MO-88735_91533_CA_IAR_20190424_Initial Action Abatement Report

0 '�OpROFF5510NAL CORFOR 0�
INITIAL SITE ASSESSMENT REPORT
Shiloh Church Road Heating Oil AST
3901 Shiloh Church Road
Davidson, North Carolina 28036
Prepared for:
Ms. Trudy Beverly
North Carolina DEQ
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Prepared by:
Enviro-Pro, PC
2646 Farmlake Lane
Fort Mill, South Carolina 29708
Project No. EP-1492
April 24, 2019
2646 Farmlake Lane • Fort Mill, SC 29708 • [phone] • Fax [phone]

Initial Site Assessment Report
A. Site Information
1. Site Identi#ication
~'Date of Report:
'I=aciiity I.D.: Incident Number: ��_ Site Risk.Tlo€t-L S 1 Rank:
21--aq
, ,.`'`'SiteName:slfCYC rat c � �t_ t — A T
Site Street Address:
-,C'ity/TOvrn: A lip Code: �' County:tt n1A5 �v
--Description oi'(reopraphicaf Data Point (c.g., dispenser): mot`
'E.ocation Method (GYS, topographical neap, other):_
Latitude (decimal degrees): I.on«nude (decimal de�recs):
?. Information about Contacts Associated with the Release (Addresses musl include street, city, state. zip code
and mailing address, if different,t
,US'1/AS'1 Owner:
Address
­JiST,"AS I Operator: 01,
Address: 1 ---
y ���_
'Other° Person ���ssisciatect with Re}case: 2r0
Address:
Tropert-v Owner; —5A
Addresa:"
'Property' Occt€p"uu:
Address
'C onsultsnit;C'c>ntracAr€
Address: ?
'Analytical Latx>Fato� _
Address- M/ 4ts. —Z",
Information ttbOL11 Release
})ate Discovered: __' 4--
--L
Tstiniated Quantit,
'Catrse o f Rel ease:
Source of Release
l el:
Certification No.
—Sizes and Contents of•'fank or Other Containment from which the lZelease Occurred: ��� ��of !
4. Certification (Tire titde pa e most disd)dal, the seat and signature of the certify>ing P.E. or L.G. and the name and
certification number of the corrpcareq ar corporation CSee I5A ! CAC .2L . €103(e),I)
L _I b��t�'i��S�r_. a k�rc�te5si�rnal }€rig€eer I foes€sz�i t:ir�,I�s<,,i��ir�°l��a1ie� fir �e€�isrn� ��� f:�.
di3 c i rtttZ that the iniirrntation contaiurd irr this report , ,co"cit nil <€zeur.€te to the bzst u,'ni Jtuii��Ieil c.
-- f �_ (? acne c�f-company or corporation) is licensed topracttc t gcolo�� nc�iatecrin (circle Dore or�� z P-���r
bott€) in Mort e Carolina. the certilicati�>n number ot'the company or corporatiura is
spaa4�a�
0
rl� L
;

-2_
. Site History and Characterization
The current owner of the property Iocated at 3901 Shiloh Church Road, Davidson, North
Carolina (Figure 1) is the Shiloh Church Development Group, LLC. Prior to their recent
acquisition, this property was owned by C. B. Gardner, who is now deceased. This information
is summarized on Table B-2.
Two heating oil ASTs were historically operated on this residential property, as indicated on
Figure 2. AST 41 was utilized to heat a large shed, while AST #2 was used as a heat source for
the residence. Both tanks have a 275-gallon capacity, as indicated in Table B-1. The ASTs were
identified during a Phase I Environmental Site Assessment of the properly conducted by Enviro-
Pro, P.C. (EP) dated January 4, 2019 and a recommendation was made to sample around both.
tanks. Preliminary soil sampling in the immediate vicinity of both ASTs by Enviro-Pro, PC (EP)
personnel on February 26, 2019 indicated a petroleum release associated with AST #1, but no
significant contamination around AST 42. Table B-3(1) summarizes the initial soil sampling
laboratory results and the laboratory reports are included in Appendix D.
C. Free Product Investigation and Recovery Report
During this initial site assessment no groundwater was encountered. It appears that petroleum
contamination is limited to the soil and has not impacted groundwater, which is estimated to be
between 25 and 35 feet below ground surface (bgs) at this site.
D. Groundwater and Surface Water Investigation
The deepest soil boring advanced in the vicinity of heating oil AST #1 was 15 feet bgs. No
groundwater or bedrock was encountered in this boring and it does not appear that soil
contamination extends beyond a depth of around 10 feet bgs.

E. Initial Response and Abatement Actions
In order to confirm the preliminary shallow soil sampling results in the vicinity of AST #1, a
Geoprobe was utilized to collect soil samples from depths of 8 to 10 feet bgs at four locations
around the tank on March 11,2019. The laboratory results of this sampling are summarized on
Table B-3(2) and are included in Appendix D.
Upon receipt of these laboratory results, EP submitted a Notification of Discharge Report
(Appendix A) to Ms. Trudy Beverly with the North Carolina DEQ on March 27, 2019_
Both AST 41 and AST #2 appeared to be in good condition and no visual signs of leaking
heating oil were observed. Both tanks also appear to be empty of product.
F. Excavation of Contaminated Soil
Utilizing the results of the Geoprobe soil sampling conducted on March 11, EP personnel used a
Mini Excavator to remove soils directly beneath AST #1 on March 29, 2019. Photographs of the
soil excavation before, during, and after are included in Appendix B. A total of 4.52 tons of
petroleum contaminated soil was loaded onto a dump trailer and transported to Environmental
Soils, .Inc. in Lattimore, North Carolina for disposal. A Non -Hazardous Waste Manifest for the
soil disposal is included in Appendix C.
The final dimensions of the excavation were approximately four feet wide by six feet long by 10
feet deep. EP personnel collected soil samples from each sidewall and the base of the excavation
at a depth of approximately 10 feet bgs. No groundwater or bedrock were encountered in the
excavation. Clean disposable gloves were utilized to collect each sample and only laboratory -
supplied sample containers were used. Soil samples were packed on ice in a cooler and
transported to the Shealy Environmental Services laboratory facility in West Columbia, South
Carolina. All five soil samples were analyzed for volatiles (EPA 8260D), semi-volatiles (EPA
8270E), VPH (MADEP), and EPH (MADEP). The laboratory results are summarized in Table
B-3(3) and are included in Appendix D. The excavation was backfilled with clean soil from
another area on site.

-4-
G. Conclusions
Confirmatory soil sampling within the soil excavation indicate that all petroleum contamination
associated with the historical operation of the heating oil tank AST #1 has been successfully
removed. Since no groundwater or bedrock was encountered during the soil excavation, no
further action. should be required at this site.
H. Figures
Figure 1: Site Location and Topographic Map
Figure 2: Site and Vicinity Map
. Tables
Table B-1: Site history -- UST/AST System and Other Release Information
Table B-2. Site History— UST/AST Owner/Operator and Other Responsible Party Information
Table B-3(1): Summary of Soil Sampling Results
Table B--3(2): Summary of Soil Sampling Results
Table B-3(3): Summary of Soil Sampling Results
�
Appendix A: Notification of Discharge Report
Appendix B: Site Excavation Activities
Appendix C: Soil Disposal Waste Manifest
Appendix D: Shealy Laboratory Reports

FIGURE 1: SITE LOCATION AND TOPOGRAPHIC MAP
3901 and 3821 Shiloh Church Road
Davidson, North Carolina
DRAWN BY: I SCALE: P=2,000'
CiC BY: PROD NC: EP-1487
PROJ MGR: THB FILE NAME:
DATE: 1/3/19 rs�

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Table -2: Site History o USUAST Owner/Operator and Other Responsible
Party Information
Revision Bate: Incident Number and Name: 5kikA (,kv vcX Ro,4
L4ea:ti q ON ivs'r
UST ID Facility ED
Number Number IA
Owner Naine (and Contact) Dates of Operation
mm/y)dad} /y n to mm/dd! )
V��f�V� �'��=�1-'Yl 1��'4«1 �°G ii� 3��'PC F�4/ YVi�i.ir'. t/i!✓li V. VIP✓'i.
Street Address
city State Zip Telephone Number
M0- AkO
Operator Name (and Contact) Dates of Operation
m/dd/ to mm/dd/
Street Address
city State Zip Telephone Number
e, 2-s, 4
t ° Heide`' is site r 1 1ose roil . P
Incident Date Incident
Nuunber MIA Occurred
Name of Responsible Party Date Incident
for Other Incident Reported
Date Incident
Closed (ila)
Street Address
city State Zip Telephone Number
Add additional records for all owners, operalors and responsible parries as necessary.

Notification of Discharge Report
1. o f die of Dischame Reglort
Appendix A
Report Formats
UST-62 [_ our Motifileation of Discharge
For M -t., 57 This form should be completed and submitted to the LIST Section's regional office follao.,ing a knovan or suspected
Releases ®f release of petroleum from a source other than an underground storage tank. This form is required to be submitted
Pe-tireloum in NG within 24 hours of discovery of a known or suspected petroleum release
(DWW, USE ONLY)
Incident// Priority Rank (H,l,L,U)
Received (time/date)
Received by Region
Reported by (circle cane), Phone, Fax or Report
Incident Name
-
Address (street number/name) �� I
City/Tovm
Latitude (decimal degrees)
Describe suspected or confirmed release
product
Suspected Contamination? (YIN) _-
Confirmed GW Contamination? (YIN)
Confirmed Soil Contamination ?(YIN) __--
Samples take0(,Y/N) _ tree product? (YIN]
It Yes('reu product) state greatest thickness. _.__ — feet
INCi T DESCRIPTION
� 5 --- __ -
I County.
Zip Code. a. Hcgc onal Office (circle one).
Ralei n Washin ion ;Nilrnfr
Longitude (decimal degrees] - S-be
relevse, {f e/dale of release goantity of ,• rieass_ Hmount of tree
_._ ---
i:? s ritsc niivat t msc'ahatenicrrt (t1m. 1d raleast stopp£d c e.: - p bcigupcompob quantr y or product soil a-
rjerrroved, conirrmafion samptlrcij�'_
Dcscrilxinipa.IiA ry cot, r. - -
OW RELEASE WAS DISCOVERED (Release Code)
(Cock one)
Cf Observation of Re'ease at Occurrence t tutor Supply'€rieil Contamination
iJ Visual or Olfactory Evidence JSurEace'1,ialer Contamination
Soal Contamination Jother (specify)
€J Groundvrater Contamination
Source of Release
(Check
One to 111jiCale rinnian,
S'Alrcel
AST (tank)
LJ
AST Piping/ Dispenser
U
AST Delivery Problem
!•1
O FR Vehicle Tank
0
OTR Sulk Transport Tank
J
RR Buk Transport Tank
!
Transformer
J
Unbnov,
J
Other
Definitions presenters on reverse
1 Municipal 2 Mirtary 3
Q ae-Han T_yp e
1 Public Service 2 Agricullum
Guidance presented on reverse
UST Form 62 (041 00)
SOURCE OF CONTAMNATION
Cause of Pelease Type of Release
Wheck one to indicate pnman cause) (('hctk one)
J Spiel (Accrc!ental) Petrcieum
J
Spill (intentional)
J Cloth Petroieurrr
J
Corrosion
& lion-Petroleurn
J
Phystcal or Mechamcal
Damage
Location
.J
Lquipment Failure
(Checl, one)
AST Overfill
J
AST Installation Problem
J .citify
�j
Unlcnot+rn
€da?n<uP
J
Otherr ._._—
J Higliviayi, ,Do
J Railway
prE:SP.f`ttzaf onff,V£:r5rr'
J Other
4 Pnvaie-,iS Federal 6 County i State
Release discovered
tirneldate
r 1ltta�rrcd he
J GPS
JEfectron€c top-ographic map
J GIS Address matching
.Other tlCsrae�[��
J Unkno%, n
llczci7ite l���ast€�fn�j y
Product Type Released
(('hctk ,,ne to to l€t:.rte pntnar, pt:tri,lcur q r(xiuct r p�
16mscd r
J Gasoline/ Diesetl
Kerosene
U E11 -L20
.J L21 - F 84
J E85 - L99
J Ethanol lDU o
Education+Zelicg 5 Inclustnal 0 Commercial 7 iMining
J DieselNeg Oil
Blend
J Vegetable Oil 100ag
Heating Ors
J Waste Oil
J klinem I Oif-no PCBs
? Mineral oikpcss
J Other Petroleum
Products
Page I of 2
60 C 11an�� l

Notification of Discharge Report appendix A
Report Fon-nats
IMPACT ON' DRDMIKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes k 2. No ; 3. Unknwin Number of plater Supply Wells Affected
List of Water Supply 'Wens Contaminated (fncfuds Users fWames, Addresses an
1. d Phone Numbers. Attach additional sheet if necessary)
2.
3
PARTY RESPONSIBLE FOR RELEASE
(if the source of tfte release is not an AST system or if it is an AST system and there is a responsible party other than the AST system owrner/ operatcr)
-_ `^Y �_-__- j—.r:.w_�— ._......___ w.rZ...-_sr4OF.FG'_-.!__.�-f.d,.... _L7./_�E-__.�74�
City , L�'v I State i Zip Cacle� �i hor g
-� j -
�� R(f ff3e source of the rele Fs an AST system)
AST OwnerFCgqmpan • "- -- m_ __�__---_ _1 Address — � —
I . r 1. 1 ) Z...._ 1 _ 1" � _ . � P7 , � 3 �---, / t -,? [ I
State �' Zip Code r- _.,. __ f.._.s��._— -_
4, _ T e.pht�ne tvt�ml er
AST SYSTEM OPER TORfif rite source of the rt lease is ,art AST systen?)
ST __--
paratori om�gpany � Address ,, j f
Cit i i Zip Code Telephone
LANDOWNER 71 t_C3CA IBN OF INME T
LGndo��ner t p I Address
t
ity atat� • ; Zi Cate f e3 .tm -Number —
i 71, -^ fi
Draw ie€;$E of Areaor Provide Mp{sf371vin the=deaf site. focataon of reset se_ faro Mi3jer road intersections. potenti'al receptors)
Attach sketrtt or map to farm
Co
- r Give DiFOCt OnS 'M InCide: It Site Atfcc,h dlrnctiars t,,) form if necass<arl
art L-%I'Ake 't; rI5 it '3�'rbtres��- e "kh
Y- qfPVPX, �. ;I � �1�� is �i�e lc � josh- ��4vekin_qsvt bh
Person Reporting In idea i Carrtt %:n}r Telephone
__? 1" - Nrnhr
Title i Address,[late
UST Form 62lli,-, Page
Definitions of sources �
A,, i (lank) means the tattle is used D' atllre 1,a,drtLt
AST Piping means the piping and conneonor, , niimint, th,oi the lank to the dts!tenai:r ur .,ther cnd-u,e Lquipmew
AST Dispenses includes the dispen,er and the equipment u,ed to cunn ,:I the di,pen,e, to the piping
AST I?dnery Prohient idenillie; relcasc, that cn urrrd dur-:ng. txiuiucr deh%Vn to the tank
01R Vehicle "I'ank moans the tank is used to!,tore prOduet W fUCI ,tn rwe°r tits read %Ch:cis
0 JR Bulk "I'ransport "Tank means a tank that v, u,ed i�, iran%.rort prodtact in t,uik ,,.cr the r. id dv, truck i
RR bulk Transp«ti Tattle nieam a tank that rs used CE, u.tlt,pnrt 111�.uuct ut btiik €+ tt.iln
1,rensforincr moans eJe�it7e:ti Iran iirtnter
Other set':csa.,tPivoplionfoum: +,,hcn dictelca3.c«,wLet,kno,'%ltlike «E>rtitmi.E,rtc.,(dcpre,:CJED, tittr,,,rt
ttnknimit ,dendties �shich thL s wu :c han n,4 ki:�Jclemank:d
Definl€3 is of f lmc£ ,
1ptJl ihcndentttlj use do, i4m-e %xiten:, "pill E�ccetr. �s c,tteaEk,iltte t' .vheit thedehcct ""h„,c a, ch--ar:ected Jjunt .r tilt pipe;
Spill (lntentton: J ) us' tht� cause when a s ill ~Euctsr. asteatttEatalt 3 (c-�' . ;rttent,,,nsl ciusttpmti ,a :,rc i.;a„tI
c.'ojl'ortoa use •: 'ni a ntet<tt ptpnng, E3n v€her Q,fflI,e'ICntt Jt .':tt ;`(:F,;c duo 11.
Phgsieai car t lecham"I Dania!?u use 3E11 it t-p,. E,I t,he.;ea! =r r t.c!runrc 1 anst.v•c_ i _ii,t .
i-qutpnica! Patio ne e5_ �%hGte a reJea .. tisn :; disc F, e,la,,; tttent r.�._ir � thu tl�art �.aE.,+ran C?ra�u�.t! wr3a�
A57 Overt1LE nertinl �.�u4ust rp.,V,Ccklr nI)c tjnor hc:a tht n r_- !,IIIhol rt ;he 3t,}�enae; 3
AST Jltsialla€ton ProMmi tie %then the proi,Irn; t ettmiluteu tc. Itne o, ,x reel !,C.3u -c t,jle As 1 ;tent .4t;; tint an rt!Icd pi,t
Olhcr use this LEplion k%hen the anus: i, 1tito:at !-t dr,e, nut nit nao ,air E,S the prccednr-
t rtJaxttal use Mien the cause h-�noI t,c�r. dcicrnssntd
Guidarcr: Owncr.%hip and Operator .lype
f wnershtp belecl Elte categc,r% %%htch de,crIhc, o"TwT Eat the A,� J �sstctn, hulh to tk ol, � alter- retcasr 4nurce
i)iicr8litr I", i7l 5?lCt l the i 1th ,1trr V.j1€CI3 CSCriJ3e5 flit l?(1Cf llt.,t[ i❑ M.10. omer the A - f CZ ti';(' n hu1e; E n'?Sl=ot1 i3p'{'(_ ;tf E�i:3[i rCl� ISc tt3(lNe
2
t htimw 1

'all Uri

Photo 1: Residential heating oil AST prior to removal.
Photo 2: Excavation of contaminated soil beneath the heating oil AST.

Photo 3. Backfilled soil excavation area.

_ a)�� �3
�- 3 -

Environmental Soils Inc.
PO Box 295 ® Lattimore, IBC 28089
Phone [phone] ° Fax [phone]
/ Non -hazardous Taste Manifest ,� # =
Date _3 AM O / 7 Load Dumber
(numbered sequentially as trucks are dispatched)
Fax:��
Address: . % . r � 5x t,. /&C, County: A15� v �-_5
Contact: Phone:
XST®. G1N,4TTGNP®INT. Complete Address: 3201
vt C_ 2Sv
Class &Type of Contaminate in soil i 0(cZ i
SOURCE OF C0NTX i MTION..• (ex. UST or other source) A:5-F
GENERATORS CERTIRIC-4TION OF WASTE CONSTITUENTS ENT=S: In lien of submitting analytical data (methods
S24 nd S270) vereyingthatihewaste in question does not contain organic constituents other than those which would
no rin tally ca pear in analysis of virgin etroleumproduct residue, I aria submitting this Certificate of Waste
Constituents. I cert that I rani fcanailicar with the source of contcamin ation of the soil sand fiurther certiry the source, to
the best of nzy knoqvledge, contains no contaanain ants other than that &ted above.
Generators Si
$ S 1OR ER
Date:
Contact: # ,"OIL � 1". Phone: •— 57I
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date: %-2 q �t
TRUCK #: AG #l: VOLUME:
TRUCK DRIVER SIGNATURE: DATE:-3129 b S
3ES7" ,4TION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit 4SR0300038
I certify that the carries- has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: g Date:/n,
� C
Signature: ra Date:
Company l
Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

�, ¢ _ � - �-
i �

Enviro-Pro, P.C.
2646 Farmlake Lane
Fort Mill, SC 29708
Attention: Tom Bolyard
Project Name: Shileh Res.
Project Number: P-1489
Lot Nurrlber:UB27071
Date Completed:03/05/2019
A - S C';'�\ t
03/06/2019 3:54 PM
Approved and released by:
Project Manager: Nisreen Saikaly
�/
Yt
a CC �E D, T ED
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wmv.shealylab.com
Page 1 of 16

ENVIRONMENTALSHEALY SERVICES, INC.
5C DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Caste Narrative
Enviro-Pro, P.C.
Lot Number: UB27071
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NEL.AC standards, the Shealy Environmental Services, Inc. ('Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies, Any
exceptions to the NEtAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
D RO
Dilutions greater than 5X impact the surrogate recoveries, thus negating their usefulness concerning
quality control. The sample results are reported and no corrective action is required.
The matrix spike and matrix spike duplicate (MSIMSD) recoveries in batch 99135 were outside
acceptance criteria. All other QC criteria for the batch was within acceptance criteria and method control
limits. The MSIMSD recovery results are attributed to matrix interference. The associated sample results
were reported and no corrective action was required.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] umnv.shealylab.com
Page 2 of 16

Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
SS-1
Solid
02/26120191200
02127/2019
002
SS-2
Solid
02126120191210
02/27/2019
003
SS-3
Solid
02/26120191220
02/27/2019
004
SS-4
Solid
02/26120191230
02/27/2019
(4 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] w w✓.shealylab,com
Page 3 of 16

Detection Summary
Envir®-Pro, P.C.
Lot Number: UB27071
Sample Sample ID
Matrix
Parameter
Method
Result
Q
Units
Page
001 SS-1
Solid
TPH-DRO
8015C
13000000
B
uglkg
5
002 SS-2
Solid
TPH-DRO
8015C
890000
B
uglkg
6
003 SS-3
Solid
TPH-DRO
8015C
8300
B
uglkg
7
004 SS-4
Solid
TPH-DRO
8015C
6100
BJ
uglkg
8
(4 detections)
Shealy Environmental Services, inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 4 of 16

Client:Bnviro-Pro, P.C, Laboratory ID:UB27071-001
Description: SS-1 Matrix: Solid
Date Sampled:0212612019 1200 % Solids: 36.2 02/28/2019 0132
Date Received:0212712019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 10 03/04/2019 1656 CHG 03/03/2019 2247 99135
CAS Analytical
Parameter Number Method Result Q LOQ DL units Run
TPH-DRO 8015C 13000000 B 77000 29000 uglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl N 328 55-120
LOQ = Limit of Quantitalion B = Detected in the method blank E = Quantltation of compound exceeded the calibration range DL W Detection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4M'� J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis �.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvvw.sheaiylab,com
Page 5 of 16

Client: Enviro-Pro, P.C. Laboratory ID: UB27071-002
Description: SS-2 Matrix: Solid
Date Sampled:0212612019 1210 % Solids: 89.4 02128/2019 0132
Date Received: 0212712019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/04/2019 1559 CHG 03/03/2019 2247 99135
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TPH-DRO 8015C 390000 B 7300 2700 uglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl 100 55-120
LOO = Limit of Ouantdalion 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Delection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 405`6 J = Estmated result - LOD and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wwvr.sheatylald com
Page 6 of 16

Client: Enviro•Pro, P.C. Laboratory ID: UB27071-003
Description: SS-3 Matrix: Solid
Date Sampled:0212612019 1220 % Solids: 90.5 02/28/2019 0132
Date Received:0212712019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/04/2019 1618 CHG 03/03/2019 2247 99135
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TPH-DRO 8015C 8300 B 7400 2700 uglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl 78 55-120
L04 = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery is out of cnler€a P = The RPD behieen two GC columns exceeds 4M'c J = Estimated result c LOD and a ©L
H = Out of holding lime W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab,corn
Page 7 of 16

Client: Enviro-Pro, P.C. Laboratory lD: UB27071-004
Description: SS-4 Matrix: Solid
Date Sampled:0212612019 1230 % Solids: 88.1 02/2812019 0132
Date Received:02127/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/04/2019 1637 C G 03/03/2019 2247 99135
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TPH-DRO 8015C 6100 BJ 7500 2800 uglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl 77 55-120
LOO = Limit of Quantilation e = Detected in the method btenk E = Quantltation of compound exceeded the calibration range DL = Datection Limit
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40', J = Estimated result < LOQ and > DL
H = Out of holding time W= Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www shealyiab cam
Page 8 of 16

Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,sheolylab,com
Page 9of16

Sample ID: UQ99135-001 Matrix: Solid
Batch: 99135 Prep Method: 3550C
Analytical Method: 8015C Prep Date: 03/03/2019 2247
Parameter Result Q Dil LOQ DL Units Analysis Date
TPH-DRO 2600 J 1 6700 2600 uglkg 03104/20191034
Surrogate Q % Rec Acceptance
Limit
o - Terphenyl 99 55-120
LOG = Limit of Ouantitation P = The RPD between two GC columns exceeds 404o N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOG and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the OL
Note: Calculations are Performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wwty shealylab,com
Page 10 of 16

Sample ID: UQ99135-002
Matrix: Solid
Batch.99135
Prep method: 3550C
Analytical method: 8015C
Prep Date: 03/03/2019 2247
Spike
Amount
Result
% Rec
Parameter
tug/kg)
(uglkg) Q
Dil % Rec Limit Analysis Date
TPH-13R0
83000
72000
1 86 70-130 03104/20191053
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl 105 55-120
LOD = Limit of Quantnation P = The RPO between two CC columns exceeds 4M1. N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOO and a DL + = RPp is out of mtena
LOD = Limit of Detection NO = Not detected at or above the OL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wyw shealylab.com
Page I i of 16

Sam pfe ID: UB27071 -001 MS
Matrix: Solid
Batch: 99135
Prep Method: 3550C
Analytical Method: 8015C
Prep Date: 03/03/2019 2247
Sample
Spike
Amount
Amount
Result % Rec
Parameter
(uglkg)
(uglkg)
(uglkg) Q Dil % Roc Limit Analysis Date
TPH-DRO
13000000
95000
10000000 N 10 -2840 70-130 03104/20191715
Surrogate
Q % Roc
Acceptance
Limit
o - Terphenyl N 282 55-120
LOQ = Limit of Quantilation P = The RPD between two GC columns exceeds 40% N = Recovery is out of cnlena
OL = Detection Limit J = Estimated resutt < LOQ and > DL . = RPD is out of entena
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.sheatyiab,com
Page 12 of 16

Sample ID: UB27071-001MD Matrix: Solid
Batch: 99135 Prep Method: 3550C
Analytical Method: 8015C Prep Date: 03/03/2019 2247
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (uglk9) (u9rk9) (uglkg) Q pil % Rec % RPD Limit limit --Analysis Date
TPH-DRO 13000000 96000 7400000 N,+ 10 -5880 33 70-130 20 03/04/2019 1735
Surrogate
o - Terphenyl
LOQ = Limit of Cluantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Roc Limit
N 226 55-120
P = The RPD between two GC columns exceeds Oft,, N = Recovery is out of criteria
J = Estimated recuit < LOQ and > DL + = RPD is out of criteria
NO = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab com
Page 13 of 16

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Enviro-Pro, P.C.
2646 Farmlake Lane
Fort Mill, SC 29708
Attention: Tom Bolyard
Project Name: Shiloh Res.
Project Number: FP-1492
Lot Number:UC12075
Date Completed:03/15/2019
A-SC'\t
03/18/2019 8.58 AM
Approved and released by:
Project Manager: Nisreen Saikaly
An¢©,B
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point thrive West Columbia, SC 29172 [phone] Fax [phone] vrvnv.shealytab.wrn
Page t of 15

ENVIRONMENTALSHEALY
i INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Enviro-Pro, P.C.
Lot Plumber: UC12075
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W°
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Shealy Environmental Services, Inc,
106 Vantage Point Drive west Columbia, SC 29172 [phone] Fax [phone] vivwshealyiab.com
Page 2 of 15

SHEALT ENVIRONMENTAL SVC -S. I
Sample Summary
Enviro-Pro, P.C.
Lot Number, UC12075
Sample Number
Sample ID
Matrix
Date Sampled
Elate Received
001
GP-1(3`)
Solid
03/11120191200
03/12/2019
002
GP-1(10')
Solid
03111120191240
03/12/2019
003
GP-2
Solid
03/11/20191210
03/12/2019
004
GP-3
Solid
03111/20191220
03/12/2019
005
GP-4
Solid
03/11/20191230
03/1212019
(5 samples)
Shealy Environmental Services, Inc
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 15

{
Detection Summary
Enviro-Pro, P.C.
Lot Number: UC12075
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001 GP-1(3')
Solid
TPH-DRO
8015C
91000
uglkg
5
002 GP-1(10')
Solid
TPH-DRO
8015C
4200 J
ug/kg
6
005 GP-4
Solid
TPH-DRO
8015C
11000
ugtkg
9
(3 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] www.shealyiab,com
Page 4 of 15

T'PH - CAR®
Client:Bnviro-Pro, P.C. Laboratory ID:UC12075-001
Description: GP-1(3') Matrix: Solid
Date Sampled:0311112019 1200 % Solids: 83.7 03/13/2019 0100
Date Received:0311212019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/14/2019 1216 CHG 03/13/2019 2138 10200
...................-
CAS Analytical
Parameter Plumber Method Result Q LOQ DL Units Run
TPH-DRO 8015C 91000 8000 3000 ugfkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl
87 55-120
LOQ = Limit of Quantitabon 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not datected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds Q la J = Estimated result , LQQ and > DL
H = Out of holding time W = Reported an wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Pate 5 of 15

Client: Enviro-Pro, P.C. Laboratory ID: UC12075-002
Description: GP-1(10') Matrix: Solid
Date Sampled:0311112019 1240 °'o Solids: 89.8 03/13/2019 0100
Date Received: 03/1212019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/14/2019 1235 CHG 03/13/2019 2138 10200
CAS Analytical
Parameter Plumber Method Result Q LOQ OL Units Run
TPH-DRO 8015C 4200 J 7400 2800 uglkg 1
Run 1 Acceptance
Surrogate 0 % Recovery Limits
o - Terphenyl
84 55-120
LOQ = Limit of Quantitalion 8 = Detected in the method b€ank E = QuaNilation of compound exceeded the calibrat€on range OL = Oetection Limit
ND = Not detected at or above the OL N = Recovery is out of criteria P = The RPiD between Vm GC columns exceeds 4051 J = Estimated result c LOQ and > DL
H = Out of holding time W = Reported on vret weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv,shealylab,com
Page 6 of 15

Client: Enviro-Pro, P.C. Laboratory ID: UC12075-003
Description: GP-2 Matrix: Solid
Date Sarnpled:0311112019 1210 % Solids: 77.1 03/1312019 0100
Date Received:0311212019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/14/2019 1254 CHG 03/13/2019 2138 10200
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TPH-DRO 8015C ND 8700 3200 ugtkg 1
Run i Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl 82 55-120
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
ND = Not detected at or above the DL N = Recovery rs out of criteria P = The RPD between two GC corumns exceeds 40% J = Estimated result < LOQ and > DL
H = Out at holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] flax [phone] www,shealylab.com
Page 7 of 15

Client: Enviro-Pro, P.C. Laboratory 1D: UC12075-004
Description: GP-3 Matrix: Solid
Date Sampled:0311112019 1220 % Solids: 73.9 03/13/2019 0100
Date Received: 0311212019
Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/14/2019 1313 CHG 03/13/2019 2138 10200
CAS Analytical
Parameter Plumber Method Result Q LCIQ DL Units Run
TPH-DRQ 8015C IND 8500 3200 uglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl 89 55-120
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ❑L = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% J = Estimated result t LOQ and a OL
H = Out of holding time W W Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wmv.shealylab,com
Page 8 of 15

Client:Enviro-Pro, P.C. Laboratory ID: UC12075-005
Description: GP-4 Matrix: Solid
Date Sampled:0311112019 1230 % Solids: 85.5 03113/2019 0100
Date Received:0311212019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 8015C 1 03/14/2019 1332 CHG 03/13/2019 2138 10200
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
TPH-DRO 8015C 11000 7600 2800 uglkg 1
Surrogate
o - Terphenyl
Run 1 Acceptance
Q % Recovery Limits
87 55-120
LOQ = Limit of Quanitation B = Detected in the method blank E = Quantization of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the OL N = Recovery is out of cn is P = The RPD between two GC columns exceeds 40% J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Pax [phone] wwvv.shealylab.com
Page 9 of 15

Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, 8C 29172 [phone] Fax [phone] www shealylab.com
Page 10 of 15

Sample ID: UQ10200-001 matrix: Solid
Batch:10200 Prep method: 3550C
Analytical method: 8015C Prep Date: 03/13/2019 2138
Parameter Result Q Dil LQQ DL Units Analysis Date
TPH-DRO ND 1 6700 2500 uglkg 03114120191041
Surrogate
o - Terphenyl
LOQ = Limit of Quantilation
DL = Detection Limit
LOD = Limlt of Detection
Acceptance
Q % Rec Limit
95 55-120
P = The RPO behveen two GC columns exceeds 409'o N = Recovery io out of criteria
J w Estimated result K LOO and > OL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed lofore rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page l 1 of 15

Sample ID: IJQ10200-002
Matrix: Solid
Batch: 10200
Prep Method: 3550C
Analytical Method: 8015C
Prep Date; 03/13/2019 2138
Spike
Amount
Result
% Rec
Parameter
(uglkg)
(uglkg) Q
oil % Rec Limit Analysis Date
TPH-DRO
83000
69000
1 83 70-130 03/14/20191100
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyi
LOQ = Limit of Quanlitation
DL W Detection Limit
LOD = Limit of Detection
95 55-120
P = The RPD between two GC columns exceeds 4095 N = Recovery is out of cnteria
J = Estimated result < LOCI and > DL + = RPD is out of criteria
No » Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 12 of 15

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Enviro-Pro, P.C.
2646 Farmlake Lane
Fort Mill, SC 29700
Attention: Tom Bolyard
Project Name: Shilo Residence
Project Number: EP-1492
Lot Number:UD0103
Date Completed:0411112019
Project Manager.Nisreen Saika y
04/11/2019 4:18 PM
Approved and released by:
Project Manager: Kelly M. Nance
A
A16
A.GCREP3TfD
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive Writ Columbia, SC 29172 [phone] Fax [phone] =Ni.shealylab.com
Page I of 78

SHEALY ENVIRONMENTAL I , INC.
SC OHEC No: 32010DO1 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Enviro-Pro, P.C.
Lot Number: UD01039
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "V11"
qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
volatiles
The RPM for chloromethane and dichlorodifluoromethane exceeded method control limits in batch 12345;
however, all other criteria for this compound in the laboratory control samplellaboratory control sample
duplicate (LCSILCS©) were within acceptance criteria and method control limits. The associated sample
results were reported and no corrective action was required.
MADEP VPH
Sample -004 had the surrogate 2,5-dibromotoluene recovered above the acceptance limits. This reflects a
high bias for compounds associated with this surrogate. There were no detections in the sample;
therefore, there is no impact on data quality and no corrective action is required.
Shealy Environmental Services, Inc.
106 Vantage Point Drive west Columbia. SC 29172 [phone] Fax [phone] vNimshealylab.corn
Page 2 of 78

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Enviro-Pro, P.C.
Lot Number, UD01039
Sample Number
Sample ID
Matrix
Date Sampled
❑ate Received
001
SS-1
Solid
03129120191145
04/01/2019
002
SS-2
Solid
03/29/20191155
04/01/2019
003
SS-3
Solid
03129/20191200
04/01/2019
004
SS-4
Solid
03129/20191210
04/01/2019
005
SS-5
Solid
03129/20191215
04/01/2019
(5 samples)
Shealy Environmental Services, Inc.
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www shealylab.com
Page 3 of 78

�`� �� I - I SERVICES,
INC.-
Detection Summary
Enviro-Pro, P.C.
Lot Number: UD01039
Sample Sample ID Matrix Parameter Method Result Q Units Page
(n detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab,com
Page 4 of 78

Client: Enviro-Pro, P.C. Laboratory ID: UD01039-001
Description: SS-1 Matrix: Solid
Date Sampled:0312912019 1145 °fo Solids: 04.0 04/02/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 04/04/2019 0102 MNS 12204 5A5
Parameter
CAS
Number
Analytical
Method
Result Q
LOQ
Units
Run
Acetone
67-64-1
8260D
ND
23
uglkg
1
Benzene
71-43-2
8260D
ND
5.8
uglkg
1
Bromodichloromethane
75-27-4
8260D
ND
5.8
uglkg
1
Bromoform
75-25-2
8260D
ND
5.8
uglkg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
5.8
uglkg
1
2-Butanone (MEK)
78-93-3
8260D
ND
23
uglkg
1
Carbon disulfide
75-15-0
8260D
ND
5.8
uglkg
1
Carbon tetrachloride
56-23-5
8260D
ND
5.8
uglkg
1
Chlorobenzene
108-90-7
8260D
NO
5.8
uglkg
1
Chloroethane
75-00-3
8260D
ND
5.8
uglkg
1
Chloroform
67-56-3
8260D
ND
5.8
uglkg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
5.8
uglkg
1
Cyclohexane
110-82-7
8260D
ND
5.8
uglkg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
5.8
uglkg
1
Dib€omochloromethane
124-48-1
8260D
ND
5.8
uglkg
1
1,2-Dibromoethane (EDB)
108-93-4
8260D
ND
5.8
uglkg
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
5.8
uglkg
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
5.8
uglkg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
5.8
uglkg
1
Dichl orod ifl uoromethane
75-71-8
8260D
ND
5.8
uglkg
1
1,1-Dichloroethane
75-34-3
8260D
ND
5.8
uglkg
1
1,2-Dichloroethane
107-06-2
8260D
NO
5.8
uglkg
1
1,1-Dichloroethene
75-35-4
8260D
ND
5.8
uglkg
1
cis-1,2-Dichloroethene
156-59-2
8260D
ND
5.8
uglkg
1
trans-1,2-Dichloroethene
155-60-5
8260D
ND
5.8
uglkg
1
1,2-Dichloropropane
78-87-5
8260D
ND
5.8
uglkg
1
cis- 1,3-Dichlorepropene
10061-01-5
8260D
ND
5.8
uglkg
1
trans- l,3-Dichloropropene
10061-02-6
8260D
ND
5.8
uglkg
1
Ethylbenzene
100-41-4
8260D
ND
5.8
uglkg
1
2-Hexanone
591-78-6
8260D
ND
12
uglkg
1
Isopropylbenzene
98-82-8
8260D
ND
5.8
uglkg
1
Methyl acetate
79-20-9
8260D
ND
5.8
uglkg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
5.8
uglkg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
12
uglkg
1
Methylcyclohexane
108-87-2
8260D
ND
5.8
uglkg
1
Methylene chloride
75-09-2
8260D
ND
5.8
uglkg
1
Styrene
100-42-5
8260D
ND
5.8
uglkg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
5.8
uglkg
1
Tetrachloroethene
127-18-4
8260D
ND
5.8
uglkg
1
Toiuene
108-88-3
8260D
ND
5.8
uglkg
1
1,1,2-Trichloro-1,2,2- ritluoroethane
76-13-1
8260D
ND
5.8
uglkg
1
1,2,4-Trichlo robe nzene
120-82-1
8260D
ND
5.8
uglkg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
5.8
uglkg
1
1,1,2-Trichloroethane
79-00-5
82601)
NO
5.8
uglkg
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of cnteria
P = The Ri i two GC columns exceeds 4D%
H = Out of holding time W = Reported on suet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Orive West Columbia, SC 29172 [phone] Fax [phone] wvhv.shealylab.com
Page 5 of 78

Client: Enviro-Pro, P.C. Laboratory ID: UD01039-001
Description: SS-1 Matrix: Solid
Date Sampled:03129/2019 1145 % Solids: 84.0 04/02/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 04/04/2019 0102 MINIS 12204 5.15
CAS
Analytical
Parameter
Plumber
Method
Result
LOQ
Units
Run
Trichloroethene
79-01-6
8260D
ND
5.8
uglkg
1
Trichloroftuoromethane
75-69-4
8260D
ND
5.8
uglkg
1
Vinyl chloride
75-01-4
8260D
ND
5.8
uglkg
1
Xylenes (total)
1330-20-7
8260D
ND
12
uglkg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
Bromofluorobenzene
104
47-138
12-Dichloroethane-d4
93
53-142
Toluene-d8
101
68-124
1-00 = Limit of Cuantitation B = Detected in the method blank E = Quanfitstion of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4V'b
H = Out of holding time W = Reported an wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 78

r
Client: Env! ro-Pro, P.C. Laboratory ID: UDO1039.001
Description: SS-1 Matrix: Solid
Date Sampled:0312912019 1145 % Solids: 34.0 04/0212019 0253
Date Received:0410112019
Run Prep i Gthod Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 04/0512019 1913 JCG 04/03/2019 2212 12197
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
16
uglkg
1
Acenaphthylene
208-96-8
8270E
ND
16
uglkg
1
Acetophenone
98-86-2
8270E
ND
79
uglkg
1
Anthracene
120-12-7
8270E
ND
16
uglkg
1
Atrazine
1912-24-9
8270E
N❑
79
uglkg
1
Benzaldehyde
100-52-7
8270E
ND
79
uglkg
1
Benzo(a)anthracene
56-55-3
8270E
ND
16
uglkg
1
Benzo(a)pyrene
50.32-8
8270E
ND
16
uglkg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
16
uglkg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
16
uglkg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
16
uglkg
1
1,1'-Biphenyl
92-52-4
8270E
ND
79
uglkg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
79
uglkg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
79
uglkg
1
Caprolactem
105-60-2
8270E
NO
79
uglkg
1
Carbazole
86-74-8
8270E
ND
79
uglkg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
79
uglkg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
79
uglkg
1
4-Chloroaniline
106-47-8
8270E
ND
79
uglkg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
79
uglkg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
79
uglkg
1
2-Chloronaphthalene
91-58-7
8270E
ND
79
uglkg
1
2-Chlorophenol
95-57-8
8270E
ND
79
uglkg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
79
uglkg
1
Chrysene
218-01-9
8270E
ND
16
uglkg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
16
uglkg
1
Dibenzofuran
132-64-9
8270E
ND
79
uglkg
1
3,3'-Dichlorobe nzidine
91-94-1
8270E
ND
79
uglkg
1
2,4-Dichlorophenol
120-83-2
8270E
ND
79
uglkg
1
Diethylphthalate
84-66-2
8270E
ND
79
uglkg
1
Dimethyl phthalate
131-11-3
8270E
ND
79
uglkg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
79
uglkg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
79
uglkg
1
4,6-Dinitro-2-methyiphenol
534-52-1
8270E
ND
390
uglkg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
390
uglkg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
150
uglkg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
150
uglkg
1
Di-n-octylphthalate
117-84-0
8270E
ND
79
uglkg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
79
uglkg
1
Fluoranthene
206-44-0
8270E
ND
16
uglkg
1
Fluorene
86-73-7
8270E
ND
15
uglkg
1
Hexachlorobe nzene
118-74.1
8270E
ND
79
uglkg
1
Hexachlorobutadiene
87-68-3
8270E
ND
79
uglkg
1
Hexachlorocyclopentadiene
77-47-4
8274E
ND
390
uglkg
1
LOO = Limit of Ounnlitalion B = Detected in the method blank E = Cluantitation of compound exceeded the calibration range
ND = Not detected at or above the LOD N = Recovery is out of criteria P = The RPD between riae GC columns exceeds 401:0
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab com
Page 7 o£78

Client:Enviro-Pro, P.C. Laboratory ID: UD01039-001
Description: SS-1 Matrix: Solid
Date Sampled:0312912019 1146 % Solids: 84.0 G410212019 0253
Date Received:04/0112019
Run Prep Method Analytical Method Dilution Analysis ©ate Analyst Prep Date Batch
1 3546 8270E 1 04/05/2019 1913 JCC, 04/03/2019 2212 12197
CAS Analytical
Parameter
Number
Method
Result Q
Li
Units
Run
Hexachloroethane
67-72-1
8270E
ND
79
uglkg
1
lndeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
16
uglkg
1
isophorone
78-59-1
8270E
ND
79
uglkg
1
2-Methy)naphthalene
91-57-6
8270E
ND
16
uglkg
1
2-Methylphenol
95-48-7
8270E
ND
79
uglkg
1
3+4-Methylphenol
106-44-5
8270E
ND
150
uglkg
1
Naphthalene
91-20-3
8270E
ND
16
uglkg
1
2-Nitroaniline
88-74-4
8270E
ND
150
uglkg
1
3-Nitroaniline
99-09-2
8270E
ND
150
uglkg
1
4-Nitroaniline
100-01-6
8270E
ND
150
uglkg
1
Nitrobenzene
98-95-3
8270E
ND
79
uglkg
1
2-Nitrophenol
88-75-5
8270E
ND
150
uglkg
1
4-Nitrophenol
100-02-7
8270E
ND
390
uglkg
1
N-N itrosed i-n-pro pyl a mine
621-64-7
8270E
ND
79
uglkg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
79
uglkg
1
Pentachlorophenoi
87-86-5
8270E
ND
390
ugtkg
1
Phenanthrene
85-01-8
8270E
ND
16
uglkg
1
Phenol
108-95-2
8270E
ND
79
uglkg
1
Pyrene
129-00-0
8270E
ND
16
uglkg
1
2,4,5-Trichlorophenoi
95-95-4
8270E
ND
79
uglkg
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
79
uglkg
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
73
24-137
2-Fluorophenol
84
16-136
Nitrobenzene-d6
92
12-144
Phenol-d5
87
26-148
Terphenyi-d14
88
20-127
2,4,6-Tribromophenol
61
27-128
LOQ = Limit of Quantilation S = Detected in the method blank E = Quantltation of compound exceeded the calibration range
ND = Not delected at or above the LOQ N = Recovery is out of criiena P = The RPD between two GC columns exceeds 4MG
H = Out of holding time W = Reported an vest weight band
Shealy Environmental Services, Inc
106 Vantage Point Chive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 8 of 78

A EPH (aromatics)
Client:Enviro-Pro, P.C. Laboratory ID:UD01039-001
Description: SS-1 Matrix: Solid
Date Sampled:0312912019 1145 % Solids: 84.0 04/0212019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep bate Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 1923 CHG 04/04/2019 0837 12217
CAS Analytical
Parameter Number Method Result Q LCIQ Units Run
011 - C22 Aromatics MADEP-EPH-04 ND 12 mglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-B romo naphthalene (fractionation 2) 67 40-140
2-Fluorobiphenyl (fractionation 1) 88 40-140
o - Terphenyl (aromatic) 73 40-140
LQQ = Limit of Quantitation S = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery i5 out of criteria P = The RPD between two GC columns exceeds 401;0
H = Out of holding time W W Reported on wet weghl basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] WWWLshealylab,com
Page 9 of 78

MA EPH (alipha ics)
Client:Enviro-Pro, P.C. Laboratory ID:UD01039-001
Description: SS-1 Matrix: Solid
Date Sampled:0312912019 1145 % Solids: 84.0 04/0212019 0253
Date Received:04101/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 1426 CHG 04/04/2019 0837 12193
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 12 mglkg 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 12 mglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) 85 40-140
LDQ = Limit of Quantitntion B = Detected €n the method blank E = Quantilalion of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between thao GC columns exceeds 4M'.
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] www.shenlylab,com
Pate 10 of 79

A®EP \/PH (aiphatics)
Client;Enviro-Pro, P.C. Laboratory ID:UD01039-001
Description: SS-1 Matrix: Solid
Date Sampled:0312912019 1145 % Solids: 84.0 04102/2019 0253
Date Received:0410112019
Run Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1 VPH
MADEP-VPH-18-2.1 1
04/03120191729 JJG
12262
CAS Analytical
Parameter
Number Method
Result Q LOQ Units Run
C5 - C8 Aliphatics
MADEP-VPH-
ND 5.5 mglkg 1
C9 - C12 Aliphatics
MADEP-VPH-
ND 5.5 mglkg 1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2,5-Dibromotoluene (FID)
116
70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between Two GC columns exceeds 4D%
H = Out of holding tEme W= Reported on wet weight basis
Shealy EnvironmenW Services, Inc.
108 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv.shealylab.com
Page 1 1 of 78

Client: Enviro-Pro, P.C. Laboratory ID: UD01039-001
Description: SS-1 Matrix: Solid
Date Sampled:0312912019 1145 % Solids: 84.0 04/0212019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 04103120191729 JJG 12261
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH- NO 1.8 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID) 113 70-130
LOO = Limit of Quantitation B = Detected in the method blank E = Quant(tation of compound exceeded the cafibratton range
ND = Not detected at or above the LOQ N = Recovery is out of cnteria P = The RPO between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-97D0 Fax [phone] www,shealylab.com
Page 12 of 78

Client:Enviro-Pro, P.C. Laboratory ID: UD01039-002
Description: SS-2 Matrix: Solid
Date Sampled:0312912019 1155 % Solids: 31.6 04/02/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 04/04/2019 0124 MNS 12204 4.50
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acetone
67-64-1
8260D
NO
27
ug/kg
1
Benzene
71-43-2
8260D
NO
6.8
uglkg
1
Bromodichloro methane
75-27-4
8260D
ND
6.8
uglkg
1
Bromoform
75-25-2
8260D
ND
6.8
ug/kg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
6.8
uglkg
1
2-Butanone (MEK)
78-93-3
82601)
ND
27
uglkg
1
Carbon disulfide
75-15-0
8260D
NO
6.8
uglkg
1
Carbon tetrachloride
56-23-5
8260D
ND
6.8
uglkg
1
Chlorobenzene
108-90-7
8260D
ND
6.8
uglkg
1
Chloroethane
75-00-3
8260D
ND
6.8
ug/kg
1
Chloroform
67-66-3
8260D
ND
6.8
uglkg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
6.8
uglkg
1
Cyclohexane
110-82-7
8260D
ND
6.8
ug/kg
1
1,2- Dibro m o-3-chloro propane (DBCP)
96-12-8
8260D
ND
6.8
ug/kg
1
Dibromochloromethane
124-48-1
8260D
ND
6.8
ug/kg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
6.8
ug/kg
1
1,2-Dichlorobenzene
95-50-1
8260D
NO
6.8
ug/kg
1
1,3-Dichlorobenzene
541-73-1
8260D
NO
6.8
uglkg
1
1,4-Dichlorobenzene
106.46-7
8260D
NO
6.8
uglkg
1
Dichlorodifluoromethane
75-71-8
8260D
NO
6.8
uglkg
1
1,1-Dichloroethane
75-34-3
8260D
NO
6.8
uglkg
1
1,2-Dichloroethane
107-06-2
8260D
NO
6.8
ug/kg
1
1,1-Dichloroethene
75-35-4
8260D
NO
6.8
uglkg
1
cis-1,2-Dichloroethene
156-59-2
8260D
NO
6.8
uglkg
1
trans-1,2-Dichloroethene
156-60-5
8260D
NO
6.8
uglkg
1
1,2-Dichloropropane
78-87-5
8260D
NO
6.8
uglkg
1
cis-1,3-Dichloropropene
10061-01-5
8260D
ND
6.8
uglkg
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
NO
6.8
uglkg
1
Ethylbenzene
100-41-4
8260D
ND
6.8
uglkg
1
2-Fiexanone
591-78-6
82600
ND
14
uglkg
1
Isopropylbenzene
98-82-8
8260D
NO
6.8
uglkg
1
Methyl acetate
79-20-9
8260D
ND
6.8
uglkg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
Nil
6.8
uglkg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
14
uglkg
1
Methylcyclohexane
108-87-2
8260D
NO
6.8
uglkg
1
Methylene chloride
75-09-2
8260D
ND
6.8
uglkg
1
Styrene
100-42-5
8260D
ND
6.8
uglkg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
6.8
uglkg
1
Tetra chlorcethene
127-18-4
3260D
ND
68
uglkg
1
Toluene
108-88-3
8260D
ND
6.8
uglkg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
6,8
ug/kg
1
1,2,4-Trichoorobenzene
120-82-1
8260D
NO
6.8
uglkg
1
1,1,1-Trichloro ethane
71-55-6
8260D
ND
6.8
ug/kg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
6.8
ug/kg
1
LOD = Limit of Quantitalion B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOD N = Recovery is out of cnleria P = The RPD between two GC columns exceeds 404'�
H = Out of holding time "I' Reported on vret weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vavmv,shealylab com
Pabe 13 of 78

Client: Enviro-Pro, P.C. Laboratory ID: UD01039-002
Description: SS-2 Matrix: Solid
Date Sampled:0312912019 1155 % Solids: 81.6 04/02/2019 0253
Date Received: 0410112019
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Sample Wt.(g)
1 5035
8260D 1 04104l2019 0124 MNS
12204 4.50
CAS Analytical
Parameter
Number Method
Result Q
i_©Q
Units
Run
Trichloroethene
79-01-6 8260D
NO
6.8
uglkg
1
Trichlorofluoromethane
75-69-4 8260D
ND
6.8
uglkg
1
Vinyl chloride
75-01-4 8260D
ND
6.8
uglkg
1
Xylenes (total)
1330-20-7 8260D
ND
14
uglkg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
105 47-138
1,2-Dichloroethane-d4
95 53-142
Toluene-d8
104 68-124
LOQ = Limit of Quanlilation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4Mi
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 14 of 78

Client:Eriviro-Pro, P.C. Laboratory ID:UD01039-002
Description: SS-2 Matrix: Solid
Date 5amp1ed:0312912019 1155 % Solids: 81.6 04/02/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 04/05/2019 2046 JCG 04/03/2019 2212 12197
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
15
ugikg
1
Acenaphthylene
208-96-8
8270E
ND
15
ugikg
1
Acetophenone
98-86-2
8270E
ND
78
ugikg
1
Anthracene
120-12-7
8270E
ND
15
ugikg
1
Atrazine
1912-24-9
8270E
ND
78
ugikg
1
Benzaldehyde
100-52-7
8270E
ND
78
ugikg
1
Benzo(a)anthracene
56-55-3
8270E
ND
15
ugikg
1
Senzo(a)pyrene
50-32-8
8270E
ND
15
ugikg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
15
ugikg
1
Benzo(g,hJ)perylene
191-24-2
827DE
ND
15
ugikg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
15
ugikg
1
1,1'-Biphenyl
92-52-4
8270E
ND
78
ugikg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
78
ugikg
1
Butyl benzyi phthalate
85-68-7
8270E
ND
78
ugikg
1
Caprolactam
105-60-2
8270E
ND
78
ugikg
1
Carbazole
86-74-8
8270E
ND
78
ugikg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
78
ugikg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
78
ugikg
1
4-Chloroaniline
106-47-8
8270E
ND
78
ugikg
1
bis (2-C hloroethoxy) methane
111-91-1
827DE
ND
78
ugikg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
NO
78
ugikg
1
2-Chlaronaphthalene
91-58-7
8270E
ND
78
ugikg
1
2-Chlorophenol
95-57-8
8270E
ND
78
ugikg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
78
ugikg
1
Chrysene
218-01-9
8270E
ND
15
ugikg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
15
ugikg
1
Dibenzofuran
132-64-9
8270E
ND
78
ugikg
1
3,3'-Dichlorobenzidine
91.94-1
8270E
ND
78
ugikg
1
2,4-Dichlorophenoi
120-83-2
8270E
ND
78
ugikg
1
Diethylphthalate
84-66-2
8270E
ND
78
ugikg
1
Dimethyl phthalate
131-11-3
8270E
ND
78
ugikg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
78
ugikg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
78
ugikg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
380
ugikg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
380
ugikg
1
2,4-Dinit€otoluene
121-14-2
8270E
ND
150
ugikg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
150
ugikg
1
Di-n-octylphthalate
117-84-0
8270E
ND
78
ugikg
1
bis(2- Ethylhexyl)phthal ate
117-81-7
8270E
ND
78
ugikg
1
Fluoranthene
206-44.0
8270E
ND
15
ugikg
1
Fluorene
86-73-7
8270E
ND
15
ugikg
1
I-iexachlorobenzene
118-74-1
8270E
ND
78
ugikg
1
Hexachlorobutadiene
87-68-3
827DE
ND
78
ugikg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
380
ugikg
1
LOO T Limit of Quantitation B = Detected in the method blank E = Quantitatlon of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is cut of criteria P = The RPD between two GC columns exceeds 4041�
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com
Page 15 o(78

Client:Enviro-Pro, P.C. Laboratory ID:U©01039-002
Description: SS-2 Matrix: Solid
Date Sampled:0312912019 1155 % Solids: 81.6 04/0212019 0253
Date Received : 0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 04/05/2019 2046 JCG 04/03/2019 2212 12197
CAS Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
78
uglkg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
15
uglkg
1
lsophorone
78-59-1
8270E
ND
78
uglkg
1
2-Methylnaphthalene
91-57-6
8270E
NO
15
ug/kg
1
2-Methylphenol
95-48-7
8270E
ND
78
uglkg
1
3+4-M ethyl phenol
106-44-5
8270E
ND
150
uglkg
1
Naphthalene
91-20-3
8270E
ND
15
uglkg
1
2-Nitroaniline
88-74-4
8270E
ND
150
uglkg
1
3-Nitroaniline
99-09-2
8270E
ND
150
uglkg
1
4-Nitroaniline
100-01-6
8270E
ND
150
uglkg
1
Nitrobenzene
98-95-3
8270E
ND
78
uglkg
1
2-Nitrophenol
88-75-5
8270E
ND
150
uglkg
1
4-Nitrophenol
100-02-7
8270E
ND
380
uglkg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
78
uglkg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
78
uglkg
1
Pentachlorophenol
87-86-5
8270E
ND
380
uglkg
1
Phenanthrene
85-01-8
8270E
ND
15
uglkg
1
Phenol
108-95-2
8270E
ND
78
uglkg
1
Pyrene
129-00-0
8270E
ND
15
uglkg
1
2,4,5-Trichlorophenol
95.95-4
8270E
ND
78
uglkg
1
2,4,6-Trichlorophenol
88.06-2
8270E
ND
78
uglkg
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
74
24-137
2-Fiuorophenol
81
16-136
Nitrobenzene-d5
92
12-144
Phenol-d5
84
26-148
Terphenyl-d14
88
20-127
2,4,6-Tribromephenol
68
27-128
LOG = Limit of Quantitation 8 = Detected in the method blank E w Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOG N = Recovery is out of crito€ia P = The RPO between hvo GC columns exceeds 40�0
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv.shealylab,com
Page 16 of 78

SWUNUEEMM
Client:Enviro-Pro, P.C. Laboratory ID: UD01039-002
Description: SS-2 Matrix: Solid
Date Sampled:0312912019 1155 °lo Solids: 81.6 04/02/2019 0253
Date Received: 0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04l10l2019 1953 CHG 04/04/2019 0837 12217
CAS Analytical
Parameter Number Method Result 4 LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 12 mg/kg 1
Run 1 Acceptance
Surrogate Cd % Recovery Limits
2-Bromonaphthalene (fractionation 2) 57 40-140
2-Fluorobiphenyl (fractionation 1) 88 40-140
o - Terphenyl (aromatic) 71 40-140
LOO = Limit of auantitation B = Detected in the method blank E = Quantitation of Compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC cotumns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab com
Page 17 of 78

A EPH (aiiphatics)
Client: Enviro-Pro, P.C. Laboratory ID: UD01039-002
Description: SS-2 Matrix: Solid
Date Sampled:0312912019 1165 % Solids: 31.6 04/02/2019 0253
]ate Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 1456 CHG 04/04/2019 0837 12193
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 12 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 12 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) 84 40-140
LOC2 = Limit of Quantitation 9 = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND � Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4095
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point thrive West Columbia, SC 29172 [phone] Fax [phone] wsvw.sheaiylab,com
Page 18 of 78

Client Enviro-Pro, P.C. Laboratory ID: UD01 039-002
Description: SS-2 Matrix: Solid
Date Sampied:0312912019 1155 % Solids: 81.6 04102/2019 0263
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 04/03120191757 JJG 12262
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP VPH- ND 6.6 mg/kg 1
C9 - C12 Aliphatics MADEP-VPH- ND 6.6 nri 1
Surrogate
2,5-Dibromotoluene (FID)
Run 1 Acceptance
Q % Recovery Limits
106 70-130
LOQ = Limit of Quantitation 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GG columns exceeds 40"0
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www,sheatylab,cam
Page 19 of 79

Client:Enviro-Pro, P.C. Laboratory ID: UD01 039-002
Description: SS-2 Matrix: Solid
Date Sampled:0312912019 1155 % Solids: 81.6 04/02/2019 0253
]ate Received:04/0112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 04103120191757 JJG 12261
CAS Analytical
Parameter dumber Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH- ND 2.2 mgtkg 1
Surrogate Run 1 Acceptance
9 Q % Recovery limits
2,5-Dibromotoluene (PD) 105 70-130
LOQ = Limit of Quantitation B = Detected to the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LQQ N = Recovery is out of criteria P = The RPD between rNo GO columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] =N;.shealylab.corn
Page 20 of 78

Client:Enviro-Pro, P.C. Laboratory ID: UD01039-003
Description: SS-3 Matrix: Solid
Date Sampled:03129/2019 1200 % Solids: 79.2 0410212019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 04/04/2019 0146 MNS 12204 4.57
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acetone
67-64-1
8260D
ND
28
uglkg
1
Benzene
71-43-2
8260D
ND
6.9
uglkg
1
Bromodichloromethane
75-27-4
82600
ND
6.9
uglkg
1
Bromoform
75-25-2
8260D
ND
6.9
uglkg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
6.9
uglkg
1
2-Butanone (MEK)
78-93-3
8260D
ND
28
uglkg
1
Carbon disulfide
75-15-0
8260D
ND
6.9
uglkg
1
Carbon tetrachloride
56-23-5
8260D
ND
6.9
uglkg
9
Chlorobenzene
108-90-7
8260D
ND
6.9
uglkg
1
Chloroethane
75-00-3
8260D
ND
6.9
uglkg
1
Chloroform
67-66-3
8260D
ND
6.9
uglkg
1
Chlo€omethane (Methyl chloride)
74-87-3
8260D
ND
6.9
uglkg
1
Cyclohexane
110-82-7
8260D
ND
6.9
uglkg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
NO
6.9
uglkg
1
Dibromochloromethane
124-48-1
8260D
NO
6.9
uglkg
1
1,2-Dibromoethane (EDB)
106-93-4
B260D
ND
6.9
uglkg
1
1,2-Dichlorobenzene
95.50-1
8260D
NE)
6.9
uglkg
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
6.9
uglkg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
6.9
uglkg
1
Dichlorodifluoromethane
75-71-8
8260D
ND
6.9
uglkg
1
1,1-Dichloroethane
75-34-3
8260D
ND
6.9
uglkg
1
1,2-Dichloroethane
107-06-2
8260D
ND
6.9
uglkg
1
1,1-Dichloroethene
75-35-4
8260D
ND
6.9
uglkg
1
cis-1,2-Dichloroethene
156-59-2
8260D
ND
6.9
uglkg
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
6.9
uglkg
1
1,2-Dichloropropene
78-87-5
8260D
ND
6.9
uglkg
1
cis-1,3-Dichloropropene
10061-01-5
8260D
ND
6.9
uglkg
1
trans-1,3-Dichloropropene
10061-02-6
8260D
ND
6.0
uglkg
1
Ethylbenzene
100-41-4
8260D
ND
6.9
uglkg
1
2-Hexanone
591-78-6
8260D
ND
14
uglkg
1
Isopropylbenzene
98-82-8
8260D
ND
6.9
uglkg
1
Methyl acetate
79-20-9
8260D
ND
6.9
uglkg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
5.9
uglkg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
14
uglkg
1
Methylcyclohexane
108-87-2
8260D
ND
6.9
uglkg
1
Methylene chloride
75-09-2
8260D
ND
6.9
uglkg
1
Styrene
100-42-5
B260D
ND
6.9
uglkg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
6.9
uglkg
1
Tetra chloroethene
127-18-4
82601)
ND
6.9
uglkg
1
Toluene
108-88-3
8260D
ND
6.9
uglkg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
6.9
uglkg
1
1,2,4-Trichlorobenzene
120-32-1
8260D
ND
6.9
uglkg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
6.9
uglkg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
6.9
uglkg
1
LOQ = Limit of Quantitabon e = Detected in the method blank E = Quantilation of compound exceeded the calibration range
ND W Not detected at or above the LOQ N = Recovery is cut of criteria P = The RP€i between two GC columns exceeds 4D4'
H = Out of hoidmg lime VV = Reported on wet weight bas, s
_..................................................................
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wtiw�.shealylab com
Page 21 of 78

Client:Enviro-Pro, P.C. Laboratory ID:UD01039-003
Description: SS-3 Matrix: Solid
Date Sampled:0312912019 1200 % Solids: 79.2 04/02/2019 0253
]ate Received: 0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 04/04/2019 0146 MNS 12204 4.57
CAS Analytical
Parameter
Number Method
Result Q
LCQ
Units
Run
Trichloroethene
79-01-6 82600
ND
6.9
uglkg
1
Trichloroifuoromethane
75-69-4 82600
ND
6.9
uglkg
1
Vinyl chloride
75-01-4 8260D
ND
6.9
uglkg
1
Xylenes (total)
1330-20-7 8260D
ND
14
uglkg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
105 47-138
1,2-Dichloroethane-d4
95 53-142
Toluene-d8
104 68-124
LOCI = Limit of Quantitation 6 = Detected in the method blank E = Quantitation of compound exceeded the calibration ranee
NO = Not detected at or above the LQQ N = Recovery is out of criletia P = The RPD between two GC columns exceeds 4M:
14 = Out of holding time VV = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vrww.shealylab,com
Page 22 of 78

KMIMARM1,a M„
Client: Enviro•Pro, P.G. Laboratory ]D: t1D01039.003
Description: SS-3 Matrix: Solid
Date Sampled:0312912019 1200 % Solids: 79.2 04/0212019 0253
Date Received:0410112019
Run Prep Method Anatytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 04/05/2019 1936 JCG 04/03/2019 2212 12197
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
units
Run
Acenaphthene
83-32-9
8270E
ND
16
uglkg
1
Acenaphthylene
208-96-8
8270E
ND
16
uglkg
1
Acetophenone
98-86-2
8270E
ND
82
uglkg
1
Anthracene
120-12-7
8270E
NO
16
uglkg
1
Atrazine
1912-24-9
8270E
ND
82
uglkg
1
Benzaldehyde
100-52-7
8270E
ND
82
uglkg
1
6enzo(a)anthracene
56-55-3
8270E
ND
16
uglkg
1
Benzo(a)pyrene
50-32-8
8270E
ND
16
uglkg
1
Benzo(k)fluoranthene
205-99-2
8270E
ND
16
uglkg
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
16
uglkg
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
16
uglkg
1
1,1'-Biphenyl
92-52-4
8270E
ND
82
uglkg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
82
uglkg
1
Butyl benzy] phthalate
85-68-7
8270E
ND
82
uglkg
1
Caprolactam
105-60-2
8270E
ND
82
uglkg
1
Carbazole
86-74-8
8270E
ND
82
uglkg
1
bis (2-Chloro-l-methylethyl) ether
108-60-1
8270E
ND
82
uglkg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
82
uglkg
1
4-Chloroaniline
106-47-8
8270E
ND
82
uglkg
1
bis(2-C hloroethoxy)m ethane
111-91-1
827DE
ND
82
uglkg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
82
uglkg
1
2-Chloronaphthalene
91-58-7
8270E
ND
82
uglkg
1
2-Chlorophenol
95-57-8
8270E
ND
82
uglkg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
82
uglkg
1
Chrysene
218-01-9
8270E
ND
16
uglkg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
16
uglkg
1
Dibenzofuran
132-64-9
8270E
ND
82
uglkg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
82
uglkg
1
2,4-Dichlorophenot
120-83-2
8270E
ND
82
uglkg
1
Diethylphthalate
84-66-2
827DE
ND
82
uglkg
1
Dimethyl phthalate
131-11-3
8270E
ND
82
uglkg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
82
uglkg
1
DI-n-butyl phthalate
84-74-2
8270E
ND
82
uglkg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
410
uglkg
1
2,4-Dinitrophenol
51-28-5
8270E
ND
410
uglkg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
160
uglkg
1
2,6-Dinitrotoluene
60-20-2
8270E
ND
160
uglkg
1
Di-n-octylphthalate
117-84-0
8270E
ND
82
uglkg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
82
uglkg
1
Fluoranthene
206-44-0
827DE
ND
16
uglkg
1
Fluorene
86-73-7
8270E
ND
16
uglkg
1
Hexachlorobenzene
118-74-1
8270E
ND
82
uglkg
1
Hexachlorobutadiene
87-68-3
8270E
ND
82
uglkg
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
410
uglkg
1
LOD = Limit of Quantitation B = Detected in the method bunk E = Quanlilalion of compound exceeded the calibration range
ND = Not detected at or above the LOD N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4090
H = Out of holding time Vv = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] w>wa-shealylab.com
Page 23 of 78

Semivolatile Organic Compounds
Client:Enviro-Pro, P.C. Laboratory ID:Ub01039.003
Description: SS-3 Matrix: Solid
Date Sampled:0312912019 1200 % Solids: 79.2 04/02/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 04/05/2019 1936 JCG 04/03/2019 2212 12197
CAS Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
82
uglkg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
16
uglkg
1
Isophorone
78-59-1
8270E
ND
82
uglkg
1
2-Methylnaphthalene
91-57-6
8270E
ND
16
uglkg
1
2-Methylphenol
95-48-7
8270E
ND
82
uglkg
1
3+4-Methylphenol
106-44-5
8270E
ND
160
uglkg
1
Naphthalene
91-20-3
8270E
ND
16
uglkg
1
2-Nitroaniline
88-74-4
8270E
ND
160
uglkg
1
3-Nitroaniline
99-09-2
8270E
ND
160
uglkg
1
4-Nitroaniline
100-01-6
8270E
ND
160
uglkg
1
Nitrobenzene
98-95-3
8270E
ND
82
uglkg
1
2-Nitrophenot
88-75-5
8270E
ND
160
uglkg
1
4-Nitrophenol
100-02-7
8270E
ND
410
uglkg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
82
uglkg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
82
uglkg
1
Pentachlorophenol
87-86-5
8270E
ND
410
uglkg
1
Phenanthrene
85-01-8
8270E
ND
16
uglkg
1
Phenol
108-95-2
8270E
ND
82
uglkg
1
Pyrene
129-00-0
8270E
ND
16
uglkg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
82
uglkg
1
2,4,6-Trichlorophenol
88-06-2
8270E
NO
82
uglkg
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyi
74
24-137
2-Eluorophenol
78
16-136
Nitrobenzene-d5
90
12-144
Phenol-d5
84
26-148
Terphenyl-dl4
87
20-127
2,4,6-Tribromophenol
64
27-128
LOQ = Limit of Quar nation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not defected at or above the LOQ N = Recovery is out of criteria P = The RPD between hvo GC columns exceeds 40%
H = Out of holding lime W = Reported an wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 24 of 78

MA EPH (aromatics)
Client: Enviro-Pro, P.C. Laboratory ID: UD01039-003
Description: SS-3 Matrix: Solid
Date Sampled:03/2912019 1200 % Solids: 79.2 04/02/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 2023 CHG 04/04/2019 0837 12217
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 12 mglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) 50 40-140
2-Fluorobiphenyi (fractionation 1) 87 40-140
o - Terphenyl (aromatic) 73 40-140
LOO = Limit of ©uantitation 6 = Detected in the methad blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding lime W = Reported an wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vv�vw.shealylab,ccm
Page 25 of 78

A EPH (aliphatics)
Client:Enviro-Pro, P.C. Laboratory ID:UD01039-003
Description: SS-3 Matrix: Solid
Date Sampled: 0312912019 1200 % Solids: 79.2 04102/2019 0253
Date Received: 04101/2019
Run Prep !method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 1525 CHG 04/04/2019 0837 12193
CAS Analytical
Parameter dumber Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 12 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 12 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) 82 40-140
LOQ = Limit of Quantilahon 8 = Detected in the method blank E = Quanlilahon of compound exceeded the calibration range
Nil = Not detected at or above the LOD N = Recovery is out of cntena P = The RPD between two GC columns exceeds 40 %
H = Out of holding lime W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www sheaiyfab.com
Cage 26 of 78

A®EP VPH (a iphaiics)
Client:Enviro-Pro, P.C. Laboratory ID:UD01039-003
Description: SS-3 Matrix: Solid
Date Sampled:0312912019 1200 % Solids: 79.2 04/02/2019 0253
Date Received :0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 04/03120191826 JJG 12262
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Afiphatics MADEP-VPH- ND 6.2 mgtkg 1
C9 - C12 Aliphatics MADEP-VPH- ND 6.2 mglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID) 106 70-130
LOO = Limit of Ouantitation B = Detected in the method bianK E = Ouantitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40�'.
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wwvishealylab,com
Page 27 of 78

Client:Enviro-Pro, P.C. Laboratory ID: UD01039-003
Description: SS-3 Matrix: Solid
Date Sampled:03/2912019 1200 % Solids: 79.2 04102/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis hate Analyst Prep Date Batch
1 VPH MADE P-VPH-18-2.1 1 04103/20191826 JJG 12261
...............
CAS Analytical
Parameter Number Method Result Q LCQ Units Run
C9 - C10 Aromatics MADEP-VPH- ND 21 mglkg 1
Surrogate
2,5-Dibromotoluene (PID)
Run 1 Acceptance
Q % Recovery Limits
100 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitaticn of compound exceeded the calibration range
ND = Not detected at or above the 1-00 N = Recovery is out of criteria P W The RPD between two GC columns exceeds 401,1
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv,shealylab,cam
Page 28 of 73

Client:Enviro-Pro, P.C. Laboratory ID: UD01039.004
Description: SS-4 Matrix: Solid
Date Sampled:03/2912019 1210 % Solids: 81.2 04/0212019 0253
Date Received:04101/2019
Run Prep Method Analytical !method
Dilution Analysis Date Analyst
Prep Date
Batch Sample Wt.(g)
1 5035 9260D
1 04/04/2019
0208 MNS
12204 4.87
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acetone
67-64-1
8260D
NO
25
uglkg
1
Benzene
71-43-2
8260D
NO
6.3
uglkg
1
Bromodichloromethane
75-27-4
8260D
NO
6.3
uglkg
1
Bromoform
75-25-2
8260D
ND
6.3
uglkg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
6.3
uglkg
1
2-Butanone (MEK)
78-93-3
8260D
ND
25
uglkg
1
Carbon disulfide
75-15-0
8260D
NO
6.3
uglkg
1
Carbon tetrachloride
56-23-5
8260D
NO
6.3
uglkg
1
Chlorobenzene
108-90-7
8260D
NO
6.3
uglkg
1
Chloroethane
75-00-3
8260D
NO
6.3
uglkg
1
Chloroform
67-66-3
8260D
NO
6.3
uglkg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
NO
6.3
uglkg
1
Cyclohexane
110-82-7
8260D
ND
6.3
uglkg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
6.3
uglkg
1
Dibromochloromethane
124-48-1
8260D
NO
6.3
uglkg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
NO
6.3
uglkg
1
1,2-Dichlorobenzene
95-50-1
8260D
NO
6.3
uglkg
1
1,3-Dichlorobenzene
541-73-1
8260D
NO
6.3
uglkg
1
1,4-Dichlorobenzene
106-46-7
8260D
NO
6.3
uglkg
1
Dichlorodifluoromethane
75-71-8
8260D
NO
6.3
uglkg
1
1,1-Dichloroethane
75-34-3
8260D
ND
6.3
uglkg
1
1,2-Dichforoetliane
107-06-2
8260D
ND
6.3
uglkg
1
1,1-Dichloroethene
75-35-4
8260D
ND
6.3
uglkg
1
cis- 1,2-Dichloroethene
156-59-2
8260D
NO
6.3
uglkg
1
trans-1,2-Dichloroethene
156-60-5
8260D
NO
6.3
uglkg
1
1,2-Dichloropropene
78-87-5
8260D
ND
6.3
uglkg
1
cis-1,3-Dichloropropene
10061-01-5
8260D
ND
6.3
uglkg
1
trans-1,3-Dichloropropene
10061-02-6
8260D
NO
6.3
uglkg
1
Ethylbenzene
100-41-4
8260D
ND
6 3
uglkg
1
2-Hexanone
591-78-6
8260D
NO
13
uglkg
1
lsopropylbenzene
98-82-8
8260D
NO
6.3
uglkg
1
Methyl acetate
79-20-9
8260D
ND
6.3
uglkg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
6.3
uglkg
1
4-Methyl-2-pentanone
108-10-1
8260D
NO
13
uglkg
1
Methylcyclohexane
108-87-2
8260D
NO
6.3
uglkg
1
Methylene chloride
75-09-2
8250D
NO
6.3
uglkg
1
Styrene
100-42-5
8260D
NO
6.3
uglkg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
NO
6.3
uglkg
1
Tetrachloroethene
127-18-4
8260D
ND
6.3
uglkg
1
Toluene
108-88-3
8260D
NO
6.3
uglkg
1
1,1,2-Trichloro-1,2,2-Trifluoroeth2ne
76-13-1
8260D
ND
6.3
uglkg
1
1,2,4-Trichlorobenzene
120-82-1
82600
ND
6.3
uglkg
1
1,1,1-Trichloroethane
71-55-6
8260D
NO
5.3
uglkg
1
1,1,2-Trichloroethane
79-00-5
8260D
NO
6.3
uglkg
1
LOO = Limit of Quantitntion B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria
P = The RPD betvnen
two GC columns exceed, 40°'0
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
1€76 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 29 of78

Client:5nviro-Pro, P.C. Laboratory ID: UD01039-004
Description: SS-4 Matrix: Solid
Date Sampled:0312912019 1210 % Solids: 81.2 04102/2019 0253
late Received: 04/0112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Latch Sample Wt.(g)
1 5035 8260D 1 04104/2019 0208 MNS 12204 4.87
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Trichloroethene
79-01-6 8260D
ND
6.3
uglkg
1
Trichlorofluoromethane
75-69-4 8260D
ND
6.3
uglkg
1
Vinyl chloride
75-01-4 8260D
ND
6.3
uglkg
1
Xylenes (total)
1330-20-7 8260D
ND
13
uglkg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
105 47-138
1,2-Dichloroethane-d4
96 53-142
Toluene-d8
104 68-124
LQQ = Limit of Quanlitation 0 = Detected in the method blank E = Quanlitation of compound exceeded the calibration range
ND = Not detected at or above the LCQ N = Recovery is out of Ontario P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported an wet weight basis
Shealy Environmental Services, Ine-
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] vAvw.shealylab.com
Page 30 of 78

Client: Enviro-Pro, P.C. Laboratory 0: UD01039-004
Description: SS-4 Matrix: Solid
Date Sampled:0312912019 1210 % Solids: 81.2 04/02/2019 0253
Date Received:04/0112019
Run Prep method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 827DE 1 04/05/2019 1959 JCG 04103/2019 2212 12197
Parameter
CAS
Number
Analytical
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
NO
16
uglkg
1
Acenaphthylene
208-96-8
8270E
ND
16
uglkg
1
Acetophenone
98-86-2
8270E
ND
78
uglkg
1
Anthracene
120-12-7
8270E
NO
16
uglkg
1
Atrazine
1912-24-9
8270E
NO
78
uglkg
1
Benzaldehyde
100-52-7
8270E
NO
78
uglkg
1
Benzo(a)anthracene
56-55-3
8270E
NO
16
uglkg
1
Benzo(a)pyrene
50-32-8
8270E
NO
16
uglkg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
16
uglkg
1
Benzo(g,hJ)perylene
191-24-2
8270E
NO
16
uglkg
1
Benzo(k)fluoranthene
207-08-9
8270E
NO
16
uglkg
1
1,1'-Biphenyl
92-52-4
8270E
ND
78
uglkg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
78
uglkg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
78
uglkg
1
Caprolactam
105-60-2
8270E
NO
78
uglkg
1
Carbazole
86-74-8
8270E
NO
78
uglkg
1
big (2-Chloro-l-methylethyl) ether
108-60-1
8270E
NO
78
uglkg
1
4-Chloro-3-methyl phenol
59-50-7
8270E
NO
78
uglkg
1
4-Chloroaniiine
106-47-8
8270E
NO
78
uglkg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
NO
78
uglkg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
NO
78
uglkg
1
2-Chloronaphthalene
91-58-7
8270E
NO
78
uglkg
1
2-Chlorophenol
95-57-8
8270E
ND
78
uglkg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
78
uglkg
1
Chrysene
218-01-9
8270E
ND
16
uglkg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
16
uglkg
1
Dibenzofuran
132-64-9
8270E
NO
78
uglkg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
NO
78
uglkg
1
2,4-Dichlorophenol
120-83-2
8270E
NO
78
uglkg
1
Diethyl phthalate
84-66-2
8270E
NO
78
ug/kg
1
Dimethyl phthalate
131-11-3
8270E
NO
78
ug/kg
1
2,4-Dimethylphenol
105-67-9
8270E
NO
78
uglkg
1
Di-n-butyl phthalate
84-74-2
8270E
NO
78
uglkg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
NO
390
uglkg
1
2,4-Dinit€ophenol
51-28-5
8270E
NO
390
uglkg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
150
uglkg
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
150
uglkg
1
D 1-n-octylphth a late
117-84-0
8270E
ND
78
uglkg
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
NO
78
uglkg
1
Fluoranthene
206-44-0
8270E
NO
16
uglkg
1
Fluorene
86-73-7
827DE
NO
16
uglkg
1
Hexachlorobe nzene
118-74-1
827DE
NO
78
uglkg
1
Hexachlorobutadiene
87-68-3
8270E
NO
78
ug/Rg
1
Hexachlorocyclopentad iene
77-47-4
8270E
ND
390
uglkg
1
LOQ = Limit of Quanlitalion 8 = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40"/
H = Out of holding lime W = Reported an wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com
Page 31 of 78

Client: Enviro-Pro, P.C. Laboratory ID: UD01039-004
Description: SS-4 Matrix: Solid
Date Sampled:0312912019 1210 % Solids: 81.2 04102/2019 0253
Date Received:04101/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270E 1 04/05/2019 1959 JCG 04/03/2019 2212 12197
CAS Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
ND
78
uglkg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
NO
16
ug/kg
1
Isophorone
78-59-1
8270E
ND
78
uglkg
1
2-Methylnaphthalene
91-57-6
8270E
ND
16
uglkg
1
2-Methylphenol
95-48-7
8270E
ND
78
uglkg
1
3+4-Methylphenoi
106-44-5
8270E
ND
150
ug/kg
1
Naphthalene
91-20-3
8270E
NO
16
uglkg
1
2-Nitroaniline
88-74-4
8270E
NO
150
uglkg
1
3-Nitroaniline
99-09-2
8270E
NO
150
uglkg
1
4-Nitroaniline
100-01-6
8270E
ND
150
uglkg
1
Nitrobenzene
98-96-3
8270E
ND
78
uglkg
1
2-Nitrophenol
88-75-5
8270E
NO
150
ug/kg
1
4-Nitrophenof
100-02-7
8270E
NO
390
ug/kg
1
N-Nitrosodi-n-p€opylamine
621-54-7
8270E
NO
78
ug/kg
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
78
uglkg
1
Pentachlorophenol
87-86-5
8270E
NO
390
uglkg
1
Phenanthrene
85-01-8
8270E
ND
16
ug/kg
1
Phenol
108-95-2
8270E
NO
78
uglkg
1
Pyrene
129-00-0
8270E
NO
16
uglkg
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
78
uglkg
1
2,4,6-Trichlore phenol
88-06-2
8270E
ND
78
uglkg
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
77
24-137
2-Fluorophenol
80
16-136
Nitrobenzene-d5
92
12-144
Phenol-d5
84
26-148
Terphenyl-d14
90
20-127
2,4,6-Tribromophenol
69
27-128
LOO = Limkt of Quantitation B = Detected in the method blank E = Quanlitation of compound excucclod the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD betvrecn two GC columns exceeds 40 %
H = Out of ho€ding time +W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] w�nv shealylab-com
Page 32 of 79

IMONEEMM
Client:Enviro-Pro, P.C. Laboratory ID: UD01039-004
Description: SS-4 Matrix: Solid
Date Sampled:0312912019 1210 % Solids: 81.2 0410212019 0253
Date Received: 0410112019
Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/40/2019 2052 CHG 04/04/2019 0837 12217
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 12 mglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) 66 40-140
2-Eluorobiphenyl (fractionation 1) 90 40-140
o - Terphenyl (aromatic) 75 40-140
LOO = Limit of Quaniilolion B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD behveen two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wmv shealylab.com
Page 33 of 79

IAA EPIC (alphatics)
Client: Enviro-P ro, P.C. Laboratory ID:UD01039-004
Description: SS-4 Matrix: Solid
Date Sampled:03/2912019 1210 % Solids: 81.2 04102/2019 0253
Date Received:04/0112019
Run Prop Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 1555 CHG 04/04/2019 0837 12193
_..... ............_. ..... .......................
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 12 mglkg 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 12 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) 83 40-140
LCQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Net detected at or above the LQQ N = Recovery is out of cmena P = The RPD between two GC columns exceeds 4WW
H = Out of hofdmg time W = Reported an wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv,shealylab.com
Page 34 of 78

MADEP VP (aiiphatics)
Client: Enviro-Pro, P.C. Laboratory ID: UD01039-004
Description: SS-4 Matrix: Solid
Date Sampled:0312912019 1210 % Solids: 81.2 04/0212019 0263
)ate Received:04101/2019
Run Prep Method Analytical method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 04/03/20191854 JJG 12262
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH- NO 6.7 mglkg 1
C9 - C12 Aliphatics MADEP-VPH- ND 6.7 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID) N 151 70-130
LQQ = Limit of Quantitation 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 41M�
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wmv,shealylab,com
Page 35 of 78

Client:Enviro-Pro, P.G. Laboratory ID: UD01039.004
Description: SS-4 Matrix: Solid
Date Sam pled:O3/2912019 1210 % Solids: 81.2 04/0212019 0253
)ate Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADE P-VPH-18-2.1 1 04/03/20191854 JJG 12201
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C9 - C10 Aromatics MADEP-VPH- ND 2.2 mglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID) N 147 70-130
LOQ = Limit of Quantitation 3 = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 4V'o
H = Out of holding time VV = Reported on wat weight basEs
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab corn
PalTe 36 of 78

Client:Enviro-Pro, P.C. Laboratory ID: UD01039.005
Description: SS-5 Matrix: Solid
Date Sampled:0312912019 1215 % Solids: 80.6 04/0212019 0253
Date Received: 0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 04/05/2019 0210 WINS 12345 5.48
CAS
Analytical
Parameter
Number
Method
Result 4
LOQ
Units
Run
Acetone
67-64-1
8260D
ND
23
uglkg
1
Benzene
71-43-2
8260D
ND
5.7
uglkg
1
Bromodichloromethane
75-27-4
8260D
ND
5.7
uglkg
1
Bromoform
75-25-2
8260D
ND
5.7
uglkg
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
5.7
uglkg
1
2-Buianone (MEK)
78-93-3
8260D
NO
23
uglkg
1
Carbon disulfide
75-15-0
8260D
ND
51
uglkg
1
Carbon tetrachloride
56-23-5
8260D
ND
5.7
uglkg
1
Chlorobenzene
108-90-7
8260D
ND
5.7
uglkg
1
Chloroethane
75-00-3
8260D
ND
5.7
uglkg
1
Chloroform
67-66-3
8260D
ND
5.7
uglkg
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
5.7
uglkg
1
Cyclohexane
110-82-7
8260D
ND
5.7
uglkg
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
5.7
uglkg
1
Dibromochloromethane
124-48-1
8260D
ND
5.7
uglkg
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
5.7
uglkg
1
1,2-Dichlorabenzene
95-50-1
9260D
ND
5.7
uglkg
1
1.3-Dichloll benzene
541-73-1
8260D
ND
5.7
uglkg
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
5.7
uglkg
1
Dichlorodifluoromethane
75.71-8
8260D
ND
5.7
uglkg
1
1,1-Dichloroethane
75-34-3
8260D
ND
5.7
uglkg
1
1,2-Dichloroethane
107-06-2
8260D
ND
5.7
uglkg
1
1,1-Dichloroethene
75-35-4
8260D
ND
5.7
uglkg
1
cis-1,2-Dichloroethene
156-59-2
8260D
ND
5.7
uglkg
1
trans-1,2-Dichloroethene
156.60-5
8260D
ND
5.7
uglkg
1
1,2-Dichioropropene
78-87-5
8260D
ND
5.7
ug/kg
1
cis-1,3-Dichioropropene
10061-01-5
8260D
ND
5.7
uglkg
1
trans-1,3-Dichioropropene
10061-02-6
8260D
ND
5.7
uglkg
1
Ethylbenzene
100-41-4
8260D
ND
5.7
uglkg
1
2-Hexanone
591-78-6
8260D
ND
11
uglkg
1
lsopropylbenzene
98-82-8
8260D
ND
5,7
uglkg
1
Methyl acetate
79-20-9
8260D
ND
5.7
uglkg
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
5.7
uglkg
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
11
uglkg
1
Methyl cyclohexane
108-87-2
8260D
ND
5.7
uglkg
1
Methylene chloride
75-09-2
8260D
ND
5.7
uglkg
1
Styrene
100-42-5
8260D
ND
5.7
uglkg
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
5.7
uglkg
1
Tetrachloroethene
127-18-4
8260D
ND
5.7
uglkg
1
Toluene
108-88-3
8260D
ND
5.7
uglkg
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
5.7
uglkg
1
1,2,4-TrichIorobenzene
120-82-1
3260D
ND
5.7
uglkg
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
5.7
uglkg
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
5.7
uglkg
1
ll = Limit of 4uanlitation B W Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the li N = Recavery is out of cntena P = The RPD between two GC columns exceeds 405E
H = Out of holding time Vv = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shenlylob com
PaSe 37 of 78

Client:Enviro-Pro, P.C. Laboratory ID: UD01 039-005
Description: SS-5 Matrix: Solid
Date Sampled:0312912019 1215 % Solids: 80.6 04102/2019 0263
Date Received:04101/2019
Run Prep Method Analytical method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260D 1 04/05/2019 0210 MNS 12345 5.48
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Trichloroethene
79-01-6 8260D
ND
5.7
uglkg
1
Trichlorofluoromethane
75-69-4 8260D
ND
5.7
uglkg
1
Vinyl chloride
75-01-4 8260D
ND
5.7
uglkg
1
Xylenes (total)
1330-20-7 8260D
ND
11
uglkg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene 105 47-138
1,2-Dichloroethane-d4 94 53-142
Toluene-d8 103 68-124
LOO = Limit of Quantitation B = Detected in the method blank E = Quantitalion of compound exceeded the calibration range
ND = Not detected at or above the 1-00 N = Recovery is out of criteria P = The RPD between two GC co€umns exceeds 40%
H = Out of holding time W w Reported on vent weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvvw,shealylab.com
Page 38 of?8

Client:Enviro-Pro, P.C. Laboratory ID: UD01039-006
Description: SS-5 Matrix: Solid
Date Sampled:0312912019 1215 % Solids: 80.6 04/02/2019 0263
Date Received: 04tO112019
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270E
1 04/05/2019 2023 .)CG
04/03/2019 2212 12197
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
8270E
ND
16
uglkg
1
Acenaphthylene
208-96-8
8270E
ND
16
uglkg
1
Acetophenone
98-86-2
8270E
ND
83
uglkg
1
Anthracene
120-12-7
827DE
ND
16
uglkg
1
Atrazine
1912-24-9
8270E
ND
83
uglkg
1
Benzaldehyde
100-52-7
8270E
ND
83
uglkg
1
Benzo(a)anthracene
56-55-3
8270E
ND
16
uglkg
1
Benzo(a)pyrene
50-32-8
8270E
ND
16
uglkg
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
16
uglkg
1
Senzo(g,h,i)perylene
191-24-2
8270E
ND
16
uglkg
1
Berizo(k)fluoranthene
207-08-9
8270E
ND
16
uglkg
1
1,1'-Bipheny€
92-52-4
8270E
ND
83
uglkg
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
83
uglkg
1
Butyl benzyl phthalate
85-68-7
8270E
ND
83
uglkg
1
Caprolactam
105-60-2
8270E
ND
83
uglkg
1
Carbazole
86-74-8
8270E
ND
83
uglkg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
83
uglkg
1
4-Chloro-3-methyl phenol
59-50.7
8270E
ND
83
uglkg
1
4-Chloroaniline
106-47-8
8270E
ND
83
uglkg
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
83
uglkg
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
83
uglkg
1
2-Chloronaphthalene
91-58-7
8270E
ND
83
uglkg
1
2-Chlorophenol
95-57-8
8270E
ND
83
uglkg
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
83
uglkg
1
Chrysene
218-01-9
8270E
ND
16
uglkg
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
16
uglkg
1
Dibenzofuran
132-64-9
8270E
ND
83
uglkg
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
83
uglkg
1
2,4-Dichlorophenol
120-83-2
827DE
ND
83
uglkg
1
Diethylphthalate
84-66-2
8270E
ND
83
uglkg
1
Dimethyl phthalate
131-11-3
8270E
ND
83
uglkg
1
2,4-Dimethylphenol
105-67-9
8270E
ND
83
uglkg
1
Di-n-butyl phthalate
84-74-2
8270E
ND
83
uglkg
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
410
uglkg
1
2,4-Dinitropheno€
51-28-5
8270E
ND
410
uglkg
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
160
uglkg
1
2,6-Dinitrotoluene
6D6-20-2
8270E
ND
160
uglkg
1
Di-n-octylphthalate
117-84-0
827DE
ND
83
uglkg
1
bis(2- Ethyl hexyl)phthalate
117-81-7
8270E
ND
83
uglkg
1
Fluoranthene
206-44-0
8270E
ND
16
uglkg
1
Fluorene
86-73-7
8270E
ND
16
uglkg
1
Hexachlorobenzene
118-74-1
8270E
ND
83
uglkg
1
Hexachlorobutadiene
87-68-3
8270E
ND
83
uglkg
1
I-lexachlorocyclopentadiene
77-47-4
8270E
Nil
410
uglkg
1
LOQ = Limit of Quantitation
6 = Detected in the method blank
E = Quanlitahon of compound exceeded the calibration range
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between
two GC columns exceeds 403b
H = Out of holding time
W = Reported on wet woe ght basis
Shealy Environmental Services, Inc
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com
Page 39 of 78

Client:Enviro-Pro, P.C. Laboratory ID: UDG1 039-005
Description: SS-5 Matrix: Solid
Date Sampled:0312912019 1215 °>a So€ids; 80.6 04102/2019 0253
Date Received:04/0112019
Run Prep Method Analytical Method
1 3546 8270E
Dilution Analysis Date Analyst
1 04/05/2019 2023 JCG
Prep pate Batch
04/03/2019 2212 12197
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1
8270E
NO
83
uglkg
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
NO
16
uglkg
1
Isophorone
78-59-1
827DE
NO
83
ug/kg
1
2-Methylnaphthalene
91-57-6
8270E
NO
16
uglkg
1
2-Methylphenol
95-48-7
8270E
NO
83
uglkg
1
3+4-Methylphenol
106-44-5
8270E
NO
160
uglkg
1
Naphthalene
91-20-3
8270E
NO
16
ug/kg
1
2-Nitroaniline
88-74-4
8270E
NO
160
ug/kg
1
3-Nitroaniline
99-00-2
8270E
NO
160
uglkg
1
4-Nitroaniline
100-01-6
8270E
NO
160
uglkg
1
Nitrobenzene
98-95-3
8270E
NO
83
uglkg
1
2-Nitrophenol
88-75-5
8270E
NO
160
ug/kg
1
4-Nitrophenol
100-02-7
8270E
NO
410
ug/kg
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
NO
83
uglkg
1
N-Nitrosod iphenyla mine (Diphenylamine)
86-30-6
8270E
NO
83
uglkg
1
Pentachlorophenoi
87-86-5
8270E
NO
410
uglkg
1
Phenanthrene
85-01-8
8270E
NO
16
uglkg
1
Phenol
108-95-2
8270E
NO
83
ug/kg
1
Pyrene
129-00-0
8270E
ND
16
uglkg
1
2,4,5-Trichlorophenol
95-95-4
827DE
NO
83
uglkg
1
2,4,6-Trichlorophenol
88-06-2
8270E
NO
83
uglkg
1
Run 1
Acceptance
Surrogate
Q % Recovery
Limits
2-Fluorobiphenyl
72
24-137
2-Fiuorophenol
78
16-136
Nitrobenzene-d5
89
12-144
Phenol-d5
82
26-148
Terphenyl-d14
88
20-127
2,4,6-Tribromophenol
67
27-128
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between hvo GC column, exceeds 401.10
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] w%vw [e-mail]
Page 40 of 78

I
Client:Enviro-Pro, P.C. Laboratory ID: UD01039-006
Description: SS-5 Matrix: Solid
Date Sampled:0312912019 1215 % Solids: 80.6 D410212019 0253
Date Received:04/01/2019
Run Prep Method Analytical Method Dilution Analysis [gate Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 2122 CHG 04/04/2019 0837 12217
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 12 mg/kg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Bromanaphthalene (fractionation 2) 61 40-140
2-Fluorobiphenyl (fractionation 1) 92 40-140
o - Terphenyl (aromatic) 77 40-140
LOQ = Limit of Quanlitation B = Detected in the method blank E = Quantilation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of entena P = The RPD between two GC columns exceeds 405E
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc
106 vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnrj shealylab,com
Page41 of78

MA EPH (aliphat cs)
Client: Enviro-Pro, P.C. Laboratory ID: UD01039-005
Description: SS-5 Matrix: Solid
Date Sampled:0312912019 1215 % Solids: 80.6 04/02/2019 0253
Date Received; 04/0112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 04/10/2019 1624 CHG 04/04/2019 0837 12193
CAS Analytical
Parameter Number Method Result 0 LOQ Units Run
C9 - C18 Aliphatics MADEP-EPH-04 NO 12 mg/kg 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 12 mglkg 1
Run 1 Acceptance
Surrogate (Q % Recovery Limits
1-Chloro-octadecane (aliphatic) 86 40-140
LOQ = Limit of Quantitation B = Dotected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40?'0
H = Out of holding time W = Reported on vet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 42 of 78

Client:Enviro-Pro, P.C. Laboratory ID:UD01039-005
Description: SS-5 Matrix: Solid
Date Sampied:0312912019 1215 % Solids: 30.6 04/02/2019 0253
Date Received:0410112019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 04103120191923 JJG 12262
GAS Analytical
Parameter Number Method Result Q LOQ Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 5A rnglkg 1
C9 - C12 Aliphatics MADEP-VPH- ND 5A tnglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID) 117 70-130
LOO = Limit of Quant€tatien 6 = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40';
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab,cam
Pare 43 of 78

Client: Enviro-Pro, P.C. Laboratory ID: UD01039-006
Description: SS-5 Matrix: Solid
Date Sample d:0312912019 1215 % Solids: 80.6 04/02/2019 0253
Date Received:04101/2019
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 04/03/20191923 JJG 12261
CAS Analytical
Parameter Number Method Result Q LOO Units Run
C9 - C10 Aromatics MADEP-VPH- ND 1.7 mglkg 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID) 107 70-130
LOO = Limit of Quontitntion 8 = Detected in the method blank E = Quanlitation of compound exceeded the calibration range
ND = Not detected at or above the LOO N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40%
H = Out of holding time W = Reported on wet weight bass
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvnri.shealylab.com
Page 44 of 78

Sheaiy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com
Page 45 of 78

Sample ID: UQ12204-001 Matrix: Solid
Batch: 12204 Prep method: 5035
Analytical method: 821330D
Parameter
Result
Oil
LOQ
Units
Analysis Date
Acetone
NO
1
20
uglkg
04/03/2019 2102
Benzene
NO
1
5.0
uglkg
04/03/2019 2102
Bromodichloromethane
NO
1
5.0
uglkg
04/03/2019 2102
Bromoform
NO
1
5.0
uglkg
04/03/2019 2102
Bromomethane (Methyl bromide)
NO
1
5.0
uglkg
04/03/2019 2102
2-Sutanone (MEK)
NO
1
20
uglkg
04/03/2019 2102
Carbon disulfide
NO
1
5.0
uglkg
04/03/2019 2102
Carbon tetrachloride
NO
1
5.0
uglkg
04/03/2019 2102
Chlorobenzene
ND
1
5.0
uglkg
04/03/2019 2102
Chloroethane
NE)
1
5.0
uglkg
04/03/2019 2102
Chloroform
NO
1
5.0
uglkg
04/03/2019 2102
Chloromethane (Methyl chloride)
ND
1
5.0
uglkg
04/03/2019 2102
Cyclohexane
NO
1
5.0
LI
04/03/2019 2102
1,2-Dibromo-3-chloropropane (DBCP)
NO
1
5.0
uglkg
04/03/2019 2102
Dibromochloromethane
NO
1
5.0
uglkg
04/03/2019 2102
1,2-Dibromoethane (EOB)
NO
1
5.0
uglkg
04/03/2019 2102
1,2-Dichlorobenzene
ND
1
5.0
uglkg
04/0312019 2102
1,3-Dichlorobenzene
NO
1
5.0
uglkg
04/03/2019 2102
1,4-Dichlorobenzene
NO
1
5.0
uglkg
04/03/2019 2102
Dichlorodifluoromethane
NO
1
5.0
uglkg
04/0312019 2102
1,1-Dichloroethane
NO
1
5.0
uglkg
04/03/2019 2102
1,2-Dichloroethane
ND
1
5.0
LI
04/03/2019 2102
1,1-Dichloroethene
NO
1
5.0
uglkg
04/03/2019 2102
cis-1,2-Dichloroethene
NO
1
5.0
uglkg
04/03/2019 2102
trans-1,2-Dichloroethene
NO
1
5.0
uglkg
04/03/2019 2102
1,2-Dichlaropropane
NO
1
5.0
uglkg
04/03/2019 2102
cis-1,3-Oichloropropene
ND
1
5.0
ug/kg
04/03/2019 2102
trans-1,3-Dichloropropene
ND
1
5.0
uglkg
04/03/2019 2102
Ethyibenzene
NO
1
5.0
uglkg
04/03/2019 2102
2-Fiexanone
ND
1
10
uglkg
04/03/2019 2102
Isopropylbenzene
ND
1
5.0
uglkg
04/03/2019 2102
Methyl acetate
NO
1
5.0
uglkg
04/03/2019 2102
Methyl tertiary butyl ether (MTBE)
ND
1
5.0
uglkg
04/03/2019 2102
4-Methy[-2-pentanone
ND
1
10
uglkg
04/03/2019 2102
Methyl cyclohexane
ND
1
5.0
uglkg
04/0312019 2102
Methylene chloride
NO
1
5.0
uglkg
04/03/2019 2102
Styrene
NO
1
5.0
uglkg
04/03/2019 2102
1,1,2,2-Tetrachloroethane
NO
1
5.0
uglkg
04/03/2019 2102
Tetrachloroethene
ND
1
5.0
uglkg
04103/2019 2102
Toluene
NO
1
5.0
uglkg
04/03/2019 2102
1,1,2-Trichloro-1,2,2-Trifluoroethane
NO
1
5.0
uglkg
04/03/2019 2102
1,2,4-Trichlorobenzene
NO
1
5.0
uglkg
04/03/2019 2102
1,11-Trichloroethane
NO
1
5.0
uglkg
04/03/2019 2102
1,1,2-Trichloroethane
NO
1
5.0
uglkg
04/03/2019 2102
LOQ = Limit of Quantitation
DI, = Detection Limit
LOD = Limit of Detection
P W The RPD between two GC columns exceeds 46% N = Recovery is out of cnteria
J = Estimated result < LOCI and � DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvflv.sheafylab,com
Page 46 of 78

Sample ID: UQ12204-001 Matrix: Solid
Batch: 122D4 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Trichloroethene
ND
1
5.0
uglkg
04/03/2019 2102
Trichlorofluoromethane
ND
1
5.0
uglkg
04/03/2019 2102
Vinyl chloride
ND
1
5.0
uglkg
04/03/2019 2102
Xylenes (total)
ND
1
10
uglkg
04/03/2019 2102
Surrogate
Q % Ree
Acceptance
Limit
Bromofluorobenzene
102
47-138
1,2-Dichloroethane-d4
96
53-142
Toluene-d8
104
68-124
LOCI = Limit of Quantilalion P = The RPD between two GC columns exceeds 401,o N = Recovery is out of triter€a
OL = Detection Limit J = Estimated result e LOCI and a DL > = RPD is out of crilena
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
....................... .
Shealy Environmentaf Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vwwvw.shealylab.com
Page 47 of 78

Volatile Organic Compounds by GG/MS - LCS
Sample ID: UQ12204-002
Matrix:
Solid
Batch: 12204
Prep Method:
5035
Analytical Method. 8260D
Spike
Amount
Result
% Rec
Parameter
(uglkg)
(uglkg)
Q Dii
% Rec
Limit
Analysis Date
Acetone
100
95
1
95
60-140
04/03/2019 1941
Benzene
50
54
1
108
70-130
04/03/2019 1941
Bromodichloromethane
50
53
1
106
70-130
04/03120191941
Bromoform
50
51
1
101
70-130
04/03/2019 1941
Bromomethane (Methyl bromide)
50
49
1
98
70-130
04/03/2019 1941
2-Butanone (MEK)
100
92
1
92
60-140
04/03/2019 1941
Carbon disuifde
50
52
1
105
70-130
04/03/2019 1941
Carbon tetrachloride
50
54
1
109
70-130
04/03/2019 1941
Chlorobenzene
50
56
1
111
70-130
04103120191941
Chloroethane
50
47
1
94
70-130
04103120191941
Chloroform
50
52
1
104
70-130
04103120191941
Chloromethane (Methyl chloride)
50
48
1
95
60-140
04/03/2019 1941
Cyclohexane
50
53
1
105
70.130
04/03120191941
1,2-Dibromo-3-chloropropane (DBCP)
50
44
1
89
70.130
04/03/2019 1941
Dibromochloromethane
50
53
1
107
70-130
04/03120191941
1,2-Dibromoethane (EDB)
50
51
1
103
70-130
04/03/2019 1941
1,2-Dichlorobenzene
50
55
1
109
70-130
04/03/2019 1941
1,3-Dichlorobenzene
50
57
1
113
70-130
04/03/2019 1941
1,4-Dichlorobenzene
50
56
1
112
70-130
04/03/2019 1941
Dichiorodifluoromethane
50
47
1
94
60-140
04103/20191941
1,1-Dichloroethane
50
51
1
102
70-130
04103/20191941
1,2-Dichloroethene
50
52
1
104
70-130
04103/20191941
1,1-Dichloroethene
50
53
1
106
70-130
04103120191941
cis-12-Dichloreethene
50
52
1
103
70-130
04103/20191941
trans- l,2-Dichloroethene
50
53
1
105
70-130
04103120191941
1,2-Dichloropropane
50
52
1
104
70-130
04103120191941
cis- 1,3-Dichloropropene
50
52
1
103
70-130
04103120191941
trans- l,3-Dichloropropene
50
53
1
105
70-130
04/03/2019 1941
Ethyibenzene
50
57
1
113
70-130
04103120191941
2-Hexanone
100
97
1
97
70-130
04/03/2019 1941
Isopropyibenzene
50
56
1
113
70-130
04/03/2019 1941
Methyl acetate
50
42
1
84
70-130
04/03/2019 1941
Methyl tertiary butyl ether (MTBE)
50
47
1
95
70-130
04/03/2019 1941
4-Methyl-2-pentanone
100
90
1
90
70-130
04103/20191941
Methylcyclohexane
50
57
1
114
70-130
04/03/2019 1941
Methylene chloride
50
47
1
95
70-130
04/03/2019 1941
Styrene
50
55
1
111
70-130
04/03/2019 1941
1,1,2,2-Tetrachlorcethane
50
51
1
103
70-130
04/03120191941
Tetrachloroethene
50
59
1
118
70-130
04103120191941
Toluene
50
57
1
115
70-130
04103120191941
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
56
1
112
70-130
04103/20191941
1,2,4-Trichlorobe nzene
50
52
1
105
70-130
04103/20191941
1,1,1-Trichioroethane
50
53
1
107
70-130
04103/20191941
1,1,2-Trichloroethane
50
51
1
102
70-130
04/03/2019 1941
LOQ = Limit of Quantitation
DL =Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 401,9 N = Recovery is out of criteria
J = Estimated result < LOD and > OL + = RPD is out of cr€tena
NO = Not detected at or above the LOCI
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Sheaiy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv,shealylab.com
Page 48 of 78

s
Sample ID: UQ12204-002
Matrix:
Solid
Batch: 12204
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(uglkg)
(uglkg)
Dil
% Rec
Limit
Analysis Date
Trichloroethene
50
55
1
111
70-130
04/03120191941
Trichlorofl uorom ethane
50
54
1
109
70-130
04/03120191941
Vinyl chloride
50
54
1
107
70-130
04/03/2019 1941
Xylenes (total)
100
110
1
112
70-130
04/03/2019 1941
Surrogate
Q % Rec
Acceptance
Limit
Bromofluarobenzene 99 47-138
1,2-Dichloroethane-d4 88 53-142
Toluene-d8 97 68-124
LOQ = Lim€t of QuaMation P = The RPD between two GC columns exceeds 4WD N = Recovery is out of criteria
DL = Detection Limit J = Estimates result < LOD and > DL > = RPC) is out of cntena
LOB= Limit of Detection ND = Not detected at or above the LOO
Note: Calculations are performed before rounding to avoid round -oft errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage point give West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 49 of 78

Sample ID: U012345-001 Matrix: Solid
Batch: 12345 Prop method: 5035
Analytical Method: 8260D
Parameter
Result
Q Dil
LOO
Units
Analysis Date
Acetone
NO
1
20
uglkg
04104/2019 2128
Benzene
NO
1
5.0
uglkg
04/04/2019 2128
Bromodichloromethane
NO
1
5.0
ug/kg
04/04/2019 2128
Bromoform
NO
1
5.0
uglkg
04/04/2019 2128
Bromomethane (Methyl bromide)
ND
1
5.0
uglkg
04/04/2019 2128
2-Butanone (MEK)
NO
1
20
uglkg
04/04/2019 2128
Carbon disulfide
NO
1
5.0
uglkg
04/04/2019 2128
Carbon tetrachloride
ND
1
5.0
uglkg
04/04/2019 2128
Chlorobenzene
NO
1
5.0
uglkg
04/04/2019 2128
Chloroethane
ND
1
5.0
uglkg
04/04/2019 2128
Chloroform
NO
1
5.0
ug/kg
04/04/2019 2128
Chlo€omethane (Methyl chloride)
ND
1
5.0
uglkg
04/0412019 2128
Cyclohexane
ND
1
5.0
uglkg
04/04/2019 2128
1,2-Dibroma-3-chloropropane (DBCP)
NO
1
5.0
uglkg
04/04/2019 2128
Dibromochloromethane
ND
1
5.0
ug/kg
04/04/2019 2128
12-Dibromoethane (EDS)
NO
1
5.0
ug/kg
04/04/2019 2128
1,2-Dichlorobenzene
NO
1
5.0
uglkg
04/04/2019 2128
1,3-Dichlorobenzene
NO
1
5.0
uglkg
04/04/2019 2128
1,4-Dichlorobenzene
Nil
1
5.0
uglkg
04/04/2019 2128
Dichlorodifluoromethane
NO
1
510
uglkg
04/04/2019 2128
1,1-Dichloroethane
ND
1
5.0
uglkg
04/0412019 2128
1,2-Dichloroethane
ND
1
5.0
uglkg
04/04/2019 2128
1,1-Dichloroethene
ND
1
5.0
uglkg
04/04/2019 2128
cis- 1,2-Dichloroethene
NO
1
5.0
uglkg
04/0412019 2128
trans- 1,2-Dichloroethene
ND
1
5.0
uglkg
04/04/2019 2128
1,2-Dichloropropane
ND
1
5.0
uglkg
04/04/2019 2128
cis- 1,3-Dichloropropene
ND
1
5.0
ug/kg
04/04/2019 2128
trans- l,3-Dichloropropene
NO
1
5.0
uglkg
04/04/2019 2128
Ethylbenzene
NO
1
5.0
uglkg
04/04/2019 2128
2-Hexanone
NO
1
10
uglkg
04/04/2019 2128
Isopropylbenzene
NO
1
5.0
uglkg
04/0412019 2128
Methyl acetate
NO
1
5.0
uglkg
04/04/2019 2128
Methyl tertiary butyl ether (MTBE)
NO
1
5.0
uglkg
04/04/2019 2128
4-Methyl-2-pentanone
ND
1
10
uglkg
04/04/2019 2128
Methylcyclohexane
ND
1
5.0
ug/kg
04/04/2019 2128
Methylene chloride
NO
1
5.0
ug/kg
04/04/2019 2128
Styrene
ND
1
5.0
uglkg
04/04/2019 2128
1,1,2,2-Tetrachloroethane
NO
1
5.0
uglkg
04/04/2019 2128
Tetrachloroelhene
ND
1
5.0
uglkg
04/04/2019 2128
Toluene
ND
1
5.0
uglkg
04/04/2019 2128
1,1,2-Trichloro-1,2,2-Trifluaroethane
ND
1
5.0
uglkg
04/04/2019 2128
1,2,4-Trichloro benzene
NO
1
5.0
uglkg
04/04/2019 2128
1,1,1-Trichloroethane
ND
1
5.0
uglkg
04/04/2019 2128
1,1,2-Tr€chloroethane
NO
1
5.0
uglkg
04/04/2019 2128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between hvo GC cotumns exceeds 40% N = Recovery is out of criteria
J = Estimated result < LOO and > DL + T RPD is out of criteria
ND = Not detected at or al)ove the LOO
Vote: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, So 29172 [phone] Fax (S03) 791-9111 www.shealylab,com
Page 50 of 78

Sample 1D: UQ12345-001 Matrix: Solid
Batch: 12345 Prep Method: 5035
Analytical Method: 8260D
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Trichloroethene
ND
1
5.0
uglkg
04/04/2019 2128
Trichlorofluo€omethane
ND
1
5.0
uglkg
04/04/2019 2128
Vinyl chloride
ND
1
5.0
uglkg
04/04/2019 2128
Xylenes (total)
ND
1
10
uglkg
04/04/2019 2128
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene
104
47-138
1,2-Dichloroethane-d4
95
53-142
Toluene-d8
103
68-124
LOD = Limit of Quantitotion P = The RPD between tvo GC columns exceeds 40% N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and - DL = RPD is out of criteria
LOD = OW of Detection NO = Not detected at or above the LOO
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.eom
Page 51 of 78

Sample ID. UQ12345-002
Matrix: Solid
Batch: 12345
Prep Method:
5035
Analytical Method: 8260D
Spike
Amount
Result
% Roo
Parameter
(uglkg)
(uglkg)
Q pit
% Rec
Limit
Analysis Date
Acetone
100
100
1
100
60-140
04/04/2019 2005
Benzene
50
51
1
102
70-130
04/04/2019 2005
Bromodichloromethane
50
50
1
101
70-130
04/04/2019 2005
Bromoform
50
51
1
102
70-130
04/04/2019 2005
Bromomethane (Methyl bromide)
50
45
1
91
70-130
04/04/2019 2005
2-Butanone (MEK)
100
97
1
97
60-140
04/04/2019 2005
Carbon disulfide
50
49
1
99
70-130
04/04/2019 2005
Carbon tetrachloride
50
53
1
105
70-130
04/04/2019 2005
Chlorobenzene
50
53
1
105
70-130
04/04/2019 2005
Chloroethane
50
44
1
88
70-130
04/04/2019 2005
Chloroform
50
50
1
99
70-130
04/04/2019 2005
Chloromethane (Methyl chloride)
50
43
1
86
60-140
04/04/2019 2005
Cyclohexane
50
49
1
99
70-130
04/04/2019 2005
1,2-Dibromo-3-chloropro pane (DBCP)
50
47
1
93
70-130
04/04/2019 2005
Dibromochloromethane
50
52
1
104
70-130
04/0412019 2005
1,2-Dibromoethane (EDB)
50
50
1
100
70-130
04/04/2019 2005
1,2-Dichlorobenzene
50
52
1
105
70-130
04/04/2019 2005
1,3-Dichlorobenzene
50
53
1
106
70-130
04/04/2019 2005
1,4-Dichlorobenzene
50
53
1
106
70-130
04/04/2019 2005
Dichlorodifiuoromethane
50
43
1
85
60-140
04/04/2019 2005
1,1-Dichloroethane
50
48
1
97
70-130
04/04/2019 2005
1,2-Dichloroethane
50
50
1
100
70-130
04/04/2019 2005
1,1-Dichloroethene
50
50
1
101
70-130
04/04/2019 2005
cis-1,2-Dichloroethene
50
49
1
99
70-130
04/04/2019 2005
trans- l,2-Dichloroethene
50
50
1
101
70-130
04/04/2019 2005
1,2-Dichloropropane
50
50
1
99
70-130
04/04/2019 2005
cis- 1,3-Dichloropropene
50
50
1
99
70-130
04/04/2019 2005
trans-1,3-Dichloropropene
50
51
1
102
70-130
04/04/2019 2005
Ethylbenzene
50
53
1
106
70-130
04/04/2019 2005
2-Hexanone
100
110
1
106
70-130
04/04/2019 2005
Isopropylbenzene
50
54
1
107
7D-130
04/04/2019 2005
Methyl acetate
50
43
1
85
70-130
04/04/2019 2005
Methyl tertiary butyl ether (MTBE)
50
47
1
94
70-130
04/04/2019 2005
4-Methyl-2-pentanone
100
93
1
93
70-130
04/04/2019 2005
Methylcyclohexane
50
54
1
108
70-130
04/04/2019 2005
Methylene chloride
50
46
1
92
70-130
04/04/2019 2005
Styrene
50
53
1
105
70-130
04/04/2019 2005
1,1,2,2-Tetrachloroethane
50
49
1
97
70-130
04/04/2019 2005
Tetrachloroethene
50
56
1
111
70-130
04/04/2019 2005
Toluene
50
53
1
106
70-130
04/04/2019 2005
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
52
1
104
70-130
04/04/2019 2005
1,2,4-Trichlorobenzene
50
54
1
107
70-130
04/04/2019 2005
1,1,1-Tr€chloroethane
50
51
1
103
70-130
04/04/2019 2005
1,1,2-Trichi oroethane
50
50
1
100
70-130
04/04/2019 2005
LOO = Limit of Cuanlitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between hvo GC columns exceeds 40sfl N = Recovery is out of criteria
J = Estimated result < LOO and > DL + = RPD is out of criteria
NO = Not detected at or above the LOO
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, inc,
106 Vantage Point Drive West Columbia. SC 29172 [phone] Fax [phone] v✓ww.shealyiab,corn
Passe 52 of78

Volatile Organic Compounds
Sample ID: UQ12345-002
Matrix: Solid
Batch: 12345
Prep Method: 5035
Analytical Method: 8260D
Spike:
Amount
Result
% Rec
Parameter
(uglkg)
(uglkg) Q
Dil % Rec
Limit
Analysis Date
Trichloroethene
50
52
1 105
70-130
04/0412019 2005
Trichlorof€uoromethane
50
52
1 103
70-130
04/04/2019 2005
Vinyl chloride
50
50
1 100
70-130
04/04/2019 2005
Xylenes (total)
100
110
1 106
70-130
04/04/2019 2005
Surrogate
(� % Rec
Aecepta
Limit r�
Limit
8romofluorobenzene 96 47-138
1,2-Dichloroethane-d4 84 53-142
Toluene-d8 89 68-124
LOOP = Limit of Quantitaton
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40io N = Recovery is out of criteria
J = Estimated result < LOQ and � DL + = RPD is out of Cnteria
NO = Not detected at or above the LOQ
!dote: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 53 of 78

Sample 1D: UQ12345-003 matrix: Solid
Batch: 12345 Prep Method: 5035
Analvtical method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(uglkg)
(ug/kg) Q
Dil
% Rec
% RPD
Limit
Limit
-Analysis Date
Acetone
100
95
1
95
5.5
60-140
20
04/04/2019 2106
Benzene
50
47
1
94
8.4
70-130
20
04/04/2019 2106
Bromodichloromethane
50
48
1
96
5.0
70-130
20
04/04/2019 2106
B€omoform
50
45
1
91
12
70-130
20
04/04/2019 2106
Bromomethane (Methyl bromide)
50
51
1
102
12
70-130
20
04/04/2019 2106
2-Butanone (ME€C)
100
95
1
95
1.6
60-140
20
04/04/2019 2106
Carbon disulfide
50
41
1
82
19
70-130
20
04/04/2019 2106
Carbon tetrachloride
50
47
1
94
11
70-130
20
04/04/2019 2106
Chlorobenzene
50
48
1
96
8.7
70-130
20
04/04/2019 2106
Chloroethane
50
44
1
88
0.29
70-130
20
04/04/2019 2106
Chloroform
50
46
1
91
8.7
70-130
20
04/04/2019 2106
Chloromethane (Methyl! chloride)
50
54 +
1
108
22
60-140
20
04/04/2019 2106
Cyclohexane
50
51
1
102
2.7
70-130
20
04/04/2019 2106
1,2-Dibromo-3-chloropropane (DBCP)
50
47
1
95
1.6
70-130
20
04/04/2019 2106
Dibromochloromethane
50
48
1
96
7.6
70-130
20
04/04/2019 2106
1,2-Dibromoethane (EDB)
50
51
1
102
1.2
70-130
20
04104/2019 2106
1,2-Dichlorobenzene
50
49
1
98
6A
70-130
20
04/04/2019 2106
1,3-Dichlorobenzene
50
48
1
97
91
70-130
20
04/04/2019 2106
IA-Dichiorobenzene
50
48
1
96
10
70-130
20
04/04/2019 2106
D ichlorodifluoro methane
50
57 +
1
114
29
60-140
20
04/04/2019 2106
1, 1 -Dichloroethane
50
45
1
89
8,0
70-130
20
04/04/2019 2106
1,2-Dichloroethane
50
51
1
103
2.7
70-130
20
04/04/2019 2106
1,1-Dichloroethene
50
45
1
89
12
70-130
20
04/04/2019 2106
cis-1,2-Dichloroethene
50
45
1
90
9A
70-130
20
04/04/2019 2106
trans- l,2-Dichloroethene
50
45
1
89
12
70-130
20
04/04/2019 2106
1,2-Dichloropropene
50
47
1
94
5.7
70-130
20
04/04/2019 2106
cis-1,3-Dichloropropene
50
48
1
95
4.2
70-130
20
04/04/2019 2106
trans-1,3-Dichloropropene
50
48
1
97
5.0
70-130
20
04/04/2019 2106
Ethylbenzene
50
49
1
97
8.8
70-130
20
04/04/2019 2106
2-1-iexanone
100
100
1
104
2.0
70-130
20
04/04/2019 2106
[so propylbenzene
50
49
1
97
9.8
70-130
20
04/04/2019 2106
Methyl acetate
50
41
1
81
4.9
70-130
20
04/04/2019 2106
Methyl tertiary butyl ether (MTBE)
50
45
1
89
5.3
70-130
20
04/04/2019 2106
4-M ethyl-2-penta none
100
90
1
90
3.0
70-130
20
04/04/2019 2106
Methylcyciohexane
50
52
1
103
4.7
70-130
20
04/04/2019 2106
Methylene chloride
50
42
1
84
8.6
70-130
20
04/04/2019 2106
Styrene
50
48
1
96
9.2
70-130
20
04/04/2019 2106
1.1.2,2-Tetrachloroethane
50
48
1
96
0,91
70-130
20
04/04/2019 2106
Teirachloroethene
50
50
1
100
10
70-130
20
04/04/2019 2106
Toluene
50
49
1
97
9.0
70-130
20
04/04/2019 2106
1,1,2-Trichloro-1.2,2-Trifuoroethane
50
46
1
93
11
70-130
20
04/04/2019 2106
1,2,4-Trichlorobenzene
50
48
1
95
12
70-130
20
04/04/2019 2106
1,1,1-Trichloroethane
50
47
1
93
9.7
70-130
20
04/04/2019 2106
1,1,2-Trichloroethane
50
49
1
97
2.6
70-130
20
04/04/2019 2106
LOD = Limit of Quantitation
DL v Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40". N = Recovery is out of cnlena
J = Estimated result < LOQ and a DL + = RPD is out of criteria
ND = Not detected at or above the LOD
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wwvv,shealylab.com
Page 54 of 78

Tolatile OrganicCompounds
Semple ID: UQ12345-003
Matrix: Solid
Batch:12345
Prep
Method: 5035
Analytical Method: 8260D
Spike
Amount
Result
% Rec
% RPD
Parameter
(uglkg)
(uglkg) Q
Dil
% Rec % RPD
Limit
Limit
Analysis Date
Trichloroethene
50
51
1
101
3.7
70-130
20
04/04/2019 2106
Trichlorol1uoromethane
50
51
1
101
2,2
70-130
20
04/04/2019 2106
Vinyl chloride
50
50
1
99
0,99
70-130
20
04/04/2019 2106
Xylenes (total)
100
97
1
97
9.7
70-130
20
04/04/2019 2106
Acceptance
Surrogate Q % Rec Limit
BrDM oflu oro benzene
104
47-138
1,2-Dichloroethane-d4
93
53-142
Toluene-d8
102
68-124
LOD = Limit of Quantctatian P W The RPD betwoan two GC columns exceeds 40',o N = Recovery is out of criteria
DL = Detection Limit J = Estimated result � LOQ and > DL + = RPD 3s out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOD
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 55 of 78

Sample ID: UQ12197-001 Matrix: Solid
Batch:12197 Prep Method: 3546
Analytical Method: 8270E Prep Date: 04/03/2019 2212
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Acenaphthene
NO
1
13
ug/kg
04/05/2019 0955
Acenaphthylene
NO
1
13
ugfkg
04/05/2019 0955
Acetophenone
NO
1
67
ugfkg
04/05/2019 0955
Anthracene
ND
1
13
ugfkg
04/05/2019 0955
Atrazine
ND
1
67
ugfkg
04/05/2019 0955
Benzaldehyde
ND
1
67
ug/kg
04/05/2019 0955
Benzo(a)anthracene
NO
1
13
ugfkg
04/05/2019 0955
Benzo(a)pyrene
NO
1
13
ugfkg
04/05/2019 0955
Benzo(b)fluoranthene
NO
1
13
ugfkg
04/05/2019 0955
Benzo(g,h,i)perylene
NO
1
13
uglkg
04/05/2019 0955
Benzo(k)fluoranthene
NO
1
13
uglkg
04/05/2019 0955
1,1'-Biphenyl
NO
1
67
uglkg
04/05/2019 0955
4-Bromophenyl phenyl ether
ND
1
67
ugfkg
04/05/2019 0955
Butyl benzyl phthalate
NO
1
67
ugfkg
04/05/2019 0955
Caprolactam
NO
1
67
ugfkg
04/05/2019 0955
Ca€bazole
NO
1
67
ugfkg
04/05/2019 0955
bis (2-Chloro-1-methylethyl) ether
NO
1
67
ugfkg
04/05/2019 0955
4-Chloro-3-methyl phenol
NO
1
67
ugfkg
04/05/2019 0955
4-Chloroaniline
NO
1
67
ugfkg
04/05/2019 0955
bis(2-Chloroethoxy)methane
NO
1
67
ugfkg
04105/2019 0955
b is (2-C hl oroethyl) ether
ND
1
67
uglkg
04/05/2019 0955
2-Chloronaph£halene
NO
1
67
uglkg
04/05/2019 0955
2-Chlorophenol
NO
1
67
ugfkg
04/05/2019 0955
4-Chlorophenyl phenyl ether
ND
1
67
ug/kg
04/05/2019 0955
Chrysene
NO
1
13
ugfkg
04/05/2019 0955
Dibenzo(a,h)anth race ne
NO
1
13
ugfkg
04/05/2019 0955
Dibenzofuran
NO
1
67
ugfkg
04/05/2019 0955
3,3'-Dichlorobenzidine
ND
1
67
ug/kg
04/05/2019 0955
2,4-Dichlorophenol
NO
1
67
ugfkg
04/05/2019 0955
Diethylphthalate
NO
1
67
ugfkg
04/05/2019 0955
Dimethyl phthalate
NO
1
67
ugfkg
04/05/2019 0955
2,4-Dimethylphenol
NO
1
67
ugfkg
04/05/2019 0955
Di-n-butyl phthalate
NO
1
67
ugfkg
04/05/2019 0955
4,6-Dinitro-2-methylphenol
NO
1
330
uglkg
04/05/2019 0955
2,4-Dinitrophenol
ND
1
330
ugfkg
04/05/2019 0955
2,4-Dinitrotoluene
ND
1
130
uglkg
04/05/2019 0955
2,6-Dinitrotoluene
NO
1
130
ug/kg
04/05/2019 0955
Di-n-octylphthalate
NO
1
67
ug/kg
04/05/2019 0955
bis(2-Ethylhexyl)phthalate
NO
1
67
ug/kg
04/05/2019 0955
Fluoranthene
ND
1
13
ugfkg
04/05/2019 0955
Fluorene
ND
1
13
uglkg
04/05/2019 0955
Hexachlorobenzene
NO
1
67
ugfkg
04/05/2019 0955
Hexachlorobutadiene
ND
1
67
ugfkg
04/05/2019 0955
Hexachlorocyclopentadiene
ND
1
330
ugfkg
04105/2019 0955
L00 = Limit of 4uantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two CC columns exceeds 40% N = Recovery is out of criteria
J = Estimated result < LOO and > DL + = RPD is out of criteria
ND = Not detected at or above the LDQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 56 of 78

Sample ID: UQ12197-001 Matrix: Solid
Satch:12197 Prep Method: 3546
Analytical Method: 8270E Prep Date: 04/03/2019 2212
Parameter
Result Q
Dil
LOQ
Units
Analysis Date
Hexachforoethane
ND
1
67
uglkg
04/05/2019 0955
Indeno(1,2,3-c,d)pyrene
ND
1
13
uglkg
04/05/2019 0955
Isophorone
ND
1
67
uglkg
04/05/2019 0955
2-Methylnaphthalene
ND
1
13
uglkg
04/05/2019 0955
2-Methylphenol
ND
1
67
uglkg
04/05/2019 0955
3+4-Methylphenol
ND
1
130
uglkg
04/05/2019 0955
Naphthalene
ND
1
13
uglkg
04/05/2019 0955
2-Nitroaniline
ND
1
130
uglkg
04/05/2019 0955
3-Nitroaniline
ND
1
130
uglkg
04/05/2019 0955
4-Nitroaniline
ND
7
130
uglkg
04/05/2019 0955
Nitrobenzene
ND
1
67
uglkg
04/05/2019 0955
2-Nitrophenol
ND
1
130
uglkg
04/05/2019 0955
4-Nitrophenol
ND
1
330
uglkg
04/05/2019 0955
N-Nitrosodi-n-propylamine
Nil
1
67
uglkg
04/05/2019 0955
N-Nitrosodiphenylamine (Diphenylamine) ND
1
67
uglkg
04/05/2019 0955
Pentachlorophenol
ND
1
330
uglkg
04/05/2019 0955
Phenanth€ene
ND
1
13
uglkg
04/05/2019 0955
Phenol
ND
1
67
uglkg
04/05/2019 0955
Pyrene
ND
1
13
uglkg
04/05/2019 0955
2,4,5-Trichlorophenol
ND
1
67
uglkg
04/05/2019 0955
2,4,6-Trichlorophenol
ND
1
67
uglkg
04/05/2019 0955
Surrogate
Q
% Rec
Acceptance
LEmit
2-Fluorobiphenyl
97
24-137
2-Fluorophenol
97
16-136
Nitrobenzene-d5
81
12-144
Phenoi-d5
99
26-148
Terphenyl-d14
126
20-127
2,4,6-Tribromophenol
102
27-128
LOU = Limit of Quantilation
❑L = Detection Limit
LOD = Lima of Detection
P = The RPD between two GC columns exceeds 40% N = Recovery is out of cntena
J = Estimated result < LOU and > OL + = RPO is out of cntena
NO = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors In calculated results
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv,shealylab com
Page 57 of 79

r, x
Sample ID: UQ12197-002
Matrix: Solid
Batch:12197
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 04/03/2019 2212
Spike
Amount
Result
% Rec
Parameter
(uglkg)
(ug/kg)
4 Dil
% Rec
Limit
Anal sis Date
Acenaphthene
570
560
1
85
12-111
04105/20191020
Acenaphthylerie
670
610
1
91
44-122
04/05/2019 1020
Acetophenone
670
500
1
75
48-111
04105/20191020
Anthracene
670
650
1
98
16-122
04/05/2019 1020
Atrazine
670
690
1
103
48-116
04105120191020
Benzaldehyde
670
290
1
44
10-110
04105120191020
Benzo(a)anthracene
670
670
1
100
40-121
04/05/2019 1020
Benzo(a)pyrene
670
600
1
90
36-114
04/05/2019 1020
Benzo(b)fluoranthene
670
570
1
86
38-123
04/05/2019 1020
Benzo(g,h,i)perylene
670
730
1
110
43-120
04/05/2019 1020
Benzo(k)fluoranthene
670
590
1
88
40-126
04/05120191020
1,1'-Biphenyl
670
560
1
84
49-110
04105120191020
4-Bromophenyl phenyl ether
670
640
1
96
46-118
04/05/2019 1020
Butyl benzyl phthalate
670
730
1
109
46-128
04/05/2019 1020
Caprolactam
670
740
1
112
43-121
04/05120191020
Carbazole
670
680
1
103
47-128
04105120191020
bis (2-Chloro-l-methylethyl) ether
670
500
1
75
31-102
04/05/2019 1020
4-Chloro-3-methyl phenol
670
640
1
96
49-118
04/05/2019 1020
4-Chloroaniline
670
590
1
88
17-106
04105120191020
bis(2-Chloroethoxy)methane
670
540
1
81
39-108
04/05/2019 1020
bis(2-Chloroethyl)ether
670
520
1
78
32-105
04/05/2019 1020
2-Chloronaphthalene
670
560
1
85
31-127
04/05/2019 1020
2-Chlorophenol
670
570
1
85
37-106
04105120191020
4-Chlorophenyl phenyl ether
670
600
1
90
47-116
04/05/2019 1020
Chrysene
670
660
1
99
41-124
04105/20191020
Dibenzo(a,h)anthracene
670
590
1
88
38-125
04/05/2019 1020
Dibenzofuran
670
590
1
89
45.112
04105/20191020
3,3'-Dichlorobenz€dine
670
640
1
96
10-119
04105120191020
2,4-Dichlorophenol
670
610
1
92
41-113
04105120191020
Diethylphthalate
670
620
1
93
49-123
04105120191020
Dimethyl phthalate
670
620
1
93
48-120
04105/2019 1020
2,4-Dimethyiphenol
670
760
1
114
33-123
04105120191020
Di-n-butyl phthalate
670
670
1
100
51-129
04/05/2019 1020
4,6- Din itro-2-methylphenol
670
490
1
74
40-130
04/05120191020
2,4-Dinitrophenol
1300
520
1
39
10-113
04/05/2019 1020
2,4-Dinitrotoluene
670
660
1
99
48-124
04105/20191020
2,6-Dinitrotoluene
670
650
1
98
47-125
04/05/2019 1020
Di-n-octylphth a late
670
590
1
88
49-142
04/05120191020
bis(2-E1hylhexyl)phthalate
670
650
1
97
45-128
04105/20191020
Fluoranthene
670
680
1
102
26-133
04105120191020
Fluorene
670
620
1
92
19-108
04105/20191020
Hexachlorobenzene
670
680
1
102
44-122
04/05120191020
Hexachlorobutadiene
670
540
1
81
33-103
04105120191020
Hexachlorocyclopentadiene
3300
2400
1
72
18-121
04105120191020
LOCI = Limit of Quantltation
1A = Detection Lima
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 ' N = Recovery is out of criteria
J = Estimated result < LOQ and a DL + = RPD is cut of criteria
NO = Not detected at or above the LOQ
Rote: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com
Page 58 of 78

olatile Organic Compoundsby
Sample ID: UQ12197-002
Matrix: Solid
Batch: 12197
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 04/03/2019 2212
Spike
Amount
Result
% Rec
Parameter
(ugl(g)
(uglkg)
{2 Dil
% Rec
Limit
Analysis Date
Hexachioroethane
670
490
1
74
30-96
04/05/2019 1020
Indeno(1,2,3-c,d)pyrene
670
600
1
89
42-123
04/05/2019 1020
Isophorone
670
550
1
83
41-113
04/05120191020
2-Methylnaphthalene
670
560
1
85
10-107
04105120191020
2-Methylphenol
670
580
1
87
32-107
04/05120191020
3+4-Methylphenol
670
610
1
92
39-108
04105120191020
Naphthalene
670
560
1
83
10-112
04/05/2019 1020
2-Nitroaniline
670
720
1
107
45-123
04/05/2019 1020
3-Nitroaniline
670
670
1
100
24-127
04/05/2019 1020
4-Nitroaniline
570
710
1
106
48-127
04105/20191020
Nitrobenzene
670
520
1
78
33-114
04105/20191020
2-Nitrophenol
670
560
1
84
35-108
04/05/2019 1020
4-Nitrophenol
1300
1100
1
85
18-154
04/05120191020
N-Nitrosodi-n-propylamine
670
540
1
81
32-115
04/05120191020
N-Nitrosodiphenylamine (Diphenylamine) 670
660
1
98
53-150
04/05/2019 1020
Pentachlorophenol
1300
1300
1
94
27-138
04105120191020
Phenanthrene
670
630
1
94
16-123
04105120191020
Phenol
670
580
1
87
36-108
04/05/2019 1020
Pyrene
670
670
1
100
34-121
04/05/2019 1020
2,4,5-Trichlorophenol
670
650
1
98
46-122
04105120191020
2,4,6-Trichlorophenol
670
660
1
99
38-115
04105120191020
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
85
24-137
2-Fluoropheno€
83
16-136
Nitrobenzene-d5
81
12-144
Phenol-d5
86
26-148
Terphenyl-d14
117
20-127
2,4,6-Tribromophenol
109
27-128
LOQ = Limit of Quantitntion
OT W Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 401.16 N = Recovery is out of criteria
J = Estimated result , LOQ and > DL + = RPO is out of cntena
ND = Not detected at or above the LOQ
Note: Calculations are perforated before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc,
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com
Page 59 of 78

Sample ID: UD01039-002MS Matrix: Solid
Batch: 12197 Prep Method. 3546
Analytical Method: 82717E Prep bate: 04/03/2019 2212
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(uglkg)
(uglkg)
(ugfkg) Q
Dil
% Rec
Limit
Analysis Date
Acenaphthene
NO
820
790
1
97
12-111
04/05/2019 2109
Acenaphthylene
ND
820
690
1
84
44-122
04/05/2019 2109
Acetophenone
ND
820
820
1
101
30-130
04/05/2019 2109
Anthracene
ND
820
750
1
92
16.122
04/05/2019 2109
Atrazine
ND
820
820
1
101
30-130
04/05/2019 2109
Benzaldehyde
ND
820
250
1
30
10-110
04/05/2019 2109
Benzo(a)anthracene
ND
820
710
1
86
40-121
04/05/2019 2109
Benzo(a)pyrene
ND
820
760
1
93
36-114
04/05/2019 2109
Benzo(b)Duo ranthene
ND
820
740
1
90
38-123
04/05/2019 2109
Benxo(g,h,i)perylene
ND
820
720
1
88
43-120
04/05/2019 2109
Benzo(k)fluoranthene
ND
820
770
1
94
40-126
04/05/2019 2109
1,1'-Biphenyl
ND
820
690
1
85
30-130
04/05/2019 2109
4-Bromopheny€ phenyl ether
ND
820
680
1
83
30-130
04/05/2019 2109
Butyl benzyl phthalate
ND
820
960
1
118
30-130
04/05/2019 2109
Caprolactam
ND
820
800
1
98
30-130
04/05/2019 2109
Carbazole
ND
820
760
1
93
30-130
04/05/2019 2109
bis (2-Chloro-l-methylethyl) ether
ND
820
590
1
73
30-130
04/05/2019 2109
4-Chloro-3-methyl phenol
ND
820
750
1
91
30-130
04/05/2019 2109
4-Chloroaniline
ND
820
530
1
65
17-106
04/05/2019 2109
bis(2-Chloroethoxy)me1hane
ND
820
770
1
94
30-130
04/05/2019 2109
bis(2-Ch€oroethyl)ether
ND
820
850
1
103
30-130
04/05/2019 2109
2-Chloronaphthalene
ND
820
660
1
81
30-130
04/0612019 2109
2-Chlorophenol
ND
820
710
1
87
30-130
04/051201D 2109
4-Chlorophenyl phenyl ether
ND
820
670
1
82
30-130
04/05/2019 2109
Chrysene
ND
820
740
1
91
41-124
04/05/2019 2109
Dibenzo(a,h)anthracene
ND
820
780
1
96
38-125
04/05/2019 2109
Dibenzofuran
ND
82D
690
1
84
30-130
04/05/2019 2109
3,3'-Dichlorobenzidine
ND
820
670
1
82
10-119
04/05/2019 2109
2,4-Dichlorophenol
ND
820
650
1
80
30.130
04/05/2019 2109
Diethylphthalate
ND
820
840
1
102
30-130
04/05/2019 2109
Dimethyl phthalate
ND
820
690
1
84
30-130
04/05/2019 2109
2,4-Dimethylphenol
ND
820
1000
1
127
30-130
04/05/2019 2109
Di-n-butyl phthalate
ND
820
850
1
104
30-130
04/05/2019 2109
4,6-Dinitro-2-methyl phenol
ND
820
880
1
108
30-130
04/05/2019 2109
2,4-Dinitrophenoi
ND
1600
1600
1
100
30-130
04/05/2019 2109
2,4-Dinitrotoluene
ND
820
730
1
90
30-130
04/05/2019 2109
2,6-Dinitrotoluene
ND
820
740
1
90
30-130
04/05/2019 2109
Di-n-octylphthalate
ND
820
870
1
107
30-130
04/05/2019 2109
bis(2-Ethylhexyl)phthalate
ND
820
860
1
105
30-130
04/05/2019 2109
Fluoranthene
ND
820
710
1
87
26-133
04/05/2019 2109
Fluorene
ND
820
720
1
88
19-108
04105/2019 2109
Hexachlorobenzene
ND
820
620
1
75
30-130
04/05/2019 2109
Hexachlorobutadiene
ND
820
640
1
78
30-130
04/05/2019 2109
Hexachlorocyclopentadiene
ND
4100
3800
1
94
30-130
0410512019 2109
LQQ = Limit of Quantitation
OL = Detection Limit
LOO = Limit of Detection
P = The RPO between two GC columns exceeds 4055 N = Recovery is out of criteria
J = Estimated result , LOO and � DL + = RPM is out of enteric
NO = Not detected at or above the LOCI
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 00 of 78

Sample ID: UD01039-002MS
Matrix: Solid
Batch: 12197
Prep Method: 3546
Analytical Method: 8270E
Prep Date: 04/03/2019 2212
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/kg)
(u9/k9)
(u91kg)
Q DIE
% Roe
Limit
Analysis Date
ftexachloroethane
NO
820
840
1
102
30-130
04/05/2019 2109
Indeno(1,2,3-c,d)pyrene
ND
820
770
1
94
42-123
04/05/2019 2109
Isophorone
ND
820
890
1
108
30-130
04/05/2019 2109
2-Methylnaphthalene
ND
820
660
1
81
10-107
04/05/2019 2109
2-Methylphenol
NO
820
860
1
105
30-130
04/06/2019 2109
3+4-Methylphenol
NO
820
800
1
97
30-130
04/05/2019 2109
Naphthalene
ND
820
730
1
90
10-112
04/05/2019 2109
2-Nitroaniline
ND
820
850
1
104
30-130
04/05/2019 2109
3-Nitroaniline
ND
820
500
1
61
30-130
04/05/2019 2109
4-Nitroaniline
ND
820
810
1
99
30-130
04/05/2019 2109
Nitrobenzene
ND
820
970
1
118
30-130
04/05/2019 2109
2-Nitrophenol
ND
820
690
1
85
30-130
04/05/2019 2109
4-Nitrophenol
NO
1600
2100
1
129
30-130
04/05/2019 2109
N-Nitrosodi-n-propylamine
NO
820
1000
1
122
30-130
04/05/2019 2109
N-Nitrosodiphenylamine (Diphenylamine)
NO
820
780
1
95
30-130
04/05/2019 2109
Pentachlo€ophenol
NO
1600
1600
1
97
30-130
04/05/2019 2109
Phenanthrene
NO
820
790
1
96
16-123
04/05/2019 2109
Phenol
NO
820
840
1
103
30-130
04/05/2019 2109
Pyrene
NO
820
690
1
85
34-121
04/05/2019 2109
2,4,5-Trichlorophenol
NO
820
650
1
80
30-130
04/05/2019 2109
2,4,6-Trichlorophenol
ND
820
670
1
82
30-130
04/05/2019 2109
Surrogate
Q % Roc
Acceptance
Limit
2-Fluorobiphenyl
81
24-137
2-Fluorophenol
82
16-136
Nitrobenzene-d5
123
12-144
Phenol-d5
93
26-148
Terphenyl-d14
93
20-127
2,4,E-Tribromophenol
81
27-128
LOQ = Limit of Quantitation
OL = detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
J = Estimated result � LOQ and � Dl, + = RPD is out of criteria
ND = Not detected at or above the LOD
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] svww.sheaiyiab,com
Page 61 of 78

Sample ID: D01039-002MD
Matrix: Solid
Batch: 12197
Prep Method: 3546
Analytical Method: 8270E
Prep Date: 04/03/2019 2212
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(uglkg)
(uglkg)
(uglkg)
Q Dil
% Rec
% RPD
Limit
limit
Analysis Date
Acenaphthene
NO
800
700
1
87
13
12-111
30
04/05/2019 2132
Acenaphthylene
ND
800
610
1
77
12
44-122
30
04/05/2019 2132
Acetophenone
NO
800
760
1
95
8.4
30-130
40
04/05/2019 2132
Anthracene
NO
800
700
1
88
7.1
16-122
30
04/05/2019 2132
Atrazine
ND
800
770
1
97
6A
30-130
40
04/05/2019 2132
Benzaldehyde
ND
800
320
1
40
25
10-110
40
04/05/2019 2132
Benzo(a)anthracene
ND
800
670
1
84
5.9
40-121
30
04/05/2019 2132
Benzo(a)pyrene
ND
800
700
1
88
8.5
36-114
30
04/05/2019 2132
Benzo(b)fluoranthene
NO
800
700
1
88
4.9
38-123
30
04/05/2019 2132
Benzo(g,h,i)perylene
NO
800
680
1
85
5.6
43-120
30
04/05/2019 2132
Benzo(k)fluoranthene
NO
800
710
1
89
7.6
40-126
30
04/05/2019 2132
1,1'-Biphenyl
NO
300
600
1
75
15
30-130
40
04/05/2019 2132
4-Bromophenyl phenyl ether
NO
800
620
1
77
9.8
30-130
40
04/05/2019 2132
Butyl benzyl phthalate
ND
800
910
1
114
5.3
30-130
40
04/05/2019 2132
Caprolactam
NO
800
730
1
91
9.8
30-130
40
04/05/2019 2132
Carbazole
NO
800
700
1
88
8.4
30-130
40
04/05/2019 2132
bis (2-Chloro-l-methylethyl) ether
NO
800
530
1
66
12
30-130
40
04/05/2019 2132
4-Chloro-3-methyl phenol
NO
800
680
1
85
9.4
30-130
40
04/05/2019 2132
4-Chloroanilfne
NO
800
520
1
66
24
17-106
40
04/05/2019 2132
bis(2-Chloroethoxy)methane
ND
800
680
1
86
12
30-130
40
04/05/2019 2132
bis(2-Chloroethyl)ether
ND
800
760
1
96
10
30-130
40
04/05/2019 2132
2-Chloro naphthalene
ND
800
590
1
74
12
30-130
40
04/05/2019 2132
2-Chlorophenol
NO
800
660
1
83
7,6
30-130
40
04/05/2019 2132
4-Chlorophenyl phenyl ether
NO
800
570
1
72
16
30-130
40
04/05/2019 2132
Chrysene
NO
800
710
1
89
4.8
41-124
30
04105/2019 2132
Dibenzo(a,h)anthracene
NO
800
730
1
92
6.9
38-125
30
04/05/2019 2132
Dibenzofuran
NO
800
610
1
77
12
30-130
40
04/05/2019 2132
3,3'-Dichlorobenzidine
ND
800
670
1
84
0.77
10-119
40
04/05/2019 2132
2,4-Dichlorophenol
NO
800
580
1
73
11
30-130
40
04/05/2019 2132
Diethylphthalate
ND
800
760
1
95
10
30-130
40
04/05/2019 2132
Dimethyl phthalate
ND
800
640
1
80
7.4
30-130
40
04/05/2019 2132
2,4-Dimethylphenol
NO
800
920
1
115
12
30-130
40
04/05/2019 2132
Di-n-butyl phthalate
NO
800
790
1
100
6.9
30-130
40
04/05/2019 2132
4,6-Dinitro-2-methylphenol
ND
800
830
1
104
6.0
30-130
40
04/05/2019 2132
2,4-Dinitrophenol
NO
1600
1500
1
91
12
30-130
40
04/05/2019 2132
2,4-Dinitrotoluene
ND
800
670
1
84
9.5
30-130
40
04/05/2019 2132
2,6-Dinitrotoluene
ND
800
680
1
86
8.0
30-130
40
04/05/2019 2132
Di-n-octylphthalate
NO
800
820
1
103
5.8
30-130
40
04/05/2019 2132
bis(2-Ethylhexyl)phthalate
ND
800
810
1
102
5.4
30-130
40
04/05/2019 2132
Fluoranthene
NO
800
660
1
82
7.4
26-133
30
04/05/2019 2132
Fluorene
NO
800
640
1
80
12
19-108
30
04/05/2019 2132
Hexachlorobenzene
ND
800
560
1
71
8.8
30-130
40
04/05/2019 2132
Hexachlorobutadiene
NO
800
540
1
68
16
30-130
40
04/05/2019 2132
Hexachiorocyciopentadiene
NO
4000
3200
1
80
19
30-130
40
04/05/2019 2132
LQQ = Limit of Quantitation
DL = Detection Limit
LOB W Limit of Detection
P W The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
NO = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab,com
Page 62 of 78

Semivolatile Organic Compounds by GC/MS - MSD
Sample ID: UD01039-002MD
Matrix: Solid
Batch: 12197
Prep Method:
3546
Analytical Method: 8270E
Prep Date: 04/03/2019 2212
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/kg)
(uglkg)
(ug1kg)
Q Dil
% Rec
% RPD
Limit
Limit
Anal sis Date
Hexachloroethane
NO
800
720
1
90
15
30-130
40
04/05/2019 2132
Indeno(1,2,3-c,d)pyre ne
NO
800
720
1
91
6.6
42-123
30
04/05/2019 2132
Isopho€one
NO
800
80o
1
100
10
30-130
40
04/05/2019 2132
2-Methylnaphthalene
NO
800
570
1
72
15
10-107
30
04/05/2019 2132
2-Methylphenol
ND
800
860
1
108
0.36
30-130
40
04/05/2019 2132
3+4-Methylphenol
NO
Boo
750
1
95
5.5
30-130
40
04/05/2019 2132
Naphthalene
NO
800
630
1
80
14
10-112
30
04/05/2019 2132
2-Nitroaniline
ND
800
77D
1
96
9.9
30-130
40
04/05/2019 2132
3-Nitroaniline
NO
800
520
1
65
3.8
30-130
40
04/05/2019 2132
4-Nitroaniline
NO
800
780
1
97
4.1
30-130
40
04/05/2019 2132
Nitrobenzene
NO
800
850
1
107
12
30-130
40
04/05/2019 2132
2-Nitrophenol
ND
800
630
1
80
9.0
30-130
40
04/05/2019 2132
4-Nitrophenol
Nil
1600
2000
1
123
7.8
30-130
40
04/05/2019 2132
N-Nitrosodi-n-propylamine
NO
800
910
1
114
9.5
30-130
40
04/06/2019 2132
N-Nitrosodiphenylamine (Diphenylamine)
NO
800
710
1
89
9.7
30-130
40
04/05/2019 2132
Pentachlorophenol
NO
1600
1400
1
88
12
30-130
40
04/05/2019 2132
Phenanthrene
NO
Soo
720
1
90
9.0
16-123
30
04/05/2019 2132
Phenol
NO
800
780
1
98
8.2
30-130
40
04/05/2019 2132
Pyrene
Nil
800
650
1
82
6A
34-121
30
04/05/2019 2132
2,4,5-Trichlorophenol
NO
Soo
580
1
73
12
30-130
40
04/05/2019 2132
2,4,6-T€ichlorophenol
ND
800
580
1
73
14
30-130
40
04/05/2019 2132
Surrogate
Q % Rec
Acceptance
Limit
2-Fluorobiphenyl
72
24-137
2-Fluorophenol
79
16-136
Nitrobenzene-d5
110
12-144
Phenol-d5
88
26-148
Terphenyl-d14
92
20-127
2,4,6-Tribromophenol
72
27-128
LOO = Ltmit of Quantitat=
DL = Detection Limit
LOD : Limit of Detection
P = The RPO behveert two GC columns exceeds 40% N = Recovery is out of criteria
J = Estimated result a LCQ and? DL + T RPD is out of criteria
ND = Not detected at or above the tOQ
Note: Calculations are performed before rounding to avoid round -oft errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Dnve West Columbia, SC 29172 [phone] Fax [phone] wvmi.sheaiytah,cam
Page 63 of 78

A EPEE (alipha ics) - MB
Sample ID: Q12193-001 Matrix, Solid
Batch: 12193 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 04/04/2019 837
Parameter Result Q Dil LOQ Units Analysis Date
C9 - C18 Aliphatics ND 1 10 mglkg 04/10/2019 1158
C19 - C36 Aliphatics ND 1 10 mg/kg 04/10/2019 1158
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 87 40-140
LOQ = Limit of Quantitalion
DL = Detection Limit
LOD = Limit of Detection
P = The RPO between two GC columns exceeds 405b N = Recovery is out of cntena
J = Estimated result < LOQ and > DL + = RPl7 is out of cnteria
ND W Not detected al or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc,
106 Vantage Point Drive west Columbia, SC 29172 [phone] Fax [phone] a %VY�Lshealylab.com
Page 64 of 79

MA EPH (aiiphatics) - LCS
Sample ID: U012193-002
Matrix, Solid
Batch: 12193
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Prate: 04/04/2019 837
Spike
Amount
Result
% Rec
Parameter
(mglkg)
(mglkg) L2
Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
30
19
1 65
40-140 04/10/2019 1228
C19 - C36 Aliphatics
40
33
1 82
40-140 04/10/2019 1228
Surrogate
Q % ReC
Acceptance
Limit
1-Chloro-octadecane (aliphatic) 85 40-140
LOQ = Limit of Ouantitation
CL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 4090 N = Recovery it out of criteria
J = Estimated result , LOO and > OL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc,
106 Vantage Point Chive West Colombia, SC 29172 [phone] Fax [phone] www,shealylab.com
Page 65 of 79

A EPH (aliphatcs) - LCS®
Sample ID: UQ12193-003
Matrix: Solid
Batch: 12193
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 04/04/2019 837
Spine
Amount
Result
% Rec
% RPD
Parameter
(mglkg)
(mg/kg) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
30
19
1 63 2,3 40-140
25 04/10/2019 1257
C19 - C36 Aliphatics
40
31
1 77 6.4 40-140
25 04/10/2019 1257
Surrogate Q % Rec Acceptance
Limit
1-Chloro-octadecane (aliphatic) 86 40-140
LOO = Limit of Quntitation P = The RPD behveen Ivro GC columns exceeds 4M° N = Recovery is out of tritons
DL = Detection Limit J = Estimated result , LOO and > OL } = RPD is out of Warm
t OD = Limit of Detection ND = Not detected at or above the LOO
(Vote: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv.shealylab.com
Page 66 of 78

A EPH (aromatics) - MB
Sample ID: LJQ12217-001 Matrix: Solid
Batch: 12217 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 04/04/2019 837
Parameter Result Q Dil LOQ Units Analysis Date
C11 - C22 Aromatics NO 1 10 mg/kg 04/10/2019 1654
Acceptance
Surrogate Q % Rec Limit
2-B€omonaphthalene (fractionation 2) 72 40-140
2-Fluorobiphenyl (fractionation 1) 92 40-140
o - Terphenyl (aromatic) 79 40-140
LOQ = Limit of Quanlitation P = The RPD between two GC columns exceeds 40"/ N = Recovery is out of criteria
DL = Detection Limit J = Estimated result e LOQ and > DL + = RPD is out of criteria
LOD = Limit of Defection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Sheaty Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 (8173) 791.9700 Fax [phone] wvm shealylab.com
Page 67 of 78

MA EPH (aromatics) - LCS
Sample 1D: UQ12217-002
Matrix: Solid
Batch: 12217
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 04/04/2019 837
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(m91k9) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
85
72
1 84 40-140 04/10/2019 1724
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthaiene (fractionation 2) 68 40-140
2-Flucrobiphenyl (fractionation 1) 95 40-140
o - Terphenyl (aromatic) 82 40-140
LQQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two CC columns exceeds 40% N = Recovery is out of criteria
J = Estimated result c LOQ and > DL + = RPO is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvoi shealylab corn
Page 69 of 78

Sample 10: UQ12217-003 Matrix: Solid
Batch: 12217 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 04/04/2019 837
Spike
Amount Result % Rec % RPD
Parameter (mglkg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 85 65 1 77 9.4 40-140 25 04/10/2019 1754
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 72 40-140
2-Fluorobiphenyl (fractionation 1) 87 40-140
o - Terphenyl (aromatic) 76 40-140
LOQ = Limit of Quantitation P = The RPO between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOSS = Limit of Detection NO = Not detected at of above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, $G 29172 [phone] Fax [phone] www.shealylab,cam
Page 69 of 78

Sample ID: UQ12261-001 Matrix; Solid
Batch: 12261 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LQQ Units Analysis Date
C9 - C10 Aromalics ND 1 1.3 mgfkg 04/03/2019 1453
Surrogate
2,5-Dibromotoluene (PID)
LOD = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
Acceptance
Q % Roe Limit
117 7D-130
P = The RPD behveen two GC columns exceeds 40% N = Recovery is out of cntena
J = Estimated resuit < LOO and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv,shealylab,corn
Page 70 of 78

Sample ID: UQ12261-002 Matrix: Solid
Batch: 12261 Prep Method: VPH
Analytical Method: MADE P-VPH-18-2.1
Spike
Amount Result % Rae
Parameter (mglkg) (mglkg) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 1.3 1.3 1 104 70-130 04/03/2019 1356
Acceptance
Surrogate Q % Rae Limit
2,5-Dibromotoluene (PID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOO = Limit of Detection
108 70-130
P = The RPD between hvo GC columns exceeds 40 ' N = Recovery is out of criteria
J = Estimated result < IM and > DL + = RPD is out of triter€a
ND = Not detected at of above the LOQ
Note: Calculations are performed before rounding to avoid round -oil' errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv.shealylab,com
Page 71 of 78

Sample ID: UQ12261-003 Matrix: Solid
Batch: 12261 Prep Method: VPH
Analytical Method: MADE P-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (mglkg) (mglkg) Q Dif % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 1.3 1.2 1 96 8.0 70-130 25 04/03/2019 1425
Acceptance
Surrogate 4 % Rec Limit
2,5-Dibromotoluene (PO) 108 70-130
LOO = Limit of Quantitahon P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
DL = Detection Limit J = Estimated result - LCQ and ? OL e = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOO
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] wvnv,shenlylab-eom
Page 72 of 78

ADEP VPH (alipha ics) - M
Sample ID: UQ12262-001 Matrix: Solid
Batch: 12262 Prep Method: VPH
Analytical Method: MADFP-VPH-18-2.1
Parameter Result Q Dil LOQ Units Analysis Date
C5 - C8 Aliphatics ND 1 3.8 mg/kg 04/03/2019 1453
C9 - C12 Aliphatics ND 1 3.8 mg/kg 04/03/2019 1453
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 116 70.130
LOD = Limit of Ouantitation P =The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOO and > OL + = RPD is out of criteria
LOD = Limit of Detection NO = Not detected at or Z"ve the LOO
Note: Calculations are performed before rounding to avoid round -oil errors in calculated results
Shealy Environmental Services, Inc,
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 73 of 78

MADEP VPH a
Sample ID: UQ12262-002
Matrix: Solid
Batch: 12262
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter (mglkg)
(mg/kg)
Q Dil % Rec
Limit Analysis Date
C5 - C8 Aliphatics 7.5
7.0
1 94
70-130 04/03/2019 1356
C9 - C12 Allphatics 8.8
9.1
1 104
70-130 04/03/2019 1356
Surrogate
2,5-Dibromotoluene (FID)
LOQ = Limit of Quantitation
DL = Detection Limit
LOD m Limit of Detection
Acceptance
Q % Rec Limit
107 70-130
P = The RPD between two GC columns exceeds 4W4 N = Recovery is out of criteria
J = Estimated result < LOD and > OL + = RPD is out of criteria
NO � Not detected at or above the LOO
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Ina
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] WWW.shealylab.com
Page 74 of 78

A®EP VPH (aiiphatics) - LGS®
Sample ID: U012262-003
Matrix: Solid
Batch: 12262
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
% RPD
Parameter (m91k9)
(mg/kg) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics 7.5
6.7
1 90 4.5
70-130
25 04/03/2019 1425
C9 - C12 Aliphatics 8.8
8.5
1 98 6.3
70-130
25 04/03/2019 1425
Surrogate
2,5-Dibromotoluene (FID)
LOG = Limit of Guantltation
DL w Detection Limit
LOD = Limit of Detection
Acceptance
Q % Rec Limit
105 70-130
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated resu€t < LOG and ? OL + = RPD is out of criteria
NO = Not detected at or above the LOO
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Paint Drive West Columbia, SC 29172 [phone] Fax [phone] vvirrva-shenlylab.com
Page 75 of 78

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Beverly, Trudy
From: Tommy Bolyard <[e-mail]>
Sent: Wednesday, April 24, 2019 4:12 PM
To: Beverly, Trudy
Subject: RE: [External] FW: Initial Site Assessment Report - 3901ShilohChurchRoad Site
AST
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to [e-mail]
OK, that's what I'll use. Thanks.
Sent from Mail for Windows 10
From: Beverly, Trudy
Sent: Wednesday, April 24, 2019 3:47 PM
To: Tommy Bolvard
Subject: RE: [External] FW: Initial Site Assessment Report - 3901ShilohChurchRoad Site AST
Below would be a good name for the report file.
MO-XXXX_XXXXXX_CA_SAR_20190424_Initial Site Assessment Report
Trudy
From: Tommy Bolyard [mailto:[e-mail]]
Sent: Wednesday, April 24, 2019 3:43 PM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] FW: Initial Site Assessment Report - 3901 ShilohChurchRoad Site AST
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to [e-mail]
I'm still confused as to how this site should be numerically classified for submittal based on the link you
provided. Can you clarify?
Sent from Mail for Windows 10
From: Beverly, Trudy
Sent: Wednesday, April 24, 2019 3:38 PM
To: Tommy Bolvard
Subject: RE: [External] FW: Initial Site Assessment Report - 3901 ShilohChurchRoad Site AST
I will add it to the database after I receive your data. You can use and X in place of the incident number.
i

Trudy
From: Tommy Bolyard [mailto:[e-mail]]
Sent: Wednesday, April 24, 2019 3:36 PM
To: Beverly, Trudy <[e-mail]>
Subject: RE: [External] FW: Initial Site Assessment Report - 3901 ShilohChurch Road Site AST
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to [e-mail]
Is there an incident number for this site?
Sent from Mail for Windows 10
From: Beverly, Trudy
Sent: Wednesday, April 24, 2019 2:45 PM
To: Tommy Bolyard
Subject: RE: [External] FW: Initial Site Assessment Report - 3901 ShilohChurch Road Site AST
Hey Tom,
Please submit documents per UST policies below for review.
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/Electronic%20Document%20Submittal
%20Memo%20Update.pdf
hops://files.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/UST%20file%20names%20for%20Las
erfiche.docx
Thanks,
Trudy
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-
program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-mana eg merit- ig's-maps

File Review Procedures:
hiips:Hdeq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https:Hedocs.deq.nc.gov/WasteManagement/Search.aspx
Document Submittal & UST File Names for Laserfiche Policies:
hM2s:Hfiles.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/Electronic%2ODocument%2OSubmittal
%20Memo%20Update.pdf
hiips:Hfiles.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%2Ofile%20names%20for%2OLas
erfiche.docx
From: Tommy Bolyard [mailto:[e-mail]]
Sent: Wednesday, April 24, 2019 2:32 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] FW: Initial Site Assessment Report - 3901 Shiloh Church Road Site AST
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to [e-mail]
Trudy:
Attached is the Initial Site Assessment Report for the AST heating oil site we discussed previously. It appears
that we have removed all the petroleum contaminated soil. Let me know if you need any additional
information.
Thanks,
Tom Bolyard, PG
Sr. Hydrogeologist
Sent from Mail for Windows 10