MO-9459_40900_CA_IAR_20190329_Initial Action Abatement Report

E&
ECS SOUTHEAST, L L P "Setting the Standard for Service"
Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm FA078
NC Registered Geologists Firm C-006
SC Registered Engineering Firm 3239
March 29, 2019
Mr. Jim Griffith
E.C. Griffith Company
1944 Brunswick Avenue
Charlotte, North Carolina 28207
Reference: Report of Soil Removal Activities
Morehead Ridge Apartments
1808 W. Morehead Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49-8751
Dear Mr. Griffith:
The project site is located at 1808 West Morehead Street in Charlotte, Mecklenburg County,
North Carolina. ECS previously conducted a Phase I Environmental Site Assessment dated
December 28, 2017 (ECS Project Numbers 49-5698). The results of the Phase I ESA identified
five offsite recognized environmental conditions and no evidence of an onsite UST was
observed during site reconnaissance.
During redevelopment activities at the subject property, the grading contractor encountered
petroleum hydrocarbon odors, stained soil, and ultimately uncovered an apparent heating oil
UST in the western/central portion of the site. The grading contractor removed the UST and
notified ECS of the odorous soil associated with the UST system.
Initial Sampling
On Monday January 21, 2019, ECS mobilized
collected two soil samples, for characterization
soil. The soil samples detected concentrations
range organics at concentrations above the
Quality (NCDEQ) division of waste managemi
soils.
to the above -referenced subject property and
purposes, from the apparent area of impacted
of total petroleum hydrocarbons (TPH) diesel
North Carolina Department of Environmental
,nt (DWM) guidelines for petroleum impacted
In an effort to remove the impacted soils from the subject property, ECS was requested by E.C.
Griffith Company to provide oversight and document the excavation activities.
Soil Removal & Post Excavation/Confirmation Sampling
On January 31, 2019, ECS personnel mobilized to observe and document the excavation and
soil removal activities at the subject property. ECS remobilized to the subject property February
1, 2019, February 4 through February 8, 2019, February 15, 2019, and March 5, 2019 to
observe and document the excavation and soil removal activities.
ECS field screened the soil as it was excavated using a photoionization detector (PID) as well
as documented visual and olfactory observations. Approximately 1,947 tons of soil was
excavated and transported to Alternative Energy Solutions (AES) facility in Thomasville, North
ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid-Atlantc, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP
www.ecslimited.com

Report of Soil Removal Activities
1808 West Morehead Street
Charlotte, North Carolina
ECS Project No. 49-8751
March 29, 2019
Carolina. The final area of excavation measured approximately 32 feet by 26 feet and 17 feet
deep.
Post -excavation soil samples were collected from the base and sidewalls of the excavation (S-1,
E-1, B-1, and N-1). The western side wall of the excavation was not sampled due to the
sidewall being a rock face. The soil in the base of the excavation appeared dry during the
excavation and sample activities. Additionally, previous geotechnical borings advanced to 50
feet below the ground surface (bgs) at the site did not indicate the presence of groundwater.
The soil samples were submitted to Prism Laboratories, a North Carolina Certified Laboratory,
for chemical analysis of volatile and semi -volatile organic compounds (VOCs/SVOCs) using
EPA Methods 8260 and 8270, respectively, and extractable and volatile petroleum
hydrocarbons (EPH/VPH) using the MADEP Method.
Based on the results of the initial post -excavation soil samples collected, exceedances of the
North Carolina Department of Environmental Quality (NCDEQ) Soil -to -Water Maximum
Contaminant Concentrations (MSCCs) were detected in soil samples N-1 (C-11-C22 Aromatics
& 1-Methyl naphthalene) and B-1 (1-Methyl naphthalene). Various other targeted compounds
were detected in the soil samples N-1, B-1, and E-1, but at concentrations below their
respective NCDEQ Soil -to -Water MSCCs. Exceedances of the NCDEQ Residential MSCCs
were not identified in the soil samples collected.
Due to the detections of targeted compounds above the NCDEQ Soil -to -Water MSCCs in the
soil samples collected from N-1 and B-1, ECS remobilized to the site to remove additional soil
from the base and north wall of the excavation. Approximately 41 tons of soil was removed and
two soil samples were collected, one from the north wall (NW), and one from the base (B). The
soil samples collected were submitted to Prism Laboratories for chemical analysis of
VOCs/SVOCs using EPA Methods 8260 and 8270, respectively, and EPH/VPH using the
MADEP Method.
Based on the results of the soil samples collected, exceedances of the NCDEQ Soil -to -Water
MSCCs (as well as the NCDEQ Residential MSCCs) were not identified in the soil samples (NW
and B) collected from the base and north wall of the excavation.
ECS did not observe water -supply or monitoring wells within 150 feet of the excavation limits.
The excavation is located within the western/central portion of the site with property boundaries
greater than 150 feet away. Wells associated with the site were not identified.
Conclusions & Recommendations
Based on the results of the post excavation samples collected, and the lack of receptors within
150 feet of the excavation, ECS understands that this incident may be eligible to receive
regulatory closure with no deed restrictions or further action required. ECS recommends that a
copy of this report be submitted to the NCDEQ Underground Storage Tank (UST) Section for
their review.
This report is provided for the exclusive use of E.C. Griffith Company. This report is not intended
to be used or relied upon in connection with other projects or by other third parties. ECS
disclaims liability for any such third party use or reliance without express written permission. If
you have any questions or comments concerning the contents of the enclosed documents or other
related topics, please contact us.

Report of Soil Removal Activities
1808 West Morehead Street
Charlotte, North Carolina
ECS Project No. 49-8751
March 29, 2019
Sincerely,
ECS SOUTHEAST, LLP
Christopher D. Orrell, P.G.
Staff Project Manager
[e-mail]
704-525-5152
Attachments:
Figures
Tables
Laboratory Analytical Data
Soil Disposal Manifests
w
OL O G1C,� a4a`,r
DAB
Matthew H. McDufFie, P.G.
Environmental Principal
mmcdufFie ecslimited.com
704-525-5152

s
79
A
It
SOURCE:
GOOGLE EARTH 2O18
SCALE:
AS SHOWN
,,- 74 �WL'14iN5 N-BLVD��
O
P.
27
49
lZb
LEGEND:
Approximate Site Boundary
FIGURE 1
"CIF SITE TOPOGRAPHIC MAP
s
MOREHEAD RIDGE APARTMENTS
1808 W MOREHEAD STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH
CAROLINA
ECS PROJECT NO. 49-8751
SA

M.'.t
Q]
600 ft

�wir.•W �' z4 ��1i4`4 :'.�{� �y�k: �a ',' :3"� � =�' "-`r'' 1rt'�� ', .;,-'JT�f `!•��'..
�4c • J r 1�. 1. j � i. _- " t� ,��.-. � r '��-'i ��• -tip:+: .,
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,J 4• ti-.. k' �1 L i;"�. � 4` y1t (�� rrr -_� J r. .'.+KlT R Y" F,
"''a Y�_ .fir /y� a-� ,; ., !". y..'r31� # -- • �•��.fi �! 'l i�i'i� ice` � F � L
-� - 4 +., ' • = v' - �'�yr _"• t-�'"
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;:-
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:azit e -
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��� 3 .�izr, '� ', �y,~ii� ti .�, i .='� ��+-i 1' - - {` i` i_+ _ . •r.- sµ .rt„-,+
it j `J a�f� e _ a a �'• ik "�i�ldd
:.T ` -,' '>: ; ''. y5,t1,•-y 1. ;„-..r _ey,
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irp
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•ti 1 + ^F _ROCK
-
.lam • �.'�r.� d
FACE
ek
SOURCE:
GOOGLE EARTH 2O18
SCALE:
AS SHOWN
TM
LEGEND:
® Approximate Sample Location
" FIGURE 3
"CIF SAMPLE LOCATION MAP
s
MOREHEAD RIDGE APARTMENTS
1808 W MOREHEAD STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH
CAROLINA
ECS PROJECT NO. 49-8751

TABLE 1: SUMMARY OF SOIL ANALYTICAL RESULTS
1808 WEST MOREHEAD STREET
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-87S1
Parameter
ANALYTICAL RESULTS
COMPARISION CRITERIA
Sample ID
S-1
E-1
B-1
N-1
B
NW
Soil -to -Water MSCC
(mg/kg)
Residential MSCC
(mg/kg)
Industrial MSCC
(mg/kg)
Collection Date
3/5/19
6/28/17
Sample Depth
15ft
15ft
17ft
15ft
18ft
15ft
Semivolatile Organic Compounds
1-Methyl naphthalene
BRL
BRL
0.20J
0.64
BRL
BRL
0.004
20
100
2-Methyl naphthalene
BRL
BRL
BRL
0.69
BRL
BRL
3.6
63
1,635
Benzoic Acid
BRL
BRL
BRL
BRL
0.22 J
BRL
120
62,571
1,635,200
Phenanthrene
BRL
BRL
0.17 J
0.30 J
BRL
BRL
56
469
12,264
Volatile Organic Compounds
4-Isopropyltoluene
BRL
BRL
BRL
0.0050 J
BRL
BRL
0.12
100
4,000
Naphthalene
BRL
0.0049 J
BRL
0.038
BRL
BRL
0.16
313
8,176
n-Butylbenzene
BRL
BRL
BRL
0.0057 J
BRL
BRL
4.3
626
16,350
sec-Butylbenzene
BRL
BRL
BRL
0.0055 J
BRL
BRL
3.3
626
16,350
Extractable and Volatile Petroleum Hydrocarbons
C9-C12 Aliphatics
BRL
BRL
4.9 J
8.6 J
BRL
540
1,500
40,000
C9-C18 Aliphatics
BRL
5.2 J
44
120
3.4 J
0.77 J
540
1,500
40,000
C19-06 Aliphatics
BRL
BRL
101
19 J
BRL
NS
31,000
810,000
C11-C22 Aromatics
BRL
2.0 J
26
60
BRL
31
469
12,264
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
MSCC = Maximum Soil Contaminant Concentration
BRL = Compound not detected at a concentration above the method reporting limit
Bold denotes an exceedance of the Soil -to -Water MSCC
Results compared to the North Carolina Department of Environmental Quality (NCDEQ) Underground Storage Tank (UST) MSCCs

Case Narrative
PRISM Full -Service Analytical &
Environmental Solutions
`,. LABORATORIES, INC.
ECS Carolinas, LLP (Charlotte)
Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
NC Certification No. 402
NC Drinking Water Cent No. 37735
SC Certification No. 99012
Project: W. Morehead
Lab Submittal Date: 03/06/2019
Prism Work Order: 9030103
03/12/2019
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a,j
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
Reviewed By Terri W. Cole For Angela D. Overcash
Project Manager
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
RLM Sample container suspected to have low methanol content. Results possibly biased high.
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 37

/P R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES INC.
Sample Receipt Summary
03/12/2019
Prism Work Order: 9030103
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
S-1
9030103-01
Solid
03/05/19
9:30
03/06/19
16:00
E-1
9030103-02
Solid
03/05/19
9:40
03/06/19
16:00
B-1
9030103-03
Solid
03/05/19
9:50
03/06/19
16:00
N-1
9030103-04
Solid
03/05/19
9:55
03/06/19
16:00
Samples were received in good condition at 2.5 degrees C unless otherwise noted
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 37

P R I S M Full Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Summary of Detections
03/12/2019
Prism Work Order: 9030103
Prism ID
Client ID
Parameter
Method
Result
Units
9030103-02
E-1
C9-Cl8 Aliphatics
MADEP EPH
5.2
J
mg/kg dry
9030103-02
E-1
C11-C22 Aromatics
MADEP EPH
2.0
1
mg/kg dry
9030103-02
E-1
Naphthalene
8260B
0.0049
1
mg/kg dry
9030103-03
B-1
C9-C18 Aliphatics
MADEP EPH
44
mg/kg dry
9030103-03
B-1
C19-C36 Aliphatics
MADEP EPH
10
1
mg/kg dry
9030103-03
B-1
C11-C22 Aromatics
MADEP EPH
26
mg/kg dry
9030103-03
B-1
1-Methylnaphthalene
8270D
0.20
1
mg/kg dry
9030103-03
B-1
Phenanthrene
8270D
0.17
1
mg/kg dry
9030103-03
B-1
C9-C12 Aliphatics
MADEP VPH
4.9
1
mg/kg dry
9030103-04
N-1
C9-Cl8 Aliphatics
MADEP EPH
120
mg/kg dry
9030103-04
N-1
C19-C36 Aliphatics
MADEP EPH
19
J
mg/kg dry
9030103-04
N-1
C11-C22 Aromatics
MADEP EPH
60
mg/kg dry
9030103-04
N-1
1-Methylnaphthalene
8270D
0.64
mg/kg dry
9030103-04
N-1
2-Methylnaphthalene
8270D
0.69
mg/kg dry
9030103-04
N-1
Phenanthrene
8270D
0.30
J
mg/kg dry
9030103-04
N-1
4-Isopropyltoluene
8260E
0.0050
1
mg/kg dry
9030103-04
N-1
Naphthalene
8260B
0.038
mg/kg dry
9030103-04
N-1
n-Butylbenzene
8260B
0.0057
.1
mg/kg dry
9030103-04
N-1
sec -Butyl benzene
8260E
0.0055
1
mg/kg dry
9030103-04
N-1
C9-C12 Aliphatics
MADEP VPH
8.6
1
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 37

P R S M Laboratory Report
` Full -Service Analytical &
/ environmental Solutions 03/12/2019
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Client Sample ID: S-1
Attn: Chris Orrell Prism Sample ID: 9030103-01
1812 Center Park Drive, Suite D Prism Work Order: 9030103
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 03/05/19 09:30
Time Submitted: 03/06/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-Cl8 Aliphatics BRL
mg/kg dry
27 0.17 1
MADEP EPH 3/11/19 18:20
BGB P9C0135
C19-C36 Aliphatics BRL
mg/kg dry
27 3.2 1
MADEP EPH 3/11/19 18:20
BGB P9C0135
C11-C22 Aromatics BRL
mg/kg dry
11 1.9 1
MADEP EPH 3/11/19 18:20
BGB P9C0135
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
81 %
40-140
o-Terphenyl
91 %
40-140
2-Fluorobiphenyl
103 %
40-140
2-Bromonaphthalene
91 %
40-140
General Chemistry Parameters
% Solids 93.4
Semivolatile Organic Compounds by GC/MS
% by
Weight
0.100
0.100
1
SM2540 G
3/12/19 9:31
KBS
P9C0167
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.35
0.055
1
8270D
3/11/19 12:17
JMV
P9C0132
1,2-Dichlorobenzene
BRL
mg/kg dry
0.35
0.054
1
8270D
3/11/19 12:17
JMV
P9C0132
1,3-Dichlorobenzene
BRL
mg/kg dry
0.35
0.050
1
8270D
3/11/19 12:17
JMV
P9C0132
1,4-Dichlorobenzene
BRL
mg/kg dry
0.35
0.052
1
8270D
3/11/19 12:17
JMV
P9C0132
1-Methyl naphthalene
BRL
mg/kg dry
0.35
0.068
1
8270D
3/11/19 12:17
JMV
P9C0132
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.35
0.057
1
8270D
3/11/19 12:17
JMV
P9C0132
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.35
0.066
1
8270D
3/11/19 12:17
JMV
P9C0132
2,4-Dichlorophenol
BRL
mg/kg dry
0.35
0.068
1
8270D
3/11/19 12:17
JMV
P9C0132
2,4-Dimethylphenol
BRL
mg/kg dry
0.35
0.054
1
8270D
3/11/19 12:17
JMV
P9C0132
2,4-Dinitrophenol
BRL
mg/kg dry
0.35
0.049
1
8270D
3/11/19 12:17
JMV
P9C0132
2,4-Dinitrotoluene
BRL
mg/kg dry
0.35
0.043
1
8270D
3/11/19 12:17
JMV
P9C0132
2,6-Dinitrotoluene
BRL
mg/kg dry
0.35
0.047
1
8270D
3/11/19 12:17
JMV
P9C0132
2-Chloronaphthalene
BRL
mg/kg dry
0.35
0.051
1
8270D
3/11/19 12:17
JMV
P9C0132
2-Chlorophenol
BRL
mg/kg dry
0.35
0.050
1
8270D
3/11/19 12:17
JMV
P9C0132
2-Methyl naphthalene
BRL
mg/kg dry
0.35
0.056
1
8270D
3/11/19 12:17
JMV
P9C0132
2-Methylphenol
BRL
mg/kg dry
0.35
0.045
1
8270D
3/11/19 12:17
JMV
P9C0132
2-Nitrophenol
BRL
mg/kg dry
0.35
0.064
1
8270D
3/11/19 12:17
JMV
P9C0132
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.35
0.070
1
8270D
3/11/19 12:17
JMV
P9C0132
3/4-Methyl phenol
BRL
mg/kg dry
0.35
0.044
1
8270D
3/11/19 12:17
JMV
P9C0132
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.35
0.053
1
8270D
3/11/19 12:17
JMV
P9C0132
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.35
0.061
1
8270D
3/11/19 12:17
JMV
P9C0132
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.35
0.049
1
8270D
3/11/19 12:17
JMV
P9C0132
4-Chloroaniline
BRL
mg/kg dry
0.35
0.042
1
8270D
3/11/19 12:17
JMV
P9C0132
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.35
0.046
1
8270D
3/11/19 12:17
JMV
P9C0132
4-Nitrophenol
BRL
mg/kg dry
0.35
0.054
1
8270D
3/11/19 12:17
JMV
P9C0132
Acenaphthene
BRL
mg/kg dry
0.35
0.048
1
8270D
3/11/19 12:17
JMV
P9C0132
Acenaphthylene
BRL
mg/kg dry
0.35
0.051
1
8270D
3/11/19 12:17
JMV
P9C0132
Anthracene
BRL
mg/kg dry
0.35
0.057
1
8270D
3/11/19 12:17
JMV
P9C0132
Azobenzene
BRL
mg/kg dry
0.35
0.047
1
8270D
3/11/19 12:17
JMV
P9C0132
Benzo(a)anthracene
BRL
mg/kg dry
0.35
0.046
1
8270D
3/11/19 12:17
JMV
P9C0132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 37

Laboratory Report
` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
03/12/2019
ECS Carolinas, LLP (Charlotte)
Project: W. Morehead
Client Sample ID: S-1
Attn: Chris Orrell
Prism Sample ID: 9030103-01
1812 Center Park Drive, Suite D
Prism Work Order: 9030103
Charlotte, NC 28217
Sample Matrix: Solid
Time Collected:
03/05/19 09:30
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.35
0.038
1
8270D
3/11/19 12:17
JMV
P9C0132
Benzo(b)fluoranthene
BRL
mg/kg dry
0.35
0.041
1
8270D
3/11/19 12:17
JMV
P9C0132
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.35
0.039
1
8270D
3/11/19 12:17
JMV
P9C0132
Benzo(k)fluoranthene
BRL
mg/kg dry
0.35
0.046
1
8270D
3/11/19 12:17
JMV
P9C0132
Benzoic Acid
BRL
mg/kg dry
0.35
0.030
1
8270D
3/11/19 12:17
JMV
P9C0132
Benzyl alcohol
BRL
mg/kg dry
0.35
0.046
1
8270D
3/11/19 12:17
JMV
P9C0132
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.35
0.061
1
8270D
3/11/19 12:17
JMV
P9C0132
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.35
0.050
1
8270D
3/11/19 12:17
JMV
P9C0132
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.35
0.060
1
8270D
3/11/19 12:17
JMV
P9C0132
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.35
0.052
1
8270D
3/11/19 12:17
JMV
P9C0132
Butyl benzyl phthalate
BRL
mg/kg dry
0.35
0.050
1
8270D
3/11/19 12:17
JMV
P9C0132
Chrysene
BRL
mg/kg dry
0.35
0.044
1
8270D
3/11/19 12:17
JMV
P9C0132
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.35
0.043
1
8270D
3/11/19 12:17
JMV
P9C0132
Dibenzofuran
BRL
mg/kg dry
0.35
0.054
1
8270D
3/11/19 12:17
JMV
P9C0132
Diethyl phthalate
BRL
mg/kg dry
0.35
0.049
1
8270D
3/11/19 12:17
JMV
P9C0132
Dimethyl phthalate
BRL
mg/kg dry
0.35
0.047
1
8270D
3/11/19 12:17
JMV
P9C0132
Di-n-butyl phthalate
BRL
mg/kg dry
0.35
0.050
1
8270D
3/11/19 12:17
JMV
P9C0132
Di-n-octyl phthalate
BRL
mg/kg dry
0.35
0.043
1
8270D
3/11/19 12:17
JMV
P9C0132
Fluoranthene
BRL
mg/kg dry
0.35
0.045
1
8270D
3/11/19 12:17
JMV
P9C0132
Fluorene
BRL
mg/kg dry
0.35
0.051
1
8270D
3/11/19 12:17
JMV
P9C0132
Hexachlorobenzene
BRL
mg/kg dry
0.35
0.056
1
8270D
3/11/19 12:17
JMV
P9C0132
Hexachlorobutadiene
BRL
mg/kg dry
0.35
0.063
1
8270D
3/11/19 12:17
JMV
P9C0132
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.35
0.063
1
8270D
3/11/19 12:17
JMV
P9C0132
Hexachloroethane
BRL
mg/kg dry
0.35
0.059
1
8270D
3/11/19 12:17
JMV
P9C0132
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.35
0.041
1
8270D
3/11/19 12:17
JMV
P9C0132
Isophorone
BRL
mg/kg dry
0.35
0.048
1
8270D
3/11/19 12:17
JMV
P9C0132
Naphthalene
BRL
mg/kg dry
0.35
0.057
1
8270D
3/11/19 12:17
JMV
P9C0132
Nitrobenzene
BRL
mg/kg dry
0.35
0.050
1
8270D
3/11/19 12:17
JMV
P9C0132
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.35
0.056
1
8270D
3/11/19 12:17
JMV
P9C0132
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.35
0.054
1
8270D
3/11/19 12:17
JMV
P9C0132
Pentachlorophenol
BRL
mg/kg dry
0.35
0.042
1
8270D
3/11/19 12:17
JMV
P9C0132
Phenanthrene
BRL
mg/kg dry
0.35
0.046
1
8270D
3/11/19 12:17
JMV
P9C0132
Phenol
BRL
mg/kg dry
0.35
0.052
1
8270D
3/11/19 12:17
JMV
P9C0132
Pyrene
BRL
mg/kg dry
0.35
0.047
1
8270D
3/11/19 12:17
JMV
P9C0132
Pyridine
BRL
mg/kg dry
0.35
0.062
1
8270D
3/11/19 12:17
JMV
P9C0132
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
112 %
39-132
2-Fluorobiphenyl
110 %
44-115
2-Fluorophenol
112 %
35-115
Nitrobenzene-d5
103 %
37-122
Phenol-d5
107 %
34-121
Terphenyl-d14
111 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 37

` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead
Sample Matrix: Solid
Laboratory Report
03/12/2019
Client Sample ID: S-1
Prism Sample ID: 9030103-01
Prism Work Order: 9030103
Time Collected: 03/05/19 09:30
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0032
0.00027
1
8260B
3/7/19 16:10
JLB
P9C0139
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0032
0.00016
1
8260B
3/7/19 16:10
JLB
P9C0139
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0032
0.00022
1
8260B
3/7/19 16:10
JLB
P9C0139
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0032
0.00029
1
8260B
3/7/19 16:10
JLB
P9C0139
1,1-Dichloroethane
BRL
mg/kg dry
0.0032
0.000090
1
8260B
3/7/19 16:10
JLB
P9C0139
1,1-Dichloroethylene
BRL
mg/kg dry
0.0032
0.00014
1
8260B
3/7/19 16:10
JLB
P9C0139
1,1-Dichloropropylene
BRL
mg/kg dry
0.0032
0.00018
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0032
0.00018
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0032
0.00041
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0032
0.00024
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0032
0.00025
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2-Dibromoethane
BRL
mg/kg dry
0.0032
0.00013
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0032
0.00015
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2-Dichloroethane
BRL
mg/kg dry
0.0032
0.00019
1
8260B
3/7/19 16:10
JLB
P9C0139
1,2-Dichloropropane
BRL
mg/kg dry
0.0032
0.00020
1
8260B
3/7/19 16:10
JLB
P9C0139
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0032
0.00024
1
8260B
3/7/19 16:10
JLB
P9C0139
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0032
0.00021
1
8260B
3/7/19 16:10
JLB
P9C0139
1,3-Dichloropropane
BRL
mg/kg dry
0.0032
0.00016
1
8260B
3/7/19 16:10
JLB
P9C0139
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0032
0.00013
1
8260B
3/7/19 16:10
JLB
P9C0139
2,2-Dichloropropane
BRL
mg/kg dry
0.0032
0.00015
1
8260B
3/7/19 16:10
JLB
P9C0139
2-Chlorotoluene
BRL
mg/kg dry
0.0032
0.00017
1
8260B
3/7/19 16:10
JLB
P9C0139
4-Chlorotoluene
BRL
mg/kg dry
0.0032
0.00019
1
8260B
3/7/19 16:10
JLB
P9C0139
4-Isopropyltoluene
BRL
mg/kg dry
0.0032
0.00016
1
8260B
3/7/19 16:10
JLB
P9C0139
Acetone
BRL
mg/kg dry
0.032
0.00079
1
8260B
3/7/19 16:10
JLB
P9C0139
Benzene
BRL
mg/kg dry
0.0019
0.00019
1
8260B
3/7/19 16:10
JLB
P9C0139
Bromobenzene
BRL
mg/kg dry
0.0032
0.00027
1
8260B
3/7/19 16:10
JLB
P9C0139
Bromochloromethane
BRL
mg/kg dry
0.0032
0.00018
1
8260B
3/7/19 16:10
JLB
P9C0139
Bromodichloromethane
BRL
mg/kg dry
0.0032
0.00018
1
8260B
3/7/19 16:10
JLB
P9C0139
Bromoform
BRL
mg/kg dry
0.0032
0.00037
1
8260B
3/7/19 16:10
JLB
P9C0139
Bromomethane
BRL
mg/kg dry
0.0065
0.00040
1
8260B
3/7/19 16:10
JLB
P9C0139
Carbon Tetrachloride
BRL
mg/kg dry
0.0032
0.00016
1
8260B
3/7/19 16:10
JLB
P9C0139
Chlorobenzene
BRL
mg/kg dry
0.0032
0.00017
1
8260B
3/7/19 16:10
JLB
P9C0139
Chloroethane
BRL
mg/kg dry
0.0065
0.00027
1
8260B
3/7/19 16:10
JLB
P9C0139
Chloroform
BRL
mg/kg dry
0.0032
0.00023
1
8260B
3/7/19 16:10
JLB
P9C0139
Chloromethane
BRL
mg/kg dry
0.0032
0.00022
1
8260B
3/7/19 16:10
JLB
P9C0139
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0032
0.00014
1
8260B
3/7/19 16:10
JLB
P9C0139
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0032
0.00011
1
8260B
3/7/19 16:10
JLB
P9C0139
Dibromochloromethane
BRL
mg/kg dry
0.0032
0.00013
1
8260B
3/7/19 16:10
JLB
P9C0139
Dichlorodifluoromethane
BRL
mg/kg dry
0.0032
0.00015
1
8260B
3/7/19 16:10
JLB
P9C0139
Ethylbenzene
BRL
mg/kg dry
0.0032
0.00012
1
8260B
3/7/19 16:10
JLB
P9C0139
Isopropyl Ether
BRL
mg/kg dry
0.0032
0.00013
1
8260B
3/7/19 16:10
JLB
P9C0139
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0032
0.00019
1
8260B
3/7/19 16:10
JLB
P9C0139
m,p-Xylenes
BRL
mg/kg dry
0.0065
0.00030
1
8260B
3/7/19 16:10
JLB
P9C0139
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 37

Laboratory Report
` Full -Service
Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
03/12/2019
ECS Carolinas, LLP (Charlotte)
Project: W. Morehead
Client
Sample ID: S-1
Attn: Chris Orrell
Prism
Sample ID: 9030103-01
1812 Center Park Drive, Suite D
Prism
Work Order: 9030103
Charlotte, NC 28217
Sample Matrix: Solid
Time
Collected: 03/05/19 09:30
Time
Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.032
0.00029
1
8260B 3/7/19 16:10
JLB
P9C0139
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.065
0.00029
1
8260B 3/7/19 16:10
JLB
P9C0139
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.032
0.00028
1
8260B 3/7/19 16:10
JLB
P9C0139
Methylene Chloride
BRL
mg/kg dry
0.0065
0.00018
1
8260B 3/7/19 16:10
JLB
P9C0139
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0065
0.00010
1
8260B 3/7/19 16:10
JLB
P9C0139
Naphthalene
BRL
mg/kg dry
0.0065
0.00010
1
8260B 3/7/19 16:10
JLB
P9C0139
n-Butylbenzene
BRL
mg/kg dry
0.0032
0.00016
1
8260B 3/7/19 16:10
JLB
P9C0139
n-Propylbenzene
BRL
mg/kg dry
0.0032
0.00019
1
8260B 3/7/19 16:10
JLB
P9C0139
o-Xylene
BRL
mg/kg dry
0.0032
0.00013
1
8260B 3/7/19 16:10
JLB
P9C0139
sec-Butylbenzene
BRL
mg/kg dry
0.0032
0.00016
1
8260B 3/7/19 16:10
JLB
P9C0139
Styrene
BRL
mg/kg dry
0.0032
0.00019
1
8260B 3/7/19 16:10
JLB
P9C0139
tert-Butylbenzene
BRL
mg/kg dry
0.0032
0.00011
1
8260B 3/7/19 16:10
JLB
P9C0139
Tetrachloroethylene
BRL
mg/kg dry
0.0032
0.00015
1
8260B 3/7/19 16:10
JLB
P9C0139
Toluene
BRL
mg/kg dry
0.0032
0.00019
1
8260B 3/7/19 16:10
JLB
P9C0139
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0032
0.00019
1
8260B 3/7/19 16:10
JLB
P9C0139
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0032
0.00017
1
8260B 3/7/19 16:10
JLB
P9C0139
Trichloroethylene
BRL
mg/kg dry
0.0032
0.00021
1
8260B 3/7/19 16:10
JLB
P9C0139
Trichlorofluoromethane
BRL
mg/kg dry
0.0032
0.00021
1
8260B 3/7/19 16:10
JLB
P9C0139
Vinyl acetate
BRL
mg/kg dry
0.016
0.00044
1
8260B 3/7/19 16:10
JLB
P9C0139
Vinyl chloride
BRL
mg/kg dry
0.0032
0.00016
1
8260B 3/7/19 16:10
JLB
P9C0139
Xylenes, total
BRL
mg/kg dry
0.0097
0.00061
1
8260B 3/7/19 16:10
JLB
P9C0139
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
101 %
70-130
Dibromofluoromethane
103 %
84-123
Toluene-d8
90 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
20
0.65
100
MADEP VPH 3/11/19 11:53
TBL
P9C0146
C9-Cl2 Aliphatics
BRL
mg/kg dry
20
1.1
100
MADEP VPH 3/11/19 11:53
TBL
P9C0146
C9-Cl0 Aromatics
BRL
mg/kg dry
20
0.23
100
MADEP VPH 3/11/19 11:53
TBL
P9C0146
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
104 %
70-130
2,5-Dibromotoluene (FID)
111 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 37

P R S M Laboratory Report
` Full -Service Analytical &
/ environmental Solutions 03/12/2019
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Client Sample ID: E-1
Attn: Chris Orrell Prism Sample ID: 9030103-02
1812 Center Park Drive, Suite D Prism Work Order: 9030103
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 03/05/19 09:40
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
5.2 J
mg/kg dry
28 0.18
1
MADEP EPH 3/11/19 18:56
BGB
P9C0135
C19-C36 Aliphatics
BRL
mg/kg dry
28 3.3
1
MADEP EPH 3/11/19 18:56
BGB
P9C0135
C11-C22 Aromatics
2.0 J
mg/kg dry
11 2.0
1
MADEP EPH 3/11/19 18:56
BGB
P9C0135
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
87 %
40-140
o-Terphenyl
97 %
40-140
2-Fluorobiphenyl
93 %
40-140
2-Bromonaphthalene
77 %
40-140
General Chemistry Parameters
Solids
89.0
% by
0.100
0.100
1
SM2540 G
3/12/19 9:31
KBS
P9C0167
Weight
Semivolatile Organic Compounds by GUMS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.37
0.058
1
8270D
3/11/19 12:39
JMV
P9C0132
1,2-Dichlorobenzene
BRL
mg/kg dry
0.37
0.056
1
8270D
3/11/19 12:39
JMV
P9C0132
1,3-Dichlorobenzene
BRL
mg/kg dry
0.37
0.052
1
8270D
3/11/19 12:39
JMV
P9C0132
1,4-Dichlorobenzene
BRL
mg/kg dry
0.37
0.054
1
8270D
3/11/19 12:39
JMV
P9C0132
1-Methyl naphthalene
BRL
mg/kg dry
0.37
0.071
1
8270D
3/11/19 12:39
JMV
P9C0132
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.37
0.060
1
8270D
3/11/19 12:39
JMV
P9C0132
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.37
0.069
1
8270D
3/11/19 12:39
JMV
P9C0132
2,4-Dichlorophenol
BRL
mg/kg dry
0.37
0.071
1
8270D
3/11/19 12:39
JMV
P9C0132
2,4-Dimethylphenol
BRL
mg/kg dry
0.37
0.057
1
8270D
3/11/19 12:39
JMV
P9C0132
2,4-Dinitrophenol
BRL
mg/kg dry
0.37
0.052
1
8270D
3/11/19 12:39
JMV
P9C0132
2,4-Dinitrotoluene
BRL
mg/kg dry
0.37
0.045
1
8270D
3/11/19 12:39
JMV
P9C0132
2,6-Dinitrotoluene
BRL
mg/kg dry
0.37
0.049
1
8270D
3/11/19 12:39
JMV
P9C0132
2-Chloronaphthalene
BRL
mg/kg dry
0.37
0.053
1
8270D
3/11/19 12:39
JMV
P9C0132
2-Chlorophenol
BRL
mg/kg dry
0.37
0.052
1
8270D
3/11/19 12:39
JMV
P9C0132
2-Methyl naphthalene
BRL
mg/kg dry
0.37
0.059
1
8270D
3/11/19 12:39
JMV
P9C0132
2-Methylphenol
BRL
mg/kg dry
0.37
0.047
1
8270D
3/11/19 12:39
JMV
P9C0132
2-Nitrophenol
BRL
mg/kg dry
0.37
0.067
1
8270D
3/11/19 12:39
JMV
P9C0132
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.37
0.073
1
8270D
3/11/19 12:39
JMV
P9C0132
3/4-Methyl phenol
BRL
mg/kg dry
0.37
0.045
1
8270D
3/11/19 12:39
JMV
P9C0132
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.37
0.055
1
8270D
3/11/19 12:39
JMV
P9C0132
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.37
0.063
1
8270D
3/11/19 12:39
JMV
P9C0132
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.37
0.052
1
8270D
3/11/19 12:39
JMV
P9C0132
4-Chloroaniline
BRL
mg/kg dry
0.37
0.044
1
8270D
3/11/19 12:39
JMV
P9C0132
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.37
0.048
1
8270D
3/11/19 12:39
JMV
P9C0132
4-Nitrophenol
BRL
mg/kg dry
0.37
0.057
1
8270D
3/11/19 12:39
JMV
P9C0132
Acenaphthene
BRL
mg/kg dry
0.37
0.050
1
8270D
3/11/19 12:39
JMV
P9C0132
Acenaphthylene
BRL
mg/kg dry
0.37
0.053
1
8270D
3/11/19 12:39
JMV
P9C0132
Anthracene
BRL
mg/kg dry
0.37
0.059
1
8270D
3/11/19 12:39
JMV
P9C0132
Azobenzene
BRL
mg/kg dry
0.37
0.049
1
8270D
3/11/19 12:39
JMV
P9C0132
Benzo(a)anthracene
BRL
mg/kg dry
0.37
0.048
1
8270D
3/11/19 12:39
JMV
P9C0132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 37

Laboratory Report
` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
03/12/2019
ECS Carolinas, LLP (Charlotte)
Project: W. Morehead
Client Sample ID: E-1
Attn: Chris Orrell
Prism Sample ID: 9030103-02
1812 Center Park Drive, Suite D
Prism Work Order:
9030103
Charlotte, NC 28217
Sample Matrix: Solid
Time Collected:
03/05/19 09:40
Time Submitted:
03/06/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.37
0.040
1
8270D
3/11/19 12:39
JMV
P9C0132
Benzo(b)fluoranthene
BRL
mg/kg dry
0.37
0.043
1
8270D
3/11/19 12:39
JMV
P9C0132
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.37
0.040
1
8270D
3/11/19 12:39
JMV
P9C0132
Benzo(k)fluoranthene
BRL
mg/kg dry
0.37
0.048
1
8270D
3/11/19 12:39
JMV
P9C0132
Benzoic Acid
BRL
mg/kg dry
0.37
0.031
1
8270D
3/11/19 12:39
JMV
P9C0132
Benzyl alcohol
BRL
mg/kg dry
0.37
0.049
1
8270D
3/11/19 12:39
JMV
P9C0132
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.37
0.064
1
8270D
3/11/19 12:39
JMV
P9C0132
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.37
0.052
1
8270D
3/11/19 12:39
JMV
P9C0132
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.37
0.063
1
8270D
3/11/19 12:39
JMV
P9C0132
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.37
0.055
1
8270D
3/11/19 12:39
JMV
P9C0132
Butyl benzyl phthalate
BRL
mg/kg dry
0.37
0.053
1
8270D
3/11/19 12:39
JMV
P9C0132
Chrysene
BRL
mg/kg dry
0.37
0.046
1
8270D
3/11/19 12:39
JMV
P9C0132
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.37
0.045
1
8270D
3/11/19 12:39
JMV
P9C0132
Dibenzofuran
BRL
mg/kg dry
0.37
0.056
1
8270D
3/11/19 12:39
JMV
P9C0132
Diethyl phthalate
BRL
mg/kg dry
0.37
0.051
1
8270D
3/11/19 12:39
JMV
P9C0132
Dimethyl phthalate
BRL
mg/kg dry
0.37
0.049
1
8270D
3/11/19 12:39
JMV
P9C0132
Di-n-butyl phthalate
BRL
mg/kg dry
0.37
0.052
1
8270D
3/11/19 12:39
JMV
P9C0132
Di-n-octyl phthalate
BRL
mg/kg dry
0.37
0.045
1
8270D
3/11/19 12:39
JMV
P9C0132
Fluoranthene
BRL
mg/kg dry
0.37
0.047
1
8270D
3/11/19 12:39
JMV
P9C0132
Fluorene
BRL
mg/kg dry
0.37
0.053
1
8270D
3/11/19 12:39
JMV
P9C0132
Hexachlorobenzene
BRL
mg/kg dry
0.37
0.059
1
8270D
3/11/19 12:39
JMV
P9C0132
Hexachlorobutadiene
BRL
mg/kg dry
0.37
0.066
1
8270D
3/11/19 12:39
JMV
P9C0132
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.37
0.066
1
8270D
3/11/19 12:39
JMV
P9C0132
Hexachloroethane
BRL
mg/kg dry
0.37
0.062
1
8270D
3/11/19 12:39
JMV
P9C0132
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.37
0.042
1
8270D
3/11/19 12:39
JMV
P9C0132
Isophorone
BRL
mg/kg dry
0.37
0.050
1
8270D
3/11/19 12:39
JMV
P9C0132
Naphthalene
BRL
mg/kg dry
0.37
0.059
1
8270D
3/11/19 12:39
JMV
P9C0132
Nitrobenzene
BRL
mg/kg dry
0.37
0.052
1
8270D
3/11/19 12:39
JMV
P9C0132
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.37
0.058
1
8270D
3/11/19 12:39
JMV
P9C0132
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.37
0.056
1
8270D
3/11/19 12:39
JMV
P9C0132
Pentachlorophenol
BRL
mg/kg dry
0.37
0.044
1
8270D
3/11/19 12:39
JMV
P9C0132
Phenanthrene
BRL
mg/kg dry
0.37
0.048
1
8270D
3/11/19 12:39
JMV
P9C0132
Phenol
BRL
mg/kg dry
0.37
0.054
1
8270D
3/11/19 12:39
JMV
P9C0132
Pyrene
BRL
mg/kg dry
0.37
0.049
1
8270D
3/11/19 12:39
JMV
P9C0132
Pyridine
BRL
mg/kg dry
0.37
0.064
1
8270D
3/11/19 12:39
JMV
P9C0132
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
90 %
39-132
2-Fluorobiphenyl
88 %
44-115
2-Fluorophenol
83 %
35-115
Nitrobenzene-d5
77 %
37-122
Phenol-d5
82 %
34-121
Terphenyl-d14
93 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 37

` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead
Sample Matrix: Solid
Laboratory Report
03/12/2019
Client Sample ID: E-1
Prism Sample ID: 9030103-02
Prism Work Order: 9030103
Time Collected: 03/05/19 09:40
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0049
0.00041
1
8260B
3/7/19 16:40
JLB
P9C0139
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0049
0.00024
1
8260B
3/7/19 16:40
JLB
P9C0139
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0049
0.00033
1
8260B
3/7/19 16:40
JLB
P9C0139
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0049
0.00044
1
8260B
3/7/19 16:40
JLB
P9C0139
1,1-Dichloroethane
BRL
mg/kg dry
0.0049
0.00014
1
8260B
3/7/19 16:40
JLB
P9C0139
1,1-Dichloroethylene
BRL
mg/kg dry
0.0049
0.00022
1
8260B
3/7/19 16:40
JLB
P9C0139
1,1-Dichloropropylene
BRL
mg/kg dry
0.0049
0.00027
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0049
0.00028
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0049
0.00063
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0049
0.00037
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0049
0.00038
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2-Dibromoethane
BRL
mg/kg dry
0.0049
0.00020
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0049
0.00023
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2-Dichloroethane
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 16:40
JLB
P9C0139
1,2-Dichloropropane
BRL
mg/kg dry
0.0049
0.00031
1
8260B
3/7/19 16:40
JLB
P9C0139
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0049
0.00037
1
8260B
3/7/19 16:40
JLB
P9C0139
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0049
0.00033
1
8260B
3/7/19 16:40
JLB
P9C0139
1,3-Dichloropropane
BRL
mg/kg dry
0.0049
0.00025
1
8260B
3/7/19 16:40
JLB
P9C0139
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0049
0.00019
1
8260B
3/7/19 16:40
JLB
P9C0139
2,2-Dichloropropane
BRL
mg/kg dry
0.0049
0.00023
1
8260B
3/7/19 16:40
JLB
P9C0139
2-Chlorotoluene
BRL
mg/kg dry
0.0049
0.00025
1
8260B
3/7/19 16:40
JLB
P9C0139
4-Chlorotoluene
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 16:40
JLB
P9C0139
4-Isopropyltoluene
BRL
mg/kg dry
0.0049
0.00024
1
8260B
3/7/19 16:40
JLB
P9C0139
Acetone
BRL
mg/kg dry
0.049
0.0012
1
8260B
3/7/19 16:40
JLB
P9C0139
Benzene
BRL
mg/kg dry
0.0030
0.00029
1
8260B
3/7/19 16:40
JLB
P9C0139
Bromobenzene
BRL
mg/kg dry
0.0049
0.00041
1
8260B
3/7/19 16:40
JLB
P9C0139
Bromochloromethane
BRL
mg/kg dry
0.0049
0.00027
1
8260B
3/7/19 16:40
JLB
P9C0139
Bromodichloromethane
BRL
mg/kg dry
0.0049
0.00028
1
8260B
3/7/19 16:40
JLB
P9C0139
Bromoform
BRL
mg/kg dry
0.0049
0.00056
1
8260B
3/7/19 16:40
JLB
P9C0139
Bromomethane
BRL
mg/kg dry
0.0099
0.00061
1
8260B
3/7/19 16:40
JLB
P9C0139
Carbon Tetrachloride
BRL
mg/kg dry
0.0049
0.00025
1
8260B
3/7/19 16:40
JLB
P9C0139
Chlorobenzene
BRL
mg/kg dry
0.0049
0.00026
1
8260B
3/7/19 16:40
JLB
P9C0139
Chloroethane
BRL
mg/kg dry
0.0099
0.00041
1
8260B
3/7/19 16:40
JLB
P9C0139
Chloroform
BRL
mg/kg dry
0.0049
0.00036
1
8260B
3/7/19 16:40
JLB
P9C0139
Chloromethane
BRL
mg/kg dry
0.0049
0.00033
1
8260B
3/7/19 16:40
JLB
P9C0139
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0049
0.00021
1
8260B
3/7/19 16:40
JLB
P9C0139
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0049
0.00017
1
8260B
3/7/19 16:40
JLB
P9C0139
Dibromochloromethane
BRL
mg/kg dry
0.0049
0.00020
1
8260B
3/7/19 16:40
JLB
P9C0139
Dichlorodifluoromethane
BRL
mg/kg dry
0.0049
0.00022
1
8260B
3/7/19 16:40
JLB
P9C0139
Ethylbenzene
BRL
mg/kg dry
0.0049
0.00019
1
8260B
3/7/19 16:40
JLB
P9C0139
Isopropyl Ether
BRL
mg/kg dry
0.0049
0.00020
1
8260B
3/7/19 16:40
JLB
P9C0139
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 16:40
JLB
P9C0139
m,p-Xylenes
BRL
mg/kg dry
0.0099
0.00045
1
8260B
3/7/19 16:40
JLB
P9C0139
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 37

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 03/12/2019
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Client Sample ID: E-1
Attn: Chris Orrell Prism Sample ID: 9030103-02
1812 Center Park Drive, Suite D Prism Work Order: 9030103
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 03/05/19 09:40
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
Limit
MDL
Dilution
Factor
Method
Analysis
Date/Time
Analyst
Batch
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.049
0.00045
1
8260B
3/7/19 16:40
JLB
P9C0139
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.099
0.00045
1
8260B
3/7/19 16:40
JLB
P9C0139
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.049
0.00042
1
8260B
3/7/19 16:40
JLB
P9C0139
Methylene Chloride
BRL
mg/kg dry
0.0099
0.00028
1
8260B
3/7/19 16:40
JLB
P9C0139
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0099
0.00016
1
8260B
3/7/19 16:40
JLB
P9C0139
Naphthalene
0.0049 J
mg/kg dry
0.0099
0.00016
1
8260B
3/7/19 16:40
JLB
P9C0139
n-Butylbenzene
BRL
mg/kg dry
0.0049
0.00025
1
8260B
3/7/19 16:40
JLB
P9C0139
n-Propylbenzene
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 16:40
JLB
P9C0139
o-Xylene
BRL
mg/kg dry
0.0049
0.00020
1
8260B
3/7/19 16:40
JLB
P9C0139
sec-Butylbenzene
BRL
mg/kg dry
0.0049
0.00024
1
8260B
3/7/19 16:40
JLB
P9C0139
Styrene
BRL
mg/kg dry
0.0049
0.00030
1
8260B
3/7/19 16:40
JLB
P9C0139
tert-Butylbenzene
BRL
mg/kg dry
0.0049
0.00017
1
8260B
3/7/19 16:40
JLB
P9C0139
Tetrachloroethylene
BRL
mg/kg dry
0.0049
0.00023
1
8260B
3/7/19 16:40
JLB
P9C0139
Toluene
BRL
mg/kg dry
0.0049
0.00028
1
8260B
3/7/19 16:40
JLB
P9C0139
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 16:40
JLB
P9C0139
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0049
0.00026
1
8260B
3/7/19 16:40
JLB
P9C0139
Trichloroethylene
BRL
mg/kg dry
0.0049
0.00032
1
8260B
3/7/19 16:40
JLB
P9C0139
Trichlorofluoromethane
BRL
mg/kg dry
0.0049
0.00032
1
8260B
3/7/19 16:40
JLB
P9C0139
Vinyl acetate
BRL
mg/kg dry
0.025
0.00068
1
8260B
3/7/19 16:40
JLB
P9C0139
Vinyl chloride
BRL
mg/kg dry
0.0049
0.00024
1
8260B
3/7/19 16:40
JLB
P9C0139
Xylenes, total
BRL
mg/kg dry
0.015
0.00092
1
8260B
3/7/19 16:40
JLB
P9C0139
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
70-130
Dibromofluoromethane
106 %
84-123
Toluene-d8
90 %
76-129
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics BRL mg/kg dry
25 0.81 100
MADEP VPH 3/11/19 12:22
TBL P9C0146
C9-Cl2 Aliphatics BRL mg/kg dry
25 1.3 100
MADEP VPH 3/11/19 12:22
TBL P9C0146
C9-Cl0 Aromatics BRL mg/kg dry
25 0.28 100
MADEP VPH 3/11/19 12:22
TBL P9C0146
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
130 %
70-130
2,5-Dibromotoluene (FID)
139 %
70-130 PLM, SF
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 11 of 37

P R S M Laboratory Report
` Full -Service Analytical &
/ environmental Solutions 03/12/2019
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Client Sample ID: B-1
Attn: Chris Orrell Prism Sample ID: 9030103-03
1812 Center Park Drive, Suite D Prism Work Order: 9030103
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 03/05/19 09:50
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
44
mg/kg dry
27 0.17
1
MADEP EPH 3/11/19 19:33
BGB
P9C0135
C19-C36 Aliphatics
10 J
mg/kg dry
27 3.2
1
MADEP EPH 3/11/19 19:33
BGB
P9C0135
C11-C22 Aromatics
26
mg/kg dry
11 1.9
1
MADEP EPH 3/11/19 19:33
BGB
P9C0135
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
91 %
40-140
o-Terphenyl
103 %
40-140
2-Fluorobiphenyl
100 %
40-140
2-Bromonaphthalene
99 %
40-140
General Chemistry Parameters
% Solids
90.9
% by
0.100
0.100
1
SM2540 G
3/12/19 9:31
KBS
P9C0167
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/11/19 13:01
JMV
P9C0132
1,2-Dichlorobenzene
BRL
mg/kg dry
0.36
0.055
1
8270D
3/11/19 13:01
JMV
P9C0132
1,3-Dichlorobenzene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:01
JMV
P9C0132
1,4-Dichlorobenzene
BRL
mg/kg dry
0.36
0.053
1
8270D
3/11/19 13:01
JMV
P9C0132
1-Methyl naphthalene
0.20 J
mg/kg dry
0.36
0.070
1
8270D
3/11/19 13:01
JMV
P9C0132
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.36
0.058
1
8270D
3/11/19 13:01
JMV
P9C0132
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.36
0.068
1
8270D
3/11/19 13:01
JMV
P9C0132
2,4-Dichlorophenol
BRL
mg/kg dry
0.36
0.070
1
8270D
3/11/19 13:01
JMV
P9C0132
2,4-Dimethylphenol
BRL
mg/kg dry
0.36
0.056
1
8270D
3/11/19 13:01
JMV
P9C0132
2,4-Dinitrophenol
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:01
JMV
P9C0132
2,4-Dinitrotoluene
BRL
mg/kg dry
0.36
0.044
1
8270D
3/11/19 13:01
JMV
P9C0132
2,6-Dinitrotoluene
BRL
mg/kg dry
0.36
0.048
1
8270D
3/11/19 13:01
JMV
P9C0132
2-Chloronaphthalene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/11/19 13:01
JMV
P9C0132
2-Chlorophenol
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:01
JMV
P9C0132
2-Methyl naphthalene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/11/19 13:01
JMV
P9C0132
2-Methylphenol
BRL
mg/kg dry
0.36
0.046
1
8270D
3/11/19 13:01
JMV
P9C0132
2-Nitrophenol
BRL
mg/kg dry
0.36
0.066
1
8270D
3/11/19 13:01
JMV
P9C0132
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.36
0.072
1
8270D
3/11/19 13:01
JMV
P9C0132
3/4-Methyl phenol
BRL
mg/kg dry
0.36
0.045
1
8270D
3/11/19 13:01
JMV
P9C0132
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.36
0.054
1
8270D
3/11/19 13:01
JMV
P9C0132
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.36
0.062
1
8270D
3/11/19 13:01
JMV
P9C0132
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:01
JMV
P9C0132
4-Chloroaniline
BRL
mg/kg dry
0.36
0.044
1
8270D
3/11/19 13:01
JMV
P9C0132
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:01
JMV
P9C0132
4-Nitrophenol
BRL
mg/kg dry
0.36
0.056
1
8270D
3/11/19 13:01
JMV
P9C0132
Acenaphthene
BRL
mg/kg dry
0.36
0.049
1
8270D
3/11/19 13:01
JMV
P9C0132
Acenaphthylene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/11/19 13:01
JMV
P9C0132
Anthracene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/11/19 13:01
JMV
P9C0132
Azobenzene
BRL
mg/kg dry
0.36
0.048
1
8270D
3/11/19 13:01
JMV
P9C0132
Benzo(a)anthracene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:01
JMV
P9C0132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 37

Laboratory Report
` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
03/12/2019
ECS Carolinas, LLP (Charlotte)
Project: W. Morehead
Client Sample ID: B-1
Attn: Chris Orrell
Prism Sample ID: 9030103-03
1812 Center Park Drive, Suite D
Prism Work Order:
9030103
Charlotte, NC 28217
Sample Matrix: Solid
Time Collected:
03/05/19 09:50
Time Submitted:
03/06/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.36
0.039
1
8270D
3/11/19 13:01
JMV
P9C0132
Benzo(b)fluoranthene
BRL
mg/kg dry
0.36
0.042
1
8270D
3/11/19 13:01
JMV
P9C0132
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.36
0.040
1
8270D
3/11/19 13:01
JMV
P9C0132
Benzo(k)fluoranthene
BRL
mg/kg dry
0.36
0.048
1
8270D
3/11/19 13:01
JMV
P9C0132
Benzoic Acid
BRL
mg/kg dry
0.36
0.031
1
8270D
3/11/19 13:01
JMV
P9C0132
Benzyl alcohol
BRL
mg/kg dry
0.36
0.048
1
8270D
3/11/19 13:01
JMV
P9C0132
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.36
0.063
1
8270D
3/11/19 13:01
JMV
P9C0132
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:01
JMV
P9C0132
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.36
0.062
1
8270D
3/11/19 13:01
JMV
P9C0132
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.36
0.054
1
8270D
3/11/19 13:01
JMV
P9C0132
Butyl benzyl phthalate
BRL
mg/kg dry
0.36
0.052
1
8270D
3/11/19 13:01
JMV
P9C0132
Chrysene
BRL
mg/kg dry
0.36
0.046
1
8270D
3/11/19 13:01
JMV
P9C0132
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.36
0.044
1
8270D
3/11/19 13:01
JMV
P9C0132
Dibenzofuran
BRL
mg/kg dry
0.36
0.055
1
8270D
3/11/19 13:01
JMV
P9C0132
Diethyl phthalate
BRL
mg/kg dry
0.36
0.050
1
8270D
3/11/19 13:01
JMV
P9C0132
Dimethyl phthalate
BRL
mg/kg dry
0.36
0.048
1
8270D
3/11/19 13:01
JMV
P9C0132
Di-n-butyl phthalate
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:01
JMV
P9C0132
Di-n-octyl phthalate
BRL
mg/kg dry
0.36
0.045
1
8270D
3/11/19 13:01
JMV
P9C0132
Fluoranthene
BRL
mg/kg dry
0.36
0.046
1
8270D
3/11/19 13:01
JMV
P9C0132
Fluorene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/11/19 13:01
JMV
P9C0132
Hexachlorobenzene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/11/19 13:01
JMV
P9C0132
Hexachlorobutadiene
BRL
mg/kg dry
0.36
0.065
1
8270D
3/11/19 13:01
JMV
P9C0132
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.36
0.065
1
8270D
3/11/19 13:01
JMV
P9C0132
Hexachloroethane
BRL
mg/kg dry
0.36
0.061
1
8270D
3/11/19 13:01
JMV
P9C0132
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.36
0.042
1
8270D
3/11/19 13:01
JMV
P9C0132
Isophorone
BRL
mg/kg dry
0.36
0.049
1
8270D
3/11/19 13:01
JMV
P9C0132
Naphthalene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/11/19 13:01
JMV
P9C0132
Nitrobenzene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:01
JMV
P9C0132
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.36
0.057
1
8270D
3/11/19 13:01
JMV
P9C0132
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.36
0.055
1
8270D
3/11/19 13:01
JMV
P9C0132
Pentachlorophenol
BRL
mg/kg dry
0.36
0.043
1
8270D
3/11/19 13:01
JMV
P9C0132
Phenanthrene
0.17
J mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:01
JMV
P9C0132
Phenol
BRL
mg/kg dry
0.36
0.053
1
8270D
3/11/19 13:01
JMV
P9C0132
Pyrene
BRL
mg/kg dry
0.36
0.048
1
8270D
3/11/19 13:01
JMV
P9C0132
Pyridine
BRL
mg/kg dry
0.36
0.063
1
8270D
3/11/19 13:01
JMV
P9C0132
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
96 %
39-132
2-Fluorobiphenyl
95 %
44-115
2-Fluorophenol
91 %
35-115
Nitrobenzene-d5
86 %
37-122
Phenol-d5
88 %
34-121
Terphenyl-d14
95 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 37

` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead
Sample Matrix: Solid
Laboratory Report
03/12/2019
Client Sample ID: B-1
Prism Sample ID: 9030103-03
Prism Work Order: 9030103
Time Collected: 03/05/19 09:50
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0049
0.00040
1
8260B
3/7/19 17:10
JLB
P9C0139
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0049
0.00024
1
8260B
3/7/19 17:10
JLB
P9C0139
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0049
0.00033
1
8260B
3/7/19 17:10
JLB
P9C0139
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0049
0.00043
1
8260B
3/7/19 17:10
JLB
P9C0139
1,1-Dichloroethane
BRL
mg/kg dry
0.0049
0.00014
1
8260B
3/7/19 17:10
JLB
P9C0139
1,1-Dichloroethylene
BRL
mg/kg dry
0.0049
0.00022
1
8260B
3/7/19 17:10
JLB
P9C0139
1,1-Dichloropropylene
BRL
mg/kg dry
0.0049
0.00027
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0049
0.00028
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0049
0.00063
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0049
0.00036
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0049
0.00037
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2-Dibromoethane
BRL
mg/kg dry
0.0049
0.00020
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0049
0.00023
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2-Dichloroethane
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 17:10
JLB
P9C0139
1,2-Dichloropropane
BRL
mg/kg dry
0.0049
0.00030
1
8260B
3/7/19 17:10
JLB
P9C0139
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0049
0.00037
1
8260B
3/7/19 17:10
JLB
P9C0139
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0049
0.00032
1
8260B
3/7/19 17:10
JLB
P9C0139
1,3-Dichloropropane
BRL
mg/kg dry
0.0049
0.00025
1
8260B
3/7/19 17:10
JLB
P9C0139
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0049
0.00019
1
8260B
3/7/19 17:10
JLB
P9C0139
2,2-Dichloropropane
BRL
mg/kg dry
0.0049
0.00023
1
8260B
3/7/19 17:10
JLB
P9C0139
2-Chlorotoluene
BRL
mg/kg dry
0.0049
0.00025
1
8260B
3/7/19 17:10
JLB
P9C0139
4-Chlorotoluene
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 17:10
JLB
P9C0139
4-Isopropyltoluene
BRL
mg/kg dry
0.0049
0.00024
1
8260B
3/7/19 17:10
JLB
P9C0139
Acetone
BRL
mg/kg dry
0.049
0.0012
1
8260B
3/7/19 17:10
JLB
P9C0139
Benzene
BRL
mg/kg dry
0.0029
0.00029
1
8260B
3/7/19 17:10
JLB
P9C0139
Bromobenzene
BRL
mg/kg dry
0.0049
0.00041
1
8260B
3/7/19 17:10
JLB
P9C0139
Bromochloromethane
BRL
mg/kg dry
0.0049
0.00027
1
8260B
3/7/19 17:10
JLB
P9C0139
Bromodichloromethane
BRL
mg/kg dry
0.0049
0.00027
1
8260B
3/7/19 17:10
JLB
P9C0139
Bromoform
BRL
mg/kg dry
0.0049
0.00056
1
8260B
3/7/19 17:10
JLB
P9C0139
Bromomethane
BRL
mg/kg dry
0.0098
0.00061
1
8260B
3/7/19 17:10
JLB
P9C0139
Carbon Tetrachloride
BRL
mg/kg dry
0.0049
0.00024
1
8260B
3/7/19 17:10
JLB
P9C0139
Chlorobenzene
BRL
mg/kg dry
0.0049
0.00026
1
8260B
3/7/19 17:10
JLB
P9C0139
Chloroethane
BRL
mg/kg dry
0.0098
0.00041
1
8260B
3/7/19 17:10
JLB
P9C0139
Chloroform
BRL
mg/kg dry
0.0049
0.00035
1
8260B
3/7/19 17:10
JLB
P9C0139
Chloromethane
BRL
mg/kg dry
0.0049
0.00033
1
8260B
3/7/19 17:10
JLB
P9C0139
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0049
0.00021
1
8260B
3/7/19 17:10
JLB
P9C0139
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0049
0.00016
1
8260B
3/7/19 17:10
JLB
P9C0139
Dibromochloromethane
BRL
mg/kg dry
0.0049
0.00020
1
8260B
3/7/19 17:10
JLB
P9C0139
Dichlorodifluoromethane
BRL
mg/kg dry
0.0049
0.00022
1
8260B
3/7/19 17:10
JLB
P9C0139
Ethylbenzene
BRL
mg/kg dry
0.0049
0.00019
1
8260B
3/7/19 17:10
JLB
P9C0139
Isopropyl Ether
BRL
mg/kg dry
0.0049
0.00020
1
8260B
3/7/19 17:10
JLB
P9C0139
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0049
0.00029
1
8260B
3/7/19 17:10
JLB
P9C0139
m,p-Xylenes
BRL
mg/kg dry
0.0098
0.00045
1
8260B
3/7/19 17:10
JLB
P9C0139
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 37

Laboratory Report
` Full -Service
Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
03/12/2019
ECS Carolinas, LLP (Charlotte)
Project:
W. Morehead
Client
Sample ID: B-1
Attn: Chris Orrell
Prism
Sample ID: 9030103-03
1812 Center Park Drive, Suite D
Prism
Work Order: 9030103
Charlotte, NC 28217
Sample Matrix: Solid
Time
Collected: 03/05/19 09:50
Time
Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.049
0.00044
1
8260B 3/7/19 17:10
JLB
P9C0139
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.098
0.00044
1
8260B 3/7/19 17:10
JLB
P9C0139
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.049
0.00042
1
8260B 3/7/19 17:10
JLB
P9C0139
Methylene Chloride
BRL
mg/kg dry
0.0098
0.00028
1
8260B 3/7/19 17:10
JLB
P9C0139
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0098
0.00016
1
8260B 3/7/19 17:10
JLB
P9C0139
Naphthalene
BRL
mg/kg dry
0.0098
0.00015
1
8260B 3/7/19 17:10
JLB
P9C0139
n-Butylbenzene
BRL
mg/kg dry
0.0049
0.00025
1
8260B 3/7/19 17:10
JLB
P9C0139
n-Propylbenzene
BRL
mg/kg dry
0.0049
0.00029
1
8260B 3/7/19 17:10
JLB
P9C0139
o-Xylene
BRL
mg/kg dry
0.0049
0.00020
1
8260B 3/7/19 17:10
JLB
P9C0139
sec-Butylbenzene
BRL
mg/kg dry
0.0049
0.00024
1
8260B 3/7/19 17:10
JLB
P9C0139
Styrene
BRL
mg/kg dry
0.0049
0.00030
1
8260B 3/7/19 17:10
JLB
P9C0139
tert-Butylbenzene
BRL
mg/kg dry
0.0049
0.00017
1
8260B 3/7/19 17:10
JLB
P9C0139
Tetrachloroethylene
BRL
mg/kg dry
0.0049
0.00023
1
8260B 3/7/19 17:10
JLB
P9C0139
Toluene
BRL
mg/kg dry
0.0049
0.00028
1
8260B 3/7/19 17:10
JLB
P9C0139
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0049
0.00029
1
8260B 3/7/19 17:10
JLB
P9C0139
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0049
0.00026
1
8260B 3/7/19 17:10
JLB
P9C0139
Trichloroethylene
BRL
mg/kg dry
0.0049
0.00032
1
8260B 3/7/19 17:10
JLB
P9C0139
Trichlorofluoromethane
BRL
mg/kg dry
0.0049
0.00032
1
8260B 3/7/19 17:10
JLB
P9C0139
Vinyl acetate
BRL
mg/kg dry
0.025
0.00067
1
8260B 3/7/19 17:10
JLB
P9C0139
Vinyl chloride
BRL
mg/kg dry
0.0049
0.00024
1
8260B 3/7/19 17:10
JLB
P9C0139
Xylenes, total
BRL
mg/kg dry
0.015
0.00092
1
8260B 3/7/19 17:10
JLB
P9C0139
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
102 %
70-130
Dibromofluoromethane
102 %
84-123
Toluene-d8
90 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
17
0.56
100
MADEP VPH 3/11/19 12:50
TBL
P9C0146
C9-C12 Aliphatics
4.9 J
mg/kg dry
17
0.90
100
MADEP VPH 3/11/19 12:50
TBL
P9C0146
C9-Cl0 Aromatics
BRL
mg/kg dry
17
0.19
100
MADEP VPH 3/11/19 12:50
TBL
P9C0146
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
118 %
70-130
2,5-Dibromotoluene (FID)
127 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 15 of 37

P R S M Laboratory Report
` Full -Service Analytical &
/ environmental Solutions 03/12/2019
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Client Sample ID: N-1
Attn: Chris Orrell Prism Sample ID: 9030103-04
1812 Center Park Drive, Suite D Prism Work Order: 9030103
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 03/05/19 09:55
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
120
mg/kg dry
27 0.17
1
MADEP EPH 3/11/19 20:09
BGB
P9C0135
C19-C36 Aliphatics
19 J
mg/kg dry
27 3.2
1
MADEP EPH 3/11/19 20:09
BGB
P9C0135
C11-C22 Aromatics
60
mg/kg dry
11 1.9
1
MADEP EPH 3/11/19 20:09
BGB
P9C0135
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
90 %
40-140
o-Terphenyl
104 %
40-140
2-Fluorobiphenyl
110 %
40-140
2-Bromonaphthalene
101 %
40-140
General Chemistry Parameters
% Solids
92.4
% by
0.100
0.100
1
SM2540 G
3/12/19 9:31
KBS
P9C0167
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.36
0.056
1
8270D
3/11/19 13:23
JMV
P9C0132
1,2-Dichlorobenzene
BRL
mg/kg dry
0.36
0.054
1
8270D
3/11/19 13:23
JMV
P9C0132
1,3-Dichlorobenzene
BRL
mg/kg dry
0.36
0.050
1
8270D
3/11/19 13:23
JMV
P9C0132
1,4-Dichlorobenzene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/11/19 13:23
JMV
P9C0132
1-Methyl naphthalene
0.64
mg/kg dry
0.36
0.069
1
8270D
3/11/19 13:23
JMV
P9C0132
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.36
0.058
1
8270D
3/11/19 13:23
JMV
P9C0132
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.36
0.067
1
8270D
3/11/19 13:23
JMV
P9C0132
2,4-Dichlorophenol
BRL
mg/kg dry
0.36
0.069
1
8270D
3/11/19 13:23
JMV
P9C0132
2,4-Dimethylphenol
BRL
mg/kg dry
0.36
0.055
1
8270D
3/11/19 13:23
JMV
P9C0132
2,4-Dinitrophenol
BRL
mg/kg dry
0.36
0.050
1
8270D
3/11/19 13:23
JMV
P9C0132
2,4-Dinitrotoluene
BRL
mg/kg dry
0.36
0.043
1
8270D
3/11/19 13:23
JMV
P9C0132
2,6-Dinitrotoluene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:23
JMV
P9C0132
2-Chloronaphthalene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/11/19 13:23
JMV
P9C0132
2-Chlorophenol
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:23
JMV
P9C0132
2-Methyl naphthalene
0.69
mg/kg dry
0.36
0.057
1
8270D
3/11/19 13:23
JMV
P9C0132
2-Methylphenol
BRL
mg/kg dry
0.36
0.046
1
8270D
3/11/19 13:23
JMV
P9C0132
2-Nitrophenol
BRL
mg/kg dry
0.36
0.065
1
8270D
3/11/19 13:23
JMV
P9C0132
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.36
0.071
1
8270D
3/11/19 13:23
JMV
P9C0132
3/4-Methyl phenol
BRL
mg/kg dry
0.36
0.044
1
8270D
3/11/19 13:23
JMV
P9C0132
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.36
0.054
1
8270D
3/11/19 13:23
JMV
P9C0132
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.36
0.061
1
8270D
3/11/19 13:23
JMV
P9C0132
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.36
0.050
1
8270D
3/11/19 13:23
JMV
P9C0132
4-Chloroaniline
BRL
mg/kg dry
0.36
0.043
1
8270D
3/11/19 13:23
JMV
P9C0132
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.36
0.046
1
8270D
3/11/19 13:23
JMV
P9C0132
4-Nitrophenol
BRL
mg/kg dry
0.36
0.055
1
8270D
3/11/19 13:23
JMV
P9C0132
Acenaphthene
BRL
mg/kg dry
0.36
0.049
1
8270D
3/11/19 13:23
JMV
P9C0132
Acenaphthylene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/11/19 13:23
JMV
P9C0132
Anthracene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/11/19 13:23
JMV
P9C0132
Azobenzene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:23
JMV
P9C0132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 37

` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead
Sample Matrix: Solid
Laboratory Report
03/12/2019
Client Sample ID: N-1
Prism Sample ID: 9030103-04
Prism Work Order: 9030103
Time Collected: 03/05/19 09:55
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)anthracene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:23
JMV
P9C0132
Benzo(a)pyrene
BRL
mg/kg dry
0.36
0.039
1
8270D
3/11/19 13:23
JMV
P9C0132
Benzo(b)fluoranthene
BRL
mg/kg dry
0.36
0.041
1
8270D
3/11/19 13:23
JMV
P9C0132
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.36
0.039
1
8270D
3/11/19 13:23
JMV
P9C0132
Benzo(k)fluoranthene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:23
JMV
P9C0132
Benzoic Acid
BRL
mg/kg dry
0.36
0.030
1
8270D
3/11/19 13:23
JMV
P9C0132
Benzyl alcohol
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:23
JMV
P9C0132
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.36
0.062
1
8270D
3/11/19 13:23
JMV
P9C0132
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.36
0.050
1
8270D
3/11/19 13:23
JMV
P9C0132
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.36
0.061
1
8270D
3/11/19 13:23
JMV
P9C0132
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.36
0.053
1
8270D
3/11/19 13:23
JMV
P9C0132
Butyl benzyl phthalate
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:23
JMV
P9C0132
Chrysene
BRL
mg/kg dry
0.36
0.045
1
8270D
3/11/19 13:23
JMV
P9C0132
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.36
0.043
1
8270D
3/11/19 13:23
JMV
P9C0132
Dibenzofuran
BRL
mg/kg dry
0.36
0.054
1
8270D
3/11/19 13:23
JMV
P9C0132
Diethyl phthalate
BRL
mg/kg dry
0.36
0.049
1
8270D
3/11/19 13:23
JMV
P9C0132
Dimethyl phthalate
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:23
JMV
P9C0132
Di-n-butyl phthalate
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:23
JMV
P9C0132
Di-n-octyl phthalate
BRL
mg/kg dry
0.36
0.044
1
8270D
3/11/19 13:23
JMV
P9C0132
Fluoranthene
BRL
mg/kg dry
0.36
0.046
1
8270D
3/11/19 13:23
JMV
P9C0132
Fluorene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:23
JMV
P9C0132
Hexachlorobenzene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/11/19 13:23
JMV
P9C0132
Hexachlorobutadiene
BRL
mg/kg dry
0.36
0.064
1
8270D
3/11/19 13:23
JMV
P9C0132
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.36
0.064
1
8270D
3/11/19 13:23
JMV
P9C0132
Hexachloroethane
BRL
mg/kg dry
0.36
0.060
1
8270D
3/11/19 13:23
JMV
P9C0132
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.36
0.041
1
8270D
3/11/19 13:23
JMV
P9C0132
Isophorone
BRL
mg/kg dry
0.36
0.048
1
8270D
3/11/19 13:23
JMV
P9C0132
Naphthalene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/11/19 13:23
JMV
P9C0132
Nitrobenzene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/11/19 13:23
JMV
P9C0132
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.36
0.056
1
8270D
3/11/19 13:23
JMV
P9C0132
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.36
0.054
1
8270D
3/11/19 13:23
JMV
P9C0132
Pentachlorophenol
BRL
mg/kg dry
0.36
0.042
1
8270D
3/11/19 13:23
JMV
P9C0132
Phenanthrene
0.30
J mg/kg dry
0.36
0.046
1
8270D
3/11/19 13:23
JMV
P9C0132
Phenol
BRL
mg/kg dry
0.36
0.053
1
8270D
3/11/19 13:23
JMV
P9C0132
Pyrene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/11/19 13:23
JMV
P9C0132
Pyridine
BRL
mg/kg dry
0.36
0.062
1
8270D
3/11/19 13:23
JMV
P9C0132
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
99 %
39-132
2-Fluorobiphenyl
96 %
44-115
2-Fluorophenol
96 %
35-115
Nitrobenzene-d5
89 %
37-122
Phenol-d5
92 %
34-121
Terphenyl-d14
96 %
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 37

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/12/2019
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead Client Sample ID: N-1
Prism Sample ID: 9030103-04
Prism Work Order: 9030103
Sample Matrix: Solid Time Collected: 03/05/19 09:55
Time Submitted: 03/06/19 16:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0074
0.00061
1
8260B
3/7/19 17:41
JLB
P9C0139
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0074
0.00036
1
8260B
3/7/19 17:41
JLB
P9C0139
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0074
0.00050
1
8260B
3/7/19 17:41
JLB
P9C0139
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0074
0.00066
1
8260B
3/7/19 17:41
JLB
P9C0139
1,1-Dichloroethane
BRL
mg/kg dry
0.0074
0.00021
1
8260B
3/7/19 17:41
JLB
P9C0139
1,1-Dichloroethylene
BRL
mg/kg dry
0.0074
0.00033
1
8260B
3/7/19 17:41
JLB
P9C0139
1,1-Dichloropropylene
BRL
mg/kg dry
0.0074
0.00041
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0074
0.00042
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0074
0.00094
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0074
0.00055
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0074
0.00056
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2-Dibromoethane
BRL
mg/kg dry
0.0074
0.00030
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0074
0.00035
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2-Dichloroethane
BRL
mg/kg dry
0.0074
0.00044
1
8260B
3/7/19 17:41
JLB
P9C0139
1,2-Dichloropropane
BRL
mg/kg dry
0.0074
0.00046
1
8260B
3/7/19 17:41
JLB
P9C0139
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0074
0.00056
1
8260B
3/7/19 17:41
JLB
P9C0139
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0074
0.00049
1
8260B
3/7/19 17:41
JLB
P9C0139
1,3-Dichloropropane
BRL
mg/kg dry
0.0074
0.00037
1
8260B
3/7/19 17:41
JLB
P9C0139
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0074
0.00029
1
8260B
3/7/19 17:41
JLB
P9C0139
2,2-Dichloropropane
BRL
mg/kg dry
0.0074
0.00035
1
8260B
3/7/19 17:41
JLB
P9C0139
2-Chlorotoluene
BRL
mg/kg dry
0.0074
0.00038
1
8260B
3/7/19 17:41
JLB
P9C0139
4-Chlorotoluene
BRL
mg/kg dry
0.0074
0.00044
1
8260B
3/7/19 17:41
JLB
P9C0139
4-Isopropyltoluene 0.0050
J
mg/kg dry
0.0074
0.00036
1
8260B
3/7/19 17:41
JLB
P9C0139
Acetone
BRL
mg/kg dry
0.074
0.0018
1
8260B
3/7/19 17:41
JLB
P9C0139
Benzene
BRL
mg/kg dry
0.0044
0.00043
1
8260B
3/7/19 17:41
JLB
P9C0139
Bromobenzene
BRL
mg/kg dry
0.0074
0.00062
1
8260B
3/7/19 17:41
JLB
P9C0139
Bromochloromethane
BRL
mg/kg dry
0.0074
0.00041
1
8260B
3/7/19 17:41
JLB
P9C0139
Bromodichloromethane
BRL
mg/kg dry
0.0074
0.00041
1
8260B
3/7/19 17:41
JLB
P9C0139
Bromoform
BRL
mg/kg dry
0.0074
0.00084
1
8260B
3/7/19 17:41
JLB
P9C0139
Bromomethane
BRL
mg/kg dry
0.015
0.00091
1
8260B
3/7/19 17:41
JLB
P9C0139
Carbon Tetrachloride
BRL
mg/kg dry
0.0074
0.00037
1
8260B
3/7/19 17:41
JLB
P9C0139
Chlorobenzene
BRL
mg/kg dry
0.0074
0.00039
1
8260B
3/7/19 17:41
JLB
P9C0139
Chloroethane
BRL
mg/kg dry
0.015
0.00062
1
8260B
3/7/19 17:41
JLB
P9C0139
Chloroform
BRL
mg/kg dry
0.0074
0.00053
1
8260B
3/7/19 17:41
JLB
P9C0139
Chloromethane
BRL
mg/kg dry
0.0074
0.00050
1
8260B
3/7/19 17:41
JLB
P9C0139
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0074
0.00032
1
8260B
3/7/19 17:41
JLB
P9C0139
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0074
0.00025
1
8260B
3/7/19 17:41
JLB
P9C0139
Dibromochloromethane
BRL
mg/kg dry
0.0074
0.00030
1
8260B
3/7/19 17:41
JLB
P9C0139
Dichlorodifluoromethane
BRL
mg/kg dry
0.0074
0.00034
1
8260B
3/7/19 17:41
JLB
P9C0139
Ethylbenzene
BRL
mg/kg dry
0.0074
0.00028
1
8260B
3/7/19 17:41
JLB
P9C0139
Isopropyl Ether
BRL
mg/kg dry
0.0074
0.00030
1
8260B
3/7/19 17:41
JLB
P9C0139
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0074
0.00044
1
8260B
3/7/19 17:41
JLB
P9C0139
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 37

P R S M Laboratory Report
` Full -Service Analytical &
/ Environmental Solutions 03/12/2019
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Client Sample ID: N-1
Attn: Chris Orrell Prism Sample ID: 9030103-04
1812 Center Park Drive, Suite D Prism Work Order: 9030103
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 03/05/19 09:55
Time Submitted: 03/06/19 16:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
BRL
mg/kg dry
0.015
0.00068
1
8260B
3/7/19 17:41
JLB
P9C0139
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.074
0.00067
1
8260B
3/7/19 17:41
JLB
P9C0139
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.15
0.00067
1
8260B
3/7/19 17:41
JLB
P9C0139
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.074
0.00063
1
8260B
3/7/19 17:41
JLB
P9C0139
Methylene Chloride
BRL
mg/kg dry
0.015
0.00042
1
8260B
3/7/19 17:41
JLB
P9C0139
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.015
0.00024
1
8260B
3/7/19 17:41
JLB
P9C0139
Naphthalene
0.038
mg/kg dry
0.015
0.00023
1
8260B
3/7/19 17:41
JLB
P9C0139
n-Butylbenzene
0.0057 J
mg/kg dry
0.0074
0.00038
1
8260B
3/7/19 17:41
JLB
P9C0139
n-Propylbenzene
BRL
mg/kg dry
0.0074
0.00044
1
8260B
3/7/19 17:41
JLB
P9C0139
o-Xylene
BRL
mg/kg dry
0.0074
0.00030
1
8260B
3/7/19 17:41
JLB
P9C0139
sec-Butylbenzene
0.0055 J
mg/kg dry
0.0074
0.00036
1
8260B
3/7/19 17:41
JLB
P9C0139
Styrene
BRL
mg/kg dry
0.0074
0.00045
1
8260B
3/7/19 17:41
JLB
P9C0139
tert-Butylbenzene
BRL
mg/kg dry
0.0074
0.00025
1
8260B
3/7/19 17:41
JLB
P9C0139
Tetrachloroethylene
BRL
mg/kg dry
0.0074
0.00035
1
8260B
3/7/19 17:41
JLB
P9C0139
Toluene
BRL
mg/kg dry
0.0074
0.00042
1
8260B
3/7/19 17:41
JLB
P9C0139
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0074
0.00044
1
8260B
3/7/19 17:41
JLB
P9C0139
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0074
0.00039
1
8260B
3/7/19 17:41
JLB
P9C0139
Trichloroethylene
BRL
mg/kg dry
0.0074
0.00048
1
8260B
3/7/19 17:41
JLB
P9C0139
Trichlorofluoromethane
BRL
mg/kg dry
0.0074
0.00048
1
8260B
3/7/19 17:41
JLB
P9C0139
Vinyl acetate
BRL
mg/kg dry
0.037
0.0010
1
8260B
3/7/19 17:41
JLB
P9C0139
Vinyl chloride
BRL
mg/kg dry
0.0074
0.00036
1
8260B
3/7/19 17:41
JLB
P9C0139
Xylenes, total
BRL
mg/kg dry
0.022
0.0014
1
8260B
3/7/19 17:41
JLB
P9C0139
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
102 %
84-123
Toluene-d8
91 %
76-129
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
19
0.62
100
MADEP VPH
3/11/19 13:18
TBL
P9C0146
C9-C12 Aliphatics
8.6 J
mg/kg dry
19
1.0
100
MADEP VPH
3/11/19 13:18
TBL
P9C0146
C9-Cl0 Aromatics
BRL
mg/kg dry
19
0.22
100
MADEP VPH
3/11/19 13:18
TBL
P9C0146
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
110 %
70-130
2,5-Dibromotoluene (FID)
106 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 19 of 37

P R I IS M EService Analytical
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9C0139-BLK1)
Prepared & Analyzed: 03/07/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.0050
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.0050
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.050
mg/kg wet
Benzene
BRL
0.0030
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.0050
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.0050
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.050
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.10
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.050
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 37

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9C0139-BLK1)
Prepared & Analyzed: 03/07/19
Methylene Chloride
BRL
0.010
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.010
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.0050
mg/kg wet
Vinyl acetate
BRL
0.025
mg/kg wet
Vinyl chloride
BRL
0.0050
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
51.3
ug/L
50.00 103 70-130
Surrogate: Dibromofluoromethane
50.7
ug/L
50.00 101 84-123
Surrogate: Toluene-d8
45.5
ug/L
50.00 91 76-129
LCS (P9C0139-BS1)
Prepared
& Analyzed: 03/07/19
1,1,1,2-Tetrachloroethane
0.0520
0.0050
mg/kg wet
0.05000
104
72-115
1, 1,1 -Trichloroethane
0.0492
0.0050
mg/kg wet
0.05000
98
67-131
1,1,2,2-Tetrachloroethane
0.0435
0.0050
mg/kg wet
0.05000
87
56-126
1,1,2-Trichloroethane
0.0480
0.0050
mg/kg wet
0.05000
96
70-133
1,1-Dichloroethane
0.0489
0.0050
mg/kg wet
0.05000
98
74-127
1,1-Dichloroethylene
0.0495
0.0050
mg/kg wet
0.05000
99
67-149
1, 1 -Dichloropropylene
0.0511
0.0050
mg/kg wet
0.05000
102
71-130
1,2,3-Trichlorobenzene
0.0513
0.0050
mg/kg wet
0.05000
103
68-130
1,2,3-Trichloropropane
0.0448
0.0050
mg/kg wet
0.05000
90
60-137
1,2,4-Trichlorobenzene
0.0517
0.0050
mg/kg wet
0.05000
103
66-125
1,2,4-Trimethylbenzene
0.0455
0.0050
mg/kg wet
0.05000
91
69-129
1,2-Dibromoethane
0.0497
0.0050
mg/kg wet
0.05000
99
70-132
1,2-Dichlorobenzene
0.0437
0.0050
mg/kg wet
0.05000
87
72-123
1,2-Dichloroethane
0.0443
0.0050
mg/kg wet
0.05000
89
68-128
1,2-Dichloropropane
0.0499
0.0050
mg/kg wet
0.05000
100
73-130
1,3,5-Trimethylbenzene
0.0449
0.0050
mg/kg wet
0.05000
90
69-128
1,3-Dichlorobenzene
0.0445
0.0050
mg/kg wet
0.05000
89
71-120
1,3-Dichloropropane
0.0456
0.0050
mg/kg wet
0.05000
91
75-124
1,4-Dichlorobenzene
0.0445
0.0050
mg/kg wet
0.05000
89
71-123
2,2-Dichloropropane
0.0499
0.0050
mg/kg wet
0.05000
100
50-142
2-Chlorotoluene
0.0416
0.0050
mg/kg wet
0.05000
83
67-124
4-Chlorotoluene
0.0417
0.0050
mg/kg wet
0.05000
83
71-126
4-Isopropyltoluene
0.0466
0.0050
mg/kg wet
0.05000
93
68-129
Acetone
0.100
0.050
mg/kg wet
0.1000
100
29-198
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 37

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9C0139-BSI)
Prepared & Analyzed: 03/07/19
Benzene
0.0496
0.0030
mg/kg wet
0.05000
99
74-127
Bromobenzene
0.0399
0.0050
mg/kg wet
0.05000
80
73-125
Bromochloromethane
0.0537
0.0050
mg/kg wet
0.05000
107
72-134
Bromodichloromethane
0.0477
0.0050
mg/kg wet
0.05000
95
75-122
Bromoform
0.0538
0.0050
mg/kg wet
0.05000
108
66-135
Bromomethane
0.0404
0.010
mg/kg wet
0.05000
81
20-180
Carbon Tetrachloride
0.0513
0.0050
mg/kg wet
0.05000
103
64-143
Chlorobenzene
0.0467
0.0050
mg/kg wet
0.05000
93
74-118
Chloroethane
0.0439
0.010
mg/kg wet
0.05000
88
33-149
Chloroform
0.0474
0.0050
mg/kg wet
0.05000
95
73-127
Chloromethane
0.0514
0.0050
mg/kg wet
0.05000
103
45-143
cis-1,2-Dichloroethylene
0.0481
0.0050
mg/kg wet
0.05000
96
76-134
cis-1,3-Dichloropropylene
0.0517
0.0050
mg/kg wet
0.05000
103
71-125
Dibromochloromethane
0.0490
0.0050
mg/kg wet
0.05000
98
73-122
Dichlorodifluoromethane
0.0511
0.0050
mg/kg wet
0.05000
102
26-146
Ethylbenzene
0.0480
0.0050
mg/kg wet
0.05000
96
74-128
Isopropyl Ether
0.0486
0.0050
mg/kg wet
0.05000
97
59-159
Isopropylbenzene (Cumene)
0.0459
0.0050
mg/kg wet
0.05000
92
68-126
m,p-Xylenes
0.0969
0.010
mg/kg wet
0.1000
97
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0540
0.050
mg/kg wet
0.05000
108
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0550
0.10
mg/kg wet
0.05000
110
63-149
Methyl Isobutyl Ketone
0.0557
0.050
mg/kg wet
0.05000
ill
57-162
Methylene Chloride
0.0470
0.010
mg/kg wet
0.05000
94
74-129
Methyl-tert-Butyl Ether
0.0515
0.010
mg/kg wet
0.05000
103
70-130
Naphthalene
0.0496
0.010
mg/kg wet
0.05000
99
57-157
n-Butylbenzene
0.0453
0.0050
mg/kg wet
0.05000
91
65-135
n-Propylbenzene
0.0429
0.0050
mg/kg wet
0.05000
86
67-130
o-Xylene
0.0493
0.0050
mg/kg wet
0.05000
99
74-126
sec-Butylbenzene
0.0454
0.0050
mg/kg wet
0.05000
91
66-131
Styrene
0.0510
0.0050
mg/kg wet
0.05000
102
77-121
tert-Butyl benzene
0.0462
0.0050
mg/kg wet
0.05000
92
67-132
Tetrachloroethylene
0.0581
0.0050
mg/kg wet
0.05000
116
68-130
Toluene
0.0515
0.0050
mg/kg wet
0.05000
103
71-129
trans- 1,2-Dichloroethylene
0.0487
0.0050
mg/kg wet
0.05000
97
73-132
trans- 1,3-Dichloropropylene
0.0501
0.0050
mg/kg wet
0.05000
100
68-123
Trichloroethylene
0.0528
0.0050
mg/kg wet
0.05000
106
75-133
Trichlorofluoromethane
0.0431
0.0050
mg/kg wet
0.05000
86
44-146
Vinyl acetate
0.0596
0.025
mg/kg wet
0.05000
119
85-161
Vinyl chloride
0.0481
0.0050
mg/kg wet
0.05000
96
48-147
Xylenes, total
0.146
0.015
mg/kg wet
0.1500
97
74-126
Surrogate:4-Bromofluorobenzene
51.0
ug/L
50.00
102
70-130
Surrogate: Dibromofluoromethane
49.7
ug/L
50.00
99
84-123
Surrogate: Toluene-d8
46.0
ug/L
50.00
92
76-129
J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 37

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9CO139-BSD1)
Prepared & Analyzed: 03/07/19
1,1,1,2-Tetrachloroethane
0.0526
0.0050
mg/kg wet
0.05000
105
72-115
1 20
1, 1,1 -Trichloroethane
0.0479
0.0050
mg/kg wet
0.05000
96
67-131
3 20
1,1,2,2-Tetrachloroethane
0.0451
0.0050
mg/kg wet
0.05000
90
56-126
4 20
1,1,2-Trichloroethane
0.0485
0.0050
mg/kg wet
0.05000
97
70-133
1 20
1,1-Dichloroethane
0.0477
0.0050
mg/kg wet
0.05000
95
74-127
3 20
1,1-Dichloroethylene
0.0471
0.0050
mg/kg wet
0.05000
94
67-149
5 20
1, 1 -Dichloropropylene
0.0498
0.0050
mg/kg wet
0.05000
100
71-130
3 20
1,2,3-Trichlorobenzene
0.0517
0.0050
mg/kg wet
0.05000
103
68-130
0.8 20
1,2,3-Trichloropropane
0.0470
0.0050
mg/kg wet
0.05000
94
60-137
5 20
1,2,4-Trichlorobenzene
0.0528
0.0050
mg/kg wet
0.05000
106
66-125
2 20
1,2,4-Trimethylbenzene
0.0458
0.0050
mg/kg wet
0.05000
92
69-129
0.7 20
1,2-Dibromoethane
0.0503
0.0050
mg/kg wet
0.05000
101
70-132
1 20
1,2-Dichlorobenzene
0.0446
0.0050
mg/kg wet
0.05000
89
72-123
2 20
1,2-Dichloroethane
0.0445
0.0050
mg/kg wet
0.05000
89
68-128
0.6 20
1,2-Dichloropropane
0.0498
0.0050
mg/kg wet
0.05000
100
73-130
0.1 20
1,3,5-Trimethylbenzene
0.0447
0.0050
mg/kg wet
0.05000
89
69-128
0.4 20
1,3-Dichlorobenzene
0.0451
0.0050
mg/kg wet
0.05000
90
71-120
1 20
1,3-Dichloropropane
0.0465
0.0050
mg/kg wet
0.05000
93
75-124
2 20
1,4-Dichlorobenzene
0.0453
0.0050
mg/kg wet
0.05000
91
71-123
2 20
2,2-Dichloropropane
0.0479
0.0050
mg/kg wet
0.05000
96
50-142
4 20
2-Chlorotoluene
0.0416
0.0050
mg/kg wet
0.05000
83
67-124
0.05 20
4-Chlorotoluene
0.0422
0.0050
mg/kg wet
0.05000
84
71-126
1 20
4-Isopropyltoluene
0.0469
0.0050
mg/kg wet
0.05000
94
68-129
0.5 20
Acetone
0.108
0.050
mg/kg wet
0.1000
108
29-198
8 20
Benzene
0.0486
0.0030
mg/kg wet
0.05000
97
74-127
2 20
Bromobenzene
0.0401
0.0050
mg/kg wet
0.05000
80
73-125
0.5 20
Bromochloromethane
0.0526
0.0050
mg/kg wet
0.05000
105
72-134
2 20
Bromodichloromethane
0.0479
0.0050
mg/kg wet
0.05000
96
75-122
0.4 20
Bromoform
0.0547
0.0050
mg/kg wet
0.05000
109
66-135
2 20
Bromomethane
0.0408
0.010
mg/kg wet
0.05000
82
20-180
1 20
Carbon Tetrachloride
0.0499
0.0050
mg/kg wet
0.05000
100
64-143
3 20
Chlorobenzene
0.0463
0.0050
mg/kg wet
0.05000
93
74-118
0.8 20
Chloroethane
0.0423
0.010
mg/kg wet
0.05000
85
33-149
4 20
Chloroform
0.0467
0.0050
mg/kg wet
0.05000
93
73-127
1 20
Chloromethane
0.0498
0.0050
mg/kg wet
0.05000
100
45-143
3 20
cis-1,2-Dichloroethylene
0.0482
0.0050
mg/kg wet
0.05000
96
76-134
0.2 20
cis-1,3-Dichloropropylene
0.0518
0.0050
mg/kg wet
0.05000
104
71-125
0.2 20
Dibromochloromethane
0.0494
0.0050
mg/kg wet
0.05000
99
73-122
0.9 20
Dichlorodifluoromethane
0.0490
0.0050
mg/kg wet
0.05000
98
26-146
4 20
Ethylbenzene
0.0472
0.0050
mg/kg wet
0.05000
94
74-128
2 20
Isopropyl Ether
0.0488
0.0050
mg/kg wet
0.05000
98
59-159
0.2 20
Isopropylbenzene (Cumene)
0.0457
0.0050
mg/kg wet
0.05000
91
68-126
0.5 20
m,p-Xylenes
0.0950
0.010
mg/kg wet
0.1000
95
75-124
2 20
Methyl Butyl Ketone (2-Hexanone)
0.0556
0.050
mg/kg wet
0.05000
111
61-157
3 20
Methyl Ethyl Ketone (2-Butanone)
0.0585
0.10
mg/kg wet
0.05000
117
63-149
6 20
Methyl Isobutyl Ketone
0.0578
0.050
mg/kg wet
0.05000
116
57-162
4 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 37

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9C0139-BSD1)
Prepared & Analyzed: 03/07/19
Methylene Chloride
0.0474
0.010
mg/kg wet
0.05000
95
74-129
0.8 20
Methyl-tert-Butyl Ether
0.0522
0.010
mg/kg wet
0.05000
104
70-130
1 20
Naphthalene
0.0515
0.010
mg/kg wet
0.05000
103
57-157
4 20
n-Butylbenzene
0.0450
0.0050
mg/kg wet
0.05000
90
65-135
0.6 20
n-Propylbenzene
0.0427
0.0050
mg/kg wet
0.05000
85
67-130
0.5 20
o-Xylene
0.0491
0.0050
mg/kg wet
0.05000
98
74-126
0.3 20
sec-Butylbenzene
0.0455
0.0050
mg/kg wet
0.05000
91
66-131
0.1 20
Styrene
0.0506
0.0050
mg/kg wet
0.05000
101
77-121
0.7 20
tert-Butyl benzene
0.0463
0.0050
mg/kg wet
0.05000
93
67-132
0.2 20
Tetrachloroethylene
0.0564
0.0050
mg/kg wet
0.05000
113
68-130
3 20
Toluene
0.0508
0.0050
mg/kg wet
0.05000
102
71-129
1 20
trans- 1,2-Dichloroethylene
0.0477
0.0050
mg/kg wet
0.05000
95
73-132
2 20
trans- 1,3-Dichloropropylene
0.0505
0.0050
mg/kg wet
0.05000
101
68-123
0.9 20
Trichloroethylene
0.0520
0.0050
mg/kg wet
0.05000
104
75-133
2 20
Trichlorofluoromethane
0.0417
0.0050
mg/kg wet
0.05000
83
44-146
3 20
Vinyl acetate
0.0603
0.025
mg/kg wet
0.05000
121
85-161
1 20
Vinyl chloride
0.0469
0.0050
mg/kg wet
0.05000
94
48-147
3 20
Xylenes, total
0.144
0.015
mg/kg wet
0.1500
96
74-126
1 20
Surrogate:4-Bromofluorobenzene
51.4
ug/L
50.00
103
70-130
Surrogate: Dibromofluoromethane
49.5
ug/L
50.00
99
84-123
Surrogate: Toluene-d8
45.5
ug/L
50.00
91
76-129
Matrix Spike (P9CO139-MS1)
Source: 9030103-01
Prepared: 03/07/19 Analyzed: 03/08/19
1,1,1,2-Tetrachloroethane
0.0478
0.0053
mg/kg dry
0.05279
BRL
90
60-120
1,1,1-Trichloroethane
0.0453
0.0053
mg/kg dry
0.05279
BRL
86
52-139
1,1,2,2-Tetrachloroethane
0.0406
0.0053
mg/kg dry
0.05279
BRL
77
39-135
1,1,2-Trichloroethane
0.0450
0.0053
mg/kg dry
0.05279
BRL
85
44-140
1,1-Dichloroethane
0.0457
0.0053
mg/kg dry
0.05279
BRL
87
59-137
1,1-Dichloroethylene
0.0406
0.0053
mg/kg dry
0.05279
BRL
77
54-162
1, 1 -Dichloropropylene
0.0462
0.0053
mg/kg dry
0.05279
BRL
87
55-137
1,2,3-Trichlorobenzene
0.0428
0.0053
mg/kg dry
0.05279
BRL
81
34-120
1,2,3-Trichloropropane
0.0429
0.0053
mg/kg dry
0.05279
BRL
81
45-139
1,2,4-Trichlorobenzene
0.0406
0.0053
mg/kg dry
0.05279
BRL
77
35-116
1,2,4-Trimethylbenzene
0.0394
0.0053
mg/kg dry
0.05279
BRL
75
38-142
1,2-Dibromoethane
0.0467
0.0053
mg/kg dry
0.05279
BRL
88
49-132
1,2-Dichlorobenzene
0.0388
0.0053
mg/kg dry
0.05279
BRL
73
42-130
1,2-Dichloroethane
0.0427
0.0053
mg/kg dry
0.05279
BRL
81
51-131
1,2-Dichloropropane
0.0481
0.0053
mg/kg dry
0.05279
BRL
91
55-138
1,3,5-Trimethylbenzene
0.0388
0.0053
mg/kg dry
0.05279
BRL
74
44-140
1,3-Dichlorobenzene
0.0387
0.0053
mg/kg dry
0.05279
BRL
73
41-129
1,3-Dichloropropane
0.0437
0.0053
mg/kg dry
0.05279
BRL
83
53-129
1,4-Dichlorobenzene
0.0384
0.0053
mg/kg dry
0.05279
BRL
73
44-134
2,2-Dichloropropane
0.0437
0.0053
mg/kg dry
0.05279
BRL
83
30-147
2-Chlorotoluene
0.0362
0.0053
mg/kg dry
0.05279
BRL
69
46-132
4-Chlorotoluene
0.0363
0.0053
mg/kg dry
0.05279
BRL
69
44-135
4-Isopropyltoluene
0.0392
0.0053
mg/kg dry
0.05279
BRL
74
32-144
Acetone
0.112
0.053
mg/kg dry
0.1056
BRL
106
34-143
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 37

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P9C0139-MS1)
Source: 9030103-01
Prepared: 03/07/19 Analyzed: 03/08/19
Benzene
0.0468
0.0032
mg/kg dry
0.05279
BRL
89
60-135
Bromobenzene
0.0356
0.0053
mg/kg dry
0.05279
BRL
68
45-135
Bromochloromethane
0.0524
0.0053
mg/kg dry
0.05279
BRL
99
55-136
Bromodichloromethane
0.0444
0.0053
mg/kg dry
0.05279
BRL
84
55-127
Bromoform
0.0475
0.0053
mg/kg dry
0.05279
BRL
90
40-136
Bromomethane
0.0332
0.011
mg/kg dry
0.05279
BRL
63
30-137
Carbon Tetrachloride
0.0452
0.0053
mg/kg dry
0.05279
BRL
86
48-153
Chlorobenzene
0.0426
0.0053
mg/kg dry
0.05279
BRL
81
57-125
Chloroethane
0.0413
0.011
mg/kg dry
0.05279
BRL
78
16-177
Chloroform
0.0449
0.0053
mg/kg dry
0.05279
BRL
85
56-137
Chloromethane
0.0496
0.0053
mg/kg dry
0.05279
BRL
94
40-145
cis-1,2-Dichloroethylene
0.0462
0.0053
mg/kg dry
0.05279
BRL
87
58-140
cis-1,3-Dichloropropylene
0.0485
0.0053
mg/kg dry
0.05279
BRL
92
42-135
Dibromochloromethane
0.0439
0.0053
mg/kg dry
0.05279
BRL
83
49-127
Dichlorodifluoromethane
0.0457
0.0053
mg/kg dry
0.05279
BRL
87
25-151
Ethylbenzene
0.0429
0.0053
mg/kg dry
0.05279
BRL
81
44-144
Isopropyl Ether
0.0467
0.0053
mg/kg dry
0.05279
BRL
88
51-155
Isopropylbenzene (Cumene)
0.0401
0.0053
mg/kg dry
0.05279
BRL
76
41-140
m,p-Xylenes
0.0858
0.011
mg/kg dry
0.1056
BRL
81
36-148
Methyl Butyl Ketone (2-Hexanone)
0.0517
0.053
mg/kg dry
0.05279
BRL
98
30-147
Methyl Ethyl Ketone (2-Butanone)
0.0574
0.11
mg/kg dry
0.05279
BRL
109
24-160
Methyl Isobutyl Ketone
0.0548
0.053
mg/kg dry
0.05279
BRL
104
25-163
Methylene Chloride
0.0447
0.011
mg/kg dry
0.05279
BRL
85
53-144
Methyl-tert-Butyl Ether
0.0501
0.011
mg/kg dry
0.05279
BRL
95
49-135
Naphthalene
0.0482
0.011
mg/kg dry
0.05279
BRL
91
32-127
n-Butylbenzene
0.0363
0.0053
mg/kg dry
0.05279
BRL
69
23-148
n-Propylbenzene
0.0368
0.0053
mg/kg dry
0.05279
BRL
70
35-144
o-Xylene
0.0447
0.0053
mg/kg dry
0.05279
BRL
85
43-143
sec-Butylbenzene
0.0387
0.0053
mg/kg dry
0.05279
BRL
73
34-144
Styrene
0.0462
0.0053
mg/kg dry
0.05279
BRL
88
42-132
tert-Butyl benzene
0.0405
0.0053
mg/kg dry
0.05279
BRL
77
36-150
Tetrachloroethylene
0.0518
0.0053
mg/kg dry
0.05279
BRL
98
47-142
Toluene
0.0480
0.0053
mg/kg dry
0.05279
BRL
91
57-135
trans- 1,2-Dichloroethylene
0.0448
0.0053
mg/kg dry
0.05279
BRL
85
58-141
trans- 1,3-Dichloropropylene
0.0477
0.0053
mg/kg dry
0.05279
BRL
90
41-124
Trichloroethylene
0.0495
0.0053
mg/kg dry
0.05279
BRL
94
38-164
Trichlorofluoromethane
0.0392
0.0053
mg/kg dry
0.05279
BRL
74
30-157
Vinyl acetate
0.0492
0.026
mg/kg dry
0.05279
BRL
93
61-154
Vinyl chloride
0.0454
0.0053
mg/kg dry
0.05279
BRL
86
40-156
Xylenes, total
0.130
0.016
mg/kg dry
0.1584
BRL
82
36-148
Surrogate:4-Bromofluorobenzene
51.1
ug/L
50.00
102
70-130
Surrogate: Dibromofluoromethane
49.7
ug/L
50.00
99
84-123
Surrogate: Toluene-d8
45.0
ug/L
50.00
90
76-129
J
J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 37

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9C0139-MSD1)
Source: 9030103-01
Prepared: 03/07/19 Analyzed: 03/08/19
1,1,1,2-Tetrachloroethane
0.0495
0.0053
mg/kg dry
0.05343
BRL
93
60-120
4
15
1,1,1-Trichloroethane
0.0476
0.0053
mg/kg dry
0.05343
BRL
89
52-139
5
21
1,1,2,2-Tetrachloroethane
0.0408
0.0053
mg/kg dry
0.05343
BRL
76
39-135
0.4
22
1,1,2-Trichloroethane
0.0460
0.0053
mg/kg dry
0.05343
BRL
86
44-140
2
21
1,1-Dichloroethane
0.0474
0.0053
mg/kg dry
0.05343
BRL
89
59-137
4
21
1,1-Dichloroethylene
0.0473
0.0053
mg/kg dry
0.05343
BRL
88
54-162
15
22
1, 1 -Dichloropropylene
0.0487
0.0053
mg/kg dry
0.05343
BRL
91
55-137
5
19
1,2,3-Trichlorobenzene
0.0444
0.0053
mg/kg dry
0.05343
BRL
83
34-120
4
41
1,2,3-Trichloropropane
0.0429
0.0053
mg/kg dry
0.05343
BRL
80
45-139
0.05
25
1,2,4-Trichlorobenzene
0.0416
0.0053
mg/kg dry
0.05343
BRL
78
35-116
2
62
1,2,4-Trimethylbenzene
0.0406
0.0053
mg/kg dry
0.05343
BRL
76
38-142
3
24
1,2-Dibromoethane
0.0479
0.0053
mg/kg dry
0.05343
BRL
90
49-132
3
15
1,2-Dichlorobenzene
0.0398
0.0053
mg/kg dry
0.05343
BRL
74
42-130
3
21
1,2-Dichloroethane
0.0437
0.0053
mg/kg dry
0.05343
BRL
82
51-131
2
13
1,2-Dichloropropane
0.0489
0.0053
mg/kg dry
0.05343
BRL
91
55-138
2
16
1,3,5-Trimethylbenzene
0.0401
0.0053
mg/kg dry
0.05343
BRL
75
44-140
3
29
1,3-Dichlorobenzene
0.0394
0.0053
mg/kg dry
0.05343
BRL
74
41-129
2
24
1,3-Dichloropropane
0.0443
0.0053
mg/kg dry
0.05343
BRL
83
53-129
1
15
1,4-Dichlorobenzene
0.0389
0.0053
mg/kg dry
0.05343
BRL
73
44-134
1
21
2,2-Dichloropropane
0.0453
0.0053
mg/kg dry
0.05343
BRL
85
30-147
4
20
2-Chlorotoluene
0.0376
0.0053
mg/kg dry
0.05343
BRL
70
46-132
4
29
4-Chlorotoluene
0.0371
0.0053
mg/kg dry
0.05343
BRL
69
44-135
2
23
4-Isopropyltoluene
0.0405
0.0053
mg/kg dry
0.05343
BRL
76
32-144
3
22
Acetone
0.104
0.053
mg/kg dry
0.1069
BRL
97
34-143
7
49
Benzene
0.0485
0.0032
mg/kg dry
0.05343
BRL
91
60-135
4
20
Bromobenzene
0.0365
0.0053
mg/kg dry
0.05343
BRL
68
45-135
2
25
Bromochloromethane
0.0520
0.0053
mg/kg dry
0.05343
BRL
97
55-136
0.8
18
Bromodichloromethane
0.0459
0.0053
mg/kg dry
0.05343
BRL
86
55-127
3
17
Bromoform
0.0483
0.0053
mg/kg dry
0.05343
BRL
90
40-136
2
35
Bromomethane
0.0366
0.011
mg/kg dry
0.05343
BRL
69
30-137
10
30
Carbon Tetrachloride
0.0485
0.0053
mg/kg dry
0.05343
BRL
91
48-153
7
23
Chlorobenzene
0.0444
0.0053
mg/kg dry
0.05343
BRL
83
57-125
4
14
Chloroethane
0.0426
0.011
mg/kg dry
0.05343
BRL
80
16-177
3
47
Chloroform
0.0467
0.0053
mg/kg dry
0.05343
BRL
87
56-137
4
18
Chloromethane
0.0527
0.0053
mg/kg dry
0.05343
BRL
99
40-145
6
26
cis-1,2-Dichloroethylene
0.0477
0.0053
mg/kg dry
0.05343
BRL
89
58-140
3
28
cis-1,3-Dichloropropylene
0.0490
0.0053
mg/kg dry
0.05343
BRL
92
42-135
1
32
Dibromochloromethane
0.0455
0.0053
mg/kg dry
0.05343
BRL
85
49-127
4
24
Dichlorodifluoromethane
0.0488
0.0053
mg/kg dry
0.05343
BRL
91
25-151
7
37
Ethylbenzene
0.0451
0.0053
mg/kg dry
0.05343
BRL
84
44-144
5
19
Isopropyl Ether
0.0475
0.0053
mg/kg dry
0.05343
BRL
89
51-155
2
13
Isopropylbenzene (Cumene)
0.0419
0.0053
mg/kg dry
0.05343
BRL
78
41-140
4
27
m,p-Xylenes
0.0899
0.011
mg/kg dry
0.1069
BRL
84
36-148
5
20
Methyl Butyl Ketone (2-Hexanone)
0.0509
0.053
mg/kg dry
0.05343
BRL
95
30-147
2
42
Methyl Ethyl Ketone (2-Butanone)
0.0533
0.11
mg/kg dry
0.05343
BRL
100
24-160
7
42
Methyl Isobutyl Ketone
0.0533
0.053
mg/kg dry
0.05343
BRL
100
25-163
3
44
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 37

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO139 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9C0139-MSD1)
Source: 9030103-01
Prepared: 03/07/19 Analyzed: 03/08/19
Methylene Chloride
0.0459
0.011
mg/kg dry
0.05343
BRL
86
53-144
3
14
Methyl-tert-Butyl Ether
0.0493
0.011
mg/kg dry
0.05343
BRL
92
49-135
2
22
Naphthalene
0.0475
0.011
mg/kg dry
0.05343
BRL
89
32-127
2
44
n-Butylbenzene
0.0371
0.0053
mg/kg dry
0.05343
BRL
69
23-148
2
39
n-Propylbenzene
0.0382
0.0053
mg/kg dry
0.05343
BRL
72
35-144
4
27
o-Xylene
0.0464
0.0053
mg/kg dry
0.05343
BRL
87
43-143
4
17
sec-Butylbenzene
0.0405
0.0053
mg/kg dry
0.05343
BRL
76
34-144
4
28
Styrene
0.0477
0.0053
mg/kg dry
0.05343
BRL
89
42-132
3
28
tert-Butylbenzene
0.0428
0.0053
mg/kg dry
0.05343
BRL
80
36-150
6
29
Tetrachloroethylene
0.0532
0.0053
mg/kg dry
0.05343
BRL
100
47-142
3
26
Toluene
0.0497
0.0053
mg/kg dry
0.05343
BRL
93
57-135
3
22
trans-1,2-Dichloroethylene
0.0463
0.0053
mg/kg dry
0.05343
BRL
87
58-141
3
18
trans- 1,3-Dichloropropylene
0.0482
0.0053
mg/kg dry
0.05343
BRL
90
41-124
1
20
Trichloroethylene
0.0513
0.0053
mg/kg dry
0.05343
BRL
96
38-164
4
18
Trichlorofluoromethane
0.0414
0.0053
mg/kg dry
0.05343
BRL
77
30-157
5
27
Vinyl acetate
0.0546
0.027
mg/kg dry
0.05343
BRL
102
61-154
10
35
Vinyl chloride
0.0470
0.0053
mg/kg dry
0.05343
BRL
88
40-156
3
35
Xylenes, total
0.136
0.016
mg/kg dry
0.1603
BRL
85
36-148
4
20
Surrogate:4-Bromofluorobenzene
50.2
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
48.5
ug/L
50.00
97
84-123
Surrogate: Toluene-d8
45.1
ug/L
50.00
90
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 37

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030103
Attn: Chris Orrell Time Submitted: 3/6/2019 4:00:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9CO132 - 3546
Blank (P9C0132-BLK1)
Prepared: 03/08/19 Analyzed: 03/11/19
1,2,4-Trichlorobenzene
BRL
0.33
mg/kg wet
1,2-Dichlorobenzene
BRL
0.33
mg/kg wet
1,3-Dichlorobenzene
BRL
0.33
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
1-Methyl naphthalene
BRL
0.33
mg/kg wet
2,4,5-Trichlorophenol
BRL
0.33
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.33
mg/kg wet
2,4-Dichlorophenol
BRL
0.33
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
0.33
mg/kg wet
2,4-Dinitrotoluene
BRL
0.33
mg/kg wet
2,6-Dinitrotoluene
BRL
0.33
mg/kg wet
2-Chloronaphthalene
BRL
0.33
mg/kg wet
2-Chlorophenol
BRL
0.33
mg/kg wet
2-Methyl naphthalene
BRL
0.33
mg/kg wet
2-Methylphenol
BRL
0.33
mg/kg wet
2-Nitrophenol
BRL
0.33
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.33
mg/kg wet
3/4-Methyl phenol
BRL
0.33
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
0.33
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.33
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Nitrophenol
BRL
0.33
mg/kg wet
Acenaphthene
BRL
0.33
mg/kg wet
Acenaphthylene
BRL
0.33
mg/kg wet
Anthracene
BRL
0.33
mg/kg wet
Azobenzene
BRL
0.33
mg/kg wet
Benzo(a)anthracene
BRL
0.33
mg/kg wet
Benzo(a)pyrene
BRL
0.33
mg/kg wet
Benzo(b)fluoranthene
BRL
0.33
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.33
mg/kg wet
Benzo(k)fluoranthene
BRL
0.33
mg/kg wet
Benzoic Acid
BRL
0.33
mg/kg wet
Benzyl alcohol
BRL
0.33
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.33
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.33
mg/kg wet
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.33
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.33
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.33
mg/kg wet
Dibenzofuran
BRL
0.33
mg/kg wet
Diethyl phthalate
BRL
0.33
mg/kg wet
Dimethyl phthalate
BRL
0.33
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 37

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO132 - 3546
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9C0132-BLK1)
Prepared: 03/08/19 Analyzed: 03/11/19
Di-n-butyl phthalate
BRL
0.33
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.33
mg/kg wet
Fluorene
BRL
0.33
mg/kg wet
Hexachlorobenzene
BRL
0.33
mg/kg wet
Hexachlorobutadiene
BRL
0.33
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.33
mg/kg wet
Hexachloroethane
BRL
0.33
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.33
mg/kg wet
Isophorone
BRL
0.33
mg/kg wet
Naphthalene
BRL
0.33
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.33
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.33
mg/kg wet
Pentachlorophenol
BRL
0.33
mg/kg wet
Phenanthrene
BRL
0.33
mg/kg wet
Phenol
BRL
0.33
mg/kg wet
Pyrene
BRL
0.33
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
3.16
mg/kg wet
3.333
95
39-132
Surrogate: 2-Fluorobiphenyl
1.55
mg/kg wet
1.667
93
44-115
Surrogate: 2-Fluorophenol
3.09
mg/kg wet
3.333
93
35-115
Surrogate: Nitrobenzene-d5
1.44
mg/kg wet
1.667
86
37-122
Surrogate: Phenol-d5
2.93
mg/kg wet
3.333
88
34-121
Surrogate: Terphenyl-d14
1.64
mg/kg wet
1.667
98
54-127
LCS (P9C0132-113SI)
Prepared: 03/08/19 Analyzed: 03/11/19
1,2,4-Trichlorobenzene
1.29
0.33
mg/kg wet
1.667
78
34-118
1,2-Dichlorobenzene
1.32
0.33
mg/kg wet
1.667
79
33-117
1,3-Dichlorobenzene
1.29
0.33
mg/kg wet
1.667
77
30-115
1,4-Dichlorobenzene
1.31
0.33
mg/kg wet
1.667
79
31-115
1-Methyl naphthalene
1.38
0.33
mg/kg wet
1.667
83
40-119
2,4,5-Trichlorophenol
1.56
0.33
mg/kg wet
1.667
93
62-124
2,4,6-Trichlorophenol
1.69
0.33
mg/kg wet
1.667
101
39-126
2,4-Dichlorophenol
1.38
0.33
mg/kg wet
1.667
83
40-122
2,4-Dimethylphenol
1.84
0.33
mg/kg wet
1.667
110
30-127
2,4-Dinitrophenol
0.996
0.33
mg/kg wet
1.667
60
27-129
2,4-Dinitrotoluene
1.64
0.33
mg/kg wet
1.667
98
48-126
2,6-Dinitrotoluene
1.69
0.33
mg/kg wet
1.667
101
46-124
2-Chloronaphthalene
1.57
0.33
mg/kg wet
1.667
94
41-114
2-Chlorophenol
1.57
0.33
mg/kg wet
1.667
94
34-121
2-Methyl naphthalene
1.35
0.33
mg/kg wet
1.667
81
38-122
2-Methylphenol
1.63
0.33
mg/kg wet
1.667
98
32-122
2-Nitrophenol
1.35
0.33
mg/kg wet
1.667
81
36-123
3,3'-Dichlorobenzidine
1.57
0.33
mg/kg wet
1.667
94
22-121
3/4-Methyl phenol
1.44
0.33
mg/kg wet
1.667
86
34-119
4,6-Dinitro-2-methylphenol
1.45
0.33
mg/kg wet
1.667
87
29-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 37

Level II QC Report
P R I S M Full -Service Analytical & 3/12/19
Environmental Solutions
LABORATOR,
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030103
Attn: Chris Orrell Time Submitted: 3/6/2019 4:00:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting
Spike
Source
%REC RPD
Analyte
Result
Limit
Units
Level
Result %REC
Limits RPD Limit Notes
Batch P9CO132 - 3546
LCS (P9C0132-BSI)
Prepared:
03/08/19 Analyzed:
03/11/19
4-Bromophenyl phenyl ether
1.59
0.33
mg/kg wet
1.667
95
46-124
4-Chloro-3-methylphenol
1.49
0.33
mg/kg wet
1.667
90
45-122
4-Chloroaniline
1.35
0.33
mg/kg wet
1.667
81
17-106
4-Chlorophenyl phenyl ether
1.66
0.33
mg/kg wet
1.667
100
45-121
4-Nitrophenol
1.60
0.33
mg/kg wet
1.667
96
30-132
Acenaphthene
1.64
0.33
mg/kg wet
1.667
98
40-123
Acenaphthylene
1.63
0.33
mg/kg wet
1.667
98
32-132
Anthracene
1.77
0.33
mg/kg wet
1.667
106
47-123
Azobenzene
1.61
0.33
mg/kg wet
1.667
97
39-125
Benzo(a)anthracene
1.68
0.33
mg/kg wet
1.667
100
49-126
Benzo(a)pyrene
1.59
0.33
mg/kg wet
1.667
95
45-129
Benzo(b)fluoranthene
1.57
0.33
mg/kg wet
1.667
94
45-132
Benzo(g,h,i)perylene
1.58
0.33
mg/kg wet
1.667
95
43-134
Benzo(k)fluoranthene
1.60
0.33
mg/kg wet
1.667
96
47-132
Benzoic Acid
BRL
0.33
mg/kg wet
1.667
10-83 L
Benzyl alcohol
1.54
0.33
mg/kg wet
1.667
93
29-122
bis(2-Chloroethoxy)methane
1.37
0.33
mg/kg wet
1.667
82
36-121
Bis(2-Chloroethyl)ether
1.40
0.33
mg/kg wet
1.667
84
31-120
Bis(2-chloroisopropyl)ether
1.41
0.33
mg/kg wet
1.667
84
33-131
Bis(2-Ethylhexyl)phthalate
1.73
0.33
mg/kg wet
1.667
104
51-133
Butyl benzyl phthalate
1.68
0.33
mg/kg wet
1.667
101
48-132
Chrysene
1.66
0.33
mg/kg wet
1.667
100
50-124
Dibenzo(a,h)anthracene
1.19
0.33
mg/kg wet
1.667
71
45-134
Dibenzofuran
1.59
0.33
mg/kg wet
1.667
95
44-120
Diethyl phthalate
1.72
0.33
mg/kg wet
1.667
103
50-124
Dimethyl phthalate
1.67
0.33
mg/kg wet
1.667
100
48-124
Di-n-butyl phthalate
1.74
0.33
mg/kg wet
1.667
104
51-128
Di-n-octyl phthalate
1.62
0.33
mg/kg wet
1.667
97
45-140
Fluoranthene
1.68
0.33
mg/kg wet
1.667
101
50-127
Fluorene
1.73
0.33
mg/kg wet
1.667
104
43-125
Hexachlorobenzene
1.56
0.33
mg/kg wet
1.667
94
45-122
Hexachlorobutadiene
1.35
0.33
mg/kg wet
1.667
81
32-123
Hexachlorocyclopentadiene
1.62
0.33
mg/kg wet
1.667
97
32-117
Hexachloroethane
1.28
0.33
mg/kg wet
1.667
77
28-117
Indeno(1,2,3-cd)pyrene
1.85
0.33
mg/kg wet
1.667
ill
45-133
Isophorone
1.38
0.33
mg/kg wet
1.667
82
30-122
Naphthalene
1.31
0.33
mg/kg wet
1.667
78
35-123
Nitrobenzene
1.26
0.33
mg/kg wet
1.667
76
34-122
N-Nitroso-di-n-propylamine
1.48
0.33
mg/kg wet
1.667
89
36-120
N-Nitrosodiphenylamine
1.90
0.33
mg/kg wet
1.667
114
38-127
Pentachlorophenol
1.08
0.33
mg/kg wet
1.667
65
25-133
Phenanthrene
1.70
0.33
mg/kg wet
1.667
102
50-121
Phenol
1.71
0.33
mg/kg wet
1.667
103
34-121
Pyrene
1.68
0.33
mg/kg wet
1.667
101
47-127
Pyridine
1.02
0.33
mg/kg wet
1.667
61
10-60 L1
Surrogate: 2,4,6-Tribromophenol
3.19
mg/kg wet
3.333
96
39-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 37

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO132 - 3546
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9C0132-BS1)
Prepared: 03/08/19 Analyzed: 03/11/19
Surrogate: 2-Fluorobiphenyl
1.63
mg/kg wet
1.667
98
44-115
Surrogate: 2-Fluorophenol
3.19
mg/kg wet
3.333
96
35-115
Surrogate: Nitrobenzene-d5
1.30
mg/kg wet
1.667
78
37-122
Surrogate: Phenol-d5
3.04
mg/kg wet
3.333
91
34-121
Surrogate: Terphenyl-d14
1.68
mg/kg wet
1.667
101
54-127
LCS Dup (M0132-13SD1)
Prepared: 03/08/19 Analyzed: 03/11/19
1,2,4-Trichlorobenzene
1.23
0.33
mg/kg wet
1.667
74
34-118
5
20
1,2-Dichlorobenzene
1.28
0.33
mg/kg wet
1.667
77
33-117
3
20
1,3-Dichlorobenzene
1.25
0.33
mg/kg wet
1.667
75
30-115
3
20
1,4-Dichlorobenzene
1.27
0.33
mg/kg wet
1.667
76
31-115
3
20
1-Methyl naphthalene
1.35
0.33
mg/kg wet
1.667
81
40-119
2
20
2,4,5-Trichlorophenol
1.56
0.33
mg/kg wet
1.667
94
62-124
0.1
20
2,4,6-Trichlorophenol
1.65
0.33
mg/kg wet
1.667
99
39-126
2
20
2,4-Dichlorophenol
1.33
0.33
mg/kg wet
1.667
80
40-122
4
20
2,4-Dimethylphenol
1.81
0.33
mg/kg wet
1.667
109
30-127
2
20
2,4-Dinitrophenol
1.05
0.33
mg/kg wet
1.667
63
27-129
5
20
2,4-Dinitrotoluene
1.62
0.33
mg/kg wet
1.667
97
48-126
1
20
2,6-Dinitrotoluene
1.63
0.33
mg/kg wet
1.667
98
46-124
4
20
2-Chloronaphthalene
1.55
0.33
mg/kg wet
1.667
93
41-114
1
20
2-Chlorophenol
1.53
0.33
mg/kg wet
1.667
92
34-121
2
20
2-Methyl naphthalene
1.30
0.33
mg/kg wet
1.667
78
38-122
4
20
2-Methylphenol
1.55
0.33
mg/kg wet
1.667
93
32-122
5
20
2-Nitrophenol
1.31
0.33
mg/kg wet
1.667
78
36-123
3
20
3,3'-Dichlorobenzidine
1.56
0.33
mg/kg wet
1.667
94
22-121
0.4
20
3/4-Methyl phenol
1.40
0.33
mg/kg wet
1.667
84
34-119
3
20
4,6-Dinitro-2-methylphenol
1.47
0.33
mg/kg wet
1.667
88
29-132
2
20
4-Bromophenyl phenyl ether
1.57
0.33
mg/kg wet
1.667
94
46-124
1
20
4-Chloro-3-methylphenol
1.41
0.33
mg/kg wet
1.667
85
45-122
5
20
4-Chloroaniline
1.31
0.33
mg/kg wet
1.667
79
17-106
3
20
4-Chlorophenyl phenyl ether
1.61
0.33
mg/kg wet
1.667
97
45-121
3
20
4-Nitrophenol
1.55
0.33
mg/kg wet
1.667
93
30-132
3
20
Acenaphthene
1.64
0.33
mg/kg wet
1.667
98
40-123
0.02
20
Acenaphthylene
1.59
0.33
mg/kg wet
1.667
96
32-132
2
20
Anthracene
1.70
0.33
mg/kg wet
1.667
102
47-123
5
20
Azobenzene
1.58
0.33
mg/kg wet
1.667
95
39-125
2
20
Benzo(a)anthracene
1.64
0.33
mg/kg wet
1.667
99
49-126
2
20
Benzo(a)pyrene
1.56
0.33
mg/kg wet
1.667
94
45-129
2
20
Benzo(b)fluoranthene
1.53
0.33
mg/kg wet
1.667
92
45-132
3
20
Benzo(g,h,i)perylene
1.55
0.33
mg/kg wet
1.667
93
43-134
2
20
Benzo(k)fluoranthene
1.54
0.33
mg/kg wet
1.667
92
47-132
4
20
Benzoic Acid
BRL
0.33
mg/kg wet
1.667
10-83
20 L
Benzyl alcohol
1.50
0.33
mg/kg wet
1.667
90
29-122
3
20
bis(2-Chloroethoxy)methane
1.32
0.33
mg/kg wet
1.667
79
36-121
4
20
Bis(2-Chloroethyl)ether
1.38
0.33
mg/kg wet
1.667
83
31-120
2
20
Bis(2-chloroisopropyl)ether
1.32
0.33
mg/kg wet
1.667
79
33-131
6
20
Bis(2-Ethylhexyl)phthalate
1.69
0.33
mg/kg wet
1.667
101
51-133
2
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030103
Attn: Chris Orrell Time Submitted: 3/6/2019 4:00:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9CO132 - 3546
LCS Dup (P9C0132-BSD1)
Prepared: 03/08/19 Analyzed: 03/11/19
Butyl benzyl phthalate
1.63
0.33
mg/kg wet
1.667
98
48-132
3
20
Chrysene
1.64
0.33
mg/kg wet
1.667
98
50-124
2
20
Dibenzo(a,h)anthracene
1.13
0.33
mg/kg wet
1.667
68
45-134
6
20
Dibenzofuran
1.58
0.33
mg/kg wet
1.667
95
44-120
0.4
20
Diethyl phthalate
1.67
0.33
mg/kg wet
1.667
100
50-124
3
20
Dimethyl phthalate
1.65
0.33
mg/kg wet
1.667
99
48-124
1
20
Di-n-butyl phthalate
1.69
0.33
mg/kg wet
1.667
101
51-128
3
20
Di-n-octyl phthalate
1.57
0.33
mg/kg wet
1.667
94
45-140
3
20
Fluoranthene
1.64
0.33
mg/kg wet
1.667
98
50-127
2
20
Fluorene
1.68
0.33
mg/kg wet
1.667
101
43-125
3
20
Hexachlorobenzene
1.55
0.33
mg/kg wet
1.667
93
45-122
0.9
20
Hexachlorobutadiene
1.32
0.33
mg/kg wet
1.667
79
32-123
3
20
Hexachlorocyclopentadiene
1.55
0.33
mg/kg wet
1.667
93
32-117
4
20
Hexachloroethane
1.24
0.33
mg/kg wet
1.667
74
28-117
4
20
Indeno(1,2,3-cd)pyrene
1.80
0.33
mg/kg wet
1.667
108
45-133
3
20
Isophorone
1.30
0.33
mg/kg wet
1.667
78
30-122
5
20
Naphthalene
1.27
0.33
mg/kg wet
1.667
76
35-123
3
20
Nitrobenzene
1.24
0.33
mg/kg wet
1.667
74
34-122
2
20
N-Nitroso-di-n-propylamine
1.42
0.33
mg/kg wet
1.667
85
36-120
4
20
N-Nitrosodiphenylamine
1.87
0.33
mg/kg wet
1.667
112
38-127
2
20
Pentachlorophenol
1.05
0.33
mg/kg wet
1.667
63
25-133
2
20
Phenanthrene
1.67
0.33
mg/kg wet
1.667
100
50-121
2
20
Phenol
1.61
0.33
mg/kg wet
1.667
96
34-121
7
20
Pyrene
1.64
0.33
mg/kg wet
1.667
98
47-127
2
20
Pyridine
0.945
0.33
mg/kg wet
1.667
57
10-60
8
20
Surrogate: 2,4,6-Tribromophenol
3.12
mg/kg wet
3.333
94
39-132
Surrogate: 2-Fluorobiphenyl
1.57
mg/kg wet
1.667
94
44-115
Surrogate: 2-Fluorophenol
3.06
mg/kg wet
3.333
92
35-115
Surrogate: Nitrobenzene-d5
1.24
mg/kg wet
1.667
74
37-122
Surrogate: Phenol-d5
2.94
mg/kg wet
3.333
88
34-121
Surrogate: Terphenyl-d14
1.60
mg/kg wet
1.667
96
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Page 32 of 37

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030103
Attn: Chris Orrell Time Submitted: 3/6/2019 4:00:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9CO146 - MADEP VPH (S)
Blank (P9C0146-BLK1)
Prepared & Analyzed: 03/11/19
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl2 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
11800
ug/L
10000 118
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11400
ug/L
10000 114
70-130
LCS (P9C0146-13SI)
Prepared & Analyzed: 03/11/19
C5-C8 Aliphatics
24.5
5.0
mg/kg wet
32.00 77
70-130
C9-Cl0 Aromatics
12.3
5.0
mg/kg wet
10.67 115
70-130
C9-Cl2 Aliphatic
33.3
5.0
mg/kg wet
32.00 104
70-130
Surrogate: 2,5-Dibromotoluene (PID)
11300
ug/L
10000 113
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11000
ug/L
10000 110
70-130
LCS Dup (P9C0146-BSD1)
Prepared & Analyzed: 03/11/19
C5-C8 Aliphatics
24.2
5.0
mg/kg wet
32.00 76
70-130 1 50
C9-Cl0 Aromatics
11.9
5.0
mg/kg wet
10.67 112
70-130 3 50
C9-Cl2 Aliphatic
32.3
5.0
mg/kg wet
32.00 101
70-130 3 50
Surrogate: 2,5-Dibromotoluene (PID)
10800
ug/L
10000 108
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10600
ug/L
10000 106
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 33 of 37

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Analyte
Batch P9C0135 - 3546
Reporting
Result Limit Units
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9C0135-BLK1)
Prepared: 03/08/19 Analyzed: 03/11/19
C9-Cl8 Aliphatics
BRL
25
mg/kg wet
C19-C36 Aliphatics
BRL
25
mg/kg wet
C11-C22 Aromatics
BRL
10
mg/kg wet
Surrogate: 1-Chlorooctadecane
1.53
mg/kg wet
2.000
77
40-140
Surrogate: o-Terphenyl
1.75
mg/kg wet
2.000
88
40-140
Surrogate: 2-Fluorobiphenyl
3.96
mg/kg wet
4.000
99
40-140
Surrogate: 2-Bromonaphthalene
3.55
mg/kg wet
4.000
89
40-140
LCS (P9C0135-BSI)
Prepared: 03/08/19
Analyzed: 03/11/19
C9-Cl8 Aliphatics
46.0
25
mg/kg wet
60.00
77
40-140
C19-C36 Aliphatics
84.9
25
mg/kg wet
80.00
106
40-140
C11-C22 Aromatics
178
10
mg/kg wet
170.0
105
40-140
Surrogate: 1-Chlorooctadecane
1.69
mg/kg wet
2.000
84
40-140
Surrogate: o-Terphenyl
2.00
mg/kg wet
2.000
100
40-140
Surrogate: 2-Fluorobiphenyl
4.11
mg/kg wet
4.000
103
40-140
Surrogate: 2-Bromonaphthalene
3.51
mg/kg wet
4.000
88
40-140
LCS Dup (P9C0135-BSD1)
Prepared: 03/08/19
Analyzed: 03/11/19
C9-Cl8 Aliphatics
48.9
25
mg/kg wet
60.00
81
40-140
C19-C36 Aliphatics
93.4
25
mg/kg wet
80.00
117
40-140
C11-C22 Aromatics
191
10
mg/kg wet
170.0
113
40-140
Surrogate: 1-Chlorooctadecane
1.84
mg/kg wet
2.000
92
40-140
Surrogate: o-Terphenyl
1.92
mg/kg wet
2.000
96
40-140
Surrogate: 2-Fluorobiphenyl
4.08
mg/kg wet
4.000
102
40-140
Surrogate: 2-Bromonaphthalene
3.45
mg/kg wet
4.000
86
40-140
Matrix Spike (P9C0135-MS1)
Source: 9030103-02
Prepared: 03/08/19
Analyzed: 03/11/19
C9-Cl8 Aliphatics
92.9
28
mg/kg dry
67.37 5.21
130
40-140
C19-C36 Aliphatics
102
28
mg/kg dry
89.83 BRL
114
40-140
C11-C22 Aromatics
244
11
mg/kg dry
190.9 BRL
128
40-140
Surrogate: 1-Chlorooctadecane
2.17
mg/kg dry
2.246
96
40-140
Surrogate: o-Terphenyl
2.29
mg/kg dry
2.246
102
40-140
Surrogate: 2-Fluorobiphenyl
4.78
mg/kg dry
4.491
107
40-140
Surrogate: 2-Bromonaphthalene
4.42
mg/kg dry
4.491
98
40-140
6 50
10 50
7 50
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 34 of 37

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/12/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Reporting
Analyte Result Limit Units
Batch P9C0135 - 3546
Prism Work Order: 9030103
Time Submitted: 3/6/2019 4:00:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9C0135-MSD1)
Source: 9030103-02
Prepared: 03/08/19 Analyzed: 03/11/19
C9-Cl8 Aliphatics
61.0
28 mg/kg dry
67.24 5.21
83
40-140 41 50
C19-C36 Aliphatics
95.8
28 mg/kg dry
89.65 BRL
107
40-140 6 50
C11-C22 Aromatics
211
11 mg/kg dry
190.5 BRL
ill
40-140 15 50
Surrogate: 1-Chlorooctadecane
1.87
mg/kg dry
2.241
83
40-140
Surrogate: o-Terphenyl
2.21
mg/kg dry
2.241
99
40-140
Surrogate: 2-Fluorobiphenyl
4.33
mg/kg dry
4.482
97
40-140
Surrogate: 2-Bromonaphthalene
3.94
mg/kg dry
4.482
88
40-140
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 35 of 37

Level II QC Report
P R I S M Full -Service Analytical & 3/12/19
Environmental Solutions
LABORATOR,
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030103
Attn: Chris Orrell Time Submitted: 3/6/2019 4:00:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9CO167 - NO PREP
Duplicate (P9C0167-DUP1)
Source: 9030103-02 Prepared: 03/11/19 Analyzed: 03/12/19
% Solids
88.7
0.100 % by Weight
89.0 0.3 20
Sample Extraction Data
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
9030103-01
P9C0135
10.06 g
2 mL
03/08/19 10:00
9030103-02
P9C0135
10.18 g
2 mL
03/08/19 10:00
9030103-03
P9C0135
10.24 g
2 mL
03/08/19 10:00
9030103-04
P9C0135
10.07 g
2 mL
03/08/19 10:00
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
9030103-01
P9C0132
30.05 g
1 mL
03/08/19 10:00
9030103-02
P9C0132
30.17 g
1 mL
03/08/19 10:00
9030103-03
P9C0132
30.09 g
1 mL
03/08/19 10:00
9030103-04
P9C0132
30.02 g
1 mL
03/08/19 10:00
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
9030103-01 P9C0139
8.29 g
5 mL
03/07/19 11:28
9030103-02 P9C0139
5.7 g
5 mL
03/07/19 11:28
9030103-03 P9C0139
5.61 g
5 mL
03/07/19 11:28
9030103-04 P9C0139
3.66 g
5 mL
03/07/19 11:28
Prep Method: MADEP VPH (S)
Lab Number Batch
Initial
Final
Date/Time
9030103-01
P9C0146
3.98
g 16 mL
03/11/19
8:44
9030103-02
P9C0146
3.35
g 16 mL
03/11/19
8:44
9030103-03
P9C0146
4.77
g 16 mL
03/11/19
8:44
9030103-04
P9C0146
4.2
g 16 mL
03/11/19
8:44
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Client Company Name: t '
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Short Hold Analysis: (Yes) (No) UST Project: (Yes) (NO)
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QC Requirements
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PROPER CONTAINERS used++?22
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(SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
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MILITARY
(SOIL,
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SEE BELOW
NO. SIZE
f
ID NO.
l
1
2
Lto
>`
A_
-'
I
7`
r
c,3
Sampler's Signature lily(
Sampled By (Print Name) Affiliation �X�S
Upon relinquishing, this Chain of Custody is your authorization
for Prism to pp -teed with the analyses as requested above. Any changes must be
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submitted in writing to the Prism Project Manager. There will be charges for ny changes after analyses have been initialized.
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❑NC El ` ❑NC ❑SC ❑NC❑SCI O❑SC�❑NC ❑SC❑NC ❑SC
I
rr n rl
n n ❑ ❑ ❑ ❑
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Organics Analysis (Zero Head Space) ORIGINAL

Case Narrative
PRISM Full -Service Analytical &
Environmental Solutions
`,. LABORATORIES, INC.
ECS Carolinas, LLP (Charlotte)
Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
NC Certification No. 402
NC Drinking Water Cent No. 37735
SC Certification No. 99012
Project: W. Morehead
Lab Submittal Date: 03/14/2019
Prism Work Order: 9030248
03/18/2019
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a,j
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
Reviewed By Terri W. Cole For Angela D. Overcash
Project Manager
A Surrogate recovery is below range.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
M Matrix spike outside of the control limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 28

/rP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES INC.
Sample Receipt Summary
03/18/2019
Prism Work Order: 9030248
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
NW 9030248-01 Solid 03/14/19 9:50 03/14/19 12:25
B 9030248-02 Solid 03/14/19 9:55 03/14/19 12:25
Samples were received in good condition at 3.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 28

Summary of Detections
Full -Service Analytical &
�P R I S M
Environmental Solutions
03/18/2019
LABORATORIES, INC.
Prism Work Order: 9030248
Prism ID Client ID
Parameter
Method Result Units
9030248-01 NW
C9-Cl8 Aliphatics
MADEP EPH 0.77 J mg/kg dry
9030248-02 B
C9-Cl8 Aliphatics
MADEP EPH 3.4 1 mg/kg dry
9030248-02 B
Benzoic Acid
8270D 0.22 1 mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 28

P R S M Laboratory Report
` Full -Service Analytical &
/ environmental Solutions 03/18/2019
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Client Sample ID: NW
Attn: Chris Orrell Prism Sample ID: 9030248-01
1812 Center Park Drive, Suite D Prism Work Order: 9030248
Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 03/14/19 09:50
Time Submitted: 03/14/19 12:25
Parameter
Result
Units
Report MDL
Dilution
Method Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics
0.77 J
mg/kg dry
27 0.17
1
MADEP EPH 3/15/19 16:04
BGB
P9CO262
C19-C36 Aliphatics
BRL
mg/kg dry
27 3.2
1
MADEP EPH 3/15/19 16:04
BGB
P9CO262
C11-C22 Aromatics
BRL
mg/kg dry
11 2.0
1
MADEP EPH 3/15/19 16:04
BGB
P9CO262
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
89 %
40-140
o-Terphenyl
97 %
40-140
2-Fluorobiphenyl
97 %
40-140
2-Bromonaphthalene
90 %
40-140
General Chemistry Parameters
% Solids
91.8
% by
0.100
0.100
1
'SM2540 G
3118/19 9:35
KBS
P9CO281
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.36
0.056
1
8270D
3/15/19 15:03
JMV
P9CO261
1,2-Dichlorobenzene
BRL
mg/kg dry
0.36
0.054
1
8270D
3/15/19 15:03
JMV
P9CO261
1,3-Dichlorobenzene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:03
JMV
P9CO261
1,4-Dichlorobenzene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/15/19 15:03
JMV
P9CO261
1-Methyl naphthalene
BRL
mg/kg dry
0.36
0.069
1
8270D
3/15/19 15:03
JMV
P9CO261
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.36
0.058
1
8270D
3/15/19 15:03
JMV
P9CO261
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.36
0.067
1
8270D
3/15/19 15:03
JMV
P9CO261
2,4-Dichlorophenol
BRL
mg/kg dry
0.36
0.069
1
8270D
3/15/19 15:03
JMV
P9CO261
2,4-Dimethylphenol
BRL
mg/kg dry
0.36
0.055
1
8270D
3/15/19 15:03
JMV
P9CO261
2,4-Dinitrophenol
BRL
mg/kg dry
0.36
0.050
1
8270D
3/15/19 15:03
JMV
P9CO261
2,4-Dinitrotoluene
BRL
mg/kg dry
0.36
0.044
1
8270D
3/15/19 15:03
JMV
P9CO261
2,6-Dinitrotoluene
BRL
mg/kg dry
0.36
0.048
1
8270D
3/15/19 15:03
JMV
P9CO261
2-Chloronaphthalene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/15/19 15:03
JMV
P9CO261
2-Chlorophenol
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:03
JMV
P9CO261
2-Methyl naphthalene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/15/19 15:03
JMV
P9CO261
2-Methylphenol
BRL
mg/kg dry
0.36
0.046
1
8270D
3/15/19 15:03
JMV
P9CO261
2-Nitrophenol
BRL
mg/kg dry
0.36
0.065
1
8270D
3/15/19 15:03
JMV
P9CO261
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.36
0.071
1
8270D
3/15/19 15:03
JMV
P9CO261
3/4-Methyl phenol
BRL
mg/kg dry
0.36
0.044
1
8270D
3/15/19 15:03
JMV
P9CO261
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.36
0.054
1
8270D
3/15/19 15:03
JMV
P9CO261
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.36
0.062
1
8270D
3/15/19 15:03
JMV
P9CO261
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.36
0.050
1
8270D
3/15/19 15:03
JMV
P9CO261
4-Chloroaniline
BRL
mg/kg dry
0.36
0.043
1
8270D
3/15/19 15:03
JMV
P9CO261
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
4-Nitrophenol
BRL
mg/kg dry
0.36
0.055
1
8270D
3/15/19 15:03
JMV
P9CO261
Acenaphthene
BRL
mg/kg dry
0.36
0.049
1
8270D
3/15/19 15:03
JMV
P9CO261
Acenaphthylene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/15/19 15:03
JMV
P9CO261
Anthracene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/15/19 15:03
JMV
P9CO261
Azobenzene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
Benzo(a)anthracene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 28

Laboratory Report
` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
03/18/2019
ECS Carolinas, LLP (Charlotte)
Project: W. Morehead
Client Sample ID: NW
Attn: Chris Orrell
Prism Sample ID: 9030248-01
1812 Center Park Drive, Suite D
Prism Work Order:
9030248
Charlotte, NC 28217
Sample Matrix: Solid
Time Collected:
03/14/19 09:50
Time Submitted:
03/14/19 12:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.36
0.039
1
8270D
3/15/19 15:03
JMV
P9CO261
Benzo(b)fluoranthene
BRL
mg/kg dry
0.36
0.042
1
8270D
3/15/19 15:03
JMV
P9CO261
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.36
0.039
1
8270D
3/15/19 15:03
JMV
P9CO261
Benzo(k)fluoranthene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
Benzoic Acid
BRL
mg/kg dry
0.36
0.030
1
8270D
3/15/19 15:03
JMV
P9CO261
Benzyl alcohol
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.36
0.062
1
8270D
3/15/19 15:03
JMV
P9CO261
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:03
JMV
P9CO261
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.36
0.061
1
8270D
3/15/19 15:03
JMV
P9CO261
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.36
0.053
1
8270D
3/15/19 15:03
JMV
P9CO261
Butyl benzyl phthalate
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:03
JMV
P9CO261
Chrysene
BRL
mg/kg dry
0.36
0.045
1
8270D
3/15/19 15:03
JMV
P9CO261
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.36
0.044
1
8270D
3/15/19 15:03
JMV
P9CO261
Dibenzofuran
BRL
mg/kg dry
0.36
0.055
1
8270D
3/15/19 15:03
JMV
P9CO261
Diethyl phthalate
BRL
mg/kg dry
0.36
0.049
1
8270D
3/15/19 15:03
JMV
P9CO261
Dimethyl phthalate
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
Di-n-butyl phthalate
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:03
JMV
P9CO261
Di-n-octyl phthalate
BRL
mg/kg dry
0.36
0.044
1
8270D
3/15/19 15:03
JMV
P9CO261
Fluoranthene
BRL
mg/kg dry
0.36
0.046
1
8270D
3/15/19 15:03
JMV
P9CO261
Fluorene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:03
JMV
P9CO261
Hexachlorobenzene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/15/19 15:03
JMV
P9CO261
Hexachlorobutadiene
BRL
mg/kg dry
0.36
0.064
1
8270D
3/15/19 15:03
JMV
P9CO261
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.36
0.064
1
8270D
3/15/19 15:03
JMV
P9CO261
Hexachloroethane
BRL
mg/kg dry
0.36
0.060
1
8270D
3/15/19 15:03
JMV
P9CO261
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.36
0.041
1
8270D
3/15/19 15:03
JMV
P9CO261
Isophorone
BRL
mg/kg dry
0.36
0.049
1
8270D
3/15/19 15:03
JMV
P9CO261
Naphthalene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/15/19 15:03
JMV
P9CO261
Nitrobenzene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:03
JMV
P9CO261
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.36
0.056
1
8270D
3/15/19 15:03
JMV
P9CO261
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.36
0.055
1
8270D
3/15/19 15:03
JMV
P9CO261
Pentachlorophenol
BRL
mg/kg dry
0.36
0.042
1
8270D
3/15/19 15:03
JMV
P9CO261
Phenanthrene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
Phenol
BRL
mg/kg dry
0.36
0.053
1
8270D
3/15/19 15:03
JMV
P9CO261
Pyrene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:03
JMV
P9CO261
Pyridine
BRL
mg/kg dry
0.36
0.063
1
8270D
3/15/19 15:03
JMV
P9CO261
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
59 %
39-132
2-Fluorobiphenyl
45 %
44-115
2-Fluorophenol
38 %
35-115
Nitrobenzene-d5
35 %
37-122
A
Phenol-d5
41 %
34-121
Terphenyl-d14
72 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 28

` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead
Sample Matrix: Solid
Laboratory Report
03/18/2019
Client Sample ID: NW
Prism Sample ID: 9030248-01
Prism Work Order: 9030248
Time Collected: 03/14/19 09:50
Time Submitted: 03/14/19 12:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0053
0.00044
1
8260B
3/14/19 23:47
JLB
P9CO277
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0053
0.00026
1
8260B
3/14/19 23:47
JLB
P9CO277
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0053
0.00036
1
8260B
3/14/19 23:47
JLB
P9CO277
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0053
0.00047
1
8260B
3/14/19 23:47
JLB
P9CO277
1,1-Dichloroethane
BRL
mg/kg dry
0.0053
0.00015
1
8260B
3/14/19 23:47
JLB
P9CO277
1,1-Dichloroethylene
BRL
mg/kg dry
0.0053
0.00023
1
8260B
3/14/19 23:47
JLB
P9CO277
1,1-Dichloropropylene
BRL
mg/kg dry
0.0053
0.00029
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0053
0.00030
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0053
0.00068
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0053
0.00040
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0053
0.00041
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2-Dibromoethane
BRL
mg/kg dry
0.0053
0.00021
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0053
0.00025
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2-Dichloroethane
BRL
mg/kg dry
0.0053
0.00032
1
8260B
3/14/19 23:47
JLB
P9CO277
1,2-Dichloropropane
BRL
mg/kg dry
0.0053
0.00033
1
8260B
3/14/19 23:47
JLB
P9CO277
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0053
0.00040
1
8260B
3/14/19 23:47
JLB
P9CO277
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0053
0.00035
1
8260B
3/14/19 23:47
JLB
P9CO277
1,3-Dichloropropane
BRL
mg/kg dry
0.0053
0.00027
1
8260B
3/14/19 23:47
JLB
P9CO277
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0053
0.00021
1
8260B
3/14/19 23:47
JLB
P9CO277
2,2-Dichloropropane
BRL
mg/kg dry
0.0053
0.00025
1
8260B
3/14/19 23:47
JLB
P9CO277
2-Chlorotoluene
BRL
mg/kg dry
0.0053
0.00027
1
8260B
3/14/19 23:47
JLB
P9CO277
4-Chlorotoluene
BRL
mg/kg dry
0.0053
0.00032
1
8260B
3/14/19 23:47
JLB
P9CO277
4-Isopropyltoluene
BRL
mg/kg dry
0.0053
0.00026
1
8260B
3/14/19 23:47
JLB
P9CO277
Acetone
BRL
mg/kg dry
0.053
0.0013
1
8260B
3/14/19 23:47
JLB
P9CO277
Benzene
BRL
mg/kg dry
0.0032
0.00031
1
8260B
3/14/19 23:47
JLB
P9CO277
Bromobenzene
BRL
mg/kg dry
0.0053
0.00044
1
8260B
3/14/19 23:47
JLB
P9CO277
Bromochloromethane
BRL
mg/kg dry
0.0053
0.00029
1
8260B
3/14/19 23:47
JLB
P9CO277
Bromodichloromethane
BRL
mg/kg dry
0.0053
0.00030
1
8260B
3/14/19 23:47
JLB
P9CO277
Bromoform
BRL
mg/kg dry
0.0053
0.00060
1
8260B
3/14/19 23:47
JLB
P9CO277
Bromomethane
BRL
mg/kg dry
0.011
0.00066
1
8260B
3/14/19 23:47
JLB
P9CO277
Carbon Tetrachloride
BRL
mg/kg dry
0.0053
0.00026
1
8260B
3/14/19 23:47
JLB
P9CO277
Chlorobenzene
BRL
mg/kg dry
0.0053
0.00028
1
8260B
3/14/19 23:47
JLB
P9CO277
Chloroethane
BRL
mg/kg dry
0.011
0.00044
1
8260B
3/14/19 23:47
JLB
P9CO277
Chloroform
BRL
mg/kg dry
0.0053
0.00038
1
8260B
3/14/19 23:47
JLB
P9CO277
Chloromethane
BRL
mg/kg dry
0.0053
0.00036
1
8260B
3/14/19 23:47
JLB
P9CO277
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0053
0.00023
1
8260B
3/14/19 23:47
JLB
P9CO277
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0053
0.00018
1
8260B
3/14/19 23:47
JLB
P9CO277
Dibromochloromethane
BRL
mg/kg dry
0.0053
0.00022
1
8260B
3/14/19 23:47
JLB
P9CO277
Dichlorodifluoromethane
BRL
mg/kg dry
0.0053
0.00024
1
8260B
3/14/19 23:47
JLB
P9CO277
Ethylbenzene
BRL
mg/kg dry
0.0053
0.00020
1
8260B
3/14/19 23:47
JLB
P9CO277
Isopropyl Ether
BRL
mg/kg dry
0.0053
0.00022
1
8260B
3/14/19 23:47
JLB
P9CO277
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0053
0.00031
1
8260B
3/14/19 23:47
JLB
P9CO277
m,p-Xylenes
BRL
mg/kg dry
0.011
0.00049
1
8260B
3/14/19 23:47
JLB
P9CO277
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 28

Laboratory Report
` Full -Service
Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
03/18/2019
ECS Carolinas, LLP (Charlotte)
Project: W. Morehead
Client
Sample ID: NW
Attn: Chris Orrell
Prism
Sample ID: 9030248-01
1812 Center Park Drive, Suite D
Prism
Work Order: 9030248
Charlotte, NC 28217
Sample Matrix: Solid
Time
Collected: 03/14/19 09:50
Time
Submitted: 03/14/19 12:25
Parameter
Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.053
0.00048
1
8260B 3/14/19 23:47
JLB
P9CO277
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.11
0.00048
1
8260B 3/14/19 23:47
JLB
P9CO277
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.053
0.00045
1
8260B 3/14/19 23:47
JLB
P9CO277
Methylene Chloride
BRL
mg/kg dry
0.011
0.00030
1
8260B 3/14/19 23:47
JLB
P9CO277
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.011
0.00017
1
8260B 3/14/19 23:47
JLB
P9CO277
Naphthalene
BRL
mg/kg dry
0.011
0.00017
1
8260B 3/14/19 23:47
JLB
P9CO277
n-Butylbenzene
BRL
mg/kg dry
0.0053
0.00027
1
8260B 3/14/19 23:47
JLB
P9CO277
n-Propylbenzene
BRL
mg/kg dry
0.0053
0.00032
1
8260B 3/14/19 23:47
JLB
P9CO277
o-Xylene
BRL
mg/kg dry
0.0053
0.00022
1
8260B 3/14/19 23:47
JLB
P9CO277
sec-Butylbenzene
BRL
mg/kg dry
0.0053
0.00026
1
8260B 3/14/19 23:47
JLB
P9CO277
Styrene
BRL
mg/kg dry
0.0053
0.00032
1
8260B 3/14/19 23:47
JLB
P9CO277
tert-Butylbenzene
BRL
mg/kg dry
0.0053
0.00018
1
8260B 3/14/19 23:47
JLB
P9CO277
Tetrachloroethylene
BRL
mg/kg dry
0.0053
0.00025
1
8260B 3/14/19 23:47
JLB
P9CO277
Toluene
BRL
mg/kg dry
0.0053
0.00031
1
8260B 3/14/19 23:47
JLB
P9CO277
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0053
0.00032
1
8260B 3/14/19 23:47
JLB
P9CO277
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0053
0.00028
1
8260B 3/14/19 23:47
JLB
P9CO277
Trichloroethylene
BRL
mg/kg dry
0.0053
0.00034
1
8260B 3/14/19 23:47
JLB
P9CO277
Trichlorofluoromethane
BRL
mg/kg dry
0.0053
0.00034
1
8260B 3/14/19 23:47
JLB
P9CO277
Vinyl acetate
BRL
mg/kg dry
0.027
0.00073
1
8260B 3/14/19 23:47
JLB
P9CO277
Vinyl chloride
BRL
mg/kg dry
0.0053
0.00026
1
8260B 3/14/19 23:47
JLB
P9CO277
Xylenes, total
BRL
mg/kg dry
0.016
0.0010
1
8260B 3/14/19 23:47
JLB
P9CO277
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
100 %
70-130
Dibromofluoromethane
97 %
84-123
Toluene-d8
81 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
16
0.52
100
MADEP VPH 3/14/19 17:33
TBL
P9C0199
C9-Cl2 Aliphatics
BRL
mg/kg dry
16
0.85
100
MADEP VPH 3/14/19 17:33
TBL
P9C0199
C9-Cl0 Aromatics
BRL
mg/kg dry
16
0.18
100
MADEP VPH 3/14/19 17:33
TBL
P9C0199
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
107 %
70-130
2,5-Dibromotoluene (FID)
116 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 28

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
03/18/2019
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead Client Sample ID: B
Prism Sample ID: 9030248-02
Prism Work Order: 9030248
Sample Matrix: Solid Time Collected: 03/14/19 09:55
Time Submitted: 03/14/19 12:25
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics 3.4 J
mg/kg dry 27 0.17 1 MADEP EPH 3/15/19 16:41 BGB P9CO262
C19-C36 Aliphatics BRL
mg/kg dry 27 3.2 1 MADEP EPH 3/15/19 16:41 BGB P9CO262
C11-C22 Aromatics BRL
mg/kg dry 11 1.9 1 MADEP EPH 3/15/19 16:41 BGB P9CO262
Surrogate Recovery Control Limits
1-Chlorooctadecane
74 %
40-140
o-Terphenyl
87 %
40-140
2-Fluorobiphenyl
96 %
40-140
2-Bromonaphthalene
90 %
40-140
General Chemistry Parameters
% Solids
92.2
% by
0.100
0.100
1
'SM2540 G
3118/19 9:35
KBS
P9CO281
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.36
0.056
1
8270D
3/15/19 15:26
JMV
P9CO261
1,2-Dichlorobenzene
BRL
mg/kg dry
0.36
0.054
1
8270D
3/15/19 15:26
JMV
P9CO261
1,3-Dichlorobenzene
BRL
mg/kg dry
0.36
0.050
1
8270D
3/15/19 15:26
JMV
P9CO261
1,4-Dichlorobenzene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/15/19 15:26
JMV
P9CO261
1-Methyl naphthalene
BRL
mg/kg dry
0.36
0.069
1
8270D
3/15/19 15:26
JMV
P9CO261
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.36
0.058
1
8270D
3/15/19 15:26
JMV
P9CO261
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.36
0.067
1
8270D
3/15/19 15:26
JMV
P9CO261
2,4-Dichlorophenol
BRL
mg/kg dry
0.36
0.069
1
8270D
3/15/19 15:26
JMV
P9CO261
2,4-Dimethylphenol
BRL
mg/kg dry
0.36
0.055
1
8270D
3/15/19 15:26
JMV
P9CO261
2,4-Dinitrophenol
BRL
mg/kg dry
0.36
0.050
1
8270D
3/15/19 15:26
JMV
P9CO261
2,4-Dinitrotoluene
BRL
mg/kg dry
0.36
0.043
1
8270D
3/15/19 15:26
JMV
P9CO261
2,6-Dinitrotoluene
BRL
mg/kg dry
0.36
0.048
1
8270D
3/15/19 15:26
JMV
P9CO261
2-Chloronaphthalene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/15/19 15:26
JMV
P9CO261
2-Chlorophenol
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:26
JMV
P9CO261
2-Methyl naphthalene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/15/19 15:26
JMV
P9CO261
2-Methylphenol
BRL
mg/kg dry
0.36
0.046
1
8270D
3/15/19 15:26
JMV
P9CO261
2-Nitrophenol
BRL
mg/kg dry
0.36
0.065
1
8270D
3/15/19 15:26
JMV
P9CO261
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.36
0.071
1
8270D
3/15/19 15:26
JMV
P9CO261
3/4-Methyl phenol
BRL
mg/kg dry
0.36
0.044
1
8270D
3/15/19 15:26
JMV
P9CO261
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
0.36
0.054
1
8270D
3/15/19 15:26
JMV
P9CO261
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.36
0.061
1
8270D
3/15/19 15:26
JMV
P9CO261
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.36
0.050
1
8270D
3/15/19 15:26
JMV
P9CO261
4-Chloroaniline
BRL
mg/kg dry
0.36
0.043
1
8270D
3/15/19 15:26
JMV
P9CO261
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
0.36
0.046
1
8270D
3/15/19 15:26
JMV
P9CO261
4-Nitrophenol
BRL
mg/kg dry
0.36
0.055
1
8270D
3/15/19 15:26
JMV
P9CO261
Acenaphthene
BRL
mg/kg dry
0.36
0.049
1
8270D
3/15/19 15:26
JMV
P9CO261
Acenaphthylene
BRL
mg/kg dry
0.36
0.052
1
8270D
3/15/19 15:26
JMV
P9CO261
Anthracene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/15/19 15:26
JMV
P9CO261
Azobenzene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:26
JMV
P9CO261
Benzo(a)anthracene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:26
JMV
P9CO261
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 28

` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead
Sample Matrix: Solid
Laboratory Report
03/18/2019
Client Sample ID: B
Prism Sample ID: 9030248-02
Prism Work Order: 9030248
Time Collected: 03/14/19 09:55
Time Submitted: 03/14/19 12:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.36
0.039
1
8270D
3/15/19 15:26
JMV
P9CO261
Benzo(b)fluoranthene
BRL
mg/kg dry
0.36
0.042
1
8270D
3/15/19 15:26
JMV
P9CO261
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.36
0.039
1
8270D
3/15/19 15:26
JMV
P9CO261
Benzo(k)fluoranthene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:26
JMV
P9CO261
Benzoic Acid
0.22
J mg/kg dry
0.36
0.030
1
8270D
3/15/19 15:26
JMV
P9CO261
Benzyl alcohol
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:26
JMV
P9CO261
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.36
0.062
1
8270D
3/15/19 15:26
JMV
P9CO261
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.36
0.050
1
8270D
3/15/19 15:26
JMV
P9CO261
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.36
0.061
1
8270D
3/15/19 15:26
JMV
P9CO261
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.36
0.053
1
8270D
3/15/19 15:26
JMV
P9CO261
Butyl benzyl phthalate
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:26
JMV
P9CO261
Chrysene
BRL
mg/kg dry
0.36
0.045
1
8270D
3/15/19 15:26
JMV
P9CO261
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.36
0.044
1
8270D
3/15/19 15:26
JMV
P9CO261
Dibenzofuran
BRL
mg/kg dry
0.36
0.054
1
8270D
3/15/19 15:26
JMV
P9CO261
Diethyl phthalate
BRL
mg/kg dry
0.36
0.049
1
8270D
3/15/19 15:26
JMV
P9CO261
Dimethyl phthalate
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:26
JMV
P9CO261
Di-n-butyl phthalate
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:26
JMV
P9CO261
Di-n-octyl phthalate
BRL
mg/kg dry
0.36
0.044
1
8270D
3/15/19 15:26
JMV
P9CO261
Fluoranthene
BRL
mg/kg dry
0.36
0.046
1
8270D
3/15/19 15:26
JMV
P9CO261
Fluorene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:26
JMV
P9CO261
Hexachlorobenzene
BRL
mg/kg dry
0.36
0.057
1
8270D
3/15/19 15:26
JMV
P9CO261
Hexachlorobutadiene
BRL
mg/kg dry
0.36
0.064
1
8270D
3/15/19 15:26
JMV
P9CO261
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.36
0.064
1
8270D
3/15/19 15:26
JMV
P9CO261
Hexachloroethane
BRL
mg/kg dry
0.36
0.060
1
8270D
3/15/19 15:26
JMV
P9CO261
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.36
0.041
1
8270D
3/15/19 15:26
JMV
P9CO261
Isophorone
BRL
mg/kg dry
0.36
0.048
1
8270D
3/15/19 15:26
JMV
P9CO261
Naphthalene
BRL
mg/kg dry
0.36
0.058
1
8270D
3/15/19 15:26
JMV
P9CO261
Nitrobenzene
BRL
mg/kg dry
0.36
0.051
1
8270D
3/15/19 15:26
JMV
P9CO261
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.36
0.056
1
8270D
3/15/19 15:26
JMV
P9CO261
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.36
0.054
1
8270D
3/15/19 15:26
JMV
P9CO261
Pentachlorophenol
BRL
mg/kg dry
0.36
0.042
1
8270D
3/15/19 15:26
JMV
P9CO261
Phenanthrene
BRL
mg/kg dry
0.36
0.046
1
8270D
3/15/19 15:26
JMV
P9CO261
Phenol
BRL
mg/kg dry
0.36
0.053
1
8270D
3/15/19 15:26
JMV
P9CO261
Pyrene
BRL
mg/kg dry
0.36
0.047
1
8270D
3/15/19 15:26
JMV
P9CO261
Pyridine
BRL
mg/kg dry
0.36
0.062
1
8270D
3/15/19 15:26
JMV
P9CO261
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
71 %
39-132
2-Fluorobiphenyl
70 %
44-115
2-Fluorophenol
69 %
35-115
Nitrobenzene-d5
63 %
37-122
Phenol-d5
67 %
34-121
Terphenyl-d14
79 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 28

` Full -Service Analytical &
/ environmental Solutions
P R S M
LABORATORIES INC.
ECS Carolinas, LLP (Charlotte)
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: W. Morehead
Sample Matrix: Solid
Laboratory Report
03/18/2019
Client Sample ID: B
Prism Sample ID: 9030248-02
Prism Work Order: 9030248
Time Collected: 03/14/19 09:55
Time Submitted: 03/14/19 12:25
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00050
1
8260B
3/15/19
0:17
JLB
P9CO277
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0060
0.00029
1
8260B
3/15/19
0:17
JLB
P9CO277
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0060
0.00041
1
8260B
3/15/19
0:17
JLB
P9CO277
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0060
0.00053
1
8260B
3/15/19
0:17
JLB
P9CO277
1,1-Dichloroethane
BRL
mg/kg dry
0.0060
0.00017
1
8260B
3/15/19
0:17
JLB
P9CO277
1,1-Dichloroethylene
BRL
mg/kg dry
0.0060
0.00027
1
8260B
3/15/19
0:17
JLB
P9CO277
1,1-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00033
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.0060
0.00034
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0060
0.00077
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.0060
0.00045
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2,4-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00046
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2-Dibromoethane
BRL
mg/kg dry
0.0060
0.00024
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00028
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2-Dichloroethane
BRL
mg/kg dry
0.0060
0.00036
1
8260B
3/15/19
0:17
JLB
P9CO277
1,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00037
1
8260B
3/15/19
0:17
JLB
P9CO277
1,3,5-Trimethyl benzene
BRL
mg/kg dry
0.0060
0.00046
1
8260B
3/15/19
0:17
JLB
P9CO277
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00040
1
8260B
3/15/19
0:17
JLB
P9CO277
1,3-Dichloropropane
BRL
mg/kg dry
0.0060
0.00030
1
8260B
3/15/19
0:17
JLB
P9CO277
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0060
0.00024
1
8260B
3/15/19
0:17
JLB
P9CO277
2,2-Dichloropropane
BRL
mg/kg dry
0.0060
0.00029
1
8260B
3/15/19
0:17
JLB
P9CO277
2-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00031
1
8260B
3/15/19
0:17
JLB
P9CO277
4-Chlorotoluene
BRL
mg/kg dry
0.0060
0.00036
1
8260B
3/15/19
0:17
JLB
P9CO277
4-Isopropyltoluene
BRL
mg/kg dry
0.0060
0.00029
1
8260B
3/15/19
0:17
JLB
P9CO277
Acetone
BRL
mg/kg dry
0.060
0.0015
1
8260B
3/15/19
0:17
JLB
P9CO277
Benzene
BRL
mg/kg dry
0.0036
0.00035
1
8260B
3/15/19
0:17
JLB
P9CO277
Bromobenzene
BRL
mg/kg dry
0.0060
0.00050
1
8260B
3/15/19
0:17
JLB
P9CO277
Bromochloromethane
BRL
mg/kg dry
0.0060
0.00033
1
8260B
3/15/19
0:17
JLB
P9CO277
Bromodichloromethane
BRL
mg/kg dry
0.0060
0.00034
1
8260B
3/15/19
0:17
JLB
P9CO277
Bromoform
BRL
mg/kg dry
0.0060
0.00068
1
8260B
3/15/19
0:17
JLB
P9CO277
Bromomethane
BRL
mg/kg dry
0.012
0.00074
1
8260B
3/15/19
0:17
JLB
P9CO277
Carbon Tetrachloride
BRL
mg/kg dry
0.0060
0.00030
1
8260B
3/15/19
0:17
JLB
P9CO277
Chlorobenzene
BRL
mg/kg dry
0.0060
0.00032
1
8260B
3/15/19
0:17
JLB
P9CO277
Chloroethane
BRL
mg/kg dry
0.012
0.00050
1
8260B
3/15/19
0:17
JLB
P9CO277
Chloroform
BRL
mg/kg dry
0.0060
0.00044
1
8260B
3/15/19
0:17
JLB
P9CO277
Chloromethane
BRL
mg/kg dry
0.0060
0.00040
1
8260B
3/15/19
0:17
JLB
P9CO277
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.00026
1
8260B
3/15/19
0:17
JLB
P9CO277
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00020
1
8260B
3/15/19
0:17
JLB
P9CO277
Dibromochloromethane
BRL
mg/kg dry
0.0060
0.00025
1
8260B
3/15/19
0:17
JLB
P9CO277
Dichlorodifluoromethane
BRL
mg/kg dry
0.0060
0.00027
1
8260B
3/15/19
0:17
JLB
P9CO277
Ethylbenzene
BRL
mg/kg dry
0.0060
0.00023
1
8260B
3/15/19
0:17
JLB
P9CO277
Isopropyl Ether
BRL
mg/kg dry
0.0060
0.00025
1
8260B
3/15/19
0:17
JLB
P9CO277
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0060
0.00036
1
8260B
3/15/19
0:17
JLB
P9CO277
m,p-Xylenes
BRL
mg/kg dry
0.012
0.00056
1
8260B
3/15/19
0:17
JLB
P9CO277
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 28

Laboratory Report
` Full -Service
Analytical &
/ Environmental Solutions
P R S M
LABORATORIES INC.
03/18/2019
ECS Carolinas, LLP (Charlotte)
Project: W. Morehead
Client
Sample ID: B
Attn: Chris Orrell
Prism
Sample ID: 9030248-02
1812 Center Park Drive, Suite D
Prism
Work Order: 9030248
Charlotte, NC 28217
Sample Matrix: Solid
Time
Collected: 03/14/19 09:55
Time
Submitted: 03/14/19 12:25
Parameter
Result
Units
Report
MDL Dilution
Method Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.060
0.00054
1
8260B 3/15/19 0:17
JLB
P9CO277
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.12
0.00054
1
8260B 3/15/19 0:17
JLB
P9CO277
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.060
0.00051
1
8260B 3/15/19 0:17
JLB
P9CO277
Methylene Chloride
BRL
mg/kg dry
0.012
0.00034
1
8260B 3/15/19 0:17
JLB
P9CO277
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.012
0.00019
1
8260B 3/15/19 0:17
JLB
P9CO277
Naphthalene
BRL
mg/kg dry
0.012
0.00019
1
8260B 3/15/19 0:17
JLB
P9CO277
n-Butylbenzene
BRL
mg/kg dry
0.0060
0.00031
1
8260B 3/15/19 0:17
JLB
P9CO277
n-Propylbenzene
BRL
mg/kg dry
0.0060
0.00036
1
8260B 3/15/19 0:17
JLB
P9CO277
o-Xylene
BRL
mg/kg dry
0.0060
0.00025
1
8260B 3/15/19 0:17
JLB
P9CO277
sec-Butylbenzene
BRL
mg/kg dry
0.0060
0.00029
1
8260B 3/15/19 0:17
JLB
P9CO277
Styrene
BRL
mg/kg dry
0.0060
0.00036
1
8260B 3/15/19 0:17
JLB
P9CO277
tert-Butylbenzene
BRL
mg/kg dry
0.0060
0.00020
1
8260B 3/15/19 0:17
JLB
P9CO277
Tetrachloroethylene
BRL
mg/kg dry
0.0060
0.00029
1
8260B 3/15/19 0:17
JLB
P9CO277
Toluene
BRL
mg/kg dry
0.0060
0.00035
1
8260B 3/15/19 0:17
JLB
P9CO277
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0060
0.00036
1
8260B 3/15/19 0:17
JLB
P9CO277
trans- 1,3-Dichloropropylene
BRL
mg/kg dry
0.0060
0.00032
1
8260B 3/15/19 0:17
JLB
P9CO277
Trichloroethylene
BRL
mg/kg dry
0.0060
0.00039
1
8260B 3/15/19 0:17
JLB
P9CO277
Trichlorofluoromethane
BRL
mg/kg dry
0.0060
0.00039
1
8260B 3/15/19 0:17
JLB
P9CO277
Vinyl acetate
BRL
mg/kg dry
0.030
0.00083
1
8260B 3/15/19 0:17
JLB
P9CO277
Vinyl chloride
BRL
mg/kg dry
0.0060
0.00029
1
8260B 3/15/19 0:17
JLB
P9CO277
Xylenes, total
BRL
mg/kg dry
0.018
0.0011
1
8260B 3/15/19 0:17
JLB
P9CO277
Surrogate
Recovery
Control Limits
4-13romofluorobenzene
99 %
70-130
Dibromofluoromethane
99 %
84-123
Toluene-d8
81 %
76-129
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
18
0.59
100
MADEP VPH 3/14/19 18:01
TBL
P9C0199
C9-Cl2 Aliphatics
BRL
mg/kg dry
18
0.96
100
MADEP VPH 3/14/19 18:01
TBL
P9C0199
C9-Cl0 Aromatics
BRL
mg/kg dry
18
0.21
100
MADEP VPH 3/14/19 18:01
TBL
P9C0199
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
76 %
70-130
2,5-Dibromotoluene (FID)
81 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 11 of 28

P R I IS M EService Analytical
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9CO277-BLK1)
Prepared & Analyzed: 03/14/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.0050
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.0050
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.050
mg/kg wet
Benzene
BRL
0.0030
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.0050
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.0050
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.050
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.10
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.050
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 28

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9CO277-BLK1)
Prepared & Analyzed: 03/14/19
Methylene Chloride
BRL
0.010
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.010
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.0050
mg/kg wet
Vinyl acetate
BRL
0.025
mg/kg wet
Vinyl chloride
BRL
0.0050
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
50.5
ug/L
50.00 101 70-130
Surrogate: Dibromofluoromethane
48.5
ug/L
50.00 97 84-123
Surrogate: Toluene-d8
41.0
ug/L
50.00 82 76-129
LCS (P9CO277-BS1)
Prepared
& Analyzed: 03/14/19
1,1,1,2-Tetrachloroethane
0.0484
0.0050
mg/kg wet
0.05000
97
72-115
1, 1,1 -Trichloroethane
0.0487
0.0050
mg/kg wet
0.05000
97
67-131
1,1,2,2-Tetrachloroethane
0.0402
0.0050
mg/kg wet
0.05000
80
56-126
1,1,2-Trichloroethane
0.0484
0.0050
mg/kg wet
0.05000
97
70-133
1,1-Dichloroethane
0.0507
0.0050
mg/kg wet
0.05000
101
74-127
1,1-Dichloroethylene
0.0480
0.0050
mg/kg wet
0.05000
96
67-149
1, 1 -Dichloropropylene
0.0515
0.0050
mg/kg wet
0.05000
103
71-130
1,2,3-Trichlorobenzene
0.0465
0.0050
mg/kg wet
0.05000
93
68-130
1,2,3-Trichloropropane
0.0412
0.0050
mg/kg wet
0.05000
82
60-137
1,2,4-Trichlorobenzene
0.0460
0.0050
mg/kg wet
0.05000
92
66-125
1,2,4-Trimethylbenzene
0.0396
0.0050
mg/kg wet
0.05000
79
69-129
1,2-Dibromoethane
0.0500
0.0050
mg/kg wet
0.05000
100
70-132
1,2-Dichlorobenzene
0.0399
0.0050
mg/kg wet
0.05000
80
72-123
1,2-Dichloroethane
0.0481
0.0050
mg/kg wet
0.05000
96
68-128
1,2-Dichloropropane
0.0531
0.0050
mg/kg wet
0.05000
106
73-130
1,3,5-Trimethylbenzene
0.0390
0.0050
mg/kg wet
0.05000
78
69-128
1,3-Dichlorobenzene
0.0400
0.0050
mg/kg wet
0.05000
80
71-120
1,3-Dichloropropane
0.0457
0.0050
mg/kg wet
0.05000
91
75-124
1,4-Dichlorobenzene
0.0401
0.0050
mg/kg wet
0.05000
80
71-123
2,2-Dichloropropane
0.0475
0.0050
mg/kg wet
0.05000
95
50-142
2-Chlorotoluene
0.0362
0.0050
mg/kg wet
0.05000
72
67-124
4-Chlorotoluene
0.0369
0.0050
mg/kg wet
0.05000
74
71-126
4-Isopropyltoluene
0.0402
0.0050
mg/kg wet
0.05000
80
68-129
Acetone
0.102
0.050
mg/kg wet
0.1000
102
29-198
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 28

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9CO277-BSI)
Prepared & Analyzed: 03/14/19
Benzene
0.0518
0.0030
mg/kg wet
0.05000
104
74-127
Bromobenzene
0.0352
0.0050
mg/kg wet
0.05000
70
73-125 L
Bromochloromethane
0.0589
0.0050
mg/kg wet
0.05000
118
72-134
Bromodichloromethane
0.0491
0.0050
mg/kg wet
0.05000
98
75-122
Bromoform
0.0473
0.0050
mg/kg wet
0.05000
95
66-135
Bromomethane
0.0441
0.010
mg/kg wet
0.05000
88
20-180
Carbon Tetrachloride
0.0468
0.0050
mg/kg wet
0.05000
94
64-143
Chlorobenzene
0.0455
0.0050
mg/kg wet
0.05000
91
74-118
Chloroethane
0.0469
0.010
mg/kg wet
0.05000
94
33-149
Chloroform
0.0502
0.0050
mg/kg wet
0.05000
100
73-127
Chloromethane
0.0597
0.0050
mg/kg wet
0.05000
119
45-143
cis-1,2-Dichloroethylene
0.0513
0.0050
mg/kg wet
0.05000
103
76-134
cis-1,3-Dichloropropylene
0.0545
0.0050
mg/kg wet
0.05000
109
71-125
Dibromochloromethane
0.0451
0.0050
mg/kg wet
0.05000
90
73-122
Dichlorodifluoromethane
0.0680
0.0050
mg/kg wet
0.05000
136
26-146
Ethylbenzene
0.0452
0.0050
mg/kg wet
0.05000
90
74-128
Isopropyl Ether
0.0522
0.0050
mg/kg wet
0.05000
104
59-159
Isopropylbenzene (Cumene)
0.0392
0.0050
mg/kg wet
0.05000
78
68-126
m,p-Xylenes
0.0917
0.010
mg/kg wet
0.1000
92
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0511
0.050
mg/kg wet
0.05000
102
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0576
0.10
mg/kg wet
0.05000
115
63-149 J
Methyl Isobutyl Ketone
0.0596
0.050
mg/kg wet
0.05000
119
57-162
Methylene Chloride
0.0504
0.010
mg/kg wet
0.05000
101
74-129
Methyl-tert-Butyl Ether
0.0547
0.010
mg/kg wet
0.05000
109
70-130
Naphthalene
0.0456
0.010
mg/kg wet
0.05000
91
57-157
n-Butylbenzene
0.0385
0.0050
mg/kg wet
0.05000
77
65-135
n-Propylbenzene
0.0367
0.0050
mg/kg wet
0.05000
73
67-130
o-Xylene
0.0471
0.0050
mg/kg wet
0.05000
94
74-126
sec-Butylbenzene
0.0391
0.0050
mg/kg wet
0.05000
78
66-131
Styrene
0.0493
0.0050
mg/kg wet
0.05000
99
77-121
tert-Butyl benzene
0.0401
0.0050
mg/kg wet
0.05000
80
67-132
Tetrachloroethylene
0.0594
0.0050
mg/kg wet
0.05000
119
68-130
Toluene
0.0540
0.0050
mg/kg wet
0.05000
108
71-129
trans- 1,2-Dichloroethylene
0.0496
0.0050
mg/kg wet
0.05000
99
73-132
trans- 1,3-Dichloropropylene
0.0530
0.0050
mg/kg wet
0.05000
106
68-123
Trichloroethylene
0.0546
0.0050
mg/kg wet
0.05000
109
75-133
Trichlorofluoromethane
0.0451
0.0050
mg/kg wet
0.05000
90
44-146
Vinyl acetate
0.0641
0.025
mg/kg wet
0.05000
128
85-161
Vinyl chloride
0.0526
0.0050
mg/kg wet
0.05000
105
48-147
Xylenes, total
0.139
0.015
mg/kg wet
0.1500
92
74-126
Surrogate:4-Bromofluorobenzene
50.4
ug/L
50.00
101
70-130
Surrogate: Dibromofluoromethane
47.3
ug/L
50.00
95
84-123
Surrogate: Toluene-d8
41.4
ug/L
50.00
83
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 28

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9CO277-BSD1)
Prepared & Analyzed: 03/14/19
1,1,1,2-Tetrachloroethane
0.0491
0.0050
mg/kg wet
0.05000
98
72-115
1 20
1, 1,1 -Trichloroethane
0.0503
0.0050
mg/kg wet
0.05000
101
67-131
3 20
1,1,2,2-Tetrachloroethane
0.0392
0.0050
mg/kg wet
0.05000
78
56-126
2 20
1,1,2-Trichloroethane
0.0481
0.0050
mg/kg wet
0.05000
96
70-133
0.4 20
1,1-Dichloroethane
0.0520
0.0050
mg/kg wet
0.05000
104
74-127
3 20
1,1-Dichloroethylene
0.0493
0.0050
mg/kg wet
0.05000
99
67-149
3 20
1, 1 -Dichloropropylene
0.0520
0.0050
mg/kg wet
0.05000
104
71-130
0.9 20
1,2,3-Trichlorobenzene
0.0468
0.0050
mg/kg wet
0.05000
94
68-130
0.6 20
1,2,3-Trichloropropane
0.0412
0.0050
mg/kg wet
0.05000
82
60-137
0.07 20
1,2,4-Trichlorobenzene
0.0460
0.0050
mg/kg wet
0.05000
92
66-125
0.02 20
1,2,4-Trimethylbenzene
0.0404
0.0050
mg/kg wet
0.05000
81
69-129
2 20
1,2-Dibromoethane
0.0494
0.0050
mg/kg wet
0.05000
99
70-132
1 20
1,2-Dichlorobenzene
0.0403
0.0050
mg/kg wet
0.05000
81
72-123
1 20
1,2-Dichloroethane
0.0481
0.0050
mg/kg wet
0.05000
96
68-128
0.08 20
1,2-Dichloropropane
0.0540
0.0050
mg/kg wet
0.05000
108
73-130
2 20
1,3,5-Trimethylbenzene
0.0396
0.0050
mg/kg wet
0.05000
79
69-128
2 20
1,3-Dichlorobenzene
0.0405
0.0050
mg/kg wet
0.05000
81
71-120
1 20
1,3-Dichloropropane
0.0455
0.0050
mg/kg wet
0.05000
91
75-124
0.5 20
1,4-Dichlorobenzene
0.0406
0.0050
mg/kg wet
0.05000
81
71-123
1 20
2,2-Dichloropropane
0.0492
0.0050
mg/kg wet
0.05000
98
50-142
4 20
2-Chlorotoluene
0.0370
0.0050
mg/kg wet
0.05000
74
67-124
2 20
4-Chlorotoluene
0.0370
0.0050
mg/kg wet
0.05000
74
71-126
0.4 20
4-Isopropyltoluene
0.0409
0.0050
mg/kg wet
0.05000
82
68-129
2 20
Acetone
0.0988
0.050
mg/kg wet
0.1000
99
29-198
3 20
Benzene
0.0528
0.0030
mg/kg wet
0.05000
106
74-127
2 20
Bromobenzene
0.0356
0.0050
mg/kg wet
0.05000
71
73-125
1 20
Bromochloromethane
0.0588
0.0050
mg/kg wet
0.05000
118
72-134
0.1 20
Bromodichloromethane
0.0501
0.0050
mg/kg wet
0.05000
100
75-122
2 20
Bromoform
0.0469
0.0050
mg/kg wet
0.05000
94
66-135
0.8 20
Bromomethane
0.0452
0.010
mg/kg wet
0.05000
90
20-180
2 20
Carbon Tetrachloride
0.0495
0.0050
mg/kg wet
0.05000
99
64-143
6 20
Chlorobenzene
0.0458
0.0050
mg/kg wet
0.05000
92
74-118
0.6 20
Chloroethane
0.0476
0.010
mg/kg wet
0.05000
95
33-149
1 20
Chloroform
0.0509
0.0050
mg/kg wet
0.05000
102
73-127
1 20
Chloromethane
0.0622
0.0050
mg/kg wet
0.05000
124
45-143
4 20
cis-1,2-Dichloroethylene
0.0518
0.0050
mg/kg wet
0.05000
104
76-134
1 20
cis-1,3-Dichloropropylene
0.0546
0.0050
mg/kg wet
0.05000
109
71-125
0.1 20
Dibromochloromethane
0.0451
0.0050
mg/kg wet
0.05000
90
73-122
0.02 20
Dichlorodifluoromethane
0.0708
0.0050
mg/kg wet
0.05000
142
26-146
4 20
Ethylbenzene
0.0461
0.0050
mg/kg wet
0.05000
92
74-128
2 20
Isopropyl Ether
0.0529
0.0050
mg/kg wet
0.05000
106
59-159
1 20
Isopropylbenzene (Cumene)
0.0401
0.0050
mg/kg wet
0.05000
80
68-126
2 20
m,p-Xylenes
0.0926
0.010
mg/kg wet
0.1000
93
75-124
1 20
Methyl Butyl Ketone (2-Hexanone)
0.0499
0.050
mg/kg wet
0.05000
100
61-157
2 20
Methyl Ethyl Ketone (2-Butanone)
0.0568
0.10
mg/kg wet
0.05000
114
63-149
1 20
Methyl Isobutyl Ketone
0.0582
0.050
mg/kg wet
0.05000
116
57-162
2 20
L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 28

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9CO277-BSD1)
Prepared & Analyzed: 03/14/19
Methylene Chloride
0.0510
0.010
mg/kg wet
0.05000
102
74-129
1 20
Methyl-tert-Butyl Ether
0.0541
0.010
mg/kg wet
0.05000
108
70-130
1 20
Naphthalene
0.0453
0.010
mg/kg wet
0.05000
91
57-157
0.8 20
n-Butylbenzene
0.0390
0.0050
mg/kg wet
0.05000
78
65-135
1 20
n-Propylbenzene
0.0373
0.0050
mg/kg wet
0.05000
75
67-130
2 20
o-Xylene
0.0479
0.0050
mg/kg wet
0.05000
96
74-126
2 20
sec-Butylbenzene
0.0400
0.0050
mg/kg wet
0.05000
80
66-131
2 20
Styrene
0.0496
0.0050
mg/kg wet
0.05000
99
77-121
0.7 20
tert-Butyl benzene
0.0408
0.0050
mg/kg wet
0.05000
82
67-132
2 20
Tetrachloroethylene
0.0604
0.0050
mg/kg wet
0.05000
121
68-130
2 20
Toluene
0.0549
0.0050
mg/kg wet
0.05000
110
71-129
2 20
trans- 1,2-Dichloroethylene
0.0509
0.0050
mg/kg wet
0.05000
102
73-132
3 20
trans- 1,3-Dichloropropylene
0.0528
0.0050
mg/kg wet
0.05000
106
68-123
0.3 20
Trichloroethylene
0.0564
0.0050
mg/kg wet
0.05000
113
75-133
3 20
Trichlorofluoromethane
0.0468
0.0050
mg/kg wet
0.05000
94
44-146
4 20
Vinyl acetate
0.0632
0.025
mg/kg wet
0.05000
126
85-161
1 20
Vinyl chloride
0.0548
0.0050
mg/kg wet
0.05000
110
48-147
4 20
Xylenes, total
0.141
0.015
mg/kg wet
0.1500
94
74-126
1 20
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
47.7
ug/L
50.00
95
84-123
Surrogate: Toluene-d8
41.2
ug/L
50.00
82
76-129
Matrix Spike (P9CO277-MS1)
Source: 9030248-01
Prepared: 03/14/19 Analyzed: 03/15/19
1,1,1,2-Tetrachloroethane
0.0478
0.0054
mg/kg dry
0.05444
BRL
88
60-120
1,1,1-Trichloroethane
0.0487
0.0054
mg/kg dry
0.05444
BRL
89
52-139
1,1,2,2-Tetrachloroethane
0.0383
0.0054
mg/kg dry
0.05444
BRL
70
39-135
1,1,2-Trichloroethane
0.0483
0.0054
mg/kg dry
0.05444
BRL
89
44-140
1,1-Dichloroethane
0.0509
0.0054
mg/kg dry
0.05444
BRL
94
59-137
1,1-Dichloroethylene
0.0481
0.0054
mg/kg dry
0.05444
BRL
88
54-162
1, 1 -Dichloropropylene
0.0503
0.0054
mg/kg dry
0.05444
BRL
92
55-137
1,2,3-Trichlorobenzene
0.0409
0.0054
mg/kg dry
0.05444
BRL
75
34-120
1,2,3-Trichloropropane
0.0400
0.0054
mg/kg dry
0.05444
BRL
74
45-139
1,2,4-Trichlorobenzene
0.0377
0.0054
mg/kg dry
0.05444
BRL
69
35-116
1,2,4-Trimethylbenzene
0.0334
0.0054
mg/kg dry
0.05444
BRL
61
38-142
1,2-Dibromoethane
0.0497
0.0054
mg/kg dry
0.05444
BRL
91
49-132
1,2-Dichlorobenzene
0.0367
0.0054
mg/kg dry
0.05444
BRL
67
42-130
1,2-Dichloroethane
0.0477
0.0054
mg/kg dry
0.05444
BRL
88
51-131
1,2-Dichloropropane
0.0536
0.0054
mg/kg dry
0.05444
BRL
98
55-138
1,3,5-Trimethylbenzene
0.0350
0.0054
mg/kg dry
0.05444
BRL
64
44-140
1,3-Dichlorobenzene
0.0358
0.0054
mg/kg dry
0.05444
BRL
66
41-129
1,3-Dichloropropane
0.0460
0.0054
mg/kg dry
0.05444
BRL
84
53-129
1,4-Dichlorobenzene
0.0363
0.0054
mg/kg dry
0.05444
BRL
67
44-134
2,2-Dichloropropane
0.0472
0.0054
mg/kg dry
0.05444
BRL
87
30-147
2-Chlorotoluene
0.0331
0.0054
mg/kg dry
0.05444
BRL
61
46-132
4-Chlorotoluene
0.0331
0.0054
mg/kg dry
0.05444
BRL
61
44-135
4-Isopropyltoluene
0.0353
0.0054
mg/kg dry
0.05444
BRL
65
32-144
Acetone
0.147
0.054
mg/kg dry
0.1089
BRL
135
34-143
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 28

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike (P9CO277-MS1)
Source: 9030248-01
Prepared: 03/14/19 Analyzed: 03/15/19
Benzene
0.0515
0.0033
mg/kg dry
0.05444
BRL
95
60-135
Bromobenzene
0.0336
0.0054
mg/kg dry
0.05444
BRL
62
45-135
Bromochloromethane
0.0589
0.0054
mg/kg dry
0.05444
BRL
108
55-136
Bromodichloromethane
0.0485
0.0054
mg/kg dry
0.05444
BRL
89
55-127
Bromoform
0.0443
0.0054
mg/kg dry
0.05444
BRL
81
40-136
Bromomethane
0.0370
0.011
mg/kg dry
0.05444
BRL
68
30-137
Carbon Tetrachloride
0.0453
0.0054
mg/kg dry
0.05444
BRL
83
48-153
Chlorobenzene
0.0445
0.0054
mg/kg dry
0.05444
BRL
82
57-125
Chloroethane
0.0479
0.011
mg/kg dry
0.05444
BRL
88
16-177
Chloroform
0.0505
0.0054
mg/kg dry
0.05444
BRL
93
56-137
Chloromethane
0.0641
0.0054
mg/kg dry
0.05444
BRL
118
40-145
cis-1,2-Dichloroethylene
0.0513
0.0054
mg/kg dry
0.05444
BRL
94
58-140
cis-1,3-Dichloropropylene
0.0535
0.0054
mg/kg dry
0.05444
BRL
98
42-135
Dibromochloromethane
0.0439
0.0054
mg/kg dry
0.05444
BRL
81
49-127
Dichlorodifluoromethane
0.0680
0.0054
mg/kg dry
0.05444
BRL
125
25-151
Ethylbenzene
0.0438
0.0054
mg/kg dry
0.05444
BRL
80
44-144
Isopropyl Ether
0.0525
0.0054
mg/kg dry
0.05444
BRL
96
51-155
Isopropylbenzene (Cumene)
0.0365
0.0054
mg/kg dry
0.05444
BRL
67
41-140
m,p-Xylenes
0.0860
0.011
mg/kg dry
0.1089
BRL
79
36-148
Methyl Butyl Ketone (2-Hexanone)
0.0522
0.054
mg/kg dry
0.05444
BRL
96
30-147
Methyl Ethyl Ketone (2-Butanone)
0.0681
0.11
mg/kg dry
0.05444
BRL
125
24-160
Methyl Isobutyl Ketone
0.0597
0.054
mg/kg dry
0.05444
BRL
110
25-163
Methylene Chloride
0.0502
0.011
mg/kg dry
0.05444
BRL
92
53-144
Methyl-tert-Butyl Ether
0.0513
0.011
mg/kg dry
0.05444
BRL
94
49-135
Naphthalene
0.0284
0.011
mg/kg dry
0.05444
BRL
52
32-127
n-Butylbenzene
0.0301
0.0054
mg/kg dry
0.05444
BRL
55
23-148
n-Propylbenzene
0.0326
0.0054
mg/kg dry
0.05444
BRL
60
35-144
o-Xylene
0.0458
0.0054
mg/kg dry
0.05444
BRL
84
43-143
sec-Butylbenzene
0.0339
0.0054
mg/kg dry
0.05444
BRL
62
34-144
Styrene
0.0465
0.0054
mg/kg dry
0.05444
BRL
85
42-132
tert-Butyl benzene
0.0376
0.0054
mg/kg dry
0.05444
BRL
69
36-150
Tetrachloroethylene
0.0573
0.0054
mg/kg dry
0.05444
BRL
105
47-142
Toluene
0.0529
0.0054
mg/kg dry
0.05444
BRL
97
57-135
trans- 1,2-Dichloroethylene
0.0497
0.0054
mg/kg dry
0.05444
BRL
91
58-141
trans- 1,3-Dichloropropylene
0.0517
0.0054
mg/kg dry
0.05444
BRL
95
41-124
Trichloroethylene
0.0556
0.0054
mg/kg dry
0.05444
BRL
102
38-164
Trichlorofluoromethane
0.0459
0.0054
mg/kg dry
0.05444
BRL
84
30-157
Vinyl acetate
0.0211
0.027
mg/kg dry
0.05444
BRL
39
61-154
Vinyl chloride
0.0541
0.0054
mg/kg dry
0.05444
BRL
99
40-156
Xylenes, total
0.132
0.016
mg/kg dry
0.1633
BRL
81
36-148
Surrogate:4-Bromofluorobenzene
49.9
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
47.2
ug/L
50.00
94
84-123
Surrogate: Toluene-d8
41.2
ug/L
50.00
82
76-129
J
J
M,J
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 28

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9CO277-MSD1)
Source: 9030248-01
Prepared: 03/14/19 Analyzed: 03/15/19
1,1,1,2-Tetrachloroethane
0.0447
0.0054
mg/kg dry
0.05444
BRL
82
60-120
7
15
1,1,1-Trichloroethane
0.0446
0.0054
mg/kg dry
0.05444
BRL
82
52-139
9
21
1,1,2,2-Tetrachloroethane
0.0374
0.0054
mg/kg dry
0.05444
BRL
69
39-135
2
22
1,1,2-Trichloroethane
0.0458
0.0054
mg/kg dry
0.05444
BRL
84
44-140
5
21
1,1-Dichloroethane
0.0474
0.0054
mg/kg dry
0.05444
BRL
87
59-137
7
21
1,1-Dichloroethylene
0.0439
0.0054
mg/kg dry
0.05444
BRL
81
54-162
9
22
1, 1 -Dichloropropylene
0.0464
0.0054
mg/kg dry
0.05444
BRL
85
55-137
8
19
1,2,3-Trichlorobenzene
0.0406
0.0054
mg/kg dry
0.05444
BRL
75
34-120
0.5
41
1,2,3-Trichloropropane
0.0396
0.0054
mg/kg dry
0.05444
BRL
73
45-139
1
25
1,2,4-Trichlorobenzene
0.0385
0.0054
mg/kg dry
0.05444
BRL
71
35-116
2
62
1,2,4-Trimethylbenzene
0.0321
0.0054
mg/kg dry
0.05444
BRL
59
38-142
4
24
1,2-Dibromoethane
0.0472
0.0054
mg/kg dry
0.05444
BRL
87
49-132
5
15
1,2-Dichlorobenzene
0.0355
0.0054
mg/kg dry
0.05444
BRL
65
42-130
3
21
1,2-Dichloroethane
0.0460
0.0054
mg/kg dry
0.05444
BRL
84
51-131
4
13
1,2-Dichloropropane
0.0515
0.0054
mg/kg dry
0.05444
BRL
95
55-138
4
16
1,3,5-Trimethylbenzene
0.0332
0.0054
mg/kg dry
0.05444
BRL
61
44-140
5
29
1,3-Dichlorobenzene
0.0355
0.0054
mg/kg dry
0.05444
BRL
65
41-129
1
24
1,3-Dichloropropane
0.0437
0.0054
mg/kg dry
0.05444
BRL
80
53-129
5
15
1,4-Dichlorobenzene
0.0357
0.0054
mg/kg dry
0.05444
BRL
66
44-134
2
21
2,2-Dichloropropane
0.0438
0.0054
mg/kg dry
0.05444
BRL
80
30-147
7
20
2-Chlorotoluene
0.0318
0.0054
mg/kg dry
0.05444
BRL
58
46-132
4
29
4-Chlorotoluene
0.0320
0.0054
mg/kg dry
0.05444
BRL
59
44-135
3
23
4-Isopropyltoluene
0.0339
0.0054
mg/kg dry
0.05444
BRL
62
32-144
4
22
Acetone
0.132
0.054
mg/kg dry
0.1089
BRL
121
34-143
11
49
Benzene
0.0483
0.0033
mg/kg dry
0.05444
BRL
89
60-135
6
20
Bromobenzene
0.0326
0.0054
mg/kg dry
0.05444
BRL
60
45-135
3
25
Bromochloromethane
0.0578
0.0054
mg/kg dry
0.05444
BRL
106
55-136
2
18
Bromodichloromethane
0.0468
0.0054
mg/kg dry
0.05444
BRL
86
55-127
4
17
Bromoform
0.0426
0.0054
mg/kg dry
0.05444
BRL
78
40-136
4
35
Bromomethane
0.0372
0.011
mg/kg dry
0.05444
BRL
68
30-137
0.7
30
Carbon Tetrachloride
0.0416
0.0054
mg/kg dry
0.05444
BRL
76
48-153
9
23
Chlorobenzene
0.0417
0.0054
mg/kg dry
0.05444
BRL
77
57-125
6
14
Chloroethane
0.0436
0.011
mg/kg dry
0.05444
BRL
80
16-177
9
47
Chloroform
0.0472
0.0054
mg/kg dry
0.05444
BRL
87
56-137
7
18
Chloromethane
0.0590
0.0054
mg/kg dry
0.05444
BRL
108
40-145
8
26
cis-1,2-Dichloroethylene
0.0481
0.0054
mg/kg dry
0.05444
BRL
88
58-140
6
28
cis-1,3-Dichloropropylene
0.0510
0.0054
mg/kg dry
0.05444
BRL
94
42-135
5
32
Dibromochloromethane
0.0418
0.0054
mg/kg dry
0.05444
BRL
77
49-127
5
24
Dichlorodifluoromethane
0.0615
0.0054
mg/kg dry
0.05444
BRL
113
25-151
10
37
Ethylbenzene
0.0409
0.0054
mg/kg dry
0.05444
BRL
75
44-144
7
19
Isopropyl Ether
0.0500
0.0054
mg/kg dry
0.05444
BRL
92
51-155
5
13
Isopropylbenzene (Cumene)
0.0344
0.0054
mg/kg dry
0.05444
BRL
63
41-140
6
27
m,p-Xylenes
0.0801
0.011
mg/kg dry
0.1089
BRL
74
36-148
7
20
Methyl Butyl Ketone (2-Hexanone)
0.0495
0.054
mg/kg dry
0.05444
BRL
91
30-147
5
42
Methyl Ethyl Ketone (2-Butanone)
0.0628
0.11
mg/kg dry
0.05444
BRL
115
24-160
8
42
Methyl Isobutyl Ketone
0.0577
0.054
mg/kg dry
0.05444
BRL
106
25-163
3
44
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO277 - 5035
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Matrix Spike Dup (P9CO277-MSD1)
Source: 9030248-01
Prepared: 03/14/19 Analyzed: 03/15/19
Methylene Chloride
0.0473
0.011
mg/kg dry
0.05444
BRL
87
53-144
6
14
Methyl-tert-Butyl Ether
0.0503
0.011
mg/kg dry
0.05444
BRL
92
49-135
2
22
Naphthalene
0.0254
0.011
mg/kg dry
0.05444
BRL
47
32-127
11
44
n-Butylbenzene
0.0289
0.0054
mg/kg dry
0.05444
BRL
53
23-148
4
39
n-Propylbenzene
0.0311
0.0054
mg/kg dry
0.05444
BRL
57
35-144
5
27
o-Xylene
0.0427
0.0054
mg/kg dry
0.05444
BRL
78
43-143
7
17
sec-Butylbenzene
0.0318
0.0054
mg/kg dry
0.05444
BRL
58
34-144
6
28
Styrene
0.0435
0.0054
mg/kg dry
0.05444
BRL
80
42-132
7
28
tert-Butylbenzene
0.0353
0.0054
mg/kg dry
0.05444
BRL
65
36-150
6
29
Tetrachloroethylene
0.0529
0.0054
mg/kg dry
0.05444
BRL
97
47-142
8
26
Toluene
0.0497
0.0054
mg/kg dry
0.05444
BRL
91
57-135
6
22
trans-1,2-Dichloroethylene
0.0458
0.0054
mg/kg dry
0.05444
BRL
84
58-141
8
18
trans- 1,3-Dichloropropylene
0.0498
0.0054
mg/kg dry
0.05444
BRL
91
41-124
4
20
Trichloroethylene
0.0517
0.0054
mg/kg dry
0.05444
BRL
95
38-164
7
18
Trichlorofluoromethane
0.0412
0.0054
mg/kg dry
0.05444
BRL
76
30-157
11
27
Vinyl acetate
0.0167
0.027
mg/kg dry
0.05444
BRL
31
61-154
23
35 M, J
Vinyl chloride
0.0491
0.0054
mg/kg dry
0.05444
BRL
90
40-156
10
35
Xylenes, total
0.123
0.016
mg/kg dry
0.1633
BRL
75
36-148
7
20
Surrogate:4-Bromofluorobenzene
50.9
ug/L
50.00
102
70-130
Surrogate: Dibromofluoromethane
47.2
ug/L
50.00
94
84-123
Surrogate: Toluene-d8
40.6
ug/L
50.00
81
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030248
Attn: Chris Orrell Time Submitted: 3/14/2019 12:25:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9CO261 - 3546
Blank (P9CO261-BLK1)
Prepared & Analyzed: 03/15/19
1,2,4-Trichlorobenzene
BRL
0.33
mg/kg wet
1,2-Dichlorobenzene
BRL
0.33
mg/kg wet
1,3-Dichlorobenzene
BRL
0.33
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
1-Methyl naphthalene
BRL
0.33
mg/kg wet
2,4,5-Trichlorophenol
BRL
0.33
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.33
mg/kg wet
2,4-Dichlorophenol
BRL
0.33
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
0.33
mg/kg wet
2,4-Dinitrotoluene
BRL
0.33
mg/kg wet
2,6-Dinitrotoluene
BRL
0.33
mg/kg wet
2-Chloronaphthalene
BRL
0.33
mg/kg wet
2-Chlorophenol
BRL
0.33
mg/kg wet
2-Methyl naphthalene
BRL
0.33
mg/kg wet
2-Methylphenol
BRL
0.33
mg/kg wet
2-Nitrophenol
BRL
0.33
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.33
mg/kg wet
3/4-Methyl phenol
BRL
0.33
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
0.33
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.33
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
0.33
mg/kg wet
4-Nitrophenol
BRL
0.33
mg/kg wet
Acenaphthene
BRL
0.33
mg/kg wet
Acenaphthylene
BRL
0.33
mg/kg wet
Anthracene
BRL
0.33
mg/kg wet
Azobenzene
BRL
0.33
mg/kg wet
Benzo(a)anthracene
BRL
0.33
mg/kg wet
Benzo(a)pyrene
BRL
0.33
mg/kg wet
Benzo(b)fluoranthene
BRL
0.33
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.33
mg/kg wet
Benzo(k)fluoranthene
BRL
0.33
mg/kg wet
Benzoic Acid
BRL
0.33
mg/kg wet
Benzyl alcohol
BRL
0.33
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.33
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.33
mg/kg wet
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.33
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.33
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.33
mg/kg wet
Dibenzofuran
BRL
0.33
mg/kg wet
Diethyl phthalate
BRL
0.33
mg/kg wet
Dimethyl phthalate
BRL
0.33
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO261 - 3546
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9CO261-BLK1)
Prepared & Analyzed: 03/15/19
Di-n-butyl phthalate
BRL
0.33
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.33
mg/kg wet
Fluorene
BRL
0.33
mg/kg wet
Hexachlorobenzene
BRL
0.33
mg/kg wet
Hexachlorobutadiene
BRL
0.33
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.33
mg/kg wet
Hexachloroethane
BRL
0.33
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.33
mg/kg wet
Isophorone
BRL
0.33
mg/kg wet
Naphthalene
BRL
0.33
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.33
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.33
mg/kg wet
Pentachlorophenol
BRL
0.33
mg/kg wet
Phenanthrene
BRL
0.33
mg/kg wet
Phenol
BRL
0.33
mg/kg wet
Pyrene
BRL
0.33
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
2.91
mg/kg wet
3.333
87
39-132
Surrogate: 2-Fluorobiphenyl
1.44
mg/kg wet
1.667
86
44-115
Surrogate: 2-Fluorophenol
2.66
mg/kg wet
3.333
80
35-115
Surrogate: Nitrobenzene-d5
1.21
mg/kg wet
1.667
72
37-122
Surrogate: Phenol-d5
2.69
mg/kg wet
3.333
81
34-121
Surrogate: Terphenyl-d14
1.62
mg/kg wet
1.667
97
54-127
LCS (P9CO261-113SI)
Prepared & Analyzed: 03/15/19
1,2,4-Trichlorobenzene
1.18
0.33
mg/kg wet
1.667
71
34-118
1,2-Dichlorobenzene
1.17
0.33
mg/kg wet
1.667
70
33-117
1,3-Dichlorobenzene
1.11
0.33
mg/kg wet
1.667
67
30-115
1,4-Dichlorobenzene
1.12
0.33
mg/kg wet
1.667
67
31-115
1-Methyl naphthalene
1.30
0.33
mg/kg wet
1.667
78
40-119
2,4,5-Trichlorophenol
1.49
0.33
mg/kg wet
1.667
89
62-124
2,4,6-Trichlorophenol
1.54
0.33
mg/kg wet
1.667
92
39-126
2,4-Dichlorophenol
1.30
0.33
mg/kg wet
1.667
78
40-122
2,4-Dimethylphenol
1.72
0.33
mg/kg wet
1.667
103
30-127
2,4-Dinitrophenol
0.687
0.33
mg/kg wet
1.667
41
27-129
2,4-Dinitrotoluene
1.53
0.33
mg/kg wet
1.667
92
48-126
2,6-Dinitrotoluene
1.57
0.33
mg/kg wet
1.667
94
46-124
2-Chloronaphthalene
1.47
0.33
mg/kg wet
1.667
88
41-114
2-Chlorophenol
1.40
0.33
mg/kg wet
1.667
84
34-121
2-Methyl naphthalene
1.26
0.33
mg/kg wet
1.667
75
38-122
2-Methylphenol
1.48
0.33
mg/kg wet
1.667
89
32-122
2-Nitrophenol
1.18
0.33
mg/kg wet
1.667
71
36-123
3,3'-Dichlorobenzidine
1.65
0.33
mg/kg wet
1.667
99
22-121
3/4-Methyl phenol
1.34
0.33
mg/kg wet
1.667
80
34-119
4,6-Dinitro-2-methylphenol
1.21
0.33
mg/kg wet
1.667
73
29-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO261 - 3546
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (M0261-113SI)
Prepared & Analyzed: 03/15/19
4-Bromophenyl phenyl ether
1.57
0.33
mg/kg wet
1.667
94
46-124
4-Chloro-3-methylphenol
1.38
0.33
mg/kg wet
1.667
83
45-122
4-Chloroaniline
1.32
0.33
mg/kg wet
1.667
79
17-106
4-Chlorophenyl phenyl ether
1.55
0.33
mg/kg wet
1.667
93
45-121
4-Nitrophenol
1.51
0.33
mg/kg wet
1.667
91
30-132
Acenaphthene
1.49
0.33
mg/kg wet
1.667
90
40-123
Acenaphthylene
1.51
0.33
mg/kg wet
1.667
91
32-132
Anthracene
1.73
0.33
mg/kg wet
1.667
104
47-123
Azobenzene
1.60
0.33
mg/kg wet
1.667
96
39-125
Benzo(a)anthracene
1.64
0.33
mg/kg wet
1.667
98
49-126
Benzo(a)pyrene
1.70
0.33
mg/kg wet
1.667
102
45-129
Benzo(b)fluoranthene
1.63
0.33
mg/kg wet
1.667
98
45-132
Benzo(g,h,i)perylene
1.67
0.33
mg/kg wet
1.667
100
43-134
Benzo(k)fluoranthene
1.79
0.33
mg/kg wet
1.667
108
47-132
Benzoic Acid
0.419
0.33
mg/kg wet
1.667
25
10-83
Benzyl alcohol
1.41
0.33
mg/kg wet
1.667
84
29-122
bis(2-Chloroethoxy)methane
1.26
0.33
mg/kg wet
1.667
76
36-121
Bis(2-Chloroethyl)ether
1.20
0.33
mg/kg wet
1.667
72
31-120
Bis(2-chloroisopropyl)ether
1.27
0.33
mg/kg wet
1.667
76
33-131
Bis(2-Ethylhexyl)phthalate
1.66
0.33
mg/kg wet
1.667
100
51-133
Butyl benzyl phthalate
1.67
0.33
mg/kg wet
1.667
100
48-132
Chrysene
1.67
0.33
mg/kg wet
1.667
100
50-124
Dibenzo(a,h)anthracene
1.28
0.33
mg/kg wet
1.667
77
45-134
Dibenzofuran
1.51
0.33
mg/kg wet
1.667
91
44-120
Diethyl phthalate
1.60
0.33
mg/kg wet
1.667
96
50-124
Dimethyl phthalate
1.58
0.33
mg/kg wet
1.667
95
48-124
Di-n-butyl phthalate
1.66
0.33
mg/kg wet
1.667
100
51-128
Di-n-octyl phthalate
1.70
0.33
mg/kg wet
1.667
102
45-140
Fluoranthene
1.66
0.33
mg/kg wet
1.667
99
50-127
Fluorene
1.61
0.33
mg/kg wet
1.667
97
43-125
Hexachlorobenzene
1.54
0.33
mg/kg wet
1.667
92
45-122
Hexachlorobutadiene
1.21
0.33
mg/kg wet
1.667
72
32-123
Hexachlorocyclopentadiene
1.36
0.33
mg/kg wet
1.667
82
32-117
Hexachloroethane
1.09
0.33
mg/kg wet
1.667
66
28-117
Indeno(1,2,3-cd)pyrene
1.92
0.33
mg/kg wet
1.667
115
45-133
Isophorone
1.23
0.33
mg/kg wet
1.667
74
30-122
Naphthalene
1.21
0.33
mg/kg wet
1.667
72
35-123
Nitrobenzene
1.18
0.33
mg/kg wet
1.667
71
34-122
N-Nitroso-di-n-propylamine
1.31
0.33
mg/kg wet
1.667
78
36-120
N-Nitrosodiphenylamine
1.92
0.33
mg/kg wet
1.667
115
38-127
Pentachlorophenol
1.04
0.33
mg/kg wet
1.667
63
25-133
Phenanthrene
1.66
0.33
mg/kg wet
1.667
100
50-121
Phenol
1.47
0.33
mg/kg wet
1.667
88
34-121
Pyrene
1.69
0.33
mg/kg wet
1.667
101
47-127
Pyridine
0.813
0.33
mg/kg wet
1.667
49
10-60
Surrogate: 2,4,6-Tribromophenol
3.05
mg/kg wet
3.333
91
39-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9CO261 - 3546
Reporting
Result Limit Units
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9CO261-BS1)
Prepared & Analyzed: 03/15/19
Surrogate: 2-Fluorobiphenyl
1.51
mg/kg wet
1.667
91
44-115
Surrogate: 2-Fluorophenol
2.84
mg/kg wet
3.333
85
35-115
Surrogate: Nitrobenzene-d5
1.20
mg/kg wet
1.667
72
37-122
Surrogate: Phenol-d5
2.79
mg/kg wet
3.333
84
34-121
Surrogate: Terphenyl-d14
1.67
mg/kg wet
1.667
100
54-127
LCS Dup (M0261-13SD1)
Prepared & Analyzed: 03/15/19
1,2,4-Trichlorobenzene
1.15
0.33
mg/kg wet
1.667
69
34-118
3
20
1,2-Dichlorobenzene
1.15
0.33
mg/kg wet
1.667
69
33-117
1
20
1,3-Dichlorobenzene
1.11
0.33
mg/kg wet
1.667
67
30-115
0.2
20
1,4-Dichlorobenzene
1.14
0.33
mg/kg wet
1.667
68
31-115
2
20
1-Methyl naphthalene
1.26
0.33
mg/kg wet
1.667
76
40-119
2
20
2,4,5-Trichlorophenol
1.35
0.33
mg/kg wet
1.667
81
62-124
10
20
2,4,6-Trichlorophenol
1.43
0.33
mg/kg wet
1.667
86
39-126
7
20
2,4-Dichlorophenol
1.26
0.33
mg/kg wet
1.667
76
40-122
3
20
2,4-Dimethylphenol
1.67
0.33
mg/kg wet
1.667
100
30-127
3
20
2,4-Dinitrophenol
0.512
0.33
mg/kg wet
1.667
31
27-129
29
20 D
2,4-Dinitrotoluene
1.40
0.33
mg/kg wet
1.667
84
48-126
9
20
2,6-Dinitrotoluene
1.45
0.33
mg/kg wet
1.667
87
46-124
8
20
2-Chloronaphthalene
1.42
0.33
mg/kg wet
1.667
85
41-114
3
20
2-Chlorophenol
1.43
0.33
mg/kg wet
1.667
86
34-121
2
20
2-Methyl naphthalene
1.22
0.33
mg/kg wet
1.667
73
38-122
3
20
2-Methylphenol
1.46
0.33
mg/kg wet
1.667
87
32-122
2
20
2-Nitrophenol
1.14
0.33
mg/kg wet
1.667
68
36-123
3
20
3,3'-Dichlorobenzidine
1.50
0.33
mg/kg wet
1.667
90
22-121
9
20
3/4-Methyl phenol
1.31
0.33
mg/kg wet
1.667
79
34-119
2
20
4,6-Dinitro-2-methylphenol
0.965
0.33
mg/kg wet
1.667
58
29-132
23
20 D
4-Bromophenyl phenyl ether
1.41
0.33
mg/kg wet
1.667
85
46-124
10
20
4-Chloro-3-methylphenol
1.28
0.33
mg/kg wet
1.667
77
45-122
7
20
4-Chloroaniline
1.27
0.33
mg/kg wet
1.667
76
17-106
4
20
4-Chlorophenyl phenyl ether
1.45
0.33
mg/kg wet
1.667
87
45-121
7
20
4-Nitrophenol
1.32
0.33
mg/kg wet
1.667
79
30-132
14
20
Acenaphthene
1.41
0.33
mg/kg wet
1.667
85
40-123
5
20
Acenaphthylene
1.45
0.33
mg/kg wet
1.667
87
32-132
4
20
Anthracene
1.54
0.33
mg/kg wet
1.667
92
47-123
12
20
Azobenzene
1.47
0.33
mg/kg wet
1.667
88
39-125
8
20
Benzo(a)anthracene
1.47
0.33
mg/kg wet
1.667
88
49-126
11
20
Benzo(a)pyrene
1.52
0.33
mg/kg wet
1.667
91
45-129
11
20
Benzo(b)fluoranthene
1.45
0.33
mg/kg wet
1.667
87
45-132
12
20
Benzo(g,h,i)perylene
1.49
0.33
mg/kg wet
1.667
90
43-134
11
20
Benzo(k)fluoranthene
1.56
0.33
mg/kg wet
1.667
93
47-132
14
20
Benzoic Acid
0.431
0.33
mg/kg wet
1.667
26
10-83
3
20
Benzyl alcohol
1.38
0.33
mg/kg wet
1.667
83
29-122
2
20
bis(2-Chloroethoxy)methane
1.25
0.33
mg/kg wet
1.667
75
36-121
1
20
Bis(2-Chloroethyl)ether
1.16
0.33
mg/kg wet
1.667
69
31-120
4
20
Bis(2-chloroisopropyl)ether
1.27
0.33
mg/kg wet
1.667
76
33-131
0.7
20
Bis(2-Ethylhexyl)phthalate
1.48
0.33
mg/kg wet
1.667
89
51-133
12
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030248
Attn: Chris Orrell Time Submitted: 3/14/2019 12:25:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9CO261 - 3546
LCS Dup (P9CO261-BSD1)
Prepared & Analyzed: 03/15/19
Butyl benzyl phthalate
1.45
0.33
mg/kg wet
1.667
87
48-132
14
20
Chrysene
1.49
0.33
mg/kg wet
1.667
89
50-124
11
20
Dibenzo(a,h)anthracene
1.32
0.33
mg/kg wet
1.667
79
45-134
3
20
Dibenzofuran
1.41
0.33
mg/kg wet
1.667
85
44-120
7
20
Diethyl phthalate
1.47
0.33
mg/kg wet
1.667
88
50-124
9
20
Dimethyl phthalate
1.45
0.33
mg/kg wet
1.667
87
48-124
8
20
Di-n-butyl phthalate
1.48
0.33
mg/kg wet
1.667
89
51-128
12
20
Di-n-octyl phthalate
1.49
0.33
mg/kg wet
1.667
89
45-140
13
20
Fluoranthene
1.47
0.33
mg/kg wet
1.667
88
50-127
12
20
Fluorene
1.49
0.33
mg/kg wet
1.667
90
43-125
7
20
Hexachlorobenzene
1.40
0.33
mg/kg wet
1.667
84
45-122
9
20
Hexachlorobutadiene
1.18
0.33
mg/kg wet
1.667
71
32-123
2
20
Hexachlorocyclopentadiene
1.29
0.33
mg/kg wet
1.667
77
32-117
6
20
Hexachloroethane
1.13
0.33
mg/kg wet
1.667
68
28-117
3
20
Indeno(1,2,3-cd)pyrene
1.76
0.33
mg/kg wet
1.667
106
45-133
8
20
Isophorone
1.18
0.33
mg/kg wet
1.667
71
30-122
5
20
Naphthalene
1.18
0.33
mg/kg wet
1.667
71
35-123
2
20
Nitrobenzene
1.17
0.33
mg/kg wet
1.667
70
34-122
0.4
20
N-Nitroso-di-n-propylamine
1.28
0.33
mg/kg wet
1.667
77
36-120
2
20
N-Nitrosodiphenylamine
1.72
0.33
mg/kg wet
1.667
103
38-127
11
20
Pentachlorophenol
0.831
0.33
mg/kg wet
1.667
50
25-133
23
20 D
Phenanthrene
1.52
0.33
mg/kg wet
1.667
91
50-121
9
20
Phenol
1.48
0.33
mg/kg wet
1.667
89
34-121
0.7
20
Pyrene
1.49
0.33
mg/kg wet
1.667
89
47-127
13
20
Pyridine
0.871
0.33
mg/kg wet
1.667
52
10-60
7
20
Surrogate: 2,4,6-Tribromophenol
2.62
mg/kg wet
3.333
79
39-132
Surrogate: 2-Fluorobiphenyl
1.41
mg/kg wet
1.667
84
44-115
Surrogate: 2-Fluorophenol
2.74
mg/kg wet
3.333
82
35-115
Surrogate: Nitrobenzene-d5
1.13
mg/kg wet
1.667
68
37-122
Surrogate: Phenol-d5
2.71
mg/kg wet
3.333
81
34-121
Surrogate: Terphenyl-d14
1.46
mg/kg wet
1.667
88
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 24 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead Prism Work Order: 9030248
Attn: Chris Orrell Time Submitted: 3/14/2019 12:25:OOPM
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9C0199 - MADEP VPH (S)
Blank (P9C0199-BLK1)
Prepared: 03/13/19 Analyzed: 03/14/19
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl2 Aliphatics
1.32
5.0
mg/kg wet
J
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
9450
ug/L
10000 95 70-130
Surrogate: 2,5-Dibromotoluene (FID)
10200
ug/L
10000 102 70-130
LCS (P9C0199-BSI)
Prepared: 03/13/19 Analyzed: 03/14/19
C5-C8 Aliphatics
37.3
5.0
mg/kg wet
32.00 117 70-130
C9-Cl0 Aromatics
10.6
5.0
mg/kg wet
10.67 100 70-130
C9-Cl2 Aliphatic
32.3
5.0
mg/kg wet
32.00 101 70-130
Surrogate: 2,5-Dibromotoluene (PID)
8890
ug/L
10000 89 70-130
Surrogate: 2,5-Dibromotoluene (FID)
9670
ug/L
10000 97 70-130
LCS Dup (P9C0199-BSD1)
Prepared: 03/13/19 Analyzed: 03/14/19
C5-C8 Aliphatics
34.5
5.0
mg/kg wet
32.00 108 70-130 8 50
C9-Cl0 Aromatics
10.4
5.0
mg/kg wet
10.67 97 70-130 2 50
C9-Cl2 Aliphatic
31.2
5.0
mg/kg wet
32.00 97 70-130 4 50
Surrogate: 2,5-Dibromotoluene (PID)
8630
ug/L
10000 86 70-130
Surrogate: 2,5-Dibromotoluene (FID)
9450
ug/L
10000 95 70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 25 of 28

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
3/18/19
ECS Carolinas, LLP (Charlotte) Project: W. Morehead
Attn: Chris Orrell
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Reporting
Analyte Result Limit Units
Batch P9CO262 - 3546
Prism Work Order: 9030248
Time Submitted: 3/14/2019 12:25:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9CO262-BLK1)
Prepared & Analyzed: 03/15/19
C9-Cl8 Aliphatics
BRL
25
mg/kg wet
C19-C36 Aliphatics
BRL
25
mg/kg wet
C11-C22 Aromatics
BRL
10
mg/kg wet
Surrogate: 1-Chlorooctadecane
1.33
mg/kg wet
2.000 66
40-140
Surrogate: o-Terphenyl
1.58
mg/kg wet
2.000 79
40-140
Surrogate: 2-Fluorobiphenyl
3.81
mg/kg wet
4.000 95
40-140
Surrogate: 2-Bromonaphthalene
3.72
mg/kg wet
4.000 93
40-140
LCS (M0262-13SI)
Prepared & Analyzed: 03/15/19
C9-Cl8 Aliphatics
43.7
25
mg/kg wet
60.00 73
40-140
C19-C36 Aliphatics
83.7
25
mg/kg wet
80.00 105
40-140
C11-C22 Aromatics
194
10
mg/kg wet
170.0 114
40-140
Surrogate: 1-Chlorooctadecane
1.66
mg/kg wet
2.000 83
40-140
Surrogate: o-Terphenyl
1.98
mg/kg wet
2.000 99
40-140
Surrogate: 2-Fluorobiphenyl
4.46
mg/kg wet
4.000 112
40-140
Surrogate: 2-Bromonaphthalene
4.13
mg/kg wet
4.000 103
40-140
LCS Dup (P9CO262-BSD1)
Prepared & Analyzed: 03/15/19
C9-Cl8 Aliphatics
46.9
25
mg/kg wet
60.00 78
40-140 7 50
C19-C36 Aliphatics
89.1
25
mg/kg wet
80.00 ill
40-140 6 50
C11-C22 Aromatics
191
10
mg/kg wet
170.0 112
40-140 2 50
Surrogate: 1-Chlorooctadecane
1.67
mg/kg wet
2.000 83
40-140
Surrogate: o-Terphenyl
1.85
mg/kg wet
2.000 93
40-140
Surrogate: 2-Fluorobiphenyl
3.80
mg/kg wet
4.000 95
40-140
Surrogate: 2-Bromonaphthalene
3.49
mg/kg wet
4.000 87
40-140
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 26 of 28

Sample Extraction Data
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
9030248-01
P9CO262
10.05 g
2 mL
03/15/19 9:30
9030248-02
P9CO262
10.1 g
2 mL
03/15/19 9:30
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
9030248-01
P9CO281
30 g
30 g
03/15/19 16:22
9030248-02
P9CO281
30 g
30 g
03/15/19 16:22
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
9030248-01
P9CO261
30.07 g
1 mL
03/15/19 9:30
9030248-02
P9CO261
30.03 g
1 mL
03/15/19 9:30
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
9030248-01
P9CO277
5.12 g
5 mL
03/14/19 12:57
9030248-02
P9CO277
4.5 g
5 mL
03/14/19 12:57
Prep Method: MADEP VPH (S)
Lab Number
Batch
Initial
Final
Date/Time
9030248-01
P9C0199
5.03 g
16 mL
03/14/19 12:23
9030248-02
P9C0199
4.43 g
16 mL
03/14/19 12:23
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 28

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S
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asp
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1
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By (Print Name)RhJl Affiliation
Upon relinquishing, this Chain of Custody is your authorization
for Prism to proceed with the analyses as requested above. Any changes must be
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NF Ur-b. U7 I: UKUUNLIVVAI tK: I L1K514AI14l7VVAI r_K: ,ULILI VVAS I t: KtoKA: LLLKI-LA LANUrILL I U I NIMIK:
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ORIGINAL

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC W IGH ASTER
LICENSE E� NE 304267Z
J NO
IN LI NLESS SIGNED
i XT uA 7Annnrra WASTE MANIFEST
Project Number: V
Load Number:
'a 113 Li
Consultant
Contact: ,
C G
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight 02[ W 440 1
H0.19
Tare Weight: 27130 lb TR RECAL'.
Net Weight:
T
Generator's Certitication: i ce'nty mat me marerrms oescrnoeu auovo ou �..� ...a...��• W ••�•
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material:
Drivers Signature Date
Noted Discrepancies:
Inspected & Ace ed (except as not d above by: AES of NC)
Accepted By �� Date:

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
A 04:13Pro 02/06/2019
N P �P left20 q 248 ID. N0.
d�NEg ,4V12 64120 lb uR
Q
-L\CEfB p6G gtGNEO
)GE \3N�E55
1pvP
v v♦ v♦ nnnrm W A STR MANTFRST
Project Number:
Load Number:
Consultant
Contact:
GCPhone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #: 6 2-Grass
Weight: 04:26Pre 02/06/2019
248 ID- NO
Tare Weight: 64120 lb aR RECAL:.:
23 lb TR
Net Weight: 373'• lh NT
Generator's Certification: 1 certity mat the marenais aescnueu nwvc
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
IN
Generator / Agent Signature �`�j�tie Date
Acknowledgment of Receipt of Material{�A �+�.. n .��_ Oofb
Drivers Signature Vale
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC) Q
Accepted By: Z,�— Date: �— —

AES ofNC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
N
TN LINA
ASTER
pUBLI
DUNE 1041671
LICENSE
JOE F. N
0
Slow
1W
UNLESS
nrnx uA 7 Avnnrtc W A.CTF. MANIFEST
Project Nurnber:
Load Number:
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd, Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #: L ^ l O
T• l
Gross Weight:
Tare Weight: 04:52pm 02/06/2019
Net Weight: 65420 lb fiR
26 lb TR RECAL.
39720 Ib NT
I
Generator's Certification: I certify that the materials described above on this mamf st are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title D
Acknowledgment of Receipt of Materi
r re Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Date:
Accepted By: 1� ! I

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone 4: 336-481-9777
NORT AR01.10,EB
PUBLIC 5 30, 301:
UCENSEp DER �;
dU6 F.H gg g16
INVAUO NL ,
w.nwr u A o A nnnrrs W ARTF MANIFEST
Project Number:
Load Number:
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
K- 3�
Gross Weight: 240 ID. NO.
63320 Ili LR
Tare Weight 2,
359M lb HT
Net Weight: S
Generator's Certification: I certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material: z-4, —?q
r' i, ature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
r
Accepted By: Date:

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMAS'r
LICENSEE) IRES E70, Z019
612
JOE F. HOL
INyAL UNLESS SIGNED
.anv aA7AV7H11TC VVACTF. MANIFEST
Load Number:
Project Number:
at3J -'SD
Consultant
Contact:
Phone:
erator.
ontact:
Phone:
reasporter:
anted:
Phone:
eshuatron: a
3841 Cudnidgham Rd., lkomasville, NC
mdact Scott er r e a
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste originafton:
Truck
Gross Weight:
Tare Weight:
at eig t
.g
Generator's Certificahon: 1 certily that me matmars described abdve w dd= ...m. .—
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE -
Acknowledgment
Noted Discrepancies:
Inspected & Accepted (dtcept as
AcceptedBy:- t;4,,I Date:_

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
30, 2019
42612
ogre xv A c9`F. MANiFFRT
lvVrv-nnre VUN
—.----..--_..-----
Load Number:
Project Number:
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller
/ Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight:
05:26pm 02/05/2019
-K-
244 ID. 40•
Tare Weight:
64200 lb GR
27180 ib TR RECPL'..
Net Weight:
Generator's Certification: 1 cenIty that the matertais oescnoeu auuvc ou
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title,,,,Date
Acknowledgment of Receipt of Material:
Driver gna ure Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: 02, Date: 2 -6 r-/

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PURLIC WEIOHMASTER
LIC EXPfR JUNE 30, 2019 9J HO 42672
INYA IE UNLESS SIGNED
.ro. tt• M t
Project Number:
Load Number:
�I13N-7D �
Consultant
Contact
Phone:
erator:Contact:
Phone:
Transporter:
contact,
Phone:
est ahan: AES of NC
Contact Scott Keller e Holder
3841 Cunningham Rd., Thomesville, NC
phone: [phone] m 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight:
p
k �D
an
Tare Weight:
-%,00
et erg t: - .- „
Generator's Certi6cati= I certify that the materials described above oo this m,rest we not
subject to federal regulations far reporting proper disposal of HAZARDOUS WASTE.
Generator/ Agent Signature Title Date
Acknowledgment of Receipt of Material: — -
Title
re. Date
Noted Discr�paacies:
Inspected &Accepted (except as noto above by: M of )
AcceptedBy;,� Dow 7

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone#: [phone]
NORTH CAROLINA
P BLIC W IG ASTER
LI E EX JUNE 30,42�Z
HO _
INV LID UNLESS SIGNED,
Wnx u A 7 A unn1TR W ASTF MANIFEST
Project Number:
Load Number:
o 11.30
Consultant
Contact:
De
1&
C)
Phone: JPX
C
Generator:
Contact: "
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Fmnkie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone]
or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight
10:53aN 02/07/2019
K 3�6.
Tare Weight:
64800 16 0R
2180 lb TR REC91
Net Weight:
37620 lb HT
loll
Generator's Certification: I certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature it ,,P' Date
Acknowledgment of Receipt of Material:
Drive Tgnature Date -
Noted Discrepancies:
Inspected & Accepted (excepjt as noted above by: AES of NC)
Accepted By: Y Date: off/

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LI SE Ej(PI ES JUNE 30, 2019
H 42672
IN L UNLESS SIGNEQ
NON HAZARDOUS WASTE MANIFEST
Load Number:
Project Number:
1139 -"To
Consultant
aT
Contact:
Phone: E f'4' I I I S e4Z'.--
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight: 12: 40vre 02/0711?019
2P TO fie
Tare Weight: 65NO lb 6R
Net Weight: 73240 lb NT
Is
Generator's Certification: I certify that the materials described above on mis manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature ' le �DateAcknowledgment of Receipt of Material; irivers Signature
Noted Discn
Inspected &
Accepted By:
of NC)
Date: Qe7 l

NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30,2
JOE F. HOLDER
INVALID S8IGNEC
AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
onrvrre W A CTPi MANrFRRT
Load Number:
Project Number:
113y --j0
T
Contact: __
Phone:
Fr —
Contact:
rDestination:
Phone:
r:
Contact:
Phone:
AES of NC
Contact: Scott Keller
/ Frankie Holder
unningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck#: _
Gross Weight:
I `T,D• No.
Tare Weight:
27130 lb TR RECA .-
38620 lb HT
Net Weight:
( � 31 4��5
Generator's Certification: I certify that the materials cescnoec aoove on uus ulmu vc i
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material:
Drivers lure e
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By:Date:�9

z
:cc 4NC
post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGH ASTER
LIREfJ5E EX RE NE 36, 2619
J HOLdE 4267:
INVALID UNLESS SIGNED
NON_HAZARDOUS WASTE. MANMST
project Number:
LoadNumber:
z��34 -SD
Consultant (l n `(
Contact:
Phone:
-Generator
ontact
Phone:
ransporter:
ontact:
Phone:
eshnahaa: o
3841 Cemoingh m Rd., Thocuesville, NC
otdact colt Of e
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #: I
Gross Weight:
Tare Weight:
New erg t: -- i
Generator's Cerfificahon: 1 cemry out on mnenals de —Aced avo.e ,.._...._ ...-•••___• —_ --
subject to federal relialion, for repotting proper disposal of HAZARDOUS WASTE.
Generator! Agent Signature 'tle Date
Acknowledgment of Receipt of Material:
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepted (ex as noted above by: AES of NC)
Accepted By: . / Date

NOP," EA HMASTER
PUB CAW SJUNE 30, 2019
O.ICENSE Ift 42672
90E F. NO
INY I UNLESS SIGNED
AES of NC
Post Office Box 310
Sanford NC 27331
Phone #: [phone]
wT w rsav AVnnirC WACTF MANInST
Project Number: yv —
LoadNumher:
Consultant
Contact:
Phone:
Generator. C C I
l
ontact:
Phone:
ransporter:
ontact:
Phone:
eshaahon: a
3941 Cunningham Rd., Thomasville, NC
ontact: colt er i e Holder
Phone: [phone] or 919-770-7705
27360
Waste Description:
waste Or g nd nn:
Truck #:
Gross Weight:
k-3ca
Tare Weight: '
( b-
et eight:
Generator"s Cerhhcana¢ 1 cemry mar the meac..n u.». ......
•�
subject to federal r atioos for reporting proper disposal of HAZARDOUS WASTE
orator/AgmtSignature Tit Date
Acknowledgment of Receipt of Material: ^Qs
Inspected & Accepted (except as noted at)Wt oy: A k v5 or lv�/
Accepted By: J

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
NGN ,NEIGH g02010
P�B�t Xpt ESd g207g
Lie se
SOH I Llg UHLEss
NON -HAZARDOUS WASTE MANIFEST
Project Number: _3U
Load Number:
Consultant
Contact:
9 siz°Fw-
L
Phone:
erator.
Contact:
Phone:
ransporter:
ontact:
Phone:
eshaahun: AES oFAU
Contact Scott Keller I Ffankie
Holder
3841 Cunningham Rd., Thumamfle, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck#: '/3b
Gross eight
c
/,
Tare Weigh':
et et t:
-4V _„ ,-
4 3i 70
Generator's Cerhticahoo: 1 certify that the matenals described above on Has ma lest we not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator! Agent Signature Title Date
Acknowledgment of Receipt of Material:
rivet!,§, gm sure 5We
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of C)
Accepted By: / Date:

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NON-HAZARDOITS WASTE MANIFEST
Project Number:
tlri aot
oadNumber:
l
Consultant
Contact: i
C�
Phone:
erator.
ontact:
Phone:
ransporter:Contact:
Phone:
f
3941 Cuooingh ro Rd,, Thorne W-, NC
ornactSeaffireller rm Td-
Phone: [phone] m 919-770-7705
27360
Waste Description:
Waste Orig nation:
Truck #: 2
i
Gross eeght:
Tare Weight:
at Weight:
fest
Gmeratm's Certi6catios I certitythat the outenals desenbed above oo s mm� are
subject to feduaUggulations for reporting proper disposal of HAZARDOUS WASTE.
,2
erator / Agent Signature Title Date
Acknowledgment of Receipt of Material: _ 2
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepted (except as nMe ova )
Accepted By: Date: �

N04TN CAROLI yAEi2
o
PUBI-IC Vd'clG� Utd"'30, 3074
LICENSE S�%T qE,5 g2672
JOE F. HO'_JE
INVALID E S S GNED
AES of NC
Post Office Sox 310
Sanford, NC 27331
Phone #:[phone]
NnN_RA7.ARnOUS WASTE MANIFEST
Project Number:---
Load Number:
Consultant
Contact:
Phone:
Bator:
ontact:
Phone:
ransporter:
ontact:
Phone:
eshnahm: Anh o
odact Mott miler i Frankie Tiolder
3841 Cmoidghem Rd., Thomasville, NC
Phone. [phone] m 919-770-7705
27360
Waste Description:
Waste Orig nation:
Truck
K1D
I Gross Weigle':
Tare Weight:
et erg t:
Iq
Generator's Ceetificaho¢ 1 cerhry nut the mutants described above m ens d..d...­ m. —.
subject to federal regulations for reporting Proper disposal of HAZARDOUS WASTE.
+v
erator/ ntSignature r Date
Acknowledgment of Receipt of Material:
rive gnature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: of 1
Accepted By: Date: L��
4a"

NORTN CA30� c IER
PU"LVC
LICENSE E�, :i ' iE $u,
J0E F• "U"
1tp1At1 U SS 816
AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NON -HAZARDOUS WASTE MANLIEST
Project Number:
Load Number:
Consultant
C(ZA
Contact:
Phone:
—GEerator.Contact:
Phone:
Transporter:Contact:
Phone
estination: AES oFNC
ct colt er)
e Hiolder
3841 Cuomnshem Rd., Thomasville, NC
Phone: [phone] m 919-770-7705
27360
W as[e Description:
Waste Orlginahon:
Truck#:
Gross eight:
Tare eight:Kj-
AL
Net t:
L ( 125 'lfl
Generetor's C.erhncanon: 1 cemty that the matena's cesmoeo aoove uu vas u.vuaaex m= ....
mx
alions for reporting proper disposalofHAZARDOUS WASTE
.
Generator AgentSignature Title Date
Acknowledgment of Receipt of Material:
Drivers Sighature Date
Noted Discrepancies:
Inspected & Accepted (except as noted aab(
bove AES o C) q
Accepted By: �9 0 - Date: �—,—I

NORTH GAR M I $TER
PUBLIC E30,�2
LICENSE Ell E
JOE F. HGLUER
INVALIC 'N
E55 SIGNED
AESofNC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
VAN_AA7.AIIflnTT% WASTE MANIFEST
Project Number: - -'
Load Number:
2 8Y-Sp
Consultant
Contact:
CCy
Phone:
gym.Contact:
Phone:
ransporta:Contact:
Phone:
shnahon: AES o
3841 Cttonioghem Rd., Thomasville, NC
ott9d: con er rankie Holder
phone: [phone] or 919-770-7705
27360
Waste Description:
Waste O iginahon:
Track #:
Gross We 4ht: _
Tare eight:
Net t:
Cmneratov's Cerbticahm 1 cemty mat me matena,s oesmee...rove w uo• ..•_.•••__. _•_ ••..•
wbiectto federal reg"ons for repotting proper disposal of HAZARDOUS WASTE.
Gegerator Agent Signature e �D e
Acknowledgment of Receipt of Material: T
ve ignature Datd
Noted Discrepancies:
Inspected & Accepted (except as noted abovi 1:13 of )
Accepted By: �' u D —i—�

NORTH
PUBLIC N
LICENSE EXPI
JOE F. HOADq
AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NON -HAZARDOUS WASTE MANIFEST
Project Number:
Load Number:
Consultant
Contact:
CC
Phone:
eratorContact:
Phone:
Transporter.
Contact
Phone:
Destination: AES a
fact Scaft er I Ff­za9e—T0'(Wf
3841 Cunningham Rd., Tho svihe, NC
Phone: [phone] w 919-770-7705
27360
a e Description:
Waste Origination:
Track #:
ross Weight:
Tare eight:
Net Weight:
13 �S i�J
---- - 's Certi6cahan: i certify that the materials desmbed above on tors --rest are nor
subject to Federal regulations Por reporting proper disposal of EL47ARDOUS WASTE.
Gletteriffor J Agent Signature Title Date ��� ��
Acknowledgment of Receipt of Material: ! T / J / t )
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By:Date: Z —��

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone#:[phone]
R& tN CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 30, 20G72
JOE F. HO DER
INV N ESSSIGNED
NON -HAZARDOUS WASTE MANIFEST
R vECiA..
Project Number:
ii
Load Number:
Consultant
C CZ
Contact:
Phone:
-Giiierffior.Contact:
Phone:
Transporter:Contact:
Phone:
eyydhun: AES afNC
3841 Cunningham Rd., llmmesvilte, NC
27360
C-on-fa-ctgcott K eller Fr2da e Hal
Phone: [phone] or 919-770-7705
Waste Description:
Waste Origination:
Tcueh #:
Gross weight
Tare Weight:
Net Weight:
�7r SrP n
Cm ator's Cerhhcahuu 1 cemty that the maim W s aescrroeu above ou mrs mamnsr are unr
subject to federal reostious for reporting proper disposal ofE AZ.4RDOUS WASTE.
Generator rMent Signature Tit �} ,D, ate
Arlmtm4edgment of Receipt of Material: �� ,t r
D ' s 5i ffiur Dat
Noted Discrepancies:
Inspected & Accepted (except as noted above �C)
Accepted By: -t4 L— t Fob^ Date: 5'/

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLKA
PUBLIC WEIGHMAST tt
T
NOES NE 0, 73 UNLE 5.1^.•"dEC
NON -HAZARDOUS WASTE MANIFEST
Project Number. ` r-
Load Number:
Consultant
Contact:
Phone:
erffior.
ontact:
Phone:
Transporter:Contact:
Phone:
Destination: AES of NU
3841 Cunningham Rd., Thomasville, NC
27360
Contact
Phone: [phone] or 919-770-7705
Waste Description:
Waste ongination:
Truck #: / I
V`
Gross Weight:
Tare Weight:
Net Weight:
i r
Generator's Certification: I certify that the materials described above on this manifest are not
subject to federal
regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator/Age�ntSr� a Dffie
Acknowledgment of Reeeipt of Material 2 `(
Drivers Signature Date
Noted Disutpancies:
Iaspeded As AAcccepted except as noted above by: AES o )
Accepted By: Date: 2" ` 17

1R" CAIMINA
p11SLIC WEtGHMASTE ga19
(,j�ENSE E7 IRE�1E
jot F.HOL
AES of NC IN UNLESS SIGNED
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
Nr1N-11A7.A2M11TS WASTE MANIFEST
19,a4 Mans
Project Number: - —-
4-
LaadNumber:
Consultant
CG
Contact:
Phone:
eratotContact:
Phone:
Transporter:Contact:
Phone:
eshnation: AES o
3941 Crmaingham Rd., Thomasville, NC
27360
Contact ScottKella/FrackieHolder
Phone: [phone] or 919-770-T705
Waste Description:
Waste Or g nation: -'T -,
Truck #:
Gross Weight:
Tare Weight:
et erg t:
Generator's Certification 1 cerhty UNt the u,uMA13 aesnroen aoove oa mrs oaaruresr are uvi
subject to &deral regulations for reporting proper disposal of HAZARDOUS WASTE.
Generators Agent Signature Title Date
Acknowledgment of Receipt of Material: -
D Iveirs Sipaure Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AFS of
Accepted By: , �.ta...1— 61Date: 2-a-ll

AESofNC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUN 30448T2
JOill
EF.H01 I<R--
INVA UNLESS SIGNED
NON -HAZARDOUS WASTE MANIFEST
Project Number: Load Number:
0-1134S -D
Consultant I ContactGen :
Phone:
orator.
o aect:
Phone:
ransporter:Contact:
Phone
emnation: AES oFNC
Catitact Scott Killer I Fraidde Holder
3841 Cuon vCham Rd., Thomesville, NC
Phone: [phone] ar 919-770-7705
27360
Waste Description:
Waste OVnal on:
Truck #:
Gross Weight:
_ s
Tare Weight:
Net Weight:
8D
Geaeratols Uerhbcaho 1 cerbry that the materials described above off tms Homiest are aot
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material:
Dritw Si re Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NQ
Accepted By: �.te l 156� Date: 2 5- l9
fig

AES of NC
Post CffceBox 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUN 30, 2019
JOE F. HOLD 2t j 4 &i2
INVALID NLESS SIGNED
ernx a A 7 ART%nTTC W ACTF. MANIFEST
Projec'Number:all _
Load Number:
_
Con"'
Content:
�^
`--C_
Phone:
erator..
ontact:
Phone:
Transporter,
ontact:
Phone:
Destination: ALS of NU
contact: ScottKeller/krankieHolder
3841 Cunningham Rd,, Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Goss Weight'
K-54
Tare Weight:
_
Net Weight:
l9,`f5
Generator's CeAacahon: t cer ttq that the ma[enats nestxtoeo above on uas man =e are vo.
subject to federal regulations for repotting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Titre Date
Acknowledgment of Receipt of Material: A�,�
Dri & s Signature Date
Noted Discrepancies:
Inspected & Accepted (except as note above by: of NC)
Accepted By: t�� _ Date: a'S�

AES of NC
Post Office Box 310
Sanford NC 27331
Phone #: [phone]
fAOWM CAROLINA
PUBLIC WEIGHMASTER
LICENSE XPIRES U E30q�8T2
JOE F. HO
INV D UNLESS SIDNED
NIIN-AA7Al2mTTC WA%TTP_MANEMST
ProjectNamber: — ---
LoadNamber:
Consultant
Contact:
CCT
Phone:
erator.Contact:
Phone:
ransporter:
ontact:
Phone:
esaaahon: AES of NC
Contact Scaftmner/riankiellolder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Originatton:
Truck #:
Gross Weight:
K- /d
Tare Weight:
Net Weight:
L $.
ator's Certification I certify that the matenals described above on tans mean es[ ere not
subject to federal regulations For reporting proper disposal of HAZARDOUS WASTE.
GeneratorI Agent Signature Tit Date
Acknowledgment of Receipt of Material:
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepts except as noted above
Accepted By: d rfa Date:
5

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LIC I E E7ES UNE 30, 2014
J .HO ,ER 42672
rr
INVALID UNLESS SIGNED
xnm ve7s12r1nN7C WA-CTE MANIFEST
Project Number: — ---
LoadNumbar:
aJl
Consultant
Contact:
Phone: :3-(a /S�r
erffiorContact:
Phone:
Transporter:
ontact:
Phone:
eshmhon: AES o
ombet Scott er I Ff—a—dE—e
3841 Cunningham Rd, Themtamile, NC
Phone: 919-VO4258 m 919-770-7M5
2736D
Waste Description:
Waste Origination:
Track
Gross Weight:
Tare Weight:
Net Weight:
ILIR0 ?QfIS
Generator's t:ernticaum : 1 cetnty tit me matemes aesenoen aoave on uvh a„c..,ea.
subject to federal regulations for repotting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Date „
Acknowledgment of Receipt ofMffienal: e /%'��---�- ii —
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepted (except as
Accepted By: Yze d4%..- Date:

NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE %PjRESJUNE3042019
JOHN GO F Y
673
AES of NC tN p UM;,zQQ SIGN6p
Post Dice Box 310
Sanford, NC 27331
Phone #:336A81-9777
N0N-HAZARD0US WASTE MAN> T
Project Number: Load Number ,
'/Its SO
Consultant
Contact:
C t t
Phone:
enerazor:
ontact:
Phone:
ransporter
ontact:
Phone:
eshnahon: o
ontact: Cott er
f e a
3841 Cumonghem Rd., Thomomfle, NC
Phone: [phone]
or 919-770-7705
27360
Waste Description:
Waste Origination:
ruck #:
mss Weight:
i
Tare Weight:
et erg t:
---- - --a —" ..._ Wove on Cuts —test ere not
subject to federal regulatiom for reporting proper disposal of HAZARDOUS WASTE
Generator / Agent Signature Ti Date
Acknowledgment of Receipt of Material:
Noted Disnaes: Drivers Signature Date
crepa
Inspected & Accepted (except as note above bv: . .1

AES of NC
Post Office Sox 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
J
LIC EXP E OUNE 30, 2019
F OL ,V_ 42111
INVALID UNLESS SIGNED
NON-E[A7ARDOUs WA.r.TF IUAXFFiF¢T
Project Number:
Load Number*
/ _
Fconsuftant
Contact:
Phone: aFF �qr
erator.
ontack
Phone:
raospofter:
ontact:
Phone:
eshnenon: °Contact
ScattYenerfr e
3841 Cunningham Rd., Thomasvike, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross welght..
1 AI
Tare Weight: _,
a
Net W it.
+ cv u+Y ma[ me uul[g1815 deaeribed above on aus ,,fast are not
subject to federal regulations for reporting proper dispos l of HAZARDOUS WASTE.
Generator/ Agent Signature Title D e
Acknowledgment of Receipt of Material: _�
. Drive tgnature Date'
Accepted $Yyy�, 4d `� Dater

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: 33"1-9777
NORTH CAROLINA
P BLIC WEIGHMASTER
LI E EX IR UNE 30, 2070
HO 42672
INVALID UNLESS SIGNED
• ;15 'ac II uas119 1
Project Number:
50
Load Number: —
Consultant
Contact:
Phone:j j(
Generatoi�'
Cont
Phone:
ransporter:
ontact:
Phone:
estmahon: AES of NC
T5iffe-t-rco-ftTM--77rianWe
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] m 919-770-7705
27360
Waste Description:
Waste Or(gtnaaon:
Truck #:
Gross welgw
k 3ia
Tare Weight:
et We1g t:
Tons
�_
-LL = «u•r W.. use matmais nescrroea some mums manliest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Acknowledgment
Generator ledgm ent of Receatureipt
Till D�
Aclmowledgment of Receipt of Material: /
tlatllfe
Noted Discrepancies: Driv tg
Inspected & Accepted except as pole we

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGH ASTER
rLIC EX JUNE 30, 2019
-J . HO 42672
INVALI NLESS SIGNED
10:35aN 02/04/2019
242 ID. 110.
71840 lb 13R
NON-HAZARDOTS WASTE. MANIEE,ST
Project Number: 113 _
Load Number:
Consultant
Contact: �G
F /3a ter
Phone:
Generator: -
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #: a S
Gross Weight:
10:51aH 02l04f2019
Tare Weight:
71a40 lb IiR RBCAL-'.
Net Weight:
45040 lb HT
52
Generator s Cerrmcanon: t cermy that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material: '/>7s,ils,./ �%,rio�lT- .2- y-/ 9
Drivers Signature Date
Noted Discrepancies: _
Inspected & Accepto i (except aspoted above by: AES of NC)
Accepted Byyly.,%_�,� Date: 024�

AES of INC NORTH CAROLINA
Post Office Box 310 PUBLIC WEIGHMASTER
Sanford, NC 27331 LICE SO`XPIyES NE30,2019
3042672
Phone #: [phone] kk
INVALI UNLESS SIGNED
N0N-3TA7Al2nr%TTe WAVE er..
Project Number: -- ---
Load Number-,
11 -30
Consultant
Contact:
CC^
Phone: Tyepp 11S,Pb�-r
ontact:
Phone -
transport
ontact:
Phone:
eshoatibn: o
3841 ��� ,Thomasville, NC
aotact olt er r e
Pie: 919-7704258 or 919-770-7705
27360
Waste Description:
Waste Orlgtnatlan:
Truck #:
Gross Weight:
Tare Weight:
et et t
U T S
Mims
b s] -vm above en ml5 mamtest are not
subject to federal regulations for reporting proper disposal IfE L7ARDOUS WASTE
Generator / Agent Signature Title Dat
Noted Diancies: Dal
Acknowledgment of Receipt of Material:
Dnvars Signahre Date
screp
Inspected& cepje exceptasnot e v

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGH ASTER
LIC SE EXP E NE 30, 2019
JP HOL 42672
1NVALIO UNLESS SIGNED
NON_11A7.A11nnrm WAg� x
Project Number:
Load Number:
13
Consultant
Contact:
CG
Phone: Te CL Pellmot.
ontact:
Phone:
ranspotter:
ontact:
Phone:
es On: o
3841 Cunningham Rd., T6omasYiUe, NC
outset on: of e
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origtnallon:
Truck #:
Cross Weight:
K
a
Tare Weight:
et et t
—ra xbeb above an ans mmtrest are net
mbject to fedefel re9W atiom for reporting proper disposal ofEAZARDOUS WASTE -
or I Agent Signature Title Date
Acknowledgment of Receipt of Material: e
Drivers Signature Dffie
Noted Discrepancies:
Inspected & Accepte except as note v: o
Accepted By:
Date:-��

AES ofNC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
P LIC INE HNI STER
LIC EXP S E 30, 2019
JO . HOL 42672
INVALID UNLESS SIGNED
NON -HAZARDOUS WASTE M
Project Number:
+L
Load Number:
Consultant PROGRESS ENVIRONMENT
Contact: JEFF BALLSIEPER
Phone: [phone]
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scoff Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
SOIL
UST GAS
Truck #:
Gross Weight
10:40ara 02l04/2019
Tare Weight: 68360 Ill GR
26700 Ib TR RECAL .
Net Weight: 41660 lb NT
l—L'Vn: r cemry mat me materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Ti Date
Acknowledgment of Receipt of Material: 1
rivers ignature Date
Noted Discrepancies:
Inspected & Accep d (exce rt as i led above by: AES of NC)
Accepted By: Date: a4Z
rT

AES of NC
Post Office Box 310
Sanford, NC 273:
Phone #:[phone]
NORTH CAROLINA
PUBLIC WEIGH STER
LICf E EXPI S NE 30, 2019
JQP: HOLD 42672
7��N-V-"ALIO UNLESS SIGNED
Project Number:
Load Number:
1I3 - C
Consultant
Contact:
6f
Phone: 5e''�
erator.
C ontact:
Phone-
ransporterContact:
Phone :
a Go: a
ontact can er e
3841 Cumtingham Rd, Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Orig nat on:
Truck #:
Gmss eight:
K 10
Tare Weight:
et erg t
»..��
aescrweo amve m tons manetest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator/ Agent Signature Tit Da
e
AcknoMMedgment of Receipt didaterial: — tee— '
tvers Stgaature Date
Noted Discrepancies:
Inspected & Accepted except as UWCU above bv� flT lNt.1
Accepted By:
Date_

AES dNC
Post Office Boa 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LIC SE EXPIRES JUNE 30, 2019
J' HO 42672
INVALID UNLESS SIGNED
NON-HA7.ARMTTC WSCTV XXAN vv
Project Number: ' ------
Load Number:
Consultant
Contact
CCT
Phone: aE �I iePt4-
01
ontact:
Phone:
rapsporter:
oatact:
Phone:
eso
ontact colt er e
1 Cunningham
uopipgl Rd, Thomasvillq NC
Phone: [phone] or 919-770-7705
273
273 60
Waste Description:
Waste OHgination:
Truck #:
Gross Weight:
k
Tare Weight:
et et "
SFl
CiPlIMe/1V'[ n�fi ne1iM .LLJ LL__
S t �
--• — ---- ac r— soave on mt5 --rest ere not
subject to federal regulations for reporting proper ditpasel of HA7ARDOUS WASTE.
Generator/ Agent Signature ' le Date
Acknowledgment of Receipt of Material:
Drives Signature Date
Noted Discrepancies:
Inspected & Accepte (except asuote ova s:
AcceptedBy- Date.

AES of NC
Post Office Sox 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
MASTER
LICE tSB EIX 11 EEGN aNE 30, 2019
J F OL 42672
INVALID UNLESS SIGNED
NON -I AZAADOIIS WACTF MANTYri eT
Project Number:
Load Number:
'qjov-
Cons iltant
Contact:
(f C1
Phone:
erffior.Contact:
Phone:
ransportcrContact"
Phone:
esh-t—i-: a
ootact ott w r—ACLe
3841 CummnghemRd., Thomasville, NC
Phone: [phone] or919-770-7705
27360
Waste Description:
Waste Or{gination:
Truck #:
K
Gross Weight:
Tare Weight:
Net Wetg
Iq,'?& ions
Crem°. r_..:c__�__. • _
•Y L zmu mscnoeo aeove on uns m,west we not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
General /Agent Signature Tit �j / Dffie
Acknowledgment of Receipt of Material:
Noted Discrenanries-
Signature Date
Inspected & Accepted except as
AcceptedEyi — �..�w Date:2�y/ri

AES ofNC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NOR fri CAkULINA
PUBLIC WEIGHMASTER
LICLI E EXPIRES JUNE 30, 2019
J0� R OLDE 42672
IWALIn UNLAIGNEO
NON -HAZARDOUS WASTE MANIFEST
Project Number�J13 \
y - 's
Load Number:
y
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone]
or 919-770-7705
27360
Waste Description:
Waste Origination:
02:11Pm 02!01/2019
Truck #:
Gross Weight:
69480 lb GR
Tare Weight:
42860 lb HT
Net Weight:
^2:iL ro 02101/2019
64460 lb GR
Generator s Certificanon: I certify that the materials described above on thislQ94tift 4f9 not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Ge ator / Agent Signature Title
Acknowledgment of Receipt of Material: //--` (i�--•y date /! 9
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
a1 H3
10N5

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICE I 8pE%PJ ES NE 30, 2019
J .yfOLD 42072
INVALID UNLESS ✓}IGNED
NON-14AZARntutc WA.QTF MA
Project Number:
Load Number: v
3
Consultant:
Contact:
Phone:
Generator:
Comae
Phone:
TransporterT
Contact:.
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight
05:49pro
p(
41/31:2tJ15
Tare Weight: 6,.�%0 lb 6R
?94811 1 T
Net Weight: 39580 lb NT
Cie
.... Luamuou: r cernry mar me materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Ge ator / Agent Signature Title Date
Acknowledgment of Receipt of Material:,,, 41, J 3
D vernvern s Signature %-Date
Noted Discrepancies:
htspected & Acceptei
Accepted
AES
Date: / 3/ /

NORTH CAROLINA
AES of NC PUBLIC WEIGHMASTER
Post Office Box 310 LIC ! E EXPI ES J AE 30, 2019
Sanford, NC 27331 .HOLD 42672
Phone #: [phone] INVALI NLESS SIGNEO
NON-HAZARDOii.0 WARTR MAX
05:42pm 01/31/2019
r ,24U ID• NO•
Project Number:
Load Number:
67240 lb TR REeCALL"F
31i
14100 lb NT
Consultant:
Contact:
G L S
Phone:
Generator:
Contac
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scoff Keller / Frmkie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone]
or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight:
h
30
os:29pm 01J31r2a19
-
Tare Weight:
-4200 1b dR RECRL.;
7r l 1h To
Net Weight:
700L, lb HT
Uancruwr a Ceruncanon: !certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
lJ✓�-V;--
Generator / Agent Signature Tie Date
Acknowledgment of Receipt of Material: l-3/—/If
rver Signature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: '4� 41Z Date: )/3, /,9

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
NORTH CAROLINA
PUBLIC WAIGHMASTER
LICENSEAXWS JUNE 30, 2019
JOHN G F 42673
1NW6,10 UNLI IS SIGNS
NON-RAZARDOTTC WAR TF MAN1WVe9r
Project Number:
Load Number: -,
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #: D
Gross Weight
Tare Weight:
237 ID. H0.
67180 lb 6R
Net Weight:
25700 lb TR RECHL:...
40480 lb HT
Generator s Certification: 1 certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature itle Date
Acknowledgment of Receipt of Material: ---
rivers ' ature Date
Noted Discrepancies:
Inspected & Accepted (exceft as noted above by: AES of NC)
Accepted By: Date:

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBLIC WEIO ASTER
LIC��yy3E IR JUNE30,2019
JO�.�. HOLOE 42672
INVAT.IffUNLESS SIGNED
NON -HAZARDOUS WASTE MA
Number:
Number:..,jant:
3 C _��
ct:e:or:
c:rterT
ct::on:
AES of NC
FDescription:
ct: Scoff Keller / Frankie Holdernningham
6Origination:
Rd., Thomasville, NC
: 919-770-4258
or 919-770-7705escription:
Origination:
Weight'
10:37ad 02N1:20f9.
eight:
`"58860 lb GReight:
42240 lb `a
I
a. b a.cn.uIwuon: r cernry mat me materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
r� n
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material: „ �21_ I -
Drivers Sign tare Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By��„' Date: i

AES of NC NORTH CAROLINA 50:43an 02I01; 2019
PUBLIC INEIGHMASTER
Post Office Box 310 LIC E EXP E UNE 39, 2019 240 ID • NO•
Sanford, NC 27331 1 . HOL 42672 58060 lb OR
Phone #: [phone]
INVALfO IN FIRS SIGNED
NON-HAZARUOII.0 WACTB. MANiFFRT
Project Number:
Load Number: 1)?:5an 02/01/2019
-SD
240 ID• N0.
Consultant:
Contact:
�Y4213
CC L
Phone: in TR
Generator:
Contac --
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight:
k-3o
Tare Weight:
Net Weight:
3d- %c
Goneramr s Cermtcanon: t cemty that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material: .'___ �.� 2_7�7y
7ignature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By:�fj',.. // Date:-W-1 //9

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
NORTH CAROLINA
PIIIU WEIGHMASTER
LICEN 'fit EXPIRES JUNE 30, 2019
JOE IQER
LM UNLESS SIGNED
NON -HAZARDOUS WASTE MANIFEST
Project Number:
Load Number:
ZI3 --
Consultant:
Contact:
Phone:
Generator:
Contac
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Fmnkie Holder
3941 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight: 7240 D. No.
Tare Weight:
Net Weight:
01:49Pm 02Jo1/2019
Venerator's CertiTication: l certify that the materials described ab a on thistie not
subject to federal regulations for reporting proper disposal o£HA ARDOUS- 5if"t.TR RECPLU!
-040 1b NT
G or Ag nt Signature Titl Date
Acknowledgment of Receipt of Material: -—/— /q
ers Siature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: met—�6ui Date: 2. J - / 9
IN
p-or

NORTH CAROLINA
PUBLIC WEIGHMASTER
AES of NC LIC u EXPI}tES NE 30, 2019 10: -'r3am 02/01/2019
Post Office Box 310 J�F OL k 42672 241 10• NO.
Sanford, NC 27331 69940 lb OR
Phone #: [phone] INVALID UNLESS SIGNED
NON-HAZARDOTS WASTF. MANTFFST
Project Number:
Load Number:
-
Consultant:
Contact:
Phone:
Generator:
Comac
Phone:
TransporterT
Contact:
Phone :
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd, Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight:
I(-
11:11are 02/01l2019
Tare Weight:
69940 lb OR RECALL: ;
Tr -
Net Weight: 42760 lb ITT
")1,3 7
s Cuna'canon: r cemry mat the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator/Agent Signature Title �� Date
Acknowledgment of Receipt of Material: fJ// 7 - I- I,
Drivers Signature Date
Noted Discrepancies:
Inspected & Accep (exce t as led above by: AES of NC)
Accepted By Date: / J

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
P IRWEGNSTE LPII'ZRU2019
J DER 42672
INVALID DNLESS SIGNED
NON-HAZARDOUR WARTF M
Project Number:
Load Number:
Consultant
Contact:
Phone:
Generator:
Contact:
eGZ
Phone:
Transporter:
Contact:
Phone :
Destination: AES of NC
Contact: Scott Kelle;or919-7170-7705
3841 Cunningham Rd., Thomasville, NC
Phone: [phone]
27360
Waste Description:
Waste Origination:
Truck #:
Gross Weight:
K-
'I`.:07>m 02/01/2019
Tare Weight < 0•
-`Q0 lb 6R
_
Net Weight-,r._'S. 16 NT
O
Generator s Certification: I certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Genr / Agent Signature Till Date
Acknowledgment of Receipt of Material: ntT74
vers ignature Date
Noted Discrepancies:
Inspected & Accepted (except noted 16ove by: AES of NC)
Accepted By: z Date: / /

NORTH CAROLINA
AES of NC PUSUC INEIGHMASTER
LICE EXPIRES JUNE 30, 2019
Post Office Box 310 JOE LDER _ 42672
Sanford, NC 27331 1t-
Phone #: [phone] INVALID UNLESS SIGNEDp3:23pm 02/01/2019
241 ID. N0.
NON -HAZARDOUS WARTF. MANIFURT 'D44i lb GR RECALI. "'7
Project Num_,ber:
Load Number: _
437p13 lb NT
Consultant:
Contact:
Phone:
�t /
Generator:
Contac
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller/ Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination.
0 :09vm 02/01/2019
Truck #:
Gross Weight:AT-lu-
i
70420 lb GR
Tare Weight:
440 lb NT
Net Weight:
P1:Cli: rA v2mv^D19
I . NG
-r 440 lb 'aR
srl-
Sot
s •.cnuicauon: i certify that the materials described above on this" ` . i t hbVML .
subject to federal regulations for reporting proper disposal of HAZARDOUS S
Generator / Agent Signature Title �/ p.,� {"� Date
Acknowledgment of Receipt of Material: Z- 1- f ti
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
NORTH CAROLINAf
PUBLIC WEIGHMAST R
LICEN E PIRES.d NE 0,2 1A
JOI E
ALID UNLESS SI EO
NON -HAZARDOUS WASTE MANIFEST
Project her: `J�
Load Number:
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone :
Destination: AES of NC
Contact: Scott Keller / Fmnkie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone]
or 919-770-7705
27360
Waste 5escr10011
Waste Origination:
Track #: 7
J
Gross Weight:
Tare Weight:-
241 10, No.
Net Weight:
-16740 lh 1R RECAL'.
44260 1 b HT
oau,�uumr, i certify mat the matenms aescnbea above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material: (y .„�" Z — (— / q
Drivers Signature Date
Noted Discrepancies: _
Inspected & Accepted (except as noted above by: AES of NC)
Accepted B .- Date: & — -`

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NORTH CAROLINA
PUBI IC WEI HMAS ER
LIC S E%PI J 30, 2019
LD JO F O42572
INVALID UNLESS SIGNED
NON -HAZARDOUS WASTE MANIFEST
Project Number: �\
`U
Load Number:
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
-
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone]
or 919-770-7705
27360
Waste Description:
Waste Origination.
Truck #:
Gross Weight:
Tare Weight:
65760 1b i3R
'6620 1R R
Net Weight:
42140 Ib HT
�Vao, awl s UV1 U11wnon: t cernry mat the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
ator / Agent Signature Title Date
Acknowledgment of Receipt of Material: -;_ /+✓T `q — IL Ict—
Drivers Signature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: ,may Date: o� r i

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
06" CRpaLINK
PUBLIC
NIRESN UNH 90, 20I'
LICENSEE
I / _ t 462
JOEF.NOL
i`l
Nrypl
ONLESS SIGNED
':4:I?aa 011,71"2019
239 1D• N0•
NON -HAZARDOUS WASTE MANIFEST
Project Number:
Load Number:
ai
Consultant:
Contact:
CC-T
Phone:
Generator:
Contac
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
C-�(S
Gross Weight:
Tare Weight: > a 19
0D.
239 ID. Nu
hsj0.
Net Weight: _NU0 it r
2. 1h T
('0L rl
- , � i,c, uucauu E i ceniiy mat the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Tit] Date
Acknowledgment of Receipt of Material: ( `' -°`y __? -
Drivers ignature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: ti_�— /"—. Date:

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
C p 1NA
Ra S a pE 3D, 2010
PUBi.1C g261%
�N l0
ut„y¢SS SIGi1FA
NON -HAZARDOUS WASTE MANIFEST
Project Number.
Load Number:
Consultant
Contact:
Phone:
Generator:
�1
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
3841 Cunningham Rd., Thomasville, NC
27360
Contact: Scott Keller / Frankie Holder
Phone: [phone] or 919-770-7705
Waste Description:
Waste Origination:
Truck #:
Gross Weight:
m 1
236 ID. NO.
Tare Weight:
OR
29480 1h IR RECAL
Net Weight:
tj^
Generator's Certification: I certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature - Ti e Date
Acknowledgment of Receipt of Material:Af�%/- 3/- L9
Drivers Signatunk Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
N
Accepted By: L(�2_ c-� Dater=��

nl:19Pm 01/31/2019
240 ID. NO.
74200 lb GR
AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NON-HAZ.ARDOi1.0 WACTF MANTV CT
Project Number:
Load Number:
Consultant:
CG
Contact:
Phone:
Generator:
Course
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone]
or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #: o
Gross Weight.
Tare Weight:
o L PM 01 3 / 2019
240 ID• No.
Net Weight:
26900 It TR
2 -4-0
16S
Generator s certification: t certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Titl
Acknowledgment of Receipt of Material:
ers 3 gnature
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Date
Date
Accepted By: Date:
S

NOR[R CAROU'A'A
PUBLIC'ttEtCIWASIER
d10ENSE E%Plit DUNE �gy66T2
JGE F R
IN NLESS SIGNED

VORTH CAROLINA
PUBUC WE1GHMASTER 2019
LICENSE FU' S J NE 39,
4':V2
JOE F. HOL^-'
_...
CGI catA21,a-fl�)
DIaZ'I
# Flo
a
Iq

NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIRES JUNE 90, 20iY
JOEF.HOW
AES of NC M4YRtIO U StGNEO
Post Office Box 310
Sanford, NC 27331
Phone #: [phone]
NON -HA ZA RIInTIR W A QTV "A
12:55am 01/31/2019
236 ID. NO.
67040 lb OR
Project Number: _
Load Number: Y
Consultant: �I
Contact:
Phone:
Generator:
Course
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description: D 1
Waste Origination:
Truck #: II rr
Gross Weight:
Tare Weight:
01:07Pm 01,13112019
Net Weight:
67040 lb 3R RECRLL
29880 1b TR
tee_,._�_..__.�__�:_.
MILVu. l ccnuy mar me marena:s descr bed above on this manifest are not
subject to federal regulations for reporting proper dispo HAZ OU WASTE.
Generator / Agent Signature a Date
Acknowledgment of Receipt of Material: %-'(—
Drivers Sign lure Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: f!'L— Date: 1 —�

12:58am 01/31/2019
NVL
MASTER OLINX 239?D. No.
PURJ ASTE 1a�373320 lb GR
AESofNC LICENSE4�il
Post Office Box 310 JGE F. ER
Sanford, NC 27331 1—IM UNLESS SIG100
Phone #: [phone]
NON-HAZARDOIi.0 W A RTF. MANT V V QT
Project Number:
Load Number: v
Consultant:
CC(
Contact:
Phone:
Generator:
Contac
Phone:
TransporterT
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd, Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description: � I
Waste Origination:
Truck #:
��
Gross Weight:
tom—
O1:llPm 01/3i,'2Jf9
Tare Weight:
7T.320 lib % RECt1L'-
Net Weight: 46620 lb NT
G
1
enerator s Certification: I certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature Title Date
Acknowledgment of Receipt of Material: It, -�—= %� f� 3/-1
Noted Discrepancies:
Drive ignature Date
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: Date:--/ai/-- /I?

AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICE SE E P UNE 30, 2019
JOE p42672
(VALID UNLESS SIGNED
NnN-tTA7.Aunn1TQ WAQWE nR
03:43vn 01/31/2019
237 ID. No.
66860 lb OR
Project Number:
Load Number: y
Consultant
Contact:
Phone:
Generator:
Contact:
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
Truck #:
<-
Gross Weight:
D
Tme Weight: P@
237 ID. NO.
Net Weight: -67Ch7 lb TR
i ceraty that me materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature le ate
Acknowledgment of Receipt of Material:
Sri rs Signature Date
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)

NORTH C LINA
AES of NC
Post Office Box 310
Sanford, NC 27331
Phone #:[phone]
NON -HAZARDOUS WASTF. MANTVVRT
PUBLI MASTER
LICENSE X JUNE 30, 2079
JOE F. HO R 42672
INVAL IJNLEFc SIRNEO
Project Number:
Load Number:
Consultant
Contact:
Phone:
Generator:
Contact:
W
Phone:
Transporter:
Contact:
Phone:
Destination: AES of NC
Contact: Scott Keller / Frankie Holder
3841 Cunningham Rd., Thomasville, NC
Phone: [phone] or 919-770-7705
27360
Waste Description:
Waste Origination:
- 238 ID. NO.
678 b GR
Truck #:
Gross Weight:
Tare Weight:
Net Weight:
03r46PA Ot!31f 19
23�3 10. NO.
67800 1b M RECALL (.:'
vcuc,wvl s a,cnun:auun: t cemry mat me materials d crNwe
t Sid not
subject to federal regulations for reporting proper dis s S NT j c{, p9
Generator / Agent Signature Title ^
Acknowledgment of Receipt of Material:
DriversDate
Noted Discrepancies:
Inspected & Accepted (except as noted above by: AES of NC)
Accepted By: �lJ°t- Date:_L(

Alternative Energy Solutions of NC, LL(
Post Office Box 310
Sanford, NC 27331
Phone p: 336-302-0889 .I
Pax #: 704-973-9573
NORTH CAROLINA
PUBLIC WEIG MASTER
LICENSE EX RE LINE 30, 2010
JOHN GODF 42673
INVALIDIINI EBB SIGNED
ASTE M
NUN HA�anDOUS W
Project Number:
Land Number:
Consultant:
Contact: �3h,
S � -
Phone: ri -0
Generator:
Contact: ),m
Phone: - ..l
Transporter:
kcrh S Tn k naJ
Contact:}, k,Ay+l.Z�.lV4-
Phone:
Destination: AES
Contact: Scott Keller
3841 Cunningham Road
Thomasville, NC 27360
Phone: (1I -77 -
Waste Description: -1-P1+ LY I
aste
-I
Origination: (, f„c�
Truck Y:
Gross Weight: ]1:3SaR 03/05/2015
Tare Weight:
Net Weight: ""— "=-
2,
Gernerator's Certification: 1 certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Acknowledgment of Receipt of Material:
Noted Discrepancies:
Inspected & Accepted (except as noted ab ve By: Earthtec Environmental, Inc.)
Accepted By: Date: - n

Alternative Energy Solutions of NC, LLC
Post Office Box 310
Sanford, NC 27331
Phone#: [phone]
Fax #: [phone]
NORTH CAROLINA
PUBLIC WEIGH M STER
LICENSE EXPIRE 30, 2011
JOHN GODFREY11 JL }�E Lk- 42673
NONNd7ADINHIc art A O u—
SS SN3NED
Project Number:
al i S�It - �n
Load Number:
Consultant: \` \
�S �X»TJeL-2a1-
Contact: c
vdG.UYi
/L�.V�
Generator:
E„C. Goy{{=inn (\
Phone:
Contact:
Transporter:
.Lerh'6
Phone:
Phone:
Destination: AES
Contact: Scott Keller
3841 Cunningham Road
Thomasvillq NC 27360
Phone:
Waste Description: -.I+ _k -)
ash,
Origination: U6'I
Truck#:
J I
Gross Weight:
Tare Weight:
i',j ;+ ID. NO,
Net Weight:
:1F700 10 TP. k::
V! /
a
Gernerator's Certification: I certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Generator / Agent Signature
Aclmowledgment of Reeeipt of Material:
Noted Discrepancies:
Inspected & Accepted (except as noted above By: Earthtec Environmental, Inc.)
Accepted By: Date: 9

Alternative Energy Solutions of NC, LLC
Post Office Box 310
Sanford, NC27331
Phone#: [phone]
Fax #: [phone]
NORTH CAROLINA
PUBLIC WEIGOMASTER
LICENSED 3042673
JOHN GOD Y
INVALI NLESSSIGNED
NON RAZ&nnn le WAQ cv a&
Project Number:
Load Number
Consultant-.
E:GS "�Yxx
Contact:
'Sha Kn I6�
Phone: qV -'
Generator: EcGC K'4,
Contact:, mV�
Phone:
Transporter: �.'.erF)�S T ry
Contact:'6 {
Phone:
Destination: AES
Contact: Scott Keller
3841 Cunningham Road
Thomasville, NC 27360
Phone:Waste
Description:
sate
Origination: U�� -I
Track#:
L
Gross Weight:
Tare Weight
Net Weight: - -
/ ?D
Gernerator's Certification: I certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Noted Discrepancies: p
Inspected & Accept cept/ s note above By: Earthtec Environmental, Inc.)
Accepted By: / AJ\ Dale: 3a lq
--.���
�J

Alternative Energy Solutions of NC, LLC
Post Office Box 310
Sanford, NC 27331
Phone#: [phone]
Fax #: [phone]
NORTH CAROLINA
PUBLIC WEIGHMASTER
LICENSE EXPIR S UNE 30, 2019
JOHN GODFRE 42673
INVALID UlXESS SIGNED
NnN HAYAnHlllle c1
Project Number:
Load Number:
Consultant:
Contact:
Phone: Ci
Generator: \'
l
Contact:
Transporter:
k.r.-f1S Tr ck�,r.
Phone:
Contact:,
Phone:
Destination: AES
Contact: Scott Keller
3841 Cunningham Road
Thomasville, NC 27360
Phone:
Waste Description: �-7µ
as[e
Origination: O„,
Truck
Gross Weight: 21R
_ ..
Tare Weight: 51A4:1
t i,
-�68r'
to TP REGAL_
Net Weight: '=5'nO
jo HT
6i ra]
Gernerator-s Certification: 1 certify that the materials described above on this manifest are not
subject to federal regulations for reporting proper disposal of HAZARDOUS WASTE.
Acknowledgment of Receipt of Material:
—S— i
Date
Noted Discrepancies: U
Inspected & Accepted (except as notid above By: Earthtec Environmental, Inc.)
Accepted By: �. Date:

Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, April 8, 2019 9:51 AM
To: 'Chris Orrell, P.G.'
Subject: RE: [External] 1808 W. Morehead Street, Charlotte, NC - Soil Removal Report
Great.
Thank you,
Trudy
From: Chris Orrell, P.G. [mailto:[e-mail]]
Sent: Monday, April 8, 2019 9:48 AM
To: Beverly, Trudy <[e-mail]>
Cc: Jim Griffith ([e-mail]) <[e-mail]>; Matthew H. McDuffie, P.G.
<[e-mail]>; [e-mail]; Michelle Forness <[e-mail]>
Subject: RE: [External] 1808 W. Morehead Street, Charlotte, NC - Soil Removal Report
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
[e-mail]
Trudy,
Please see the attached document with the revised title. Let me know if you need anything else. We will be sending the
hard copy (minus the lab reports) and the CD copy today.
Thanks!
CHRIS ORRELL, P.G. I Environmental Staff Project Manager
ECS SOUTHEAST, LLP T 704.525.5152 1 D 704.409.7740 1 C 704.200.3436
www.ecslimited.com
Confidential/proprietary message/attachments. Delete message/attachments if not intended recipient.
From: Beverly, Trudy[mailto:[e-mail]]
Sent: Monday, April 08, 2019 6:46 AM
To: Chris Orrell, P.G.
Cc: Jim Griffith 0griffith0)ecgriffith.us); Matthew H. McDuffie, P.G.; ESherlock@ robin son bradshaw.com
Subject: RE: [External] 1808 W. Morehead Street, Charlotte, NC - Soil Removal Report
Good Morning Chris,
Please see the following document submittal policies,
Document Submittal & UST File Names for Laserfiche Policies:
https://ddei3-0-
ctn.trendmicro. com:443/wis/clicktime/v 1/auerv?url=httos%3 a%2f%2ffiles.nc. gov%2fncdea%2f W aste%2520ManaLyement%2fD WM
%2f1JST%2fCorrective%2520Action%2fElectronic%2520Document%2520Submittal%2520Memo%2520Update.pdf&umid=401 FA9
73-8605-1505-84F 1-56A45B707FEA&auth=993f245b85fc94fa7fee52bac4e2fe2b8d03da9e-
3a26697613e53cab75c35c6bl52fc8957ealc26e
https://ddei3-0-
ctp.trendmicro. com:443/wis/clicktime/v 1 /query?url=https%3 a%2f%2ffiles.nc. gov%2fncdeq%2f W aste%2520Management%2fDWM

%2fUST%2fCorrective%2520Action%2fUST%2520file%2520names%2520for%2520Laserfiche.docx&umid=401FA973-8605-
1505-84F 1-56A45B707FEA&auth=993 f245b85fc94fa7fee52bac4e2fe2b8d03 da9e-7fc50be47027433 7a92b 1 b260019M20969fl fl
Thanks,
Trudy
DE
NORTH CAROLINA
Department of Environmental Duality
r ' , LA
�� QrMhWMM*Pllll=
Noah Cade DWKMM offthm=d QWt
varsedm moareeaw Rgomd omm
(7" 23S,21i2 (OR*
Trr &I off"
Email corrPsirx)ndenc a to arxl from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deq.nc.aov/about/divisions/waste-management/waste-management-rules-data/waste-mana eg ment- ig s-mates
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https:Hedocs.deq.nc.gov/WasteManagement/Search.aspx
Document Submittal St UST File Names for Laserfiche Policies:
htt2s://ddei3-0-
ct 2.trendmicro.com:443/wis/clicktime/v 1 /query?url=https%3 a%2f%2ffiles.nc. gov%2fncdeq%2f WasteD/o2520Management%2fD WM
%2fLJST%2fCorrective%2520Action%2fElectronic%2520Document%2520Submittal%2520Memo%2520Update.pdf&umid=401 FA9
73-8605-1505-84F 1-56A45B707FEA&auth=993f245b85fc94fa7fee52bac4e2fe2b8d03da9e-
3a26697613e53cab75c35c6bl52fc8957ealc26e
https://ddei3-0-
ctp.trendmicro. com:443/wis/clicktime/v 1 /query?url=https%3 a%2f%2ffiles.nc. gov%2fncdeq%2fWaste%2520Management%2fD WM
%2f UST%2fCorrective%2520Action%2fUST%2520file%2520names%2520for%2520Laserfiche.docx&umid=401 FA973-8605-
1505-84F 1-56A45B707FEA&auth=993f245b85fc94fa7fee52bac4e2fe2b8d03da9e-7fc50be470274337a92b lb260c919bf20969fl fl
From: Chris Orrell, P.G. [mailto:[e-mail]]
Sent: Friday, April 5, 2019 5:29 PM
To: Beverly, Trudy <[e-mail]>
Cc: Jim Griffith ([e-mail]) <[e-mail]>; Matthew H. McDuffie, P.G.
<[e-mail]>; [e-mail]
Subject: [External] 1808 W. Morehead Street, Charlotte, NC - Soil Removal Report
CAUTION:I email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
c. ov
Trudy,
Please see the attached report which documents the soil sampling and subsequent over -excavation of soil associated
with an apparent unregulated heating oil UST that was encountered during grading operations at 1808 W. Morehead
Street in Charlotte, North Carolina. Feel free to reach out to me if you have any questions or comments.

Thanks!
CHRIS ORRELL, P.G. I Environmental Staff Project Manager
T 704.525.5152 1 D 704.409.7740 1 C 704.200.3436
1812 Center Park Drive, Suite D I Charlotte I NC 1 28217
ECS SOUTHEAST, LLP
www.ecslimited.com
Linkedln I Facebook I Twitter
Confidential/proprietary message/attachments. Delete message/attachments if not intended recipient.
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