MO-9318_40776_CA_IAR_20171121_Initial Abatement Action Report

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Risk Well Managed
INITIAL ABATEMENT ACTION REPORT
FOR
Joyce Needham Residence
1830 Old Salisbury -Concord Road
Concord, Cabarrus County, North Carolina
North Carolina
8320 University Executive Park Dr.,
Suite 106
Charlotte, NC 28262
f: 877.884.6775
t: 704.782.0555
Facility I.D. Number: N/A
Incident Number: Pending
Risk Classification: Pending
Latitude: 35' 26' 30.87" North Longitude: 800 32' 48.80" West
November 21, 2017
PREPARED FOR:
Ms. Joyce Needham
257 Ponderosa Circle
Mooresville, North Carolina 28117
704-363-9942
CONSULTANT:
PM Environmental, Inc.
8320 University Executive Park Drive, Suite 106
Charlotte, North Carolina 28216
704-782-0555
PM Project No. 15-4139-0-0002
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INCIDENT INFORMATION:
On August 29, 2017 PM Environmental collected soil samples for the based and sidewall of a
former 550-gallon UST basin. The soil samples revealed concentrations of TPH-DRO ranging
from 70 mg/kg to 18,200 mg/kg, and TPH-GRO ranging from non -detect to 888 mg/kg.
Donald D. Warren John W. Hargraves, P.G.
Regional Manager Regional Manager/Senior Geologist
ALABAMA I FLORIDA I ILLINOIS I MICHIGAN I MISSISSIPPI I NEW JERSEY I NORTH CAROLINA I OHIO I TENNESSEE I WWW.PMENV.COM
QUALITY - SERVICE SOLUTIONS

OPNI
ENVIRONMENTAL
Risk Well Managed
November 21, 2017
Mr. Brett Morris
NCDEQ, Division of Waste Management, UST Section
610 East Center Avenue, Suite 301
Mooresville, North Carolina, 28115
Re: Initial Abatement Action Report
Joyce Needham Residence
1830 Old Salisbury -Concord Road
Concord, Cabarrus County, North Carolina 28025
PM Project Number 15-4231-0-0002
Incident No. Not Assigned or Pending
Dear Mr. Morris:
North Carolina
8320 University Executive Park Dr.,
Suite 106
Charlotte, NC 28262
f: 877.884.6775
t: 704.782.0555
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>, �� � I D
NO 2 9 2017
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On behalf of the owner for the subject property, PM Environmental, Inc. (PM) is submitting the
attached Initial Abatement Action Report. Please contact me at 704-782-0555 should you have
any questions or comments concerning this submittal.
Sincerely,
PM Environmental, Inc.
Donald D. Warren.
Regional Manager/Senior Consultant
Attachment
ALABAMA I FLORIDA I ILLINOIS I MICHIGAN 1 MISSISSIPPI I NEW JERSEY I NORTH CAROLINA I OHIO I TENNESSEE I WWWPMENV.COM
QUALITY - SERVICE SOLUTIONS

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No, 15-4231-0-0002; November 21, 2017
A. Site Information
1. Site Identification
Date of Report: November 21, 2017
Facility ID#:
N/A
UST Incident#:
Pending
Site Name:
Joyce Needham Residence
Site Street Address: 1830 Old Salisbury -Concord Road
Nearest City/Town:
Concord, North Carolina
Zip Code:
28025
County:
Cabarrus
Latitude:
35.26'30.87" North Longitude:
2. Contact Information
UST Owner:
Address:
Phone:
UST Operator:
Property Owner:
Property Owner Address:
Property Owner Phone:
Property Occupant:
Consultant/Contractor:
Address:
Analytical Laboratory:
Address:
State Certification:
Phone:
3. Release Information
1'`i J if2 9 2017
80.32'48.80" West
Ms. Joyce Needham
257 Ponderosa Circle, Mooresville, North Carolina 28117
704-363-9942
N/A
Ms. Joyce Needham
257 Ponderosa Circle, Mooresville, North Carolina 28117
704-363-9942
Vacant Residence
PM Environmental, Inc.
8230 University Executive Park Drive, Suite 106, Charlotte, North
Carolina 28216
SGS Accutest
4405 Vinland Road, Suite C-15
Orlando, Florida 32811
573
407-425-6700
Date Discovered: August 2017
Estimated Quantity of Release: Unknown
Cause of Release: In August 2017, soil samples confirmed subsurface hydrocarbon -affected
soil post the removal of the fuel oil UST. The release timing and quantity are not known.
Source of Release: UST
Size and Contents of UST System(s) from which the release occurred: One 550-gallon
petroleum UST.
PM Environmental, Inc.
Page 1

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4231-0-0002; November 21, 2017
4. Report Certification
I, John. W. Hargraves, a Licensed Geologist for PM Environmental, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
i'? cwc�• `SEAL a • g�
John W. Hargraves, P.G.QL,®�'
Regional Manager/Senior Geol'dgt.,, ; c IV
ED
,N'0,V 2 92017
PM Environmental, Inc.
Page 2

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4231-0-0002; November 21, 2017
B. Executive Summary
The subject property consists of one parcel totaling approximately 23.47 acres located at 1830
Old Salisbury -Concord Road in Concord, Cabarrus County, North Carolina (Parcel ID No.
56329072940000). This property includes a single parcel and is developed with one single -
story residence with partial basement totaling approximately 2,750 square foot. The property is
currently unoccupied. The property location is illustrated on Figure 1.
The adjacent and surrounding properties are primarily residential and undeveloped land and Old
Salisbury -Concord Road fronts the subject property to the west, beyond which is residential
properties. The adjoining properties to the south and east are also residential properties. The
subject property bordered to the north by Kiser Road Southwest, beyond which is residential
properties. The subject property layout and adjoining properties are illustrated on Figure 2.
In August 2017, one estimated 550-gallon fuel oil underground storage tank (UST) was
removed from the southwestern side of the onsite residence. The UST was removed from the
ground by the current property owner. During the UST removal olfactory indications of
hydrocarbon affected soil in the vicinity of the UST were detected.
On August 29, 2017, PM was contracted to collect soil samples at the sidewalls and base of the
former UST location. PM collected a total of five soil samples (TP-1 through TP-5). The soil
sample was submitted for laboratory analysis of Total Petroleum Hydrocarbons - Gasoline
Range Organics (TPH-GRO), Total Petroleum Hydrocarbons - Diesel Range Organics (TPH-
DRO). Additionally one soil sample (TP-5) was also submitted for laboratory analysis for
benzene, toluene, ethylbenzene and xylenes (BTEX), which was also used for soil disposal
profiling. Review of the soil analytical results indicated TPH-DRO at concentrations of TPH-
DRO ranging from 70 mg/kg to 18,200 milligrams per kilograms (mg/kg) exceeding the North
Carolina Department of Environmental Quality (NCDEQ) reporting limit of 100 mg/kg. TPH-
GRO was also detected at concentrations of ranging from below laboratory method reporting
limit (MRL) to 888 mg/kg exceeding the NCDEQ reporting limit of 50 mg/kg. No additional target
analytes were detected in soil sample B-1 above the laboratory MRLs.
Based on the results of the August 2017 sampling results, PM submitted a 24-hour Release
Notification to the NCDEQ- Division of Waste Management Underground Storage Tank Section.
On September 27, 2017, PM performed the oversight of approximately 21.47 tons of soil from
the basin. The excavated soil was transported to Republic Services, Inc. of Concord, North
Carolina. Five subsurface confirmation soil samples (OE-1 through OE-5) were obtained from
native material from the tank basin sidewalls and base following the soil excavation. Each of
the confirmation soil samples were submitted for laboratory analysis of volatile organic
compounds (VOCs), semi -volatile organic compounds (SVOCs), and Massachusetts
Department of Environmental Protection Volatile Petroleum Hydrocarbons and Extractable
Petroleum Hydrocarbons (MADEP VPH/EPH).
A review of the analytical results from confirmation soil samples obtained from the former tank
basin indicated various concentrations of VOCs, SVOCs, and MADEP-VPH and EPH analytes
in each of the soil samples above the laboratory method detection limit. However, only soil
samples collected from OE-2 and OE-3 (north and east side walls) revealed concentrations
exceeding the NCDEQ Soil to Groundwater Maximum Soil Contaminant Concentration (MSCC)
PM Environmental, Inc.
Page 3

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4231-0-0002; November 21, 2017
criteria. Detected concentrations of two MADEP VPH/EPH analytes exceeded the Residential
MSCC but not the Industrial / Commercial MSCC criteria in samples OE-2 and OE-3-
In accordance with regulatory guidelines for the closure of USTs when soil remains in the
subsurface that exceeds the Soil to Groundwater MSCCs and/or a water supply well is located
within 150 feet of the source area, additional assessment of the onsite groundwater is required
(e.g. Limited Site Assessment). However, due to the uncertainty of encountering groundwater
based on the potential of bedrock in the area of the former UST basin and cost, the subject
property owner has opted to abandon the current water supply well and replace the well at a
location of the subject property at a distance greater than 150 feet from the source area.
Based on the proposed abandonment of the current water supply well, replacement of the well
at a distance of greater than 150 feet from the source area, and no additional wells within 500
feet of the property boundary, PM recommends that the incident be classified as low risk and
granted a conditional No Further Action at the completion of the following actions:
The current water supply well be abandoned in accordance with state and local
guidelines by a Certified North Carolina well contractor. At the completion of the
abandonment a well abandonment record be submitted to the NCDEQ — UST Section.
• A notice of residual petroleum (NORP) be filed with the Cabarrus County Register of
Deeds Office, restricting soils in the area of the former UST and groundwater use with
the exception of the proposed planned water supply well which will be located greater
than 150 feet from the source area.
PM Environmental, Inc.
Page 4

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4231-0-0002; November 21, 2017
C. Table of Contents
A. Site Information.....................................................................................................................................I
1. Site Identification......................................................................................................................1
2. Contact Information.................................................................................................................1
3. Release Information.................................................................................................................1
4. Report Certification..................................................................................................................2
B. Executive Summary .............................................................................................................................3
C. Table of Contents.................................................................................................................................5
D. Site History and Characterization......................................................................................................6
E. Site Check Report (Not Applicable to this Investigation)................................................................7
F. UST Closure Report.............................................................................................................................7
G. Initial Response and Abatement Action............................................................................................7
H. Groundwater and Surface Water Investigation................................................................................7
I. Excavation of Contaminated Soil.........................................................................................................8
J. Recommendations................................................................................................................................9
FIGURES
Figure 1 Property Location Map
Figure 2 Site Plan
Figure 3 Site Plan with Sample Locations and Analytical Results - UST Basin
Figure 3A Site Plan with Sample Locations and Analytical Results - Over Excavation
TABLES
Table 1 Site History - Release Information
Table 2 Site History- Property Owner and Responsible Party Information
Table 3 Summary of Soil Analytical Results - TPH, VOCs, SVOCs, VPH and EPH
APPENDICES
Appendix A Disposal Manifests for Soil
Appendix B Laboratory Reports - SGS Accutest
Appendix C Chain of Custody for Soil Samples
PM Environmental, Inc.
Page 5

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 154231-0-0002; November 21, 2017
D. Site History and Characterization
UST system details:
UST
Was Release
ID#
Product
Capacity
Date Installed
Date Removed
Assoc. with UST
(gallons)
System
1
Fuel Oil
550
Unknown
August, 2017
Yes
UST Owner/Operator information:
UST
ID#
Name of Owner/
Dates of
Ownership/
Owner or
Address
Telephone
Operator
Operation
Operator
Number
257 Ponderosa
Information
Property
Circle,
1
Joyce Needham
Not
Owner
Mooresville,
704-363-9942
Available
North Carolina
28117
The subject property consists of one parcel totaling approximately 23.47 acres located at 1830
Old Salisbury -Concord Road in Concord, Cabarrus County, North Carolina (Parcel ID No.
56329072940000). This property includes a single parcel and is developed with one single -
story residence with partial basement totaling approximately 2,750 square foot. The property
location is illustrated on Figure 1.
The adjacent and surrounding properties are primarily residential and undeveloped land and Old
Salisbury -Concord Road fronts the subject property to the west, beyond which is residential
properties. The adjoining properties to the south and east are also residential properties. The
subject property bordered to the north by Kiser Road Southwest, beyond which is residential
properties. The subject property layout and adjoining properties are illustrated on Figure 2.
In August 2017, one estimated 550-gallon fuel oil underground storage tank (UST) was
removed from the southwestern side of the onsite residence. The UST was removed from the
ground by the current property owner. During the UST removal olfactory indications of
hydrocarbon affected soil in the vicinity of the UST were detected.
On August 29, 2017, PM was contracted to collect soil samples at the sidewalls and base of the
former UST location. PM collected a total of five soil samples (TP-1 through TP-5). The soil
sample was submitted for laboratory analysis of TPH-GRO, and TPH-DRO. Additionally one
soil sample (TP-5) was also submitted for laboratory analysis for BTEX, which was also used for
soil disposal profiling. Review of the soil analytical results indicated TPH-DRO at
concentrations of TPH-DRO ranging from 70 mg/kg to 18,200 mg/kg exceeding the NCDEQ
reporting limit of 100 mg/kg. TPH-GRO was also detected at concentrations of ranging from
below laboratory MRL to 888 mg/kg exceeding the NCDEQ reporting limit of 50 mg/kg. No
additional target analytes were detected in soil sample B-1 above the laboratory MRLs.
PM Environmental, Inc.
Page 6

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 154231-0-0002; November 21, 2017
Based on the results of the August 2017 sampling results, PM submitted a 24-hour Release
Notification to the NCDEQ- Division of Waste Management Underground Storage Tank Section.
On September 27, 2017, PM performed the oversight of approximately 21.47 tons of soil from
the basin. The excavated soil was transported to Republic Services, Inc. of Concord, North
Carolina.
E. Site Check Report (Not Applicable to this Investigation)
F. UST Closure Report
In August, 2017 the subject property owner removed one fuel oil UST from the west elevation of
the onsite residence. During the UST removal olfactory indications of hydrocarbon affected soil
in the vicinity of the UST were detected.
The UST was estimated to have a capacity of 550-gallons, measured 3.5 feet in diameter and
seven feet in length. Additional information pertaining to the date of installation, use, or
contents of the UST is unknown. The location of the tank is illustrated on Figure 2.
The overburden soil was removed with an excavator and stockpiled. The top of the tank was
encountered approximately two -feet below the ground surface. Tank measurements were:
• Diameter: 3.5 feet.
• Length: 7.0 feet.
• Capacity: 550 gallons.
• Construction: Steel.
Soil excavation and subsurface sampling are discussed in Section I.
G. Initial Response and Abatement Action
On September 27, 2017, PM performed the oversight during the excavation and disposal of
approximately 21.47 tons of hydrocarbon affected soil from the former UST basin.
H. Groundwater and Surface Water Investigation
Groundwater was riot encountered during this Initial Abatement investigation. Surface water
was not addressed during this investigation.
The subject site is currently obtains potable drinking water from one onsite water supply well
located approximately 120 feet northeast of the former UST basin. The well is six inches in
diameter with a casing depth of 102 feet, and a total depth of 325 feet.
A review of the adjoining properties revealed on additional water supply wells located with 500
feet of the former UST basin.
PM Environmental, Inc.
Page 7

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4231-0-0002; November 21, 2017
I. Excavation of Contaminated Soil
Excavation and Samplinq:
On September 271h, 2017, PM performed the oversight of Elite Environmental Services, Inc.
(Elite), utilized an excavator to remove subsurface soil, including hydrocarbon affected soil, from
the former UST basin. The final excavation dimensions of the basin, located near the southern
portion of the residence, are as follows:
• Excavation Length (north -south): 13 feet.
• Excavation Width (east -west): 11 feet.
• Excavation Depth (bgs): 10.5 feet.
Soil was excavated approximately 1.5 to 2.5 feet laterally and approximately 3.5 feet vertically
from the former tank location, and directly loaded into dump trailers. The excavated soil
consisted primarily of silty/clay and weathered rock with a hydrocarbon odor. Excavation was
limited to the north and east by the residential structure.
Five soil samples were collected from the sidewalls and base of the soil excavation (OE-1
through OE-5). The soil sample locations are illustrated on Figure 3.
Each of the soil samples were placed into laboratory containers, labeled, and transported to
SGS/Accutest. in Orlando, Florida (a North Carolina certified laboratory) under chain of custody
procedures. The samples were analyzed for volatile organic compounds (VOCs) by EPA
Method 8260, semi -volatile organic compounds (SVOCs) by EPA Method 8270, and
Massachusetts Department of Environmental Protection Volatile Petroleum Hydrocarbons and
Extractable Petroleum Hydrocarbons (MADEP VPH/EPH).
Following the soil excavation the basin was backfilled with clean soil.
Approximately 21.47 tons of hydrocarbon affected soil were removed from the former UST
basin. The excavated soil was transported to Republic Services, Inc. in Concord, North
Carolina for disposal. Soil disposal manifests are included in Appendix A.
Analytical Results:
Confirmation soil samples were obtained from the excavated basin sidewalls and basin floor,
examined, and scanned with a photoionization detector (PID). The sample identifications,
locations, and PID results were as follows:
• OE-1, south sidewall, 6 ft. bgs, 0.0 ppm (PID).
• OE-2, east side wall, 6 ft. bgs, 117.8 ppm (PID).
• OE-3, north side wall, 6 ft. bgs, 273.4 ppm (PID).
• OE-4, west side wall, 9 ft. bgs, 0.0 ppm (PID).
• OE-5, basin bottom, 10.5 ft. bgs, 0.8 ppm (PID).
Reference: ppm refers to parts -per -million; bgs refers to below ground surface.
PM Environmental, Inc.
Page 8

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4231-0-0002; November 21, 2017
Analysis of the subsurface confirmation soil samples obtained from the former tank basin
indicated various concentrations of VOCs, SVOCs, and MADEP-VPH and EPH analytes in each
of the soil samples above the laboratory method detection limit. However, only soil samples
collected from OE-2 and OE-3 (north and east side walls) revealed concentrations exceeding
the NCDEQ Soil to Groundwater Maximum Soil Contaminant Concentration (MSCC) criteria.
Detected concentrations of two MADEP VPH/EPH analytes exceeded the Residential MSCC
but not the Industrial / Commercial MSCC criteria in samples OE-2 and OE-3.
The analytical results are summarized in Table 3 and illustrated on Figure 3.
The Soil to Groundwater MSCC criteria is used as the guideline for limiting the over -excavation
of soil in a UST basin. The analytical results indicated that the sidewall excavation was
completed within this guideline, with the exception of the result from sample OE-2 and OE-3
which indicated an estimated concentration of a various VOCs, SVOCs and VPH/EPH
constituents.
The analytical results are summarized in Table 3 along with the criteria used by the NCDEQ,
Division of Waste Management — UST Section. The laboratory analytical report and chain of
custody is provided in Appendix C.
J. Recommendations
In accordance with regulatory guidelines for the closure of USTs when soil remains in the
subsurface that exceeds the Soil to Groundwater MSCCs and/or a water supply well is located
within 150 feet of the source area, additional assessment of the onsite groundwater is required
(e.g. Limited Site Assessment). However, due to the uncertainty of encountering groundwater
based on the potential of bedrock in the area of the former UST basin and cost, the subject
property owner has opted to abandon the current water supply well and replace the well at a
location of the subject property at a distance greater than 250 feet from the source area.
Based on the proposed abandonment of the current water supply well, replacement of the well
at a distance of greater than 250 feet from the source area, and no additional wells within 500
feet of the property boundary, PM recommends that the incident be classified as low risk and
granted a conditional No Further Action at the completion of the following actions:
• The current water supply well be abandoned in accordance with state and local
guidelines by a Certified North Carolina well contractor. At the completion of the
abandonment a well abandonment record be submitted to the NCDEQ — UST Section.
• A notice of residual petroleum (NORP) be filed with the Cabarrus County Register of
Deeds Office, restricting soils in the area of the former UST and groundwater use with
the exception of the proposed planned water supply well which will be located greater
than 250 feet from the source area.
PM Environmental, Inc.
Page 9

Initial Abatement Action Report for the Joyce Needham Residence
Located at 1830 Old Salisbury -Concord Road, Concord, North Carolina
PM Environmental, Inc., Project No. 15-4231-0-0002; November 21, 2017
If you have any questions related to this document, please contact our Charlotte, North Carolina
office at 704-782-0555.
Sincerely,
PM ENVIRONMENTAL, INC.
9"� 0
Donald D. Warren John W. Hargraves, P.G.
Regional Manager Regional Manager/Senior Geologist
PM Environmental, Inc.
Page 10

CABARRUS COUNTY
SCALE 1:24.000
1 MILE 1/2 MILE 0 1 MILE
F==- =._..-_
FIGURE 1
PROPERTY VICINITY MAP
USGS, 7.6 MINUTE SERIES
CONCORD, NC QUADRANGLE, 1969. PHOTO REVISED 1987.
PROD:__ ---_---
RESIDENTIAL PROPER I Y
1830 OLD SALISBURY ROAD
CONCORD, NC

LA
$Z
I
LEGEND:
SURJECr PROPFRIY

OE
9 27
1(
A[—C9—C1
AI—C19—(
METH CHI
ACETONE
OTHER V(
SVOCs
OE-2
9 27/2017
6.0,
AI—05—C8
30.6
AI—C9—C78
2,409
AI—C19—C36
565
7r—C9—C22
1,060
METH CHLR
0.76
n—BUTYLB
2.15
sec—BUTYLB
1.83
tert—BUTYLB 0.057
E
0.421
ISOP
0.578
p—ISOPT
1.33
n—PROP
1.36
NAPH
3.03
1,2,4—TMB
5.1
1,3,5—TMB
2.1
X
2.13
OTHER VOCs
dADL
ACE
0.915
ANT
2.52
FL
0.153
F
1,24
1—M
5.24
2—M
7.16
NAPH
1.25
N—Nit
1.54
Ph
2.59
PY
1.05
OTHER SVOCs : L
G N ts,
LEGEND:
— — — — SUBJECT PROPERTY
EXCAVATION LIMITS
LIMITS OF FORMER UST BASIN
0
OVER EXCAVATION SAMPLE
ACE
ACENAPHTIfENE
ANT
ANTHRACENE
F
FLUORENE
FL
FLUORANTHENE
1—M
1-METHYLNAPiTHALENE
2—M
2-NIETHYLNAPHTHALENE
NAPH
NAPHTHALENE
Ph
PIIENANTHRENE
Py
PYRENE
T
TOLUENE
E
ETHYLBENZENE
X
XYLENES
AI—05—C8
ALIPHATICS C5-C8
AI—C9—C18
ALIPHATICS C9-C18
AI—C19—C36
ALIPHATICS C19-C36
Ar—C9—C22
AROMATICS C9-C22
N—Nit
NITROSDIPHENYLAMINE
1,3,5—TMB
1.15-FRIMETH'YLBENZENE
ISOP
ISOPROPYLBENZENE
p—ISOPT
p-ISOPROPYLTOLUENE
n—PROP
n-PROPYLBENZENE
n—BUTYLB
n-BUTYLBENZENE
sec—BUTYLB
sec-BUTYLBENZENE
tert—BUTYLB
tert-BUTYLBENZENE
METH CHLR
METHYLENE CHLORIDE
VOCs
VOLATILE ORGANIC COMPOUNDS
SVOCs
SEMI VOLATILE ORGANIC COMPOUNDS
MDL
METHOD DETECTION LIMIT
UNITS
mgfKg
7
VALUE EXCEEDS APPLICABLE CRITERIA
NOTES:
REFER TO TAELES FOR SPECIFIC
COMPOUNDS ANALYZED
EmlronmentW
& Egki ming
Seale"
FIGURE 3A
DETAILED DIAGRAM Of 1*1 IE SUBJE(I AREA
WITH OVER EXCAVATION SAMPLE LOCATIONS
AND ANALYTICAL RESULTS
RESIDENTIAL PROPIiR IY
1830 OLD SALISHt TRY ROAD
CONCORD, NC-
1= 199NURm 1E(LL DRN BY: CS 'l0/23/2017
0 VE1Nr•,f AL 20' CHKD BY: DDW SCALE. 1 = 20'
r Nor 1. oN TNS FILE NAME
SCUMAcc� r. 15-4231-0-002FOOROQ

Table 1: Site History — UST/AST System and Other Release Information
Revision Date:
Incident Number and Name: Pending/Joyce Needham Residence
Description
Was release
UST ID
Current/Last
Previous
Capacity
Construction
Tank
of Associated
Date
Status
associated
Number
Contents*
Contents*
(in gallons)
Details **
Dimensions
Piping and
Tank
of
with the UST
Installed
UST
Pumps
System?
Remove
1
Fuel Oil
Fuel Oil
Approx. 550
Steel
Unknown
1/4" copper
Unknown
8/17
Yes
lines
Description
Was release
AST ID
Current/Last
Previous
Capacity
Construction
Tank
of Associated
Date
Status
associated
Number
Contents*
Contents*
(in gallons)
Details **
Dimensions
Piping and
Tank
o ***
With the AST
Pumps
Installed
AST
System?
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Incident
Number
Material
Released
Date of
Release
Description of Release
Pending
Fuel Oil
Unknown —
A release of petroleum was suspected during UST removal in August 2017. Sample results
(suspected)
Discovered
confirmed a release which prompted the release notification.
on 8/ 17
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal
(specify date).

Table 2: Site History — UST/AST Owner/Operator and Other Responsible Party
Information
Revision Date:
Residence
Incident Number and Name: Pending/Joyce Needham
UST ID Number
1
Facility ID Number: N/A
Name of Owner: Joyce Needham
Dates of Operation: Unknown to Unknown
(mm/dd/yy to mm/dd. )
Street Address
257 Ponderosa Circle
City
State
Zip
Telephone Number
Mooresville
NC
28117
704-363-9942
Name of Operator
Date of Operation
(mm/dd/yy to mm/dd/yy)
Unknown
Unknown to Unknown
Street Address
1830 Old Salisbury -Concord Road
City
State
Zip
Tele hone Number
Concord
NC
28025
704-363-9942
-7
Incident Number
Pending
Name of Other Responsible Party
Date of Operation
(mm/dd/yy to mm/dd/yy)
Same as Owner
Street Address
City
State
Zip
Telephone Number
Add additional records for all owners, operators and responsible parties as necessary

TABLE 3
SUMMARY OF SOIL ANALYTICAL RESULTS
JOYCE NEEDHAM RESIDENCE
TPH-GRO, TPH-DRO, ALIPHATICSIAROMATICS, VOCS, AND SVOCS
1830 OLD SALISBURY-CONCORD ROAD IN CONCORD, NORTH CAROLINA
PM PROJECTS 15.4231-0-0002
TOTAL PETROLEUM HYDROCARBONS
GASOLINE RANGE ORGANICS (TPH-
GRO ,TOTAL PETROEEUM
HYDROCARBONS DIESEL RANGE
ORGANICS TPH-0RO , ALIPHATICS I
( )
AROMATICS, VOLATILE ORGANIC
COMPOUNDS (VOCs), AND SEMI
VOLATILE ORGANIC COMPOUNDS
(SVOCs). UNITS: (mglkg)
OD
U
io
Al_�
a
co
U
d'
U
a
(0
M
(�)
T
U
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a
a
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Chemical Abstract Service Number
(CAS#)
NA
NA
NA
NA
15.09.2
"-80-1
1-1A
13598-8
98-0&8
100>13
9&82-B
9J-B7d
1-11
91-20-3
108A&3
.3-6
108A7.8
1330-20-7
NA
83.32-9
120-12.7
20644-0
-73-7
90.12-0
91576
91-20.3
86-3M
8501-8
129.00-0
NA
71.43.2
108-BB-3
100i1i
1330.20.7
NA
NA
Sample ID
Sample Date
Sample Depth
(bgs)
MADEP VPH and EPH
VOCs
SVOCs
VOCs
(BTEX)
TPH
TPH
TP-1
8/29/2017
4.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
888
18,200
TP-2
8/29/2017
4.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
445
10,600
TP-3
8/29/2017
4.6
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
296
11,700
TP4
8/29/2017
4.5
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
BRL
70
TP-6
8/29/2017
7.0
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
BRL
BRL
0.44
2.43
104
8,010
OE-1
9/27/217
6.0
BRL
BRL
BRL
BRL
BRL
0.0453
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
OE-2
9/27/2017
6.0
30.6
2,409
565
1,060
0.76
BRL
2.15
1.83
0.057J
0.421
0.578
1.33
1.36
3.03
BRL
5.1
2.1
2.13
BRL
0.915
2.52
0.153J
1.24
5.24
7.10
1.25
1.54
2.59
1.05
BRL
BRL
BRL
0.421
2.13
NA
NA
OE-3
9/27/2017
6.0
42.2
2,846
575
1,674
0.636
BRL
2.33
2.13
0.1091
1.45
1
2.37
2.1
7.4
0.129J
9.07
5.16
7.94
BRL
1.67
BRL
0.248J
3.02
12.1
16.9
3.89
2.95
5.6
1.63J
BRL
BRL
0.129.1
1.45
7.94
NA
NA
OE4
9/27/2017
6.0
BRL
BRL
BRL
6.57J
0.0053J
0.0276J
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
OE-5
9/27I2017
t0.5
BRL
15
4.i6J
BRL
0.0042J
0.0317J
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
North Carolina Department of Environmental Quality, Division of Waste ManagementSoil, UST Section (NCDEQ UST) Soil Criteria
TPH
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
5o 100
Soil to Groundwater MSCC
68
540
IMMOBILE
31
0.02
24
4.3
3.3
3.4
4.9
1.7
0.12
1.7
0.16
4.3
8.5
8.3
4.6
Various
8.2
940
290
47
0.004
3.6
0.16
NE
56
270
Various
0.0056
4.3
4.9
4.6
NA NA
Residential MSCC
939
11500
31,000
469
85
14.000
626
626
626
1,560
1,564
100
626
313
1.200
782
782
3,129
Various
940
4,600
620
620
20
63
313
NE
469
469
Various
18
1200
1660
3129
NA NA
Industrial/Commercial MSCC
24,528
40.000
810,000
12,264
763
360.000
16.350
16,350
16,350
40,000
40,880
4,000
16,350
8,176
32,000
20,440
20,440
81,760
Various
24,000
122,000
16.400
16,400
100
1,635
8,176
NE
12,264
12,264
Various
164
32000
40000
81760
NA NA
Applicable Criterion/RBSL Exceeded
BOLD
Value Exceeds Applicable Criterion/RBSL
bgs
Below Ground Surface (feet)
BRL
Below the Laboratory Reporting Limit
NA
Not Applicable/Not Analyzed
NE
Not Established
TPH Total Petroleum Hydrocarbons
MADEP Massechusetts Department of Environmental Protection
J Estimated value above the laboratory method detecion limit (MDL) but below the Reporting Limit

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SGS ACCUTEST CCU ST �r
Southeast t
SGS ACCUTEST IS PART OF SGS, THE WORLD'S LEADING INSPECTION,
VERIFICATION, TESTING AND CERTIFICATION COMPANY.
Technical Report for
PM Environmental
Residential Property; Concord, NC
15-4231-0-0001
SGS Accutest Job Number: FA47950
Sampling Date: 09/27/17
Report to:
PM Environmental
8320 University Executive Park Dr Suite 106
Charlotte, NC 28262
[e-mail]
TTN: Don Warren
e-Hardeopy 2.0
Atttoinated Report
Total number of pages in report: 78
A FO
2
Test results contained within this data package meet the requirements Caitlin Brice, M.S.
of the National Environmental Laboratory Accreditation Program General Manager
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NQ573), N1(FLO02), NY(12022), SC(96038001)
Doll) ELAP(L-A-B L2229), AZ(AZO806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except In its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • hnp://www.accutest.com
SGS Accutest is the sole authority for authorizing edits or modifications to this document. 1 of 78
Unauthorized modification of this report is strictly prohibited. SGS ACCUTEST
Review standard terms at: http://www.sgs.com/en/terms-and-conditions FA47950

Sections:
Table of Contents
Section1: Sample Summary...................................................................................................
3
Section2: Summary of Hits....................................................................................................
4
Section3: Sample Results........................................................................................................
6
3.1: FA47950-1: OE-1.........................................................................................................
7
3.2: FA47950-2: OE-2.........................................................................................................
14
a
3.3: FA47950-3: OE-3.........................................................................................................
3.4: FA47950-4: OE-4.........................................................................................................
21
28
3.5: FA47950-5: OE-5.........................................................................................................
Section4: Misc. Forms....................................................................................................
35
42
4.1: Chain of Custody...........................................................................................................
Section 5: MS Volatiles - QC Data Summaries.....................................................................
43
45
5.1: Method Blank Summary................................................................................................
46
5.2: Blank Spike Summary...................................................................................................
49
..
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
52
Section 6: MS Semi-volatiles - QC Data Summaries............................................................
55
6.1: Method Blank Summary
6.2: Blank Spike Summary...................................................................................................
60
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
62
Section 7: GC/LC Semi-volatiles - QC Data Summaries.....................................................
64
7.1: Method Blank Summary................................................................................................
65
7.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
66
7.3: Duplicate Summary.......................................................................................................
67
Section 8: Misc. Forms (SGS Accutest Lafayette).................................................................
68
8.1: Chain of Custody...........................................................................................................
69
Section 9: GC Volatiles - QC Data (SGS Accutest Lafayette) ..............................................
72
9.1: Method Blank Summary................................................................................................
73
9.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
75
9.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
77
SGS2U
of 78
ACCT
T EST
v
FA47950

SGS Accutest
Sample Summary
PM Environmental
Residential Property; Concord, NC
Project No: 15-4231-0-0001
Job No: FA47950
;ample Collected Matrix Client
Dumber Date Time By Received Code Type Sample ID
FA47950-1 09/27/17 10:00 DW 09/29/17 SO Soil OE-1
FA47950-2 09/27/17 09:30 DW 09/29/17 SO Soil OE-2
FA47950-3 09/27/17 14:00 DW 09/29/17 SO Soil OE-3
FA47950-4 09/27/17 15:30 DW 09/29/17 SO Soil OE-4
FA47950-5 09/27/17 15:45 DW 09/29/17 SO Soil OE-5
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
SGS� 1 3 of 78
, ACCUTEST
FA47950

Summary of Hits Page 1 of 2
Job Number:
FA47950
Account:
PM Environmental
Project:
Residential Property; Concord, NC
Collected:
09/27/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA47950-1 OE-1
Acetone
0.0453 JB
0.057
0.011
mg/kg
SW846 8260B
FA47950-2 OE-2
n-Butylbenzene
2.15
0.26
0.053
mg/kg
SW846 8260B
sec-Butylbenzene
1.83
0.26
0.053
mg/kg
SW846 8260B
tert-Butylbenzene
0.0570 J
0.26
0.053
mg/kg
SW846 8260B
Ethylbenzene
0.421
0.26
0.053
mg/kg
SW846 8260B
Isopropylbenzene
0.578
0.26
0.053
mg/kg
SW846 8260B
p-Isopropyltoluene
1.33
0.26
0.053
mg/kg
SW846 8260B
Methylene Chloride a
0.760 B
0.53
0.21
mg/kg
SW846 8260B
Naphthalene
3.03
0.26
0.11
mg/kg
SW846 8260B
n-Propylbenzene
1.36
0.26
0.053
mg/kg
SW846 8260B
1,2,4-Trimethylbenzene
5.10
0.26
0.053
mg/kg
SW846 8260B
1,3,5-Trimethylbenzene
2.10
0.26
0.053
mg/kg
SW846 8260B
m,p-Xylene
1.37
0.53
0.058
mg/kg
SW846 8260B
o-Xylene
0.760
0.26
0.053
mg/kg
SW846 8260B
Xylene (total)
2.13
0.79
0.11
mg/kg
SW846 8260B
Acenaphthene
0.915
0.90
0.096
mg/kg
SW846 8270D
Andwacene
2.52
0.90
0.10
mg/kg
SW846 8270D
Fluoranthene
0.153 J
0.90
0.090
mg/kg
SW846 8270D
Fluorene
1.24
0.90
0.097
mg/kg
SW846 8270D
1-Methylnaphthalene
5.24
0.90
0.090
mg/kg
SW846 8270D
2-Methylnaphthalene
7.16
0.90
0.090
mg/kg
SW846 8270D
Naphthalene
1.25
0.90
0.090
mg/kg
SW846 8270D
N-Nitrosodiphenylamine
1.54
0.90
0.097
mg/kg
SW846 8270D
Phenanthrene
2.59
0.90
0.090
mg/kg
SW846 8270D
Pyrene
1.05
0.90
0.10
mg/kg
SW846 8270D
C5-C8 Aliphatics (Unadj.) b
30.6
12
mg/kg
MADEP VPH REV 1.1
C9-02 Aliphatics (Unadj.) b
149
12
mg/kg
MADEP VPH REV 1.1
C9-CIO Aromatics (Unadj.) b
67.0
12
mg/kg
MADEP VPH REV 1.1
C11-C22 Aromatics (Unadj.)
993
220
87
mg/kg
MADEP EPH REV 1.1
C9-C18 Aliphatics
2260
430
110
mg/kg
MADEP EPH REV 1.1
C19-C36 Aliphatics
565
220
54
mg/kg
MADEP EPH REV 1.1
FA47950-3 OE-3
n-Butylbenzene
2.33
0.32
0.063
mg/kg
SW846 8260B
sec-Butylbenzene
2.13
0.32
0.063
mg/kg
SW846 8260B
tert-Butylbenzene
0.109 J
0.32
0.063
mg/kg
SW846 8260B
Ethylbenzene
1.45
0.32
0.063
mg/kg
SW846 8260B
Isopropylbenzene
1.00
0.32
0.063
mg/kg
SW846 8260B
p-Isopropyltoluene
2.37
0.32
0.063
mg/kg
SW846 8260B
t%1% 1 4 of 78
_...s -U ACCUTEST
FA47950

Summary of Hits Page 2 of 2
Job Number:
FA47950
Account:
PM Environmental
Project:
Residential Property; Concord, NC
Collected:
09/27/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Methylene Chloride a
0.636 B
0.63
0.25
mg/kg
SW846 8260B
Naphthalene
7.40
0.32
0.13
mg/kg
SW846 8260B
n-Propylbenzene
2.10
0.32
0.063
mg/kg
SW846 8260B
Toluene
0.129 JB
0.32
0.063
mg/kg
SW846 8260B
1,2,4-Trimethylbenzene
9.07
0.32
0.063
mg/kg
SW846 8260B
1,3,5-Trimethylbenzene
5.16
0.32
0.063
mg/kg
SW846 8260B
m,p-Xylene
5.23
0.63
0.069
mg/kg
SW846 8260B
o-Xylene
2.71
0.32
0.063
mg/kg
SW846 8260B
Xylene (total)
7.94
0.95
0.13
mg/kg
SW846 8260B
Acenaphthene
1.67 J
1.9
0.20
mg/kg
SW846 8270D
Fluoranthene
0.248 J
1.9
0.19
mg/kg
SW846 8270D
Fluorene
3.02
1.9
0.20
mg/kg
SW846 8270D
1-Methylnaphthalene
12.1
1.9
0.19
mg/kg
SW846 8270D
2-Methylnaphthalene
16.9
1.9
0.19
mg/kg
SW846 8270D
Naphthalene
3.89
1.9
0.19
mg/kg
SW846 8270D
N-Nitrosodiphenylamine
2.95
1.9
0.20
mg/kg
SW846 8270D
Phenanthrene
5.60
1.9
0.19
mg/kg
SW846 8270D
Pyrene
1.63 J
1.9
0.22
mg/kg
SW846 8270D
C5-C8 Aliphatics (Unadj.) b
42.2
12
mg/kg
MADEP VPH REV 1.1
C9-C12 Aliphatics (Unadj.) b
286
12
mg/kg
MADEP VPH REV 1A
C9-CIO Aromatics (Unadj.) b
174
24
mg/kg
MADEP VPH REV 1.1
C11-C22 Aromatics (Unadj.)
1500
230
90
mg/kg
MADEP EPH REV 1.1
C9-C18 Aliphatics
2560
450
110
mg/kg
MADEP EPH REV 1.1
C19-C36 Aliphatics
575
230
56
mg/kg
MADEP EPH REV 1.1
FA47950-4 OE4
Acetone
0.0276 JB
0.055
0.011
mg/kg
SW846 8260B
Methylene Chloride a
0.0053 JB
0.011
0.0044
mg/kg
SW846 8260B
C11-C22 Aromatics (Unadj.)
6.57 J
11
4.4
mg/kg
MADEP EPH REV 1.1
FA47950-5 OE-5
Acetone
0.0317 JB
0.049
0.0098
mg/kg
SW846 8260B
Methylene Chloride a
0.0042 JB
0.0098
0.0039
mg/kg
SW846 8260B
C9-02 Aliphatics (Unadj.) b
3.44 J
11
mg/kg
MADEP VPH REV 1.1
C9-C18 Aliphatics
15.0
11
2.7
mg/kg
MADEP EPH REV 1.1
C19-C36 Aliphatics
4.16 J
11
2.7
mg/kg
MADEP EPH REV 1.1
(a) Suspected laboratory contaminant.
(b) Analysis performed at SGS Accutest, Lafayette, LA.
5of78
_..� ACCUTEST
FA47950

SGS, ACCUTEST
Southeast
Sample Results
Report of Analysis
Section 3
SGS ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-1
Lab Sample ID: FA47950-1 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.0
Project: Residential Property; Concord, NC
Page 1 of 3
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0123663.1) 1 09/29/17 16:25 EP n/a n/a VC4896
Run #2
Initial Weight Final Volume
Run #1 4.79 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units
67-64-1
Acetone
0.0453
0.057
0.011
mg/kg
71-43-2
Benzene
ND
0.0057
0.0014
mg/kg
108-86-1
Bromobenzene
ND
0.0057
0.0011
mg/kg
74-97-5
Bromochloromethane
ND
0.0057
0.0017
mg/kg
75-27-4
Bromodichloromethane
ND
0.0057
0.0011
mg/kg
75-25-2
Bromoform
ND
0.0057
0.0011
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.029
0.0083
mg/kg
104-51-8
n-Butylbenzene
ND
0.0057
0.0011
mg/kg
135-98-8
sec-Butylbenzene
ND
0.0057
0.0011
mg/kg
98-06-6
ter[-Butylbenzene
ND
0.0057
0.0011
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0057
0.0012
mg/kg
108-90-7
Chlorobenzene
ND
0.0057
0.0011
mg/kg
75-00-3
Chloroethane
ND
0.0057
0.0023
mgAg
67-66-3
Chloroform
ND
0.0057
0.0015
mg/kg
95-49-8
o-Chlorotoluene
ND
0.0057
0.0011
mg/kg
106-43-4
p-Chlorotoluene
ND
0.0057
0.0011
mg/kg
124-48-1
Dibromochloromethane
ND
0.0057
0.0011
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0057
0.0011
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0057
0.0023
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0057
0.0011
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0057
0.0011
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0057
0.0013
mgAg
75-34-3
1,1-Dichloroethane
ND
0.0057
0.0020
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0057
0.0011
mg/kg
75-35-4
1,1-Dichloroethylene
ND
0.0057
0.0011
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0057
0.0016
mg/kg
156-60-5
trans- 1, 2-Dichloroethylene a
ND
0.0057
0.0011
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0057
0.0011
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.0057
0.0011
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.0057
0.0011
mg/kg
563-58-6
1,1-Dichloropropee
ND
0.0057
0.0012
mg/kg
10061-01-5
cis-1,3-Dichloropropene a
ND
0.0057
0.0011
mgAg
L
JB
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS. ACCUTEST
FA47050

SGS Accutest
Report of Analysis
Client Sample ID: OE-1
Lab Sample ID: FA47950-1 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.0
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units
10061-02-6
trans-1,3-Dichloropropene
ND
0.0057
0.0011
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.0057
0.0027
mg/kg
64-17-5
Ethyl Alcohol
ND
0.46
0.086
mg/kg
100-41-4
Ethylbenzene
ND
0.0057
0.0011
mg/kg
591-78-6
2-Hexamme
ND
0.029
0.0086
mg/kg
98-82-8
Isopropylbenzene
ND
0.0057
0.0011
mg/kg
99-87-6
p-Isopropyltoluene
ND
0.0057
0.0011
mg/kg
74-83-9
Methyl Bromide
ND
0.0057
0.0023
mg/kg
74-87-3
Methyl Chloride
ND
0.0057
0.0023
mg/kg
75-09-2
Methylene Chloride
ND
0.011
0.0046
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.029
0.0086
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0057
0.0011
mg/kg
91-20-3
Naphthalene
ND
0.0057
0.0023
mg/kg
103-65-1
n-Propylbenzene
ND
0.0057
0.0011
mg/kg
100-42-5
Styrene
ND
0.0057
0.0011
mg/kg
630-20-6
1, 1, 1, 2-Tetrachloroethane
ND
0.0057
0.0012
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0057
0.0011
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0057
0.0015
mg/kg
108-88-3
Toluene
ND
0.0057
0.0011
mg/kg
87-61-6
1,2,3-Trichlorobenzene
ND
0.0057
0.0016
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.0057
0.0011
mg/kg
71-55-6
1,1,1-Trichloroethane
ND
0.0057
0.0011
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.0057
0.0011
mg/kg
79-01-6
Trichloroethylene
ND
0.0057
0.0011
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0057
0.0023
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.0057
0.0014
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0057
0.0011
mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.0057
0.0011
mg/kg
108-05-4
Vinyl Acetate a
ND
0.029
0.019
mg/kg
75-01-4
Vinyl Chloride
ND
0.0057
0.0011
mg/kg
m,p-Xylene
ND
0.011
0.0013
mg/kg
95-47-6
o-Xylene
ND
0.0057
0.0011
mg/kg
1330-20-7
Xylene (total)
ND
0.017
0.0024
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
105%
75-124%
17060-07-0
1,2-Dichloroethane-D4
113%
72-135%
2037-26-5
Toluene-D8
89%
75-126%
460-00-4
4-Bromofluorobenzene
97%
71-133%
c
Page 2 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
S$ TEST SG ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-1
Lab Sample ID: FA47950-1 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.0
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
Page 3 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 78
SGS" ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:
OE-1
Lab Sample ID:
FA47950-1 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8270D SW846 3550C Percent Solids: 91.0
Project:
Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X056141.1) 1 10/06/17 12:35 MV 10/04/17 08:22 OP67062 SX2373
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid
ND
0.92
0.18
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.18
0.021
mg/kg
95-57-8
2-Chlorophenol
ND
0.18
0.022
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.18
0.021
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.18
0.049
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.92
0.18
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.37
0.073
mg/kg
95-48-7
2-Methylphenol
ND
0.18
0.022
mg/kg
3&4-Methylphenol
ND
0.18
0.030
mg/kg
88-75-5
2-Nitrophenol
ND
0.18
0.020
mg/kg
100-02-7
4-Nitrophenol
ND
0.92
0.18
mg/kg
87-86-5
Pentachlorophenol
ND
0.92
0.18
mg/kg
108-95-2
Phenol
ND
0.18
0.018
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.18
0.021
mg/kg
83-32-9
Acenaphthene
ND
0.18
0.019
mg/kg
208-96-8
Acenaphthylene
ND
0.18
0.018
mg/kg
120-12-7
Anthracene
ND
0.18
0.021
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.18
0.018
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.18
0.022
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.18
0.020
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.18
0.019
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.18
0.024
mgAg
100-51-6
Benzyl Alcohol
ND
0.18
0.018
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.18
0.019
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.18
0.037
mg/kg
106-47-8
4-Chloroaniline
ND
0.18
0.046
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.18
0.018
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.18
0.021
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.18
0.023
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.18
0.018
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.18
0.018
mg/kg
218-01-9
Chrysene
ND
0.18
0.019
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 78
SGS ACCUTEST
FA47959

SGS Accutest
Report of Analysis
Page 2 of 2
Client Sample ID:
OE-1
Lab Sample ID:
FA47950-1 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8270D SW846 3550C Percent Solids: 91.0
Project:
Residential Property; Concord, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.18
0.023
mg/kg
132-64-9
Dibenzofuran
ND
0.18
0.018
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.18
0.018
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.18
0.020
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.18
0.024
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.18
0.044
mg/kg
84-66-2
Diethyl Phthalate
ND
0.37
0.037
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.18
0.037
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.18
0.037
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.37
0.073
mg/kg
122-66-7
1,2-Dipheny1hydrazine
ND
0.18
0.018
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.37
0.037
mg/kg
206-44-0
Fluoranthene
ND
0.18
0.018
mg/kg
86-73-7
Fluorene
ND
0.18
0.020
mg/kg
118-74-1
Hexachlorobenzene
ND
0.18
0.019
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.18
0.019
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.18
0.037
mg/kg
67-72-1
Hexachloroethane
ND
0.18
0.022
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.18
0.022
mg/kg
78-59-1
Isophorone
ND
0.18
0.018
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.18
0.018
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.18
0.018
mg/kg
91-20-3
Naphthalene
ND
0.18
0.018
mg/kg
98-95-3
Nitrobenzene
ND
0.18
0.018
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.18
0.018
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.18
0.020
mg/kg
85-01-8
Phenanthrene
ND
0.18
0.018
mg/kg
129-00-0
Pyrene
ND
0.18
0.021
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.18
0.022
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
77%
40-102%
4165-62-2
Phenol-d5
77%
41-100%
118-79-6
2,4,6-Tribromophenol
86%
42-108%
4165-60-0
Nitrobenzene-d5
76%
40-105%
321-60-8
2-Fluorobiphenyl
77%
43-107%
1718-51-0
Terphenyl-d14
85%
45-119%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
/+
11 of 78
SGS; ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-1
Lab Sample ID: FA47950-1 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP VPH REV 1.1 Percent Solids: 91.0
Project: Residential Property; Concord, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE328995.D 1 10/11/17 14:04 ALA n/a n/a L:GLE1105
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.0 g 5.0 ml 50.0 ul
Run #2
MA VPH list
CAS No. Compound
Result
RL
Units Q
C5-C8 Aliphatics (Unadj.)
ND
12
mg/kg
C9-02 Aliphatics (Unadj.)
ND
12
mg/kg
C9-CIO Aromatics (Unadj.)
ND
12
mg/kg
CAS No. Surrogate Recoveries
Run# 1
Run# 2
Limits
615-59-8 2,5-Dibromotoluene
93% b
70-130%
615-59-8 2,5-Dibromotoluene
86% c
70-130%
(a) Analysis performed at SGS Accutest, Lafayette,
LA.
(b) Recovery from Aliphatics fraction.
(c) Recovery from Aromatics fraction.
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
12 of 78
SAGS ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Page 1 of 1
Client Sample ID: OE-1
Lab Sample ID: FA47950-1 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 91.0
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN020655.1) 1 10/13/17 16:47 MRE 10/04/1711:50 OP67067 GNN1021
Run #2
Initial Weight Final Volume
Run #1 20.4 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
C11-C22 Aromatics (Unadj.)
ND
C9-C18 Aliphatics
ND
C19-06 Aliphatics
ND
CAS No.
Surrogate Recoveries
Run# 1
3386-33-2
1-Chlorooctadecane
64%
580-13-2
2-Bromonaphthalene
89%
84-15-1
o-Terphenyl
78%
321-60-8
2-Fluorobiphenyl
87%
RL
MDL Units Q
11
4.3 mg/kg
11
2.7 mg/kg
11
2.7 mg/kg
Run# 2
Limits
40-140%
40-140%
40-140%
40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS_ ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of 3
Client Sample ID: OE-2
Lab Sample ID: FA47950-2 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.2
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0123664.1) 1 09/29/17 16:50 EP n/a n/a VC4896
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.72 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
2.6
0.53
mg/kg
71-43-2
Benzene
ND
0.26
0.064
mg/kg
108-86-1
Bromobenzene
ND
0.26
0.053
mg/kg
74-97-5
Bromochloromethane
ND
0.26
0.078
mg/kg
75-27-4
Bromodichloromethane
ND
0.26
0.053
mg/kg
75-25-2
Bromoform
ND
0.26
0.053
mg/kg
78-93-3
2-Butanone (MEK)
ND
1.3
0.38
mg/kg
104-51-8
n-Butylbenzene
2.15
0.26
0.053
mg/kg
135-98-8
sec-Butylbenzene
1.83
0.26
0.053
mg/kg
98-06-6
tert-Butylbenzene
0.0570
0.26
0.053
mg/kg J
56-23-5
Carbon Tetrachloride
ND
0.26
0.054
mg/kg
108-90-7
Chlorobenzene
ND
0.26
0.053
mg/kg
75-00-3
Chloroethane
ND
0.26
0.11
mg/kg
67-66-3
Chloroform
ND
0.26
0.070
mg/kg
95-49-8
o-Chlorotoluene
ND
0.26
0.053
mg/kg
106-43-4
p-Chlorotoluene
ND
0.26
0.053
mg/kg
124-48-1
Dibromochloromethane
ND
0.26
0.053
mgAg
106-93-4
1,2-Dibromoethane
ND
0.26
0.053
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.26
0.11
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.26
0.053
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.26
0.053
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.26
0.061
mgAg
75-34-3
1,1-Dichloroethane
ND
0.26
0.093
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.26
0.053
mg/kg
75-35-4
1,1-Dichloroethylene
ND
0.26
0.053
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.26
0.073
mg/kg
156-60-5
Mans- 1,2-Dichloroethylene a
ND
0.26
0.053
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.26
0.053
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.26
0.053
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.26
0.053
mgAg
563-58-6
1,1-Dichloropropene
ND
0.26
0.054
mg/kg
10061-01-5
cis-1,3-Dichloropropene a
ND
0.26
0.053
mgAg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
+ 14of78
SGS; ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-2
Lab Sample ID: FA47950-2 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.2
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans-1,3-Dichloropropene
ND
0.26
0.053
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.26
0.12
mg/kg
64-17-5
Ethyl Alcohol
ND
21
4.0
mg/kg
100-41-4
Ethylbenzene
0.421
0.26
0.053
mg/kg
591-78-6
2-Hexanone
ND
1.3
0.40
mg/kg
98-82-8
Isopropylbenzene
0.578
0.26
0.053
mg/kg
99-87-6
p-Isopropyltoluene
1.33
0.26
0.053
mg/kg
74-83-9
Methyl Bromide
ND
0.26
0.11
mg/kg
74-87-3
Methyl Chloride
ND
0.26
0.11
mg/kg
75-09-2
Methylene Chloride b
0.760
0.53
0.21
mg/kg B
108-10-1
4-Methyl-2-pentanone (MIBK) ND
1.3
0.40
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.26
0.053
mg/kg
91-20-3
Naphthalene
3.03
0.26
0.11
mg/kg
103-65-1
n-Propylbenzene
1.36
0.26
0.053
mg/kg
100-42-5
Styrene
ND
0.26
0.053
mg/kg
630-20-6
1, 1, 1, 2-Tetrachloroethane
ND
0.26
0.054
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.26
0.053
mg/kg
127-18-4
Tetrachloroethylene
ND
0.26
0.068
mg/kg
108-88-3
Toluene
ND
0.26
0.053
mg/kg
87-61-6
1,2,3-Trichlorobenzene
ND
0.26
0.074
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.26
0.053
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.26
0.053
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.26
0.053
mg/kg
79-01-6
Trichloroethylene
ND
0.26
0.053
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.26
0.11
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.26
0.066
mg/kg
95-63-6
1,2,4-Trimethylbenzene
5.10
0.26
0.053
mg/kg
108-67-8
1,3,5-Trimethylbenzene
2.10
0.26
0.053
mg/kg
108-05-4
Vinyl Acetate a
ND
1.3
0.87
mg/kg
75-01-4
Vinyl Chloride
ND
0.26
0.053
mg/kg
m,p-Xylene
1.37
0.53
0.058
mg/kg
95-47-6
o-Xylene
0.760
0.26
0.053
mg/kg
1330-20-7
Xylene (total)
2.13
0.79
0.11
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
101%
75-124%
17060-07-0
1, 2-Dichloroethane-D4
108%
72-135%
2037-26-5
Toluene-D8
98%
75-126%
460-00-4
4-Bromofluorobenzene
98%
71-133%
Page 2 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
w
N
a
SG AC15 of 78
CUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-2
Lab Sample ID: FA47950-2 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.2
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Suspected laboratory contaminant.
Page 3 of 3 r;
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
78
SG ACC of UTEST
FA47950

SGS Accutest
Report of Analysis
Page 1 of 2
Client Sample ID:
OE-2
Lab Sample ID:
FA47950-2
Date Sampled: 09/27/17
Matrix:
SO - Soil
Date Received: 09/29/17
Method:
SW846 8270D SW846 3550C
Percent Solids: 91.2
Project:
Residential Property; Concord, NC
File ID
DF Analyzed By
Prep Date Prep Batch Analytical Batch
Run #1 X056142.1)
5 10/06/17 13:01 MV
10/04/17 08:22 OP67062 SX2373
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
4.5
0.90
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.90
0.10
mg/kg
95-57-8
2-Chlorophenol
ND
0.90
0.11
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.90
0.10
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.90
0.24
mg/kg
51-28-5
2,4-Dinitrophenol
ND
4.5
0.90
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
1.8
0.36
mg/kg
95-48-7
2-Methylphenol
ND
0.90
0.11
mg/kg
3&4-Methylphenol
ND
0.90
0.15
mg/kg
88-75-5
2-Nitrophenol
ND
0.90
0.098
mg/kg
100-02-7
4-Nitrophenol
ND
4.5
0.90
mg/kg
87-86-5
Pentachlorophenol
ND
4.5
0.90
mg/kg
108-95-2
Phenol
ND
0.90
0.090
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.90
0.10
mg/kg
83-32-9
Acenaphthene
0.915
0.90
0.096
mg/kg
208-96-8
Acenaphthylene
ND
0.90
0.090
mg/kg
120-12-7
Anthracene
2.52
0.90
0.10
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.90
0.090
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.90
0.11
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.90
0.099
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.90
0.093
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.90
0.12
mg/kg
100-51-6
Benzyl Alcohol
ND
0.90
0.090
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.90
0.094
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.90
0.18
mg/kg
106-47-8
4-Chloroaniline
ND
0.90
0.23
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.90
0.090
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.90
0.10
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.90
0.11
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.90
0.090
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.90
0.090
mg/kg
218-01-9
Chrysene
ND
0.90
0.092
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
(►
17 of 78
SGS, ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-2
Lab Sample ID: FA47950-2 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8270D SW846 3550C Percent Solids: 91.2
Project: Residential Property; Concord, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.90
0.11
mg/kg
132-64-9
Dibenzofuran
ND
0.90
0.090
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.90
0.090
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.90
0.097
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.90
0.12
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.90
0.21
mg/kg
84-66-2
Diethyl Phthalate
ND
1.8
0.18
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.90
0.18
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.90
0.18
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
1.8
0.36
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
0.90
0.090
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
1.8
0.18
mg/kg
206-44-0
Fluoranthene
0.153
0.90
0.090
mg/kg J
86-73-7
Fluorene
1.24
0.90
0.097
mg/kg
118-74-1
Hexachlorobenzene
ND
0.90
0.092
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.90
0.091
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.90
0.18
mg/kg
67-72-1
Hexachloroethane
ND
0.90
0.11
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.90
0.11
mg/kg
78-59-1
Isophorone
ND
0.90
0.090
mg/kg
90-12-0
1-Methylnaphthalene
5.24
0.90
0.090
mg/kg
91-57-6
2-Methylnaphthalene
7.16
0.90
0.090
mg/kg
91-20-3
Naphthalene
1.25
0.90
0.090
mg/kg
98-95-3
Nitrobenzene
ND
0.90
0.090
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.90
0.090
mg/kg
86-30-6
N-Nitrosodiphenylamine
1.54
0.90
0.097
mg/kg
85-01-8
Phenanthrene
2.59
0.90
0.090
mg/kg
129-00-0
Pyrene
1.05
0.90
0.10
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.90
0.11
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
71%
40-102%
4165-62-2
Phenol-d5
71%
41-100%
118-79-6
2,4,6-Tribromophenol
85%
42-1089,6'
4165-60-0
Nitrobenzene-d5
100%
40-105%
321-60-8
2-Fluorobiphenyl
78%
43-107%
1718-51-0
Terphenyl-d14
89%
45-119%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS 18 of T
of
FA47959

SGS Accutest
Report of Analysis
Client Sample ID: OE-2
Lab Sample ID: FA47950-2
Matrix: SO - Soil
Method: MADEP VPH REV 1.1
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date
Run #1 a LE328999.1) 1 10/11/17 16:15 ALA n/a
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.9 g 5.0 ml 50.0 ul
Run #2
MA VPH list
CAS No. Compound
Result
C5-C8 Aliphatics (Unadj.)
30.6
C9-C12 Aliphatics (Unadj.)
149
C9-C10 Aromatics (Unadj.)
67.0
CAS No. Surrogate Recoveries
Run# 1
615-59-8 2,5-Dibromotoluene
109% b
615-59-8 2,5-Dibromotoluene
82% c
(a) Analysis performed at SGS Accutest, Lafayette, LA.
(b) Recovery from Aliphatics fraction.
(c) Recovery from Aromatics fraction.
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
RL Units Q
12 mg/kg
12 mg/kg
12 mg/kg
Run# 2 Limits
Page 1 of 1 N
Date Sampled: 09/27/17
Date Received: 09/29/17
Percent Solids: 91.2
70-130%
70-130%
Prep Batch Analytical Batch
n/a L:GLE1105
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
SGS19 of 78
ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-2
Lab Sample ID: FA47950-2 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 91.2
Project: Residential Property; Concord, NC
Page 1 of 1
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 NN020675.1)
20
10/16/17 14:36
MRE
10/04/1711:50
OP67067
GNN1022
Run #2 NN020678.1)
40
10/16/17 16:10
MRE
10/04/1711:50
OP67067
GNN1022
Initial Weight Final Volume
Run #1 20.2 g 2.0 ml
Run #2 20.2 g 2.0 ml
MAEPH List
CAS No.
Compound
Result
C11-C22 Aromatics (Unadj.)
993
C9-C18 Aliphatics
2260 a
C19-06 Aliphatics
565
CAS No.
Surrogate Recoveries
Run# 1
3386-33-2
1-Chlorooctadecane
0% b
580-13-2
2-Bromonaphthalene
0% b
84-15-1
o-Terphenyl
0% b
321-60-8
2-Fluorobiphenyl
0% b
(a) Result is
from Run# 2
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
RL MDL Units Q
220
87 mg/kg
430
110 mg/kg
220
54 mg/kg
Run# 2
Limits
0% b
40-140%
0% b
40-140%
0% b
40-140%
0% b
40-140%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
SGS ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of 3
Client Sample ID:
OE-3
Lab Sample ID:
FA47950-3 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8260B Percent Solids: 88.4
Project:
Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0123666.1) 1 09/29/17 17:39 EP n/a n/a VC4896
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.00 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
3.2
0.63
mg/kg
71-43-2
Benzene
ND
0.32
0.077
mg/kg
108-86-1
Bromobenzene
ND
0.32
0.063
mg/kg
74-97-5
Bromochloromethane
ND
0.32
0.093
mg/kg
75-27-4
Bromodichloromethane
ND
0.32
0.063
mg/kg
75-25-2
Bromoform
ND
0.32
0.063
mg/kg
78-93-3
2-Butanone (MEK)
ND
1.6
0.46
mg/kg
104-51-8
n-Butylbenzene
2.33
0.32
0.063
mg/kg
135-98-8
sec-Butylbenzene
2.13
0.32
0.063
mg/kg
98-06-6
tert-Butylbenzene
0.109
0.32
0.063
mg/kg J
56-23-5
Carbon Tetrachloride
ND
0.32
0.064
mg/kg
108-90-7
Chlorobenzene
ND
0.32
0.063
mg/kg
75-00-3
Chloroethane
ND
0.32
0.13
mg/kg
67-66-3
Chloroform
ND
0.32
0.084
mg/kg
95-49-8
o-Chlorotoluene
ND
0.32
0.063
mg/kg
106-43-4
p-Chlorotoluene
ND
0.32
0.063
mg/kg
124-48-1
Dibromochloromethane
ND
0.32
0.063
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.32
0.063
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.32
0.13
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.32
0.063
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.32
0.063
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.32
0.073
mg/kg
75-34-3
1,1-Dichloroethane
ND
0.32
0.11
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.32
0.063
mg/kg
75-35-4
1,1-Dichloroethylene
ND
0.32
0.063
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.32
0.087
mg/kg
156-60-5
trAm-1,2-Dichloroethylene a
ND
0.32
0.063
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.32
0.063
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.32
0.063
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.32
0.063
mg/kg
563-58-6
1,1-Dichloropropene
ND
0.32
0.064
mg/kg
10061-01-5
cis-1,3-Dichloropropene a
ND
0.32
0.063
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
Of% 21 of 78
�?.US ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-3
Lab Sample ID: FA47950-3 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 88.4
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans-1,3-Dichloropropene
ND
0.32
0.063
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.32
0.15
mg/kg
64-17-5
Ethyl Alcohol
ND
25
4.7
mg/kg
100-41-4
Ethylbenzene
1.45
0.32
0.063
mg/kg
591-78-6
2-Hexanone
ND
1.6
0.47
mg/kg
98-82-8
Isopropylbenzene
1.00
0.32
0.063
mg/kg
99-87-6
p-Isopropyltoluene
2.37
0.32
0.063
mg/kg
74-83-9
Methyl Bromide
ND
0.32
0.13
mg/kg
74-87-3
Methyl Chloride
ND
0.32
0.13
mg/kg
75-09-2
Methylene Chloride b
0.636
0.63
0.25
mg/kg B
108-10-1
4-Methyl-2-pentanone (MIBK) ND
1.6
0.47
mg/kg
1634-04-4
Methyl Teri Butyl Ether
ND
0.32
0.063
mg/kg
91-20-3
Naphthalene
7.40
0.32
0.13
mg/kg
103-65-1
n-Propylbenzene
2.10
0.32
0.063
mg/kg
10042-5
Styrene -
ND
0.32
0.063
mg/kg
630-20-6
1, 1, 1, 2-Tetrachloroethane
ND
0.32
0.065
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.32
0.063
mg/kg
127-18-4
Tetrachloroethylene
ND
0.32
0.081
mg/kg
108-88-3
Toluene
0.129
0.32
0.063
mg/kg JB
87-61-6
1,2,3-Trichlorobenzene
ND
0.32
0.088
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.32
0.063
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.32
0.063
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.32
0.063
mg/kg
79-01-6
Trichloroethylene
ND
0.32
0.063
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.32
0.13
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.32
0.079
mg/kg
95-63-6
1,2,4-Trimethylbenzene
9.07
0.32
0.063
mg/kg
108-67-8
1,3,5-Trimethylbenzene
5.16
0.32
0.063
mg/kg
108-05-4
Vinyl Acetate a
ND
1.6
1.0
mg/kg
75-01-4
Vinyl Chloride
ND
0.32
0.063
mg/kg
m,p-Xylene
5.23
0.63
0.069
mg/kg
95-47-6
o-Xylene
2.71
0.32
0.063
mg/kg
1330-20-7
Xylene (total)
7.94
0.95
0.13
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
98%
75-124%
17060-07-0
1,2-Dichloroethane-D4
105%
72-135%
2037-26-5
Toluene-D8
100%
75-126%
460-00-4
4-Bromofluorobenzene
98%
71-133%
Page 2 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
(�
22 of 78
SGS; ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-3
Lab Sample ID: FA47950-3 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 88.4
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Suspected laboratory contaminant.
Page 3 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
G ACCUTEST
FA47960

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:
OE-3
Lab Sample ID:
FA47950-3 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8270D SW846 3550C Percent Solids: 88.4
Project:
Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X056143.1) 10 10/06/17 13:26 MV 10/04/17 08:22 OP67062 SX2373
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
9.3
1.9
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
1.9
0.21
mg/kg
95-57-8
2-Chlorophenol
ND
1.9
0.23
mg/kg
120-83-2
2,4-Dichlorophenol
ND
1.9
0.21
mg/kg
105-67-9
2,4-Dimethylphenol
ND
1.9
0.50
mg/kg
51-28-5
2,4-Dinitrophenol
ND
9.3
1.9
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
3.7
0.75
mg/kg
95-48-7
2-Methylphenol
ND
1.9
0.22
mg/kg
3&4-Methylphenol
ND
1.9
0.31
mg/kg
88-75-5
2-Nitrophenol
ND
1.9
0.20
mg/kg
100-02-7
4-Nitrophenol
ND
9.3
1.9
mg/kg
87-86-5
Pentachlorophenol
ND
9.3
1.9
mg/kg
108-95-2
Phenol
ND
1.9
0.19
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
1.9
0.22
mg/kg
83-32-9
Acenaphthene
1.67
1.9
0.20
mg/kg J
208-96-8
Acenaphthylene
ND
1.9
0.19
mg/kg
120-12-7
Anthracene
ND
1.9
0.21
mg/kg
56-55-3
Benzo(a)anthracene
ND
1.9
0.19
mg/kg
50-32-8
Benzo(a)pyrene
ND
1.9
0.22
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
1.9
0.20
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
1.9
0.19
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
1.9
0.24
mg/kg
100-51-6
Benzyl Alcohol
ND
1.9
0.19
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
1.9
0.19
mg/kg
85-68-7
Butyl benzyl phthalate
ND
1.9
0.37
mg/kg
106-47-8
4-Chloroaniline
ND
1.9
0.47
mg/kg
111-91-1
bis(2-Chloroetboxy)methane
ND
1.9
0.19
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
1.9
0.22
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
1.9
0.23
mg/kg
91-58-7
2-Chloronaphthalene
ND
1.9
0.19
mg/kg
7005-72-3
4-Chlorophenol phenyl ether
ND
1.9
0.19
mg/kg
218-01-9
Chrysene
ND
1.9
0.19
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-3
Lab Sample ID: FA47950-3 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8270D SW846 3550C Percent Solids: 88.4
Project: Residential Property; Concord, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units
53-70-3
Dibenzo(a,h)anthracene
ND
1.9
0.23
mg/kg
132-64-9
Dibenzofuran
ND
1.9
0.19
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
1.9
0.19
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
1.9
0.20
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
1.9
0.25
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
1.9
0.44
mg/kg
84-66-2
Diethyl Phthalate
ND
3.7
0.37
mg/kg
131-11-3
Dimethyl Phthalate
ND
1.9
0.37
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
1.9
0.37
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
3.7
0.75
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
1.9
0.19
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
3.7
0.37
mg/kg
206-44-0
Fluoranthene
0.248
1.9
0.19
mg/kg
86-73-7
Fluorene
3.02
1.9
0.20
mg/kg
118-74-1
Hexachlorobenzene
ND
1.9
0.19
mg/kg
87-68-3
Hexachlorobutadiene
ND
1.9
0.19
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
1.9
0.37
mg/kg
67-72-1
Hexachloroethane
ND
1.9
0.22
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
1.9
0.23
mg/kg
78-59-1
Isophorone
ND
1.9
0.19
mg/kg
90-12-0
1-Methylnaphthalene
12.1
1.9
0.19
mg/kg
91-57-6
2-Methylnaphthalene
16.9
1.9
0.19
mg/kg
91-20-3
Naphthalene
3.89
1.9
0.19
mg/kg
98-95-3
Nitrobenzene
ND
1.9
0.19
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
1.9
0.19
mg/kg
86-30-6
N-Nitrosodiphenylamine
2.95
1.9
0.20
mg/kg
85-01-8
Phenanthrene
5.60
1.9
0.19
mg/kg
129-00-0
Pyrene
1.63
1.9
0.22
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
1.9
0.22
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
65%
40-102%
4165-62-2
Phenol-d5
68%
41-100%
118-79-6
2,4,6-Tribromophenol
79%
42-108%
4165-60-0
Nitrobenzene-d5
107% a
40-105%
321-60-8
2-Fluorobiphenyl
76%
43-107%
1718-51-0
Terphenyl-d14
87%
45-119%
(a) Outside control limits due to dilution.
0
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 78
SGS
ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of I
Client Sample ID:
OE-3,
Lab Sample ID:
FA47950-3
Date Sampled:
09/27/17
Matrix:
SO - Soil
Date Received:
09/29/17
Method:
MADEP VPH REV 1.1
Percent Solids:
88.4
Project:
Residential Property; Concord, NC
File ID
DF Analyzed By
Prep Date Prep Batch
Analytical Batch
Run #1 a LE328996.1) 1 10/11/17 14:36 ALA
n/a n/a
L:GLE1105
Run #2 a LE329033.1) 1 10/12/17 11:30 ALA
n/a n/a
L:GLE1107
Initial Weight Final Volume Methanol Aliquot
Run #1 5.2 g 5.0 ml 50.0 ul
Run #2 5.2 g 5.0 ml 25.0 ul
MA VPH list
CAS No. Compound
Result
RL
Units Q
C5-C8 Aliphatics (Unadj.)
42.2
12
mg/kg
C9-Cl2 Aliphatics (Unadj.)
286
12
mg/kg
C9-CIO Aromatics (Unadj.)
174 b
24
mg/kg
CAS No. Surrogate Recoveries
Run# 1
Run# 2
Limits
615-59-8 2,5-Dibromotoluene
163% c
143% c
70-130%
615-59-8 2,5-Dibromotoluene
88% d
104% d
70-130%
(a) Analysis performed at SGS Accutest, Lafayette, LA.
(b) Result is from Run# 2
(c) Recovery from Aliphatics fraction. Outside control limits due to matrix interference.
(d) Recovery from Aromatics fraction.
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
SGS ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-3
Lab Sample ID: FA47950-3 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 88.4
Project: Residential Property; Concord, NC
Page 1 of 1
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 NN020676.D
20
10/16/17 15:07
MRE
10/04/1711:50
OP67067
GNN1022
Run #2 NN020679.1)
40
10/16/17 17:01
MRE
10/04/1711:50
OP67067
GNN1022
Initial Weight Final Volume
Run #1 20.1 g 2.0 ml
Run #2 20.1 g 2.0 ml
MAEPH List
CAS No. Compound
Result
Cll-C22 Aromatics (Unadj.)
1500
C9-C18 Aliphatics
2560 a
C19-06 Aliphatics
575
CAS No. Surrogate Recoveries
Run# 1
3386-33-2-1-Chlorooctadecane
0% b
580-13-2 2-Bromonaphthalene
0% b
84-15-1 o-Terphenyl
0% b
321-60-8 2-Fluorobiphenyl
0% b
(a) Result is from Run# 2
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
RL MDL Units Q
230
90 mg/kg
450
110 mg/kg
230
56 mg/kg
Run# 2
Limits
0% b
40-140%
0% b
40-140%
0% b
40-140%
0% b
40-140%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
27 of 78
SGS ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-4
Lab Sample ID: FA47950-4
Matrix: SO - Soil
Method: SW846 8260B
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date
Run #1 C0123668.1) 1 09/29/17 18:29 EP n/a
Run #2
Initial Weight Final Volume
Run #1 5.00 g 5.0 ml
Run #2
VOA List for NC, May 2012
Page 1 of 3
r:
Date Sampled: 09/27/17
Date Received: 09/29/17
Percent Solids: 91.7
CAS No. Compound Result RL MDL Units
67-64-1
Acetone
0.0276
0.055
0.011
mg/kg
71-43-2
Benzene
ND
0.0055
0.0013
mg/kg
108-86-1
Bromobenzene
ND
0.0055
0.0011
mg/kg
74-97-5
Bromochloromethane
ND
0.0055
0.0016
mg/kg
75-27-4
Bromodichloromethane
ND
0.0055
0.0011
mg/kg
75-25-2
Bromoform
ND
0.0055
0.0011
mg/kg
78-93-3
2-Butanone (MEK)
ND
0.027
0.0079
mgAg
104-51-8
n-Butylbenzene
ND
0.0055
0.0011
mgNg
135-98-8
sec-Butylbenzene
ND
0.0055
0.0011
mg/kg
98-06-6
tert-Butylbenzene
ND
0.0055
0.0011
mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0055
0.0011
mg/kg
108-90-7
Chlorobenzene
ND
0.0055
0.0011
mgAg
75-00-3
Chloroethane
ND
0.0055
0.0022
mg/kg
67-66-3
Chloroform
ND
0.0055
0.0015
mg/kg
95-49-8
o-Chlorotoluene
ND
0.0055
0.0011
mgAg
106-43-4
p-Chlorotoluene
ND
0.0055
0.0011
mg/kg
124-48-1
Dibromochloromethane
ND
0.0055
0.0011
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0055
0.0011
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0055
0.0022
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0055
0.0011
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0055
0.0011
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0055
0.0013
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.0055
0.0019
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0055
0.0011
mgAg
75-35-4
1,1-Dichloroethylene
ND
0.0055
0.0011
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0055
0.0015
mg/kg
156-60-5
tram-1,2-Dichloroethylene a
ND
0.0055
0.0011
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0055
0.0011
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.0055
0.0011
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.0055
0.0011
mg/kg
563-58-6
1, 1 -Dichloropropene
ND
0.0055
0.0011
mg/kg
10061-01-5
cis-1,3-Dichloropropene a
ND
0.0055
0.0011
mg/kg
Prep Batch Analytical Batch
n/a VC4896
I
JB
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SG(� (� 28 of 78
ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Page 2 of 3
Client Sample ID:
OE-4
Lab Sample ID:
FA47950-4 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8260B Percent Solids: 91.7
Project:
Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans-1,3-Dichloropropene
ND
0.0055
0.0011
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.0055
0.0025
mg/kg
64-17-5
Ethyl Alcohol
ND
0.44
0.082
mg/kg
100-41-4
Ethylbenzene
ND
0.0055
0.0011
mg/kg
591-78-6
2-Hexanone
ND
0.027
0.0082
mg/kg
98-82-8
Isopropylbenzene
ND
0.0055
0.0011
mg/kg
99-87-6
p-Isopropyltoluene
ND
0.0055
0.0011
mg/kg
74-83-9
Methyl Bromide
ND
0.0055
0.0022
mg/kg
74-87-3
Methyl Chloride
ND
0.0055
0.0022
mg/kg
75-09-2
Methylene Chloride b
0.0053
0.011
0.0044
mg/kg JB
108-10-1
4-Methyl-2-pentanone (MIBK) ND
0.027
0.0082
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0055
0.0011
mg/kg
91-20-3
Naphthalene
ND
0.0055
0.0022
mg/kg
103-65-1
n-Propylbenzene
ND
0.0055
0.0011
mg/kg
100-42-5
Styrene
ND
0.0055
0.0011
mg/kg
630-20-6
1, 1, 1, 2-Tetrachloroethane
ND
0.0055
0.0011
mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0055
0.0011
mg/kg
127-18-4
Tetrachloroethylene
ND
0.0055
0.0014
mg/kg
108-88-3
Toluene
ND
0.0055
0.0011
mg/kg
87-61-6
1,2,3-Trichlorobenzene
ND
0.0055
0.0015
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.0055
0.0011
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0055
0.0011
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.0055
0.0011
mg/kg
79-01-6
Trichloroethylene
ND
0.0055
0.0011
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0055
0.0022
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.0055
0.0014
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0055
0.0011
mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.0055
0.0011
mg/kg
108-05-4
Vinyl Acetate a
ND
0.027
0.018
mg/kg
75-01-4
Vinyl Chloride
ND
0.0055
0.0011
mg/kg
m,p-Xylene
ND
0.011
0.0012
mg/kg
95-47-6
o-Xylene
ND
0.0055
0.0011
mg/kg
1330-20-7
Xylene (total)
ND
0.016
0.0023
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
105%
75-124%
17060-07-0
1,2-Dichloroethane-D4
115%
72-135%
2037-26-5
Toluene-D8
92%
75-126%
460-00-4
4-Bromofluorobenzene
100%
71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SG AC29 of 78
CUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-4
Lab Sample ID: FA47950-4 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.7
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Suspected laboratory contaminant.
Page 3 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
/�(�
30 of 78
SG8, ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:
OE-4
Lab Sample ID:
FA47950-4 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8270D SW846 3550C Percent Solids: 91.7
Project:
Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X056144.1) 1 10/06/17 13:52 MV 10/04/17 08:22 OP67062 SX2373
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid
ND
0.90
0.18
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.18
0.020
mg/kg
95-57-8
2-Chlorophenol
ND
0.18
0.022
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.18
0.021
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.18
0.048
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.90
0.18
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.36
0.072
mg/kg
95-48-7
2-Methylphenol
ND
0.18
0.022
mg/kg
3&4-Methylphenol
ND
0.18
0.030
mg/kg
88-75-5
2-Nitrophenol
ND
0.18
0.020
mg/kg
100-02-7
4-Nitrophenol
ND
0.90
0.18
mg/kg
87-86-5
Pentachlorophenol
ND
0.90
0.18
mg/kg
108-95-2
Phenol
ND
0.18
0.018
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.18
0.021
mg/kg
83-32-9
Acenaphthene
ND
0.18
0.019
mg/kg
208-96-8
Acenaphthylene
ND
0.18
0.018
mg/kg
120-12-7
Anthracene
ND
0.18
0.020
mg/kg
56-55-3
Benzo(a)anfluacene
ND
0.18
0.018
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.18
0.021
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.18
0.020
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.18
0.019
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.18
0.024
mg/kg
100-51-6
Benzyl Alcohol
ND
0.18
0.018
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.18
0.019
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.18
0.036
mgAg
106-47-8
4-Chloroaniline
ND
0.18
0.045
mg/kg
111-91-1
bis(2-Chloroetboxy)methane
ND
0.18
0.018
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.18
0.021
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.18
0.023
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.18
0.018
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.18
0.018
mg/kg
218-01-9
Chrysene
ND
0.18
0.018
mg/kg
G
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
$��31 of 78
ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-4
Lab Sample ID: FA47950-4 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8270D SW846 3550C Percent Solids: 91.7
Project: Residential Property; Concord, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units
53-70-3
Dibenzo(a,h)anthracene
ND
0.18
0.023
mg/kg
132-64-9
Dibenzoftran
ND
0.18
0.018
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.18
0.018
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.18
0.019
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.18
0.024
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.18
0.043
mg/kg
84-66-2
Diethyl Phthalate
ND
0.36
0.036
mg/kg
131-I1-3
Dimethyl Phthalate
ND
0.18
0.036
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.18
0.036
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.36
0.072
mg/kg
122-66-7
1,2-Diphenylhydraztne
ND
0.18
0.018
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.36
0.036
mg/kg
206-44-0
Fluoranthene
ND
0.18
0.018
mg/kg
86-73-7
Fluorene
ND
0.18
0.019
mg/kg
118-74-1
Hexachlorobenzene
ND
0.18
0.018
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.18
0.018
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.18
0.036
mg/kg
67-72-1
Hexachloroethane
ND
0.18
0.021
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.18
0.022
mg/kg
78-59-1
Isophorone
ND
0.18
0.018
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.18
0.018
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.18
0.018
mg/kg
91-20-3
Naphthalene
ND
0.18
0.018
mg/kg
98-95-3
Nitrobenzene
ND
0.18
0.018
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.18
0.018
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.18
0.019
mg/kg
85-01-8
Phenanthrene
ND
0.18
0.018
mg/kg
129-00-0
Pyrene
ND
0.18
0.021
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.18
0.021
mg/kg
CAS No.
Surrogate Recoveries
Run# l
Run# 2
Limits
367-12-4
2-Fluorophenol
64%
40-102%
4165-62-2
Phenol-d5
69%
41-100%
118-79-6
2,4,6-Tribromophenol
72%
42-108%
4165-60-0
Nitrobenzene-d5
63%
40-105%
321-60-8
2-Fluorobiphenyl
65%
43-107%
1718-51-0
Terphenyl-d14
88%
45-119%
0
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 78
SGACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-4
Lab Sample ID: FA47950-4 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP VPH REV 1.1 Percent Solids: 91.7
Project: Residential Property; Concord, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE329034.1) 1 10/12/17 12:03 ALA n/a n/a L:GLE1107
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.9 g 5.0 ml 50.0 ul
Run #2
MA VPH list
CAS No. Compound
Result
C5-C8 Aliphatics (Unadj.)
ND
C9-C12 Aliphatics (Unadj.)
ND
C9-C10 Aromatics (Unadj.)
ND
CAS No. Surrogate Recoveries
Run# 1
615-59-8 2,5-Dibromotoluene
103% b
615-59-8 2,5-Dibromotoluene
106% c
(a) Analysis performed at SGS Accutest, Lafayette,
LA.
(b) Recovery from Aliphatics fraction.
(c) Recovery from Aromatics fraction.
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
RL Units Q
12 mg/kg
12 mg/kg
12 mg/kg
Run# 2 Limits
70-130%
70-130%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
33 of 78
ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-4
Lab Sample ID: FA47950-4 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 91.7
Project: Residential Property; Concord, NC
Page 1 of I
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN020677.D 1 10/16/17 15:37 MRE 10/04/1711:50 OP67067 GNN1022
Run #2
Initial Weight Final Volume
Run #1 19.8 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
C11-C22 Aromatics (Unadj.)
6.57
C9-C18 Aliphatics
ND
C19-06 Aliphatics
ND
CAS No.
Surrogate Recoveries
Run# 1
3386-33-2
1-Chlorooctadecane
62%
580-13-2
2-Bromonaphthalene
90%
84-15-1
o-Terphenyl
81%
321-60-8
2-Fluorobiphenyl
87%
RL
MDL Units Q
11
4.4 mg/kg J
11
2.8 mg/kg
11
2.8 mgAg
Run# 2
Limits
40-140%
40-140%
40-140%
40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of 3
Client Sample ID:
OE-5
Lab Sample ID:
FA47950-5 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8260B Percent Solids: 91.6
Project:
Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0123669.1) 1 09/29/17 18:53 EP n/a n/a VC4896
Run #2
Initial Weight Final Volume
Run #1 5.56 g 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
0.0317
0.049
0.0098 mg/kg JB
71-43-2
Benzene
ND
0.0049
0.0012 mg/kg
108-86-1
Bromobenzene
ND
0.0049
0.00098 mg/kg
74-97-5
Bromochloromethane
ND
0.0049
0.0015 mg/kg
75-27-4
Bromodichloromethane
ND
0.0049
0.00098 mg/kg
75-25-2
Bromoform
ND
0.0049
0.00098 mg/kg
78-93-3
2-Butanone (MEK)
ND
0.025
0.0071 mg/kg
104-51-8
n-Butylbenzene
ND
0.0049
0.00098 mg/kg
135-98-8
sec-Butylbenzene
ND
0.0049
0.00098 mg/kg
98-06-6
ter(-Butylbenzene
ND
0.0049
0.00098 mg/kg
56-23-5
Carbon Tetrachloride
ND
0.0049
0.0010 mg/kg
108-90-7
Chlorobenzene
ND
0.0049
0.00098 mg/kg
75-00-3
Chloroethane
ND
0.0049
0.0020 mg/kg
67-66-3
Chloroform
ND
0.0049
0.0013 mg/kg
95-49-8
o-Chlorotoluene
ND
0.0049
0.00098 mg/kg
106-43-4
p-Chlorotoluene
ND
0.0049
0.00098 mg/kg
124-48-1
Dibromochloromethane
ND
0.0049
0.00098 mg/kg
106-93-4
1,2-Dibromoethane
ND
0.0049
0.00098 mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.0049
0.0020 mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.0049
0.00098 mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.0049
0.00098 mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.0049
0.0011 mg/kg
75-34-3
1,1-Dichloroethane
ND
0.0049
0.0017 mg/kg
107-06-2
1,2-Dichloroethane
ND
0.0049
0.00098 mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.0049
0.00098 mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.0049
0.0014 mg/kg
156-60-5
trans- 1, 2-Dichloroethylene a
ND
0.0049
0.00098 mg/kg
78-87-5
1,2-Dichloropropane
ND
0.0049
0.00098 mg/kg
142-28-9
1,3-Dichloropropane
ND
0.0049
0.00098 mg/kg
594-20-7
2,2-Dichloropropane
ND
0.0049
0.00098 mg/kg
563-58-6
1,1-Dichloropropene
ND
0.0049
0.0010 mg/kg
10061-01-5
cis- 1, 3-Dichloropropene a
ND
0.0049
0.00098 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
--SG� 1 35 of 78
_ ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-5
Lab Sample ID: FA47950-5 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.6
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
Page 2 of 3
CAS No.
Compound
Result
RL
MDL Units Q
10061-02-6
trans- 1, 3-Dichloropropene
ND
0.0049
0.00098 mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.0049
0.0023 mg/kg
64-17-5
Ethyl Alcohol
ND
0.39
0.074 mg/kg
100-41-4
Ethylhenzene
ND
0.0049
0.00098 mg/kg
591-78-6
2-Hexanone
ND
0.025
0.0074 mg/kg
98-82-8
Isopropylbenzene
ND
0.0049
0.00098 mg/kg
99-87-6
p-Isopropyltoluene
ND
0.0049
0.00098 mg/kg
74-83-9
Methyl Bromide
ND
0.0049
0.0020 mg/kg
74-87-3
Methyl Chloride
ND
0.0049
0.0020 mg/kg
75-09-2
Methylene Chloride b
0.0042
0.0098
0.0039 mg/kg JB
108-10-1
4-Methyl-2-pentanone (MIBK)
ND
0.025
0.0074 mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.0049
0.00098 mg/kg
91-20-3
Naphthalene
ND
0.0049
0.0020 mg/kg
103-65-1
n-Propylbenzene
ND
0.0049
0.00098 mg/kg
100-42-5
Styrene
ND
,0.0049
0.00098 mg/kg
630-20-6
1, 1, 1, 2-Tetrachloroethane
ND
0.0049
0.0010 mg/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
0.0049
0.00098 mg/kg
127-18-4
Tetrachloroethylene
ND
0.0049
0.0013 mg/kg
108-88-3
Toluene
ND
0.0049
0.00098 mg/kg
87-61-6
1,2,3-Trichlorobenzene
ND
0.0049
0.0014 mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.0049
0.00098 mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.0049
0.00098 mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.0049
0.00098 mg/kg
79-01-6
Trichloroethylene
ND
0.0049
0.00098 mg/kg
75-69-4
Trichlorofluoromethane
ND
0.0049
0.0020 mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.0049
0.0012 mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.0049
0.00098 mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.0049
0.00098 mg/kg
108-05-4
Vinyl Acetate a
ND
0.025
0.016 mg/kg
75-01-4
Vinyl Chloride
ND
0.0049
0.00098 mg/kg
m,p-Xylene
ND
0.0098
0.0011 mg/kg
95-47-6
o-Xylene
ND
0.0049
0.00098 mg/kg
1330-20-7
Xylene (total)
ND
0.015
0.0021 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
102%
75-124%
17060-07-0
1,2-Dichloroethane-D4
112%
72-135%
2037-26-5
Toluene-D8
88%
75-1269/6
460-00-4
4-Bromofluorobenzene
101%
71-133%
ND = Not detected MDL = Method Detection Limit J
= Indicates an estimated value
RL = Reporting Limit
B
= Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
36 of 78
Ms ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-5
Lab Sample ID: FA47950-5 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8260B Percent Solids: 91.6
Project: Residential Property; Concord, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Suspected laboratory contaminant.
Page 3 of 3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
(�
37 of 78
SG$ ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of 2
Client Sample ID:
OE-5
Lab Sample ID:
FA47950-5 Date Sampled: 09/27/17
Matrix:
SO - Soil Date Received: 09/29/17
Method:
SW846 8270D SW846 3550C Percent Solids: 91.6
Project:
Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X056145.1) 1 10/06/17 14:18 MV 10/04/17 08:22 OP67062 SX2373
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
0.90
0.18
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.18
0.020
mg/kg
95-57-8
2-Chlorophenol
ND
0.18
0.022
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.18
0.021
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.18
0.048
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.90
0.18
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.36
0.072
mg/kg
95-48-7
2-Methylphenol
ND
0.18
0.022
mg/kg
3&4-Methylphenol
ND
0.18
0.030
mg/kg
88-75-5
2-Nitrophenol
ND
0.18
0.019
mg/kg
100-02-7
4-Nitrophenol
ND
0.90
0.18
mgAg
87-86-5
Pentachlorophenol
ND
0.90
0.18
mg/kg
108-95-2
Phenol
ND
0.18
0.018
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.18
0.021
mg/kg
83-32-9
Acenaphthene
ND
0.18
0.019
mg/kg
208-96-8
Acenaphthylene
ND
0.18
0.018
mgAg
120-12-7
Anthracene
ND
0.18
0.020
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.18
0.018
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.18
0.021
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.18
0.020
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.18
0.019
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.18
0.024
mg/kg
100-51-6
Benzyl Alcohol
ND
0.18
0.018
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.18
0.019
mgAg
85-68-7
Butyl benzyl phthalate
ND
0.18
0.036
mg/kg
106-47-8
4-Chloroaniline
ND
0.18
0.045
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.18
0.018
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.18
0.021
mg/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
0.18
0.023
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.18
0.018
mg/kg
7005-72-3
4-Chlorophenol phenyl ether
ND
0.18
0.018
mg/kg
218-01-9
Chrysene
ND
0.18
0.018
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
/^��
38 of 78
SGS' ACCUTEST
FA47950

SGS Accutest
Report of Analysis
Client Sample ID: OE-5
Lab Sample ID: FA47950-5 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: SW846 8270D SW846 3550C Percent Solids: 91.6
Project: Residential Property; Concord, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units
53-70-3
Dibenzo(a,h)andwacene
ND
0.18
0.022
mg/kg
132-64-9
Dibenzofuran
ND
0.18
0.018
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.18
0.018
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.18
0.019
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.18
0.024
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.18
0.043
mg/kg
84-66-2
Diethyl Phthalate
ND
0.36
0.036
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.18
0.036
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.18
0.036
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.36
0.072
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
0.18
0.018
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.36
0.036
mg/kg
206-44-0
Fluoranthene
ND
0.18
0.018
mg/kg
86-73-7
Fluorene
ND
0.18
0.019
mg/kg
118-74-1
Hexachlorobenzene
ND
0.18
0.018
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.18
0.018
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.18
0.036
mg/kg
67-72-1
Hexachloroethane
ND
0.18
0.021
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.18
0.022
mg/kg
78-59-1
Isophorone
ND
0.18
0.018
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.18
0.018
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.18
0.018
mg/kg
91-20-3
Naphthalene
ND
0.18
0.018
mg/kg
98-95-3
Nitrobenzene
ND
0.18
0.018
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.18
0.018
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.18
0.019
mg/kg
85-01-8
Phenanthrene
ND
0.18
0.018
mg/kg
129-00-0
Pyrene
ND
0.18
0.021
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.18
0.021
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
78%
40-1020/6
4165-62-2
Phenol-d5
78%
41-100%
118-79-6
2,4,6-Tribromophenol
85%
42-1080/6
4165-60-0
Nitrobenzene-d5
77%
40-105%
321-60-8
2-Fluorobiphenyl
79%
43-107%
1718-51-0
Terphenyl-dl4
91%
45-119%
X
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SG(� �+ 39 of 78
ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page 1 of 1 t;
Client Sample ID: OE-5
Lab Sample ID: FA47950-5 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP VPH REV 1.1 Percent Solids: 91.6
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a LE328998.1) 1 10/11/17 15:42 ALA n/a n/a L:GLE1105
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.3 g 5.0 ml 50.0 ul
Run #2
MA VPH list
CAS No. Compound
Result
RL
Units Q
C5-C8 Aliphatics (Unadj.)
ND
11
mg/kg
C9-C12 Aliphatics (Unadj.)
3.44
11
mg/kg J
C9-C10 Aromatics (Unadj.)
ND
11
mg/kg
CAS No. Surrogate Recoveries
Run# 1
Run# 2
Limits
615-59-8 2,5-Dibromotoluene
104% b
70-130%
615-59-8 2,5-Dibromotoluene
94% c
70-130%
(a) Analysis performed at SGS Accutest, Lafayette, LA.
(b) Recovery from Aliphatics fraction.
(c) Recovery from Aromatics fraction.
ND = Not detected
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
SS;40 of 78
G ACCUTEST
FA47950

SGS Accutest
Report of Analysis Page I of 1;
Client Sample ID: OE-5 i
Lab Sample ID: FA47950-5 Date Sampled: 09/27/17
Matrix: SO - Soil Date Received: 09/29/17
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 91.6
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN020659.1) 1 10/13/17 18:51 MRE 10/04/1711:50 OP67067 GNN1021
Run #2
Initial Weight Final Volume
Run #1 20.2 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
C11-C22 Aromatics (Unadj.)
ND
C9-C18 Aliphatics
15.0
C19-06 Aliphatics
4.16
CAS No.
Surrogate Recoveries
Run# 1
3386-33-2
1-Chlorooctadecane
67%
580-13-2
2-Bromonaphthalene
93%
84-15-1
o-Terphenyl
74%
321-60-8
2-Fluorobiphenyl
89%
RL
MDL Units Q
11
4.3 mg/kg
11
2.7 mg/kg
11
2.7 mg/kg J
Run# 2
Limits
40-140%
40-140%
40-140%
40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 78
ACCUTEST
FA47950

SGS ACCUTEST
Southeast
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of custody
��
' 42 of 78
SGS, ACCUTEST
FA47950

UVU C Swllwu onee%va Uvaaaaaeaaoa a - a . . • — —
Chain of Custody SGS ACCUTEST JOB# : PAGE OF
ACCUTESTa.DSYm.m.da�a.sahoc.Is o �:ao.Fla:atl
111. 4674zs-GmD FAX: [phone] SGS Accutest Quote # SKIFF #
m.—
Client I Reporting Information I Project Information
Ana tical Information
Matrix Codes
Comps"Name: —
Pro)ect Name: I
Q
'9
0
r-
S
C
7 1
i
DVv - urnking
Water
G W . Ground
Water
SW Sur ace
Wate•
SO. Soil
SL- Sludge
OI-Ofi
LIO - Other Liquid
Alli-Air
lid
Address:
Street
CRY: L ka Stets: fp:
G State0 G
Project Conte Email:
1 Cw
Project#
Phone #:
Fax te
Samplers) Names) (PTlnted)
Sam ler 1: Sampler 2:
Client Purchase Order # t/
— y.Z31-dfJpG 2.
Act nest
Sam le #
Field ID I Point of Collection
COLLECTION
Corn-EReaca
ATbn
LAB USE ONLY
DATE
T.1
�n LEA
w�TRu
Tmu a
OF
ao*n rs
f
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X k
3
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IV06
X
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x k
q
— 4
v
x
.x )L
Turnaround Time Business days)
Data
Deliverable
Information
Comments
I
Remarks
W Day,Busineae) Approved By: I Date:
7 Day
3 Day RUSH
2 Day RUSH
1 Day RUSH
Other
Rush TIA Data Available VIA Email or LaWinN
COMMERCIAL "A" (RESULTS ONLY)
COMMEEE]RE��'R���CIALty,(E"B" (RESIAO 00'Fi } T (�
❑FU'TT 12 tTE'¢4, AEU,`:E'• C%T ( D'`
�EDD'S CL1 NC 282J3
Sample Custody must be
documented below each t e sem
as change —asslon includin
courier
very,
Relinquished ySamplerlA Ilatlon
Date Time:
It ce mllat '
Relin, ylARill
D Tlms:
Recelvad ByfrAftfilellorn
Rolinqulehod bylANlll tlo
5 -e d ['-
Data Time:
Recol IIa11
�NS�
Relinquished BylAf illatlon
7
Date Tlme:
Received BylARllakon
a
Lab Use Only : Cooler Temperature s) Celsius corrected): hill f/n coMsn/iwma�r _on<Iaions
ElfeOve Date C412412017
SGS COC Flo•ida new art 5 2 17 rev C42417 SI
511
FA47950: Chain of Custody
Page 1 of 2
SGS, ACCUTEST
FA47950

SGS Accutest Sample Receipt Summary
Job Number: FA47950 Client: PM ENV. Project: RESIDENTIAL PROPERTY
Date / Time Received: 9/29/2017 9:45:00 AM Delivery Method: FED EX Airbill Ws: 8110 6225 1703
Therm ID: IR 1; Therm CF: -0.2; # of Coolers: 1
Cooler Temps (Raw Measured) °C: Cooler 1: (5.9);
Cooler Temps (Corrected) °C: Cooler 1: (5.7);
NIA
1. Custody Seals Present
©
❑
1. Sample labels present on bottles
©
❑
2. Custody Seals Intact
©
❑
2. Samples preserved properly
©
❑
3. Temp criteria achieved
©
❑
3. Sufficient volume/containers recvd for analysis:
©
❑
4. Cooler temp verification
IR Gun
4. Condition of sample
)!
5. Cooler media
Ice (gaol
5. Sample recvd within HT
©
❑
6. Dates/Times/IDs on COC match Sample Label
©
❑
Trio Blank Information
Y or
N N/A
7. VOCs have headspace
❑
❑
1. Trip Blank present / cooler
❑
0 ❑
8. Bottles received for unspecified tests
❑
91
2. Trip Blank listed on CDC
❑
© ❑
9. Composiling instructions clear
❑
❑
W or
S NIA
10. Voa Soil Kits/Jars received past 48hrs?
El
ElW
11. %Solids Jar received?
©
El
❑
3. Type Of TB Received
❑
❑ P]
12. Residual Chlorine Present?
❑
❑
Sd
Misc. Information
Number of Encores: 25-Gram 5-Gram
Test Strip Lot #s: pH 0-3 230315
Residual Chlorine Test Strip Lot #:
Comments
Number of 5035 Field Kits: 5 Number of Lab Filtered Metals:
pH 10-12 219813A Other: (Specify)
shoot Rev. Date 05/24/17 Technician: SHAYLAP Date: 9/29/2017 9:45:00 AM
Reviewer: SP Date: 9/29/2017
FA47950: Chain of Custody
Page 2 of 2
$��44 of 78
ACCUTEST
FA47950

SGS
ACCUTEST
Southeast
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Section 5
SGS ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VC4896-MB
C0123649.1)
1
09/29/17
EP
n/a
n/a
VC4896
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Result RL
Method: SW846 8260B
MDL Units Q
67-64-1
Acetone
24.0
50
10
ug/kg
71-43-2
Benzene
ND
5.0
1.2
ug/kg
108-86-1
Bromobenzene
ND
5.0
1.0
ug/kg
74-97-5
Bromochloromethane
ND
5.0
1.5
ug/kg
75-27-4
Bromodichloromethane
ND
5.0
1.0
ug/kg
75-25-2
Bromoform
ND
5.0
1.0
ug/kg
78-93-3
2-Butanone (MEK)
ND
25
7.3
ug/kg
104-51-8
n-Butylbenzene
ND
5.0
1.0
ug/kg
135-98-8
sec-Butylbenzene
ND
5.0
1.0
ug/kg
98-06-6
ter[-Butylbenzene
ND
5.0
1.0
ug/kg
56-23-5
Carbon Tetrachloride
ND
5.0
1.0
ug/kg
108-90-7
Chlorobenzene
ND
5.0
1.0
ug/kg
75-00-3
Chloroethane
ND
5.0
2.0
ug/kg
67-66-3
Chloroform
ND
5.0
1.3
ug/kg
95-49-8
o-Chlorotoluene
ND
5.0
1.0
ug/kg
106-43-4
p-Chlorotoluene
ND
5.0
1.0
ug/kg
124-48-1
Dibromochloromethane
ND
5.0
1.0
ug/kg
106-93-4
1,2-Dibromoethane
ND
5.0
1.0
ug/kg
75-71-8
Dichlorodifluoromethane
ND
5.0
2.0
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
5.0
1.0
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
5.0
1.0
ug/kg
106-46-7
1,4-Dichlorobenzene
ND
5.0
1.2
ug/kg
75-34-3
1,1-Dichloroethane
ND
5.0
1.8
ug/kg
107-06-2
1,2-Dichloroethane
ND
5.0
1.0
ug/kg
75-35-4
1,1-Dichloroethylene
ND
5.0
1.0
ug/kg
156-59-2
cis-1,2-Dichloroethylene
ND
5.0
1.4
ug/kg
156-60-5
trans-1,2-Dichloroethylene
ND
5.0
1.0
ug/kg
78-87-5
1,2-Dichloropropane
ND
5.0
1.0
ug/kg
142-28-9
1,3-Dichloropropane
ND
5.0
1.0
ug/kg
594-20-7
2, 2-Dichloropropane
ND
5.0
1.0
ug/kg
563-58-6
1, 1 -Dichloropropene
ND
5.0
1.0
ug/kg
10061-01-5 cis-1,3-Dichloropropene
ND
5.0
1.0
ug/kg
10061-02-6 trans-1,3-Dichloropropene
ND
5.0
1.0
ug/kg
108-20-3
Di -Isopropyl Ether
ND
5.0
2.3
ug/kg
64-17-5
Ethyl Alcohol
ND
400
75
ug/kg
100-41-4
Ethylbenzene
ND
5.0
1.0
ug/kg
SGS ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 2 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VC4896-MB
C0123649.1)
1
09/29/17
EP
n/a
n/a
VC4896
The C reported here applies to the following samples: Method: SW846 8260B
Q P PP g P
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Result RL MDL Units Q
591-78-6
2-Hexanone
ND
25
7.5
ug/kg
98-82-8
Isopropylbenzene
ND
5.0
1.0
ug/kg
99-87-6
p-Isopropyltoluene
ND
5.0
1.0
ug/kg
74-83-9
Methyl Bromide
ND
5.0
2.0
ug/kg
74-87-3
Methyl Chloride
ND
5.0
2.0
ug/kg
75-09-2
Methylene Chloride
5.6
10
4.0
ug/kg J
108-10-1
4-Methyl-2-pentanone (MIBK) ND
25
7.5
ug/kg
1634-04-4
Methyl Ter( Butyl Ether
ND
5.0
1.0
ug/kg
91-20-3
Naphthalene
ND
5.0
2.0
ug/kg
103-65-1
n-Propylbenzene
ND
5.0
1.0
ug/kg
100-42-5
Styrene
ND
5.0
1.0
ug/kg
630-20-6
1, 1, 1, 2-Tetrachloroethane
ND
5.0
1.0
ug/kg
79-34-5
1, 1, 2,2-Tetrachloroethane
ND
5.0
1.0
ug/kg
127-18-4
Tetrachloroethylene
ND
5.0
1.3
ug/kg
108-88-3
Toluene
2.5
5.0
1.0
ug/kg J
87-61-6
1,2,3-Trichlorobenzene
ND
5.0
1.4
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
1.0
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
5.0
1.0
ug/kg
79-00-5
1, 1, 2-Trichloroethane
ND
5.0
1.0
ug/kg
79-01-6
Trichloroethylene
ND
5.0
1.0
ug/kg
75-69-4
Trichlorofluoromethane
ND
5.0
2.0
ug/kg
96-18-4
1,2,3-Trichloropropane
ND
5.0
1.3
ug/kg
95-63-6
1,2,4-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-67-8
1,3,5-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-05-4
Vinyl Acetate
ND
25
16
ug/kg
75-01-4
Vinyl Chloride
ND
5.0
1.0
ug/kg
m,p-Xylene
ND
10
1.1
ug/kg
95-47-6
o-Xylene
ND
5.0
1.0
ug/kg
1330-20-7
Xylene (total)
ND
15
2.1
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
102%
75-124%
17060-07-0
1,2-Dichloroethane-D4
105%
72-135%
2037-26-5
Toluene-D8
92%
75-126%
47 of 78
SGS, ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 3 of 3
sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
rC4896-MB
C0123649.D
1
09/29/17
EP
n/a
n/a
VC4896
The C reported here applies to the following samples: Method: SW846 8260B
Q P PP g P
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Surrogate Recoveries
Limits
460-00-4 4-Bromofluorobenzene 96% 71-133%
car
SG�+ �+ 48 of 78
ACCUTEST
FA47950

Blank Spike Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VC4896-BS
C0123650.D
1
09/29/17
EP
n/a
n/a
VC4896
The QC reported here applies to the following samples: Method: SW846 8260B
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Spike BSP BSP
ug/kg ug/kg % Limits
67-64-1
Acetone
250
322
129
61-152
71-43-2
Benzene
50
55.4
111
76-126
108-86-1
Bromobenzene
50
53.3
107
76-122
74-97-5
Bromochloromethane
50
53.2
106
77-120
75-27-4
Bromodichloromethane
50
58.5
117
74-130
75-25-2
Bromoform
50
56.0
112
76-127
78-93-3
2-Butanone (MEK)
250
281
112
75-137
104-51-8
n-Butylbenzene
50
53.8
108
71-128
135-98-8
sec-Butylbenzene
50
53.5
107
79-135
98-06-6
tert-Butylbenzene
50
50.9
102
77-133
56-23-5
Carbon Tetrachloride
50
56.0
112
78-133
108-90-7
Chlorobenzene
50
54.9
110
81-129
75-00-3
Chloroethane
50
65.9
132
68-133
67-66-3
Chloroform
50
55.5
111
72-123
95-49-8
o-Chlorotoluene
50
53.7
107
77-129
106-43-4
p-Chlorotoluene
50
54.2
108
80-134
124-48-1
Dibromochloromethane
50
57.6
115
76-127
106-93-4
1,2-Dibromoethane
50
56.6
113
77-126
75-71-8
Dichlorodifluoromethane
50
53.2
106
68-168
95-50-1
1,2-Dichlorobenzene
50
54.9
110
80-129
541-73-1
1,3-Dichlorobenzene
50
56.9
114
81-129
106-46-7
1,4-Dichlorobenzene
50
56.0
112
76-130
75-34-3
1,1-Dichloroethane
50
58.8
118
73-125
107-06-2
1,2-Dichloroethane
50
58.5
117
74-128
75-35-4
1, 1 -Dichloroethylene
50
56.9
114
81-136
156-59-2
cis-1,2-Dichloroethylene
50
53.8
108
74-126
156-60-5
trans-1,2-Dichloroethylene
50
61.0
122
70-127
78-87-5
1,2-Dichloropropane
50
55.3
111
74-125
142-28-9
1,3-Dichloropropane
50
52.8
106
76-122
594-20-7
2,2-Dichloropropane
50
54.5
109
77-133
563-58-6
1,1-Dichloropropene
50
53.2
106
75-130
10061-01-5 cis-1,3-Dichloropropene
50
60.0
120
80-123
10061-02-6 trans-1,3-Dichloropropene
50
51.0
102
75-131
108-20-3
Di -Isopropyl Ether
50
56.7
113
75-122
64-17-5
Ethyl Alcohol
1000
852
85
53-154
100-41-4
Ethylbenzene
50
53.6
107
77-123
* = Outside of Control Limits.
SGS ACCUTEST
FA47950

Blank Spike Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 2 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VC4896-BS
C0123650.D
1
09/29/17
EP
n/a
n/a
VC4896
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
591-78-6
2-Hexanone
250
267
107
72-133
98-82-8
Isopropylbenzene
50
54.8
110
80-136
99-87-6
p-Isopropyltoluene
50
54.9
110
77-131
74-83-9
Methyl Bromide
50
52.5
105
65-139
74-87-3
Methyl Chloride
50
53.1
106
71-144
75-09-2
Methylene Chloride
50
60.0
120
74-137
108-10-1
4-Methyl-2-pentanone (MIBK) 250
271
108
76-132
1634-04-4
Methyl Tert Butyl Ether
50
56.4
113
77-120
91-20-3
Naphthalene
50
54.8
110
79-129
103-65-1
n-Propylbenzene
50
52.8
106
80-135
100-42-5
Styrene
50
56.8
114
78-125
630-20-6
1, 1, 1, 2-Tetrachloroethane
50
57.8
116
78-126
79-34-5
1,1,2,2-Tetrachloroethane
50
51.0
102
71-126
127-18-4
Tetrachloroethylene
50
56.0
112
79-130
108-88-3
Toluene
50
49.4
99
76-124
87-61-6
1,2,3-Trichlorobenzene
50
53.4
107
77-128
120-82-1
1,2,4-Trichlorobenzene
50
55.6
111
78-130
71-55-6
1, 1, 1 -Trichloroethane
50
52.4
105
70-129
79-00-5
1, 1, 2-Trichloroethane
50
54.8
110
74-124
79-01-6
Trichloroethylene
50
56.0
112
75-128
75-69-4
Trichlorofluoromethane
50
58.9
118
73-145
96-18-4
1,2,3-Trichloropropane
50
53.0
106
74-127
95-63-6
1,2,4-Trimethylbenzene
50
54.0
108
74-123
108-67-8
1,3,5-Trimethylbenzene
50
52.8
106
73-122
108-05-4
Vinyl Acetate
250
328
131
48-164
75-01-4
Vinyl Chloride
50
51.9
104
76-141
m,p-Xylene
100
108
108
80-128
95-47-6
o-Xylene
50
55.3
111
80-132
1330-20-7
Xylene (total)
150
163
109
80-129
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
100%
75-124%
17060-07-0
1,2-Dichloroethane-D4
99%
72-135%
2037-26-5
Toluene-D8
94%
75-126%
* = Outside of Control Limits.
Method: SW846 8260B
P
is
50 of 78
SG S ACCUTEST
FA47950

Blank Spike Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 3 of 3
;ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
IC4896-BS
C0123650.D
1
09/29/17
EP
n/a
n/a
VC4896
The QC reported here applies to the following samples: Method: SW846 8260B
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 97% 71-133%
* = Outside of Control Limits.
� 51 of 78
SGa? ACCUTEST
FA47950

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA47921-3MS
C0123661.1)
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3MSD
C0123662.1)
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3 a
C0123653.1)
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3 b
C0123660.1)
1
09/29/17
EP
n/a
n/a
VC4896
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
FA47921-3 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
67-64-1
Acetone
ND c
13600
15500
114
13600
15600
114
1
61-152/27
71-43-2
Benzene
ND c
2730
2460
90
2730
2520
92
2
76-126/26
108-86-1
Bromobenzene
ND c
2730
2550
93
2730
2700
99
6
76-122/32
74-97-5
Bromochloromethane
ND c
2730
2570
94
2730
2650
97
3
77-120/24
75-27-4
Bromodichloromethane
ND c
2730
2690
99
2730
2820
103
5
74-130/25
75-25-2
Bromoform
ND c
2730
2530
93
2730
2610
96
3
76-127/26
78-93-3
2-Butanone (MEK)
ND c
13600
15000
110
13600
15300
112
2
75-137/25
104-51-8
n-Butylbenzene
277c
2730
2770
91
2730
2840
94
2
71-128/35
135-98-8
sec-Butylbenzene
312 c
2730
2820
92
2730
3040
100
8
79-135/34
98-06-6
'ter(-Butylbenzene
ND c
2730
2550
93
2730
2710
99
6
77-133/34
56-23-5
Carbon Tetrachloride
ND c
2730
2260
83
2730
2400
88
6
78-133/29
108-90-7
Chlorobenzene
ND c
2730
2630
96
2730
2710
99
3
81-129/29
75-00-3
Chloroethane
ND c
2730
1740
64*
2730
1750
64*
1
68-133/29
67-66-3
Chloroform
ND c
2730
2530
93
2730
2630
96
4
72-123/26
95-49-8
o-Chlorotoluene
ND c
2730
3330
122
2730
3580
131*
7
77-129/33
106-43-4
p-Chlorotoluene
ND c
2730
2700
99
2730
2920
107
8
80-134/33
124-48-1
Dibromochloromethane
ND c
2730
2700
99
2730
2810
103
4
76-127/27
106-93-4
1,2-Dibromoethane
ND c
2730
2850
104
2730
2930
107
3
77-126/26
75-71-8
Dichlorodifluoromethane
ND c
2730
2050
75
2730
2110
77
3
68-168/29
95-50-1
1,2-Dichlorobenzene
ND c
2730
2710
99
2730
2800
103
3
80-129/32
541-73-1
1,3-Dichlorobenzene
ND c
2730
2760
101
2730
2900
106
5
81-129/33
106-46-7
1,4-Dichlorobenzene
ND c
2730
2760
101
2730
2860
105
4
76-130/32
75-34-3
1,1-Dichloroethane
111 c
J 2730
2690
95
2730
2770
97
3
73-125/27
107-06-2
1,2-Dichloroethane
ND c
2730
2820
103
2730
2880
106
2
74-128/23
75-35-4
1,1-Dichloroethylene
ND c
2730
2420
89
2730
2530
93
4
81-136/28
156-59-2
cis- 1, 2-Dichloroethylene
218 c
J 2730
2670
90
2730
2740
92
3
74-126/26
156-60-5
trans-1,2-Dichloroethylene
ND c
2730
2710
99
2730
2790
102
3
70-127/27
78-87-5
1,2-Dichloropropane
ND c
2730
2700
99
2730
2820
103
4
74-125/25
142-28-9
1,3-Dichloropropane
ND c
2730
2800
103
2730
2900
106
4
76-122/26
594-20-7
2,2-Dichloropropane
ND c
2730
2120
78
2730
2190
80
3
77-133/28
563-58-6
1,1-Dichloropropene
ND c
2730
2500
92
2730
2570
94
3
75-130/28
10061-01-5 cis- 1, 3-Dichloropropene
ND c
2730
3030
111
2730
3210
118
6
80-123/26
10061-02-6 trans- 1, 3-Dichloropropene
ND c
2730
2500
92
2730
2670
98
7
75-131/28
108-20-3
Di -Isopropyl Ether
ND c
2730
2810
103
2730
2910
107
3
75-122/25
64-17-5
Ethyl Alcohol
ND c
54600
47800
88
54600
48300
88
1
53-154/42
100-41-4
Ethylbenzene
ND c
2730
2480
91
2730
2560
94
3
77-123/31
* = Outside of Control Limits.
GS ACCUTEST
FA47950

Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA47921-3MS
C0123661.1)
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3MSD
C0123662.1)
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3 a
C0123653.1)
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3 b
C0123660.1)
1
09/29/17
EP
n/a
n/a
VC4896
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
FA47921-3 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
591-78-6
2-Hexanone
ND c
13600
14000
103
13600
14200
104
1
72-133/26
98-82-8
Isopropylbenzene
1690 c
2730
3990
84
2730
4080
88
2
80-136/32
99-87-6
p-Isopropyltoluene
167c
J
2730
2730
94
2730
2870
99
5
77-131/34
74-83-9
Methyl Bromide
ND c
2730
2280
84
2730
2190
80
4
65-139/31
74-87-3
Methyl Chloride
ND c
2730
2360
86
2730
2450
90
4
71-144/27
75-09-2
Methylene Chloride
236 c
JB
2730
2890
97
2730
2990
101
3
74-137/28
108-10-1
4-Methyl-2-pentanone (MIBK)
ND c
13600
13900
102
13600
14100
103
1
76-132/26
1634-04-4
Methyl Teri Butyl Ether
ND c
2730
2790
102
2730
2830
104
1
77-120/24
91-20-3
Naphthalene
286 c
2730
2650
87
2730
2840
94
7
79-129/33
103-65-1
n-Propylbenzene
5080c
2730
6330
46*
2730
6770
62*
7
80-135/33
100-42-5
Styrene
ND c
2730
2610
96
2730
2670
98
2
78-125/30
630-20-6
1,1,1,2-Tetiachloroethane
ND c
2730
2550
93
2730
2620
96
3
78-126/27
79-34-5
1,1,2,2-Tetachloroethane
ND c
2730
2560
94
2730
2690
99
5
71-126/30
127-18-4
Tetrachloroethylene
5210 c
2730
7650
89
2730
8100
106
6
79-130/31
108-88-3
Toluene
ND c
2730
2280
84
2730
2380
87
4
76-124/30
87-61-6
1,2,3-Trichlorobenzene
ND c
2730
2260
83
2730
2460
90
8
77-128/35
120-82-1
1,2,4-Trichlorobenzene
ND c
2730
2470
91
2730
2660
97
7
78-130/34
71-55-6
1,1,1-Trichloroethane
237 c
J
2730
2500
83
2730
2560
85
2
70-129/27
79-00-5
1,1,2-Trichloroethane
ND c
2730
3250
119
2730
3250
119
0
74-124/28
79-01-6
Trichloroethylene
1250 c
2730
3810
94
2730
3940
99
3
75-128/27
75-69-4
Trichlorofluoromethane
ND c
2730
965
35*
2730
995
36*
3
73-145/31
96-18-4
1,2,3-Trichloropropane
ND c
2730
2680
98
2730
2910
107
8
74-127/27
95-63-6
1,2,4-Trimethylbenzene
7390 c
2730
8220
30* d
2730
8810
52* d
7
74-123/34
108-67-8
1,3,5-Trimethylbenzene
6220c
2730
7350
41* d
2730
7950
63* d
8
73-122/33
108-05-4
Vinyl Acetate
ND c
13600
14900
109
13600
15200
111
2
48-164/37
75-01-4
Vinyl Chloride
ND c
2730
2370
87
2730
2490
91
5
76-141/27
m,p-Xylene
272c
J
5460
5300
92
5460
5480
95
3
80-128/30
95-47-6
o-Xylene
243c
J
2730
2880
97
2730
2950
99
2
80-132/30
1330-20-7
Xylene (total)
515 c
J
8190
8180
94
8190
8430
97
3
80-129/30
CAS No.
Surrogate Recoveries
MS
MSD
FA47921-3
FA47921-3
Limits
1868-53-7
Dibromofluoromethane
95%
95%
107%
101%
75-124%
17060-07-0
1,2-Dichloroethane-D4
95%
96%
123%
105%
72-135%
2037-26-5
Toluene-D8
96%
98%
117%
95%
75-126%
* = Outside of Control Limits.
c((%53 of 78
O-u _ ACCUTEST
FA47950

Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA47921-3MS
C0123661.D
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3MSD
C0123662.D
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3 a
C0123653.D
1
09/29/17
EP
n/a
n/a
VC4896
FA47921-3 b
C0123660.D
1
09/29/17
EP
n/a
n/a
VC4896
The QC reported here applies to the following samples: Method: SW846 8260B
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Surrogate Recoveries MS MSD FA47921-3 FA47921-3 Limits
460-00-4 4-Bromofluorobenzene 101% 105% 137%* a 102% 71-133%
(a) Confirmation run for surrogate recoveries.
(b) Dilution required due to matrix interference (internal standard failure).
(c) Result is from Run #2.
(d) Outside control limits due to high level in sample relative to spike amount.
(e) Outside control limits due to matrix interference.
* = Outside of Control Limits.
54 of 78
S-G ACCUTEST
FA47950

ACCUTEST
Southeast
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Section 6
(�
55 of 78
c
sZG$- ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-MB
X056092.1)
1
10/05/17
MV
10/04/17
OP67062
SX2372
The QC reported here applies to the following samples: Method: SW846 8270D
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
830
170
ug/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
170
19
ug/kg
95-57-8
2-Chlorophenol
ND
170
20
ug/kg
120-83-2
2,4-Dichlorophenol
ND
170
19
ug/kg
105-67-9
2,4-Dimethylphenol
ND
170
44
ug/kg
51-28-5
2,4-Dinitrophenol
ND
830
170
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
330
67
ug/kg
95-48-7
2-Methylphenol
ND
170
20
ug/kg
3&4-Methylphenol
ND
170
27
ug/kg
88-75-5
2-Nitrophenol
ND
170
18
ug/kg
100-02-7
4-Nitrophenol
ND
830
170
ug/kg
87-86-5
Pentachlorophenol
ND
830
170
ug/kg
108-95-2
Phenol
ND
170
17
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
170
19
ug/kg
83-32-9
Acenaphthene
ND
170
18
ug/kg
208-96-8
Acenaphthylene
ND
170
17
ug/kg
120-12-7
Anthracene
ND
170
19
ug/kg
56-55-3
Benzo(a)anthracene
ND
170
17
ug/kg
50-32-8
Benzo(a)pyrene
ND
170
20
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
170
18
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
170
17
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
170
22
ug/kg
100-51-6
Benzyl Alcohol
ND
170
17
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
170
17
ug/kg
85-68-7
Butyl benzyl phthalate
ND
170
33
ug/kg
106-47-8
4-Chloroaniline
ND
170
42
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
170
17
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
170
19
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
170
21
ug/kg
91-58-7
2-Chloronaphthalene
ND
170
17
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
170
17
ug/kg
218-01-9
Chrysene
ND
170
17
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
170
21
ug/kg
132-64-9
Dibenzofuran
ND
170
17
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
170
17
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
170
18
ug/kg
G 56 of 78
ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-MB
X056092.1)
1
10/05/17
MV
10/04/17
OP67062
SX2372
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Result RL
Method: SW846 8270D
MDL Units Q
106-46-7
1,4-Dichlorobenzene
ND
170
22
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
170
40
ug/kg
84-66-2
Diethyl Phthalate
ND
330
33
ug/kg
131-11-3
Dimethyl Phthalate
ND
170
33
ug/kg
117-84-0
Di-n-oclyl Phthalate
ND
170
33
ug/kg
84-74-2
Di-n-butyl Phthalate
ND
330
67
ug/kg
122-66-7
1,2-Diphenylhydrazine
ND
170
17
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
330
33
ug/kg
206-44-0
Fluoranthene
ND
170
17
ug/kg
86-73-7
Fluorene,
ND
170
18
ug/kg
118-74-1
Hexachlorobenzene
ND
170
17
ug/kg
87-68-3
Hexachlorobutadiene
ND
170
17
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
170
33
ug/kg
67-72-1
Hexachloroethane
ND
170
20
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
170
20
ug/kg
78-59-1
Isophorone
ND
170
17
ug/kg
90-12-0
1-Methylnaphthalene
ND
170
17
ug/kg
91-57-6
2-Methylnaphthalene
ND
170
17
ug/kg
91-20-3
Naphthalene
ND
170
17
ug/kg
98-95-3
Nitrobenzene
ND
170
17
ug/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
170
17
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
170
18
ug/kg
85-01-8
Phenanthrene
ND
170
17
ug/kg
129-00-0
Pyrene
ND
170
19
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
170
20
ug/kg
CAS No. Surrogate Recoveries Limits
367-12-4
2-Fluorophenol
73%
40-102%
4165-62-2
Phenol-d5
73%
41-100%
118-79-6
2,4,6-Tribromophenol
76%
42-108%
4165-60-0
Nitrobenzene-d5
72%
40-105%
321-60-8
2-Fluorobiphenyl
73%
43-107%
1718-51-0
Terphenyl-d14
83%
45-119%
GS ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-MB
X056134.D
1
10/06/17
MV
10/04/17
OP67062
SX2373
The QC reported here applies to the following samples: Method: SW846 8270D
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
830
170
ug/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
170
19
ug/kg
95-57-8
2-Chlorophenol
ND
170
20
ug/kg
120-83-2
2,4-Dichlorophenol
ND
170
19
ug/kg
105-67-9
2,4-Dimethylphenol
ND
170
44
ug/kg
51-28-5
2,4-Dinitrophenol
ND
830
170
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
330
67
ug/kg
95-48-7
2-Methylphenol
ND
170
20
ug/kg
3&4-Methylphenol
ND
170
27
ug/kg
88-75-5
2-Nitrophenol
ND
170
18
ug/kg
100-02-7
4-Nitrophenol
ND
830
170
ug/kg
87-86-5
Pentachlorophenol
ND
830
170
ug/kg
108-95-2
Phenol
ND
170
17
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
170
19
ug/kg
83-32-9
Acenaphthene
ND
170
18
ug/kg
208-96-8
Acenaphthylene
ND
170
17
ug/kg
120-12-7
Anthracene
ND
170
19
ug/kg
56-55-3
Benzo(a)anthracene
ND
170
17
ug/kg
50-32-8
Benzo(a)pyrene
ND
170
20
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
170
18
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
170
17
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
170
22
ug/kg
100-51-6
Benzyl Alcohol
ND
170
17
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
170
17
ug/kg
85-68-7
Butyl benzyl phthalate
ND
170
33
ug/kg
106-47-8
4-Chloroaniltne
ND
170
42
ug/kg
111-91-1
bis(2-Chloroetboxy)methane
ND
170
17
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
170
19
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
170
21
ug/kg
91-58-7
2-Chloronaphthalene
ND
170
17
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
170
17
ug/kg
218-01-9
Chrysene
ND
170
17
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
170
21
ug/kg
132-64-9
Dibenzofuran
ND
170
17
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
170
17
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
170
18
ug/kg
S ACCUof 78
TEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-MB
X056134.1)
1
10/06/17
MV
10/04/17
OP67062
SX2373
The QC reported here applies to the following samples: Method: SW846 8270D
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Result RL MDL Units Q
106-46-7
1,4-Dichlorobenzene
ND
170
22
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
170
40
ug/kg
84-66-2
Diethyl Phthalate
ND
330
33
ug/kg
131-11-3
Dimethyl Phthalate
ND
170
33
ug/kg
117-84-0
Di-n-octyl Phthalate
ND
170
33
ug/kg
84-74-2
Di-n-butyl Phthalate
ND
330
67
ug/kg
122-66-7
1,2-Diphenylhydrazine
ND
170
17
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
330
33
ug/kg
206-44-0
Fluoranthene
ND
170
17
ug/kg
86-73-7
Fluorene
ND
170
18
ug/kg
118-74-1
Hexachlorobenzene
ND
170
17
ug/kg
87-68-3
Hexachlorobutadiene
ND
170
17
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
170
33
ug/kg
67-72-1
Hexachloroethane
ND
170
20
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
170
20
ug/kg
78-59-1
Isophorone
ND
170
17
ug/kg
90-12-0
1-Metbylnaphthalene
ND
170
17
ug/kg
91-57-6
2-Methylnaphthalene
ND
170
17
ug/kg
91-20-3
Naphthalene
ND
170
17
ug/kg
98-95-3
Nitrobenzene
ND
170
17
ug/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
170
17
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
170
18
ug/kg
85-01-8
Phenanthrene
ND
170
17
ug/kg
129-00-0
Pyrene
ND
170
19
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
170
20
ug/kg
CAS No. Surrogate Recoveries Limits
367-12-4
2-Fluorophenol
56%
40-102%
4165-62-2
Phenol-d5
57%
41-100%
118-79-6
2,4,6-Tribromophenol
61%
42-108%
4165-60-0
Nitrobenzene-d5
57%
40-105%
321-60-8
2-Fluorobiphenyl
57%
43-107%
1718-51-0
Terphenyl-d14
63%
45-119%
59 of 78
SGS ACCUTEST
FA47950

Blank Spike Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-BS
X056091.D
1
10/05/17
MV
10/04/17
OP67062
SX2372
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
65-85-0
Benzoic Acid
3330
3090
93
36-118
59-50-7
4-Chloro-3-methyl Phenol
1670
1450
87
52-108
95-57-8
2-Chlorophenol
1670
1410
85
48-104
120-83-2
2,4-Dichlorophenol
1670
1440
86
51-105
105-67-9
2,4-Dimethylphenol
1670
1290
77
43-96
51-28-5
2,4-DInitrophenol
3330
2680
80
40-119
534-52-1
4,6-Dinitro-o-cresol
3330
3170
95
64-121
95-48-7
2-Methylphenol
1670
1360
82
46-107
3&4-Methylphenol
3330
2840
85
44-111
88-75-5
2-Nitrophenol
1670
1410
85
49-104
100-02-7
4-Nitrophenol
3330
3080
92
56-116
87-86-5
Pentachlorophenol
3330
3350
101
61-114
108-95-2
Phenol
1670
1410
85
45-110
88-06-2
2,4,6-Trichlorophenol
1670
1530
92
56-109
83-32-9
Acenaphthene
1670
1450
87
56-109
208-96-8
Acenaphthylene
1670
1540
92
56-106
120-12-7
Anthracene
1670
1470
88
61-110
56-55-3
Benzo(a)anthracene
1670
1540
92
66-111
50-32-8
Benzo(a)pyrene
1670
1570
94
59-104
205-99-2
Benzo(b)fluoranthene
1670
1590
95
67-113
191-24-2
Benzo(g,h,i)perylene
1670
1580
95
67-113
207-08-9
Benzo(k)fluoranthene
1670
1580
95
67-114
100-51-6
Benzyl Alcohol
1670
1440
86
53-108
101-55-3
4-Bromophenyl phenyl ether
1670
1510
91
62-110
85-68-7
Butyl benzyl phthalate
1670
1550
93
65-113
106-47-8
4-Chloroaniline
1670
1500
90
30-115
111-91-1
bis(2-Chloroethoxy)methane
1670
1250
75
48-105
111-44-4
bis(2-Chloroethyl)ether
1670
1330
80
46-103
108-60-1
bis(2-Chloroisopropyl)ether
1670
1310
79
40-110
91-58-7
2-Chloronaphthalene
1670
1450
87
53-106
7005-72-3
4-Chlorophenyl phenyl ether
1670
1480
89
58-106
218-01-9
Chrysene
1670
1530
92
65-112
53-70-3
Dibenzo(a,h)andwacene
1670
1630
98
68-115
132-64-9
Dibenzofuran
1670
1500
90
57-108
95-50-1
1,2-Dichlorobenzene
1670
1330
80
44-102
541-73-1
1,3-Dichlorobenzene
1670
1290
77
42-100
* = Outside of Control Limits.
Method: SW846 8270D
SGS ACCUTEST
FA47950

Blank Spike Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-BS
X056091.D
1
10/05/17
MV
10/04/17
OP67062
SX2372
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound
Spike BSP BSP
ug/kg ug/kg % Limits
106-46-7
1,4-Dichlorobenzene
1670
1310
79
40-106
91-94-1
3,3'-Dichlorobenzidine
1670
1680
101
36-114
84-66-2
Diethyl Phthalate
1670
1540
92
61-109
131-11-3
Dimethyl Phthalate
1670
1490
89
59-108
117-84-0
Di-n-octyl Phthalate
1670
1630
98
64-119
84-74-2
Di-n-butyl Phthalate
1670
1550
93
63-108
122-66-7
1,2-Diphenylhydrazine
1670
1490
89
58-112
117-81-7
bis(2-Ethylhexyl)phthalate
1670
1590
95
64-115
206-44-0
Fluoranthene
1670
1530
92
60-108
86-73-7
Fluorene
1670
1520
91
58-109
118-74-1
Hexachlorobenzene
1670
1540
92
59-111
87-68-3
Hexachlorobutadiene
1670
1220
73
41-108
77-47-4
Hexachlorocyclopentadiene
1670
1390
83
49-110
67-72-1
Hexachloroethane
1670
1310
79
40-105
193-39-5
Indeno(1,2,3-cd)pyrene
1670
1720
103
66-116
78-59-1
Isophorone
1670
1410
85
42-89
90-12-0
1-Metbylnaphthalene
1670
1380
83
49-106
91-57-6
2-Methylnaphthalene
1670
1390
83
47-106
91-20-3
Naphthalene
1670
1360
82
44-104
98-95-3
Nitrobenzene
1670
1370
82
43-108
621-64-7
N-Nitrosodi-n-propylamine
1670
1390
83
48-108
86-30-6
N-Nitrosodiphenylamine
1670
1550
93
62-110
85-01-8
Phenanthrene
1670
1510
91
63-111
129-00-0
Pyrene
1670
1550
93
65-115
120-82-1
1,2,4-Trichlorobenzene
1670
1360
82
45-100
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
83%
40-102%
4165-62-2
Phenol-d5
84%
41-100%
118-79-6
2,4,6-Tribromophenol
93%
42-108%
4165-60-0
Nitrobenzene-d5
81%
40-105%
321-60-8
2-Fluorobiphenyl
85%
43-107%
1718-51-0
Terphenyl-d14
94%
45-119%
* = Outside of Control Limits.
Method: SW846 8270D
a)
N
a
61 of 78
ACCUTEST
FA47950

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-MS
X056095.D
1
10/05/17
MV
10/04/17
OP67062
SX2372
OP67062-MSD
X056096.D
1
10/05/17
MV
10/04/17
OP67062
SX2372
FA47967-2
X056094.1)
1
10/05/17
MV
10/04/17
OP67062
SX2372
The QC reported here applies to the following samples: Method: SW846 8270D
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
FA47967-2
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
65-85-0
Benzoic Acid
ND
3940
3480
88
3910
3780
97
8
36-118/41
59-50-7
4-Chloro-3-methyl Phenol
ND
1970
1630
83
1950
1700
87
4
52-108/21
95-57-8
2-Chlorophenol
ND
1970
1370
69
1950
1470
75
7
48-104/26
120-83-2
2,4-Dichlorophenol
ND
1970
1510
77
1950
1600
82
6
51-105/27
105-67-9
2,4-Dimethylphenol
ND
1970
1370
69
1950
1430
73
4
43-96/23
51-28-5
2,4-Dinitrophenol
ND
3940
3500
89
3910
3600
92
3
40-119/32
534-52-1
4,6-Dinitro-o-cresol
ND
3940
3800
96
3910
3940
101
4
64-121/29
95-48-7
2-Methylphenol
ND
1970
1380
70
1950
1460
75
6
46-107/24
3&4-Methylphenol
ND
3940
2900
74
3910
3050
78
5
44-111/24
88-75-5
2-Nitrophenol
ND
1970
-1420
72
1950
1520
78
7
49-104/27
100-02-7
4-Nitrophenol
NO
3940
3730
95
3910
3840
98
3
56-116/23
87-86-5
Pentachlorophenol
ND
3940
3940
100
3910
4130
106
5
61-114/23
108-95-2
Phenol
ND
1970
1390
70
1950
1480
76
6
45-110/24
88-06-2
2,4,6-T'richlorophenol
ND
1970
1710
87
1950
1720
88
1
56-109/25
83-32-9
Acenaphthene
ND
1970
1570
80
1950
1640
84
4
56-109/23
208-96-8
Acenaphthylene
ND
1970
1660
84
1950
1710
88
3
56-106/23
120-12-7
Anthracene
ND
1970
1630
83
1950
1710
88
5
61-110/21
56-55-3
Benzo(a)anthracene
ND
1970
1700
86
1950
1770
91
4
66-111/23
50-32-8
Benzo(a)pyrene
ND
1970
1710
87
1950
1770
91
3
59-104/23
205-99-2
Benzo(b)fluoranthene
ND
1970
1820
92
1950
1870
96
3
67-113/24
191-24-2
Benzo(g,h,i)perylene
ND
1970
1710
87
1950
1810
93
6
67-113/21
207-08-9
Benzo(k)fluoranthene
ND
1970
1670
85
1950
1750
90
5
67-114/22
100-51-6
Benzyl Alcohol
ND
1970
1480
75
1950
1550
79
5
53-108/24
101-55-3
4-Bromophenyl phenyl ether
ND
1970
1660
84
1950
1730
89
4
62-110/21
85-68-7
Butyl benzyl phthalate
ND
1970
1730
88
1950
1800
92
4
65-113/20
106-47-8
4-Chloroaniline
ND
1970
1570
80
1950
1600
82
2
30-115/30
111-91-1
bis(2-Chloroethoxy)methane
ND
1970
1260
64
1950
1340
69
6
48-105/24
111-44-4
bis(2-Chloroethyl)ether
ND
1970
1300
66
1950
1380
71
6
46-103/27
108-60-1
bis(2-Chloroisopropyl)ether
ND
1970
1260
64
1950
1350
69
7
40-110/25
91-58-7
2-Chloronaphthalene
ND
1970
1550
79
1950
1580
81
2
53-106/23
7005-72-3
4-Chlorophenyl phenyl ether
ND
1970
1610
82
1950
1670
86
4
58-106/21
218-01-9
Chrysene
ND
1970
1680
85
1950
1770
91
5
65-112/25
53-70-3
Dibenzo(a,h)anthracene
ND
1970
1770
90
1950
1850
95
4
68-115/23
132-64-9
Dibenzofuran
ND
1970
1720
87
1950
1740
89
1
57-108/22
95-50-1
1,2-Dichlorobenzene
ND
1970
1270
64
1950
1350
69
6
44-102/28
541-73-1
1,3-Dichlorobenzene
ND
1970
1230
62
1950
1300
67
6
42-100/30
* = Outside of Control Limits.
M
w
62 of 78
G ACCUTEST
FA47950

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67062-MS
X056095.1)
1
10/05/17
MV
10/04/17
OP67062
SX2372
OP67062-MSD
X056096.D
1
10/05/17
MV
10/04/17
OP67062
SX2372
FA47967-2
X056094.D
1
10/05/17
MV
10/04/17
OP67062
SX2372
The QC reported here applies to the following samples: Method: SW846 8270D
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
FA47967-2
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
106-46-7
1,4-Dichlorobenzene
ND
1970
1240
63
1950
1300
67
5
40-106/29
91-94-1
3,3'-Dichlorobenzidine
ND
1970
1850
94
1950
1950
100
5
36-114/28
84-66-2
Diethyl Phthalate
ND
1970
1710
87
1950
1770
91
3
61-109/20
131-11-3
Dimethyl Phthalate
ND
1970
1670
85
1950
1700
87
2
59-108/20
117-84-0
Di-n-octyl Phthalate
ND
1970
1860
94
1950
1910
98
3
64-119/21
84-74-2
Di-n-butyl Phthalate
ND
1970
1770
90
1950
1900
97
7
63-108/19
122-66-7
1,2-Diphenylhydrazine
ND
1970
1660
84
1950
1710
88
3
58-112/22
117-81-7
bis(2-Ethylbexyl)phthalate
1210
1970
3920
137*
1950
3760
131*
4
64-115/23
206-44-0
Fluoranthene
ND
1970
1720
87
1950
1800
92
5
60-108/25
86-73-7
Fluorene
ND
1970
1680
85
1950
1730
89
3
58-109/21
118-74-1
Hexachlorobenzene
ND
1970
1690
86
1950
1770
91
5
59-111/21
87-68-3
Hexachlorobutadiene
ND
1970
1180
60
1950
1240
63
5
41-108/27
77-47-4
Hexachlorocyclopentadiene
ND
1970
1390
70
1950
1440
74
4
49-110/31
67-72-1
Hexachloroethane
ND
1970
1210
61
1950
1280
66
6
40-105/32
193-39-5
Indeno(1,2,3-cd)pyrene
ND
1970
1760
89
1950
1880
96
7
66-116/22
78-59-1
Isophorone
ND
1970
1460
74
1950
1530
78
5
42-89/22
90-12-0
1-Methy1naphthalene
ND
1970
1430
73
1950
1520
78
6
49-106/26
91-57-6
2-Methylnaphthalene
ND
1970
1500
76
1950
1570
80
5
47-106/27
91-20-3
Naphthalene
ND
1970
1380
70
1950
1470
75
6
44-104/27
98-95-3
Nitrobenzene
ND
1970
1370
69
1950
1460
75
6
43-108/25
621-64-7
N-Nitrosodi-n-propylamine
ND
1970
1380
70
1950
1450
74
5
48-108/27
86-30-6
N-Nitrosodiphenylamine
ND
1970
1750
89
1950
1800
92
3
62-110/21
85-01-8
Phenanthrene
ND
1970
1680
85
1950
1750
90
4
63-111/22
129-00-0
Pyrene
ND
1970
1660
84
1950
1770
91
6
65-115/25
120-82-1
1,2,4-Trichlorobenzene
ND
1970
1340
68
1950
1420
73
6
45-100/26
CAS No.
Surrogate Recoveries
MS
MSD
FA47967-2
Limits
367-12-4
2-Fluorophenol
71%
76%
74%
40-102%
4165-62-2
Phenol-d5
73%
77%
75%
41-100%
118-79-6
2,4,6-Tribromophenol
92%
96%
83%
42-108%
4165-60-0
Nitrobenzene-d5
73%
77%
75%
40-105%
321-60-8
2-Fluorobiphenyl
80%
81%
77%
43-107%
1718-51-0
Terphenyl-d14
90%
95%
85%
45-119%
* = Outside of Control Limits.
w
w
i
SG aC63 of 78
CUTEST
FA47950

SGS, ACCUTEST
Southeast
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
1�
64 of 78
SGS,' ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
IP67067-MB
NN020652.D
1
10/13/17
MRE
10/04/17
OP67067
GNN1021
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
CAS No. Compound Result RL MDL Units Q
C11-C22 Aromatics (Unadj.) ND 10000 4000 ug/kg
C9-C18 Aliphatics ND 10000 2500 ug/kg
C19-C36 Aliphatics ND 10000 2500 ug/kg
CAS No.
Surrogate Recoveries
Limits
3386-33-2
1-Chlorooctadecane
64%
40-140%
580-13-2
2-Bromonaphthalene
95%
40-140%
84-15-1
o-Terphenyl
76%
40-140%
321-60-8
2-Fluorobiphenyl
92%
40-140%
-_S���/ 65 of 78
__ ACCUTEST
FA47950

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67067-BS
NN020653.1)
1
10/13/17
MRE
10/04/17
OP67067
GNN1021
OP67067-BSD
NN020654.1)
1
10/13/17
MRE
10/04/17
OP67067
GNN1021
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
Spike
BSP
BSP
BSD
BSD
Limits
CAS No. Compound
ug/kg
ug/kg
%
ug/kg
%
RPD
Rec/RPD
Cll-C22 Aromatics (Unadj.)
85000
69400
82
70000
82
1
40-140/30
C9-C18 Aliphatics
30000
17900
60
16400
55
9
40-140/30
C19-C36 Aliphatics
40000
26700
67
26900
67
1
40-140/30
CAS No. Surrogate Recoveries
BSP
BSD
Limits
3386-33-2 1-Chlorooctadecane
66%
63%
40-140%
580-13-2 2-Bromonaphthalene
82%
79%
40-140%
84-15-1 o-Terphenyl
67%
66%
40-140%
321-60-8 2-Fluorobiphenyl
78%
75%
40-140%
Sample Compound
Col #1
Col #2
Breakthrough
Limit
OP67067-BS 2-Methylnaphthalene
2960
ND
0.0%
5.0
OP67067-BS Naphthalene
2740
ND
0.0%
5.0
OP67067-BSD 2-Methylnaphthalene
2970
ND
0.0%
5.0
OP67067-BSD Naphthalene
2750
ND
0.0%
5.0
* = Outside of Control Limits.
y
N
:.a
66 of 78
SGS"++
;"I ACCUTEST
FA47950

Duplicate Summary
Job Number: FA47950
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP67067-DUP
NN020660.D
1
10/13/17
MRE
10/04/17
OP67067
GNN1021
FA47950-5
NN020659.D
1
10/13/17
MRE
10/04/17
OP67067
GNN1021
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA47950-1, FA47950-2, FA47950-3, FA47950-4, FA47950-5
FA47950-5
DUP
CAS No.
Compound
ug/kg Q
ug/kg Q
RPD Limits
C11-C22 Aromatics (Unadj.)
ND
ND
nc 30 a
C9-C18 Aliphatics
15000
3690 J
121* 30 a
C19-C36 Aliphatics
4160 J
2840 J
38* 30 a
CAS No.
Surrogate Recoveries
DUP
FA47950-5
Limits
3386-33-2
1-Chlorooctadecane
65%
67%
40-140%
580-13-2
2-Bromonaphthalene
80%
93%
40-140%
84-15-1
o-Terphenyl
74%
74%
40-140%
321-60-8
2-Fluorobiphenyl
75%
89%
40-140%
(a) Advisory control limits.
* = Outside of Control Limits.
(c(�
67 of 78
SG8, ACCUTCST
FA47950

SGS, ACCUTEST
Southeast
Section 8
Misc. Forms
Custody Documents and Other Forms
(SGS Accutest Lafayette)
Includes the following where applicable:
• Chain of Custody
(�
68 of 78
SG$ ACCUTEST
FA47950

CHAIN OF CUSTODY
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Page 1 of 3
SGS Accutest Lafayette
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FA47960

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FA47950: Chain of Custody
Page 2 of 3
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SGS( � 70 of 78
ACCUTEST
FA47950

SGS Accutest Sample Receipt Summary
Job Number: FA47950 Client: SGS ACCUTEST
Date / Time Received: 10/11/2017 9:50:00 AM Delivery Method:
Cooler Temps (Initial/Adjusted): #1: (6l6):
Cooler Security Y
1. Custody Seals Present: ❑
or N
❑
Y or N
3. COC Present: © ❑
2. Custody Seals Intact: ©
❑
4. Smpl Dates/Time OK 0 ❑
Cooler Temperature
1. Temp criteria achieved:
Y or
©
N
❑
2. Thermometer ID:
DV441;
3. Cooler media:
Ice (direct
contact)
4. No. Coolers:
1
Quality Control Preservation
Y or
❑
N NIA
❑
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
❑
❑
3. Samples preserved properly:
©
❑
4. VOCs headspace free:
❑
❑
Comments
Project: RESIDENTIAL PROPERTY, CONCORD, NC
FedEx Alrbill fPs: 727200003158
Sample Integrity - Documentation
1. Sample labels present on bottles:
Y
®
or N
❑
2. Container labeling complete:
®
❑
3. Sample container label / COC agree:
®
❑
Sample Integrity - Condition
1. Sample recvd within HT:
Y
®
or N
❑
2. All containers accounted for:
®
❑
3. Condition of sample:
Intact
Sample Integrity - Instructions
Y
or N N/A
1. Analysis requested is clear:
©
❑
2. Bottles received for unspecified tests
❑
3. Sufficient volume recvd for analysis:
©
❑
4. Compositing instructions clear:
❑
❑
5. Filtering instructions clear:
❑
❑ R]
FA47950: Chain of Custody
Page 3 of 3
�+�
' 71 of 78
SGS ACCUTEST
FA47950

SGS. ACCUTEST
Southeast
GC Volatiles
QC Data Summaries
(SGS Accutest Lafayette)
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
9
�e
SG
� 72 of 78
ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: ALSE Accutest Laboratories Southeast, Inc.
Project: PMENCC: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLE1105-MB2
LE328988.1)
1
10/11/17
JF
n/a
n/a
GLE1105
The QC reported here applies to the following samples:
FA47950-1, FA47950-2, FA47950-3, FA47950-5
CAS No. Compound Result
RL Units Q
C5-C8 Aliphatics (Unadj.) ND
5000 ug/kg
C9-C12 Aliphatics (Unadj.) ND
5000 ug/kg
C9-C10 Aromatics (Unadj.) ND
5000 ug/kg
CAS No. Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 94% a 70-130%
615-59-8 2,5-Dibromotoluene 90% b 70-130%
(a) Recovery from Aromatics fraction.
(b) Recovery from Aliphatics fraction.
Method: MADEP VPH REV 1.1
SGS, ACCUTEST
FA47950

Method Blank Summary
Job Number: FA47950
Account: ALSE Accutest Laboratories Southeast, Inc.
Project: PMENCC: Residential Property; Concord, NC
Page 1 of 1
'ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
:LE1107-MB2
LE329031.1)
1
10/12/17
JF
n/a
n/a
GLE1107
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA47950-3; FA47950-4
CAS No. Compound Result RL Units Q
co
C5-C8 Aliphatics (Unadj.) ND 5000 ug/kg
C9-C12 Aliphatics (Unadj.) ND 5000 ug/kg N
C9-C10 Aromatics (Unadj.) ND 5000 ug/kg
CAS No. Surrogate Recoveries Limits
615-59-8 2,5-Dibromotoluene 95% a 70-130%
615-59-8 2,5-Dibromotoluene 93% b 70-130%
(a) Recovery from Aliphatics fraction.
(b) Recovery from Aromatics fraction.
74 of 78
�- ACCUTEST
FA47950

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA47950
Account: ALSE Accutest Laboratories Southeast, Inc.
Project: PMENCC: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLE1105-BS2
LE328985.1)
1
10/11/17
JF
n/a
n/a
GLE1105
GLE1105-BSD2
LE328986.1)
1
10/11/17
JF
n/a
n/a
GLE1105
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA47950-1, FA47950-2, FA47950-3, FA47950-5
Spike
BSP
BSP
BSD
BSD
Limits
CAS No. Compound
ug/kg
ug/kg
%
ug/kg
%
RPD
Rec/RPD
P
C5-C8 Aliphatics (Unadj.)
15000
14400
96
14700
98
2
70-130/25 Pi
C9-C12 Aliphatics (Unadj.)
15000
12900
86
12800
85
1
70-130/25 'L
C9-C10 Aromatics (Unadj.)
4000
3530
88
3500
88
1
70-130/25
CAS No. Surrogate Recoveries
BSP
BSD
Limits
615-59-8 2,5-Dibromotoluene 95% a 97% a 70-130%
615-59-8 2,5-Dibromotoluene 97% b 97% b 70-130%
(a) Recovery from Aromatics fraction.
(b) Recovery from Aliphatics fraction.
* = Outside of Control Limits.
SGS ACCUTEST
FA47950

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA47950
Account: ALSE Accutest Laboratories Southeast, Inc.
Project: PMENCC: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GLE1107-BS2
LE329028.D
1
10/12/17
JF
n/a
n/a
GLE1107
GLE1107-BSD2
LE329029.D
1
10/12/17
JF
n/a
n/a
GLE1107
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA47950-3, FA47950-4
Spike
BSP BSP
BSD
BSD
Limits
CAS No. Compound
ug/kg
ug/kg %
ug/kg
%
RPD
Rec/RPD
co
C5-C8 Aliphatics (Unadj.)
15000
17400 116
18300
122
5
70-130/25
C9-C12 Aliphatics (Unadj.)
15000
13900 93
14100
94
1
70-130/25
C9-CIO Aromatics (Unadj.)
4000
3980 100
3880
97
3
70-130/25
CAS No. Surrogate Recoveries
BSP
BSD
Limits
615-59-8 2,5-Dibromotoluene
105% a
107% a
70-130%
615-59-8 2,5-Dibromotoluene
111% b
110% b
70-130%
(a) Recovery from Aliphatics fraction.
(b) Recovery from Aromatics fraction.
* = Outside of Control Limits.
SGS/► 76 of 78
, ACCUTEST
fA47950

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number: FA47950
Account: ALSE Accutest Laboratories Southeast, Inc.
Project: PMENCC: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA47950-2MS
LE329000.1)
1
10/11/17
JF
n/a
n/a
GLE1105
FA47950-2MSD
LE329001.D
1
10/11/17
JF
n/a
n/a
GLE1105
FA47950-2
LE328999.D
1
10/11/17
JF
n/a
n/a
GLE1105
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA47950-1, FA47950-2, FA47950-3, FA47950-5
FA47950-2
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No. Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
cn
C5-C8 Aliphatics (Unadj.)
30600
182000
208000
97
182000
187000
86
11
70-130/50 w
C9-C12 Aliphatics (Unadj.)
149000
182000
429000
154*
182000
413000
145*
4
70-130/50
C9-C10 Aromatics (Unadj.)
67000
48600
150000
171*
48600
145000
160*
3
70-130/50
CAS No. Surrogate Recoveries
MS
MSD
FA47950-2
Limits
615-59-8 2,5-Dibromotoluene 114% a 105% a 109% a 70-130%
615-59-8 2,5-Dibromotoluene 104% b 101% b 82% b 70-130%
(a) Recovery from Aliphatics fraction.
(b) Recovery from Aromatics fraction.
* = Outside of Control Limits.
SGS ACCUTEST
FA47950

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number: FA47950
Account: ALSE Accutest Laboratories Southeast, Inc.
Project: PMENCC: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA48021-9MS
LE329050.1)
1
10/12/17
JF
n/a
n/a
GLE1107
FA48021-9MSD
LE329051.1)
1
10/12/17
JF
n/a
n/a
GLE1107
FA48021-9
LE329049.1)
1
10/12/17
JF
n/a
n/a
GLE1107
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA47950-3, FA47950-4
FA48021-9
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No. Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
co
C5-C8 Aliphatics (Unadj.)
ND
107000
128000
120
107000
128000
120
0
70-130/50 w
C9-C12 Aliphatics (Unadj.)
ND
107000
93900
88
107000
92800
87
1
70-130/50 N
C9-C10 Aromatics (Unadj.)
ND
28500
26000
91
28500
25300
89
3
70-130/50
CAS No. Surrogate Recoveries
MS
MSD
FA48021-9
Limits
615-59-8 2,5-Dibromotoluene 106% a 104% a 108% a 70-130%
615-59-8 2,5-Dibromotoluene 104% b 104% b 101% b 70-130%
(a) Recovery from Aliphatics fraction.
(b) Recovery from Aromatics fraction.
* = Outside of Control Limits.
SGS ACCUTEST
FA47950

SGS ACCUTEST
Southeast 09/08/17
ISGS ACCUTEST IS PART OF SGS, THE WORLD'S LEADING INSPECTION, e-Hardcopy 2. 0
VERIFICATION, TESTING AND CERTIFICATION COMPANY. Automated Report
Technical Report for
PM Environmental
Residential Property; Concord, NC
15-4231-0-0001
SGS Accutest Job Number: FA47237
Sampling Date: 08/29/17
Report to:
PM Environmental
8320 University Executive Park Dr Suite 106
Charlotte, NC 28262
warren@pmenv. com
ATTN: Don Warren
Total number of pages in report: 34
P�
Z' 1
Test results contained within this data package meet the requirements Zflin Brice, M.S.
of the National Environmental Laboratory Accreditation Program General Manager
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FLO02), NY(12022), SC(96038001)
DoD ELAP(L-A-B 1.2229), AZ(AZ0806), CA(2937), TX(Tl04704404), PA(68-03573), VA(460177),
AK, AR, GA, IA, KY, MA, NV, OK, OR, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of SGS Accutest.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • bftp://www.accutest.com
SGS Accutest is the sole authority for authorizing edits or modifications to this document. c/►(� 1 of 34
Unauthorized modification of this report is strictly prohibited. SGS. ACCUTEST
Review standard terms at: http://www.sgs.com/en/tertns-and-conditions FA47237

Table of Contents
Section1: Sample Summary...................................................................................................
Section2: Summary of Hits....................................................................................................
Section 3: Sample Results........................................................................................................
3.1: FA47237-1: TP-1..........................................................................................................
3.2: FA47237-2: TP-2..........................................................................................................
3.3: FA47237-3: TP-3..........................................................................................................
3.4: FA47237-4: TP-4..........................................................................................................
3.5: FA47237-5: TP-5..........................................................................................................
Section4: Misc. Forms............................................................................................................
4.1: Chain of Custody...........................................................................................................
Section 5: MS Volatiles - QC Data Summaries.....................................................................
5.1: Method Blank Summary................................................................................................
5.2: Blank Spike Summary...................................................................................................
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Section 6: GC Volatiles - QC Data Summaries.....................................................................
6.1: Method Blank Summary................................................................................................
6.2: Blank Spike Summary...................................................................................................
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Section 7: GGLC Semi-volatiles - QC Data Summaries.....................................................
7.1: Method Blank Summary................................................................................................
7.2: Blank Spike Summary...................................................................................................
7.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
Sections:
3
4
5
6
8
10
12
14
17
18
20
21
22
23
24
25
27
29
31
32
33
34
SGS ACCUTEST
FA47237

SGS Accutest
Sample Summary
PM Environmental
Residential Property; Concord, NC
Project No: 15-4231-0-0001
Job No: FA47237
ample Collected Matrix Client
Dumber Date Time By Received Code Type Sample ID
FA47237-1 08/29/17 10:15 DW 08/31/17 SO Soil TP-1
FA47237-2 08/29/17 10:20 DW 08/31/17 SO Soil TP-2
FA47237-3 08/29/17 10:25 DW 08/31/17 SO Soil TP-3
FA47237-4 08/29/17 10:30 DW 08/31/17 SO Soil TP-4
FA47237-5 08/29/17 10:35 DW 08/31/17 SO Soil TP-5
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
3 of34
ACCUTESTS7
FA47237

Summary of Hits
Job Number:
FA47237
Account:
PM Environmental
Project:
Residential Property; Concord, NC
Collected:
08/29/17
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA47237-1 TP-1
TPH-GRO (C6-C10)
TPH (C10-C28)
FA47237-2 TP-2
TPH-GRO (C6-C10)
TPH (C10-C28)
FA47237-3 TP-3
TPH-GRO (C6-C10)
TPH (C10-C28)
FA47237-4 TP-4
TPH (C10-C28)
FA47237-5 TP-5
Toluene
Ethylbenzene
Xylene (total)
TPH-GRO (C6-C10)
TPH (C10-C28)
888
260
130
mg/kg
SW846 8015C
18200 B
540
270
mg/kg
SW846 8015C
445
60
30
mg/kg
SW846 8015C
10800
1100
530
mg/kg
SW846 8015C
296
58
29
mg/kg
SW846 8015C
11700
1100
550
mg/kg
SW846 8015C
70.0
5.4
2.7
mg/kg
SW846 8015C
0.0662 J
0.28
0.055
mg/kg
SW846 8260B
0.440
0.28
0.055
mg/kg
SW846 8260B
2.43
0.83
0.12
mg/kg
SW846 8260B
104
12
5.9
mg/kg
SW846 8015C
8010 B
540
270
mg/kg
SW846 8015C
Page 1 of 1
�+ Si 4 of 34 Va ACCUTEST
FA47237

SGS ACCUTEST
Southeast
Sample Results
Report of Analysis
Section 3
SGS ACCUTEST
FA47237

SGS Accutest
Report of Analysis Page 1 of 1
Client Sample ID: TP-1
Lab Sample ID: FA47237-1 Date Sampled: 08/29/17
Matrix: SO - Soil Date Received: 08/31/17
Method: SW846 8015C Percent Solids: 91.6
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD145810.D 1 09/05/17 18:28 EG n/a n/a GCD6082
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.46 g 5.0 ml 2.5 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
Result
RL MDL Units Q
888
260 130 mg/kg
Run# 1
Run# 2 Limits
108%
56-149%
76%
66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
sG$ 6 of 34
ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID:
TP-1
Lab Sample ID:
FA47237-1
Matrix:
SO - Soil
Method:
SW846 8015C SW846 3546
Project:
Residential Property; Concord, NC
File ID
DF Analyzed By
Run #1 JJ016665.D
100 09/06/17 17:15 SJL
Run #2
Initial Weight Final Volume
Run #1 20.2 g 1.0 ml
Run #2
Page 1 of 1
Date Sampled: 08/29/17
Date Received: 08/31/17
Percent Solids: 91.6
Prep Date Prep Batch Analytical Batch
09/05/1710:19 OP66706 GJJ701
CAS No. Compound Result RL MDL Units Q
TPH (C10-C28) 18200 540 270 mg/kg B
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 0% a 56-122%
(a) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 34
SG ... ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID:
TP-2
Lab Sample ID:
FA47237-2
Matrix:
SO - Soil
Method:
SW846 8015C
Project:
Residential Property; Concord, NC
File ID
DF Analyzed By
Run #1 CD145811.D 1 09/05/17 18:55 EG
Run #2
Page 1 of 1
Date Sampled: 08/29/17
Date Received: 08/31/17
Percent Solids: 91.4
Prep Date Prep Batch Analytical Batch
n/a n/a GCD6082
Initial Weight Final Volume Methanol Aliquot
Run #1 4.94 g 5.0 ml 10.0 ul
Run #2
CAS No.
Compound
Result
RL MDL Units Q
TPH-GRO (C6-C10)
445
60 30 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2 Limits
460-00-4
4-Bromofluorobenzene
120%
56-149%
98-08-8
aaa-Trifluorotoluene
80%
66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS. ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID: TP-2
Lab Sample ID: FA47237-2 Date Sampled: 08/29/17
Matrix: SO - Soil Date Received: 08/31/17
Method: SW846 8015C SW846 3546 Percent Solids: 91.4
Project: Residential Property; Concord, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 JJ016702.1) 200 09/07/17 17:50 SJL 09/05/1710:19 OP66706 GJJ703
Run #2
Initial Weight Final Volume
Run #1 20.5 g 1.0 ml
Run #2
CAS No. Compound
Result
RL MDL Units Q
TPH (C10-C28)
10800
1100 530 mg/kg
CAS No. Surrogate Recoveries
Run# I
Run# 2 Limits
84-15-1 o-Terphenyl
0% a
56-122%
(a) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
r.;
Q
9 of 34
S-G$-_ ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID:
TP-3
Lab Sample ID:
FA47237-3
Matrix:
SO - Soil
Method:
SW846 8015C
Project:
Residential Property; Concord, NC
File ID
DF Analyzed By
Run #1 CD145793.D 1 09/02/17 03:57 EG
Run #2
Page 1 of 1 f ,
Date Sampled: 08/29/17 ,?
Date Received: 08/31/17
Percent Solids: 90.6
Prep Date Prep Batch Analytical Batch
n/a n/a GCD6081
Initial Weight Final Volume Methanol Aliquot
Run #1 5.21 g 5.0 ml 10.0 ul
Run #2
CAS No.
Compound
Result
RL MDL Units Q
TPH-GRO (C6-C10)
296
58 29 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2 Limits
460-00-4
4-Bromofluorobenzene
109%
56-149%
98-08-8
aaa-Trifluorotoluene
78%
66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SUS10 of 34
sr`{ ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID: TP-3
Lab Sample ID: FA47237-3
Matrix: SO - Soil
Method: SW846 8015C SW846 3546
Project: Residential Property; Concord, NC
File ID DF Analyzed By
Run #1 JJ016703.1) 200 09/07/17 18:18 SJL
Run #2
Initial Weight Final Volume
Run #1 20.2 g 1.0 ml
Run #2
CAS No. Compound
Result
TPH (C10-C28)
11700
CAS No. Surrogate Recoveries
Run# 1
84-15-1 o-Terphenyl
0% a
(a) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
Page 1 of 1
Date Sampled: 08/29/17
Date Received: 08/31/17
Percent Solids: 90.6
Prep Date Prep Batch Analytical Batch
09/05/1710:19 OP66706 GJJ703
RL MDL Units Q
1100 550 mg/kg
Run# 2 Limits
56-122%
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
-G$11 of 34
ACCUTEST
FA47237

SGS Accutest
Client Sample ID: TP-4
Report of Analysis Page 1 of 1
Lab Sample ID: FA47237-4 Date Sampled: 08/29/17
Matrix: SO - Soil Date Received: 08/31/17
Method: SW846 8015C Percent Solids: 91.3
Project: Residential Property; Concord, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD145788.D 1 09/02/17 01:43 EG n/a n/a GCD6081
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.04 g 5.0 ml 100 al
Run #2
CAS No.
Compound
TPH-GRO (C6-C10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
Result
RL MDL Units Q
ND
5.9 3.0 mg/kg
Run# 1
Run# 2 Limits
95%
56-149%
75%
66-132%
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
12 of 34
_a7 ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID: TP-4
Lab Sample ID: FA47237-4
Matrix: SO - Soil
Method: SW846 8015C SW846 3546
Project: Residential Property; Concord, NC
File ID DF Analyzed By
Run #1 JJ016704.D 1 09/07/17 18:47 SJL
Run #2
Initial Weight Final Volume
Run #1 20.4 g 1.0 ml
Run #2
Page 1 of 1
Date Sampled: 08/29/17
Date Received: 08/31/17
Percent Solids: 91.3
Prep Date Prep Batch Analytical Batch
09/05/1710:19 OP66706 GJJ703
CAS No. Compound Result RL MDL Units Q
TPH (C10-C28) 70.0 5.4 2.7 mg/kg
CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits
84-15-1 o-Terphenyl 121% 56-122%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SG ac13 of 34
curEsr
FA47237

SGS Accutest
Report of Analysis
Client Sample ID: TP-5
Lab Sample ID: FA47237-5
Matrix: SO - Soil
Method: SW846 8260B
Project: Residential Property; Concord, NC
File ID DF Analyzed By
Run #1 Y35986.D 1 09/O1/17 18:16 EP
Run #2
Page 1 of 1
Date Sampled: 08/29/17
Date Received: 08/31/17
Percent Solids: 91.2
Prep Date Prep Batch Analytical Batch
n/a n/a VY1429
Initial Weight Final Volume Methanol Aliquot
Run #1 5.44 g 5.0 ml 100 ul
Run #2
Purgeable Aromatics
CAS No.
Compound
Result
RL
MDL Units Q
71-43-2
Benzene
ND
0.28
0.067 mg/kg
108-88-3
Toluene
0.0662
0.28
0.055 mg/kg J
100-41-4
Ethylbenzene
0.440
0.28
0.055 mg/kg
1330-20-7
Xylene (total)
2.43
0.83
0.12 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
100%
75-124%
17060-07-0
1,2-Dichloroethane-D4
104%
72-135%
2037-26-5
Toluene-D8
96%
75-126%
460-00-4
4-Bromofluorobenzene
95%
71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14of34
.1 ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID: TP-5
Lab Sample ID: FA47237-5 Date Sampled: 08/29/17
Matrix: SO - Soil Date Received: 08/31/17
Method: SW846 8015C Percent Solids: 91.2
Project: Residential Property; Concord, NC
Page 1 of 1
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD145794.1) 1 09/02/17 04:23 EG n/a n/a GCD6081
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.08 g 5.0 ml 50.0 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
Result
RL MDL Units Q
104
12 5.9 mg/kg
Run# l
Run# 2 Limits
111%
56-149%
85%
66-132%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
SGS ACCUTEST
FA47237

SGS Accutest
Report of Analysis
Client Sample ID:
TP-5
Lab Sample ID:
FA47237-5
Matrix:
SO - Soil
Method:
SW846 8015C SW846 3546
Project:
Residential Property; Concord, NC
File ID
DF Analyzed By
Run #1 JJ016671.D 100 09/06/17 20:07 SJL
Run #2
Initial Weight Final Volume
Run #1 20.2 g 1.0 ml
Run #2
Page 1 of 1
Date Sampled: 08/29/17 r
Date Received: 08/31/17
Percent Solids: 91.2
Prep Date Prep Batch Analytical Batch
09/05/1710:19 OP66706 GJJ701
CAS No. Compound
Result
RL MDL Units Q
TPH (C10-C28)
8010
540 270 mg/kg B
CAS No. Surrogate Recoveries
Run# 1
Run# 2 Limits
84-15-1 o-Terphenyl
0% a
56-122%
(a) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
S-G916 of 34
ACCUTEST
FA47237

SGS ACCUTEST
Southeast
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Section 4
SG(� 17 of 34
ACCUTEST
FA47237

�+
SGS Accutest southeast FA Lyny
SGSChain of Custody SOSACCUTESTJOSO: PAGE_LOF.
FA47237: Chain of Custody
Page l of 2
SGAC18 of 34
a�.h CUTEST
FA47237

SGS Accutest Sample Receipt Summary
Job Number: FA47237 Client: PM ENV. Project: RESIDENTIAL PROPERTY
Date / Time Received: 8/31/2017 9:00:00 AM Delivery Method: FED EX Airbill #'s: 8043 9730 3933
Therm ID: IR 1; Therm CF: -0.2; # of Coolers: 1
Cooler Temps (Raw Measured) °C: Cooler 1: (0.8);
Cooler Temps (Corrected) °C: Cooler 1: (0.6);
Cooler Information
Y or
N
Sample Information
Y or
N
N/A
1. Custody Seals Present
W
❑
1. Sample labels present on bottles
©
❑
2. Custody Seals Intact
©
❑
2. Samples preserved properly
©
❑
3. Temp criteria achieved
©
❑
3. Sufficient volume/containers recvd for analysis:
©
❑
4. Cooler temp verification
IR Gun
4. Condition of sample
Intact
5. Cooler media
Ice IBao)
5. Sample recvd within HT
©
❑
6. Dates/Times/IDs on COC match Sample Label
©
❑
Trio Blank Information
Y or
N
N/A
7. VOCs have headspace
❑
❑
1. Trip Blank present / cooler
❑
©
❑
8. Bottles received for unspecified tests
❑
2. Trip Blank listed on COC
❑
Q
❑
9. Composiling instructions clear
❑
❑
W
W or S
N/A
10. Voa Soil Kits/Jars received past 48hrs?
❑
❑
11. % Solids Jar received?
WJ
❑
❑
3. Type Of TB Received
❑
❑66
12. Residual Chlorine Present?
❑
❑
Misc. Information
Number of Encores: 25-Gram
Test Strip Lot #s: pH 0-3
Residual Chlorine Test Strip Lot #:
I Comments
snmool Technician: SHAYLAP
Rev. Date 05/24/17
5-Gram Number of 5035 Field Kits: 5 Number of Lab Filtered Metals:
230315 pH 10-12 219813A Other: (Specify)
Date: 8/31/2017 9:00:00 AM Reviewer:
Date:
FA47237: Chain of Custody
Page 2 of 2
'�(�
19 of 34
SG$ ACCUTEST
FA47237

SGS
ACCUTEST
Southeast
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• -Matrix Spike and Duplicate Summaries
Section 5
SGS ACCUTEST
FA47237

Method Blank Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1429-MB
Y35967.D
1
09/01/17
EP
n/a
n/a
VY1429
The QC reported here applies to the following samples:
Method: SW846 8260B
FA47237-5
CAS No.
Compound
Result
RL
MDL
Units Q
71-43-2
Benzene
ND
5.0
1.2
ug/kg
100-41-4
Ethylbenzene
ND
5.0
1.0
ug/kg
108-88-3
Toluene
ND
5.0
1.0
ug/kg
1330-20-7
Xylene (total)
ND
15
2.1
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
107%
75-124%
17060-07-0
1,2-Dichloroethane-D4
104%
72-135%
2037-26-5
Toluene-D8
97%
75-126%
460-00-4
4-Bromofluorobenzene
106%
71-133%
SGS ACCUTEST
FA47237

Blank Spike Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY1429-BS
Y35968.D
1
09/O1/17
EP
n/a
n/a
VY1429
The QC reported here applies to the following samples: Method: SW846 8260B
FA47237-5
CAS No. Compound
71-43-2
Benzene
100-41-4
Ethylbenzene
108-88-3
Toluene
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
1868-53-7 Dibromofluoromethane
17060-07-0 1, 2-Dichloroethane-D4
2037-26-5 Toluene-D8
460-00-4 4-Bromofluorobenzene
* = Outside of Control Limits.
Spike
BSP
BSP
ug/kg
ug/kg
%
Limits
50
58.0
116
76-126
50
56.8
114
77-123
50
56.6
113
76-124
150
170
113
80-129
BSP Limits
104% 75-124%
98% 72-135%
101% 75-126%
101% 71-133%
SGS' ACCUTEST
FA47237

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA47224-33MS
Y35984.D
1
09/O1/17
EP
n/a
n/a
VY1429
FA47224-33MSD
Y35985.D
1
09/O1/17
EP
n/a
n/a
VY1429
FA47224-33
Y35973.D
1
09/01/17
EP
n/a
n/a
VY1429
The QC reported here applies to the following samples: Method: SW846 8260B
FA47237-5
FA47224-33 Spike
MS MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg
Q ug/kg
ug/kg %
ug/kg
ug/kg
%
RPD
Rec/RPD
71-43-2
Benzene
ND
60.2
53.7 89
61.7
55.1
89
3
76-126/26
100-41-4
Ethylbenzene
ND
60.2
51.9 86
61.7
52.2
85
1
77-123/31
108-88-3
Toluene
ND
60.2
53.0 88
61.7
53.1
86
0
76-124/30
1330-20-7
Xylene (total)
ND
181
159 88
185
161
87
1
80-129/30
CAS No.
Surrogate Recoveries
MS
MSD
FA47224-33 Limits
1868-53-7
Dibromofluoromethane
98%
104%
107%
75-124%
17060-07-0
1,2-Dichloroethane-D4
100%
99%
104%
72-135%
2037-26-5
Toluene-D8
99%
99%
97%
75-126%
460-00-4
4-Bromofluorobenzene
102%
104%
102%
71-133%
* = Outside of Control Limits.
P
is
SG$23 of 34
ACCUTEST
FA47237

SG�
ACCUTEST
Southeast
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
u
24 of 34
ACCUTEST
FA47237

Method Blank Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GCD6081-MB
CD145770.1)
1
09/O1/17
EG
n/a
n/a
GCD6081
The QC reported here applies to the following samples:
FA47237-3, FA47237-4, FA47237-5
CAS No. Compound Result RL
TPH-GRO (C6-C10) ND 5.0
Method: SW846 8015C
MDL Units Q
2.5 mg/kg
CAS No.
Surrogate Recoveries
Limits
460-00-4
4-Bromofluorobenzene
76% 56-149%
98-08-8
aaa-Trifluorotoluene
74% 66-132%
SGS ACCUTEST
FA47237

Method Blank Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GCD6082-MB
CD145809.1)
1
09/05/17
EG
n/a
n/a
GCD6082
The QC reported here applies to the following samples:
FA47237-1, FA47237-2
CAS No. Compound Result RL
TPH-GRO (C6-C10) ND 5.0
Method: SW846 8015C
MDL Units Q
2.5 mgAg
CAS No.
Surrogate Recoveries
Limits
460-00-4
4-Bromofluorobenzene
87% 56-149%
98-08-8
aaa-Trifluorotoluene
74% 66-132%
rn
N
SlG5 ACCUTEST
FA47237

Blank Spike Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GCD6081-BS
CD145769.D
1
09/O1/17
EG
n/a
n/a
GCD6081
The QC reported here applies to the following samples: Method: SW846 8015C
FA47237-3, FA47237-4, FA47237-5
CAS No. Compound
TPH-GRO (C6-C10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
* = Outside of Control Limits.
Spike
BSP
BSP
mg/kg
mg/kg
% Limits
20
19.5
98 74-128
BSP Limits
91% 56-149%
93% 66-132%
G ACCUTEST
FA47237

Blank Spike Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of i
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GCD6082-BS
CD145808.1)
1
09/05/17
EG
n/a
n/a
GCD6082
The QC reported here applies to the following samples: Method: SW846 8015C
FA47237-1, FA47237-2
CAS No. Compound
TPH-GRO (C6-C10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
* = Outside of Control Limits.
Spike BSP BSP
mg/kg mg/kg % Limits
20 19.3 97 74-128
BSP
Limits
97%
56-149%
90%
66-132%
rn
N
N
0
SGS ACCUTEST
FA47237

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA47201-1MS
CD145777.D
1
09/01/17
EG
n/a
n/a
GCD6081
FA47201-1MSD
CD145778.D
1
09/01/17
EG
n/a
n/a
GCD6081
FA47201-1
CD145771.D
1
09/01/17
EG
n/a
n/a
GCD6081
The QC reported here applies to the following samples: Method: SW846 8015C
FA47237-3, FA47237-4, FA47237-5
FA47201-1 Spike MS MS Spike MSD MSD Limits
CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg mg/kg % RPD Rec/RPD
TPH-GRO (C6-C10) ND 18 18.1 101 18 17.3 96 5 74-128/17
CAS No.
Surrogate Recoveries
MS
MSD
FA47201-1
Limits
460-00-4
4-Bmmofluorobenzene
90%
86%
77%
56-149%
98-08-8
aaa-Trifluorotoluene
93%
93%
74%
66-132%
* = Outside of Control Limits.
G 29 of 34
ACCUTEST
FA47237

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA47238-1MS
CD145813.D
1
09/05/17
EG
n/a
n/a
GCD6082
FA47238-1MSD
CD145814.D
1
09/05/17
EG
n/a
n/a
GCD6082
FA47238-1
CD145812.1)
1
09/05/17
EG
n/a
n/a
GCD6082
The QC reported here applies to the following samples: Method: SW846 8015C
FA47237-1, FA47237-2
FA47238-1 Spike MS MS Spike MSD MSD Limits
CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg mg/kg % RPD Rec/RPD
TPH-GRO (C6-C10) 165 129 286 94 129 290 97 1 74-128/17
CAS No.
Surrogate Recoveries
MS
MSD
FA47238-1
Limits
460-00-4
4-Bromofluorobenzene
108%
108%
104%
56-149%
98-08-8
aaa-Trifluorotoluene
94%
94%
79%
66-132%
* = Outside of Control Limits.
//''++��**
30 of 34
SGS ACCUl"EST
FA47237

SGS ACCUTEST
Southeast
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Section 7
SY�.731 of 34
ACCUTEST
FA47237

Method Blank Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP66706-MB
JJ016664.D
1
09/06/17
SJL
09/05/17
OP66706
GJJ701
The QC reported here applies to the following samples:
FA47237-1, FA47237-2, FA47237-3, FA47237-4, FA47237-5
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
(a) Outside control limits.
Method: SW846 8015C
Result RL MDL Units Q
2.70 5.0 2.5 mg/kg J
Limits
116% a 56-122%
SG(�(�� 32 of 34
ACCUTEST
FA47237

Blank Spike Summary
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP66706-BS
JJ016663.D
1
09/06/17
SJL
09/05/17
OP66706
GJJ701
The QC reported here applies to the following samples:
FA47237-1, FA47237-2, FA47237-3, FA47237-4, FA47237-5
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
(a) Outside control limits.
* = Outside of Control Limits.
Spike
BSP
BSP
mg/kg
mg/kg
% Limits
50
53.5
107 62-116
BSP Limits
123%* a 56-122%
Method: SW846 8015C
74
iv
O�r(%� 33 of 34
__lau$ . ACCUTEST
FA47237

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number: FA47237
Account: PMENCC PM Environmental
Project: Residential Property; Concord, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP66706-MS
JJ016672.D
100
09/06/17
SJL
09/05/17
OP66706
GJJ701
OP66706-MSD
JJ016673.D
100
09/06/17
SJL
09/05/17
OP66706
GJJ701
FA47237-5
JJ016671.D
100
09/06/17
SJL
09/05/17
OP66706
GJJ701
The QC reported here applies to the following samples: Method: SW846 8015C
V
FA47237-1, FA47237-2, FA47237-3, FA47237-4, FA47237-5 is
FA47237-5 Spike MS MS Spike MSD MSD Limits
CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg mg/kg % RPD Rec/RPD
TPH (C10-C28) 8010 B 53.7 7550 -856* a 53.5 7290 -1346* a4 62-116/35
CAS No. Surrogate Recoveries MS MSD FA47237-5 Limits
84-15-1 o-Terphenyl 0%* b 0%* b 0%* b 56-122%
(a) Outside control limits due to high level in sample relative to spike amount.
(b) Outside control limits due to dilution.
* = Outside of Control Limits.
SCE AC34 of 34
CUTEST
FA47237

CHAIN OF CUSTODY
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Page 1 of 3
SGS Accutest Lafayette
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ACCUTEST
FA47950

SUS Accutest Southeast . F'A LR231
S7� ��urecr Chain of Custody SOS ACCUTEST JOB l: PAGE_/OF__
FA47237: Chain of Custody
Page l of 2
18 of 34
SG$ ACCUTEST
FA47237