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HomeMy WebLinkAboutMO-7037_27784_CA_LTRRPT_20190415ECS SOUTHEAST, LLP "Setting the Standard for Service" ®� Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F-1078 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 April 15, 2019 Ms. Trudy Beverly, L.G. North Carolina Department of Environmental Quality Underground Storage Tank Section 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 Reference: Soil Sampling Letter Report Blythe Property W.T. Harris Boulevard & 1-485 Southbound On -Ramp Charlotte, Mecklenburg County, North Carolina ECS Project No. 49-6382-B Dear Ms. Beverly: The project site is located off W.T. Harris Boulevard in Charlotte, Mecklenburg County, North Carolina (Figure 1 & 2). ECS previously conducted a Phase I and Limited Phase II Environmental Site Assessment (ESA) dated April 18, 2018 (ECS Project Number 49-6382). The open Blythe Property Leaking Underground Storage Tank (LUST) incident was identified during the regulatory database search. According to the Underground Storage Tank Closure Report prepared by AMEC Earth and Environmental, Inc. (AMEC) in October 2004 (included in the attachments), a residential heating oil UST was removed at the site and the initial soil samples collected from the base of the UST excavation detected total petroleum hydrocarbon (TPH) diesel and gasoline range organics (DRO/GRO) at concentrations above the North Carolina Action level. Based on the exceedances of the North Carolina Action Level, over -excavation activities were conducted and samples were collected from the base and sidewalls of the excavation. Results of the over - excavation samples collected detected TPH DRO and GRO at concentrations above the current North Carolina Action Level in the sample collected from one of the side walls (15-PE-S6) at a depth of 12 feet below the ground surface (bgs). The sample collected from the base and remaining side walls of the excavation did not detect TPH DRO/GRO at concentrations above the current North Carolina Action Level. In an effort to receive regulatory closure for the above referenced incident, ECS was requested to collect a soil sample from the location of the previous 15-PE-S6 soil sample location and submit it for laboratory analysis of volatile and semi -volatile organic compounds (VOCs & SVOCs) using EPA Methods 8260 and 8270, respectively, and extractable and volatile petroleum hydrocarbons (EPH/VPH) using the MADEP Method (risk -based sample). ECS mobilized to the site on March 20, 2019 to advance a boring to 12 feet in the vicinity of the former UST basin and the previous 15-PE-S6 sample location. ECS located the former UST basin using the two larger trees to the northwest and southeast of the excavation and the onsite water -supply well observed during the October 2004 UST Closure. ECS observed a depression in the ground with approximately the same dimensions of the former excavation and further observed that apparent fill material was in the depression. Based on the field observation, it appears that the depression was the location of the former excavation. ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecs[imited.com Report of Soil Removal Activities Blythe Property Charlotte, North Carolina ECS Project No. 49-6382-B April 15, 2019 ECS advanced a boring to 12 feet bgs using a decontaminated stainless steel hand auger on the southwestern edge of the depression to collect a soil sample from the approximately same location and depth as the previous 15-PE-S6 sample location. ECS screened the soil as the boring was advanced using a photo -ionization detector (PID) as well as visual and olfactory senses. ECS collected a soil sample (C-2R) from 12 feet bgs and placed it directly into laboratory provided containers. The soil sample was submitted to Pace National in Huntersville, North Carolina for laboratory analysis of VOCS & SVOCs using EPA Methods 8260 and 8270, respectively, and EPH/VPH using the MADEP Method. Laboratory results of the soil sample collected, C-2R, did not detect VOCs, SVOCs, EPH, or VPH, at concentrations exceeding the laboratory reporting limit. The laboratory analytical report is included in the attachments. The onsite water -supply well is not in use and will be properly abandoned by a North Carolina Licensed Well Driller at the start of site redevelopment activities as access is currently limited. Based on the results of the risk based sample collected in the vicinity of the previous 15-PE-S6 sample location, the inactive status of the onsite water -supply well and plans for abandonment, and the lack of other receptors within 500 feet of the former excavation, ECS requests that the Blythe Property incident be closed out with no further action required. Sincerely, ECS SOUTHEAST, LLP ,�,•w++++e+ CA N t� Christopher D. Orrell, P.G. ��6�� t� Matthew H. McDuffie, P,G. Staff Project Manager i w Environmental Principal correll@ecslimited.comE`Q 0 G_M 5� mmcduffie(a�ecslimited.com 704-525-5152 �,�Q '0L QQa� 704-525-5152 7y, R DPA'D .e Attachments: Figures Laboratory Analytical Data Underground Storage Tank Closure Report — October 2004 Figures S RSVILLE -� G �l I t LEGEND: 9 Approximate Site Boundary SOURCE: � FIGURE 1 F SITE TOPOGRAPHIC MAP USGS TOPOGRAPHIC MAPS s DERITA & MOUNTAIN ISLAND LAKE QUADRANGLES BLYHTE PROPERTY DATED 2016 W.T. HARRIS BOULEVARD CHARLOTTE, MECKLENBURG COUNTY, NORTH SCALE: CAROLINA 1"=2,000' TM ECS PROJECT NO. 49-6382-B Laboratory Analytical Data aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 April 01, 2019 Shaun Brewer ECS Charlotte 1812 Center Park Dr. Suite D Charlotte, NC 28217 RE: Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 Dear Shaun Brewer: Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, p Taylor Ezell taylor.ezell@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 27 acmnalytical www.pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: PROPOSED STORE NO 1087 92422085 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92422085001 C-2R MADEP EPH SEM 7 PASI-C MADEP VPH LMB 6 PASI-C EPA 8270E BPJ 74 PASI-C EPA 8260D DLK 70 PASI-C ASTM D2974-87 KDF 1 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 Sample: C-2R Lab ID: 92422085001 Collected: 03/20/19 15:50 Received: 03/20/19 16:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Aliphatic (C09-C18) ND mg/kg 13.7 1 03/25/19 08:43 03/26/19 22:12 N2 Aliphatic (C19-C36) ND mg/kg 13.7 1 03/25/19 08:43 03/26/19 22:12 N2 Aromatic (C11-C22) ND mg/kg 13.7 1 03/25/19 08:43 03/26/19 22:12 N2 Surrogates Nonatriacontane (S) 100 % 40-140 1 03/25/19 08:43 03/26/19 22:12 7194-86-7 o-Terphenyl (S) 62 % 40-140 1 03/25/19 08:43 03/26/19 22:12 84-15-1 2-Fluorobiphenyl (S) 68 % 40-140 1 03/25/19 08:43 03/26/19 22:12 321-60-8 2-Bromonaphthalene (S) 72 % 40-140 1 03/25/19 08:43 03/26/19 22:12 580-13-2 VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Aliphatic (C05-CO8) ND mg/kg 2.9 1 03/22/19 13:22 03/22/19 14:21 N2 Aliphatic (C09-C12) ND mg/kg 2.9 1 03/22/19 13:22 03/22/19 14:21 N2 Aliphatic(C09-C12) Adjusted ND mg/kg 2.9 1 03/22/19 13:22 03/22/19 14:21 N2 Aromatic (C09-C10) ND mg/kg 2.9 1 03/22/19 13:22 03/22/19 14:21 N2 Surrogates 4-Bromofluorobenzene (FID) (S) 99 % 70-130 1 03/22/19 13:22 03/22/19 14:21 460-00-4 4-Bromofluorobenzene (PID) (S) 100 % 70-130 1 03/22/19 13:22 03/22/19 14:21 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Acenaphthene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 83-32-9 Acenaphthylene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 208-96-8 Aniline ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 62-53-3 Anthracene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 120-12-7 Benzo(a)anthracene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 56-55-3 Benzo(a)pyrene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 50-32-8 Benzo(b)fluoranthene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 205-99-2 Benzo(g,h,i)perylene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 191-24-2 Benzo(k)fluoranthene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 207-08-9 Benzoic Acid ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 65-85-0 Benzyl alcohol ND ug/kg 894 1 03/22/19 13:06 03/22/19 22:42 100-51-6 4-Bromophenylphenyl ether ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 101-55-3 Butylbenzylphthalate ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 894 1 03/22/19 13:06 03/22/19 22:42 59-50-7 4-Chloroaniline ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 111-44-4 2-Chloronaphthalene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 91-58-7 2-Chlorophenol ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 7005-72-3 Chrysene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 218-01-9 Dibenz(a,h)anthracene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 53-70-3 Dibenzofuran ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 132-64-9 1,2-Dichlorobenzene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 95-50-1 1,3-Dichlorobenzene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 541-73-1 1,4-Dichlorobenzene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 91-94-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 Sample: C-2R Lab ID: 92422085001 Collected: 03/20/19 15:50 Received: 03/20/19 16:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 2,4-Dichlorophenol ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 120-83-2 Diethylphthalate ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 84-66-2 2,4-Dimethylphenol ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 105-67-9 Dimethylphthalate ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 131-11-3 Di-n-butylphthalate ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 894 1 03/22/19 13:06 03/22/19 22:42 534-52-1 2,4-Dinitrophenol ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 51-28-5 2,4-Dinitrotoluene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 121-14-2 2,6-Dinitrotoluene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 606-20-2 Di-n-octylphthalate ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 117-81-7 Fluoranthene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 206-44-0 Fluorene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 87-68-3 Hexachlorobenzene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 118-74-1 Hexachlorocyclopentadiene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 77-47-4 Hexachloroethane ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 193-39-5 Isophorone ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 78-59-1 1-Methylnaphthalene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 90-12-0 2-Methylnaphthalene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 15831-10-4 Naphthalene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 91-20-3 2-Nitroaniline ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 88-74-4 3-Nitroaniline ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 99-09-2 4-Nitroaniline ND ug/kg 894 1 03/22/19 13:06 03/22/19 22:42 100-01-6 Nitrobenzene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 98-95-3 2-Nitrophenol ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 88-75-5 4-Nitrophenol ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 100-02-7 N-Nitrosodimethylamine ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 621-64-7 N-Nitrosodiphenylamine ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 108-60-1 Pentachlorophenol ND ug/kg 2230 1 03/22/19 13:06 03/22/19 22:42 87-86-5 Phenanthrene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 85-01-8 Phenol ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 108-95-2 Pyrene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 129-00-0 1,2,4-Trichlorobenzene ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 120-82-1 2,4,5-Trichlorophenol ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 95-95-4 2,4,6-Trichlorophenol ND ug/kg 447 1 03/22/19 13:06 03/22/19 22:42 88-06-2 Surrogates Nitrobenzene-d5 (S) 55 % 23-110 1 03/22/19 13:06 03/22/19 22:42 4165-60-0 2-Fluorobiphenyl (S) 55 % 30-110 1 03/22/19 13:06 03/22/19 22:42 321-60-8 Terphenyl-d14 (S) 63 % 28-110 1 03/22/19 13:06 03/22/19 22:42 1718-51-0 Phenol-d6 (S) 57 % 22-110 1 03/22/19 13:06 03/22/19 22:42 13127-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 27 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 Sample: C-2R Lab ID: 92422085001 Collected: 03/20/19 15:50 Received: 03/20/19 16:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Surrogates 2-Fluorophenol (S) 52 % 13-110 1 03/22/19 13:06 03/22/19 22:42 367-12-4 2,4,6-Tribromophenol (S) 63 % 27-110 1 03/22/19 13:06 03/22/19 22:42 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone ND ug/kg 109 1 03/25/19 14:42 03/29/19 20:22 67-64-1 L1 Benzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 71-43-2 Bromobenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 108-86-1 Bromochloromethane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 74-97-5 Bromodichloromethane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 75-27-4 Bromoform ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 75-25-2 Bromomethane ND ug/kg 10.9 1 03/25/19 14:42 03/29/19 20:22 74-83-9 2-Butanone (MEK) ND ug/kg 109 1 03/25/19 14:42 03/29/19 20:22 78-93-3 n-Butylbenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 104-51-8 sec-Butylbenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 135-98-8 tert-Butyl benzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 98-06-6 Carbon tetrachloride ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 56-23-5 Chlorobenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 108-90-7 Chloroethane ND ug/kg 10.9 1 03/25/19 14:42 03/29/19 20:22 75-00-3 Chloroform ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 67-66-3 Chloromethane ND ug/kg 10.9 1 03/25/19 14:42 03/29/19 20:22 74-87-3 2-Chlorotoluene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 95-49-8 4-Chlorotoluene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 96-12-8 Dibromochloromethane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 106-93-4 Dibromomethane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 74-95-3 1,2-Dichlorobenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 95-50-1 1,3-Dichlorobenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 541-73-1 1,4-Dichlorobenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 106-46-7 Dichlorodifluoromethane ND ug/kg 10.9 1 03/25/19 14:42 03/29/19 20:22 75-71-8 1,1-Dichloroethane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 75-34-3 1,2-Dichloroethane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 107-06-2 1,1-Dichloroethene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 75-35-4 cis-1,2-Dichloroethene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 156-59-2 trans-1,2-Dichloroethene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 156-60-5 1,2-Dichloropropane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 78-87-5 1,3-Dichloropropane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 142-28-9 2,2-Dichloropropane ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 594-20-7 1,1-Dichloropropene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 563-58-6 cis-1,3-Dichloropropene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 10061-02-6 Diisopropyl ether ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 108-20-3 Ethylbenzene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 87-68-3 2-Hexanone ND ug/kg 54.3 1 03/25/19 14:42 03/29/19 20:22 591-78-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 Sample: C-2R Lab ID: 92422085001 Collected: 03/20/19 15:50 Received: 03/20/19 16:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D/5035A Volatile Organics Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 98-82-8 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 99-87-6 ND ug/kg 21.7 1 03/25/19 14:42 03/29/19 20:22 75-09-2 ND ug/kg 54.3 1 03/25/19 14:42 03/29/19 20:22 108-10-1 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 1634-04-4 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 91-20-3 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 103-65-1 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 100-42-5 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 630-20-6 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 79-34-5 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 127-18-4 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 108-88-3 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 87-61-6 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 120-82-1 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 71-55-6 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 79-00-5 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 79-01-6 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 75-69-4 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 96-18-4 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 95-63-6 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 108-67-8 ND ug/kg 54.3 1 03/25/19 14:42 03/29/19 20:22 108-05-4 L1 ND ug/kg 10.9 1 03/25/19 14:42 03/29/19 20:22 75-01-4 ND ug/kg 10.9 1 03/25/19 14:42 03/29/19 20:22 1330-20-7 ND ug/kg 10.9 1 03/25/19 14:42 03/29/19 20:22 179601-23-1 ND ug/kg 5.4 1 03/25/19 14:42 03/29/19 20:22 95-47-6 118 % 70-130 1 03/25/19 14:42 03/29/19 20:22 2037-26-5 104 % 70-130 1 03/25/19 14:42 03/29/19 20:22 460-00-4 75 % 70-132 1 03/25/19 14:42 03/29/19 20:22 17060-07-0 Analytical Method: ASTM D2974-87 27.1 % 0.10 1 REPORT OF LABORATORY ANALYSIS 03/21/19 13:41 This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 QC Batch: 464904 Analysis Method: MADEP VPH QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil Associated Lab Samples: 92422085001 METHOD BLANK: 2528207 Associated Lab Samples: 92422085001 Parameter Units Aliphatic (C05-008) mg/kg Aliphatic (C09-C12) mg/kg Aromatic (C09-C10) mg/kg 4-Bromofluorobenzene (FID) (S) % 4-Bromofluorobenzene (PID) (S) % Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 03/22/1913:51 N2 ND 2.5 03/22/1913:51 N2 ND 2.5 03/22/1913:51 N2 101 70-130 03/22/1913:51 102 70-130 03/22/1913:51 LABORATORY CONTROL SAMPLE & LCSD: 2528208 2528209 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C05-CO8) mg/kg 14.9 16.2 16.1 109 108 70-130 1 25 N2 Aliphatic (C09-C12) mg/kg 14.9 13.9 13.9 93 93 30-130 0 25 N2 Aromatic (C09-C10) mg/kg 5 4.8 4.8 96 97 70-130 1 25 N2 4-Bromofluorobenzene (FID) (S) % 106 104 70-130 4-Bromofluorobenzene (PID) (S) % 106 106 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 27 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 QC Batch: 465244 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics Associated Lab Samples: 92422085001 METHOD BLANK: 2529786 Associated Lab Samples: 92422085001 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 03/29/19 15:02 1,1,1-Trichloroethane ug/kg ND 5.0 03/29/19 15:02 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 03/29/19 15:02 1,1,2-Trichloroethane ug/kg ND 5.0 03/29/19 15:02 1,1-Dichloroethane ug/kg ND 5.0 03/29/19 15:02 1,1-Dichloroethene ug/kg ND 5.0 03/29/19 15:02 1,1-Dichloropropene ug/kg ND 5.0 03/29/19 15:02 1,2,3-Trichlorobenzene ug/kg ND 5.0 03/29/19 15:02 1,2,3-Trichloropropane ug/kg ND 5.0 03/29/19 15:02 1,2,4-Trichlorobenzene ug/kg ND 5.0 03/29/19 15:02 1,2,4-Trimethylbenzene ug/kg ND 5.0 03/29/19 15:02 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 03/29/19 15:02 1,2-Dibromoethane (EDB) ug/kg ND 5.0 03/29/19 15:02 1,2-Dichlorobenzene ug/kg ND 5.0 03/29/19 15:02 1,2-Dichloroethane ug/kg ND 5.0 03/29/19 15:02 1,2-Dichloropropane ug/kg ND 5.0 03/29/19 15:02 1,3,5-Trimethylbenzene ug/kg ND 5.0 03/29/19 15:02 1,3-Dichlorobenzene ug/kg ND 5.0 03/29/19 15:02 1,3-Dichloropropane ug/kg ND 5.0 03/29/19 15:02 1,4-Dichlorobenzene ug/kg ND 5.0 03/29/19 15:02 2,2-Dichloropropane ug/kg ND 5.0 03/29/19 15:02 2-Butanone (MEK) ug/kg ND 100 03/29/19 15:02 2-Chlorotoluene ug/kg ND 5.0 03/29/19 15:02 2-Hexanone ug/kg ND 50.0 03/29/19 15:02 4-Chlorotoluene ug/kg ND 5.0 03/29/19 15:02 4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 03/29/19 15:02 Acetone ug/kg ND 100 03/29/19 15:02 Benzene ug/kg ND 5.0 03/29/19 15:02 Bromobenzene ug/kg ND 5.0 03/29/19 15:02 Bromochloromethane ug/kg ND 5.0 03/29/19 15:02 Bromodichloromethane ug/kg ND 5.0 03/29/19 15:02 Bromoform ug/kg ND 5.0 03/29/19 15:02 Bromomethane ug/kg ND 10.0 03/29/19 15:02 Carbon tetrachloride ug/kg ND 5.0 03/29/19 15:02 Chlorobenzene ug/kg ND 5.0 03/29/19 15:02 Chloroethane ug/kg ND 10.0 03/29/19 15:02 Chloroform ug/kg ND 5.0 03/29/19 15:02 Chloromethane ug/kg ND 10.0 03/29/19 15:02 cis-1,2-Dichloroethene ug/kg ND 5.0 03/29/19 15:02 cis-1,3-Dichloropropene ug/kg ND 5.0 03/29/19 15:02 Dibromochloromethane ug/kg ND 5.0 03/29/19 15:02 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 27 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 METHOD BLANK: 2529786 Associated Lab Samples: 92422085001 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed Dibromomethane ug/kg ND 5.0 03/29/19 15:02 Dichlorodifluoromethane ug/kg ND 10.0 03/29/19 15:02 Diisopropyl ether ug/kg ND 5.0 03/29/19 15:02 Ethylbenzene ug/kg ND 5.0 03/29/19 15:02 Hexachloro-1,3-butadiene ug/kg ND 5.0 03/29/19 15:02 Isopropylbenzene (Cumene) ug/kg ND 5.0 03/29/19 15:02 m&p-Xylene ug/kg ND 10.0 03/29/19 15:02 Methyl-tert-butyl ether ug/kg ND 5.0 03/29/19 15:02 Methylene Chloride ug/kg ND 20.0 03/29/19 15:02 n-Butylbenzene ug/kg ND 5.0 03/29/19 15:02 n-Propylbenzene ug/kg ND 5.0 03/29/19 15:02 Naphthalene ug/kg ND 5.0 03/29/19 15:02 o-Xylene ug/kg ND 5.0 03/29/19 15:02 p-Isopropyltoluene ug/kg ND 5.0 03/29/19 15:02 sec-Butylbenzene ug/kg ND 5.0 03/29/19 15:02 Styrene ug/kg ND 5.0 03/29/19 15:02 tert-Butyl benzene ug/kg ND 5.0 03/29/19 15:02 Tetrachloroethene ug/kg ND 5.0 03/29/19 15:02 Toluene ug/kg ND 5.0 03/29/19 15:02 trans-1,2-Dichloroethene ug/kg ND 5.0 03/29/19 15:02 trans- 1,3-Dichloropropene ug/kg ND 5.0 03/29/19 15:02 Trichloroethene ug/kg ND 5.0 03/29/19 15:02 Trichlorofluoromethane ug/kg ND 5.0 03/29/19 15:02 Vinyl acetate ug/kg ND 50.0 03/29/19 15:02 Vinyl chloride ug/kg ND 10.0 03/29/19 15:02 Xylene (Total) ug/kg ND 10.0 03/29/19 15:02 1,2-Dichloroethane-d4 (S) % 73 70-132 03/29/19 15:02 4-Bromofluorobenzene (S) % 108 70-130 03/29/19 15:02 Toluene-d8 (S) % 121 70-130 03/29/19 15:02 Qualifiers LABORATORY CONTROL SAMPLE: 2529787 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg 50 53.7 107 70-130 1,1,1-Trichloroethane ug/kg 50 50.7 101 70-130 1,1,2,2-Tetrachloroethane ug/kg 50 54.6 109 55-130 1,1,2-Trichloroethane ug/kg 50 53.0 106 70-130 1,1-Dichloroethane ug/kg 50 49.4 99 68-130 1,1-Dichloroethene ug/kg 50 49.8 100 70-130 1,1-Dichloropropene ug/kg 50 46.4 93 70-130 1,2,3-Trichlorobenzene ug/kg 50 51.8 104 70-130 1,2,3-Trichloropropane ug/kg 50 50.1 100 70-130 1,2,4-Trichlorobenzene ug/kg 50 49.9 100 70-130 1,2,4-Trimethylbenzene ug/kg 50 49.7 99 69-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 27 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 LABORATORY CONTROL SAMPLE: Parameter 2529787 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2-Dibromo-3-chloropropane ug/kg 50 48.9 98 57-141 1,2-Dibromoethane (EDB) ug/kg 50 52.5 105 70-130 1,2-Dichlorobenzene ug/kg 50 49.3 99 70-130 1,2-Dichloroethane ug/kg 50 49.4 99 70-130 1,2-Dichloropropane ug/kg 50 51.6 103 70-130 1,3,5-Trimethylbenzene ug/kg 50 49.3 99 70-130 1,3-Dichlorobenzene ug/kg 50 49.3 99 70-130 1,3-Dichloropropane ug/kg 50 47.9 96 70-130 1,4-Dichlorobenzene ug/kg 50 49.6 99 70-130 2,2-Dichloropropane ug/kg 50 52.8 106 70-130 2-Butanone (MEK) ug/kg 100 107 107 60-130 2-Chlorotoluene ug/kg 50 48.9 98 70-130 2-Hexanone ug/kg 100 99.7 100 70-132 4-Chlorotoluene ug/kg 50 48.2 96 70-130 4-Methyl-2-pentanone (MIBK) ug/kg 100 97.5 97 69-130 Acetone ug/kg 100 171 171 49-148 L1 Benzene ug/kg 50 50.1 100 70-130 Bromobenzene ug/kg 50 49.0 98 70-130 Bromochloromethane ug/kg 50 48.7 97 70-130 Bromodichloromethane ug/kg 50 50.7 101 70-130 Bromoform ug/kg 50 49.5 99 68-136 Bromomethane ug/kg 50 48.5 97 60-140 Carbon tetrachloride ug/kg 50 47.7 95 70-130 Chlorobenzene ug/kg 50 47.5 95 70-130 Chloroethane ug/kg 50 53.0 106 51-147 Chloroform ug/kg 50 45.5 91 70-130 Chloromethane ug/kg 50 48.3 97 48-130 cis-1,2-Dichloroethene ug/kg 50 48.8 98 70-130 cis-1,3-Dichloropropene ug/kg 50 51.4 103 70-130 Dibromochloromethane ug/kg 50 52.8 106 70-130 Dibromomethane ug/kg 50 46.7 93 70-130 Dichlorodifluoromethane ug/kg 50 49.8 100 49-130 Diisopropyl ether ug/kg 50 46.4 93 66-130 Ethylbenzene ug/kg 50 48.1 96 70-130 Hexachloro-1,3-butadiene ug/kg 50 52.6 105 70-130 Isopropylbenzene (Cumene) ug/kg 50 48.6 97 70-130 m&p-Xylene ug/kg 100 97.5 97 70-130 Methyl-tert-butyl ether ug/kg 50 46.7 93 70-130 Methylene Chloride ug/kg 50 46.2 92 50-137 n-Butylbenzene ug/kg 50 51.9 104 70-130 n-Propylbenzene ug/kg 50 49.6 99 70-130 Naphthalene ug/kg 50 51.8 104 70-131 o-Xylene ug/kg 50 48.3 97 70-130 p-Isopropyltoluene ug/kg 50 51.0 102 70-130 sec-Butylbenzene ug/kg 50 50.6 101 70-130 Styrene ug/kg 50 48.4 97 70-130 tert-Butyl benzene ug/kg 50 49.9 100 69-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 27 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 LABORATORY CONTROL SAMPLE: Parameter 2529787 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Tetrachloroethene ug/kg 50 30.1 60 56-130 Toluene ug/kg 50 44.9 90 70-130 trans-1,2-Dichloroethene ug/kg 50 50.4 101 70-130 trans- 1,3-Dichloropropene ug/kg 50 52.6 105 70-130 Trichloroethene ug/kg 50 47.7 95 70-141 Trichlorofluoromethane ug/kg 50 51.9 104 67-130 Vinyl acetate ug/kg 100 237 237 10-136 L1 Vinyl chloride ug/kg 50 51.9 104 67-130 Xylene (Total) ug/kg 150 146 97 70-130 1,2-Dichloroethane-d4 (S) % 105 70-132 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 92 70-130 MATRIX SPIKE SAMPLE: Parameter 2529820 Units 92421683002 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND 19.5 15.2 78 52-133 1,1,1-Trichloroethane ug/kg ND 19.5 18.2 94 49-137 1,1,2,2-Tetrachloroethane ug/kg ND 19.5 110 566 39-150 M1 1,1,2-Trichloroethane ug/kg ND 19.5 18.8 96 48-140 1,1-Dichloroethane ug/kg ND 19.5 24.2 124 46-135 1,1-Dichloroethene ug/kg ND 19.5 24.5 126 38-149 1,1-Dichloropropene ug/kg ND 19.5 15.0 77 41-140 1,2,3-Trichlorobenzene ug/kg ND 19.5 15.6 80 10-158 1,2,3-Trichloropropane ug/kg ND 19.5 19.5 100 33-157 1,2,4-Trichlorobenzene ug/kg ND 19.5 ND 0 10-155 M1 1,2,4-Trimethylbenzene ug/kg ND 19.5 14.8 76 24-154 1,2-Dibromo-3-chloropropane ug/kg ND 19.5 28.0 144 33-158 1,2-Dibromoethane (EDB) ug/kg ND 19.5 18.3 94 40-136 1,2-Dichlorobenzene ug/kg ND 19.5 16.9 87 27-146 1,2-Dichloroethane ug/kg ND 19.5 22.2 114 49-140 1,2-Dichloropropane ug/kg ND 19.5 18.6 95 44-143 1,3,5-Trimethylbenzene ug/kg ND 19.5 15.3 78 40-144 1,3-Dichlorobenzene ug/kg ND 19.5 16.7 86 33-140 1,3-Dichloropropane ug/kg ND 19.5 18.3 94 47-147 1,4-Dichlorobenzene ug/kg ND 19.5 17.4 90 35-139 2,2-Dichloropropane ug/kg ND 19.5 19.9 102 41-140 2-Butanone (MEK) ug/kg ND 38.9 31.9J 82 10-181 2-Chlorotoluene ug/kg ND 19.5 19.3 99 38-147 2-Hexanone ug/kg ND 38.9 27.6J 71 18-169 4-Chlorotoluene ug/kg ND 19.5 19.7 101 36-145 4-Methyl-2-pentanone (MIBK) ug/kg ND 38.9 32.2J 83 16-175 Acetone ug/kg ND 38.9 63.1J 162 10-200 Benzene ug/kg ND 19.5 18.0 92 46-136 Bromobenzene ug/kg ND 19.5 23.0 118 38-149 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 27 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 MATRIX SPIKE SAMPLE: 2529820 92421683002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromochloromethane ug/kg ND 19.5 25.4 131 44-142 Bromodichloromethane ug/kg ND 19.5 19.4 100 41-140 Bromoform ug/kg ND 19.5 18.0 93 34-145 Bromomethane ug/kg ND 19.5 27.6 142 14-162 Carbon tetrachloride ug/kg ND 19.5 16.1 83 44-141 Chlorobenzene ug/kg ND 19.5 16.2 83 39-141 Chloroethane ug/kg ND 19.5 28.6 147 10-182 Chloroform ug/kg ND 19.5 23.9 123 45-140 Chloromethane ug/kg ND 19.5 27.3 140 19-149 cis-1,2-Dichloroethene ug/kg ND 19.5 23.7 122 38-150 cis-1,3-Dichloropropene ug/kg ND 19.5 16.9 87 30-144 Dibromochloromethane ug/kg ND 19.5 16.5 85 36-145 Dibromomethane ug/kg ND 19.5 22.0 113 41-145 Dichlorodifluoromethane ug/kg ND 19.5 23.8 122 16-146 Diisopropyl ether ug/kg ND 19.5 19.1 98 41-143 Ethylbenzene ug/kg ND 19.5 14.1 72 35-144 Hexachloro-1,3-butadiene ug/kg ND 19.5 3.6J 19 10-160 Isopropylbenzene (Cumene) ug/kg ND 19.5 10.6 54 30-152 m&p-Xylene ug/kg ND 38.9 26.5 68 33-145 Methyl-tert-butyl ether ug/kg ND 19.5 20.2 104 49-140 Methylene Chloride ug/kg ND 19.5 25.4 130 10-174 n-Butylbenzene ug/kg ND 19.5 11.4 59 10-160 n-Propylbenzene ug/kg ND 19.5 15.4 79 24-159 Naphthalene ug/kg ND 19.5 19.3 80 10-171 o-Xylene ug/kg ND 19.5 13.8 71 31-150 p-Isopropyltoluene ug/kg ND 19.5 10.9 56 21-154 sec-Butylbenzene ug/kg ND 19.5 10.9 56 19-159 Styrene ug/kg ND 19.5 14.4 74 15-152 tert-Butyl benzene ug/kg ND 19.5 14.0 68 31-141 Tetrachloroethene ug/kg ND 19.5 7.6 39 19-141 Toluene ug/kg ND 19.5 17.1 88 31-146 trans-1,2-Dichloroethene ug/kg ND 19.5 23.4 120 28-157 trans- 1,3-Dichloropropene ug/kg ND 19.5 17.5 90 25-146 Trichloroethene ug/kg ND 19.5 14.1 73 34-149 Trichlorofluoromethane ug/kg ND 19.5 23.3 120 10-167 Vinyl acetate ug/kg ND 38.9 ND 21 10-200 Vinyl chloride ug/kg ND 19.5 27.3 140 36-155 Xylene (Total) ug/kg ND 58.4 40.4 69 29-148 1,2-Dichloroethane-d4 (S) % 128 70-132 4-Bromofluorobenzene (S) % 124 70-130 Toluene-d8(S) % 101 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 SAMPLE DUPLICATE: 2529821 Parameter Units 92421683003 Result Dup Result 1,1,1,2-Tetrachloroethane ug/kg ND ND 1,1,1-Trichloroethane ug/kg ND ND 1,1,2,2-Tetrachloroethane ug/kg ND ND 1,1,2-Trichloroethane ug/kg ND ND 1,1-Dichloroethane ug/kg ND ND 1,1-Dichloroethene ug/kg ND ND 1,1-Dichloropropene ug/kg ND ND 1,2,3-Trichlorobenzene ug/kg ND ND 1,2,3-Trichloropropane ug/kg ND ND 1,2,4-Trichlorobenzene ug/kg ND ND 1,2,4-Trimethylbenzene ug/kg ND ND 1,2-Dibromo-3-chloropropane ug/kg ND ND 1,2-Dibromoethane (EDB) ug/kg ND ND 1,2-Dichlorobenzene ug/kg ND ND 1,2-Dichloroethane ug/kg ND ND 1,2-Dichloropropane ug/kg ND ND 1,3,5-Trimethylbenzene ug/kg ND ND 1,3-Dichlorobenzene ug/kg ND ND 1,3-Dichloropropane ug/kg ND ND 1,4-Dichlorobenzene ug/kg ND ND 2,2-Dichloropropane ug/kg ND ND 2-Butanone (MEK) ug/kg ND ND 2-Chlorotoluene ug/kg ND ND 2-Hexanone ug/kg ND ND 4-Chlorotoluene ug/kg ND ND 4-Methyl-2-pentanone (MIBK) ug/kg ND ND Acetone ug/kg ND ND Benzene ug/kg ND ND Bromobenzene ug/kg ND ND Bromochloromethane ug/kg ND ND Bromodichloromethane ug/kg ND ND Bromoform ug/kg ND ND Bromomethane ug/kg ND ND Carbon tetrachloride ug/kg ND ND Chlorobenzene ug/kg ND ND Chloroethane ug/kg ND ND Chloroform ug/kg ND ND Chloromethane ug/kg ND ND cis-1,2-Dichloroethene ug/kg ND ND cis-1,3-Dichloropropene ug/kg ND ND Dibromochloromethane ug/kg ND ND Dibromomethane ug/kg ND ND Dichlorodifluoromethane ug/kg ND ND Diisopropyl ether ug/kg ND ND Ethylbenzene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Isopropylbenzene (Cumene) ug/kg ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 SAMPLE DUPLICATE: 2529821 Parameter Units 92421683003 Result Dup Result m&p-Xylene ug/kg ND ND Methyl-tert-butyl ether ug/kg ND ND Methylene Chloride ug/kg ND ND n-Butylbenzene ug/kg ND ND n-Propylbenzene ug/kg ND ND Naphthalene ug/kg ND ND o-Xylene ug/kg ND ND p-Isopropyltoluene ug/kg ND ND sec-Butylbenzene ug/kg ND ND Styrene ug/kg ND ND tert-Butyl benzene ug/kg ND ND Tetrachloroethene ug/kg ND ND Toluene ug/kg ND ND trans-1,2-Dichloroethene ug/kg ND ND trans- 1,3-Dichloropropene ug/kg ND ND Trichloroethene ug/kg ND ND Trichlorofluoromethane ug/kg ND ND Vinyl acetate ug/kg ND ND Vinyl chloride ug/kg ND ND Xylene (Total) ug/kg ND ND 1,2-Dichloroethane-d4 (S) % 75 86 4-Bromofluorobenzene (S) % 103 99 Toluene-d8 (S) % 121 118 RPD Qualifiers 3 15 13 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 QC Batch: 464893 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Associated Lab Samples: 92422085001 METHOD BLANK: 2528154 Associated Lab Samples: 92422085001 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/kg ND 325 03/22/19 15:10 1,2-Dichlorobenzene ug/kg ND 325 03/22/19 15:10 1,3-Dichlorobenzene ug/kg ND 325 03/22/19 15:10 1,4-Dichlorobenzene ug/kg ND 325 03/22/19 15:10 1-Methylnaphthalene ug/kg ND 325 03/22/19 15:10 2,2'-Oxybis(1-chloropropane) ug/kg ND 325 03/22/19 15:10 2,4,5-Trichlorophenol ug/kg ND 325 03/22/19 15:10 2,4,6-Trichlorophenol ug/kg ND 325 03/22/19 15:10 2,4-Dichlorophenol ug/kg ND 325 03/22/19 15:10 2,4-Dimethylphenol ug/kg ND 325 03/22/19 15:10 2,4-Dinitrophenol ug/kg ND 1620 03/22/19 15:10 2,4-Dinitrotoluene ug/kg ND 325 03/22/19 15:10 2,6-Dinitrotoluene ug/kg ND 325 03/22/19 15:10 2-Chloronaphthalene ug/kg ND 325 03/22/19 15:10 2-Chlorophenol ug/kg ND 325 03/22/19 15:10 2-Methylnaphthalene ug/kg ND 325 03/22/19 15:10 2-Methylphenol(o-Cresol) ug/kg ND 325 03/22/19 15:10 2-Nitroaniline ug/kg ND 1620 03/22/19 15:10 2-Nitrophenol ug/kg ND 325 03/22/19 15:10 3&4-Methyl phenol (m&p Cresol) ug/kg ND 325 03/22/19 15:10 3,3'-Dichlorobenzidine ug/kg ND 1620 03/22/19 15:10 3-Nitroaniline ug/kg ND 1620 03/22/19 15:10 4,6-Dinitro-2-methyl phenol ug/kg ND 649 03/22/19 15:10 4-Bromophenylphenyl ether ug/kg ND 325 03/22/19 15:10 4-ChIoro-3-methyl phenol ug/kg ND 649 03/22/19 15:10 4-Chloroaniline ug/kg ND 1620 03/22/19 15:10 4-Chlorophenylphenyl ether ug/kg ND 325 03/22/19 15:10 4-Nitroaniline ug/kg ND 649 03/22/19 15:10 4-Nitrophenol ug/kg ND 1620 03/22/19 15:10 Acenaphthene ug/kg ND 325 03/22/19 15:10 Acenaphthylene ug/kg ND 325 03/22/19 15:10 Aniline ug/kg ND 325 03/22/19 15:10 Anthracene ug/kg ND 325 03/22/19 15:10 Benzo(a)anthracene ug/kg ND 325 03/22/19 15:10 Benzo(a)pyrene ug/kg ND 325 03/22/19 15:10 Benzo(b)fluoranthene ug/kg ND 325 03/22/19 15:10 Benzo(g,h,i)perylene ug/kg ND 325 03/22/19 15:10 Benzo(k)fluoranthene ug/kg ND 325 03/22/19 15:10 Benzoic Acid ug/kg ND 1620 03/22/19 15:10 Benzyl alcohol ug/kg ND 649 03/22/19 15:10 bis(2-Chloroethoxy)methane ug/kg ND 325 03/22/19 15:10 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 METHOD BLANK: 2528154 Associated Lab Samples: 92422085001 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed bis(2-Chloroethyl) ether ug/kg ND 325 03/22/19 15:10 bis(2-Ethylhexyl)phthalate ug/kg ND 325 03/22/19 15:10 Butylbenzylphthalate ug/kg ND 325 03/22/19 15:10 Chrysene ug/kg ND 325 03/22/19 15:10 Di-n-butylphthalate ug/kg ND 325 03/22/19 15:10 Di-n-octylphthalate ug/kg ND 325 03/22/19 15:10 Dibenz(a,h)anthracene ug/kg ND 325 03/22/19 15:10 Dibenzofuran ug/kg ND 325 03/22/19 15:10 Diethylphthalate ug/kg ND 325 03/22/19 15:10 Dimethylphthalate ug/kg ND 325 03/22/19 15:10 Fluoranthene ug/kg ND 325 03/22/19 15:10 Fluorene ug/kg ND 325 03/22/19 15:10 Hexachloro-1,3-butadiene ug/kg ND 325 03/22/19 15:10 Hexachlorobenzene ug/kg ND 325 03/22/19 15:10 Hexachlorocyclopentadiene ug/kg ND 325 03/22/19 15:10 Hexachloroethane ug/kg ND 325 03/22/19 15:10 Indeno(1,2,3-cd)pyrene ug/kg ND 325 03/22/19 15:10 Isophorone ug/kg ND 325 03/22/19 15:10 N-Nitroso-di-n-propylamine ug/kg ND 325 03/22/19 15:10 N-Nitrosodimethylamine ug/kg ND 325 03/22/19 15:10 N-Nitrosodiphenylamine ug/kg ND 325 03/22/19 15:10 Naphthalene ug/kg ND 325 03/22/19 15:10 Nitrobenzene ug/kg ND 325 03/22/19 15:10 Pentachlorophenol ug/kg ND 1620 03/22/19 15:10 Phenanthrene ug/kg ND 325 03/22/19 15:10 Phenol ug/kg ND 325 03/22/19 15:10 Pyrene ug/kg ND 325 03/22/19 15:10 2,4,6-Tribromophenol (S) % 90 27-110 03/22/19 15:10 2-Fluorobiphenyl (S) % 75 30-110 03/22/19 15:10 2-Fluorophenol (S) % 66 13-110 03/22/19 15:10 Nitrobenzene-d5 (S) % 71 23-110 03/22/19 15:10 Phenol-d6 (S) % 73 22-110 03/22/19 15:10 Terphenyl-d14 (S) % 86 28-110 03/22/19 15:10 Qualifiers LABORATORY CONTROL SAMPLE: 2528155 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg 1660 1310 79 52-130 1,2-Dichlorobenzene ug/kg 1660 1260 76 51-130 1,3-Dichlorobenzene ug/kg 1660 1320 80 50-130 1,4-Dichlorobenzene ug/kg 1660 1350 82 49-130 1-Methylnaphthalene ug/kg 1660 1520 92 55-130 2,2'-Oxybis(1-chloropropane) ug/kg 1660 1470 89 30-130 2,4,5-Trichlorophenol ug/kg 1660 1330 81 55-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 LABORATORY CONTROL SAMPLE: Parameter 2528155 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 2,4,6-TrichIorophenol ug/kg 1660 1440 87 57-130 2,4-DichIorophenol ug/kg 1660 1380 83 56-130 2,4-Dimethylphenol ug/kg 1660 1350 81 51-130 2,4-Dinitrophenol ug/kg 8280 6150 74 27-133 2,4-Dinitrotoluene ug/kg 1660 1450 88 61-130 2,6-Dinitrotoluene ug/kg 1660 1460 88 60-130 2-Chloronaphthalene ug/kg 1660 1340 81 52-130 2-Chlorophenol ug/kg 1660 1370 83 54-130 2-Methylnaphthalene ug/kg 1660 1480 89 54-130 2-Methylphenol(o-Cresol) ug/kg 1660 1450 87 51-130 2-Nitroaniline ug/kg 3310 2630 79 51-130 2-Nitrophenol ug/kg 1660 1380 83 49-130 3&4-Methyl phenol (m&p Cresol) ug/kg 1660 1330 80 11-163 3,3'-Dichlorobenzidine ug/kg 3310 2230 67 10-132 3-Nitroaniline ug/kg 3310 2280 69 55-130 4,6-Dinitro-2-methyl phenol ug/kg 3310 3010 91 47-142 4-Bromophenylphenyl ether ug/kg 1660 1360 82 59-130 4-Chloro-3-methylphenol ug/kg 3310 2880 87 55-130 4-Chloroaniline ug/kg 3310 2480 75 54-130 4-Chlorophenylphenyl ether ug/kg 1660 1410 85 58-130 4-Nitroaniline ug/kg 3310 2560 77 54-130 4-Nitrophenol ug/kg 8280 6240 75 48-130 Acenaphthene ug/kg 1660 1490 90 60-130 Acenaphthylene ug/kg 1660 1580 95 60-130 Aniline ug/kg 1660 1220 74 43-130 Anthracene ug/kg 1660 1510 91 63-130 Benzo(a)anthracene ug/kg 1660 1590 96 59-130 Benzo(a)pyrene ug/kg 1660 1510 91 57-130 Benzo(b)fluoranthene ug/kg 1660 1490 90 54-130 Benzo(g,h,i)perylene ug/kg 1660 1570 95 59-130 Benzo(k)fluoranthene ug/kg 1660 1470 89 54-130 Benzoic Acid ug/kg 8280 5560 67 19-130 Benzyl alcohol ug/kg 3310 2750 83 50-130 bis(2-Chloroethoxy)methane ug/kg 1660 1350 82 54-130 bis(2-Chloroethyl) ether ug/kg 1660 1390 84 48-130 bis(2-Ethylhexyl)phthalate ug/kg 1660 1590 96 45-134 Butylbenzylphthalate ug/kg 1660 1440 87 46-138 Chrysene ug/kg 1660 1650 100 58-130 Di-n-butylphthalate ug/kg 1660 1400 85 60-130 Di-n-octylphthalate ug/kg 1660 1590 96 53-130 Dibenz(a,h)anthracene ug/kg 1660 1640 99 59-130 Dibenzofuran ug/kg 1660 1400 84 60-130 Diethylphthalate ug/kg 1660 1420 86 60-130 Dimethylphthalate ug/kg 1660 1450 87 60-130 Fluoranthene ug/kg 1660 1550 93 65-130 Fluorene ug/kg 1660 1490 90 63-130 Hexachloro-1,3-butadiene ug/kg 1660 1290 78 46-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 27 Pace Analytical Services, LLC ceAnalX cal ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 LABORATORY CONTROL SAMPLE: Parameter 2528155 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Hexachlorobenzene ug/kg 1660 1390 84 58-130 Hexachlorocyclopentadiene ug/kg 1660 1040 63 23-130 Hexachloroethane ug/kg 1660 1270 77 47-130 Indeno(1,2,3-cd)pyrene ug/kg 1660 1550 93 60-130 Isophorone ug/kg 1660 1310 79 49-130 N-Nitroso-di-n-propylamine ug/kg 1660 1350 81 47-130 N-Nitrosodimethylamine ug/kg 1660 1120 68 45-130 N-Nitrosodiphenylamine ug/kg 1660 1400 85 59-130 Naphthalene ug/kg 1660 1460 88 55-130 Nitrobenzene ug/kg 1660 1260 76 49-130 Pentachlorophenol ug/kg 3310 2200 67 10-132 Phenanthrene ug/kg 1660 1510 91 62-130 Phenol ug/kg 1660 1380 83 46-130 Pyrene ug/kg 1660 1540 93 53-130 2,4,6-Tribromophenol (S) % 90 27-110 2-Fluorobiphenyl (S) % 79 30-110 2-Fluorophenol(S) % 77 13-110 Nitrobenzene-d5 (S) % 77 23-110 Phenol-d6 (S) % 82 22-110 Terphenyl-d14 (S) % 87 28-110 MATRIX SPIKE SAMPLE: Parameter 2528156 Units 92421683001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg ND 1830 1020 56 18-130 1,2-Dichlorobenzene ug/kg ND 1830 982 54 14-130 1,3-Dichlorobenzene ug/kg ND 1830 998 54 12-130 1,4-Dichlorobenzene ug/kg ND 1830 1050 58 10-130 1-Methylnaphthalene ug/kg ND 1830 1140 62 12-130 2,2'-Oxybis(1-chloropropane) ug/kg ND 1830 1090 59 10-130 2,4,5-Trichlorophenol ug/kg ND 1830 862 47 13-130 2,4,6-Trichlorophenol ug/kg ND 1830 1280 70 17-130 2,4-Dichlorophenol ug/kg ND 1830 1160 63 10-130 2,4-Dimethylphenol ug/kg ND 1830 1010 55 10-130 2,4-Dinitrophenol ug/kg ND 9170 4140 45 10-130 2,4-Dinitrotoluene ug/kg ND 1830 1080 59 24-130 2,6-Dinitrotoluene ug/kg ND 1830 1070 58 23-130 2-Chloronaphthalene ug/kg ND 1830 1070 58 19-130 2-Chlorophenol ug/kg ND 1830 1020 56 10-130 2-Methylnaphthalene ug/kg ND 1830 1060 58 18-130 2-Methylphenol(o-Cresol) ug/kg ND 1830 1010 55 10-130 2-Nitroaniline ug/kg ND 3670 1690J 46 17-130 2-Nitrophenol ug/kg ND 1830 1260 69 10-130 3&4-Methyl phenol (m&p Cresol) ug/kg ND 1830 894 49 10-130 3,3'-Dichlorobenzidine ug/kg ND 3670 1150J 31 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 MATRIX SPIKE SAMPLE: 2528156 92421683001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 3-Nitroaniline ug/kg ND 3670 2220 61 24-130 4,6-Dinitro-2-methyl phenol ug/kg ND 3670 2230 61 10-152 4-Bromophenylphenyl ether ug/kg ND 1830 1100 60 29-130 4-Chloro-3-methylphenol ug/kg ND 3670 2110 58 17-130 4-Chloroaniline ug/kg ND 3670 1740J 48 14-130 4-Chlorophenylphenyl ether ug/kg ND 1830 1110 60 25-130 4-Nitroaniline ug/kg ND 3670 1670 46 22-130 4-Nitrophenol ug/kg ND 9170 5220 57 10-130 Acenaphthene ug/kg ND 1830 1140 62 20-130 Acenaphthylene ug/kg ND 1830 1180 64 25-130 Aniline ug/kg ND 1830 791 43 10-130 Anthracene ug/kg ND 1830 1460 79 29-130 Benzo(a)anthracene ug/kg ND 1830 1240 68 19-130 Benzo(a)pyrene ug/kg ND 1830 1200 66 12-130 Benzo(b)fluoranthene ug/kg ND 1830 1210 66 14-130 Benzo(g,h,i)perylene ug/kg ND 1830 1150 63 10-130 Benzo(k)fluoranthene ug/kg ND 1830 1200 65 14-130 Benzoic Acid ug/kg ND 9170 4300 47 10-130 Benzyl alcohol ug/kg ND 3670 1920 52 13-130 bis(2-Chloroethoxy)methane ug/kg ND 1830 1060 58 16-130 bis(2-Chloroethyl) ether ug/kg ND 1830 1050 57 11-130 bis(2-Ethylhexyl)phthalate ug/kg ND 1830 1390 76 21-130 Butylbenzylphthalate ug/kg ND 1830 1150 63 23-130 Chrysene ug/kg ND 1830 1350 74 22-130 Di-n-butylphthalate ug/kg ND 1830 1150 62 30-130 Di-n-octylphthalate ug/kg ND 1830 1370 75 23-142 Dibenz(a,h)anthracene ug/kg ND 1830 1230 67 10-130 Dibenzofuran ug/kg ND 1830 1110 61 24-130 Diethylphthalate ug/kg ND 1830 983 54 26-130 Dimethylphthalate ug/kg ND 1830 930 51 22-130 Fluoranthene ug/kg ND 1830 1240 68 33-130 Fluorene ug/kg ND 1830 1200 65 22-130 Hexachloro-1,3-butadiene ug/kg ND 1830 1040 57 13-130 Hexachlorobenzene ug/kg ND 1830 1140 62 29-130 Hexachlorocyclopentadiene ug/kg ND 1830 716 39 10-130 Hexachloroethane ug/kg ND 1830 975 53 10-130 Indeno(1,2,3-cd)pyrene ug/kg ND 1830 1190 65 10-130 Isophorone ug/kg ND 1830 473 26 13-130 N-Nitroso-di-n-propylamine ug/kg ND 1830 1230 67 12-130 N-Nitrosodimethylamine ug/kg ND 1830 744 41 11-130 N-Nitrosodiphenylamine ug/kg ND 1830 2100 115 15-130 Naphthalene ug/kg ND 1830 1190 65 15-130 Nitrobenzene ug/kg ND 1830 1040 57 12-130 Pentachlorophenol ug/kg ND 3670 1660J 45 10-130 Phenanthrene ug/kg ND 1830 1190 65 27-130 Phenol ug/kg ND 1830 950 52 10-130 Pyrene ug/kg 461 1830 1730 69 19-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 MATRIX SPIKE SAMPLE: Parameter 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol (S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) 2528156 Units 92421683001 Spike MS MS Result Conc. Result % Rec % Rec Limits Qualifiers % 67 27-110 % 54 30-110 % 52 13-110 % 197 23-110 SO % 54 22-110 % 63 28-110 SAMPLE DUPLICATE: 2528157 Parameter Units 92421683001 Result Dup Result 1,2,4-Trichlorobenzene ug/kg ND ND 1,2-Dichlorobenzene ug/kg ND ND 1,3-Dichlorobenzene ug/kg ND ND 1,4-Dichlorobenzene ug/kg ND ND 1-Methylnaphthalene ug/kg ND ND 2,2'-Oxybis(1-chloropropane) ug/kg ND ND 2,4,5-Trichlorophenol ug/kg ND ND 2,4,6-Trichlorophenol ug/kg ND ND 2,4-Dichlorophenol ug/kg ND ND 2,4-Dimethylphenol ug/kg ND ND 2,4-Dinitrophenol ug/kg ND ND 2,4-Dinitrotoluene ug/kg ND ND 2,6-Dinitrotoluene ug/kg ND ND 2-Chloronaphthalene ug/kg ND ND 2-Chlorophenol ug/kg ND ND 2-Methylnaphthalene ug/kg ND ND 2-Methylphenol(o-Cresol) ug/kg ND ND 2-Nitroaniline ug/kg ND ND 2-Nitrophenol ug/kg ND ND 3&4-Methyl phenol (m&p Cresol) ug/kg ND ND 3,3'-Dichlorobenzidine ug/kg ND ND 3-Nitroaniline ug/kg ND ND 4,6-Dinitro-2-methyl phenol ug/kg ND ND 4-Bromophenylphenyl ether ug/kg ND ND 4-ChIoro-3-methyl phenol ug/kg ND ND 4-Chloroaniline ug/kg ND ND 4-Chlorophenylphenyl ether ug/kg ND ND 4-Nitroaniline ug/kg ND ND 4-Nitrophenol ug/kg ND ND Acenaphthene ug/kg ND ND Acenaphthylene ug/kg ND ND Aniline ug/kg ND ND Anthracene ug/kg ND ND Benzo(a)anthracene ug/kg ND ND Benzo(a)pyrene ug/kg ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 SAMPLE DUPLICATE: 2528157 Parameter Units 92421683001 Result Dup Result Benzo(b)fluoranthene ug/kg ND ND Benzo(g,h,i)perylene ug/kg ND ND Benzo(k)fluoranthene ug/kg ND ND Benzoic Acid ug/kg ND ND Benzyl alcohol ug/kg ND ND bis(2-Chloroethoxy)methane ug/kg ND ND bis(2-Chloroethyl) ether ug/kg ND ND bis(2-Ethylhexyl)phthalate ug/kg ND ND Butylbenzylphthalate ug/kg ND ND Chrysene ug/kg ND ND Di-n-butylphthalate ug/kg ND ND Di-n-octylphthalate ug/kg ND ND Dibenz(a,h)anthracene ug/kg ND ND Dibenzofuran ug/kg ND ND Diethylphthalate ug/kg ND ND Dimethylphthalate ug/kg ND ND Fluoranthene ug/kg ND ND Fluorene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Hexachlorobenzene ug/kg ND ND Hexachlorocyclopentadiene ug/kg ND ND Hexachloroethane ug/kg ND ND Indeno(1,2,3-cd)pyrene ug/kg ND ND Isophorone ug/kg ND ND N-Nitroso-di-n-propylamine ug/kg ND ND N-Nitrosodimethylamine ug/kg ND ND N-Nitrosodiphenylamine ug/kg ND ND Naphthalene ug/kg ND ND Nitrobenzene ug/kg ND ND Pentachlorophenol ug/kg ND ND Phenanthrene ug/kg ND ND Phenol ug/kg ND ND Pyrene ug/kg 461 146J 2,4,6-Tribromophenol (S) % 56 63 2-Fluorobiphenyl (S) % 39 42 2-Fluorophenol(S) % 45 61 Nitrobenzene-d5 (S) % 61 63 Phenol-d6 (S) % 49 66 Terphenyl-d14 (S) % 64 54 RPD Qualifiers 11 6 31 2 30 18 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 QC Batch: 465134 Analysis Method: MADEP EPH QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil Associated Lab Samples: 92422085001 METHOD BLANK: 2529325 Matrix: Solid Associated Lab Samples: 92422085001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aliphatic (C09-C18) mg/kg ND 9.9 03/26/19 16:43 N2 Aliphatic (C19-C36) mg/kg ND 9.9 03/26/19 16:43 N2 Aromatic (C11-C22) mg/kg ND 9.9 03/26/19 16:43 N2 2-Bromonaphthalene (S) % 64 40-140 03/26/19 16:43 2-Fluorobiphenyl (S) % 62 40-140 03/26/19 16:43 Nonatriacontane (S) % 94 40-140 03/26/19 16:43 o-Terphenyl (S) % 58 40-140 03/26/19 16:43 LABORATORY CONTROL SAMPLE & LCSD: 2529326 2529327 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C09-C18) mg/kg 9.9 ND ND 75 73 40-140 50 N2 Aliphatic (C19-C36) mg/kg 13.2 10.7 11.4 81 86 40-140 6 50 N2 Aromatic (C11-C22) mg/kg 28.1 14.3 16.7 51 60 40-140 15 50 N2 2-Bromonaphthalene (S) % 58 73 40-140 2-Fluorobiphenyl (S) % 57 71 40-140 Nonatriacontane (S) % 88 87 40-140 o-Terphenyl(S) % 54 66 40-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 QC Batch: 464605 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92422085001 SAMPLE DUPLICATE: 2526586 92421873003 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 17.0 16.9 0 SAMPLE DUPLICATE: 2526587 92421481001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 95.3 95.3 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. SO Surrogate recovery outside laboratory control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/01 /2019 03:57 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 27 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: PROPOSED STORE NO 1087 Pace Project No.: 92422085 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92422085001 C-2R MADEP EPH 465134 MADEP EPH 465429 92422085001 C-2R MADEP VPH 464904 MADEP VPH 464922 92422085001 C-2R EPA 3546 464893 EPA 8270E 465125 92422085001 C-2R EPA 5035A 465244 EPA 8260D 465262 92422085001 C-2R ASTM D2974-87 464605 Date: 04/01 /2019 03:57 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 26 of 27 m m m c C 4. 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N K7 N a KJ 't7 M K rt F-• rt rt D, N y a M N h C M b I f~G n n M n a a WMW M n m P• P• a W m G: a P• It a rt k 'C 3 ro m rororo N m m o ro O = 0 a o n � Z = 6 P•q rtroa 5w P•G van mr-iH u, to N3' w " O a n vaG n n n n tD Z a H •• n r r a m rt 0 7 P. 10 m a mmn no rtra r+mN m' nrt rp 3 co 3 3 •ma wf1G rrrt�d 0 rra r-G m oG a o o m v P•n� aaa �4 D �0r aro3 ra.p. Fl t--� YC e @ It a rt1-1 nmxrtn nH rt 7 PpH m n@ 3 m 0 a m m ICN a 3nJ ■ `/ �f1acmpnL 3 . VoQ "�.uY'n07+ 3 m HNm p rt m 3 K m 9 rt 0 H (HG @n 3 v V Qos� a m am mart n .. O m K arl fx-` m o� n M n A m 3 w ro a -R n _ t•'-, m a rt a H It n A rt rt 3 m m �V�I o ro o' o KQj I .e O = z z zzzzzzzzzzz S � n n e' r"� �� Page 27 of 27 Underground Storage Tank Closure Report — October 2004 MICHAEL F. EASLEY GOVERNOR STATE OF NORTH CAROLINA DEPARTMENT OF TRANSPORTATION October 15, 2004 LYNDo TIPPETT SECRETARY Mr. Steve Bograd, LG E $ ' R " NCDENR, Mooresville Regional Office £;z. Vy 610 East Center Avenue, Suite 301 0 C T 1 9 2004 Mooresville, NC 28115 Subject: TIP: R-2248D AHO iciF'i.tr�SLLtvi',"€tt €FF€C C County: Mecklenburg UST Closure Report, Franklin Blythe Property NCDOT Parcel 15 8910 Vance Road, Charlotte Dear Mr. Bograd: Enclosed for your file is a copy of the UST Closure Report for the above referenced site. During the construction of the Charlotte Outer Loop, the heating oil UST located on this property was discovered. The NCDOT currently has a Temporary Construction Easement on this parcel. After the construction of the Charlotte Outer Loop is complete, control of the property will revert to the heirs of Franklin Blythe. Property Owner: Ruth J. Blythe in care of Dorothy B. Canady 4921 South Hill View Drive Charlotte, NC 28210 704-552-8729 Sincerely, C kF.Parker, LG GeoEnvironmental Project Manager Geotechnical Engineering Unit Enclosure cc: William Wilhelm Division 10 Right of Way (w/ Enclosure) File MAILING ADDRESS: TELEPHONE: 919-250-4088 LOCATION: NC DEPARTMENT OF TRANSPORTATION FAX: 919-250-4237 CENTURY CENTER COMPLEX GEOTECHNICAL ENGINEERING UNIT BUILDING B GEOENVIRONMENTAL SECTION WEBSITE: WWW.DOH.DOT.STATE.NC.US 1020 BIRCH RIDGE DRIVE 1589 MAIL SERVICE CENTER RALEIGH NC 27610 RALEIGH NC 27699-1589 PREPARED FOR: NORTH CAROLINA DEPARTMENT OF TRANSPORTATION 1020 BIRCH RIDGE DRIVE RALEIGH, NORTH CAROLINA 27610 RE C.".E OCT 1 9 2004 REPORT ON: UNDERGROUND STORAGE TANK CLOSURE REPORT FORMER FRANKLIN BLYTHE PROPERTY (PARCEL # 15) 8910 VANCE ROAD CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA OCTOBER 2004 PREPARED BY: AMEC EARTH AND ENVIRONMENTAL, INC. OF NORTH CAROLINA 9800 WEST KINCEY AVE, SUITE 190 HUNTERSVILLE, NORTH CAROLINA 28078 CEodED OCT 0 6 2004 NCDOT•Geokdrtal Urit UNDERGROUND STORAGE TANK CLOSURE REPORT General..I Information° A. Ownership of UST(s) 1. Name of UST owner: NA — Abandoned in NCDOT Right -of -Way 2. Owner address and telephone number: Land owned by: Ruth J. Blythe In care of Dorothy B. Canady 4921 South Hill View Drive Charlotte, North Carolina 28210 Telephone: 704-552-8729 B. Facility Information 1. Facility name: Former Franklin Blythe Property Parcel #15 State DOT Project: (R-2248D) WBS Element: 34410.3.21 Unknown content, filled with heating fuel & water 2. Facility ID #: Not Applicable 3. Facility address, telephone number and county: 8910 Vance Road Charlotte, Mecklenburg County, North Carolina Telephone — N/A C. Contacts Primary contact person: Mr. Cyrus F. Parker, L.G. - GeoEnvironmental Project Manager North Carolina Department of Transportation - Geotechnical Engineering Unit 1020 Birch Ridge Drive Raleigh, NC 27610 Telephone: 919-250-4088 2. Closure contractor: A & D Environmental and Industrial Services, Inc. P.O. Box 484 High Point, NC 27261 Telephone: (336) 434-7750 3. Primary consultant: AMEC Earth and Environmental of North Carolina 9800 West Kincey Ave., Suite 190 Huntersville, NC 28078 Telephone: 704-875-3570 NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page I October 4, 2004 Telephone: 704-875-3570 4. Laboratory: Prism Laboratories, Inc. 449 Springbrook Road Charlotte, NC 28224 Telephone: 704-529-6364, State Certification # 402 D. UST Information Tank No. Installation Dates Size in Gallons Liters Tank Dimensions Feet (Meters) Last Contents Previous Contents (if any) 550 3.5 ft dia. X 7.5 ft long 1 Unknown (2,082) (1.07 m dia. X 2.29 m Unknown Heating Fuel long) E. Site Characteristics 1. Describe any past releases at this site: There are no known previous releases of petroleum products that occurred at this site. When AMEC arrived on -site for the August 5, 2004 UST removal, the UST had been removed and was placed next to the pit by an unknown party. Petroleum odors were present and staining was observed in soils beneath the UST. Holes had been made in the UST from unknown party causing leakage during removal. A flame ionization detector (FID) was used during field screening of soils. 2. Is the facility active or inactive at this time? If the facility is inactive note the last time the UST was in operation: At the time of closure the site was occupied by a former residential structure. The residential structure is being relocated for the beginning stages of Interstate 485 (1-485). The last active use of the UST was some time before the clearing of the land for 1-485. The site is shown in Photographs 3 and 4 in Appendix A. The UST's previous contents were heating fuels. 3. Describe surrounding property use (for example, residential, commercial, farming, etc.) In the past, the surrounding properties of the site were all residential. Currently, to the south of the site is wooded area and north, east, and west of the site is cleared land. Vance Road runs east to west on the north side of the property. Figure 1 presents the surrounding site area. NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page 2 October 4, 2004 4. Describe site geology/hydrogeology The Former Franklin Blythe property is located in the Charlotte Belt of North Carolina. The Charlotte Belt consists of metamorphosed quartz diorite. The metamorphosed quartz diorite consists of intrusive rocks that are strongly foliated to massive. The general age of the rocks is 350 to 650 million years old. Soils encountered during excavation consisted of approximately six inches of surface cover (fine-grained sandy silt topsoil) overlying 2-3 feet of reddish orange, micaceous, dry silt with minor plasticity. Underlying the silt is saprolite, consisting of yellow and tan sandy silt with minor clay and black manganese staining. The top of bedrock was not encountered. An excavation log is included as Appendix B. Groundwater was not encountered in the excavation. The site is situated very near a local topographic high. The local topography suggests that ground -water flow is likely toward the southwest in the site vicinity. The excavation extended to a depth of 15.2 feet (4.63m) below ground surface (bgs). A well survey was not undertaken since groundwater was not encountered. See Table 1. A. Describe preparations for closure including the steps taken to notify authorities, permits obtained and the steps taken to clean and purge the tank(s): On March 22, 2004 AMEC was presented with a Request For Technical and Cost Proposal of a UST closure at the Blythe property, 8910 Vance Road, Parcel 15, from NCDOT. Notice to proceed was given on April 9, 2004 by NCDOT to AMEC. The UST had been discovered during preparation for the Interstate 485 Bypass around Charlotte. It was noted that the UST formerly contained heating oil and was thus considered unregulated. AMEC performed a site visit on March 31, 2004 to assess UST conditions. A second site visit was performed on the April 16, 2004 to vacuum fluids within the UST. Fluids were vacuumed by A&D Environmental of High Point, North Carolina, (A&D). A vacuum hose was inserted into the UST via the fill port accessible from ground surface above the UST. A total of 389 gallons (1,472.53 liters) of heating fuel and sludge was removed from the UST for non -hazardous disposal. It was noted on both visits that the residential structure remained in place. The UST was not to be removed till the residential structure was relocated. The structure was relocated in late July. A Notice of Intent: UST Permanent Closure or Change -In -Service form (GW/UST-3) was completed and faxed to the North Carolina Department of Environment and Natural Resources (NCDENR) Division of Waste Management (DWM) Mooresville Regional Office. A Construction NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page 3 October 4, 2004 43 C. V 1. Fire Permit was also completed as part of UST Closure Activities and is presented as Appendix 1. Closure activities commenced on August 5, 2004. A permit was obtained from the Mecklenburg County Fire Marshal, to remove the UST from the site. Upon arrival, AMEC field personnel noticed that the UST had been removed from its bed and placed on the ground next to the tank bed (Photograph 1). The bed was left open with strong petroleum odors emanating. The Fire Marshal was on -site to issue the permit and to witness the removed UST. Figure 2 presents the site layout depicting the former UST location and excavation. Note the amount of residual material pumped from the tank(s): On April 16, 2004 approximately 389 gallons (1,472.53 liters) of liquid classified as non- hazardous contaminated heating fuel and sludge were removed from the UST by a vacuum pump truck prior to its excavation. A&D transferred the fluids from the UST to their vacuum truck. By the time of the August 5, 2004 removal, the UST had filled with approximately 35 gallons (132.49 liters) of liquid classified as non -hazardous contaminated water and sludge that were removed before disposal. Describe the storage, sampling and disposal of the residual material: The heating fuel, water and sludge removed from the UST were temporarily stored in a vacuum truck until they were transported by A&D for disposal. The heating fuel, water and sludge were taken to a water separator facility. Appendix C includes the Certificate for Disposal for the removed liquids. The UST was removed by A&D and taken to Carolina. It was removed and disposed of in includes a copy of the tank disposal certificate. Excavation D.H. Griffin Scrap Metals of Greensboro, North accordance with API 1604, 1987. Appendix D Describe excavation procedures noting the condition of the soils and the dimensions of the excavation in relation to the tank, piping and/or pumps: Since the UST was removed before AMEC personnel arrived on site on August 5, 2004, AMEC immediately interviewed the NCDOT personnel regarding the UST. They indicated that they were unaware of the unsupervised removal activities and that it could have been done by one of the contractors, contracted by NCDOT for the 1-485 project. The UST had been removed and placed on the ground next to the open bed. Soils excavated during the removal were stock piled to the east of the bed. AMEC noted petroleum odors and some staining on the underlying soil. Before the continuation of the excavation, two soil samples were collected at the bottom of the exposed bed. All AMEC directed excavation activities were conducted using a backhoe operated by A&D personnel on August 5, 2004. A total of six confirmatory soil samples were taken from the bottom and the sidewalls of the excavation. Soils impacted with petroleum hydrocarbons were excavated and stocked piled on the east side of the bed till the completion of the excavation and then loaded for transport to a non -hazardous waste disposal landfill. A&D transported petroleum -contaminated soils to Environmental Soil Inc. located in Shelby, North Carolina. The excavation was then back filled NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page 4 October 4, 2004 in with clean backfill. The dimensions of the final excavation were approximately 19 feet (5.79m) long by 11 feet (3.35m) wide by 15.2 (4.63m) feet deep (Photograph 5). Visual inspection and screening with a field -calibrated FID was performed on soils removed from the excavation. Soils from directly beneath the UST did indicate the presence of petroleum hydrocarbons. FID responses and odors were observed in the soils. The excavation was continued until there were no FID responses. Upon inspection of the relocated UST numerous holes were observed. It had also been partially crushed (Photograph 2). Piping and vents had been removed previously. Before the UST was removed, it was placed on poly and emptied by the vacuum truck. Once the UST was lifted onto a truck, soil was excavated under where the UST had been relocated in the event that fluids had seeped out. 2. Note the depth of tank burial(s) (from land surface to top of tank): The UST was fully removed from the ground prior to AMEC's arrival on site. 3. Quantity of soil removed: As part of the UST removal, A&D excavated approximately 18.80 tons of apparently impacted soils. The soils were field screened with a combination of FID readings and visual observations. Soils deemed impacted through field screening were loaded onto trucks and disposed of at Environmental Soils, Inc. of Lattimore, NC. 4. Describe soil type(s): The soil removed for the UST closure consisted of fine-grained sandy clayey silt. The soils were red brown, semi -plastic, stiff, and dry. The soils are considered to be residual and derived from chemical weathering of the underlying metamorphic parent rock. Competent bedrock was not encountered during UST closure. 5. Type and source of backfill used: The excavation was backfilled with material from the Arart Quarry, in Dobson North Carolina. The material was fine-grained sandy clayey silt. E. Contaminated Soil Soils believed to be impacted were disposed by A&D in a manner approved by the NCDENR. Appendix E includes the Certificates for Disposal for the removed soils. Note: Suspected contaminated soil should be segregated from soil that appears to be uncontaminated and should be treated as contaminated until proven otherwise. It should not be used as backfill. NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page S October 4, 2004 Describe how it was determined to what extent to excavate the soil: Soils removed from the excavation were screened in the field using a calibrated FID to determine if the soil had been impacted by petroleum hydrocarbons. The soil was screened immediately after removal from the excavation while still in the backhoe bucket. Soils indicating the presence of organic vapors and petroleum odors were encountered. Excavation and field screening continued until soils were encountered that had no indication of petroleum impact. Final field screening results are presented in Table 2. 2. Describe method of temporary storage, sampling and treatment/disposal of soil: Soils believed to be contaminated were field screened then stock piled on site. They were later loaded onto trucks for disposal and treatment at Environmental Soils Inc. facility. The treatment methods employed were those needed to eliminate gasoline and diesel range compounds. III.Site investigation A. Provide information on field screening and observations, include methods used to calibrate field screening instrument(s): Field screening was performed using both FID readings and visual observations during the removal activities. The FID was used to screen soil samples from excavated areas for petroleum hydrocarbons. Visual staining was observed within the soils. The FID was calibrated on -site using calibration gases. Table 2 in Section VI summarizes the results of the FID field screening for the UST removal. B. Describe soil sampling points and sampling procedures used: Note: Refer to the "Groundwater Section Guidelines for the Investigation and Remediation of Soils and Groundwater" for information about sampling requirements. Two soil samples were collected from the bottom of the exposed bed, respectively, where petroleum odors, FID responses and some staining on the soil were noted. At the approximate depth of 4 feet below grade surface (bgs) (1.22m), soil samples 15-SS-01 and 15-SS-02 were taken directly beneath the UST's former location. Excavation was initially performed in all directions to a distance of approximately 2 feet (0.61 m) from the UST's former location. Continued FID responses were observed. Excavation was continued until field screening did not indicate the presence of petroleum hydrocarbons in the sidewalls. Due to restriction of the reach on the backhoe the excavation could only reach a depth of 15.2 feet (4.63m). The final field screening still indicated slight impact at the floor bottom. A total of eight soil samples were taken within the excavation pit. In addition to the two samples mentioned, six soil samples were taken from the pit floor and sidewalls after additional excavation was completed. Soil samples. 15-PE-Bl and —132 were taken from the final excavation floor at 15.2 feet (4.63m) bgs directly beneath the UST centerline. Soil samples 15- NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page 6 October 4, 2004 PE-N3, -E4, -W5 and —S6 were collected at the approximate depths of 12 feet (3.66m) bgs from the excavation sidewalls. Sample locations are shown on Figure 3. All samples collected from the excavation pit were analyzed for total petroleum hydrocarbons (TPH) gasoline range organics (GRO) and TPH diesel range organics (DRO). All sampling was performed according to NCDENR's Guidelines for Tank Closure dated September 2003. Sample depths and analyses are shown in Table 3. C. Describe groundwater or surface water sampling procedures used: Note: Refer to the "Groundwater Section Guidelines for the Investigation and Remediation of Soils and Groundwater" for information about sampling requirements. The UST excavation extended to a depth of 15.2 feet (4.63m) bgs. Soils in the base of the excavation were dry. No groundwater or surface water was encountered during UST removal activities. Consequently, no water samples were collected. D. Quality control measures All samples were collected using nitrile-gloved hands to fill sample containers. Samples were placed into clean, laboratory -supplied, glass sample containers, compacted to minimize headspace, and immediately placed on ice for preservation. All samples, that were collected, were hand delivered to Prism Laboratories, Inc. of Charlotte, North Carolina (NC Laboratory Certification Number 402) within 48 hours of the sampling time. All samples were properly labeled and recorded on chain -of -custody, which accompanied the samples at all times. A copy of the chain of custody is included in Appendix F. Table 3 lists all of the samples collected and the analyses performed on each sample. A copy of the complete analytical results and laboratory QA/QC data is included in Appendix G. E. Investigation results Laboratory analyses of the two UST closure samples, collected directly underneath the UST's former location, did report TPH/GRO detections of 77 and 14 mg/kg in samples 15-SS-01 and 15-SS-02, respectively. The TPH/DRO detections were measured to be significantly elevated with 25,000 mg/kg in sample 15-SS-01 and 33,000 mg/kg in 15-SS-02. The initial action levels for GRO and DRO are 10 mg/kg. All TPH/GRO and DRO results are presented on Figure 3 and tabulated in Table 4. The soil from the area of the UST closure samples was removed and further excavation occurred vertically and horizontally. Results from the two confirmatory post -excavation floor samples indicated no further measurable release in the gasoline range for both samples or in the diesel range for one sample. Sample 15-PE-132, however, from the eastern side of the floor indicated a TPH-DRO of 38 mg/kg. Confirmatory post -excavation sidewall sample results also indicated some residual impacted soil remaining. TPH-GRO was measured in just one sidewall sample, the southern, at 53 mg/kg. The corresponding TPH -DRO in the southern sidewall sample was 26,000 mg/kg. TPH-DRO was not measurable in the northern or eastern sidewall samples, but minimally reported at 12 mg/kg in the western sidewall..... Sample locations and analytical results are presented on Figure 3 and compiled in Table 4. Appendix G presents a copy of the laboratory analytical report. NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page 7 October 4, 2004 F. Exploration For Additional USTs The property was surveyed for indication of any other UST and none were found. Include probable sources of contamination, further investigation or remediation tasks, or whether no further action is required. The following conclusions can be drawn based on the field and laboratory data resulting from the August 5, 2004 UST closure; • The former heating oil tank caused a release to the subsurface soil; • Impacted soils with gasoline range impact have been removed vertically; • Impacted soils with diesel range impact have almost been removed vertically, with the exception of a detection of 38 mg/kg in one floor sample; • Excavation has accomplished the removal of gasoline and diesel range impacted soils to the north and east of the former UST's location; • Excavation has accomplished the removal of gasoline range impacted soils and most of the diesel range impacted soils to the west, with a 12 mg/kg of DRO remaining. • In the direction of the southern sidewall impacted soils remain particularly in the diesel range where 26,000 mg/kg was measured in the confirmatory sample despite little to no field indication of contamination; • The heating oil UST release likely occurred some time ago. The lack of much staining and the lack of volatile fuel components as noted by the FID during UST closure suggests that the released petroleum product was already quite weathered by the time of UST removal; • Based on the lack of ground -water interception and the excavation floor sample results, impacted ground water is not expected underlying this site; • It is recommended that further excavation or exploratory drilling and sampling occur in the direction south of the former UST location; and, • It is recommended that a type of field test kit or fast turnaround lab analysis is utilized to improve identification of the weathered petroleum release in soils. NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page 8 October 4, 2004 V. Signature of Professional Engineer or Licensed Geologist ❑Licensed Geologist Li Im4Fm"jI,,w,w,4- 10 mh M40 Helen Corley, LG ttlyy®10/111/®/0j,, f A,90 IV SEAL 1485 � CL®G\c��®o� �Qo,qprwa�AapY@ a� � ®® ®eaaeesoa®® North Carolina License # 1485 Anna Turlik Engineering Technician NCDOT TIP Number R-2248D) WBS Element: 34410.3.28 Page 9 October 4, 2004 VI Enclosures A. Figures Area Map(s) (can be USGS Topographic Quadrangle) showing: • Adjacent streets, roads, highways with names and numbers • Buildings • Surface water bodies • Groundwater flow direction (if available) • Scale • North arrow 2. Site map of UST excavation area drawn to scale, showing: • Buildings • Underground utilities such as sewer lines and other conduits • Orientation of UST(s), pumps, and product lines • Sample locations for GRO and DRO (identified by letter or number) • Final limits of excavation • North arrow • Scale • Sample locations and identifications • Analytical results • Final limits of excavation(s) 3. Site map of UST excavation area drawn to scale, showing: • Sample locations for 8260, 8270, EPH & VPH • Along with items noted in map 2 4. Site map of UST excavation area drawn to scale, showing: • Estimated area of contamination remaining • Along with items noted in map 2 B. Tables 1. Water Supply Wells within a 1500' (457.2m) radius 2. Field screening results 3. Sample identifications, depths and analyses 4. Sample identifications with results and dates that samples were taken C. Appendices Appendix A: Photographs Appendix B: Geologic Log for Excavation Appendix C: Fluid Disposal Certificate Appendix D: Certificate of Tank Disposal Appendix E: Soil Disposal Certificates Complete Appendix F: Chain -of -Custody Records Appendix G: Copy of All Laboratory Analytical Records Appendix H: UST-2 Form, Site Investigation Report for Permanent Closure or Change -in -Service of UST Appendix I: Construction Fire Permit TABLES Table 1 Water Supply Wells Within 1,500-Foot (457.2Meter) Radius Distance/Direction and Address Active? Depth Topographic Relation No ground water was encountered; soils were dry at 15.2 feet (3.50m) below ground surface; No well survey necessary Table Field Screening Results Field`Observations/ _ Date Sample Location" FID Measurements in arts per million August 5, 2004 North end, midline of 550 gallon UST, -4 feet 978 1.22m bgs August 5, 2004 South end, midline of 550 gallon UST, -4 feet 259 1.22m bgs August 5, 2004 South end, midline of 550 gallon UST, -15.2 feet 4.63m bgs 0.0 August 5, 2004 North end, midline of 550 gallon UST, -15.2 feet 0.8 4.63m bgs August 5, 2004 North sidewall, -12 feet (3.66m) bgs 2.1 August 5, 2004 East sidewall, -12 feet (3.66m) bgs 0.8 August 5, 2004 West sidewall, -12 feet (3.66m) bgs 1.2 August 5, 2004 South sidewall, -12 feet (3.66m) bgs 0.0 Table 3 Sample Information Sample Identification Depth of Sample (bgs) Analyses Performed 15-SS-01 -4 feet (1.22m) bgs EPA Method 8015MOD/5030 15-SS-02 -4 feet (1.22m) bgs EPA Method 8015MOD/5030 15-PE-B1 -15.2 feet (4.63m) bgs EPA Method 8015MOD/5030 15-PE-62 -15.2 feet (4.63m) bgs EPA Method 8015MOD/5030 15-PE-N3 -12 feet (3.66m)bgs EPA Method 8015MOD/5030 15-PE-E4 -12 feet (3.66m)bgs EPA Method 8015MOD/5030 15-PE-W5 -12 feet (3.66m)bgs EPA Method 8015MOD/5030 15-PE-S6 -12 feet (3.66m)bgs EPA Method 8015MOD/5030 Table 4 Analytical Detections Sample Identification Initial Action Level for `TFH Analytical Results (mg/kg) 15-SS-01 GRO 10 77 DRO 10 25,000 15-SS-02 GRO 10 14 DRO 10 33,000 15-PE-B1 GRO 10 ND DRO 10 ND 15-PE-B2 GRO 10 ND DRO 10 38 15-PE-N3 GRO 10 ND DRO 10 ND 15-PE-E4 GRO 10 ND DRO 10 ND 15-PE-W5 GRO 10 ND DRO 10 12 15-PE-S6 GRO 10 53 DRO 10 26,000 FIGURES a-i 82� . ..... W it 7 .0m v .4, Im- Z/ X, < 4, Ak� cs; j v X. BM ,774. , e�, 'Y -V & t 7., 1 :6 i'l 41, Wo v mo X v pc SCALE 0- Y IF R ;P4 100 0 FT 0 7000 FT U W 'ter' DERITA QUADRANGLE Tan Kv - NORTH CAROLINA, 1993 Y I i. f .." - -,, . . I q IL SL x ibilatit Y MAP VICINIT v 1� PARCEL #15 Ilk FORMER FRANKLIN BLYTHE vl CHARLOTTE, NC f ------ - -TDATE-. f%DRAWING NAME: N:\NCD0T\B1yth�\YIG1 10103104 4✓ SCALE: I MCH - 1,000 XXXT I' AMT IOMHPC IU A, - PREPARED FOR: NC Depar•tment of Transportation NCDOT PROJECT # -2248D) GEOTECHNICAL UNIT ! %%"i ;;. ``, £�' `.\\ r--,. �� 1, ':; _{ :1, -: �, WBS ELEMENT. 34410.3.21 PREPARED BY: FIGURE: E jr ERSVILLE, NC 28078 -3570 IM LImcw FIGURE I (7N)875 TEMPORARY CONSTRUCTION EASEMENT 15 FRANKLIN BLYTHE DB 1602 PG 1 X Location of UST upon AMEC's arrival. Xx x x � 0 X X X Legend ® Soil Sample Location Beneath UST ♦ Post Excavation Soil Sample Location 1:::3 Limits of Excavation ID Former Location of House Site Map 8910 Vance Rd (Parcel 15) Former Franklin Blythe Property Auaust 2004 rDRAWING NAME: J;\NCDOT\Yanoa I DATE: 1014104 I SCALE: 1 Snoh a 30 fact '"T I a,HpC I , PREPARED FOR: NC Drpartmwnt of Transportation NCDOT PROJECT / (R-2240D) GEOTEC9NICIL UNIT LIDS ELEMENT: 34410.3.21 PREPARED BY: I FIGURE: 9800 T KINCEY AVE SUITE iWES90 FIGURE 2 HUNTERSVILLE, NC 28078 (704)875-3570 15-PE-WS 75-PE-W5 (12.0' bgs) GRO I ND DRO 1 12 15-PE-B1, 15-PE-B1 (15.1' bgs) GRO I ND DRO I ND 1 S-PF-S 15-PE-S6 (12.0' bgs) GRO 53 DRO 26,000 15-SS-02------ 15-SS-02 (4.25' bgs) GRO 1 14 DRO 1 33,000 15-PE-E4 15-PE-E4 (12.0' bgs) GRO ND DRO ND ,15-PE-B2 15-PE-B2 (15.1' bgs)] GRO I ND D RO 1 38 j 15-SS-01 I 15-SS-01 (4.25' bgs) GRO 77 DRO 25,000 15-PE-N3 15-PE-N3 (12.0' bgs) GRO ND DRO ND Note: To Vance Rd. 11 GRO Lime] bgs /,36)/ KD ActionLeveQare��igchlig�itededin boldespective Soil Sample Location Beneath UST Post Excavation Soil Sample Location Limits of Excavation Former Location of House Gasoline Range Organics Diesel Range Organics below grade surface Parcel 15 Former Franklin Blythe Property Sample Locations August 2004 DRAWING NAME: LCDOT Yanot DATE: 8/76/04 SCALE: Iftnoh - f0 1�ot °RIMY "RPC ' PREPARED FOR: NC Department of 71�tton NCDOT PRO✓6CT # (R-8848D) GBOTSCD'NICAL UNIT 1BS RLMENT: 34410.3.21 PREPARED BY: FIGURE: 9800 WEST KINCEY AVE SUITE 190 FIGURE 3 HUNTERSVILLE, NC 28078 (704)875-3570 Appendix A Photographs ameO Photograph 1: Location of UST upon AMEC's Arrival on August 5, 2004. Photograph 2: Crushed UST Photograph 3: Looking North and East towards adjacent properties. Photograph 4: Looking East towards stock pile. • -111 M-Q Photograph 5: Looking North into the bottom of Excavation Pit. Photograph 6: Beginning Stages of Clean Up. W -- i_ g-n P AM Photograph 9: UST being loaded for transport. Photograph 10: Partially hackfilled pit with clean dirt. Photograph 11: Site restored to original condition. .1140iMmso'l lof4iK] us -sfp�'. , I I ftqj; ixi"I,"141 Appendix B Geologic Log for Excavation PROJECT NAME: NCDOT — UST Permanent Closure and Soil Excavation — 8910 Vance Rd., Charlotte, Mecklenburg County, North Carolina, 28216 PROJECT NUMBER: 2-7763-R248 EXCAVATION COMPANY: A&D Environmental OPERATOR: PAGE 1 OF 1 DATE: August 5, 2004 COMPLETION DEPTH: 15.2 ft WATER LEVEL: N/A II EXCAVATION EQUIPMENT: Backhoe II LOGGED BY: Anna M. Turlik II NOTES: Logged directly beneath UST 0.0 (0.0) 0.3 (0.09) Red Orange, micaceous silt, dry w/ minor clay, minor plasticity, saprolite with yellow -tan mottling ML Petroleum Odor; FID = 978 0.3 9.0 Orange, micaceous silt, dry and brittle non -plastic, ML Petroleum Odor; (0.09) (2.74) saprolite with yellow -tan mottling FID = 510 to 658 9.0 15.2 Orange, micaceous silt, dry and brittle non -plastic, ML Light Petroleum Odor; FID = 45.8 (2.74) (4.63) saprolite with yellow -tan mottling to 105.2 Appendix C Fluid Disposal Certificate GENERATOR INFORMATION :«::::<:::>::«::>:::::::>:>�:::»:::<>::<:::::<>:_�.:::<.:<:>�::::;•:::»::<::::>:<>:>::>::»»>:>;::;:>:::::;:><:;::::>::::»:::::. Name US EPA ID No. Street Address Mailing Address Phone No. Contact DESCRIPTION OF MATERIALS USDOT Proper Shipping Name Hazard UN / NA Packing Containers Total Unit HM (Complete All Items for Hazardous Materials Class or Div. ID No. Group Qty. Type Quantity Wt./ Vol. a. b. C. ADDITIONAL INFORMATION ERG No. A;&.D:Prnflle:Code , : t aCilfty ilse a. ,.. ......:::_:;..: .; •w:::..:.: �: :.: v.:... b c. .. GENERATOR'S CERTIFICATION This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in proper condition for transportation according to the applicable regulations of the Department of Transportation. I further certify that none of the materials described above are a hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law, and unless specifically identified above, the materials contain less than 1,000 ppm total halogens and do not contain quantifiable levels 2 m of PCBs as defined by EPA 40 CFR Parts 279 and 761. Printed I Typed Name Signature -'" Mo. / Day I Yr. TRANSPORTER INFORMATION Transporter i hereby acknowledge receipt of the above -described materials for transport A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES from the generator site listed above. Address 2718 UWHARRIE ROAD J ARCHDALE, NC 27263 Signature Shipment Date I hereby acknowledge that the above described materials were received from the generator site and were transported to the facility listed below. Transporter or Unit No. EPA ID No. NCD986232221 Phone (336) 434-7750 ` Signature - Delivery Date INFORMATION :::.::.:..`::;:.;::':."...::.`.::.::':::.:::::;`.::.;;;:;:>:><:::: ::..........FACILITY .....:..: Facility l hereby acknowledge receipt of the materials covered by this manifest A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES except for any discrepancy noted below. Address 2718 UWHARRIE ROAD ORMUNAI - Facility Rafninr r1PY 7 - Roturn to r:onarntnr (-r)PY 3 - Tranennr Pr Retain COPY d - riPnFrntnr Retain Name ✓Mailing Street Addiess Address Phone No. J, Contact DESCRIPTION OF MATERIALS USDOT Proper Shipping Name Hazard UN/NA Packing Containers Total Unit HMI (Complete All Items for Hazardous Materials) Class or Div. ID No. Group at . Type Quantity WtJ Vol. a. B 10: ADDITIONAL INFORMATION ERG No. ::A:& 0 Profile:Code, . . .. ...... .. ............... a. ...... .. . . ........... ...... ... ... .. .... .... .................................. .................................... ........... ............... b. ........ . .......... ......... ....... ........ .. .......... .... . . . ... ... .......... . ........... ......... ... ..... ......... . . ........ .......... ......... .... ......... ..... 11 ..... ................. .... ... .. .... ... ......... C-1 ....... ....... ...... ......... ... ......................... . ............. ............ . GENERATOR'S CERTIFICATION This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in proper condition for transportation according to the applicable regulations of the Department of Transportation. / further certify that none of the materials described above are a hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law, and unless specifically identified above, the materials contain less than 1,000 ppm total halogens and do not contain quantifiable levels (2 ppm) of PCBs as defined by EPA 40 CFR Parts 279 and 761. Printed Typed Name Signature Mo. l Day I Yr. .......... .................. TRANSPORTER INFORMATION .. .. Transporter I hereby acknowledge receipt of the above -described materials for transport A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES from the generator site listed above. Address 2718 UWHARRIE ROAD Signature Shipment Date ARCHDALE, NC 27263 1 hereby acknowledge that the above -described materials were received Transporter or Unit Np.,- from the generatorsite and were transported to the facility listed below. EPA ID No, NCD986232221 Phone (336) 434-7750 Signature Delivery Date .... . ..... . .... FACILITY INFORMATION•. . . . . ..... ... . . . . .... Facility /hereby acknowledge receipt of the materials covered by this —manifest A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES except for any discrepancy noted below. Address ?-'S LTWHARRIE ROAD Signature Receipt Date NC 27263- Q' a cjes I.Rouflnc� Codes I P,,ihd ... ............. .......... Phone....... .... ............ ............ ........... (336) 434-7750 ........ ..... ................. Contact ...... j ............ ................... ERIC McMANUS .. ......... .. . .... .. .. .... .... . .................. ... . .... ....... ...... . ........ ................... fnDv (.r)PV 3 - Tr!2ncnnr4Pr Retain CnPY 4 - Generator Retain A&D 10125 AManifest Document No. MATERIAL & Environmental and - MANIFEST D Industrial Services, Inc. Pige7 of ,. EMERGENCY PHONE NO. POST OFFICE BOX 484 TEL (336) 434-7750 A8:7:;Jofs:;iVo, HIGH POINT, 6 434 - 75 0 P NC 272 2 FAX 336 434-7752 800 7 >;>r GENERATOR O INFORMATION I F Name US EPA ID No. j Stf6et Address "` ez Mailing Address Phone No. Contact DESCRIPTION OF MATERIALS USDOT Proper Shipping Name Hazard UN I NA Packing Containers Total Unit HM (Complete All Items for Hazardous Materials Class or Div. ID No. Group Qty. Type Quantit Wtj vol. a. ram: b. C. ADDITIONAL INFORMATION' ERG No. :A rs:,q,Proflle:Code _aclllty iJse a , s-� :::::: b. c GENERATOR'S CERTIFICATION This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in proper condition for transportation according to the applicable regulations of the Department of Transportation. I further certify that none of the materials described above are a hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law, and unless specifically identified above, the materials contain less than 1,000 ppm total halogens and do not contain quantifiable levels 2 m of PCBs as defined by EPA 40 CFR Parts 279 and 761. Printed ! Typed Name Signature Mo. I Day! Yr. TRANSPORTER INFORMATI ON R R I Transporter ! hereby acknowledge receipt of the above -described materials for transport A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES from the generator site listed above. Address 2718 UWHARRIE ROAD Signature Shipment Date ARCHDALE, NC 27263 I hereby acknowledge that the above -described materials were received Transporter or Unit No.,. from the generator site and were transported to the facility listed below. EPA ID No, NCD986232221, Phone (336) 434-7750 Signr ature Delivery Date C INFORMATION ...............................................................................:.........:::...................... Facility i hereby acknowledge receipt of the materials covered by this manifest A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES except for any discrepancy noted below. Address 2718 UWHARRIE ROAD Signature ."- Receipt Date �CF-iD.�?.E, NC 2?2�3 � �,;s�i-eba�cres i.=ccautinc Codes i 'r?�rsdTirib'fi�efho.��_:: , l-. '. Nc. `'none (336) 434-7750 Contact C ERIC MCMANUS - ORIGINAL - Farility Potnin rOPY 7 _ Potnrn to r Amorntnr rr)PY 3 _ Trnnennrtor Potnin COPY d - r;onorntnr Pptain Appendix D Certificate of Tank Disposal A & Environmental and Industrial Services DP.O. Box 484 • High Point, NC • Phone (336) 434-7750 • FAX (336) 434-7752 TANK DISPOSAL MANIFEST 1) Tank Owner/Authorized Representative:., Name and Mailing. Addressl" �s { 2) Tank Owner/Authorized Representative: Contact Phone#: ' t, , a. 3) Description Of Tanks: Tank No. Capacity Previous Contents Comments OTIM-10 MR? 4) Tank Owner/Authorized '- Representative Certification: The undersigned certifies that the above listed storage tanks have been removed from the premises of the tank owner. r.; f F ,tin _ PrintedlTyped Name Signature Month/DaylYear 5) Transporter: The undersigned certifies that the above listed storage tanks have been transported to A&D Environmental' and Indtrstnal_vServides, 2748, Uwhame Road;"Archdale, N C:-.27263.' PrintedlTyped Name Signature Month/DaylYear 6) Disposal Certification: The undersigned certifies that the above -named storage tank(s) have been cut into scrap pieces and accepted by the metal recycling facility. Recycling Facility: Printed/Typed Name Signature MfontME) ay!Yea r Appendix E Soil Disposal Certificates Complete .:...DRIVER IN TRUCK UNLESS -.CHECKED HERE — Jdrgs and phone number to GEf2TiFIED WR1�F1'� :. (IF RAW) iQHj 998 SAT Scale CgMpany 04K ENVIRONMENTAL SOILS, INC. APPROVAL# LOCATION OF SOIL TRANSPORTER P.O. BOX 295 LATTIMORE, N.C. 28089 704-434-0075 NON -HAZARDOUS PETROLEUM CONTAMINATED SOIL MANIFEST# F'L-. l TIME, g E TRUCK # GROSS WT. '`.tBS. DATE: LICENSE # TARE WT. - :LBS. DRIVER SIGNATURE TIME:. TRUCK# GROSS WT. LBS: DATE: LICENSE # TARE WT. LBS. DRIVER I ER SIGT A U RE NATURE TIME: TRUCK # GROSS WT. LBS. i DATE: LICENSE # TARE WT. LBS. DRIVER SIGN IGN AT UR E ATURE TIME: 'i. TRUCK # GROSS WT. LBS. DATE: LICENSE # TARE WT. LBS. DR V I ER SI GN ATU R E TOTAL NET WT .t I TOTAL EQUIV-TONS INSPECTED & ACCEPTED BY ENVIRONMENTAL SOILS, INC. i SUPERVISOR'S SIGN.^,TURE ENVIRONMENTAL SOILS, INC. P.O. BOX 295 LATTIMORE, N.C. 28086-0489 ,704/434-0075 (704) 434-9533 FAX Job Name: ENVIRONMENTAL SOILS, INC. P.O. BOX,295 LATTIMORE, N.C...28086-0489 704/43470075 (704) 434-9533 FAX Job Name:. ENVIRONMENTAL SOILS, INC. RO. BOX 295: LATTIMORE, N.C. 28086-0489 704/434-0.075 (704) 434-9533 FAX Environmental Soils Inc. PO Box 295 - Lattimore, NC 28089 Phone 704r434-0075 - Fax 704-434-9533 Non -Hazardous Waste Manifest # 116, F Date Load Number .(numbered sequentially as trucks are dispatched) EArVIRONMENTAL CONS ULT,4NT- Contact: -77 : 7 Phone: Fax: GENERATOR: Address: x5-- County: Contact: Phone: WASTE ORIGIN,4T]ONPOINT- Complete Address: ..,Class &Type of Contaminate in soil SOURCE OF CONE431INATION.• (ex. UST or other source) GENERATORS CERTIFICATION OF WASTE CONSTITUENTS.- In lieu ofsubmitting analytical data (metbods 8240 and.82 70). verjoing that the waste in question does not contain organic tonstituents other than those which would normally ap n'analysisofvirgin pearipetroleumproduct residue, I am submitting this Certificate of Waste i Constituents. I cert� that I anifamiliar with the source of contamination of the soil and furtber cert� the source, to the best o that listed above. my hnowledge, contains no contaminants other than t f i TP,4NSPORTER- Contact: Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the IV facility designate. Carrier Signature: Date: TRUCK#: TAG #: VOLUME: TRUCK DRIVER SIGNATURE: DATE: DESTINATION.- Environmental Soils Inc.._,910 Crowdy Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038' I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. FP ",ty Signature Name ,_ N L , i. d- -,: Date: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator ?r O GENERATOR INFORM ATION N Name US EPA ID No. F r �...: Street Addr-ess Mailing Address Phone No. f Contact DESCRIPTION OF MATERIALS USDOT Proper Shipping Name Hazard UN / NA Packing Containers Total Unit HM ____(Complete All Items for Hazardous Materials Class or Div. ID No. Group Qty. Type Quantity Wt./ Vol. a. F b. C. ADDITIONAL INFORMATION ERG No. A.&D:ProtileCode ;acillryIlse` a. b .'>;.»> .:::......:..:.. GENERATOR'S CERTIFICATION This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in proper condition for transportation according to the applicable regulations of the Department of Transportation. I further certify that none of the materials described above are a hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law, and unless specifically identified above, the materials contain less than 1,000 ppm total halogens and do not contain quantifiable levels 2 m of PCBs as defined by EPA 40 CFR Parts 279 and 761. Printed / Typed Name Signature v - Mo. i Day I Yr. �., ;i TRANSPORTER AT Transporter I hereby acknowledge receipt of the above -described materials for transport A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES from the generator site listed above. F Address 2718 UWHARRIE ROAD ARCHDALE, NC 27263 Signature r' „ Shipment Date I hereby acknowledge jh*' the above -described materials were received Transporter or Unit No. from the generatorsite`and weredransported'to the facility listed below. EPA ID No. NCD986232221 Phone (336) 434-7750 Signature ���' ;'' ` Delivery Date ..::..::....::.::.:.:.:.::..::.::.FAC :ILIINFORMATION :::.::: . Facility, l hereby acknowledge receipt' of the materials covered by this manifest A-'& DENVIRONMENTAL AND'R- DUSTRIAL,SERVICES` except for any discrepancy noted below. Address 2718" UWHARRIE ROAD Signature Receipt Date_ ARCHDAILE, NC 27263o ail lQ COdes- F ^ S I d l i nC. Msth CfS hcnc l (336) 434-7750 k CantactERIC McMANUSc ORIGINAI - Facility Patain COPY 7 - RPtttrn fn GPnarafnr COPY 3 - Transnorter Retain COPY 4 - Generator Retain Environmental Soils Inc. PO Box 295 • Lattimore, NC 28089 Phone 704r434-0075• Fax 704-434-9533 Non -Hazardous Waste Manifest #1 1 1P Date Load Number e (numbered sequentially as trucks are dispatched) EAWRONMENT4L CONSULT4NT _ B Contact: F r - f� Phone: TM 7 ax: Address: Contact:' WASTE ORIGINATIONPOINT.•.Complete Address: Class &Type of Contaminate in soil SOURCE OF CONT4MINATION.• (ex. UST or other source) f County` �. -Phone: GENERATORS CERTIFICfITION OF WASTE CONSTITUENTS. In lieu ofsubmitting analytical data (metbods 8240 and.8270). tiering that the waste in question does not contain organic constituents other than those wbicb would normally appear in analysis of virgi.npetroleunaproduct residue, Iam submitting this Certificate of Waste. Constituents. I cert�o that I am familiar with the source of contamination ofthe soil and furtber certio the source, to the best of my knowledge, contains no contaminants other than that listed above. TRANSPORTER: Contact: t' Phone: As the carrier, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Carrier Signature: Date: TRUCK #: `� F TAG #: �` VOLUME t TRUCK DRIVER SIGNATURE. DATE = " F DESTINATION.- Environmental Soils Inc. 910 Crowdy Rd, Shelby, NC 28150 Dedicated Land Application Site Permit #SR0300038 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina. cility Signature: Date: Company Name Title: White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator A&D 1019,5 Manifest Document No. Page of Name US EPA ID No. Street Address Mailing Add riss Phone No, AD Contact DESCRIPTION OF MATERIALS USDOT Proper Shipping Name Hazard UN/NA Packing Containers Total Unit HM (Complete All Items for Hazardous Materials) Class or Div. ID No. Group Qty. Type Quantity Wt./ Vol. a. b. C. L ADDITIONAL INFORMATION ERG No. :,A:.& 0-Profile Code.-. ....... ... .. a. .... .. . . . ........ ...... .. .. ............ . ............ .... .... . ..... ............ ................ ..... ................ b . ... ...... ......... ............................. ......... .... .. ... .... .. ............... . ...... ........... ............ . ........... . .............. .......... ................... ........... C. .................. ................... GENERATOR'S CERTIFICATION This is to certify that the above -described materials are properly classified, described, packaged, marked and labeled, and are in proper condition for transportation according to the applicable regulations of the Department of Transportation. / further certify that none of the materials described above are a hazardous waste as defined by EPA 40 CFR Part 261 or any applicable state law, and unless specifically identified above, the materials contain less than 1,000 ppm total halogens and do not contain quantifiable levels (2 ppm) of PCBs as defined by EPA 40 CFR Parts 279 and 761. Printed Typed Name Signature Mo. Day Yr. .................... .. ... ..... TRANPORTER INFORMATION Transporter I hereby acknowledge receipt of the above -described materials for transport A & D ENVIRONMENTAL AND INDUSTRIAL SERVICES from the generator site listed above. Address 2718 LTWHARRIE ROAD Sig I nature Shipment Date ARCHDALE, NC 27263 / hereby acknowledge that the above -described materials were received Transporter or Unit No. from the generator site and were transported to the facility listed below. EPA ID No. NCD986232221 Phone (336) 434-7750 Slgnaft_iidDelivery Date . .. ..... ........ . ................. ...... ........... i . .... . .......... ..... .. . .................. FACILITY INFORMATION .................... ....... . . . ... ..................... ................. ............... . .......................................... Facility 1hereby acknowledge receipt of the materials covered by this manifest A,& D ENVIRONMENTALLAND�`IiITDUSTki ERVICES=' except for any discrepancy noted below. Address 2718 ' LJWHARRrE ROAD Slanature Receipt Date ARCIFIDALE, NC 27263 'ino �'O_ andflint Vietho-_� t e S scre:�Snciee [Rou ................... .......... .............. ........... ..... ..... .......... ............ ....... .................. ............ - ............... ............ ... ................. ............ - ........ .. .............................. ...... (33 16) 434-7750 ...... ..... .............. ............. ........ ..... ........... ... ..... ..... ............. ........ contact . ..... .......... .. ......... .... -:-`;:......' .............. .......... . . .... . ....... .. ................ ERIC McMANUS ....... .......... I ........ . .... .. ORIGINAL - Facility Retain COPY 2 Ppfitrn to (',PnPr=fnr (C)PY.'1 - Trnn-tnnr-ter Retain rr)PY A (-,e-ns-r:2tr)r Retain Appendix F Chain -of -Custody Records Om V � la�.� W m J o`. C1 Q s ' c o Q o a C[L W w L V � V F N m m W Z H / � v H N d cD p m U6 ' OCC >� U N Cv �N {0' L T O O R � _a (D m a W N 0 W d Q d LO L pL amaCL I V y N i o U ` 0 � CD O i 1 1 1 U n • O V y W _v x a 00 m O x N N, ° LL a-,E y t0 ? UJ Ix co Z v y c c ' oars 'a .n C. V 'O Q to E �. ko- cm CL V �o 0 0 c �a m a a U �.� W ¢ z Z U a -r o Z Z . O IW O LJ- Z O I� I s� LU w GC O } oC W Z I I O O *' U I m aVa w 'LL U Z Z d O .w:. a o c C o m UF) J t V LU IL cu O :i w mY= � Ca' OC t f0 G W lco W co❑ CLO WN NY LU D 0.zzm Q W❑ oc.¢Wa x U U❑ N y I Z? a c m C N>� y V T, O N ;0:W wN. ❑ nyZO m N d U Q W \ O -d0 co N c ❑ m w N ❑ m LU rnocZ y` r co �ai F _ O m. g Fr z O z �mWm U Z 3.LU m. y j O w w J O o m 5•Eww 2 3 m ,II G y'O c0 Q W y rn c w z U) . d w. a' cc U) in c� �LU 3 r x ..Ow C7 1- O lu � = a (n �--.3N V � ¢ w 6 2 LU ui S \ ~ J J O m V.� O 1� LUU, I y F V y- UJ W � 0 0 Q Q V W U Z E LL N 'y O W a mm ,t a_ o z Z c C Z N a U J � 1 Ea.°= y L4 W. W U) to rr .0 er 1 _ .4 . .� . . OE F'C La Um V1 1 I 1 1 Y w. CO CD Qc. N ,c mm . ., .,.., . U) D N y 15 E 0 U tea.' L i W OC z ITT- 2 2 ' M J f!J � ILLJac O z U ga cc U J ❑ of U z O U ❑ W U 2 Cf) F ❑ O a� o Z V H o cc oIL wo W CO m LU = Q ❑ LL, n N< G -+ W =) z e �' (n ❑ L �� L Ir uj ;� 6c UZ W H 0 3 coy 0 =y z ❑ N= m Y LLI O w z U a< ❑ 2 Z raG ❑ a W M: pj m 2jr OZ n W 2 Q v f- N W LL 3 LU iL y 0 H 4 VQ a ? ❑ t jF Z �. a-z m O❑❑ Nw m v, 'C > a U LU Cl) a' � ❑ O N }- z a � Ia.❑ 0 O U) `o w N ❑ 0 m o� LL aZ i O z❑❑ Appendix G Copy of All Laboratory Analytical Records Case Narrative Date: 8/18/04 Company: AMEC Earth & Environmental Contact: Helen Corley Address: 9800 West Kincey Ave. Ste 190 Huntersville, NC 28078 The attached Laboratory Report contains the analytical results for the project identified above and includes Quality Control Data and a Chain -of -Custody copy. Data qualifiers are flagged individually on each sample. A Key Reference for the data qualifiers appears at the bottom of this page. Quality control statements and/or sample specific remarks are included in the sample comments section of the laboratory report for each sample affected. Please call if you have any questions relating to this analytical report. Data Reviewed by: Paula A. Gilleland Project Manager: An ela D vercash Signature: " A' , � �Q 6 d Signature: Review Date: 8/18/04 Approval Date: 8/18/04 Data Qualifier Key Reference: #. Result outside of QC Limits B: Compound also detected in the method blank DO: Compound diluted out. E: Estimated concentration, calibration range exceeded J: The analyte was positively identified but the value is estimated below the reporting limit JH: Estimated concentration with a high bias JL: Estimated concentration with a low bias M: A matrix effect is present T: Tentatively identified compound. The concentration is estimated. Note: This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road, P. 0. Box 240543, Charlotte, NC, 28224-0403 Phone: 7,04/529-6364 Toll Free: 800/529-6364 Fax: 704/525-0409 F:lcommonlcasenarrative Revised 4/20/04 Lab Report 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Huntersville, NC 28078 R.ISM LA86RAT04IES, INC. Full Service Analytical And Environmental Solution Page 1 of 10 Customer Project ID: Parcel 15, Former Franklin Blyth Customer Sample ID: 15-SS-01 Prism Sample ID: AD25359 Matrix: soil Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 09:30 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST PARAMETER TEST RESULT UNITS REPORTING LIMIT METHOD DATE/TIME REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) 77 mg/kg 10 5035/5030/8015B 8/16/04 13:16 JYS SURR: GRO 37 # M % 55-129 5035/5030/8015B 8/16/04 13:16 JYS DILUTION FACTOR 1 mg/kg 5035/5030/8015B 8/16/04 13:16 JYS CALCULATIONS BASED ON DRY WT. 73.2 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.05g-1mL SW846-3545 8/13/04 09:00 CWC DIESEL RANGE ORGANICS (DRO) 25000 mg/kg 5000 SW846-8015B 8/16/04 13:29 JMV SURR: o-TERPHENYL DO % 49-124 SW846-8015B 8/16/04 13:29 JMV DILUTION FACTOR 500 mg/kg SW846-8015B 8/16/04 13:29 JMV Sample Comments: Analysis note for GR: # M - One surrogate recovery was below the control limit. The sample was re- analyzed at a 500 x dilution with no improvement in recovery. Matrix interference is suspected. Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 Lab Report 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Huntersville, NC 28078 LASORATORIE§, WC :, s Full Service Analytical And Environmental Solution Page 2 of 10 Customer Project ID: Parcel 15, Former Franklin Blyth Customer Sample ID: 15-SS-02 Prism Sample ID: AD25360 Matrix: soil Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 09:35 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST PARAMETER TEST RESULT UNITS REPORTING LIMIT METHOD DATEmME REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) 14 mg/kg 10 5035/5030/8015B 8/13/04 16:49 JYS SURR: GRO 88 % 55-129 5035/5030/8015B 8/13/04 16:49 JYS DILUTION FACTOR 1 mg/kg 5035/5030/8015B 8/13/04 16:49 JYS CALCULATIONS BASED ON DRY WT. 75.3 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.01g-1mL SW846-3545 8/13/04 09:00 CWC DIESEL RANGE ORGANICS (DRO) 33000 mg/kg 5000 SW846-8015B 8/16/04 14:43 JMV SURR: o-TERPHENYL DO % 49-124 SW846-8015B 8/16/04 14:43 JMV DILUTION FACTOR 500 mg/kg SW846-8015B 8/16/04 14:43 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 Lab Report , "_LABORA gRlEB IP�C`. `; Full Service Analytical And Environmental Solution 8/18/04 Page 3 of 10 AMEC Earth & Environmental Customer Project ID: Parcel 15, Former Franklin Blyth Attn: Helen Corley Customer Sample ID: 15-PE-B1 9800 West Kincey Ave. Ste 190 Prism Sample ID: AD25361 Matrix: soil Huntersville, NC 28078 Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 11:10 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST PARAMETER TEST RESULT UNITS REPORTING LIMIT METHOD DATElrIME REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) Not Detected mg/kg 10 5035/5030/8015B 8/13/04 17:25 JYS SURR: GRO 70 % 55-129 5035/5030/8015B 8/13/04 17:25 JYS DILUTION FACTOR 1 mg/kg 5035/5030/8015B 8/13/04 17:25 JYS CALCULATIONS BASED ON DRY WT. 66.2 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.25g-1mL SW846-3545 8/13/04 09:00 CWC DIESEL RANGE ORGANICS (DRO) Not Detected mg/kg 10 SW846-8015B 8/13/04 17:32 JMV SURR: o-TERPHENYL 75 % 49-124 SW846-8015B 8/13/04 17:32 JMV DILUTION FACTOR 1 mg/kg SW846-8015B , 8/13/04 17:32 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 , Lab Report 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Hunte.rsville, NC 28078 PRISM LABOIRATORIES; INC. Full Service Analytical And Environmental Solution Page 4 of 10 Customer Project ID: Parcel 15, Former Franklin Blyth Customer Sample ID: 15-PE-132 Prism Sample ID: AD25362 Matrix: soil Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 11:15 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST PARAMETER TEST RESULT UNITS REPORTING LIMIT METHOD DATE/TIME REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) Not Detected mg/kg 10 5035/5030/8015B 8/13/04 18:02 JYS SURR: GRO 101 % 55-129 5035/5030/8015B 8/13/04 18:02 JYS DILUTION FACTOR 1 mg/kg 5035/5030/8015B 8/13/04 18:02 JYS CALCULATIONS BASED ON DRY WT. 69.5 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.04g-1mL SW846-3545 8/13/04 09:00 CWC DIESEL RANGE ORGANICS (DRO) 38 mg/kg 10 SW846-8015B 8/13/04 18:15 JMV SURR: o-TERPHENYL 118 % 49-124 SW846-8015B 8/13/04 18:15 JMV DILUTION FACTOR 1 mg/kg SW846-8015B 8/13/04 18:15 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 Lab Report 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Huntersville NC 28078 PRISM LA6044TORIES, INC. Full Service Analytical And Environmental Solution Page 5 of 10 Customer Project ID: Parcel 15, Former Franklin Blyth Customer Sample ID: 15-PE-N3 Prism Sample ID: AD25363 Matrix: soil Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 11:30 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST TEST REPORTING METHOD DATElrIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) Not Detected mg/kg 10 5035/5030/8015B 8/13/04 18:38 JYS SURR: GRO 83 % 55-129 5035/5030/8015B 8/13/04 18:38 JYS DILUTION FACTOR. 1 mg/kg 5035/5030/8015B 8/13/04 18:38 JYS CALCULATIONS BASED ON DRY WT. 68.2 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.20g-1mL SW846-3545 8/13/04 09:00 CWC DIESEL RANGE ORGANICS (DRO) Not Detected mg/kg 10 SW846-8015B 8/13/04 18:57 JMV SURR: o-TERPHENYL 74 % 49-124 SW846-8015B 8/13/04 18:57 JMV DILUTION FACTOR 1 mg/kg SW846-8015B 8/13/04 18:57 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 • • • 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Huntersville, NC 28078 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST PARAMETER TEST RESULT UNITS REPORTING LIMIT METHOD DATE/TIME REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) Not Detected mg/kg 10 5035/5030/8015B 8/13/04 19:14 JYS SURR: GRO 63 % 55-129 5035/5030/8015B 8/13/04 19:14 JYS DILUTION FACTOR 1 mg/kg 5035/5030/8015B 8/13/04 19:14 JYS CALCULATIONS BASED ON DRY WT. 67.9 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.09g-imL SW846-3545 8/13/04 09:00 cWC DIESEL RANGE ORGANICS (DRO) Not Detected mg/kg 10 SW846-8015B 8/13/04 19:39 JMV SURR: o-TERPHENYL 57 % 49-124 SW846-8015B 8/13/04 19:39 JMV DILUTION FACTOR 1 mg/kg SW846-8015B 8/13/04 19:39 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Spdngbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 Lab Report . PRISM LABORATORIES INC;, s�- Full Service Analytical And Environmental Solution 8/18/04 Page 7 of 10 AMEC Earth & Environmental Customer Project ID: Parcel 15, Former Franklin Blyth Attn: Helen Corley Customer Sample ID: 15-PE-W5 9800 West Kincey Ave. Ste 190 Prism Sample ID: AD25365 Matrix: soil Huntersville, NC 28078 Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 11:50 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) Not Detected mg/kg 10 5035/5030/8015B 8/13/04 19:51 JYS SURR: GRO 99 % 55-129 5035/5030/8015B 8/13/04 19:51 JYS DILUTION FACTOR 1 mg/kg 5035/5030/8015B 8/13/04 19:51 JYS CALCULATIONS BASED ON DRY WT. 71.3 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.18g-1mL SW846-3545 8/13/04 09:00 CWC DIESEL RANGE ORGANICS (DRO) 12 mg/kg 10 SW846-8015B 8/13/04 20:21 JMV SURR: o-TERPHENYL 91 % 49-124 SW846-8015B 8/13/04 20:21 JMV DILUTION FACTOR 1 mg/kg SW846-8015B 8/13/04 20:21 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 r p M 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Huntersville, NC 28078 LABORAT4RWS; IN6>,t Full Service Analytical And Environmental Solution Page 8 of 10 Customer Project ID: Parcel 15, Former Franklin Blyth Customer Sample ID: 15-PE-SS Prism Sample ID: AD25366 Matrix: soil Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 11:55 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST PARAMETER TEST RESULT UNITS REPORTING LIMIT METHOD DATE/TIME REFERENCE STARTED ANALYST GASOLINE RANGE ORGANICS (GRO) 53 mg/kg 10 5035/5030/8015B 8113/04 21:40 JYS SURR: GRO 66 % 55-129 5035/5030/8015B 8/13/04 21:40 JYS DILUTION FACTOR 1 mg/kg 5035/5030/8015B 8/13/04 21:40 JYS CALCULATIONS BASED ON DRY WT. 75.2 % DRY WT. 0.01 SM 2540 G 8/6/04 09:55 DMO PREP. METHOD 3545 FOR DIESEL 25.03g-1mL SW846-3545 8113/04 09:00 CWC DIESEL RANGE ORGANICS (DRO) 2600Q— mg/kg 4000 SW846-8015B 8/16/04 14:01 JMV SURR: o-TERPHENYL DO % 49-124 SW846-8015B 8/16/04 14:01 JMV DILUTION FACTOR 400 mg/kg SW846-8015B 8/16/04 14:01 JMV Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Celt. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 • • • 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Huntersville, NC 28078 Lab Submittal Date/Time: .8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory TEST TEST REPORTING METHOD DATElrIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST DRO QC REPORT xDRO-8015/MOD 8/13/04 10:29 JMv QC DATA FOR DRO-3545/8015B Batch ID: SDRO-081304 Spiked Sample: AD26346 True Value Observed % Recovery Acceptance Range mg/kg mg/kg Method Blank N/A < 10 N/A < 10 Blank Spike 80.0 58.5 73 55-109% Spiked Sample Result N/A < 10 N/A Matrix Spike 89.5 73.1 82 50-117% MS Duplicate 89.2 77.9 87 50-117% RPD 6 < 24 GRO QC REPORT - 5035 xGRO/8015MOD 8/13/04 14:40 QC DATA FOR 8015/5035 GRO Batch ID: VGC-E-081304 Spiked sample: AD25140 True Value Observed % Recovery Acceptance Range mg/kg ---------- mg/kg ------------------ Method Blank N/A < 10 N/A ---------------- < 10 LCS 50 47.5 95 67-116% Spiked Sample < 10 N/A Matrix Spike 46.5 35.51 76 57-113% MS Duplicate 46.5 35.88 77 57-113% RPD 1.0 < 23 JYS NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 Lab Report 8/18/04 AMEC Earth & Environmental Attn: Helen Corley 9800 West Kincey Ave. Ste 190 Huntersville, NC 28078 'RIsm," 'LABORATORIES, jNC.: Full Service Analytical And Environmental Solution Page 10 of 10 Customer Project ID: Parcel 15, Former Franklin Blyth Customer Sample ID: QC Prism Sample ID: AD25367 Matrix: n/a Login Group: 2359M9 Sample Collection Date/Time: 8/5/04 Lab Submittal Date/Time: 8/5/04 15:01 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory I LST TEST REPORTING METHOD DATE/TIME PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST Sample Comments: Angela D. Overcash, V.P. Laboratory Services NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519 449 Springbrook Road - PO Box 240543 - Charlotte, NC 28224-0543 Phone: 704-529-6364 - Toll Free Number: 1-800-529-6364 - Fax: 704-525-0409 o� Sy to 0 �.d � 3 3 P. 0 CO) .(Amm a tl1 a m o v 3 0 vd rrV- (�` M Nm O3o Z ^ z0-1 m Z c z A m a a Lk o v D C O two -n -f 13 r° 0 r O m Qh CO) w v � r CpmOD �mFR m 0- x y w i2 C m w v M O M. O0 m- rm N zin o m � Zm N O y r- .D v1.yac a 0 m m N y Q ~B°. . !� N. 0 70 p_ O n m o A)0� m 0 Z yO.y O 9 ❑❑� i N j 3m.co W O CD v C)O m N r a tm0 R?.�ym N c'; No°�wozi co -w w❑eN mto f O)Ny f1 V x na () X . mN mm OOaaw 70 Q � N in" to N N D Z2� ❑ i C - A C, O <CL , W m o a ❑ yUl o v CL r — � m 18 m CID) y ;� W A 0 = :M S � tm p n rt O O o r m v CL 7 m c 7 v y o Cl) Z Z = a o w o n ` m n Its I = Z z m c -� rn m ° D n I ca > �� m; S S n 3 Yu o o o n a o 0 0 a t4 a o d roo 4� . o O VW 0 �. x y N .la Go zn n 3 ID � 7 1 co c Z n o co N C � d. a F)' N � m m p m m S O N p, 0 ).. o a 1 7aO n- for Z o S y n 5 y C O C tD (D O C Im A � O to 1 W v S IS o, r tD . z m m ,� o v v to ZLo 1 J m N u Z Z A, n, z n m ��� k o Appendix H UST-2 Form, Site Investigation Report for Permanent Closure of UST CHARLOTTE FIRE DEPARTMENT REQUIREMENT FOR TANK INSTALLATIONS AND REMOVALS/ABANDONMENTS THIS IS TO CERTIFY THAT THE TANK(S) LOCATED AT fl# f'c%- HAVE BEEN INSTALLED OR REMOVED ACCORDING'TO NFPA CODES, VOLUME 5 OF THE N.C. STATE FIRE CODE, MANUFACTURER'S STANDARDS AND THE FOLLOWING REQUIREMENTS. UL# TANK PERMIT CAPACITY CATAGORY CONTENTS TYPE (GALS) ABOVE/BELOW TANK #1- •,fit 'r- ,r_;� ;;� `T- %..j,; �� , ;,,��., nLQ TANK #2 V --� TANK #3 TANK COMPLETE FOR TANK INSTALLATIONS INITIAL APPROPRIATE SECTION LB. PSI TEST ON EACH TANK FOR HOURS. FOUND FREE OF LEAKS. CORROSION PROTECTION BY CATHODIC PROTECTION BY INSTALLATION OF ANODE(S) (IF REQUIRED) ALL PIPING CHECKED FOR LEAKS COMPLETE FOR TANK REMOVALS/ABANDONMENTS ALL FLAMMABLE OR COMBUSTIBLE LIQUIDS REMOVED FROM THE TANK AND CONNECTING LINES. U as TANKS WERE PURGED AT SCENE SUCTION, VENT, INLET, GAGE DISCONNECTED AND REMOVED TANK INLETS AND OUTLETS CAPPED IF TANK(S) REMAIN IN PLACE, TANK AND STUBS WILL BE FILLED COMPLETELY WITH CONCRETE, SAND, OR OTHER APPROVED MATERIALS DATE REMOVED/INSTALLED r FIRE INSPECTORIEMPLOYEE NO. COMPANY NAME COMPANY ADDRESS STATE ZIP CODE PHONE NO. Z" f, ORIGINAL-INPECTOR SIGNATURE OF REMOVER CANARY -OCCUPANT CHARLOTTE FIRE DEPARTMENT 441 BEAUMONT AVENUE CHARLOTTE, NC 28204 ON SITE PERMIT APPLICANT OR MAIL TO: Name Cl - Address Apt.Blde. No. r%.1'l1t i / -e- , ;/� C_ City State OCCUPANT AND LOCATION FOR WHICH PERMIT IS VALID: Name 0 '7�) ZIP Code Address Apt.Bldg. No. City State ZIP Code USE OF BUILDING, STRUCTURE OR PREMISES PERMIT FOR: �.. b Va- CODE I (n FEE $ a' 0 iCHECK NO. c it PERMIT GUIDELINES 1. THIS PERMIT SHALL BE POSTED ON PREMISES FOR WHICH ISSUED. 2. ANY CHANGE IN THIS PERMIT SHALL REQUIRE PRIOR APPROVAL OF THE FIRE MARSHAL. 3. THE ISSUANCE OF A PERMIT OR APPROVAL OF PLANS SHALL NOT BE DEEMED OR CONSTRUED TO BE A PERMIT FOR AN APPROVAL OF ANY VIOLATION OF ANY OF THE PROVISIONS OF THE BUILDING AND FIRE CODES. VALID FROM: / s / Cl I � 1.+� `� , 1?_! , L l REPRESENT TIVE/EMERGENCY CONTACT (PRINT NAME) VALID / THROUGH: 4 / G REPRESENTATIVE/EMERGENCY CONTACT (SIGNATURE) PHONE NUMBER r'•C�_�=7;_�r--�, �• FIRE INSPECTORIEMPL OYEE NO. ORIGINAL -INSPECTOR CANARY -OCCUPANT --j col cn O Cm tz� m OF m -n m > m-: yC� cn� ra SZ Appendix I Construction Fire Permit UST-2 Site Investigation Report for Permanent Closure or Change -in -Service of UST FOR TANKS Return completed form to: STATE USE ONLY: The DWM Regional office in the area the facility is located. SEE MAP ON THE BACK OF THIS IN FORM FOR REGIONAL OFFICE ADDRESSES. Return the yellow copy to the Central Office in l.D. # NCRaleigh so that the status of the tank may be changed to "PERMANENTLY CLOSED"' Date Received 1. OWNERSHIP OF +NKS III. LOCATIONOF + Abandoned in DOT Riaht-of-Way. Franklin Blythe Parcel 15 Former Franklin Blythe Property Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company Vance Road NA _8910 Street Address Facility ID # (If known) Charlotte Mecklenburg 8910 Vance Road City County Street Address Carolina 28216 Charlotte Mecklenburg 28216 _North State Zip Code City County Zip Code A Area Code Phone Number NA Area Code Phone Number CONTACT PERSONNEL Name Cyrus E. Parker LG Job Title NCDOT Project Manager Tel. No. 919.250.4088 Closure Contractor A&D Environmental Address P n So, 484 High Point Nc. 27262 Tel. No. 336.434,7750 Primary Consultant AMEC E & E Address emn WP t Kinrey Ave Siira ten HuntP sviila NC 9m7A Tel. No. 704.875.3570 Lab Prism Laboratory Address P.O. Box240543, Charlotte, NC28224 Tel. No. _1,800,529,6364 IV. LIST INFORMATION EXCAVATION CONDITION VI. ADDITIONAL INFORMATION Tank Size in Tank Last Water inFFree Notable odor or visible See reverse side of pink copy (owners No. Gallons Dimensions Contents excavatbnuct soil contaminationcopy) for additional information required by Yes No No Yes No NC DWM in the written report and sketch. 1 550 Heating Oil NOTE: If a release from the tank(s) has occurred, the site assessment portion of the tank closure must be conducted under the supervision of a P.E. or L.G., with all closure site assessment reports bearing the signature and seal of the P.E. or L.G. CHECKLIST (CHECK THE ACTIVITIES COMPLETED)VII. PERMANENT CLOSURE ABANDONMENT IN PLACE (For Removal or Abandonment4n-Place) ❑• Fill tank until material overflows tank opening 0- Contact local fire marshal ❑- Plug or cap all openings 0- Notify DWM Regional Office before abandonment ❑- Disconnect and cap or remove vent line 0- Drain and flush piping into tank ❑- Solid inert material used —specify & Remove all product and residuals from tank ®• Excavate down to tank REMOVAL ®- Clean and inspect tank ❑• Remove drop tube, fill pipe, gauge pipe, vapor recovery tank U- Create vent hole connections, submersible pumps, and all other tank fixtures U- Label tank ❑- Cap or plug all lines except the vent and fill lines ❑- Dispose of tank in approved manner. Final tank destination: ❑- Purge the tank of all product and flammable vapors ❑- Cut one or more large holes in the tank 0- Backfill the area Date tank(s) Permanently Closed: 08-05-04 Date of Change in-service: I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete Print name and official title of owner or owner's authorized representative Signature Date Signed Helen P. Corley, LG, NCDOT Program Manager 10-04-04 UST-2 Rev 02/2001 vvnite copy — Regional umce TeuoW wpy — i.anudi vnwe rn m Py - _v ­ C E i O CO • C U) y CP a) a) C) v U3 V E Q: M co it OA rnO N �. co rn0) U' 40< Z C t a: ai mY N�rn C ,U CEO �� yU �NQ iti L M 0 Z LL Q. 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O S n` cr) W M T O >N� Cl) P�UO» w=Z�— Vance 07 N • c �N � Granville O X ���CLLL $ ffi a 3 D U UC _ f� L' Q T O NCCNc3 � �(5z NOC ff i- ti a)--r-- z CO tMU) M t^ C � CAM Oto c 3: O bim C_ L r) C_ O XCo v00 O m �CDLo (ate OCpL-tt 0 0_-�N�' UNcCv C Z O O�O-N �L woo CD2 O(- =a) =0 N —M co = (D Q (_- Lo < a- LL- I 46 S Evan IL � U • U o Edgecombe i! � Ya 0 cc � o I � a � m m •3 � •m Durham = $ U Orange al o Namance U m Scotland c� 0 U } • Mecklenburg a C U � C OLO 00 OMO O >N6cD N NC)ZMO C EOM O;E5 Omp c CU C r� E 0 �T�0 � U r I`pTp� M 'Lo 1� COUjN�O a)cm�z�C.b _ 00 Cll� UjC�,d �M .�N=dj� C UL Cij L�d (L Beverly, Trudy From: Chris Orrell, P.G. <COrrell@ecslimited.com> Sent: Friday, May 10, 2019 7:03 AM To: Beverly, Trudy Cc: Matthew H. McDuff ie, P.G. Subject: RE: [External] LUST Incident -Blythe Property (Franklin), 8910 Vance Road, Charlotte, NC Attachments: MO-7037_27784_CA_LTRRPT_20190415.pdf External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to report.spam@nc.gov Hey Trudy, Just wanted to touch base and see if you have had a chance to review the letter report and had any questions. Thanks! CHRIS ORRELL, P.G. I Environmental Staff Project Manager ECS SOUTHEAST, LLP T 704.525.5152 1 D 704.409.7740 1 C 704.200.3436 www.ecslimited.com Confidential/proprietary message/attachments. Delete message/attachments if not intended recipient. From: Chris Orrell, P.G. Sent: Monday, April 15, 2019 12:37 PM To: Beverly, Trudy Cc: Matthew H. McDuffie, P.G. Subject: RE: [External] LUST Incident -Blythe Property (Franklin), 8910 Vance Road, Charlotte, NC Trudy, Please see the attached letter report documenting the soil sampling activities at the Blythe Property. We will have the hard copy and CD mailed to you today. Feel free to reach out to me if you have any questions. Thanks! CHRIS ORRELL, P.G. I Environmental Staff Project Manager ECS SOUTHEAST, LLP T 704.525.5152 1 D 704.409.7740 1 C 704.200.3436 www.ecslimited.com Confidential/proprietary message/attachments. Delete message/attachments if not intended recipient. 1