7407_Pitt_CandDLandfillInc_20190517_Fall2018GW_FID1320983

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ANC DENR I I Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Sheri Knox
E-mail: sheri.knox(a)woodplc.com
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
C&D Landfill, Inc. 802 Recycling Lane 7406-CDLF- .0500 December 4, 5, 12, 13, 2018
CDLF Phases 1&@ Greenville, NC 27834 2009
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑ Detection Monitoring ❑X Assessment Monitoring Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data ❑
Surface water monitoring data
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
RX Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Facility;f�-,prese�tative Name (Print)
Senior Geologist 919.381.9000
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Signature Date
4021 Stirrup Creek Drive, Suite 100, Durham, NC 27703
Facility Representative Address
F-1253
NC PE Firm License Number (if applicable effective May 1, 2009)
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WATER QUALITY MONITORING REPORT
DECEMBER 2018
SEMIANNUAL SAMPLING EVENT
CONSTRUCTION AND DEMOLITION
DEBRIS LANDFILL, PITT COUNTY
FACILITY PERMIT NO. 7407-CDLF-2001
Prepared For:
C&D Landfill, Inc.
802 Recycling Lane
Greenville, North Carolina 27834
[phone]
Prepared By:
Wood Environment & Infrastructure Solutions, Inc.
4021 Stirrup Creek Drive, Suite 100
Durham, North Carolina 27703
[phone]
Woodplc.com
Registered in North Carolina
Engineering and Land Surveying License No. F-1253
Wood Project No.: 6480-19-9035
May 2019

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May 7, 2019
Ms. Jackie Drummond, Hydrogeologist
North Carolina Department of Environmental Quality
Division of Waste Management, Solid Waste Section
2090 US Highway 70
Swannanoa, North Carolina 28778
Subject: C&D Landfill, Inc., Phases 1 and 2
Facility Permit Number 7407-CDLF-2001
Water Quality Monitoring Report
December 2019 Semiannual Sampling Event
Wood Project No.: 6480-19-9035
Dear Ms. Drummond:
On behalf of C&D Landfill, Inc., Wood Environment & Infrastructure Solutions, Inc. (Wood; formerly Amec Foster
Wheeler) is submitting the enclosed Water Quality Monitoring Report for the December 2018 semiannual
monitoring event. The monitoring event was performed between December 4 and 13, 2018. This sampling event
included analyzing groundwater samples from each of the active wells for Appendix II constituents, natural
attenuation parameters, and 1,4-dioxane.
This report provides details of the field activities,
recommendations based on current and historical data
May 2019.
laboratory analyses, and presents conclusions and
The next semiannual monitoring event is scheduled for
Please call Sheri Knox at 919-381-9913 if you have any questions or comments.
Sincerely,
Wood Environment & Infrastructure Solutions, Inc.
Damian Hriciga, PG
Senior Geologist
Enclosed: Water Quality Monitoring Report
Wood Environment & Infrastructure Solutions, Inc.
4021 Stirrup Creek Drive, Suite 100
Durham, North Carolina 27703
Tel: [phone] / Fax: [phone]
www.woodplc.com
Licensure: NC Engineering F-1253 / NC Geology C-247
Sheri Knox, PE, PMP
Associate Project Manager
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Water Quality Monitoring Report
December 2018 Semiannual Sampling Event
Wood Project No. 6468-19-9035
Table of Contents
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1.0 INTRODUCTION............................................................................................................... 2
2.0 FIELD ACTIVITIES.............................................................................................................3
3.0 GROUNDWATER LEVELS AND FLOW.............................................................................3
4.0 GROUNDWATER AND SURFACE WATER ANALYTICAL RESULTS................................4
4.1 Volatile Organic Compounds (VOCs).................................................................4
4.2 Semi -Volatile Organic Compounds (SVOCs), Herbicides and Pesticides, and
Polychlorinated biphenyls (PCBs).......................................................................5
4.3 Appendix I and Appendix II Metals....................................................................5
4.4 Appendix II Inorganics (Cyanide and Sulfide)...................................................6
5.0 DISCUSSION OF CONTAMINANTS OF CONCERN.........................................................6
5.1.1 Volatile Organic Compounds...................................................................... 6
5.1.2 Appendix I and Appendix II Metals.............................................................. 7
6.0 CONCLUSIONS................................................................................................................8
TABLES
Table 1— Groundwater Level and Flow Data
Table 2 — Summary of Groundwater Analytical Data — December 2018
Table 3 — Summary of Surface Water Analytical Data — December 2018
Table 4 — Summary of Natural Attenuation Parameters — December 2018
FIGURES
Figure 1 — Site Location Map
Figure 2 — Monitoring Well and Surface Water Sampling Location Map
Figure 3 — Groundwater Elevation Map — December 2018
Figure 4 — Groundwater and Surface Water Standard Exceedance Map — December 2018
APPENDICES
Appendix A
— Laboratory Analytical Report
Appendix B —
Historical Data for Selected Analytes
Appendix C —
Mann -Kendall Trend Analyses
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Water Quality Monitoring Report
December 2018 Semiannual Sampling Event
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1.0 INTRODUCTION
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C&D Landfill, Inc. owns and operates the Construction and Demolition Debris Landfill located at 802 Recycling
Lane, Greenville, Pitt County, North Carolina (Site; Figure 1). Phase 1 became operational in 2001 and Phase 2
became operational in 2009. The landfill is permitted by the North Carolina Department of Environmental Quality
(NCDEQ), Division of Waste Management (DWM), Solid Waste Section (SWS) under Permit 7407-CDLF-2009,.
Groundwater and surface water monitoring have been performed at Phase 1 since May 2001, and at Phase 2 since
August 2009. Both phases are in the assessment stage of the Assessment and Corrective Action Program for C&DLF
Facilities and Units. An Assessment of Corrective Actions (ACM) Report was prepared in October 2017, and
monitoring data is currently being evaluated to select a corrective action.
This report presents the results of the second semiannual monitoring event for year 2018, and the third semiannual
analysis of parameters to evaluate monitored natural attenuation (MNA). Analytical data are compared to the 15A
NCAC 02L .0202 Groundwater Standards (2L Groundwater Standards), Interim Maximum Allowable Concentrations
(IMACs), 15A NCAC 02B Water Quality Standards for Surface Water (2B Surface Water Standards), or other
applicable standards, as appropriate.
Phases 1 and 2 of the landfill are separated by a channelized central drainage feature that originates onsite and
predates either phase of the landfill. Phase 2 is located north of the drainage feature, while Phase 1 is located to
the south. Both phases are isolated from their surroundings by tributaries to Grindle Creek and wetlands. Permitting
studies have established the adjacent water bodies as on -site discharge points for the uppermost aquifer.
Downgradient areas consist of agricultural and wooded marshland leading to Grindle Creek and on to the Tar River.
Much of the downgradient area is beneath the 100-year flood level and is not anticipated to undergo development.
No groundwater users have been identified down gradient of the site. The groundwater in the uppermost aquifer
is intercepted by the surface streams within and just beyond the facility boundary. The October 2017 ACM Report
identified an Area of Concern (AOC) centered on the channelized drainage feature where volatile organic
compounds (VOCs) have been reported in groundwater samples. The AOC originates north of the drainage feature,
along the south side of Phase 2, and extends south from the drainage feature near MW-8 to the southwest corner
of Phase 1 near MW-3S. In 2014 and 2015, an Alternate Source Demonstration (ASD) was performed that focused
on the soils within and near the drainage feature, however, the results were inconclusive.
The groundwater monitoring network consists of 12 wells within Phase 1 and 10 wells within Phase 2. Within Phase
1 there is one upgradient, background well (MW-1S), eight downgradient compliance wells (MW-2S, MW-3S, MW-
4, MW-5, MW-6, MW-7, MW-3A, and MW-8), and three deeper wells (MW-1D, MW-2D, and MW-3D). Within Phase
2 there are three upgradient wells (MW-9A [background], MW-16, and MW-17), six down gradient compliance
(MW-10, MW-11, MW-12S, MW-13, MW-14S, and MW-15), and one deeper well (MW-14D). The well locations are
illustrated in Figure 2.
Four surface water sampling locations have been defined at the Site (SW-1, SW-2, SW-3, and SW-4). Sampling
locations SW-1 and SW-2 monitor the tributary on the south side of Phase 1, which originates offsite to the east
with SW-1 monitoring background conditions. Sampling locations SW-3 and SW-4 monitor the tributary (itself
partially channelized) on the west side of Phase 2, which originates offsite to the north with SW-4 monitoring
background. SW-2 is located below the confluence of the western tributary and the channelized central drainage
feature south of Phase 2. The surface water sampling locations are illustrated in Figure 2.
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2.0 FIELD ACTIVITIES
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Groundwater and surface water sampling activities were conducted by Environment 1, Inc. (Environment 1).
Environment 1 personnel collected groundwater samples from 22 groundwater monitoring wells and 4 surface
water sampling locations between December 4 and 13, 2018. The sampling event was conducted in accordance
with the Sampling and Analysis Plan dated May 2008, the Groundwater Assessment Work Plan dated June 2009,
and the SWS Guidelines for Groundwater, Soil, and Surface Water Sampling.
Prior to sampling the monitoring wells, the wellheads were inspected and the depth to water in each was were
measured using an electronic water level meter. Depth to water measurements were recorded after a sufficient
time for water levels within the wells to have equilibrated with atmospheric pressure.
Groundwater was purged and sampled using a peristaltic pump and low -flow methodology by Environment 1.
Temperature, pH, dissolved oxygen, oxidation/reduction potential (ORP), and turbidity were measured and
recorded. Surface water samples were collected by direct submersion of sample containers into the streams at
designated locations.
Each sample was placed into laboratory -supplied sample bottles by a technician wearing new nitrile gloves. The
samples were preserved according to the requirements for the type of analysis, chilled, and returned to
Environment 1 in Greenville, North Carolina within the appropriate holding times under chain -of -custody protocols.
Environment 1 is a North Carolina certified water quality laboratory (Certification 10).
The laboratory analyzed each groundwater sample for the constituents listed in 40 CFR Part 258 Appendix II
(Appendix II), plus tetrahydrofuran. Additionally, each groundwater sample was analyzed for 1,4-dioxane in
accordance with the SWS May 29, 2018 memorandum. Each surface water sample was analyzed for the constituents
in 40 CFR Part 258 Appendix I (Appendix I), plus tetrahydrofuran.
In addition to the potential contaminants listed above, each groundwater sample was analyzed for parameters to
assess the potential of the aquifer to naturally attenuate contaminant concentrations. To obtain baseline values,
each sample was analyzed for the full suite of natural attenuation parameters per the MNA Excerpt from Examples
of Approved Groundwater Corrective Measures for Solid Waste Management Facilities. The parameters included:
• Carbon Dioxide
• Ethene
• Sulfate
• Nitrate
• Total Organic Carbon (TOC)
• Chemical Oxygen Demand (COD)
• Alkalinity
• Hardness
3.0 GROUNDWATER LEVELS AND FLOW
• Methane
• Ethane
• Sulfide
• Hydrogen
• Biological Oxygen Demand (BOD)
• Total Dissolved Residue
• Volatile Fatty Acids
• Iron
Depth to groundwater measurements were collected at 22 wells during the December 2018 monitoring event.
Groundwater elevations, which increased in some areas and deceased in others, were typically within one foot of
those measured during the June 2018 monitoring event. The horizontal direction of groundwater flow is generally
to the south and locally away from the landfill phases, which is consistent with historical observations. Groundwater
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elevation contours are illustrated on Figure 3. Estimated values for hydraulic conductivity and porosity, as well as
the horizontal hydraulic gradients and groundwater flow velocities, are presented in Table 1.
The horizontal hydraulic gradients near MW-3A, MW-10, MW-11, and MW-12S were calculated based on data
from Figure 1 and vary from approximately 0.002 to 0.02 (ft/ft; Table 1). Comparison of elevation data at MW-2S
and MW-2D, and MW-3S and MW-3D indicated the presence of downward vertical gradients of -0.03 and -0.02
ft/ft, respectively. Vertical gradients at the site are typically downward.
4.0 GROUNDWATER AND SURFACE WATER ANALYTICAL RESULTS
Reported concentrations of groundwater constituents were compared to the 2L Groundwater Standards or IMACs.
Concentrations of surface water constituents were compared to the 2B Surface Water Standards or other applicable
water quality criteria for Class C surface waters. Reported concentrations that are greater than the laboratory
method detection limit (MDL), but less than the laboratory method reporting limit (MRL) are estimated and are
indicated with a "J" qualifier. Note that for tabulated data prior to the discontinuing of the Solid Waste Section
Limit (SWSL) in 2018, "J" qualified data indicates that a concentration was greater than the MDL, but less than the
SWSL. Contaminants are summarized below and discussed in Section 5 in context with historical data and natural
attenuation parameters as appropriate.
Contaminant concentrations in groundwater samples are summarized in Table 2 and concentrations in surface
water samples are summarized in Table 3. Concentrations in groundwater and surface water that exceeded the
applicable standards are illustrated on Figure 4. The laboratory reports, with chain -of -custody documentation and
the electronic data deliverables (EDDs) are included in Appendix A. Historical analytical results for selected
contaminants are summarized in Appendix B.
4.1 Volatile Organic Compounds (VOCs)
Based on the laboratory analytical report, volatile organic compounds (VC)Cs) that exceeded their 2L Groundwater
Standards during the December 2018 monitoring event included benzene, vinyl chloride (VC), and 1,4-dioxane
(Table 2 and Figure 3).
Reported benzene concentrations exceeded the 1 pg/L 2L Groundwater Standard in the samples from MW-3S (1.3
pg/L), MW-3A (1.69 pg/L), MW-10 (1.57 pg/L), and MW-12S (1.48 pg/L).
Reported VC concentrations exceeded the 0.3 pg/L 2L Groundwater Standard in the samples from MW-3S (1.82
pg/L), MW-3A (1.09 pg/L ), MW-6 (0.18 J pg/L ), MW-7 (1.25 pg/L ), MW-8 (1.48 pg/L ), MW-10 (2.2 pg/L), and MW-
12S (2.21 pg/L).
Reported 1,4-dioxane concentrations exceeded the 3 pg/L 2L Groundwater Standard in the samples from MW-1S,
(5.33 pg/L), MW-2S (6.2 pg/L), MW-3S (184 pg/L), MW-3A (87 pg/L ), MW-5 (16.4 pg/L), MW-6 (13.5 pg/L ), MW-7
(18.2 pg/L ), MW-8 (49.3 pg/L ), MW-10 (5.4 pg/L), MW-11 (8.15 pg/L), and MW-12S (2.21 pg/L).
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Other VOCs that were reported in December 2018 at concentrations below their 2L Groundwater Standards
included:
• Acetone
• Cis-1,2-Dichloroethene
• Ethylbenzene
• Toluene
• 1,2-Dichloroethane
• 1,2-Dichloropropane
• Naphthalene
In addition to the VOCs noted above, tetrahydrofuran was reported in the samples from 11 wells at concentrations
ranging from 5.33 pg/L (MW-1S) to 184 pg/L (MW-3S). Analysis for this constituent is required because the VOC
is a common constituent of groundwater at construction and debris landfills; however, neither a 2L Groundwater
Standard nor an IMAC have been established for tetrahydrofuran.
Toluene was reported at a concentration of 0.38 J in the surface water sample from location SW-1, below the 600
pg/L 2B Standard (Table 3 and Figure 3). No other VOCs were not reported in the surface water samples collected
during the December 2018 monitoring event.
4.2 Semi -Volatile Organic Compounds (SVOCs), Herbicides and Pesticides, and Polychlorinated
biphenyls (PCBs)
Based on the laboratory analytical report, dibenzofuran was the single semi -volatile organic compound (SVOC)
reported at a concentration that exceeded a 2L Groundwater Standard in samples during the December 2018
monitoring event (Table 2 and Figure 3). The 9.19 pg/L dibenzofuran concentration reported in the sample from
MW-3S exceeded the 0.98 pg/L IMAC.
Other SVOCs reported at concentrations below their 2L Groundwater Standards in December 2018 include:
• Acenaphthene
• Fluorene
• Benzo[g,h,i]perylene
• Indeno[1,2,3-Cd]pyrene
Beta -BHA was the single herbicide/pesticide reported at a concentration that exceeded a 2L Groundwater Standard
in samples during the December 2018 monitoring event (Table 2 and Figure 4). The 0.04 J pg/L beta -BHA
concentration reported in the sample from MW-3S exceeded the 0.02 pg/L IMAC. Endrin aldehyde was also
reported in the sample from MW-3S at a concentration of 0.1 pg/L, which is below the 2L Groundwater Standard
of 2 pg/L. No other herbicides or pesticides were reported.
Polychlorinated biphenyls (PCBs) were not reported in the groundwater samples collected during the December
2018 monitoring event.
4.3 Appendix I and Appendix II Metals
Based on the laboratory analytical report, Appendix II metals concentrations in groundwater samples that exceeded
their 2L Groundwater Standards or IMACs during the December 2018 monitoring event included arsenic, cobalt,
chromium, and vanadium (Table 2). Concentrations that exceeded the 2L Groundwater Standard are summarized
below.
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• Arsenic concentrations reported in the samples from MW-3S (27 pg/L), MW-3A (21 pg/L), MW-7 (15 pg/L),
MW-8 (15 pg/L) and MW-12S (22 pg/L) exceeded the 10 pg/L 2L Groundwater Standard.
• Cobalt concentrations reported in the samples from MW-2S (1.4 pg/L), MW-3S
(3 pg/L), MW-3A (8.3 pg/L), MW-5 (1.2 pg/L), MW-6 (2.9 pg/L), MW-7 (12 pg/L), MW-8 (3.4 pg/L), MW-10
(1.8 pg/L), and MW-12S (1.6 pg/L) exceeded the 1 pg/L IMAC.
• Chromium concentrations reported in the samples from MW-3S (32 pg/L), MW-3A (13 pg/L), MW-7 (12
pg/L), MW-8 (15 pg/L), MW-10 (14 pg/L) and MW-12S (24 pg/L) exceeded the 10 pg/L 2L Groundwater
Standard.
• Vanadium concentrations reported in the samples from MW-1S (1.8 pg/L), MW-2S (1.2 pg/L), MW-3S (7.2
pg/L), MW-3A (3.1 pg/L), MW-4 (5 pg/L), MW-5 (1.3 pg/L), MW-6 (2 pg/L), MW-7 (2.4 pg/L), MW-8 (1.6
pg/L), MW-11D (2 pg/L), MW-10 (8.1 pg/L), MW-11 (1.5 pg/L), MW-12S (17.5 pg/L), MW-13 (1.3 pg/L), MW-
14S (2.3 pg/L), MW-15 (3.5 pg/L ), MW-16 (9.1 pg/L), and MW-17 (1.2 pg/L) exceeded the 0.3 pg/L IMAC.
Appendix I metals concentrations did not exceed their 2B Surface Water Quality Standards in surface water samples
collected during the December 2018 monitoring event (Table 3).
4.4 Appendix II Inorganics (Cyanide and Sulfide)
Based on the laboratory analytical report, cyanide was not detected in the groundwater samples collected during
the December 2018 monitoring event.
The laboratory reported sulfide concentrations in the groundwater samples from MW-5 (390 J pg/L), MW-10 (328
J pg/L), and MW-12S (115 J pg/L). Inorganics concentrations in groundwater samples are summarized in Table 2.
Neither a 2L Groundwater Standard nor an IMAC have been established for Sulfide.
5.0 DISCUSSION OF CONTAMINANTS OF CONCERN
Contaminants of concern identified in the 2017 ACM Report are discussed in the following sections with historical
context and in relation to natural attenuation parameters in the following sections. Mann -Kendall statistical analysis
was used to assess trends in selected VOC concentrations over time. The Mann -Kendall analysis documentation,
which includes time versus concentration graphs, is provided in Appendix C.
5.1.1 Volatile Organic Compounds
Benzene concentrations that exceed the 2L Groundwater Standard have historically been reported in samples from
wells MW-3A, MW-3S, MW-8, and MW-12S in AOC 1, on the margins of the central drainage between Phases 1
and 2. The highest benzene concentration reported to date was 3.1 pg/L in the sample from MW-3S in May 2010.
Mann -Kendall trend analysis of benzene concentrations in samples from these wells indicates that concentrations
over the past three years are stable at MW-3S and MW-8, and trends cannot be identified at MW-3A and MW-12
(i.e., similar to stable; Appendix C). Benzene has previously been reported in samples from MW-10, however, the
December 2018 concentration is the first reported concentration to exceed the 2L Groundwater Standard.
Field measurements and natural attenuation parameters reported during the December 2018 monitoring event
suggest that groundwater conditions in the AOC and the western portion of Phase 1 are somewhat reducing and
not conducive to aerobic attenuation of benzene; however the absence of identifiable concentration trends at MW-

Water Quality Monitoring Report
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3A and MW-12S and the apparent stability at MW-3S and MW-8 suggests that benzene is attenuating naturally at
these locations at a rate roughly equivalent to the "input" of mass to the aquifer system.
Vinyl chloride (VC) concentrations that exceed the 2L Groundwater Standard have consistently been reported in
samples from MW-12S since 2012 and MW-10 since 2016. Mann -Kendall trend analysis of VC concentrations in
samples from these wells indicates that concentrations over the past three years are stable at MW-12S and a trend
cannot be identified at MW-10 (Appendix Q. Sporadic exceedances have also been reported in samples from
MW-3S, MW-6, and MW-8, and VC concentrations exceeded the 2L Standard in samples from MW-3A and MW-7
for the first time in December 2018.
VC in groundwater is often the result of the reduction of larger chlorinated ethenes, such as trichloroethylene (TCE)
and cis-1,2-dichloroethylene (cis-1,2-DCE). Based on the historical presence of low concentrations of these
compounds at the Site and considering the reducing groundwater conditions indicated by the natural attenuation
monitoring, this reduction appears to be the source of VC at the Site. Future sampling data will be assessed to
determine if the sporadic and new exceedances reported in December 2018 represent increasing trends.
1,4-Dioxane concentrations exceeded the 2L Groundwater Standard in shallow samples from across the AOC and
Phase 1 in December 2018. The highest concentrations were reported in samples from MW-3S, MW-3A, and MW-
8 within the AOC. 1,4-dioxane was commonly used as stabilizer for other VOCs, but the compound can be found
in a variety of household products and materials. Groundwater samples collected during the December 2018 event
were the first to be analyzed for 1,4-dioxane at the Site, and additional sampling data is necessary to determine
the persistence of the detections and trends in concentrations.
Tetrahydrofuran has been consistently detected in the groundwater samples from across the Site since sampling
for this compound began in 2011. Concentrations in samples from individual wells tend to fluctuate over time. The
tetrahydrofuran concentrations reported in samples from upgradient deep well MW-1D are unexpected because
MW-1D is screened in the deeper aquifer and tetrahydrofuran has not been reported in samples from collocated
shallow well MW-1S. Together, these data suggest that the concentration in the sample from MW-1D may be
related to the construction of the well itself and not representative of conditions in the aquifer.
5.1.2 Appendix I and Appendix It Metals
Each of the metals discussed below occur naturally at the Site and are present in background samples. Changes in
the concentrations of these metals likely reflect changing groundwater conditions and may result from the reducing
conditions suggested by field measurements and other natural attenuation parameters.
Arsenic has been reported in samples from each Site monitoring well and surface water sampling location,
including those monitoring background conditions. Concentrations exceeding the 2L Groundwater Standard have
been reported in MW-3S, MW-3A, MW-5, MW-6, MW-7, MW-8, and MW-12S. Currently, MW-3S, MW-3A, MW-7,
MW-8, and MW-12S contain arsenic concentrations above its respective 2L Standard.
Barium has been reported in samples from each Site monitoring well and surface water sampling location,
including those monitoring background conditions. Concentrations exceeding the 2L Groundwater Standard have
been reported in MW-3S and MW-7; however, concentrations in samples from MW-7 have not exceeded the 2L
Groundwater Standard since May 2016 and the December 2018 barium concentration in MW-3S did not exceed
the 2L Groundwater Standard.
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Chromium has been reported in samples from each Site monitoring well and surface water sampling location,
including those monitoring background conditions. Historically, elevated chromium concentrations in several wells
decreased over time to below the 2L Groundwater Standard. More recently, chromium concentrations reported in
samples from MW-3S, MW-5, MW-7, MW-8, MW-10, and MW-12S have exceeded the 2L Groundwater Standard.
In December 2018, the concentrations reported in the samples from MW-3S, MW-3A, MW-7, MW-8, MW-10 and
MW-12S exceed the 2L Groundwater Standard.
Cobalt has been reported in samples from each Site monitoring well and surface water sampling location, including
those monitoring background conditions. Reported cobalt concentrations typically exceed the IMAC by less than
an order of magnitude in samples from MW-2S, MW-3S, MW-3A, MW-5, MW-6, MW-7, MW-8, MW-12S, and MW-
14S; however, the concentration in MW-14S did not exceed the IMAC in December 2018.
Vanadium has been reported in samples from each Site monitoring well and surface water sampling location,
including those monitoring background conditions. Reported concentrations fluctuate over time and generally
exceed the low 0.3 pg/L IMAC. Higher concentrations are reported in samples from MW-12S more consistently
than in samples from other wells.
6.0 CONCLUSIONS
VOCs reported in groundwater samples at concentrations that exceed their 2L Groundwater Standard include
Benzene, VC, and 1,4-dioxane. Based on Mann -Kendall trend analysis of benzene and VC concentrations over the
past three years, concentrations of these compounds do not appear to be increasing. The absence of an apparent
increasing trend suggests that natural attenuation of the compounds is roughly equivalent to the input of
additional mass to the aquifer system. While the reducing groundwater conditions in the AOC indicated by the
natural attenuation monitoring support the anaerobic degradation of VC, the conditions are not ideal for the
aerobic biodegradation of benzene. However, the minimal benzene concentrations reported at the site are
expected to rapidly degrade as they encounter oxygenated groundwater downgradient. Concentration trends will
continue to be monitored. Concentrations of 1,4-dioxane exceed the 2L Groundwater Standard in samples from
wells in the AOC and across Phase 1. Data from future sampling events will be used to evaluate the persistence of
the detections and concertation trends.
The SVOC dibenzofuran was reported in the sample from MW-3S at an estimated J-flagged concentration that
exceeded the IMAC. This result will be confirmed during future sampling events.
The pesticide Beta-BHC was reported in the sample from MW-3S at estimated J-flagged concentration that
exceeded IMAC. The trends for this pesticides will also be evaluated.
Metals identified in groundwater samples at elevated concentrations continue to appear to be naturally occurring
at the Site, and the elevated concentrations are likely related to the moderately reducing groundwater conditions
indicated by the natural attenuation monitoring. Trends in groundwater conditions at the Site, and their effect on
metals concentrations will be evaluated as additional field measurements and natural attenuation data are
collected during subsequent semiannual monitoring events.
Groundwater and surface water monitoring, including natural attenuation parameters, will continue on a
semiannual schedule in accordance with the Assessment and Corrective Action Program.
8

Water Quality Monitoring Report
December 2018 Semiannual Sampling Event
Wood Project No. 6468-19-9035
TABLES
wood.

Table 1
Groundwater Level and Flow Data
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Well ID
TOC
Elevation
(feet MSL)
Well Depth
(feet BGS)
Screened
Interval
(feet BGS)
Depth To
Water
(feet TOC)
Water Level
Elevation
(feet MSL)
MW-is
(Well #1)
20.91
13
3 -13
6.74
14.17
MW-2S
(Well #2)
21.44
13
3 -13
10.36
11.08
MW-3S
(Well #3)
23.02
18
8-18
11.50
11.52
MW-3A
21.93
20
5 -20
10.74
11.19
MW-4
18.42
13
3 -13
8.72
9.70
MW-5
17.90
18
3 -18
5.60
12.30
MW-6
20.03
13
3 -13
9.05
10.98
MW-7
19.40
13
3 -13
7.95
11.45
MW-8
21.21
18
3 -18
8.99
12.22
MW-9A
20.58
20
5 -20
4.82
15.76
MW-10
16.61
20
5 -20
2.89
13.72
MW-11
14.49
20
5 -20
2.80
11.69
MW-12S
16.18
20
5 -20
4.15
12.03
MW-13
20.69
20
5 -20
7.57
13.12
MW-14S
16.60
20
15 -20
3.24
13.36
MW-15
19.67
20
15 -20
5.20
14.47
MW-16
NA
20
NA
6.45
NA
MW-17
20.74
20
15 -20
6.15
14.59
MW-14D
17.45
40
35 - 40
5.24
12.21
MW-1D
21.14
50
40 - 50
7.80
13.34
MW-2D
21.80
49
39 - 49
11.72
10.08
MW-3D
22.83
50
40 - 50
11.95
10.88
Page l of 2

Table 1
Groundwater Level and Flow Data
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Well ID
Water Level
Elevation
Reference
Elevation
Vertical
Change
Horizontal
Change
K
n
I
v
(feet MSL)
(feet MSL)
feet
feet
(feet/day)
(feet/foot)
(feet/day)
MW-3A
11.19
12
0.81
65
0.805
0.08
0.012
0.125
MW-10
13.72
14
0.28
85
0.116
0.05
0.003
0.008
MW-11
11.69
1 12
1 0.31
70
0.009
10.04
1 0.004
1 0.001
MW-12S
12.03
1 13
1 0.97
1 80
1 0.322
1 0.06
1 0.012
1 0.065
NOTES:
1. Depth To Water was measured between December 4 and 13, 2018.
2. TOC = top of casing.
3. BGS = below ground surface
4. MSL = mean sea level
5. K - hydraulic conductivity. Values obtained from slug testing performed by EFM, Inc.
6. n - effective porosity. Values approximated based on grain size data from Phase II Design Hydrogeologic Report.
7. I - hydraulic gradient. Determined by dividing head change by horizontal distance to nearest contour line at each well location.
8. v - flow rate; GW flow rate calculated based on the modified Darcy equation: v = (K*I)/n.
Page 2 of 2

Table 2
Summary of Groundwater Analytical Data
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Analyte Group
Parameter
Phase 1 Monitoring Wells
GWPS
MW-is
(Well #1)
MW-2S
(Well #2)
MW-3S
(Well #3)
MW-3A
MW-4
MW-5
MW-6
MW-7
MW-8
MW-11)
MW-21D
MW-31)
Antimony
1
0.52 J
0.16 J
0.28 J
0.20 J
0.08 J
0.18 J
0.19 J
0.17 J
0.22 J
0.111
0.03 U
0.04 J
Arsenic
10
0.96 J
4.1 J
27
21
0.48 J
4.1 J
5.7
15
15
2.5 J
0.911
0.12 J
Barium
700
38.5
135
689
312
52.5
140
470
566
358
35.5
15.6
10.1
Beryllium
4*
0.05 U
0.05
0.10 J
0.05 U
0.07 J
0.06 J
0.05 U
0.05 U
Cadmium
2
0.14J
0.111
0.111
0.04J
0.14J
0.08J
0.17J
0.16J
0.08J
0.111
0.02U
0.02U
Cobalt
1*
0.27 J
1.4
3.0
8.3
0.22 J
1.2
2.9
12
3.4
0.27 J
0.12 J
0.08 J
Chromium
10
0.77 J
3.0 J
32
13
4.4 J
3.3 J
4.3 J
12
15
1.4 J
0.35 J
0.15 l'
Metals
Copper
1,000
1.9 J
1.5 J
1.5 J
1.2 J
0.65 J
0.87 J
1.3 J
1.2 J
1.11
1.6 J
0.35 J
0.54 J
(pg/L)
Lead
15
0.28 J
0.41 J
0.03 J
0.04 J
0.28 J
0.16 J
0.03 U
0.20 J
0.04 J
1.0 J
0.03 U
0.03 U
Nickel
100
3.1J
3.9J
8.1J
7.1J
1.5J
3.91
6.3J
6.3J
7.4J
1.6J
1.11
1.01
Selenium
20
1.9 J
4.6 J
0.53 U
0.53 U
0.74 J
4.4 J
3.7 J
0.53 U
0.53 U
0.30 J
0.19 J
0.60 J
Silver
20
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.09 J
0.05 U
0.05 U
Thallium
0.2*
0.05 U
0.08 J
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Tin
2,000*
0.05 U
0.05 U
0.05 U
0.05 U
0.24 J
0.55 J
0.05 U
0.05 U
0.05 U
0.17 J
0.05 U
0.05 U
Vanadium
0.3*
1.8
1.2
7.2
3.1
5.0
1.3
2.0
2.4
1.6
2.0
0.03 U
0.03 U
Zinc
1,000
8.1J
2.3J
3.6J
3.1J
4.0J
3.5J
2.3J
3.4J
3.0J
14
1.8J
1.8J
Acetone
6,000
9.06 U
0.12 U
9.44 J
9.06 U
9.06 U
9.06 U
10.30 J
9.63 J
9.06 U
9.06 U
9.06 L)
Benzene
1
0.24 U
9.06 U
1.30
1.69
0.24 U
0.24 U
0.24 U
0.24 U
0.48 J
0.24 U
0.24 U
0.24 U
1,2-Dichloroethane
0.4
0.02 U
0.25 U
0.24
0.13 J
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
cis-1,2-Dichloroethene
70
0.25 U
0.24 U
0.25 U
0.25 �
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
1,2,-Dichloropropane
0.6
0.04 U
0.0�
0.04 U
0.04 U
0.04 U
0.04
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
VOCs
Ethylbenzene
600
0.21 U
0.04 U
3.23 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
(pg/L)
Naphthalene
6
0.47 U
0.23 U
0.21 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
Toluene
600
0.23 U
0.21 U
) 47 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
Vinyl chloride
0.03
0.12 U
0.47 U
1.82
1.09
0.12 U
0.12 U
0.18 J
1.25
1.48
0.12 U
0.12 U
0.12 U
Tetrahydrofuran
NE
0.39 U
4.85
35.30
24.40
0.39 U
2.27
6.88
32.00
21.20
42.70
0.39 U
0.39 U
1,4-Dioxane
3
5.33
6.20
184
87
2.71 U
16.40
13.50
18.20
49.30
2.71 U
2.71 U
2.71 U
Acenaphthene
80
2.66 U
2.66 U
24.30
3.10 J
2.66 U
2.66 U
2.66 U
2.66 U
3.57 J
2.66 U
2.66 U
2.66 U
Benzo[g,h,i]perylene
200
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
SVOCs (pg/L)
Dibenzofuran
0.98*
4.28 U
4.28 U
9.191
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
Fluorene
300
2.95 U
2.95 U
13.90
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
Indeno[1,2,3-Cd]pyrene
0.05
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
Pesticides
Beta-BHC
0.02*
0.031 U
0.031 U
0.04 J
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
(pg/L)
Endrin Aldehyde
2
0.068 U
0.068 U
0.10
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
Inorganics (pg/L)
Sulfide
NE
100 U
100 U
100 U
100 U
3901
100 U
100 U
100 U
100 U
100 U
100 U
Page 1 of 2

Table 2
Summary of Groundwater Analytical Data
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Analyte Group
Parameter
Phase 2 Monitoring Wells
GWPS
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14S
MW-15
MW-16
MW-17
MW-14D
Antimony
1
0.10 J
0.06 J
0.17 J
0.13 J
0.06 J
0.05 J
0.05 J
0.04 J
0.04 J
Arsenic
10
0.03 J
9
3.2 J
22
1.11
0.59 J
1.4 J
3.2 J
0.03 U
0.03 U
Barium
700
48.8
368
55.0
398
47.5
49.3
95.2
256
67.7
8.5 J
Beryllium
4*
US J
0.05 I
0.05 U
0.05
0.05 U
0.05 J
0.09 J
0.05 J
0.05 l
Cadmium
2
0.02J
0.14J
0.10J
0.02U
0.06J
0.07J
0.08J
0.15J
0.04J
0.06J
Cobalt
1*
0.12 J
1.8
1.0
1.6
0.54 J
0.36 J
0.15 J
0.53 J
0.32 J
0.07 J
Metals
Chromium
10
0.15 Li
14
0.56 J
24
0.311
0.48 J
0.15 U
1.5 J
0.94 J
0.15 U
Copper
1,000
0.38 J
0.96 J
0.30 J
1.11
0.38 J
0.52 J
0.44 J
0.25 J
0.12 J
0.41 J
(pg/L)
Lead
15
0.03 U
0.03 J
0.04 J
0.03 U
0.16 J
0.73 J
0.10 J
0.12 J
0.06 J
0.03 U
Nickel
100
2.1J
12.1
5.7J
6.6J
3.91
1.8J
2.1J
1.51
5.2J
1.4J
Selenium
20
0.15 U
7.9 J
1.11
8.1 J
0.85 J
0.15 U
0.15 U
2.1 J
0.15 U
0.15 U
Silver
20
0.05 U
O.U5 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Thallium
0.2*
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Tin
2,000*
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Vanadium
0.3*
0.03 U
8.1
1.5
17.5
1.3
2.3
3.5
9.1
1.2
0.03 U
Zinc
1,000
3.3J
1.51
1.3J
1.2J
0.911
4.6J
0.87J
0.84J
1.51
2.0J
VOCs
(pg/L)
Acetone
6,000
9.06 U
'.06 U
11.80 J
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
Benzene
1
0.24 U
1.57
0.48 J
1.48
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
1,2-Dichloroethane
0.4
0.02 U
0.34
0.08 J
0.13 J
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
cis-1,2-Dichloroethene
70
0.25 U
0.311
0.25 U
0.34 J
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
1,2,-Dichloropropane
0.6
0.04 U
0.23
0.04 J
0.07 J
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
Ethylbenzene
600
0.21 U
0.44 J
0.21 U
0.23 J
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
Naphthalene
6
0.47 U
0.47 U
0.47 U
1.08 J
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
Toluene
600
0.23 U
') 23 U
0.23 1,
0.24 J
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
Vinyl chloride
0.03
0.12U
2.20
0.12U
2.21
0.12U
0.12U
0.12U
0.12U
0.12U
0.12U
Tetrahydrofuran
NE
0.39 U
25.42
8.02
38.75
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
1,4-Dioxane
3
2.71 U
5.40
8.15
8.82
2.71 U
2.71 U
2.71 U
2.71 U
2.71 U
2.71 U
SVOCs (pg/L)
Acenaphthene
80
2.66 U
2.66 U
2.66 U
2.66 U
2.66 U
2.66 U
2.66 U
2.66 U
2.66 U
2.66 U
Benzo[g,h,i]perylene
200
2.61 U
3.16 J
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
2.61 U
Dibenzofuran
0.98*
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
4.28 U
Fluorene
300
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
Indeno[1,2,3-Cd]pyrene
0.05
2.91 U
3.06 J
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
2.91 U
Pesticides (pg/L)
Beta-BHC
0.02*
0.031 U
U.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
0.031 U
Endrin Aldehyde
2
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
0.068 U
Inorganics (pg/L)
Sulfide
NE
100 U
328 J
100 U
115 J
100 U
100 U
100 U
100 U
100 U
100 U
Page 2 of 2

Table 2
Summary of Groundwater Quality Data - Detected Constituents Only
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
NOTES:
1. Table 2 lists analytes detected in the groundwater samples. Please refer to Environment 1, Incorporated laboratory analysis report for further details.
2. Groundwater samples were collected between December 4 - 13, 2018.
3. MDL = Method Detection Limit.
4. MRL = Method Reporting Limit.
5. GWPS = Groundwater Protection Standard: NCAC Title 15A Subchapter 2L Groundwater Standards or Interim Maximum Allowable Concentration (IMAC
6. 2L Standard = NCAC Title 15A Subchapter 2L Classifications and Water Quality Standards Applicable to the GWs of North Carolina (April 1, 2013).
7. J indicates the detected result is between MDL and MRL.
8. U indicates analyte not detected at indicated method detection limit.
9. pg/L = micrograms per liter.
10. ND = Not Detected. NE = Not Established. NA = Not Applicable.
11. Bold font indicates concentration exceeds 2L Standard or IMAC.
12. S.U. = Standard Units.
13. pS/cm = microsiemens per centimeter.
14.*=IMAC
Page 1

Table 3
Summary of Surface Water Analytical Results
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter
Surface
Water
Standard
Sample Locations and Analytical Results
SW-1
SW-2
SW-3
SW-4
Metals
(pg/L)
Antimony
640
0.17 J
0.04 J
0.05 J
0.04 J
Arsenic
10
1.6 J
0.68 J
0.44 J
0.16 J
Barium
21,000
108
53.8
77.5
74.1
Beryllium
6.5
0.31 J
0.05 U
0.05 J
0.111
Cadmium
2
0.15 J
0.02 U
0.02 J
0.04 J
Cobalt
4
0.79 J
0.19 J
0.32 J
0.62 J
Chromium
50
6.1
0.53 J
0.37 J
0.60 J
Copper
7
3.11
0.26 J
0.46 J
0.43 J
Lead
25
9.6
0.21 J
0.32 J
0.38 J
Nickel
88
2.1 J
0.65 J
0.79 J
0.75 J
Selenium
5
1.4 J
Thallium
0.47
0.08 J
0.07 J
Vanadium
NE
8.4
0.111
0.57 J
0.70 J
Zinc
50
22
1.7 J
3.6 J
4.5 J
VOCs (pg/L)
Toluene
11
0.38 J
Field
Parameters
pH (S.U.)
6.0 - 9.0
6.6
6.8
6.6
6.4
Conductivity at 25 °C (pS/cm)
NE
192
143
147
118
Temperature (°C)
NE
10
9
10
10
Turbidity (NTU)
50
106
7.86
8.30
8.83
Page 1 of 2

Table 3
Summary of Surface Water Analytical Results
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
NOTES:
1. Table 3 lists detected compounds in the surface water. Please refer to Environment 1, Incorporated laboratory report for further details.
2. Surface water samples were collected on December 5, 2018.
3. Surface Water Standard = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters, EPA Nationally
Recommended Water Quality Criteria for Aquatic Life & Human Life, or North Carolina Protective Values for Surface Waters
4. J indicates the reported result is estimated between the laboratry method detection limit and reporting limit.
5. U = indicates analyte not detected at indicated method detection limit.
6. pg/L = micrograms per liter.
7. NE = Not Established.
8. Bold font indicates analyte detection above the Surface Water Standard.
S.U. = Standard Units.
PS/cm = microsiemens per centimeter.
NTU = Nephelometric Turbidity Units.
Page 2 of 2

Table 4
Summary of Natural Attenuation Parameters
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Analyte Group
Parameter
Phase I Monitoring Wells
GWPS
MW-is
(Well #1 )
MW-2S
(Well #2)
MW-3S
(Well #3)
MW-3A
MW-4
MW-5
MW-6
MW-7
MW-8
MW-16
MW-1D
MW-2D
MW-3D
Carbon Dioxide
NE
72,000
119,000
346,000
214,000
46,000
164,000
278,000
354,000
348,000
346,000
22,000
8,000
6,000
Dissolved
Ethane
NE
0.0039 Jn
0.015 n
0.10 n
0.056 n
0.015 n
0.060 n
0.011 n
0.024 n
0.16 n
0.011 n
1.4 n
0.018 n
0.045 n
Gasses
(pg/L;
Ethene
NE
0.0050 Jn
0.0075 Jn
0.020 n
0.013 n
0.0089 Jn
0.0030 Un
0.019 n
0.017 n
0.0030 Un
0.0074 Jn
0.0030 Un
0.032 n
0.011 n
unless
noted)
Methane
NE
6.5 n
440 n
590 n
440 n
320 n
890 n
620 n
760 n
2,000 n
650 n
5600 n
45 n
54 n
Hydrogen(nM)
NE
2.1n
2.3n
3.3n
3.3n
2.5n
2.4n
2.8n
2.5n
3.0n
3.3n
4.8n
2.8n
2.1n
Acetic Acid
5,000'
110
150
270
200
170
240
230
170
200
44 J
220
130
180
Butyric Acid
NE
14 J
4.7 U
79 J
13 J
20 J
8 J
520
920
24 J
12 J
13 J
13 J
Hexanoic Acid
NE
12 U
17 J
220
160 J
12 U
28 J
100 J
250
180 J
12 U
12 U
12 U
12 U
i-Hexanoic Acid
NE
4.9U
4.9U
4.9U
4.9U
4.9U
4.9U
4.9U
4.9U
4g1J
4.9U
4.9U
4.9U
4.9U
Fatty Acids
(pg/L)
i-Pentanoic Acid
NE
7.5U
7.5U
9.7J
111
7.5U
7.5U
7.5U
7.5U
J
7.5U
7.5U
7.5U
7.5U
Lactic Acid
NE
14 U
14 U
14 U
58 J
14 U
14 U
14 U
14 U
1
27 J
20 J
55 J
27 J
Pentanoic Acid
NE
12 U
12 U
33 J
30 J
12 U
12 U
12 U
12 U
26 J
12 U
12 U
12 U
12 U
Propionic Acid
NE
55 J
71 J
110
120
81 J
89 J
93 J
80 J
89 J
4.4 U
60 J
66 J
86 J
Pyruvic Acid
NE
5.1 -
12 J
72 J
57 J
5.7 U
9.11
16 J
36 J
57 J
6.5 J
5.7 U
5.7 U
Chloride
250,000
33,000
54,000
190,000
178,000
5,000
59,000
34,000
88,000
144,000
30,000
13,000
13,000
21,000
Nitrate (as N)
NE
9 U
1,200
9 U
9 U
9 U
290
4,540
480
410
9 U
9 U
9 U
50
Total Dissolved Residue (TDR)
500,000
457,000
732,000
2,300,000
1,520,000
162,000
695,000
1,120,000
1,350,000
1,650,000
440,000
232,000
243,000
312,000
Sulfate
250,000
127,000
214,000
256,000
136,000
5,600
138,000
5,600
5,700
234,000
110,000
5,000 U
17,500
5,700
Other Natural
Attenuation
Biolo
Biological Oxygen Demand
NE
2,000 U
2,000 U
12,000
4,700
2,000 U
2,000 U
2,700
4,600
4,000
2,000 U
6,600
2,000 U
2,000 U
Parameters
Chemical Oxygen Demand
(COD)
NE
27,000
69,000
474,000
333,000
34,000
72,000
111,000
124,000
335,000
113,000
33,000
840 U
840 U
(pg/L)
Alkalinity (CaCO3)
NE
154,000
256,000
1,600,000
1,080,000
88,000
336,000
975,000
396,000
1,070,000
164,000
158,000
168,000
208,000
Iron
300
573
3,908
19,510
32,980
1,098
8,810
10,890
40,540
31,400
25,860
5,405
174
152
Manganese
50
12
284
642
954
36
172
436
578
1,093
117
273
30
0.31 U
Total Organic Carbon (TOC)
NE
7,710
22,860
164,000
115,000
10,540
22,580
38,480
74,560
90,280
41,000
8,270
1,700
2,350
Ferrous Iron
NE
345
3,510
19,170
30,200
764
3,950
11,080
28,600
30,700
23,000
5,100
50 U
50 U
Total Hardness
NE
339
453
917
620
94
420
938
771
910
180
139
139
126
pH (S.U.)
6.5 - 8.5
6.5
6.6
6.9
6.7
6.9
6.6
6.8
6.7
6.7
6.1
7.0
8.1
8.2
Conductivity at 25°C (pS/cm)
NE
773
688
1,390
1,488
233
773
984
1,964
1,249
370
420
414
511
Field
Temperature (°C)
NE
14
17
19
17
15
14
16
16
16
17
16
17
19
Parameters
Turbidity (NTU)
NE
6.11
7.25
3.31
4.38
25.8
8.12
1.26
6.23
7.42
7.82
7.58
3.50
1 U
ORP (mV)
NE
43
79
-51
-68
44
44
80
70
-25
97
78
22
31
Dissolved Oxygen ( /L)
NE
630
850
950
5,480
330
810
330
180
800
180
1,220
120
360
Page 1 of 3

Table 4
Summary of Natural Attenuation Parameters
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Analyte Group
Parameter
Phase II Monitoring Wells
GWPS
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14S
MW-15
MW-16
MW-17
MW-14D
Carbon Dioxide
NE
42,000
444,000
180,000
318,000
122,000
30,000
35,000
346,000
110,000
13,000
Dissolved
Ethane
NE
0.012 n
0.060 n
0.012 n
0.026 n
0.0032 Jn
0.0037 Jn
0.014 n
0.011 n
0.013 n
0.015 n
Gasses
(Ng/L; unless
Ethene
NE
0.0038 Jn
0.16 n
0.045 n
0.15 n
0.0068 Jn
0.011 n
0.0047 Jn
0.0074 Jn
0.0038 Jn
0.0085 Jn
noted)
Methane
NE
30 n
6,400 n
140 n
920 n
200 n
170 n
460 n
650 n
120 n
8.8 n
Hydrogen(nM)
NE
2.9n
2.6n
3.2n
3.4n
3.0n
2.9n
3.0n
3.3n
3.1n
3.0n
Acetic Acid
5,000'
45 J
24 U
45 J
130
46 J
52 J
37 J
44 J
32 J
42 J
Butyric Acid
NE
4.7 U
380
4.7 U
660
4.7 U
4.7 U
18 J
24 J
4.7 U
4.7 U
Hexanoic Acid
NE
12 U
250
24 J
12 U
12 U
12 U
12 U
12 U
12 U
12 U
i-Hexanoic Acid
NE
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
Fatty Acids
(Ng/L)
i-Pentanoic Acid
NE
7.5 U
7.5 U
7.5 U
7.5 U
7.5 U
7.5 U
7.5 U
7.5 U
7.5 U
7.5 U
Lactic Acid
NE
32J
95J
191
991
17J
18J
31J
27J
18J
52J
Pentanoic Acid
NE
12U
12U
12U
60J
12U
12U
12U
12U
12U
12U
Propionic Acid
NE
5.5 J
111
4.4 U
21 J
5.8 J
4.4 U
4.4 U
4.4 U
4.4 U
4.4 U
Pyruvic Acid
NE
5.7 U
130
5.7 U
140
5.7 U
5.7 U
5.7 U
6.5 J
5.7 U
5.7 U
Chloride
250,000
9,000
52,000
14,000
117,000
5,000 U
5,000 U
10,000
30,000
14,000
14,000
Nitrate (as N)
NE
9 U
9 U
9 U
250
50
9 U
9 U
9 U
90
Total Dissolved Residue (TDR)
500,000
373,000
1,670,000
691,000
1,290,000
379,000
196,000
260,000
440,000
654,000
287,000
Sulfate
250,000
63,700
211,000
146,000
6,100
10,100
67,100
103,000
110,000
383,000
6,100
Other Natural
Attenuation
Biolo
Biological Oxygen Demand
NE
2,000 U
6,200
2,000 U
6,600
2,000 U
2,000 U
2,000 U
2,000 U
2,000 U
2,000 U
Parameters
Chemical Oxygen Demand
(COD)
NE
840 U
259,000
54,000
317,000
45,000
23,000
36,000
113,000
54,000
840 U
(pg/L)
Alkalinity (CaCO3)
NE
244,000
1,320,000
550,000
630,000
292,000
74,000
63,000
164,000
36,000
258,000
Iron
300
557
363
13,560
2,075
917
2,303
2,645
25,860
1,470
12.08 U
Manganese
50
74
253
284
460
22
237
83
117
170
6.9 J
Total Organic Carbon (TOC)
NE
4,700
99,200
20,920
114,000
20,520
8,360
12,800
41,000
21,800
2,310
Ferrous Iron
NE
464
302
13,070
1,951
802
1,198
2,200
23,000
1,382
50 U
Total Hardness
NE
278
1,030
498
451
306
129
153
180
384
149
pH (S.U.)
6.5 - 8.5
6.9
6.5
6.8
6.6
6.0
6.4
6.5
6.1
5.8
7.8
Conductivity at 25°C (pS/cm)
NE
529
1,607
857
941
558
246
401
370
775
522
Field
Temperature (°C)
NE
13
11
11
13
16
13
16
17
17
17
Parameters
Turbidity (NTU)
NE
8.62
2.29
18.6
2.33
1 U
38.8
6.42
7.82
2.76
1 U
ORP (mV)
NE
99
108
64
105
72
99
85
97
71
94
Dissolved Oxygen ( /L)
NE
340
280
210
330
300
100 U
250
180
320
100 U
Page 2 of 3

Table 4
Summary of Natural Attenuation Parameters
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
NOTES:
1. Table 4 lists analytes detected in the groundwater samples. Please refer to Environment 1, Incorporated laboratc
2. Groundwater samples were collected between December 4 - 13, 2018.
5. MDL = Method Detection Limit. If multiple MDLs were reported for a single analyte, the highest MDL is presents
6. Compliance Limit = SWSL or 2L Standard.
5. GWPS = Groundwater Protection Standard: NCAC Title 15A Subchapter 2L Groundwater Standards or Interim M
8. J indicates the detected result is between MDL and MRL.
9. U = analyte not detected at indicated MDL.
10. pg/L = micrograms per liter.
11. NE = Not Established.
12. Bold font indicates concentration exceeds GWPS.
13. S.U. = Standard Units.
14. pS/cm = microsiemens per centimeter.
15. NTU = Nephelometric Turbidity Units.
16. nM = nanomoles
17. * = Interim Maximum Allowable Concentration (IMAC)
18. NS = Not sampled
19. n = The Laboratory does not hold NELAP/TNI accreditation for thwis method or analyte.
Page 3 of 3

Water Quality Monitoring Report
December 2018 Semiannual Sampling Event
Wood Project No. 6468-19-9035
FIGURES
wood.

SITE: Figure
TITLE: FI
C&D Landfill 9
802 RECYCLING LANE
GREENVILLE, NC 27834
SITE LOCATION MAP
CLIENT: w
wood* C&D LANDFILL INC.
SCALE: 1 "=2,001
,00 bATE: 05/01/2019 PROJECT: 6480199035
Wood Environment & Infrastructure Solutions, Inc.
4021 Stirrup Creek Drive, Suite 100 DRAWN BY: D. Hriciga TC
HECKED BY: D. Hriciga
Durham, NC 27703
[phone] LOCATION: 56548 142P t RTig\NC\NC DENR DSCA\DSCA Projects\DC640004 - CleanCleanDrycleaners\
565480142_PAR\Figures

MW-14D
MW-13x
_ - r
A �6e'
rip
MW-17 r
MW-9A
r
p w
MW-15 .114
-
7 si ;
MW-1+4S
-10 P
Phase 2
1 MW-12S MW-11
•� MW-8
'r . if - -
1
MW-1 D
MW-1
MW-2S - MW-6
-.
0.
Legend SW-2
® Surface Water Sampling Location
• Shallow Monitoring Well
Deep Monitoring Well y
Approximate Stream Location r ' ` Feet
Site Boundary Source. Esri, Digi 'I'�I � oEye, Earthstar Geographics, CNES/Airbus
AeroGRID, IGN, nd the GISa��ser Community
SITE: Figure
TITLE: FI
C&D Landfill 9
802 RECYCLING LANE
GREENVILLE, NC 27834 MONITORING WELL AND
SURFACE WATER SAMPLING LOCATION MAP
CLIENT: ^
wood* C&D LANDFILL INC.
SCALE: 1 " = 200 ' DATE: 05/01 /2019 PROJECT: 6480199035
Wood Environment & Infrastructure Solutions, Inc.
4021 Stirrup Creek Drive, Suite 100 DRAWN BY: D. Hriciga CHECKED BY: D. Hriciga
Durham, NC 27703
[phone] LOCATION: 56548 142P t RTig\NC\NC DENR DSCA\DSCA Projects\DC640004 - CleanCleanDrycleaners\
565480142_PAR\Figures

C&D Landfill
802 RECYCLING LANE
GREENVILLE, NC 27834
CLIENT:
wood* C&D LANDFILL INC.
Wood Environment & Infrastructure Solutions, Inc.
4021 Stirrup Creek Drive, Suite 100
Durham, NC 27703
[phone]
TITLE:
Figure
GROUNDWATER ELEVATION MAP
- DECEMBER 2018
3
SCALE: 1 " = 2001 DATE: 04/30/2019 1 PROJECT: 6480199035
DRAWN BY: D. Hriciga I CHECKED BY: D. Hriciga
LOCATION: P:\Government\State\NC\NC DENR DSCA\DSCA Projects\DC640004 - CleanCleanDrycleaners\
565480142PAR\Figures

Notes:
Metals concentrations in excess of standards are not illustrated.
Units are micrograms per liter (mg/L).
BRL = Contaminant concentrations were below reporting limits.
NE = No exceedances of applicable groundwater or surface water standards were reported.. e -
NS = Not Sampled
J = Estimated value below the laboratory reporting limit
IM MW-17 ; r
r.
...... .� � ,�. BRL _ :� ''•� z
YMW-15
BRL
f 5
q MW-14S
BRL
•i -
�.�� + MW-14D
�f BRL
MW-13,'
+NJ / "' BRL
Phase 2
MW-12S
jr Benzene 1.48
Vinyl Chloride 2.21 MW-11
1,4-Dioxane 8.82 1,4-Dioxane 8.15
SW-3 _
.�M
MW-3S
Benzene 1.3 MW-3D
Vinyl Chloride 1.82 -
1,4-Dioxane 184
Dibenzofuran 9.19 J
Oka
Beta-BHC 0.04 J
,j# � MW-3A
Benzene 1.69
r� Vinyl Chloride 1.09
1,4-Dioxane 87rq
_
*-'
I
MW-10
Benzene 1.57
Vinyl Chloride 2.2
1,4-Dioxane 5.4
i ' 1 MW=1 D
'' MW-1 S
"'. 1,4-Dioxane 5.33
MW-8
Vinyl Chloride 1.48
1 oxane 49.3
lip
7-1 - • � ' k F' 4 F i r
Nak-
Phase 1
MW-4
BRL
MW-5
1,4-Dioxane 16.4
I<
Vinyl Chloride 0.18 J
1,4-Dioxane 13.5
N
MW-7 SW-1
Vinyl Chloride 1.25 NE
1,4-Dioxane 18.2
f _-
x'I
J i �f c !. 7 4k; I—
,kM1 w 1,4-Dioxane 6.2AFK
s
Legend i4;'j�"► l`NIr. # sV,.
® Surface Water Sampling Location 40L 0-
• Shallow Monitoring Well
' ., - � i SW
Deep Monitoring Well ,�� " BRL 0 200 400
- Approximate Stream Location ��t'%._ Feet
Site Boundaryr, +►
Source: Es, Di,gi 11�I•L� , Earth�tarGeographics, CNES/Airbus DS, SDA, G
AeroGRID, IGN, d the G1= r ' mmu ity L
SITE: Figure
TITLE: FI
C&D Landfill 9
802 RECYCLING LANE GREENVILLE, NC 27834 GROUNDWATER AND SURFACE WATER
STANDARD EXCEEDANCE MAP - DECEMBER 2018
CLIENT: w
wood* C&D LANDFILL INC.
SCALE: 1 " = 200 ' DATE: 04/24/2019 PROJECT: 6480199035
Wood Environment & Infrastructure Solutions, Inc.
4021 Stirrup Creek Drive, Suite 100 DRAWN BY: D. Hriciga CHECKED BY: D. Hriciga
Durham, NC 27703
[phone] LOCATION: 56548 142P t RTig\NC\NC DENR DSCA\DSCA Projects\DC640004 - CleanCleanDrycleaners\
565480142_PAR\Figures

Water Quality Monitoring Report
December 2018 Semiannual Sampling Event
Wood Project No. 6468-19-9035
Attachment A
Laboratory Analytical Report
wood.

Environment 1,
rated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
PHONE [phone]
FAX [phone]
*** THIS IS A CORRECTED COPY OF PREVIOUSLY REPORTED DATA ***
ID#: 6003
JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE DATE COLLECTED: 12/05/18
4021 STIRRUP CREEK DR. STE 100 DATE REPORTED ; 02/21/19
DURHAM ,NC 27703
REVIEWED BY:
MW-4 MW-5 MW-6 MW-7 MW-8 Analysis Method
PARAMETERS MDI, MRL Date Analyst Code
PH (field measurement), Unite
6.9
fi.6
6.8
6.7
fi,7
12/05/18
PTC
4500NB-11
BOD, mg/1
2.0
2.0
--- U
--- U
2.7
4.6
4.0
SZ/06/18
HMM
5210B-1i
COD, mg/1
O.B40
20,0
34
72
ill
124
335
12/10/18
SBJ
H8000-79
Nitrate Nitrogen as N, mg/1
0.009
0004
--- U
0,29
4,54
12/06/18
BLD
353.2 R2-
Nitrate Nitrogen as N, mg/1
0.009
0,04
0,48
0.41
12/07/18
CLO
353.2 R2-
Total Organic Carbon, mg/1
0,129
1.0
10,54
22,58
38,48
74,56
90,28
12/11/18
SBJ
531OC-11
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
88
336
975
396
1070
12/10/18
OM9
2320H-11
Chloride, mg/l
5,0
5.0
5
59
34
88
144
12/10/18
BOB
4500CLB-1
Cyanide, ug/1
5.0
5.0
--- U
--- U
--- U
--- U
--- U
12/10/18
BBJ
450OCNE-1
Total Hardness, mg/1
94
420
939
771
910
12/10/18
HMM
2340C-11
Total Dissolved Residual mg/1
14
10
162
695
12/06/18
JTH
254OC-21
Total Dissolved Residue, mg/1
1.0
30
1120
1350
1650
12/11/10
JMH
2540C-11
Sulfate, mg/1
5.0
5.0
5.6
130
5.6
517
234
12/06/18
8BJ
4500SO429
Antimony, ug/l
0,03
1.0
0.08 J
O.is J
0,19 J
0,17 J
0,22 J
12/11/18
AKS
BPA200.8
Arsenic, ug/1
0,03
5.0
0.48 J
4.1 J
5.7
15
15
12/11/18
AKS
EPA200.8
Barium, ug/1
0,03
10.0
52.5
140
470
566
358
12/11/18
Axe
EPA200.8
Beryllium, ug/1
0.05
1.0
0.10 J
--- U
--- U
0.07 J
0,06 J
12/11/10
AK8
EPA200.8
Cadmium, ug/1
0.02
140
0,14 J
0.08 J
0,17 J
0.16 J
.08 J
12/11/18
ASH
EPA200.8
Cobalt, ug/1
0.03
100
0,22 J
1,2
2.9
12
3,4
12/11/18
AK8
EPA200.8
Total Chromium, ug/1
0.15
5.0
4.4J
3.3 J
4.3 J
12
15
12/11/19
ASH
HPA200.8
Copper, Ug/1
0,03
10.0
0.65 J
0,87 J
1.3 J
1,20
1.1J
12/11/18
AKS
BPA200.8
Iron, ug/l
12,OB
solo
1098
8810
10990
40540
31400
01/10/19
AKS
3111E-ll
Manganese, ug/1
0.31
10.0
36
172
436
12/28/18
LFJ
EPA2D0.7
Manganese, ug/1
0.31
10.0
578
1093
01/03/19
LFJ
EPA200.7
Lead, ug/1
0,03
5.0
0, 28J
0416 J
--- U
0,20 J
.D4J
12/11/18
AKS
EPA200.0
Mercury, ug/1
0.05
0.20
--- U
--- U
0.06 J
--- U
--- U
12/17/10
RIM
245.1 R3-
Nickel, ug/l
0903
10.0
1.5J
3,9J
6,3J
6.3 J
7.4 J
12/11/18
ASS
EPA200.8
Selenium, ug/1
0,53
10.0
0.74 J
4.4J
3,7 J
12/11/18
ASS
EPA200.8
Selenium, ug/l
0,53
10.0
--- U
--- U
12/26/18
HIM
3113E-10
Silvan, u9/1
0.05
5.0
--- U
--- U
--- U
--- U
--- U
01/02/19
AKS
EPA200.8
Thallium, ug/1
0105
1.0
--- U
--- U
--- U
___ U
--- U
12/11/18
AKS
EPA200.8
Tin, ug/1
0,05
100.0
0,24 J
0455 J
--- U
--- U
--- U
12/11/18
AKS
HPA200lS
Vanadium, ug/1
0,03
1.0
5.0
1,3
2.0
2,4
1.6
12/11/18
AK8
EPA200.8
zinc, ug/l
0.11
10.0
4.0 J
3.5J
2.3J
3,4J
3.0 J
12/11/10
Ass
EPA200.8
Sulfide, ug/1
100
1000
--- U
390 J
--- V
--- U
--- U
12/07/18
LFJ
4500020-1
Conductivity (at 25c), uMhos/cm
1.0
1.0
233
773
984
1964
1249
12/05/18
PJC
2510E-11
Dissolved Oxygen, mg/1
0.1
0,1
0,33
0,81
0,33
Otis
0,80
12/05/18
PJC
450000-11
Temperature, °C
15
14
16
16
16
12/05/18
PJC
2550E-10
Iron, Perroue, ug/l
50.00
200.0
764
3950
11080
28600
30700
12/05/18
SBJ
3500FEB-1
Static Water Level, feet
8.72
5.60
9.05
7,95
8.99
12/05/18
PJC
Well Depth, feet
15098
9.50
16. 65
16,33
20,26
12/05/18
PJC
Carbon Dioxide, mg/l
1,0
1.0
46
164
270
354
348
12/05/18
NMM
45000O2C-
J = Ha trmflted valu0 between the MUL find MAL, U = Below ALL Quantltation Llmita.

Environment 1, Incorporated
114 OAKMONT DRIVE
PNONE
(252)
756-6208
GREENVILLE, N.C. 27858
FAX
(252)
756-0633
*** THIS IS A CORRECTED COPY OF PREVIOUSLY REPORTED DATA ***
ID#: 6003
JUDSON WHITEHURST (C&D
LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
DATE COLLECTED:
12/05/18
4021 STIRRUP CREEK DR*
STE 100
DATE REPORTED
02/21/19
DURHAM ,NC 27703
REVIEWED BY:
MW-4 MW-5
MW-6 MW-'/ MW-8
Analysis
Method
PARAMETERS MDL
MRL
Date Analyst
Code
ORP, m
Turbidity (Field), NTU 1.0
+44 +44
1.0 25.8 8,12
+00 +70 -25
1.26 6.23 7.42
12/05/18 PJC
12/05/18 PJC
2580B
213OB-11
S Betimflted value between the MDL end MAL, U = Below ALL QuantltaClon Llmita.

Environment 1�
GREENVILLE, N.C. 27658
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WEITEHURST (C&D LANDFILL) CLIENT ZD: 6003
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: HIC
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/05/18
DURHAM, NC 27703 DATE EXTRACTED: 12/07/18
DATE ANALYZED: 12/14/18
REVIEWED BY: DATE REPORTED: 02/21/19
PESTICIDES AND PCB'S
EPA METHOD 8081B R2(07)
PARAMETERS, ug/l
MDL
MRL
W-4
MW-5
MW-6
mw-7
MW-8
1,
Aldrin
0.029
0.050
---
V
___
U
___
U
___
U
2,
Alpha-BHC
0,032
0.050
---
U
---
U
---
U
---
U
---
U
3,
Beta -HNC
0.031
0.050
---
U
---
U
---
U
---
U
---
U
4,
Delta-BHC
0,030
0.050
---
U
---
U
---
U
---
U
---
U
5.
Gamma-HHC (Llndane)
0.032
0.050
---
U
---
U
---
U
---
U
---
U
6,
Chlordane
0,320
0.500
---
U
---
U
---
U
---
U
---
U
7,
414-DDD
0.051
0.100
---
U
---
U
---
U
---
U
---
U
8,
4,4-DD8
0.049
0.100
---
V
---
U
---
U
---
U
---
U
9.
4,4-DDT
0,052
0.100
---
U
---
U
---
U
---
U
---
U
10.
Dieldrin
0.042
0,075
---
U
---
U
---
U
---
U
---
U
11,
Endosulfan I
0.056
0.100
---
U
---
U
---
U
---
U
---
U
12.
Endosulfan II
0,046
0.100
---
U
---
U
---
U
---
U
---
U
13,
8ndoeulEan Sulfate
0.072
0.100
---
V
---
U
---
U
---
U
---
U
14,
Endrin
0.053
0.100
---
U
---
U
---
U
---
U
---
U
15.
Endrin Aldehyde
0.068
0,100
---
U
---
U
---
U
---
U
---
U
16.
Heptachlor
0.039
0.050
---
U
---
U
---
U
---
U
---
U
17.
Heptachlor Epoxide
0,042
0,075
---
U
---
U
---
U
---
U
---
U
18.
Methoxychlor
0.530
1.000
---
U
---
U
___
U
___
U
"""
U
19,
Pcb's (Aroclors)
0.500
2.000
---
U
---
U
---
U
---
U
---
U
20,
Toxaphene
0.690
1.500
___
U
__.
U
U
___
U
U
J = Estimated value between the MBL and MRL, ll = Below ALL puantl tfltion Limlte.

Environment 1, Incorporated
l l4 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8151A R1(96)
CLIENT ID:
ANALYST:
DATE COLLECTED:
DATE EXTRACTED:
DATE REPORTED:
1Q
PHONE [phone]
FAX [phone]
6003
HIC
12/05/18
12/06/18
02/21/19
Date Analyzed
12/08/18
12/00/18
12/08/18
la/08/18
la/21/18
MW-9
m-5
MW-6
MW-0
mw-8
PARAMETBR9t U9/l MOL MRL
1. 2,4-D
0.36
2.000
--- U
--- U
--- U
--- U
--- U
2. Dinoeeb
0.54
1.000
--- U
--- U
--- U
--- U
--- U
3, 2t4t5-TP
0,42
2.000
--- U
--- U
--- U
--- U
--- U
9, 2t9o5-T
0.49
2.000
--- U
--- U
--- U
--- U
--- U
J Eetimflted Value between the MDL and MRL, U = BeloN ALL Quantitation Llmite.

Environment 1, Inco
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DRe STE 100 DATE COLLECTED: 12/05/18 Page: 1
DURHAM, NC 27703 DATE EXTRACTED: 12/10/18
DATE REPORTED: 02/21/19
REVIEWED BY*
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
PARAMETERS, ug/1
Data
NDL
Analyzed
MRL
12/18/18
Mw-4
12/18/18
MW-5
12/19/18
MW-6
11/19/18
MW-7
11/19/18
MW-8
1,
Acenaphthene
2,66
10.000
---
U
---
U
---
U
---
U
3,57
J
2,
Acenaphthylene
2,60
10,000
---
U
---
U
---
u
---
u
---
V
3,
Anthracene
2.97
10.000
___
U
___
U
___
U
___
U
___
u
4.
Benzo [a]antrhacane
4.16
10.000
---
V
---
U
---
U
---
u
---
U
5.
Benzo[b]Lluoranthens
3,32
10,000
---
V
---
U
---
U
---
U
---
U
6,
Benzo[k]Lluoranthene
4.23
104000
---
U
---
u
---
U
---
V
---
U
7,
Henzo[g,h,i]psrylsne
2.61
10.000
---
U
---
u
---
V
---
U
---
U
8,
Benzo[alpyrens
3.27
10.000
---
U
---
V
---
U
---
V
---
U
9.
4-Bromophenyl Phenyl Ether
2.63
10,000
---
u
---
U
---
U
---
U
---
U
10,
Butyl Benzyl Phthalate
5.78
10,000
---
U
---
U
---
V
---
U
---
U
11,
Bis(2-Chloroethoxy) Methane
3.14
20,000
---
V
---
U
---
U
---
U
---
U
12,
Bis(2-Chloroethyl) Ether
2.59
10,000
---
U
---
V
---
U
---
U
---
V
13,
Eia(2-Chloro-l-methylethyl) Ether
2.58
104000
---
U
---
U
---
U
---
V
---
U
14,
2-Chloronaphthalene
2,17
10.000
---
U
---
U
---
U
---
U
---
U
15,
4-Chlorophenyl Phenyl Ether
5.42
30.000
---
V
---
U
---
V
---
U
---
U
16,
Chryeena
4.04
10.000
---
u
---
U
---
U
---
U
---
U
17,
Dibenzo[a,hlanthracens
2,78
10.000
---
U
---
U
---
U
---
U
---
U
18,
Di-N-Butyl Phthalate
3,09
10400
---
U
---
U
---
u
---
U
---
U
19,
Dlmethyl Phthalate
3.78
10.000
---
U
---
V
---
U
U
U
20.
Diethyl Phthalate
3,92
10.000
---
U
---
U
---
U
---
U
---
u
21,
2,4-Dinitrotoluene
3,95
10,000
---
U
---
U
---
U
---
u
---
U
22.
2,6-Dinitrotoluene
3.88
10,000
---
V
---
U
---
U
---
U
---
U
23,
Di-N-Oetyl Phthalate
2.81
10.000
---
V
---
U
---
U
---
U
---
U
24.
Bis-(2-Ethylhexyl) Phthalate
9,97
15.000
---
V
---
U
---
u
---
U
---
V
25.
Fluoranthene
3,92
10,000
---
U
---
V
---
U
---
0
---
U
26,
Fluorene
2.95
10,000
---
U
---
U
---
U
---
U
---
U
27,
Hexachlorobenzene
2,61
10,000
---
U
---
U
---
U
---
U
---
u
28,
Hexachlorocyclopentadlens
4.16
10,000
---
V
---
U
---
U
---
U
---
U
29,
Indeno[1,2,3-Cd3pyrene
2,91
106000
---
U
---
V
---
U
---
U
---
U
30,
Ieophorone
3,74
10,000
---
U
---
U
---
U
---
U
---
U
31,
Nitrobenzene
1,85
10400
---
V
---
V
---
U
u
U
32,
N-Nitroeodimethylamine
4.25
10,000
---
U
---
V
---
U
---
U
---
U
33,
N-Nitroeodiphanylamine
3,95
10,000
---
U
---
U
---
V
---
U
---
U
34,
N-Nitr000di-N-Propylamine
4,06
104000
---
U
---
U
---
U
---
U
---
U
35.
Phenanthrene
3,24
104000
---
U
---
u
---
U
---
U
---
V
36,
Pyrene
3,63
104000
---
U
---
U
---
U
---
U
---
U
37.
4-Chloro-3-Methylphenol
3,79
20,000
---
u
---
U
---
u
---
U
---
u
38.
2-Chlorophenol
2,75
10,000
---
V
---
U
---
U
---
U
---
U
39,
0-Cresol
3.69
10.000
---
U
---
U
---
U
---
U
---
U
40,
P-Cresol
9.12
10.000
---
U
---
U
---
V
U
U
41.
2,4-DSchlorophanol
5,19
10,000
---
U
---
U
---
U
---
U
---
U
42,
2,6-Dichlorophenol
4,89
100000
---
U
---
U
---
U
---
U
---
u
43,
2,4-Dimethylphenol
3,21
10.000
---
V
---
u
---
V
---
V
---
V
44.
4,6-Dinitro-2-Methylphenol
4,77
50,000
---
U
---
U
---
U
---
U
---
V
45,
2,4-Dinitrophsnol
4,37
50,000
---
U
---
V
---
U
---
V
---
u
46.
Ethyl Methaneeul Lonate
5.26
20.000
---
U
---
U
---
U
---
U
---
u
47,
Methyl MethanesulLonate
4.92
10,000
---
U
---
U
---
U
---
U
---
U
J • Estimated value between the MDL and MRL, U • Below ALL Quantitation LSmite.

Environment 1, Inco
Q& W
GREENVILLE, N.C. 27858
FAX [phone]
CLIENT: JUDSON WHITES PA (C&D LANDFILL) CLIENT IDs 6003
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DRe STE 100 DATE COLLECTED: 12/05/18 Page: 2
DURHAM, NC 27703 DATE EXTRACTED: 12/10/18
DATE REPORTED: 02/21/19
REVIEWED BY:
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
PARAMRTBRB, ug/1
Date
MDL
Analyzed
MRL
12/18/19
MW-4
12/18/18
MW-5
12/19/18
NW-6
12/19/18
MW-7
la/19/18
NW-8
48,
2-Nitrophenol
3,64
104000
---
U
---
U
---
U
---
U
---
U
99.
4-NStroBhenol
3.17
50.000
---
U
---
V
---
U
V
---
U
50,
Pentachlozophenol
5,33
25.000
M.
U
---
U
---
U
---
U
---
U
1186
104000
---
U
---
U
---
U
---
U
---
U
51,
Phenol
52,
2,31416-Tetrachlorophenol
3,12
30,000
---
U
---
U
---
U
W.
V
---
U
53,
2,4,5-Trichlorophanol
4,17
10,000
---
U
---
U
---
U
---
U
---
U
54,
2,406-Trichlorophenol
3.84
10,000
---
U
---
U
---
U
M.
U
---
U
55,
Acetophenone
2.89
10.000
---
U
---
U
---
U
---
U
---
U
56,
2-Acetylaminofluorene
3,98
20.000
---
U
---
U
---
U
---
U
---
U
57.
4-Aminobiphenyl
4,12
20,000
---
U
---
U
---
U
---
U
---
U
58,
Benzyl Alcohol
4,47
20,000
---
U
---
U
---
U
---
U
---
U
59,
4-Chloroaniline
3,36
20.000
---
U
---
U
---
U
---
D
---
V
60,
Chlorobenailate
5,12
10,000
W.
U
---
U
---
U
---
U
---
U
61,
Diallate
2,98
10,000
---
U
---
V
---
U
---
U
---
U
62,
Dlbenzofuran
4,28
10,000
---
U
---
U
---
D
---
U
---
V
63,
3,3-Dichlorobenzldine
4,22
20,000
---
U
---
U
---
U
---
U
---
U
64,
Dimethoate
3,98
20,000
---
U
---
U
---
U
M.
U
---
U
65,
P-Dlmethylaminoazobenzens
2,89
10.000
---
U
---
D
---
V
---
U
---
U
66,
7,12-Dimethylbsnz[a3anthzacene
5,26
10,000
---
U
---
U
---
U
---
U
---
U
67.
3,3-Dimethylbenzadine
3,21
10,000
---
U
---
U
---
U
---
U
---
U
68,
1,3-Dinitrobenzene
2.89
20,000
---
U
---
U
---
U
---
V
---
U
69.
Diphenylamine
5.10
10,000
---
V
---
U
---
U
---
V
---
U
70,
Diaulfoton
4.28
10.000
---
U
---
U
---
U
---
U
---
U
71.
Famphur
3,98
20,000
---
U
---
U
---
U
---
O
---
U
72,
Hexachloropropene
4,31
10,000
---
U
---
V
---
U
---
U
---
U
73,
IeoeaEzole
2.88
30.000
---
U
---
V
---
U
--
U
---
U
74,
Kepone
2,78
20,000
---
U
---
V
---
U
---
U
---
U
75,
Methapyrilene
3,54
100,000
---
U
---
U
---
U
---
U
---
U
76,
3-Msthylchloroanthrene
4,21
10,000
---
V
---
U
---
N
---
U
---
V
77,
2-Mathylnaphthalens
3,79
10,000
---
U
---
V
---
U
---
U
---
U
78,
Methyl Parathion
4,32
10,000
---
U.
---
V
---
U
---
V
---
U
79,
m-Cresol
3.81
10,000
---
U
---
U
---
U
---
U
---
V
B0,
1,4-Naphtho9uinons
4.00
10,000
---
U
M.
U
---
U
---
U
---
U
81.
1-Naphthylamine
5161
10,000
---
U
---
U
---
U
---
U
---
V
82.
2-Naphthylamine
4.62
10.000
---
U
---
U
---
U
U
---
U
83,
2-Nitroaniline
3,61
501000
---
U
---
V
---
U
---
U
---
U
84,
3-Nitroaniline
4181
504000
---
U
---
U
---
U
---
U
---
U
85.
4-Nitroaniline
4.22
20,000
---
U
---
V
---
U
---
V
---
U
86.
5-Nitro-O-Toluidine
4.01
10,000
---
U
---
U
---
U
---
U
---
V
87,
N-Nitroaodi-n-butylamine
3.63
10.000
---
U
---
U
---
U
---
U
---
U
88%
N-Nitroeodiethylamine
3.83
20.000
---
U
---
U
---
U
---
U
---
V
89,
N-Nitrosomethylethylamine
3,83
10,000
---
U
---
U
---
V
---
U
---
U
90,
N-Nitrosopiperldine
5.19
20,000
---
U
---
U
---
V
---
V
---
U
91.
N-Nitr000pyrrolidine
2.89
10,000
---
V
---
U
---
U
---
U
---
V
92,
Parathion
3,12
10,000
---
V
---
U
---
U
---
U
---
U
93,
Pentaahlorobenzene
3,92
10,000
---
U
---
U
---
U
---
U
---
U
94,
Pentachloronitrobanzane
3.71
20,000
---
V
---
U
---
U
---
U
---
U
J Estimated value between the MDL and MRL, V a Below ALL puantitation Limits.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR, STE 100
DURHAM, NC 27703
REVIEWED BY:
SEMI -VOLATILE ORGANICS
F.PA METHOD 8270D R4(07)
CLIENT ID:
iPaetewater 1DI i0
PHONE [phone]
FAX [phone]
6003
ANALYST:
JAP
DATE COLLECTED:
12/05/18
DATE EXTRACTED:
12/10/18
DATE REPORTED:
02/21/19
Page: 3
PARAMETBRS, ug/l
Date
MDL
Analyzed
MRL
12/18/18
Mw-4
12/18/18
Mw-5
12/19/19
MW-6
11/19/10
MW-7
12/19/18
MW-0
95,
Phenacetin
4,41
20,000
---
U
---
U
---
U
---
U
---
U
96.
1,4 eenzenediamine
2,99
10.000
---
U
--'
U
'-'
U
---
U
---
U
97,
Phorate
3,96
10,000
---
U
---
U
---
U
---
U
---
U
98.
Pronamide
3,69
10,000
---
U
---
U
---
U
---
U
---
U
99.
eafrole
4,12
10,000
---
D
---
U
---
U
---
U
---
U
100,
1,2,4,5-Tetrachlorobenzene
5.01
10,000
---
U
---
U
---
U
---
U
---
U
101,
Thionazin
4,62
20.000
---
U
---
U
---
U
---
U
---
U
102,
0-Toluidine
4.11
10,000
---
U
---
U
---
U
---
U
---
U
103,
1,3,5-Tzinitrobenzene
3,98
10,000
---
U
---
U
---
U
---
U
---
U
104.
010,0-Triethyl Phoaphorothioate
3.61
10,000
---
U
---
U
---
U
---
U
---
V
105,
Hexachloroethane
1,49
30.000
---
U
---
U
---
U
---
U
---
U
106,
Zeodrin
3,11
209000
---
U
---
U
---
U
---
U
---
U
J = 8etlmated value between the MDL and MRL, U Below ALL Duantitation Limits.

Environment 1, Incorporated
114 OAKMON 1 DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
LANDFILL APPENDIX 2I
EPA METHOD 8260E R2(96)
CLIENT ID:
PHONE [phone]
FAX [phone]
6003
ANALYST:
JAP
DATE COLLECTED:
12/05/18
DATE ANALYZED:
12/18/18
DATE REPORTED:
02/21/19
Page: 1
PARAMETBRS, ug/1
MDL
MRL
MW-4
MW-5
MW-6
MW-7
MW-B
1,
Chloromethane
0,77
3,000
---
u
---
U
---
U
---
D
---
U
2.
Vinyl Chloride
0.12
0,200
---
V
---
U
0.10
J
1.25
1,48
3.
Bromomethane
0.67
10.000
---
V
---
U
---
U
---
V
---
U
4.
Chloroethans
0.48
10.000
---
U
---
U
---
U
---
U
---
U
5,
Trichlorofluoromethane
0,24
1.000
---
U
---
U
---
U
---
U
---
V
6,
1,1-Dichloroethene
0.17
5.000
---
V
---
V
M.
U
__
U
___
U
7,
Acetone
9.06
100,000
---
U
---
V
---
U
10,30
J
9.63
J
8.
Iodomethane
0.16
10.000
---
U
•--
U
---
U
---
U
---
D
9.
Carbon Disulfide
0.13
300.000
---
U
---
U
---
V
---
U
---
U
10,
Methylene Chloride
0.64
1.000
---
V
___
V
___
V
___
U
___
U
11.
trans-1,l-Dichloroethene
0.13
54000
---
V
---
U
___
U
___
U
-__
V
12,
1,1-Dichloroethane
0.20
5.000
---
U
---
U
---
U
---
U
---
u
13.
Vinyl Acetate
0.20
50,000
---
U
---
U
---
U
---
U
---
U
14,
Cie-1,2-Dichloroethene
0,25
5.000
---
U
---
U
---
V
---
U
---
U
15,
1-Butanone
2.21
100,000
---
V
---
V
---
U
---
U
---
U
16.
Bromochloromethane
0.27
3,000
---
U
---
U
---
V
---
V
---
U
17.
Chloroform
0,25
5.000
---
U
•--
V
---
U
---
V
---
V
18,
1,1,1-Trichloroothane
0.19
1.000
---
U
---
D
---
U
---
U
---
U
19,
Carbon Tetrachloride
0.04
B.apo
---
U
---
U
---
U
---
U
---
U
20,
Benzene
0,24
1.000
---
U
---
U
M.
U
---
U
0.48
J
21,
1,1-Dichloroethane
0,02
0,200
---
V
---
U
---
U
---
U
---
U
22,
Trichloroethene
0,23
1.000
---
U
---
V
---
U
---
V
---
U
23.
1,2-Dichloropropane
0.04
0.200
---
U
---
u
---
U
---
V
---
U
24,
Bromodichloromethane
0,04
0.200
---
V
---
V
---
U
---
V
---
U
25.
Cie-10-Dichloropropene
0.06
0,200
---
❑
---
U
---
U
---
U
---
U
26,
4-Methyl-2-Pentanone
1.19
100.000
---
V
---
V
---
U
---
U
---
V
27.
Toluene
0.13
1.000
---
u
---
U
---
U
---
U
---
U
28.
trans-1,3-Dichloropropene
0,04
0,200
---
U
---
V
---
U
---
U
---
U
19,
1, 1,2-Triohloroethana
0.03
0.100
---
V
---
U
---
U
---
U
---
U
30,
Tetrachloroethens
0.10
0,200
---
U
---
V
---
U
---
U
---
u
31.
2-Hexanone
1.57
50.000
---
U
---
U
---
U
---
D
---
V
32,
Dibromochloromethans
0.03
0,200
---
U
---
U
---
U
---
u
---
u
33,
1,2-DSbromeethene
0,03
0,200
---
V
---
U
---
V
---
U
---
V
34,
Chlorobenzene
0,30
3,000
---
U
---
U
---
U
---
u
---
U
35,
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
---
U
---
U
---
U
---
U
36,
Bthylbenzene
0,21
1.000
---
V
---
U
---
U
---
U
---
U
37,
Xylenes
0.68
5,000
---
U
---
U
---
U
---
U
---
U
38,
Dibromomethans
0.28
10,000
---
U
---
U
---
U
---
U
---
V
39,
Styrene
0.19
1.000
---
U
---
V
---
U
---
U
---
U
40,
Bromoform
0.20
3,000
---
V
---
U
---
U
---
U
-•-
U
41,
1,1,1,2-Tetrachloroethane
0.03
0,200
---
U
---
U
---
V
---
U
---
V
42.
1,.2,3-Trichl oropropana
0.09
0.100
---
U
---
V
---
U
---
U
---
V
43,
1,4-Dichlorobenzene
o.39
1.000
---
U
---
U
---
U
---
U
---
U
44.
1,1-Dichlorobenzene
0,32
5.000
---
U
---
U
---
U
M.
V
---
U
45.
1,1-Dlbromo-3-Chloroprapane
0.07
0.200
---
u
--
U
---
U
---
U
---
U
96,
Acrylonitrile
2.71
200.000
---
U
---
U
---
U
---
U
---
u
47.
Crane-1,4-Dlchl0ro-2-Butane
0,42
100.000
---
U
---
V
---
U
---
u
---
V
40,
Aorolein
1.97
4,000
---
U
---
U
--^
U
---
U
---
U
J Estimated value between the MDL and MRL, V Below ALL Quantitatlon Limlta.

Environment 1, I
lS@d
GREENVILLEI N.C. 27858
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/05/18 Page: 2
DURHAM, NC 27703 DATE ANALYZED: 12/18/18
DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260E R2(96)
PARAMETERS, Ug/l
MDL
MRL
MW-4
MN-5
MN-6
MW-7
MN-8
491
Allyl Chloride
0,20
10.000
---
U
---
V
---
U
---
V
---
U
50,
Chloroprene
0,21
20,000
---
U
---
U
---
V
---
V
---
V
51,
1,3-Dichlorobanaene
0,41
5.000
---
U
---
U
---
V
---
U
---
U
52,
Dichloroditluoromethane
0,51
5.000
---
U
---
U
---
U
---
U
---
U
53.
10-Dichloropropane
0,28
1.000
---
U
---
U
---
U
---
U
---
U
54,
2,2-Dichloropropane
0,17
15,000
---
U
---
U
---
U
---
D
---
U
55,
1,1-Dichloropropane
0.22
5.000
---
U
---
U
---
U
---
U
---
D
56.
Ethyl Methacryl ate
0.16
10.000
---
U
---
U
---
U
--
D
V
57,
Eexachlozobut adlene
0430
0.100
---
V
---
U
---
U
---
U
---
U
5B,
Ieobutyl Alcohol
12,80
100.000
---
V
---
U
---
U
---
U
---
U
59,
Methacrylonitrile
1,93
100,000
---
U
---
V
---
U
---
U
---
V
60,
Methyl Methacrylate
0,25
30,000
---
V
---
D
---
U
---
U
---
U
61,
Naphthalene
0,47
6,000
---
U
---
U
---
V
---
V
---
V
62,
Propionitrile
3,26
150,000
---
U
---
U
---
U
---
U
---
U
63,
1,2,4-Trichlorobenaene
0.50
10,000
---
V
---
U
---
U
---
V
---
U
69,
Acetonitrile
36.29
55.000
---
U
---
U
---
U
---
V
---
U
65,
Tetrahydro[uran
0,39
1.000
---
U
2,27
6.88
32,00
21.20
66,
1,4-Dioxane
2,71
3,000
---
U
16,40
13,50
18,20
49,30
J eetlmated value between the MDL and MRL, U Below ALL Quantltation Limits.

.Environment 1, Incorporated
GREENVILLE, N.C. 27858
wastewater IDi 10
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/05/18
DURHAM, NC 27703 DATE ANALYZED: 12/18/18
/f� DATE REPORTED: 02/21/19
REVIEWED BY: _� j%f'
LANDFILL APPENDIX II
EPA METHOD 8260E R2(96)
PARAMETERS, ug/l
MDL
HAL
Trip
Blank
1,
Chloromethane
0,77
3,000
---
U
2,
Vinyl Chloride
0,12
0.290
---
U
3,
Bromomethane
0,67
10,000
---
U
4,
Chloroethane
0.48
10.00D
---
U
5,
Trichlorofluoromethane
0,24
1.000
---
U
6,
111-Dichloroethens
0,17
5.000
---
U
7,
Acetone
9,06
100,000
--
U
8,
Iodomethane
0,26
10,000
---
U
9,
Carbon Disulfide
0.23
ID0.000
---
U
10,
Methylene Chloride
0.64
1.000
---
U
11.
Crane-1,2-Dichloroethane
0.23
5.000
---
U
12,
1,1-Dichloroethane
0.20
5.000
---
U
13,
Vinyl Acetate
0,20
50.000
---
U
14,
Cie-1,2-Dichloroethene
0,25
5.000
---
U
15.
2-Butanons
2,21
100,000
---
U
16,
Bromochloromethane
0,27
3.000
---
U
17,
Chloroform
0,25
5.000
---
U
18.
1,1,1-Trichloroethane
0.19
11000
---
U
19.
Carbon Tetrachloride
0.04
0,200
---
U
20,
Benzene
0.24
1.000
W.
U
21,
1,2-Dichloroethane
0.02
0,200
---
U
22.
Trichloroethane
0,23
1.000
---
U
23.
1,2-Dichloropropans
0,04
0,200
---
U
24.
Bromodichloromethane
0,04
0,200
---
U
25,
Cie-1,3-Diohloropropene
0.06
0,200
---
U
26,
4-Methyl-2-Pentanone
1.19
100,000
---
U
27,
Toluene
0,23
1.000
---
U
28,
trans-1,3-Dichloropropene
0,04
0,200
---
U
29,
1,1,2-Trichloroethane
0,03
0.200
---
U
30,
Tetrachloroethene
0.10
0.200
---
U
31,
2-Hexanone
1,57
50,000
---
U
32.
Dibromochloromethane
0.03
0,200
---
U
33,
1,2-Dibromosthans
0,03
0.200
---
U
34.
Chlorobenzens
0.30
3,000
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
36,
Ethylbenzene
0,21
1.000
---
U
37,
Xylenes
0.68
5.000
---
U
39,
Dibromomethane
0.28
10,000
---
U
39,
Styrene
0.19
1.000
---
U
40.
Bromoform
0.20
3.000
---
U
41,
1,1,2,2-Tetrachloroethane
0.03
0.200
---
U
42,
1,2,3-Trichloropropans
0.09
0,200
---
U
43,
1,4-Dlchlorobenaene
0.39
1.000
---
U
44.
1,2-Dichlorobenzens
0,32
5.000
---
U
45.
1,2-Dibromo-3-Chloropropane
0,07
0.200
---
U
46,
ACrylonitrile
2,72
200,000
---
U
47.
Crane-1,4-Dichloro-2-Butene
0,42
100,000
---
U
48.
Acrolein
1,97
4.000
---
U
Page: 3
J Satimated value between the MOL and MRL, U Below ALL Ouantitation Limits.

Environment 1, Incorporated)
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC ,�Je03
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260B R2(96)
CLIENT ID:
PHONE [phone]
FAX [phone]
6003
ANALYST:
JAP
DATE COLLECTED:
12/05/18
DATE ANALYZED:
12/18/18
DATE REPORTED:
02/21/19
PARAMETERS, ug/l
MDL
EEL
Trlp
Blank
49.
Allyl Chloride
0.20
10,000
---
U
50.
Chloroprene
0.21
20,000
---
U
51.
1,3-Dichlorobenzene
0.41
5.000
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
53,
1,3-Dlchloiopropane
0.28
1.000
---
54.
2,2-DSchloropropane
0.17
15,000
---
U
55,
1,1-DSchloropropene
0,22
5.000
---
U
56,
Ethyl Methacrylate
0.16
10.000
---
U
57,
Eexachlorobutadlene
0.10
0,200
---
U
5B,
Ieabutyl Alcohol
12.00
100.000
---
U
59,
Methacrylonitrile
1,93
100.000
---
U
60,
Methyl Methacrylate
0.25
30,000
---
U
61,
Naphthalene
0.47
6.000
---
U
62,
Proplonitrile
3.26
150,000
---
U
63,
1,2,4-Trichlorobenzene
0.50
10,000
---
U
64.
Acetonitrlle
36.29
55,000
---
U
65,
Tetrahydro£uran
0,39
1.000
---
U
66,
1,4-Dioxane
2.71
3,000
---
U
Page: 4
J Betimated value between the MDL and MRL, U = Helow ALL Quantltation Limlta.

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ro
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8260 Dup. 1
O
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MMMMMMM
N
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m
m
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9
O
p
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9
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C
1
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a
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9
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m
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N

Environment 1, Incorporated
GREENVILLE, N.C. 27858 FAX [phone]
ID#: 6003 A
JUDSON WHITEHURST (C&D
LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
DATE
COLLECTED:
12/04/18
4021 STIRRUP CREEK DR.
STE 100
DATE
REPORTED
02/21/19
DURHAM ,NC 27703
REVIEWED BY:
MW-IS MW-1D
MW-2S MW-2D
MW-3S
Analysis Method
PARAMETERS MDL
MRL
Date Analyst Code
PH (field me nsurement), Unite
81
69
32/04/18
JNL
45DOHH-11
J Estimated value between the MDL and MRL, U Below ALL Ouantltation Limits.

Enwhfi[impm Flo D[0wroOP gd
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
JfJDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM INC 27703
PAAAMSTBRS
Turbidity (field), NTU
MW-1S MW-1D
MOL MRL
1.0 1.0 6.11 7.58
PHONE [phone]
FAX [phone]
ID#: 6003 A
DATE COLLECTED: 12/04/18
DATE REPORTED : 02/21/19
REVIEWED BY: N -
MW-2S MW-2D MW-3S Analysis Method
Date Analyst Code
7.25 3.50 3,31 12/04/10 JNL 213OB-11
J e 8atlmated value between the MDL end MAL, U = Belew ALL Quantltation Llmlte.

Environment 1, Incorporated
GREENVILLE, N.C. 27858
JUD SON WHITEHURST (C&D LANDFILL)
AMC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR, STE 100
DURHAM INC 27703
i
Wastewater ID, 10
PHONE [phone]
FAX [phone]
ID#: 6003 A
DATE COLLECTED: 12/04/18
DATE REPORTED : 02/21/19
REVIEWED BY:
MW-3➢
MW-3A
Analy ele
Method
PARAMETERS
MEL
HELPDate
Analyst
CO de
PH (field measurement), Unite
8.2
6.7
12/04/IB
JNL
4500HB-11
BOD, mg/l
2.0
2.0
--- U
4.7
12/05/18
EDE
5210E-11
COD, mg/1
0,040
2090
--- U
333
12/06/18
SEJ
II8000-79
Nitrate Nitrogen as N, mg/1
0.009
0.04
0.05
--- U
12/05/18
OIL
353.2 R2-93
Total Organic Carbon, mg/1
0,129
1.0
2,35
Ile
12/11/19
SEJ
531OC-11
Alkalinity (to PH 4.5), mg CaCO3/1
1.0
1.0
209
1080
12/10/18
JMS
2320D-11
Chloride, mg/1
5.0
5.0
21
178
12/10/18
ADS
4500CLB-11
Cyanide, ug/1
5.0
5.0
--- U
--- U
12/30/18
SBJ
450OCNE-11
Total Hardness, mg/1
126
620
12/10/18
HHN
2340C-11
Total Dissolved Residue, mg/1
1.0
10
312
12/06/18
JTH
254OC-11
Total Dissolved Residue, mg/1
1.0
10
1520
12/11/10
ME
254OC-.11
Sulfate, mg/1
5.0
5.0
5.7
136
12/06/18
SHJ
45009042811
Antimony, ug/l
0,03
1.0
0.04 J
0,20 J
12/11/18
AAS
EPA200.B
Arsenic, ug/l
0,03
5.0
0,12 J
21
12/11/18
ARE
BPA200.0
Barium, ug/l
0.03
10.0
10.1
312
12/11/18
ASS
BPA200.8
Beryllium, ug/I
0.05
1.0
--- U
--- U
12/11/18
ASS
BPA200.8
Cadmium, ug/l
0,02
1.0
--- U
0.04 J
12/11/18
ARE
EPA200.8
Cobalt, ug/1
0.03
1.0
aloe J
8.3
12/11/18
ARE
EPA200.8
Total Chromium, ug/1
0.15
5.0
--- U
13
12/11/18
ARE
HPA200.e
Copper, ug/1
0,03
10.0
0.54a
1.2 J
12/11/18
AKS
BPA200.8
Iron, ug/1
12,08
Solo
152
32980
12/26/18
ARE
3111H-11
Manganese, ug/1
0,31
10.0
--- U
954
12/11/18
LFJ
EPA200.7
Lead, ug/l
0,03
5 6 a
--- U
0,04 J
12/11/18
ARE
HPA200.8
Mercury, up/1
D.05
0.20
--- U
--- U
12/17/10
MTM
245.1 R3-94
Nickel, ug/l
0,03
10.0
1.OJ
7,1J
12/11/18
ARE
BPA200.8
Selenium, ug/1
0.53
10.0
0.60 J
12/11/18
ASS
8PA200.8
Selenium, ug/1
0.53
10.0
--- U
12/26/18
MTM
3113B-30
Silver, ug/1
0.05
5.0
--- U
--- U
01/02/19
ARE
SPA200.8
Thallium, ug/I
0.05
1.0
--- U
--- V
12/21/18
AKE
HPA200.8
Tin, ug/1
0.05
100.0
--- U
--- U
12/11/10
AKE
8PA200.8
Vanadium, ug/1
0,03
1.0
--- U
3.1
12/11/18
AKS
EPA200.8
Zinc, ug/1
0.11
10.0
1.ea
3.1J
12/11/18
AKS
EPA200.8
Sulfide, ug/1
100
1000
--- U
--- U
12/07/18
LFJ
450052➢-11
Conductivity (at 25c), uMhos/cm
1.0
1.0
511
1488
12/04/18
PHL
25100-11
Dissolved Oxygen, mg/1
0.1
0.1
0,36
5,48
12/04/18
JNL
450000-11
Temperature, °C
19
17
12/04/18
JNL
2550E-10
Iron, Ferrous, ug/1
50,00
200.0
--- U
30200
12/05/18
SEJ
3500FEB-11
Static Water Level, feet
30,35
12,70
12/04/18
JNL
Well Depth, feet
52,30
23,44
12/04/18
JNL
Carbon Dioxide, mg/l
1.0
1.0
6
214
12/05/18
HIS
45000O2C-11
ORP, m
+31
-60
12/04/18
JNL
2580E
Turbidity (Field), NTU
1.0
1.0
--- U
4,38
12/04/18
JNL
2130E-11
J setimated value between the NOL and MRL, U 0elaw ALL Quantitation Llmite.

Environment 1I Inco
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
waatewater 1Di 10
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 A
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: HIC
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18
DURHAM, NC 2,703 DATE EXTRACTED: 12/07/18
/ DATE ANALYZED: 12/14/18
REVIEWED BY: DATE REPORTED: 02/21/19
PESTICIDES AND PCB'S
EPA METHOD 8081E R2(07)
Page: 1
PARAMETERS, ug/l
MDL
MHL
M -18
MW-10
Mw-28
Mw-2D
MH-36
1,
Aldrin
0,029
0.050
---
U
---
U
---
u
---
V
---
V
2,
Alpha-BHC
0.032
0.050
---
V
---
U
---
U
---
U
---
U
3.
Bete-BHC
0,031
0.050
---
U
---
V
---
U
---
U
0,04
J
4.
Delta-8HC
0.030
0.050
---
V
---
V
---
U
---
U
---
U
5.
Gamma-HHC (Lindana)
0.032
0.050
---
U
---
u
---
u
---
U
---
U
6.
Chlordane
0.320
0.500
---
V
---
U
---
a
---
U
---
U
7,
4,4-ODD
0.051
0.100
---
U
---
U
---
U
--
II
--
U
8.
4,4-DDE
0,049
0.100
---
U
---
V
---
U
---
u
---
U
9.
4,4-DDT
0.052
0.300
---
U
---
V
---
U
---
U
---
U
10.
Dieldrin
0,042
0,075
---
U
---
U
---
U
---
a
---
U
11,
EndoaulEan I
0$056
0.100
---
U
---
U
---
U
---
V
---
U
12,
8ndoeul Ean II
0.046
0.100
---
II
---
U
---
U
---
U
---
V
13,
8ndoaul Ean Sulfate
0.072
0.300
___
u
___
V
___
U
___
u
___
U
14,
Endrin
0.053
0.100
---
U
---
V
---
U
---
U
---
u
15.
Endrin Aldehyde
0.068
0.100
---
U
---
V
---
U
---
U
0.30
16.
Heptachlor
0.039
0.050
---
U
---
U
---
U
---
U
---
U
17,
Heptachlor Epoxide
0,042
0,075
---
V
---
U
---
U
---
U
---
U
18,
Methoxychlor
0,530
1.000
---
V
---
U
---
U
---
U
---
U
19.
Pab'e (Aroclose)
0.500
2.000
---
V
---
U
---
U
U
p
20.
Toxaphene
0.690
1.500
J.
---
U
---
U
---
U
---
U
---
U
T = Eetlmated value between the MDL and MRL, U HalOw ALL Uuantltatlon Limits.

Environment 1, 11
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
�gd
CLIENT: J'UDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
PESTICIDES AND PCH'S
EPA METHOD 8081E R2(07)
CLIENT ID:
Drinking Water Dt 37715
Wastewater I➢i 10
PHONE [phone]
FAX [phone]
6003 A
ANALYST:
HIC
DATE
COLLECTED:
12/04/18
DAT E
EXTRACTED:
12/07/18
DAT E
ANALYZED:
12/14/18
DATE
REPORTED:
02/21/19
PARAMETERS, ug/1
MDL
MRL
MW-3D
MW-3A
1,
Aldrin
0,029
0.050
---
U
---
U
2,
Alpha -HNC
0.032
0.050
---
U
---
U
3.
Beta-BHC
0,031
0.050
---
U
---
V
4.
Delta-BHC
0,030
0.050
---
U
---
U
5.
Gamma-BHC (Lindane)
0.032
0.050
---
U
---
V
6,
Chlordane
0.320
0.500
---
U
---
U
7,
4,4-DDD
0.051
0.100
---
V
---
U
8.
4,4-DDE
0,049
0.300
---
U
---
U
9,
4,4-DDT
0,052
0.100
---
U
---
U
10,
Dleldrin
0,042
0,075
---
D
---
U
11,
Endoaulfan I
0.056
0.100
---
U
---
U
12,
Endoaulfan II
0,046
O.lDO
---
U
---
U
13,
Endoeulfan Sulfate
0,072
0.100
---
U
---
U
14,
Endrin
0,053
0.100
---
U
---
D
15.
Endrin Aldehyde
0.068
0.100
---
V
---
U
16.
Heptachlor
0.039
0.050
---
U
---
U
17.
Heptachlor Epoxide
0.042
0,075
---
U
---
U
18,
Methoxychlor
0,530
1.000
---
U
---
V
19.
Peb'e (Aroclore)
0.500
2,000
---
❑
---
U
20,
Toxaphene
0.690
1.500
---
U
---
V
Page: 2
J 8etimated value between the MDL 8rtd MRL, U Below ALL Ouantitation Limits.

Environment 1,
1140AKMONT DRIVE F HVNt (Loz) /bb-b2Otl
GREENVILLE, N.C. 27858 FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 A
A14EC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: SIC
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18
DURHAM, NC 27703 DATE EXTRACTED: 12/06/18
DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8151A R1(96)
Page: 1
Date Analyses
12/07/18
12/07/18
12/08/18
la/07/18
la/al/18
w-19
MW-lD
[ -2S
MW-2D
MW-39
PARR TRRR. ug/l MDL MRL
1, 214-D
0.36
2,000
--- U
--- U
--- U
--- U
--- U
2, Dinaaeb
0.54
11000
--- U
--- U
--- U
--- U
--- U
3, 2,4,5-TP
0,42
2.000
--- U
--- U
--- U
--- U
--- U
4, 114, 5-T
0.97
1.000
--- U
--- u
--- u
-- u
--- U
J BetimaEed value between thB RDL anfl D:RL, U Relow ALL Quantitation Limits,

��dorro����� Flo D�c�oQpoQ��c��l
wastewater IDi 10
ago
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 A
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: HIC
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18 Page: 2
DURHAM, NC 27703 DATE EXTRACTED: 12/06/18
DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8151A R1(96)
Date
Analyzed
12/08/le
la/21/18
MW-3D
MW-3A
PARAMETERS, ug/1
MDL
MRL
1.
2,4-D
0.36
2.000
--- u
--- u
2.
DSneeeb
0.54
1.000
--- V
--- u
3.
2,4,5-TP
0,42
2.000
--- V
--- V
4,
2,415-T
0,47
2.000
--- u
--- V
T = Eetlmated value between the MDL end MRL, V = Below ALL Quantitation Limite.

Environment 1, Incorporated
GREENVILLEI NI 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 A
ANALYST:
JAP
DATE COLLECTED:
12/04/18
DATE EXTRACTED:
12/10/18
DATE REPORTED:
02/21/19
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
Page: 1
PARAMeTERH, ug/l
Date
MDL
Analyzes
MEL
12/18/18
W-10
12/18/18
Mw-lD
1211811e
Mw-2B
la/18/18
Nw-2D
12/x7/IB
Mw"3S
1,
Acenaphthene
2,66
10,000
---
U
---
U
---
V
---
U
24,30
2,
Acenaphthylene
2,60
10,000
---
U
---
V
---
U
---
U
---
U
3,
Anthracene
2,97
10,000
---
D
---
U
---
U
---
U
---
U
4,
Benzo[alantrhacene
4,16
10,000
---
V
---
U
---
U
---
U
---
U
5.
eenzo [b]Eluorenthene
3.32
10.000
---
U
---
V
---
U
U
U
6.
Benzo[klfluoranthene
4,23
10,000
---
U
---
u
---
V
---
U
---
U
7,
BeRZO[g,h,ilperylene
2,61
10,000
---
U
---
U
---
U
---
U
---
U
8,
Benzo[alpyrene
3,27
10,000
---
U
---
U
---
U
---
U
---
U
9,
4-Bromophenyl Phanyl Ether
2,63
10,000
---
V
---
U
---
U
---
V
---
U
10,
Butyl Benzyl Phthalate
5.78
10,000
---
U
---
U
---
U
M.
U
---
U
11.
Bie(2-Chloroethoxy) Methane
3.14
10,000
---
U
---
U
---
V
---
U
---
U
12.
Bie(2-Chloroethyl) Ether
2,58
10,000
---
U
---
U
---
V
---
U
---
U
13.
Bie(2-Chloro-l-methylethyl) Ether
2,58
10,000
---
U
---
V
---
V
---
U
---
U
14,
2-Chloronaphthalene
2,17
10,000
---
U
---
U
---
U
---
U
---
U
15,
4-Chlorophenyl Phenyl Ether
2,42
10,000
---
U
---
U
---
U
---
U
---
U
16,
Chryeene
4,04
10,000
---
U
---
U
---
u
---
U
---
U
17,
Dibenzo[a,hlanthracene
2.78
10,000
---
U
---
U
---
U
---
U
---
U
18,
Di-N-Butyl Phthalate
3,09
104000
---
U
---
u
---
U
---
U
---
U
19,
Dimethyl Phthalate
3,78
10,000
---
U
---
U
---
U
---
U
---
U
20,
Diethyl Phthalate
3,92
10,000
---
U
---
U
---
U
---
ll
---
U
21.
2,4-Dinlerotoluene
3.95
30.000
---
U
---
U
---
U
--
D
U
22.
2,6-Di nitrotoluerte
3,08
10.000
---
U
---
V
---
U
--
U
U
23.
Di-N-Octyl Phthalate
2,01
10,000
---
U
---
U
---
U
---
U
---
U
244
Big-(2-Hthylhexyl) Phthalate
9,97
154000
---
U
---
U
---
U
---
U
---
U
25,
Fluoranthene
3,92
10.000
---
U
---
U
---
V
---
U
---
U
26,
Fluorene
2,95
10,000
---
V
---
U
---
U
---
U
13.90
27,
Hexachlorobenzene
2,61
10,000
---
V
---
U
---
U
---
V
---
V
20,
Hexachlorocyclopentadiene
4,16
10.000
---
U
---
U
---
U
---
U
---
V
29,
Pndeno[1,2,3-Cdlpyrene
2191
10,000
---
U
---
U
---
U
---
U
---
U
30,
Iaophorone
3,74
10400
---
U
---
U
---
U
---
U
---
U
31,
Nitrobenzene
2,85
10,000
---
U
---
U
---
U
---
U
---
U
32.
N-Nitroaodimethylamine
4.25
10,000
---
U
---
U
---
V
---
U
---
u
33.
N-Nitroeodlphenylamine
3195
10,000
---
U
---
U
---
U
---
U
---
U
34,
N-Nitroeodi-N-Propylamine
4,06
10,000
---
U
---
V
---
U
---
U
---
U
35,
Phenanthrene
3,24
10,000
---
U
---
U
---
U
---
U
---
U
36,
Pyrene
3,63
10,000
---
U
---
U
---
U
---
U
---
V
37,
4-Chloro-3-Methylphenol
3,79
20,000
---
U
---
u
---
U
---
U
---
D
384
2-Chlorophenol
2,75
10.000
---
U
---
U
---
V
---
U
---
u
39.
0-Creaol
3,68
104000
---
U
---
V
---
V
---
U
---
V
40,
P-Creaol
4.12
10.000
---
U
---
V
---
V
--
u
---
U
41.
2,4-Dichlorophanol
5119
10.000
---
U
---
U
---
U
---
u
---
U
42,
2,6-Dichlorophanol
4189
10.000
---
U
---
U
---
U
---
U
---
U
43,
2,4-Dimethylphenol
3,21
10.000
---
U
---
a
---
U
---
U
---
U
44.
416-Dinitro-2-Methylphenol
4,77
50.000
---
U
---
U
---
U
---
U
---
U
45.
2,4-Dinitrophenol
4,37
50,000
---
U
---
V
---
U
---
U
---
U
46,
Ethyl Methaneeulfonate
5,26
20,000
---
U
---
U
---
V
---
U
---
U
47,
Methyl Metheneeulfonate
4,92
10,000
---
U
---
U
---
V
---
U
---
U
J = Estimated value between the MDL and MRL, U e Below ALL puantitation Limits.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
Dxin king Water Its 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 A
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18
DURHAM, NC 27703 DATE EXTRACTED: 12/10/18
DATE REPORTED: 02/21/19
REVIEWED BY:
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
Page: 2
PARAMHT8R8, u9/1
Date
MDL
Analyzes
MRL
12/10/18
MW-18
12/18/18
MW-ID
12,18,8
MW-28
Sa/18/18
MW-aD
12/17/18
MW-38
48,
2-Nitrophanol
3,64
10,000
---
V
---
U
---
u
---
U
---
U
49.
4-Nitrophen0l
3,17
50,000
---
V
---
U
---
U
---
U
---
U
50,
Pentachlorophenol
5,33
25,000
---
U
---
V
---
U
---
U
---
U
51,
Phenol
1186
10.000
---
U
___
u
___
V
___
U
___
u
52.
2,3, 9,6-Tet rachlorophenol
3.12
10.000
---
V
---
U
---
u
---
v
---
u
53.
2,4,5-Triohlorophenol
4.17
30.000
---
V
---
U
___
u
___
U
___
u
54.
2,4,6-Trlohlorophenol
3.84
104000
---
V
---
U
---
U
u
___
u
55,
Acetophenone
2,89
10.000
---
U
---
U
---
U
---
U
---
U
56,
2-Acetylamino[luorene
3.98
20,000
---
U
---
U
---
U
---
U
---
U
57.
4-Aminobiphenyl
4.12
20,000
---
U
---
U
---
U
---
U
---
U
58,
Benzyl Alcohol
4,47
20,000
---
U
---
U
---
U
---
U
---
U
59,
4-Chlorcaniline
3,36
M000
---
V
---
u
---
u
---
u
---
u
60.
Chlorobensil me
5112
304000
---
V
---
U
---
U
---
U
---
U
61,
➢iallate
2,98
10.000
---
U
---
U
---
U
---
U
---
U
62,
Dibenzofuran
4,28
10.000
---
U
---
U
---
U
---
U
9.19
0
63,
3,3-Dichlorobenzidine
4,22
20.000
---
V
---
U
---
U
---
U
---
U
64,
Dimethoate
3.98
20,000
---
U
---
U
---
U
---
U
---
U
65.
P-Dimathylamino azobensene
2.89
104000
---
U
---
U
66,
7,12-Dimethylbenz(a)anthracene
5,26
10.000
---
U
---
U
---
U
---
v
---
U
67.
3,3-Dimethylbenzadine
3,21
10. 000
---
U
---
U
---
D
---
U
---
U
68.
1,3-Dinitrobenzens
2,89
20.000
---
U
---
U
---
U
---
U
---
u
69,
Diphenylamine
5.10
10,000
---
U
---
U
---
U
---
U
---
V
70,
Dieulioton
4,28
10,000
---
U
---
U
---
U
---
V
---
II
71,
Famphur
3,98
20,000
---
V
---
u
---
U
---
U
---
U
72,
Hexachloropropene
4,31
10,000
---
V
---
u
---
U
---
U
---
U
73,
Isosairols
2080
10,000
---
U
---
V
---
U
---
U
---
U
74,
Kepone
2,78
20.000
---
U
---
U
---
U
---
V
---
U
75,
Methapyrilene
3,54
100,000
---
U
---
V
---
U
---
U
---
U
76%
3-Methylchloroanthrene
4,21
10.000
---
U
---
U
---
U
---
D
---
u
77,
2-Methylnaphthalens
3,79.
10,000
---
U
---
U
---
U
---
U
---
u
78.
Methyl Parathion
4.32
30.000
___
U
_--
U
___
U
___
u
___
U
79,
m-Cresol
3,81
10.000
---
U
---
U
---
U
---
U
---
U
80,
1,9-NaphthoquSnone
4.00
10.000
---
U
---
U
---
V
U
---
U
01.
1-Naphthylamine
5.61
10.000
---
U
---
V
---
U
---
U
---
U
82.
2-Naphthylamine
4,62
10.000
---
U
---
U
---
U
---
U
---
U
B3.
2-Nitroaniline
3,61
50,000
---
U
---
U
---
U
---
U
---
U
84.
3-Nitroaniline
4.81
50.000
---
U
---
u
---
D
--
u
U
85.
4-Nitroaniline
4..12
20.000
---
U
---
U
---
U
--
V
V
86.
5-Nitro-O-Toluidine
4.01
104000
---
U
---
U
---
U
---
V
---
U
87.
N-NitrOeodl-n-butylamine
3.63
10.000
---
U
---
U
---
U
---
U
---
U
88.
W-Nitroeodiethylamine
3.83
20.000
---
V
---
V
---
U
---
U
---
U
89.
N-Nitroecmethyl ethylamine
3.83
10.000
---
v
---
U
---
U
---
U
---
U
90.
N-Nitrosopiperidine
5.19
20,000
---
U
---
U
---
V
---
U
---
U
91.
N-Nltrosopyrrolidlne
2.89
10,000
---
V
---
u
---
u
---
U
---
U
92.
Parathion
3,12
10,000
---
V
---
U
---
V
---
U
---
U
93.
Pentachlorobenzene
3,92
10,000
---
U
---
U
---
V
---
V
---
U
94,
Pentachloronitrobanzene
3.71
20,000
---
U
---
U
---
U
---
II
---
U
S It Estimated value between the MDL and MRL, O � Below ALL Qunntltation Llmite.

Environment 1, Incorporated
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHVRST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 A
ANALYST:
JAP
DATE COLLECTED:
12/04/18
DATE EXTRACTED:
12/10/18
DATE REPORTED:
02/21/19
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
Page: 3
PARAMETERS, ug/l
Date
MDL
Analyzes
MRL
12/18/18
MW-18
12/18/18
Mw-1D
12/1S/le
mw-2s
12/18/18
MW-2D
12/29/18
MW-39
95,
Phenacetin
9.41
20.000
---
V
---
U
---
V
D
U
96,
1,4 Henzenediamine
2,99
10,000
---
V
---
U
---
U
---
V
---
V
99,
Phorata
3.86
10.000
---
U
---
U
---
V
V
U
98,
Pronamlde
3.69
10,000
---
U
---
D
---
D
---
V
'--
U
99,
Safrole
9.12
10.000
---
V
---
U
---
V
---
V
---
U
100,
1,2,4,5-Tetraohlorobenzene
5.01
10.000
---
V
---
U
---
V
---
V
---
V
101.
Thionazin
4,62
20,000
---
V
---
U
---
V
---
V
---
U
102,
0-Toluidine
4011
10,000
---
D
---
D
---
V
---
U
---
V
103,
1,3,5-Trinitrobenzene
3.98
10,000
---
U
---
V
---
U
---
U
---
U
104.
0,0,0-Triethyl Phosphorothloate
3.61
10,000
---
V
---
D
---
V
---
U
---
U
105.
Hexaohloroethane
1.49
10,000
---
V
---
V
---
U
---
V
---
U
106,
Ieodrin
3,11
20,000
---
V
---
U
---
V
---
U
---
V
S = Eetlmated value between the MDL and MRL, U ealOW ALL Vuantltation Limits.

Environment 1, Inco
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
LIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 A
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18
DURHAM, NC 27703 DATE EXTRACTED: 12/10/18
DATE REPORTED: 02/21/19
REVIEWED BY:
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
C
PARAMETERS, ug/1
Date
MDL
Analyzes
MEL
la/18/1B
Mw-3D
12/18/18
Mw-3A
1,
Acenaphthens
2,66
10:000
---
U
3,10
J
2,
Acenaphthylene
2,60
10.000
---
U
---
U
3,
Anthracene
2,97
10.000
---
U
---
U
4,
Benzo[a]antrhaoene
4.16
10.000
---
u
---
U
5,
Benzo[blfluoranthene
3,32
10,000
---
U
---
U
6,
Benzo(klfluoranthene
4.23
10.000
---
U
---
U
7.
eenzo[g,h,llperylene
2,61
10.000
---
U
---
U
Be
Eenzo[alpyrens
3,27
10,000
---
V
---
U
9.
4-BYom0phenyl Phenyl Ether
2,63
10,000
---
U
---
U
10.
Butyl Benzyl Phthalate
5,78
10,000
---
U
---
U
11,
Bis(2-Chloroathoxy) Methane
3.14
l0.ODO
---
U
---
U
12,
Bis(2-Chloroethyl) Ether
2,50
10,000
---
V
---
U
13,
Bis(2-Chloro-l-methylethyl) Ether
2.58
10,000
---
U
---
U
14.
2-Chloronaphthalens
2,17
1D.000
---
V
---
U
15,
4-Chlorophenyl Phenyl Ether
2,42
10,000
---
U
---
V
16.
Chrysens
4,04
10,000
---
U
---
U
17.
DSbenzo[a,hlanthracene
2,78
10,000
---
U
---
U
18.
Di-N-Butyl Phthalate
3.09
10,000
•--
U
---
U
19.
Dimethyl Phthalate
3,78
10,000
---
U
---
U
20.
Diethyl Phthalate
3,92
10,000
---
U
---
U
21.
2,4-Dinitrotoluene
3.95
10,000
---
U
---
U
22.
2,6-Dinitrotoluene
3.BB
10.000
---
U
---
U
23.
Di-N-Octyl Phthalate
2,81
10.000
---
U
---
D
24,
Bis-(2-Ethylhexyl) Phthalate
9,97
15:000
---
U
---
U
25,
Fluoranthens
3,92
10,000
---
U
---
u
26,
Fluorene
2,95
10.000
---
u
---
U
27.
Hexachlorobenaens
2,61
10.000
---
U
---
U
28,
Eexachlorocyelopentadiene
4,16
10,000
---
U
---
U
29,
Indeno[1,2,3-Cd)pyrene
2,91
10,000
---
V
---
u
30,
Isophorone
3,74
10.000
---
U
---
U
31.
Nitrobenzene
2.85
10,000
---
U
---
U
32.
N-Nitroeodimethylamine
4.25
10,000
---
U
---
U
33.
N-Nitroeodiphenylamine
3,95
10,000
---
U
---
V
34.
N-NStroeodi-N-Propylamine
4,06
10,000
---
U
---
U
35,
Phenanthrens
3,24
10.000
---
U
---
U
36,
Pyrene
3,63
10.000
---
U
---
U
37.
4-Chloro-3-Methylphenol
3.79
20.D00
---
U
---
U
38,
2-Chlorophenol
2,75
10,000
W.
U
---
U
39.
0-Cresol
3,68
10,000
---
U
---
u
40,
P-Cresol
4.12
10,000
---
u
---
u
41.
2,4-Dichlorophenol
5.19
10,000
---
U
---
u
42,
2,6-Dichlorophenol
4.09
10,000
---
U
---
V
43,
2,4-Dimethylphenol
3.21
10,000
---
U
---
U
44,
4,6-Dinitro-2-Nethylphenol
4.77
50,000
---
U
---
U
45,
2,4-Dinitrophenol
4,37
50,000
---
U
---
U
46,
Ethyl Methaneeulfonate
5.26
20,000
---
U
---
U
47,
Methyl Methaneeulfonate
4.92
10.000
---
U
---
U
Page: 4
J Estimated value between the :4DL and MRL, U = Below ALL Quantlt atlon Limits.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 A
ANALYST:
JAP
DATE COLLECTED:
12/04/18
DATE EXTRACTED:
12/10/18
DATE REPORTED:
02/21/19
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
PARAMETERS, ug/1
Date
"L
Analyzed
MRL
la/18/1B
Mw-3D
12/18/18
MW 3A
48,
2-Nitrophenol
3,64
10,000
---
U
---
U
49,
4-Nitrophenol
3,17
50,000
---
U
---
u
50,
Pentachlorophenol
5,33
25.000
---
D
---
U
51,
Phenol
1.86
10.000
---
V
---
u
52,
2,3,4,6-Tetrachlorophanol
3,12
10,000
---
U
---
U
53,
2,4,5-Trichlorophenol
4.17
30.000
---
u
---
u
54.
2,4,6-Trichlorophenol
3,84
10.000
---
U
---
u
55,
Acetophenone
2,89
10,000
---
U
---
u
56.
2-Acetylaminofluorene
3,98
20,000
---
U
---
u
57,
4-Aminobiphanyl
4,12
20,000
---
U
---
U
50,
Benzyl Alcohol
4,47
20,000
---
U
---
U
59.
4-Chloroaniline
3,36
20,000
---
U
---
U
60,
Chlorobenzilate
5,12
10.000
---
U
---
U
61,
Diallate
2,98
10,000
---
U
---
U
62,
Dibenzofuran
4,28
10,000
---
U
---
u
63.
3,3-Dichlorobenzidine
4,22
20,000
---
U
---
u
64,
Dimethoats
3,98
20,000
---
V
---
U
65.
P-Dimethylaminoazobenzene
2,89
10,000
---
u
---
u
66,
7,12-Dimethylbenz[alanthracene
5,26
106000
---
U
---
U
67,
3,3-Dimethylbenzadine
3,21
10,000
---
V
---
U
68,
1,3-Dinitrobenzens
2,39
209000
---
V
---
V
69,
Diphanylamine
5.10
10,000
---
U
---
U
70,
Dieulioton
4,28
10,000
---
U
---
U
71,
Famphur
3.98
204000
---
U
---
U
72,
Hexachloropropens
4,31
10,000
---
U
---
U
73,
IaosaTrole
2.88
10,000
---
U
---
U
74,
Kepone
2,79
204000
---
U
---
U
75,
Metbapyrilene
3,54
100,000
---
U
---
U
76,
3-Methylchloroanthrens
4,21
100000
---
u
---
u
77,
2-Methylnaphthalene
3,79
10,000
---
u
---
U
78.
Methyl Parathion
4,32
10,000
---
U
---
u
79,
m-Cresol
3,81
10,000
---
U
---
u
80,
1,4-Naphthoquinone
4,00
10,000
---
U
---
u
81,
1-Naphthylamine
5061
10.000
---
u
---
V
82,
2-Naphthylamine
4.62
30.000
---
u
---
u
63,
2-Nitroaniline
3,61
50,000
---
u
---
u
84,
3-Nitroaniline
4,81
50,000
---
u
---
U
85.
4-Nitroaniline
4,22
20,000
---
U
---
U
86,
5-Nitro-O-Toluidine
4101
10,000
---
V
---
V
67,
N-Nitroeodi-n-butylamine
3,63
10,000
---
U
---
U
88.
N-Nitroeodiethylamine
3,83
20,000
---
u
---
U
89.
N-Nitrosomethylethylamine
3983
10.000
---
u
---
u
90,
N-Nitrosopiperidine
5.19
20,000
---
V
---
U
91,
N-Nitrosopyrrolidine
2,89
30.000
---
u
---
U
92,
Parathion
3,12
10,000
---
u
---
U
93,
Pentachlorobenzens
3,92
10,000
---
u
---
U
94,
Pentachloronitrobenzene
3,71
20,000
---
u
---
U
Page: 5
S = Setimated value between the MDL and MRL, U . Below ALL Quantltation Limits.

Environment 1, Incorporated
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DRa STE 100
DURHAM, NC 27703
REVIEWED BY:
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
CLIENT ID:
Wastewater ZUi 10
PHONE [phone]
FAX [phone]
6003 A
ANALYST:
JAP
DATE COLLECTED:
12/04/18
DATE EXTRACTED:
12/10/18
DATE REPORTED:
02/21/19
PARAMSTERS, ug/1
Date
MDL
Analysed
MRL
12/18/18
MW-3D
12/18/18
MW-3A
95,
PhenaOetin
4,41
20.000
---
V
---
U
96,
1,4 Benaenediamine
2.99
10,000
---
V
---
V
97,
Phorate
3,86
10.000
---
U
---
U
98,
Pronamlde
3.69
10,000
---
U
---
U
99,
Safrole
4,12
30.000
---
V
---
U
100,
1,2,4,5-Tetraehlorobenrene
5.01
10,000
---
V
---
U
101,
Thionaain
4,62
20.000
---
U
---
U
102,
0-Toluidins
4.11
10.000
---
U
---
U
103,
1,3,5-Trinitrobeneene
3,98
10,000
---
U
---
U
104,
0,0,0-Trlethyl Phosphorothl0ate
3,61
10,000
---
V
---
U
105.
HexaOhloroethane
1.49
10.00D
---
u
---
V
106.
Ieodrin
3,11
20,000
---
V
---
❑
Page: 6
T = Sstimetetl value between the MOL and MRL, U = BelON ALL Quantit atlon Llmite.

Environment 1, Incorporated
114 OAKMONT DRIVE
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CLIENT: JUDSON WHITERVRST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
407
LANDFILL APPENDIX II
RPA MRTHOD 8260B R2(96)
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 A
ANALYST:
JAP
DATE COLLECTED:
12/04/18
DATE ANALYZED:
12/13/18
DATE REPORTED:
02/21/19
Page: 1
PARANHTHRB, ug/l
MDL
MRL
MW-10
MW-1D
MW-2S
MW-1D
NN-38
1,
Chloromethane
0.77
3.000
---
U
---
V
---
U
---
U
-'"
U
2.
Vinyl Chloride
0,12
0.200
---
U
---
u
---
V
---
U
1.B2
3,
Bromomethane
0.67
10.000
---
U
---
U
---
U
---
V
---
U
9.
Chl oroathana
0.98
10.000
---
U
---
U
---
V
--•
U
---
V
5,
Trichlorofluoromethans
0,24
1.000
---
U
---
U
---
V
---
U
---
U
6.
1,1-Dichloroethene
0,17
5.000
---
U
---
U
---
U
---
U
---
U
7.
Acetone
9.06
1009000
---
U
---
U
---
U
---
U
9,44
J
8,
Iodomethans
0,26
10.000
---
U
---
U
---
U
---
U
---
U
9.
Carbon Disulfide
0.23
100,000
---
V
---
U
---
U
---
V
---
U
10,
Methylene Chloride
0,64
1.000
W.
V
---
U
---
U
---
U
---
U
11.
trans-1,2-Dichloroethene
0,23
5,000
---
U
---
u
---
U
M.
U
---
U
12,
1,1-Dichloroethens
0,20
5.000
---
U
---
U
---
U
---
U
---
U
13,
Vinyl Acetate
0,20
50.000
---
U
---
U
---
U
---
U
---
U
14,
Cie-1,2-Dichloroethene
0,25
5.000
---
U
---
V
---
U
---
U
---
u
15,
2-Butanone
1.21
100,000
---
U
---
V
---
U
---
U
---
U
16,
Bromochloromethane
0.27
3,000
---
U
---
V
---
U
---
U
---
U
17,
Chloroform
0.25
5.000
---
V
---
U
---
U
---
U
---
U
18,
1,1,1-Trichloroethane
0.19
1.000
---
D
---
U
---
U
---
U
---
U
19,
Carbon Tetrachloride
0.04
0,200
---
V
---
U
...
U
...
U
---
U
20,
Benzene
0,24
1.000
---
U
---
U
---
U
---
U
1,30
21.
1,2-Dichloroethans
0.02
0,200
---
U
---
U
---
U
---
V
0,24
22,
Trichlorcethene
0,23
1.000
---
U
---
U
---
U
---
U
---
U
23.
1,2-Dichlo ropropane
0.04
0.200
---
V
---
U
---
V
U
---
U
24.
Bromodlchloromethans
0,04
0.200
---
U
---
V
---
u
---
U
---
U
15.
Cie-1,3-Dichlc ropropene
0.06
0.200
---
U
'--
U
"'"
U
'--
V
---
U
16.
4-Methyl-2-Pent none
1.19
100.000
---
V
---
U
---
D
---
U
---
V
17,
Toluene
0.23
1.000
---
V
---
U
---
U
---
U
---
U
28,
trans-1,3-Dichloropropens
0,04
0,200
---
❑
--•
U
---
u
---
U
---
U
29.
1,1,2-Trichloroethane
0.03
0.200
---
U
---
U
---
U
---
U
---
U
30,
Tetrachloroethene
0.10
0.200
---
U
---
U
---
U
---
U
---
U
31.
2-Maxanone
1.57
50,000
---
U
---
U
---
V
---
U
---
U
32.
Dibromochloromethane
0,03
0.200
---
U
---
D
---
U
---
U
---
U
33,
1,2.Dibromoethane
0,03
0.200
...
U
---
U
---
U
---
U
---
U
34,
Chlorobenaene
0,30
3,000
---
U
---
U
---
U
---
U
---
U
35,
1,1,1,2-Tetsachloroethane
0.11
1.000
___
D
_._
V
___
U
___
U
___
Q
36,
Ethylbenrene
0.21
1.000
___
U
___
Q
___
U
___
Q
___
U
37.
Xyl anee
0.68
5.000
---
U
---
U
---
U
U
---
U
38,
Dibromomethans
0.28
10.000
---
V
---
U
---
U
---
U
---
U
39,
Styrene
0.19
1.000
---
V
---
U
---
U
---
U
---
V
40,
Bromoform
0,20
3.000
---
U
---
U
---
U
---
V
---
U
41.
1,1,2,2-Tetraohloroethane
0.03
0.200
---
U
...
U
---
U
---
U
---
U
42.
1,2,3-Trichloropropane
0.09
0.208
---
V
---
U
---
D
---
U
---
V
43,
1,4-DSchlorobenaene
0.39
1.000
---
V
---
U
---
U
U
U
44,
1,1-Dlahlorobanaene
0.32
5.000
__.
U
-__
U
___
V
_-.
U
___
U
45.
1,2-Dibromo-3-Chloropropans
0.07
0.200
---
V
---
U
---
u
---
U
---
U
46,
Acrylonitrile
2,72
200,000
---
u
---
U
---
U
---
U
---
U
47,
trans-1,4-Dichloro-2-Butene
0,42
100,000
---
U
---
U
---
U
---
V
---
U
48.
Acxolein
1.97
4.000
---
V
___
U
___
U
___
u
___
U
J Batlmated Value between the MDL and MRL, V Below ALL Ouantltation Limits.

Environment 1„
GREENVILLE, N.C. 27858
�t 71
wastewater IDi 10
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 A
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18
DURHAM, NC 27703 DATE ANALYZED: 12/13/18
DATE REPORTED: 02/21/19
REVIEWED BY:
407
LANDFILL APPENDIX II
EPA METHOD 8260B R2(96)
Page: 2
PARAMETERS, ug/l
MDL
HAD
Mw-l0
Mw-ln
Mw-26
Mw-2D
Mw-3H
49,
Allyl Chloride
0,20
10,000
---
U
---
U
---
U
---
V
---
U
50,
Chloroprene
oval
20,000
---
V
---
U
---
V
---
V
---
U
51,
1,3-Dichlorobenaene
0,41
5.000
---
U
---
U
---
V
---
U
---
U
52v
Dichlorodifluoromethans
0,51
50000
---
U
---
U
---
U
---
U
---
U
53,
1,3-Dichloropropane
0,28
1.000
---
V
---
D
---
U
---
U
---
U
54.
2,2-Dichloropropane
0,17
15,000
---
U
---
U
---
U
---
V
---
U
55,
1,1-D1ohloroHroPene
o.aa
5.000
---
V
---
U
---
V
---
V
---
U
56,
Rthyl Methacrylate
0.16
10,000
---
U
---
U
---
u
---
U
---
U
57,
Hexachlorobutadiene
0.30
0,200
---
V
---
V
---
U
---
U
---
U
58,
Isobutyl Alcohol
11080
100,000
---
U
---
U
---
U
---
U
---
U
59.
Methnc rylonitrile
1.93
100.000
___
❑
__-
U
--_
U
-__
V
___
V
60v
Methyl Methacrylate
0,25
30v000
---
U
---
U
---
U
---
U
---
V
61.
Naphthalene
0v47
64000
---
U
---
U
---
U
---
U
---
U
62,
Proplonitrile
3v26
1504000
---
U
---
U
---
U
---
U
---
U
63,
1,2,4-Triohlorobanrena
0.50
10.000
---
V
---
U
---
U
U
---
U
64.
Acetonitrile
36.29
55,000
---
V
---
U
---
V
---
U
---
U
65,
Tetrahydrofuran
0,39
1.000
---
V
42,70
4v85
---
U
35,30
66,
1,4-Dioxane
2,71
3.000
5,33
---
U
6.20
---
U
184,00
S = Estimated value between the MDL and MRL, U = Haloes ALL Quantit atlon Limits,

Environment 1, Incorporated
GREENVILLE, N.C. 27858
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 A
AMEC FOSTER WHEELER
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4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18
DURHAM, NC 27703 DATE ANALYZED: 12/13/18
DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260E R2(96)
PARAMETERS, ug/l
MDL
MEL
MW-3D
MW-3A
1,
Chloromethane
0,77
3,000
---
V
---
U
2,
Vinyl Chloride
0,12
0.200
---
U
1.09
3.
Bromomethane
0,67
10.000
---
U
---
U
4.
Chloroethane
0.48
10.000
---
U
---
V
5,
Trichlorofluoromethane
0.24
1.000
---
U
---
V
6,
1,1-Dichloroethene
0.17
5.000
---
V
---
D
7,
Acetone
9.06
100,000
---
U
---
U
8,
Lodomethane
0.26
10,000
---
U
---
D
9,
Carbon Disulfide
0,23
100,000
---
V
---
u
10.
Methylene Chloride
0,64
1.000
---
V
---
U
11.
trans-1,2-Dichloroethene
0,23
5.000
---
U
---
V
12.
1,1-Dichloroothans
0,20
5,000
---
U
---
U
13,
Vinyl Acetate
0.20
50.000
---
U
M.
U
14,
Cie-1,2-Dichloroethene
0,25
5,000
---
U
---
U
15,
2-Butanons
2.21
100,000
---
U
---
U
16,
Bromochloromethane
0,27
3,000
M.
V
---
U
17.
Chloroform
0,25
5.000
---
U
---
U
18.
1,1,1-Trlchloroethane
0.19
1.000
---
U
---
U
19,
Carbon Tetrachloride
0.04
0.200
---
U
---
V
20,
Benzene
0,24
1.000
---
u
1.69
21.
1,2-Dichloroethane
0,02
0,200
---
U
0.13
J
22.
Trichloroethene
0,23
1,000
---
U
---
U
23,
1,2-Dichloropropans
0,04
0.200
---
U
---
U
24.
Bromodichloromethane
0.04
0,200
---
U
---
U
25.
Cie-1,3-Dichloropropene
0.06
0,200
---
V
---
U
26.
4-Methyl-2-Pentanone
1.19
100,000
---
U
---
U
27.
Toluene
0,23
1.000
---
U
---
D
28.
trans-1,3-Dichloropropene
0.04
0,200
---
U
---
U
29,
1,1,2-Trichloroothane
0.03
0.200
---
U
---
V
30,
Tatrachloroethene
0.10
0.200
---
U
---
U
31,
2-Hexanone
1,57
50.000
---
U
---
V
32,
Dibromochloromethans
0,03
0.200
---
U
---
U
33,
1,2-Dibromoethane
0,03
0,200
---
U
---
U
34.
Chlorobanzene
0,30
3.000
---
U
---
U
35.
1,1,1,2-Tatrachloroethans
0,22
1.000
---
U
---
U
36.
Ethylbenzene
0,21
1.000
---
U
---
U
37.
Xylenes
0.60
5.000
---
U
---
u
38,
Dibromomethans
0,28
10.000
---
U
---
U
39,
Styrene
0.19
1.000
---
U
---
U
40,
Bromoform
0.20
3.000
---
U
---
V
41,
1,1,2,2-Tetrachloroothane
0.03
0,200
---
U
---
U
42,
1,2,3-Trlchloropropans
0.09
0.200
---
U
---
U
43.
1,4-Dichlosoben2ene
0.39
1.000
---
U
---
u
44,
1,2-Dichlorobenzens
0,32
5.000
---
45.
1,2-Dibromo-3-Chloropropane
0.07
0,200
---
U
---
II
46,
Acrylonitrile
2,72
200.000
---
U
---
U
47.
trans-1,4-Dichloro-2-Butene
0,42
100.000
---
U
---
u
48.
Acrolein
1,97
4.000
---
U
---
V
Page: 3
J Estimated value between the MDL and MRL, U Below ALL Uuantitetlon Limits,

Environment 1, Inco
114 OAKMONT DRIVE PHONE [phone]
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ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/04/18
DURHAM, NC 703 DATE ANALYZED: 12/13/18
DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260E R2(96)
PARAMETERS, ug/l
MDL
MRL
Mw-3D
MW-3A
49,
Allyl Chloride
0.20
100000
---
U
---
U
50,
Chloroprene
0.21
20,000
---
D
---
U
51,
1,3-Dichlorobenaene
0,41
5.000
---
U
---
U
52.
Dichlorodifluoromethane
0.51
5.000
---
U
---
U
53,
1,3-Dichloropropane
0,28
1.000
---
U
---
U
54,
2,2-Dichloropropane
0.17
15.000
---
U
---
U
55,
1,1-Dichloropropane
0,22
5.000
---
U
---
U
56,
Ethyl Methacrylate
0.16
10,000
---
U
---
U
57.
xexachlorobutadiene
0.30
0,200
---
U
---
U
58,
Ieobutyl Alcohol
12.80
100,000
---
U
---
U
59,
Methacrylonitrile
1.93
100,000
---
U
---
U
60.
Methyl Methacrylate
0,25
30,000
---
U
---
U
61,
Naphthalene
0,47
6.000
---
U
---
U
62,
Propionitrile
3,26
150,000
---
U
---
U
63,
1,2,4-Trichlorobenrene
0.50
10,000
---
U
---
U
64,
Acetonitrile
36,29
55,000
---
U
---
U
65.
Tatrahydrofuran
0,39
1.000
---
U
24,40
66.
1,4-Dioxane
2,71
3,000
---
U
87.00
Page: 4
S = Hetlmated value between the MDL and MRL, U Helow ALL Quantitation Limits.

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Environment 1, Incorporated
waatawater Ins 30
114 OAKMONT DRIVE
PHONE
(252)
756.6208
GREENVILLE, N.C. 27858
FAX
(252)
756-0633
ID#: 6003 H
J[7D SON WHITEHURST (C&D
LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT &
INFRASTRUCTURE
DATE COLLECTED:
12/12/18
4021 STIRRUP CREEK DR.
STE 100
DATE REPORTED
02/21/19
DURHAM ,NC 27703
REVIEWED
BY:
MW-9A
MW-10
MW-11
NW-13
MW-12e
Analysis
Method
PARAMETERS
MDL
MAL
Date Analyst
Code
PH (field measurement), Units
6.9
6.5
6.8
6.0
6.6
12/12/18
RP
4500HO-11
HOD, m9/1
2.0
2.0
--- U
6.2
--- U
--- U
6.6
12/12/10
HUM
5210E-11
COD, mg/1
0.840
2010
--- U
259
54
45
317
12/14/18
SSJ
H8000-79
Nitrate Nitrogen as N, mg/1
0.009
0.04
--- U
--- U
--- U
0.25
--- U
12/13/18
BLD
353.2 R2-9
Total Organic Carbon, mg/l
0.129
1.0
4,70
99.20
20,92
20.52
114
12/17/16
SHJ
531OC-11
Alkalinity (to pH 4.5), mg CaCO3/1
1.0
1.0
244
1320
550
292
630
12/17/19
JTH
2320D-11
Chloride, mg/1
5.0
5.0
9
52
14
--- U
117
12/17/18
RDS
4500CLB-11
Cyanide, ug/1
5.0
5.0
--- U
--- U
--- U
--- U
--- U
12/18/18
SEJ
4500CHE-11
Total Hardness, mg/1
278
1030
498
306
451
12/17/18
JMS
234OC-11
Total Dissolved Residue, mg/1
1.0
10
373
1670
691
379
1290
12/13/10
KDS
254OC-11
sulfate, mg/l
54
5.0
63.7
211
146
10.1
6.1
12/24/18
SEJ
4500SO42B1
Antimony, ug/1
0,03
1.0
0.10 J
--- U
0.06 J
0,13 J
0,17 J
01/02/19
AKS
EPA200.8
Arsenic, ug/l
0.03
5.0
0.03 J
9
3.2J
ill
22
01/02/19
AKs
EPA200.8
Barium, ug/l
0,03
10.0
48.8
368
55.0
47.5
398
01/02/19
AKS
EPA200.8
Beryllium, ug/l
0.05
1.0
--- U
0.05 J
--- U
--- V
--- U
01/02/19
AKS
HPA200.8
Cadmium, ug/l
0t02
1.0
0.02 J
0.14 J
0.10 J
0.06 J
--- U
01/02/19
AKS
EPA200.8
Cobalt, ug/l
0.03
1.0
0.12 J
1.8
1.0
0,54 J
1.6
01/04/19
AKS
BPA200.8
Total Chromium, ug/1
0.15
5.0
--- U
14
0.56 J
0,31 J
24
01/04/19
AKS
BPA200.8
Copper, ug/1
0,03
10.0
0.38J
0,96 J
0.30 J
0.38 J
1.1J
01/04/19
AKS
EPA200.8
Iron, ug/1
12.08
Soto
557
363
13560
917
2075
01/10/19
AKS
311ID-11
Manganese, ug/l
0.31
30.0
74
253
284
22
460
12/20/18
LPJ
EPA200.7
Lead, ug/l
0t03
5.0
--- U
01/02/19
AKS
EPA200.8.
Lead, ug/1
0tD3
5.0
0.03 J
0,04 J
0.16 J
--- U
01/04/19
AKS
EPA200.8
Mercury, ug/1
0.05
0920
0.051
--- U
--- U
--- U
--- U
12/17/18
MTM
245.1 R3-9
Nickel, ug/1
0.03
10.0
291J
12.1
5.7 J
3,9a
6,6J
01/04/19
AKS
VPA20018
Selenium, ug/l
0.15
10.0
--- U
7,9 J
1.1J
0.B5 J
8.SJ
01/02/19
AKS
OPA20018
silver, ug/1
0.05
5.0
--- U
01/02/19
AKS
9PA2D0.8
Silver, ug/l
0.05
5.0
--- U
--- U
--- U
--- V
01/04/19
AKS
EPA200.8
Thallium, ug/l
D.05
1.0
--- U
--- U
--- U
--- U
--- U
01/04/19
ASS
EPA200.0
Tin, ug/1
0.05
100.0
--- U
--- U
--- U
--- U
--- U
01/04/19
AKS
EPA200.8
Vanadium, ug/1
0,03
190
--- U
8.1
1.5
1.3
17.5
01/04/19
AKS
EPA200.8
Zinc, ug/l
0.11
10.0
3.3J
01/02/19
ASS
EPA200.8
Zinc, ug/l
0.11
1000
1,5J
1,3J
0.91 J
1.2 J
01/04/19
AKS
HPA200.8
Sulfide, ug/1
100
1000
--- U
328 J
--- U
--- U
115 J
12/19/16
LFJ
450092D-11
Conductivity (at 25c), uMhoe/cm
1.0
1.0
529
1607
857
558
941
12/12/18
BF
2510E-11
Dissolved Oxygen, mg/1
0.1
0.1
0,34
0,28
0,21
0t30
0,33
12/12/18
BP
450000-11
°C
13
11
11
16
13
12/12/18
BF
2550E-10
Temperature,
Iron, Ferrous, ug/1
50.00
200.0
464
302
13070
802
1952
12/13/19
SEJ
3500FEB-11
Static Water Level, feet
4,82
2,89
2,80
7.57
4.15
12/12/18
BF
23.17
22,73
23.B4
22,68
22.93
12/12/16
PJC
Well Depth, feet
Carbon Dioxide, mg/l
1.0
1.0
42
444
180
122
318
12/12/16
HMM
45000O2C-1
+99
+108
+64
+72
+105
12/12/18
BF
2580E
OAP, my
T • Estimated Velue between the MOL and MRL, U = Below ALL Quantlt etion Limlte.

Environment 1, Incorporated
GREENVILLE, N.C. 27858
JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM ,NC 27703
PAAAMBTBRS
Turbidity (Field), NTU
MW-9A
MDL MRL
1.0 1.0 8,62
756-0633
ID#: 6003 B
DATE COLLECTED: 12/12/18
DATE REPORTED : 02/21/19
REVIEWED BY:
MW-10 MW-11 MW-13 MW-12s Analysis Method
Date Analyst Code
2,29 18.6 2.33 --- U 12/12/18 BF 2130E-11
S = Hetimated value between the MOL and MRL, U Helow ALL QuanCltatlon LSmSte.

Environment 1, I
n_ n
114 OAKMONT DRIVE PHONE [phone]
GREENVILLE, N.C. 27858 FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 H
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: BIC
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/12/18
DURHAM, NC 7703 DATE EXTRACTED: 12/14/18
005 DATE ANALYZED: 12/26/18
REVIEWED BY: DATE REPORTED: 02/21/19
PESTICIDES AND PCB'.S
EPA METHOD 8081E R2(07)
PARAMRTHRS, ug/1
MDL
ML
M-9A
MW-10
MW-11
Mw-13
Mw-lee
1,
Aldrin
0,029
0.050
---
U
---
U
---
U
---
U
---
U
a.
Alpha-HHC
0.032
0.050
---
U
---
U
---
U
U
---
U
3,
Beta-BHC
0.031
0.050
---
U
---
U
---
U
---
U
---
U
9,
Daltq-BHC
0.030
0.050
---
U
___
U
___
U
___
V
___
U
5.
Gamma-BHC (Lindens)
0.032
0.050
---
U
---
U
---
U
---
U
---
U
6,
Chlordane
0.320
0.500
---
U
---
U
---
U
---
U
---
U
7,
404-DDD
0.051
0.100
---
U
---
U
---
U
---
V
---
U
S.
414-DDS
0.049
0.100
---
U
---
U
---
U
---
U
---
U
9.
4t4-DDT
0,052
0.300
---
U
---
U
---
U
---
V
---
U
30,
Dleldrin
0.042
0.075
---
V
---
U
---
U
---
U
---
U
11,
Hndoeulean I
0.056
04100
---
U
---
U
---
U
---
U
---
U
la.
Hndoaulean II
0.046
0.100
---
U
---
U
---
U
---
U
---
U
13,
Hndosulfan Sulfate
0.072
0.100
---
U
---
U
---
U
---
U
---
U
14,
Endrin
0.053
0.100
---
V
---
U
---
U
---
U
---
U
15,
Endrin Aldehyde
0.068
0.100
•--
U
---
U
---
U
---
U
---
U
16,
Heptachlor
0.039
0.050
---
U
---
U
---
U
---
U
---
U
17,
Heptachlor Epoxide
0.042
0.075
---
U
---
U
___
U
___
U
---
U
18,
Methoxyohlor
0.530
1.000
---
V
---
U
---
U
---
U
---
U
19,
Pebte (Aroclore)
0.500
2,000
---
U
---
U
---
v
---
U
---
U
20,
Toxaphene
0.690
1.500
---
U
---
U
---
U
---
U
---
U
J = Betimated value between Che MDL and MRLU Belau, ALL Uuantitatlon Limlta.

Environment 1, I
rated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 B
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: HIC
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/12/18
DURHAM, NC 27703 DATE EXTRACTED: 12/18/18
Zzi DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX 22
EPA METHOD 8151A R1(96)
Date Analyzed
12/20/19
12/20/18
12/21/18
12/21/18
12/21/18
MW-9A
MW-30
MW-11
MW-13
MW-12e
PARAMETERS, ug/l MDL MRL
1. 2,4-D
0.36
2.000
--- U
--- U
--- U
U
--- U
2. Dinoeeb
0,54
1.000
--- U
--- U
--- U
--- U
--- U
3. 2,4,5-TP
0,42
2.000
--- U
--- U
--- U
--- U
--- U
4, 2,415-T
0.47
2,000
--- U
--- U
--- U
--- U
--- U
J = EetSmated value between the MDL and MRL, U = Below ALL Quantitatlort LSmite.

Environment 1, Incor
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
Drinking Water ID715
Wastewater IDt 10
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 B
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/12/18
DURHAM, NC 27703 DATE EXTRACTED: 12/17/18
DATE ANALYZED: 12/19/18
REVIEWED BY: DATE REPORTED: 02/21/19
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
Page: 1
PARAMETERS, ug/1
MDL
MAL
MW-9A
MW-10
NW-11
NW-13
MW-12e
1,
Acenaphthene
2.66
30.000
---
U
---
V
---
U
---
U
---
U
2.
Acenaphthylene
2.60
10,000
---
U
---
U
---
U
---
U
---
V
3,
Anthracene
2,97
10,000
---
V
---
U
---
U
---
U
---
V
4,
Benzo[alantrhacens
4,16
10,000
---
U
---
U
---
U
---
U
---
U
5,
Benzo[blfluoranthene
3,32
10,000
---
V
---
U
---
U
---
U
---
U
6.
eenzo[k)fluoranthene
4,23
10.000
---
U
---
U
---
U
---
U
---
U
7.
Benzo[g,h,ilperylene
2.61
10,000
---
U
3.16
J
---
U
---
U
---
U
8.
Benzo[al8yrane
3.27
10,000
---
U
---
U
---
U
---
U
---
U
9,
4-Bromophenyl Phenyl Ether
2,63
10.000
---
U
---
U
---
U
---
U
---
V
10,
Butyl Benzyl Phthalate
5,78
10.000
---
V
---
V
---
U
---
V
---
U
11,
eis(2-Chloroethoxy) Methane
3,14
10,000
---
V
---
U
---
U
---
U
---
U
12,
Ble(2-Chloroethyl) Ether
2,58
10.000
---
U
---
U
---
V
---
U
---
V
13.
Bis(2-Chloro-l-methylethyl) Ether
2.5E
10.000
---
V
---
U
---
U
---
V
---
U
14,
2-Chloronaphthalene
2,17
10.000
---
V
---
U
---
U
---
U
---
V
15.
4-Chlorophenyl Phenyl Ether
2,42
10.000
---
U
---
U
---
U
---
U
---
U
16,
Chryeene
4,04
10,000
---
V
---
V
---
U
---
U
---
U
17,
Dibenzo[a,hlanthracene
2,78
30.000
---
V
---
U
---
U
---
U
---
U
18.
Di-N-Butyl Phthalate
3,09
10,000
---
U
---
U
---
U
---
U
---
U
19.
Dimethyl Phthalate
3.7E
10,000
---
U
---
U
---
U
---
U
---
U
20.
Diethyl Phthalate
3.92
10.000
---
U
---
U
'""
U
-"-
U
---
U
21.
2,4-Dinit rotoluena
3.95
10.000
---
U
---
U
---
U
U
---
U
22.
2,6-DSnitrotoluene
3.88
10400
---
V
---
U
---
U
---
U
---
23.
Di-N-Octyl Phthalate
2,81
10.000
---
U
---
V
---
U
---
U
---
U
24,
Bio-(2-Ethylhexyl) Phthalate
9.97
15.000
---
V
---
V
---
U
---
U
---
U
25,
Fluoranthene
3.92
10.000
---
U
---
U
---
U
---
U
---
U
26.
Fluorene
2.95
30.000
---
U
---
U
---
V
--
U
v
27.
Hexachlorobenzene
2.61
10,000
---
U
---
U
---
U
---
U
---
U
28.
Hexachlorocyclopentadiens
4,16
10,000
---
U
---
U
---
U
---
U
---
U
29,
Indeno[1,2,3-Cd]pyrene
2,91
10.000
---
U
3.06
J
---
U
---
U
---
U
30,
Ieophorone
3,74
10.000
---
V
---
U
---
U
---
U
---
U
31,
Nitrobenzene
2.85
10,000
---
U
---
U
M.
U
---
U
---
U
32.
N-Nltroeodimethylemine
4.75
30.000
---
V
---
V
___
U
_"_
U
_-"
U
33.
N-Nitroeodiphanyl amine
3.95
30.000
---
V
---
V
---
U
U
U
34,
N-Nitrosodi-N-ProBylamine
4.06
10,000
---
U
---
U
---
U
---
U
---
U
35,
Phenanthrene
3,24
10,000
---
U
---
U
---
U
---
U
---
U
36,
Pyrene
3,63
10,000
---
U
---
U
---
U
---
U
---
U
37.
4-Chloro-3-Methylphenol
3,79
20,000
---
U
---
U
---
V
---
U
---
U
38.
2-Chlorophenol
2.75
30.000
---
U
---
V
""_
U
"__
U
"_'
U
39,
0-Cresol
3,68
10,000
---
U
---
U
---
U
---
U
---
V
40.
P-Cresol
4,12
10,000
---
U
---
V
---
U
---
U
---
U
41,
2,4-Dichlorophanol
5.19
10,000
---
U
---
U
---
U
---
42,
2,6-Dichloro8henol
4.89
10.000
---
U
---
U
---
U
---
U
---
V
43.
2,4-Dlmethylphanol
3.21
100000
---
U
---
U
---
U
u
---
u
44.
4,6-Dinitro-2-Methylphenol
4.77
50,000
---
U
---
U
---
V
---
V
---
U
45.
2,4-Dinitrophenol
4,37
50.000
---
U
---
U
---
U
---
V
---
U
96.
Ethyl Mathaneaulfonate
5.26
20.000
---
V
---
U
---
U
---
D
---
U
47,
Methyl Methaneeulfonate
4,92
10.000
---
U
---
U
---
U
---
U
---
U
48.
2-NStroBhenol
3.64
10.000
---
U
---
U
---
U
---
U
---
v
J Estimated value between the MDL and MRL, U = Below ALL Quantit atlon LSm1tB.

Environment 1, Inco
a�@0
114 OANVI NT DRIVE
GREENVILLE, N.C. 27858
FAX [phone]&0633
CLIENT: JUDSON WHITEHVRST (C&D LANDFILL)
CLIENT ID:
6003 B
AMEC FOSTER
WHEELER
ENVIRONMENT
& INFRASTRUCTURE
ANALYST:
JAP
4021 STIRRUP
CREEK DR. STE 100
DATE COLLECTED:
12/12/18 Page: 2
DURHAM, NC
27703
DATE EXTRACTED:
12/17/18
DATE ANALYZED:
12/19/18
REVIEWED BY:
DATE REPORTED:
02/21/19
SEMI -VOLATILE
ORGANICS
EPA METHOD 8270D R4(07)
PARAMETERS, ug/l
MDL
MRL
Mw-9A
NW-10
Mw-11
MW-13
NW-32a
49,
4-Nitrophenol
3.17
50.000
---
U
---
U
---
U
---
U
---
U
50,
Pentachlorophenol
5,33
25,000
---
U
---
V
---
U
---
V
---
u
51,
Phenol
1486
10,000
---
U
---
V
---
U
---
V
---
U
52.
2,3,4,6-Tetrachlorophenol
3.12
10.000
---
V
---
U
---
U
---
U
---
U
53,
2,9, 5-Trlohlorophenol
4.17
10.000
---
U
---
U
---
U
---
U
---
U
54,
2,9,6-Trlohlorophenol
3.89
30.000
---
U
---
U
---
V
---
U
---
U
55.
Acetophanone
2.89
10.000
---
U
---
V
---
U
---
U
---
U
56,
2-Acetylamino£luorene
3,99
20,000
---
U
---
U
---
U
---
U
---
u
57,
4-Aminobiphenyl
4,12
20,000
---
V
---
V
---
U
---
U
---
U
58,
Banzyl Aloohol
4.47
20,000
---
U
---
u
---
U
---
U
---
U
59,
4-Chlaroanlline
3.36
20.000
---
U
---
IF
---
U
---
U
---
U
60,
Chlorobenzilate
5,12
10,000
---
U
---
U
---
U
---
U
---
U
61,
Dlellate
2.98
10.000
---
U
---
U
---
U
V
___
U
62,
Dibenaofuran
4,28
10400
---
U
---
U
---
V
---
U
---
U
63,
3,3-Dichlorobenzidine
4.22
20,000
---
V
---
U
---
V
---
U
---
U
64.
Dimethoate
3.98
20.000
---
U
---
U
---
U
---
U
---
U
65.
P-Dimethyl amino eaobensene
2,89
30.000
---
U
---
V
---
U
---
U
---
U
66,
7,12-Dimethylbenz[alanthrocene
5,26
10,000
---
U
---
V
---
U
---
U
---
U
67.
3,3-Dimethylbenz afline
3.21
10.000
---
V
---
U
---
U
---
U
---
U
68,
1,3-Dinitrobenzene
2.89
20,000
---
U
---
U
---
U
---
U
---
u
69.
Diphanyl amine
5.30
10.000
---
V
___
u
___
U
___
U
___
U
70,
Diaul£oton
4,28
10.000
---
U
---
V
---
u
---
U
---
U
71,
ramphur
3,98
20.000
---
V
---
U
---
u
---
U
---
U
72,
Nexaohloropropana
4.31
30.000
---
U
---
V
---
U
U
U
73,
Ieoe of role
2,88
10.000
---
U
---
U
---
V
---
U
---
U
79,
Nepone
2.78
20400
M.
U
---
V
---
U
---
U
---
U
75,
McChapYrilene
3,54
100.000
---
U
---
V
---
U
---
U
---
U
76.
3-Methylchloro anthrane
9.21
30.000
---
V
---
V
---
U
---
U
---
U
77,
2-Methylnaphthalens
3,79
10, 000
---
U
---
U
---
U
---
V
---
V
78,
Mothyl Parathion
4,32
10,000
---
V
---
U
---
U
---
V
---
V
79.
m-Cresol
3,81
30.000
---
U
---
U
---
U
---
U
---
V
80.
1,9-Nephthoquinone
9.00
10.000
---
U
---
U
---
U
---
U
---
U
81.
1-Naphthylamine
5061
30.000
---
U
---
U
---
U
---
U
---
U
82,
2-Haphthylamine
4.62
100000
---
V
---
U
---
U
---
V
---
U
83,
2-Nitroanlllna
3.61
50.000
---
V
---
U
---
V
--
U
---
U
84.
3-Nitro aniline
4.81
50.000
---
U
---
U
---
V
U
---
V
85,
4-Nitroaniline
4,22
20,000
---
V
---
U
---
V
---
U
---
U
86,
5-Nitro-O-Toluidlne
4,01
10,000
---
U
---
U
---
U
---
U
---
U
87,
N-Nitrosodl-n-butylamine
3,63
10,000
---
V
---
U
---
U
---
U
---
U
88.
N-NS troeodiethylamine
3.83
20.000
---
V
---
U
---
U
---
U
---
U
89,
N-Nitroeomethylethylamine
3.83
10.000
---
V
---
V
---
D
---
D
---
U
90.
N-Nltroeopiperidine
5.19
20400
---
U
---
U
---
U
U
---
U
91,
N-NSCroeoHyrzolldine
2.89
30.000
---
U
---
U
---
u
---
U
---
U
92,
Parathion
3.12
10.000
---
U
---
V
---
u
---
U
---
V
93,
Pentachlorobenzone
3,92
10,000
---
U
---
U
---
U
---
V
---
V
94,
Pentachloronitrobenzene
3.71
20,000
---
V
---
U
---
U
---
U
---
U
95,
Phenacetin
4,41
20,000
---
U
---
U
---
V
---
U
---
V
96.
1.4 Benzenediamine
2,99
10.000
---
V
---
U
---
U
---
U
---
V
J = Estimated value between the MDL and MRL, U = Below ALL Quantitation Limits,

Environment 1,
l l4 OAKMONT DRIVE
GREENVILLE, N.C. 27858
rued
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
ORGANICS
EPA METHOD 8270D R4(07)
SEMI -VOLATILE
CLIENT ID:
PHONE [phone]
PAX [phone]
6003 8
ANALYST:
JAP
DATE
COLLECTED:
12/12/18
DATE
EXTRACTED:
12/17/18
DATE
ANALYZED:
12/19/18
DATE
REPORTEDi
02/21/19
Page: 3
PARAMETERS, ug/1
MDL
MRL
MW-9A
MW-10
MW-11
MW-13
MW-12e
97,
Phorate
3.56
10,000
---
V
---
u
---
D
---
U
---
U
98,
Pronamide
3169
10.000
---
U
---
u
---
U
---
U
---
u
99,
Safrole
4.12
10,000
---
U
---
U
---
V
---
U
---
U
100.
1,2,4,5-Tetraphlorobenzene
5.01
10,000
---
U
---
U
---
U
---
V
---
U
301,
Thlonazin
9.62
20.000
---
V
---
U
---
u
"'-
V
---
V
102.
O-Toluldine
4.11
10,000
---
U
---
U
___
u
"_
0
-"'
V
103,
1,3,5-Trinitrobenzene
3,90
10,000
---
U
---
U
---
U
---
U
---
u
104,
0,0,0-Triethyl Phoephorothioate
3,61
10,000
---
U
---
V
---
D
---
U
---
U
105,
Raxaahloroethane
1.99
30.000
---
U
---
V
___
❑
___
u
___
D
306,
Ieodrin
3.11
20.000
---
U
---
U
---
U
--
V
V
J Eetimflted value between the MDL and MRL, U Below ALL Vuantit atlon Limits.

Enwhimum alp ��c�oQpor�a�c�d
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260B R2(96)
Drinking Water ID: 37715
Wastewater ID: 10
PHONE [phone]
FAX [phone]
CLIENT ID:
ANALYST: JAP
DATE COLLECTED: 12/12/18 Page: 1
DATE REPORTED: 02/21/19
PARAMETERS, ug/l
Date
MDL
Analyzed
MRL
12/18/18
MW-9A
12/18/18
MW-10
12/18/10
NW-11
12/19/18
MW-13
12/19/18
NW-120
1,
Chloromethane
0,77
3.000
---
U
---
U
---
u
---
U
---
U
2,
Vinyl Chloride
0,12
0,200
---
U
2,20
---
U
---
U
2,21
3.
eromomethane
0.67
10.000
---
U
---
U
---
U
---
U
---
U
4,
Chloroethane
0,48
10.000
---
u
---
U
---
U
---
U
---
u
5.
Tzlchlorofluoromethane
0.14
1.000
---
U
---
U
---
U
U
V
6.
1,1-DSchloroathane
0.17
5.000
---
U
---
U
---
V
---
U
---
U
7,
Acetone
9.06
100,000
---
U
---
u
---
U
---
U
11.80
J
8,
Iodomethane
0,26
10,000
---
U
---
u
---
V
---
U
---
U
3.
Carbon Dieulflde
0.23
100,000
---
U
---
U
---
U
---
U
---
U
10.
Methylene Chloride
0,64
1.000
---
u
---
U
---
U
---
U
---
U
11,
trana-1,2-Dichlaroethene
0,23
5.000
---
U
---
U
---
U
---
U
---
U
12.
1,1-Diahloroethane
0,20
5.000
---
U
---
U
---
u
---
U
---
U
13,
Vinyl Acetate
0,20
50.000
---
V
---
V
---
U
---
u
---
U
14,
Cie-1,2-Dichloroethene
0.15
5.000
---
U
0,31
J
---
U
---
U
0.34
J
15,
2-Hutanone
2,21
100,000
---
V
---
U
---
U
---
U
---
U
16,
Eromoahloromethane
0,27
3,000
---
U
---
U
---
U
---
U
---
u
17,
Chloroform
0,25
SA00
---
u
---
U
---
U
---
V
---
U
19,
1,1,1-Trichloroethane
0.19
1.00D
---
U
---
U
---
V
---
U
---
U
19,
Carbon Tetrachloride
0.04
0,200
---
U
---
u
---
u
---
U
---
U
20.
Benzene
0,24
1.000
---
U
1,57
D.48
J
---
U
1.48
21.
1,2-Dichloroethane
0.02
0,200
M.
U
0,34
0.08
J
---
U
0.13
J
21,
Trichloroethane
0.23
1.000
---
U
---
U
M.
U
--'
U
---
U
23.
1,2-Dichloropropane
0,04
0,200
---
U
D.23
0.04
J
---
U
0.07
J
29,
Hromodlchloromethane
0.04
0.200
---
V
---
II
---
V
U
U
25.
Cie-1,3-Dichloropropene
0.06
0.200
---
U
---
U
---
U
---
U
---
U
26.
4-Methyl-2-Pentanone
1.19
300.000
---
u
---
V
---
U
---
U
---
U
27,
Toluene
0.23
1.000
---
U
---
U
___
❑
___
U
0,24
J
28.
trans-1,3-Dichloropropene
0,04
0,200
---
U
---
u
---
D
---
U
---
V
29.
1,1,2-Trichloroethane
0.03
0.200
---
II
---
V
___
ll
___
U
___
u
30,
Tetrachloroethene
0.10
0,200
---
U
---
U
---
D
---
U
---
u
31.
2-Mexanons
1,57
50.000
---
U
---
U
---
U
---
U
---
u
32,
Dibromochloromethane
0.03
0.200
---
U
---
V
---
U
---
U
---
U
33,
1,2-Dibromoathane
0403
0.200
---
U
---
U
---
V
---
U
---
U
34.
Chlorobenzene
0,30
3.000
---
U
---
U
---
U
---
U
---
U
35,
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
---
V
---
U
---
U
---
U
36,
Ethylbenzene
0,21
1.000
---
U
0.44
J
---
U
---
U
0,23
J
37,
Xylenes
0.68
5.000
---
V
---
U
---
V
---
V
---
u
38.
Dlbromomethane
0.28
30.000
---
V
---
U
---
U
---
U
---
U
39,
Styrene
0.19
1.000
M.
V
---
U
---
u
---
u
---
U
40.
eromofOzm
0.20
3,000
---
U
---
U
---
U
---
V
---
U
41,
1,1,2,2-Tatraahloroethane
0.03
0.100
---
U
---
U
---
U
---
u
---
V
42.
1,2,3-Trlchloropropane
0.09
0,200
---
U
---
u
---
U
---
V
---
U
43.
1,4-Dichlorobenzene
0,39
1.000
---
u
---
U
---
U
---
U
---
u
44,
1,2-Dichlorobenzene
0,32
5.000
---
u
---
U
---
U
---
U
---
u
45.
1,2-Dlbromo-3-Chloropropana
0.07
0.200
---
U
---
U
---
u
---
U
---
U
46.
Acrylonitrlle
2,72
200,000
---
V
---
U
---
U
---
U
---
U
47.
Crane-1,4-Dlohloro-2-eutene
0,42
100,000
---
u
---
V
---
V
---
U
---
U
J 80tlmated value between the MDL and MRL, V = Below ALL Duantitation Llmite.

(Environment 1, Inco
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 B
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: SAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/12/18 Page: 2
DURHAM, NC 27703 DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260E R2(96)
PARAMETERS, n9/1
Date
MDL
Analyzaa
MAL
12/18/18
MW-9A
12/18/18
MW-10
12/10/18
NW-11
12/19/18
NW-13
la/39/le
MN -lee
48,
Acrolein
1,97
4.000
---
D
---
U
---
U
---
U
---
V
49.
Allyl Chloride
0,20
10.000
---
U
---
D
---
V
---
V
---
V
50,
Chloroprene
0,21
20,000
---
U
---
V
---
V
---
U
---
V
51,
1,3-Dichlorobenzene
0,41
5.000
---
U
---
V
---
V
---
U
---
U
52,
Dichlorodi Cluoromethane
0.51
5.000
---
V
---
V
---
U
---
U
---
U
53,
1,3-Dichloropropane
0,28
1.000
---
V
---
U
---
U
U
U
54,
2,2-Dichloropropane
0,17
15,000
---
U
---
U
---
D
---
U
---
V
55,
1,1-Dichloropropane
0.22
5.000
---
V
---
U
---
V
---
U
---
U
56,
Ethyl Methacrylate
0.16
10.000
---
U
---
D
---
V
---
U
---
U
57.
Hexaohlorobutadiene
0.10
0.200
---
U
---
U
---
V
---
V
---
U
58.
Seobutyl Alcohol
12.80
100.000
---
V
---
U
---
D
---
U
---
V
59.
Methacrylonitrile
1,93
1009000
---
V
---
U
---
V
---
U
---
V
60,
Methyl Methacrylate
0,25
30.000
---
V
---
V
---
U
---
U
---
V
61,
Naphthalene
0,47
6.000
---
D
---
D
---
V
---
U
1.08
0
62,
Prop Sonitrile
3.26
150,000
---
U
---
U
---
U
---
U
---
U
63.
1,2,4-Trichlorobenzene
0.50
10,000
---
V
---
V
---
U
---
U
---
U
64.
Acetonitrile
36,29
55.000
---
V
---
V
---
U
---
U
---
V
65,
Tetrahydrofuran
0,39
1.000
---
V
25,42
8,02
---
U
38,75
66,
1,4-Dioxane
2.71
3,000
---
V
5.40
8.15
---
U
8,82
T = Estimated value between the MDL find MRL, U = Below ALL Quantitation Limlte.

0
0
3
0
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TOTAL CHLORINE, mg/
U L L � Vim'
m
OR ug/1 AT COLLECTION
1.1
m
M
q n
y
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TEMPERATURE,°C
0
0
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ro
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BOD
ro
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ro
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Nitrate
n
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Hardness
n
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TDS
Sulfate
ro
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Metals
ro
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Conductivity
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ro
PARAMETERS/TESTS
Ly lu°
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m
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TOTAL CHLORINE, mg/1
C7
OR ug/l AT COLLECTION
ti
m
m
m
z q
0
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TEMPERATURE,OC
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Field Parameter
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Dup. 4
Cif
Gi
8260
EPA 8270D
m
m
m
s
8270D Dup. 1
EPA8081B
" '3
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8081B Duplicate
m
%,
8260B A II
—
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8151A Landfill
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N
CO2
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ro
go
ro
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PARAMETERS/TESTS
v
O
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D
m
=
m
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m
w
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m
m
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m
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Elowkgmmn� alp
Nor
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
�ooupon gd
ID#: 6003 C
Drinking Water I.Di 377.1
Wastewater IDI 30
PHONE [phone]
FAX [phone]
JUDSON
WHITEHURST (C&D
LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
DATE COLLECTED:
12/05/18
4021 STIRRUP CREEK DR,
STE 100
DATE REPORTED
02/21/19
DURHAM
,NC 27703
REVIEWED
BY:
SW-1
SW-2
SW-3
SW-4
Analysis
Method
PARAMBTBRS
NDL
MRL
Date Analyst
Code
PH (field measurement),
Unite
6.6
6.8
6.6
6.4
12/05/18
PJC
4500HB-11
Antimony, ug/l
0,03
110
0.17 J
12/11/18
ARS
BPA200.8
Antimony, ug/l
0,03
110
0,04 J
0,05 J
0,04 J
01/02/19
AKS
SPA200.8
Arsenio, ug/l
0.03
5,0
1.61
12/11/18
AKS
BPA200.8
Arsenio, ug/l
0,03
5.0
0168 J
0,44 J
0.16 J
01/02/19
AKS
EPA20018
Barium, ug/1
0,03
10.0
109
12/11/18
AKS
BPA200.8
Barium, ug/l
0,03
10.0
53,8
77.5
74,1
01/02/19
AKS
BPA200,8
Beryllium, ug/l
0,05
1.0
0,32 J
12/11/18
ARS
BPA200.8
Beryllium, ug/l
0.05
1.0
--- U
0.05 J
0,11 J
01/02/19
AR8
BPA200.8
Cadmium, ug/1
042
1.0
D415J
12/11/18
AR8
BPA200.8
Cadmium, ug/1
0,02
1.0
--- U
0,02 J
0,04 J
01/02/19
AKS
EPA200.6
Cobalt, ug/1
0,03
1.0
0,79J
12/11/18
AKS
BPA200.8
Cobalt, ug/1
0,03
1.0
0.19 J
0,32 J
0,62 J
01/04/19
AKS
BPA200,8
Total Chromium, ug/1
0.15
5,0
6.1
12/11/19
AKS
BPA200,8
Total Chromium, ug/1
0415
540
0,53 J
0437 J
0.6D J
01/04/19
AKS
BPA20D.8
Copper, ug/1
0,03
10:0
3.1J
12/11/18
AKS
BPA200.8
Copper, ug/1
0,03
1000
0,26 J
0,46 J
0,43 J
D1/04/19
AKS
BPA200.8
Lead, ug/1
0,03
5.0
946
12/11/18
AKS
BPA200.B
Lead, ug/1
0,03
5.0
0,21 J
0,32 J
01/02/19
AKS
EPA200.8
Lead, ug/1
0.03
5.0
0,38 J
01/04/19
AKS
SPA200.8
Nickel, ug/1
0,03
1010
2,1J
12/11/18
AKS
EPA200.8
Nickel, ug/1
0.03
10.0
0.65 J
0,79J
0,75J
01/04/19
AKS
SPA200.8
Selenium, ug/l
0.15
10.0
1.41
12/11/18
AKS
EPA200.8
Selenium, ug/l
0.15
10.0
--- U
--- U
--- U
01/02/19
ARS
BPA200.8
silver, ug/1
0,05
5.0
--- V
--- U
--- V
01/02/19
AKS
BPA200.8
Silver, ug/1
0,05
540
--- U
01/04/19
AKS
SPA200.8
Thallium, ug/1
0.05
1.0
0.08 J
12/11/18
AKS
EPA200.8
Thallium, ug/1
0.05
1,0
--- U
--- U
0.07 J
01/04/19
AKS
BPA200.8
Vanadium, ug/1
0.03
1,0
8.4
12/11/18
AKS
EPA200.8
Vanadium, ug/1
0,03
110
0111 J
0,57 J
0,70 J
01/04/19
AKS
BPA200,8
Zinc, ug/1
0.11
10.0
22
12/11/18
AKS
BPA20048
Zinc, ug/l
0011
1010
1.7 J
3,6 J
01/02/19
ARS
BPA200,8
Zino, ug/l
0,11
1010
4,5a
D1/04/19
ASS
BPA200.8
Conductivity (at 25c),
uMhos/cm 1.0
1.0
192
143
147
lie
12/05/18
PJC
2510E-11
Temperature, °C
10
9
10
10
12/05/18
PJC
2550E-10
Turbidity (Field), MTV
110
1.0
106
7,86
8,30
6,83
12/05/18
PJC
2130E-11
J = 8stimatad value between the MDL end MRL, U e Below ALL OLLantit ation Llmlts.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUD SON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, %N�JC 7703
REVIEWED BY: /f
VOLATILE ORGANICS
EPA METHOD 8260E R2(96)
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 C
ANALYST:
JAP
DATE COLLECTED:
12/05/18
DATE ANALYZED:
12/18/18
DATE REPORTED:
02/21/19
PARAMETERS, ug/l
MDL
MRL
SW-1
SW-2
SW -
awe
1,
Chloromethane
0,77
3,000
---
U
---
U
---
U
---
u
2.
Vinyl Chloride
0,12
0,200
---
V
---
D
---
U
---
U
3,
BromomeEhane
0.67
30.000
---
V
___
U
___
u
M.
D
4,
Chloroethane
0.48
10.000
---
V
---
U
---
D
---
U
5,
Trichlorofluoromethane
0.24
1.000
---
U
---
U
---
U
---
U
6.
1,1-Dichloroethena
0.17
5.000
---
U
---
U
U
___
V
7.
Acetone
9.06
100,000
---
U
---
U
---
U
---
V
8,
Iodomethane
0,26
10,000
---
U
---
U
---
U
---
U
9,
Carbon Disulfide
0,23
100.000
---
U
---
U
---
U
---
U
10,
Methylene Chloride
0.64
1*000
---
U
---
U
---
V
---
U
11,
trane-1,2-Dlahloroetheae
0,23
5.000
M.
U
---
U
---
V
---
u
12.
1,1-Diehloro ethane
0.20
5.000
---
U
---
U
V
---
U
13,
Vinyl Acetate
0.20
50.000
---
U
---
U
--
u
---
D
14,
Cis-1,2-Dichloroethena
0,25
5.000
---
u
---
U
M.
U
---
U
15,
2-Butanone
2,21
100,000
---
U
---
U
---
U
---
V
16,
Bromochloromethane
0,27
3,000
---
u
---
U
---
U
---
U
17,
Chloroform
0,25
5.000
---
u
---
U
---
U
---
U
18,
1,1,1-Trichloroethane
0.19
1.000
---
u
M.
U
---
U
---
U
19,
Carbon Tetrachloride
0.04
0.200
---
U
---
U
---
U
---
U
20,
Benzene
0.24
1.000
---
u
---
U
---
U
---
U
21,
1,2-Dichloroethane
0.02
0.200
---
V
---
V
---
U
---
U
22,
Trichloroethane
0.13
14000
---
V
---
U
---
U
---
U
23.
1,2-Dichloropropane
0.04
0.200
---
U
---
U
---
U
---
u
24,
Bromodichloramethane
0,04
0,200
---
U
---
V
---
D
---
U
25.
Cee-1,3-Dichloropropene
0.06
0,200
---
U
---
V
---
U
---
U
26.
4-Methyl-2-Pentanone
1,19
100.000
---
V
---
U
u
U
27,
Toluene
0,23
1.000
0.38
J
---
V
u
U
28.
Crane-1,3-Dichloropropene
0.04
0.200
---
U
---
U
---
U
---
U
19,
1, 1,2-Trichloroethane
0.03
0.200
---
V
---
U
--
D
---
U
30,
Tetrachloroethene
0.30
0.200
---
U
---
U
---
U
---
U
31,
2-Hexanone
1,57
40,000
---
V
---
U
---
U
---
U
32.
Dibromochloromethane
0,03
09200
---
V
---
V
---
U
---
V
33.
1,1-Dibromoethane
0.03
0.200
---
V
---
V
U
---
V
34.
Chlorobenaene
0,30
3,000
---
U
---
u
---
U
---
U
35.
1,1,1,2-Tetrachloroethane
0,22
1.000
---
U
---
U
---
U
---
U
36.
Bthylbenaane
0,21
1.000
---
V
---
a
---
u
---
U
37,
Xylenee
0.68
5.000
___
u
_'_
U
___
u
___
u
38.
Dibromomethene
0.28
10.000
---
V
"__
U
-"_
u
"__
u
39,
Styrene
0.19
1.000
---
U
---
U
---
U
---
U
40.
Bromotorm
0,20
3,000
---
U
---
U
---
U
---
V
41,
1, 1,2,2-Tetrnchloraethane
0.03
0,200
---
U
---
V
U
U
42,
1,2,3-Trichloropropane
0.09
0.200
---
D
---
U
---
V
---
u
43.
1,4-Diahlorobanaene
0.39
1.000
---
U
---
V
---
U
---
U
44.
1,2-Dichlorobenaene
0,32
5.000
---
V
---
U
---
u
---
U
45.
1,2-Dibromo-3-Chlo ropropane
0.07
0.200
___
V
___
U
_._
U
___
U
46.
Ao rylanitrile
2.72
200.000
---
V
---
U
---
U
---
U
47.
trans-1,4-Dichloro-2-Butene
0,42
100,000
---
U
---
V
---
U
---
U
48,
Tetrahydrofuran
0,39
1.000
---
U
---
V
---
V
---
V
Page: 1
S = Estimated Vfl1u0 between the MDL and MRL, V = Below ALL Quantitatlon Limits.

Environment 1,
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NCB' Ji7703
REVIEWED BY:
VOLATILE ORGANICS
EPA METHOD 8260B R2(96)
�1
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 C
ANALYST:
JAP
DATE COLLECTED:
12/05/18
DATE ANALYZED:
12/18/18
DATE REPORTED:
02/21/19
PARAMETERS, ug/1
MDL
MRL
Sw-1
8W-2
8W-3
8W-9
49, 1,4-Dioxane
2 71T
3. 000
--- D
--- D
--- u
--- u
Page: 2
a = Estimated value between the MDL and MRL, U = Eelow ALL Qeantltation LSmite.

0
n
�w
a
w �
3 c
m �
�n
w o
0 n
0
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00 o
w
� w
w a
d m
mo
� w
a G5
n _
Z
10
W
CSI
V
C.71
C.)'I
W
w�mMP> 1
n
m
m
-z
r
NOS
z
C�J
D
O
A
W
N
0
ryrygg
r1
p
z
�
(n
.iy
9
y
I�
0
r
W
m
m
m
o
�
m
C
m
m
m
TOTAL CHLORINE, mg/I
L�� C7
0
0
OR ug/I AT COLLECTION
m
m
�
—�
_
TEMPERATURE,°C
0
<
0
0 <
0
ATCOLLECTION
m O y
in
in
o
lfOFCONTAINERS
tri z
Field
9
b
pH
Metals
9
b
Conductivity
ro
Temperature
9
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8260 Dup. 1
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m
_ m
6)
8260 Dup. 2
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p
8260 Dup.3
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PARAMETERS TESTS
u
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O
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z
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x x z
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z

Environment 1, Incorporated
114 OAKMONT DRIVE
PHONE
(252)
756-6208
GREENVILLE, N.C. 27858
FAX
(252)
756-0633
ID#: 6003 D
JUDSON WHITEHURST (C&D
LANDFILL)
AMEC FOSTER
WHEELER
ENVIRONMENT
& INFRASTRUCTURE
DATE COLLECTED:
12/13/18
4021 STIRRUP
CREEK DRe
STE
100
DATE REPORTED
02/21/19
DURHAM INC 27703
REVIEWED
BY:
MW-15
MW-16
MV]-17
MW-145
MW-14D
Analysis
Method
PARAMETERS
=I
MRL
Date Analyst
Code
PH (field measurement), Unite
6.5
6.1
5.8
6.4
7.8
12/13/18
BF
450ORB-11
BOD, mg/1
2.0
2.0
--- U
--- U
--- U
--- U
---
U
12/14/19
HMM
521OB-11
COD, mg/1
0,840
20.0
36
113
54
23
---
U
12/14/18
SRJ
HBOOO-79
Nitrate Nitrogen as N, mg/l
01009
0.04
--- V
--- U
--- U
0.05
0,09
12/13/18
BID
353.2 R2-9
Total Organic Carbon, mg/1
0,129
1.0
12,80
41,00
21.80
8,36
2,31
12/17/18
SEJ
531OC-11
Alkalinity (to pH 4.5), mg CaCO3/1 1.0
1.0
63
164
36
74
258
12/17/18
JTH
232OD-11
Chloride, mg/1
5.0
5,0
30
30
14
--- U
14
12/17/18
KDS
4500CLB-11
Cyanide, ug/l
5,0
510
--- U
--- U
--- U
--- U
---
U
12/18/18
SRJ
450OCNE-11
Total Hardness, mg/1
153
180
384
129
149
12/17/18
JMS
2340C-11
Total Dissolved Residue, mg/1
110
10
260
440
654
196
287
12/17/18
KID
254OC-11
Sulfate, mg/1
5.0
5.0
103
110
383
67.1
642
12/14/18
SBJ
4500SO42El
Antimony, ug/l
0,03
1.0
0.05J
0105J
0.04 J
0.06 J
0.04
J
01/02/19
AKS
EPA200,8
Arsenic, ug/1
0,03
5.0
1.4J
3.2a
--- U
0.59 J
---
U
01/02/19
AKS
EPA200,8
Barium, ug/l
0,03
10.0
95.2
67.7
01/02/19
ARE
HPA200,8
Barium, ug/1
0,03
10.0
256
49.3
8.5a
01/04/19
ARE
EPA200.6
Beryllium, ug/1
0,05
1.0
0,05 J
0.09 J
0.05 J
--- U
---
U
01/08/19
ARE
EPA200,8
Cadmium, ug/l
0,02
1.0
0408 J
0.15 J
0,04 J
0,07 J
0.06
J
01/02/19
ARE
RPA200.B
Cobalt, ug/1
0,03
1.0
0.15 J
0,53 J
0,32 J
0,36 J
0,07
J
01/04/19
ARE
BPA200.8
Total Chromium, ug/1
0.15
5.0
--- U
1.5a
0,94 J
0,48 J
---
U
O1/04/19
AKS
BPA200.8
Copper, ug/1
0,03
10.0
0,44 J
0.25 J
0,12 J
0,52 J
0,41
J
01/04/19
AKS
EPA200,8
Iron, ug/1
12,08
50.0
2645
25B60
1470
2303
01/10/19
AKS
311ID-11
Iron, ug/1
12,08
50.0
---
U
01/19/19
AKS
31118-11
Manganese, ug/l
0,31
1090
83
117
170
237
6.9
J
12/28/10
LPJ
EPA200.7
Lead, u9/1
0,03
5,0
0.10 J
0,12 J
0.06J
0,73 J
---
U
01/02/19
AKS
EPA200,8
Mercury, ug/1
0.05
0,20
--- U
--- U
--- V
0,05 J
---
U
12/17/18
MTM
245.1 R3-9
Nickel, ug/1
0,03
10.0
2,1J
1,5J
5,2 J
1.8J
1,4J
01/04/19
AKS
EPA200.8
selenium, ug/1
0.15
1060
--- U
2,1J
--- U
--- U
---
U
01/02/19
AKS
EPA200,8
silver, ug/1
0.05
5.0
--- U
--- U
--- V
--- U
---
U
01/02/19
AKS
EPA200,8
Thallium, ug/1
0.05
1.0
--- U
--- U
--- U
--- U
---
U
01/04/19
AKS
EPA200,9
Tin, ug/1
0005
10010
--- U
--- U
--- U
--- U
---
U
01/04/19
AKS
EPA200.8
Vanadium, ug/1
0903
1.0
3.5
9.1
1,2
2,3
---
U
01/04/19
AKS
BPA200,8
zinc, ug/1
0911
10,0
0,87 J
0,84 J
1.5 J
4,6J
2.0J
01/02/19
ASS
EPA200,8
Sulfide, ug/1
100
1000
--- U
--- U
--- V
--- V
---
U
12/19/18
LFJ
450OS2D-11
Conductivity (at 25c), uNhos/cm 110
1.0
401
370
775
346
522
12/13/18
BP
251OB-11
Dissolved Oxygen, mg/1
0,1
0.1
0425
0.18
0,32
--- U
---
U
12/13/18
BP
450000-11
Temperature, °C
16
17
17
13
17
12/13/18
BF
2550E-10
Iron, Ferrous, ug/1
50,00
200.0
2200
23000
1382
1198
---
U
12/13/18
SHJ
3500FHB-11
static Water Level, feet
5.20
6,45
6.15
3,24
5,24
12/13/18
BP
Well Depth, feet
22,14
22,73
22.25
23,12
41,92
12/13/18
BP
Carbon Dioxide, mg/1
100
1.0
35
346
110
30
13
12/13/18
JTH
45000O2C-1
ORPP m
+85
+97
+71
+99
+94
12/13/18
BF
2580B
Turbidity (Field), NTU
1.0
110
6,42
7,92
2,76
38.8
---
U
12/13/18
BF
213OB-11
J Setimated value between the MDL and MRL, U Below ALL Quantitetlon Llmlte.

Environment 1, Incorporated
I [4 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
IZ
REVIEWED BY:
PESTICIDES AND PCB'S
EPA METHOD 8081B R2(07)
CLIENT ID:
ANALYST:
DATE COLLECTED:
DATE EXTRACTED:
DATE REPORTED:
PHONE [phone]
FAX [phone]
6003 D
HIC
12/13/18
12/14/18
02/21/19
PARAMETHRS, ug/l
Date
MDL
Analyzed
MRL
12/27/18
MW-15
12/27/18
NW-16
12/27/18
MW-17
11/26/18
MW-14S
12/26/18
MW-14D
1.
Al drin
0.029
0.050
---
U
---
U
---
u
---
u
---
u
2.
Alpha-BHC
0.032
0.050
---
u
---
U
---
U
---
U
---
U
3,
Beta-BHC
0.031
0.050
---
u
---
U
---
U
---
U
---
U
4,
Delta-BHC
0.030
0.050
---
U
---
V
---
U
---
u
---
V
5.
Gamma-BHC (Lindans)
0,032
0.050
---
U
---
U
---
U
---
u
---
V
6.
Chlordane
0,320
0.500
---
U
---
U
---
U
---
V
---
U
7.
4,4-DDD
0.051
0.100
---
V
---
u
---
U
---
u
---
V
8,
414-DDE
0.049
0.1D0
---
V
---
U
---
U
---
V
---
U
9,
914-D➢T
0.051
0.100
---
V
---
U
---
U
V
---
U
10.
Dieldrin
0,042
0,075
---
V
---
U
---
U
---
U
---
U
11,
Sndoeulfan I
0.056
0.100
---
V
---
O
---
V
U
U
12.
Sndoeulfan II
0.D46
0.100
---
U
---
V
---
V
---
U
---
U
13,
Endoeulfan Sulfate
0,072
0.100
---
U
---
V
---
U
---
V
---
U
14,
Endrin
0,053
0.100
---
V
---
U
---
U
---
U
---
U
15,
Endrin Aldehyde
0.068
0.100
---
U
---
u
---
U
---
U
---
U
16,
Heptachlor
0,039
0.050
---
U
---
u
---
U
---
U
---
V
17,
Heptachlor Epoxide
0..042
0,075
---
U
---
V
---
U
---
u
---
U
18,
Hethoxychlor
0,530
1.000
---
V
---
V
---
U
---
U
---
U
19,
Pab'e (Aroolors)
0.50D
2,000
---
U
---
U
---
U
---
U
---
U
20,
Toxaphene
0.690
1.500
---
V
---
V
---
U
---
U
---
U
J = Estimated value between the MDL and MRLU = Below ALL Cuantitatlon Llmite.

Environment 1, Inco
GREENVILLE, N.C. 27858
FAX [phone]
CLIENT: JUDSON WHITEHURST %C&D LANDFILL) CLIENT ID: 6003 D
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: HIC
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/13/18
DURHAM, NC 27703 DATE EXTRACTED: 12/18/18
DATE ANALYZED: 12/21/18
REVIEWED BY: DATE REPORTED: 02/21/19
LANDFILL APPENDIX II
F.PA METHbD 8151A R1(961
MW-15
MW-16
"-17
MM-198
MW-19D
PARAMETERS, eg/1
MDL
MRL
1.
2,4-D
0,36
2,000
---
U
---
U
---
U
---
U
---
U
2,
Dinoeeb
0.54
1.000
---
U
---
U
---
U
---
U
---
U
3,
2,4,5-TP
0.42
2.000
---
U
---
U
---
U
---
U
---
U
4,
2,4,5-T
0,47
2,000
---
U
---
U
--"
U
-"
U
"'
U
S = Estimated valUO between the MDL and MRL, U = Helow ALL puantlEation Limlte.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 D
ANALYST:
JAP
DATE
COLLECTED:
12/13/18
DATE
EXTRACTED:
12/17/18
DATE
ANALYZED:
12/19/18
DATE
REPORTED:
02/21/19
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
Page: 1
PARAMETERS, ug/l
MUL
MEL
NW-15
MW-16
MW-17
MW-148
MW-14D
1.
Acenaphthene
2,66
10,000
---
U
---
U
---
U
---
U
---
U
2,
Acenaphthylene
2.6D
10,000
---
u
---
U
---
V
---
V
---
U
3,
Anthracena
2.97
10.000
---
U
---
U
---
U
V
U
4.
Benzo [a]antrhaaene
4.16
10.000
---
U
---
U
---
V
---
V
---
U
5.
Benzo [b]Lluoranthene
3.32
10.000
---
U
---
U
---
U
---
U
---
U
6.
Benzo [k7 Yluoranthene
9.23
30..000
---
U
---
U
---
U
---
U
---
U
7,
Benzo[g,h,i]perylene
2,61
10,000
---
U
---
u
---
V
---
U
---
U
8,
Benzo[a]pyrens
3,27
10.o00
---
U
---
V
---
U
---
U
---
u
9.
4-eromophenyl Phenyl Ether
2,63
10,000
---
V
---
U
---
V
M.
U
---
U
10,
Butyl Benzyl Phthalate
5.78
10.000
---
V
---
U
---
U
---
U
---
U
11,
Bie(2-Chloroethoxy) Methane
3.14
10.000
---
U
---
U
---
U
---
U
---
U
12.
Bis(2-Chloroethyl) Ether
2,58
10,000
---
u
---
U
---
U
---
U
---
U
13.
Bis(2-Chloro-l-methylethyl) Ether
2,58
10,000
---
U
---
U
---
U
---
U
---
V
14,
2-Chloronaphthalens
2.17
10,000
---
U
---
U
---
U
---
U
---
U
15.
4-Chlorophenyl Phenyl Ether
2.42
10,000
---
U
---
U
---
V
---
U
---
V
16.
Chrysene
4,04
10,000
---
U
---
V
---
U
"'
U
"'
V
17,
Dibenzo[a,h]anthracene
2.78
10,000
---
U
---
U
---
U
---
U
---
V
18,
Di-N-Butyl Phthalate
3,09
10.000
---
U
---
U
---
U
---
U
---
U
19,
Dimethyl Phthalate
3,78
10,000
---
U
---
u
---
U
---
U
---
U
20.
Diethyl Phthalate
3,92
10,000
---
U
---
V
---
U
---
V
---
U
21.
2,4-D initrotoluene
3.95
10.000
---
U
---
U
---
U
--
U
V
22,
2,6-Dinitratoluene
3.88
10,000
---
U
---
U
---
U
---
U
---
U
23.
Di-N-Octyl Phthalate
2.81
10.000
---
V
---
V
___
U
___
V
___
U
24,
Hie-(2-Ethylhexyl) Phthalate
9,97
15,000
---
U
---
U
---
V
---
U
---
U
25,
Yluoranthene
3,92
10,000
---
U
---
U
---
U
---
U
---
U
26,
Pluorene
2.95
10.000
---
V
---
U
---
U
U
---
U
27,
Hexaahlorobenzane
2,61
10.000
---
U
---
U
---
U
---
u
---
U
28,
Hexachlorocyclopentadlene
4,16
10,000
---
U
---
U
---
U
---
U
---
U
29.
Indeno [1,2,3-Cd]pyrene
2.91
10.000
---
V
---
U
---
U
U
V
30,
Ieophorone
3.74
10.000
---
II
---
U
---
U
U
V
31,
Mitrobenzene
2,85
10.000
---
V
---
U
---
U
---
U
---
U
32.
N-Nitroeodimethylamine
4,25
10,000
---
U
---
U
---
U
---
U
---
U
33,
N-Nitroeodiphenylamine
3,95
10,000
---
U
---
U
---
U
---
U
---
U
34.
N-Nitroeodi-N-Propylamine
4,06
10.000
---
U
---
U
---
U
---
U
---
U
35,
Phenanthrene
3,24
10.000
---
V
---
U
---
U
---
U
---
u
36,
Pyrene
3.63
10,000
---
V
---
U
---
U
---
U
---
u
37,
4-Chloro-3-Methylphenol
3,79
20.000
---
u
---
U
---
U
---
U
---
u
38.
2-Chlorophanol
2.75
10.000
---
U
---
U
---
U
---
U
---
V
39.
O-Cresol
3.68
10.000
---
V
---
U
---
V
U
---
U
40.
P-Cresol
4,12
10.000
---
U
---
U
---
U
---
U
---
U
41.
2,4-Dichlorophenol
5.19
10,000
---
U
---
U
---
U
---
U
---
U
42.
2,6-Dichlorophenol
4,99
10.000
---
U
---
U
---
U
---
U
---
U
43.
2,4-DSmethylphenol
3,21
10,000
---
V
---
U
---
u
---
U
---
V
44.
9,6-Dlnitro-2-Methylphenol
4.77
50.000
---
U
---
U
---
U
---
U
---
V
45.
2,4-Dinitrophenol
4.37
50,000
W.
U
---
U
---
U
---
u
---
U
46.
Ethyl NathaneeulEonate
5.26
20.000
---
V
---
U
___
U
___
u
_-_
V
47.
Methyl MethaneeulEonate
9.92
10.000
---
V
---
V
---
U
U
U
48.
2-Nitrophenol
3.64
10,000
---
U
---
V
---
U
---
V
---
U
J = Estimated value between the MDL and MEL, V a Below ALL Quantlt anon Limits,

Environment 1, Incor
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
CLIENT ID:
Drinking water IDi 37715
Wastewater IDI 10
PHONE [phone]
FAX [phone]
6003 D
ANALYST:
JAP
DATE
COLLECTED:
12/13/18
DATE
EXTRACTED:
12/17/18
DATE
ANALYZED:
12/19/18
DATE
REPORTED:
02/21/19
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
Page: 2
PARAMETERS, ug/1
MDL
MEL
NN-15
MW-16
MW-17
MW-148
MW-14D
49,
4-Nitrophenol
3.17
50.000
---
U
---
V
---
U
---
V
---
U
50,
Pentachlorophenol
5.33
25,000
---
U
---
U
---
U
---
U
---
U
51,
Phenol
1.86
10,000
---
U
---
V
---
V
---
U
---
U
52,
2,3,4,6-Tetrachlorophenol
3,12
30,000
---
V
---
U
---
U
---
V
---
V
53.
2,4,5-Trichlorophenol
4,17
30.000
---
U
---
U
---
U
---
U
---
U
54,
2,4,6-Trichlorophenol
3,84
10,000
---
U
---
U
---
U
---
U
---
V
55,
Acetophanone
2,89
10,000
---
V
---
V
---
U
---
U
---
U
56.
2-Acetylaminofluorene
3.98
20,000
---
V
---
V
---
U
---
U
---
U
57.
4-Aminobiphenyl
4,12
20,000
---
V
---
U
---
U
---
U
---
U
59,
Benryl Alcohol
4,47
20,000
---
❑
---
U
---
U
---
U
---
U
59.
4-Chloroanillne
3,36
20,000
---
U
---
U
---
U
---
U
---
U
60.
Chl orobenzllate
5.12
10.000
---
U
---
U
---
U
---
U
---
U
61.
Dlall ate
1.98
10.000
---
U
---
V
---
V
---
U
---
U
62,
Dibenzofuran
4.18
10.000
---
V
---
U
---
V
---
U
---
U
63,
3,3-➢ichlorobenzidine
4,22
20,000
---
U
---
U
---
U
---
V
---
U
64,
Dimethoate
3.9B
20,000
---
U
---
U
---
V
---
U
---
U
65,
P-DSmethylaminoazobenzens
2,89
10.000
---
U
---
U
---
U
---
U
---
U
66,
7,12-Dimethylbenz[a]anthracene
5,26
10,000
---
U
---
U
---
U
---
U
---
U
67,
3,3-Dimethylbenzadine
3,21
10.000
---
U
---
V
---
U
---
V
---
U
68.
1,3-Dinitrobenrene
2,89
20,000
---
U
---
U
---
U
---
V
---
U
69,
Diphenylamine
5.10
10,000
---
V
---
U
---
U
---
V
---
U
70,
Dieulfoton
4,28
10,000
---
V
---
U
---
U
---
V
---
U
71,
Pamphur
3.98
20.000
---
U
---
V
---
U
V
V
72,
Hexachloropropene
4,31
10.000
---
U
---
V
---
U
---
U
---
U
73,
Ieosafrole
2,98
10,000
---
V
---
V
---
U
---
U
---
U
74,
Repone
2.78
20,000
___
V
___
V
___
V
__-
U
___
U
75,
Methapyrilene
3,54
100.000
---
V
---
U
---
U
---
U
---
11
76,
3-Methylchloroanthrene
4,21
10,000
---
U
---
U
---
U
---
U
---
U
77,
2-Methyluaphthalene
3.79
10,000
---
U
---
U
---
U
---
U
---
V
78,
Methyl Parathion
4.32
10.000
---
V
---
U
---
V
---
U
---
U
79,
m-Cresol
3.81
10.000
---
V
---
U
---
U
---
U
---
V
80.
1,4-Naphthoquinone
4.00
104000
---
V
---
V
---
V
---
U
---
U
el.
1-Naphthylamine
5.61
10.000
---
U
---
V
---
U
---
V
---
U
82.
2-Naphthylasine
4.62
30.000
---
V
---
U
---
U
---
V
---
U
83.
2-Nitroaniline
3,61
50.000
---
U
---
U
---
V
---
U
---
V
94.
3-Nitroanillne
4.81
50,000
---
U
---
U
---
U
---
U
---
U
85.
4-Nitroaniline
4,22
20.000
---
U
---
U
---
U
---
V
---
U
86.
5-Nitro-O-Toluidine
4.01
10.000
---
U
---
U
---
V
---
U
---
U
87.
N-Nitrosodi-n-butylamine
3,63
10,000
---
U
---
V
---
U
---
V
---
U
88,
N-Nitroeodiethylamine
3,83
20,000
---
V
---
U
---
U
---
U
---
U
89,
N-NStrosomethylethylamine
3.83
10,000
---
V
---
U
---
U
---
U
---
U
90,
N-Nitrosopiparidine
5.19
20.000
---
V
---
U
---
U
---
U
---
V
91.
N-Nitroeopyrrolifllne
2.89
10.000
---
V
---
U
---
U
V
U
92,
Parathion
3,12
10,000
---
U
---
V
---
U
---
U
---
V
93.
Pentachlorobavzene
3,92
10.000
---
V
---
U
---
U
U
V
94,
Pentachloronitrobenzene
3.71
20,000
---
U
---
U
-•-
U
---
U
--•
U
95,
Phenacetin
4,41
20.000
---
V
---
U
---
V
---
U
---
U
96,
1.4 eenzenadiamine
2,99
10,000
---
V
---
U
---
U
---
U
---
U
J = 8etlmated value between the MDL and MRL, U Below ALL Duentltation Limits.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
CLIENT ID:
PHONE [phone]
FAX [phone]
6003 D
ANALYST:
JAP
DATE
COLLECTED:
12/13/18
DATE
EXTRACTED:
12/17/18
DATE
ANALYZED:
12/19/18
DATE
REPORTED:
02/21/19
SEMI -VOLATILE ORGANICS
EPA METHOD 8270D R4(07)
Page: 3
PARAMETERS, ug/l
MDL
MRL
MW-15
MW-16
MW-17
MW-14S
MW-14D
97.
Phorate
3.86
30.000
---
V
---
U
---
D
---
D
---
U
98,
Pronamide
3.69
10,000
---
U
---
U
---
u
---
V
---
U
99.
SaErole
4,12
10.000
---
V
---
u
---
U
---
V
---
V
100,
1,2,4,5-Tetrachlorobenzene
5.01
10.000
---
U
---
u
---
U
---
V
---
V
101,
Thionazin
4,62
20,000
---
U
---
U
---
V
---
U
---
V
102,
O-Toluidlna
4.11
10,000
---
U
---
U
---
U
U
---
U
103,
1,3,5-Trinitrobenzene
3,98
10,000
---
V
---
V
---
U
---
U
---
U
104.
0,0,0-Triethyl Phoephorothioate
3,61
10,000
---
V
---
U
---
U
---
V
---
U
105,
Rexaohloroathane
1.49
30.000
---
U
---
V
---
V.
U
V
106.
Ieodrin
3.11
20.000
---
U
---
U
---
U
---
U
---
U
T = Betlmated value between the MDL and MRL, U e e010W ALL 0uantl Cation LSmite,

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHORST (C&D LANDFILL)
A14EC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
LANDFILL APPENDIX II
F.AA MR.TWnn R29OR R2(96)
CLIENT ID:
Wastewater ID,
PHONE [phone]
FAX [phone]
6003 D
ANALYST: JAP
DATE COLLECTED: 12/13/18 Page: 1
DATE REPORTED: 02/21/19
PARAMETERS, u9/1
Data
MDL
Analyzed
MEL
12/19/10
14W-15
12/19/18
MW-16
12/19/18
MW-17
12/19/18
MW-14S
12/19/18
Mw-14D
I.
Chl oromethane
0.77
3.000
---
U
---
V
---
U
V
0
2,
Vinyl Chloride
0,12
0.200
---
U
---
U
---
U
---
U
---
U
3,
Hromomathane
O.67
10.000
---
U
---
U
---
U
---
U
---
U
4,
Chloroethane
0,48
10,000
---
U
---
U
---
U
---
D
---
U
5,
Trivhlorofluoromethane
0,24
1.000
---
U
---
V
---
U
---
U
---
U
6.
1,1-Dichloroethene
0,17
5.000
M.
U
---
U
---
U
---
u
---
V
7,
Acetone
9,06
100,000
---
U
---
u
---
U
---
U
---
U
8,
Lodomethene
0,26
10,000
---
V
---
U
---
U
---
V
---
U
9,
Carbon Disulfide
0,23
100,000
---
V
M.
V
---
U
---
U
---
U
10,
Methylene Chloride
0.64
1.000
---
V
---
U
---
V
---
U
---
U
11,
trans-1,2-Dichloroethene
0.23
5.000
---
V
---
U
---
V
---
U
---
U
12.
1,1-Dichloroethane
0.20
5.000
---
U
---
U
---
U
---
U
---
U
13.
Vinyl Acetate
0.10
50.000
---
V
---
U
---
U
U
---
U
14.
Cie-1,2-DioRl oroethena
0.25
5.000
---
U
---
U
---
U
U
---
U
Ss.
x-BvtenDne
2.21
100.000
---
v
---
v
---
v
--
U
U
16,
Biomochloromethane
0,27
3,000
---
V
---
U
---
U
---
U
---
U
17,
Chloroform
0.25
5.000
---
V
---
U
---
V
V
---
U
18,
1,1,1-Trichloroethane
0.19
1.000
---
U
---
U
---
U
---
U
---
V
19,
Carbon Tetrachloride
0,04
O.200
---
U
---
V
---
U
---
U
---
U
20.
Benzene
0.29
1.000
---
V
---
V
---
U
--
U
U
21,
1,2-Dichloroethane
0,02
0.200
---
U
---
V
M.
U
---
U
---
U
22,
Trichloroethene
0,23
1.000
---
u
---
U
---
U
---
U
---
U
23,
1,2-Dichloropropane
0,04
0,200
---
U
---
U
---
U
---
V
---
U
24,
Bromodichloromethane
0,04
0,200
---
D
---
U
---
U
---
U
---
U
25.
Cia-1,3-Dichloropropene
0.06
0,200
---
V
---
U
---
U
---
U
---
U
26.
4-Methyl-2-Pentanone
1.19
100,000
---
U
---
U
---
V
---
U
---
U
27,
Toluene
0,23
1.000
---
U
---
U
---
V
---
U
---
U
28,
trans-10-Dichloropropene
0.04
0,200
---
U
---
U
---
U
---
U
---
V
29,
1,1,2-Trichloroethane
0.03
0.200
---
U
---
U
---
V
--
U
---
V
30.
Tetrachloroethane
0.10
0.200
---
V
---
U
---
V
--
U
---
U
31.
2-Hexanone
1.57
50,000
---
V
---
U
---
U
---
U
---
U
32,
Dibromovhloromethene
0.03
0.200
---
V
---
V
---
V
u
U
33,
1,2-Dlbromoathane
0.03
0.200
---
U
---
V
---
V
--
U
---
U
34.
Chlorobenzene
0,30
3.000
---
U
---
U
---
U
---
U
---
U
35.
1,1,1,2-Tetrachloroethane
0.22
1.000
---
U
---
U
---
U
---
u
---
u
36.
Ethylbenzene
0.21
1.000
---
V
---
U
---
V
---
U
---
U
37.
%ylenes
0.68
5,000
---
U
---
U
---
V
---
U
---
U
38,
Dibromomethane
0,28
10400
---
U
---
U
---
U
---
U
---
U
39,
Styrene
0.19
1.000
---
U
---
U
---
U
---
U
---
V
90,
Bromoform
0.20
3.000
---
U
---
U
---
U
---
U
---
U
41,
1,1,2,2-Tetrachloroethane
0.03
0,200
---
U
---
U
---
V
---
V
---
U
42,
1,2,3-Trichloropropane
0.09
0,200
---
U
---
U
---
U
---
V
---
U
43,
1,4-Dichlorobenzene
0,39
1.000
---
U
---
U
---
u
---
V
---
V
44.
1,2-Dichlorobenzene
0,32
5.000
---
u
---
V
---
U
---
U
---
U
45,
1,2-Dibromo-3-Chloropropens
0,07
0,200
---
U
---
U
---
U
---
U
---
U
46.
Acrylonitrile
2,72
200,000
---
U
---
U
---
V
---
U
---
U
47,
trans-1,4-Dichloro-2-Butene
0,42
100,000
---
U
---
U
---
U
---
U
---
U
J w Estimated value between the MDL and MRL, V = Below ALL 0uantlt ation Limits.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
CLIENT: JUDSON WHITEHURST (C&D LANDFILL)
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE
4021 STIRRUP CREEK DR. STE 100
DURHAM, NC 27703
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260B R2(96)
CLIENT ID:
Wastewater ID, 10
PHONE [phone]
FAX [phone]
6003 D
ANALYST: JAP
DATE COLLECTED: 12/13/18 Page: 2
DATE REPORTED: 02/21/19
PARANBTERS, ug/l
Date
NDL
Analyzed
MRL
12/19/18
NW-15
12/19/18
MW-16
121191 8
MW-17
12/19/1B
NW-198
12/19/18
MW-14D
48,
Acrolein
1,97
4,000
---
U
---
U
---
V
---
V
---
U
49,
Allyl Chloride
0.20
10.000
---
V
---
U
---
V
V
U
50.
Chloroprene
0,21
20.000
---
V
---
V
---
U
---
U
---
U
51,
1,3-Dlchlorobenzene
0,41
5.000
---
U
---
U
---
U
---
U
---
U
52.
Dichlorodiflucromethane
0.51
5.000
---
U
---
V
---
V
---
U
---
U
53.
1,3-Dichloropropane
0.2B
1.000
---
U
---
U
---
V
---
V
---
U
54.
2,2-Dichloropropane
0,17
15,000
---
V
---
U
---
V
---
U
---
U
55.
1,1-Dichloropropene
0,22
5.000
---
U
---
U
---
V
---
V
---
U
56,
Ethyl Methacrylate
0.16
10,000
---
U
---
U
---
U
---
U
---
U
57.
Hexaohlorobut adiene
0.10
0.100
---
V
---
U
---
U
U
---
U
58,
I00butyl Alcohol
12,80
100,000
---
U
---
U
---
D
---
U
---
U
59,
Methacrylonitrlle
1.93
100,000
---
U
---
V
---
U
---
U
---
U
60,
Methyl Methacrylate
0.25
30,000
---
U
---
V
---
U
---
U
---
V
61,
Naphthalene
0.47
6,000
---
U
---
V
---
U
---
D
---
U
62.
Propionitrile
3,26
150.000
---
U
---
U
---
U
---
U
---
V
63,
1,2,4-Trichlorobenzene
0.50
10,000
---
U
---
U
---
V
---
U
---
V
64,
Acetonitrile
36929
55.000
---
V
---
U
---
V
---
U
---
V
65,
Tetrahydro[uran
0.39
1.000
---
U
---
U
---
U
---
U
---
U
66,
1,4-Dioxane
2.71
3,000
---
U
---
V
---
U
---
U
---
V
J = Setimated value between the MDL and MRL, U eeloW ALL QUBntlt anon Limlte,

Environment 1,
rated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
FAX
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT ID: 6003 D
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/13/18
DURHAM, NC 27703 DATE REPORTED: 02/21/19
REVIEWED BY:
gr
LANDFILL APPENDIX II
EPA METHOD 8260B R2(96)
PARAMETBRR, ug/1
Date
MDL
Analyzed
MRL
11/18/18
Trip
Blank
1,
Chloromethane
0,77
3,000
---
U
2.
Vinyl Chloride
0,12
0,2u0
---
U
3,
Bromomethane
0,67
10,000
---
V
4,
Chloroethans
0,48
10.0D0
---
U
5,
Trichlorofluoromethane
0,24
1.000
---
U
6.
1,1-Dlchloroethene
0,17
54000
---
U
7,
Acetone
9,06
100,000
---
U
8,
Iodomethane
0,26
10,000
---
U
9,
Carbon Disulfide
0,23
100,000
---
U
10,
Hethylens Chloride
0,64
1.000
---
U
11,
Crane-112-Dichloroethene
0,23
5.000
---
U
12.
1,1-Diahloroethane
0.20
5.000
---
V
13.
Vinyl Acetate
0.20
50,000
---
U
14,
Cie-1,2-Dichloroethene
0.25
5.000
---
U
15.
2-Butanone
2,21
100,000
---
U
16,
Bromochloromethane
0,27
3,000
---
U
17,
Chloroform
0,25
5,000
---
U
18,
1,1,1-Triahloroethane
D.19
1,000
---
U
19,
Carbon Tetrachloride
0.04
0,200
---
U
20,
Benzene
0,24
1.000
---
U
21.
1,2-Diahloroethans
0,02
0,200
---
U
22,
Trichloroethene
0923
1.000
---
U
23,
1,2-Dichloropropane
0,04
0.200
---
U
24,
Bromodichloromethane
0,04
0,200
---
U
25.
Cie-1,3-Dichloropropene
0406
0,200
---
V
26,
4-Methyl-2-Pentanone
1,19
100.000
---
U
27,
Toluene
0.23
1.000
---
U
28.
trans-1,3-Dichloropropene
0.04
0,200
---
U
29.
1,1,2-Trichloroethane
0,03
0.200
---
U
30,
Tetrachloroethene
0.30
0,200
---
U
31,
2-Hexanone
1,57
504000
---
U
32,
➢fbromoahloromethane
0,03
0,200
---
U
33.
1,2-Dibromoethane
0,03
0,200
---
V
34,
Chlorobenzene
0,30
3,000
---
U
35,
1,1,1,2-Tatraahloroothane
0,22
1.000
---
U
36,
Ethylbenzene
0,21
1.000
---
U
37.
xylenes
0.68
5.000
---
U
38,
Dibromomethane
0.28
10.000
---
V
39,
Styrene
0.19
1,000
---
U
40,
Bromoform
0,20
3.000
---
U
41,
1,1,2,2-Tetrachloroethans
0,03
0.200
---
U
42.
1,2,3-Triahloropropans
0.09
0,200
---
V
43,
1,4-Dichlorobenzene
0,39
1.000
---
U
44.
1,2-Dichlorobenzene
0.32
5.000
---
U
45.
1,2-Dlbromo-3-Chloropropane
0.07
0,200
---
U
46.
Aarylonitrile
2,72
200.000
---
U
47,
trans-1,4-Diahloro-2-Butene
0,42
100,000
---
U
756-0633
Page: 3
J Eetimat ed value between the MDL and Mho U Below ALL Quantitation LSm 1te.

Environment 1, Incorporated
114 OAKMONT DRIVE
GREENVILLE, N.C. 27858
Drinking Wgff.n1 37715
Wastewater ID: 30
PHONE [phone]
FAX [phone]
CLIENT: JUDSON WHITEHURST (C&D LANDFILL) CLIENT IDs 6003 D
AMEC FOSTER WHEELER
ENVIRONMENT & INFRASTRUCTURE ANALYST: JAP
4021 STIRRUP CREEK DR. STE 100 DATE COLLECTED: 12/13/18
DURHAM, NC 27703 DATE REPORTED: 02/21/19
REVIEWED BY:
LANDFILL APPENDIX II
EPA METHOD 8260E R2(96)
PARAMETERS, ug/l
Data
MDL
Analy eed
MRL
12/18/18
Trip
Blank
48,
Acrolein
1,97
4.DOD
---
u
49,
Allyl Chloride
0,20
10,000
---
V
50,
Chloroprene
0.21
20,000
---
U
51,
1,3-Dichlorobenrene
0.41
5,000
---
u
52,
Dichlorodifluoromethene
0.51
5,000
---
D
53.
1,3-Dichloropropans
0,28
1.000
---
V
54,
2,2-Dichloropropans
0,17
15,000
---
V
55,
1,1-Dichloropropene
0.22
5.000
---
u
56,
Ethyl Methacrylate
0116
10,000
---
u
57,
Nexachlorobutadiene
0.10
0,200
---
u
59,
Isobutyl Alcohol
12,80
100.000
---
u
59,
Methaorylonitr11e
1,93
1009000
---
D
60.
Methyl Methacrylate
0,25
30,000
---
V
61,
Naphthalene
0,47
6.000
---
u
62,
Propionitrile
3,26
150.000
---
D
63,
1,2,4-Trlchlorobenaene
0.50
10.000
---
u
64,
Acetonitrile
36.29
55.000
---
u
65.
Tetrahydroiuran
0.39
1.000
---
u
66.
1,4-Dioxane
2.71
3.000
---
U
Page: 4
J = HetlmaEsd value between the MDL and Mat, V = Below ALL Cuantitation Limits.

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lacmnalyficalo
December 28, 2018
Steve Jones
Environment 1, Inc.
PO Box 7085
114 Oakmont Drive
Greenville, NC 27835
RE: JUDSON WHITEHURST / 6003
Pace Workorder. 28909
Dear Steve Jones:
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory between Thursday, December 06,
2018 and Friday, December 14, 2018. Results reported herein conform to the most current NELAC standards,
where applicable, unless otherwise narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ruth Welsh 12/28/2018
[e-mail]
Customer Service Representative
Enclosures
As a valued client we would appreciate your comments on our service.
Please email [e-mail].
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Total Number of Pages 63
Page 1 of 59

Pace Analytical Energy Services LLC
220 William Pitt Way
.,-- A__1.X__1 o Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
LABORATORY ACCREDITATIONS & CERTIFICATIONS
Accreditor: Pennsylvania Department of Environmental Protection, Bureau of Laboratories
Accreditation ID: 02-00538
Scope: NELAP Non -Potable Water
Accreditor:
West Virginia Department of Environmental Protection, Division of Water and Waste
Management
Accreditation ID:
395
Scope:
Non -Potable Water
Accreditor:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
Accreditation ID:
89009003
Scope:
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
Accreditor:
State of Virginia
Accreditation ID:
460201
Scope:
Non -Potable Water
Accreditor:
NELAP: New Jersey, Department of Environmental Protection
Accreditation ID:
PA026
Scope:
Non -Potable Water
Accreditor:
NELAP: New York, Department of Health Wadsworth Center
Accreditation ID:
11815
Scope:
Non -Potable Water
Accreditor:
State of Connecticut, Department of Public Health, Division of Environmental Health
Accreditation ID:
PH-0263
Scope:
Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor:
NELAP: Texas, Commission on Environmental Quality
Accreditation ID:
T104704453-09-TX
Scope:
Non -Potable Water
Accreditor:
State of New Hampshire
Accreditation ID:
299409
Scope:
Non -potable water
Accreditor:
State of Georgia
Accreditation ID:
Chapter 391-3-26
Scope:
As per the Georgia EPD Rules and Regulations for Commercial Laboratories, PAES is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 2 of 59

lacmnalyficalo
SAMPLE SUMMARY
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
289090001
MW1S
Bubble Strip
12/4/2018 09:45
12/6/2018 11:15
289090002
MW1D
Bubble Strip
12/4/2018 15:45
12/6/2018 11:15
289090003
MW2S
Bubble Strip
12/4/2018 15:20
12/6/2018 11:15
289090004
MW2D
Bubble Strip
12/4/2018 14:26
12/6/2018 11:15
289090005
MW3S
Bubble Strip
12/4/2018 13:05
12/6/2018 11:15
289090006
MW3D
Bubble Strip
12/4/2018 12:10
12/6/2018 11:15
289090007
MW3A
Bubble Strip
12/4/2018 11:10
12/6/2018 11:15
289090008
MW4
Bubble Strip
12/5/2018 13:05
12/6/2018 11:15
289090009
MW5
Bubble Strip
12/5/2018 10:48
12/6/2018 11:15
289090010
MW6
Bubble Strip
12/5/2018 11:35
12/6/2018 11:15
289090011
MW7
Bubble Strip
12/5/2018 12:25
12/6/2018 11:15
289090012
MW8
Bubble Strip
12/5/2018 09:35
12/6/2018 11:15
289090013
MW1 S
Water
12/4/2018 09:45
12/6/2018 11:15
289090014
MW1 D
Water
12/4/2018 15:45
12/6/2018 11:15
289090015
MW2S
Water
12/4/2018 15:20
12/6/2018 11:15
289090016
MW2D
Water
12/4/2018 14:26
12/6/2018 11:15
289090017
MW3S
Water
12/4/2018 13:05
12/6/2018 11:15
289090018
MW3D
Water
12/4/2018 12:10
12/6/2018 11:15
289090019
MW3A
Water
12/4/2018 11:10
12/6/2018 11:15
289090020
MW4
Water
12/5/2018 13:05
12/6/2018 11:15
289090021
MW5
Water
12/5/2018 10:48
12/6/2018 11:15
289090022
MW6
Water
12/5/2018 11:35
12/6/2018 11:15
289090023
MW7
Water
12/5/2018 12:25
12/6/2018 11:15
289090024
MW8
Water
12/5/2018 09:35
12/6/2018 11:15
289090025
MW9A
Bubble Strip
12/12/2018 09:40
12/14/2018 11:30
289090026
MW10
Bubble Strip
12/12/2018 10:35
12/14/2018 11:30
289090027
MW11
Bubble Strip
12/12/2018 11:40
12/14/2018 11:30
289090028
W12S
Bubble Strip
12/12/2018 12:45
12/14/2018 11:30
289090029
MW13
Bubble Strip
12/12/2018 13:45
12/14/2018 11:30
289090030
W14S
Bubble Strip
12/13/2018 09:45
12/14/2018 11:30
289090031
W14D
Bubble Strip
12/13/2018 10:35
12/14/2018 11:30
289090032
MW15
Bubble Strip
12/13/2018 11:40
12/14/2018 11:30
289090033
MW16
Bubble Strip
12/13/2018 12:40
12/14/2018 11:30
289090034
MW17
Bubble Strip
12/13/2018 13:40
12/14/2018 11:30
289090035
MW9A
Water
12/12/2018 09:40
12/14/2018 11:30
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 3 of 59

lacmnalyficalo
SAMPLE SUMMARY
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
289090036
M W 10
Water
12/12/2018 10:35
12/14/2018 11:30
289090037
M W 11
Water
12/12/2018 11:40
12/14/2018 11:30
289090038
W 12S
Water
12/12/2018 12:45
12/14/2018 11:30
289090039
M W 13
Water
12/12/2018 13:45
12/14/2018 11:30
289090040
W14S
Water
12/13/2018 09:45
12/14/2018 11:30
289090041
W 14D
Water
12/13/2018 10:35
12/14/2018 11:30
289090042
M W 15
Water
12/13/2018 11:35
12/14/2018 11:30
289090043
M W 16
Water
12/13/2018 12:40
12/14/2018 11:30
289090044
M W 17
Water
12/13/2018 13:40
12/14/2018 11:30
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 4 of 59

lacmnalyficalo
PROJECT SUMMARY
Workorder: 28909 JUDSON WHITEHURST / 6003
Batch Comments
Batch: EDON/3951 -Low Level Volatile Fatty Acids
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
The method blank contains a concentration above the reporting limit. Analyte Acetic acid. Results for this analyte in associated
samples may be bias high.
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 5 of 59

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090001
Sample ID: MW1S
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/4/2018 09:45
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
6.5 ug/I
0.10
0.023 1 12/12/2018 05:52 TD
n
Ethane
0.0039J ug/I
0.010
0.0020 1 12/12/2018 05:52 TD
n
Ethene
0.0050J ug/I
0.010
0.0030 1 12/12/2018 05:52 TD
n
Hydrogen
2.1 nM
1.0
0.65 1 12/12/2018 05:52 TD
n
Report ID: 28909 - 1127864 Page 6 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090002
Sample ID: MW1D
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/4/2018 15:45
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
5600 ug/I
0.10
0.023 1 12/12/2018 06:05 TD
n
Ethane
1.4 ug/I
0.010
0.0020 1 12/12/2018 06:05 TD
n
Ethene
0.00301.11 ug/I
0.010
0.0030 1 12/12/2018 06:05 TD
n
Hydrogen
4.8 nM
1.0
0.65 1 12/12/2018 06:05 TD
n
Report ID: 28909 - 1127864 Page 7 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090003
Sample ID: MW2S
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/4/2018 15:20
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
440 ug/I
0.10
0.023 1 12/12/2018 06:17 TD
n
Ethane
0.015 ug/I
0.010
0.0020 1 12/12/2018 06:17 TD
n
Ethene
0.0075J ug/I
0.010
0.0030 1 12/12/2018 06:17 TD
n
Hydrogen
2.3 nM
1.0
0.65 1 12/12/2018 06:17 TD
n
Report ID: 28909 - 1127864 Page 8 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090004
Sample ID: MW21)
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/4/2018 14:26
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
45 ug/I
0.10
0.023 1 12/12/2018 06:34 TD
n
Ethane
0.018 ug/I
0.010
0.0020 1 12/12/2018 06:34 TD
n
Ethene
0.032 ug/I
0.010
0.0030 1 12/12/2018 06:34 TD
n
Hydrogen
2.8 nM
1.0
0.65 1 12/12/2018 06:34 TD
n
Report ID: 28909 - 1127864 Page 9 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090005
Sample ID: MW3S
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/4/2018 13:05
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
590 ug/I
0.10
0.023 1 12/12/2018 06:46 TD
n
Ethane
0.10 ug/I
0.010
0.0020 1 12/12/2018 06:46 TD
n
Ethene
0.020 ug/I
0.010
0.0030 1 12/12/2018 06:46 TD
n
Hydrogen
3.3 nM
1.0
0.65 1 12/12/2018 06:46 TD
n
Report ID: 28909 - 1127864 Page 10 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090006
Sample ID: MW31)
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/4/2018 12:10
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
54 ug/I
0.10
0.023 1 12/12/2018 06:58 TD
n
Ethane
0.045 ug/I
0.010
0.0020 1 12/12/2018 06:58 TD
n
Ethene
0.011 ug/I
0.010
0.0030 1 12/12/2018 06:58 TD
n
Hydrogen
2.1 nM
1.0
0.65 1 12/12/2018 06:58 TD
n
Report ID: 28909 - 1127864 Page 11 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090007
Sample ID: MW3A
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/4/2018 11:10
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
440 ug/I
0.10
0.023 1 12/12/2018 07:12 TD
n
Ethane
0.056 ug/I
0.010
0.0020 1 12/12/2018 07:12 TD
n
Ethene
0.013 ug/I
0.010
0.0030 1 12/12/2018 07:12 TD
n
Hydrogen
3.3 nM
1.0
0.65 1 12/12/2018 07:12 TD
n
Report ID: 28909 - 1127864 Page 12 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090008
Sample ID: MW4
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/5/2018 13:05
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
320 ug/I
0.10
0.023 1 12/12/2018 07:24 TD
n
Ethane
0.015 ug/I
0.010
0.0020 1 12/12/2018 07:24 TD
n
Ethene
0.0089J ug/I
0.010
0.0030 1 12/12/2018 07:24 TD
n
Hydrogen
2.5 nM
1.0
0.65 1 12/12/2018 07:24 TD
n
Report ID: 28909 - 1127864 Page 13 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090009
Sample ID: MW5
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/5/2018 10:48
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
890 ug/I
0.10
0.023 1 12/12/2018 07:37 TD
n
Ethane
0.060 ug/I
0.010
0.0020 1 12/12/2018 07:37 TD
n
Ethene
0.00301.11 ug/I
0.010
0.0030 1 12/12/2018 07:37 TD
n
Hydrogen
2.4 nM
1.0
0.65 1 12/12/2018 07:37 TD
n
Report ID: 28909 - 1127864 Page 14 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090010
Sample ID: MW6
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/5/2018 11:35
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
620 ug/I
0.10
0.023 1 12/12/2018 07:49 TD
n
Ethane
0.011 ug/I
0.010
0.0020 1 12/12/2018 07:49 TD
n
Ethene
0.019 ug/I
0.010
0.0030 1 12/12/2018 07:49 TD
n
Hydrogen
2.8 nM
1.0
0.65 1 12/12/2018 07:49 TD
n
Report ID: 28909 - 1127864 Page 15 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090011
Sample ID: MW7
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/5/2018 12:25
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
760 ug/I
0.10
0.023 1 12/12/2018 08:02 TD
n
Ethane
0.024 ug/I
0.010
0.0020 1 12/12/2018 08:02 TD
n
Ethene
0.017 ug/I
0.010
0.0030 1 12/12/2018 08:02 TD
n
Hydrogen
2.5 nM
1.0
0.65 1 12/12/2018 08:02 TD
n
Report ID: 28909 - 1127864 Page 16 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090012
Sample ID: MW8
Date Received: 12/6/2018 11:15 Matrix:
Date Collected: 12/5/2018 09:35
Bubble Strip
Parameters
Results Units
PQL
MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
2000 ug/I
0.10
0.023 1 12/12/2018 08:14 TD
n
Ethane
0.16 ug/I
0.010
0.0020 1 12/12/2018 08:14 TD
n
Ethene
0.00301.11 ug/I
0.010
0.0030 1 12/12/2018 08:14 TD
n
Hydrogen
3.0 nM
1.0
0.65 1 12/12/2018 08:14 TD
n
Report ID: 28909 - 1127864 Page 17 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090013
Sample ID: MW1S
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/4/2018 09:45
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/10/2018 22:09
KB
Acetic Acid
0.11 mg/I
0.10
0.024 1
12/10/2018 22:09
KB
B
Propionic Acid
0.055J mg/I
0.10
0.0044 1
12/10/2018 22:09
KB
B
Butyric Acid
0.014J mg/I
0.10
0.0047 1
12/10/2018 22:09
KB
B
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/10/2018 22:09
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/10/2018 22:09
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/10/2018 22:09
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/10/2018 22:09
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/10/2018 22:09
KB
Report ID: 28909 - 1127864 Page 18 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090014
Sample ID: MW1D
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/4/2018 15:45
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.020J mg/I
0.20
0.014 1
12/10/2018 23:05
KB
Acetic Acid
0.22 mg/I
0.10
0.024 1
12/10/2018 23:05
KB
B
Propionic Acid
0.060J mg/I
0.10
0.0044 1
12/10/2018 23:05
KB
B
Butyric Acid
0.012J mg/I
0.10
0.0047 1
12/10/2018 23:05
KB
B
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/10/2018 23:05
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/10/2018 23:05
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/10/2018 23:05
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/10/2018 23:05
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/10/2018 23:05
KB
Report ID: 28909 - 1127864 Page 19 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090015
Sample ID: MW2S
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/4/2018 15:20
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/11/201800:01
KB
Acetic Acid
0.15 mg/I
0.10
0.024 1
12/11/201800:01
KB
B
Propionic Acid
0.071J mg/I
0.10
0.0044 1
12/11/201800:01
KB
B
Butyric Acid
0.029J mg/I
0.10
0.0047 1
12/11/201800:01
KB
B
Pyruvic Acid
0.012J mg/I
0.10
0.0057 1
12/11/201800:01
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201800:01
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/11/201800:01
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 00:01
KB
Hexanoic Acid
0.017J mg/I
0.20
0.012 1
12/11/201800:01
KB
Report ID: 28909 - 1127864 Page 20 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090016
Sample ID: MW211)
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/4/2018 14:26
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.055J mg/I
0.20
0.014 1
12/11/201800:58
KB
Acetic Acid
0.13 mg/I
0.10
0.024 1
12/11/201800:58
KB
B
Propionic Acid
0.066J mg/I
0.10
0.0044 1
12/11/201800:58
KB
B
Butyric Acid
0.013J mg/I
0.10
0.0047 1
12/11/201800:58
KB
B
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/11/201800:58
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201800:58
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/11/201800:58
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 00:58
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/11/201800:58
KB
Report ID: 28909 - 1127864 Page 21 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090017
Sample ID: MW3S
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/4/2018 13:05
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/11/201801:54
KB
Acetic Acid
0.27 mg/I
0.10
0.024 1
12/11/201801:54
KB
B
Propionic Acid
0.11 mg/I
0.10
0.0044 1
12/11/201801:54
KB
B
Butyric Acid
0.0047U mg/I
0.10
0.0047 1
12/11/201801:54
KB
B
Pyruvic Acid
0.072J mg/I
0.10
0.0057 1
12/11/201801:54
KB
i-Pentanoic Acid
0.0097J mg/I
0.10
0.0075 1
12/11/201801:54
KB
Pentanoic Acid
0.033J mg/I
0.10
0.012 1
12/11/201801:54
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 01:54
KB
Hexanoic Acid
0.22 mg/I
0.20
0.012 1
12/11/201801:54
KB
Report ID: 28909 - 1127864 Page 22 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090018
Sample ID: MW311)
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/4/2018 12:10
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.027J mg/I
0.20
0.014 1
12/11/201802:50
KB
Acetic Acid
0.18 mg/I
0.10
0.024 1
12/11/201802:50
KB
B
Propionic Acid
0.086J mg/I
0.10
0.0044 1
12/11/201802:50
KB
B
Butyric Acid
0.013J mg/I
0.10
0.0047 1
12/11/201802:50
KB
B
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/11/201802:50
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201802:50
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/11/201802:50
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 02:50
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/11/201802:50
KB
Report ID: 28909 - 1127864 Page 23 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090019
Sample ID: MW3A
Date Received: 12/6/2018 11:15
Date Collected: 12/4/2018 11:10
Matrix: Water
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.058J mg/I
0.20
0.014 1
12/11/201803:47
KB
Acetic Acid
0.20 mg/I
0.10
0.024 1
12/11/201803:47
KB
B
Propionic Acid
0.12 mg/I
0.10
0.0044 1
12/11/201803:47
KB
B
Butyric Acid
0.079J mg/I
0.10
0.0047 1
12/11/201803:47
KB
B
Pyruvic Acid
0.057J mg/I
0.10
0.0057 1
12/11/201803:47
KB
i-Pentanoic Acid
0.011J mg/I
0.10
0.0075 1
12/11/201803:47
KB
Pentanoic Acid
0.030J mg/I
0.10
0.012 1
12/11/201803:47
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 03:47
KB
Hexanoic Acid
0.16J mg/I
0.20
0.012 1
12/11/201803:47
KB
Report ID: 28909 - 1127864 Page 24 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090020
Sample ID: MW4
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/5/2018 13:05
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/11/201804:43
KB
Acetic Acid
0.17 mg/I
0.10
0.024 1
12/11/201804:43
KB
B
Propionic Acid
0.081J mg/I
0.10
0.0044 1
12/11/201804:43
KB
B
Butyric Acid
0.013J mg/I
0.10
0.0047 1
12/11/201804:43
KB
B
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/11/201804:43
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201804:43
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/11/201804:43
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 04:43
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/11/201804:43
KB
Report ID: 28909 - 1127864 Page 25 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090021
Sample ID: MW5
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/5/2018 10:48
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/11/201805:40
KB
Acetic Acid
0.24 mg/I
0.10
0.024 1
12/11/201805:40
KB
B
Propionic Acid
0.089J mg/I
0.10
0.0044 1
12/11/201805:40
KB
B
Butyric Acid
0.020J mg/I
0.10
0.0047 1
12/11/201805:40
KB
B
Pyruvic Acid
0.0091J mg/I
0.10
0.0057 1
12/11/201805:40
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201805:40
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/11/201805:40
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 05:40
KB
Hexanoic Acid
0.028J mg/I
0.20
0.012 1
12/11/201805:40
KB
Report ID: 28909 - 1127864 Page 26 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090022
Sample ID: MW6
Date Received: 12/6/2018 11:15
Date Collected: 12/5/2018 11:35
Matrix: Water
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/11/201806:36
KB
Acetic Acid
0.23 mg/I
0.10
0.024 1
12/11/201806:36
KB
B
Propionic Acid
0.093J mg/I
0.10
0.0044 1
12/11/201806:36
KB
B
Butyric Acid
0.0080J mg/I
0.10
0.0047 1
12/11/201806:36
KB
B
Pyruvic Acid
0.016J mg/I
0.10
0.0057 1
12/11/201806:36
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201806:36
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/11/201806:36
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 06:36
KB
Hexanoic Acid
0.10J mg/I
0.20
0.012 1
12/11/201806:36
KB
Report ID: 28909 - 1127864 Page 27 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090023
Sample ID: MW7
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/5/2018 12:25
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/11/201807:33
KB
Acetic Acid
0.17 mg/I
0.10
0.024 1
12/11/201807:33
KB
B
Propionic Acid
0.080J mg/I
0.10
0.0044 1
12/11/201807:33
KB
B
Butyric Acid
0.52 mg/I
0.10
0.0047 1
12/11/201807:33
KB
B
Pyruvic Acid
0.036J mg/I
0.10
0.0057 1
12/11/201807:33
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201807:33
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/11/201807:33
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 07:33
KB
Hexanoic Acid
0.25 mg/I
0.20
0.012 1
12/11/201807:33
KB
Report ID: 28909 - 1127864 Page 28 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
I_1►F-1w,�I[IllfnT1111110*411>MiV
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090024
Sample ID: MW8
Date Received: 12/6/2018 11:15 Matrix: Water
Date Collected: 12/5/2018 09:35
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.014U mg/I
0.20
0.014 1
12/11/201808:29
KB
Acetic Acid
0.20 mg/I
0.10
0.024 1
12/11/201808:29
KB
B
Propionic Acid
0.089J mg/I
0.10
0.0044 1
12/11/201808:29
KB
B
Butyric Acid
0.92 mg/I
0.10
0.0047 1
12/11/201808:29
KB
B
Pyruvic Acid
0.057J mg/I
0.10
0.0057 1
12/11/201808:29
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/11/201808:29
KB
Pentanoic Acid
0.026J mg/I
0.10
0.012 1
12/11/201808:29
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/11 /2018 08:29
KB
Hexanoic Acid
0.18J mg/I
0.20
0.012 1
12/11/201808:29
KB
Report ID: 28909 - 1127864 Page 29 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090025
Sample ID: MW9A
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/12/2018 09:40
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
30 ug/I
0.10
0.023 1
12/21/201811:56
MM
n
Ethane
0.012 ug/I
0.010
0.0020 1
12/21/201811:56
MM
n
Ethene
0.0038J ug/I
0.010
0.0030 1
12/21/201811:56
MM
n
Hydrogen
2.9 nM
1.0
0.65 1
12/21/201811:56
MM
n
Report ID: 28909 - 1127864 Page 30 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090026
Sample ID: MW10
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/12/2018 10:35
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
6400 ug/I
0.10
0.023 1
12/21/201812:09
MM
n
Ethane
0.060 ug/I
0.010
0.0020 1
12/21/201812:09
MM
n
Ethene
0.16 ug/I
0.010
0.0030 1
12/21/201812:09
MM
n
Hydrogen
2.6 nM
1.0
0.65 1
12/21/201812:09
MM
n
Report ID: 28909 - 1127864 Page 31 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090027
Sample ID: MW11
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/12/2018 11:40
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
140 ug/I
0.10
0.023 1
12/21/201812:31
MM
n
Ethane
0.012 ug/I
0.010
0.0020 1
12/21/201812:31
MM
n
Ethene
0.045 ug/I
0.010
0.0030 1
12/21/201812:31
MM
n
Hydrogen
3.2 nM
1.0
0.65 1
12/21/201812:31
MM
n
Report ID: 28909 - 1127864 Page 32 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090028
Sample ID: W12S
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/12/2018 12:45
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
920 ug/I
0.10
0.023 1
12/21/201812:46
MM
n
Ethane
0.026 ug/I
0.010
0.0020 1
12/21/201812:46
MM
n
Ethene
0.15 ug/I
0.010
0.0030 1
12/21/201812:46
MM
n
Hydrogen
3.4 nM
1.0
0.65 1
12/21/201812:46
MM
n
Report ID: 28909 - 1127864 Page 33 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090029
Sample ID: MW13
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/12/2018 13:45
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
200 ug/I
0.10
0.023 1
12/21/201812:58
MM
n
Ethane
0.0032J ug/I
0.010
0.0020 1
12/21/201812:58
MM
n
Ethene
0.0068J ug/I
0.010
0.0030 1
12/21/201812:58
MM
n
Hydrogen
3.0 nM
1.0
0.65 1
12/21/201812:58
MM
n
Report ID: 28909 - 1127864 Page 34 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090030
Sample ID: W14S
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/13/2018 09:45
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
170 ug/I
0.10
0.023 1
12/21/201813:11
MM
n
Ethane
0.0037J ug/I
0.010
0.0020 1
12/21/201813:11
MM
n
Ethene
0.011 ug/I
0.010
0.0030 1
12/21/201813:11
MM
n
Hydrogen
2.9 nM
1.0
0.65 1
12/21/201813:11
MM
n
Report ID: 28909 - 1127864 Page 35 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090031
Sample ID: W14D
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/13/2018 10:35
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
8.8 ug/I
0.10
0.023 1
12/21/201813:23
MM
n
Ethane
0.015 ug/I
0.010
0.0020 1
12/21/201813:23
MM
n
Ethene
0.0085J ug/I
0.010
0.0030 1
12/21/201813:23
MM
n
Hydrogen
3.0 nM
1.0
0.65 1
12/21/201813:23
MM
n
Report ID: 28909 - 1127864 Page 36 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090032
Sample ID: MW15
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/13/2018 11:40
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
460 ug/I
0.10
0.023 1
12/21/201813:40
MM
n
Ethane
0.014 ug/I
0.010
0.0020 1
12/21/201813:40
MM
n
Ethene
0.0047J ug/I
0.010
0.0030 1
12/21/201813:40
MM
n
Hydrogen
3.0 nM
1.0
0.65 1
12/21/201813:40
MM
n
Report ID: 28909 - 1127864 Page 37 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090033
Sample ID: MW16
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/13/2018 12:40
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
650 ug/I
0.10
0.023 1
12/21/201813:52
MM
n
Ethane
0.011 ug/I
0.010
0.0020 1
12/21/201813:52
MM
n
Ethene
0.0074J ug/I
0.010
0.0030 1
12/21/201813:52
MM
n
Hydrogen
3.3 nM
1.0
0.65 1
12/21/201813:52
MM
n
Report ID: 28909 - 1127864 Page 38 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090034
Sample ID: MW17
Date Received: 12/14/2018 11:30 Matrix:
Date Collected: 12/13/2018 13:40
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
120 ug/I
0.10
0.023 1
12/21/201814:05
MM
n
Ethane
0.013 ug/I
0.010
0.0020 1
12/21/201814:05
MM
n
Ethene
0.0038J ug/I
0.010
0.0030 1
12/21/201814:05
MM
n
Hydrogen
3.1 nM
1.0
0.65 1
12/21/201814:05
MM
n
Report ID: 28909 - 1127864 Page 39 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090035
Sample ID: MW9A
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/12/2018 09:40
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.032J mg/I
0.20
0.014 1
12/21/2018 21:28
KB
Acetic Acid
0.045J mg/I
0.10
0.024 1
12/21/2018 21:28
KB
Propionic Acid
0.0055J mg/I
0.10
0.0044 1
12/21/2018 21:28
KB
Butyric Acid
0.0047U mg/I
0.10
0.0047 1
12/21/2018 21:28
KB
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/21/2018 21:28
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/21/2018 21:28
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/21/2018 21:28
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/21/2018 21:28
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/21/2018 21:28
KB
Report ID: 28909 - 1127864 Page 40 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090036
Sample ID: MW10
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/12/2018 10:35
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.095J mg/I
0.20
0.014 1
12/22/2018 00:17
KB
Acetic Acid
0.024U mg/I
0.10
0.024 1
12/22/2018 00:17
KB
Propionic Acid
0.011J mg/I
0.10
0.0044 1
12/22/2018 00:17
KB
Butyric Acid
0.38 mg/I
0.10
0.0047 1
12/22/2018 00:17
KB
Pyruvic Acid
0.13 mg/I
0.10
0.0057 1
12/22/2018 00:17
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 00:17
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 00:17
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 00:17
KB
Hexanoic Acid
0.25 mg/I
0.20
0.012 1
12/22/2018 00:17
KB
Report ID: 28909 - 1127864 Page 41 of 59
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without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090037
Sample ID: MW11
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/12/2018 11:40
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.019J mg/I
0.20
0.014 1
12/22/2018 01:14
KB
Acetic Acid
0.045J mg/I
0.10
0.024 1
12/22/2018 01:14
KB
Propionic Acid
0.0044U mg/I
0.10
0.0044 1
12/22/2018 01:14
KB
Butyric Acid
0.0047U mg/I
0.10
0.0047 1
12/22/2018 01:14
KB
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/22/2018 01:14
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 01:14
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 01:14
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 01:14
KB
Hexanoic Acid
0.024J mg/I
0.20
0.012 1
12/22/2018 01:14
KB
Report ID: 28909 - 1127864 Page 42 of 59
F` CERTIFICATE OF ANALYSIS
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lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090038
Sample ID: W12S
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/12/2018 12:45
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.099J mg/I
0.20
0.014 1
12/22/2018 02:11
KB
Acetic Acid
0.13 mg/I
0.10
0.024 1
12/22/2018 02:11
KB
Propionic Acid
0.021J mg/I
0.10
0.0044 1
12/22/2018 02:11
KB
Butyric Acid
0.66 mg/I
0.10
0.0047 1
12/22/2018 02:11
KB
Pyruvic Acid
0.14 mg/I
0.10
0.0057 1
12/22/2018 02:11
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 02:11
KB
Pentanoic Acid
0.060J mg/I
0.10
0.012 1
12/22/2018 02:11
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 02:11
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/22/2018 02:11
KB
Report ID: 28909 - 1127864 Page 43 of 59
F` CERTIFICATE OF ANALYSIS
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without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090039
Sample ID: MW13
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/12/2018 13:45
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.017J mg/I
0.20
0.014 1
12/22/2018 03:08
KB
Acetic Acid
0.046J mg/I
0.10
0.024 1
12/22/2018 03:08
KB
Propionic Acid
0.0058J mg/I
0.10
0.0044 1
12/22/2018 03:08
KB
Butyric Acid
0.0047U mg/I
0.10
0.0047 1
12/22/2018 03:08
KB
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/22/2018 03:08
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 03:08
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 03:08
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 03:08
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/22/2018 03:08
KB
Report ID: 28909 - 1127864 Page 44 of 59
F` CERTIFICATE OF ANALYSIS
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without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090040
Sample ID: W14S
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/13/2018 09:45
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.018J mg/I
0.20
0.014 1
12/22/2018 04:04
KB
Acetic Acid
0.052J mg/I
0.10
0.024 1
12/22/2018 04:04
KB
Propionic Acid
0.0044U mg/I
0.10
0.0044 1
12/22/2018 04:04
KB
Butyric Acid
0.0047U mg/I
0.10
0.0047 1
12/22/2018 04:04
KB
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/22/2018 04:04
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 04:04
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 04:04
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 04:04
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/22/2018 04:04
KB
Report ID: 28909 - 1127864 Page 45 of 59
F` CERTIFICATE OF ANALYSIS
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without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090041
Sample ID: W14D
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/13/2018 10:35
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.052J mg/I
0.20
0.014 1
12/22/2018 05:01
KB
Acetic Acid
0.042J mg/I
0.10
0.024 1
12/22/2018 05:01
KB
Propionic Acid
0.0044U mg/I
0.10
0.0044 1
12/22/2018 05:01
KB
Butyric Acid
0.0047U mg/I
0.10
0.0047 1
12/22/2018 05:01
KB
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/22/2018 05:01
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 05:01
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 05:01
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 05:01
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/22/2018 05:01
KB
Report ID: 28909 - 1127864 Page 46 of 59
F` CERTIFICATE OF ANALYSIS
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without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090042
Sample ID: MW15
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/13/2018 11:35
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.031J mg/I
0.20
0.014 1
12/22/2018 05:57
KB
Acetic Acid
0.037J mg/I
0.10
0.024 1
12/22/2018 05:57
KB
Propionic Acid
0.0044U mg/I
0.10
0.0044 1
12/22/2018 05:57
KB
Butyric Acid
0.018J mg/I
0.10
0.0047 1
12/22/2018 05:57
KB
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/22/2018 05:57
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 05:57
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 05:57
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 05:57
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/22/2018 05:57
KB
Report ID: 28909 - 1127864 Page 47 of 59
F` CERTIFICATE OF ANALYSIS
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without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090043
Sample ID: MW16
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/13/2018 12:40
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.027J mg/I
0.20
0.014 1
12/22/2018 06:54
KB
Acetic Acid
0.044J mg/I
0.10
0.024 1
12/22/2018 06:54
KB
Propionic Acid
0.0044U mg/I
0.10
0.0044 1
12/22/2018 06:54
KB
Butyric Acid
0.024J mg/I
0.10
0.0047 1
12/22/2018 06:54
KB
Pyruvic Acid
0.0065J mg/I
0.10
0.0057 1
12/22/2018 06:54
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 06:54
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 06:54
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 06:54
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/22/2018 06:54
KB
Report ID: 28909 - 1127864 Page 48 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

lacmnalyficalo
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 289090044
Sample ID: MW17
Date Received: 12/14/2018 11:30 Matrix: Water
Date Collected: 12/13/2018 13:40
Parameters
Results Units
PQL
MDL DF
Analyzed
By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.018J mg/I
0.20
0.014 1
12/22/2018 07:50
KB
Acetic Acid
0.032J mg/I
0.10
0.024 1
12/22/2018 07:50
KB
Propionic Acid
0.0044U mg/I
0.10
0.0044 1
12/22/2018 07:50
KB
Butyric Acid
0.0047U mg/I
0.10
0.0047 1
12/22/2018 07:50
KB
Pyruvic Acid
0.0057U mg/I
0.10
0.0057 1
12/22/2018 07:50
KB
i-Pentanoic Acid
0.0075U mg/I
0.10
0.0075 1
12/22/2018 07:50
KB
Pentanoic Acid
0.012U mg/I
0.10
0.012 1
12/22/2018 07:50
KB
i-Hexanoic Acid
0.0049U mg/I
0.20
0.0049 1
12/22/2018 07:50
KB
Hexanoic Acid
0.012U mg/I
0.20
0.012 1
12/22/2018 07:50
KB
Report ID: 28909 - 1127864 Page 49 of 59
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ANALYTICAL RESULTS QUALIFIERS
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
DEFINITIONS/QUALIFIERS
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
ND Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
U Indicates the compound was analyzed for, but not detected at or above the noted concentration.
J Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL).
n The laboratory does not hold NELAP/TNI accreditation for this method or analyte.
B The analyte was detected in the associated blank.
Report ID: 28909 - 1127864
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Page 50 of 59

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QUALITY CONTROL DATA
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QC Batch: EDON/3951
Analysis Method:
AM23G
QC Batch Method: AM23G
Associated Lab Samples:
289090013, 289090014, 289090015, 289090016, 289090017, 289090018,
289090019,
289090020, 289090021,
289090022,289090023,289090024
METHOD BLANK: 58854
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
EDonors
Lactic Acid
mg/I
0.014U
0.014
Acetic Acid
mg/I
0.13
0.024 B
Propionic Acid
mg/I
0.066J
0.0044 B
Butyric Acid
mg/I
0.0089J
0.0047 B
Pyruvic Acid
mg/I
0.0057U
0.0057
i-Pentanoic Acid
mg/I
0.0075U
0.0075
Pentanoic Acid
mg/I
0.012U
0.012
i-Hexanoic Acid
mg/I
0.0049U
0.0049
Hexanoic Acid
mg/I
0.012U
0.012
LABORATORY CONTROL SAMPLE:
58855
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result %
Rec
Limits
Qualifiers
EDonors
Lactic Acid
mg/I
2
2.2
108
70-130
Acetic Acid
mg/I
2
2.3
116
70-130
B
Propionic Acid
mg/I
2
2.1
105
70-130
B
Butyric Acid
mg/I
2
2.0
102
70-130
B
Pyruvic Acid
mg/I
2
1.8
88
70-130
i-Pentanoic Acid
mg/I
2
2.0
99
70-130
Pentanoic Acid
mg/I
2
2.0
99
70-130
i-Hexanoic Acid
mg/I
2
1.9
95
70-130
Hexanoic Acid
mg/I
2
1.9
94
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 58856
58857
Original:
289050001
Original Spike
MS MSD
MS
MSD
% Rec Max
Parameter
Units
Result Conc.
Result Result
% Rec
% Rec
Limit RPD RPD
Qualifiers
EDonors
Lactic Acid
mg/I
0.072 20
21 22
107
109
70-130 2.1 30
d
Acetic Acid
mg/I
1.8 20
24 24
113
109
70-130 3.2 30
d,B
Report ID: 28909 - 1127864
Page 51 of 59
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in full,
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of Pace Analytical Energy Services LLC.

lacmnalyficalo
QUALITY CONTROL DATA
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
58856
58857
Original:
289050001
Original
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Result
Result
% Rec
% Rec
Limit
RPD
RPD
Qualifiers
Propionic Acid
mg/I
0.75
20
23
22
112
109
70-130
2.9
30
d,B
Butyric Acid
mg/I
0.16
20
23
22
114
110
70-130
3.8
30
d,B
Pyruvic Acid
mg/I
0
20
20
20
99
99
70-130
0.33
30
d
i-Pentanoic Acid
mg/I
0
20
23
22
113
108
70-130
4.7
30
d
Pentanoic Acid
mg/I
0
20
24
22
120
111
70-130
7.3
30
d
i-Hexanoic Acid
mg/I
0
20
24
22
120
111
70-130
7.7
30
d
Hexanoic Acid
mg/I
0
20
25
23
127
117
70-130
8.4
30
d
Report ID: 28909 - 1127864 Page 52 of 59
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laceAnalytical
220 William Pitt Way
o
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Workorder: 28909 JUDSON WHITEHURST / 6003
QC Batch: DISG/7267
Analysis Method:
AM20GAX
QC Batch Method: AM20GAX
Associated Lab Samples: 289090001, 289090002,
289090003, 289090004,
289090005, 289090006, 289090007,
289090008, 289090009,
289090010,289090011,289090012
METHOD BLANK: 58925
Blank
Reporting
Parameter Units
Result
Limit Qualifiers
RISK
Methane ug/I
0.023U
0.023 n
Ethane ug/I
0.0020U
0.0020 n
Ethene ug/I
0.0030U
0.0030 n
METHOD BLANK: 58927
Blank
Reporting
Parameter Units
Result
Limit Qualifiers
RISK
Hydrogen nM
0.65U
0.65 n
LABORATORY CONTROL SAMPLE & LCSD:
58928
58931
Spike LCS
LCSD LCS
LCSD
% Rec
Max
Parameter Units
Conc. Result
Result % Rec
% Rec
Limit
RPD
RPD
Qualifiers
RISK
Methane ug/I
8.1 7.9
7.7 97
95
80-120
2.2
20
n
Ethane ug/I
6.4 6.2
6.1 98
96
80-120
2.2
20
n
Ethene ug/I
16 16
16 99
97
80-120
2.2
20
n
LABORATORY CONTROL SAMPLE & LCSD:
58930
58933
Spike LCS
LCSD LCS
LCSD
% Rec
Max
Parameter Units
Conc. Result
Result % Rec
% Rec
Limit
RPD
RPD
Qualifiers
RISK
Hydrogen nM
24 24
24 100
101
80-120
0.5
20
n
Report ID: 28909 - 1127864
.4r-tielac�,
CERTIFICATE OF ANALYSIS
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Page 53 of 59

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QUALITY CONTROL DATA
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QC Batch: EDON/3959
Analysis Method:
AM23G
QC Batch Method: AM23G
Associated Lab Samples:
289090035, 289090036, 289090037, 289090038, 289090039, 289090040,
289090041,
289090042, 289090043,
289090044
METHOD BLANK: 59094
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
EDonors
Lactic Acid
mg/I
0.014U
0.014
Acetic Acid
mg/I
0.024U
0.024
Propionic Acid
mg/I
0.0044U
0.0044
Butyric Acid
mg/I
0.0047U
0.0047
Pyruvic Acid
mg/I
0.0057U
0.0057
i-Pentanoic Acid
mg/I
0.0075U
0.0075
Pentanoic Acid
mg/I
0.012U
0.012
i-Hexanoic Acid
mg/I
0.0049U
0.0049
Hexanoic Acid
mg/I
0.012U
0.012
LABORATORY CONTROL SAMPLE: 59095
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result %
Rec
Limits
Qualifiers
EDonors
Lactic Acid
mg/I
2
2.2
112
70-130
Acetic Acid
mg/I
2
2.1
106
70-130
Propionic Acid
mg/I
2
2.1
105
70-130
Butyric Acid
mg/I
2
2.1
106
70-130
Pyruvic Acid
mg/I
2
2.0
101
70-130
i-Pentanoic Acid
mg/I
2
2.0
103
70-130
Pentanoic Acid
mg/I
2
2.1
106
70-130
i-Hexanoic Acid
mg/I
2
2.0
102
70-130
Hexanoic Acid
mg/I
2
2.1
103
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 59096
59097
Original:
289090035
Original Spike
MS MSD
MS
MSD
% Rec Max
Parameter
Units
Result Conc.
Result Result
% Rec
% Rec
Limit RPD RPD Qualifiers
EDonors
Lactic Acid
mg/I
0.032 2
2.2 2.3
111
112
70-130 1.1 30
Acetic Acid
mg/I
0.045 2
2.2 2.2
106
107
70-130 0.58 30
Report ID: 28909 - 1127864
Page 54 of 59
F`
CERTIFICATE OF ANALYSIS
"`~
This report shall
not be reproduced, except
in full,
without the written consent
of Pace Analytical Energy Services LLC.

lacmnalyficalo
QUALITY CONTROL DATA
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
59096
59097
Original:
289090035
Original
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Cone.
Result
Result
% Rec
% Rec
Limit
RPD
RPD Qualifiers
Propionic Acid
mg/I
0.0055
2
2.2
2.2
110
109
70-130
0.87
30
Butyric Acid
mg/I
0.0042
2
2.2
2.2
112
111
70-130
1.1
30
Pyruvic Acid
mg/I
0
2
2.0
2.0
103
103
70-130
0.03
30
i-Pentanoic Acid
mg/I
0
2
2.2
2.2
111
108
70-130
2.5
30
Pentanoic Acid
mg/I
0
2
2.3
2.3
117
115
70-130
1.6
30
i-Hexanoic Acid
mg/I
0
2
2.3
2.2
116
113
70-130
2.7
30
Hexanoic Acid
mg/I
0
2
2.4
2.4
122
119
70-130
2.2
30
Report ID: 28909 - 1127864 Page 55 of 59
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

Pace Analytical Energy Services LLC
laceAnalytical
220 William Pitt Way
o
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Workorder: 28909 JUDSON WHITEHURST / 6003
QC Batch: DISG/7293
Analysis Method:
AM20GAX
QC Batch Method: AM20GAX
Associated Lab Samples: 289090025, 289090026,
289090027, 289090028, 289090029, 289090030, 289090031,
289090032, 289090033,
289090034
METHOD BLANK: 59144
Blank
Reporting
Parameter Units
Result
Limit Qualifiers
RISK
Methane ug/I
0.023U
0.023 n
Ethane ug/I
0.0020U
0.0020 n
Ethene ug/I
0.0030U
0.0030 n
METHOD BLANK: 59145
Blank
Reporting
Parameter Units
Result
Limit Qualifiers
RISK
Hydrogen nM
0.65U
0.65 n
LABORATORY CONTROL SAMPLE & LCSD:
59146
59148
Spike
LCS LCSD LCS
LCSD
% Rec
Max
Parameter Units
Conc. Result Result % Rec
% Rec
Limit
RPD
RPD
Qualifiers
RISK
Methane ug/I
8.1
8.4 8.5 104
105
80-120
0.86
20
n
Ethane ug/I
6.4
6.7 6.7 105
105
80-120
0.82
20
n
Ethene ug/I
16
17 17 106
106
80-120
0.61
20
n
LABORATORY CONTROL SAMPLE & LCSD:
59147
59149
Spike
LCS LCSD LCS
LCSD
% Rec
Max
Parameter Units
Conc. Result Result % Rec
% Rec
Limit
RPD
RPD
Qualifiers
RISK
Hydrogen nM
24
24 24 99
100
80-120
1.8
20
n
Report ID: 28909 - 1127864
.4r-tielac�,
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 56 of 59

lacmnalyficalo
QUALITY CONTROL DATA QUALIFIERS
Workorder: 28909 JUDSON WHITEHURST / 6003
QUALITY CONTROL PARAMETER QUALIFIERS
The analyte was detected in the associated blank.
The analyte concentration was determined from a dilution.
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Page 57 of 59

lacmnalyficalo
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Prep Method Prep Batch Analysis Method
Analysis
Batch
289090013
MW1S
AM23G
EDON/3951
289090014
MW1D
AM23G
EDON/3951
289090015
MW2S
AM23G
EDON/3951
289090016
MW2D
AM23G
EDON/3951
289090017
MW3S
AM23G
EDON/3951
289090018
MW3D
AM23G
EDON/3951
289090019
MW3A
AM23G
EDON/3951
289090020
MW4
AM23G
EDON/3951
289090021
MW5
AM23G
EDON/3951
289090022
MW6
AM23G
EDON/3951
289090023
MW7
AM23G
EDON/3951
289090024
MW8
AM23G
EDON/3951
289090001
MW1S
AM20GAX
DISG/7267
289090002
MW1D
AM20GAX
DISG/7267
289090003
MW2S
AM20GAX
DISG/7267
289090004
MW2D
AM20GAX
DISG/7267
289090005
MW3S
AM20GAX
DISG/7267
289090006
MW3D
AM20GAX
DISG/7267
289090007
MW3A
AM20GAX
DISG/7267
289090008
MW4
AM20GAX
DISG/7267
289090009
MW5
AM20GAX
DISG/7267
289090010
MW6
AM20GAX
DISG/7267
289090011
MW7
AM20GAX
DISG/7267
289090012
MW8
AM20GAX
DISG/7267
289090035
MW9A
AM23G
EDON/3959
289090036
MW10
AM23G
EDON/3959
289090037
MW11
AM23G
EDON/3959
289090038
W12S
AM23G
EDON/3959
289090039
MW13
AM23G
EDON/3959
289090040
W14S
AM23G
EDON/3959
289090041
W14D
AM23G
EDON/3959
289090042
MW15
AM23G
EDON/3959
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 58 of 59

lacmnalyficalo
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Workorder: 28909 JUDSON WHITEHURST / 6003
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Prep Method Prep Batch Analysis Method
Analysis
Batch
289090043
MW16
AM23G
EDON/3959
289090044
MW17
AM23G
EDON/3959
289090025
MW9A
AM20GAX
DISG/7293
289090026
MW10
AM20GAX
DISG/7293
289090027
MW11
AM20GAX
DISG/7293
289090028
W12S
AM20GAX
DISG/7293
289090029
MW13
AM20GAX
DISG/7293
289090030
W14S
AM20GAX
DISG/7293
289090031
W14D
AM20GAX
DISG/7293
289090032
MW15
AM20GAX
DISG/7293
289090033
MW16
AM20GAX
DISG/7293
289090034
MW17
AM20GAX
DISG/7293
Report ID: 28909 - 1127864
F` CERTIFICATE OF ANALYSIS
"`~ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 59 of 59

a
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CHent Name:
40 e ct
A. Shipping/Container Information (circle appropriate response}
Courier: Fed Ex
W
LabWork Order:
UPS USPS Client Other: Air bill Present: Yes No
Custody Seal on Coolerj�ox Present: Yes
Cooler/Box Packing Material: Kbble Wrap
T�rpe of Ice: et ��� B I u e Non e
Coo%AI
Comrr�ents:
No Seals Intact:
Absorbent Foam
. Ice Intact: Yes Melted
s
Padiation Screened: Yeso
B. Laboratory Assignment/Lbg-in (check appropriate response)
Other:
YesF No
Comments.
YES
NO
N/A
Comment
Reference non -Conformance
Chain of Custody properly filled out
Chain of Custody relinquished
�ry
Sampler Name & Signature on COC
"Containers intact i
¢
Were samples in separate bags
Sample container labels match COCp
Sample name/date and time collected
Sufficient volume provided
PAES containers used
Are containers properly preserved for the requested testing?
(as labeled)
V�
It
If an unknown preservation state, were containers checked?
If yes, see pH form.
Exception: vOA's coliform
r
Was volume for dissolved testing field filtered, as noted on
the COC? Was volume received in a preserved container?
Headspace present?
Cooler contents examined/received b� : ��� � ��� date: F ���. � �� ��
•
Project Manager Review. Date .
Q�009-rev.01., 3 Oct2� 17

Clrent Name:
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Courser: Fed Ex UPS r' CUSPS
:
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'Op wofto
Cooler/C ox Packing Material. Babble Wra
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Type of Cce: Wet B(ue� None
Cooler Temperature:_
Comments:
Air hill Present:
Flo Seals intact:
Absorbent Foam
Cce intact: Yes
radiation Screened:
lVE e lted
Laboratory Assignment/Log-in (check appropriate response)
Yes
No
Other:
u�
r order:
Gain of Custody Present:
No
Comments.
YES
NO
N/A
Comment
Reference non -Conformance
Chain of Custody properly filled out
Chain of Custody relinquished
Sampler Name N Signature on COC
,Containers intact
�
Were samples in separate bags
Sample container labels match COCX
Sample name/date and time collected
}
Sufficient volume provided
PAES containers used
Are containers properly preserved for the requested testing?
r.
(as labeled)
If an unknown preservation state, were containers checked?
.
If yes, see pH form.
Exception: VOA's coliform
Was volume for dissolved testing field filtered, as noted on
the COC? Was volume received in a preserved container?
l-leadspace present?
Cooler contents exarninedf recei�red h� : ©ate: � : ` �hf& t
Project (tanager Review : � A date: lf)�v
F-P.A..E-C2-0Q9-rev.01, 3 act.2017

Water Quality Monitoring Report
December 2018 Semiannual Sampling Event
Wood Project No. 6468-19-9035
Attachment B
Historical Data for Selected Analytes
wood.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Antimony CAS No. 7440-36-0
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
SW Std
MW-1D
MW-Is
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
1*
5300
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Nov-2007
NS
0.05 U
NS
0.41
0.05 U
0.11
0.05 U
0.05 U
0.2 J
0.05 U
0.05 U
Dry
0.05 U
0.05 U
May-2008
0.2 J
0.44 U
0.44 U
0.44 U
0.11
0.44 U
0.11
0.51
0.2 J
0.2 J
0.11
0.2 J
0.44 U
0.44 U
Nov-2008
NS
0.11
NS
0.11
0.05 U
0.11
0.11
0.11
0.2 1
0.11
0.05 U
Dry
0.61
0.11
May-2009
NS
0.11
0.061
0.11
0.06 J
0.06 J
0.7 J
0.2 J
0.11
0.06 J
0.06 J
0.11
0.061
0.06 J
Aug-2009
NS
NS
NS
NS
NS
2.95 U
2.95 U
NS
NS
NS
NS
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
2.95 U
NS
NS
NS
Jan-2010
NS
0.06 J
NS
0.11
NS
0.06 J
0.061
0.06 J
0.50
0.06 J
0.06 J
0.06 J
0.4 J
0.06 J
0.06 J
0.06 J
0.06 J
0.11
0.2 J
0.3 J
0.11
0.11
0.6 J
0.2 J
May-2010
NS
0.22 U
NS
0.7 1
NS
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.7 J
0.22 U
0.22 U
NS
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
Nov-2010
NS
0.22 U
NS
0.22 U
NS
0.22 U
0.22 U
0.22 U
0.6 J
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
0.8 J
0.22 U
NS
0.22 U
0.22 U
0.22 U
0.22 U
0.22 U
May-2011
NS
0.191
NS
0.14U
NS
0.14U
0.14U
0.14U
0.4J
0.14U
0.14U
0.14U
0.14U
0.14U
0.14U
0.47J
0.14U
NS
0.14U
0.14U
0.2J
0.14U
0.29J
Nov-2011
Damaged
0.14U
0.14U
0.14U
0.14U
0.14U
0.14U
0.14U
0.55J
0.14U
0.14U
0.14U
0.14U
0.14U
0.14U
0.51J
0.14U
0.14U
0.14U
0.14U
0.14U
0.14U
0.14U
May-2012
NS
0.121
NS
0.121
NS
0.27 J
0.101
0.15 J
0.36 J
0.17J
0.161
0.13 J
0.03 1
0.04 J
0.061
0.24 J
0.101
NS
0.341
0.131
0.091
0.05 J
0.04 J
Nov-2012
Damaged
0.14 J
0.11
0.28 J
0.17 J
0.16 J
0.501
0.14 J
0.51
0.07 J
0.15 J
0.16 J
0.06 J
0.09 J
0.08 J
0.3 J
0.101
0.91
0.14 J
0.02 U
0.02 U
0.02 U
0.02 U
May-2013
Damaged
0.071
0.04 J
0.091
0.031
0.02 U
0.071
0.02 U
0.341
0.07 J
0.02 U
0.14 J
0.041
0.04 J
0.051
0.18 J
0.031
0.4 J
0.151
0.141
0.04 J
0.031
Dry
May-2014
NS
0.191
NS
0.02 U
NS
0.02 U
0.03 J
0.02 U
0.34 J
0.02 U
0.12 J
0.07 J
0.02 U
0.02 U
0.02 U
0.10 J
0.02 U
NS
0.17 J
0.02 U
0.02 U
0.02 U
Dry
Nov-2014
NS
16
NS
0.16 J
NS
0.14 J
0.12 U
0.78 J
Damaged
0.18 J
0.22 J
0.20 J
0.12 U
0.241
0.24 J
0.34 J
0.12 U
NS
0.211
0.12 U
0.12 U
0.46 J
Dry
May-2015
0.57 J
0.26 J
0.21 J
0.03 J
0.05 J
0.06 J
0.02 U
0.23 J
0.52 J
0.08 J
0.22 J
0.111
0.02 U
0.02 U
0.02 U
0.70 J
0.02 U
0.06 J
0.18 J
0.65 J
0.18 J
0.06 J
0.04 J
Nov-2015
NS
0.951
NS
0.15 J
NS
0.16 J
0.24 J
0.19 J
1.4 J
0.24 J
0.271
0.32 J
0.201
0.17 J
0.121
0.14 J
0.16 J
NS
0.12 J
0.101
0.091
0.061
0.86 J
May-2016
NS
0.56 J
NS
0.05 U
NS
0.101
0.05 U
0.05 U
Dry
0.12 J
0.13 J
0.12 J
0.05 U
0.27 J
0.05 U
0.26 J
0.12 J
NS
0.12 J
0.05 U
0.091
0.05 U
0.05 U
Nov-2016
NS
0.451
NS
0.07 J
NS
0.191
0.111
0.05 U
Dry
0.08 J
0.12 J
0.24 J
0.05 U
0.21 J
0.05 U
0.28 J
0.111
NS
0.081
0.05 U
0.05 U
0.06 J
Dry
May-2017
0.3J
0.66 J
0.081
0.081
0.06U
0.151
0.191
0.06U
0.44 J
0.06U
0.08 J
0.19 J
0.06U
0.31 J
0.07 J
0.29 J
0.16 J
0.091
0.14 J
0.101
0.06U
0.06U
0.06U
0.06U
0.06U
Dec-2017
0.261
0.371
0.06 U
0.171
0.06 U
0.191
0.2 J
0.06 J
0.691
0.11 J
0.12 J
0.26 J
0.1 J
0.15 J
0.071
0.25 J
0.131
0.08 J
0.111
0.081
0.14 J
0.091
Dry
0.06 U
0.06 U
0.07 J
Jun-2018
0.08J
0.41J
0.04J
0.07J
0.07J
0.21J
0.06J
0.07J
0.18J
0.08J
0.06J
0.09J
0.04J
0.12J
0.1J
0.18J
0.13J
0.03U
0.03U
0.04J
0.04J
0.04J
Dry
0.07J
0.05J
Dry
Dec-2018
0.111
0.52 J
0.03 U
0.161
0.041
0.28 J
0.2 J
0.08 J
0.18 J
0.191
0.17 J
1 0.221
0.11
0.03 U
0.061
0.17 J
0.131
0.04 J
0.061
0.051
0.05 J
0.041
0.171
0.04 J
0.051
0.04 J
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3. * = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Arsenic CAS No. 7440-38-2
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPs
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
10
10
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
13
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
6.4 J
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
14
3.6
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
22
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
5.3
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
51
ND
ND
ND
ND
ND
ND
May-07
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
Nov-2007
NS
0.47 U
NS
4.2 1
0.6 J
6.71
1.3 1
5.3 J
16
6.4 J
0.47 U
Dry
2.01
0.51
May-2008
0.3J
0.51
0.4J
1.3J
7.3J
0.4J
1.01
5.01
5.3J
3.6J
4.51
11
1.11
0.11
Nov-2008
NS
1.11
NS
5.61
0.2 J
8.41
0.3 1
2.1 J
11
3.3 J
2.7 J
Dry
5.31
0.91
May-2009
NS
1.81
1.2 J
2.2 1
0.51
7.01
2.81
1.3 J
2.91
1.01
1.61
6.3 J
1.4 J
0.81
Aug-2009
NS
NS
NS
NS
NS
6.4 J
4.9 U
NS
NS
NS
NS
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
4.9 U
NS
NS
NS
Jan-2010
NS
2.1J
NS
0.8J
NS
6.8J
2.6J
2.8J
5.81
6.4J
0.51
4.01
1.3J
0.51
0.17U
0.17U
2.4J
0.21
1.31
3.6J
3.9J
0.3J
0.17U
0.21
May-2010
NS
0.71
NS
1.71
NS
9.21
1.01
2.61
3.91
6.11
4.51
7.5 1
0.3 J
0.5 1
0.04 U
0.4 J
1.4 J
NS
0.04 U
0.91
1.31
0.4 J
0.61
Nov-2010
NS
1.91
NS
5.6J
NS
0.04U
5.4J
2.3J
0.04U
4.8J
0.91
4.0J
0.6J
1.11
0.6J
5.31
1.81
NS
1.6J
2J
1.11
0.6J
0.51
May-2011
NS
0.361
NS
3.11
NS
3.81
0.931
1.61
6.4 J
2.21
1.5 J
3.21
0.601
0.52 J
0.10 U
5.9 J
0.291
NS
1.51
3.1 J
0.82 J
1.11
1.3 J
Nov-2011
Damaged
1.11
0.48 J
0.91
0.36 J
4.9 J
2.2 J
1.91
3.3 J
2.4 J
0.811
2.7 J
0.501
2.5 J
0.23 J
11
0.52 J
0.32 J
1.7 J
2.0 J
2.5 J
0.991
0.51 J
May-2012
NS
0.881
NS
6.11
NS
4.2 1
2.8 J
2.91
6.8 J
2.2 1
2.3 J
5.81
0.50 J
1.11
0.41 J
24
0.621
NS
4.0 J
4.7 J
2.01
1.01
0.92 J
Nov-2012
Damaged
0.74 J
0.35 J
91
0.33 J
5.7 J
5.51
0.91
1.91
2.4 J
0.72 J
8.0 J
0.17 J
1.5 J
0.82 J
15
0.76 J
0.24 J
3.7 J
0.93 J
0.68 J
0.501
0.82 J
May-2013
Damaged
0.02 J
0.861
5.31
0.511
3.71
2.4 J
0.83 J
2.4 J
2.41
5.0 J
6.21
0.151
0.74 J
0.581
19
0.341
0.081
5.0 J
1.2 J
0.811
0.351
Dry
May-2014
NS
0.05 U
NS
0.12 J
NS
3.8 J
0.05 U
0.05 U
0.28 J
0.05 U
2.1 J
5.8 J
0.05 U
0.05 U
0.05 U
11
0.05 U
NS
0.30 J
0.67 J
1.4 J
0.26 J
Dry
Nov-2014
NS
0.86 J
NS
7 J
NS
91
4.5 J
0.66 J
Damaged
3.4 J
4.1 J
10
0.14 U
0.84 J
0.171
36
0.371
NS
6.9 J
0.781
0.47 J
0.331
Dry
May-2015
0.49J
2.2J
0.39J
0.151
0.26J
6.1J
0.14U
1.7J
11
1.3J
5J
4.3J
0.14U
0.73J
0.46J
15
0.41J
0.23J
1.2J
0.82J
0.56J
0.71J
0.80J
Nov-2015
NS
1.01
NS
1.2 1
NS
11
81
3.61
3.5 J
3.61
2.9 J
2.11
0.14 U
1.21
0.241
2.8 1
0.261
NS
2.4 J
0.711
0.55 J
0.521
0.39 J
May-2016
NS
2.7 J
NS
0.66 U
NS
10
1.51
2.1 J
Dry
5.2 J
5.6 J
11
0.66 U
10
0.66 U
38
0.66 U
NS
0.84 J
0.92 J
0.89 J
0.88 J
0.66 U
Nov-2016
NS
1.91
NS
1.21
NS
7
6.81
0.911
Dry
13
5.1 J
21
0.66 U
71
1.3 J
42
0.851
NS
2.1 J
1.91
0.96 J
0.721
Dry
May-2017
0.07U
0.31J
0.07U
1.2 J
0.40J
11
11
0.75 J
5.11
6.4 J
4.0 J
16
0.21 J
81
0.44 J
52
1.3 J
0.07U
0.901
6AJ
0.41J
1.81
1.5 J
1.11
1.2 1
Dec-2017
4.9 J
0.42 J
0.791
8.01
0.41 1
14
13
0.74 J
2.11
10
0.47 U
15
0.361
2.61
2.2 J
41
1.5 J
0.581
2.61
2.81
3.2 J
2.4 J
Dry
0.54 J
0.491
0.14 J
Jun-2018
2.6J
1.5J1
1.3J
2J
0.681
25
4.4J
1.11
51
1.2J
1.91
6
0.64J
2.2J
3.6J
37
5
0.24J
2.4J
3J
2.4J 0.54J
Dry
.3
1.7J
Dry
Dec-2018
2.5 J
0.961
0.911
4.11
0.121
27
21
0.48 J
4.1 J
5.7
15
15
0.031
9
3.21
22
1.11
0.03 U
0.591
1.41
3.21 0.03 U
1.61�0168JJ
0.441
0.161
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Barium CAS No. 7440-39-3
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
2B Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-Ol
700
21000
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-Ol
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.04 U
0.04 U
NS
0.04 U
100
0.04 U
112
144
0.04 U
0.04 U
0.04 U
0.04 U
Nov-2007
NS
62.41
NS
96.9 J
4.6 J
357
207
115
233
136
214
Dry
126
571
May-2008
11 J
27.5 J
16 J
51.8 J
394
4 J
203
101
65 J
31 J
127
174
71.2 J
63 J
Nov-2008
NS
62.51
NS
165
51
447
196
48.31
161
103
121
Dry
268
75.11
May-2009
NS
26 J
1.8 J
6.9 J
5.3 J
460
266
117
56.1
31 J
113
181
61.6 J
78.7 J
Aug-2009
NS
NS
NS
NS
NS
701 B
125 B
NS
NS
NS
NS
127 B
112 B
76.1 B
39.8 B
56.6 B
411 JB
13.91B
ill
NS
NS
NS
Jan-2010
NS
77.4 J
NS
15.4 J
NS
492
84.2 J
165
83.8 J
137
29.1 J
169
55.4 J
113.0
23.4 J
98.5 J
82.8 J
13.1 J
100
51.5 J
89.2 J
71.3 J
76.1 J
70.9 J
May-2010
NS
23.51
NS
47.51
NS
527
42.71
202
92.11
215
266
140
29.41
129
14.21
39.2 J
86.71
NS
107
33.31
79.41
69.21
82.11
Nov-2010
NS
56.6 J
NS
149
NS
254
100
141
129.0
155
34.3 J
164
32.9 J
63.2 J
31.4 J
177
106
NS
177
49.8 J
59.1 J
75.5 J
94.2 J
May-2011
NS
361
NS
101
NS
242
36 J
174
80.5 1
124
174
124
50.71
89.2 J
19.21
346
92.31
NS
127
70.81
71.61
77.81
137
Nov-2011
Damaged
58.7 J
2.0 J
34.3 J
7.6 J
484
70.7 J
183
150
157
67.4 J
184
43.6 J
43.6 J
17.3 J
467
67.8 J
9.9 J
223
48.7 J
69.4 J
73.3 J
81.2 J
May-2012
NS
68.31
NS
166
NS
342
86.6 J
278
122
128
294
142
48.91
87.5 J
23.91
291
74.21
NS
105
78.81
84.81
60.81
74.31
Nov-2012
Damaged
37.1 J
1.8 J
152
7.0 J
425
120
151
117
53.4 J
100
133
36.5 J
132
19.3 J
504
76.6 J
11.2 J
74.7 J
38.0 J
49.1 J
74.1 J
70.6 J
May-2013
Damaged
73.91
16.5 J
80.21
7.81
288
62.51
108
115
209
560
144
39.51
169
19.81
342
69.71
10.2 J
69.41
50.21
64.61
30.31
Dry
May-2014
NS
20.3 J
NS
33.0 J
NS
343
28.6 J
80.2 J
67.9 J
110
291
157
29.3 J
58.9 J
18.3 J
368
52.4 J
NS
90.9 J
94.3 J
72.9 J
37.9 J
Dry
Nov-2014
NS
64.51
NS
273
NS
675
123
7.31
Damaged
246
398
189
32.11
100
19.71
515
69.91
NS
207
86.61
57.71
46.61
Dry
May-2015
71.1 J
19.9 J
6.1 J
34.3 J
10.8 J
412
17.9 J
151
130
271
819
202
25.8 J
63.2 J
24.4 J
292
57.1 J
10.7 J
54.3 J
57.6 J
59.7 J
54.2 J
78.3 J
Nov-2015
NS
21.41
NS
34.61
NS
625
145
109
233
131
294
131
54.31
119
21.31
69.2 J
57.71
NS
93.81
55.81
44.71
63.21
74.01
May-2016
NS
24.6 J
NS
89.5 J
NS
648
78.9 J
68.1 J
Dry
561
751
325
51.0 J
344
23.6 J
550
46.2 J
NS
52.1 J
56.3 J
51.8 J
75.1 J
76.1 J
Nov-2016
NS
49.41
NS
55.21
NS
945
198
123
Dry
336
411
285
45.31
260
31.31
654
53.11
NS
73.11
50.0 J
65.81
99.11
Dry
May-2017
74.6J
31.4 J
15.11
39.9 J
11.81
515
191
149
187
98.11
367
340
39.0 J
200
20.3 J
507
36.3 J
9.901
75.0 J
88.7J
136
128
77.5 J
65.7 J
83.3 J
Dec-2017
115
25 1
16.71
281
11.11
709
253
68.7 J
76.1 J
633.0
312
323
68.41
184
42.41
541
56.31
10.91
92.0 J
134
251
84.21
Dry
54.41
79.01
83.01
Jun-2018
36
33.7
19.8
63
11.4
879
56
93
83
348.0
132
328
56.8
161
78.3
466
38.7
10.2
65.0
100
196
89.1
Dry
58.3
117
Dry
Dec-2018
35.5
38.5
15.6
135
10.1
689
312
52.5
140
470
566
358
48.8
368
55
398
47.5
8.51
49.3
95.2
67.7
256
108
53.8
77.5
74.1
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Beryllium CAS No. 7440-41-7
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
2B Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
4*
6.5
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
2
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
Nov-2007
NS
0.61
NS
0.06 U
0.06 U
0.06 U
0.8 J
0.11
0.91
0.11
0.11
Dry
0.06 U
0.11
May-2008
0.06 U
1
0.06 U
0.1 1
0.06 U
0.06 U
0.4 J
0.11
0.11
0.11
0.11
0.7 J
0.11
0.11
Nov-2008
NS
0.71
NS
0.06 U
0.06 U
0.06 U
0.2 J
0.11
0.11
0.11
0.06 U
Dry
0.41
0.11
May-2009
NS
2.6
0.06 U
0.06 U
0.06 U
0.06 U
0.91
0.51
0.11
0.11
0.06 U
0.6 J
0.06 U
0.11
Aug-2009
NS
NS
NS
NS
0.44 U
0.44 U
NS
NS
NS
NS
0.44 U
0.44 U
044 U
0.44 U
0.44 U
0.44 U
0.44 U
0.44 U
NS
NS
NS
Jan-2010
NS
0.2 J
NS
0.91
NS
0.06 U
0.11
1
1
0.11
0.06 U
0.11
0.2 J
0.21
0.3 J
0.06 U
0.3 J
0.06 U
0.6 J
1.0
0.2 J
0.06 U
0.2 J
0.11
May-2010
NS
0.51
NS
0.11
NS
0.02 U
0.02 U
0.81
0.51
0.11
0.11
0.41
0.02 U
0.11
0.11
0.11
0.31
NS
0.11
0.11
0.11
0.11
0.11
Nov-2010
NS
0.3 J
NS
0.11
NS
0.11
0.11
0.7 J
1
0.11
0.11
0.2 J
0.02 U
0.11
0.2 J
0.11
0.3 J
NS
0.2 J
0.11
0.11
0.11
0.11
May-2011
NS
0.16 J
NS
0.11
NS
0.02 U
0.02 U
0.57 J
0.921
0.02 U
0.02 U
0.06 J
0.02 U
0.29 J
0.311
0.02 U
0.12 J
NS
0.21
0.12 J
0.061
0.02 U
0.57 J
Nov-2011
Damaged
0.26 J
0.02 U
0.07 J
0.02 U
0.02 U
0.02 U
0.65 J
0.24 J
0.06 J
0.06 J
0.24 J
0.02 U
0.16 J
0.10 J
0.02 U
0.14 J
0.02 U
0.29 J
0.02 U
0.06 J
0.091
0.101
May-2012
NS
0.191
NS
0.17 J
NS
0.07 U
0.07 U
0.50 J
0.501
0.07 U
0.07 U
0.13 J
0.07 U
0.091
0.081
0.07 U
0.12 J
NS
2
0.191
0.07 U
0.07 U
0.15 J
Nov-2012
Damaged
0.181
0.07 U
0.091
0.07 U
0.07 U
0.07 U
0.47 J
0.13 J
0.091
0.07 U
0.091
0.07 U
0.081
0.29 J
0.07 U
0.13 J
0.07 U
0.39 J
0.07 U
0.07 U
0.07 U
0.12 J
May-2013
Damaged
0.04 J
0.031
0.101
0.03 U
0.091
0.03 U
0.03 U
0.231
0.16 J
0.03 U
0.03 U
0.03 U
0.081
1.0
0.031
0.12 J
0.03 U
0.481
0.12 J
0.071
0.111
Dry
May-2014
NS
0.03 U
NS
0.06 J
NS
0.03 U
0.03 U
0.23 J
0.03 U
0.051
0.04 J
0.12 J
0.03 U
0.04 J
0.03 U
0.03 U
0.04 J
NS
0.03 U
0.16 J
0.04 J
0.04 J
Dry
Nov-2014
NS
0.04 U
NS
0.111
NS
0.04 U
0.04 U
0.04 U
Damaged
0.04 U
0.04 U
0.04 J
0.04 U
0.04 J
0.241
0.04 U
0.08 J
NS
0.081
0.04 U
0.04 U
0.081
Dry
May-2015
0.02 U
0.03 J
0.02 U
0.081
0.02 U
0.04 J
0.02 U
0.55 J
0.02 U
0.151
0.06 J
0.26 J
0.02 U
0.04 J
0.18 J
0.02 U
0.02 U
0.02 U
0.04 J
0.06 J
0.051
0.11 J
0.04 J
Nov-2015
NS
0.04 U
NS
0.07 J
NS
0.04 J
0.04 J
0.30 J
0.08 J
0.05 J
0.051
0.02 U
0.02 U
0.05 J
0.061
0.041
0.03 J
NS
0.481
0.02 U
0.031
0.131
0.091
May-2016
NS
0.07 J
NS
0.08 J
NS
0.06 J
0.05 J
0.181
Dry
0.07 J
0.07 J
0.06 J
0.04 U
0.051
0.05 J
0.04 U
0.06 J
NS
0.13 J
0.04 U
0.04 U
0.101
0.04 U
Nov-2016
NS
0.05 J
NS
0.04 U
NS
0.14 J
0.081
0.15 J
Dry
0.13 J
0.101
0.24 J
0.04 U
0.101
0.12 J
0.101
0.04 U
NS
0.06 J
0.05 J
0.04 U
0.091
Dry
May-2017
0.07U
0.07U
0.07U
0.07U
0.07U
0.081
0.091
0.17 J
0.46 J
0.18 J
0.07 J
0.18 J
0.07U
0.07U
0.07U
0.07U
0.07U
0.07U
0.101
0.42J
0.13J
0.07U
0.07U
0.07U
0.07U
Dec-2017
0.07 J
0.07 U
0.07 U
0.181
0.07 U
0.081
0.071
0.31 J
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.09 J
0.07 U
0.07 U
0.07 U
0.32 J
0.33 J
0.161
0.311
Dry
0.07 U
0.07U
0.07U
Jun-2018
0.05 U
0.051
0.11
0.06 J
0.06 J
0.07 J
0.12 J
0.26 J
0.13 J
0.05 U
0.05 U
0.09 J
0.05 U
0.06 J
0.1 J
0.07 J
0.06 J
0.05 U
0.05 U
0.27 J
0.07 J
0.16 J
Dry
0.051
0.091
Dry
Dec-2018
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.11
0.05 U
0.05 U
0.07 J
0.06 J
0.05 U
0.051
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.051
0.091
0.051
0.311
0.05 U
0.05 J
0.111
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3. * = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Cadmium CAS No. 7440-43-9
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
2
2**
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
4
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
1
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
1
3
ND
ND
Nov-06
NS
1
NS
1
ND
ND
ND
1
ND
S
2
1
May-07
1
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
1
Nov-2007
NS
0.71
NS
0.3 1
0.5 J
0.71
0.5 1
0.6 J
0.6 J
0.41
0.3 J
Dry
0.11
0.2 J
May-2008
0.1 J
0.6 J
0.35 J
0.11
0.11
1
0.2 J
0.11
0.4 J
0.04 U
0.11
0.4 J
0.11
0.11
Nov-2008
NS
0.31
NS
0.11
0.04 U
0.04 U
0.3 J
0.04 U
0.4 J
0.04 U
0.11
Dry
0.31
0.04 U
May-2009
NS
2.3
3.6
0.04 U
0.11
0.11
0.91
0.3 J
0.91
0.8 J
0.2 J
0.7 J
0.04 U
0.04 U
Aug-2009
NS
NS
NS
NS
NS
0.16 J
0.18 J
NS
NS
NS
NS
0.3 J
0.16 J
0.171
0.3J
0.158 U
0.161
0.41
0.23 J
NS
NS
NS
Jan-2010
NS
0.2J
NS
0.4J
NS
0.04U
0.2J
0.3J
0.6J
0.3J
0.2J
0.21
0.11
0.04U
0.2J
0.2J
0.2J
1
0.2J
2
1.9
1.2
0.3J
0.11
May-2010
NS
0.21
NS
0.81
NS
0.3 J
0.11
1.2
0.3 J
2.2
2
0.2 1
0.2 J
1.0
0.11
0.2 J
0.4 J
NS
0.11
0.2 J
0.11
0.11
0.11
Nov-2010
NS
0.2J
NS
0.6J
NS
0.11
0.11
0.5J
2
0.6J
0.4J
0.31
0.11
0.11
0.2J
0.11
0.2J
NS
0.3J
0.11
0.11
0.11
0.2J
May-2011
NS
0.111
NS
0.291
NS
0.071
0.11
0.35 J
0.641
0.43 J
0.4 J
0.06 J
0.051
0.81
0.171
0.11
0.161
NS
0.121
0.22 J
0.111
0.291
0.14 J
Nov-2011
Damaged
0.37 J
0.091
0.17 J
0.24 J
0.12 J
0.36 J
0.43 J
0.69 J
0.29 J
0.38 J
0.13 J
0.08 J
0.08 J
0.13 J
0.06 J
0.13 J
0.43 J
0.29 J
0.02 J
0.02 J
0.14 J
0.051
May-2012
NS
0.03 U
NS
0.251
NS
0.041
0.081
0.16 J
0.221
0.27 J
0.121
0.06 J
0.141
0.05 J
0.221
0.05 J
0.181
NS
0.181
0.171
0.03 U
0.03 U
0.03 U
Nov-2012
Damaged
0.16 J
0.03 J
0.181
0.03 U
0.051
0.34 J
0.22 J
0.12 J
0.12 J
0.16 J
0.04 J
0.04 J
0.08 J
0.64 J
0.13 J
0.12 J
0.43 J
0.36 J
0.07 J
0.03 J
0.04 J
0.07 J
May-2013
Damaged
0.151
0.391
0.291
0.481
0.111
0.071
0.09 J
0.201
0.311
0.141
0.13 J
0.641
0.06 J
0.971
0.68 J
0.211
2
0.18 1
0.081
0.05 J
0.081
Dry
May-2014
NS
0.11 J
NS
0.14 J
NS
0.191
0.15 J
0.08 J
0.05 J
0.31 J
0.29 J
0.39 J
1.0
0.17 J
0.25 J
0.09 J
1
NS
2
0.22 J
0.05 U
0.05 U
Dry
Nov-2014
NS
0.121
NS
0.441
NS
0.171
0.121
0.04 U
Damaged
0.20 J
0.261
0.08 J
0.311
0.21 J
0.581
0.26 J
0.181
NS
0.26 J
0.051
0.04 J
0.041
Dry
May-2015
0.85 J
0.13 J
0.23 J
0.13 J
0.18 J
0.03 J
0.011
0.33 J
0.62 J
0.48 J
0.44 J
0.101
0.101
0.08 J
0.33 J
0.091
0.101
0.50 J
0.86 J
0.07 J
0.02 J
0.03 J
0.03 J
Nov-2015
NS
0.081
NS
0.261
NS
0.041
0.151
0.21 J
0.38 J
0.45 J
0.351
0.12 J
0.181
0.621
0.451
1
1
NS
0.661
0.041
0.04 J
0.071
0.081
May-2016
NS
0.12 J
NS
0.10 J
NS
0.05 U
0.07 J
0.08 J
Dry
0.48 J
0.15 J
0.05 U
0.12 J
0.13 J
0.16 J
0.14 J
0.23 J
NS
0.44 J
0.05 U
0.05 U
0.05 U
0.05 U
Nov-2016
NS
0.131
NS
0.101
NS
0.05 U
0.08 J
0.09 J
Dry
0.18 J
0.301
0.20 J
0.13 J
0.09 J
0.501
0.15 J
0.05 J
NS
0.291
0.05 U
0.05 U
0.05 U
Dry
May-2017
0.60J
0.11
0.23J
0.131
0.40J
0.08U
0.08U
0.091
0.88J
0.25J
OAJ
0.11J
0.08U
0.17J
0.151
0.08U
0.08U
0.25J
0.61J
0.20J
0.14J
0.08U
0.08U
0.08U
0.08U
Dec-2017
0.55 J
0.08 U
0.08 U
0.171
0.08 U
0.08 U
0.09 J
0.11 J
0.08 U
0.08 U
0.091
0.08 U
0.09 J
0.15 J
0.08 U
0.15 J
0.08 U
0.19 J
0.441
0.121
0.21 J
0.08 U
Dry
0.08U
0.08U
0.08U
Jun-2018
0.27 J
0.051
0.09 J
0.06 J
0.2 J
0.02 U
0.06 J
0.09 J
0.12 J
0.15 J
0.06 J
0.06 J
0.04 J
0.04 J
0.08 J
0.13 J
0.04 J
0.22 J
0.1 J
0.171
0.13 J
0.11 J
Dry
0.02 U
0.03 J
Dry
Dec-2018
0.111
0.14 J
0.02 U
0.111
0.02 U
0.11 J
0.041
0.14 J
0.081
0.171
0.161
0.081
0.02 J
0.141
0.11
0.02 U
0.061
0.06 J
0.071
0.08 J
0.151
0.041
0.151
0.02 U
0.021
0.04 J
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3. * = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Chromium CAS No. 7440-47-3
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS 26 Std
MW-iD
MW-IS
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
10 WER
NS
ND
29
ND
ND
ND
ND
ND
ND
ND
Nov-01
83
ND
NS
ND
29
ND
1s
ND
ND
May-02
NS
ND
NS
85
42
ND
ND
ND
ND
Nov-02
NS
ND
NS
69
13
ND
ND
ND
ND
ND
ND
May-03
NS
ND
24
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
22
15
NS
ND
ND
ND
11
ND
122
ND
ND
ND
May-04
NS
ND
NS
42
12
ND
15
ND
10
ND
ND
ND
Nov-04
NS
ND
NS
33
25
ND
22
ND
25
ND
ND
ND
May-05
Damaged
ND
NS
33
30
ND
20
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
15
ND
ND
11
40
ND
ND
ND
ND
May-06
Damaged
ND
11
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
12
ND
ND
ND
ND
ND
May-07
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
Nov-2007
NS
0.31
NS
0.51
0.24 U
1.2 1
2.7 J
0.41
13
1.31
1.01
Dry
1.51
0.24 U
May-2008
0.3J
0.2J
0.3J
0.6J
1.51
0.2J
1.2J
1.2J
3.1J
1.11
1.11
8.01
1.11
0.4J
Nov-2008
NS
0.51
NS
1.71
0.11 U
1.41
1.01
1.11
4.7 J
1.11
0.4 J
Dry
5.01
0.31
May-2009
NS
0.10U
1.7J
0.7J
0.10U
1.6J
2.1J
0.7J
2.5J
0.51
0.11
5.11
0.5J
0.51
Aug-2009
NS
NS
NS
NS
NS
8.81B
3.361B
NS
NS
NS
NS
4.76 JB
3 JB
31B
3.091B
2.48 JB
1.771B
4.24 JB
2.81B
NS
NS
NS
Jan-2010
NS
0.10U
NS
0.10U
NS
11
0.10U
2.8J
2.7J
0.8J
0.10U
0.10U
2.7J
0.91
0.10U
0.10U
0.7J
1.8J
2.6J
3.3J
2.1J
0.7J
0.4J
0.3J
May-2010
NS
0.51
NS
0.71
NS
21
0.11
2.1 1
2.31
4.2 1
2.51
0.81
0.3 J
0.61
0.3 J
0.6 J
0.8 J
NS
0.5 J
0.4 J
0.91
0.4 J
0.91
Nov-2010
NS
0.5J
NS
0.6J
NS
1.7J
0.3J
3.1J
11
2J
0.4J
0.8J
0.03U
0.11
0.11
1.7J
0.91
NS
0.51
0.5J
0.5J
0.2J
0.3J
May-2011
NS
0.441
NS
0.621
NS
0.761
0.31
31
6.21
2.41
1.21
0.84 J
0.171
0.83 J
0.231
2.61
0.511
NS
0.481
1.81
0.581
0.991
3.1 J
Nov-2011
Damaged
0.66 J
0.04 U
0.29 J
0.15 J
1.7 J
0.67 J
3.7 J
9.51
2.7 J
0.92 J
2.1 J
0.23 J
0.86 J
0.04 J
14
0.57 J
0.04 U
1.3 J
0.74 J
1.2 J
0.63 J
0.46 J
May-2012
NS
0.911
NS
1.71
NS
1.01
1.51
5.71
6.11
2.5 J
2.01
1.71
0.18 U
0.50 J
0.18 U
6.5 1
0.611
NS
2.01
2.61
1.41
0.381
1.001
Nov-2012
Damaged
0.45J
0.18U
1.91
0.18U
1.5J
2.3J
3.6J
5.2J
1.8J
1.51
3.01
0.18U
0.80J
0.25J
16
0.68J
0.4J
1.2J
0.54J
0.545J
0.18J
1.11
May-2013
Damaged
0.50 J
0.7 J
0.57 J
0.38 J
0.50 J
1.0 J
2.2 J
4.8 J
3.2 J
7.41
2.21
0.131
1.11
0.78 J
19
0.591
0.27 J
5.81
2.41
1.61
1.61
Dry
May-2014
NS
0.45 J
NS
0.81 J
NS
1.8 J
0.29 J
1.91
3.1 J
0.38 J
6.1 J
3.8 J
0.04 U
0.83 J
0.20 J
9.01
0.46 J
NS
2.1 J
1.91
0.951
0.511
Dry
Nov-2014
NS
1.61
NS
3.51
NS
5.11
2.81
0.14 U
Damaged
2.61
11
5.81
0.14 U
1.11
0.341
21
0.351
NS
14
0.981
0.811
0.14 U
Dry
May-2015
0.24J
0.17J
0.31J
0.14J
0.40J
2.6J
0.12U
3.01
9.3J
0.86J
18
2.9J
0.18J
1.4J
1.11
8.9J
0.63J
0.12U
0.82J
1.2J
1.11
1.2J
0.951
Nov-2015
NS
0.12 U
NS
1.21
NS
7.31
5.11
3.31
9.81
1.3 1
9.91
1.3 1
0.12 U
1.7 J
0.651
2.7 J
0.421
NS
8.41
0.861
0.431
0.851
0.53 1
May-2016
NS
0.52J
NS
0.70J
NS
9.8J
1.01
1.91
Dry
4.0J
18
8.7J
0.08J
9.2J
0.85J
27
0.811
NS
3.0J
1.6J
0.80J
1.11
0.71J
Nov-2016
NS
0.531
NS
0.371
NS
18
4.11
2.01
Dry
4.81
8.81
9.31
0.06 U
11
0.43 J
28
0.261
NS
1.21
0.951
1.01
0.61 J
Dry
May-2017
0.13J
0.17 J
0.63J
0.82 J
0.58J
13
8.7 J
2.0 J
13
3.4 J
8.91
12
0.08U
12
0.08U
28
0.15 J
0.08U
2.1 J
2.9J
1.51
1.3 J
0.46 J
0.08U
3.1 J
Dec-2017
2.1 J
0.11 J
0.57 J
7.61
0.08 U
17
10
3.21
6.71
7.71
8.21
17
0.36 J
4.71
0.81
31
0.41
0.081
9.11
2.91
6.9 J
2.41
Dry
0.641
0.41
0.081
Jun-2018
0.15U
0.15U
2J
0.43J
4.6J
24
2.5J
2.4J
4.9J
1.31
2.7J
3.91
0.15U
4.1J
1.3J
26
0.15U
0.15U
0.84J
2.6J
2.5J
2.9J
Dry
0.15U
1.2J
Dry
Dec-2018
1.41
0.77 J
0.35 J
31
0.15 U
32
13
4.41
3.31
4.31
12
15
0.15 U
14
0.561
24
0.311
0.15 U
0.481
0.15 U
1.51
0.941
6.1
0.531
0.371
0.61
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Cobalt CAS No. 7440-48-4
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPs
2B Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MIN-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
1*
4
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
19
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
16
ND
ND
11
17
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
52
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
23
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
11
ND
21
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
12
15
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
13
ND
29
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
17
11
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
43
ND
ND
ND
May-07
0.41U
0.41U
0.41U
0.41U
0.41U
0.41U
0.41U
12
38
0.41U
0.41U
0.41U
Nov-2007
NS
1.5 J
NS
9.3 J
0.41 U
9.4 J
1.01
2.3 J
6.3 J
17.0
Dry
0.81
0.71
May-2008
0.11
0.81
0.11
1.3 J
13
0.11
1.01
1.7 J
1.7 J
2.6 J
19
1.2 J
0.8 J
1.01
Nov-2008
NS
0.91
NS
10
0.11
17
0.41
0.5 J
4.4 J
2.8 J
12
Dry
1.91
5.11
May-2009
NS
1.2J
0.4J
5.81
0.11
12.6
1.3J
1.2J
1.11
2.3J
8.4J
1.01
0.4J
1.3J
Aug-2009
NS
NS
NS
NS
NS
10.6
19.9
NS
NS
NS
NS
12.3
1.72 U
1.72 U
1.72 U
1.72 U
1.72 U
1.72 U
1.72 U
NS
NS
NS
Jan-2010
NS
2.5J
NS
0.4J
NS
5.7J
15
0.91
1.6J
0.6J
1.11
10
0.7J
0.3J
0.51
0.2J
1.3J
0.2J
0.4J
1.2J
0.6J
0.3J
1.2J
0.2J
May-2010
NS
0.71
NS
1.11
NS
18
3.8J
0.91
2.8J
5.4J
9.01
21
0.21
0.2J
0.31
0.21
0.91
NS
0.2J
0.3J
0.6J
0.6J
0.51
Nov-2010
NS
0.8J
NS
3.3J
NS
37
17
1.11
7.8J
0.7J
0.81
24
0.2J
0.3J
0.3J
0.8J
1.01
NS
0.3J
0.4J
0.5J
1.01
0.7J
May-2011
NS
0.411
NS
3.7 J
NS
14
7.7 J
0.58 J
1.5 J
1.4 J
4.2 J
31
0.091
2.2 J
0.261
1.5 J
1.2 J
NS
0.181
0.841
1.51
0.421
1.6 J
Nov-2011
Damaged
0.48 J
0.03 U
1.11
0.05 J
6.8 J
15
0.76 J
1.6 J
1.11
1.2 J
17
0.111
0.26 J
0.20 J
0.84 J
0.60 J
0.08 J
0.42 J
0.501
0.75 J
1.3 J
0.86 J
May-2012
NS
0.381
NS
7.0 J
NS
2.6 J
25
0.63 J
1.7 J
1.3 J
3.6 J
31
0.06 J
0.45 J
0.221
0.72 J
1.5 J
NS
3.4 J
0.891
0.791
0.761
0.721
Nov-2012
Damaged
0.31 J
0.04 J
8.6 J
0.03 J
15
28
0.38 J
1.11
0.55 J
1.3 J
27
0.08 J
0.86 J
0.53 J
1.11
0.46 J
0.10 J
1.6 J
0.42 J
0.31 J
0.891
1.7 J
May-2013
Damaged
0.201
0.261
2.0 J
0.081
2.2 J
18
0.35 J
1.6 J
3.0 J
9.2 J
24
0.04 J
0.33 J
0.731
0.88 J
0.471
0.04 J
2.4 J
0.731
0.521
0.481
Dry
May-2014
NS
0.13 J
NS
1.0 J
NS
5.9 J
0.281
0.30 J
0.34 J
0.22 J
5.2 J
22
0.05 J
0.44 J
0.191
0.82 J
0.32 J
NS
0.24 J
0.38 J
0.88 J
0.31 J
Dry
Nov-2014
NS
0.331
NS
5.6 J
NS
2.6 J
15
0.13 J
Damaged
2.8 J
5.0 J
12
0.12 U
0.49 J
0.661
1.11
0.471
NS
1.8 J
0.411
0.341
0.751
Dry
May-2015
0.22 J
0.44 J
0.04 J
0.29 J
0.051
0.89 J
0.12 J
0.80 J
2.6 J
0.911
18
14
0.06 J
0.31 J
0.43 J
0.81 J
0.28 J
0.05 J
0.79 J
0.33 J
0.32 J
0.48 J
0.34 J
Nov-2015
NS
0.301
NS
0.391
NS
2.7 J
11
1.3 J
1.5 J
1.11
4.1 J
4.0 J
0.101
0.38 J
0.521
0.30 J
0.351
NS
1.6 J
0.261
0.201
0.741
0.261
May-2016
NS
0.20 J
NS
0.49 J
NS
3.1 J
7.6 J
0.38 J
Dry
4.5 J
16
11
0.07 J
0.92 J
0.30 J
1.7 J
0.26 J
NS
0.61 J
0.27 J
0.28 J
0.72 J
0.181
Nov-2016
NS
0.311
NS
1.7 J
NS
3.0 J
6.2 J
0.33 J
Dry
2.5 J
3.3 J
9.8 J
0.113 J
1.01
0.701
2.0 J
0.941
NS
1.3 J
0.341
0.321
0.471
Dry
May-2017
0.38J
0.24U
0.24U
1.11
0.24U
2.5 J
8.6 J
0.36 J
2.9 J
1.4 J
8.3 J
8.0 J
0.24U
0.87 J
0.28 J
1.8 J
0.501
0.24 U
0.74 J
0.3
0.33J
0.35 J
0.35 J
0.36 J
0.47 J
Dec-2017
0.57 J
0.24 U
0.24 U
4.1 J
0.24 U
3.9 J
9.5 J
0.51 J
0.991
2.9 J
3.5 J
3.3 J
0.29 J
0.56 J
0.731
2.0 J
0.371
0.24 U
1.6 J
0.361
0.861
0.281
Dry
0.241
0.511
0.24 U
Jun-2018
E
0.22 J
0.2 J
0.511
1.1
0.26 J
4.7
2.1
0.46 J
1.1
1.6
2.4
3.2
0.27 J
0.42 J
1.4 J
1.9
0.85 J
0.091
0.591
0.33 J
0.55 J
0.33 J
Dry
0.3 J
0.65 J
Dry
Dec-2018
0.271
0.27 J
0.12 1
1.4
0.081
3
8.3
0.221
1 1.2
2.9
12
3.4
0.121
1 1.8
1
1.6
0.541
0.07 J
0.361
0.151
0.531
0.321
0.791
0.191
0.321
0.621
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3. * = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Copper CAS No. 7440-50-8
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
1000
WER
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
Nov-2007
NS
1.7
NS
2.0
1.3
1.8
2.3
1.6
6.7
2.7
1.6
)ry
1.9
1.6
May-2008
0.4
1.5
0.7
1.0
1.3
0.8
0.7
0.9
2.1
2.0
0.9
5.5
0.8
0.6
Nov-2008
NS
1.3
NS
1.2
1.3
1.3
0.9
3.3
2.8
3.0
0.8
Dry
5.6
1.1
May-2009
NS
0.7
5.5
1.9
0.7
1.4
1.8
2.6
2.3
1.6
0.6
4.9
1.5
0.4
Aug-2009
NS
NS
NS
NS
3.641
2.351
NS
NS
NS
NS
2.311
2.131
2.341
2.44J
1.861
1.331
1.29 U
1.341
2.7 J
0.81
0.8 J
0.71
Jan-2010
NS
0.91
NS
1.2J
NS
1.91
1.3J
1.81
1.6J
1.11
2.4J
0.7J
1.3J
1.01
0.8J
0.7J
1.2J
2.41
2.4J
4.81
0.4J
0.4J
0.3J
0.51
May-2010
NS
0.71
NS
0.91
NS
1.11
4.01
1.4 J
1.11
2.41
2.91
1.11
0.11
0.61
0.2 J
0.3 1
0.5 J
NS
0.11
0.3 J
0.11
0.11
0.3 1
Nov-2010
NS
0.5 J
NS
1.11
NS
1.11
0.51
1.3 J
3.9 J
1.5 J
0.81
0.8 J
0.03 U
0.03 U
0.03 U
1.11
0.81
NS
0.11
1.7 J
0.94 J
1.11
1.5 J
May-2011
NS
1.11
NS
1.51
NS
1.3 1
1.11
1.91
4.4 J
1.61
1.51
1.3 1
0.291
1.71
0.67 J
1.5 J
2.11
NS
0.811
0.171
0.461
0.301
0.02 U
Nov-2011
Damaged
0.89 J
0.15 J
0.49 J
0.52 J
1.5 J
0.88 J
1.11
7.1 J
1.7 J
0.93 J
0.69 J
0.05 J
0.18 J
0.09 J
0.53 J
0.82 J
0.66 J
0.59 J
2.3 J
1.2 J
0.34 J
0.42 J
May-2012
NS
0.871
NS
1.31
NS
0.911
0.851
1.81
3.41
2.21
1.91
1.11
0.111
0.371
0.501
0.871
0.771
NS
1.91
2.11
0.361
0.581
1.21
Nov-2012
Damaged
1.01
0.76 J
1.3 J
1.3 J
1.6 J
1.4 J
0.88 J
4.2 J
1.2 J
1.91
1.4 J
0.501
0.64 J
0.70 J
0.911
1.01
1.2 J
0.57 J
1.3 J
1.4 J
1.11
Dry
May-2013
Damaged
0.961
2.0 J
1.61
1.61
0.771
1.01
0.61 J
4.81
1.81
1.91
1.31
0.351
0.68 J
1.41
1.5 J
0.631
0.941
1.81
2.41
0.461
0.401
Dry
May-2014
NS
1.0 J
NS
0/8 U
NS
1.11
0.54 J
0.31 J
4.0 J
0.52 J
1.7 J
2.0 J
0.67 J
0.38 J
0.37 J
0.63 J
1.01
NS
1.81
0.46 J
0.37 J
0.41 J
Dry
Nov-2014
NS
0.941
NS
2.01
NS
1.51
0.741
5.51
Damaged
0.61 J
4.81
1.21
0.511
0.76 J
0.961
1.2 J
0.401
NS
1.11
0.801
0.621
0.72 J
0.601
May-2015
4.8J
0.60J
1.51
0.36J
0.92J
0.56J
0.12J
0.911
3.5J
0.84J
1.6J
0.66J
0.23J
0.27J
0.901
0.35J
0.60J
1.3J
0.55J
0.66J
0.87J
0.72J
0.74J
Nov-2015
NS
1.61
NS
2.71
NS
2.3 1
1.3 J
1.01
4.9 J
1.91
5.6 J
0.71 J
0.461
0.75 J
1.11
1.5 J
2.01
NS
3.61
0.681
0.521
0.641
0.601
May-2016
NS
3.0J
NS
1.2J
NS
2.2J
1.3J
0.50J
Dry
2.5J
1.91
1.7J
0.43J
0.97J
0.511
1.6J
1.3J
NS
1.81
0.48J
0.34J
0.39J
Dry
Nov-2016
NS
1.81
NS
0.341
NS
1.71
1.11
0.36 J
Dry
1.01
4.11
1.81
0.161
0.70 J
0.351
1.5 J
0.501
NS
0.62 J
0.451
0.561
0.571
1.6 J
May-2017
4.1J
3.0 J
1AJ
1.3 J
1.6J
2.0 J
1.51
0.53 J
5.51
1.5 J
1.2 J
1.8 J
0.22 J
0.70 J
3.5 J
1.11
0.69 J
1.2J
1.4 J
1AJ
0.35J
0.45 J
0.56 J
0.57 J
1.6 J
Dec-2017
3.1 J
1.71
0.55 1
2.71
0.861
2.71
2.2 J
0.92 J
3.6 J
1.61
4.6 J
2.01
0.681
0.95 J
0.661
2.41
0.71
0.6 J
3.81
0.61
2.61
0.771
Dry
0.431
0.471
0.681
Jun-2018
1.5J
1.3J
1.11
1.3J
1.81
2.6J
1.11
11
1.6J
1.4J
0.65J
1J
0.35J
0.69J
0.46J
0.76J
0.89J
0.77J
0.56J
1.1J
1.2J
0.88J
Dry
0.58J
0.66J
Dry
Dec-2018
1.6 J
1.91
0.35 1
1.5 1
0.541
1.5 1
1.2 J
0.65 J
0.871
1.3 1
1.21
1.11
0.381
0.96 J
0.31
1.11
0.381
0.41 J
0.521
0.441
0.251
0.121
3.1
0.261
0.461
0.431
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Lead CAS No. 7439-92-1
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-Is
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
15
WER
NS
ND
ND
29
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
27
11
ND
ND
ND
ND
May-02
NS
ND
NS
ND
13
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
2.8J
ND
ND
ND
Nov-03
ND
ND
NS
22
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
20
25
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
19
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
14
ND
ND
Nov-05
NS
ND
NS
ND
14
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
Nov-2007
NS
1.3
NS
0.3
0.1
0.1
7.2
0.4
5.9
0.3
0.3
Dry
1.6
0.2
May-2008
0.04 U
1.6
0.2
0.5
0.1
0.04 U
4.8
0.4
0.5
0.7
0.2
25
0.7
0.3
Nov-2008
NS
2.8
NS
0.4
0.1
0.1
3.4
0.6
0.4
0.3
0.2
Dry
14
0.9
May-2009
NS
3.7
0.7
0.5
0.04 U
0.04 U
11
0.2
0.3
0.1
0.1
23
0.5
0.2
Aug-2009
NS
NS
NS
NS
NS
6.79 U
6.79 U
NS
NS
NS
NS
6.79 U
6.79 U
6.79 U
6.79 U
6.79 U
6.79 U
6.79 U
6.79 U
NS
NS
NS
Jan-2010
NS
0.8J
NS
3.9J
NS
0.11
0.2J
14
1.51
0.51
0.11
0.41
1.81
1.4J
0.2J
0.4J
3.2J
1.2J
21
5.3J
8.01
0.3J
0.6J
0.31
May-2010
NS
3.01
NS
1.11
NS
0.11
0.01 U
6.3 1
0.71
0.2 1
0.11
0.41
0.11
2.01
0.2 J
1.11
1.8 J
NS
1.5 J
0.91
0.5 1
0.6 J
1.61
Nov-2010
NS
2.0J
NS
0.5J
NS
0.11
0.2J
6.41
3.9J
0.31
0.2J
0.41
0.01U
1.11
0.2J
1.91
3.1J
NS
2.2J
11
0.11
0.5J
0.2J
May-2011
NS
0.61
NS
0.921
NS
0.16 J
0.15 1
4.81
3.01
0.18 J
0.121
0.13 J
0.161
1.21
0.11
0.83 J
0.81
NS
4.41
4.31
0.51
0.281
5.7 J
Nov-2011
Damaged
1.71
0.06J
0.68J
0.08J
0.42J
0.17J
7.3J
2.1J
0.24J
0.29J
1.2J
0.16J
1.91
0.12J
0.64J
0.93J
0.17J
3.21
0.95J
0.79J
1.11
0.29J
May-2012
NS
1.1 1
1.31
NS
0.22 J
0.25 1
7.61
3.51
0.39 J
0.331
0.20 J
0.08 U
0.74 J
0.091
0.90 J
1.01
NS
11
7.01
2.11
0.461
1.31
Nov-2012
Damaged
1.11
0.07 J
0.64 J
0.08 U
0.31 J
0.35 J
3.1 J
1.4 J
0.55 J
0.20 J
0.19 J
0.12 J
0.43 J
0.49 J
0.65 J
1.51
0.22 J
7.9 J
0.45 J
0.43 J
0.111
1.3 J
May-2013
Damaged
0.141
0.331
0.551
0.13 J
0.03 J
0.041
0.29 J
1.51
0.05 J
0.081
0.06 J
0.121
0.23 J
0.531
0.07 J
0.931
0.07 J
0.751
1.61
1.21
3.01
Dry
May-2014
NS
0.111
NS
0.191
NS
0.16 J
0.06 J
0.74 J
0.511
0.04 J
0.14 J
0.19 J
0.07 J
0.10 J
0.04 J
0.02 U
0.40 J
NS
0.42 J
5.2 J
0.39 J
1.2 J
Dry
Nov-2014
NS
0.181
NS
83.0
NS
0.13 U
0.13 U
0.31 J
Damaged
0.13 U
0.22 J
0.13 U
0.13 U
0.13 U
0.13 U
0.13 U
0.52 J
NS
1.41
0.301
0.211
0.781
Dry
May-2015
0.27 J
0.34 J
0.05 J
0.27 J
0.07 J
0.16 J
0.06 J
3.81
3.9 J
0.09 J
0.25 J
0.39 J
0.03 U
0.05 J
0.101
0.03 U
0.111
0.05 J
0.56 J
0.69 J
0.53 J
2.5 J
0.84 J
Nov-2015
NS
0.261
NS
2.61
NS
0.091
0.281
2.01
0.65 J
0.19 J
0.351
0.16 J
0.16 J
0.111
0.091
0.191
1.01
NS
13
0.381
0.461
11
0.681
May-2016
NS
1.8J
NS
0.32J
NS
0.24J
0.34J
0.87J
Dry
0.14J
0.27J
0.20J
0.191
0.12J
0.07J
0.07J
2.1J
NS
2.7J
0.82J
0.62J
1.01
0.60J
Nov-2016
NS
0.691
NS
0.131
NS
0.191
0.261
0.45 J
Dry
0.66 J
0.241
0.69 J
0.06 J
0.06 U
0.24 J
0.06 J
0.08 J
NS
1.01
0.32 J
0.401
0.421
Dry
May-2017
0.29J
0.56 J
.27J
0.37 J
0.16J
0.30 J
0.42 J
1.71
7.8 J
2.2 J
0.44 J
0.22 J
0.08U
0.08U
0.08U
0.08U
0.17 J
0.08U
2.1 J
10
0.34J
0.28 J
0.42 J
0.56 J
4.3 J
Dec-2017
2.1 J
0.191
0.241
1.81
0.111
0.46 J
0.781
1.91
0.31
0.35 J
0.241
0.14 J
0.35 J
0.76 J
0.11 J
0.24 J
1.11
0.18 J
8.61
5.61
3.1 J
1.71
Dry
0.331
0.411
0.241
Jun-2018
0.53J
0.48J
0.98J
0.48J
0.6J
0.13J
0.91J
1.8J
1.11
0.07J
0.14J
0.26J
0.19J
0.18J
0.13J
0.6J
2.8J
0.12J
0.69J
6.8J
0.81
0.97J
Dry
0.81J
1.11
Dry
Dec-2018
11
0.28 J
0.03 U
0.411
0.03 U
0.031
0.041
0.28 J
0.161
0.03 U
0.21
0.041
0.03 U
0.03 J
0.041
0.03 U
0.161
0.03 U
0.731
0.1 1
0.121
0.061
9.6
0.211
0.321
0.381
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Mercury CAS No. 7439-97-6
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-ID
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
1
0.012
Nov-01
May-02
Nov-02
May-03
Nov-03
May-04
Nov-04
May-05
Nov-05
May-06
Nov-06
May-07
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
Nov-2007
May-2008
Nov-2008
May-2009
Aug-2009
0.024 U
0.024 U
0.024 U
0.024 U
0.024 U
0.024 U
Jan-2010
0.03 U
0.09
0.03 U
May-2010
0.08 U
0.08 U
0.08 U
Nov-2010
0.08 U
0.08 U
0.08 U
May-2011
0.05 U
0.051
0.08 J
Nov-2011
0.05 U
0.05 J
0.05 U
May-2012
0.091
0.041
0.04 J
Nov-2012
0.02 U
0.07 J
0.03 J
0.02 J
0.05 J
0.02 U
May-2013
0.04 J
0.041
0.05 1
0.031
0.031
0.03 J
May-2014
0.01U
0.01U
0.01U
0.01U
0.01U
Nov-2014
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
May-2015
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Nov-2015
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
May-2016
0.04 U
0.04 J
0.04 U
0.04 J
0.04 J
Nov-2016
0.04 U
4.93
0.04 U
0.04 U
0.04 U
May-2017
0.07 U
NS
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
NS
NS
NS
NS
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
Dec-2017
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
Jun-2018
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
Dec-2018
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.06 J
0.05 U
0.05 U
0.051
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 J
0.05 U
0.05 U
0.05 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Nickel CAS No. 7440-02-0
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPs
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
100
WER
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
0.66 U
Nov-2007
NS
3.31
NS
3.61
1.6 1
5.91
2.71
9.11
9.11
7.51
5.3 J
Dry
2.91
0.7 J
May-2008
0.91
5.2J
1.4J
2.1J
7.4J
0.51
2.3J
4.3J
3.2J
2.0J
7.81
3.5J
1.4J
0.81
Nov-2008
NS
4 J
NS
6 J
0.6 J
7.11
1.71
3.4 J
6.11
4.61
4.7 J
Dry
4.21
1.3 J
May-2009
NS
2.11
1.7J
1.8J
0.4J
5.4J
1.21
2.5J
1.01
0.91
3.3J
1.91
0.2J
0.4J
Aug-2009
NS
NS
NS
NS
NS
3.47 J
2.36 U
NS
NS
NS
NS
3.91 J
2.36 U
2.36 U
2.75J
2.431
2.441
2.36 U
2.36 U
NS
NS
NS
Jan-2010
NS
1.7J
NS
3.1J
NS
5.8J
2.6J
2.1J
4.8J
1.11
0.6J
5.1J
2.5J
0.8J
2.2J
0.91
1.6J
2.14J
1.0J
5.2J
1.3J
0.91
0.8J
0.6J
May-2010
NS
3.21
NS
1.71
NS
10.8J
1.5J
2.01
7.1J
7.51
10.4J
9.2J
2.01
1.5J
1.81
0.91
1.71
NS
1.11
0.4J
1.21
0.8J
0.81
Nov-2010
NS
3.9J
NS
6.2J
NS
12.1J
6.4J
2.1J
16.8J
5.7J
1.7J
9.11
1.8J
4.1J
1.6J
4.1J
2.2J
NS
1.9J
0.7J
1.6J
0.81
0.8J
May-2011
NS
1.21
NS
3.11
NS
3.31
1.6J
1.41
5.5J
2J
2.3J
5.2J
0.77J
1.11
1.21
6.8J
2.11
NS
0.861
1.3J
1.81
1.11
1.51
Nov-2011
Damaged
1.4J
0.3J
1.2J
0.71J
4.3J
3.6J
1.8J
6.9J
2.7J
1.5J
5.4J
0.78J
1.3J
1.2J
7.6J
1.3J
1.41
2J
0.88J
0.991
0.76J
0.55J
May-2012
NS
2.61
NS
4.41
NS
3.61
4.8J
1.71
4.7J
2.91
4.3J
7.21
0.231
2.31
3.4J
5.61
3.4J
NS
5.2J
3.8J
2.91
5.0J
6.11
Nov-2012
Damaged
2.6J
1.11
6.6J
0.88J
5.8J
8.81
1.8J
5.4J
1.4J
2.5J
8.6J
1.3J
1.6J
2.3J
7.3J
1.7J
1.7J
1.9J
0.46J
0.46J
0.78J
1.11
May-2013
Damaged
1.81
1.6 J
4.61
0.901
3.5 1
5.01
1.81
5.61
4.3 J
5.5 1
9.3 J
0.981
1.5 J
2.4 J
4.8 J
0.841
0.96 J
4.4 J
0.971
0.65 J
0.471
Dry
May-2014
NS
1.3J
NS
1.6J
NS
3.1J
1.51
0.87J
2.2J
0.71J
3.5J
7.8J
1.3J
1.01
2.7J
5.91
1.2J
NS
1.6J
0.98J
0.89J
0.45U
Dry
Nov-2014
NS
2.61
NS
5.91
NS
5.71
6.7 J
1.51
Damaged
3.11
6.0 J
8.41
1.2 J
1.81
4.5 J
6.71
1.11
NS
6.9 J
1.2 J
1.41
0.531
Dry
May-2015
3.4J
1.6J
1.51
0.57J
0.68J
2.3J
0.43J
2.0J
6.4J
1.7J
6.8J
4.4J
0.87J
1.20J
3.20J
4.90J
1.40J
1.1 J
1.60J
0.67J
0.70J
0.60J
0.74J
Nov-2015
NS
2.91
NS
1.31
NS
5.71
9.7 J
2.51
10.11
2.3 1
5.4 J
2.5 1
1.91
1.71
4.1 J
2.3 1
2.5 J
NS
4.1 J
0.801
0.74 J
0.881
0.75 J
May-2016
NS
2.0J
NS
2.0J
NS
4.5J
2.6J
1.3J
Dry
5.5J
6.3J
6.4J
1.2J
4.1J
3.6J
6.6J
1.4J
NS
2.5J
0.92J
0.86J
0.75J
0.78J
Nov-2016
NS
3.81
NS
2.61
NS
8.51
5.5 J
2.41
Dry
3.61
10.41
10.4 J
1.81
6.71
5.2 J
8.9 J
3.4 J
NS
3.0 J
0.721
1.01
0.641
Dry
May-2017
4AJ
2.4J
1.3J
2.5J
0.83J
4.7J
6.2J
2.1J
8.7J
1.8J
4.2J
8.3J
1.51
6.3J
9.3J
7.6J
1.8J
1.7J
2.6J
1.11
3.0J
1.4J
1.2J
1.1J
1.4J
Dec-2017
4.4J
2.71
1.2J
6.01
0.681
6.41
7.4J
1.51
4.4J
4.91
5.1 J
8.0J
2.1 1
3.4J
4.81
6.9J
2.3J
3.0J
4.5J
0.94J
1.7J
2.2J
Dry
0.61
0.671
0.94J
Jun-2018
2J
2J
21
3.3J
1.51
7.9J
1.81
1.7J
3.6J
3.6J
2J
3.1J
1.8J
3.3J
5.3J
5.6J
2.1J
0.99J
1.51
11
0.97J
2.4J
Dry
0.73J
1.11
Dry
Dec-2018
1.6J
3.11
1.11
3.91
11
8.11
7.1J
1.51
3.9J
6.31
6.3J
7.41
2.1J
12.1
5.7J
6.61
3.91
1.41
1.8J
2.11
1.5J
5.21
2.1
0.651
1 0.791
1 0.15J
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Selenium CAS No. 7782-49-2
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
20
5
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
0.35 U
Nov-2007
NS
1.91
NS
2.31
0.14 U
5.61
0.14 U
2.3 J
7.9 J
6.0 J
4.7 J
Dry
2.2 1
0.14 U
May-2008
0.3J
1.91
0.21
1.2J
0.14U
0.31
0.91
2.5J
1.7J
1.7J
5.91
1.3J
0.91
0.2J
Nov-2008
NS
1.61
NS
4.81
0.3 J
9.8 J
0.14 U
1.2 J
5.31
5.9 J
3.5 J
Dry
3.01
0.3 J
May-2009
NS
5.21
0.12 U
2.51
0.3 J
8.2 J
0.51
1.5 J
0.51
0.8 J
2.2 J
0.81
0.12 U
0.12 U
Aug-2009
NS
NS
NS
NS
NS
17
4.141
NS
NS
NS
NS
4.59 J
6.611
ND
4.22J
2.78 U
2.78 U
2.78 U
2.78 U
NS
NS
NS
Jan-2010
NS
5.2J
NS
1.91
NS
0.12U
2.7J
0.2J
5.01
2.0J
0.2J
3.01
0.12U
0.2J
0.12U
0.21
0.51
0.12U
0.4J
2.8J
0.12U
0.12U
0.12U
0.12U
May-2010
NS
1.01
NS
3.51
NS
11
1.01
1.11
7.3 J
7.5 1
9.81
4.41
0.32 U
0.61
0.32 U
0.32 U
0.32 U
NS
0.32 U
0.32 U
0.71
0.32 U
0.32 U
Nov-2010
NS
1.8 J
NS
0.32 U
NS
0.32 U
8.8 J
0.7 J
0.32 U
7.2 J
1.11
4.7 J
0.32 U
0.32 U
0.32 U
1.3 J
0.8 J
NS
0.32 U
0.32 U
0.6 J
0.32 U
0.32 U
May-2011
NS
0.46 J
NS
0.20 U
NS
3.5 1
1.11
0.73 J
4.9 J
1.3 1
3 1
3.0 J
0.20 U
1.11
0.20 U
1.71
0.381
NS
0.441
0.3 J
0.22 J
0.641
0.33 J
Nov-2011
Damaged
1.2 J
0.38 J
1.3 J
0.20 U
6.61
2.3 J
0.61 J
5.91
1.6 J
1.11
1.91
0.20 U
0.62 J
0.20 U
2.5 J
0.78 J
0.20 U
0.33 J
0.20 J
0.29 J
0.21 J
0.20 U
May-2012
NS
1.71
NS
13
NS
3.81
4.3 J
1.61
5.0 J
1.5 1
4.3 J
4.5 1
0.17 U
0.93 J
0.72 J
3.71
0.641
NS
1.4 J
0.411
0.57 J
0.17 U
0.17 U
Nov-2012
Damaged
1.2J
0.55J
15
0.52J
0.3J
11
1.2J
4.3J
0.64J
1.91
6.9J
0.21J
2.1J
1.11
4.1J
1.01
0.23J
0.94J
0.17J
0.30J
0.26J
0.17U
May-2013
Damaged
1.61
0.06 J
14
0.231
5.41
4.9 J
1.11
4.4 J
2.71
9.91
6.81
0.081
1.71
1.11
5.7 J
0.831
0.271
5.5 J
0.39 J
0.38 J
0 191
Dry
May-2014
NS
0.06 U
NS
0.38 J
NS
2.9 J
0.06 U
0.06 U
0.06 U
0.06 U
3.4 J
4.9 J
0.06 U
0.06 U
0.06 U
1.3 J
0.06 U
NS
0.06 U
0.06 U
0.06 U
0.06 U
Dry
Nov-2014
NS
3.01
NS
0.16 U
NS
0.16 U
7.2 J
2.6 J
Damaged
1.7 J
0.44 U
0.16 U
0.44 U
1.8 1
0.44 U
0.44 U
0.621
NS
0.16 U
0.16 U
0.16 U
0.16 U
Dry
May-2015
0.24 J
0.35 J
0.71 J
0.22 U
0.22 U
9.4 J
0.53 U
1.4 J
0.53 U
0.46 J
0.53 U
4.3 J
0.22 U
1.10 J
1.40 J
3.40 J
0.591
0.22 U
0.28 J
0.22 U
0.29 J
0.22 U
0.22 U
Nov-2015
NS
0.23 J
NS
0.26 J
NS
0.791
0.22 U
1.81
10
0.81 J
9.6 J
1.7 J
0.22 U
2.51
0.911
0.911
0.631
NS
0.22 U
0.46 J
0.22 U
0.22 U
0.22 U
May-2016
NS
0.54 U
NS
1.31
NS
2 J
1.11
0.76 J
Dry
3.21
9.9 J
8.6 J
0.54 U
4.6 J
0.77 J
6.71
0.73 J
NS
0.54 U
0.54 U
0.54 U
0.54 U
0.54 U
Nov-2016
NS
1.61
NS
2.61
NS
0.62 U
9.7 J
1.71
Dry
6.31
0.62 U
0.62 U
0.62 U
9 4 U
1.4 J
0.62 U
1.11
NS
0.69 J
0.54 U
0.76 J
0.54 U
Dry
May-2017
0.51U
0.51U
0.51U
1.31
0.51 U
0.51 U
0.51U
1.01
3.6 J
0.52 J
5.0 J
0.51U
0.51U
SAJ
0.74J
9.91
0.771
0.51 U
0.51U
1.81
0.51U
0.95 J
0.89 J
ND
ND
Dec-2017
0.631
0.71J
0.51U
0.5U
0.741
0.51U
0.5U
0.59J
3.8J
03U
0.5U
0.5U
0.5U
3.11
1.81
0.5U
0.771
0.51 U
0.571
1.81
3.0J
1.2J
Dry
0.86J
0.51U
0.51U
Jun-2018
E
0.33J
0.56J
0.311
2.1J
0.3J
0.15U
2.5J
0.79J
2.2J
2.5J
2.7J
4.5J
0.38J
4.3J
2J
0.53U
1.2J
0.36J
11
0.96J
2.7J
0.891
Dry
0.6J
0.56J
Dry
Dec-2018
0.3 J
1.91
0.191
I 4.61
I 0.6 J
NS
NS
0.74 J
1 4.4 J
3.71
NS
NS
0.15 U
1 7.91
1.11
8.11
0.851
1 0.15 U
0.15 U
0.15 U
2.11
1.4
0.15 U
0.15 U
0.15 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell Shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Silver CAS No. 7440-22-4
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MIN-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
20
WER
NS
ND
ND
ND
ND
ND
ND
B - DETECTED
IN TRIP
BLANK
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
0.52 U
Nov-2007
NS
0.04 U
NS
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
Dry
0.04 U
0.04 U
May-2008
0.04 U
0.2 J
0.04 U
0.11
0.11
0.04 U
0.11
0.11
0.11
0.04 U
0.04 U
0.11
0.04 U
0.11
Nov-2008
NS
0.04 U
NS
0.04 U
0.04 U
0.11
0.04 U
0.11
0.04 U
0.11
0.04 U
Dry
0.11
0.11
May-2009
NS
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.11
0.04 U
0.04 U
0.04 U
0.04 U
0.11
0.11
0.04 U
Aug-2009
NS
NS
NS
NS
NS
8.22 JB
7.151B
NS
NS
NS
NS
7.77 JB
7.15 JB
6.95JB
6.92JB
6.87JB
6.91 JB
6.77 JB
7.2 JB
NS
NS
NS
Jan-2010
NS
0.11
NS
0.2 1
NS
0.2 J
0.11
0.11
0.11
0.11
0.3 1
0.31
0.11
0.11
0.04 U
0.11
0.11
1.11
0.11
0.2 J
0.2 J
0.11
0.2 J
0.11
May-2010
NS
0.11
NS
0.03 U
NS
0.11
0.03 U
0.11
0.11
0.03 U
0.03 U
0.11
0.03 U
0.03 U
0.11
0.03 U
0.03 U
NS
0.03 U
0.03 U
0.11
0.03 U
0.03 U
Nov-2010
NS
0.03 U
NS
0.03 U
NS
0.03 U
0.03 U
0.03 U
0.11
0.11
0.11
0.11
0.03 U
0.03 U
0.03 U
0.11
0.03 U
NS
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
May-2011
NS
0.02 U
NS
0.02 U
NS
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
NS
0.02 U
0.02 U
0.02 U
0.041
0.02 U
Nov-2011
Damaged
0.02 U
0.02 U
0.02 U
0.02 U
0.04 J
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
May-2012
NS
0.1U
NS
0.1U
NS
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
NS
0.1U
0.1U
0.1U
0.1U
0.1U
Nov-2012
Damaged
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
0.1U
May-2013
Damaged
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 J
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
Dry
May-2014
NS
0.03 U
NS
0.03 U
NS
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
NS
0.03 U
0.03 U
0.03 U
0.03 U
Dry
Nov-2014
NS
0.04 U
NS
0.04 U
NS
0.04 U
0.04 U
0.06 J
Damaged
0.04 U
0.04 U
0.04 U
0.04 U
0.04 U
0.04 J
0.04 U
0.04 U
NS
0.04 U
0.04 U
0.04 U
0.04 U
Dry
May-2015
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
0.02J
0.02J
0.01U
0.02J
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
0.01U
o.01U
Nov-2015
NS
0.01U
NS
0.01U
NS
0.01U
0.03J
0.02J
0.03J
0.011
0.01U
0.02J
0.01U
0.01U
0.01U
0.031
0.01U
NS
0.02J
0.01U
0.01U
0.01U
0.031
May-2016
NS
0.06 U
NS
0.06 U
NS
0.06 U
0.06 U
0.06 U
Dry
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
NS
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
Nov-2016
NS
0.06 U
NS
0.06 U
NS
0.06 U
0.06 U
0.06 U
Dry
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
0.06 U
NS
0.06 U
0.06 U
0.06 U
0.06 U
Dry
May-2017
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
Dec-2017
0.24 J
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
0.20 U
Dry
0.20U
0.20U
0.20U
Jun-2018
0.06 J
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Dry
Us U
0.05 U
Dry
Dec-2018
0.09 J
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.1
0.05 U
0.05 U
0.05 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell Shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Sulfide CAS No. 18496-25-8
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
213 Std
MW-ID
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MIN-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
NE
0.21
Nov-01
May-02
Nov-02
May-03
Nov-03
May-04
Nov-04
May-05
Nov-05
May-06
Nov-06
May-07
Jun-2007
Nov-2007
May-2008
Nov-2008
May-2009
Aug-2009
1341
ND
ND
ND
ND
ND
Jan-2010
100 U
100 U
100 U
May-2010
100 U
100 U
100 U
Nov-2010
1380
100 U
100 U
May-2011
544 J
100 U
100 U
Nov-2011
2795
100 U
100 U
May-2012
137 J
100 U
100 U
Nov-2012
100 U
100 U
100 U
644 J
100 U
100 U
May-2013
100 U
100 U
100 U
272 J
100 U
100 U
May-2014
100 U
467 J
100 U
100 U
2301
Nov-2014
100 U
100 U
100 U
100 U
100 U
May-2015
1041
100 U
100 U
100 U
100 U
Nov-2015
100 U
100 U
100 U
100 U
100 U
May-2016
100 U
100 U
100 U
100 U
100 U
346 J
Nov-2016
100 U
100 U
100 U
100 U
240 J
May-2017
1000
1000
1000
1000
1000
1000
1000
NA
NA
NA
NA
1000
1000
4,790
1000
537J
1000
1000
1000
1000
1000
Dec-2017
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
Jun-2018
100.0
1471
1611
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
1182
100 U
298 J
1581
100 U
100 U
100 U
100 U
100 U
Dec-2018
100 U
100 U
100 U
100 U
100 U
100 U
100 U
100 U
390 J
100 U
100 U
100 U
100 U
328 J
100 U
115 J
100 U
100 U
100 U
100 U
100 U
100 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, J (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Thallium CAS No. 7440-28-0
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
0.2
0.47
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
ND
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
Nov-2007
NS
0.04 U
NS
0.2 1
0.04 U
0.04 U
0.04 U
0.04 U
0.2 J
0.04 U
0.04 U
Dry
0.04 U
0.04 U
May-2008
ND
0.1 J
0.04 U
0.11
0.04 U
0.04 U
0.11
0.11
0.21
0.11
0.04 U
0.2 J
0.04 U
0.04 U
Nov-2008
NS
0.04 U
NS
0.11
0.04 U
0.04 U
0.04 U
0.04 U
0.11
0.11
0.04 U
Dry
0.11
ND
May-2009
NS
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
Aug-2009
NS
NS
NS
NS
NS
0.198 U
0.198 U
NS
NS
NS
NS
0.198 U
0.198 U
0.198 U
0.198 U
0.198 U
0.198 U
0.198 U
0.198 U
NS
NS
NS
Jan-2010
NS
0.11
NS
0.03 U
NS
0.03 U
0.11
0.11
0.11
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 U
0.03 11
0.11
0.11
0.11
0.03 U
May-2010
NS
0.05 U
NS
0.05 U
NS
0.05 U
0.05 U
0.11
0.05 U
0.05 U
0.5 J
0.11
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
NS
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
Nov-2010
NS
0.05 U
NS
0.11
NS
0.05 U
0.05 U
0.11
0.5 J
0.11
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
NS
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
May-2011
NS
0.02 U
NS
0.11
NS
0.02 U
0.02 U
0.03 J
0.07 1
0.91
0.241
0.02 U
0.02 U
0.05 J
0.02 U
0.08 J
0.041
NS
0.041
0.051
0.02 U
0.02 U
0.091
Nov-2011
Damaged
0.02 U
0.02 U
0.07 J
0.02 U
0.24 J
0.141
0.05 J
0.161
0.08 J
0.08 J
0.02 U
0.08 J
0.05 J
0.12 1
0.04 J
0.07 J
0.02 U
0.051
0.02 U
0.02 U
0.12 1
0.09 J
May-2012
NS
0.35 J
NS
0.22 J
NS
0.07 U
0.101
0.07 U
0.07 U
0.10 J
0.261
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
NS
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
Nov-2012
Damaged
0.07 U
0.07 U
0.10 J
0.07 U
0.07 U
0.13 J
0.07 U
0.07 U
0.07 U
0.29 J
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
0.07 U
May-2013
Damaged
0.04 J
0.02 U
0.07 J
0.181
0.02 U
0.081
0.02 U
0.071
0.10 J
0.201
0.06 J
0.02 U
0.02 U
0.141
0.02 U
0.02 U
0.02 U
0.30 J
0.05 1
0.02 U
0.061
Dry
May-2014
NS
0.02 U
NS
0.07 J
NS
0.02 U
0.06 J
0.02 U
0.021
0.02 U
0.26 J
0.03 J
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
NS
0.13 J
0.021
0.02 U
0.02 U
Dry
Nov-2014
NS
0.13U
NS
0.13U
NS
0.13U
0.13U
0.13U
Damaged
0.13U
0.13U
0.13U
0.13U
0.13U
0.13U
0.13U
0.13U
NS
0.151
0.13U
0.13U
0.13U
Dry
May-2015
0.03 J
0.02 U
0.04 J
0.06 J
0.03 J
0.02 U
0.02 U
0.05 J
0.07 J
0.10 J
0.101
0.06 J
0.02 U
0.02 U
0.30 J
0.02 U
0.03 J
0.02 U
0.02 J
0.03 J
0.02 J
0.03 J
0.04 J
Nov-2015
NS
0.02 U
NS
0.07 J
NS
0.02 U
0.16 J
0.05 J
0.09 1
0.06 J
0.041
0.18 J
0.02 U
0.02 U
0.031
0.07 J
0.061
NS
0.13 1
0.02 U
0.02 U
0.041
0.07 J
May-2016
NS
0.05 U
NS
0.07 J
NS
0.05 U
0.05 U
0.05 U
Dry
0.18 J
0.09 J
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.07 J
NS
0.07 J
0.05 U
0.06 J
0.05 U
0.05 U
Nov-2016
NS
0.05 U
NS
0.101
NS
0.05 U
0.05 U
0.05 U
Dry
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
NS
0.05 U
0.05 U
0.05 U
0.05 J
Dry
May-2017
0.08U
0.08U
0.08U
0.08U
0.08U
0.08U
0.08U
0.08U
0.11 J
0.08U
0.08U
0.08U
0.08U
0.08U
0.08U
0.08U
0.08 J
0.08U
0.08U
0.08U
0.08U
0.08U
0.08U
0.10 J
Dec-2017
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 J
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.08 U
0.12 J
1
0.13 1
0.08 U
Dry
0.08 U
0.08 U
0.08 U
Jun-2018
0.05 U
0.05 U
0.11 J
0.05 U
0.05 U
0.05 U
0.05 U
0.06 J
0.05 U
0.1 1
0.06 J
0.05 U
0.05 U
0.05 U
0.06 J
0.05 U
0.05 U
0.05 U
0.06 J
0.07 J
0.11
0.05 U
Dry
0.05 U
0.05 U
Dry
Dec-2018
0.05 U
0.05 U
0.05 U
0.08 J
0.05 U
0.05 U
0.05 U
1 0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.0511
0.05 U
0.05 U
0.05 U
0.1
0.05 U
0.05 U
0.07 J
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Tin CAS No. 7440-31-5
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPs
26 Std
MW-ID
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
2000*
800
B = DETECTED
IN TRIP
BLANK
Nov-01
May-02
Nov-02
May-03
Nov-03
May-04
Nov-04
May-05
Nov-05
May-06
Nov-06
May-07
Nov-2007
May-2008
Nov-2008
May-2009
Aug-2009
12.9 JB
5.341B
5.12 JB
5.36 JB
6.021B
41B
Jan-2010
0.08 U
0.08 U
0.08 U
May-2010
1.51
3.9 J
0.4 J
Nov-2010
0.5 J
0.6 J
0.5 J
May-2011
0.23 J
0.321
0.95 J
Nov-2011
0.26 J
0.47 J
0.24 J
May-2012
0.15 J
0.241
0.10 U
Nov-2012
0.1 U
0.1 U
0.17 J
0.13 J
0.28 J
0.92 J
May-2013
0.241
0.24 J
0.201
0.08 J
May-2014
0.06 U
0.06 U
0.06 J
0.06 U
0.06 U
Nov-2014
0.05 U
0.96 J
0.05 U
0.22 J
0.18 J
May-2015
0.6 U
0.13 J
0.06 U
0.06 J
0.12 J
Nov-2015
0.11 J
0.14 J
0.35 J
0.20 J
0.35 J
May-2016
0.6 U
0.11 J
0.06 U
0.09 J
0.33 J
Nov-2016
0.6 U
0.06 U
0.06 U
0.06 U
0.06 U
May-2017
0.52J
0.13 U
0.14J
0.13U
0.28J
0.22 J
0.21 J
NA
NA
NA
NA
0.20 J
0.13U
0.13U
0.13U
0.13U
0.13U
0.13U
NA
0.13U
0.13U
Dec-2017
0.911
0.13U
0.13U
0.13U
0.13U
0.23J
0.241
0.13U
0.13U
0.14J
0.13U
0.13U
0.13U
0.13U
0.13U
0.24J
0.13U
0.21J
0.241
0.13U
0.181
0.22J
Jun-2018
0.1 J
0.05 U
0.05 U
0.05 U
1.2 J
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.43 J
0.57 J
Dec-2018
0.171
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.24 J
0.55 J
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
0.05 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3. * = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Vanadium CAS No. 7440-62-2
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-ID
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
0.3*
NE
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
48
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
124
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
98
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
115
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
44
45
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
0.42 U
ND
ND
ND
Nov-2007
NS
1.51
NS
0.91
0.7 J
1.7 J
6.9 J
1.6 J
17 J
2.5 J
2.4 J
Dry
2.01
0.71
May-2008
0.07 U
0.81
0.07 U
0.07 U
1.11
0.07 U
3.4 J
1.2 J
4.6 J
3.1 J
1.0 J
40
1.41
0.81
Nov-2008
NS
2.6 J
NS
1.3 J
0.11
1.51
3.1 J
1.8 1
4.2 J
1.3 J
0.8 J
Dry
9.2 1
1.21
May-2009
NS
3.5 J
2.6 J
1.81
1.01
2.7 J
10.01
1.61
7.5 J
1.81
1.3 J
30
2.3 1
1.91
Aug-2009
NS
NS
NS
NS
NS
0.586 U
0.586 U
NS
NS
NS
NS
0.586 U
0.586 U
0.586 U
0.586 U
0.586 U
0.586 U
0.586 U
0.586 U
NS
NS
NS
Jan-2010
NS
11
NS
3.5J
NS
2.3J
2.1J
11.4J
5.21
11.61
0.81
0.91
4.9J
4.5J
1.3J
2.4J
4.9J
1AJ
35
15.7J
18.9J
0.81
0.91
0.61
May-2010
NS
3.8J
NS
2.1J
NS
2J
0.81
8.3J
2.3J
5.8J
1.3J
2.6J
0.6J
3.2J
1.01
3.7J
2.4J
NS
3.3J
2.01
1.51
1.41
3.0J
Nov-2010
NS
3.3J
NS
0.6J
NS
2.6J
1.6J
9.4J
3.2J
4.4J
1.11
1.91
0.91
1.91
0.6J
4.4J
3.6J
NS
8.51
3.1J
1.11
0.91
0.91
May-2011
NS
1.2J
NS
0.94J
NS
1.4J
0.69J
7.5J
4.3J
3.9J
0.75J
0.76J
1.2J
3.1J
0.54J
2.9J
1.01
NS
11.81
6.81
0.86J
0.931
7.2J
Nov-2011
Damaged
2.5J
2.0J
0.75J
0.41
3J
0.88J
8.5J
2.4J
3.3J
1.2J
4.1J
1.3J
9.2J
0.55J
4.81
1.4J
0.3J
8.4J
2.2J
3.4J
1.11
0.88J
May-2012
NS
1.7J
NS
2.0J
NS
1.4J
2.0J
7.2J
5.6J
3.0J
1.3J
1.3J
0.96J
5.9J
0.78J
6.9J
2.2J
NS
31
9.51
2.5J
1.01
3.0J
Nov-2012
Damaged
1.2J
1.5J
1.7J
0.1U
1.81
1.6J
5.8J
2.0J
4.7J
0.52J
1.2J
0.25J
4.1J
0.44J
6.4J
3.0J
0.41J
22.7J
1.51
0.83J
0.67J
2.3J
May-2013
Damaged
1.0 J
1.3 J
0.62 J
0.93 J
1.9 J
0.39 J
3.3 J
3.5 J
1.5 J
1.3 J
1.3 J
0.071
4.6 J
0.35 J
7.8 J
2.0 J
0.07 U
8.2 J
3.11
1.5 1
3.41
Dry
May-2014
NS
0.16J
NS
0.07U
NS
1.3J
0.07U
3.2J
1.11
0.34J
1.3J
1.01
0.07U
2.9J
0.07U
4.1J
1.4J
NS
1.4J
6.0J
0.48J
1.2J
Dry
Nov-2014
NS
0.96 J
NS
2.3 J
NS
2.5 J
0.141
0.44 J
Damaged
1.2 J
1.3 J
1.11
0.48 J
4.4 J
0.34 J
11.0 J
1.3 J
NS
4.3 J
0.30 J
0.06 U
1.31
Dry
May-2015
0.88J
1.01
1.91
0.591
0.26J
2.2J
0.46J
6.3J
5.5J
1.11
2.9J
0.94J
0.22U
4.90J
0.22U
5.10J
1.20J
0.22U
1.60J
1.1J
0.94J
2.5J
1.11
Nov-2015
NS
2.3J
NS
2.8J
NS
3.2J
1.5J
5.3J
1.2J
4.1J
1.91
1.2J
0.911
5.3J
0.54J
3.2J
5.8J
NS
27
1.31
0.841
1.71
1.5J
May-2016
NS
4.0J
NS
0.36U
NS
3.4J
1.5J
3.4J
Dry
4.9J
3.0J
1.8J
0.36U
8.7J
0.36U
16.5J
10.51
NS
5.7J
1.6J
0.70J
1.7J
0.53J
Nov-2016
NS
2.0J
NS
0.39J
NS
3.3J
1.91
2.7J
Dry
5.6J
1.6J
3.0J
0.36U
8.5J
0.59J
16.4J
1.5J
NS
2.6J
0.571
0.541
1.01
Dry
May-2017
2.2J
2.8J
2.0J
2.4J
1.6J
5.3J
4.3J
5.91
17.2J
17.9J
4.3J
3.7J
0.24U
8.51
0.24U
17.9J
0.911
1.41
5.91
71
4.5J
0.74J
0.71J
0.95J
5.6J
Dec-2017
4.2J
1.11
0.98J
5.3J
0.35J
5.2J
4.1J
4.6J
3.0J
7.5J
1.11
2.7J
1.5J
9.1J
1.5J
21.3J
6.6J
0.59J
20.1J
34
12.0J
8.8
7.1J
Dry
1.31
1.31
1.11
Jun-2018
E
1.4
1.2
2.7
0.83 J
3.0
5.8
4.0
5.1
4.6
1.2
1.3
1.7
1.2
8.0
2.7
16.0
15.0
0.05 J
2.1
21
5.2
Dry
1.4
1.8
Dry
Dec-2018
2
1.8
0.03 U
1.2
0.03 U
7.2
3.1
5
1.3
2
2.4
1.6
0.03 U
8.1
1.5
17.5
1.3
0.03 U
2.3
3.5
9.1
1.2
8.4
0.111
0.571
0.7 J
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3. * = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Zinc CAS No. 7440-66-6
Sample
BG BG Assessment Wells Asst. BG Asst. old B-20
BG BG
Date
GWPS
26 Std
MW-lD
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
1000
WER
NS
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
53
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
99
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
57
ND
ND
ND
ND
ND
ND
ND
ND
May-03
NS
ND
ND
ND
ND
ND
ND
ND
134
ND
ND
ND
Nov-03
ND
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
16
0.2U
19
0.2U
0.2U
0.2U
0.2U
0.2U
0.2U
26
0.2U
15
Nov-2007
NS
7.91
NS
3.3 1
3.6 J
8 J
16
5.9 J
20.0
3.4 J
5.11
Dry
24
71
May-2008
1.0
4.5J
2.2
1.91
2.6J
1.6J
7.8J
4.1J
3.01
3.4J
2.7J
43
7.8J
19
Nov-2008
NS
5.11
NS
2.41
3.3 J
3.3 1
5.3 1
3.9 J
3.6 J
3.01
1.7 J
Dry
96
36
May-2009
NS
9.41
14
5 J
5.91
5.91
12
3.3 J
2.5 J
2.8 J
3.2 J
21
4.8 J
18
Aug-2009
NS
NS
NS
NS
NS
1.29 U
1.29 U
NS
NS
NS
NS
1.29 U
1.661B
1.29 U
1.29 U
1.29 U
4.631B
1.29 U
1.481B
NS
NS
NS
Jan-2010
NS
2.2J
NS
3J
NS
1.31
3.1J
16
4.8J
3.9J
1.5J
3.1J
7.5J
2.6J
2.9J
2.8J
8.5J
21
4.7J
15.0
15.0
8.1J
14.0
8.81
May-2010
NS
2.21
NS
5.81
NS
2.3J
2.91
8.51
4.3J
3.31
3.8J
6.31
1.5J
4.01
2.0J
1.11
7.5J
NS
1.2J
2.3J
5.31
11.0
3.01
Nov-2010
NS
5.6J
NS
3.5J
NS
3.4J
4.1J
8.1J
14.0
4.5J
4.3J
5.4J
2.6J
2.1J
3.2J
3.1J
8.51
NS
2.6J
5.6J
6.8J
17.0
3.9J
May-2011
NS
2.61
NS
3.11
NS
3.61
3.2J
6.11
7.4J
1.81
2.4J
5.41
3.2J
3.51
2.1J
3.51
32
NS
2.6J
9.6J
12.0
5.8J
9.41
Nov-2011
Damaged
3.2J
1.11
2.0J
1.7J
2.7J
4.7J
9.4J
7.7J
3.3J
1.8J
5.3J
2.3J
1.7J
1.91
1.8J
3.2J
3.21
4.7J
1.91
8.2J
16.0
2.4J
May-2012
NS
1.41
NS
2.01
NS
0.72 J
5.7 J
4.71
6.6 J
0.911
0.661
3.21
0.661
0.48 U
1.7 J
0.48 U
8.11
NS
6.2 J
6.4 J
18.0
6.0 J
0.70 J
Nov-2012
Damaged
4.7J
1.81
4.6J
2.5J
7.6J
8.4J
6.7J
5.81
4.9J
4.6J
5.5J
4.4J
3.1J
6.4J
4.1J
3.3J
6.1J
4.6J
4.8J
6.5J
8.2J
11.0
May-2013
Damaged
0.76J
5.4J
2.41
5.0J
1.21
3.8J
1.61
6.1J
0.911
1.01
2.91
3.7J
2.11
3.8J
1.91
3.5J
4.21
5.6J
4.1J
5.21
6.8J
Dry
May-2014
NS
0.88J
NS
1.11
NS
2.6J
1.4J
1.8J
2.0J
0.84J
1.91
3.4J
3.4J
1.3J
1.3J
2.0J
2.4J
NS
2.6J
9.9J
2.3J
2.7J
Dry
Nov-2014
NS
1.21
NS
3.21
NS
2.41
3.0 J
50
Damaged
0.54 J
1.4 J
2.81
1.3 J
1.41
3.1 J
1.91
4.6 J
NS
5.7 J
3.7 J
2.01
5.7 J
Dry
May-2015
16
3.3J
3.5J
0.37J
3.3J
0.94J
0.27J
8.3J
15
2.5J
2.5J
1.51
2.0J
1.101
3.0J
13
1.30J
11
16
2.9J
3.0J
6.4J
5.2J
Nov-2015
NS
1.71
NS
3.21
NS
1.71
6.9J
5.91
6.61
6.21
6.1J
1.31
4.8J
2.81
4.5J
6.01
3.6J
NS
35
4.7J
4.8J
9.4J
9.8J
May-2016
NS
3.4J
NS
2.5J
NS
3.8J
3.7J
3.4J
Dry
3.2J
2.3J
1.91
3.1J
2.1J
1.91
2.0J
4.5J
NS
12
3.6J
2.4J
5.2J
6.3J
Nov-2016
NS
1.81
NS
1.61 U
NS
2.5 1
2.6 1
1.81
Dry
1.91
2.7 J
3.5 1
1.91
1.61 U
2.4 J
2.01
1.61 U
NS
6.8 J
2.4 J
2.91
5.0 J
Dry
May-2017
11
1.81
5.4J
3.41
5.2J
2.6J
3.7J
3.3J
27.0
6.1J
2.8J
2.9J
2.5J
1.91
2.5J
1.51
1.91
8AJ
13
4.9J
32J
0.76J
1.81
2.6J
8.1J
Dec-2017
51
4.3J
2.71
4.0J
2.11
4.2J
8.21
5.6J
2.7J
2.81
1.11
1.91
3.7J
3.81
3.2J
5.51
2.3J
7.41
21
5.81
6.9J
5.01
Dry
2.1J
4.6J
10.0
Jun-2018
6.5J
1.11
5.7J
5.2J
6.8J
1.11
3.2J
3.3J
4.5J
0.11U
0.191
1.5J
1.6J
0.32J
2.2J
2J
1.6J
4.7J
51
2.4J
5.4J
8.6J
Dry
1.6J
5.2J
Dry
Dec-2018
14
8.11
1.81
2.3J
1.8J
3.61
3.1J
4J
3.5J
1 2.31
3.4J
3J
3.3J
1.51
1.3J
1 1.21
0.911
2J
4.6J
0.87J
0.841
1.51
22.0
1.71
3.6J
4.51
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Acetone CAS No. 67-64-1
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-II
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
6,000
2,000
ND
ND
ND
NU
ND
ND
ND
ND
ND
Nov-01
NA
ND
NA
ND
ND
ND
ND
ND
ND
May-02
NA
ND
NA
ND
ND
ND
ND
ND
ND
Nov-02
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
247
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Jun-2007
20.21
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2007
NA
ND
NA
2.2J
ND
3.3J
ND
1.8J
2.7J
1.7J
2.3J
Dry
2.31
2.2J
May-2008
2.1J
3.31
2.5J
2.71
3.5J
5.61
3.11
4.1J
4.51
3.4J
4.51
4.5J
5.51
3.8J
Nov-2008
NA
1.7 J
NA
3.4J
ND
4.5J
1.31
1.51
2.7J
2.4J
2.8J
ND
3.71
5.3J
May-2009
NA
3 J
ND
ND
2.1 J
ND
ND
ND
ND
ND
ND
1.31
ND
Aug-2009
NA
NS
NA
NS
NA
ND
ND
NS
NS
NS
NS
ND
ND
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
Jan-2010
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2010
NA
ND
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
ND
ND
Nov-2010
NA
ND
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
29J
ND
NA
ND
ND
ND
ND
ND
May-2011
NA
ND
NA
ND
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NA
ND
ND
ND
ND
ND
Nov-2011
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
10.101
ND
ND
ND
ND
ND
ND
ND
May-2012
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2012
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2013
NA
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Dry
May-2014
NA
ND
NA
9.06 U
NA
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
NA
9.06 U
9.06 U
9.06 U
9.06 U
Dry
Nov-2014
NA
ND
NA
9.06 U
NA
9.06 U
9.06 U
9.06 U
Damaged
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
NA
9.06 U
12.50 J
9.06 U
9.06 U
Dry
May-2015
9.06 U
9.06 U
9.501
9.06 U
9.06 U
9.101
9.06 U
9.06 U
22.0 J
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
16.401
9.06 U
9.06 U
9.06 U
9.06 U
9.20 J
9.06 U
9.06 U
Nov-2015
NA
9.06 U
NA
9.06 U
NA
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
NA
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
May-2016
NA
9.06 U
NA
9.06 U
NA
9.06 U
9.06 U
9.06 U
Dry
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
NA
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
Nov-2016
NA
9.06 U
NA
9.06 U
NA
9.60 J
12.00 J
9.06 U
Dry
9.06 U
9.06 U
17.20 J
9.06 U
9.06 U
9.06 U
12.30 J
9.06 U
NA
9.06 U
9.06 U
9.06 U
9.06 U
NS
May-2017
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
10.31
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
9.06U
Dec-2017
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
12.2 J
9.06 U
9.06 U
9.06 U
13.3 J
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
Dry
9.06U
9.06U
9.06U
Jun-2018
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
10.3 J
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
Dry
9.06 U
9.06 U
Dry
Dec-2018
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.44 J
9.06 U
9.06 U
1 9.06 U
9.06 U
10.3 J
9.63 J
9.06 U
9.06 U
9.06 U
11.8 J
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
9.06 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Benzene CAS No. 71-43-2
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
2B Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-II
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
1
51
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
NS
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Jun-2007
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2007
NS
ND
NS
ND
ND
1
ND
ND
0.2 J
0.3 J
0.7 J
Dry
ND
ND
May-2008
ND
ND
ND
ND
ND
1.1
ND
ND
ND
ND
0.5 J
ND
ND
ND
Nov-2008
NS
ND
NS
ND
ND
2.1
ND
ND
ND
ND
0.5 J
ND
ND
ND
May-2009
NS
ND
ND
ND
ND
1.5
ND
ND
ND
ND
0.3 J
ND
ND
ND
Aug-2009
NS
NS
NS
NS
NS
1.3
ND
NS
NS
NS
NS
1.9
ND
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
Jan-2010
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2010
NS
ND
NS
ND
NS
3.1
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2010
NS
0.61
NS
ND
NS
2.1
0.91
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
May-2011
NS
0.3 J
NS
ND
NS
1
ND
ND
ND
ND
ND
0.40 J
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2011
NS
ND
ND
ND
ND
2.1
0.61
ND
ND
ND
ND
0.40 J
ND
ND
ND
0.30 J
ND
ND
ND
ND
ND
ND
ND
May-2012
NS
ND
NS
ND
NS
1
0.60J
ND
ND
ND
ND
1.1
ND
ND
ND
1.2
ND
NS
ND
ND
ND
ND
ND
Nov-2012
NS
ND
ND
0.61
ND
2.2
0.701
ND
ND
ND
ND
1.6
ND
ND
ND
0.70 J
ND
ND
ND
ND
ND
ND
ND
May-2013
NS
ND
ND
ND
ND
ND
0.30J
ND
ND
ND
ND
ND
ND
ND
ND
1.1
ND
ND
0.40J
ND
ND
ND
Dry
May-2014
NS
0.24 U
NS
0.24 U
NS
1.1
0.24 U
0.24 U
0.24 U
0.24 U
0.30 J
1.9
0.24 U
0.24 U
0.24 U
0.4 J
ND
NS
ND
ND
ND
ND
Dry
Nov-2014
NS
0.24 U
NS
0.60 J
NS
2.1
0.50 J
0.24 U
Damaged
0.24 U
0.30 J
0.80 J
0.24 U
0.24 U
0.24 U
1.1
0.24 U
NS
0.50 J
0.24 U
0.24 U
0.24 U
Dry
May-2015
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
1.5
0.24 U
0.24 U
0.24 U
0.24 U
0.601
0.24 U
0.24 U
0.24 U
0.24 U
0.501
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
Nov-2015
NS
0.24 U
NS
0.24 U
NS
1.7
1.7
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
NS
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
May-2016
NS
0.24 U
NS
0.24 U
NS
1.3
0.24 U
0.24 U
Dry
0.24 U
0.401
0.90 J
0.24 U
0.50 J
0.24 U
1.4
0.24 U
NS
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
Nov-2016
NS
0.24 U
NS
0.24 U
NS
1.2
0.80 J
0.24 U
Dry
0.24 U
0.40 J
1.5
0.24 U
0.60 J
0.24 U
1.9
0.24 U
NS
0.24 U
0.24 U
0.24 U
0.24 U
Dry
May-2017
0.24U
0.24U
0.24U
0.24U
0.24U
2.8
2
0.24U
0.24U
0.24U
0.24U
1.2
0.24U
0.401
0.24U
1.7
0.24U
0.24U
0.24U
0.24U
0.24U
0.24U
0.24U
0.24U
0.24U
Dec-2017
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
1.7
2.7
0.24 U
0.24 U
0.24 U
0.24 U
0.6 J
0.24 U
0.24 U
1.0
2.0
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
Dry
0.24U
0.24U
0.24U
Jun-2018
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
1.2
0.51
0.24 U
0.24 U
0.24 U
0.24 U
0.3 J
0.24 U
0.24 U
0.91
1.4
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
Dry
0.24 U
0.24 U
Dry
Dec-2018
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
1.3
1.69
1 0.24 U
1 0.24 U
1 0.24 U
0.24 U
1 0.48 J
1 0.24 U
1.57
0.48 J
1 1.48
1 0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
0.24 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the Sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: 1,2-Dichloroethane CAS No. 78-87-5
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
26 Std
MW-lD
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-II
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
0.4
100
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
NS
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May -OS
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Jun-2007
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2007
NS
ND
NS
ND
ND
0.4J
ND
ND
ND
ND
ND
Dry
ND
ND
May-2008
ND
ND
ND
ND
ND
0.4J
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2008
NS
ND
NS
ND
ND
0.7J
ND
ND
ND
ND
ND
ND
ND
ND
May-2009
NS
ND
ND
ND
ND
0.5 J
ND
ND
ND
ND
ND
ND
ND
ND
Aug-2009
NS
NS
NS
NS
NS
ND
ND
NS
NS
NS
NS
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
NS
ND
Jan-2010
NS
ND
ND
ND
ND
0.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2010
NS
ND
NS
ND
NS
0.5
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2010
NS
ND
NS
ND
NS
0.3 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
May-2011
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.6 J
ND
NS
ND
ND
ND
ND
ND
Nov-2011
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.4J
ND
ND
ND
ND
ND
ND
ND
May-2012
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.1
ND
NS
ND
ND
ND
ND
Nov-2012
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2013
NS
ND
ND
ND
ND
1.0
ND
ND
ND
ND
0.40J
1.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Dry
May-2014
NS
0.27 U
NS
0.27 U
NS
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
NS
0.27 U
0.27 U
0.27 U
0.27 U
Dry
Nov-2014
NS
0.27 U
NS
0.27 U
NS
0.27 U
0.27 U
0.27 U
Damaged
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
NS
0.27 U
0.27 U
0.27 U
0.27 U
Dry
May-2015
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
Nov-2015
NS
0.27 U
NS
0.27 U
NS
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
NS
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
May-2016
NS
0.27 U
NS
0.27 U
NS
0.27 U
0.27 U
0.27 U
Dry
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
NS
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
Nov-2016
NS
0.27 U
NS
0.27 U
NS
0.30 J
0.27 U
0.27 U
Dry
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
NS
0.27 U
0.27 U
0.27 U
0.27 U
Dry
May-2017
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
0.27 U
Dec-2017
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
Dry
0.21U
0.21U
0.21U
Jun-2019
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
Dry
0.27U
0.27U
Dry
Dec-2018
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.24
0.13 J
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.34
0.08 J
0.13 J
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
0.02 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: cis-1,2-Dichloroethene CAS No. 156-59-2
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
26 Std
MW-lD
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-II
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
70
720
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
NS
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Jun-2007
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2007
NS
ND
NS
ND
ND
0.2 J
ND
ND
ND
ND
0.2 J
Dry
ND
ND
May-2008
ND
ND
ND
ND
ND
0.2 J
ND
ND
ND
ND
0.2 J
ND
ND
ND
Nov-2008
NS
1.01
NS
1.4 J
ND
1.3 J
ND
ND
ND
ND
0.2 1
ND
ND
1.6 J
May-2009
NS
ND
ND
ND
ND
0.2J
ND
ND
ND
ND
ND
ND
ND
ND
Aug-2009
NS
NS
NS
NS
NS
0.67J
ND
NS
NS
NS
NS
0.07J
ND
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
Jan-2010
NS
ND
ND
ND
ND
0.3J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2010
NS
ND
NS
ND
NS
0.5 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2010
NS
ND
NS
ND
NS
0.3 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
May-2011
NS
ND
NS
ND
NS
0.3J
ND
ND
ND
ND
ND
0.41
ND
ND
ND
0.6J
ND
NS
ND
ND
ND
ND
ND
Nov-2011
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.21
ND
ND
ND
ND
ND
ND
ND
May-2012
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
8.5
ND
NS
ND
ND
ND
ND
ND
Nov-2012
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4.11
ND
ND
ND
ND
ND
ND
ND
May-2013
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.9J
ND
ND
1.4J
ND
ND
ND
Dry
May-2014
NS
0.25 U
NS
0.25 U
NS
0.25 U
0.25 U
0.25 U
0.25U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.7 J
0.25 U
NS
0.3 J
0.25 U
0.25 U
0.25 U
Dry
Nov-2014
NS
0.25 U
NS
0.25 U
NS
0.25 U
0.25 U
0.25 U
Damaged
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
1.7 J
0.25 U
NS
1.6 J
0.25 U
0.25 U
0.25 U
Dry
May-2015
0.25 U
0.25 U
0.25 U
0.25 U
0.25U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.3 J
0.51
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Nov-2015
NS
0.25 U
NS
0.25 U
NS
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
NS
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
May-2016
NS
0.25 U
NS
0.25 U
NS
0.25 U
0.25 U
0.25 U
Dry
0.25 U
0.25 U
0.25 U
0.25 U
0.5 1
0.25 U
0.8 1
0.25 U
NS
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Nov-2016
NS
0.25 U
NS
0.25 U
NS
0.25 U
0.25 U
0.25 U
Dry
0.25 U
0.25 U
0.25 U
0.25 U
0.41
0.3 J
1.61
0.25 U
NS
0.25 U
0.25 U
0.25 U
0.25 U
Dry
May-2017
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Dec-2017
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.6 J
1.4 J
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Dry
0.25 U
0.25 U
0.25 U
Jun-2018
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.41
0.5 J
0.61
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Dry
0.25 U
0.25 U
Dry
Dec-2018
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.31 J
0.25 U
0.34 J
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Ethylbenzene CAS No. 100-41-4
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-II
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW -I
SW-2
SW-3
SW-4
May-01
600
97
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
NS
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Jun-2007
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2007
NS
ND
NS
0.3J
ND
0.4J
ND
ND
ND
ND
ND
Dry
ND
ND
May-2008
ND
ND
ND
ND
ND
0.3 J
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2008
NS
ND
NS
ND
ND
0.3 J
ND
ND
ND
ND
ND
ND
ND
ND
May-2009
NS
ND
ND
ND
ND
0.2 J
ND
ND
ND
ND
ND
ND
ND
ND
Aug-2009
NS
NS
NS
NS
NS
0.48
ND
NS
NS
NS
NS
ND
0.95J
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
Jan-2010
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2010
NS
ND
NS
ND
NS
0.7J
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2010
NS
ND
NS
ND
NS
0.3 J
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.0
ND
NS
ND
ND
ND
ND
ND
May-2011
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2011
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.61
ND
ND
ND
ND
ND
ND
ND
May-2012
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2.1
ND
NS
ND
ND
ND
ND
ND
Nov-2012
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.5
ND
ND
ND
ND
ND
ND
ND
May-2013
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.2
ND
ND
0.30J
ND
ND
ND
Dry
May-2014
NS
0.21U
NS
0.21U
NS
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
NS
0.21U
0.21U
0.21U
0.21U
Dry
Nov-2014
NS
0.21U
NS
0.21U
NS
0.21U
0.21U
0.21U
Damaged
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.50J
0.21U
NS
0.60J
0.21U
0.21U
0.21U
Dry
May-2015
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
Nov-2015
NS
0.21U
NS
0.21U
NS
0.80J
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
NS
0.21U
0.21U
0.21U
0.21U
0.21U
May-2016
NS
0.21U
NS
0.21U
NS
0.21U
0.21U
0.21U
Dry
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
NS
0.21U
0.21U
0.21U
0.21U
0.21U
Nov-2016
NS
0.21U
NS
0.21U
NS
0.30J
0.21U
0.21U
Dry
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
NS
0.21U
0.21U
0.21U
0.21U
Dry
May-2017
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.30J
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
Dec-2017
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.21 U
0.4J
0.21 U
0.21U
0.21 U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21 U
0.21U
0.21U
0.21U
0.21U
Dry
0.21U
0.21U
0.21U
Jun-2018
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
Dry
0.21U
0.21U
Dry
Dec-2018
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
1 0.21U
1 0.21U
0.21U
0.21U
0.21U
0.44J
0.21U
0.23J
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
0.21U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. ) (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Naphthalene CAS No. 91-20-3
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPs
26 Std
MW-ID
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
6
12
Nov-01
May-02
Nov-02
May-03
Nov-03
May-04
Nov-04
May-05
Nov-05
May-06
Nov-06
May-07
Jun-2007
Nov-2007
May-2008
Nov-2008
May-2009
Aug-2009
ND
ND
ND
ND
ND
Jan-2010
NS
NS
NS
May-2010
ND
ND
ND
Nov-2010
ND
ND
ND
May-2011
ND
ND
ND
Nov-2011
ND
ND
ND
May-2012
ND
ND
ND
Nov-2012
NS
NS
NS
May-2013
NS
NS
NS
May-2014
NS
NS
NS
Nov-2014
2.9 J
0.47 U
0.47 U
0.47U
May-2015
NS
NS
NS
NS
Nov-2015
0.47U
0.47 U
0.47 U
0.47U
May-2016
NS
NS
NS
NS
Nov-2016
0.8 J
0.47 U
0.47 U
0.47U
May-2017
0.47 U
NS
0.47 U
0.47 U
0.47 U
7.7 J
1.81
0.47 U
0.47 U
0.47 U
0.47 U
0.9 J
0.47 U
0.47U
0.47 U
0.47 U
0.47 U
Dec-2017
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.7 J
3.1 J
0.47 U
0.47 U
2.5 1
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.6 J
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
Jun-2018
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0,47 U
0.47 U
0,47 U
0.47 U
0,47 U
0.47 U
047 U
0.47 U
047 U
0.47 U
1.6 J
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
Dec-2018
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
1.08 J
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
0.47 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, J (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Tetrahydrofuran CAS No. 109-99-9
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPs
26 Std
MW-ID
MW-1S
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-125
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-2011
NE
NE
NS
ND
NS
0.7
ND
2.5
ND
ND
0.91
2.3
4.5
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
0.6
ND
Nov-2011
NS
ND
NS
ND
NS
6.7
3.3
ND
ND
1.9
ND
3.9
ND
ND
ND
4.2
ND
ND
0.9
ND
ND
ND
ND
May-2012
NS
1.8
NS
2.4
NS
4.4
5.1
1.4
1.7
2.7
6.4
5.2
ND
ND
18.4
2.5
ND
NS
14.0
ND
ND
ND
ND
Nov-2012
NS
ND
ND
8.5
ND
4.6
3.8
ND
ND
ND
1.2
5.5
ND
ND
6.2
10.9
ND
ND
0.7
ND
ND
ND
ND
May-2013
NS
ND
ND
1.8
ND
5.6
2.4
ND
ND
4.4
20.9
5.4
ND
ND
ND
3.3
ND
ND
7.4
ND
ND
ND
Dry
May-2014
NS
0.39 U
NS
1.0
NS
6.5
0.39 U
0.39 U
0.39 U
0.39 U
10.8
10.2
0.39 U
0.39 U
0.39 U
5.5
0.39 U
NS
0.8
0.39 U
0.39 U
0.39 U
Dry
Nov-2014
NS
0.39 U
NS
17.7
NS
15.6
5.7
0.39 U
Damaged
3.4
7.1
7.7
0.39 U
0.39 U
2.7
10.0
0.39 U
NS
17.3
0.39 U
0.39 U
0.39 U
Dry
May-2015
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
16.9
0.39 U
1.1
0.39 U
0.9
34.7
4.9
0.39 U
0.39 U
6.1
7.1
0.39 U
0.39 U
1.0
0.39 U
0.39 U
0.39 U
0.39 U
Nov-2015
NS
0.39 U
NS
0.39 U
NS
20.9
8.6
0.39 U
0.5
0.39 U
1.6
2.6
0.39 U
0.39 U
2.5
1.8
0.39 U
NS
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
May-2016
NS
0.39 U
NS
0.39 U
NS
14.4
1.3
0.39 U
Dry
8.2
29.7
8.1
0.39 U
14.3
1.5
46.2
0.39 U
NS
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
Nov-2016
NS
0.39 U
NS
0.39 U
NS
10.6
6.1
0.5
Dry
5.6
16.3
11.7
0.39 U
8.8
0.39 U
49.0
0.39 U
NS
0.6
0.7
0.9
0.39 U
Dry
May-2017
14.4
0.39U
0.39U
1.0
0.39U
19.1
12.7
0.5
1.5
0.5
12.8
15.0
0.39U
6.4
0.9
36.4
0.39U
0.39U
0.39U
0.39U
0.39U
0.39U
1.2
0.39U
0.39U
117.0
0.39 U
0.39 U
13.1
0.39 U
23.5
19.1
0.39 U
0.39 U
12.3
3.0
22.2
0.39 U
0.39 U
17.0
58.4
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
Dry
0.39 U
0.39 U
0.39 U
�21
30.5
0.39 U
0.39 U
1.1
0.39 U
28.8
4.5
0.39 U
1.3
5.6
6.3
10.5
0.39 U
3.4
16.0
32.7
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
Dry
0.39 U
0.39 U
Dry
1
1 42.7
0.39 U
1 0.39 U
1 4.85
1 0.39 U
1 35.3
1 24.4
1 0.39 U
1 2.27
1 6.88
1 32
1 21.2
1 0.39 U
25.42
8.02
1 38.75
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
0.39 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRU
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Toluene CAS No. 108-88-3
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MIN-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
600
11
ND
ND
ND
ND
LND
ND
ND
ND
ND
ND
Nov-01
NS
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Jun-2007
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2007
NS
ND
NS
ND
ND
0.20 J
ND
ND
ND
ND
ND
Dry
ND
ND
May-2008
ND
ND
ND
ND
ND
0.301
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2008
NS
ND
NS
ND
ND
0.40J
ND
ND
ND
ND
ND
ND
ND
0.20J
May-2009
NS
ND
ND
ND
ND
0.201
ND
ND
ND
ND
ND
ND
ND
ND
Aug-2009
NS
NS
NS
NS
NS
0.191
0.121
NS
NS
NS
NS
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
NS
ND
Jan-2010
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2010
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2010
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
0.301
ND
ND
ND
May-2011
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2011
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.40 J
0.40 J
0.40 J
May-2012
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.60J
ND
NS
ND
0.501
ND
ND
ND
Nov-2012
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2013
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.30 J
0.30 J
1.3
ND
Dry
May-2014
NS
0.23 U
NS
0.23 U
NS
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
NS
0.23 U
3.3
3.0
0.23 U
Dry
Nov-2014
NS
0.23 U
NS
0.23 U
NS
0.23 U
0.23 U
0.23 U
Damaged
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.30 J
0.23 U
NS
0.23 U
0.23 U
0.30 J
0.23 U
Dry
May-2015
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.301
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.30 J
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
Nov-2015
NS
0.23 U
NS
0.23 U
NS
0.40 J
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
NS
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
May-2016
NS
0.23 U
NS
0.23 U
NS
0.23 U
0.23 U
0.23 U
NS
0.23 U
0.23 U
0.23 U
0.23 U
0.11
0.23 U
0.23 U
0.23 U
NS
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
Nov-2016
NS
0.23 U
NS
0.23 U
NS
0.23 U
0.23 U
0.23 U
NS
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
NS
0.23 U
0.23 U
0.23 U
0.23 U
Dry
May-2017
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.501
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
0.23U
Dec-2017
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.5 J
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
Dry
0.23 U
0.23 U
0.23 U
Jun-2018
2.6
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.3 J
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
Dry
0.23 U
0.23 U
Dry
Dec-2018
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
1 0.23 U
1 0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.24 J
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.23 U
0.38 J
0.23 U
0.23 U
0.23 U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Vinyl Chloride CAS No. 75-01-4
Sample
BG BG Assessment Wells Assmt. BG Assmt. old B-20
BG BG
Date
GWPS
26 Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MIN-5
MW-6
MW-7
MW-8
MW-9A
MW-10
MW-11
MW-12S
MW-13
MW-14D
MW-14S
MW-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
0.03
2.4
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-01
NS
ND
NS
ND
ND
ND
ND
ND
ND
May-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
Nov-02
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-03
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-03
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-04
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-05
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-05
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-06
Damaged
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-06
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-07
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Jun-2007
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2007
NS
ND
NS
ND
ND
0.4
ND
ND
ND
ND
ND
Dry
ND
ND
May-2008
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Nov-2008
NS
ND
NS
ND
ND
0.5
ND
ND
ND
ND
ND
ND
ND
ND
May-2009
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Aug-2009
NS
NS
NS
NS
NS
ND
ND
NS
NS
NS
NS
ND
ND
ND
ND
ND
ND
ND
ND
NS
NS
NS
NS
Jan-2010
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2010
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2010
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
May-2011
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NS
ND
ND
ND
ND
ND
Nov-2011
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
May-2012
NS
ND
NS
ND
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.8
ND
NS
ND
ND
ND
ND
ND
Nov-2012
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.9
ND
ND
ND
ND
ND
ND
ND
May-2013
NS
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
3.0
ND
ND
ND
ND
ND
ND
Dry
May-2014
NS
0.63 U
NS
0.63 U
NS
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
1.1
0.63 U
NS
0.63 U
0.63 U
0.63 U
0.63 U
Dry
Nov-2014
NS
0.63 U
NS
0.63 U
NS
2.0
0.63 U
0.63 U
Damaged
0.63 U
0.63 U
1.4
0.63 U
0.63 U
0.63 U
3.4
0.63 U
NS
0.63 U
0.63 U
0.63 U
0.63 U
Dry
May-2015
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
1.7
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
Nov-2015
NS
0.63 U
NS
0.63 U
NS
0.63 U
0.63 U
0.63 U
0.63 U
0.8
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
NS
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
May-2016
NS
0.63 U
NS
0.63 U
NS
0.63 U
0.63 U
0.63 U
Dry
0.63 U
0.63 U
0.63 U
0.63 U
1.9
0.63 U
3.7
0.63 U
NS
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
Nov-2016
NS
0.63 U
NS
0.63 U
NS
0.63 U
0.63 U
0.63 U
Dry
0.63 U
0.63 U
0.63 U
0.63 U
1.7
0.63 U
4.3
0.63 U
NS
0.63 U
0.63 U
0.63 U
0.63 U
Dry
May-2017
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
1.1
0.63U
4.3
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
0.63U
Dec-2017
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.9 J
0.63 U
3.7
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
Dry
0.63 U
0.63 U
0.63 U
Jun-2018
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
2.7
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
2.0
0.63 U
2.9
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
0.63 U
Dry
0.63 U
0.63 U
Dry
Dec-2018
0.12U
0.12U
0.12U
0.12U
0.12U
1.82
1.09
0.12U
1 0.12U
1 0.18J
1.25
1.48
0.12U
2.2
0.12U
1 2.21
1 0.12U
0.12U
0.12U
0.12U
0.12U
0.12U
0.12U
0.12U
0.12U
0.12U
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = NCAC Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, J (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the Sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
Parameter: Groundwater Elevation
Sample
BG BG Assessment Wells Assmt. BG Assmt. BG old B-20
BG BG
Date
GWPS
2B Std
MW-1D
MW-15
MW-2D
MW-2S
MW-3D
MW-3S
MW-3A
MW-4
MW-S
MIN-6
MW-7
MIN-8
MW-9A
MIN-10
MW-II
MW-12S
MW-13
MW-14D
MW-14S
MIN-15
MW-16
MW-17
SW-1
SW-2
SW-3
SW-4
May-01
NE
NE
11.12
12.00
9.11
10.54
11.48
10.19
10.74
Nov-01
NM
10.83
NM
9.70
10.95
9.57
10.08
May-02
NM
13.06
NM
10.91
11.80
10.30
10.89
Nov-02
NM
12.35
NM
9.95
11.66
10.92
9.73
10.33
11.03
May-03
11.98
13.08
9.74
11.24
11.82
11.72
10.57
10.92
11.85
Nov-03
NM
13.57
NM
11.06
11.96
11.52
10.75
11.24
11.63
May-04
NM
12.42
NM
10.70
11.62
11.29
10.48
10.90
11.60
Nov-04
NM
12.01
NM
10.18
11.46
10.78
10.16
10.61
10.92
May-05
NM
12.63
9.47
10.89
11.69
11.29
10.66
11.10
11.42
Nov-05
NM
13.50
NM
11.55
12.02
11.80
11.03
11.42
11.81
May-06
Damaged
12.45
9.45
10.57
11.68
11.10
10.40
10.89
11.21
Nov-06
NM
13.71
NM
11.29
11.99
11.58
10.95
11.41
11.56
May-07
12.52
13.64
9.85
11.14
11.92
11.59
10.85
11.40
11.63
Nov-2007
NM
11.03
NM
9.56
9.06
10.28
10.74
10.47
9.65
9.98
10.63
May-2008
12.24
11.05
9.52
10.93
10.31
11.02
11.84
11.30
10.58
11.00
11.35
Nov-2008
NM
11.77
NM
10.32
9.83
10.56
11.62
10.90
10.19
10.72
10.76
May-2009
NM
10.31
8.99
9.14
8.41
9.77
10.03
10.14
9.35
9.51
10.07
Aug-2009
NM
NS
NM
NS
NM
9.6
7.8
NS
NS
NS
NS
10.3
12.9
9.4
8.5
8.5
9.4
10.5
11.9
Jan-2010
NM
13.74
NM
11.65
NM
11.42
11.12
12.19
12.04
11.07
11.60
11.70
14.94
13.61
11.52
11.71
12.45
9.49
12.51
14.19
May-2010
NM
11.87
NM
10.83
NM
10.70
10.36
11.62
11.33
10.64
11.06
12.74
13.76
12.50
11.02
12.03
11.22
NM
11.41
Nov-2010
NM
12.71
NM
11.43
NM
11.14
10.61
11.61
11.70
10.88
11.24
11.62
14.50
12.78
8.35
11.25
12.44
NM
12.59
May-2011
NM
11.97
NM
10.56
NM
10.71
10.39
11.49
11.19
10.40
10.85
11.25
13.57
12.33
10.26
11.00
12.01
NM
12.03
Nov-2011
Damaged
12.71
9.47
11.88
10.18
11.29
10.83
11.92
11.64
10.61
11.14
11.76
14.46
12.69
11.24
11.51
12.10
11.71
12.03
May-2012
NM
12.04
NM
10.43
NM
10.53
10.31
11.49
11.10
10.30
10.79
11.36
13.67
12.21
10.33
11.06
11.86
NM
11.99
Nov-2012
Damaged
12.71
9.65
10.50
10.47
10.68
10.50
11.80
11.32
10.49
10.79
11.49
14.60
12.68
10.94
10.70
11.51
11.86
11.49
May-2013
Damaged
12.55
9.42
10.71
10.3
10.9
10.42
11.85
11.45
10.44
11.08
11.58
13.99
12.28
10.32
10.50
10.77
11.44
11.00
May-2014
NM
13.31
NM
11.43
NM
11.55
11.13
11.86
11.60
11.13
10.70
12.27
13.97
12.68
10.82
10.93
11.29
NM
11.49
Nov-2014
NM
12.17
NM
10.33
NM
10.38
10.03
11.70
Damaged
10.68
11.75
11.21
14.39
12.59
11.15
10.58
10.57
NM
10.84
May-2015
13.33
14.21
10.59
12.14
11.01
12.21
11.73
12.03
13.08
11.58
11.89
12.80
14.47
13.20
11.23
11.32
11.69
12.43
11.86
Nov-2015
NM
15.71
NM
11.84
NM
12.08
11.66
12.59
13.47
11.49
12.02
12.74
15.46
14.05
12.06
11.98
12.24
NM
12.70
May-2016
NM
14.48
NM
11.73
NM
12.11
11.81
12.26
Dry
11.50
11.98
12.62
14.58
13.42
11.47
11.64
12.33
NM
12.65
Nov-2016
NM
13.31
NM
11.94
NM
11.99
11.53
11.87
Dry
11.71
11.95
12.78
14.47
13.42
11.29
11.38
12.17
NM
12.09
May-2017
13.01
13.34
9.94
11.43
10.71
11.86
11.43
11.86
12.66
11.28
11.48
12.63
14.28
13.36
11.76
11.58
12.35
12.05
12.50
13.54
13.52
Dec-2017
Damaged
14.35
9.80
10.44
10.60
11.74
11.17
12.12
11.95
10.88
11.69
12.46
15.11
13.05
11.89
12.04
12.69
11.84
12.60
14.06
NA
13.72
Jun-2018
Damaged
13.81
9.99
11.62
11.48
12.12
12.35
11.87
12.45
11.38
11.65
16.36
14.38
13.37
11.62
11.58
13.03
12.15
12.80
14.37
NA
13.44
Dec-2018
13.34
14.17
10.08
11.08
10.88
11.52
11.19
9.70
12.30
10.98
11.45
12.22
15.76
13.72
11.69
12.03
13.12
12.21
13.36
14.47
NA
14.59
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VDC's, only those constituents that have been detected are included.
,2. GW Std = N[A[ Title 15A 02L D202 Groundwater Standards or Interim Maximum Allowable Standard UMAC)
3.' = 1MAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. MDL = Method Detection Limit.
6. MRL = Method Reporting Limit.
7. pg/L = micrograms per liter. mg/L = milligrams per liter.
S. ND = not detected above the method detection limit (MDL) under old analytical requirements.
9. U = not detected above specified MDL under new analytical requirements.
10, ! (prior to 2019) = detected result is above MDL and below the Solid Waste Section Limit.
11. 1 (2018 and later) = detected result is above MDL and below the MRL.
12. NA = Not Analyzed or Not Applicable. NE = Not Established. NS = Not Sampled,
13. Bald font indicates analyte detected above GW Std.
14. Blank cell shaded blue indicates the well was not in the sampling program at the time of the sampling event.
15. Blank cell shaded green indicates the well was in the sampling program but not sampled.

Appendix B
Historical Data For Selected Analytes
Construction and Demolition Debris (C&D) Landfill (Permit #74-07), Pitt County, North Carolina
December 2018
NOTES:
1. This table shows a historic summary of the ground water monitoring data. With respect to VOC's, only those constituents that have been detected are included.
2. GWPS = Groundwater Protection Standard: NCAC 15A 02L .0202 Groundwater Standards or Interim Maximum Allowable Standard (IMAC)
3.*=IMAC
4. SW Std = 15A NCAC 02B Water Quality Standards for Surface Water, or other applicable state or national surface water standards, as appropriate.
5. Concentrations are micrograms per liter (Ng/L).
6. ND = Not Detected
7. NE = Not Established
8. ND = Not Detected
9. U = not detected at specified detection limit.
10. J (prior to 2018) = detected result is above MDL and below the Solid Waste Section Limit.
11. J (2018 and later) = detected result is above MDL and below the MRL.
12. Bold font indicates concentrations exceeds GWPS or Surface Water Standard.
13. Blank cell shaded blue indicates the well or sampling location was not in the sampling program at the time of the event.
Page 1 of 1

Water Quality Monitoring Report
December 2018 Semiannual Sampling Event
Wood Project No. 6468-19-9035
Attachment C
Mann -Kendall Trend Analyses
wood.

TOOLKIT
for Constituent• Analysis
Evaluation Date: 26-Apr-19 Job ID: 6480199035
Facility Name: C&D Landfill Constituent: Benzene
Conducted By: DH Concentration Units: N /L
Sampling Point ID:
MW-31S
I MW-3A
I MW-8
I MW-12S
BENZENE
•
•
1
1-Nov-15
1.1
1.1
0.24
0.24
2
1-Ma -16
1.3
0.24
0.9
1.4
3
1-Nov-16
1.2
0.8
1.5
1.9
4
1-May-17
2.8
2
1.2
1.7
5
1-Dec-17
1.7
2.7
0.6
2
6
1-Jun-1 8
1.2
0.5
0.3
1.4
7
1-Dec-19
1.3
1.69
0.48
1.48
8
9
10
11
12
13
14
15
16
17
18
19
20
Coefficient of Variation: �fii•
Mann -Kendall Statistic (S):
Confidence Factor:
Concentration Trend:
10
�MW35
�MW3A
0M 1
or
L
d
V
C
O
U
0.1
07115 01116 08116 03117 09117 04118 10118 05119 12119 06120
Sampling Date
Notes:
1. At least four independent sampling events per well are required for calculating the trend. Methodology is valid for 4 to 40 samples.
2. Confidence in Trend = Confidence (in percent) that constituent concentration is increasing (S>0) or decreasing (S<0): >95% = Increasing or Decreasing;
>_ 90% = Probably Increasing or Probably Decreasing; < 90% and S>0 = No Trend; < 90%, S<_0, and COV >_ 1 = No Trend; < 90% and COV < 1 = Stable.
3. Methodology based on "MAROS: A Decision Support System for Optimizing Monitoring Plans", J.J. Aziz, M. Ling, H.S. Rifai, C.J. Newell, and J.R. Gonzales,
Ground Water, 41(3):355-367, 2003.
4 MDL value used for ND concentrations.
DISCLAIMER: The GSI Mann -Kendall Toolkit is available "as is". Considerable care has been exercised in preparing this software product; however, no party, including without
limitation GSI Environmental Inc., makes any representation or warranty regarding the accuracy, correctness, or completeness of the information contained herein, and no such
party shall be liable for any direct, indirect, consequential, incidental or other damages resulting from the use of this product or the information contained herein. Information in
this publication is subject to change without notice. GSI Environmental Inc., disclaims any responsibility or obligation to update the information contained herein.
GSI Environmental Inc., www.gsi-net.com

TOOLKIT
for • • Analysis
Evaluation Date: 26-Apr-19 Job ID: 6480199035
Facility Name: C&D Landfill Constituent: Vinyl Chloride
Conducted By: DH Concentration Units: N IL
VINYL CHLORIDE CONCENTRATION (N9Coefficient of /
U)
Variation:
Confidence
Concentration
I 0.43
I 61.4%
�end Stable
I
I
I
I