
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.6
21.4
108
107
70-141
1
30
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.3
22.0
106
110
70-137
4
30
Dibromochloromethane
ug/L
ND
20
20
21.0
20.8
105
104
70-134
1
30
Dibromomethane
ug/L
ND
20
20
23.1
23.8
116
119
70-138
3
30
Ethylbenzene
ug/L
ND
20
20
22.2
21.6
111
108
66-153
3
30
lodomethane
ug/L
ND
40
40
23.4
32.5
59
81
20-138
32
30 R1
Isobutanol
ug/L
ND
400
400
399
398
100
99
41-152
0
30
Methylene Chloride
ug/L
ND
20
20
17.3
17.5
86
87
42-159
1
30
Styrene
ug/L
ND
20
20
22.7
21.3
114
107
70-135
6
30
Tetrachloroethene
ug/L
ND
20
20
22.4
21.4
112
107
59-143
4
30
Tetrahydrofuran
ug/L
ND
200
200
192
193
96
97
70-133
1
30
Toluene
ug/L
ND
20
20
21.7
22.4
109
112
59-148
3
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.9
22.2
109
111
70-146
1
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.6
22.7
108
113
70-135
5
30
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
15.6
15.1
78
75
47-135
3
30
Trichloroethene
ug/L
ND
20
20
23.5
23.9
117
119
70-147
2
30
Trichlorofluoromethane
ug/L
ND
20
20
22.0
21.3
110
107
70-148
3
30
Vinyl acetate
ug/L
ND
40
40
28.7
28.4
72
71
49-151
1
30
Vinyl chloride
ug/L
ND
20
20
19.5
19.8
97
99
70-156
2
30
Xylene (Total)
ug/L
ND
60
60
68.0
65.8
113
110
63-158
3
30
1,2-Dichloroethane-d4 (S)
%
91
92
70-130
4-Bromofluorobenzene (S)
%
104
102
70-130
Toluene-d8 (S)
%
97
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 36 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447984 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92410048003
METHOD BLANK: 2454142
Associated Lab Samples: 92410048003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.33
12/19/18 14:54
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
12/19/18 14:54
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.40
12/19/18 14:54
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
12/19/18 14:54
1,1-Dichloroethane
ug/L
ND
1.0
0.32
12/19/18 14:54
1,1-Dichloroethene
ug/L
ND
1.0
0.56
12/19/18 14:54
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
12/19/18 14:54
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
2.0
12/19/18 14:54
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
12/19/18 14:54
1,2-Dichlorobenzene
ug/L
ND
1.0
0.30
12/19/18 14:54
1,2-Dichloroethane
ug/L
ND
1.0
0.24
12/19/18 14:54
1,2-Dichloropropane
ug/L
ND
1.0
0.27
12/19/18 14:54
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
12/19/18 14:54
2-Butanone (MEK)
ug/L
ND
5.0
0.96
12/19/18 14:54
2-Hexanone
ug/L
ND
5.0
0.46
12/19/18 14:54
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
0.33
12/19/18 14:54
Acetone
ug/L
ND
25.0
10.0
12/19/18 14:54
Acrylonitrile
ug/L
ND
10.0
1.9
12/19/18 14:54
Benzene
ug/L
ND
1.0
0.25
12/19/18 14:54
Bromochloromethane
ug/L
ND
1.0
0.17
12/19/18 14:54
Bromodichloromethane
ug/L
ND
1.0
0.18
12/19/18 14:54
Bromoform
ug/L
ND
1.0
0.26
12/19/18 14:54
Bromomethane
ug/L
ND
2.0
0.29
12/19/18 14:54
Carbon disulfide
ug/L
ND
2.0
1.2
12/19/18 14:54
Carbon tetrachloride
ug/L
ND
1.0
0.25
12/19/18 14:54
Chlorobenzene
ug/L
ND
1.0
0.23
12/19/18 14:54
Chloroethane
ug/L
ND
1.0
0.54
12/19/18 14:54
Chloroform
ug/L
ND
1.0
0.14
12/19/18 14:54
Chloromethane
ug/L
ND
1.0
0.11
12/19/18 14:54
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.19
12/19/18 14:54
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
12/19/18 14:54
Dibromochloromethane
ug/L
ND
1.0
0.21
12/19/18 14:54
Dibromomethane
ug/L
ND
1.0
0.21
12/19/18 14:54
Ethylbenzene
ug/L
ND
1.0
0.30
12/19/18 14:54
lodomethane
ug/L
ND
5.0
0.32
12/19/18 14:54
Isobutanol
ug/L
ND
100
35.0
12/19/18 14:54
Methylene Chloride
ug/L
ND
1.0
0.97
12/19/18 14:54
Styrene
ug/L
ND
1.0
0.26
12/19/18 14:54
Tetrachloroethene
ug/L
ND
1.0
0.46
12/19/18 14:54
Tetrahydrofuran
ug/L
ND
10.0
3.1
12/19/18 14:54
Toluene
ug/L
ND
1.0
0.26
12/19/18 14:54
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
METHOD BLANK: 2454142
Associated Lab Samples: 92410048003
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.49
12/19/18 14:54
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
12/19/18 14:54
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
1.0
12/19/18 14:54
Trichloroethene
ug/L
ND
1.0
0.47
12/19/18 14:54
Trichlorofluoromethane
ug/L
ND
1.0
0.20
12/19/18 14:54
Vinyl acetate
ug/L
ND
2.0
0.35
12/19/18 14:54
Vinyl chloride
ug/L
ND
1.0
0.62
12/19/18 14:54
Xylene (Total)
ug/L
ND
1.0
0.66
12/19/18 14:54
1,2-Dichloroethane-d4 (S)
%
101
70-130
12/19/18 14:54
4-Bromofluorobenzene (S)
%
91
70-130
12/19/18 14:54
Toluene-d8 (S)
%
111
70-130
12/19/18 14:54
LABORATORY CONTROL SAMPLE:
2454143
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
54.5
109
70-130
1,1,1-Trichloroethane
ug/L
50
50.7
101
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
54.7
109
70-130
1,1,2-Trichloroethane
ug/L
50
55.9
112
70-130
1,1-Dichloroethane
ug/L
50
48.0
96
70-130
1,1-Dichloroethene
ug/L
50
53.5
107
70-130
1,2,3-Trichloropropane
ug/L
50
60.0
120
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
48.5
97
70-130
1,2-Dibromoethane (EDB)
ug/L
50
51.3
103
70-130
1,2-Dichlorobenzene
ug/L
50
50.9
102
70-130
1,2-Dichloroethane
ug/L
50
49.3
99
70-130
1,2-Dichloropropane
ug/L
50
53.8
108
70-130
1,4-Dichlorobenzene
ug/L
50
49.2
98
70-130
2-Butanone (MEK)
ug/L
100
115
115
64-135
2-Hexanone
ug/L
100
117
117
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
121
121
70-130
Acetone
ug/L
100
114
114
61-157
Acrylonitrile
ug/L
250
273
109
61-143
Benzene
ug/L
50
52.6
105
70-130
Bromochloromethane
ug/L
50
51.4
103
70-130
Bromodichloromethane
ug/L
50
53.7
107
70-130
Bromoform
ug/L
50
49.5
99
70-130
Bromomethane
ug/L
50
33.5
67
38-130
Carbon disulfide
ug/L
50
46.3
93
68-130
Carbon tetrachloride
ug/L
50
53.0
106
70-130
Chlorobenzene
ug/L
50
48.9
98
70-130
Chloroethane
ug/L
50
37.2
74
37-142
Chloroform
ug/L
50
46.8
94
70-130
Chloromethane
ug/L
50
43.1
86
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
LABORATORY CONTROL SAMPLE:
2454143
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
49.5
99
70-130
cis-1,3-Dichloropropene
ug/L
50
55.0
110
70-130
Dibromochloromethane
ug/L
50
53.3
107
70-130
Dibromomethane
ug/L
50
52.8
106
70-130
Ethylbenzene
ug/L
50
48.3
97
70-130
lodomethane
ug/L
100
79.3
79
40-130
Isobutanol
ug/L
1000
1200
120
44-144
Methylene Chloride
ug/L
50
51.8
104
67-132
Styrene
ug/L
50
51.6
103
70-130
Tetrachloroethene
ug/L
50
48.9
98
69-130
Tetrahydrofuran
ug/L
500
609
122
62-130
Toluene
ug/L
50
48.9
98
70-130
trans-1,2-Dichloroethene
ug/L
50
49.0
98
70-130
trans- 1,3-Dichloropropene
ug/L
50
56.2
112
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
60.5
121
35-189
Trichloroethene
ug/L
50
53.6
107
70-130
Trichlorofluoromethane
ug/L
50
46.2
92
63-130
Vinyl acetate
ug/L
100
117
117
55-143
Vinyl chloride
ug/L
50
43.0
86
70-131
Xylene (Total)
ug/L
150
151
101
70-130
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
2454145
92409765013
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.7
103
73-134
1,1,1-Trichloroethane
ug/L
ND
20
21.3
106
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.9
99
70-136
1,1,2-Trichloroethane
ug/L
ND
20
22.6
113
70-135
1,1-Dichloroethane
ug/L
ND
20
21.5
107
70-139
1,1-Dichloroethene
ug/L
ND
20
23.3
117
70-154
1,2,3-Trichloropropane
ug/L
ND
20
19.2
96
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
18.7
94
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.2
96
70-137
1,2-Dichlorobenzene
ug/L
ND
20
19.0
95
70-133
1,2-Dichloroethane
ug/L
ND
20
21.0
105
70-137
1,2-Dichloropropene
ug/L
ND
20
21.0
105
70-140
1,4-Dichlorobenzene
ug/L
ND
20
18.5
93
70-133
2-Butanone (MEK)
ug/L
ND
40
41.8
105
60-139
2-Hexanone
ug/L
ND
40
45.7
114
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
45.7
114
65-135
Acetone
ug/L
ND
40
49.9
125
60-148
Acrylonitrile
ug/L
ND
100
108
108
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
MATRIX SPIKE SAMPLE:
Parameter
2454145
Units
92409765013
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
21.4
107
70-151
Bromochloromethane
ug/L
ND
20
23.0
115
70-141
Bromodichloromethane
ug/L
ND
20
21.0
105
70-138
Bromoform
ug/L
ND
20
17.1
86
63-130
Bromomethane
ug/L
ND
20
11.5
58
15-152
Carbon disulfide
ug/L
ND
20
18.7
94
69-149
Carbon tetrachloride
ug/L
ND
20
21.2
106
70-143
Chlorobenzene
ug/L
ND
20
19.9
99
70-138
Chloroethane
ug/L
ND
20
22.7
114
52-163
Chloroform
ug/L
ND
20
20.1
101
70-139
Chloromethane
ug/L
ND
20
18.6
93
41-139
cis-1,2-Dichloroethene
ug/L
2.8
20
23.7
105
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
16.4
82
70-137
Dibromochloromethane
ug/L
ND
20
19.9
99
70-134
Dibromomethane
ug/L
ND
20
21.6
108
70-138
Ethylbenzene
ug/L
ND
20
19.0
95
66-153
lodomethane
ug/L
ND
40
28.0
70
20-138
Isobutanol
ug/L
ND
400
390
98
41-152
Methylene Chloride
ug/L
ND
20
21.1
106
42-159
Styrene
ug/L
ND
20
19.4
97
70-135
Tetrachloroethene
ug/L
ND
20
18.5
93
59-143
Tetrahydrofuran
ug/L
ND
200
223
112
70-133
Toluene
ug/L
ND
20
19.4
97
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
20.6
103
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
18.6
93
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
16.1
81
47-135
Trichloroethene
ug/L
ND
20
20.4
102
70-147
Trichlorofluoromethane
ug/L
ND
20
21.0
105
70-148
Vinyl acetate
ug/L
ND
40
13.0
32
49-151 M1
Vinyl chloride
ug/L
ND
20
18.6
93
70-156
Xylene (Total)
ug/L
ND
60
58.7
98
63-158
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
98
70-130
SAMPLE DUPLICATE: 2454144
92409765012
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
SAMPLE DUPLICATE: 2454144
Parameter
Units
92409765012
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
Isobutanol
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Tetrahydrofuran
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
98
103
4-Bromofluorobenzene (S)
%
92
94
Toluene-d8 (S)
%
109
105
Max
RPD RPD Qualifiers
6
2
4
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447986 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92410048005
METHOD BLANK: 2454151
Associated Lab Samples: 92410048005
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.33
12/19/18 15:11
1,1,1-Trichloroethane
ug/L
ND
1.0
0.48
12/19/18 15:11
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.40
12/19/18 15:11
1,1,2-Trichloroethane
ug/L
ND
1.0
0.29
12/19/18 15:11
1,1-Dichloroethane
ug/L
ND
1.0
0.32
12/19/18 15:11
1,1-Dichloroethene
ug/L
ND
1.0
0.56
12/19/18 15:11
1,2,3-Trichloropropane
ug/L
ND
1.0
0.41
12/19/18 15:11
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
2.0
12/19/18 15:11
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.27
12/19/18 15:11
1,2-Dichlorobenzene
ug/L
ND
1.0
0.30
12/19/18 15:11
1,2-Dichloroethane
ug/L
ND
1.0
0.24
12/19/18 15:11
1,2-Dichloropropane
ug/L
ND
1.0
0.27
12/19/18 15:11
1,4-Dichlorobenzene
ug/L
ND
1.0
0.33
12/19/18 15:11
2-Butanone (MEK)
ug/L
ND
5.0
0.96
12/19/18 15:11
2-Hexanone
ug/L
ND
5.0
0.46
12/19/18 15:11
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
0.33
12/19/18 15:11
Acetone
ug/L
ND
25.0
10.0
12/19/18 15:11
Acrylonitrile
ug/L
ND
10.0
1.9
12/19/18 15:11
Benzene
ug/L
ND
1.0
0.25
12/19/18 15:11
Bromochloromethane
ug/L
ND
1.0
0.17
12/19/18 15:11
Bromodichloromethane
ug/L
ND
1.0
0.18
12/19/18 15:11
Bromoform
ug/L
ND
1.0
0.26
12/19/18 15:11
Bromomethane
ug/L
ND
2.0
0.29
12/19/18 15:11
Carbon disulfide
ug/L
ND
2.0
1.2
12/19/18 15:11
Carbon tetrachloride
ug/L
ND
1.0
0.25
12/19/18 15:11
Chlorobenzene
ug/L
ND
1.0
0.23
12/19/18 15:11
Chloroethane
ug/L
ND
1.0
0.54
12/19/18 15:11
Chloroform
ug/L
ND
1.0
0.14
12/19/18 15:11
Chloromethane
ug/L
ND
1.0
0.11
12/19/18 15:11
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.19
12/19/18 15:11
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.13
12/19/18 15:11
Dibromochloromethane
ug/L
ND
1.0
0.21
12/19/18 15:11
Dibromomethane
ug/L
ND
1.0
0.21
12/19/18 15:11
Ethylbenzene
ug/L
ND
1.0
0.30
12/19/18 15:11
lodomethane
ug/L
ND
5.0
0.32
12/19/18 15:11
Isobutanol
ug/L
ND
100
35.0
12/19/18 15:11
Methylene Chloride
ug/L
ND
1.0
0.97
12/19/18 15:11
Styrene
ug/L
ND
1.0
0.26
12/19/18 15:11
Tetrachloroethene
ug/L
ND
1.0
0.46
12/19/18 15:11
Tetrahydrofuran
ug/L
ND
10.0
3.1
12/19/18 15:11
Toluene
ug/L
ND
1.0
0.26
12/19/18 15:11
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
METHOD BLANK: 2454151
Associated Lab Samples: 92410048005
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.49
12/19/18 15:11
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.26
12/19/18 15:11
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
1.0
12/19/18 15:11
Trichloroethene
ug/L
ND
1.0
0.47
12/19/18 15:11
Trichlorofluoromethane
ug/L
ND
1.0
0.20
12/19/18 15:11
Vinyl acetate
ug/L
ND
2.0
0.35
12/19/18 15:11
Vinyl chloride
ug/L
ND
1.0
0.62
12/19/18 15:11
Xylene (Total)
ug/L
ND
1.0
0.66
12/19/18 15:11
1,2-Dichloroethane-d4 (S)
%
97
70-130
12/19/18 15:11
4-Bromofluorobenzene (S)
%
91
70-130
12/19/18 15:11
Toluene-d8 (S)
%
105
70-130
12/19/18 15:11
LABORATORY CONTROL SAMPLE:
2454152
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
56.6
113
70-130
1,1,1-Trichloroethane
ug/L
50
56.7
113
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
50.5
101
70-130
1,1,2-Trichloroethane
ug/L
50
61.3
123
70-130
1,1-Dichloroethane
ug/L
50
52.5
105
70-130
1,1-Dichloroethene
ug/L
50
59.9
120
70-130
1,2,3-Trichloropropane
ug/L
50
55.4
111
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
48.9
98
70-130
1,2-Dibromoethane (EDB)
ug/L
50
52.7
105
70-130
1,2-Dichlorobenzene
ug/L
50
52.5
105
70-130
1,2-Dichloroethane
ug/L
50
52.2
104
70-130
1,2-Dichloropropane
ug/L
50
56.0
112
70-130
1,4-Dichlorobenzene
ug/L
50
51.2
102
70-130
2-Butanone (MEK)
ug/L
100
118
118
64-135
2-Hexanone
ug/L
100
121
121
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
129
129
70-130
Acetone
ug/L
100
118
118
61-157
Acrylonitrile
ug/L
250
288
115
61-143
Benzene
ug/L
50
56.5
113
70-130
Bromochloromethane
ug/L
50
54.1
108
70-130
Bromodichloromethane
ug/L
50
55.5
111
70-130
Bromoform
ug/L
50
49.7
99
70-130
Bromomethane
ug/L
50
37.2
74
38-130
Carbon disulfide
ug/L
50
51.0
102
68-130
Carbon tetrachloride
ug/L
50
57.0
114
70-130
Chlorobenzene
ug/L
50
51.2
102
70-130
Chloroethane
ug/L
50
36.2
72
37-142
Chloroform
ug/L
50
50.2
100
70-130
Chloromethane
ug/L
50
47.3
95
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
LABORATORY CONTROL SAMPLE:
2454152
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
53.1
106
70-130
cis-1,3-Dichloropropene
ug/L
50
58.2
116
70-130
Dibromochloromethane
ug/L
50
56.5
113
70-130
Dibromomethane
ug/L
50
53.8
108
70-130
Ethylbenzene
ug/L
50
51.9
104
70-130
lodomethane
ug/L
100
89.2
89
40-130
Isobutanol
ug/L
1000
1270
127
44-144
Methylene Chloride
ug/L
50
54.4
109
67-132
Styrene
ug/L
50
55.2
110
70-130
Tetrachloroethene
ug/L
50
52.6
105
69-130
Tetrahydrofuran
ug/L
500
634
127
62-130
Toluene
ug/L
50
51.9
104
70-130
trans-1,2-Dichloroethene
ug/L
50
54.5
109
70-130
trans- 1,3-Dichloropropene
ug/L
50
60.3
121
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
54.5
109
35-189
Trichloroethene
ug/L
50
56.4
113
70-130
Trichlorofluoromethane
ug/L
50
51.7
103
63-130
Vinyl acetate
ug/L
100
123
123
55-143
Vinyl chloride
ug/L
50
46.7
93
70-131
Xylene (Total)
ug/L
150
165
110
70-130
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
94
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
2456543
92410090009
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
19.9
99
73-134
1,1,1-Trichloroethane
ug/L
ND
20
20.9
105
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.5
97
70-136
1,1,2-Trichloroethane
ug/L
ND
20
20.1
100
70-135
1,1-Dichloroethane
ug/L
ND
20
21.2
106
70-139
1,1-Dichloroethene
ug/L
ND
20
23.1
116
70-154
1,2,3-Trichloropropane
ug/L
ND
20
18.3
91
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
18.3
92
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
18.3
91
70-137
1,2-Dichlorobenzene
ug/L
ND
20
20.0
100
70-133
1,2-Dichloroethane
ug/L
ND
20
19.0
95
70-137
1,2-Dichloropropene
ug/L
ND
20
20.5
103
70-140
1,4-Dichlorobenzene
ug/L
5.2
20
24.5
96
70-133
2-Butanone (MEK)
ug/L
ND
40
39.4
98
60-139
2-Hexanone
ug/L
ND
40
40.7
102
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40.5
101
65-135
Acetone
ug/L
ND
40
46.3
116
60-148
Acrylonitrile
ug/L
ND
100
97.0
97
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 72

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
MATRIX SPIKE SAMPLE:
Parameter
2456543
Units
92410090009
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Benzene
ug/L
2.8
20
23.2
102
70-151
Bromochloromethane
ug/L
ND
20
22.7
113
70-141
Bromodichloromethane
ug/L
ND
20
19.9
100
70-138
Bromoform
ug/L
ND
20
17.0
85
63-130
Bromomethane
ug/L
ND
20
10.6
53
15-152
Carbon disulfide
ug/L
ND
20
19.1
96
69-149
Carbon tetrachloride
ug/L
ND
20
21.4
107
70-143
Chlorobenzene
ug/L
22.2
20
40.5
91
70-138
Chloroethane
ug/L
ND
20
22.7
114
52-163
Chloroform
ug/L
ND
20
19.4
97
70-139
Chloromethane
ug/L
ND
20
17.5
88
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
21.3
106
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
16.3
81
70-137
Dibromochloromethane
ug/L
ND
20
18.8
94
70-134
Dibromomethane
ug/L
ND
20
21.0
105
70-138
Ethylbenzene
ug/L
ND
20
19.3
97
66-153
lodomethane
ug/L
ND
40
36.1
90
20-138
Isobutanol
ug/L
ND
400
345
86
41-152
Methylene Chloride
ug/L
ND
20
18.3
91
42-159
Styrene
ug/L
ND
20
18.8
94
70-135
Tetrachloroethene
ug/L
ND
20
18.8
94
59-143
Tetrahydrofuran
ug/L
ND
200
201
101
70-133
Toluene
ug/L
ND
20
19.8
99
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
20.9
104
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
17.1
85
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
15.6
78
47-135
Trichloroethene
ug/L
ND
20
20.3
101
70-147
Trichlorofluoromethane
ug/L
ND
20
20.7
103
70-148
Vinyl acetate
ug/L
ND
40
15.3
38
49-151 M1
Vinyl chloride
ug/L
3.4
20
21.5
91
70-156
Xylene (Total)
ug/L
ND
60
58.5
98
63-158
1,2-Dichloroethane-d4 (S)
%
92
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2456542
92410048005
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
5.2
5.3 0
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
SAMPLE DUPLICATE: 2456542
Parameter
Units
92410048005
Result
Dup
Result
RPD
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
16.9
17.0
0
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
5.6
5.8
3
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
0.83J
0.77J
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
6.9
6.9
0
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
0.86J
0.98J
lodomethane
ug/L
ND
ND
Isobutanol
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Tetrahydrofuran
ug/L
447
443
1
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
4.3
4.3
2
Xylene (Total)
ug/L
14.7
13.8
6
1,2-Dichloroethane-d4 (S)
%
103
101
3
4-Bromofluorobenzene (S)
%
100
97
3
Toluene-d8(S)
%
104
106
1
Max
RPD Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 46 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447655 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92410048001, 92410048002, 92410048003, 92410048004, 92410048006
METHOD BLANK: 2452726
Matrix:
Water
Associated Lab Samples:
92410048001, 92410048002, 92410048003, 92410048004, 92410048006
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0 1.9
12/14/18 14:58
1,2-Dichloroethane-d4 (S)
%
90
50-150
12/14/18 14:58
Toluene-d8 (S)
%
81
50-150
12/14/18 14:58
LABORATORY CONTROL SAMPLE: 2452727
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.5 98 71-125
1,2-Dichloroethane-d4 (S) % 92 50-150
Toluene-d8 (S) % 84 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2452728
2452729
MS
MSD
92410019001 Spike
Spike MS
MSD MS
MSD
% Rec
Max
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 14.7
18.8 72
92
50-150
24 30
1,2-Dichloroethane-d4 (S)
%
91
89
50-150
30
Toluene-d8 (S)
%
77
76
50-150
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 47 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447659 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92410048005
METHOD BLANK: 2452743
Associated Lab Samples: 92410048005
Parameter
Units
1,4-Dioxane (p-Dioxane)
ug/L
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
Matrix: Water
Blank Reporting
Result Limit
ND 2.0
91 50-150
82 50-150
MDL Analyzed
1.9 12/14/18 14:38
12/14/18 14:38
12/14/18 14:38
Qualifiers
LABORATORY CONTROL SAMPLE: 2452744
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 16.9 85 71-125
1,2-Dichloroethane-d4 (S) % 93 50-150
Toluene-d8(S) % 86 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2452745
2452746
MS
MSD
92409256015 Spike
Spike MS
MSD MS
MSD
% Rec
Max
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 52.6 20
20 63.0
59.6 52
35
50-150
6 30 M1
1,2-Dichloroethane-d4 (S)
%
102
105
50-150
30
Toluene-d8(S)
%
104
106
50-150
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 48 of 72

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447977
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92410048001, 92410048002,
92410048004, 92410048006
METHOD BLANK: 2454102
Matrix: Water
Associated Lab Samples: 92410048001, 92410048002,
92410048004, 92410048006
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 12/17/18 14:07
LABORATORY CONTROL SAMPLE: 2454103
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 48700 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2454104 2454105
MS MSD
92410744002
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 103 mg/L
50000 50000 154000 154000 102 101
80-120 0 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2454106 2454107
MS MSD
92410751002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 69.4 mg/L 50000 50000 120000 118000 100 98 80-120 1 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 448260
Analysis Method: SM 2320B-2011
QC Batch Method: SM 2320B-2011
Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92410048003, 92410048005
METHOD BLANK: 2455377
Matrix: Water
Associated Lab Samples: 92410048003, 92410048005
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Alkalinity, Total as CaCO3 ug/L
ND 5000 1000 12/18/18 20:52
LABORATORY CONTROL SAMPLE: 2455378
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Alkalinity, Total as CaCO3 ug/L
50000 51700 103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2455379 2455380
MS MSD
92410660003
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 52.3 mg/L
50000 50000 104000 106000 104 107
80-120 1 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2455381 2455382
MS MSD
92409256015 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Alkalinity, Total as CaCO3 ug/L 278000 50000 50000 333000 347000 109 136 80-120 4 25 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 50 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 446787
Analysis Method: SM 2540C-2011
QC Batch Method: SM 2540C-2011
Analysis Description:
2540C Total Dissolved Solids
Associated Lab Samples: 92410048001, 92410048002, 92410048004
METHOD BLANK: 2448689
Matrix:
Water
Associated Lab Samples: 92410048001, 92410048002, 92410048004
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND
25000 25000
12/11/18 17:29
LABORATORY CONTROL SAMPLE:
2448690
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
252000
268000 106
90-110
SAMPLE DUPLICATE: 2448691
92409879001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
251 mg/L
248000 1
5
SAMPLE DUPLICATE: 2448692
92409804002
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
159000
153000 4
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 446816
Analysis Method: SM 2540C-2011
QC Batch Method: SM 2540C-2011
Analysis Description:
2540C Total Dissolved Solids
Associated Lab Samples: 92410048006
METHOD BLANK: 2448953
Matrix:
Water
Associated Lab Samples: 92410048006
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND
25000 25000
12/11/18 21:02
LABORATORY CONTROL SAMPLE: 2448954
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
250000
244000 97
90-110
SAMPLE DUPLICATE: 2448955
92410048006
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
37000
37000 0
5
SAMPLE DUPLICATE: 2448956
92409978010
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
143 mg/L
146000 2
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 446818
Analysis Method: SM 2540C-2011
QC Batch Method: SM 2540C-2011
Analysis Description:
2540C Total Dissolved Solids
Associated Lab Samples: 92410048003, 92410048005
METHOD BLANK: 2448961
Matrix:
Water
Associated Lab Samples: 92410048003, 92410048005
Blank
Reporting
Parameter
Units
Result
Limit MDL
Analyzed Qualifiers
Total Dissolved Solids
ug/L
ND
25000 25000
12/11/18 21:12
LABORATORY CONTROL SAMPLE:
2448962
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits Qualifiers
Total Dissolved Solids
ug/L
250000
266000 106
90-110
SAMPLE DUPLICATE: 2448963
92409923001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
263 mg/L
265000 1
5
SAMPLE DUPLICATE: 2448964
92410019002
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Total Dissolved Solids
ug/L
32000
29000 10
5 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 448652
Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92410048001, 92410048002,
92410048003, 92410048004, 92410048005, 92410048006
METHOD BLANK: 2457472
Matrix: Water
Associated Lab Samples: 92410048001, 92410048002,
92410048003, 92410048004, 92410048005, 92410048006
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Sulfate ug/L
ND 1000 500 12/20/18 03:20
LABORATORY CONTROL SAMPLE: 2457473
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Sulfate ug/L
50000 52900 106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2457474 2457475
MS MSD
92410048001
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Sulfate ug/L ND
50000 50000 53900 53600 107 107
90-110 1 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2457480 2457481
MS MSD
92410824002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfate ug/L 3.5 mg/L 50000 50000 59300 59900 112 113 90-110 1 10 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
QC Batch: 447930
Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011
Analysis Description: 4500 Chloride
Associated Lab Samples: 92410048001, 92410048002,
92410048003, 92410048004, 92410048005, 92410048006
METHOD BLANK: 2453960
Matrix: Water
Associated Lab Samples: 92410048001, 92410048002,
92410048003, 92410048004, 92410048005, 92410048006
Blank Reporting
Parameter Units
Result Limit MDL Analyzed
Qualifiers
Chloride ug/L
ND 1000 500 12/17/18 09:58
LABORATORY CONTROL SAMPLE: 2453961
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Chloride ug/L
20000 19500 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2453962 2453963
MS MSD
92410164001
Spike Spike MS MSD MS MSD
% Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec
Limits RPD RPD Qual
Chloride ug/L 22.2 mg/L
10000 10000 32400 32400 103 102
90-110 0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2453964 2453965
MS MSD
92410030001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chloride ug/L 9.0 mg/L 10000 10000 18900 19000 99 100 90-110 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Page 55 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Lab ID
92410048005
92410048006
92410048001
92410048002
92410048003
92410048004
92410048005
92410048006
92410048001
92410048002
92410048003
92410048004
92410048005
92410048006
92410048001
92410048002
92410048003
92410048004
92410048005
92410048006
92410048001
92410048002
92410048003
92410048004
92410048005
92410048006
92410048001
92410048002
92410048003
92410048004
92410048005
92410048006
92410048001
92410048002
92410048003
92410048004
92410048005
92410048006
92410048001
Sample ID
1203-MW-38
1203-MW-35
1203-MW-20
1203-MW-23S
1203-MW-24S
1203-MW-30
1203-MW-38
1203-MW-35
1203-MW-20
1203-MW-23S
1203-MW-24S
1203-MW-30
1203-MW-38
1203-MW-35
1203-MW-20
1203-MW-23S
1203-MW-24S
1203-MW-30
1203-MW-38
1203-MW-35
1203-MW-20
1203-MW-23S
1203-MW-24S
1203-MW-30
1203-MW-38
1203-MW-35
1203-MW-20
1203-MW-23S
1203-MW-24S
1203-MW-30
1203-MW-38
1203-MW-35
1203-MW-20
1203-MW-23S
1203-MW-24S
1203-MW-30
1203-MW-38
1203-MW-35
1203-MW-20
Date: 12/27/2018 04:11 PM
QC Batch Method
RSK 175 Modified
RSK 175 Modified
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 7470A
EPA 7470A
EPA 7470A
EPA 7470A
EPA 7470A
EPA 7470A
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B
EPA 8260B Mod.
EPA 8260B Mod.
EPA 8260B Mod.
EPA 8260B Mod.
EPA 8260B Mod.
EPA 8260B Mod.
SM 2320B-2011
SM 2320B-2011
SM 2320B-2011
SM 2320B-2011
SM 2320B-2011
SM 2320B-2011
SM 2540C-2011
QC Batch Analytical Method
446939
447111
446531
446531
446531
446531
446531
446531
447050
447050
447050
446925
446925
446925
446706
446706
446706
446706
446706
446706
447864
447864
447984
447864
447986
447864
447655
447655
447655
447655
447659
447655
447977
447977
448260
447977
448260
447977
446787
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA6010D
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 6020B
EPA 7470A
EPA 7470A
EPA 7470A
EPA 7470A
EPA 7470A
EPA 7470A
Analytical
Batch
446542
446542
446542
446542
446542
446542
447100
447100
447100
447089
447089
447089
446845
446845
446845
446845
446845
446845
Page 57 of 72

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Burke Co. Johns R C&D Exp.
Pace Project No.: 92410048
Lab ID
Sample ID
QC Batch Method
QC Batch
92410048002
1203-MW-23S
SM 2540C-2011
446787
92410048003
1203-MW-24S
SM 2540C-2011
446818
92410048004
1203-MW-30
SM 2540C-2011
446787
92410048005
1203-MW-38
SM 2540C-2011
446818
92410048006
1203-MW-35
SM 2540C-2011
446816
92410048001
1203-MW-20
EPA 300.0 Rev 2.1 1993
448652
92410048002
1203-MW-23S
EPA 300.0 Rev 2.1 1993
448652
92410048003
1203-MW-24S
EPA 300.0 Rev 2.1 1993
448652
92410048004
1203-MW-30
EPA 300.0 Rev 2.1 1993
448652
92410048005
1203-MW-38
EPA 300.0 Rev 2.1 1993
448652
92410048006
1203-MW-35
EPA 300.0 Rev 2.1 1993
448652
92410048001
1203-MW-20
SM 4500-CI-E-2011
447930
92410048002
1203-MW-23S
SM 4500-CI-E-2011
447930
92410048003
1203-MW-24S
SM 4500-CI-E-2011
447930
92410048004
1203-MW-30
SM 4500-CI-E-2011
447930
92410048005
1203-MW-38
SM 4500-CI-E-2011
447930
92410048006
1203-MW-35
SM 4500-CI-E-2011
447930
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/27/2018 04:11 PM without the written consent of Pace Analytical Services, LLC.
Analytical
Analytical Method Batch
Page 58 of 72

VG2Altc1lyf 01
Document Name:
Sample Condition Upon Receipt(SCUR)
Document No.:
F-CAR-CS•033-Rev.06
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ HuntersvillVel Raleigh[] Mechanicsville[]
Sample Condition Client Name: Upon � Project #: WO# : 92410048
- 1 _ ��- �I � J
❑ Commercial ❑Pa e� ❑UPS ❑QUtheSr ❑Client
92410048
Custody Seal Present? [—]Yes QMo Seals Intact? ❑Yes L[,No
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bubble Sags ❑None ❑ Other Biological Tissue Frozen?.
Thermometer )�''/� ❑Yes ❑No ❑N/A
IR Gun lo: 92TO46 Type of Ice: �Lret []Blue ❑None
Cooler Temp i°Cj: 4 14 Correction Factor: Add/Subtract ('Q 0.0
Temp should be above freezing to 6°C
Cooler Temp Corrected (°C): ❑samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil ([TN/A, water sample]
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
MYas FlNn inrludine Hawaii and Puerto Rico)? ❑Yes ONO
Comments/Dis crepe ncy:
Chain of Custody Present?
Yes
[—]No
El N/A
1.
Samples Arrived within Hold Time?
LCJYes
ON.
❑NIA
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
Qa
El N/A
3.
Rush Turn Around Time Requested?
[:]Yes
�No
❑N/A
4.
Sufficient Volume?
Oyes
❑Na
El N/A
S.
Correct Containers Used?
es
❑No
❑N/A
6.
-Pace Containers Used?
Y/es
❑No
❑N/A
Containers Intact?
Yes
❑No
[]N/A.
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
❑No
ON/A
8.
Sample Labels MatchCOC?
[34s
❑No
El NIA
9.
i/ll 1
-Includes Date/Tirne/ID/Analysis Matrix:
Headspace in VGA Vials(>5-6mmj?
❑Yes
\AfNo
❑N/A
10.
Trip Blank Present?
[]Yes
[]No
_❑N/A
11.
Trip Blank Custody Seals Present?
❑Yes
❑No
N/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Field Data Required? []Yes []No
Lot ID of split containers:
Date:
Date:
Page 59 of 72

Document Name:
Condition Upon Recel
Document No.:
F•CAR-CS•033-Rev.06
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority;
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VO& to[iform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
WO#:92410048
PM: NMG Due Date: 12/21/18
CLIENT: 92-Joyce Eng
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pH Adjustment Log for preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot p
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification office (i.e.
Out of hold, incorrect preservative, out of temp, in correctcontainers.
Page 60 of 72

/G
aceArlalylica!
section A
Required Client Information:
Company Joyce Engineering-VF
Address, 2211 West Meadowvi
Greensboro, INC 27407
Email To- vburbach 'o ce_ engir
Phone, [phone] Eax
Requested Due DatelfAT: 10 Dav ll
SAMPLE ID
One Character per box.
to-2, D-9 I , -)
N
O
CHAIN -OF -CUSTODY 1 Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C.
Required Project Information: Invoice Information: Page : 1 Of 1
ReponTo. Van Burbach Attention: Lecia Jones
Copy To:LLaniLdTieF r Company Name. Joyce Engineering
Address 1604 Ownby Lane. Richmond, VA 23220 Regulatory Agency
Purchase Order No. 2181871 pace Quote Reference -
Client Project 10: Burke Co. Johns River C&D Exp. Pace Project Manager. Nicole Gasiorowski State! Location
Container Order Number: Pace Profile;V North Carolina
Requested Analysis Filtered
MATRIX
CODE
—
0
COLLECTED
Preservatives
Y
D—king Wate,
OW
Water
WT
V
V
r-
y
Wasla Wale,
VW
Q
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Zw Sample Ids must be unique any, pT v z Z y 7 Y v
Tissue 73 X J w O N D o — — m 6 ..a
a o_ o t Q a= a a r
h DATE TIME DATE TIME ,�.� Wi z=if
= i z ji O z m z v
1 1203-MW-20 >M
G
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2 1203-MW-23S WT
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3 1203-MW-24S WT
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4 1203-MW-30 WT
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ADDITIONAL COTMENTS RELINQUISHED
13Y I
AFFILIATION
—
I,
.
i " J
i
4,.-�
n
DATE TIME
/d Y /v '�v
2
i
L
U
a
RZLA1 Dull
>r
DD
I AFFILIATION I DATE I TIME I SAMPLE CONDITIONS
K
SAMPLER NAME AND SIGNATURE
u
PRINT Name of SAMPLER-
� Z
SIGNATURE of
,4AMPLER- „ ,pAT igned: .�i 2 m } o E z
r D' m U U`-

Cooler Receipt Form
Client Name: Project: 6U__ - 6 C_&Lab Work Order:
A. Shipping/Container Information (circle appropriate response "
Courier: FedE " UPS USPS Client Other: Air bill Present:GYsNo
Tracking Number:
Custody Seal on Cooler/Box Present: Yes No Seals Intact: Yes No
Cooler/Box Packing Material: �eW Absorbent Foam Other:
Type of ice: Wet Blue None Ice Intact: oYe-sMelted
Cooler Temperature: J Radiation Screened: Yes L
1 Chain of Custody Presen Yes No
Comme
B. Laboratory Assign ment/Lbg-in (check appropriate response)
YES
NO
N/A
Comment
Reference non -Conformance
Chain of Custody properly filled out
Chain of Custody relinquished
Sampler Name & Signature on COC
")Containers intact
Were samples in separate bags
Sample container labels match COC
Sample name/date and time collected
Sufficient volume provided
PAES containers used
Are containers properly preserved for the requested testing?
(as labeled)
If an unknown preservation state, were containers checked?
Exception: VOA's coliform
If yes, see pH form.
Was volume for dissolved testing field filtered, as noted on
the COC? Was volume received in a preserved container?
EHe7adspa]c'e present?
Comments:
F-PAE-Q-009-rev.01, 30ct2017
Cooler contents examined/received by : 4 z J Date:
Project Manager Review !` Date:I L' s _.
Page 72 of 72