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9203_Wake_Feltonsville_MSWLF_GW_FID1323015_20190620
Closed Feltonsville Landfill Facility Permit No. 9203- MSWLF-1980 Semi -Annual Sampling Report (April 2019 Sampling Event) Wake County Report Prepared June 2019 WAKE COUNTY NORTH CAROLINA Electronic Data -Email CD NC DENR t Division of Waste Management -Solid Waste Doc/Event if: Environmental Monitoring �rtinq Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: • Prepare one form for each individually monitored unit. • Please type or print legibly. • Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. • Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). • Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): Consultant - CDM Smith Inc. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Mathew F. Colone Phone: (919) 325-3500 E-mail: colonemf cdmsmith.com Facility name: Wake County -Closed Feltonsville Landfill Facility Address: 6000 Old Smithfield Road Apex, North Carolina 27539 Permit # 9203-MSWLF- 1980 NC Landfill Rule: (.0500 or .1600) .0500 and .1600 Actual sampling dates (e.g., October 20-24, 2006) April 29-30 and May 1-2, 2019 Environmental Status: (Check all that apply) InitiallBackground Monitoring �X Detection Monitoring � Assessment Monitoring ❑X Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Groundwater monitoring data from private water supply wells Leachate monitoring data ❑ Surface water monitoring data - EVO injection performed March 2013 Methane gas monitoring data -performance monitoring Corrective action data (specify) - MNA data Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Mathew F Colone Consultant (919) 325-3500 Title (Area Code) Telephone Number. ;_.�'� �' °'' ' `` • r• Facility Reprgsentatiye Narpp (Print) � 1 _�, • - , > : A ; �' ��r.._ Affix NC Signature 5400 Glenwood Avenue Suite 400 Raleigh North Carolina 27612 Facility Representative Address F-0412 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 Seal smith 5400 Glenwood Ave, Suite 400 Raleigh, North Carolina 27612 tel: 919 325-3500 fax: 919 781-5730 June 20, 2019 Ms. Jaclynne Drummond North Carolina Department of Environmental Quality Division of Waste Management Solid Waste Section 2090 U.S. 70 Highway Swannanoa, North Carolina 28778 Subject: April 2019 Semi -Annual Groundwater Sampling Report Closed Feltonsville Landfill - Wake County Facility Permit No. 9203-MSWLF-1980 Dear Ms. Drummond: CDM Smith Inc., on behalf of Wake County, is submitting an electronic copy of the April 2019 semi- annual sampling event report. This letter report presents the results of the semi-annual sampling event that was recently completed at the Closed Feltonsville Landfill and constitutes the first semi-annual sampling event for 2019. The current groundwater monitoring network consists of the following wells: MW-2, -4, -6, -8, -9, -10, -11, -12, -13, -14, -15, -16, -17, -18, -19, -20, -21, -22, -23, -24, -25, -26, -27, -28, and -29 as well as surface water sampling locations SW-1, -2, and -3. Monitoring wells MW-2, -6, -8, -9, -10, -11, -12, -13, -14, -15, -16, -17, -18, -19, -20, -28, and -29 monitor the closed Feltonsville Landfill. The remaining wells (i.e. MW-4, -21, -22, -23, -24, -25, -26, and -27) monitor the old cells located in the back of the property. Field activities, sampling results for all wells and surface water locations, an evaluation of the groundwater corrective action effectiveness, and recommendations are discussed below. Field Activities Groundwater and surface water samples from the Closed Feltonsville Landfill were collected on April 29- 30 and May 1-2, 2019. Monitoring well and surface water sample locations are shown on Figure 1. Construction details for each monitoring well are summarized in Table 1. Samples were collected from the monitoring wells by use of a peristaltic pump or disposable, laboratory decontaminated bailers. Groundwater elevations were measured at each well on April 29, 2019, using an electronic water level indicator with an accuracy of 0.01 feet and are presented in Table 1. These groundwater elevations were used to construct potentiometric contours for this sampling event and are shown on Figure 1. The groundwater elevations and potentiometric contours were also used to estimate groundwater velocities at each well as presented in Table 2. 0 WATER + ENVIRONMENT +TRANSPORTATION + ENERGY + FACILITIES smith Ms. Jaclynne Drummond June 20, 2019 Page 2 After depth to groundwater was determined, three well volumes of water were removed from each well prior to sampling to provide fresh formation water within the well water column. Each well volume and surface water sample was measured in the field for pH, conductivity, temperature, turbidity, dissolved oxygen, and oxidation-reduction potential using a YSI-556 multi -parameter water quality meter and a HANNA HI 98703 turbidity meter. Wells that had elevated turbidity were allowed to stabilize prior to sample collection. The water quality parameters at the time of sampling are provided in Table 3. Sampling Results Groundwater and surface water samples were analyzed by Shealy Environmental Services, Inc. located in West Columbia, South Carolina, for the North Carolina Appendix I volatile organic compounds (VC)Cs) plus dichlorodifluoromethane and 1,4-dioxane, and Appendix I metals plus mercury. Additional samples were collected from select monitoring wells to evaluate natural attenuation and the effectiveness of the corrective action. Results of the additional sampling and an evaluation of natural attenuation are discussed in the next section of this report. The analytical results were reported to the laboratory specific method detection limit (MDL) and are quantifiable at or below the laboratory limit of quantitation (LOQ). All monitoring wells for the Closed Feltonsville Landfill had detections of analytes above the MDL but below the LOQs and were qualified as estimated or "J" flags. Most detections of zinc had "B" flags, indicating that the analyte was detected in the method blank. MW-26 had a detection of 1,4-dioxane with a "D" flag, indicating that the sample was analyzed at a dilution greater than 1. Additionally, the chloroethane and 1,1-dichloroethane detections in MW-29 had "D" flags. MW-29 was run at a dilution of 5 due to laboratory analyst error. The following list indicates the analytes detected above the LOQ at each sampling location. No "J" flag detections are provided. Underlined groundwater analytes exceeded the 15A NCAC 02L .0202 (NC 2L) Groundwater Quality Standard or Interim Maximum Allowable Concentration (IMAC). Underlined surface water analytes exceeded the 15A NCAC 02B or Protective Value Surface Water Quality Standard for Class C Waters. A complete summary of all detected and estimated concentrations for the March 2011 through the April 2019 sampling events is provided in Table 4. Laboratory data reports are provided in Appendix A. MW-2 (Background) Metals: Barium, Zinc Volatile Organic Compounds: None Detected M W-4 Metals: None Detected Volatile Organic Compounds: Chloroform, Dichlorodifluoromethane, 1,1-Dichloroethane, cis- 1,2-Dichloroethene, Tetrachloroethene 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 3 MW-6 Metals: Volatile Organic Compounds: Barium, Cobalt, Zinc Benzene, Chlorobenzene, Chloroethane, 1,4-Dichlorobenzene, 1,1-Dichloroethane, cis- 1,2-Dichloroethene, 1,4-Dioxane, Tetra hydrofuran, Vinyl Chloride MW-8 Inorganics: Barium, Chromium, Cobalt, Nickel, Sodium, Total Dissolved Solids (TDS) Volatile Organic Compounds: Chloroethane, Dichlorodifluoromethane, 1,1-Dichloroethane, 1,1-Dichloroethene, Tetrachloroethene, Trichloroethene MW-9 Inorganics: Barium, Cobalt, Nickel, Sodium, TDS Volatile Organic Compounds: Benzene, Chlorobenzene, Chloroethane, 1,4-Dichlorobenzene, 1,1-Dichloroethane, cis-1,2-Dichloroethene, 1,4-Dioxane MW-10 Inorganics: Arsenic, Barium, Cobalt, Nickel, Sodium, TDS Volatile Organic Compounds: Benzene, Chlorobenzene, Chloroethane, 1,4-Dichlorobenzene, 1,1-Dichloroethane, cis-1,2-Dichloroethane, 1,4-Dioxane, Methylene Chloride, Tetra hyd rofura n, Vinyl Chloride MW-11 Metals: Barium, Zinc Volatile Organic Compounds: Chloroethane, cis-1,2-Dichloroethene MW-12 Metals: Barium Volatile Organic Compounds: Chloroethane, 1,4-Dioxane MW-13 Metals: Barium, Mercury, Zinc Volatile Organic Compounds: Benzene, Chlorobenzene, Chloroethane, 1,4-Dichlorobenzene, cis- 1,2-Dichloroethene MW-14 Metals: Barium, Mercury Volatile Organic Compounds: Benzene, Chlorobenzene, 1,4-Dichlorobenzene, 1,1-Dichloroethane, cis- 1,2-Dichloroethene, 1,4-Dioxane 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 4 MW-15 Metals: Barium Volatile Organic Compounds: Chlorobenzene, 1,4-Dioxane MW-16 Metals: Arsenic, Barium Volatile Organic Compounds: Benzene, Chloroethane, Dichlorodifluoromethane, 1,1-Dichloroethane, cis- 1,2-Dichloroethene, Tetrachloroethene, Trichloroethene MW-17 Metals: Arsenic, Barium, Copper, Zinc Volatile Organic Compounds: Chloroethane, 1,1-Dichloroethane, cis-1,2-Dichloroethene, 1,4-Dioxane MW-18 Metals: Barium Volatile Organic Compounds: Chloroform MW-19 Inorganics: Barium, Sodium, TDS Volatile Organic Compounds: None Detected MW-20 Metals: Barium Volatile Organic Compounds: None Detected MW-21 Metals: Zinc Volatile Organic Compounds: None Detected M W-22 Metals: Arsenic, Barium Volatile Organic Compounds: None Detected MW-23 Metals: Barium Volatile Organic Compounds: None Detected 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 5 M W-24 Metals: Volatile Organic Compounds: MW-25 Metals: Volatile Organic Compounds: MW-26 Metals: Volatile Organic Compounds: MW-27 Metals: Volatile Organic Compounds: MW-28 Metals: Volatile Organic Compounds: Barium, Zinc Benzene, Chlorobenzene, Chloroethane, 1,4-Dichlorobenzene, 1,1-Dichloroethane, cis- 1,2-Dichloroethene, 1,4-Dioxane Barium Benzene, Chloroethane, 1,1-Dichloroethane, 1,4-Dioxane Barium, Cobalt, Zinc Benzene, Chlorobenzene, Chloroethane, 1,4-Dichlorobenzene, 1,1-Dichloroethane, cis- 1,2-Dichloroethene, 1,4-Dioxane, Tetrahydrofuran Arsenic, Barium, Cobalt, Copper, Zinc Chloroethane, 1,1-Dichloroethane, 1,1-Dichloroethene, 1,4-Dioxane Barium Chloroform MW-29 Inorganics: Barium, Cobalt, Zinc, Sodium, TDS Volatile Organic Compounds: Chloroethane, 1,1-Dichloroethane SW-1 Metals: Volatile Organic Compounds: SW-2 Metals: Volatile Organic Compounds: None Detected None Detected DRY DRY SW-3 Metals: Barium, Zinc Volatile Organic Compounds: None Detected 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 6 Equipment Blank Metals: None Detected Volatile Organic Compounds: None Detected Trip Blank Metals: Not analyzed Volatile Organic Compounds: None Detected "J" flags were not included in the previous list, but several sampling locations had "J" flag detections that exceeded the standards. The "J" flag constituents above the standards along with their location are listed below: Cobalt: MW-2, -11, -12, -13, -14, -15, -16, -17, -19, -21, -22, -23, and -24 Copper: SW-3 Lead: SW-3 Vanadium: MW-2, -4, -8, -9, -11, -14, -17, -18, -19, -20, -21, -23, -24, -27, -28, and -29 1,2-Dichloroethane: MW-10 Equipment and trip blanks were analyzed for quality control. A duplicate sample was also collected for quality control. The equipment blank had estimated detections of acetone, 2-butanone, and chloroethane below their respective NC 2L Standards. Two trip blanks were analyzed for VOCs only. An estimated detection of chloroethane was detected in one of the trip blanks below its NC 2L Standard. The duplicate sample, labeled DUP, was collected from MW-13 and had similar concentrations to the MW-13 parent sample, with the exception of a detection of chloroethane in the parent sample below its NC 2L Standard. Additionally, 1,4-dioxane was detected in the parent and duplicate samples, but the parent sample had an estimated detection below the NC 2L Standard, whereas the duplicate sample detection was above the NC 2L Standard. Table 5 presents a summary of all parameters detected during the April 2019 sampling event that exceeded the NC 2L or IMAC Standards. Pesticides, herbicides, and polychlorinated biphenyls have not been detected above the NC 2L or IMAC Standards in groundwater monitoring wells since the May 2010 sampling event. Samples were last collected for these parameters during the April 2011 sampling event. Historical data is available upon request. As part of an ongoing Alternate Source Demonstration for the landfill, filtered samples were collected from monitoring wells MW-4, -6, -9, -11, -12, -17, -18, -20, -21, -22, -24, -25, -28, and -29 during the April 2019 sampling event due to elevated turbidity (i.e. greater than 10 Nephelometric Turbidity Units). These samples were collected to demonstrate that select metals exceeding the NC 2L or IMAC Standards are naturally occurring and not related to a release from the landfill. Total metals that exceeded the NC 2L or IMAC Standards from these wells were analyzed for dissolved metals to determine if turbidity was 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 7 a contributing factor to total reported metals. Below is a summary of the dissolved metals exceedances. Wells with a "*' qualifier had a "J" flag detection for that analyte. Barium: MW-6, -9, and 25 Cobalt: MW-6, -9, -11, -22, -24*, and -29 Vanadium: MW-17, and -20* Dissolved metal sample results are provided in Table 4 and the laboratory data report is provided in Appendix A. Based on qualitative and quantitative evaluation of current and historic groundwater sampling data, the NC 2L or IMAC Standard metal exceedances from the April 2019 sampling event were determined to be indicative of naturally occurring background concentrations as opposed to a release from the landfill. Monitored Natural Attenuation Sampling Additional groundwater samples were collected from the background well, MW-2, and downgradient monitoring wells MW-8, -9, -10, -12, -13, and -14. The samples were analyzed for alkalinity, biochemical oxygen demand, chemical oxygen demand, carbon dioxide, chloride, dissolved hydrogen, methane, ethane, ethene, volatile fatty acids (i.e. acetic, butyric, lactic, propionic, and pyruvic), nitrate, sulfate, sulfide, and total organic carbon. Ferrous iron was also analyzed using a HACH test field kit due to the short hold time (i.e. 15 minutes). These additional samples were collected to monitor for natural attenuation as part of the approved corrective action program as required by Solid Waste Section (SWS) guidelines. Additional samples were also collected from wells MW-19 and -29, which are located downgradient of the injection area, in order to monitor the effectiveness of the injection. Samples collected from MW-8, -9, -10, -19, and -29 were also analyzed for sodium and TDS. Sampling results are provided in Table 6 and trend figures of total detected VOCs for select wells are presented on Figures 2- 10. Corrective Action via In situ Bioremediation Injection In accordance with the Corrective Action Plan that was approved by the SWS in a letter dated December 1, 2011, two in situ bioremediation injections have been completed. Phase I consisted of injecting sodium lactate into 5 injection wells upgradient of monitoring wells MW-8, -9, and -10 on June 18-21, 2012. A total of 1,268 gallons of a 10 percent sodium lactate solution were injected resulting in each well receiving approximately 254 gallons of the sodium lactate solution. Phase I post -injection samples were collected 1, 2, and 5 months after injection. During each sampling event, samples from MW-8, -9, -10, -19, and -29 were analyzed for the following field measurements: pH, temperature, oxidation-reduction potential, dissolved oxygen, conductivity, turbidity, nitrate, sulfate, ferrous iron, carbon dioxide, and alkalinity along with laboratory analyses of chlorides, chemical oxygen demand, VOCs, dissolved gases (i.e. methane, ethane, and ethene), sodium, and TDS. Volatile fatty acids were also collected during the 1-month post -injection sampling event. Additionally, samples 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 8 were collected from MW-8, -9, and -10 and analyzed for bacterial population size and functional gene presence during the baseline and 5-month post -injection sampling events. Analytical results for each sampling event are summarized in Tables 4 and 6. Analytical results post -sodium lactate injection for MW-8, -9, and -10 indicated that bioremediation was occurring with no VOCs detected above NC 2L standards in MW-8 or -10, with the exception of 1,1- dichloroethane detected in samples collected from MW-10 in July 2012. MW-9 had detections of 1,1- dichloroethane, tetrachloroethene, trichloroethene, and vinyl chloride above NC 2L standards, but contaminant concentrations were decreasing. DNA analyses revealed healthy populations of bacteria (Deholococcoides sp) in MW-9 and -10 that continued to reduce contaminant concentrations. Bacterial populations in MW-8 decreased as a result of little to no VOCs being detected during the post -injection sampling. The Phase I injection of sodium lactate successfully caused degradation of trichloroethene and tetrachloroethene to daughter products using enhanced anaerobic bioremediation in the injection area. Although the Phase I injection reduced contaminant concentrations, a second injection was needed to supply a longer lasting source of electron donors. Biodegradation can be sustained for as long as sufficient concentrations of substrate remain in the groundwater. For this reason, emulsified vegetable oil was utilized in the Phase 2 injection as it is a slow -release compound, and therefore should release organic carbon into the groundwater for three to five years, depending on site conditions. During the Phase 2 injection, a 10 percent emulsified vegetable oil solution was injected into the injection wells on March 25-27, 2013. Injection at each well consisted of approximately 220 gallons of water containing approximately 22 gallons of the emulsified vegetable oil product. The emulsified vegetable oil product consisted of 60 percent emulsified vegetable oil and 4 percent sodium lactate by weight, which resulted in a total injection volume of 1,100 gallons of water and 110 gallons of emulsified vegetable oil product. Post -injection samples were collected 1, 4, 7, 10, and 12 months after injection. The April 2014 monitoring event concluded the post -injection monitoring. Analyses for each sampling event were similar to the Phase I events except that a DNA analyses to determine bacterial population size and functional gene presence was only done during the April 2014 sampling event. No VOCs have been detected above the standards in MW-8 since the November 2011 semi-annual sampling event, with the exception of the April 2019 sampling event. Samples collected from MW-8 during the April 2019 sampling event had detections of 1,1-dichloroethane and tetrachloroethene above their respective NC 2L Standards. Benzene, 1,1-dichloroethane, and 1,4-dioxane were detected above their respective NC 2L Standards in samples collected from MW-9 during the April 2019 sampling event. The concentration of 1,1- dichloroethane in MW-9 shows a decreasing trend. Benzene was detected slightly above the standard (1 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 9 part per billion (ppb)) at 2.3 ppb. Historically, benzene has been detected slightly above the standard since May 2015, with the exception of the November 2015 and April 2016 sampling events and was either reported as an estimated concentration below the standard or was not detection from September 1994 to October 2014. 1,4-Dioxane was detected above the standard (3 ppb) at 8.7 ppb and was added to the sampling program in the fall of 2018. MW-10 samples had concentrations of benzene, 1,1-dichloroethane, 1,2-dichloroethane, 1,4-dioxane, and vinyl chloride above their respective NC 2L Standards. The concentration of 1,1-dichloroethane has fluctuated but shows a decreasing trend since the May 2015 sampling event. Concentrations of benzene have historically fluctuated at MW-10. Benzene was detected above the NC 2L Standard in April 2019 (4.2 ppb). 1,2-Dichloroethane has not been detected above the NC 2L Standard or the MDL since the November 2016 sampling event. Additionally, 1,4-dioxane was detected above the standard at a concentration of 19 ppb. As expected, the concentration of vinyl chloride has fluctuated following the Phase 2 injection. No VOCs were detected in samples collected from bedrock monitoring well MW-19 during the April 2019 sampling event. Historically, VOCs have never been detected above the standards in monitoring well MW-19. MW-29, located at the compliance boundary, has not had any chlorinated ethenes detected above the NC 2L Standards since November 2012. Chloroethane and 1,1-dichloroethane were detected in samples collected from MW-29 during the April 2019 sampling event below their respective NC 2L Standards. Concentrations of 1,1-dichloroethane have decreased following the injection events. 1,1-Dichloroethane has been detected below the NC 2L Standard since the January 2014 post -injection sampling event with the exception of the October 2014 semi-annual sampling event (7.2 ppb) when it was detected slightly above the NC 2L Standard (6 ppb). Dechlorination of chlorinated ethenes from tetrachloroethene to ethene is ongoing. Chlorinated ethene concentrations in MW-9 and -10 remain below the NC 2L Standards. The geochemical data indicates favorable conditions for reductive dechlorination based on samples collected from MW-9 and -10 during the April 2019 monitoring event. Subsequent monitoring events will be evaluated to identify any trends. Recommendations Wake County will continue with the semi-annual assessment monitoring program. All wells will continue to be sampled for Appendix I VOCs plus dichlorodifluoromethane and 1,4-dioxane, and Appendix I metals plus mercury. Samples collected from MW-2, -8, -9, -10, -12, -13, -14, -19, and -29 will also be analyzed for natural attenuation parameters. The next semi-annual sampling event will be completed in the fall of 2019. 0 smith Ms. Jaclynne Drummond June 20, 2019 Page 10 If you have any questions or require further explanation, do not hesitate to call me at 919-325-3500. Very truly yours, Mathew F. Colone, P.G. CDM Smith Inc. cc: John Roberson, WCSWM Elliott Cornell, WCSWM 0 Table 1 Monitoring Well Construction Summary April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 Facility Permit Number 9203-MSWLF-1980 Monitoring Well Code MW-2 Installation . 1994 35.68420 78.84301 of Interval Bedrock Total .- pth (feet BTOC) 60.0 Screened Interval (feet BTOQ 50.0 - 60.0 Seal Interval (feet BTOQ 48.0 - 50.0 Too of DepthGeology Casing Groundwater Elevation Well Elevation (feet BTOC) (feet AMSL) Diameter (feet AMSL) (inches) 366.03 30.00 336.03 2.0 9203-MSWLF-1980 MW-4 1994 35.68161 78.86000 Regolith 36.0 26.0 - 36.0 24.0 - 26.0 310.80 19.88 290.92 2.0 9203-MSWLF-1980 MW-6 1994 35.68380 78.84769 Bedrock 33.5 23.5 - 33.5 21.5 - 23.5 319.71 16.32 303.39 2.0 9203-MSWLF-1980 MW-8 1994 35.68394 78.85367 Regolith 45.7 35.7 - 45.7 33.7 - 35.7 287.72 10.86 276.86 2.0 9203-MSWLF-1980 MW-9 1994 35.68402 78.85362 Bedrock 37.2 27.2 - 37.2 25.2 - 27.2 285.83 9.00 276.83 2.0 9203-MSWLF-1980 MW-10 1994 35.68406 78.85358 Regolith 22.5 12.5 - 22.5 10.5 - 12.5 287.10 10.13 276.97 2.0 9203-MSWLF-1980 MW-11 1994 35.68314 78.85380 Regolith 23.8 13.8 - 23.8 10.8 - 13.8 282.80 5.90 276.90 2.0 9203-MSWLF-1980 MW-12 1994 35.68018 78.84787 Regolith 21.8 11.8 - 21.8 9.8 - 11.8 306.52 6.92 299.60 2.0 9203-MSWLF-1980 MW-13 1994 35.68013 78.84987 Regolith 23.3 13.3 - 23.3 11.3 - 13.3 305.93 12.26 293.67 2.0 9203-MSWLF-1980 MW-14 1994 35.68010 78.84994 Bedrock 39.8 29.8 - 39.8 27.8 - 29.8 305.29 11.61 293.68 2.0 9203-MSWLF-1980 MW-15 1994 1 35.68012 78.84990 Saprolite 41.0 31.0 - 41.0 29.0 - 31.0 305.64 11.97 293.67 2.0 9203-MSWLF-1980 MW-16 1994 35.68070 78.85300 Regolith 45.0 35.0 - 45.0 33.0 - 35.0 315.30 27.41 287.89 2.0 9203-MSWLF-1980 MW-17 1994 35.68141 78.85434 Regolith 28.5 18.5 - 28.5 16.5 - 18.5 291.58 12.91 278.67 2.0 9203-MSWLF-1980 MW-18 1994 35.68389 78.85087 Regolith 26.5 16.5 - 26.5 14.5 - 16.5 300.82 11.73 289.09 2.0 9203-MSWLF-1980 MW-19 6/10/1999 35.68405 78.85366 Bedrock 68.0 58.0 - 68.0 56.0 - 58.0 286.17 9.12 277.05 2.0 9203-MSWLF-1980 MW-20 6/10/1999 35.68456 78.85302 Regolith 28.5 13.5 - 28.5 11.5 - 13.5 285.80 7.93 277.87 2.0 9203-MSWLF-1980 MW-21 6/10/19991 35.68229 78.86262 Regolith 31.0 16.0 - 31.0 14.0 - 16.0 339.25 13.00 326.25 2.0 9203-MSWLF-1980 MW-22 6/10/1999 35.67984 78.86062 Regolith 28.5 13.5 - 28.5 11.5 - 13.5 299.39 12.64 286.75 2.0 9203-MSWLF-1980 MW-23 6/10/1999 35.68029 78.85884 Regolith 27.7 12.7 - 27.7 10.7 - 12.7 286.83 14.60 272.23 2.0 9203-MSWLF-1980 MW-24 6/10/1999 35.68179 78.85827 Regolith 31.0 16.0 - 31.0 14.0 - 16.0 295.04 7.17 287.87 2.0 9203-MSWLF-1980 MW-25 6/10/1999 35.68267 78.85769 Regolith 30.6 15.6 - 30.6 13.6 - 15.6 295.87 10.10 285.77 2.0 9203-MSWLF-1980 MW-26 6/9/1999 35.67795 78.85668 Regolith 20.0 7.0 - 20.0 5.0 - 7.0 282.95 5.55 277.40 2.0 9203-MSWLF-1980 MW-27 1 6/9/1999 1 35.67585 78.85661 Regolith 31.5 16.5 - 31.5 14.5 - 16.5 297.31 15.64 281.67 2.0 9203-MSWLF-1980 MW-28 6/10/1999 1 35.68378 78.84759 Bedrock 71.0 61.0 - 71.0 59.0 - 61.0 319.70 11.90 307.80 2.0 9203-MSWLF-1980 MW-29 2/21/20111 35.68420 78.85379 Regolith 25.3 15.3 - 25.3 13.3 - 15.3 284.76 8.25 276.51 2.0 Notes: 1. Groundwater elevations were measured on April 29, 2019. 2. AMSL - Above Mean Sea Level 3. BTOC - Below Top of Casing 4. Latitude and longitude are in decimal degrees (World Geodetic System 1983). Smith Page 1 of 1 June 2019 Table 2 Summary of Calculated Groundwater Flow Velocities April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 Facility Permit Number 9203-MSWLF-1980 Hydraulic Average Linear Velocity Code Conductivity Gradient Effective Porosity Monitoring Well .. MW-2 0.42 0.018 0.13 5.71E-02 9203-MSWLF-1980 MW-6 0.42 0.023 0.05 1.92E-01 9203-MSWLF-1980 MW-8 2.63 0.018 0.13 3.72E-01 9203-MSWLF-1980 MW-9 0.33 0.018 0.05 1.21E-01 9203-MSWLF-1980 MW-10 0.52 0.019 0.13 7.43E-02 9203-MSWLF-1980 MW-11 0.42 0.018 0.13 5.86E-02 9203-MSWLF-1980 MW-12 0.42 0.018 0.25 2.97E-02 9203-MSWLF-1980 MW-13 1.24 0.014 0.05 3.38E-01 9203-MSWLF-1980 MW-14 0.26 0.017 0.05 8.64E-02 9203-MSWLF-1980 MW-15 2.00 0.017 0.18 1.85E-01 9203-MSWLF-1980 MW-16 0.42 0.015 0.05 1.24E-01 9203-MSWLF-1980 MW-17 0.42 0.016 0.13 5.22E-02 9203-MSWLF-1980 MW-18 6.43 0.020 0.08 1.59E+00 9203-MSWLF-1980 MW-19 1.84 0.018 0.13 2.59E-01 Notes. 1. Hydraulic conductivity and effective porosity values are estimated from previously performed slug tests and grain size analyses. 2. The gradient and linear velocity values shown for MW-2 are based on the average of all the listed wells. Smith Page 1 of 1 June 2019 Table 3 Water Quality Parameters April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 Facility Permit Number 9203-MSWLF-1980 Monitoring Well .. MW-2 Water Quality Measurements ConductivityPH Turbidity�. .R .U. (11S) kdegrees IT(N 6.99 2,914 17.4 6 8.83 95.7 9203-MSWLF-1980 MW-4 5.53 247 16.6 24 7.17 170.9 9203-MSWLF-1980 MW-6 5.83 1,385 16.3 12 0.44 65.3 9203-MSWLF-1980 MW-8 5.90 424 15.8 4 0.26 18.6 9203-MSWLF-1980 MW-9 5.84 785 16.1 28 0.07 1.8 9203-MSWLF-1980 MW-10 5.56 1,003 14.4 5 0.23 27.7 9203-MSWLF-1980 MW-11 5.22 447 14.4 68 0.30 48.0 9203-MSWLF-1980 MW-12 6.29 1,527 14.3 11 0.18 27.6 9203-MSWLF-1980 MW-13 4.45 339 15.2 6 1.14 198.2 9203-MSWLF-1980 MW-14 4.64 560 16.4 1 0.07 152.4 9203-MSWLF-1980 MW-15 4.98 618 16.4 10 0.16 148.2 9203-MSWLF-1980 MW-16 5.40 278 18.7 7 0.19 77.5 9203-MSWLF-1980 MW-17 5.51 479 15.3 138 0.28 130.1 9203-MSWLF-1980 MW-18 5.83 667 15.7 18 0.44 145.6 9203-MSWLF-1980 MW-19 5.52 276 15.8 1 0.44 97.9 9203-MSWLF-1980 MW-20 6.92 320 15.3 27 2.83 149.5 9203-MSWLF-1980 MW-21 5.14 111 17.4 150 6.44 213.1 9203-MSWLF-1980 MW-22 6.24 738 14.9 15 1.20 12.3 9203-MSWLF-1980 MW-23 6.46 1,147 15.3 9 0.98 -19.4 9203-MSWLF-1980 MW-24 5.64 1,521 15.8 195 0.25 44.0 9203-MSWLF-1980 MW-25 6.08 1,613 15.4 26 0.07 79.8 9203-MSWLF-1980 MW-26 3.80 751 14.6 9 0.33 247.6 9203-MSWLF-1980 MW-27 5.82 629 16.7 6 0.17 -10.6 9203-MSWLF-1980 MW-28 6.20 795 17.3 29 6.77 110.0 9203-MSWLF-1980 Surface Water Sample 9203-MSWLF-1980 MW-29 Location SW-1 5.02 6.08 193 93 14.7 1 20.1 39 0.51 1 7 1 8.68 61.6 1 130.4 9203-MSWLF-1980 SW-2 DRY 9203-MSWLF-1980 SW-3 6.68 321 1 17.7 1 102 1 0.17 1 9.3 Notes: 1. Water quality measurements were collected on April 29-30 and May 1-2, 2019. 2. SW - Surface Water 3. ORP - Oxidation Reduction Potential (mV - millivolt) 4. DO - Dissolved Oxygen (mg/L - milligrams per liter) 5. S.U. - Standard Units 6. NTUs - Nephelometric Turbidity Units 7. µS/cm - Microsiemens per centimeter 8. Turbidity measurements recorded at the time of sample collection. Smith Page 1 of 1 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 North Carolina 2L or IMAC Standard 1. 10 700 V 2 10 1* 1,000 15 1 100 20 20 20,000* 0.2* [0.3* 1,000 FOO,000 MW-2 4-Apr-12 159 18.3 -- 7.271 -- MW-2 6-Nov-12 0.5631 401 2.391 2.241 1.971 -- 2.431 8.831 -- MW-2 15-May-13 801 0.2J 0.07J 0.51 -- 41 34 -- MW-2 6-Nov-13 210 1.01 0.21 21 0.41 11 -- 516 -- MW-2 9-Apr-14 150 0.3J 0.10J 21 0.21 0.041 0.71 2J -- 14MM 516 -- MW-2 28-Oct-14 2J 360 0.1J 0.21 21 0.021 21 21 -- 0.071 416 -- MW-2 5-May-15 0.71 190 0.11 11 0.041 11 -- 316 -- MW-2 19-Nov-15 0.51 650 21 41 61 0.061 31 21 -- 10 -- MW-2 26-Apr-16 250 -- 20 -- MW-2 17-Nov-16 0.401 370 0.161 1.5113 1.81 1.01 0.361 -- 6.416 4.21 -- MW-2 27-Apr-17 2.11 160 0.971 0.281 2.81 9.41 -- 9.6.1 -- MW-2 26-Sep-17 170 0.831 -- 14J -- MW-2 16-Jan-18 200 0.761 0.251 1.51 -- 8.7.1 -- MW-2 28-Mar-18 130 -- 8.11 4.OJ -- MW-2 31-Aug-18 170 -- 7.9.1 3.1J -- MW-2 (dissolved) 31-Aug-18 - -- -- - -- - - - -- -- -- -- -- -- -- 7.8 -- -- MW-2 28-Nov-18 180 -- 7.8.1 4.31 -- MW-2 26-Feb-19 120 -- 9.61 5.41 -- MW-2 2-May-19 170 2.5J 1.3J 1.71 4.51 2.41 1.51 -- 13J 14B -- MW-4 8-Nov-11 45.61 2.271 4.1518 -- 6.851 17.8 -- MW-4 4-Apr-12 0.911 38.81 -- 3.84.1 -- MW-4 6-Nov-12 1.101 57.41 2.851 1.62J 2.581 2.871 3.481 -- 7.651 11.1 -- MW-4 15-May-13 21 50J 0.051 2J 1.0J 21 21 21 -- 516 -- MW-4 6-Nov-13 41 901 0.11 61 4J 11 41 91 -- 27 -- 61 MW-4 9-Apr-14 2J 40J 11 0.3.1 1.01 0.51 0.021 1.01 -- 71B -- MW-4 28-Oct-14 2J 70J 0.081 4113 2J 41 31 51 -- 0.091 51 16B -- MW-4 5-May-15 41 801 0.11 0.11 Si 2.1 81 41 41 -- 51 13B -- MW-4 19-Nov-15 2J 40J 0.11 21 0.61 11 11 0.111 21 -- 61 -- MW-4 26-Apr-16 501 11 0.41 11 -- -- MW-4 16-Nov-16 1.71 48J 0.121 0.0901 2.81 0.791 2.71 2.01 2.51 -- 7.11 7.61 -- MW-4 28-Apr-17 33J -- 5.6.1 3.61 -- MW-4 26-Sep-17 0.921 2.41 56J 0.231 4.41 0.921 2.81 2.51 3.51 -- 111 10 -- MW-4(dissolved) 26-Sep-17 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 4.OJ -- -- MW-4 28-Mar-18 3.41 68J 0.181 6.71 4.11 2.81 4.61 -- 9.51 11 -- MW-4(dissolved) 28-Mar-18 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- MW-4 28-Nov-18 1.41 42J 2.21 0.721 2.41 -- 3.61 2.51 -- MW-4(dissolved) 28-Nov-18 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 2.6J -- -- MW-4 2-May-19 1.3J 40J 2.31 0.541 -- 3.51 4.0131 -- MW-4(dissolved) 2-May-19 -- -- I -- I -- -- I -- -- I -- I -- -- I -- I -- -- I-- MW-6 4-Apr-12 0.2541 248 6.791 1.491 2.521 2.181 -- 15.81 7.071 -- MW-6 6-Nov-12 509 6.42J 1.16J 1.911 2.601 -- 16.21 18.4 -- MW-6 15-May-13 0.61 280 0.81 71 11 27J 2J -- 916 -- MW-6 6-Nov-13 450 0.31 0.21 2.1 11 0.021 191 2J -- 6113 -- MW-6 9-Apr-14 11 470 0.81 0.31 10 21 0.041 31J 3J -- 301 27B -- MW-6 28-Oct-14 0.91 530 0.41 61 21 0.031 26J 2J -- 9113 -- MW-6 5-May-15 11 570 0.51 0.41 5J 31 0.061 25J 21 -- 131E -- MW-6 18-Nov-15 0.51 660 0.21 21 3.1 41 0.71 20J 11 -- 11 -- MW-6 (dup) 18-Nov-15 11 620 0.061 0.21 31 3J 41 0.91 0.031 20J 11 -- 12 -- MW-6 27-Apr-16 0.3J 11 610 0.07J 0.31 2113 3JB 41 0.81 21J 11 -- 13 -- MW-6 16-Nov-16 0.251 0.911 570 0.621 0.86J 3.91 25J 1.21 0.331 -- 2.71 5.91 -- MW-6 27-Apr-17 620D 0.671 13 4.31 191 1.81 -- 3.6.1 25 -- MW-6 27-Sep-17 0.681 1,00013 0.171 1.41 3.21 23J -- 4.41 6.31 -- MW-6 (dup) 27-Sep-17 1,00013 3.31 24J -- 3.8.1 7.11 -- MW-6 28-Mar-18 850 0.561 18 3.71 29J -- 11 -- MW-6 (dissolved) 28-Mar-18 -- - 760 - -- - 16 -- -- -- -- -- -- -- -- -- -- - MW-6 (dup) 28-Mar-18 820 0.531 18 3.31 28J -- 10 -- MW-6 dup (dissolved) 28-Mar-18 - - 800 - -- - 18 -- -- - -- -- -- -- -- -- -- -- MW-6 28-Nov-18 850 0.701 14 3.41 191 -- 8.51 -- MW-6 (dissolved) 28-Nov-18 - - 800 - -- - 10 -- -- -- -- -- -- -- -- -- -- - MW-6 2-May-19 1.31 800 0.281 13 2.11 23J -- 11B -- MW-6 (dissolved) 2-May-19 -- - 1 820 - -- I - 1 13 1 -- I -- I -- I -- I -- I -- I -- I -- I -- I -- -- Smith Page 1 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-8 4-Apr-12 0.5741 40.4.1 2.351 3.20.1 -- 30.0J -- MW-8 4-Jun-12 -- -- -- -- I -- -- -- -- -- -- -- -- -- 8,290 -- -- -- 200,000 -- -- -- -- -- -- MW-8 19-Jul-12 - -- -- -- -- -- -- 10,100 -- -- -- 240,000 MW-8 16-Aug-12 - I -- -- -- -- -- - -- -- -- -- -- -- 8,600 -- -- -- 170,000 MW-8 6-Nov-12 157y-13 0.91 104 0.41 18.7 5.60J 6J 13.2 52.3 10,000 SAM 5.201 110,000 MW-8 31 110 0.21 115 0.51 24J 9,520 12B 212,000 -- MW-8 31-Jul-13 -- -- -- -- -- -- -- -- -- -- -- -- 9,150 -- -- -- 248,000 MW-8 6-Nov-13 0.31 150 61 61 24J 7,900 216 189,000 -- MW-8 16-Jan-14 -- -- -- -- -- -- -- -- -- -- -- -- 8,280 -- -- -- 212,000 MW-8 10-Apr-14 0.61 0.51 130 0.31 71 81 0.21 0.051 34J 8,830 81 14B 212,000 MW-8 29-Oct-14 0.51 160 0.21 11 41 51 0.31 53 7,800 10B 181,000 MW-8 7-May-15 3.11 0.61 140 0.21 91 2.1 91 0.31 0.021 29J 7,900 51 196,000 MW-8 19-Nov-15 1.31 0.71 190 0.61 6J 7J 61 0.31 11 15J 41 178,000 MW-8 26-Apr-16 11 200 20 10 91 0.71 0.031 67 9,150 51 196,000 MW-8 16-Nov-16 0.521 160 6.91 0.681 73 6,000 5.81 180,000 MW-8 28-Apr-17 0.67J 120 3.2J 3.9J 4.61 0.271 30J 6,400 14J 3.91 210,000 MW-8 27-Sep-17 130 2.6J 12 2.81 6,800 24J 2.81 190,000H MW-8 28-Mar-18 0.67J 110 0.23J 7.2J 4.5J 2.01 42J 7,000 16J 3.41 170,000 MW-8 27-Nov-18 160 23 12 9.11 0.49J 95 7,100 111 4.91 190,000 MW-8 1-May-19 210 13 19 6.31 0.381 84 21,000 5.0J 4.381 160,000 MW-9 30-Mar-11 176 0.2041 8.41J 3.19J 9.171E 3.091 10.3.1 -- -- MW-9 7-Nov-11 147 0.1361 3.18J 1.28J 2.82113 -- -- MW-9 4-Apr-12 191 0.3551 10.1 3.921 12 2.581 11.6.1 -- M -- MW-9 (dup) 4-Apr-12 180 0.293J 8.31J 3.38J 9.98J 10.21 -- -- MW-9 4-Jun-12 -- -- -- -- -- -- -- -- -- -- -- -- -- 11,400 --280,000 MW79 19-Jul-12 38,600 -- -- -- 1,100,000 MW-9 16-Aug-12 -- -- I I - I -- -- -- -- -- -- -- -- 28,500 -- -- -- 650,000 MW-9 6-Nov-12 0.446J 2,130 1,320 0.546J 0.21 125 8.16J 4.15J 2J 45,300 30,100 17.4J 41 36 156 970,000 473,000 MW-9 15-May-13 61 51 57 4J 0.08J MW-9 (dup) 15-May-13 0.21 7J 1,260 0.21 31 57 41 0.071 21 -- 2J 12B -- MW-9 31-Jul-13 -- -- -- -- -- -- -- -- -- -- -- -- -- 30,800 -- -- -- 463,000 MW-9 6-Nov-13 81 jjhPO 0.41 0.11 71 65 71 0.081 471 31 23,600 0.11 191 27 431,000 MW-9 16-Jan-14 -- -- -- -- -- -- -- -- -- -- -- -- -- 21,800 -- -- -- 427,000 MW-9 10-Apr-14 8.1 1,060 0.11 0.11 11 19 39 41 0.071 31J 21 21,300 301 11B 417,000 MW-9 (dup) 10-Apr-14 0.31 10 1,050 0.11 0.31 11 19 50 41 0.06J 32J 2J IaW 17B -- MW-9 29-Oct-14 6.1 820 0.11 0.21 2113 14 29 51 0.11 32J 21,300 13B 375,000 MW-9 (dup) 29-Oct-14 61 820 0.11 0.21 1JB 14 30 51 0.04J 32J -- 10B -- MW-9 7-May-15 7.1 1,000 0.31 41 16 29 81 0.041 33J 19,800 4J 15 389,000 MW-9 20-Nov-15 6J 810 0.06J 0.81 12 18 7.1 0.10J 25J 2J 3J 383,000 MW-9 27-Apr-16 61 930 0.11 0.41E 13 11 61 24J 11 21,200 41 403,000 MW-9 16-Nov-16 6.81 1,100 0.0611 0.93J 14 10 7.4.1 0.036J 28J 19,000 2.81 4.0.1 370,000 MW-9 27-Apr-17 5.11 950D 0.181 1.41 12 14 8.31 0.0411 32J 21,000 3.3J 5.51 420,000 MW-9 27-Sep-17 6.1J 900 10 5.7.1 3.0.1 24J 20,000 4.01 380,000 MW-9 29-Mar-18 0.62J 4.9.1 850 1.61 12 11 7.41 27J 22,000 4.01 450,000 MW-9 (dissolved) 29-Mar-18 -- -- 780 -- -- -- 12 -- -- -- -- -- -- -- -- -- -- -- MW-9 28-Nov-18 3.11 1,100 14 7.21 6.01 31J 17,000 2.51 470,000 MW-9 (dissolved) 28-Nov-18 -- -- 1,100 -- -- - 13 -- -- -- -- -- -- -- -- -- -- -- MW-9 2-May-19 4.6.1 1,400 0.14J 25 7.21 4.61 57 32,000 9.71 580,000 MW-9 (dissolved) 2-May-19 -- -- 1,400 -- - - 25 -- -- -- -- -- -- -- -- -- - Smith Page 2 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-10 30-Mar-11 14.4 534 6.731 51.6 2.631B 2.931 41.61 2.011 -- -- MW-10 7-Nov-11 8.75J 476 0.1411 4.521 11.4 1.64J 3.72JB 18.71 -- 3.301 9.39J - MW-10 4-Apr-12 10.2 596 4.971 58.8 47.41 -- -- MW-10 4-Jun-12 - -- -- -- -- -- -- -- -- -- -- -- - 58,100 -- -- -- 630,000 OM MW-10 19-Jul-12 -- -- -- -- -- -- -- -- -- -- -- -- -- 1,680,000 -- -- -- 11,000,000 MW-10 16-Aug-12 -- -- -- -- - -- -- -- -- -- -- 1,900,000 -- -- -- 11,000,000 MW-10 6-Nov-12 34.2 2,050 2.94 67.6 42.5 152 0.349 7.641 595,000 111 195 2,800,000 MW-10(dup) 6-Nov-12 28.5 2,060 3.31 76.1 46.1 190 42.8 0.306 113 8.231 -- 127 231 - MW-10 15-May-13 32 1,140 2. 441 46 154 28 0.191 2J 253,000 O.3J 84 269 1,100,000 MW-10 31-Jul-13 -- -- -- -- -- -- -- -- - -- -- -- -- 121,000 -- -- -- 680,000 MW-10 6-Nov-13 21 0.81 0.11 10 31 45 81 0.061 39J 31 129,000 0.081 31 55 794,000 MW-10 (dup) 6-Nov-13 22 1.6 0.41 LLZO 37 75 16 0.101 50.1 4.1 -- 0.11 57 114 - MW-10 16-Jan-14 -- -- -- -- -- -- -- -- -- -- -- -- -- 69,600 -- -- -- 460,000 MW-30 10-Apr-14 16 310 0.081 iJ 14 21 0.41 0.071 14J 50,400 716 393,000 MW-10 26-Oct-14 13 720 0.21 31 21 12 31 0.11 23J 2J 86,300 24 670,000 MW-30 7-May-15 23 700 0.1J 21 29 31 0.61 0.021 36J 31 77,800 61 756,000 MW-10 20-Nov-15 25 730 0.1J 31 21 71 0.91 0.051 32J 31 61 680,000 MW-30 27-Apr-16 O.3J 34 850 0.lJ 0.51E 24 21 0.21 30J 21 93,400 21 832,000 MW-10 16-Nov-16 20 830 1.21 17 1.21 25J 65,000 1.6.1 1.91 760,000 MW-10 27-Apr-17 350 0.141 11 3.51 0.401 13J 40,000 2.11 2.81 350,000 MW-10 27-Sep-17 0.591 8.01 520 7.6.1 0.771 9.61 34,000 2.3J 380,000 MW-10 29-Mar-18 0.73.1 6.1J 480 0.231 2.81 35 6.51 1.11 38J 54,000 5.01 66 470,000 MW-10(dissolved) 29-Mar-18 -- -- -- -- -- -- 33 -- -- -- -- -- -- -- -- -- -- MW-10 28-Nov-18 2.91 42 4.21 1.11 49J 55,000 4.1J 10 590,000 MW-10(dissolved) 28-Nov-18 -- 600 -- -- -- 36 -- -- -- -- -- -- -- -- -- - MW-10 2-May-19 2 1.41 44 1.61 1 61 1 1.31 1 110,000 4.61 1 6.91 670,000 MW-11 31-Mar-11 75.5.1 -- 9.291 -- MW-11 8-Nov-11 83.81 1.081 -- 1. 14.7 -- MW-11 4-Apr-12 94.3.1 -- -- MW-11 6-Nov-12 93.21 2.521 -- 13.2 -- MW-11 15-May-13 O.6J 70J 0.51 2.1 0.81 2.1 -- 316 -- MW-11 6-Nov-13 0.81 70J 1.1 0.91 2.1 -- 4113 -- MW-11 10-Apr-14 1J 70J 0.7J 0.5J 11 0.31 0.041 21 -- 816 -- MW-11 29-Oct-14 0.61 70J O.41B 0.91 11 0.21 2.1 -- 5.1 -- MW-11 6-May-15 21 110 0.051 11 8.1 21 0.51 0.021 41 -- 716 -- MW-11 20-Nov-15 1.1 70J 0.051 0.21 0.51 5.1 21 0.21 31 11 -- 13 -- MW-11 27-Apr-16 1.1 110 9.1 0.81 31 -- 41 -- MW-11 16-Nov-16 0.601 91J 2.41 0.771 2.6.1 -- 1.4J 3.5.1 -- MW-11 28-Apr-17 96J 3.9J 1.51 -- 2.3J 9.8.1 -- MW-11 28-Sep-17 92J 1.8J -- 3.01 -- MW-11 29-Mar-18 87J 3.1.1 2.4J -- 3.11 - MW-11 28-Nov-18 1.61 100 5.9J 2.9J -- 6.81 - MW-11 2-May-19 2.9J 170 0. 181 1.5J 6.0J 2.4J 1.21 6.9.1 -- 15B - MW-11 (dissolved) 2-Mav-19 -- -- -- -- -- -- 5.1 -- -- -- -- -- -- -- -- -- -- CPage 3 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 North Carolina 2L or IMAC Standard 1. 10 700 V 2 10 1* 1, 0 0 OF-, 1 100 20 20 20,000* 0.2* 0.3* 1,000 500,000 MW-12 31-Mar-11 276 1.661E 2.461 9.68.1 -- 1.42J 10.1 -- MW-12 8-Nov-11 3.931 115 3.02113 -- 6.15.1 -- MW-12 3-Apr-12 182 1.281 -- -- MW-12 5-Nov-12 123 -- -- MW-12 15-May-13 21 170 0.91 0.11 0.31 2.1 -- -- MW-12 6-Nov-13 41 140 0.51 0.21 21 1.1 -- -- MW-12 10-Apr-14 21 230 0.91 0.21 0.61 0.041 2.1 -- Si 4113 -- MW-12 28-Oct-14 21 130 0.91E 0.11 0.51 1.1 -- 2113 -- MW-12 6-May-15 21 290 0.41 0.11 0.51 0.051 3.1 -- 3113 -- MW-12 20-Nov-15 61 200 0.31 0.61 11 2J -- -- MW-12 27-Apr-16 SJ 330 0.081 31 41 11 51 11 -- 6J -- = MW-12 17-Nov-16 5.11 140 0.671E 1.4.1 -- -- MW-12 27-Apr-17 3.91 260 0.821 0.0491 4.21 5.9.1 -- -- MW-12 (dup) 27-Apr-17 3.91 250 3.91 3.9.1 -- -- MW-12 28-Sep-17 0.851 3.81 130 1.31 -- -- MW-12 29-Mar-18 7.81 89.1 -- -- MW-12 28-Nov-18 5.31 220 2.11 -- -- MW-12 2-May-19 5.21 290 1.81 1.31 0.34J 4.31 2.0.1 -- 7.8.1 -- MW-12 (dissolved) 2-May-19 I -- -- I -- I -- -- I -- I -- I -- -- I -- I -- MW-13 31-Mar-11 576 2.301 11.3 3.331E 0.273 44.91 3.48.1 -- 60.9 -- MW-13 8-Nov-11 4.701 0.1301 1.21 3.081 16.8 5.291 53.2 -- 243 -- MW-13 3-Apr-12 4.411 2.481 17.0 4.641 0.384 53.4 -- 88.1 -- MW-13 5-Nov-12 0.6331 1.13J 10.4 8.361 0.487 46.2.1 -- 4.12J 234 -- MW-13 16-May-13 21 550 0.11 0.61 0.51 91 13 0.41 0.35 36J -- 103 -- MW-13 7-Nov-13 0.91 480 0.081 0.2J 7J 4JB 0.15J 33J -- 36 -- MW-13 10-Apr-14 21 590 0.11 0.61 0.31 10.0 18 0.79 35J -- 61 144 -- MW-13 28-Oct-14 2J 460 0.11 1.7 6J 13 0.2J 0.21 30J -- 0.06J 265 -- MW-13 6-May-15 2J 610 0.11 0.81 0.21 10 17 0.39 39J -- 98 -- MW-13 20-Nov-15 11 S00 0.11 0.3J 0.3J 81 13 0.50 32J 31 -- 48 -- MW-13 27-Apr-16 3J 620 0.11 0.21 0.31E 91 13 0.61 0.51 35J -- 58 -- MW-13 17-Nov-16 1.21 S00 0.181 6.4.1 4.7JB 0.20J 0.36 31J 0.17J -- 2.OJ 41 -- MW-13 28-Apr-17 2.61 380 0.16J 5.7J 5.51 0.36 24J 4.8.1 -- 3.2.1 38 -- MW-13 28-Sep-17 0.621 2.11 S10D 0.161 8.6J 2.7.1 0.43 35J -- 44 -- MW-13 29-Mar-18 1.51 490 0.331 6.7.1 1 7.91 0.351 0.56 29J -- 3.4.1 47 -- MW-13 (dissolved) 29-Mar-18 -- -- -- -- -- -- 6.5J -- -- -- -- -- -- -- -- -- -- MW-13 28-Nov-18 200 0.381 1.3J 3.81 0.37 13 -- 20 -- MW-13 29-Apr-19 1.31 450 0.191 7.31 5.7.1 0.40 26J -- 33 -- MW-13 (dup) 29-Apr-19 1 1.41 1 490 1 0.171 1 7.9.1 5.81 0.37 1 27J -- 36 -- MW-14 30-Mar-11 0.982J 36.3J 0.5041 2.89J 3.31JB -- 7.52J 13.0 -- MW-14 7-Nov-11 0.5281 5.601 26.61 1.911 -- 5.771 5.42.1 -- MW-14 3-Apr-12 0.4461 178 2.381 3.651 8.281 -- 3.09J -- MW-14 5-Nov-12 0.2991 60.01 3.59.1 -- 2.09.1 -- MW-14 16-May-13 0.7J 701 1.8 11 ]J 51 0.021 51 -- 51 -- MW-14 7-Nov-13 0.61 100J 21 0.61 0.91B 5.1 -- 8J 7113 -- MW-14 10-Apr-14 0.91 901 0.81 11 2J 51 0.21 0.091 9.1 -- 151 56.0 -- MW-14 28-Oct-14 0.31 140 0.11 0.41E 0.5J 11 5.1 -- 2113 -- MW-14 6-May-15 0.71 0.8J 140 0.11 11 11 71 0.181 10.1 -- 6113 -- MW-14 (dup) 6-May-15 1. 90 0.21 11B 11 12 0.091 6.1 -- 6J -- MW-14 20-Nov-15 0.91 150 0.71 0.7J 41 0.081 51 11 -- 4J -- MW-14 27-Apr-16 0.41 0.51 240 31B 11 0.121 18J -- -- 0.761 MW-14 17-Nov-16 0.721 0.931 210 0.17J 2.7J 2.61B 0.17J 0.80 16J 0.20J -- 4.11 3.61 -- MW-14 28-Apr-17 120 5.51 0.43 4.61 1.6.1 -- 5.5.1 5.0.1 -- 0.841 MW-14 28-Sep-17 140 0.38J 1.4J 1.91 0.13J 12J -- 4.9.1 5.3.1 -- MW-14 29-Mar-18 0.651 120 1.41 0.41 5.1.1 -- 2.9.1 160 -- MW-14 27-Nov-18 0.831 260 0.331 11 2.5J 3.61 0.361 2.5 24J -- 7.4.1 3.7.1 -- MW-14 (dup) 27-Nov-18 250 0.631 10 2.91 6.61 0.501 3.3H 24J -- 7.8.1 5.8.1 -- 0.811 MW-14 29-Apr-19 250 0.341 4.81 1 2.1.1 1 4.51 1.6 21J -- 5.61 1 5.5.1 -- Smith Page 4 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 North Carolina 2L or IMAC Standard 1. 10 700 4* 1 2 10 1* 1,00.j 15 1 100 20 20 20,000* 0.2* 0.3* 1,000 MW-15 31-Mar-11 0.4441 118 1.11 2.911 1.211 8.291E 2.421 0.1901 23.91 0.8481 -- 4.561 5.65.1 -- MW-15 8-Nov-11 118 0.7001 1.091 16.5.1 -- 2.31.1 -- MW-15 5-Apr-12 LOU 117 5.951 18.7.1 -- -- MW-15 7-Nov-12 1.20J 133 18.3.1 -- 5.03.1 -- MW-15 16-May-13 1.31 140 0.51 11 11 14 0.31 0.071 21J -- -- MW-15 7-Nov-13 220 0.051 0.11 21 4J 51B 0.111 34J -- -- MW-15 8-Apr-14 0.81 160 1 0.51 11 41 0.31 0.081 23J 2J -- 6J 716 -- MW-15 27-Oct-14 1.61 180 0.41 0.21E 2J 21 0.21 25J -- 416 -- MW-15 5-May-15 1.01 0.81 210 0.41 0.81 4.1 17 0.21 0.081 28J -- 516 -- MW-15 18-Nov-15 0.41 180 0.71 0.31 21 21 0.31 0.031 27J 11 -- 51 -- MW-15 27-Apr-16 280 0.071 0.21 51 4J 71 0.81 0.21 32J -- 61 -- MW-15 17-Nov-16 0.801 0.361 190 0.491 2.01 0.711 3.91E 0.211 0.111 30J 0.331 -- 1.81 7.0.1 -- MW-15 28-Apr-17 190 0.271 S.51 0.12J 23J 3.9.1 -- 2.7.1 5.6.1 -- MW-15 28-Sep-17 240 0.481 3.01 4.41 0.311 0.31 30J -- 4.8.1 4.6.1 -- MW-15 29-Mar-18 250 0.361 6.11 3.11 4.91 0.491 0.23 28J -- 5.3.1 5.0.1 -- MW-15 28-Nov-18 0.53J 190 0.601 2.51 1.71 26J -- 5.0.1 -- MW-15 29-Apr-19 220 0.32J 1.41 2.9J 27J -- 3.1.1 -- MW-16 1-Apr-11 10.8 451 4.401 5.911 2.721E 10.31 1.72.1 -- 6.35.1 -- MW-16 9-Nov-11 18.9 348 0.1231 6.12J 5.69.1 4.971 5.311 -- 7.0M 13.8 -- MW-16 5-Apr-12 0.267J 14.6 433 4.111 5.20J 9.341 2.681 -- -- MW-16 7-Nov-12 1.71.1 11.1 436 2.64J 6.13.1 3.981 7.561 -- 5.46.1 -- MW-16 14-May-13 14 350 11 6J 31 0.81 91 -- 316 -- MW-16 5-Nov-13 16 260 11 5.1 11 0.31 41 2J -- 716 -- MW-16 8-Apr-14 13 300 0.31 5J 11 0.31 0.021 71 21 -- 51 616 -- MW-16 27-Oct-14 10.1 330 0.11 0.2JB 5.1 iJ 0.41 71 -- 516 -- MW-16 5-May-15 13 280 11 5J 31 0.71 0.031 71 2J -- 5113 -- MW-16 3-Nov-15 12 300 0.41 51 11B 0.41 71 -- 41 -- MW-16 27-Apr-16 12 330 0.71 4J 0.51 81 11 -- 4.1 -- MW-16 16-Nov-16 14 280 0.34J 0.73J 4.4.1 1.51 0.731 6.51 0.20J -- 1.81 6.51 -- MW-16 27-Apr-17 13 230 2.01 1.01 0.281 3.9.1 -- 3.1.1 -- MW-16 26-Sep-17 12 320 4.2.1 1.31 7.11 -- 4.71 -- MW-16 29-Mar-18 14 250 1.81 4.81 6.7.1 -- 3.3.1 -- MW-16 28-Nov-18 19 170 4.4J 6.61 -- 2.5J 2.61 -- MW-16 2-May-19 1 12 210 0.131 3.8J 4.11 0.491 6.3.1 -- 5.881 -- MW-17 9-Nov-11 13.3 190 0.183J 8.34J 5.52.1 6.551 7.491 8.801 -- 10.6J 27.5 -- MW-17 5-Apr-12 5.591 105 1.701 2.00J 3.221 5.181 -- 2.42.1 -- MW-17 7-Nov-12 0.2261 3.57J 156 1.93J 2.15.1 1.781 3.231 4.981 -- 7.49J -- MW-17 14-May-13 101 120 0.08J 0.11 21 21 31 21 51 -- 6113 -- MW-17 6-Nov-13 12 120 0.91 1.1 21 0.61 31 -- 51 22 -- MW-17 10-Apr-14 81 70J 0.31 11 11 21 0.71 0.041 3.1 -- Si 916 -- MW-17 28-Oct-14 8.1 140 0.04J 2113 3.1 31 21 0.021 6.1 -- 11 -- MW-17 5-May-15 11 140 0.21 0.11 51 6J 71 31 91 -- 24 -- MW-17 19-Nov-15 14 150 0.09J 0.11 21 7.1 31 21 101 11 -- 101 - MW-17 26-Apr-16 11 110 0.21 21 4J 31 11 7.1 -- 91 -- MW-17 17-Nov-16 0.22J 12 120 0.21J 2.3J 1.8113 0.301 6.31 0.20J -- 3.71 3.51 -- MW-17 28-Apr-17 8.9J 100 1.51 0.501 2.91 2.1.1 -- 2.8J 5.7.1 -- MW-17 26-Sep-17 9.51 150 1.61 1.51 0.711 5.4.1 -- 5.0J 4.31 - MW-17 (dissolved) 26-Sep-17 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- 2.41 -- -- MW-17 29-Mar-18 0.53J 280 0.711 0.43J 25 14 33 31J -- 71 82 -- MW-17 (dissolved) 29-Mar-18 -- -- -- -- -- -- -- -- -- -- -- 44 -- -- MW-17 28-Nov-18 6.2J 93J 0.601 2.81 1.91 5.0.1 111 3.31 - MW-17 2-May-19 160 0.301 7.81 5.51 11 5.71 13J -- 16J 30B -- 7.2 MW-17 (dissolved) 2-May-19 -- -- I -- I -- I -- -- -- -- -- -- I -- -- I - 21 -- - cSPi� ith Page 5 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-18 8-Nov-11 104 1.331 2.5316 8.05.1 -- 2.ONM 8.83.1 -- MW-18 4-Apr-12 89.51 9.94.1 -- -- MW-18 6-Nov-12 104 12.1.1 -- 5.80.1 -- MW-18 15-May-13 2J 901 0.31 1.1 0.3.1 13J -- -- 7��l MW-18 6-Nov-13 4.1 120 0.2J 41 61 21 0.021 18J 2J -- 61 24 -- MW-18 10-Apr-14 2J 801 0.51 21 0.03J 15J -- 7J 6J6 -- MW-18 28-Oct-14 2J 801 1J 14J -- 3.1 -- MW-18 5-May-15 2J 901 0.31 1.1 2.1 15J -- 4.113 -- MW-18 19-Nov-15 2.1 901 0.41 11 11 16J 11 -- 4.1 -- MW-18 26-Apr-16 11 901 0.41 2.1 15J -- 4.1 -- MW-18 16-Nov-16 2.3.1 100 0.111 0.931 2.21 0.471 16J 1.2.1 -- 2.3J 7.1.1 -- MW-18 27-Apr-17 3.2.1 110 0.14J 3.21 5.6.1 1.9.1 0.0341 23J 3.7.1 -- 6.91 16 -- MW-18 26-Sep-17 2.4.1 110 0.171 2.61 4.21 1.11 18J -- 12J 14 -- MW-18 (dissolved) 26-Sep-17 - -- -- -- -- -- -- -- -- -- -- -- -- -- -- 5.9.1 -- -- MW-18 28-Mar-18 1.3.1 981 1.91 17J -- -- MW-18 28-Nov-18 1.4.1 100 1.61 18.1 -- -- MW-18 2-May-19 1.8.1 100 1.51 2.01 0.361 7.8.1 -- 2.7J 5.3BJ -- MW-18 (dissolved) 2-May-19 -- -- -- - -- -- -- -- -- -- -- -- -- -- -- -- -- MW-19 9-Nov-11 0.701J 4.521 169 0.4311 1.951 2.11.1 -- 0.1661 6.52J 5.221 -- MW-19 5-Apr-12 2.3OJ 125 2.081 I 6.001 3.03J I -- 2.781 6.08J -- MW-19 4-Jun-12 -- -- -- -- -- -- -- -- -- -- -- -- -- 44,700 -- -- -- 230,000 MW-19 19-Jul-12 -- -- -- -- ---- -- -- 40300 -- -- -- 240,000 MW-19 16-Aug-12 I -- -- -- -- -- -- -- -- -- -- -- -- 42500 -- -- -- 110,000 MW-19 7-Nov-12 16-May-13 1810.7491 4.971 3.091 0.41 6.141 34800 37,100 8.191 2J 21.2 130,000 MW-19 111jilliMMU 180 1 21 21 51 5J 220,000 -- -- MW-19 31-Jul-13 -- -- -- -- -- -- -- -- -- -- -- 40,500 -- -- -- 242,000 MW-19 7-Nov-13 2.1 170 O.S1 0.11 11B 11 36,800 41 4.113 222,000 MW-19 16-Jan-14 -- -- -- -- -- -- -- -- -- -- -- -- -- 40,900 -- -- -- 232,000 MW-19 9-Apr-14 1.OJ 3.1 ISO 0.41 2J 101 71 0.41 0.041 12J 10,200 10B 154,000 MW-19 29-Oct-14 4.11 21 150 0.91 2J13 8.1 4.1 0.31 101 14,900 9.113 170,000 MW-19 7-May-15 3.2J 2J 220 0.O9J 0.21 3J 18 14 0.31 0.031 25J 7,900 2J 27 150,000 MW-19 20-Nov-15 1.31 21 150 0.081 0.31 31 5J 51 0.41 101 11 81 134,000 MW-19 26-Apr-16 O.3J 11 160 0.O6J 2J 5.1 19 0.21 15J 7,900 8.1 120,000 MW-19 (dup) 26-Apr-16 0.41 11 160 0.O7J 0.11 21 Si 20 0.2.1 151 8J MW-19 16-Nov-16 0.59.1 2.1.1 180 0.13J 3.0J 11 6.01 0.471 16J 7,600 4.8.1 7.2J 160,000 MW-19 27-Apr-17 170 1.61 2.51 6.01 0.34.1 0.0481 9.5.1 18,000 4.71 6.21 170,000 MW-19 27-Sep-17 1.7.1 170 1.51 34,000 111 200,000 MW-19 28-Mar-18 160 3.31 1.51 3.41 0.49.1 7.8.1 16,000 7.41 160,000 MW-19 27-Nov-18 1.7.1 200 2.31 1.7J 3.1J 26,000 4.6.1 170,000 MW-19 1-May-19 1 1.61 210 4.31 1.91 2.3.1 1.1J 7.91 1 1 32,000 7.1.1 6.481 1 170,000 MW-20 1-Apr-11 4.27J 270 0.2441 19.8 11.1 18.613 12.9 21.41 1.53.1 -- 25.5 60.3 -- MW-2O 9-Nov-11 6.55.1 290 0.3711 24.2 14.1 16.6 14.4 23.1.1 -- 29.5 78.5 -- MW-2O 5-Apr-12 0.722J 4.37J 162 4.66J 1.57.1 4.301 2.521 4.25.1 -- 6.28.1 9.31J -- MW-2O 7-Nov-12 218 12.6 3.411 5.42.1 5.18.1 9.29.1 -- 11.51 24.7 -- MW-2O 14-May-13 0.31 3J 190 0.11 11 3J 14 3.1 9.1 -- 5.1 19B -- MW-2O 5-Nov-13 O.3J 41 240 0.21 0.1.1 10 7J 11 5.1 13J -- 0.081 181 47 -- MW-2O 9-Apr-14 0.51 2J 160 O.3J 31 2.1 568 2.1 0.03.1 5.1 -- 14J 51 -- MW-2O 28-Oct-14 61 450 0.31 0.2.1 71 6.1 46 3.1 0.09.1 10.1 -- 45 137 -- MW-2O 5-May-15 O.6J 4J 220 O.2J 71 5.1 14 3.1 9.1 -- 111 38 -- MW-2O 19-Nov-15 0.41 31 210 0.11 61 4.1 9.1 31 8.1 -- 8.1 26 -- MW-2O 27-Apr-16 O.2J 4J 240 O.2J 71 51 81 4.1 9.1 -- 1.1 28 -- MW-2O 17-Nov-16 0.25J 3.7.1 290 0.521 0.181 12 8.4J 19B 7.51 18J 0.20J -- 21J 56 -- MW-2O 27-Apr-17 2.OJ 110 0.821 1.6.1 -- 3.9.1 -- MW-2O 27-Sep-17 0.821 2.3.1 110 0.69.1 -- 9.9.1 -- MW-2O 29-Mar-18 2.4J 120 -- 3.4.1 -- MW-2O 28-Nov-18 2.51 120 -- 4.71 -- MW-2O 2-May-19 2.3.1 130 1.91 0.261 3.9J -- 4.51 S.213J - MW-20 (dissolved) 2-May-19 I -- I -- I -- -- I -- -- -- -- I -- -- I -- I -- I -- I -- I -- 1 3.5.1 -- I -- CPM Page 6 of 18 June 2019 Smith Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-21 31-Mar-11 5.641 68.21 3.981 2.591 7.16JB 3.891 5.661 -- 8.91J 21.6 -- MW-21 8-Nov-11 16.1 135 0.2951 L 12.7 7.881 13.1 11.88 13.21 -- 22.41 48.7 -- MW-21 4-Apr-12 6.231 58.11 1.85J 2.481 4.351 3.081 3.781 -- 6.78J 11.7 -- MW-21 6-Nov-12 3.19J 76.41 3.521 2.14) 4.731 4.371 3.131 -- 9.451 18.3 -- MW-21 15-May-13 41 70J 0.081 2J 2.1 41 21 31 -- 5.1 916 -- MW-21 6-Nov-13 2J 601 0.061 21 1.1 31B 11 21 -- 61 716 -- MW-21 9-Apr-14 61 220 0.21 7J 5.1 11 51 0.041 101 -- 37 89 -- MW-21 28-Oct-14 31 60J 0.041 2113 11 31 21 21 -- 4J 71 -- MW-21 5-May-15 51 100 0.21 6J 3.1 81 41 71 -- 13J 25 -- MW-21 19-Nov-15 2J 40J 0.051 0.21 11 1.1 31 11 21 -- 31 71 -- MW-21 26-Apr-16 21 60J 0.051 11 11 21 11 21 -- 61 -- MW-21 16-Nov-16 2.31 56J 0.0731 2.71 2.1J 5.01 2.41 4.31 -- 6.31 13 -- MW-21 28-Apr-17 8.31 0.811 -- 3.2.1 -- MW-21 26-Sep-17 4.31 65J 0.291 5.91 3.91 8.61 3.61 9.11 -- 11J 27 -- MW-21 (dissolved) 26-Sep-17 -- -- -- -- -- -- -- -- -- -- -- -- -- -- 4.7.1 -- -- MW-21 28-Mar-18 3.6J 48J 4.71 5.11 1.91 3.21 -- 7.11 10 -- MW-21 (dissolved) 28-Mar-18 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- MW-21 28-Nov-18 24J 1.41 0.491 -- 5.3.1 -- MW-21 2-May-19 3.01 55J S.SJ 1.7.1 5.11 4.01 3.91 -- 9.2.1 13B -- MW-21 (dissolved) 2-May-19 -- -- I -- -- -- -- -- I -- -- I -- I -- -- -- -- -- -- MW-22 31-Mar-11 192 4.64J 3.08.1 7.811 4.271 6.411 3.751 -- 7.3O1 21.7 -- MW-22 8-Nov-11 4.301 173 1.441 2.2118 -- 1.821 14.6 -- MW-22 4-Apr-12 4.661 159 2.17J 3.18.1 2.411 2.381 2.791 -- 3.141 8.59.1 -- MW-22 6-Nov-12 4.701 184 2.411 -- 1.471 7.721 -- MW-22 15-May-13 3J 200 0.1J 0.71 4J 4.1 71 21 0.04.1 71 -- 19B -- MW-22 6-Nov-13 31 160 0.21 0.91 31 31B 0.31 0.061 31 -- 416 -- MW-22 9-Apr-14 21 240 0.21 11 2.1 31 0.6.1 0.05.1 41 -- 81 916 -- MW-22 28-Oct-14 3J 250 0.11 0.51 4113 7J 71 21 0.111 71 -- 31 36 -- MW-22 5-May-15 41 240 0.051 11 6.1 31 0.6.1 0.06.1 51 -- 716 -- MW-22 19-Nov-15 41 240 0.091 21 7J 51 11 0.031 61 11 -- 11 -- MW-22 26-Apr-16 51 240 O.BJ 5.1 21 0.8.1 0.03.1 51 -- 91 -- MW-22 16-Nov-16 6.31 250 0.0841 4.61 1.11 0.24J 3.41 -- 1.51 5.21 -- MW-22 (dup) 16-Nov-16 6.31 250 0.058J 4.6.1 1.2.1 0.26.1 3.5.1 -- 1.8.1 4.8.1 -- MW-22 28-Apr-17 5.61 240 4.31 1.91 0.541 1.61 5.1J -- 4.11 4.91 -- MW-22 26-Sep-17 6.3J 260 4.1.1 2.0.1 0.37.1 3.3.1 -- 3.71 6.2.1 -- MW-22 (dissolved) 26-Sep-17 -- -- -- -- -- -- 3.61 -- -- -- -- -- -- -- -- 3.31 -- -- MW-22 28-Mar-18 9.0.1 310 2.2J 6.2.1 2.1J 0.75.1 4.5.1 -- 7.9J -- MW-22 (dissolved) 28-Mar-18 -- -- -- -- -- -- 5.21 -- -- -- -- -- -- -- -- -- -- -- MW-22 28-Nov-18 360 7.1.1 4.01 -- 3.2J -- 9.3 MW-22 (dissolved) 28-Nov-18 -- -- -- -- -- 6.6 -- -- -- -- -- -- -- -- -- -- -- MW-22 2-May-19 440 1.4J 8.1.1 1.51 0.431 4.9.1 -- 6.713.1 -- MW-22 (dissolved) 2-May-19 -- 3.4 -- I -- I -- I -- 1 7.2 -- -- -- -- -- -- -- -- -- -- -- MW-23 31-Mar-11 159 1.O6J 1.82J -- 2.331 41.7 -- MW-23 8-Nov-11 4.391 203 1.681 3.7818 -- 3.38.1 -- MW-23 4-Apr-12 201 1.O3J -- 2.761 7.63.1 - MW-23 5-Nov-12 MW-23 15-May-13 MW-23 5-Nov-13 No Samples Collected - Well was Dry MW-23 8-Apr-14 MW-23 27-Oct-14 MW-23 5-May-15 2J 270 0.3J 0.3J 0.91 0.021 21 -- 4113 - MW-23 19-Nov-15 30 830 0.06J 3J 71 51 21 91 11 -- 20 -- MW-23 26-Apr-16 260 1.1 0.051 -- 12 - MW-23 16-Nov-16 0.431 3.21 310 0.27J 6.7.1 0.981 6.01 0.211 -- 3.51 4.21 -- MW-23 28-Apr-17 2.3J 210 2.4.1 0.781 0.0411 7.8J -- 6.31 15 - MW-23 26-Sep-17 0.761 5.21 440 1.11 3.41 -- 3.91 3.11 -- MW-23 (dissolved) 26-Sep-17 -- -- -- - - - - -- -- -- -- - - MW-23 28-Mar-18 5.31 370 1.71 0.37J 2.21 -- 3.01 -- MW-23 (dissolved) 28-Mar-18 -- -- -- - - - 1.41 -- -- -- -- -- -- -- -- -- -- - MW-23 28-Nov-18 1.81 310 1.51 -- 5.7.1 20 -- MW-23 2-May-19 1.3J 280 2.11 2.9J -- 3.11 -- cSpmith Page 7 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 North Carolina 2L or IMAC Standard 1. 10 700 V 2 10 1. 1, 0 0 OF-, 1 100 20 20 20,000* 0.2* 0.3* 1,000 500,000 MW-24 9-Nov-11 20.1 402 0.1011 8.94J 12.6 1.671 7.001 0.237 24.41 -- 8.52J 23.8 -- MW-24 5-Apr-12 0.2971 27.2 599 0.4391 26.8 19.5 19.9 11.2 0.708 34.31 2.771 -- 31.7 64.3 -- MW-24 7-Nov-12 15.2 415 7.43J 11.7 3.441 3.751 0.1921 24.71 2.24J -- 9.92J 26.2 -- MW-24 16-May-13 15 570 0.61 0.31 21 24 41 In 0.17J 45J -- 0.101 43 132 -- MW-24 6-Nov-13 15 360 0.1J 31 M 12 41B 21 0.041 26J 2J -- 14B -- MW-24 8-Apr-14 91 550 0.61 0.41 23 31 0.26 46J -- 0.051 86 219 -- 81 51 MW-24 27-Oct-14 11 410 0.21 14 91 0.121 30J -- 49 -- MW-24 5-May-15 41 160 0.71 4J 11 0.21 11J -- 11JB -- MW-24 19-Nov-15 61 200 0.051 0.41 11 Si 31 0.91 0.021 151 11 -- 91 -- MW-24 25-Apr-16 71 140 3J 2J 41 11 10.1 -- 18 -- MW-24 15-Nov-16 0.371 7.81D 370 0.81J 0.54JD 20D 19D 36 0.20 0.40J -- 0.0841 34 96 -- MW-24 27-Apr-17 330 6.51 0.841 0.261 25J 7.3.1 -- 2.01 3.71 -- MW-24 26-Sep-17 0.501 310 1.31 5.9.1 1.51 0.531 21J -- 5.01 8.51 -- MW-24(dissolved) 26-Sep-17 -- 7.81 -- -- -- -- 4.21 -- -- -- -- -- -- -- -- 3.51 -- -- MW-24 28-Mar-18 9.31 260 1.31 7.0.1 191 -- 4.81 -- MW-24(dissolved) 28-Mar-18 -- -- -- -- -- -- 6.71 -- -- -- -- -- -- -- -- -- -- -- MW-24 28-Nov-18 310 0.191 4.81 8.6.1 5.41 3.81 22J 2.41 -- 8.3J 26 -- 2.0 MW-24(dissolved) 28-Nov-18 -- -- -- -- -- 3.51 -- -- -- -- -- -- -- -- -- -- MW-24 2-May-19 6.61 130 0.151 3.21 3.8.1 3.11 1.71 111 -- 7.7J 20B -- MW-24 (dissolved) 2-May-19 -- -- -- -- -- -- 2.71 -- -- -- I -- I -- -- -- -- I-- -- MW-25 31-Mar-11 0.8571 836 1.17J 4.621 8.851 -- 2.51J 9.051 -- MW-25 8-Nov-11 3.591 903 3.491 1.331 2.621E 6.031 -- 8.201 18.3 -- MW-25 4-Apr-12 894 1.201 4.531 -- 1.92J -- MW-25 6-Nov-12 963 4.551 -- 5.231 5.51J -- MW-25 15-May-13 21 900 0.21 0.4J 0.8J 11 0.31 81 -- -- MW-25 6-Nov-13 2J 820 0.41 0.71 11B 81 2J -- -- MW-25 9-Apr-14 21 830 0.41 0.71 21 0.31 81 31 -- 111 916 -- = 0.61 MW-25 28-Oct-14 2J 780 0.41 0.71 81 2J -- 31 -- MW-25 5-May-15 21 820 0.31 0.71 11 0.041 81 -- 316 -- MW-25 19-Nov-15 11 890 0.41 O.BJ 21 91 11 -- 41 -- MW-25 26-Apr-16 830 0.71 81 -- -- MW-25 16-Nov-16 1.61 860 0.39J 1.21 7.81 1.21 0.32.1 -- 2.01 3.91 -- MW-25 27-Apr-17 2.01 890D 1.31 13J 4.8.1 -- 1.7J 5.5.1 -- MW-25 26-Sep-17 3.81 1,00013 0.261 0.38J 7.0J 9.71 3.61 17J -- 111 31 -- MW-25 (dissolved) 26-Sep-17 -- -- 870 -- -- -- -- -- -- -- -- -- -- -- 3.2) -- -- MW-25 28-Mar-18 2.0J 960 0.40J 11J -- 2.81 -- MW-25 (dissolved) 28-Mar-18 -- -- 880 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- MW-25 28-Nov-18 930 0.68J 12J -- 21 -- MW-25 (dissolved) 28-Nov-18 -- -- 940 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- MW-25 2-May-19 1.71 900 0.44J 1.31 12J 2.51 -- 3.213.1 -- MW-25 (dissolved) 2-May-19 -- -- 930 -- -- -- -- -- -- -- -- -- -- -- MW-26 31-Mar-11 161 1.31 0.5221 6.421 31.1 9.241E 6.331 19.91 4.19.1 -- 9.0OJ 70.1 -- MW-26 8-Nov-11 3.211 230 1.66 1.751 34.0 3.04J13 16.31 -- 2.581 52.5 -- MW-26 4-Apr-12 364 2.12 1.78 60.2 4.531 23.51 -- 30.4 -- MW-26 6-Nov-12 357 1.98 47.9 1.851 21.21 -- 46.9 -- MW-26 15-May-13 0.51 340 1.9 0.41 0.4J 55 21 0.31 21J -- 25 -- MW-26 6-Nov-13 51 400 1.8 0.41 16 40 17 10.1 0.041 31J -- 0.07J 29 72 -- MW-26 9-Apr-14 330 1.6 0.41 0.6J 56 21 0.31 0.031 20J -- 30B -- MW-26 28-Oct-14 11 350 1.8 0.31 OAB 50 21 0.31 0.041 191 -- 25 -- MW-26 5-May-15 11 300 1.6 0.31 21 47 31 0.51 0.051 18J 21 -- 26 -- MW-26 19-Nov-15 0.61 180 1.4 0.31 11 32 4.1 0.71 0.041 13J 11 -- 27 -- MW-26 26-Apr-16 180 1.1 21 29 21 0.91 0.031 101 -- 36 -- MW-26 16-Nov-16 0.571 170 1.2 0.21J 1.3J 25 2.91 0.811 0.046.1 9.71 0.96.1 -- 2.0J 16 - MW-26 28-Apr-17 1.51 81J 0.661 0.131 14 2.31 1.41 0.0281 6.91 5.01 -- 3.31 17 -- MW-26 26-Sep-17 2.7J 190 1.2 1.3 8.7J 26 9.31 4.11 191 -- 15J 35 -- MW-26 (dissolved) 26-Sep-17 -- -- -- -- -- -- 22 -- -- -- -- -- -- -- -- -- -- MW-26 28-Mar-18 140 1.1 0.16J 1.41 21 1.81 0.291 8.51 -- 21 - MW-26 (dissolved) 28-Mar-18 -- -- -- -- -- -- 20 -- -- -- -- -- -- -- -- -- -- -- MW-26 28-Nov-18 190 0.831 0.16J 26 1.81 11J -- 23 -- MW-26 2-May-19 220 0.791 0.24J 34 1 2.71 0.271 131 1 2.31 -- 25B -- cSpi1'11h Page 8 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-27 31-Mar-11 0.831 0.631 1.761 1.151 4.121E 1.921 0.33 1.971 0.938.1 -- 3.51J 14.6 -- MW-27 8-Nov-11 9.701 128 0.1591 6.511 4.23.1 5.941 7.6418 0.286 7.06.1 -- 9.221 27.7 -- MW-27 4-Apr-12 4.271 110 2.36.1 -- 1.46J 5.25.1 -- MW-27 6-Nov-12 139 1.211 1.47.1 1.711 1.981 2.02.1 -- 13.31 8.97J -- MW-27 15-May-13 21 110 11 0.41 11 -- -- MW-27 6-Nov-13 4J 150 0.11 41 41 81 31 0.091 8.1 -- 29J 25 -- MW-27 9-Apr-14 31 120 0.21 21 21 0.61 0.121 2.1 -- 7J 816 -- MW-27 28-Oct-14 2J 140 0.7J 0.31 11 -- 21 2.1 -- MW-27 5-May-15 81 150 31 0.41 0.051 2.1 -- 316 -- MW-27 19-Nov-15 3J 130 11 0.41 11 11 -- 4.1 -- MW-27 26-Apr-16 160 11 0.021 4.1 -- 10 -- MW-27 16-Nov-16 0.231 2.41 120 0.0491 0.381 1.81 0.481 0.0401 1.6.1 -- 15.1 4.11 -- MW-27 28-Apr-17 0.531 2.1J 120 1.91 0.781 0.0541 1.51 -- 211 5.5J -- MW-27 26-Sep-17 6.11 470 0.541 0.341 23 33 0.29 33J -- 67 85 -- MW-27 (dissolved) 26-Sep-17 -- -- -- -- -- -- -- -- -- -- -- -- 1.5.1 -- -- MW-27 28-Mar-18 110 -- 4.41 -- MW-27 (dissolved) 28-Mar-18 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- MW-27 28-Nov-18 1.51 95J -- 7.5.1 -- MW-27 30-Apr-19 220 0.13J 9.2J 10 16 6.31 16J -- 11J 38B -- MW-28 1-Apr-11 189 10.1 6.31J 11.28 4.681 9.031 1.641 -- 25.8 47.0 -- MW-28 9-Nov-11 18.8 464 0.7911 47.1 25.5 30.3 14.2 34.0.1 -- 85.6 180 -- MW-28 5-Apr-12 2.961 233 14.0 7.61J 12.6 5.461 11.2.1 -- 30.2 51.4 -- MW-28 6-Nov-12 24.4 620 0.3591 21.7 11.0 19.7 9.091 17.01 2.19J -- 62.3 90.4 -- MW-28 15-May-13 13 1040 1.7 0.51 67 52 65 0.041 67 -- 0.31 291 683 -- 61 MW-28 6-Nov-13 5J 300 0.41 0.21 15 12 16 151 2J -- 53 94 -- MW-28 9-Apr-14 1.1 160 0.31 2J 11 144 0.61 0.041 3.1 -- 14J 31 -- MW-28 28-Oct-14 0.81 150 31B 11 91 0.51 3.1 -- 61 10 -- MW-28 5-May-15 1.1 270 0.81 0.51 11 2.1 -- 316 -- MW-28 19-Nov-15 2.1190 0.11 6J 12 11 51 11 -- 131 21 -- 0.41 MW-28 26-Apr-16 51 300 -- -- MW-28 16-Nov-16 0.381 0.581 180 O.081J 0.97J 1.71 1.6.1 -- 5.3J 2.8.1 -- MW-28 27-Apr-17 2.41 230 0.361 11 3.6J 111 -- 24J 43 -- MW-28 27-Sep-17 0.651 7.21 370 1.0 0.60J 39 12 28J -- 0.13J 75 120 -- MW-28 (dissolved) 27-Sep-17 -- -- -- -- -- -- -- -- -- -- -- -- -- 8.0.1 -- -- MW-28 28-Mar-18 7.2J 470 1.4 0.49J 60 IL 16 43J -- 0.191 81 220 -- MW-28 (dissolved) 28-Mar-18 -- -- -- -- -- -- -- -- -- -- -- -- 2.51 -- -- MW-28 28-Nov-18 2.0J 170 0.19J 5.71 1.71 12J -- 111 20 -- MW-28 (dissolved) 28-Nov-18 -- -- -- -- -- -- -- -- -- -- -- -- -- 4.2.1 -- -- MW-28 2-May-19 250 0.14J 1.51 -- 2.6J 3.9BJ -- MW-28 (dissolved) 2-May-19 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- cSpiM Page 9 of 18 June 2019 Table 4a Detected Groundwater Constituents - Inorganics April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-29 1-Apr-11 193 4.921 8.591 7.771E 2.271 10.51 1.161 -- 1.92.1 13.1 -- MW-29 9-Nov-11 142 0.1131 2.531 2.631 2.501 3.421 -- 2.961 8.541 -- MW-29 (dup) 9-Nov-11 154 0.2331 4.47J 3.01J 3.091 3.351 4.951 -- 3.95.1 16.5 -- MW-29 5-Apr-12 827 4.23 42.2 28.1 116 27.5 57.2 -- 0.2451 28.7 186 -- MW-29 4-Jun-12 -- -- -- -- -- -- -- -- -- -- -- -- -- 9,800 -- -- -- 190,000 ■ MW-29 19-Jul-12 -- -- -- -- -- - - - -- - 12,900 -- -- -- 260,000 MW-29 16-Aug-12 -- -- -- -- -- -- -- -- -- �9_ 13,500 -- -- -- 160,000 MW-29 7-Nov-12 1 375 0 2.17 28.6 2.3 31.2 140 16.9 72.2 100 1610 0.2 2001 13,400 0.1361 25,600 0.81 23.91 575 132 220,000 MW-29 16-May-13 316,000 -- MW-29 31-Jul-13 - -- -- -- -- -- -- -- -- -- - -- -- 20,000 -- -- 309,000 MW-29 7-Nov-13 71 0 25 2.4 150 100 360 176 0.29 1901,2J 22,700 0.81 707 847 312,000 MW-29 16-Jan-14 -- -- -- -- -- -- -- -- -- -- -- -- -- 13,600 -- -- -- 129,000 MW-29 9-Apr-14 71 630 4.2 0.8J 68 32 71 33 0.161 55 12,100 0.3J 124 168 268,000 MW-29 29-Oct-14 4J 330 1.5 0.51 20 11 31 18 0.091 21J 13,900 0.11 47 74 228,000 MW-29 6-May-15 71 470 2.3 0.3J 35 19 50 20 0.061 37J 12,100 0.2J 53 104 202,000 MW-29 20-Nov-15 2J 250 1.1 1.4 14 71 20 17 0.071 15J 0.11 41 87 160,000 MW-29 27-Apr-16 350 1.5 0.2J 19 11 25 21 20J 11,000 0.1J 46 70 176,000 MW-29 17-Nov-16 0.381 3.81 450 2.9 0.371 26 17 58B 27 0.0831 34J 0.391 10,000 0.12J 28 110 130,000 MW-29 27-Apr-17 83J 0.401 5.5J 2.5J 8.2J 5.8J 0.0321 7.41 9,100 111 19 180,000 MW-29 27-Sep-17 2.61 991 1.61 4.01 0.851 0.361 5.81 11,000 4.81 6.91 10,000 MW-29 29-Mar-18 1.41 150 0.871 0.13J 19 5.81 21 9.81 151 9,600 16J 46 410,000 MW-29 (dissolved) 29-Mar-18 -- -- -- -- -- -- -- - -- -- -- -- - -- -- MW-29 28-Nov-18 64J 6.51 1.91 5.61 2.2J 7.41 7,900 4.41 11 130,000 MW-29 (dissolved) 28-Nov-18 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- MW-29 2-May-19 3.3J 130 0.161 5.31 4.1J 1.91 14J 13,000 5.4J 13 -- MW-29 (dissolved) 2-Mav-19 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- Notes: 1. All units are in micrograms per liter (parts per billion). 2. * - Interim Maximum Allowable Concentration (IMAC) 3. dup - Duplicate Sample 4.1 - Indicates the analytical result is an estimated concentration between the laboratory method detection limit and the laboratory limit of quantitation. 5. B -The amount in the prep blank is greater than the method detection limit. 6. D -The analyte was run at dilution. 7. H - The anaylte was analyzed outside of hold time due to laboratory error. 8. -- Not analyzed for 9. NE - Standard Not Established 10. Dissolved metals samples were collected to evaluate the influence of turbidity on total metal concentrations as part of an ongoing Alternate Source Demonstration. - Concentration exceeds the 15A NCAC 02L .0202 or IMAC Standard - Indicates the result is below the detection limit - A sodium lactate injection was performed near MW-8, -9, and -10 on June 18-21, 2012. - An emulsified vegetable oil injection was performed near MW-8, -9, and -10 on March 25-27, 2013. Smith Page 10 of 18 June 2019 Table 4b Detected Groundwater Constituents - Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 1.,J MW-2 31-Mar-11 MW-2 8-Nov-11 7.6 MW-2 4-Apr-12 0.651 MW-2 6-Nov-12 3.1J MW-2 15-May-13 MW-2 6-Nov-13 1.7J MW-2 9-Apr-14 8.1J 1.31 MW-2 28-0cb14 1.91 MW-2 5-May-15 101 2.71 0.391 MW-2 19-Nov-15 9.1 MW-2 26-Apr-16 2.31 MW-2 17-Nov-16 3.11 MW-2 27-APr-17 1.21 MW-2 26-Sep-17 1.81 MW-2 28-Mar-18 0.66J MW-2 28-Nov-18 0.91 MW-2 2-May-19 MW-4 31-Mar-11 1.31 MW-4 8-Nov-11 2.01 MW-4 4-Apr-12 0.511 0.451 1.91 MW-4 6-Nov-12 2.21 MW-4 15-May-13 0.52J 1.21 1.91 0.321 MW-4 6-Nov-13 2.71 MW-4 9-Apr-14 0.63J 0.651 2.21 0.261 MW-4 28-0ct-14 0.43J 2.41 0.431 MW-4 5-May-15 0.641 0.511 3.51 MW-4 19-Nov-15 0.561 0.321 3.11 0.24J 0.441 MW-4 26-Apr-16 0.501 3.81 MW-4 16-Nov-16 0.521 0.68J 3.71 0.641 0.46J MW-4 28-Apr-17 0.74J 0.731 4.21 0.57J 0.54J MW-4 26 Sep-17 0.42J 3.91 MW-4 28-Mar-18 0.481 3.41 0.471 MW-4 28-Nov-18 0.52 3.8 0.461 0.62 0.43J MW-4 2-May-1 9 0.441 0.50 0.95 1 5.0 1 1 0.59 11 11 11 1 0.52 MW-6 1-Apr-11 1.01 MW-6 9-Nov-11 1.1J MW-6 4-Apr-12 1.4J MW-6 6-Nov-12 1.81 MW-6 15-May-13 0.93J 0.97J 2.7J 0.77J 5.6 5.4 0.24J MW-6 6-Nov-13 3.0J MW-6 9-Apr-14 7.1J 0.60J 0.741 4.7J 0.31J 5.4 4.11 0.52J MW-6 28-OC-14 0.281 0.941 3.2J 0.42J 3.61 2.01 MW-6 5-May-15 0.771 1.21 2.61 7.4 4.5J 1.5J 0.70J MW-6 18-Nov-15 0.741 0.361 0.351 5.01 1.11 MW-6)dup) 18-Nov-15 0.68J 0.371 0.32J 4.8J 1.1J MW-6 27-Apr-16 0.401 0.701 6.2 0.941 MW-6 16-Nov-16 0.42J 1.51 1.2J 0.50J 5.4 1.81 0.71J MW-6 27-Apr-17 1.71 0.911 0.581 5.4 0.771 MW-6 27-Sep-17 0.99J 0.691 3.91 0.42J MW-6)dup) 27-Sep-17 0.931 0.701 3.81 0.521 MW-6 28-Mar-18 1.2 6.2 3.81 1.5 5.9 4.7J 0.83J MW-6)dup) 28-Mar-18 1.1 5.9 3.71 1.5 5.7 4.SJ 0.79J MW-6 28-Nov-18 1.2 4.2 3.5 1.3 5.3 4.0 11 MW-6 2-May-19 1.1 3.4 2.9 1.1 4.8 3.8 13 1 1 6.9 MW-8 30-Mar-11 4.3J 3.8J 1.2 1.5 4.4 MW-8 7-Nov-11 0.52J MW-8 4-Apr-12 3.31 4.1J 2.7J 0.381 0.331 0.55J 0.801 3.6 MW-8 J 19-Jul-12 7.61 0.72J 0.46J MW-8 16-Au9-12 II MW-8 6-Nov-12 0.411 0.60J MW-8 15-May-13 0.81J 0.47J MW-8 31-Jul-13 0.89J 0.72J 0.261 MW-8 6-Nov-13 MW-8 16-Jan-14 0.57J 0.38J MW-8 10-Apr-14 7.4J 0.28J 0.97J MW-8 29-0ct-14 0.591 0.52J 0.31J 0.201 MW-8 7-May-15 111 0.72J 0.40J 0.961 0.30J MW-8 19-Nov-15 0.391 0.75J 0.67J 0.34J 0.221 MW-8 26-Apr-16 1.5J 0.59J MW-8 16-Nov-16 2.71 2.71 1.41 0.481 0.681 MW-8 28-Apr-17 1.2J O.60J 1.2J MW-8 27-Sep-17 0.721 0.63J MW-8 28-Mar-18 MW-8 27-Nov-18 0.86 1 0.43J MW-8 1-May-19 1.1 2.5 6.1 1.8 0.45J 0.84 Smith Page 11 of 18 June 2019 Table 4b Detected Groundwater Constituents - Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 Kul IM MW-9 dup) I 4-Apr-12 I0.421 I 3.61 I I 6,10 46 I 3.3J I 4.0 I I 0.74JI I 4.9 I0471 4.0 I 64 I I 0.94J MW-9 19-Jul-12 140 0.54J 15 2.81 0.441 37 1.6J 4T 0.491 3.3 3.2 0,46 0.83J MW-9 16-Aug-12 120 16 6.0J 41 1.2J 3.9J 0.861 2.4 1.3 MW-9 6-Nov-12 250 0.50J 37J 6.11 21 2.11 0.461 32 21 1.4J 0.42J 3.61 2.8J 0.87J 2.7 2.5 0.61 0.761 0.82J MW-9 15-May-13 0.96J 28J 2.21 0.631 MW-9)dup) 15-May-13 0.98J 281 16 1.41 20 2.5J 2.21 0.54J 0.711 MW-9 31-Jul-13 0.75J 22 3.11 1.91 0.851 MW-9 6-Nov-13 32J 0.73J 4.2J 19 1.51 12 1.7J 0.47J 1.5 MW-9 16-Jan-14 24J 0.57J 19 0.741 4.91 1.6J 0.551 4.1 0.561 MW-9 10-Apr-14 13J 0.71J 20 0.66J 11 0.17J 2.31 1.21 0.51J 2.6 1.4 MW-9)dup) 10-Apr-14 23J 0.601 21 0.59J 18 2.4J 1.21 2.2 1.4 MW-9 29-Oct-14 6.41 0.661 15 0.47J 11 1.4J 0.631 0.411 0.981 MW-9)dup) 29-OC-14 8.91 0.611 16 0.47J 0.431 10 1.3J 0.66J 0.04J 1.09J 1.7 MW-9 7-May-15 1.1 16 1 19 1.61 2.01 1.3 0.91J MW-9 20-Nov-15 0.861 15 0.741 0.61J 11 1.01 0.521 0.431 1.51 0.311 0.891 0.47J MW-9 27-Apr-16 0.961 14 0.74J 14 0.60J O.S11B 0.411 0.781 0.531 MW-9 16-Nov-16 1.3 12 0.771 0.441 7.4 2.2J 0.73J MW-9 27-Apr-17 1.1 13 0.871 12 0.67J 2.OJ 0.40J MW-9 27-Sep-17 1.1 14 0.891 6.9 1.7J 0.441 MW-9 29-Mar-18 1.1 11 0.881 8.7 0.47J 1.01 MW-9 28-Nov-18 1.7 0.55 13 1.4 9.5 0.54 7.7 0.61J MW-9 1-May-19 2.3 1.6 16 2.2 13 0.67 8.7 1.5J MW-10 4-Apr-12 6.4J 4.9 0.351 2.5 0.551 54 2.81 0.381 1.6 0.811 1.41 0.53J 0.511 1.11 4.3 MW-10 19-1ul-12 1 840 220 8.51 30 MW-10 16-Aug-12 5800 1,100 MW-10 6-Nov-12 780D 330D 21D 4.21D MW-10)dup) 6-Nov-12 700D 1.9 33OD 21D 3.91D 0.581 4.6 MW-10 15-May-13 530.0 87J 24 1.91 0.33J 1.31 1.71 0.16) MW-10 31-Jul-13 2.4 18 0.63J 0.401 0.781 0.481 0.25J 20 MW-10 6-Nov-13 2.1 21 1.2 3.01 2.5 MW-10)dup) 6-Nov-13 1.6 18 0.93J 2.41 2.6 MW-10 16-Jan-14 6.6J 2.6 17 1.5 12 1.11 1.1 0.691 0.76J 1.4 2.2 MW-10 10-Apr-14 8.01 2.8 0.311 16 1.7 20 0.221 1.11 1.4 1.3J 0.92J 2.5 4.2 MW-10 29-0ct-14 2.4 0.251 18 1.6 9.0 0.43J 0.27J 0.48J 0.66J 0.391 MW-10 7-May-15 6.6 0.821 23 3.6 68.0 0.48J 1.9J 0.361 2 2.6J 2.91 2.33J 0.27J 4.5 MW-10 20-Nov-15 17J 4.1 1.41 17 0.65J 4.0 46 1.421 0.94J 0.22J 1.1 1.1 2.0J 0.86J 1.1J 0.34J 2.9 MW-10 27-Apr-16 17J 5.6 0.771 27 4.3 44 0AM 0.951 0.94JB 2.9 MW-10 16-Nov-16 2.3J 4.7 0.71J 16 3.7 0,421 31 1,131 0.70J 0.43J 0,671 0.491 0.501 MW-10 27-Apr-17 7.11 2.4 0.40J 9.61 2.8 23 0.401 2.2 MW-10 27-Sep-17 1.2 8.51 1.3 6.5 MW-10 29-Mar-18 1.7 0.411 9.11 1.9 17 1.9 MW-10 28-Nov-18 4.3 1.7 13 4.2 29 0.59 15 1.3 0.76 2.0 2.1 MW-10 1-May-19 3.6J 4.2 3.0 17 4.2 27 0.44J 0.91 19 0.441 0.86 6.0 0.93J 1.6 MW-11 4-Apr-12 MW-11 6-Nov-12 MW-11 15-May-13 MW-11 6-Nov-13 MW-11 10-Apr-14 MW-11 29-OC-14 MW-11 6-May-15 0.55J 0.40J MW-11 20-Nov-15 0.571 MW-11 27-Apr-16 7.3J MW-11 16-Nov-16 MW-11 28-Apr-17 MW-11 28-Sep-17 MW-11 19-Mar-18 MW-11 28-Nov-18 MW-11 2-May-19 0.50 1.0 2.21 L. MW-12 3-Apr-12 MW-12 5-Nov-12 MW-12 15-May-13 MW.12 6-Nov-13 MW-12 10-Apr-14 MW-12 28-Ocb14 MW-12 6-May-15 0.33J MW-12 20-Nov-15 7.81 0.82J MW-12 27-Apr-16 MW-12 17-Nov-16 MW-12 27-Apr-17 MW-12)dup) 27-Apr-17 0.43J MW-12 28-Sep-17 MW-12 29-Mar-18 MW-12 27-Nov-18 5.3 MW.12 1-May-19 0.83 18 Smith Page 12 of 18 June 2019 Table 4b Detected Groundwater Constituents - Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 2.1 15.0 2.0 1.91 MW-13 8-Nov-11 MW-13 3-Apr-12 2.4 17.0 3.0 2.3J MW-13 5-Nov-12 1.6 13.0 2.5 0.521 1.41 MW-13 16-May-13 2.5 18 O.S2J 3.2 2.4J MW-13 7-Nov-13 1.4 12 0.73J 1.71 MW-13 10-Apr-14 1.9 12 2.4 2.1 MW-13 28-OC[-14 1.4 13 2.1 1.31 MW-13 6-May-15 2 13 2.7 2.31 0.28J 0.281 MW-13 20-Nov-15 1.2 9.0 0.631 1.9 1.41 0.321 MW-13 27-Apr-16 1.4 12 2.6 1.4J MW-13 17-Nov-16 0.941 8.3 2.0 0.461 0.96J MW-13 28-Apr-17 1.3 11 2.2 1.01 MW-13 28-Sep-17 1.3 10 2.4 1.21 MW-13 29-Mar-18 0.821 7.7 1.4 0.64J MW-13 27-Nov-18 0.71 6.6 1.5 0.47J 2.8J MW-13 29-Apr-19 0.74 6.8 0.50 1.4 0.63 2.81 MW-13 (dup) 1 29-Apr-19 1 0.76 1 1 6.9 1 1 1 1.3 1 1 1 0.61 1 1 1 3.0 MW-14 7-Nov-11 25J MW-14 3-Apr-12 0.381 0.631 1.21 MW-14 5-Nov-12 0.47J MW-14 16-May-13 0.461 MW-14 7-Nov-13 MW-14 10-Apr-14 0.23J MW-14 28-OC[-14 0.471 0.41J 0.59J 0.191 MW-14 6-May-15 0.40J 0.281 0.611 MW-14)dup) 6-May-15 11J 0.371 0.67J MW-14 20-Nov-15 8.2J 0.441 0.951 1.2 0.711 1.11 0.531 0.22J MW-14 27-Apr-16 0.75J 3.3 1.2 1.41 0.611 MW-14 17-Nov-16 0.651 3.1 0.97J 0.451 0.981 MW-14 28-Apr-17 0.801 0.43J 0.621 MW-14 28-Sep-17 2.2J 1.21 0.50J 0.621 MW-14 29-Mar-18 1.11 MW-14 27-Nov-18 0.76 5.4 1.2 0.401 0.91 0.50 9.9 MW-14)dup) 27-Nov-18 0.83 5.6 1.2 0.93 0.51 9.9 MW-14 29-Apr-19 0.86 6.7 0.40J 1.2 0.87 0.55 8.7 1.3J WZ15 M 8-Nov-11 0.851 15 5-Apr-12 0.59J MW-15 7-Nov-12 0.45J 0.481 0.97J MW-15 16-May-13 0.351 0.69J MW-15 7-Nov-13 1.0J MW-15 8-Apr-14 0.851 0.58J 0.65J MW-15 27-OC-14 1.11 0.681 0.961 MW-15 5-May-15 0.42J 3.1 0.581 1 0.661 0.47J MW-15 18-Nov-15 0.221 1.71 0.871 1.3J 0.541 0.221 MW-15 27-Apr-16 0.34J 5.3 1.5 1.2J 0.50J M W-15 17-Nov-16 1.71 0.741 0.741 MW-15 28-Apr-17 3.2 0.92J 0.56J 0.61J MW-15 28-Sep-17 3.4 0.92J 0.911 MW-15 29-Mar-18 2.81 0.73J 0.57J MW-15 28-Nov-18 0.69 0.58 6.3 MW-15 I 29-Apr-19 2.6 0.481 I L 1 5.4 MW-16 9-Nov-11 1.3 2.31 5.1 4.31 0.931 MW-16 5-Apr-12 21J 1.4 0.531 1.91 1.71 5.6 2.9J 2.0 MW-16 7-Nov-12 34J 1.5 0.561 3.71 3.61 6.8 3.31 5.5 0.35J MW-16 14-May-13 1.3 0.611 2.41 5.2J 7.1 3.3J 5.8 MW-16 5-Nov-13 1.2 2.51 6.5 3.51 2.9 MW-16 8-Apr-14 1.2 0.40J 3.51 3.31 8.3 0.191 3.61 0.92J 4.4 MW-16 27-0C[-14 0.991 0.351 2.7J 2.51 6.2 0.81J 2.71 3.7 MW-16 5-May-15 1.2 0.36J 0.48J 2.5J 7.3 3.5J 1.5J 3.5 0.361 MW-16 3-Nov-15 1.0 1.01 1.91 6.5 0.171 2.81 3.9 0.381 MW-16 27-Apr-16 1.0 0.39J 1.3J 0.26J 7.0 3.3J 2.0 0.491 MW-16 16-Nov-16 1.2 0.991 2.91 6.1 2.81 0.45J 3.4 0.431 MW-16 27-Apr-17 0.911 1.3 1.6J 6.2 3.81 1.7 MW-16 26-Sep-17 0.981 1.41 0.941 5.5 2.61 2.5 MW-16 29-Mar-18 1.3 1.71 2.01 4.0J 0.55J 2.9 5.9 MW-16 28-Nov-18 1.2 2.4 3.7 2.6 MW-16 2-May-19 0.89 1.4 3.0 5.4 2.7 0.51 MW-17 9-NOv-11 5.61 17 2.81 MW-17 5-Apr-12 2.9J 19 2.3J 0.49J MW-17 7-Nov-12 3.61 18 2.71 0.431 MW-17 14-May-13 2 . U 14 2.11 MW-17 6-Nov-13 10 1.3J MW-17 10-Apr-14 6.7J 1.51 10 1.3J MW-17 28-OC[-14 5.31 12 2.11 0.45J MW-17 5-May-15 191 1.01 0.851 14 2.0J 0.411 MW-17 19-Nov-15 7.9J 0.841 0.881 16 0.311 2.71 0.241 0.44J ■ MW-17 26-Apr-16 0.33J 10 1.41 MW-17 17-Nov-16 2.7J 2.4J 9.8 1.41 MW-17 28-Apr-17 1.81 12 1.4J MW-17 26-5ep-17 3.2J 7.1 1.21 MW-17 29-Mar-18 1.81 6.2 0.971 MW-17 28-Nov-18 9.3 1.4 14 MW-17 2-May-19 1.8 7.7 1.1 Smith Page 13 of 18 June 2019 Table 4b Detected Groundwater Constituents - Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-18 31-Mar-11 MW-18 8-Nov-11 MW-18 4-Apr-12 MW-18 6-Nov-12 MW-18 15-May-13 MW-18 6-Nov-13 MW-18 10-Apr-14 MW-18 28-0cb14 MW-18 5-May-15 7.1J 0.521 MW-18 19-Nov-15 7.3J 0.291 MW-18 26-Apr-16 MW-18 16-Nov-16 MW-18 27-Apr-17 MW-18 26-Sep-17 MW-18 28-Mar-18 MW-18 28-Nov-18 10 MW-18 2-May-19 0.471 0.69 MJ MW-19 1-Apr-11 0.641 MW-19 9-Nov-11 MW-19 5-Apr-12 1.01 MW-19 19-1u1-12 4. JJ MW-19 16-Aug-12 MW-19 7-Nov-12 MW-19 36-May-13 230 MW-19 31-Jul-13 MW-19 7-Nov-13 MW-19 16-Jan-14 MW-19 9-Apr-14 MW-19 29-0ct-14 MW-19 7-May-15 12J MW-19 20-Nov-15 MW-19 26-Apr-16 0.33J MW-19 (dup) 26-Apr-16 MW-19 16-Nov-16 0.441 0.691 MW-19 27-Apr-17 0.54J MW-19 27-Sep-17 MW-19 28-Mar-18 MW-19 27-Nov-18 MW-19 I 1-May-19 MW-20 1-Apr-11 MW-20 9-Nov-11 MW-20 5-Apr-12 MW-20 7-Nov-12 MW-20 14-May-13 MW-20 5-Nov-13 MW-20 9-Apr-14 9.3J 0.531 MW-20 28-Oct-14 MW-20 5-May-15 8.7J 0.501 MW-20 19-Nov-15 0.25J MW-20 27-Apr-16 MW-20 17-Nov-16 MW-20 27-Apr-17 2.41 MW-20 27-Sep-17 MW-20 29-Mar-18 MW-20 28-Nov-18 MW-20 2-May-19 0.451 MW-21 31-Mar-11 MW-21 8-Nov-11 MW-21 4-Apr-12 MW-21 6-Nov-12 MW-21 15-May-13 MW-21 6-Nov-13 MW-21 9-Apr-14 MW-21 28-00-14 MW-21 5-May-15 0.64J MW-21 19-Nov-15 MW-21 26-Apr-16 MW-21 16-Nov-16 MW-21 28-Apr-17 MW-21 26-Sep-17 MW-21 28-Mar-18 MW-21 21-Nov-18 MW-21 2-May-19 0.43J Smith Page 14 of 18 June 2019 Table 4b Detected Groundwater Constituents - Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 MW-22 6-Nov-12 MW-22 15-May-13 MW-22 6-Nov-13 MW-22 9-Apr-14 MW-22 28-0ct-14 MW-22 5-May-15 0.971 MW-22 19-Nov-15 MW22 26-Apr-16 MWI 16-Nov-16 MW-22 (dup) 16-Nov-16 MW-22 28-APr-17 MW-22 26-Sep-17 MW-22 28-Mar-18 MW-22 28-Nov-18 MW-22 I 2-May-19 0.43J MW-23 8-Nov-11 MW-23 4-APr-12 MW-23 5-Nov-12 MW-23 15-May-13 MW-23 5-Nov-13 No Sample Collected - Well was Dry MW-23 10-Apr-14 MW-23 27-OC-14 MW-23 5-May-15 0.71J MW-23 19-Nov-15 23J 0.811 MW-23 26-Apr-16 6.0J MW-23 16-Nov-16 15J 0.401 MW-23 28-Apr-17 11J MW-23 26-Sep-17 4.11 MW-23 28-Mar-18 3.11 MW-23 28-Nov-18 MW-23 2-May-19 2.4J MW-24 9-Nov-11 3.3 10 3.4J 3.5 9.9 1.3J MW-24 5-Apr-12 3.0 8.5 3.01 3.5 8.6 1.0J 0.481 .42J MW-24 7-Nov-12 3.2 9.5 3.A 3.2 9.0 MW-24 16-May-13 2.9 7.9 2.5J 3.2 7.8 0.31J 1.11 0.62J 0.421 MW-24 6-Nov-13 2.5 6.4 3.21 2.6 8.8 1.11 MW-24 8-Apr-14 1.4 3.6 2.21 1.7 5.3 0.64J 0.20J MW-24 27-Oct-14 2.6 6.6 2.91 2.3 9.0 1.21 0.431 0.33J MW-24 5-May-15 1.1 2.11 0.481 1.1 4.6J 0.611 1.6J 0.25J MW-24 19-Nov-15 12J 1.4 3.6 1.3 5.0 0.701 0.271 0.211 MW-24 25-Apr-16 7.6J 0.25J 2.01 0.54J MW-24 15-Nov-16 1.0 2.01 0.861 0.841 3.0J MW-24 27-Apr-17 MW-24 26-Sep-17 2.31 2.7 6.3 3.11 2.6 0.941 �56 MW-24 28-Mar-18 1.9 5.2 2.21 1.9 0.66J MW-24 28-Nov-18 0.94 1.8 88 MW-24 2-May-19 3.9 3.2 1.6 1 1 0.91 1 1 120 1 1 1 1 2.6J MW-25 8-Nov-11 1.41 3.2J MW-25 4-Apr-12 0.65J 2.91 4.4J MW-25 6-Nov-12 0.78J 2.31 3.9J MW-25 15-May-13 0.83J 2.3J 1.2J 4.0J MW-25 6-Nov-13 0.87J 3.2J MW-25 9-Apr-14 0.801 2.7J 3.11 MW-25 28-Ocb14 0.871 4.31 2.6J MW-25 5-May-15 1.4 2.11 0.77J 3.71 1.6J MW-25 19-Nov-15 171 1.2 2.7J 0.37J MW-25 26-Apr-16 12J 1.2 2.91 MW-25 16-Nov-16 0.801 1.71 0.471 2.61 MW-25 27-Apr-17 1.41 2.61 MW-25 26-5ep-17 1.41 2.01 MW-25 28-Mar-18 1.5 2.91 2.2J MW-25 28-Nov-18 0.76 1.6 52 MW-25 2-May-19 1.5 3.4 2.0 42 MW-26 8-Nov-11 1.4 0.911 MW-26 4-Apr-12 1.6 0.66J 1.11 1.41 0.49J MW-26 6-Nov-12 1.4 0.47J 0.831 1.11 0.601 MW-26 15-May-13 0.881 0.54J 0.321 0.57J MW-26 6-Nov-13 0.821 MW-26 9-Apr-14 1.5 0.69J 0.33J 1.41 0.661 0.87J MW-26 28-0ct-14 1.5 0.87J 1.91 0.37J 0.97J 0.501 MW-26 5-May-15 16J 1.4 0.77J 0.84J 1.01 0.50J 1.6J 0.21J MW-26 19-Nov-15 14J 1.3 1.11 0.421 0.71J 0.39J 0.32J MW-26 26-Apr-161.4 1.51 0.621 0.701 MW-26 16-Nov-16 3.71 2.4 3.3 2.01 1.9 0.841 0.41J 1.31 MW-26 28-Apr-17 2.1 3.3 2.61 1.9 0.951 0.671 MW-26 26-5ep-17 3.61 2.3 3.2 2.31 2.3 1.11 0.461 0.541 MW-26 28-Mar-18 1.6 2.41 1.5J 1.6 0.80J MW-26 28-Nov-18 2.4J 1.8 1.9 1.4 1.1 ISOD MW-26 2-May-19 3.0J 2.4 2.7 2.0 1.8 1.2 0.51 210D 27 0.43J Smith Page 15 of 18 June 2019 Table 4b Detected Groundwater Constituents - Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 4.11 4.71 1.4 MW-27 31-Mar-11 MW-27 8-Nov-11 1.71 4.41 1.21 0.981 MW-27 4-Apr-12 0.451 3.01 5.8 1.11 1.3 MW-27 6-Nov-12 0.46J 1.4J 5.4 1.31 1.1 MW-27 15-May-13 0.51 2.91 5.5 2.51 0.321 1.41 MW-27 6-Nov-13 S.OJ 5.7 MW-27 9-Apr-14 0.42J 2.31 0.671 0.311 MW-27 28-0ct-14 0.43J 2.OJ 6.1 1.4J 0.261 1.2J MW-27 5-May-15 9.1J 0.54J 0.501 2.81 8.6 1.21 0.381 1.61 MW-27 19-Nov-15 0.511 3.3J 7.8 1.21 0.401 0.27J 0.651 0.371 1.0 MW-27 26-Apr-16 0.441 7.6 1.31 0.37J 0.671 0.881 MW-27 16-Nov-16 7.8 1.51 0.74J 0.48J 0.66J MW-27 28-Apr-17 2.71 4,2J 9.4 1.81 0.40J 0.51J 0.601 MW-27 26-Sep-17 2.71 6.6 8.3 1.41 0.551 MW-27 28-Mar-18 7.0 1.01 0.55J 0.821 MW-27 28-Nov-18 4,3 7.2 1.3 8.8 0.68 1.1 MW-27 30-Apr-19 4.01 0.79 8.3 1.1 8.3 0.491 3.3J MW-28 1-Apr-11 MW-28 9-Nov-11 MW-28 5-Apr-12 MW-28 6-Nov-12 MW-28 15-May-13 MW-28 6-Nov-13 MW-28 9-Apr-14 4.11 MW-28 28-0ct-14 1.2J MW-28 5-May-15 6.9J 8.2 0.44J MW-28 19-Nov-15 1.81 MW-28 26-Apr-16 1.81 0.43J MW-28 16-Nov-16 0.78J MW-28 27-Apr-17 0.531 MW-28 27-Sep-17 MW-28 28-Mar-18 MW-28 28-Nov-18 MW-28 2-May-19 0.41J 3.5 MW-29 4-Mar-11 2.11 1.61 0.95J 19 1.81 0.981 MW-29 1-Apr-11 1.31 1.81 19 1.11 2.5J 1.5 1.2 0.76J 0.611 MW-29 9-Nov-11 2.11 0.89J 23 2.9J 1.0 MW-29(dup) 9-Nov-11 2.01 0.96J 23 3.0J 0.93J MW-29 5-Apr-12 1.5J 1.11 12 0.541 1.21 0.801 0.68J 0.58J MW-29 19-Jul-12 4.6J 0.45J 1.7J 21 2.61 0.81J 0,161 MW-29 16-Aug-12 2.11 20 2.4J 0.831 0.491 MW-29 7-Nov-12 1.4J 0.68J 18 12 0.451 0.491 2.61 0.761 0.51 1.3 r 0.7 61 0.491 MW-29 16-May-13 121 0.271 1.41 1.81 MW-29 31-Jul-13 0.26J 8.81 7 0.78J 2.SJ 1.5 MW-29 7-Nov-13 0.281 3.4J 13 3.0J 0.68J MW-29 16-Jan-14 6.31 0.27J MW-29 9-Apr-14 5.9J 0.891 MW-29 29-OC-14 7.2 1.21 0.36J 0.33J MW-29 6-May-15 9.4J 0.54J 1.7J 1.5J MW-29 20-Nov-15 MW-29 27-Apr-16 1.01 MW-29 17-Nov-16 0.78J 2.1J MW-29 27-Apr-17 5.5J MW-29 27-Sep-17 0.94J 5.5 0.62J MW-29 29-Mar-18 MW-29 28-Nov-18 1 1.5J MW-29 1.May-19 4.1D 3.7D Notes: 1. All units are in micrograms per liter (parts per billion). 2. - Interim Maximum Allowable Concentration (IMAC) 3. NS - No Standard 4. dup - Duplicate Sample 5. J - Indicates the analytical result is an estimated concentration between the laboratory method detection limit and the laboratory limit of quantitation. 6. D - The analyte was run at dilution. Concentration exceeds the 15A NCAC 02L .0202 or IMAC Standard - Indicates the result is below the detection limit - A sodium lactate injection was performed near MW-8, -9, and -10 on June 18-21, 2012. - An emulsified vegetable oil injection was performed near MW-8, -9, and -10 on March 25-27, 2013. Smith Page 16 of 18 June 2019 Table 4c Detected Surface Water Constituents - Metals and Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 North Carolina 2B or Protective Value SW-1 8-Nov-11 43.1 0.1111 2.90.1 5.10J 4.98J SW-1 4-Apr-12 57.1J 3.18JB 1.84J SW-1 6-Nov-12 39.4J SW-1 14-May-13 60J 0.06J 0.4J 0.91 11 0.7.1 0.8J 5JB SW-1 5-Nov-13 0.91 50J 0.6J 3JB 0.7J 4JB SW-1 9-Apr-14 40J 0.91 0.4J 2J 0.6.1 0.8J 5J 7JB 8.1J SW-1 28-Oct-14 40J 0.4JB 0.4J 0.6J 0.6J SW-1 5-May-15 40J 0.4J 11 0.2J 0.7J 3JB 0.73J SW-1 19-Nov-15 2J 70J 0.2J 0.5.1 3J 2J 4.1 3J 2J 1J 13J 16 SW-1 26-Apr-16 0.7J 40J 0.3J 11 0.3J 0.6J 3J SW-1 16-Nov-16 0.24J 0.73J 56J 0.28J 1.2J 1.11 1.91 SW-1 28-Apr-17 40J 1.6J 0.45.1 3.3J 3.1 SW-1 26-Sep-17 DRY SW-1 29-Mar-18 45J 1.3J 3.91 0.31J 4.1J SW-1 28-Nov-18 48J 1.3J 0.25J 3.4J SW-1 30-Apr-19 42J 1.6J 0.40J SW-2 8-Nov-11 3.63J 55.8J 0.165J 3.42.1 6.80J 12.3 SW-2 4-Apr-12 69.4J 2.66JB 2.04J 5.75J SW-2 6-Nov-12 3.37J 76.9J 2.30J 9.18J SW-2 14-May-13 11 801 0.11 11 2J 2J 2J 2J 3J 10B 0.21J SW-2 5-Nov-13 60J 0.11 11 0.61 3JB 0.81 11 7J 11B SW-2 8-Apr-14 0.6J 50J 11 0.61 2J 11 0.8J 6J 11B SW-2 27-Oct-14 30J 0.3JB 0.21 11 0.3J 5J SW-2 5-May-15 60J 0.21 11 0.81 0.3J 0.7J 25 0.6J SW-2 18-Nov-15 0.2J 70J 0.041 0.81 0.51 11 0.3J 0.7J 11 13 SW-2 25-Apr-16 DRY SW-2 17-Nov-16 0.34J 1.5J 130 0.20J 0.052J 3.5J 1.8J 5.4JB 4.2.1 2.8J 8.9J 23 2.8J SW-2 28-Apr-17 66J 1.5J 1.0.1 1.5J 4.0J 6.8J I SW-2 26-Sep-17 DRY SW-2 29-Mar-18 DRY SW-2 28-Nov-18 I I 50J I I I I I I 0.37J I I I I I 6.2J SW-2 30-Apr-19 DRY Smith Page 17 of 18 June 2019 Table 4c Detected Surface Water Constituents - Metals and Volatile Organic Compounds April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 North Carolina 2B or Protective Value SW-3 8-Nov-11 3.991 52.21 0.1411 2.361 3.50JB 8.01J 7.55J SW-3 4-Apr-12 46.71 2.88JB SW-3 6-Nov-12 41.51 1.62J SW-3 15-May-13 0.61 40J 0.31 0.81 0.2J 0.51 216 SW-3 5-Nov-13 0.61 40J 0.61 0.41 2113 0.4J 11 3J 616 SW-3 8-Apr-14 50J 0.051 11 0.71 21 11 11 6J 10B SW-3 27-Oct-14 40J 0.41E 0.51 0.71 0.2J 0.71 2.113 SW-3 5-May-15 0.8.1 40J 0.31 0.51 11 0.3J 0.71 416 0.94J SW-3 18-Nov-15 50J 0.41 0.61 11 0.2J 0.81 3J SW-3 26-Apr-16 40J 0.31 0.41 11 0.4J 0.71 4.113 SW-3 16-Nov-16 0.451 38J 0.931 0.19J 0.771 2.0J SW-3 28-Apr-17 41J 0.16J 1.61 0.68J 3.6J 4.6J 2.4J SW-3 26-Sep-17 DRY SW-3 28-Mar-18 47J 1.31 1.91 0.44J 5.2J SW-3 28-Nov-18 51J 1.3J 0.25J 3.2J SW-3 30-Apr-19 1.5J 6.1J 170 0.17J 7.5J 6.4J 6.8J 6.5J 6.9J 17J 38 8.1J 0.46J Notes: 1. All units are in micrograms per liter (parts per billion). 2. (2) - A Standard for total chromium has not been established. The value provided is for chromium (III). 3. NS - No Standard 4. * - North Carolina Protective Value 5. J - Indicates the analytical result is an estimated concentration between the laboratory method detection limit and the laboratory limit of quantitation. 6. B - The amount in the prep blank is greater than the method detection limit. Concentration exceeds the North Carolina 15A NCAC 02B or Protective Value Freshwater Aquatic Life Standard for Class C Waters - September 2017 Indicates the result is below the detection limit Smith Page 18 of 18 June 2019 Table 5 Constituents Detected Above Standards April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County Permit Number 9203-MSWLF-1980 PERMIT 9203-MSWLF-1980 MONITORINGFACILITY .D MW-2 APRIL 2019 PARAMETERS EXCEEDING THE NORTH CAROLINA 2L OR ALLOWABLENUMBER INTERIM MAXIMUM .. Cobalt*, Vanadium* 9203-MSW LF-1980 M W-4 Vanadium* 9203-MSWLF-1980 MW-6 Barium, Cobalt*, Benzene, 1,4-Dioxane, Vinyl Chloride 9203-MSWLF-1980 MW-8 Chromium, Cobalt*, Sodium*, Vanadium*, 1,1-Dichloroethane, Tetrachloroethene 9203-MSW LF-1980 M W-9 Barium, Cobalt*, Sodium*, Vanadium*, Total Dissolved Solids, Benzene, 1,1-Dichloroethane, 1,4-Dioxane 9203-MSWLF-1980 MW-10 Arsenic, Barium, Cobalt, Sodium*, Total Dissolved Solids, Benzene, 1,1-Dichloroethane, 1,2-Dichloroethane, 1,4-Dioxane, Vinyl Chloride 9203-MSWLF-1980 MW-11 Cobalt*, Vanadium* 9203-MSWLF-1980 MW-12 Cobalt*, 1,4-Dioxane 9203-MSWLF-1980 MW-13 Cobalt* 9203-MSWLF-1980 MW-14 Cobalt*, Mercury, Vanadium*, 1,4-Dioxane 9203-MSWLF-1980 MW-15 Cobalt*, 1,4-Dioxane 9203-MSWLF-1980 MW-16 Arsenic, Cobalt* 9203-MSWLF-1980 MW-17 Arsenic, Cobalt*, Vanadium*, 1,1-Dichloroethane, 1,4-Dioxane 9203-MSWLF-1980 MW-18 Vanadium* 9203-MSWLF-1980 MW-19 Cobalt*, Sodium*, Vanadium* 9203-MSWLF-1980 MW-20 Vanadium* 9203-MSWLF-1980 MW-21 Cobalt*, Vanadium* 9203-MSWLF-1980 MW-22 Arsenic, Cobalt* 9203-MSWLF-1980 MW-23 Cobalt*, Vanadium* 9203-MSWLF-1980 MW-24 Cobalt*, Vanadium*, Benzene, 1,4-Dioxane 9203-MSWLF-1980 MW-25 Barium, Benzene, 1,4-Dioxane 9203-MSWLF-1980 MW-26 Cobalt*, Benzene, 1,4-Dioxane 9203-MSWLF-1980 MW-27 Arsenic, Cobalt*, Vanadium*, 1,1-Dichloroethane, 1,4-Dioxane 9203-MSWLF-1980 MW-28 Vanadium* 9203-MSWLF-1980 MW-29 Cobalt*, Vanadium*, Total Dissolved Solids Notes: 1. Bold - "J" flag 2. (*) - Interim Maximum Allowable Concentration Smith Page 1 of 1 June 2019 MW-8 Total Detected VOCs 160 140 120 : 100 40 20 oi<-)�<0 �O °�1 oil �'b�'boi��°500000'yO,'OLOl O�ObONORO�O<O�00�00101 O00O4 R) C5 y0ti0 yytiy,Lyl tib�btiR�R y� yh y� y� y1 y1 y'b y� y� Date Note: Acetone was omitted as it is a common laboratory contaminant. Figure 2 April 2019 Semi -Annual Sampling Event Smith Feltonsville Landfill - Wake County MW-9 Total Detected VOCs 180 160 140 120 KII 20 �� �� 0pl�0 ��0 �1 �� Cab �� pI� �� �� �ti �ti �� �ti ��J Q�J �� Q�X (� (� �A Date Note: Acetone was omitted as it is a common laboratory contaminant. Figure 3 April 2019 Semi -Annual Sampling Event Smith Feltonsville Landfill - Wake County M 400 300 u d d to a+ O H 200 100 MW-10 Total Detected VOCs C!� 9�) C � �� C1 p1 C� 9� C� 9� l� �, Q;111 Q �� �D� �� �� ��O 0�0 �1 Date Note: Acetone was omitted as it is a common laboratory contaminant. Figure 4 April 2019 Semi -Annual Sampling Event Smith Feltonsville Landfill - Wake County 20 18 16 14 Q 12 U O RV 4 2 CI7 MW-12 Total Detected VOCs ' I Ln cn 1 0 ; o l c1 N N , _ 1 - , U i N 'A1 1 N U U p i 1 , Ln c 1 , 1 I i 1 1 U , , ( 1 1 I , 1 � 1 1 1 1 I 1 1 , � , , I 1 , , � , 1 , I , � , 1 , I , I , I , , 1 , I , I , , I , 1 , I , I , , 1 , , I , , I , 1 , 1 , � , 1 , 1 , � , 1 , 1 � , 1 , 1 , I , 1 , 1 , I , , I , 1 , 1 , I , 1 , 1 , I I , 1 , , 1 , � , 1 , 1 , 1 1 1 1 I I I ���R�h����°��°�1 �1'b�'b����0000OyOyOLOLO'�O3ORO�O�O�O�O�Oo1 01 O'bO'bO�O°� y0ti0 yytiy yL yl y'�ti� yIN y� y� y� y(0 y(0 fity1�Y. Q� �Y. Q� �Y. Q� �Y� Date Note: Acetone was omitted as it is a common laboratory contaminant. smith Figure 5 April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County MW-13 Total Detected VOCs 30 25 20 10 C!� C� C� �� �� C� �AC� C� C� C� �� �� �� Q� �� �� �� �� �� �� �� �h (� �O (A '' Date Note: Acetone was omitted as it is a common laboratory contaminant. Figure 6 April 2019 Semi -Annual Sampling Event Smith Feltonsville Landfill - Wake County 25 20 a 15 H r 10 O H 5 Fil MW-14 Total Detected VOCs 0 I Ln I �' rn o o rn o N i N � O I O i C i U U i O i C i E 02, i U N n i N i O U N i LO-0. L.L C� CO C0�\ CC'bC'bC� C�00000,O�OlOIO�O�ORO�O�O�O�00�0010A0'bO4'O°�O°�y0y0ytiytiyl yl y1y5yt yb y�yhy�Oy(Oy1 y1 y'by'byC ' Q� Date Note: Acetone was omitted as it is a common laboratory contaminant. smith Figure 7 April 2019 Semi -Annual Sampling Event Feltonsville Landfill - Wake County MW-15 Total Detected VOCs 18 16 14 12 C!� C� C� �� �� �� �A�� C� C� C� �� �� �� Q� �� �� �� �� �� �� �� �� (� �O (A ' c� '' Date Note: Acetone was omitted as it is a common laboratory contaminant. Figure 8 April 2019 Semi -Annual Sampling Event Smith Feltonsville Landfill - Wake County MW-16 Total Detected VOCs 30 25 20 10 C!� C� �� �� �� �ACb C� C� C� �� �� �� Q� �� �� �� �� �� �� �� �h (� �O (A ' c� '' Date Note: Acetone was omitted as it is a common laboratory contaminant. Figure 9 April 2019 Semi -Annual Sampling Event Smith Feltonsville Landfill - Wake County MW-29 Total Detected VOCs 35 30 25 a a u 20 t -0 15 10 y1-Y y y'y ,y y'y y'-Y 'IV 11, yL 1)) lb y'S ,'3 y05 y'S yR y� y� ytx tx tx y< yh) 4) � yh ti(0 (0 (O ti(o y(O y�o y1 y1 y1 y1 y1 y1 yob y4� yob y4� yob ti� ti� y°� Date Note: Acetone was omitted as it is a common laboratory contaminant. Figure 10 April 2019 Semi -Annual Sampling Event Smith Feltonsville Landfill - Wake County Appendix A Analytical Data SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis CDM Smith 5400 Glenwood Avenue Suite 400 Raleigh, NC 27612 Attention: Mathew Colone Project Name: Feltonsville Landfill Lot Number:UD30018 Date Completed:05/17/2019 Revision Date: 05/17/2019 06/13/2019 9:56 AM Approved and released by: Project Manager: Cathy S. Dover AM A C C R E D I T E D 4t'0'0'/ 11 000 EIAP The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 286 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative CDM Smith Lot Number: UD30018 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. This pdf report was revised to include sodium (Na) results for MW-9 (UD30018-032), MW-10 (UD30018033) and MW-29 (UD30018-035) that were inadvertently left off of the original report. VOA 8260D Due to analyst error, sample UD30018-010 (MW-29) was inadvertently analyzed at a 5x dilution and 1x (neat) analysis was needed . They accidently misidentified the sample as needing a dilution when checking the historical data. The LOQ reported is elevated to reflect the dilution. BOD The seed correction factor was above the method range of 0.6 to 1.0 (SCF = 1.11) and reported with " 7" flag. Results may be biased low for associated samples UD30018-001 (MW-13) and UD30018-002 (MW-14). The lab group leader investigated the issue and they found that the vendor seed vials that were supposed to have 6 ml had varied amounts. The issue was caught after the 48 hour holding time had expired for these two samples. The vendor has been contacted and we are working on resolution. No sample dilutions resulted in a depletion of at least 2.0 mg/L for sample UD30018-002 (MW-14). The reported BOD/CBOD value is 0 mg/L, which was computed using the lowest BOD/CBOD value that can be calculated with the available data. COD approximate values were used to determine sample dilutions. The data have been 6-flagged accordingly. Nitrate-N 300.0 The re -analysis at 10x dilution of samples UD30018-007 (MW-10) and UD30018-008 (MW-12) were performed outside of the analytical holding time. The original analysis and the 1 Ox analysis are both reported. Dissolved Gases RSK175 The following samples had an air bubble in the sample vials > 6mmfor re -analysis: UD30018-005 (MW-8), UD30018-006 (MW-9), and UD30018-007 (MW-10). If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 286 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 286 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary CDM Smith Lot Number: UD30018 Project Name: Feltonsville Landfill Project Number: Sample Number Sample ID Matrix Date Sampled Date Received 001 MW-13 Aqueous 04/29/20191130 04/30/2019 002 MW-14 Aqueous 04/29/20191250 04/30/2019 003 MW-15 Aqueous 04/29/20191420 04/30/2019 004 DUP Aqueous 04/29/2019 0800 04/30/2019 005 MW-8 Aqueous 05/01/2019 0900 05/02/2019 006 MW-9 Aqueous 05/01/20191000 05/02/2019 007 MW-10 Aqueous 05/01/20191110 05/02/2019 008 MW-12 Aqueous 05/01/20191530 05/02/2019 009 MW-19 Aqueous 05/01/20191230 05/02/2019 010 MW-29 Aqueous 05/01/20191400 05/02/2019 011 EQ BLANK Aqueous 04/30/2019 1545 05/02/2019 012 TRIP BLANK Aqueous 04/30/2019 05/02/2019 013 MW-2 Aqueous 05/02/20191720 05/03/2019 014 MW-4 Aqueous 05/02/20191355 05/03/2019 015 MW-6 Aqueous 05/02/20191600 05/03/2019 016 MW-11 Aqueous 05/02/20191655 05/03/2019 017 MW-16 Aqueous 05/02/20191245 05/03/2019 018 MW-17 Aqueous 05/02/20191705 05/03/2019 019 MW-18 Aqueous 05/02/20191615 05/03/2019 020 MW-20 Aqueous 05/02/20191630 05/03/2019 021 MW-21 Aqueous 05/02/20191500 05/03/2019 022 MW-22 Aqueous 05/02/20191335 05/03/2019 023 MW-23 Aqueous 05/02/20191315 05/03/2019 024 MW-24 Aqueous 05/02/20191425 05/03/2019 025 MW-25 Aqueous 05/02/20191435 05/03/2019 026 MW-26 Aqueous 05/02/20191515 05/03/2019 027 MW-27 Aqueous 04/30/20191820 05/03/2019 028 MW-28 Aqueous 05/02/20191540 05/03/2019 029 TRIP BLANK2 Aqueous 04/30/2019 05/03/2019 030 SW-1 Aqueous 04/30/20191520 05/03/2019 031 SW-3 Aqueous 04/30/20191430 05/03/2019 032 MW-9 Aqueous 05/02/20191640 05/03/2019 033 MW-10 Aqueous 05/02/20191645 05/03/2019 034 MW-12 Aqueous 05/02/20191530 05/03/2019 035 MW-29 Aqueous 05/02/20191650 05/03/2019 (35 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-001 Description: MW-13 Matrix: Aqueous Date Sampled:04/29/2019 1130 Project Name: Feltonsville Landfill Date Received: 04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/02/2019 0212 KFE 15392 1 (BOD, 5 day) SM 521OB-2011 1 05/05/2019 1154 HET 04/30/2019 1036 12671 1 (Chloride) 300.0 1 04/30/2019 1949 HKL 15202 1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2019 0212 MSG 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 04/30/2019 1949 HKL 15201 1 (Sulfate) 300.0 1 04/30/2019 1949 HKL 15200 1 (Sulfide) SM 4500-S2 F-2011 1 04/30/2019 2009 HET 15230 1 (TOC) SM 531 OC-2011 1 05/02/2019 0416 DMA 15351 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 200 20 20 mg/L 1 BOD, 5 day SM 521013- 2.0 U7 2.0 0.18 mg/L 1 Chloride 300.0 35 1.0 0.20 mg/L 1 CO2 (calculation) 124-38-9 SM 4500-CO2 490 27 27 mg/L 1 COD SM 5220D- 20 U 20 20 mg/L 1 Nitrate - N 300.0 0.083 0.020 0.0050 mg/L 1 Sulfate 300.0 8.3 1.0 0.20 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 TOC SM 5310C- 5.6 1.0 1.0 mg/L 1 Footnote(s): 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-001 Description: MW-13 Matrix: Aqueous Date Sampled:04/29/2019 1130 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/02/2019 1409 JJG 15469 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 2.8 J 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 Footnote(s): 7-SCF Out of range 124 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-001 Description: MW-13 Matrix: Aqueous Date Sampled:04/29/2019 1130 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191416 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.74 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 6.8 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 1.4 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.63 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 Footnote(s): 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-001 Description: MW-13 Matrix: Aqueous Date Sampled:04/29/2019 1130 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191416 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 Footnote(s): 7-SCF Out of range 101 70-130 100 70-130 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-001 Description: MW-13 Matrix: Aqueous Date Sampled:04/29/2019 1130 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2318 JJG 16314 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 120 10 2.5 ug/L 1 Footnote(s): 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-001 Description: MW-13 Matrix: Aqueous Date Sampled:04/29/2019 1130 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191616 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00040 0.00020 0.000091 mg/L 1 Footnote(s): 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-001 Description: MW-13 Matrix: Aqueous Date Sampled:04/29/2019 1130 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191503 BNW Prep Date Batch 05/02/20191704 15483 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.3 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 450 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.19 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 7.3 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 5.7 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 26 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 33 10 2.5 ug/L 1 Footnote(s): 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 11 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-002 Description: MW-14 Matrix: Aqueous Date Sampled:04/29/2019 1250 Project Name: Feltonsville Landfill Date Received: 04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/02/2019 0217 KFE 15392 1 (BOD, 5 day) SM 521OB-2011 1 05/05/2019 1154 HET 04/30/2019 1036 12671 1 (Chloride) 300.0 1 04/30/2019 2005 HKL 15202 1 (CO2 (calcula) SM 4500-CO2 D 1 05/02/2019 0217 MSG 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 04/30/2019 2005 HKL 15201 1 (Sulfate) 300.0 1 04/30/2019 2005 HKL 15200 1 (Sulfide) SM 4500-S2 F-2011 1 04/30/2019 2009 HET 15230 1 (TOC) SM 531 OC-2011 1 05/02/2019 0433 DMA 15351 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 230 20 20 mg/L 1 BOD, 5 day SM 521013- 30 U76 30 2.7 mg/L 1 Chloride 300.0 98 1.0 0.20 mg/L 1 CO2 (calculation) 124-38-9 SM 4500-CO2 890 27 27 mg/L 1 COD SM 5220D- 20 U 20 20 mg/L 1 Nitrate - N 300.0 0.020 U 0.020 0.0050 mg/L 1 Sulfate 300.0 2.2 1.0 0.20 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 TOC SM 5310C- 2.3 1.0 1.0 mg/L 1 Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-002 Description: MW-14 Matrix: Aqueous Date Sampled:04/29/2019 1250 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/02/2019 1434 JJG 15469 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 8.7 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 120 40-170 Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 13 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-002 Description: MW-14 Matrix: Aqueous Date Sampled:04/29/2019 1250 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191442 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.86 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 6.7 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.40 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 1.2 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.87 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.55 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 1.3 J 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 14 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-002 Description: MW-14 Matrix: Aqueous Date Sampled:04/29/2019 1250 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191442 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 97 70-130 100 70-130 104 70-130 Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 15 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-002 Description: MW-14 Matrix: Aqueous Date Sampled:04/29/2019 1250 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2111 JJG 16314 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 690 10 2.5 ug/L 1 Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 16 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-002 Description: MW-14 Matrix: Aqueous Date Sampled:04/29/2019 1250 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191628 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.0016 0.00020 0.000091 mg/L 1 Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 17 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-002 Description: MW-14 Matrix: Aqueous Date Sampled:04/29/2019 1250 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191509 BNW Prep Date Batch 05/02/20191704 15483 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 0.81 J 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 250 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.34 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 4.8 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 2.1 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 4.5 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 21 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 5.6 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 5.5 J 10 2.5 ug/L 1 Footnote(s): 6-D.O. depletion < 2.00 mg/L 7-SCF Out of range LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 18 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-003 Description: MW-15 Matrix: Aqueous Date Sampled:04/29/2019 1420 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/02/2019 1458 JJG 15469 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 5.4 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 122 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 19 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-003 Description: MW-15 Matrix: Aqueous Date Sampled:04/29/2019 1420 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191507 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 2.6 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.48 J 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 20 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-003 Description: MW-15 Matrix: Aqueous Date Sampled:04/29/2019 1420 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191507 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 97 70-130 101 70-130 106 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 21 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-003 Description: MW-15 Matrix: Aqueous Date Sampled:04/29/2019 1420 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191631 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 22 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-003 Description: MW-15 Matrix: Aqueous Date Sampled:04/29/2019 1420 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191515 BNW Prep Date Batch 05/02/20191704 15483 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 220 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.32 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 1.4 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 2.9 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 10 U 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 27 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 3.1 J 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 23 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-004 Description: DUP Matrix: Aqueous Date Sampled:04/29/2019 0800 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/02/2019 1523 JJG 15469 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 120 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 24 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-004 Description: DUP Matrix: Aqueous Date Sampled:04/29/2019 0800 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191532 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.76 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 6.9 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 1.3 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.61 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 25 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-004 Description: DUP Matrix: Aqueous Date Sampled:04/29/2019 0800 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191532 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 99 70-130 100 70-130 105 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 26 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-004 Description: DUP Matrix: Aqueous Date Sampled:04/29/2019 0800 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191633 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00037 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 27 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-004 Description: DUP Matrix: Aqueous Date Sampled:04/29/2019 0800 Project Name: Feltonsville Landfill Date Received:04/30/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191602 BNW Prep Date Batch 05/02/20191704 15483 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.4 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 490 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.17 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 7.9 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 5.8 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 27 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 36 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 28 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-005 Description: MW-8 Matrix: Aqueous Date Sampled:05/01/2019 0900 Project Name: Feltonsville Landfill Date Received: 05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/09/2019 0056 KFE 16220 1 (BOD, 5 day) SM 521OB-2011 1 05/07/2019 1201 MGM 05/02/2019 1600 12675 1 (Chloride) 300.0 1 05/02/2019 2134 HKL 15614 1 (CO2 (calcula) SM 4500-CO2 D 1 05/09/2019 0056 KFE 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 05/02/2019 2134 HKL 15610 1 (Sulfate) 300.0 1 05/02/2019 2134 HKL 15613 1 (Sulfide) SM 4500-S2 F-2011 1 05/07/2019 2048 HET 15976 1 (TDS) SM 2540C-2011 1 05/02/2019 1824 MGM 15419 1 (TOC) SM 531OC-2011 1 05/06/2019 1950 DMA 15800 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 260 20 20 mg/L 1 BOD, 5 day SM 521013- 2.0 U 2.0 0.18 mg/L 1 Chloride 300.0 7.2 1.0 0.20 mg/L 1 CO2 (calculation) 124-38-9 SM 4500-CO2 410 27 27 mg/L 1 COD SM 5220D- 20 U 20 20 mg/L 1 Nitrate - N 300.0 0.066 0.020 0.0050 mg/L 1 Sulfate 300.0 0.69 J 1.0 0.20 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 TDS SM 2540C- 160 25 25 mg/L 1 TOC SM 5310C- 1.0 U 1.0 1.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 29 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-005 Description: MW-8 Matrix: Aqueous Date Sampled:05/01/2019 0900 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0046 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 114 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 30 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-005 Description: MW-8 Matrix: Aqueous Date Sampled:05/01/2019 0900 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191557 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 1.1 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 2.5 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 6.1 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 1.8 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.45 J 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 1.2 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 31 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-005 Description: MW-8 Matrix: Aqueous Date Sampled:05/01/2019 0900 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191557 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.84 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 98 70-130 100 70-130 105 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 32 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-005 Description: MW-8 Matrix: Aqueous Date Sampled:05/01/2019 0900 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2127 JJG 16314 2 RSK - 175 10 05/10/2019 1917 JJG 16503 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 5600 D 100 25 ug/L 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 33 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-005 Description: MW-8 Matrix: Aqueous Date Sampled:05/01/2019 0900 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191636 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 34 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-005 Description: MW-8 Matrix: Aqueous Date Sampled:05/01/2019 0900 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191608 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 210 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 13 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 19 10 1.3 ug/L 1 Copper 7440-50-8 6020B 6.3 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.38 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 84 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Sodium 7440-23-5 6020B 21000 400 150 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 5.0 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 4.3 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 35 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-006 Description: MW-9 Matrix: Aqueous Date Sampled:05/01/2019 1000 Project Name: Feltonsville Landfill Date Received: 05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/09/2019 0104 KFE 16220 1 (BOD, 5 day) SM 521OB-2011 1 05/07/2019 1201 MGM 05/02/2019 1600 12675 1 (Chloride) 300.0 1 05/02/2019 2222 HKL 15614 1 (CO2 (calcula) SM 4500-CO2 D 1 05/09/2019 0104 KFE 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 05/02/2019 2222 HKL 15610 1 (Sulfate) 300.0 1 05/02/2019 2222 HKL 15613 1 (Sulfide) SM 4500-S2 F-2011 1 05/07/2019 2048 HET 15976 1 (TDS) SM 2540C-2011 1 05/02/2019 1824 MGM 15419 1 (TOC) SM 531 OC-2011 1 05/06/2019 2008 DMA 15800 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 470 20 20 mg/L 1 BOD, 5 day SM 5210B- 19 2.0 0.18 mg/L 1 Chloride 300.0 75 1.0 0.20 mg/L 1 CO2 (calculation) 124-38-9 SM 4500-CO2 1300 27 27 mg/L 1 COD SM 5220D- 30 20 20 mg/L 1 Nitrate - N 300.0 0.020 U 0.020 0.0050 mg/L 1 Sulfate 300.0 0.46 J 1.0 0.20 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 TDS SM 2540C- 580 25 25 mg/L 1 TOC SM 5310C- 10 1.0 1.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 36 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-006 Description: MW-9 Matrix: Aqueous Date Sampled:05/01/2019 1000 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0111 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 8.7 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 124 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 37 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-006 Description: MW-9 Matrix: Aqueous Date Sampled:05/01/2019 1000 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191622 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 2.3 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 1.6 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 16 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 2.2 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 13 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.67 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 1.5 J 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 38 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-006 Description: MW-9 Matrix: Aqueous Date Sampled:05/01/2019 1000 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191622 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 99 70-130 102 70-130 104 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 39 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-006 Description: MW-9 Matrix: Aqueous Date Sampled:05/01/2019 1000 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2142 JJG 16314 2 RSK - 175 10 05/10/2019 1933 JJG 16503 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 9.3 J 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 13000 D 100 25 ug/L 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 40 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-007 Description: MW-10 Matrix: Aqueous Date Sampled:05/01/2019 1110 Project Name: Feltonsville Landfill Date Received: 05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/09/2019 0117 KFE 16220 1 (BOD, 5 day) SM 521OB-2011 1 05/07/2019 1201 MGM 05/02/2019 1600 12675 1 (Chloride) 300.0 1 05/02/2019 2238 HKL 15614 1 (CO2 (calcula) SM 4500-CO2 D 1 05/09/2019 0117 KFE 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 05/02/2019 2238 HKL 15610 2 (Nitrate - N) 300.0 10 05/14/2019 0012 SLU 16582 1 (Sulfate) 300.0 1 05/02/2019 2238 HKL 15613 1 (Sulfide) SM 4500-S2 F-2011 1 05/07/2019 2048 HET 15976 1 (TDS) SM 2540C-2011 1 05/02/2019 1824 MGM 15419 1 (TOC) SM 531 OC-2011 1 05/06/2019 2025 DMA 15800 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320113- 440 20 20 mg/L 1 BOD, 5 day SM 5210113- 9.4 2.0 0.18 mg/L 1 Chloride 300.0 160 1.0 0.20 mg/L 1 CO2 (calculation) 124-38-9 SM 4500-CO2 1500 27 27 mg/L 1 COD SM 5220113- 79 20 20 mg/L 1 Sulfate 300.0 11 1.0 0.20 mg/L 1 Nitrate - N 300.0 0.020 U 0.020 0.0050 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 Nitrate - N 300.0 0.20 UH 0.20 0.050 mg/L 2 TDS SM 2540C- 670 25 25 mg/L 1 TOC SM 5310C- 23 1.0 1.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 41 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-007 Description: MW-10 Matrix: Aqueous Date Sampled:05/01/2019 1110 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0135 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 19 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 122 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 42 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-007 Description: MW-10 Matrix: Aqueous Date Sampled:05/01/2019 1110 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191648 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 3.6 J 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 4.2 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 3.0 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 17 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 4.2 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 27 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.44 J 0.50 0.40 ug/L 1 1, 1 -Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.91 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.44 J 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.86 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 6.0 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 43 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-007 Description: MW-10 Matrix: Aqueous Date Sampled:05/01/2019 1110 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191648 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 1.6 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 0.93 J 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 100 70-130 100 70-130 106 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 44 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-007 Description: MW-10 Matrix: Aqueous Date Sampled:05/01/2019 1110 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2158 JJG 16314 2 RSK - 175 10 05/10/2019 1950 JJG 16503 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 5400 D 100 25 ug/L 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 45 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-008 Description: MW-12 Matrix: Aqueous Date Sampled:05/01/2019 1530 Project Name: Feltonsville Landfill Date Received: 05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/09/2019 0126 KFE 16220 1 (BOD, 5 day) SM 521OB-2011 1 05/07/2019 1201 MGM 05/02/2019 1600 12675 2 (Chloride) 300.0 10 05/10/2019 1239 SLU 16330 1 (CO2 (calcula) SM 4500-CO2 D 1 05/09/2019 0126 KFE 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 05/02/2019 2255 HKL 15610 2 (Nitrate - N) 300.0 10 05/10/2019 1239 SLU 16331 1 (Sulfate) 300.0 1 05/02/2019 2255 HKL 15613 1 (Sulfide) SM 4500-S2 F-2011 1 05/07/2019 2048 HET 15976 1 (TOC) SM 531 OC-2011 1 05/06/2019 2042 DMA 15800 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 740 20 20 mg/L 1 BOD, 5 day SM 521013- 2.0 U 2.0 0.18 mg/L 1 Chloride 300.0 270 D 10 2.0 mg/L 2 CO2 (calculation) 124-38-9 SM 4500-CO2 940 27 27 mg/L 1 COD SM 5220113- 21 20 20 mg/L 1 Sulfate 300.0 34 1.0 0.20 mg/L 1 Nitrate - N 300.0 0.020 U 0.020 0.0050 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 Nitrate - N 300.0 0.20 UH 0.20 0.050 mg/L 2 TOC SM 5310C- 6.4 1.0 1.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 46 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-008 Description: MW-12 Matrix: Aqueous Date Sampled:05/01/2019 1530 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0200 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 18 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 122 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 47 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-008 Description: MW-12 Matrix: Aqueous Date Sampled:05/01/2019 1530 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191713 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.83 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 48 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-008 Description: MW-12 Matrix: Aqueous Date Sampled:05/01/2019 1530 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191713 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 97 70-130 99 70-130 106 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 49 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-008 Description: MW-12 Matrix: Aqueous Date Sampled:05/01/2019 1530 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2214 JJG 16314 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 22 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 50 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-009 Description: MW-19 Matrix: Aqueous Date Sampled:05/01/2019 1230 Project Name: Feltonsville Landfill Date Received: 05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/09/2019 0133 KFE 16220 1 (BOD, 5 day) SM 521OB-2011 1 05/07/2019 1201 MGM 05/02/2019 1600 12675 1 (Chloride) 300.0 1 05/02/2019 2311 HKL 15614 1 (CO2 (calcula) SM 4500-CO2 D 1 05/09/2019 0133 KFE 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 05/02/2019 2311 HKL 15610 1 (Sulfate) 300.0 1 05/02/2019 2311 HKL 15613 1 (Sulfide) SM 4500-S2 F-2011 1 05/07/2019 2048 HET 15976 1 (TDS) SM 2540C-2011 1 05/02/2019 1824 MGM 15419 1 (TOC) SM 531 OC-2011 1 05/06/2019 2059 DMA 15800 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 150 20 20 mg/L 1 BOD, 5 day SM 521013- 2.0 U 2.0 0.18 mg/L 1 Chloride 300.0 13 1.0 0.20 mg/L 1 CO2 (calculation) 124-38-9 SM 4500-CO2 190 27 27 mg/L 1 COD SM 5220D- 20 U 20 20 mg/L 1 Nitrate - N 300.0 0.059 0.020 0.0050 mg/L 1 Sulfate 300.0 5.3 1.0 0.20 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 TDS SM 2540C- 170 25 25 mg/L 1 TOC SM 5310C- 1.0 U 1.0 1.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 51 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-009 Description: MW-19 Matrix: Aqueous Date Sampled:05/01/2019 1230 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0224 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 112 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 52 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-009 Description: MW-19 Matrix: Aqueous Date Sampled:05/01/2019 1230 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191739 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 53 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-009 Description: MW-19 Matrix: Aqueous Date Sampled:05/01/2019 1230 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191739 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 95 70-130 103 70-130 100 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 54 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-009 Description: MW-19 Matrix: Aqueous Date Sampled:05/01/2019 1230 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2230 JJG 16314 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 10 U 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 55 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-009 Description: MW-19 Matrix: Aqueous Date Sampled:05/01/2019 1230 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191638 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 56 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-009 Description: MW-19 Matrix: Aqueous Date Sampled:05/01/2019 1230 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191614 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.6 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 210 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 4.3 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 1.9 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 2.3 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 1.1 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 7.9 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Sodium 7440-23-5 6020B 32000 400 150 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 7.1 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 6.4 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 57 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-010 Description: MW-29 Matrix: Aqueous Date Sampled:05/01/2019 1400 Project Name: Feltonsville Landfill Date Received: 05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/09/2019 0138 KFE 16220 1 (BOD, 5 day) SM 521OB-2011 1 05/07/2019 1201 MGM 05/02/2019 1600 12675 1 (Chloride) 300.0 1 05/02/2019 2327 HKL 15614 1 (CO2 (calcula) SM 4500-CO2 D 1 05/09/2019 0138 KFE 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 05/02/2019 2327 HKL 15610 1 (Sulfate) 300.0 1 05/02/2019 2327 HKL 15613 1 (Sulfide) SM 4500-S2 F-2011 1 05/07/2019 2048 HET 15976 1 (TDS) SM 2540C-2011 1 05/02/2019 1824 MGM 15419 1 (TOC) SM 531 OC-2011 1 05/06/2019 2116 DMA 15800 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 120 20 20 mg/L 1 BOD, 5 day SM 5210B- 2.2 2.0 0.18 mg/L 1 Chloride 300.0 24 1.0 0.20 mg/L 1 CO2 (calculation) 124-38-9 SM 4500-CO2 470 27 27 mg/L 1 COD SM 522013- 37 20 20 mg/L 1 Nitrate - N 300.0 0.020 U 0.020 0.0050 mg/L 1 Sulfate 300.0 3.8 1.0 0.20 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 TDS SM 2540C- 570 25 25 mg/L 1 TOC SM 5310C- 9.7 1.0 1.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 58 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-010 Description: MW-29 Matrix: Aqueous Date Sampled:05/01/2019 1400 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0249 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 125 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 59 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-010 Description: MW-29 Matrix: Aqueous Date Sampled:05/01/2019 1400 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 5 05/03/2019 2037 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 50 U 50 10 ug/L 1 Acrylonitrile 107-13-1 8260D 25 U 25 4.0 ug/L 1 Benzene 71-43-2 8260D 2.5 U 2.5 2.0 ug/L 1 Bromochloromethane 74-97-5 8260D 2.5 U 2.5 2.0 ug/L 1 Bromodichloromethane 75-27-4 8260D 2.5 U 2.5 2.0 ug/L 1 Bromoform 75-25-2 8260D 2.5 U 2.5 2.0 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 2.5 U 2.5 2.0 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 50 U 50 10 ug/L 1 Carbon disulfide 75-15-0 8260D 2.5 U 2.5 2.0 ug/L 1 Carbon tetrachloride 56-23-5 8260D 2.5 U 2.5 2.0 ug/L 1 Chlorobenzene 108-90-7 8260D 2.5 U 2.5 2.0 ug/L 1 Chloroethane 75-00-3 8260D 4.1 D 2.5 2.0 ug/L 1 Chloroform 67-66-3 8260D 2.5 U 2.5 2.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 2.5 U 2.5 2.0 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 2.5 U 2.5 2.0 ug/L 1 Dibromochloromethane 124-48-1 8260D 2.5 U 2.5 2.0 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 2.5 U 2.5 2.0 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 2.5 U 2.5 2.0 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 10 U 10 2.0 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 2.5 U 2.5 2.0 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 2.5 U 2.5 2.0 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 2.5 U 2.5 2.0 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 3.7 D 2.5 2.0 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 2.5 U 2.5 2.0 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 2.5 U 2.5 2.0 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 2.5 U 2.5 2.0 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 2.5 U 2.5 2.0 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 2.5 U 2.5 2.0 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 2.5 U 2.5 2.0 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 2.5 U 2.5 2.0 ug/L 1 Ethylbenzene 100-41-4 8260D 2.5 U 2.5 2.0 ug/L 1 2-Hexanone 591-78-6 8260D 50 U 50 10 ug/L 1 Methacrylonitrile 126-98-7 8260D 25 U 25 10 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 25 U 25 2.0 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 50 U 50 10 ug/L 1 Methylene chloride 75-09-2 8260D 2.5 U 2.5 2.0 ug/L 1 Styrene 100-42-5 8260D 2.5 U 2.5 2.1 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 2.5 U 2.5 2.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 2.5 U 2.5 2.0 ug/L 1 Tetrachloroethene 127-18-4 8260D 2.5 U 2.5 2.0 ug/L 1 Tetrahydrofuran 109-99-9 8260D 25 U 25 5.0 ug/L 1 Toluene 108-88-3 8260D 2.5 U 2.5 2.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 2.5 U 2.5 2.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 2.5 U 2.5 2.0 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 60 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-010 Description: MW-29 Matrix: Aqueous Date Sampled:05/01/2019 1400 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 5 05/03/2019 2037 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 2.5 U 2.5 2.0 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 2.5 U 2.5 2.0 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 2.5 U 2.5 2.0 ug/L 1 Vinyl acetate 108-05-4 8260D 25 U 25 5.8 ug/L 1 Vinyl chloride 75-01-4 8260D 2.5 U 2.5 2.0 ug/L 1 Xylenes (total) 1330-20-7 8260D 5.0 U 5.0 2.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 93 70-130 102 70-130 101 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 61 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-010 Description: MW-29 Matrix: Aqueous Date Sampled:05/01/2019 1400 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2246 JJG 16314 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 300 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 62 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-011 Description: EQ BLANK Matrix: Aqueous Date Sampled:04/30/2019 1545 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0313 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 124 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 63 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-011 Description: EQ BLANK Matrix: Aqueous Date Sampled:04/30/2019 1545 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191237 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 5.0 J 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 4.4 J 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.44 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 64 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-011 Description: EQ BLANK Matrix: Aqueous Date Sampled:04/30/2019 1545 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191237 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 97 70-130 98 70-130 100 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 65 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-011 Description: EQ BLANK Matrix: Aqueous Date Sampled:04/30/2019 1545 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191641 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 66 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-011 Description: EQ BLANK Matrix: Aqueous Date Sampled:04/30/2019 1545 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191620 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 100 U 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 U 10 1.3 ug/L 1 Copper 7440-50-8 6020B 10 U 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 50 U 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 10 U 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 67 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-012 Description: TRIP BLANK Matrix: Aqueous Date Sampled:04/30/2019 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/13/2019 2347 KGT 16570 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 127 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 68 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-012 Description: TRIP BLANK Matrix: Aqueous Date Sampled:04/30/2019 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191302 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.41 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 69 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-012 Description: TRIP BLANK Matrix: Aqueous Date Sampled:04/30/2019 Project Name: Feltonsville Landfill Date Received:05/02/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/03/20191302 JM1 15632 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 97 70-130 98 70-130 104 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 70 of 286 Inorganic non-metals Client:CDM Smith Laboratory ID:UD30018-013 Description: MW-2 Matrix: Aqueous Date Sampled:05/02/2019 1720 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 (Alkalinity) SM 2320B-2011 1 05/09/2019 0158 KFE 16220 1 (BOD, 5 day) SM 521OB-2011 1 05/08/2019 1715 MGM 05/03/2019 2049 12678 2 (Chloride) 300.0 10 05/10/2019 1255 SLU 16330 1 (CO2 (calcula) SM 4500-CO2 D 1 05/09/2019 0158 KFE 1 (COD) SM 5220D-2011 1 05/14/2019 2230 HET 16694 1 (Nitrate - N) 300.0 1 05/04/2019 0340 HKL 15769 1 (Sulfate) 300.0 1 05/04/2019 0340 HKL 15770 1 (Sulfide) SM 4500-S2 F-2011 1 05/07/2019 2048 HET 15976 1 (TOC) SM 531 OC-2011 1 05/06/2019 2134 DMA 15800 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Alkalinity SM 2320B- 170 20 20 mg/L 1 BOD, 5 day SM 5210B- 2.9 2.0 0.18 mg/L 1 Chloride 300.0 540 D 10 2.0 mg/L 2 CO2 (calculation) 124-38-9 SM 4500-CO2 180 27 27 mg/L 1 COD SM 5220113- 23 20 20 mg/L 1 Nitrate - N 300.0 0.081 0.020 0.0050 mg/L 1 Sulfate 300.0 33 1.0 0.20 mg/L 1 Sulfide 18496-25-8 SM 4500-S2 F- 1.0 U 1.0 0.99 mg/L 1 TOC SM 5310C- 2.4 1.0 1.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 71 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-013 Description: MW-2 Matrix: Aqueous Date Sampled:05/02/2019 1720 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0338 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 115 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 72 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-013 Description: MW-2 Matrix: Aqueous Date Sampled:05/02/2019 1720 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191452 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 73 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-013 Description: MW-2 Matrix: Aqueous Date Sampled:05/02/2019 1720 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191452 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 94 70-130 94 70-130 101 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 74 of 286 Dissolved Gases Client:CDM Smith Laboratory ID:UD30018-013 Description: MW-2 Matrix: Aqueous Date Sampled:05/02/2019 1720 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 RSK - 175 1 05/09/2019 2302 JJG 16314 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Ethane 74-84-0 RSK - 175 10 U 10 2.5 ug/L 1 Ethene 74-85-1 RSK - 175 10 U 10 2.5 ug/L 1 Methane 74-82-8 RSK - 175 10 U 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 75 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-013 Description: MW-2 Matrix: Aqueous Date Sampled:05/02/2019 1720 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191644 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 76 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-013 Description: MW-2 Matrix: Aqueous Date Sampled:05/02/2019 1720 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191626 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 170 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 2.5 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 1.3 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 1.7 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 4.5 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 2.4 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 1.5 J 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 13 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 14 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 77 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-014 Description: MW-4 Matrix: Aqueous Date Sampled:05/02/2019 1355 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0402 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 105 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 78 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-014 Description: MW-4 Matrix: Aqueous Date Sampled:05/02/2019 1355 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191517 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.44 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.95 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 5.0 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.59 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.52 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 79 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-014 Description: MW-4 Matrix: Aqueous Date Sampled:05/02/2019 1355 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191517 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 96 70-130 98 70-130 102 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 80 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-014 Description: MW-4 Matrix: Aqueous Date Sampled:05/02/2019 1355 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191646 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 81 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-014 Description: MW-4 Matrix: Aqueous Date Sampled:05/02/2019 1355 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191632 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.3 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 40 J 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 2.3 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 U 10 1.3 ug/L 1 Copper 7440-50-8 6020B 10 U 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.54 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 50 U 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 3.5 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 4.0 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 82 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-015 Description: MW-6 Matrix: Aqueous Date Sampled:05/02/2019 1600 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0427 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 13 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 116 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 83 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-015 Description: MW-6 Matrix: Aqueous Date Sampled:05/02/2019 1600 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191541 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 1.1 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 3.4 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 2.9 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 1.1 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 4.8 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 3.8 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 6.9 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 84 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-015 Description: MW-6 Matrix: Aqueous Date Sampled:05/02/2019 1600 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191541 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 2.1 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 98 70-130 99 70-130 105 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 85 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-015 Description: MW-6 Matrix: Aqueous Date Sampled:05/02/2019 1600 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191654 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 86 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-015 Description: MW-6 Matrix: Aqueous Date Sampled:05/02/2019 1600 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191650 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.3 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 800 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.28 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 13 10 1.3 ug/L 1 Copper 7440-50-8 6020B 2.1 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 23 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 11 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 87 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-016 Description: MW-11 Matrix: Aqueous Date Sampled:05/02/2019 1655 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0451 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 2.2 J 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 113 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 88 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-016 Description: MW-11 Matrix: Aqueous Date Sampled:05/02/2019 1655 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191606 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 1.0 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 1.0 J 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 89 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-016 Description: MW-11 Matrix: Aqueous Date Sampled:05/02/2019 1655 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191606 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 95 70-130 99 70-130 104 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 90 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-016 Description: MW-11 Matrix: Aqueous Date Sampled:05/02/2019 1655 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191656 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 91 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-016 Description: MW-11 Matrix: Aqueous Date Sampled:05/02/2019 1655 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191655 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 2.9 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 170 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.18 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 1.5 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 6.0 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 2.4 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 1.2 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 6.9 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 4.4 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 15 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 92 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-017 Description: MW-16 Matrix: Aqueous Date Sampled:05/02/2019 1245 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0516 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 106 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 93 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-017 Description: MW-16 Matrix: Aqueous Date Sampled:05/02/2019 1245 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191631 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.89 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 1.4 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 3.0 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 5.4 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 2.7 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.51 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 94 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-017 Description: MW-16 Matrix: Aqueous Date Sampled:05/02/2019 1245 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191631 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 2.6 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 92 70-130 99 70-130 99 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 95 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-017 Description: MW-16 Matrix: Aqueous Date Sampled:05/02/2019 1245 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191659 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 96 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-017 Description: MW-16 Matrix: Aqueous Date Sampled:05/02/2019 1245 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191701 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 12 10 1.3 ug/L 1 Barium 7440-39-3 6020B 210 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.13 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 3.8 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 4.1 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.49 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 6.3 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 5.8 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 97 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-018 Description: MW-17 Matrix: Aqueous Date Sampled:05/02/2019 1705 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0540 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 13 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 110 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 98 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-018 Description: MW-17 Matrix: Aqueous Date Sampled:05/02/2019 1705 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191657 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 1.8 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 7.7 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 1.1 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 99 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-018 Description: MW-17 Matrix: Aqueous Date Sampled:05/02/2019 1705 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191657 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 96 70-130 98 70-130 101 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 100 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-018 Description: MW-17 Matrix: Aqueous Date Sampled:05/02/2019 1705 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191701 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 101 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-018 Description: MW-17 Matrix: Aqueous Date Sampled:05/02/2019 1705 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191707 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 10 1.3 ug/L 1 Barium 7440-39-3 6020B 160 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.30 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 7.8 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 5.5 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 11 10 1.3 ug/L 1 Lead 7439-92-1 6020B 5.7 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 13 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 16 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 30 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 102 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-019 Description: MW-18 Matrix: Aqueous Date Sampled:05/02/2019 1615 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0605 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 2.8 J 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 110 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 103 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-019 Description: MW-18 Matrix: Aqueous Date Sampled:05/02/2019 1615 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191722 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.47 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.69 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 104 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-019 Description: MW-18 Matrix: Aqueous Date Sampled:05/02/2019 1615 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191722 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 100 70-130 102 70-130 108 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 105 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-019 Description: MW-18 Matrix: Aqueous Date Sampled:05/02/2019 1615 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191704 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 106 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-019 Description: MW-18 Matrix: Aqueous Date Sampled:05/02/2019 1615 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191713 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.8 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 100 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 1.5 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 U 10 1.3 ug/L 1 Copper 7440-50-8 6020B 2.0 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.36 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 7.8 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 2.7 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 5.3 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 107 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-020 Description: MW-20 Matrix: Aqueous Date Sampled:05/02/2019 1630 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0629 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 126 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 108 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-020 Description: MW-20 Matrix: Aqueous Date Sampled:05/02/2019 1630 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191747 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.45 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 109 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-020 Description: MW-20 Matrix: Aqueous Date Sampled:05/02/2019 1630 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191747 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 96 70-130 99 70-130 103 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 110 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-020 Description: MW-20 Matrix: Aqueous Date Sampled:05/02/2019 1630 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191706 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 111 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-020 Description: MW-20 Matrix: Aqueous Date Sampled:05/02/2019 1630 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191719 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 2.3 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 130 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 1.9 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 U 10 1.3 ug/L 1 Copper 7440-50-8 6020B 10 U 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.26 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 3.9 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 4.5 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 5.2 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 112 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-021 Description: MW-21 Matrix: Aqueous Date Sampled:05/02/2019 1500 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0653 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 110 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 113 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-021 Description: MW-21 Matrix: Aqueous Date Sampled:05/02/2019 1500 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191812 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.43 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 114 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-021 Description: MW-21 Matrix: Aqueous Date Sampled:05/02/2019 1500 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191812 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 95 70-130 97 70-130 103 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 115 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-021 Description: MW-21 Matrix: Aqueous Date Sampled:05/02/2019 1500 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191709 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 116 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-021 Description: MW-21 Matrix: Aqueous Date Sampled:05/02/2019 1500 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191725 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 3.0 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 55 J 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 5.5 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 1.7 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 5.1 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 4.0 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 3.9 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 9.2 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 13 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 117 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-022 Description: MW-22 Matrix: Aqueous Date Sampled:05/02/2019 1335 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0718 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 116 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 118 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-022 Description: MW-22 Matrix: Aqueous Date Sampled:05/02/2019 1335 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191838 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.43 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 119 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-022 Description: MW-22 Matrix: Aqueous Date Sampled:05/02/2019 1335 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191838 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 95 70-130 104 70-130 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 120 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-022 Description: MW-22 Matrix: Aqueous Date Sampled:05/02/2019 1335 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191711 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 121 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-022 Description: MW-22 Matrix: Aqueous Date Sampled:05/02/2019 1335 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191731 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 19 10 1.3 ug/L 1 Barium 7440-39-3 6020B 440 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 1.4 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 8.1 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 1.5 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.43 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 4.9 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 6.7 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 122 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-023 Description: MW-23 Matrix: Aqueous Date Sampled:05/02/2019 1315 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0743 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 114 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 123 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-023 Description: MW-23 Matrix: Aqueous Date Sampled:05/02/2019 1315 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191903 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 2.4 J 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 124 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-023 Description: MW-23 Matrix: Aqueous Date Sampled:05/02/2019 1315 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191903 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 98 70-130 100 70-130 105 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 125 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-023 Description: MW-23 Matrix: Aqueous Date Sampled:05/02/2019 1315 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191714 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 126 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-023 Description: MW-23 Matrix: Aqueous Date Sampled:05/02/2019 1315 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191737 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.3 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 280 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 2.1 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 10 U 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 2.9 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 3.1 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 10 U 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 127 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-024 Description: MW-24 Matrix: Aqueous Date Sampled:05/02/2019 1425 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0807 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 120 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 118 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 128 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-024 Description: MW-24 Matrix: Aqueous Date Sampled:05/02/2019 1425 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191928 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 2.0 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 3.9 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 3.2 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 1.6 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 5.6 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.91 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 2.6 J 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 129 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-024 Description: MW-24 Matrix: Aqueous Date Sampled:05/02/2019 1425 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191928 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 99 70-130 98 70-130 103 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 130 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-024 Description: MW-24 Matrix: Aqueous Date Sampled:05/02/2019 1425 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191716 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 131 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-024 Description: MW-24 Matrix: Aqueous Date Sampled:05/02/2019 1425 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191743 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 6.6 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 130 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.15 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 3.2 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 3.8 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 3.1 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 1.7 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 11 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 7.7 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 20 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 132 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-025 Description: MW-25 Matrix: Aqueous Date Sampled:05/02/2019 1435 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 0831 STM 16388 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 42 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 119 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 133 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-025 Description: MW-25 Matrix: Aqueous Date Sampled:05/02/2019 1435 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191953 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 1.5 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 3.4 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 2.0 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 134 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-025 Description: MW-25 Matrix: Aqueous Date Sampled:05/02/2019 1435 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191953 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 100 70-130 101 70-130 108 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 135 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-025 Description: MW-25 Matrix: Aqueous Date Sampled:05/02/2019 1435 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191724 JMH 05/05/20191238 15674 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 136 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-025 Description: MW-25 Matrix: Aqueous Date Sampled:05/02/2019 1435 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191801 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 1.7 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 900 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.44 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 U 10 1.3 ug/L 1 Copper 7440-50-8 6020B 1.3 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 12 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 2.5 J 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 3.2 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 137 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-026 Description: MW-26 Matrix: Aqueous Date Sampled:05/02/2019 1515 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 5030B 8260B (SIM) 5 05/14/2019 0035 KGT 16570 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 210 D 15 5.0 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 121 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 138 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-026 Description: MW-26 Matrix: Aqueous Date Sampled:05/02/2019 1515 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2017 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 3.0 J 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 2.4 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 2.7 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 2.0 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 1.8 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 1.2 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis-1,2-Dichloroethene 156-59-2 8260D 0.51 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 27 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 139 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-026 Description: MW-26 Matrix: Aqueous Date Sampled:05/02/2019 1515 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2017 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 0.43 J 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 105 70-130 105 70-130 109 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 140 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-026 Description: MW-26 Matrix: Aqueous Date Sampled:05/02/2019 1515 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191525 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 141 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-026 Description: MW-26 Matrix: Aqueous Date Sampled:05/02/2019 1515 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191807 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 220 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 0.79 J 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.24 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 34 10 1.3 ug/L 1 Copper 7440-50-8 6020B 2.7 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.27 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 13 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 2.3 J 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 25 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 142 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-027 Description: MW-27 Matrix: Aqueous Date Sampled:04/30/2019 1820 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 5030B 8260B (SIM) 1 05/14/2019 0011 KGT 16570 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 8.3 3.0 1.0 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 121 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 143 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-027 Description: MW-27 Matrix: Aqueous Date Sampled:04/30/2019 1820 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2042 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 4.0 J 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.79 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 8.3 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 1.1 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.49 J 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 3.3 J 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 144 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-027 Description: MW-27 Matrix: Aqueous Date Sampled:04/30/2019 1820 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2042 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 100 70-130 101 70-130 107 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 145 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-027 Description: MW-27 Matrix: Aqueous Date Sampled:04/30/2019 1820 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191532 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 146 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-027 Description: MW-27 Matrix: Aqueous Date Sampled:04/30/2019 1820 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191813 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 13 10 1.3 ug/L 1 Barium 7440-39-3 6020B 220 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.13 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 9.2 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 10 1.3 ug/L 1 Copper 7440-50-8 6020B 16 10 1.3 ug/L 1 Lead 7439-92-1 6020B 6.3 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 16 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 11 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 38 B 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 147 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-028 Description: MW-28 Matrix: Aqueous Date Sampled:05/02/2019 1540 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 1443 STM 16406 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 123 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 148 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-028 Description: MW-28 Matrix: Aqueous Date Sampled:05/02/2019 1540 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2107 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.41 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 3.5 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 149 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-028 Description: MW-28 Matrix: Aqueous Date Sampled:05/02/2019 1540 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2107 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 94 70-130 100 70-130 102 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 150 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-028 Description: MW-28 Matrix: Aqueous Date Sampled:05/02/2019 1540 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191535 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 151 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-028 Description: MW-28 Matrix: Aqueous Date Sampled:05/02/2019 1540 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191819 BNW Prep Date Batch 05/06/20191734 15809 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 250 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.14 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 U 10 1.3 ug/L 1 Copper 7440-50-8 6020B 10 U 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 1.5 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 2.6 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 3.9 BJ 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 152 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-029 Description: TRIP BLANK2 Matrix: Aqueous Date Sampled:04/30/2019 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 1509 STM 16406 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 123 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 153 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-029 Description: TRIP BLANK2 Matrix: Aqueous Date Sampled:04/30/2019 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191427 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 154 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-029 Description: TRIP BLANK2 Matrix: Aqueous Date Sampled:04/30/2019 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/20191427 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 100 70-130 98 70-130 105 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 155 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-030 Description: SWA Matrix: Aqueous Date Sampled:04/30/2019 1520 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 1533 STM 16406 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 119 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 156 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-030 Description: SW-1 Matrix: Aqueous Date Sampled:04/30/2019 1520 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2131 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 10 U 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.40 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 157 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-030 Description: SW-1 Matrix: Aqueous Date Sampled:04/30/2019 1520 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2131 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 96 70-130 102 70-130 106 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 158 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-030 Description: SW-1 Matrix: Aqueous Date Sampled:04/30/2019 1520 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191538 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 159 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-030 Description: SW-1 Matrix: Aqueous Date Sampled:04/30/2019 1520 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191912 BNW Prep Date Batch 05/06/20191734 15810 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 10 U 10 1.3 ug/L 1 Barium 7440-39-3 6020B 42 J 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 10 U 10 1.3 ug/L 1 Copper 7440-50-8 6020B 1.6 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 50 U 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 10 U 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 160 of 286 Volatile Organic Compounds by GC/MS (SIM) Client:CDM Smith Laboratory ID:UD30018-031 Description: SW-3 Matrix: Aqueous Date Sampled:04/30/2019 1430 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260B (SIM) 1 05/11/2019 1558 STM 16406 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run 1,4-Dioxane 123-91-1 8260B (SIM) 3.0 U 3.0 1.0 ug/L 1 Run Acceptance Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 129 40-170 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 161 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-031 Description: SW-3 Matrix: Aqueous Date Sampled:04/30/2019 1430 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2156 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Acetone 67-64-1 8260D 8.1 J 10 2.0 ug/L 1 Acrylonitrile 107-13-1 8260D 5.0 U 5.0 0.80 ug/L 1 Benzene 71-43-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromochloromethane 74-97-5 8260D 0.50 U 0.50 0.40 ug/L 1 Bromodichloromethane 75-27-4 8260D 0.50 U 0.50 0.40 ug/L 1 Bromoform 75-25-2 8260D 0.50 U 0.50 0.40 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 8260D 0.50 U 0.50 0.40 ug/L 1 2-Butanone (MEK) 78-93-3 8260D 10 U 10 2.0 ug/L 1 Carbon disulfide 75-15-0 8260D 0.50 U 0.50 0.40 ug/L 1 Carbon tetrachloride 56-23-5 8260D 0.50 U 0.50 0.40 ug/L 1 Chlorobenzene 108-90-7 8260D 0.50 U 0.50 0.40 ug/L 1 Chloroethane 75-00-3 8260D 0.46 J 0.50 0.40 ug/L 1 Chloroform 67-66-3 8260D 0.50 U 0.50 0.40 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromo-3-chloropropane (DBCP) 96-12-8 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromochloromethane 124-48-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dibromoethane (EDB) 106-93-4 8260D 0.50 U 0.50 0.40 ug/L 1 Dibromomethane (Methylene bromide) 74-95-3 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,4-Dichloro-2-butene 110-57-6 8260D 2.0 U 2.0 0.40 ug/L 1 1,2-Dichlorobenzene 95-50-1 8260D 0.50 U 0.50 0.40 ug/L 1 1,4-Dichlorobenzene 106-46-7 8260D 0.50 U 0.50 0.40 ug/L 1 Dichlorodifluoromethane 75-71-8 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethane 75-34-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloroethane 107-06-2 8260D 0.50 U 0.50 0.40 ug/L 1 1,1-Dichloroethene 75-35-4 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,2-Dichloroethene 156-59-2 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,2-Dichloroethene 156-60-5 8260D 0.50 U 0.50 0.40 ug/L 1 1,2-Dichloropropane 78-87-5 8260D 0.50 U 0.50 0.40 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 8260D 0.50 U 0.50 0.40 ug/L 1 trans- 1,3-Dichloropropene 10061-02-6 8260D 0.50 U 0.50 0.40 ug/L 1 Ethylbenzene 100-41-4 8260D 0.50 U 0.50 0.40 ug/L 1 2-Hexanone 591-78-6 8260D 10 U 10 2.0 ug/L 1 Methacrylonitrile 126-98-7 8260D 5.0 U 5.0 2.0 ug/L 1 Methyl iodide (lodomethane) 74-88-4 8260D 5.0 U 5.0 0.40 ug/L 1 4-Methyl-2-pentanone 108-10-1 8260D 10 U 10 2.0 ug/L 1 Methylene chloride 75-09-2 8260D 0.50 U 0.50 0.40 ug/L 1 Styrene 100-42-5 8260D 0.50 U 0.50 0.41 ug/L 1 1,1,1,2-Tetrachloroethane 630-20-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrachloroethene 127-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Tetrahydrofuran 109-99-9 8260D 5.0 U 5.0 1.0 ug/L 1 Toluene 108-88-3 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,1-Trichloroethane 71-55-6 8260D 0.50 U 0.50 0.40 ug/L 1 1,1,2-Trichloroethane 79-00-5 8260D 0.50 U 0.50 0.40 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 162 of 286 Volatile Organic Compounds by GC/MS Client:CDM Smith Laboratory ID:UD30018-031 Description: SW-3 Matrix: Aqueous Date Sampled:04/30/2019 1430 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 5030B 8260D 1 05/06/2019 2156 JM1 15794 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Trichloroethene 79-01-6 8260D 0.50 U 0.50 0.40 ug/L 1 Trichlorofluoromethane 75-69-4 8260D 0.50 U 0.50 0.40 ug/L 1 1,2,3-Trichloropropane 96-18-4 8260D 0.50 U 0.50 0.40 ug/L 1 Vinyl acetate 108-05-4 8260D 5.0 U 5.0 1.2 ug/L 1 Vinyl chloride 75-01-4 8260D 0.50 U 0.50 0.40 ug/L 1 Xylenes (total) 1330-20-7 8260D 1.0 U 1.0 0.40 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 1,2-Dichloroethane-d4 Toluene-d8 99 70-130 102 70-130 106 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 163 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-031 Description: SW-3 Matrix: Aqueous Date Sampled:04/30/2019 1430 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191540 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 164 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-031 Description: SW-3 Matrix: Aqueous Date Sampled:04/30/2019 1430 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191918 BNW Prep Date Batch 05/06/20191734 15810 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 1.5 J 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 6.1 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 170 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 0.17 J 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 7.5 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 6.4 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 6.8 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 6.5 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 6.9 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 17 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 38 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 165 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-032 Description: MW-9 Matrix: Aqueous Date Sampled:05/02/2019 1640 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191543 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 166 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-032 Description: MW-9 Matrix: Aqueous Date Sampled:05/02/2019 1640 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191924 BNW Prep Date Batch 05/06/20191734 15810 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 4.6 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 1400 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.14 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 10 U 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 25 10 1.3 ug/L 1 Copper 7440-50-8 6020B 7.2 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 4.6 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 57 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Sodium 7440-23-5 6020B 32000 400 150 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 4.7 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 9.7 J 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 167 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-033 Description: MW-10 Matrix: Aqueous Date Sampled:05/02/2019 1645 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191545 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 168 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-033 Description: MW-10 Matrix: Aqueous Date Sampled:05/02/2019 1645 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191930 BNW Prep Date Batch 05/06/20191734 15810 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 26 10 1.3 ug/L 1 Barium 7440-39-3 6020B 1100 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 1.4 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 44 10 1.3 ug/L 1 Copper 7440-50-8 6020B 1.6 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 10 U 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 61 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 1.3 J 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Sodium 7440-23-5 6020B 110000 400 150 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 4.6 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 6.9 J 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 169 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-034 Description: MW-12 Matrix: Aqueous Date Sampled:05/02/2019 1530 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191553 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 170 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-034 Description: MW-12 Matrix: Aqueous Date Sampled:05/02/2019 1530 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191936 BNW Prep Date Batch 05/06/20191734 15810 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 5.2 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 290 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 1.0 U 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 1.8 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 1.3 J 10 1.3 ug/L 1 Copper 7440-50-8 6020B 10 U 10 1.3 ug/L 1 Lead 7439-92-1 6020B 0.34 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 4.3 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 2.0 J 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 25 U 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 7.8 J 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 171 of 286 CVAA Client:CDM Smith Laboratory ID:UD30018-035 Description: MW-29 Matrix: Aqueous Date Sampled:05/02/2019 1650 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 7470A 1 05/06/20191555 JMH 05/05/20191242 15676 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Mercury 7439-97-6 7470A 0.00020 U 0.00020 0.000091 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 172 of 286 ICP-MS Metals Client:CDM Smith Laboratory ID:UD30018-035 Description: MW-29 Matrix: Aqueous Date Sampled:05/02/2019 1650 Project Name: Feltonsville Landfill Date Received:05/03/2019 Project Number: Run Prep Method 1 3005A Analytical Method Dilution Analysis Date Analyst 6020B 1 05/08/20191942 BNW Prep Date Batch 05/06/20191734 15810 CAS Analytical Parameter Number Method Result Q LOQ DL Units Run Antimony 7440-36-0 6020B 6.0 U 6.0 0.50 ug/L 1 Arsenic 7440-38-2 6020B 3.3 J 10 1.3 ug/L 1 Barium 7440-39-3 6020B 130 100 1.3 ug/L 1 Beryllium 7440-41-7 6020B 1.0 U 1.0 0.15 ug/L 1 Cadmium 7440-43-9 6020B 0.16 J 1.0 0.13 ug/L 1 Chromium 7440-47-3 6020B 5.3 J 10 1.3 ug/L 1 Cobalt 7440-48-4 6020B 11 10 1.3 ug/L 1 Copper 7440-50-8 6020B 4.1 J 10 1.3 ug/L 1 Lead 7439-92-1 6020B 1.9 J 10 0.25 ug/L 1 Nickel 7440-02-0 6020B 14 J 50 1.3 ug/L 1 Selenium 7782-49-2 6020B 10 U 10 1.3 ug/L 1 Silver 7440-22-4 6020B 10 U 10 0.25 ug/L 1 Sodium 7440-23-5 6020B 13000 400 150 ug/L 1 Thallium 7440-28-0 6020B 5.5 U 5.5 0.15 ug/L 1 Vanadium 7440-62-2 6020B 5.4 J 25 2.5 ug/L 1 Zinc 7440-66-6 6020B 13 10 2.5 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit U = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL H = Out of holding time W = Reported on wet weight basis D = Dilution > 1 Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 173 of 286 QC Summary Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 174 of 286 Inorganic non-metals - MB Sample ID: UQ15200-001 Matrix: Aqueous Batch: 15200 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Sulfate 1.0 U 1 1.0 0.20 mg/L 04/30/20191844 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 175 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15200-002 Matrix: Aqueous Batch: 15200 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfate 20 20 1 99 90-110 04/30/20191723 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 176 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15201-001 Matrix: Aqueous Batch: 15201 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Nitrate - N 0.020 U 1 0.020 0.0050 mg/L 04/30/2019 1844 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 177 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15201-002 Matrix: Aqueous Batch: 15201 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Nitrate - N 0.80 0.87 1 109 90-110 04/30/2019 1723 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 178 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15202-001 Matrix: Aqueous Batch: 15202 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Chloride 1.0 U 1 1.0 0.20 mg/L 04/30/20191844 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 179 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15202-002 Matrix: Aqueous Batch: 15202 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Chloride 20 21 1 107 90-110 04/30/20191723 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 180 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15230-001 Matrix: Aqueous Batch: 15230 Analytical Method: SM 4500-S2 F-2011 Parameter Result Q Dil LOQ DL Units Analysis Date Sulfide 1.0 U 1 1.0 0.99 mg/L 04/30/2019 2009 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 181 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15230-002 Matrix: Aqueous Batch: 15230 Analytical Method: SM 4500-S2 F-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfide 10 10 1 101 80-120 04/30/2019 2009 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 182 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15351-001 Matrix: Aqueous Batch: 15351 Analytical Method: SM 531 OC-2011 Parameter Result Q Dil LOQ DL Units Analysis Date TOC 1.0 U 1 1.0 1.0 mg/L 05/02/2019 0307 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 183 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15351-002 Matrix: Aqueous Batch: 15351 Analytical Method: SM 531 OC-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date TOC 20 19 1 97 90-110 05/02/2019 0324 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 184 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MS Sample ID: UD30018-002MS Matrix: Aqueous Batch: 15351 Analytical Method: SM 531 OC-2011 Sample Spike Amount Amount Result % Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date TOC 2.3 20 21 1 94 70-130 05/02/2019 0450 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 185 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MSD Sample ID: UD30018-002MD Matrix: Aqueous Batch: 15351 Analytical Method: SM 531 OC-2011 Sample Spike Amount Amount Result % Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date TOC 2.3 20 22 1 96 2.2 70-130 20 05/02/2019 0508 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 186 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15392-001 Matrix: Aqueous Batch: 15392 Analytical Method: SM 2320B-2011 Parameter Result Q Dil LOQ DL Units Analysis Date Alkalinity 20 U 1 20 20 mg/L 05/02/2019 0044 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 187 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15392-002 Matrix: Aqueous Batch: 15392 Analytical Method: SM 2320B-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Alkalinity 100 100 1 103 90-110 05/02/2019 0052 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 188 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15419-001 Matrix: Aqueous Batch: 15419 Analytical Method: SM 2540C-2011 Parameter Result Q Dil LOQ DL Units Analysis Date TDS 25 U 1 25 25 mg/L 05/02/20191824 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 189 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15419-002 Matrix: Aqueous Batch: 15419 Analytical Method: SM 2540C-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date TDS 1500 1400 1 93 90-110 05/02/20191824 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 190 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15610-001 Matrix: Aqueous Batch: 15610 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Nitrate - N 0.020 U 1 0.020 0.0050 mg/L 05/02/2019 1534 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 191 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15610-002 Matrix: Aqueous Batch: 15610 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Nitrate - N 0.80 0.78 1 98 90-110 05/02/2019 1609 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 192 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15613-001 Matrix: Aqueous Batch: 15613 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Sulfate 1.0 U 1 1.0 0.20 mg/L 05/02/20191534 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 193 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15613-002 Matrix: Aqueous Batch: 15613 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfate 20 20 1 100 90-110 05/02/20191609 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 194 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15614-001 Matrix: Aqueous Batch: 15614 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Chloride 1.0 U 1 1.0 0.20 mg/L 05/02/20191534 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 195 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15614-002 Matrix: Aqueous Batch: 15614 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Chloride 20 20 1 101 90-110 05/02/20191609 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 196 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15769-001 Matrix: Aqueous Batch: 15769 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Nitrate - N 0.020 U 1 0.020 0.0050 mg/L 05/03/2019 2007 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 197 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15769-002 Matrix: Aqueous Batch: 15769 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Nitrate - N 0.80 0.81 1 101 90-110 05/03/2019 1951 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 198 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15770-001 Matrix: Aqueous Batch: 15770 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Sulfate 1.0 U 1 1.0 0.20 mg/L 05/03/2019 2007 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 199 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15770-002 Matrix: Aqueous Batch: 15770 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfate 20 20 1 99 90-110 05/03/20191951 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 200 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15800-001 Matrix: Aqueous Batch: 15800 Analytical Method: SM 531 OC-2011 Parameter Result Q Dil LOQ DL Units Analysis Date TOC 1.0 U 1 1.0 1.0 mg/L 05/06/20191634 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 201 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15800-002 Matrix: Aqueous Batch: 15800 Analytical Method: SM 531 OC-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date TOC 20 20 1 101 90-110 05/06/20191650 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 202 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MS Sample ID: UD30018-013MS Matrix: Aqueous Batch: 15800 Analytical Method: SM 531 OC-2011 Sample Spike Amount Amount Result % Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date TOC 2.4 20 22 1 96 70-130 05/06/2019 2151 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 203 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MSD Sample ID: UD30018-013MD Matrix: Aqueous Batch: 15800 Analytical Method: SM 531 OC-2011 Sample Spike Amount Amount Result % Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date TOC 2.4 20 22 1 96 0.38 70-130 20 05/06/2019 2208 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 204 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ15976-001 Matrix: Aqueous Batch: 15976 Analytical Method: SM 4500-S2 F-2011 Parameter Result Q Dil LOQ DL Units Analysis Date Sulfide 1.0 U 1 1.0 0.99 mg/L 05/07/2019 2048 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 205 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ15976-002 Matrix: Aqueous Batch: 15976 Analytical Method: SM 4500-S2 F-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfide 10 9.9 1 99 80-120 05/07/2019 2048 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 206 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MS Sample ID: UD30018-013MS Matrix: Aqueous Batch: 15976 Analytical Method: SM 4500-S2 F-2011 Sample Spike Amount Amount Result % Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Sulfide 0.0 10 9.6 1 96 70-130 05/07/2019 2048 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 207 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MSD Sample ID: UD30018-013MD Matrix: Aqueous Batch: 15976 Analytical Method: SM 4500-S2 F-2011 Sample Spike Amount Amount Result % Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date Sulfide 0.0 10 9.3 1 93 3.4 70-130 20 05/07/2019 2048 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 208 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ16220-001 Matrix: Aqueous Batch: 16220 Analytical Method: SM 2320B-2011 Parameter Result Q Dil LOQ DL Units Analysis Date Alkalinity 20 U 1 20 20 mg/L 05/09/2019 0028 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 209 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ16220-002 Matrix: Aqueous Batch: 16220 Analytical Method: SM 2320B-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Alkalinity 100 110 1 107 90-110 05/09/2019 0036 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 210 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - Duplicate Sample ID: UD30018-006DU Matrix: Aqueous Batch: 16220 Analytical Method: SM 2320B-2011 Sample Amount Result % RPD Parameter (mg/L) (mg/L) Q Dil % RPD Limit Analysis Date Alkalinity 470 470 1 0.52 20 05/09/2019 0110 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 211 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ16330-001 Matrix: Aqueous Batch: 16330 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Chloride 1.0 U 1 1.0 0.20 mg/L 05/10/20191030 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 212 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ16330-002 Matrix: Aqueous Batch: 16330 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Chloride 20 21 1 103 90-110 05/10/20191102 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 213 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ16331-001 Matrix: Aqueous Batch: 16331 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Nitrate - N 0.020 U 1 0.020 0.0050 mg/L 05/10/2019 1030 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 214 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ16331-002 Matrix: Aqueous Batch: 16331 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Nitrate - N 0.80 0.83 1 104 90-110 05/10/2019 1102 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 215 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ16582-001 Matrix: Aqueous Batch: 16582 Analytical Method: 300.0 Parameter Result Q Dil LOQ DL Units Analysis Date Nitrate - N 0.020 U 1 0.020 0.0050 mg/L 05/13/2019 2146 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 216 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ16582-002 Matrix: Aqueous Batch: 16582 Analytical Method: 300.0 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Nitrate - N 0.80 0.82 1 102 90-110 05/13/2019 2307 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 217 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MB Sample ID: UQ16694-001 Matrix: Aqueous Batch: 16694 Analytical Method: SM 5220D-2011 Parameter Result Q Dil LOQ DL Units Analysis Date COD 20 U 1 20 20 mg/L 05/14/2019 2230 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 218 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - LCS Sample ID: UQ16694-002 Matrix: Aqueous Batch: 16694 Analytical Method: SM 5220D-2011 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date COD 40 42 1 105 95-105 05/14/2019 2230 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 219 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MS Sample ID: UD30018-007MS Matrix: Aqueous Batch: 16694 Analytical Method: SM 5220D-2011 Sample Spike Amount Amount Result % Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date COD 79 40 120 1 92 90-110 05/14/2019 2230 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 220 of 286 QC Data for Lot Number: UD30018 Inorganic non-metals - MSD Sample ID: UD30018-007MD Matrix: Aqueous Batch: 16694 Analytical Method: SM 5220D-2011 Sample Spike Amount Amount Result % Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date COD 79 40 110 N 1 88 1.6 90-110 20 05/14/2019 2230 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 221 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS (SIM) - MB Sample ID: UQ15469-001 Matrix: Aqueous Batch: 15469 Prep Method: 5030E Analytical Method: 8260B (SIM) Parameter Result Q Dil LOQ DL Units Analysis Date 1,4-Dioxane 3.0 U 1 3.0 1.0 ug/L 05/02/20191119 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 122 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 222 of 286 Volatile Organic Compounds by GC/MS (SIM) - LCS Sample ID: UQ15469-002 Matrix: Aqueous Batch: 15469 Prep Method: 5030E Analytical Method: 8260B (SIM) Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 1,4-Dioxane 50 50 1 100 70-130 05/02/20191030 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 121 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 223 of 286 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ15632-001 Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Acetone 10 U 1 10 2.0 ug/L 05/03/2019 1105 Acrylonitrile 5.0 U 1 5.0 0.80 ug/L 05/03/2019 1105 Benzene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Bromochloromethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Bromodichloromethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Bromoform 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Bromomethane (Methyl bromide) 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 2-Butanone (MEK) 10 U 1 10 2.0 ug/L 05/03/2019 1105 Carbon disulfide 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Carbon tetrachloride 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Chlorobenzene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Chloroethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Chloroform 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Chloromethane (Methyl chloride) 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,2-Dibromo-3-chloropropane (DBCP) 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Dibromochloromethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,2-Dibromoethane (EDB) 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Dibromomethane (Methylene bromide) 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 trans- 1,4-Dichloro-2-butene 2.0 U 1 2.0 0.40 ug/L 05/03/2019 1105 1,2-Dichlorobenzene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,4-Dichlorobenzene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Dichlorodifluoromethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,1-Dichloroethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,2-Dichloroethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,1-Dichloroethene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 cis- 1,2-Dichloroethene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 trans- 1,2-Dichloroethene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,2-Dichloropropane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 cis- 1,3-Dichloropropene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 trans- 1,3-Dichloropropene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Ethylbenzene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 2-Hexanone 10 U 1 10 2.0 ug/L 05/03/2019 1105 Methacrylonitrile 5.0 U 1 5.0 2.0 ug/L 05/03/2019 1105 Methyl iodide (lodomethane) 5.0 U 1 5.0 0.40 ug/L 05/03/2019 1105 4-Methyl-2-pentanone 10 U 1 10 2.0 ug/L 05/03/2019 1105 Methylene chloride 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Styrene 0.50 U 1 0.50 0.41 ug/L 05/03/2019 1105 1,1,1,2-Tetrachloroethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,1,2,2-Tetrachloroethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Tetrachloroethene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Tetrahydrofuran 5.0 U 1 5.0 1.0 ug/L 05/03/2019 1105 Toluene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,1,1-Trichloroethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,1,2-Trichloroethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 224 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ15632-001 Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Trichloroethene 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Trichlorofluoromethane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 1,2,3-Trichloropropane 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Vinyl acetate 5.0 U 1 5.0 1.2 ug/L 05/03/2019 1105 Vinyl chloride 0.50 U 1 0.50 0.40 ug/L 05/03/2019 1105 Xylenes (total) 1.0 U 1 1.0 0.40 ug/L 05/03/2019 1105 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 97 70-130 1,2-Dichloroethane-d4 97 70-130 Toluene-d8 105 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 225 of 286 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ15632-002 Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Acetone 100 94 1 94 60-140 05/03/2019 0953 Acrylonitrile 100 100 1 103 70-130 05/03/2019 0953 Benzene 50 52 1 104 70-130 05/03/2019 0953 Bromochloromethane 50 48 1 97 70-130 05/03/2019 0953 Bromodichloromethane 50 49 1 97 70-130 05/03/2019 0953 Bromoform 50 51 1 102 70-130 05/03/2019 0953 Bromomethane (Methyl bromide) 50 51 1 101 70-130 05/03/2019 0953 2-Butanone (MEK) 100 110 1 107 70-130 05/03/2019 0953 Carbon disulfide 50 48 1 96 70-130 05/03/2019 0953 Carbon tetrachloride 50 46 1 91 70-130 05/03/2019 0953 Chlorobenzene 50 51 1 103 70-130 05/03/2019 0953 Chloroethane 50 47 1 94 70-130 05/03/2019 0953 Chloroform 50 47 1 93 70-130 05/03/2019 0953 Chloromethane (Methyl chloride) 50 45 1 90 60-140 05/03/2019 0953 1,2-Dibromo-3-chloropropane (DBCP) 50 51 1 103 70-130 05/03/2019 0953 Dibromochloromethane 50 52 1 103 70-130 05/03/2019 0953 1,2-Dibromoethane (EDB) 50 52 1 105 70-130 05/03/2019 0953 Dibromomethane (Methylene bromide) 50 51 1 101 70-130 05/03/2019 0953 trans- 1,4-Dichloro-2-butene 50 51 1 102 70-130 05/03/2019 0953 1,2-Dichlorobenzene 50 52 1 105 70-130 05/03/2019 0953 1,4-Dichlorobenzene 50 52 1 105 70-130 05/03/2019 0953 Dichlorodifluoromethane 50 40 1 79 60-140 05/03/2019 0953 1,1-Dichloroethane 50 51 1 101 70-130 05/03/2019 0953 1,2-Dichloroethane 50 47 1 94 70-130 05/03/2019 0953 1,1-Dichloroethene 50 49 1 98 70-130 05/03/2019 0953 cis- 1,2-Dichloroethene 50 49 1 99 70-130 05/03/2019 0953 trans- 1,2-Dichloroethene 50 49 1 98 70-130 05/03/2019 0953 1,2-Dichloropropane 50 52 1 104 70-130 05/03/2019 0953 cis- 1,3-Dichloropropene 50 53 1 106 70-130 05/03/2019 0953 trans- 1,3-Dichloropropene 50 52 1 104 70-130 05/03/2019 0953 Ethylbenzene 50 52 1 104 70-130 05/03/2019 0953 2-Hexanone 100 110 1 113 70-130 05/03/2019 0953 Methacrylonitrile 250 260 1 105 70-130 05/03/2019 0953 Methyl iodide (lodomethane) 50 49 1 97 70-130 05/03/2019 0953 4-Methyl-2-pentanone 100 110 1 109 70-130 05/03/2019 0953 Methylene chloride 50 48 1 96 70-130 05/03/2019 0953 Styrene 50 55 1 110 70-130 05/03/2019 0953 1,1,1,2-Tetrachloroethane 50 51 1 101 70-130 05/03/2019 0953 1,1,2,2-Tetrachloroethane 50 54 1 109 70-130 05/03/2019 0953 Tetrachloroethene 50 49 1 99 70-130 05/03/2019 0953 Tetrahydrofuran 50 49 1 98 70-130 05/03/2019 0953 Toluene 50 52 1 103 70-130 05/03/2019 0953 1,1,1-Trichloroethane 50 48 1 95 70-130 05/03/2019 0953 1,1,2-Trichloroethane 50 52 1 105 70-130 05/03/2019 0953 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 226 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ15632-002 Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Trichloroethene 50 49 1 99 70-130 05/03/2019 0953 Trichlorofluoromethane 50 42 1 83 70-130 05/03/2019 0953 1,2,3-Trichloropropane 50 53 1 107 70-130 05/03/2019 0953 Vinyl acetate 50 54 1 107 60-140 05/03/2019 0953 Vinyl chloride 50 47 1 94 70-130 05/03/2019 0953 Xylenes (total) 100 110 1 106 70-130 05/03/2019 0953 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 102 70-130 1,2-Dichloroethane-d4 84 70-130 Toluene-d8 95 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 227 of 286 Volatile Organic Compounds by GC/MS - MS Sample ID: UD30018-01OMS Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Acetone 0.0 500 490 5 98 60-140 05/03/2019 2102 Acrylonitrile 0.0 500 580 5 115 70-130 05/03/2019 2102 Benzene 0.0 250 300 5 120 70-130 05/03/2019 2102 Bromochloromethane 0.0 250 280 5 113 70-130 05/03/2019 2102 Bromodichloromethane 0.0 250 290 5 115 70-130 05/03/2019 2102 Bromoform 0.0 250 280 5 112 70-130 05/03/2019 2102 Bromomethane (Methyl bromide) 0.0 250 250 5 98 70-130 05/03/2019 2102 2-Butanone (MEK) 0.0 500 570 5 114 70-130 05/03/2019 2102 Carbon disulfide 0.0 250 300 5 121 70-130 05/03/2019 2102 Carbon tetrachloride 0.0 250 290 5 114 70-130 05/03/2019 2102 Chlorobenzene 0.0 250 290 5 115 70-130 05/03/2019 2102 Chloroethane 4.1 250 290 5 116 70-130 05/03/2019 2102 Chloroform 0.0 250 280 5 110 70-130 05/03/2019 2102 Chloromethane (Methyl chloride) 0.0 250 280 5 110 60-140 05/03/2019 2102 1,2-Dibromo-3-chloropropane (DBCP) 0.0 250 240 5 97 70-130 05/03/2019 2102 Dibromochloromethane 0.0 250 280 5 114 70-130 05/03/2019 2102 1,2-Dibromoethane (EDB) 0.0 250 280 5 113 70-130 05/03/2019 2102 Dibromomethane (Methylene bromide) 0.0 250 290 5 116 70-130 05/03/2019 2102 trans- 1,4-Dichloro-2-butene 0.0 250 230 5 90 70-142 05/03/2019 2102 1,2-Dichlorobenzene 0.0 250 250 5 99 70-130 05/03/2019 2102 1,4-Dichlorobenzene 0.0 250 250 5 99 70-130 05/03/2019 2102 Dichlorodifluoromethane 0.0 250 280 5 111 60-140 05/03/2019 2102 1,1-Dichloroethane 3.7 250 310 5 122 70-130 05/03/2019 2102 1,2-Dichloroethane 0.0 250 270 5 108 70-130 05/03/2019 2102 1,1-Dichloroethene 0.0 250 300 5 119 70-130 05/03/2019 2102 cis- 1,2-Dichloroethene 0.0 250 290 5 116 70-130 05/03/2019 2102 trans- 1,2-Dichloroethene 0.0 250 290 5 118 70-130 05/03/2019 2102 1,2-Dichloropropane 0.0 250 300 5 119 70-130 05/03/2019 2102 cis- 1,3-Dichloropropene 0.0 250 290 5 118 70-130 05/03/2019 2102 trans- 1,3-Dichloropropene 0.0 250 280 5 110 70-130 05/03/2019 2102 Ethylbenzene 0.0 250 290 5 116 70-130 05/03/2019 2102 2-Hexanone 0.0 500 600 5 119 70-130 05/03/2019 2102 Methacrylonitrile 0.0 1300 1500 5 117 70-130 05/03/2019 2102 Methyl iodide (lodomethane) 0.0 250 280 5 113 70-130 05/03/2019 2102 4-Methyl-2-pentanone 0.0 500 600 5 120 70-130 05/03/2019 2102 Methylene chloride 0.0 250 280 5 111 70-130 05/03/2019 2102 Styrene 0.0 250 300 5 122 70-130 05/03/2019 2102 1,1,1,2-Tetrachloroethane 0.0 250 280 5 114 70-130 05/03/2019 2102 1,1,2,2-Tetrachloroethane 0.0 250 250 5 100 70-130 05/03/2019 2102 Tetrachloroethene 0.0 250 280 5 111 70-130 05/03/2019 2102 Tetrahydrofuran 0.0 250 280 5 112 70-130 05/03/2019 2102 Toluene 0.0 250 290 5 117 70-130 05/03/2019 2102 1,1,1-Trichloroethane 0.0 250 290 5 116 70-130 05/03/2019 2102 1,1,2-Trichloroethane 0.0 250 280 5 113 70-130 05/03/2019 2102 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 228 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS - MS Sample ID: UD30018-01OMS Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Trichloroethene 0.0 250 290 5 114 70-130 05/03/2019 2102 Trichlorofluoromethane 0.0 250 240 5 97 70-130 05/03/2019 2102 1,2,3-Trichloropropane 0.0 250 250 5 100 70-130 05/03/2019 2102 Vinyl acetate 0.0 250 280 5 111 60-140 05/03/2019 2102 Vinyl chloride 0.0 250 310 5 122 70-130 05/03/2019 2102 Xylenes (total) 0.0 500 580 5 117 70-130 05/03/2019 2102 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 100 70-130 1,2-Dichloroethane-d4 98 70-130 Toluene-d8 104 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 229 of 286 Volatile Organic Compounds by GC/MS - MSD Sample ID: UD30018-01OMD Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Acetone 0.0 500 510 5 103 4.7 60-140 20 05/03/2019 2127 Acrylonitrile 0.0 500 600 5 120 3.9 70-130 40 05/03/2019 2127 Benzene 0.0 250 320 5 128 6.8 70-130 20 05/03/2019 2127 Bromochloromethane 0.0 250 290 5 117 3.6 70-130 20 05/03/2019 2127 Bromodichloromethane 0.0 250 300 5 120 3.7 70-130 20 05/03/2019 2127 Bromoform 0.0 250 290 5 116 3.3 70-130 20 05/03/2019 2127 Bromomethane (Methyl bromide) 0.0 250 240 5 97 0.91 70-130 20 05/03/2019 2127 2-Butanone (MEK) 0.0 500 590 5 118 3.7 70-130 20 05/03/2019 2127 Carbon disulfide 0.0 250 310 5 125 3.2 70-130 20 05/03/2019 2127 Carbon tetrachloride 0.0 250 300 5 118 3.4 70-130 20 05/03/2019 2127 Chlorobenzene 0.0 250 300 5 119 3.5 70-130 20 05/03/2019 2127 Chloroethane 4.1 250 280 5 112 3.4 70-130 20 05/03/2019 2127 Chloroform 0.0 250 290 5 115 4.3 70-130 20 05/03/2019 2127 Chloromethane (Methyl chloride) 0.0 250 290 5 117 5.5 60-140 20 05/03/2019 2127 1,2-Dibromo-3-chloropropane (DBCP) 0.0 250 260 5 104 7.1 70-130 20 05/03/2019 2127 Dibromochloromethane 0.0 250 300 5 119 4.5 70-130 20 05/03/2019 2127 1,2-Dibromoethane (EDB) 0.0 250 290 5 116 2.9 70-130 20 05/03/2019 2127 Dibromomethane (Methylene bromide) 0.0 250 300 5 121 4.5 70-130 20 05/03/2019 2127 trans- 1,4-Dichloro-2-butene 0.0 250 250 5 99 8.8 70-142 20 05/03/2019 2127 1,2-Dichlorobenzene 0.0 250 270 5 108 8.3 70-130 20 05/03/2019 2127 1,4-Dichlorobenzene 0.0 250 270 5 107 8.4 70-130 20 05/03/2019 2127 Dichlorodifluoromethane 0.0 250 280 5 112 0.96 60-140 20 05/03/2019 2127 1,1-Dichloroethane 3.7 250 320 5 127 4.1 70-130 20 05/03/2019 2127 1,2-Dichloroethane 0.0 250 280 5 113 4.5 70-130 20 05/03/2019 2127 1,1-Dichloroethene 0.0 250 310 5 124 4.3 70-130 20 05/03/2019 2127 cis- 1,2-Dichloroethene 0.0 250 300 5 121 4.2 70-130 20 05/03/2019 2127 trans- 1,2-Dichloroethene 0.0 250 310 5 123 4.0 70-130 20 05/03/2019 2127 1,2-Dichloropropane 0.0 250 320 5 126 5.6 70-130 20 05/03/2019 2127 cis- 1,3-Dichloropropene 0.0 250 310 5 124 5.2 70-130 20 05/03/2019 2127 trans- 1,3-Dichloropropene 0.0 250 290 5 116 5.2 70-130 20 05/03/2019 2127 Ethylbenzene 0.0 250 300 5 122 4.6 70-130 20 05/03/2019 2127 2-Hexanone 0.0 500 620 5 124 4.4 70-130 20 05/03/2019 2127 Methacrylonitrile 0.0 1300 1500 5 122 4.4 70-130 20 05/03/2019 2127 Methyl iodide (lodomethane) 0.0 250 290 5 118 4.4 70-130 20 05/03/2019 2127 4-Methyl-2-pentanone 0.0 500 630 5 127 5.2 70-130 20 05/03/2019 2127 Methylene chloride 0.0 250 290 5 116 4.2 70-130 20 05/03/2019 2127 Styrene 0.0 250 320 5 127 4.6 70-130 20 05/03/2019 2127 1,1,1,2-Tetrachloroethane 0.0 250 300 5 119 4.2 70-130 20 05/03/2019 2127 1,1,2,2-Tetrachloroethane 0.0 250 270 5 108 7.5 70-130 20 05/03/2019 2127 Tetrachloroethene 0.0 250 290 5 117 5.0 70-130 20 05/03/2019 2127 Tetrahydrofuran 0.0 250 300 5 118 5.3 70-130 20 05/03/2019 2127 Toluene 0.0 250 300 5 121 3.8 70-130 20 05/03/2019 2127 1,1,1-Trichloroethane 0.0 250 300 5 121 3.9 70-130 20 05/03/2019 2127 1,1,2-Trichloroethane 0.0 250 300 5 119 4.5 70-130 20 05/03/2019 2127 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 230 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS - MSD Sample ID: UD30018-01OMD Matrix: Aqueous Batch: 15632 Prep Method: 5030E Analytical Method: 8260D Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Trichloroethene 0.0 250 310 5 125 8.8 70-130 20 05/03/2019 2127 Trichlorofluoromethane 0.0 250 240 5 98 0.75 70-130 20 05/03/2019 2127 1,2,3-Trichloropropane 0.0 250 270 5 108 8.2 70-130 20 05/03/2019 2127 Vinyl acetate 0.0 250 290 5 116 3.8 60-140 20 05/03/2019 2127 Vinyl chloride 0.0 250 290 5 118 3.9 70-130 20 05/03/2019 2127 Xylenes (total) 0.0 500 610 5 122 4.5 70-130 20 05/03/2019 2127 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 108 70-130 1,2-Dichloroethane-d4 98 70-130 Toluene-d8 108 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 231 of 286 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ15794-001 Matrix: Aqueous Batch: 15794 Prep Method: 5030E Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Acetone 10 U 1 10 2.0 ug/L 05/06/2019 1310 Acrylonitrile 5.0 U 1 5.0 0.80 ug/L 05/06/2019 1310 Benzene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Bromochloromethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Bromodichloromethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Bromoform 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Bromomethane (Methyl bromide) 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 2-Butanone (MEK) 10 U 1 10 2.0 ug/L 05/06/2019 1310 Carbon disulfide 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Carbon tetrachloride 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Chlorobenzene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Chloroethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Chloroform 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Chloromethane (Methyl chloride) 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,2-Dibromo-3-chloropropane (DBCP) 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Dibromochloromethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,2-Dibromoethane (EDB) 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Dibromomethane (Methylene bromide) 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 trans- 1,4-Dichloro-2-butene 2.0 U 1 2.0 0.40 ug/L 05/06/2019 1310 1,2-Dichlorobenzene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,4-Dichlorobenzene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Dichlorodifluoromethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,1-Dichloroethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,2-Dichloroethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,1-Dichloroethene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 cis- 1,2-Dichloroethene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 trans- 1,2-Dichloroethene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,2-Dichloropropane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 cis- 1,3-Dichloropropene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 trans- 1,3-Dichloropropene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Ethylbenzene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 2-Hexanone 10 U 1 10 2.0 ug/L 05/06/2019 1310 Methacrylonitrile 5.0 U 1 5.0 2.0 ug/L 05/06/2019 1310 Methyl iodide (lodomethane) 5.0 U 1 5.0 0.40 ug/L 05/06/2019 1310 4-Methyl-2-pentanone 10 U 1 10 2.0 ug/L 05/06/2019 1310 Methylene chloride 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Styrene 0.50 U 1 0.50 0.41 ug/L 05/06/2019 1310 1,1,1,2-Tetrachloroethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,1,2,2-Tetrachloroethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Tetrachloroethene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Tetrahydrofuran 5.0 U 1 5.0 1.0 ug/L 05/06/2019 1310 Toluene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,1,1-Trichloroethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,1,2-Trichloroethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 232 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS - MB Sample ID: UQ15794-001 Matrix: Aqueous Batch: 15794 Prep Method: 5030E Analytical Method: 8260D Parameter Result Q Dil LOQ DL Units Analysis Date Trichloroethene 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Trichlorofluoromethane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 1,2,3-Trichloropropane 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Vinyl acetate 5.0 U 1 5.0 1.2 ug/L 05/06/2019 1310 Vinyl chloride 0.50 U 1 0.50 0.40 ug/L 05/06/2019 1310 Xylenes (total) 1.0 U 1 1.0 0.40 ug/L 05/06/2019 1310 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 97 70-130 1,2-Dichloroethane-d4 100 70-130 Toluene-d8 107 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 233 of 286 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ15794-002 Matrix: Aqueous Batch: 15794 Prep Method: 5030E Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Acetone 100 110 1 110 60-140 05/06/2019 1059 Acrylonitrile 100 99 1 99 70-130 05/06/2019 1059 Benzene 50 52 1 103 70-130 05/06/2019 1059 Bromochloromethane 50 48 1 96 70-130 05/06/2019 1059 Bromodichloromethane 50 48 1 96 70-130 05/06/2019 1059 Bromoform 50 50 1 100 70-130 05/06/2019 1059 Bromomethane (Methyl bromide) 50 49 1 98 70-130 05/06/2019 1059 2-Butanone (MEK) 100 100 1 102 70-130 05/06/2019 1059 Carbon disulfide 50 47 1 94 70-130 05/06/2019 1059 Carbon tetrachloride 50 44 1 88 70-130 05/06/2019 1059 Chlorobenzene 50 51 1 101 70-130 05/06/2019 1059 Chloroethane 50 47 1 94 70-130 05/06/2019 1059 Chloroform 50 46 1 91 70-130 05/06/2019 1059 Chloromethane (Methyl chloride) 50 44 1 88 60-140 05/06/2019 1059 1,2-Dibromo-3-chloropropane (DBCP) 50 49 1 97 70-130 05/06/2019 1059 Dibromochloromethane 50 50 1 100 70-130 05/06/2019 1059 1,2-Dibromoethane (EDB) 50 50 1 100 70-130 05/06/2019 1059 Dibromomethane (Methylene bromide) 50 49 1 99 70-130 05/06/2019 1059 trans- 1,4-Dichloro-2-butene 50 50 1 99 70-130 05/06/2019 1059 1,2-Dichlorobenzene 50 51 1 102 70-130 05/06/2019 1059 1,4-Dichlorobenzene 50 51 1 102 70-130 05/06/2019 1059 Dichlorodifluoromethane 50 36 1 72 60-140 05/06/2019 1059 1,1-Dichloroethane 50 50 1 99 70-130 05/06/2019 1059 1,2-Dichloroethane 50 46 1 92 70-130 05/06/2019 1059 1,1-Dichloroethene 50 47 1 93 70-130 05/06/2019 1059 cis- 1,2-Dichloroethene 50 49 1 98 70-130 05/06/2019 1059 trans- 1,2-Dichloroethene 50 48 1 96 70-130 05/06/2019 1059 1,2-Dichloropropane 50 50 1 100 70-130 05/06/2019 1059 cis- 1,3-Dichloropropene 50 51 1 103 70-130 05/06/2019 1059 trans- 1,3-Dichloropropene 50 51 1 101 70-130 05/06/2019 1059 Ethylbenzene 50 51 1 102 70-130 05/06/2019 1059 2-Hexanone 100 100 1 101 70-130 05/06/2019 1059 Methacrylonitrile 250 250 1 101 70-130 05/06/2019 1059 Methyl iodide (lodomethane) 50 48 1 97 70-130 05/06/2019 1059 4-Methyl-2-pentanone 100 100 1 103 70-130 05/06/2019 1059 Methylene chloride 50 47 1 95 70-130 05/06/2019 1059 Styrene 50 54 1 107 70-130 05/06/2019 1059 1,1,1,2-Tetrachloroethane 50 50 1 100 70-130 05/06/2019 1059 1,1,2,2-Tetrachloroethane 50 51 1 103 70-130 05/06/2019 1059 Tetrachloroethene 50 48 1 97 70-130 05/06/2019 1059 Tetrahydrofuran 50 48 1 96 70-130 05/06/2019 1059 Toluene 50 50 1 101 70-130 05/06/2019 1059 1,1,1-Trichloroethane 50 46 1 93 70-130 05/06/2019 1059 1,1,2-Trichloroethane 50 51 1 101 70-130 05/06/2019 1059 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 234 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS - LCS Sample ID: UQ15794-002 Matrix: Aqueous Batch: 15794 Prep Method: 5030E Analytical Method: 8260D Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Trichloroethene 50 49 1 98 70-130 05/06/2019 1059 Trichlorofluoromethane 50 39 1 78 70-130 05/06/2019 1059 1,2,3-Trichloropropane 50 51 1 102 70-130 05/06/2019 1059 Vinyl acetate 50 48 1 96 60-140 05/06/2019 1059 Vinyl chloride 50 45 1 91 70-130 05/06/2019 1059 Xylenes (total) 100 100 1 103 70-130 05/06/2019 1059 Surrogate Q % Rec Acceptance Limit Bromofluorobenzene 99 70-130 1,2-Dichloroethane-d4 83 70-130 Toluene-d8 93 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 235 of 286 Volatile Organic Compounds by GC/MS - LCSD Sample ID: UQ15794-003 Matrix: Aqueous Batch: 15794 Prep Method: 5030E Analytical Method: 8260D Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Acetone 100 100 1 103 7.0 60-140 20 05/06/2019 1122 Acrylonitrile 100 100 1 103 4.3 70-130 40 05/06/2019 1122 Benzene 50 50 1 100 2.7 70-130 20 05/06/2019 1122 Bromochloromethane 50 49 1 99 3.5 70-130 20 05/06/2019 1122 Bromodichloromethane 50 50 1 99 3.7 70-130 20 05/06/2019 1122 Bromoform 50 45 1 90 11 70-130 20 05/06/2019 1122 Bromomethane (Methyl bromide) 50 39 + 1 77 24 70-130 20 05/06/2019 1122 2-Butanone (MEK) 100 100 1 103 1.5 70-130 20 05/06/2019 1122 Carbon disulfide 50 47 1 93 1.5 70-130 20 05/06/2019 1122 Carbon tetrachloride 50 45 1 91 3.2 70-130 20 05/06/2019 1122 Chlorobenzene 50 48 1 95 5.9 70-130 20 05/06/2019 1122 Chloroethane 50 54 1 108 15 70-130 20 05/06/2019 1122 Chloroform 50 46 1 91 0.23 70-130 20 05/06/2019 1122 Chloromethane (Methyl chloride) 50 46 1 92 4.4 60-140 20 05/06/2019 1122 1,2-Dibromo-3-chloropropane (DBCP) 50 42 1 84 14 70-130 20 05/06/2019 1122 Dibromochloromethane 50 48 1 96 4.7 70-130 20 05/06/2019 1122 1,2-Dibromoethane (EDB) 50 51 1 102 1.9 70-130 20 05/06/2019 1122 Dibromomethane (Methylene bromide) 50 52 1 103 4.5 70-130 20 05/06/2019 1122 trans- 1,4-Dichloro-2-butene 50 44 1 88 12 70-130 20 05/06/2019 1122 1,2-Dichlorobenzene 50 43 1 86 17 70-130 20 05/06/2019 1122 1,4-Dichlorobenzene 50 43 1 85 18 70-130 20 05/06/2019 1122 Dichlorodifluoromethane 50 39 1 78 8.0 60-140 20 05/06/2019 1122 1,1-Dichloroethane 50 50 1 101 1.4 70-130 20 05/06/2019 1122 1,2-Dichloroethane 50 51 1 101 10 70-130 20 05/06/2019 1122 1,1-Dichloroethene 50 48 1 96 3.3 70-130 20 05/06/2019 1122 cis- 1,2-Dichloroethene 50 50 1 100 2.0 70-130 20 05/06/2019 1122 trans- 1,2-Dichloroethene 50 49 1 98 1.9 70-130 20 05/06/2019 1122 1,2-Dichloropropane 50 54 1 107 7.1 70-130 20 05/06/2019 1122 cis- 1,3-Dichloropropene 50 52 1 104 1.0 70-130 20 05/06/2019 1122 trans- 1,3-Dichloropropene 50 48 1 97 4.2 70-130 20 05/06/2019 1122 Ethylbenzene 50 49 1 98 3.8 70-130 20 05/06/2019 1122 2-Hexanone 100 99 1 99 1.5 70-130 20 05/06/2019 1122 Methacrylonitrile 250 260 1 106 4.9 70-130 20 05/06/2019 1122 Methyl iodide (lodomethane) 50 49 1 99 2.1 70-130 20 05/06/2019 1122 4-Methyl-2-pentanone 100 110 1 109 5.1 70-130 20 05/06/2019 1122 Methylene chloride 50 50 1 99 4.7 70-130 20 05/06/2019 1122 Styrene 50 51 1 102 4.9 70-130 20 05/06/2019 1122 1,1,1,2-Tetrachloroethane 50 50 1 100 0.062 70-130 20 05/06/2019 1122 1,1,2,2-Tetrachloroethane 50 44 1 89 15 70-130 20 05/06/2019 1122 Tetrachloroethene 50 46 1 92 4.6 70-130 20 05/06/2019 1122 Tetrahydrofuran 50 49 1 99 2.7 70-130 20 05/06/2019 1122 Toluene 50 49 1 98 3.5 70-130 20 05/06/2019 1122 1,1,1-Trichloroethane 50 48 1 95 2.4 70-130 20 05/06/2019 1122 1,1,2-Trichloroethane 50 50 1 100 1.4 70-130 20 05/06/2019 1122 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 236 of 286 QC Data for Lot Number: UD30018 Volatile Organic Compounds by GC/MS - LCSD Sample ID: UQ15794-003 Matrix: Aqueous Batch: 15794 Prep Method: 5030E Analytical Method: 8260D Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Trichloroethene 50 54 1 107 9.3 70-130 20 05/06/2019 1122 Trichlorofluoromethane 50 42 1 83 7.2 70-130 20 05/06/2019 1122 1,2,3-Trichloropropane 50 44 1 87 16 70-130 20 05/06/2019 1122 Vinyl acetate 50 57 1 114 17 60-140 20 05/06/2019 1122 Vinyl chloride 50 47 1 94 3.0 70-130 20 05/06/2019 1122 Xylenes (total) 100 99 1 99 3.8 70-130 20 05/06/2019 1122 Acceptance Surrogate Q % Rec Limit Bromofluorobenzene 101 70-130 1,2-Dichloroethane-d4 97 70-130 Toluene-d8 105 70-130 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 237 of 286 Volatile Organic Compounds by GC/MS (SIM) - MB Sample ID: UQ16388-001 Matrix: Aqueous Batch: 16388 Prep Method: 5030E Analytical Method: 8260B (SIM) Parameter Result Q Dil LOQ DL Units Analysis Date 1,4-Dioxane 3.0 U 1 3.0 1.0 ug/L 05/10/2019 2354 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 122 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 238 of 286 Volatile Organic Compounds by GC/MS (SIM) - LCS Sample ID: UQ16388-002 Matrix: Aqueous Batch: 16388 Prep Method: 5030E Analytical Method: 8260B (SIM) Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 1,4-Dioxane 50 57 1 115 70-130 05/10/2019 2227 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 123 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 239 of 286 Volatile Organic Compounds by GC/MS (SIM) - LCSD Sample ID: UQ16388-003 Matrix: Aqueous Batch: 16388 Prep Method: 5030E Analytical Method: 8260B (SIM) Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date 1,4-Dioxane 50 48 1 96 18 70-130 20 05/10/2019 2251 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 109 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 240 of 286 Volatile Organic Compounds by GC/MS (SIM) - MB Sample ID: UQ16406-001 Matrix: Aqueous Batch: 16406 Prep Method: 5030E Analytical Method: 8260B (SIM) Parameter Result Q Dil LOQ DL Units Analysis Date 1,4-Dioxane 3.0 U 1 3.0 1.0 ug/L 05/11/20191312 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 119 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 241 of 286 Volatile Organic Compounds by GC/MS (SIM) - LCS Sample ID: UQ16406-002 Matrix: Aqueous Batch: 16406 Prep Method: 5030E Analytical Method: 8260B (SIM) Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 1,4-Dioxane 50 48 1 97 70-130 05/11/20191212 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 122 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 242 of 286 Volatile Organic Compounds by GC/MS (SIM) - LCSD Sample ID: UQ16406-003 Matrix: Aqueous Batch: 16406 Prep Method: 5030E Analytical Method: 8260B (SIM) Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date 1,4-Dioxane 50 45 1 91 6.4 70-130 20 05/11/2019 2052 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 125 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 243 of 286 Volatile Organic Compounds by GC/MS (SIM) - MB Sample ID: UQ16570-001 Matrix: Aqueous Batch: 16570 Prep Method: 5030E Analytical Method: 8260B (SIM) Parameter Result Q Dil LOQ DL Units Analysis Date 1,4-Dioxane 3.0 U 1 3.0 1.0 ug/L 05/13/2019 2313 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 117 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 244 of 286 Volatile Organic Compounds by GC/MS (SIM) - LCS Sample ID: UQ16570-002 Matrix: Aqueous Batch: 16570 Prep Method: 5030E Analytical Method: 8260B (SIM) Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 1,4-Dioxane 50 46 1 93 70-130 05/13/2019 2214 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 125 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 245 of 286 Volatile Organic Compounds by GC/MS (SIM) - MS Sample ID: UD30018-026MS Matrix: Aqueous Batch: 16570 Prep Method: 5030E Analytical Method: 8260B (SIM) Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date 1,4-Dioxane 210 250 410 5 79 70-130 05/14/2019 0100 Acceptance Surrogate Q % Rec Limit 1,2-Dichloroethane-d4 123 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 246 of 286 Volatile Organic Compounds by GC/MS (SIM) - MSD Sample ID: UD30018-026MD Matrix: Aqueous Batch: 16570 Prep Method: 5030E Analytical Method: 8260B (SIM) Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date 1,4-Dioxane 210 250 430 5 86 4.6 70-130 20 05/14/2019 0124 Surrogate Q % Rec Acceptance Limit 1,2-Dichloroethane-d4 120 40-170 LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria LOD = Limit of Detection U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. QC Data for Lot Number: UD30018 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 247 of 286 Dissolved Gases - MB Sample ID: UQ16314-001 Matrix: Aqueous Batch: 16314 Analytical Method: RSK - 175 Parameter Result Q Dil LOQ DL Units Analysis Date Ethane 10 U 1 10 2.5 ug/L 05/09/20191805 Ethene 10 U 1 10 2.5 ug/L 05/09/20191805 Methane 10 U 1 10 2.5 ug/L 05/09/20191805 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 248 of 286 QC Data for Lot Number: UD30018 Dissolved Gases - LCS Sample ID: UQ16314-002 Matrix: Aqueous Batch: 16314 Analytical Method: RSK - 175 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Ethane 550 570 1 102 70-130 05/09/20191735 Ethene 520 520 1 100 70-130 05/09/20191735 Methane 300 310 1 106 70-130 05/09/20191735 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 249 of 286 QC Data for Lot Number: UD30018 Dissolved Gases - LCSD Sample ID: UQ16314-003 Matrix: Aqueous Batch: 16314 Analytical Method: RSK - 175 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Ethane 550 590 1 107 4.4 70-130 30 05/09/20191749 Ethene 520 540 1 105 5.3 70-130 30 05/09/20191749 Methane 300 320 1 109 3.1 70-130 30 05/09/20191749 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 250 of 286 QC Data for Lot Number: UD30018 Dissolved Gases - MB Sample ID: UQ16503-001 Matrix: Aqueous Batch: 16503 Analytical Method: RSK - 175 Parameter Result Q Dil LOQ DL Units Analysis Date Methane 10 U 1 10 2.5 ug/L 05/10/20191648 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 251 of 286 QC Data for Lot Number: UD30018 Dissolved Gases - LCS Sample ID: UQ16503-002 Matrix: Aqueous Batch: 16503 Analytical Method: RSK - 175 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Methane 300 310 1 106 70-130 05/10/20191618 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 252 of 286 QC Data for Lot Number: UD30018 Dissolved Gases - LCSD Sample ID: UQ16503-003 Matrix: Aqueous Batch: 16503 Analytical Method: RSK - 175 Spike Amount Result % Rec % RPD Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Methane 300 300 1 101 4.1 70-130 30 05/10/20191632 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 253 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MB Sample ID: UQ15483-001 Matrix: Aqueous Batch: 15483 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/02/2019 1704 Parameter Result Q Dil LOQ DL Units Analysis Date Antimony 6.0 U 1 6.0 0.50 ug/L 05/08/20191451 Arsenic 10 U 1 10 1.3 ug/L 05/08/20191451 Barium 100 U 1 100 1.3 ug/L 05/08/20191451 Beryllium 1.0 U 1 1.0 0.15 ug/L 05/08/20191451 Cadmium 1.0 U 1 1.0 0.13 ug/L 05/08/20191451 Chromium 10 U 1 10 1.3 ug/L 05/08/20191451 Cobalt 10 U 1 10 1.3 ug/L 05/08/20191451 Copper 10 U 1 10 1.3 ug/L 05/08/20191451 Lead 10 U 1 10 0.25 ug/L 05/08/20191451 Nickel 50 U 1 50 1.3 ug/L 05/08/20191451 Selenium 10 U 1 10 1.3 ug/L 05/08/20191451 Silver 10 U 1 10 0.25 ug/L 05/08/20191451 Thallium 5.5 U 1 5.5 0.15 ug/L 05/08/20191451 Vanadium 25 U 1 25 2.5 ug/L 05/08/20191451 Zinc 10 U 1 10 2.5 ug/L 05/08/20191451 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 254 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - LCS Sample ID: UQ15483-002 Matrix: Aqueous Batch: 15483 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/02/2019 1704 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Antimony 100 99 1 99 80-120 05/08/20191457 Arsenic 100 98 1 98 80-120 05/08/20191457 Barium 100 100 1 102 80-120 05/08/20191457 Beryllium 100 100 1 100 80-120 05/08/20191457 Cadmium 100 100 1 101 80-120 05/08/20191457 Chromium 100 99 1 99 80-120 05/08/20191457 Cobalt 100 98 1 98 80-120 05/08/20191457 Copper 100 100 1 101 80-120 05/08/20191457 Lead 100 100 1 102 80-120 05/08/20191457 Nickel 100 100 1 100 80-120 05/08/20191457 Selenium 100 100 1 101 80-120 05/08/20191457 Silver 100 100 1 104 80-120 05/08/20191457 Thallium 100 100 1 100 80-120 05/08/20191457 Vanadium 100 99 1 99 80-120 05/08/20191457 Zinc 100 98 1 98 80-120 05/08/20191457 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 255 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MS Sample ID: UD30018-003MS Matrix: Aqueous Batch: 15483 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/02/2019 1704 Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Antimony 0.0 100 100 1 100 70-130 05/08/20191538 Arsenic 0.0 100 96 1 96 70-130 05/08/20191538 Barium 220 100 320 1 97 70-130 05/08/20191538 Beryllium 0.0 100 71 1 71 70-130 05/08/20191538 Cadmium 0.32 100 98 1 98 70-130 05/08/20191538 Chromium 1.4 100 94 1 93 70-130 05/08/20191538 Cobalt 2.9 100 93 1 90 70-130 05/08/20191538 Copper 0.0 100 92 1 92 70-130 05/08/20191538 Lead 0.0 100 100 1 101 70-130 05/08/20191538 Nickel 27 100 120 1 90 70-130 05/08/20191538 Selenium 0.0 100 98 1 98 70-130 05/08/20191538 Silver 0.0 100 100 1 100 70-130 05/08/20191538 Thallium 0.0 100 99 1 99 70-130 05/08/20191538 Vanadium 0.0 100 96 1 96 70-130 05/08/20191538 Zinc 3.1 100 94 1 91 70-130 05/08/20191538 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 256 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MSD Sample ID: UD30018-003MD Matrix: Aqueous Batch: 15483 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/02/2019 1704 Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Antimony 0.0 100 100 1 100 0.48 70-130 20 05/08/20191544 Arsenic 0.0 100 97 1 97 1.4 70-130 20 05/08/20191544 Barium 220 100 320 1 98 0.22 70-130 20 05/08/20191544 Beryllium 0.0 100 71 1 71 0.83 70-130 20 05/08/20191544 Cadmium 0.32 100 99 1 98 0.31 70-130 20 05/08/20191544 Chromium 1.4 100 94 1 92 0.21 70-130 20 05/08/20191544 Cobalt 2.9 100 93 1 90 0.20 70-130 20 05/08/20191544 Copper 0.0 100 93 1 93 1.5 70-130 20 05/08/20191544 Lead 0.0 100 100 1 100 0.79 70-130 20 05/08/20191544 Nickel 27 100 120 1 91 0.77 70-130 20 05/08/20191544 Selenium 0.0 100 97 1 97 1.2 70-130 20 05/08/20191544 Silver 0.0 100 100 1 100 0.040 70-130 20 05/08/20191544 Thallium 0.0 100 99 1 99 0.31 70-130 20 05/08/20191544 Vanadium 0.0 100 96 1 96 0.82 70-130 20 05/08/20191544 Zinc 3.1 100 95 1 91 0.55 70-130 20 05/08/20191544 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 257 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MB Sample ID: UQ15809-001 Matrix: Aqueous Batch: 15809 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Parameter Result Q Dil LOQ DL Units Analysis Date Antimony 6.0 U 1 6.0 0.50 ug/L 05/08/20191433 Arsenic 10 U 1 10 1.3 ug/L 05/08/20191433 Barium 100 U 1 100 1.3 ug/L 05/08/20191433 Beryllium 1.0 U 1 1.0 0.15 ug/L 05/08/20191433 Cadmium 1.0 U 1 1.0 0.13 ug/L 05/08/20191433 Chromium 10 U 1 10 1.3 ug/L 05/08/20191433 Cobalt 10 U 1 10 1.3 ug/L 05/08/20191433 Copper 10 U 1 10 1.3 ug/L 05/08/20191433 Lead 10 U 1 10 0.25 ug/L 05/08/20191433 Nickel 50 U 1 50 1.3 ug/L 05/08/20191433 Selenium 10 U 1 10 1.3 ug/L 05/08/20191433 Silver 10 U 1 10 0.25 ug/L 05/08/20191433 Sodium 400 U 1 400 150 ug/L 05/08/20191433 Thallium 5.5 U 1 5.5 0.15 ug/L 05/08/20191433 Vanadium 25 U 1 25 2.5 ug/L 05/08/20191433 Zinc 2.6 J 1 10 2.5 ug/L 05/08/20191433 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 258 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - LCS Sample ID: UQ15809-002 Matrix: Aqueous Batch: 15809 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Antimony 100 100 1 102 80-120 05/08/20191439 Arsenic 100 100 1 101 80-120 05/08/20191439 Barium 100 100 1 105 80-120 05/08/20191439 Beryllium 100 100 1 103 80-120 05/08/20191439 Cadmium 100 100 1 102 80-120 05/08/20191439 Chromium 100 100 1 102 80-120 05/08/20191439 Cobalt 100 100 1 101 80-120 05/08/20191439 Copper 100 100 1 103 80-120 05/08/20191439 Lead 100 100 1 104 80-120 05/08/20191439 Nickel 100 100 1 102 80-120 05/08/20191439 Selenium 100 110 1 106 80-120 05/08/20191439 Silver 100 110 1 107 80-120 05/08/20191439 Sodium 1000 1000 1 103 80-120 05/08/20191439 Thallium 100 100 1 102 80-120 05/08/20191439 Vanadium 100 100 1 102 80-120 05/08/20191439 Zinc 100 100 1 103 80-120 05/08/20191439 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 259 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MS Sample ID: UD30018-028MS Matrix: Aqueous Batch: 15809 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Antimony 0.0 100 99 1 99 70-130 05/08/20191825 Arsenic 0.0 100 97 1 97 70-130 05/08/20191825 Barium 250 100 350 1 102 70-130 05/08/20191825 Beryllium 0.0 100 66 N 1 66 70-130 05/08/20191825 Cadmium 0.14 100 98 1 98 70-130 05/08/20191825 Chromium 0.0 100 97 1 97 70-130 05/08/20191825 Cobalt 0.0 100 94 1 94 70-130 05/08/20191825 Copper 0.0 100 95 1 95 70-130 05/08/20191825 Lead 0.0 100 100 1 102 70-130 05/08/20191825 Nickel 1.5 100 95 1 93 70-130 05/08/20191825 Selenium 0.0 100 95 1 95 70-130 05/08/20191825 Silver 0.0 100 98 1 98 70-130 05/08/20191825 Thallium 0.0 100 100 1 101 70-130 05/08/20191825 Vanadium 2.6 100 100 1 98 70-130 05/08/20191825 Zinc 3.9 100 97 1 94 70-130 05/08/20191825 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 260 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MSD Sample ID: UD30018-028MD Matrix: Aqueous Batch: 15809 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Antimony 0.0 100 94 1 94 5.1 70-130 20 05/08/20191831 Arsenic 0.0 100 95 1 95 3.0 70-130 20 05/08/20191831 Barium 250 100 340 1 92 2.9 70-130 20 05/08/20191831 Beryllium 0.0 100 64 N 1 64 3.0 70-130 20 05/08/20191831 Cadmium 0.14 100 95 1 95 3.4 70-130 20 05/08/20191831 Chromium 0.0 100 93 1 93 3.8 70-130 20 05/08/20191831 Cobalt 0.0 100 91 1 91 2.9 70-130 20 05/08/20191831 Copper 0.0 100 92 1 92 4.0 70-130 20 05/08/20191831 Lead 0.0 100 98 1 98 4.0 70-130 20 05/08/20191831 Nickel 1.5 100 93 1 91 2.0 70-130 20 05/08/20191831 Selenium 0.0 100 94 1 94 0.32 70-130 20 05/08/20191831 Silver 0.0 100 95 1 95 3.3 70-130 20 05/08/20191831 Thallium 0.0 100 97 1 97 3.5 70-130 20 05/08/20191831 Vanadium 2.6 100 97 1 94 3.4 70-130 20 05/08/20191831 Zinc 3.9 100 96 1 92 1.3 70-130 20 05/08/20191831 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 261 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MB Sample ID: UQ15810-001 Matrix: Aqueous Batch: 15810 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Parameter Result Q Dil LOQ DL Units Analysis Date Antimony 6.0 U 1 6.0 0.50 ug/L 05/08/20191848 Arsenic 10 U 1 10 1.3 ug/L 05/08/20191848 Barium 100 U 1 100 1.3 ug/L 05/08/20191848 Beryllium 1.0 U 1 1.0 0.15 ug/L 05/08/20191848 Cadmium 1.0 U 1 1.0 0.13 ug/L 05/08/20191848 Chromium 10 U 1 10 1.3 ug/L 05/08/20191848 Cobalt 10 U 1 10 1.3 ug/L 05/08/20191848 Copper 10 U 1 10 1.3 ug/L 05/08/20191848 Lead 10 U 1 10 0.25 ug/L 05/08/20191848 Nickel 50 U 1 50 1.3 ug/L 05/08/20191848 Selenium 10 U 1 10 1.3 ug/L 05/08/20191848 Silver 10 U 1 10 0.25 ug/L 05/08/20191848 Sodium 400 U 1 400 150 ug/L 05/08/20191848 Thallium 5.5 U 1 5.5 0.15 ug/L 05/08/20191848 Vanadium 25 U 1 25 2.5 ug/L 05/08/20191848 Zinc 10 U 1 10 2.5 ug/L 05/08/20191848 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 262 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - LCS Sample ID: UQ15810-002 Matrix: Aqueous Batch: 15810 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Spike Amount Result % Rec Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Antimony 100 99 1 99 80-120 05/08/20191854 Arsenic 100 100 1 100 80-120 05/08/20191854 Barium 100 100 1 100 80-120 05/08/20191854 Beryllium 100 100 1 101 80-120 05/08/20191854 Cadmium 100 100 1 100 80-120 05/08/20191854 Chromium 100 99 1 99 80-120 05/08/20191854 Cobalt 100 100 1 100 80-120 05/08/20191854 Copper 100 100 1 101 80-120 05/08/20191854 Lead 100 100 1 101 80-120 05/08/20191854 Nickel 100 100 1 101 80-120 05/08/20191854 Selenium 100 100 1 103 80-120 05/08/20191854 Silver 100 100 1 103 80-120 05/08/20191854 Sodium 1000 980 1 98 80-120 05/08/20191854 Thallium 100 100 1 103 80-120 05/08/20191854 Vanadium 100 99 1 99 80-120 05/08/20191854 Zinc 100 100 1 100 80-120 05/08/20191854 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 263 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MS Sample ID: UD30018-035MS Matrix: Aqueous Batch: 15810 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Sample Spike Amount Amount Result % Rec Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date Antimony 0.0 100 96 1 96 70-130 05/08/20191948 Arsenic 3.3 100 99 1 96 70-130 05/08/20191948 Barium 130 100 240 1 110 70-130 05/08/20191948 Beryllium 0.0 100 64 N 1 64 70-130 05/08/20191948 Cadmium 0.16 100 98 1 98 70-130 05/08/20191948 Chromium 5.3 100 100 1 97 70-130 05/08/20191948 Cobalt 11 100 110 1 94 70-130 05/08/20191948 Copper 4.1 100 100 1 97 70-130 05/08/20191948 Lead 1.9 100 100 1 102 70-130 05/08/20191948 Nickel 14 100 110 1 95 70-130 05/08/20191948 Selenium 0.0 100 96 1 96 70-130 05/08/20191948 Silver 0.0 100 100 1 101 70-130 05/08/20191948 Sodium 13000 1000 14000 N 1 164 70-130 05/08/20191948 Thallium 0.0 100 100 1 102 70-130 05/08/20191948 Vanadium 5.4 100 100 1 99 70-130 05/08/20191948 Zinc 13 100 110 1 96 70-130 05/08/20191948 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 264 of 286 QC Data for Lot Number: UD30018 ICP-MS Metals - MSD Sample ID: UD30018-035MD Matrix: Aqueous Batch: 15810 Prep Method: 3005A Analytical Method: 6020B Prep Date: 05/06/2019 1734 Sample Spike Amount Amount Result % Rec % RPD Parameter (ug/L) (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date Antimony 0.0 100 97 1 97 0.29 70-130 20 05/08/20191954 Arsenic 3.3 100 100 1 97 0.94 70-130 20 05/08/20191954 Barium 130 100 240 1 112 0.96 70-130 20 05/08/20191954 Beryllium 0.0 100 65 N 1 65 0.53 70-130 20 05/08/20191954 Cadmium 0.16 100 98 1 98 0.15 70-130 20 05/08/20191954 Chromium 5.3 100 100 1 96 0.69 70-130 20 05/08/20191954 Cobalt 11 100 100 1 94 0.38 70-130 20 05/08/20191954 Copper 4.1 100 100 1 96 0.20 70-130 20 05/08/20191954 Lead 1.9 100 100 1 101 0.48 70-130 20 05/08/20191954 Nickel 14 100 110 1 95 0.28 70-130 20 05/08/20191954 Selenium 0.0 100 96 1 96 0.38 70-130 20 05/08/20191954 Silver 0.0 100 100 1 100 0.95 70-130 20 05/08/20191954 Sodium 13000 1000 14000 N 1 180 1.1 70-130 20 05/08/20191954 Thallium 0.0 100 100 1 100 1.8 70-130 20 05/08/20191954 Vanadium 5.4 100 100 1 97 1.5 70-130 20 05/08/20191954 Zinc 13 100 110 1 95 0.18 70-130 20 05/08/20191954 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 265 of 286 QC Data for Lot Number: UD30018 CVAA - MB Sample ID: UQ15674-001 Matrix: Aqueous Batch: 15674 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1238 Parameter Result Q Dil LOQ DL Units Analysis Date Mercury 0.00020 U 1 0.00020 0.000091 mg/L 05/06/20191610 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 266 of 286 QC Data for Lot Number: UD30018 CVAA - LCS Sample ID: UQ15674-002 Matrix: Aqueous Batch: 15674 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1238 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Mercury 0.0020 0.0021 1 104 80-120 05/06/20191613 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 267 of 286 QC Data for Lot Number: UD30018 CVAA - MS Sample ID: UD30018-001MS Matrix: Aqueous Batch: 15674 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1238 Sample Spike Amount Amount Result % Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Mercury 0.00040 0.0020 0.0017 N 1 66 85-115 05/06/20191623 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 268 of 286 QC Data for Lot Number: UD30018 CVAA - MSD Sample ID: UD30018-001MD Matrix: Aqueous Batch: 15674 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1238 Sample Spike Amount Amount Result % Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date Mercury 0.00040 0.0020 0.0017 N 1 65 1.2 85-115 20 05/06/20191626 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 269 of 286 QC Data for Lot Number: UD30018 CVAA - MB Sample ID: UQ15676-001 Matrix: Aqueous Batch: 15676 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1242 Parameter Result Q Dil LOQ DL Units Analysis Date Mercury 0.00020 U 1 0.00020 0.000091 mg/L 05/06/20191515 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 270 of 286 QC Data for Lot Number: UD30018 CVAA - LCS Sample ID: UQ15676-002 Matrix: Aqueous Batch: 15676 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1242 Spike Amount Result % Rec Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Mercury 0.0020 0.0020 1 98 80-120 05/06/20191522 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 271 of 286 QC Data for Lot Number: UD30018 CVAA - MS Sample ID: UD30018-026MS Matrix: Aqueous Batch: 15676 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1242 Sample Spike Amount Amount Result % Rec Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date Mercury 0.0 0.0020 0.0016 N 1 78 85-115 05/06/20191527 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 272 of 286 QC Data for Lot Number: UD30018 CVAA - MSD Sample ID: UD30018-026MD Matrix: Aqueous Batch: 15676 Prep Method: Analytical Method: 7470A Prep Date: 05/05/2019 1242 Sample Spike Amount Amount Result % Rec % RPD Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date Mercury 0.0 0.0020 0.0015 N 1 77 0.59 85-115 20 05/06/20191530 LOQ = Limit of Quantitation DL = Detection Limit LOD = Limit of Detection P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria J = Estimated result < LOQ and > DL + = RPD is out of criteria U = Not detected at or above the detection limit Note: Calculations are performed before rounding to avoid round -off errors in calculated results Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 273 of 286 QC Data for Lot Number: UD30018 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 274 of 286 SHEALY ENVIRONMENTAL SERVICES, INC. + s n J ti� y y -13 UL.1 m L F a m a E E- r W I$ r �in98uxa�p 1'l '{ X o {} ('SiJdttrt] c E E¢ u- r 4d z Tf a [5LJ a�OCILL X a� N z _ � a3 a '� t�1�AIhL�1[;lInS+3p IL O O C4 'r OH f o,Q + s1eJoW I >rJPuarJriy x wo _ V ¢ r .dYJg `w d v aay�r} a y o U]' o wrh 4 0 c N z� o 3 = 0 m t! T m rti b 3i -: Y a 2 4 � 12 a w. ry E & c+ °° EL a F0 ,� y� r� g 3 27 J12 3.ff i j Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 275 of 286