HomeMy WebLinkAbout60H_ThomasRd_Phase II ESA_July 2018
SUMMIT Engineering, Laboratory & Testing, Inc. 3575 Centre Circle Fort Mill, South Carolina 29715
www.SUMMIT-companies.com
Phone: (704) 504-1717
Fax: (704) 504-1125
July 16, 2018
Mr. Robert Miller Century Communities 7400 Carmel Executive Park Drive Suite 205 Charlotte, NC 28226
Subject: Limited Phase II Environmental Site Assessment
Thomas Road Site 14900 Thomas Road Charlotte, Mecklenburg County, North Carolina
SUMMIT Project No. 4319.514
Dear Mr. Miller:
SUMMIT ENGINEERING, LABORATORY & TESTING, P.C. (SUMMIT) is pleased to submit the following report of our Limited Phase II Environmental Site Assessment (ESA) of the Thomas Road Site, located at the 14900 Thomas Road, Charlotte, Mecklenburg County, North Carolina (Mecklenburg Tax IDs: 21703102 & 21703155).
This report includes a description of the methodology of our investigation and a summary of our
findings and conclusions. If you have any questions regarding our assessment of the subject
property or our conclusions, please do not hesitate to call us at (704) 504-1717.
Sincerely,
SUMMIT
Patrick W. Lowery, LG Michael D. Zavislak, NRCC-EAC, CIH, PE
Senior Environmental Manager Environmental Department Manager
NC LG No: 2421
SUMMIT’s NC Engineering Firm License No. C-2530
LIMITED PHASE II ENVIRONMENTAL SITE ASSESSMENT THOMAS ROAD SITE CHARLOTTE MECKLENBURG COUNTY
NORTH CAROLINA
SUMMIT PROJECT NO. 4319.514
Prepared For:
Century Communities
7400 Carmel Executive Park Drive
Charlotte, NC 28226
Prepared By:
SUMMIT ENGINEERING, LABORATORY & TESTING, P.C.
3575 Centre Circle
Fort Mill, South Carolina 29715
704-504-1717
July 16, 2018
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514
Charlotte, North Carolina July 16, 2018
E:\Project Forms\Projects\4319.514 Thomas Road Site - Phase I ESA\Limited Phase II ESA\4319.514 Thomas Road Site - Phase II ESA.doc i
TABLE OF CONTENTS
1.0 EXECUTIVE SUMMARY ......................................................................................................... 1
2.0 INTRODUCTION ....................................................................................................................... 2
2.1. PURPOSE .............................................................................................................................................. 2
2.2. SITE DESCRIPTION ........................................................................................................................... 2
2.3. ASSESSMENT HISTORY ................................................................................................................... 2
2.4. WORK PLAN OBJECTIVES .............................................................................................................. 3
3.0 PROPERTY SETTING ............................................................................................................... 4
3.1. TOPOGRAPHIC SETTING ................................................................................................................. 4
3.2. GEOLOGIC SETTING ......................................................................................................................... 4
3.3. HYDROLOGIC SETTING .................................................................................................................. 5
4.0 SUMMARY OF FIELD ACTIVITIES ....................................................................................... 6
4.1. DRILLING ACTIVITES AND METHODS ....................................................................................... 6
4.2. SAMPLING ........................................................................................................................................... 7
4.3. PACKING AND SHIPMENT .............................................................................................................. 7
4.4. SAMPLING POINT ABANDONMENT ............................................................................................ 8
5.0 SUMMARY OF LABORATORY ANALYSIS .......................................................................... 9
6.0 FINDINGS & CONCLUSIONS ............................................................................................... 10
7.0 QUALIFICATION OF REPORT .............................................................................................. 11
8.0 ADDITIONAL SERVICES ...................................................................................................... 12
9.0 REFERENCES .......................................................................................................................... 13
APPENDICES
Appendix I: FIGURES
Appendix II: ANALYTICAL SUMMARY
Appendix III: ANALYTICAL RESULTS Appendix IV: WELL RECORDS/PERMITS
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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1.0 EXECUTIVE SUMMARY
SUMMIT Engineering, Laboratory and Testing, P.C. (SUMMIT) personnel conducted a Limited
Phase II ESA of the Thomas Road Site, based on environmental concerns identified during the
completion of due diligence activities for the subject site. The reported concerns were in connection
with a former Construction and Land Clearing Debris landfill operated on the subject property.
Field work was completed by SUMMIT on July 1, 2018 and July 2, 2018.
In summary, three (3) groundwater samples were attempted to be collected from the subject site to
identify if the observed former construction and land clearing debris landfill on-site impacted the
environmental quality of the groundwater at the subject site. TMW-2 did not yield groundwater for
sampling at the time of this assessment. All collected groundwater samples were analyzed for the
presence of VOCs and Total RCRA Metals (dissolved phase).
Acetone was the only detection in the collected groundwater samples. Acetone was detected well
below the North Carolina Groundwater standards (NC 2L) and is considered a laboratory artifact.
No other detections were reported.
Based on the results of this Limited Phase II ESA, SUMMIT concludes that the identified former
construction and land clearing debris landfill has not significantly impacted the subject site at the
time of this report. Therefore, SUMMIT recommends no further assessment.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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2.0 INTRODUCTION
2.1. PURPOSE
SUMMIT was retained by Century Communities, to perform a Limited Phase II ESA of the Thomas
Road Site, located at 14900 Thomas Road, Charlotte, Mecklenburg County, North Carolina
(Mecklenburg Tax IDs: 21703102 & 21703155). The Limited Phase II ESA was requested in order
to assess environmental concerns adjacent to a construction and land clearing debris landfill area
located on the subject property. The landfill was reportedly operated from 1985 to 1987 by Blythe
Industries. This report presents the results of our Limited Phase II ESA of the Thomas Road Site. .
2.2. SITE DESCRIPTION
The site is irregular in shape and was noted to be comprised of two (2) parcels (Mecklenburg Tax
IDs: 21703102 & 21703155) totaling approximately 38.75 acres in area. The subject site is
primarily undeveloped and wooded, with a vacant residential home located near Thomas Road. The
landfill area was reported by the client and identified in previous reports to be located along the
southern site boundary. The site is accessible from Thomas Road to the east of the site. Refer to the
Sampling Location Map shown in Figure 2 of Appendix I for the location of the subject property.
2.3. ASSESSMENT HISTORY
SUMMIT was provided a Phase I ESA completed by others for the subject property, dated
December 1, 2016. The report did not identify the presence of RECs in connection with the site.
The report identifies the former landfill on the site. According to their findings, sampling of four 94)
water supply wells near the site by Mecklenburg County did not identify groundwater
contamination. Test pits performed as part of a geotechnical investigation identified only landscape
debris, trash and other inert materials (brick, concrete, etc.). Since the test pits did not contain
hazardous materials and the groundwater samples did not identify contaminants, the former
construction landfill was considered a De Minimus condition at the time of the December 1, 2016
report.
No other site specific or surrounding area assessment history is known at the time of this report.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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2.4. WORK PLAN OBJECTIVES
SUMMIT proposed to perform a Limited Phase II ESA according to our understanding of the most
likely potential for impact, in general accordance with ASTM E1903, and in accordance with the
USEPA Field Branches Quality System and Technical Procedures Manual. The proposed scope of
services included the installation and sampling of three (3) temporary monitoring wells in order to
assess the soil and groundwater quality adjacent to the debris area on the site. The proposed
sampling locations were placed in locations and in areas that may help identify migrating
contaminants from the area of concern. All samples collected were scheduled to be relinquished to a
NC certified laboratory for analysis. Collected groundwater samples were submitted for of Volatile
Organic Compounds by EPA method 8260 and for dissolved RCRA Metals by EPA method 6010.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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3.0 PROPERTY SETTING
3.1. TOPOGRAPHIC SETTING
The United States Geological Survey (USGS) Lake Wylie topographic quadrangle map was
reviewed for this report. The elevation of the subject property ranges from approximately 740 feet
above Mean Sea Level (MSL) to 640 msl. The contour lines indicate the general direction of
downward slope to west towards an unnamed tributary of Torrence Branch. The Torrence Branch
flows southwest and enters Lake Wylie. Refer to Figure 1 in Appendix I of this report.
3.2. GEOLOGIC SETTING
The property is located in Mecklenburg County, North Carolina, which is located in the south central
Piedmont Physiographic Province. The Piedmont Province generally consists of well-rounded hills
and ridges which are dissected by a well-developed system of draws and streams. The Piedmont
Province is predominantly underlain by metamorphic rock (formed by heat, pressure and/or
chemical action) and igneous rock (formed directly from molten material) which were initially
formed during the Precambrian and Paleozoic eras. The volcanic and sedimentary rocks deposited
in the Piedmont Province during the Precambrian era were the host from the metamorphism and
were changed to gneiss and schist. The more recent Paleozoic era had periods of igneous
emplacement, with at least episodes of regional metamorphism resulting in the majority of the rock
types seen today.
The topography and relief of the Piedmont Province has developed from differential weathering of
the igneous and metamorphic rock. Ridges and hills have been developed on the more easily
weathered and erodible rock. Because of the continued chemical and physical weathering, the rocks
in the Piedmont Province are now generally covered with a mantle of soil that has weathered in
place from the parent bedrock. These soils vary in thickness and are referred to as residuum or
residual soils. The residuum is typically finer grained and has higher clay content near the surface
because of the advanced weathering. Similarly, the soils typically become coarser grained with
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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increasing depth because of decreased weathering. As the weathering decreases, the residual soils
generally retain the overall appearance, texture, gradation and foliations of the parent rock.
3.3. HYDROLOGIC SETTING
Based on a review of the United States Geological Survey (USGS) Lake Wylie topographic
quadrangle map, the inferred groundwater flow direction based on topography appears to be to the
west towards the unnamed tributary of Torrence Branch. Refer to Figure 1 in Appendix I for a
topographic map for the subject property.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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4.0 SUMMARY OF FIELD ACTIVITIES
4.1. DRILLING ACTIVITES AND METHODS
On July 1, 2018, SUMMIT personnel conducted the temporary monitoring well installation scope
of the Limited Phase II ESA. The proposed temporary monitoring well (TMW) locations were
placed in locations and in areas that may help identify migrating contaminants from the identified
dump area on-site. The locations of the TMW locations can be viewed on the attached Sampling
Location Map, Figure 2, in appendix I.
SUMMIT utilized a CME Hollow Stem Auger drill rig to complete the soil borings and TMW
installation. At each location, a boring was advanced to 50 feet below ground surface (bgs) or
refusal. At termination depths, the TMWs were constructed within the HSA drill string. The TMWs
were constructed with solid riser and 20 feet of 2-inch Schedule 40 PVC 0.01-inch slotted well
screen encased in #3 filter sand from the base of the boring to approximately 2 feet above the well
screen. A 2 feet hydrated bentonite seal was pace on top of the well filter sand pack.
Each boring typically encountered tan/orange fine to medium grained sandy silts. Soil cuttings
generated during TMW installation were spread on-site.
TMW-1 was completed to at total depth of 48 ft bgs. TMW-2 was completed to a total depth of 40 ft
bgs. TMW-3 was completed to a total depth of 42.5 ft bgs.
Groundwater was encountered in TMW-1 and TMW-3. Depth to water (DTW) ranged from 47.5 ft
bgs to 42 ft bgs in the TMWs 24 hours after installation. Due to low groundwater yields, the TMWs
were not developed at the time of installation.
Upon completion of the drilling activities, the drilling equipment was decontaminated by the well
driller by use of a steam cleaner or Alconox and tap water wash, tap water rinse, isopropanol rinse
(sampling equipment), and deionized water rinse. Decontamination of the drilling equipment was
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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performed prior to starting drilling activities, and upon the completion of drilling activities at each
boring/well location.
4.2. SAMPLING
Groundwater was sampled from the installed TMWs on July 2, 2018, following a minimum 24 hour
equilibrium period after well installation. Groundwater was not encountered in TMW-2 at the time
of sampling.
Samples were collected utilizing new disposable bailers. Groundwater samples were containerized
in laboratory provided vials and containers, placed on ice and transported to the laboratory for
analysis. All groundwater samples were analyzed for Volatile Organic Compounds by EPA method
8260 and for RCRA Metals by EPA method 6010. Based on the turbid status of the groundwater
collected from TMW-2 and TMW-3, SUMMIT collected RCRA Metals in lab provided
unpreserved vials for the analysis of Dissolved RCRA Metals. Dissolved metal analysis utilizes
filtration to removed suspended sediment from a groundwater specimen in order to analyze only the
dissolved phase RCRA Metals. The dissolved metal analysis was chosen in order to prevent false
positives that may result from analysis of sediment laden samples.
4.3. PACKING AND SHIPMENT
Upon securing the samples in laboratory provided containers, the vial and jar lids were tightly
fastened, and the jars encapsulated in shock-resistant plastic bags. The samples and ice were double-
bagged in large plastic bags, tied off with rubber bands, and packed into a cooler. The samples were
delivered to Shealy Environmental Services, Inc, in West Columbia, SC. The vials and jars used for
the collection of the samples at this site were prepared by Shealy, and were pre-labeled and
contained analyte-appropriate preservatives. A listing of the preservatives in the sample containers
utilized for the collection of the samples at this site are cataloged in the Chain-Of-Custody record,
attached in Appendix III of this report. The secured samples were relinquished to laboratory on July
3, 2018 for laboratory analysis.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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4.4. SAMPLING POINT ABANDONMENT
All boreholes were abandoned following sampling activities.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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5.0 SUMMARY OF LABORATORY ANALYSIS
All samples were relinquished to Shealy Environmental Services on July 3, 2018 for the prescribe
analysis. Table 1.0 in Appendix II of this report summarizes all detections. The analytical detections
are summarized below:
• Acetone was detected in groundwater collected from TMW-1 at a concentration of 24 ug/L,
below the North Carolina Groundwater Standard of 6,000 ug/L.
No other detections were identified in the laboratory analysis.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
E:\Project Forms\Projects\4319.514 Thomas Road Site - Phase I ESA\Limited Phase II ESA\4319.514 Thomas Road Site - Phase II ESA.doc 10
6.0 FINDINGS & CONCLUSIONS
In summary, three (3) groundwater samples were attempted to be collected from the subject site to
identify if the observed former construction and land clearing debris landfill on-site impacted the
environmental quality of the groundwater at the subject site. TMW-2 did not yield groundwater for
sampling at the time of this assessment. All collected groundwater samples were analyzed for the
presence of VOCs and Total RCRA Metals (dissolved phase).
Acetone was the only detection in the collected groundwater samples. Acetone was detected well
below the North Carolina Groundwater standards (NC 2L) and is considered a laboratory artifact.
No other detections were reported.
Based on the results of this Limited Phase II ESA, SUMMIT concludes that the identified former
construction and land clearing debris landfill has not significantly impacted the subject site at the
time of this report. Therefore, SUMMIT recommends no further assessment.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
E:\Project Forms\Projects\4319.514 Thomas Road Site - Phase I ESA\Limited Phase II ESA\4319.514 Thomas Road Site - Phase II ESA.doc 11
7.0 QUALIFICATION OF REPORT
The Limited Phase II ESA was performed in general accordance with ASTM E1903, and in
accordance with the USEPA Field Branches Quality System and Technical Procedures Manual. The
findings detailed in this report are specific to the conditions in the immediate vicinity of the sample
locations for this particular project.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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8.0 ADDITIONAL SERVICES
This report does not include any environmental assessment of surface water, the determination of
wetlands, the determination of noise impact, the assessment of air quality, the identification of
cultural resources, or the identification of endangered species. These services are beyond the scope
of services of this limited sampling and analysis.
No additional services were provided.
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514 Charlotte, North Carolina July 16, 2018
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9.0 REFERENCES
United States Geological Survey (USGS) 7.5 minute Topographic Map of the Lake Wylie
Topographic Quadrangle, 2002.
EPA National Primary Drinking Water Regulations -
http://water.epa.gov/drink/contaminants/index.cfm
NC Groundwater Standards –
https://deq.nc.gov/about/divisions/water-resources/planning/classification-
standards/groundwater-standards
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514
Charlotte, North Carolina July 16, 2018
E:\Project Forms\Projects\4319.514 Thomas Road Site - Phase I ESA\Limited Phase II ESA\4319.514 Thomas Road Site - Phase II ESA.doc
APPENDIX I
FIGURES
Image Provided By EDR USGS Topographic Maps
Boundaries are approximate
TOPOGRAPHIC MAP
7/16/2018
Charlotte, North Carolina 28278
Thomas Road
Thomas Road Site
Source:Survey provided by Century Communities Prepared By\Date:PL/06/18
Checked By\Date:MZ/06/18
Scale
Figure 2Charlotte, NC 28226
Proposed Sampling Location Plan
Not to Scale
Century Communities
Charlotte, North Carolina
Thomas Road Site
14900 Thomas Road
7400 Carmel Executive Park Drive, Suite 205
TMW-2
TMW-3TMW-1
KEY
Temporary Monitoring Well Location
(TMW)
Approx. C&D Landfill Limits
N
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514
Charlotte, North Carolina July 16, 2018
E:\Project Forms\Projects\4319.514 Thomas Road Site - Phase I ESA\Limited Phase II ESA\PDF\Appendix II.rtf
APPENDIX II
ANALYTICAL SUMMARY
Page 1 of 1
Thomas Road Site
Charlotte, North Carolina
July 16, 2018
SUMMIT Project No: 4319.514
CAS VOC Analyte Result RL Result RL
67-64-1 Acetone 6.00E+03 24 20 Dry 20 BRL 20
CAS RCRA Metals PRG-Res
Protection
of GW Result RL Result RL
BRL = Below Reporting Limit J = Estimated Concentration RL = Lab Reporting Limit
BOLD = Concentration Above Reference Values NT = Not Tested
NC 2L
All Values in ug/L
Table 1.0: Sample Detection Summary Table
TMW-3
42.5' TD
No Sample
NCReference Values
TMW-1 TMW-2
40' TD
7/1/2018 7/1/2018 7/1/2018
48' TD
No other VOC detections
No detections
Limited Phase II ESA – Thomas Road Site SUMMIT Project No. 4319.514
Charlotte, North Carolina July 16, 2018
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APPENDIX III
ANALYTICAL RESULTS
SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.shealylab.com
Report of Analysis
SUMMIT Engineering,Laboratory &Testing,P.C.
3575 Centre Circle
Fort Mill,SC 28715
Attention:Patrick Lowery
Project Name:Thomas Road Site
Project Number:4319.514
Lot Number:TG04004
Date Completed:07/12/2018
07/13/2018 9:59 AM
Approved and released by:
Project Manager:Lucas Odom
Page 1 of 24
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.shealylab.com
Case Narrative
SUMMIT Engineering,Laboratory &Testing,P.C.
Lot Number:TG04004
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality
Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any
exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Page 2 of 24
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TG04004
Sample Number Sample ID Matrix Date Sampled Date Received
001 07/02/2018 1515TMW-1 Aqueous 07/04/2018
002 07/02/2018 1235TMW-3 Aqueous 07/04/2018
(2 samples)
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Shealy Environmental Services, Inc.
Page 3 of 24
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TG04004
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 TMW-1 Aqueous Acetone 8260B 24 ug/L 5
(1 detection)
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Page 4 of 24
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TMW-1
TG04004-001
07/02/2018 1515
07/04/2018
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/11/2018 1159 JJG 77381
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acetone 67-64-1 8260B 24 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L5.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L5.0
Bromoform 75-25-2 8260B ND 1ug/L5.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L5.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L5.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L5.0
Chlorobenzene 108-90-7 8260B ND 1ug/L5.0
Chloroethane 75-00-3 8260B ND 1ug/L5.0
Chloroform 67-66-3 8260B ND 1ug/L5.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L5.0
Cyclohexane 110-82-7 8260B ND 1ug/L5.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L5.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L5.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L5.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L5.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L5.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L5.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L5.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L5.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L5.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L5.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L5.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L5.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L5.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L5.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L5.0
Ethylbenzene 100-41-4 8260B ND 1ug/L5.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L5.0
Methyl acetate 79-20-9 8260B ND 1ug/L5.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L5.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L5.0
Styrene 100-42-5 8260B ND 1ug/L5.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L5.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L5.0
Toluene 108-88-3 8260B ND 1ug/L5.0
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Shealy Environmental Services, Inc.
Page 5 of 24
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TMW-1
TG04004-001
07/02/2018 1515
07/04/2018
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/11/2018 1159 JJG 77381
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L5.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L5.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L5.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L5.0
Trichloroethene 79-01-6 8260B ND 1ug/L5.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L5.0
Vinyl chloride 75-01-4 8260B ND 1ug/L2.0
Xylenes (total)1330-20-7 8260B ND 1ug/L5.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 86 70-130
Bromofluorobenzene 102 70-130
Toluene-d8 105 70-130
Dissolved RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 07/09/2018 1646 JCF 07/08/2018 1509 77063
1 3005A 6010D 1 07/11/2018 1955 CJZ 07/08/2018 1251 77056
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Dissolved Arsenic 7440-38-2 6010D ND 1mg/L0.015
Dissolved Barium 7440-39-3 6010D ND 1mg/L0.025
Dissolved Cadmium 7440-43-9 6010D ND 1mg/L0.0050
Dissolved Chromium 7440-47-3 6010D ND 1mg/L0.010
Dissolved Lead 7439-92-1 6010D ND 1mg/L0.010
Dissolved Mercury 7439-97-6 7470A ND 1mg/L0.00020
Dissolved Selenium 7782-49-2 6010D ND 1mg/L0.020
Dissolved Silver 7440-22-4 6010D ND 1mg/L0.010
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Shealy Environmental Services, Inc.
Page 6 of 24
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TMW-3
TG04004-002
07/02/2018 1235
07/04/2018
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/11/2018 1222 JJG 77381
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Acetone 67-64-1 8260B ND 1ug/L20
Benzene 71-43-2 8260B ND 1ug/L5.0
Bromodichloromethane 75-27-4 8260B ND 1ug/L5.0
Bromoform 75-25-2 8260B ND 1ug/L5.0
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/L5.0
2-Butanone (MEK)78-93-3 8260B ND 1ug/L10
Carbon disulfide 75-15-0 8260B ND 1ug/L5.0
Carbon tetrachloride 56-23-5 8260B ND 1ug/L5.0
Chlorobenzene 108-90-7 8260B ND 1ug/L5.0
Chloroethane 75-00-3 8260B ND 1ug/L5.0
Chloroform 67-66-3 8260B ND 1ug/L5.0
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/L5.0
Cyclohexane 110-82-7 8260B ND 1ug/L5.0
1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 1ug/L5.0
Dibromochloromethane 124-48-1 8260B ND 1ug/L5.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L5.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L5.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L5.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L5.0
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/L5.0
1,1-Dichloroethane 75-34-3 8260B ND 1ug/L5.0
1,2-Dichloroethane 107-06-2 8260B ND 1ug/L5.0
1,1-Dichloroethene 75-35-4 8260B ND 1ug/L5.0
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/L5.0
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/L5.0
1,2-Dichloropropane 78-87-5 8260B ND 1ug/L5.0
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/L5.0
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/L5.0
Ethylbenzene 100-41-4 8260B ND 1ug/L5.0
2-Hexanone 591-78-6 8260B ND 1ug/L10
Isopropylbenzene 98-82-8 8260B ND 1ug/L5.0
Methyl acetate 79-20-9 8260B ND 1ug/L5.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L5.0
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/L10
Methylcyclohexane 108-87-2 8260B ND 1ug/L5.0
Methylene chloride 75-09-2 8260B ND 1ug/L5.0
Styrene 100-42-5 8260B ND 1ug/L5.0
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/L5.0
Tetrachloroethene 127-18-4 8260B ND 1ug/L5.0
Toluene 108-88-3 8260B ND 1ug/L5.0
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Shealy Environmental Services, Inc.
Page 7 of 24
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
SUMMIT Engineering, Laboratory & Testing, P.C.
TMW-3
TG04004-002
07/02/2018 1235
07/04/2018
Aqueous
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 07/11/2018 1222 JJG 77381
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 1ug/L5.0
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/L5.0
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/L5.0
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/L5.0
Trichloroethene 79-01-6 8260B ND 1ug/L5.0
Trichlorofluoromethane 75-69-4 8260B ND 1ug/L5.0
Vinyl chloride 75-01-4 8260B ND 1ug/L2.0
Xylenes (total)1330-20-7 8260B ND 1ug/L5.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 78 70-130
Bromofluorobenzene 111 70-130
Toluene-d8 111 70-130
Dissolved RCRA Metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 7470A 7470A 1 07/09/2018 1657 JCF 07/08/2018 1509 77063
1 3005A 6010D 1 07/11/2018 2000 CJZ 07/08/2018 1251 77056
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run
Dissolved Arsenic 7440-38-2 6010D ND 1mg/L0.015
Dissolved Barium 7440-39-3 6010D ND 1mg/L0.025
Dissolved Cadmium 7440-43-9 6010D ND 1mg/L0.0050
Dissolved Chromium 7440-47-3 6010D ND 1mg/L0.010
Dissolved Lead 7439-92-1 6010D ND 1mg/L0.010
Dissolved Mercury 7439-97-6 7470A ND 1mg/L0.00020
Dissolved Selenium 7782-49-2 6010D ND 1mg/L0.020
Dissolved Silver 7440-22-4 6010D ND 1mg/L0.010
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the LOQ N = Recovery is out of criteria
H = Out of holding time W = Reported on wet weight basis
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Shealy Environmental Services, Inc.
Page 8 of 24
QC Summary
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Shealy Environmental Services, Inc.
Page 9 of 24
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ77381-001
77381 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Acetone ND 07/11/2018 091920ug/L1
Benzene ND 07/11/2018 09195.0 ug/L1
Bromodichloromethane ND 07/11/2018 09195.0 ug/L1
Bromoform ND 07/11/2018 09195.0 ug/L1
Bromomethane (Methyl bromide)ND 07/11/2018 09195.0 ug/L1
2-Butanone (MEK)ND 07/11/2018 091910ug/L1
Carbon disulfide ND 07/11/2018 09195.0 ug/L1
Carbon tetrachloride ND 07/11/2018 09195.0 ug/L1
Chlorobenzene ND 07/11/2018 09195.0 ug/L1
Chloroethane ND 07/11/2018 09195.0 ug/L1
Chloroform ND 07/11/2018 09195.0 ug/L1
Chloromethane (Methyl chloride)ND 07/11/2018 09195.0 ug/L1
Cyclohexane ND 07/11/2018 09195.0 ug/L1
1,2-Dibromo-3-chloropropane (DBCP)ND 07/11/2018 09195.0 ug/L1
Dibromochloromethane ND 07/11/2018 09195.0 ug/L1
1,2-Dibromoethane (EDB)ND 07/11/2018 09195.0 ug/L1
1,2-Dichlorobenzene ND 07/11/2018 09195.0 ug/L1
1,3-Dichlorobenzene ND 07/11/2018 09195.0 ug/L1
1,4-Dichlorobenzene ND 07/11/2018 09195.0 ug/L1
Dichlorodifluoromethane ND 07/11/2018 09195.0 ug/L1
1,1-Dichloroethane ND 07/11/2018 09195.0 ug/L1
1,2-Dichloroethane ND 07/11/2018 09195.0 ug/L1
1,1-Dichloroethene ND 07/11/2018 09195.0 ug/L1
cis-1,2-Dichloroethene ND 07/11/2018 09195.0 ug/L1
trans-1,2-Dichloroethene ND 07/11/2018 09195.0 ug/L1
1,2-Dichloropropane ND 07/11/2018 09195.0 ug/L1
cis-1,3-Dichloropropene ND 07/11/2018 09195.0 ug/L1
trans-1,3-Dichloropropene ND 07/11/2018 09195.0 ug/L1
Ethylbenzene ND 07/11/2018 09195.0 ug/L1
2-Hexanone ND 07/11/2018 091910ug/L1
Isopropylbenzene ND 07/11/2018 09195.0 ug/L1
Methyl acetate ND 07/11/2018 09195.0 ug/L1
Methyl tertiary butyl ether (MTBE)ND 07/11/2018 09195.0 ug/L1
4-Methyl-2-pentanone ND 07/11/2018 091910ug/L1
Methylcyclohexane ND 07/11/2018 09195.0 ug/L1
Methylene chloride ND 07/11/2018 09195.0 ug/L1
Styrene ND 07/11/2018 09195.0 ug/L1
1,1,2,2-Tetrachloroethane ND 07/11/2018 09195.0 ug/L1
Tetrachloroethene ND 07/11/2018 09195.0 ug/L1
Toluene ND 07/11/2018 09195.0 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 07/11/2018 09195.0 ug/L1
1,2,4-Trichlorobenzene ND 07/11/2018 09195.0 ug/L1
1,1,1-Trichloroethane ND 07/11/2018 09195.0 ug/L1
1,1,2-Trichloroethane ND 07/11/2018 09195.0 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.
Page 10 of 24
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ77381-001
77381 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Trichloroethene ND 07/11/2018 09195.0 ug/L1
Trichlorofluoromethane ND 07/11/2018 09195.0 ug/L1
Vinyl chloride ND 07/11/2018 09192.0 ug/L1
Xylenes (total)ND 07/11/2018 09195.0 ug/L1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 97 70-130
Bromofluorobenzene 106 70-130
Toluene-d8 108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.
Page 11 of 24
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ77381-002
77381 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acetone 120 07/11/2018 081112410060-1401
Benzene 50 07/11/2018 08111005070-1301
Bromodichloromethane 50 07/11/2018 08111005070-1301
Bromoform 53 07/11/2018 08111065070-1301
Bromomethane (Methyl bromide)46 07/11/2018 0811925070-1301
2-Butanone (MEK)110 07/11/2018 081111110070-1301
Carbon disulfide 51 07/11/2018 08111015070-1301
Carbon tetrachloride 47 07/11/2018 0811955070-1301
Chlorobenzene 49 07/11/2018 0811985070-1301
Chloroethane 43 07/11/2018 0811855070-1301
Chloroform 48 07/11/2018 0811965070-1301
Chloromethane (Methyl chloride)46 07/11/2018 0811935060-1401
Cyclohexane 42 07/11/2018 0811855070-1301
1,2-Dibromo-3-chloropropane (DBCP)54 07/11/2018 08111075070-1301
Dibromochloromethane 49 07/11/2018 0811995070-1301
1,2-Dibromoethane (EDB)53 07/11/2018 08111065070-1301
1,2-Dichlorobenzene 50 07/11/2018 08111005070-1301
1,3-Dichlorobenzene 50 07/11/2018 0811995070-1301
1,4-Dichlorobenzene 48 07/11/2018 0811975070-1301
Dichlorodifluoromethane 45 07/11/2018 0811895060-1401
1,1-Dichloroethane 51 07/11/2018 08111035070-1301
1,2-Dichloroethane 50 07/11/2018 08111005070-1301
1,1-Dichloroethene 55 07/11/2018 08111095070-1301
cis-1,2-Dichloroethene 54 07/11/2018 08111085070-1301
trans-1,2-Dichloroethene 54 07/11/2018 08111075070-1301
1,2-Dichloropropane 49 07/11/2018 0811985070-1301
cis-1,3-Dichloropropene 50 07/11/2018 08111015070-1301
trans-1,3-Dichloropropene 47 07/11/2018 0811945070-1301
Ethylbenzene 51 07/11/2018 08111025070-1301
2-Hexanone 96 07/11/2018 08119610070-1301
Isopropylbenzene 48 07/11/2018 0811965070-1301
Methyl acetate 52 07/11/2018 08111035070-1301
Methyl tertiary butyl ether (MTBE)53 07/11/2018 08111075070-1301
4-Methyl-2-pentanone 100 07/11/2018 081110110070-1301
Methylcyclohexane 46 07/11/2018 0811925070-1301
Methylene chloride 52 07/11/2018 08111035070-1301
Styrene 47 07/11/2018 0811955070-1301
1,1,2,2-Tetrachloroethane 50 07/11/2018 0811995070-1301
Tetrachloroethene 56 07/11/2018 08111125070-1301
Toluene 53 07/11/2018 08111065070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 48 07/11/2018 0811965070-1301
1,2,4-Trichlorobenzene 55 07/11/2018 08111115070-1301
1,1,1-Trichloroethane 53 07/11/2018 08111075070-1301
1,1,2-Trichloroethane 50 07/11/2018 08111015070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.
Page 12 of 24
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ77381-002
77381 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Trichloroethene 53 07/11/2018 08111065070-1301
Trichlorofluoromethane 45 07/11/2018 0811905070-1301
Vinyl chloride 45 07/11/2018 0811905070-1301
Xylenes (total)96 07/11/2018 08119610070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 94 70-130
Bromofluorobenzene 101 70-130
Toluene-d8 107 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.
Page 13 of 24
Dissolved RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ77056-001
77056 3005A
07/08/2018 1251Analytical Method:6010D
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Dissolved Arsenic ND 07/10/2018 12030.015 mg/L1
Dissolved Barium ND 07/10/2018 12030.025 mg/L1
Dissolved Cadmium ND 07/10/2018 12030.0050 mg/L1
Dissolved Chromium ND 07/10/2018 12030.010 mg/L1
Dissolved Lead ND 07/10/2018 12030.010 mg/L1
Dissolved Selenium ND 07/10/2018 12030.020 mg/L1
Dissolved Silver ND 07/10/2018 12030.010 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.
Page 14 of 24
Dissolved RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ77056-002
77056 3005A
07/08/2018 1251Analytical Method:6010D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Dissolved Arsenic 0.39 07/10/2018 1208980.40 80-1201
Dissolved Barium 1.8 07/10/2018 1208902.0 80-1201
Dissolved Cadmium 0.39 07/10/2018 1208970.40 80-1201
Dissolved Chromium 1.8 07/10/2018 1208922.0 80-1201
Dissolved Lead 0.39 07/10/2018 1208960.40 80-1201
Dissolved Selenium 0.40 07/10/2018 12081010.40 80-1201
Dissolved Silver 0.37 07/10/2018 1208930.40 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 15 of 24
Dissolved RCRA Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:TG04004-002MS
77056 3005A
07/08/2018 1251Analytical Method:6010D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Dissolved Arsenic 0.37 07/11/2018 2005920.40 75-125ND1
Dissolved Barium 1.9 07/11/2018 2005942.0 75-125ND1
Dissolved Cadmium 0.37 07/11/2018 2005920.40 75-125ND1
Dissolved Chromium 1.8 07/11/2018 2005892.0 75-125ND1
Dissolved Lead 0.37 07/11/2018 2005920.40 75-125ND1
Dissolved Selenium 0.38 07/11/2018 2005950.40 75-125ND1
Dissolved Silver 0.37 07/11/2018 2005910.40 75-125ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.
Page 16 of 24
Dissolved RCRA Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:TG04004-002MD
77056 3005A
07/08/2018 1251Analytical Method:6010D
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Dissolved Arsenic 0.38 07/11/2018 2010950.40 75-1252.5 20ND1
Dissolved Barium 1.9 07/11/2018 2010962.0 75-1252.9 20ND1
Dissolved Cadmium 0.38 07/11/2018 2010940.40 75-1252.5 20ND1
Dissolved Chromium 1.8 07/11/2018 2010912.0 75-1252.6 20ND1
Dissolved Lead 0.38 07/11/2018 2010950.40 75-1253.5 20ND1
Dissolved Selenium 0.39 07/11/2018 2010960.40 75-1251.6 20ND1
Dissolved Silver 0.38 07/11/2018 2010940.40 75-1252.9 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Shealy Environmental Services, Inc.
Page 17 of 24
Dissolved RCRA Metals - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ77063-001
77063 7470A
07/08/2018 1509Analytical Method:7470A
Matrix:Aqueous
Parameter Result Q LOQ Units Analysis DateDil
Dissolved Mercury ND 07/09/2018 16290.00020 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
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Page 18 of 24
Dissolved RCRA Metals - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ77063-002
77063 7470A
07/08/2018 1509Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Dissolved Mercury 0.0018 07/09/2018 1631920.0020 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Page 19 of 24
Dissolved RCRA Metals - MS
Batch:Prep Method:
Prep Date:
Sample ID:TG04004-001MS
77063 7470A
07/08/2018 1509Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Dissolved Mercury 0.0019 07/09/2018 1653960.0020 85-115ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Page 20 of 24
Dissolved RCRA Metals - MSD
Batch:Prep Method:
Prep Date:
Sample ID:TG04004-001MD
77063 7470A
07/08/2018 1509Analytical Method:7470A
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Dissolved Mercury 0.0018 07/09/2018 1655920.0020 85-1154.1 20ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the LOQ
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Page 21 of 24
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Page 22 of 24
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Page 23 of 24
SHEALY ENVIRONMENTAL SERVICES, INC.
106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com
Shealy Environmental Services, Inc.
Page 24 of 24