6002_Mecklenburg_HolbrooksRoad_MSWLF_GW_FID1319082_20190409

�ENR USE ONLY_: ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR I IEnvironmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are 'Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006)
Holbrooks Road Landfill 15401 Holbrooks Road 60-02 .0500 March 20-21, 2019 and
March 27, 2019
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring Z Detection Monitoring ❑ Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑X
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data
Surface water monitoring data ❑
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑X Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G. Project Manager
Facility pre tatiye-Na (PrirA Title
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1,
Revised 6/2009
980-314-3855
(Area Code) Telephone Number
4/9/2019 Affix NC Licensed/ Professional Geologist Seal
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MECKLENBURG COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
April 9, 2019
Jaclynne Drummond
North Carolina Department of Environmental Quality
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Holbrooks Road Landfill Permit 60-02
Semi-annual Monitoring Results
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Holbrooks Road Landfill March 20-21, 2019 in accordance with the approved sample
and analysis plan dated March 27, 2003. This report details the results of that monitoring
event. Laboratory analytical data, field -measured data table of values exceeding 2L
standards and landfill gas monitoring data is contained on the electronic data deliverable
submittal.
Samples were collected from eleven (11) monitoring wells (HRW-7, HRW-8, HRW-9,
HRW-10, HRW-11R, HRW-13, HRW-16, HRW-18, HRW-19, HRW-20 and HRW-21)
and three (3) surface -water sampling locations (HRSW-2, HRSW-3 and HRSW-4).
Samples were analyzed for metals and volatile organic compounds ("VOCs") listed in
Appendix I of 40 CFR Part 258.54 "Detection monitoring program". Samples were also
analyzed for 1,4-Dioxane as required as of July 1, 2018. Field measurements of
temperature, pH, and specific conductivity were made at each sampling location using a
calibrated instrument. Additionally, measurements of dissolved oxygen were made at
each surface -water sampling location.
The electronic data deliverable package containing the monitoring data is labeled to
reflect the units used for reporting. Surface water standards listed are the water quality
standards established for freshwater classification for aquatic life as outlined in 15A
NCAC 213 "Classification and Water Quality Standards Applicable to Surface Waters of
North Carolina". Groundwater standards listed are the standards outlined in 15A NCAC
2L "Classification of Water Quality Standards applicable to the Groundwaters of North
Carolina". If the sample is reported in parts per billion, then the standard is also reported
in parts per billion.
PEOPLE -PRIDE - PROGRESS - PARTNERSHIP
2145 Suttle Ave - Charlotte, North Carolina 28208 • [phone] Fax [phone]
www.wipeoutwaste.com

Page 2
Surface=water samples:
Barium was detected in all 3 stream sampling locations. The following table summarizes
the metals detections for the surface water sampling locations.
Sample Location
Barium
ug/l
HRSW-2 upstream
33.5
HRSW-4 mid -stream
31.2
HRSW-3 downstream
30.6
No VOCs were detected in any of the samples collected from the three surface -water
sampling locations (HRSW-2, HRSW-4 and HRSW-3). All field -measured parameters
were within the established regulatory limits. The following table summarizes field -
measured parameters for surface water samples.
Sample Location
Temp.
°C
pH
S.U.
Specific Conductivity
ms/cm
Dissolved Oxygen
mg/l
HRSW-2 upstream
10.0
7.6
0.234
13.68
HRS W-4 mid -stream
10.4
7.5
0.218
13.79
HRSW-3 downstream
10.7
7.5
0.216
13.73
Groundwater samples:
Vanadium, cobalt and chromium were detected in various wells above the 21 standard.
The following table summarizes metals detection for groundwater samples.
Well ID
As
ug/l
Ba
ug/l
Be
ug/l
Cd
ug/l
Cr
ug/l
Co
ug/l
Cu
ug/l
Pb
ug/l
Ni
ug/l
Se
ug/l
Vn
ug/l
Zn
ug/l
HRW-7
-----
107
-----
1.9
-----
-----
8.6
-----
-----
-----
-----
10.4
HRW-8
-----
93.8
-----
-----
9.5
6.6
18.1
-----
-----
-----
31.4
21.1
HRW-9
-----
274
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-10
-----
150
-----
-----
-----
-----
9.0
-----
13.0
-----
-----
-----
HRW-11R
-----
153
-----
-----
-----
-----
8.0
-----
13.0
-----
6.5
-----
HRW-13
------
109
-----
-----
6.0
-----
9.7
-----
-----
-----
9.5
11.4
HRW-16
-----
159
-----
-----
11.4
-----
27.6
-----
6.0
-----
41.2
22.8
HRW-18
-----
270
-----
-----
-----
5.9
-----
-----
6.3
-----
-----
-----
HRW-19
-----
69.2
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-20
-----
73.3
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
HRW-21
-----
52.8
-----
-----
-----
-----
-----
-----
-----
-----
-----
-----
2L Std.
10
700
4
2
10
1
1,000
15
100
20
0.3
1,000
Note: Results shown in bold exceed the 21, standard.

Page 3
VOCs were detected in six monitoring wells; HRW-7, HRW-9, HRW-10, HRW-11R,
HRW-18 and HRW-20. The following table summarizes VOC detections.
Well ID
Volatile Constituent
Concentration
2L Standard
u /1
u /1
Cis-1,2-Dichloroethene
2.3
70
HRW-7
Trichloroethene
2.1
3
HRW-9
Chlorobenzene
2.7
50
1,2-Dichlorobenzene
7.6
20
1,4-Dichlorobenzene
11.9
6
1,1-Dichloroethane
35.0
6
1,2-Dichloroethane
1.9
0.4
Cis-1,2-Dichloroethane
77.5
70
Trans-1,2-Dichloroethane
1.4
100
1,2-Dichloropropane
2.2
0.6
Tetrachloroethene
1.4
0.7
Trichloroethene
3.4
3
Trichlorofluoromethane
3.2
2000
Vinyl Chloride
14.1
0.03
1,4-Dioxane
10.2
3
HRW-10
Chlorobenzene
1.1
50
1,4-Dioxane
13.1
3
HRW-11R
Chlorobenzene
2.6
50
1,4-Dioxane
42.2
3
Benzene
43
1
HRW-18
Chlorobenzene
3.7
50
1,1-Dichloroethane
27.8
6
1,2-Dichloropropane
4.1
0.6
1,4 Dichlorobenzene
7.8
6
Vinyl Chloride
13.5
0.03
1,4-Dioxane
15.4
3
HRW-20
1,1-Dichloroethane
5.2
6
Note: Results shown in bold exceed the 2L standard.
Measurements of pH were more acidic than the 2L standard range of 6.5 to 8.5 standard
units at HRW-9, HRW-13 and HRW-16. Field- measured parameters for groundwater
samples are summarized in the following table.

Page 4
Sample Location
Temp. °C
PH
Specific Conductivity ms/cm
HRW-7
17.2
6.5
0.419
HRW-8
11.0
6.5
0.066
HRW-9
14.7
6.2
0.912
HRW-10
12.0
6.7
0.848
HRW-11R
13.0
6.5
1.950
HRW-13
11.9
6.0
0.361
HRW-16
11.3
5.9
0.091
HRW-18
15.7
6.7
1.122
HRW-19
13.8
7.7
0.345
HRW-20
14.3
7.3
0.308
HRW-21
15.2
7.4
0.495
Note: Results shown in bold are outside of the 2L standard range of 6.5 - 8.5 S.U.
Please call me at [phone] if you have any questions regarding this report.
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Amber R. Grzyms P.G.
Project Manager
Solid Waste Services

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Landfill Gas Monitoring Data Form
Facility Name: Holbrooks Road Landfill Permit Number: 60-02
Date of Sampling: 03/27/19 NC Landfill Rule (.0500 or .1600): .0500
Name and Position of Sample Collector: _David E. Coleman, Environmental Specialist
Type and Serial Number of Gas Meter: Gem 2000 #GM13774
Calibration Date of Gas Meter: 2/27/2019 Date and Time of Field Calibration:03/27/19 10:45A.M.
Type of Field Calibration Gas (15/15 or 35/50): _35/50
Expiration Date of Field Calibration Gas Canister: _October 2020
Pump Rate of Gas Meter: 120 Seconds Ambient Air Temperature: 46 degrees
Barometric Pressure: 29.64 General Weather Conditions: Sunny, I INE
Sample ID
Time
% LEL
%
CH4
%
02
%
CO2
Comments
HP-3
12:16 PM
0
0
9.3
12.5
HP-4
11:41 AM
0
0
2.2
10.2
HP-8R
11:32 AM
0
0
21.3
0
HP-9
11:09 AM
>100
30.6
0
19.5
HP-15R
1:02 PM
>100
42.3
0
16.5
Property Line Violation
HP-16R
12:47 PM
0
0
9.3
10.9
HP-18R
12:37 PM
>100
9
11.8
10.7
Property Line Violation
HP-24
11:52 AM
0
0
21.1
0.1
HP-25
11:47 AM
0
0
21.1
0
HP-26
11:26 AM
0
0
21.1
0
HP-27
11:17 AM
0
0
21.2
0 -
BUILDING
11:35 AM
0
0
21.3
0
MV-1
11:56 AM
0
0
21.1
0
Passive Methane Trench Vent
MV-2
12:00 PM
0
0
20.8
0.1
Passive Methane Trench Vent
MV-3
12:04 PM
0
0
20.9
0
Passive Methane Trench Vent
MV-4
12:08 PM
0
0
19.7
1.3
Passive Methane Trench Vent
MV-5
12:11 PM
0
0
20.3
0.6
Passive Methane Trench Vent
NW-6
12:20 PM
0
0
21.0
0
Passive Methane Trench Vent
MV-7
12:24 PM
0
0
20.4
0.6
Passive Methane Trench Vent
MV-8
12:28 PM
0
0
21.2
0
Passive Methane Trench Vent
MV-9
12:32 PM
0
0
21.2
0
Passive Methane Trench Vent
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and
attachments are true and correct. I am aware that there are significant penalties for making any false
statement, representation, or certification including the possibility of a fine and imprisonment.
SIGNATU TRE
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REFERENCES
1. PROPERTYLINES, MONITORING WELLS, AND STREAMS FROM
MECKLENBURG COUNTYGIS DEPARTMENT.
2. FROM DRAWING"GROUNDWATER MONITORING WELL AND
BORING LOCATION MAP" DATED MARCH 2O10, SHEET S2 OF 19,
PREPARED BYBP BARBER.
3. FROM DRAWING "SITE MAP WITH WELL LOCATIONS' DATED
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aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 01, 2019
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HOLBROOKS ROAD LANDFILL
92422048
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92422048001
HRW-7
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422048002
HRW18
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422048003
HRW19
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422048004
HRW20
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422048005
HRW21
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422048006
TRIP BLANK
EPA 8260D
NSCQ
52
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 30

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW-7 Lab ID: 92422048001 Collected: 03/20/19 12:00 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:09
7440-38-2
Barium
107
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:09
7440-41-7
Cadmium
1.9
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:09
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-48-4
Copper
8.6
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:09
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:09
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:09
7440-62-2
Zinc
10.4
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:09
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:22
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 04:06
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 04:06
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 04:06
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 04:06
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 04:06
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 04:06
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 04:06
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 04:06
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 04:06
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 04:06
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 04:06
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 04:06
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 04:06
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 04:06
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 04:06
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 04:06
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 04:06
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 04:06
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 04:06
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 04:06
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 04:06
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 04:06
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 04:06
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:06
75-35-4
cis-1,2-Dichloroethene
2.3
ug/L
1.0
1
03/27/19 04:06
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:06
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW-7 Lab ID: 92422048001 Collected: 03/20/19 12:00 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 04:06
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 04:06
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 04:06
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 04:06
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 04:06
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 04:06
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 04:06
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 04:06
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 04:06
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 04:06
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 04:06
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 04:06
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 04:06
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 04:06
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 04:06
79-00-5
Trichloroethene
2.1
ug/L
1.0
1
03/27/19 04:06
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 04:06
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 04:06
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 04:06
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 04:06
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 04:06
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 04:06
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 04:06
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
03/27/19 04:06
460-00-4
1,2-Dichloroethane-d4 (S)
77
%
70-130
1
03/27/19 04:06
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
03/27/19 04:06
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 01:12
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
50-150
1
03/26/19 01:12
17060-07-0
Toluene-d8 (S)
98
%
50-150
1
03/26/19 01:12
2037-26-5
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 30

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW18 Lab ID: 92422048002 Collected: 03/20/19 11:40 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:12
7440-38-2
Barium
270
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:12
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:12
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-47-3
Cobalt
5.9
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7439-92-1
Nickel
6.3
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:12
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:12
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:12
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:12
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:25
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 04:24
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 04:24
107-13-1
Benzene
4.5
ug/L
1.0
1
03/27/19 04:24
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 04:24
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 04:24
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 04:24
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 04:24
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 04:24
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 04:24
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 04:24
56-23-5
Chlorobenzene
3.7
ug/L
1.0
1
03/27/19 04:24
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 04:24
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 04:24
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 04:24
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 04:24
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 04:24
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 04:24
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 04:24
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 04:24
95-50-1
1,4-Dichlorobenzene
7.8
ug/L
1.0
1
03/27/19 04:24
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 04:24
110-57-6
1,1-Dichloroethane
27.8
ug/L
1.0
1
03/27/19 04:24
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 04:24
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:24
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:24
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:24
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW18 Lab ID: 92422048002 Collected: 03/20/19 11:40 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
4.1
ug/L
1.0
1
03/27/19 04:24
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 04:24
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 04:24
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 04:24
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 04:24
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 04:24
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 04:24
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 04:24
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 04:24
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 04:24
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 04:24
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 04:24
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 04:24
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 04:24
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 04:24
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 04:24
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 04:24
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 04:24
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 04:24
108-05-4
Vinyl chloride
13.5
ug/L
1.0
1
03/27/19 04:24
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 04:24
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 04:24
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 04:24
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
03/27/19 04:24
460-00-4
1,2-Dichloroethane-d4 (S)
76
%
70-130
1
03/27/19 04:24
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
03/27/19 04:24
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
15.4
ug/L
2.0
1
03/26/19 01:31
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
50-150
1
03/26/19 01:31
17060-07-0
Toluene-d8 (S)
97
%
50-150
1
03/26/19 01:31
2037-26-5
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 30

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW19 Lab ID: 92422048003 Collected: 03/20/19 11:00 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:15
7440-38-2
Barium
69.2
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:15
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:15
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:15
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:15
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:15
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:15
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:29
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 04:42
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 04:42
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 04:42
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 04:42
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 04:42
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 04:42
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 04:42
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 04:42
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 04:42
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 04:42
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 04:42
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 04:42
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 04:42
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 04:42
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 04:42
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 04:42
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 04:42
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 04:42
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 04:42
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 04:42
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 04:42
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 04:42
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 04:42
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 04:42
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW19 Lab ID: 92422048003 Collected: 03/20/19 11:00 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 04:42
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 04:42
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 04:42
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 04:42
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 04:42
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 04:42
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 04:42
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 04:42
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 04:42
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 04:42
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 04:42
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 04:42
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 04:42
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 04:42
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 04:42
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 04:42
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 04:42
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 04:42
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 04:42
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 04:42
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 04:42
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 04:42
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 04:42
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
03/27/19 04:42
460-00-4
1,2-Dichloroethane-d4 (S)
72
%
70-130
1
03/27/19 04:42
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
03/27/19 04:42
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 01:50
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91
%
50-150
1
03/26/19 01:50
17060-07-0
Toluene-d8 (S)
97
%
50-150
1
03/26/19 01:50
2037-26-5
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW20 Lab ID: 92422048004 Collected: 03/20/19 11:20 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:18
7440-38-2
Barium
73.3
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:18
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:18
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:18
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:18
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:18
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:18
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:33
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 05:01
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 05:01
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 05:01
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 05:01
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 05:01
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 05:01
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 05:01
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 05:01
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 05:01
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 05:01
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 05:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 05:01
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 05:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 05:01
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 05:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 05:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 05:01
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 05:01
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 05:01
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 05:01
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 05:01
110-57-6
1,1-Dichloroethane
5.2
ug/L
1.0
1
03/27/19 05:01
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 05:01
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:01
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW20 Lab ID: 92422048004 Collected: 03/20/19 11:20 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 04/01 /2019 06:18 PM
Analytical Method: EPA 8260D
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
97 %
73 %
108 %
Analytical Method: EPA 8260D Mod
ND ug/L
115 %
109 %
1.0
1
03/27/19 05:01
78-87-5
1.0
1
03/27/19 05:01
10061-01-5
1.0
1
03/27/19 05:01
10061-02-6
1.0
1
03/27/19 05:01
100-41-4
5.0
1
03/27/19 05:01
591-78-6
20.0
1
03/27/19 05:01
74-88-4
5.0
1
03/27/19 05:01
75-09-2
5.0
1
03/27/19 05:01
108-10-1
1.0
1
03/27/19 05:01
100-42-5
1.0
1
03/27/19 05:01
630-20-6
1.0
1
03/27/19 05:01
79-34-5
1.0
1
03/27/19 05:01
127-18-4
1.0
1
03/27/19 05:01
108-88-3
1.0
1
03/27/19 05:01
71-55-6
1.0
1
03/27/19 05:01
79-00-5
1.0
1
03/27/19 05:01
79-01-6
1.0
1
03/27/19 05:01
75-69-4
1.0
1
03/27/19 05:01
96-18-4
2.0
1
03/27/19 05:01
108-05-4
1.0
1
03/27/19 05:01
75-01-4
1.0
1
03/27/19 05:01
1330-20-7
2.0
1
03/27/19 05:01
179601-23-1
1.0
1
03/27/19 05:01
95-47-6
70-130 1
70-130 1
70-130 1
2.0 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/27/19 05:01 460-00-4
03/27/19 05:01 17060-07-0
03/27/19 05:01 2037-26-5
03/29/19 13:52 123-91-1
03/29/19 13:52 17060-07-0
03/29/19 13:52 2037-26-5
Page 11 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW21 Lab ID: 92422048005 Collected: 03/20/19 10:36 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:21
7440-38-2
Barium
52.8
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:21
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:21
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:21
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:21
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:21
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:21
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:36
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 05:19
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 05:19
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 05:19
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 05:19
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 05:19
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 05:19
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 05:19
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 05:19
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 05:19
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 05:19
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 05:19
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 05:19
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 05:19
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 05:19
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 05:19
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 05:19
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 05:19
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 05:19
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 05:19
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 05:19
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 05:19
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 05:19
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 05:19
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:19
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:19
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:19
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 30

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: HRW21 Lab ID: 92422048005 Collected: 03/20/19 10:36 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260D MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 04/01 /2019 06:18 PM
Analytical Method: EPA 8260D
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
96 %
73 %
108 %
Analytical Method: EPA 8260D Mod
ND ug/L
120 %
109 %
1.0
1
03/27/19 05:19
78-87-5
1.0
1
03/27/19 05:19
10061-01-5
1.0
1
03/27/19 05:19
10061-02-6
1.0
1
03/27/19 05:19
100-41-4
5.0
1
03/27/19 05:19
591-78-6
20.0
1
03/27/19 05:19
74-88-4
5.0
1
03/27/19 05:19
75-09-2
5.0
1
03/27/19 05:19
108-10-1
1.0
1
03/27/19 05:19
100-42-5
1.0
1
03/27/19 05:19
630-20-6
1.0
1
03/27/19 05:19
79-34-5
1.0
1
03/27/19 05:19
127-18-4
1.0
1
03/27/19 05:19
108-88-3
1.0
1
03/27/19 05:19
71-55-6
1.0
1
03/27/19 05:19
79-00-5
1.0
1
03/27/19 05:19
79-01-6
1.0
1
03/27/19 05:19
75-69-4
1.0
1
03/27/19 05:19
96-18-4
2.0
1
03/27/19 05:19
108-05-4
1.0
1
03/27/19 05:19
75-01-4
1.0
1
03/27/19 05:19
1330-20-7
2.0
1
03/27/19 05:19
179601-23-1
1.0
1
03/27/19 05:19
95-47-6
70-130 1
70-130 1
70-130 1
2.0 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
03/27/19 05:19 460-00-4
03/27/19 05:19 17060-07-0
03/27/19 05:19 2037-26-5
03/29/19 14:11 123-91-1
03/29/19 14:11 17060-07-0
03/29/19 14:11 2037-26-5
Page 13 of 30

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ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: TRIP BLANK Lab ID: 92422048006 Collected: 03/20/19 10:41 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 02:15
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 02:15
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 02:15
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 02:15
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 02:15
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 02:15
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 02:15
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 02:15
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 02:15
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 02:15
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 02:15
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 02:15
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 02:15
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 02:15
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 02:15
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 02:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 02:15
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 02:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 02:15
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 02:15
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 02:15
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 02:15
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 02:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:15
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:15
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 02:15
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 02:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 02:15
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 02:15
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 02:15
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 02:15
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 02:15
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 02:15
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 02:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 02:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 02:15
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 02:15
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 02:15
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 02:15
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 02:15
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 02:15
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 02:15
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 02:15
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 02:15
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 02:15
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 02:15
1330-20-7
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM
without
the written consent
of Pace Analytical Services, LLC.
Page 14 of 30

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ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
Sample: TRIP BLANK
Lab ID: 92422048006 Collected: 03/20/19 10:41
Received: 03/20/19 14:56 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
m&p-Xylene
ND ug/L
2.0
1
03/27/19 02:15
179601-23-1
o-Xylene
ND ug/L
1.0
1
03/27/19 02:15
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96 %
70-130
1
03/27/19 02:15
460-00-4
1,2-Dichloroethane-d4 (S)
72 %
70-130
1
03/27/19 02:15
17060-07-0
Toluene-d8 (S)
108 %
70-130
1
03/27/19 02:15
2037-26-5
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 30

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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
QC Batch: 465869 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92422048001, 92422048002, 92422048003, 92422048004, 92422048005
METHOD BLANK: 2532732 Matrix: Water
Associated Lab Samples: 92422048001, 92422048002, 92422048003, 92422048004, 92422048005
Blank Reporting
Parameter Units Result Limit Analyzed
Antimony
ug/L
ND
5.0
03/28/19 21:03
Arsenic
ug/L
ND
10.0
03/28/19 21:03
Barium
ug/L
ND
5.0
03/28/19 21:03
Beryllium
ug/L
ND
1.0
03/28/19 21:03
Cadmium
ug/L
ND
1.0
03/28/19 21:03
Chromium
ug/L
ND
5.0
03/28/19 21:03
Cobalt
ug/L
ND
5.0
03/28/19 21:03
Copper
ug/L
ND
5.0
03/28/19 21:03
Lead
ug/L
ND
5.0
03/28/19 21:03
Nickel
ug/L
ND
5.0
03/28/19 21:03
Selenium
ug/L
ND
10.0
03/28/19 21:03
Silver
ug/L
ND
5.0
03/28/19 21:03
Thallium
ug/L
ND
10.0
03/28/19 21:03
Vanadium
ug/L
ND
5.0
03/28/19 21:03
Zinc
ug/L
ND
10.0
03/28/19 21:03
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2532733
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
456
91
80-120
Arsenic
ug/L
500
441
88
80-120
Barium
ug/L
500
453
91
80-120
Beryllium
ug/L
500
453
91
80-120
Cadmium
ug/L
500
459
92
80-120
Chromium
ug/L
500
456
91
80-120
Cobalt
ug/L
500
453
91
80-120
Copper
ug/L
500
461
92
80-120
Lead
ug/L
500
445
89
80-120
Nickel
ug/L
500
448
90
80-120
Selenium
ug/L
500
456
91
80-120
Silver
ug/L
250
233
93
80-120
Thallium
ug/L
500
437
87
80-120
Vanadium
ug/L
500
451
90
80-120
Zinc
ug/L
500
452
90
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 30

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QUALITY CONTROL DATA
Project:
Pace Project No.:
HOLBROOKS ROAD LANDFILL
92422048
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2532734
2532735
MS
MSD
92422047001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
476
471
95
94
75-125
1
Arsenic
ug/L
ND
500
500
459
453
92
91
75-125
1
Barium
ug/L
33.5
500
500
508
497
95
93
75-125
2
Beryllium
ug/L
ND
500
500
480
470
96
94
75-125
2
Cadmium
ug/L
ND
500
500
482
477
96
95
75-125
1
Chromium
ug/L
ND
500
500
479
474
96
95
75-125
1
Cobalt
ug/L
ND
500
500
467
461
93
92
75-125
1
Copper
ug/L
ND
500
500
476
470
95
94
75-125
1
Lead
ug/L
ND
500
500
461
454
92
91
75-125
2
Nickel
ug/L
ND
500
500
466
459
93
92
75-125
1
Selenium
ug/L
ND
500
500
488
483
97
96
75-125
1
Silver
ug/L
ND
250
250
243
242
97
97
75-125
0
Thallium
ug/L
ND
500
500
454
447
91
89
75-125
2
Vanadium
ug/L
ND
500
500
472
469
94
94
75-125
1
Zinc
ug/L
ND
500
500
480
471
96
94
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 30

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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
QC Batch: 465907
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92422048001, 92422048002,
92422048003, 92422048004, 92422048005
METHOD BLANK: 2532820
Matrix: Water
Associated Lab Samples: 92422048001, 92422048002,
92422048003, 92422048004, 92422048005
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Thallium ug/L
ND 0.10 03/28/19 23:04
LABORATORY CONTROL SAMPLE: 2532821
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Thallium ug/L
10 9.7 97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2532822 2532823
MS MSD
92422253001
Spike Spike MS MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND
10 10 9.1 9.0 91 90 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 30

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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
QC Batch: 465536 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92422048001, 92422048002, 92422048003, 92422048004, 92422048005, 92422048006
METHOD BLANK: 2531202 Matrix: Water
Associated Lab Samples: 92422048001, 92422048002, 92422048003, 92422048004, 92422048005, 92422048006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,1-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
1,2,3-Trichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
03/27/19 01:20
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,4-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
2-Butanone (MEK)
ug/L
ND
5.0
03/27/19 01:20
2-Hexanone
ug/L
ND
5.0
03/27/19 01:20
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/27/19 01:20
Acetone
ug/L
ND
25.0
03/27/19 01:20
Acrylonitrile
ug/L
ND
10.0
03/27/19 01:20
Benzene
ug/L
ND
1.0
03/27/19 01:20
Bromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromodichloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromoform
ug/L
ND
1.0
03/27/19 01:20
Bromomethane
ug/L
ND
2.0
03/27/19 01:20
Carbon disulfide
ug/L
ND
2.0
03/27/19 01:20
Carbon tetrachloride
ug/L
ND
1.0
03/27/19 01:20
Chlorobenzene
ug/L
ND
1.0
03/27/19 01:20
Chloroethane
ug/L
ND
1.0
03/27/19 01:20
Chloroform
ug/L
ND
5.0
03/27/19 01:20
Chloromethane
ug/L
ND
1.0
03/27/19 01:20
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
Dibromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Dibromomethane
ug/L
ND
1.0
03/27/19 01:20
Ethylbenzene
ug/L
ND
1.0
03/27/19 01:20
lodomethane
ug/L
ND
20.0
03/27/19 01:20
m&p-Xylene
ug/L
ND
2.0
03/27/19 01:20
Methylene Chloride
ug/L
ND
5.0
03/27/19 01:20
o-Xylene
ug/L
ND
1.0
03/27/19 01:20
Styrene
ug/L
ND
1.0
03/27/19 01:20
Tetrachloroethene
ug/L
ND
1.0
03/27/19 01:20
Toluene
ug/L
ND
1.0
03/27/19 01:20
v3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 30

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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
METHOD BLANK: 2531202 Matrix: Water
Associated Lab Samples: 92422048001, 92422048002, 92422048003, 92422048004, 92422048005, 92422048006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/27/19 01:20
Trichloroethene
ug/L
ND
1.0
03/27/19 01:20
Trichlorofluoromethane
ug/L
ND
1.0
03/27/19 01:20
Vinyl acetate
ug/L
ND
2.0
03/27/19 01:20
Vinyl chloride
ug/L
ND
1.0
03/27/19 01:20
Xylene (Total)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane-d4 (S)
%
76
70-130
03/27/19 01:20
4-Bromofluorobenzene (S)
%
97
70-130
03/27/19 01:20
Toluene-d8 (S)
%
103
70-130
03/27/19 01:20
LABORATORY CONTROL SAMPLE:
Parameter
2531203
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.2
106
70-130
1,1,1-Trichloroethane
ug/L
50
45.7
91
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
47.3
95
70-130
1,1,2-Trichloroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethane
ug/L
50
47.8
96
70-130
1,1-Dichloroethene
ug/L
50
46.8
94
70-130
1,2,3-Trichloropropane
ug/L
50
36.5
73
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
46.1
92
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.5
101
70-130
1,2-Dichlorobenzene
ug/L
50
46.7
93
70-130
1,2-Dichloroethane
ug/L
50
41.5
83
70-130
1,2-Dichloropropane
ug/L
50
53.4
107
70-130
1,4-Dichlorobenzene
ug/L
50
47.3
95
70-130
2-Butanone (MEK)
ug/L
100
98.8
99
64-135
2-Hexanone
ug/L
100
89.7
90
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
86.0
86
70-130
Acetone
ug/L
100
90.4
90
61-157
Acrylonitrile
ug/L
250
246
99
61-143
Benzene
ug/L
50
50.6
101
70-130
Bromochloromethane
ug/L
50
49.5
99
70-130
Bromodichloromethane
ug/L
50
49.8
100
70-130
Bromoform
ug/L
50
49.9
100
70-130
Bromomethane
ug/L
50
31.0
62
38-130 v3
Carbon disulfide
ug/L
50
47.8
96
68-130
Carbon tetrachloride
ug/L
50
45.5
91
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
50.6
101
37-142
Chloroform
ug/L
50
43.3
87
70-130
Chloromethane
ug/L
50
50.2
100
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
LABORATORY CONTROL SAMPLE:
2531203
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
47.7
95
70-130
cis-1,3-Dichloropropene
ug/L
50
50.6
101
70-130
Dibromochloromethane
ug/L
50
51.7
103
70-130
Dibromomethane
ug/L
50
49.2
98
70-130
Ethylbenzene
ug/L
50
48.4
97
70-130
lodomethane
ug/L
100
97.7
98
40-130
m&p-Xylene
ug/L
100
98.0
98
70-130
Methylene Chloride
ug/L
50
45.6
91
67-132
o-Xylene
ug/L
50
50.4
101
70-131
Styrene
ug/L
50
50.2
100
70-130
Tetrachloroethene
ug/L
50
49.3
99
69-130
Toluene
ug/L
50
45.7
91
70-130
trans-1,2-Dichloroethene
ug/L
50
48.0
96
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.9
100
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
53.8
108
35-189
Trichloroethene
ug/L
50
50.0
100
70-130
Trichlorofluoromethane
ug/L
50
44.2
88
63-130
Vinyl acetate
ug/L
100
88.7
89
55-143
Vinyl chloride
ug/L
50
53.1
106
70-131
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
86
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.4
102
73-134
1,1,1-Trichloroethane
ug/L
ND
20
18.4
92
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.1
95
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.4
97
70-135
1,1-Dichloroethane
ug/L
ND
20
19.3
97
70-139
1,1-Dichloroethene
ug/L
ND
20
19.4
97
70-154
1,2,3-Trichloropropane
ug/L
ND
20
18.4
92
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.4
87
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.2
96
70-137
1,2-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
1,2-Dichloroethane
ug/L
ND
20
16.7
84
70-137
1,2-Dichloropropene
ug/L
ND
20
20.5
102
70-140
1,4-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
2-Butanone (MEK)
ug/L
ND
40
35.6
89
60-139
2-Hexanone
ug/L
ND
40
34.7
87
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
35.1
88
65-135
Acetone
ug/L
ND
40
36.6
92
60-148
Acrylonitrile
ug/L
ND
100
95.6
96
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
20.7
103
70-151
Bromochloromethane
ug/L
ND
20
19.8
99
70-141
Bromodichloromethane
ug/L
ND
20
18.6
93
70-138
Bromoform
ug/L
ND
20
18.8
94
63-130
Bromomethane
ug/L
ND
20
12.7
64
15-152 v3
Carbon disulfide
ug/L
ND
20
19.8
99
69-149
Carbon tetrachloride
ug/L
ND
20
19.1
95
70-143
Chlorobenzene
ug/L
ND
20
20.6
103
70-138
Chloroethane
ug/L
ND
20
21.2
106
52-163
Chloroform
ug/L
ND
20
17.2
86
70-139
Chloromethane
ug/L
ND
20
20.6
103
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
19.2
96
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
18.3
91
70-137
Dibromochloromethane
ug/L
ND
20
19.0
95
70-134
Dibromomethane
ug/L
ND
20
19.3
97
70-138
Ethylbenzene
ug/L
ND
20
20.3
101
66-153
lodomethane
ug/L
ND
40
38.6
97
20-138
m&p-Xylene
ug/L
ND
40
41.0
103
69-152
Methylene Chloride
ug/L
ND
20
18.5
92
42-159
o-Xylene
ug/L
ND
20
20.4
102
70-148
Styrene
ug/L
ND
20
19.8
99
70-135
Tetrachloroethene
ug/L
ND
20
20.5
102
59-143
Toluene
ug/L
ND
20
19.8
99
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
18.9
94
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
17.9
90
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
13.6
68
47-135
Trichloroethene
ug/L
ND
20
20.5
102
70-147
Trichlorofluoromethane
ug/L
ND
20
19.4
97
70-148
Vinyl acetate
ug/L
ND
40
21.7
54
49-151
Vinyl chloride
ug/L
ND
20
22.8
114
70-156
Xylene (Total)
ug/L
ND
60
61.4
102
63-158
1,2-Dichloroethane-d4 (S)
%
83
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2531204
92422047001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Page 22 of 30

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
SAMPLE DUPLICATE: 2531204
Parameter
Units
92422047001
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
79
78
4-Bromofluorobenzene (S)
%
96
96
Toluene-d8 (S)
%
104
103
RPD Qualifiers
v3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
QC Batch: 465021 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Associated Lab Samples: 92422048001, 92422048002, 92422048003
METHOD BLANK: 2529043
Matrix:
Water
Associated Lab Samples:
92422048001, 92422048002, 92422048003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
03/25/19 19:23
1,2-Dichloroethane-d4 (S)
%
92
50-150
03/25/19 19:23
Toluene-d8 (S)
%
98
50-150
03/25/19 19:23
LABORATORY CONTROL SAMPLE: 2529044
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 20.3 102 71-125
1,2-Dichloroethane-d4 (S) % 96 50-150
Toluene-d8(S) % 98 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2529045
2529046
MS
MSD
92422048003 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 17.2
17.4 81
82
50-150 1
1,2-Dichloroethane-d4 (S)
%
97
92
50-150
Toluene-d8(S)
%
96
96
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
QC Batch: 466277 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Associated Lab Samples: 92422048004, 92422048005
METHOD BLANK: 2534467
Associated Lab Samples: 92422048004, 92422048005
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit
Analyzed
ND 2.0
03/29/1913:32
115 50-150
03/29/1913:32
106 50-150
03/29/1913:32
Qualifiers
LABORATORY CONTROL SAMPLE: 2534468
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.4 97 71-125
1,2-Dichloroethane-d4 (S) % 121 50-150
Toluene-d8(S) % 107 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2534469
2534470
MS
MSD
92422048004 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 23.6
19.1 112
90
50-150 21
1,2-Dichloroethane-d4 (S)
%
101
98
50-150
Toluene-d8(S)
%
102
101
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422048
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HOLBROOKS ROAD LANDFILL
92422048
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92422048001
HRW-7
EPA 3010A
465869
EPA6010D
466009
92422048002
HRW18
EPA 3010A
465869
EPA6010D
466009
92422048003
HRW19
EPA 3010A
465869
EPA6010D
466009
92422048004
HRW20
EPA 3010A
465869
EPA6010D
466009
92422048005
HRW21
EPA 3010A
465869
EPA6010D
466009
92422048001
HRW-7
EPA 3010A
465907
EPA 6020B
466015
92422048002
HRW18
EPA 3010A
465907
EPA 6020B
466015
92422048003
HRW19
EPA 3010A
465907
EPA 6020B
466015
92422048004
HRW20
EPA 3010A
465907
EPA 6020B
466015
92422048005
HRW21
EPA 3010A
465907
EPA 6020B
466015
92422048001
HRW-7
EPA 8260D
465536
92422048002
HRW18
EPA 8260D
465536
92422048003
HRW19
EPA 8260D
465536
92422048004
HRW20
EPA 8260D
465536
92422048005
HRW21
EPA 8260D
465536
92422048006
TRIP BLANK
EPA 8260D
465536
92422048001
HRW-7
EPA 8260D Mod.
465021
92422048002
HRW18
EPA 8260D Mod.
465021
92422048003
HRW19
EPA 8260D Mod.
465021
92422048004
HRW20
EPA 8260D Mod.
466277
92422048005
HRW21
EPA 8260D Mod.
466277
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 30

Document Name: Document Revised: February 7, 2018
m Sample Condition Upon Receipt(SCUR) Page i of 2
aceARaVida! Document No.: Issuing Authority:
+ F•CAR•CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville ❑" Raleigh[] Mechanicsville[]
• • Client Name: wo# : 92422048
U-pon Receipt,�,} 'i Iojett I
Courier: ❑Fed Ex []UPS ❑USPS ❑CI en1� a
❑ Commercial []Pace ❑Other: 9242204
_f
Custody Seal Present? []Yes []No Seals Intact? ❑Yes ❑No ~
Datelinitials person Examining Contents:
Packing Material: ]Bubble wrap []Bubble Bags (]None ❑ Other. Biological Tissue Frozen?
[]Yes []No []N/A
Thermometer: Type of ice: pwet ❑Blue ❑None
SR Gun ID. 92Ta48
Cooler Temp (°C): Correction Factor: Add/Subtract (•C) 0.0
' Temp should be above freezing to 6°C
Cooler Temp Corrected (°C): ❑5arnples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (D/N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps? Did samples originate from a foreign source (internationally, .
I V-1 f-t�,,, including Hawaii and PuertoRlco)? Dyes []No
Chain of Custody Present?
5arnplesArfived within Hold Time? . .
Short Hold, Time Analysis (�72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CDC?
-Includes Date/Time/ID/Analysis
Headspace in VOA Vials (>5-6mm)?
Trip Blank Present?
Trio Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
[]No
❑N/A
1.
ONO
❑N/A
2.
❑No
❑N/A
3.
6o
❑N/A
4.
❑No
❑N/A
5.
[:]No
❑NIA
6.
ees ❑No ❑N/A 7.
i
Yes ❑No ❑NIA g•
;es []No ❑N/A 9.
❑No ❑N/A 10.
❑No ❑N/A 11.
i
nNO I1rl/A
Field Data Required? []Yes []NO
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:'
Project Manager SRF Review:
DatejTlme:
Date:
Date: . ? i
Page 28 of 30

Document Name:
r Sample Condition Upon Rec
'Cal Document No.:
F-CAR-CS-033-Rev.1
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
"
CP
=
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Project I W®# ; 92422048
PM: MWB Due Date: 04/03/19
CLIENT: 92-MECK CO
pH Adjustment Log for Preserved Samples
5ample 10 Type of Preservative pH upon receipt Elate preservation adjusted Tim adjust elation Amount added of Preservative
Note: Whenever there is a discrepancy affecting North Carolina compliance samptes, a ccpy of this form wllV he sent to the North Carolina OEHNR
Out of hold, incorrect preservative, out of temp, incorrect containers.
Lot a
Office li.e.
Page 29 of 30

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Page 30 of 30

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 01, 2019
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 21, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 24

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 24

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Holbrooks Road Landfill
92422267
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92422267001
HRW10
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422267002
HRW11R
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422267003
HRW13
EPA 6010D
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 24

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Sample: HRW10 Lab ID: 92422267001 Collected: 03/21/19 11:15 Received: 03/21/19 13:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:46
7440-38-2
Barium
150
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:46
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:46
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-48-4
Copper
9.0
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7439-92-1
Nickel
13.0
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:46
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:46
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:46
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:46
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 04:56
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 06:33
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 06:33
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 06:33
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 06:33
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 06:33
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 06:33
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 06:33
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 06:33
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 06:33
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 06:33
56-23-5
Chlorobenzene
1.1
ug/L
1.0
1
03/27/19 06:33
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 06:33
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 06:33
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 06:33
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 06:33
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 06:33
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 06:33
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 06:33
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 06:33
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 06:33
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 06:33
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 06:33
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 06:33
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:33
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:33
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:33
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 24

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Sample: HRW10 Lab ID: 92422267001 Collected: 03/21/19 11:15 Received: 03/21/19 13:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 06:33
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 06:33
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 06:33
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 06:33
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 06:33
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 06:33
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 06:33
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 06:33
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 06:33
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 06:33
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 06:33
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 06:33
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 06:33
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 06:33
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 06:33
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 06:33
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 06:33
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 06:33
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 06:33
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 06:33
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 06:33
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 06:33
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 06:33
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
03/27/19 06:33
460-00-4
1,2-Dichloroethane-d4 (S)
73
%
70-130
1
03/27/19 06:33
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
03/27/19 06:33
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
13.1
ug/L
2.0
1
03/26/19 23:03
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
50-150
1
03/26/19 23:03
17060-07-0
Toluene-d8 (S)
97
%
50-150
1
03/26/19 23:03
2037-26-5
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 24

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Sample: HRW11R Lab ID: 92422267002 Collected: 03/21/19 10:32 Received: 03/21/19 13:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:49
7440-38-2
Barium
153
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:49
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:49
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-48-4
Copper
8.0
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7439-92-1
Nickel
13.0
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:49
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:49
7440-28-0
Vanadium
6.5
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:49
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:49
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 04:59
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 06:51
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 06:51
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 06:51
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 06:51
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 06:51
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 06:51
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 06:51
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 06:51
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 06:51
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 06:51
56-23-5
Chlorobenzene
2.6
ug/L
1.0
1
03/27/19 06:51
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 06:51
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 06:51
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 06:51
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 06:51
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 06:51
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 06:51
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 06:51
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 06:51
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 06:51
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 06:51
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 06:51
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 06:51
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:51
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:51
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Sample: HRW11R Lab ID: 92422267002 Collected: 03/21/19 10:32 Received: 03/21/19 13:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 06:51
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 06:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 06:51
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 06:51
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 06:51
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 06:51
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 06:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 06:51
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 06:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 06:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 06:51
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 06:51
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 06:51
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 06:51
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 06:51
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 06:51
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 06:51
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 06:51
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 06:51
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 06:51
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 06:51
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 06:51
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 06:51
95-47-6
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
03/27/19 06:51
460-00-4
1,2-Dichloroethane-d4 (S)
75
%
70-130
1
03/27/19 06:51
17060-07-0
Toluene-d8 (S)
107
%
70-130
1
03/27/19 06:51
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
42.2
ug/L
2.0
1
03/27/19 14:57
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
50-150
1
03/27/19 14:57
17060-07-0
Toluene-d8 (S)
98
%
50-150
1
03/27/19 14:57
2037-26-5
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 24

aceAnalytical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Sample: HRW13 Lab ID: 92422267003 Collected: 03/21/19 10:55 Received: 03/21/19 13:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:52
7440-38-2
Barium
109
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:52
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:52
7440-43-9
Chromium
6.0
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-48-4
Copper
9.7
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:52
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:52
7440-28-0
Vanadium
9.5
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:52
7440-62-2
Zinc
11.4
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:52
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 05:03
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 07:10
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 07:10
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 07:10
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 07:10
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 07:10
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 07:10
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 07:10
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 07:10
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 07:10
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 07:10
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 07:10
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 07:10
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 07:10
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 07:10
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 07:10
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 07:10
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 07:10
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 07:10
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 07:10
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 07:10
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 07:10
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 07:10
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 07:10
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 07:10
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 07:10
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 07:10
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
Sample: HRW13 Lab ID: 92422267003 Collected: 03/21/19 10:55 Received: 03/21/19 13:09 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 07:10
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 07:10
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 07:10
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 07:10
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 07:10
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 07:10
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 07:10
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 07:10
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 07:10
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 07:10
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 07:10
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 07:10
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 07:10
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 07:10
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 07:10
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 07:10
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 07:10
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 07:10
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 07:10
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 07:10
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 07:10
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 07:10
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 07:10
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
03/27/19 07:10
460-00-4
1,2-Dichloroethane-d4 (S)
76
%
70-130
1
03/27/19 07:10
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
03/27/19 07:10
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 23:23
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
94
%
50-150
1
03/26/19 23:23
17060-07-0
Toluene-d8 (S)
97
%
50-150
1
03/26/19 23:23
2037-26-5
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
QC Batch: 465869 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92422267001, 92422267002, 92422267003
METHOD BLANK: 2532732 Matrix: Water
Associated Lab Samples: 92422267001, 92422267002, 92422267003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
1.0
03/28/19 21:03
1.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2532733
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
456
91
80-120
Arsenic
ug/L
500
441
88
80-120
Barium
ug/L
500
453
91
80-120
Beryllium
ug/L
500
453
91
80-120
Cadmium
ug/L
500
459
92
80-120
Chromium
ug/L
500
456
91
80-120
Cobalt
ug/L
500
453
91
80-120
Copper
ug/L
500
461
92
80-120
Lead
ug/L
500
445
89
80-120
Nickel
ug/L
500
448
90
80-120
Selenium
ug/L
500
456
91
80-120
Silver
ug/L
250
233
93
80-120
Thallium
ug/L
500
437
87
80-120
Vanadium
ug/L
500
451
90
80-120
Zinc
ug/L
500
452
90
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
Holbrooks Road Landfill
92422267
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2532734
2532735
MS
MSD
92422047001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
476
471
95
94
75-125
1
Arsenic
ug/L
ND
500
500
459
453
92
91
75-125
1
Barium
ug/L
33.5
500
500
508
497
95
93
75-125
2
Beryllium
ug/L
ND
500
500
480
470
96
94
75-125
2
Cadmium
ug/L
ND
500
500
482
477
96
95
75-125
1
Chromium
ug/L
ND
500
500
479
474
96
95
75-125
1
Cobalt
ug/L
ND
500
500
467
461
93
92
75-125
1
Copper
ug/L
ND
500
500
476
470
95
94
75-125
1
Lead
ug/L
ND
500
500
461
454
92
91
75-125
2
Nickel
ug/L
ND
500
500
466
459
93
92
75-125
1
Selenium
ug/L
ND
500
500
488
483
97
96
75-125
1
Silver
ug/L
ND
250
250
243
242
97
97
75-125
0
Thallium
ug/L
ND
500
500
454
447
91
89
75-125
2
Vanadium
ug/L
ND
500
500
472
469
94
94
75-125
1
Zinc
ug/L
ND
500
500
480
471
96
94
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
QC Batch: 465908
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92422267001, 92422267002,
92422267003
METHOD BLANK: 2532824
Matrix: Water
Associated Lab Samples: 92422267001, 92422267002,
92422267003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Thallium ug/L
ND 0.10
03/29/19 03:27
LABORATORY CONTROL SAMPLE: 2532825
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Thallium ug/L
10 9.5
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2532826 2532827
MS MSD
92422137001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND
10 10 8.5
8.7 84 87 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 24

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
QC Batch: 465536 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92422267001, 92422267002, 92422267003
METHOD BLANK: 2531202 Matrix:
Associated Lab Samples: 92422267001, 92422267002, 92422267003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,1-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
1,2,3-Trichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
03/27/19 01:20
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,4-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
2-Butanone (MEK)
ug/L
ND
5.0
03/27/19 01:20
2-Hexanone
ug/L
ND
5.0
03/27/19 01:20
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/27/19 01:20
Acetone
ug/L
ND
25.0
03/27/19 01:20
Acrylonitrile
ug/L
ND
10.0
03/27/19 01:20
Benzene
ug/L
ND
1.0
03/27/19 01:20
Bromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromodichloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromoform
ug/L
ND
1.0
03/27/19 01:20
Bromomethane
ug/L
ND
2.0
03/27/19 01:20
Carbon disulfide
ug/L
ND
2.0
03/27/19 01:20
Carbon tetrachloride
ug/L
ND
1.0
03/27/19 01:20
Chlorobenzene
ug/L
ND
1.0
03/27/19 01:20
Chloroethane
ug/L
ND
1.0
03/27/19 01:20
Chloroform
ug/L
ND
5.0
03/27/19 01:20
Chloromethane
ug/L
ND
1.0
03/27/19 01:20
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
Dibromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Dibromomethane
ug/L
ND
1.0
03/27/19 01:20
Ethylbenzene
ug/L
ND
1.0
03/27/19 01:20
lodomethane
ug/L
ND
20.0
03/27/19 01:20
m&p-Xylene
ug/L
ND
2.0
03/27/19 01:20
Methylene Chloride
ug/L
ND
5.0
03/27/19 01:20
o-Xylene
ug/L
ND
1.0
03/27/19 01:20
Styrene
ug/L
ND
1.0
03/27/19 01:20
Tetrachloroethene
ug/L
ND
1.0
03/27/19 01:20
Toluene
ug/L
ND
1.0
03/27/19 01:20
v3
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 24

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
METHOD BLANK: 2531202
Matrix:
Water
Associated Lab Samples: 92422267001, 92422267002, 92422267003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/27/19 01:20
Trichloroethene
ug/L
ND
1.0
03/27/19 01:20
Trichlorofluoromethane
ug/L
ND
1.0
03/27/19 01:20
Vinyl acetate
ug/L
ND
2.0
03/27/19 01:20
Vinyl chloride
ug/L
ND
1.0
03/27/19 01:20
Xylene (Total)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane-d4 (S)
%
76
70-130
03/27/19 01:20
4-Bromofluorobenzene (S)
%
97
70-130
03/27/19 01:20
Toluene-d8 (S)
%
103
70-130
03/27/19 01:20
LABORATORY CONTROL SAMPLE:
2531203
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.2
106
70-130
1,1,1-Trichloroethane
ug/L
50
45.7
91
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
47.3
95
70-130
1,1,2-Trichloroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethane
ug/L
50
47.8
96
70-130
1,1-Dichloroethene
ug/L
50
46.8
94
70-130
1,2,3-Trichloropropane
ug/L
50
36.5
73
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
46.1
92
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.5
101
70-130
1,2-Dichlorobenzene
ug/L
50
46.7
93
70-130
1,2-Dichloroethane
ug/L
50
41.5
83
70-130
1,2-Dichloropropane
ug/L
50
53.4
107
70-130
1,4-Dichlorobenzene
ug/L
50
47.3
95
70-130
2-Butanone (MEK)
ug/L
100
98.8
99
64-135
2-Hexanone
ug/L
100
89.7
90
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
86.0
86
70-130
Acetone
ug/L
100
90.4
90
61-157
Acrylonitrile
ug/L
250
246
99
61-143
Benzene
ug/L
50
50.6
101
70-130
Bromochloromethane
ug/L
50
49.5
99
70-130
Bromodichloromethane
ug/L
50
49.8
100
70-130
Bromoform
ug/L
50
49.9
100
70-130
Bromomethane
ug/L
50
31.0
62
38-130 v3
Carbon disulfide
ug/L
50
47.8
96
68-130
Carbon tetrachloride
ug/L
50
45.5
91
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
50.6
101
37-142
Chloroform
ug/L
50
43.3
87
70-130
Chloromethane
ug/L
50
50.2
100
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 24

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
LABORATORY CONTROL SAMPLE:
2531203
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
47.7
95
70-130
cis-1,3-Dichloropropene
ug/L
50
50.6
101
70-130
Dibromochloromethane
ug/L
50
51.7
103
70-130
Dibromomethane
ug/L
50
49.2
98
70-130
Ethylbenzene
ug/L
50
48.4
97
70-130
lodomethane
ug/L
100
97.7
98
40-130
m&p-Xylene
ug/L
100
98.0
98
70-130
Methylene Chloride
ug/L
50
45.6
91
67-132
o-Xylene
ug/L
50
50.4
101
70-131
Styrene
ug/L
50
50.2
100
70-130
Tetrachloroethene
ug/L
50
49.3
99
69-130
Toluene
ug/L
50
45.7
91
70-130
trans-1,2-Dichloroethene
ug/L
50
48.0
96
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.9
100
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
53.8
108
35-189
Trichloroethene
ug/L
50
50.0
100
70-130
Trichlorofluoromethane
ug/L
50
44.2
88
63-130
Vinyl acetate
ug/L
100
88.7
89
55-143
Vinyl chloride
ug/L
50
53.1
106
70-131
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
86
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.4
102
73-134
1,1,1-Trichloroethane
ug/L
ND
20
18.4
92
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.1
95
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.4
97
70-135
1,1-Dichloroethane
ug/L
ND
20
19.3
97
70-139
1,1-Dichloroethene
ug/L
ND
20
19.4
97
70-154
1,2,3-Trichloropropane
ug/L
ND
20
18.4
92
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.4
87
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.2
96
70-137
1,2-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
1,2-Dichloroethane
ug/L
ND
20
16.7
84
70-137
1,2-Dichloropropene
ug/L
ND
20
20.5
102
70-140
1,4-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
2-Butanone (MEK)
ug/L
ND
40
35.6
89
60-139
2-Hexanone
ug/L
ND
40
34.7
87
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
35.1
88
65-135
Acetone
ug/L
ND
40
36.6
92
60-148
Acrylonitrile
ug/L
ND
100
95.6
96
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 24

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
20.7
103
70-151
Bromochloromethane
ug/L
ND
20
19.8
99
70-141
Bromodichloromethane
ug/L
ND
20
18.6
93
70-138
Bromoform
ug/L
ND
20
18.8
94
63-130
Bromomethane
ug/L
ND
20
12.7
64
15-152 v3
Carbon disulfide
ug/L
ND
20
19.8
99
69-149
Carbon tetrachloride
ug/L
ND
20
19.1
95
70-143
Chlorobenzene
ug/L
ND
20
20.6
103
70-138
Chloroethane
ug/L
ND
20
21.2
106
52-163
Chloroform
ug/L
ND
20
17.2
86
70-139
Chloromethane
ug/L
ND
20
20.6
103
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
19.2
96
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
18.3
91
70-137
Dibromochloromethane
ug/L
ND
20
19.0
95
70-134
Dibromomethane
ug/L
ND
20
19.3
97
70-138
Ethylbenzene
ug/L
ND
20
20.3
101
66-153
lodomethane
ug/L
ND
40
38.6
97
20-138
m&p-Xylene
ug/L
ND
40
41.0
103
69-152
Methylene Chloride
ug/L
ND
20
18.5
92
42-159
o-Xylene
ug/L
ND
20
20.4
102
70-148
Styrene
ug/L
ND
20
19.8
99
70-135
Tetrachloroethene
ug/L
ND
20
20.5
102
59-143
Toluene
ug/L
ND
20
19.8
99
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
18.9
94
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
17.9
90
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
13.6
68
47-135
Trichloroethene
ug/L
ND
20
20.5
102
70-147
Trichlorofluoromethane
ug/L
ND
20
19.4
97
70-148
Vinyl acetate
ug/L
ND
40
21.7
54
49-151
Vinyl chloride
ug/L
ND
20
22.8
114
70-156
Xylene (Total)
ug/L
ND
60
61.4
102
63-158
1,2-Dichloroethane-d4 (S)
%
83
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2531204
92422047001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 24

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
SAMPLE DUPLICATE: 2531204
Parameter
Units
92422047001
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
79
78
4-Bromofluorobenzene (S)
%
96
96
Toluene-d8 (S)
%
104
103
RPD Qualifiers
v3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 24

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
QC Batch: 465409 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Associated Lab Samples: 92422267001, 92422267003
METHOD BLANK: 2530510
Associated Lab Samples: 92422267001, 92422267003
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit
Analyzed
ND 2.0
03/26/1913:37
91 50-150
03/26/1913:37
96 50-150
03/26/1913:37
Qualifiers
LABORATORY CONTROL SAMPLE: 2530511
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 19.7 98 71-125
1,2-Dichloroethane-d4 (S) % 90 50-150
Toluene-d8(S) % 95 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2530512
2530513
MS
MSD
92422294007 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 1.5J 20
20 19.3
17.8 89
81
50-150 8
1,2-Dichloroethane-d4 (S)
%
90
94
50-150
Toluene-d8(S)
%
95
98
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
QC Batch: 465652 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Associated Lab Samples: 92422267002
METHOD BLANK: 2531703
Associated Lab Samples: 92422267002
Parameter
Units
1,4-Dioxane (p-Dioxane)
ug/L
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 03/27/1910:45
90 50-150 03/27/1910:45
96 50-150 03/27/1910:45
LABORATORY CONTROL SAMPLE: 2531704
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 19.2 96 71-125
1,2-Dichloroethane-d4 (S) % 93 50-150
Toluene-d8(S) % 96 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2531705 2531706
MS MSD
92422294024 Spike Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc. Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 152 50 50 191
199 77
93
50-150 4
1,2-Dichloroethane-d4 (S)
%
96
96
50-150
Toluene-d8(S)
%
98
97
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: Holbrooks Road Landfill
Pace Project No.: 92422267
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 06:18 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 24

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Holbrooks Road Landfill
92422267
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92422267001
HRW10
EPA 3010A
465869
EPA6010D
466009
92422267002
HRW11R
EPA 3010A
465869
EPA6010D
466009
92422267003
HRW13
EPA 3010A
465869
EPA6010D
466009
92422267001
HRW10
EPA 3010A
465908
EPA6020B
466019
92422267002
HRW11R
EPA 3010A
465908
EPA 6020B
466019
92422267003
HRW13
EPA 3010A
465908
EPA6020B
466019
92422267001
HRW10
EPA 8260D
465536
92422267002
HRW11R
EPA 8260D
465536
92422267003
HRW13
EPA 8260D
465536
92422267001
HRW10
EPA 8260D Mod.
465409
92422267002
HRW11R
EPA 8260D Mod.
465652
92422267003
HRW13
EPA 8260D Mod.
465409
Date: 04/01 /2019 06:18 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 24

Document Name:
Condition Upon Rec
Document No.:
Document Revised: February 7, 2018
Page 1 of 2
issuing Authority:
Pace Carolinas Quai' �#fice
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Hu
Raleigh[] Mechanicsville[]
Simple Condition Client Nam : t WV# ' 9242226 r
Upon Receipt
Project #:
Courier: ❑Fed Ex ❑UPS U❑u5P5 []ClientI� I I� 111 IN III
❑ COmmerClal ❑Pace ❑01 92422267
Custody Seal Present? [—]Yes �_( Seals Intact? []Yes o
Packing Material: []Bubble Wrap on ❑ Other.
Thermo ter; 92TO48 Type of Ice: wet ❑Blue
R Gun 10;
Correction Factor: Add/Subtract (°C) 0,0
Cooler Temp('Q: —7
Cooler Temp Corrected (°C): l —
USDA Regulated Sail (6/A, water sample)
Did saMplerail0dte in a quarantine zone within the United States: CA, NY, or SC {check maps)?
Chain of Custody Present?
es
❑NO
[]N/A
1.
Samples Arrived within Hold Time?
Yes
[]NO
❑N/A
2,
Short Hdld rime Analysts (02 hr.)?
Yes
o
❑N/A
3.
Rush Turn Around Time Requested?
Y s
❑N/A
4.
sufficient Volume?
es
[]No
❑N/A
S.
Correct Containers used?
es
❑No
[]NIA
6.
-Pace Containers Used?
es
❑No
❑N/A
Containers Intact?
es
❑No
❑ /A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
&VA
g•
5ampleLabels Match CDC?
es
[:]No
[]N/A
9.
-Includes Date/Time/ID/Analysis Ivrauix: v
Headspace in VOA Vials (>5-6mm)? [!:]Yes []N/AiQ.
Trip Blank Present? ❑Yes o ❑NIA 11.
Trip Blank Custody Seals Present? ❑yes o ❑N/A
COMMENTS/SAMPLE DISCREPANCY
Date/Initials Person Examining CantentsAgz f
Biological Tis a Frozen?
[]Yes[]NoNSA
❑None
Temp should be above freezing to 6°C
❑5ample5 out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source P nte
^tIonally, .
including Hawaii and Puerto Rico)? ❑Yes N .
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
field Data Required? ❑Yes []NO
Person contacted: Datejrlrne:
i
Project Manager SCURF Review; 7 l �r Date:
� fI%
Project Manager SRF Revlew: f!. Date: 1
Page 22 of 24

Document Name:
Condition Upon Receil
Document No.:
F-CAR-CS-033-Rev.06
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check marls top half of box if pH and/or dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, eoliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project J WQ# f 92422267
PM: MWB Due Dale: 04/04/19
CLIENT: 92—MECK CO
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PH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Rate preservation adJusted Time preservation Amount of Preservative
i I added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm will he sent to the North Carolina DENNR
Out of hold, incorrect preservative, out of temp, incorrect containers.
Lot k
Office (i.e.
Page 23 of 24

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Page 24 of 24

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 01, 2019
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 21, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 25

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 25

aceAnalytical
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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HOLBROOKS ROAD LANDFILL
92422237
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92422237001
HRW8
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422237002
HRW9
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422237003
HRW16
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422237004
TRIP BLANK
EPA 8260D
NSCQ
52
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 25

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: HRW8 Lab ID: 92422237001 Collected: 03/21/19 12:15 Received: 03/21/19 14:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:31
7440-38-2
Barium
93.8
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:31
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:31
7440-43-9
Chromium
9.5
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-47-3
Cobalt
6.6
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-48-4
Copper
18.1
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:31
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:31
7440-28-0
Vanadium
31.4
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:31
7440-62-2
Zinc
21.1
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:31
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 04:38
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 05:38
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 05:38
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 05:38
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 05:38
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 05:38
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 05:38
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 05:38
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 05:38
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 05:38
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 05:38
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 05:38
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 05:38
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 05:38
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 05:38
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 05:38
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 05:38
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 05:38
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 05:38
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 05:38
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 05:38
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 05:38
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 05:38
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 05:38
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:38
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:38
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:38
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 25

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: HRW8 Lab ID: 92422237001 Collected: 03/21/19 12:15 Received: 03/21/19 14:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 05:38
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 05:38
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 05:38
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 05:38
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 05:38
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 05:38
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 05:38
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 05:38
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 05:38
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 05:38
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 05:38
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 05:38
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 05:38
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 05:38
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 05:38
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 05:38
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 05:38
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 05:38
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 05:38
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 05:38
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 05:38
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 05:38
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 05:38
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
03/27/19 05:38
460-00-4
1,2-Dichloroethane-d4 (S)
80
%
70-130
1
03/27/19 05:38
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
03/27/19 05:38
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 22:06
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92
%
50-150
1
03/26/19 22:06
17060-07-0
Toluene-d8 (S)
95
%
50-150
1
03/26/19 22:06
2037-26-5
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 25

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: HRW9 Lab ID: 92422237002 Collected: 03/21/19 11:50 Received: 03/21/19 14:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:40
7440-38-2
Barium
274
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:40
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:40
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:40
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:40
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:40
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:40
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 04:42
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 05:56
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 05:56
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 05:56
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 05:56
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 05:56
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 05:56
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 05:56
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 05:56
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 05:56
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 05:56
56-23-5
Chlorobenzene
2.7
ug/L
1.0
1
03/27/19 05:56
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 05:56
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 05:56
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 05:56
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 05:56
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 05:56
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 05:56
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 05:56
74-95-3
1,2-Dichlorobenzene
7.6
ug/L
1.0
1
03/27/19 05:56
95-50-1
1,4-Dichlorobenzene
11.9
ug/L
1.0
1
03/27/19 05:56
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 05:56
110-57-6
1,1-Dichloroethane
35.0
ug/L
1.0
1
03/27/19 05:56
75-34-3
1,2-Dichloroethane
1.9
ug/L
1.0
1
03/27/19 05:56
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 05:56
75-35-4
cis-1,2-Dichloroethene
77.5
ug/L
1.0
1
03/27/19 05:56
156-59-2
trans-1,2-Dichloroethene
1.4
ug/L
1.0
1
03/27/19 05:56
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 25

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: HRW9 Lab ID: 92422237002 Collected: 03/21/19 11:50 Received: 03/21/19 14:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
2.2
ug/L
1.0
1
03/27/19 05:56
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 05:56
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 05:56
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 05:56
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 05:56
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 05:56
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 05:56
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 05:56
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 05:56
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 05:56
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 05:56
79-34-5
Tetrachloroethene
1.4
ug/L
1.0
1
03/27/19 05:56
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 05:56
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 05:56
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 05:56
79-00-5
Trichloroethene
3.4
ug/L
1.0
1
03/27/19 05:56
79-01-6
Trichlorofluoromethane
3.2
ug/L
1.0
1
03/27/19 05:56
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 05:56
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 05:56
108-05-4
Vinyl chloride
14.1
ug/L
1.0
1
03/27/19 05:56
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 05:56
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 05:56
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 05:56
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
03/27/19 05:56
460-00-4
1,2-Dichloroethane-d4 (S)
83
%
70-130
1
03/27/19 05:56
17060-07-0
Toluene-d8 (S)
106
%
70-130
1
03/27/19 05:56
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
10.2
ug/L
2.0
1
03/26/19 22:25
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
98
%
50-150
1
03/26/19 22:25
17060-07-0
Toluene-d8 (S)
94
%
50-150
1
03/26/19 22:25
2037-26-5
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 25

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: HRW16 Lab ID: 92422237003 Collected: 03/21/19 11:40 Received: 03/21/19 14:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:43
7440-38-2
Barium
159
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:43
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 22:43
7440-43-9
Chromium
11.4
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-48-4
Copper
27.6
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7439-92-1
Nickel
6.0
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:43
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:43
7440-28-0
Vanadium
41.2
ug/L
5.0
1
03/28/19 11:05
03/28/19 22:43
7440-62-2
Zinc
22.8
ug/L
10.0
1
03/28/19 11:05
03/28/19 22:43
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 04:52
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 06:15
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 06:15
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 06:15
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 06:15
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 06:15
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 06:15
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 06:15
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 06:15
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 06:15
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 06:15
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 06:15
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 06:15
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 06:15
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 06:15
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 06:15
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 06:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 06:15
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 06:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 06:15
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 06:15
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 06:15
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 06:15
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 06:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:15
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 06:15
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 25

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: HRW16 Lab ID: 92422237003 Collected: 03/21/19 11:40 Received: 03/21/19 14:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 06:15
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 06:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 06:15
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 06:15
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 06:15
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 06:15
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 06:15
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 06:15
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 06:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 06:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 06:15
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 06:15
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 06:15
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 06:15
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 06:15
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 06:15
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 06:15
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 06:15
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 06:15
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 06:15
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 06:15
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 06:15
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 06:15
95-47-6
Surrogates
4-Bromofluorobenzene (S)
95
%
70-130
1
03/27/19 06:15
460-00-4
1,2-Dichloroethane-d4 (S)
77
%
70-130
1
03/27/19 06:15
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
03/27/19 06:15
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 22:44
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92
%
50-150
1
03/26/19 22:44
17060-07-0
Toluene-d8 (S)
96
%
50-150
1
03/26/19 22:44
2037-26-5
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 25

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ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: TRIP BLANK Lab ID: 92422237004 Collected: 03/21/19 10:10 Received: 03/21/19 14:58 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 02:34
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 02:34
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 02:34
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 02:34
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 02:34
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 02:34
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 02:34
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 02:34
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 02:34
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 02:34
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 02:34
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 02:34
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 02:34
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 02:34
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 02:34
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 02:34
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 02:34
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 02:34
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 02:34
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 02:34
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 02:34
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 02:34
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 02:34
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:34
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:34
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 02:34
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 02:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 02:34
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 02:34
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 02:34
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 02:34
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 02:34
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 02:34
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 02:34
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 02:34
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 02:34
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 02:34
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 02:34
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 02:34
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 02:34
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 02:34
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 02:34
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 02:34
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 02:34
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 02:34
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 02:34
1330-20-7
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM
without
the written consent
of Pace Analytical Services, LLC.
Page 10 of 25

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
Sample: TRIP BLANK
Lab ID: 92422237004 Collected: 03/21/19 10:10
Received: 03/21/19 14:58 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
m&p-Xylene
ND ug/L
2.0
1
03/27/19 02:34
179601-23-1
o-Xylene
ND ug/L
1.0
1
03/27/19 02:34
95-47-6
Surrogates
4-Bromofluorobenzene (S)
97 %
70-130
1
03/27/19 02:34
460-00-4
1,2-Dichloroethane-d4 (S)
75 %
70-130
1
03/27/19 02:34
17060-07-0
Toluene-d8 (S)
107 %
70-130
1
03/27/19 02:34
2037-26-5
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 25

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
QC Batch: 465869 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92422237001, 92422237002, 92422237003
METHOD BLANK: 2532732 Matrix: Water
Associated Lab Samples: 92422237001, 92422237002, 92422237003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
1.0
03/28/19 21:03
1.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2532733
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
456
91
80-120
Arsenic
ug/L
500
441
88
80-120
Barium
ug/L
500
453
91
80-120
Beryllium
ug/L
500
453
91
80-120
Cadmium
ug/L
500
459
92
80-120
Chromium
ug/L
500
456
91
80-120
Cobalt
ug/L
500
453
91
80-120
Copper
ug/L
500
461
92
80-120
Lead
ug/L
500
445
89
80-120
Nickel
ug/L
500
448
90
80-120
Selenium
ug/L
500
456
91
80-120
Silver
ug/L
250
233
93
80-120
Thallium
ug/L
500
437
87
80-120
Vanadium
ug/L
500
451
90
80-120
Zinc
ug/L
500
452
90
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 25

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HOLBROOKS ROAD LANDFILL
92422237
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2532734
2532735
MS
MSD
92422047001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
476
471
95
94
75-125
1
Arsenic
ug/L
ND
500
500
459
453
92
91
75-125
1
Barium
ug/L
33.5
500
500
508
497
95
93
75-125
2
Beryllium
ug/L
ND
500
500
480
470
96
94
75-125
2
Cadmium
ug/L
ND
500
500
482
477
96
95
75-125
1
Chromium
ug/L
ND
500
500
479
474
96
95
75-125
1
Cobalt
ug/L
ND
500
500
467
461
93
92
75-125
1
Copper
ug/L
ND
500
500
476
470
95
94
75-125
1
Lead
ug/L
ND
500
500
461
454
92
91
75-125
2
Nickel
ug/L
ND
500
500
466
459
93
92
75-125
1
Selenium
ug/L
ND
500
500
488
483
97
96
75-125
1
Silver
ug/L
ND
250
250
243
242
97
97
75-125
0
Thallium
ug/L
ND
500
500
454
447
91
89
75-125
2
Vanadium
ug/L
ND
500
500
472
469
94
94
75-125
1
Zinc
ug/L
ND
500
500
480
471
96
94
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 25

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
QC Batch: 465908
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92422237001, 92422237002,
92422237003
METHOD BLANK: 2532824
Matrix: Water
Associated Lab Samples: 92422237001, 92422237002,
92422237003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Thallium ug/L
ND 0.10
03/29/19 03:27
LABORATORY CONTROL SAMPLE: 2532825
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Thallium ug/L
10 9.5
95 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2532826 2532827
MS MSD
92422137001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND
10 10 8.5
8.7 84 87 75-125 3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 25

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
QC Batch: 465536 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92422237001, 92422237002, 92422237003, 92422237004
METHOD BLANK: 2531202 Matrix: Water
Associated Lab Samples: 92422237001, 92422237002, 92422237003, 92422237004
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,1-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
1,2,3-Trichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
03/27/19 01:20
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,4-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
2-Butanone (MEK)
ug/L
ND
5.0
03/27/19 01:20
2-Hexanone
ug/L
ND
5.0
03/27/19 01:20
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/27/19 01:20
Acetone
ug/L
ND
25.0
03/27/19 01:20
Acrylonitrile
ug/L
ND
10.0
03/27/19 01:20
Benzene
ug/L
ND
1.0
03/27/19 01:20
Bromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromodichloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromoform
ug/L
ND
1.0
03/27/19 01:20
Bromomethane
ug/L
ND
2.0
03/27/19 01:20
Carbon disulfide
ug/L
ND
2.0
03/27/19 01:20
Carbon tetrachloride
ug/L
ND
1.0
03/27/19 01:20
Chlorobenzene
ug/L
ND
1.0
03/27/19 01:20
Chloroethane
ug/L
ND
1.0
03/27/19 01:20
Chloroform
ug/L
ND
5.0
03/27/19 01:20
Chloromethane
ug/L
ND
1.0
03/27/19 01:20
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
Dibromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Dibromomethane
ug/L
ND
1.0
03/27/19 01:20
Ethylbenzene
ug/L
ND
1.0
03/27/19 01:20
lodomethane
ug/L
ND
20.0
03/27/19 01:20
m&p-Xylene
ug/L
ND
2.0
03/27/19 01:20
Methylene Chloride
ug/L
ND
5.0
03/27/19 01:20
o-Xylene
ug/L
ND
1.0
03/27/19 01:20
Styrene
ug/L
ND
1.0
03/27/19 01:20
Tetrachloroethene
ug/L
ND
1.0
03/27/19 01:20
Toluene
ug/L
ND
1.0
03/27/19 01:20
v3
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 25

Pace Analytical Services, LLC
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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
METHOD BLANK: 2531202
Matrix:
Water
Associated Lab Samples: 92422237001, 92422237002, 92422237003,
92422237004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/27/19 01:20
Trichloroethene
ug/L
ND
1.0
03/27/19 01:20
Trichlorofluoromethane
ug/L
ND
1.0
03/27/19 01:20
Vinyl acetate
ug/L
ND
2.0
03/27/19 01:20
Vinyl chloride
ug/L
ND
1.0
03/27/19 01:20
Xylene (Total)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane-d4 (S)
%
76
70-130
03/27/19 01:20
4-Bromofluorobenzene (S)
%
97
70-130
03/27/19 01:20
Toluene-d8 (S)
%
103
70-130
03/27/19 01:20
LABORATORY CONTROL SAMPLE:
2531203
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.2
106
70-130
1,1,1-Trichloroethane
ug/L
50
45.7
91
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
47.3
95
70-130
1,1,2-Trichloroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethane
ug/L
50
47.8
96
70-130
1,1-Dichloroethene
ug/L
50
46.8
94
70-130
1,2,3-Trichloropropane
ug/L
50
36.5
73
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
46.1
92
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.5
101
70-130
1,2-Dichlorobenzene
ug/L
50
46.7
93
70-130
1,2-Dichloroethane
ug/L
50
41.5
83
70-130
1,2-Dichloropropane
ug/L
50
53.4
107
70-130
1,4-Dichlorobenzene
ug/L
50
47.3
95
70-130
2-Butanone (MEK)
ug/L
100
98.8
99
64-135
2-Hexanone
ug/L
100
89.7
90
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
86.0
86
70-130
Acetone
ug/L
100
90.4
90
61-157
Acrylonitrile
ug/L
250
246
99
61-143
Benzene
ug/L
50
50.6
101
70-130
Bromochloromethane
ug/L
50
49.5
99
70-130
Bromodichloromethane
ug/L
50
49.8
100
70-130
Bromoform
ug/L
50
49.9
100
70-130
Bromomethane
ug/L
50
31.0
62
38-130 v3
Carbon disulfide
ug/L
50
47.8
96
68-130
Carbon tetrachloride
ug/L
50
45.5
91
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
50.6
101
37-142
Chloroform
ug/L
50
43.3
87
70-130
Chloromethane
ug/L
50
50.2
100
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 25

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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
LABORATORY CONTROL SAMPLE:
2531203
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
47.7
95
70-130
cis-1,3-Dichloropropene
ug/L
50
50.6
101
70-130
Dibromochloromethane
ug/L
50
51.7
103
70-130
Dibromomethane
ug/L
50
49.2
98
70-130
Ethylbenzene
ug/L
50
48.4
97
70-130
lodomethane
ug/L
100
97.7
98
40-130
m&p-Xylene
ug/L
100
98.0
98
70-130
Methylene Chloride
ug/L
50
45.6
91
67-132
o-Xylene
ug/L
50
50.4
101
70-131
Styrene
ug/L
50
50.2
100
70-130
Tetrachloroethene
ug/L
50
49.3
99
69-130
Toluene
ug/L
50
45.7
91
70-130
trans-1,2-Dichloroethene
ug/L
50
48.0
96
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.9
100
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
53.8
108
35-189
Trichloroethene
ug/L
50
50.0
100
70-130
Trichlorofluoromethane
ug/L
50
44.2
88
63-130
Vinyl acetate
ug/L
100
88.7
89
55-143
Vinyl chloride
ug/L
50
53.1
106
70-131
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
86
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.4
102
73-134
1,1,1-Trichloroethane
ug/L
ND
20
18.4
92
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.1
95
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.4
97
70-135
1,1-Dichloroethane
ug/L
ND
20
19.3
97
70-139
1,1-Dichloroethene
ug/L
ND
20
19.4
97
70-154
1,2,3-Trichloropropane
ug/L
ND
20
18.4
92
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.4
87
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.2
96
70-137
1,2-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
1,2-Dichloroethane
ug/L
ND
20
16.7
84
70-137
1,2-Dichloropropene
ug/L
ND
20
20.5
102
70-140
1,4-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
2-Butanone (MEK)
ug/L
ND
40
35.6
89
60-139
2-Hexanone
ug/L
ND
40
34.7
87
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
35.1
88
65-135
Acetone
ug/L
ND
40
36.6
92
60-148
Acrylonitrile
ug/L
ND
100
95.6
96
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
20.7
103
70-151
Bromochloromethane
ug/L
ND
20
19.8
99
70-141
Bromodichloromethane
ug/L
ND
20
18.6
93
70-138
Bromoform
ug/L
ND
20
18.8
94
63-130
Bromomethane
ug/L
ND
20
12.7
64
15-152 v3
Carbon disulfide
ug/L
ND
20
19.8
99
69-149
Carbon tetrachloride
ug/L
ND
20
19.1
95
70-143
Chlorobenzene
ug/L
ND
20
20.6
103
70-138
Chloroethane
ug/L
ND
20
21.2
106
52-163
Chloroform
ug/L
ND
20
17.2
86
70-139
Chloromethane
ug/L
ND
20
20.6
103
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
19.2
96
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
18.3
91
70-137
Dibromochloromethane
ug/L
ND
20
19.0
95
70-134
Dibromomethane
ug/L
ND
20
19.3
97
70-138
Ethylbenzene
ug/L
ND
20
20.3
101
66-153
lodomethane
ug/L
ND
40
38.6
97
20-138
m&p-Xylene
ug/L
ND
40
41.0
103
69-152
Methylene Chloride
ug/L
ND
20
18.5
92
42-159
o-Xylene
ug/L
ND
20
20.4
102
70-148
Styrene
ug/L
ND
20
19.8
99
70-135
Tetrachloroethene
ug/L
ND
20
20.5
102
59-143
Toluene
ug/L
ND
20
19.8
99
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
18.9
94
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
17.9
90
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
13.6
68
47-135
Trichloroethene
ug/L
ND
20
20.5
102
70-147
Trichlorofluoromethane
ug/L
ND
20
19.4
97
70-148
Vinyl acetate
ug/L
ND
40
21.7
54
49-151
Vinyl chloride
ug/L
ND
20
22.8
114
70-156
Xylene (Total)
ug/L
ND
60
61.4
102
63-158
1,2-Dichloroethane-d4 (S)
%
83
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2531204
92422047001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 25

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
SAMPLE DUPLICATE: 2531204
Parameter
Units
92422047001
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
79
78
4-Bromofluorobenzene (S)
%
96
96
Toluene-d8 (S)
%
104
103
RPD Qualifiers
v3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
QC Batch: 465409 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Associated Lab Samples: 92422237001, 92422237002, 92422237003
METHOD BLANK: 2530510
Matrix:
Water
Associated Lab Samples:
92422237001, 92422237002, 92422237003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
03/26/19 13:37
1,2-Dichloroethane-d4 (S)
%
91
50-150
03/26/19 13:37
Toluene-d8 (S)
%
96
50-150
03/26/19 13:37
LABORATORY CONTROL SAMPLE: 2530511
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 19.7 98 71-125
1,2-Dichloroethane-d4 (S) % 90 50-150
Toluene-d8(S) % 95 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2530512
2530513
MS
MSD
92422294007 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane(p-Dioxane)
ug/L 1.5J 20
20 19.3
17.8 89
81
50-150 8
1,2-Dichloroethane-d4 (S)
%
90
94
50-150
Toluene-d8(S)
%
95
98
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HOLBROOKS ROAD LANDFILL
Pace Project No.: 92422237
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 25

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HOLBROOKS ROAD LANDFILL
92422237
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92422237001
HRW8
EPA 3010A
465869
EPA 6010D
466009
92422237002
HRW9
EPA 3010A
465869
EPA 6010D
466009
92422237003
HRW16
EPA 3010A
465869
EPA6010D
466009
92422237001
HRW8
EPA 3010A
465908
EPA 6020B
466019
92422237002
HRW9
EPA 3010A
465908
EPA 6020B
466019
92422237003
HRW16
EPA 3010A
465908
EPA 6020B
466019
92422237001
HRW8
EPA 8260D
465536
92422237002
HRW9
EPA 8260D
465536
92422237003
HRW16
EPA 8260D
465536
92422237004
TRIP BLANK
EPA 8260D
465536
92422237001
HRW8
EPA 8260D Mod.
465409
92422237002
HRW9
EPA 8260D Mod.
465409
92422237003
HRW16
EPA 8260D Mod.
465409
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 22 of 25

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Pa Fe 1 of 2
:aceAnalytica! Document No.: Is suing Authority:
F-CAR-05-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville i Raleigh[] Mechanicsville[]
SIrnpte Condition. Client Name: Pr Wo# : 92422237
upon Receiptsect p
Courier: ❑Fed fat ❑UPS ❑UUSPSr cli111111111111111
enI� I III
❑ Commercial eta ❑ 92422237
Custody Seal Present? ❑Yes Seals intact? []Yes <L Ito
Dte/Initials Person Examining Contents:
Parking Material: []Bubble Wrap Bubble Bags lone ❑ Other.
Therrhonfgete . 92TO48 Type of ice: �—'t
[:]Bluee4 Gun ID:�J
Cooler Temp (`C): Correction Factor: Add/Subtract (°C) Q,Q
Cooler Temp Corrected ('C): _1
USDA Regulated Soit)"�N/A, water sample)
Did samples oriorfate in a quarantine zone within the United States: CA, NY, or SC {check maps)?
Chain of Custody Present?
Samples Arrived within Hold Time? . .
Short Hold Time Analysts <72 hr.)?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Ma
Headspace in VOA Vials {55-6mmj
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
1.
2,
3.
4.
[]No ❑N/A f6.
[]No❑NIA
r]Yes ❑No ❑NIA 7-
❑Yes ❑No N/A B.
YeS []No ❑NIA 9-
[]N/A 10.
❑NIA 11.
d
Biological Tissue o en?
[:]Yes ONO
❑ .
[]None
Temp should be above freezing to VC
❑Samples Out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source {i
including Hawaii and Puerto Rlco17 []Yes
Corhments/Discrepancy:_
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Field Data Required? []Yes []NO
Person contacted: Date/Time:
Project Manager SCURF Revlew: Data:
Project Manager SRF Revlew: Date: I _
Page 23 of 25

Document Name:
Sample Condition Upon Rec.
Document No.:
Document Revised: February 7, 2018
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, 0RO/8015 {water} DOC, Lft
"Bottom half of box is to list number of bottle
Project # WO# : 92422237
PM: MWB Due Dale: 04/04/19
CLIENT: 92—MECK CO
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aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
April 01, 2019
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on March 20, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HOLBROOKS ROAD SURFACE WATER
92422047
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92422047001
HRSW2
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422047002
HRSW3
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
92422047003
HRSW4
EPA 601OD
SH1
15
PASI-A
EPA 6020E
KQ
1
PASI-A
EPA 8260D
NSCQ
52
PASI-C
EPA 8260D Mod.
DLK
3
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 23

aceAnalytical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Sample: HRSW2 Lab ID: 92422047001 Collected: 03/20/19 12:19 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:09
7440-38-2
Barium
33.5
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 21:09
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 21:09
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:09
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:09
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:09
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:09
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:11
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 02:52
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 02:52
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 02:52
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 02:52
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 02:52
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 02:52
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 02:52
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 02:52
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 02:52
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 02:52
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 02:52
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 02:52
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 02:52
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 02:52
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 02:52
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 02:52
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 02:52
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 02:52
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 02:52
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 02:52
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 02:52
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 02:52
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 02:52
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:52
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:52
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 02:52
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Sample: HRSW2 Lab ID: 92422047001 Collected: 03/20/19 12:19 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 02:52
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 02:52
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 02:52
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 02:52
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 02:52
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 02:52
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 02:52
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 02:52
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 02:52
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 02:52
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 02:52
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 02:52
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 02:52
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 02:52
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 02:52
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 02:52
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 02:52
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 02:52
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 02:52
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 02:52
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 02:52
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 02:52
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 02:52
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
03/27/19 02:52
460-00-4
1,2-Dichloroethane-d4 (S)
79
%
70-130
1
03/27/19 02:52
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
03/27/19 02:52
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 00:14
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
91
%
50-150
1
03/26/19 00:14
17060-07-0
Toluene-d8 (S)
96
%
50-150
1
03/26/19 00:14
2037-26-5
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

aceAnalytical
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Sample: HRSW3 Lab ID: 92422047002 Collected: 03/20/19 12:57 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:27
7440-38-2
Barium
30.6
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 21:27
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 21:27
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:27
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:27
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:27
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:27
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:15
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 03:29
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 03:29
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 03:29
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 03:29
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 03:29
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 03:29
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 03:29
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 03:29
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 03:29
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 03:29
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 03:29
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 03:29
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 03:29
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 03:29
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 03:29
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 03:29
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 03:29
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 03:29
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 03:29
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 03:29
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 03:29
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 03:29
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 03:29
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 03:29
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 03:29
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 03:29
156-60-5
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 23

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ANALYTICAL RESULTS
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Sample: HRSW3 Lab ID: 92422047002 Collected: 03/20/19 12:57 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 03:29
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 03:29
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 03:29
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 03:29
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 03:29
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 03:29
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 03:29
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 03:29
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 03:29
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 03:29
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 03:29
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 03:29
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 03:29
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 03:29
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 03:29
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 03:29
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 03:29
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 03:29
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 03:29
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 03:29
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 03:29
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 03:29
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 03:29
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
03/27/19 03:29
460-00-4
1,2-Dichloroethane-d4 (S)
79
%
70-130
1
03/27/19 03:29
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
03/27/19 03:29
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 00:33
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
92
%
50-150
1
03/26/19 00:33
17060-07-0
Toluene-d8 (S)
97
%
50-150
1
03/26/19 00:33
2037-26-5
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

aceAnalytical
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ANALYTICAL RESULTS
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Sample: HRSW4 Lab ID: 92422047003 Collected: 03/20/19 12:42 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-36-0
Arsenic
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:30
7440-38-2
Barium
31.2
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-39-3
Beryllium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 21:30
7440-41-7
Cadmium
ND
ug/L
1.0
1
03/28/19 11:05
03/28/19 21:30
7440-43-9
Chromium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-47-3
Cobalt
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-48-4
Copper
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-50-8
Lead
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7439-92-1
Nickel
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-02-0
Selenium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:30
7782-49-2
Silver
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-22-4
Thallium
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:30
7440-28-0
Vanadium
ND
ug/L
5.0
1
03/28/19 11:05
03/28/19 21:30
7440-62-2
Zinc
ND
ug/L
10.0
1
03/28/19 11:05
03/28/19 21:30
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1
03/28/19 09:20 03/29/19 00:18
7440-28-0
8260D MSV Low Level Landfill
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
25.0
1
03/27/19 03:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
03/27/19 03:47
107-13-1
Benzene
ND
ug/L
1.0
1
03/27/19 03:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
03/27/19 03:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
03/27/19 03:47
75-27-4
Bromoform
ND
ug/L
1.0
1
03/27/19 03:47
75-25-2
Bromomethane
ND
ug/L
2.0
1
03/27/19 03:47
74-83-9 v3
2-Butanone (MEK)
ND
ug/L
5.0
1
03/27/19 03:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
03/27/19 03:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
03/27/19 03:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
03/27/19 03:47
108-90-7
Chloroethane
ND
ug/L
1.0
1
03/27/19 03:47
75-00-3
Chloroform
ND
ug/L
5.0
1
03/27/19 03:47
67-66-3
Chloromethane
ND
ug/L
1.0
1
03/27/19 03:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
03/27/19 03:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
03/27/19 03:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
03/27/19 03:47
106-93-4
Dibromomethane
ND
ug/L
1.0
1
03/27/19 03:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 03:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
03/27/19 03:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
03/27/19 03:47
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
03/27/19 03:47
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
03/27/19 03:47
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
03/27/19 03:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 03:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
03/27/19 03:47
156-60-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
Sample: HRSW4 Lab ID: 92422047003 Collected: 03/20/19 12:42 Received: 03/20/19 14:56 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Landfill Analytical Method: EPA 8260D
1,2-Dichloropropane
ND
ug/L
1.0
1
03/27/19 03:47
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 03:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
03/27/19 03:47
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
03/27/19 03:47
100-41-4
2-Hexanone
ND
ug/L
5.0
1
03/27/19 03:47
591-78-6
lodomethane
ND
ug/L
20.0
1
03/27/19 03:47
74-88-4
Methylene Chloride
ND
ug/L
5.0
1
03/27/19 03:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
03/27/19 03:47
108-10-1
Styrene
ND
ug/L
1.0
1
03/27/19 03:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 03:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
03/27/19 03:47
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
03/27/19 03:47
127-18-4
Toluene
ND
ug/L
1.0
1
03/27/19 03:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
03/27/19 03:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
03/27/19 03:47
79-00-5
Trichloroethene
ND
ug/L
1.0
1
03/27/19 03:47
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
03/27/19 03:47
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
03/27/19 03:47
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
03/27/19 03:47
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
03/27/19 03:47
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
03/27/19 03:47
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
03/27/19 03:47
179601-23-1
o-Xylene
ND
ug/L
1.0
1
03/27/19 03:47
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
03/27/19 03:47
460-00-4
1,2-Dichloroethane-d4 (S)
78
%
70-130
1
03/27/19 03:47
17060-07-0
Toluene-d8 (S)
104
%
70-130
1
03/27/19 03:47
2037-26-5
8260D MSV SIM
Analytical Method:
EPA 8260D Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
03/26/19 00:52
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
88
%
50-150
1
03/26/19 00:52
17060-07-0
Toluene-d8 (S)
95
%
50-150
1
03/26/19 00:52
2037-26-5
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
QC Batch: 465869 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92422047001, 92422047002, 92422047003
METHOD BLANK: 2532732 Matrix: Water
Associated Lab Samples: 92422047001, 92422047002, 92422047003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
1.0
03/28/19 21:03
1.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
5.0
03/28/19 21:03
10.0
03/28/19 21:03
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2532733
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
456
91
80-120
Arsenic
ug/L
500
441
88
80-120
Barium
ug/L
500
453
91
80-120
Beryllium
ug/L
500
453
91
80-120
Cadmium
ug/L
500
459
92
80-120
Chromium
ug/L
500
456
91
80-120
Cobalt
ug/L
500
453
91
80-120
Copper
ug/L
500
461
92
80-120
Lead
ug/L
500
445
89
80-120
Nickel
ug/L
500
448
90
80-120
Selenium
ug/L
500
456
91
80-120
Silver
ug/L
250
233
93
80-120
Thallium
ug/L
500
437
87
80-120
Vanadium
ug/L
500
451
90
80-120
Zinc
ug/L
500
452
90
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 10 of 23

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HOLBROOKS ROAD SURFACE WATER
92422047
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2532734
2532735
MS
MSD
92422047001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
476
471
95
94
75-125
1
Arsenic
ug/L
ND
500
500
459
453
92
91
75-125
1
Barium
ug/L
33.5
500
500
508
497
95
93
75-125
2
Beryllium
ug/L
ND
500
500
480
470
96
94
75-125
2
Cadmium
ug/L
ND
500
500
482
477
96
95
75-125
1
Chromium
ug/L
ND
500
500
479
474
96
95
75-125
1
Cobalt
ug/L
ND
500
500
467
461
93
92
75-125
1
Copper
ug/L
ND
500
500
476
470
95
94
75-125
1
Lead
ug/L
ND
500
500
461
454
92
91
75-125
2
Nickel
ug/L
ND
500
500
466
459
93
92
75-125
1
Selenium
ug/L
ND
500
500
488
483
97
96
75-125
1
Silver
ug/L
ND
250
250
243
242
97
97
75-125
0
Thallium
ug/L
ND
500
500
454
447
91
89
75-125
2
Vanadium
ug/L
ND
500
500
472
469
94
94
75-125
1
Zinc
ug/L
ND
500
500
480
471
96
94
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
QC Batch: 465907 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92422047001, 92422047002, 92422047003
METHOD BLANK: 2532820 Matrix: Water
Associated Lab Samples: 92422047001, 92422047002, 92422047003
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Thallium ug/L ND 0.10
03/28/19 23:04
LABORATORY CONTROL SAMPLE: 2532821
Spike LCS
LCS % Rec
Parameter Units Conc. Result
% Rec Limits Qualifiers
Thallium ug/L 10 9.7
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2532822 2532823
MS MSD
92422253001 Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 9.1
9.0 91 90 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
QC Batch: 465536 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92422047001, 92422047002, 92422047003
METHOD BLANK: 2531202 Matrix:
Associated Lab Samples: 92422047001, 92422047002, 92422047003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,1-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1,2-Trichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,1-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
1,2,3-Trichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
03/27/19 01:20
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloropropane
ug/L
ND
1.0
03/27/19 01:20
1,4-Dichlorobenzene
ug/L
ND
1.0
03/27/19 01:20
2-Butanone (MEK)
ug/L
ND
5.0
03/27/19 01:20
2-Hexanone
ug/L
ND
5.0
03/27/19 01:20
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
03/27/19 01:20
Acetone
ug/L
ND
25.0
03/27/19 01:20
Acrylonitrile
ug/L
ND
10.0
03/27/19 01:20
Benzene
ug/L
ND
1.0
03/27/19 01:20
Bromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromodichloromethane
ug/L
ND
1.0
03/27/19 01:20
Bromoform
ug/L
ND
1.0
03/27/19 01:20
Bromomethane
ug/L
ND
2.0
03/27/19 01:20
Carbon disulfide
ug/L
ND
2.0
03/27/19 01:20
Carbon tetrachloride
ug/L
ND
1.0
03/27/19 01:20
Chlorobenzene
ug/L
ND
1.0
03/27/19 01:20
Chloroethane
ug/L
ND
1.0
03/27/19 01:20
Chloroform
ug/L
ND
5.0
03/27/19 01:20
Chloromethane
ug/L
ND
1.0
03/27/19 01:20
cis-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
cis-1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
Dibromochloromethane
ug/L
ND
1.0
03/27/19 01:20
Dibromomethane
ug/L
ND
1.0
03/27/19 01:20
Ethylbenzene
ug/L
ND
1.0
03/27/19 01:20
lodomethane
ug/L
ND
20.0
03/27/19 01:20
m&p-Xylene
ug/L
ND
2.0
03/27/19 01:20
Methylene Chloride
ug/L
ND
5.0
03/27/19 01:20
o-Xylene
ug/L
ND
1.0
03/27/19 01:20
Styrene
ug/L
ND
1.0
03/27/19 01:20
Tetrachloroethene
ug/L
ND
1.0
03/27/19 01:20
Toluene
ug/L
ND
1.0
03/27/19 01:20
v3
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
METHOD BLANK: 2531202
Matrix:
Water
Associated Lab Samples: 92422047001, 92422047002, 92422047003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
03/27/19 01:20
trans- 1,3-Dichloropropene
ug/L
ND
1.0
03/27/19 01:20
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
03/27/19 01:20
Trichloroethene
ug/L
ND
1.0
03/27/19 01:20
Trichlorofluoromethane
ug/L
ND
1.0
03/27/19 01:20
Vinyl acetate
ug/L
ND
2.0
03/27/19 01:20
Vinyl chloride
ug/L
ND
1.0
03/27/19 01:20
Xylene (Total)
ug/L
ND
1.0
03/27/19 01:20
1,2-Dichloroethane-d4 (S)
%
76
70-130
03/27/19 01:20
4-Bromofluorobenzene (S)
%
97
70-130
03/27/19 01:20
Toluene-d8 (S)
%
103
70-130
03/27/19 01:20
LABORATORY CONTROL SAMPLE:
2531203
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
53.2
106
70-130
1,1,1-Trichloroethane
ug/L
50
45.7
91
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
47.3
95
70-130
1,1,2-Trichloroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethane
ug/L
50
47.8
96
70-130
1,1-Dichloroethene
ug/L
50
46.8
94
70-130
1,2,3-Trichloropropane
ug/L
50
36.5
73
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
46.1
92
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.5
101
70-130
1,2-Dichlorobenzene
ug/L
50
46.7
93
70-130
1,2-Dichloroethane
ug/L
50
41.5
83
70-130
1,2-Dichloropropane
ug/L
50
53.4
107
70-130
1,4-Dichlorobenzene
ug/L
50
47.3
95
70-130
2-Butanone (MEK)
ug/L
100
98.8
99
64-135
2-Hexanone
ug/L
100
89.7
90
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
86.0
86
70-130
Acetone
ug/L
100
90.4
90
61-157
Acrylonitrile
ug/L
250
246
99
61-143
Benzene
ug/L
50
50.6
101
70-130
Bromochloromethane
ug/L
50
49.5
99
70-130
Bromodichloromethane
ug/L
50
49.8
100
70-130
Bromoform
ug/L
50
49.9
100
70-130
Bromomethane
ug/L
50
31.0
62
38-130 v3
Carbon disulfide
ug/L
50
47.8
96
68-130
Carbon tetrachloride
ug/L
50
45.5
91
70-130
Chlorobenzene
ug/L
50
48.8
98
70-130
Chloroethane
ug/L
50
50.6
101
37-142
Chloroform
ug/L
50
43.3
87
70-130
Chloromethane
ug/L
50
50.2
100
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 23

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
LABORATORY CONTROL SAMPLE:
2531203
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
47.7
95
70-130
cis-1,3-Dichloropropene
ug/L
50
50.6
101
70-130
Dibromochloromethane
ug/L
50
51.7
103
70-130
Dibromomethane
ug/L
50
49.2
98
70-130
Ethylbenzene
ug/L
50
48.4
97
70-130
lodomethane
ug/L
100
97.7
98
40-130
m&p-Xylene
ug/L
100
98.0
98
70-130
Methylene Chloride
ug/L
50
45.6
91
67-132
o-Xylene
ug/L
50
50.4
101
70-131
Styrene
ug/L
50
50.2
100
70-130
Tetrachloroethene
ug/L
50
49.3
99
69-130
Toluene
ug/L
50
45.7
91
70-130
trans-1,2-Dichloroethene
ug/L
50
48.0
96
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.9
100
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
53.8
108
35-189
Trichloroethene
ug/L
50
50.0
100
70-130
Trichlorofluoromethane
ug/L
50
44.2
88
63-130
Vinyl acetate
ug/L
100
88.7
89
55-143
Vinyl chloride
ug/L
50
53.1
106
70-131
Xylene (Total)
ug/L
150
148
99
70-130
1,2-Dichloroethane-d4 (S)
%
86
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.4
102
73-134
1,1,1-Trichloroethane
ug/L
ND
20
18.4
92
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.1
95
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.4
97
70-135
1,1-Dichloroethane
ug/L
ND
20
19.3
97
70-139
1,1-Dichloroethene
ug/L
ND
20
19.4
97
70-154
1,2,3-Trichloropropane
ug/L
ND
20
18.4
92
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.4
87
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.2
96
70-137
1,2-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
1,2-Dichloroethane
ug/L
ND
20
16.7
84
70-137
1,2-Dichloropropene
ug/L
ND
20
20.5
102
70-140
1,4-Dichlorobenzene
ug/L
ND
20
19.1
96
70-133
2-Butanone (MEK)
ug/L
ND
40
35.6
89
60-139
2-Hexanone
ug/L
ND
40
34.7
87
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
35.1
88
65-135
Acetone
ug/L
ND
40
36.6
92
60-148
Acrylonitrile
ug/L
ND
100
95.6
96
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 23

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
MATRIX SPIKE SAMPLE:
2531205
92422047002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
20.7
103
70-151
Bromochloromethane
ug/L
ND
20
19.8
99
70-141
Bromodichloromethane
ug/L
ND
20
18.6
93
70-138
Bromoform
ug/L
ND
20
18.8
94
63-130
Bromomethane
ug/L
ND
20
12.7
64
15-152 v3
Carbon disulfide
ug/L
ND
20
19.8
99
69-149
Carbon tetrachloride
ug/L
ND
20
19.1
95
70-143
Chlorobenzene
ug/L
ND
20
20.6
103
70-138
Chloroethane
ug/L
ND
20
21.2
106
52-163
Chloroform
ug/L
ND
20
17.2
86
70-139
Chloromethane
ug/L
ND
20
20.6
103
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
19.2
96
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
18.3
91
70-137
Dibromochloromethane
ug/L
ND
20
19.0
95
70-134
Dibromomethane
ug/L
ND
20
19.3
97
70-138
Ethylbenzene
ug/L
ND
20
20.3
101
66-153
lodomethane
ug/L
ND
40
38.6
97
20-138
m&p-Xylene
ug/L
ND
40
41.0
103
69-152
Methylene Chloride
ug/L
ND
20
18.5
92
42-159
o-Xylene
ug/L
ND
20
20.4
102
70-148
Styrene
ug/L
ND
20
19.8
99
70-135
Tetrachloroethene
ug/L
ND
20
20.5
102
59-143
Toluene
ug/L
ND
20
19.8
99
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
18.9
94
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
17.9
90
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
13.6
68
47-135
Trichloroethene
ug/L
ND
20
20.5
102
70-147
Trichlorofluoromethane
ug/L
ND
20
19.4
97
70-148
Vinyl acetate
ug/L
ND
40
21.7
54
49-151
Vinyl chloride
ug/L
ND
20
22.8
114
70-156
Xylene (Total)
ug/L
ND
60
61.4
102
63-158
1,2-Dichloroethane-d4 (S)
%
83
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2531204
92422047001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 16 of 23

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
SAMPLE DUPLICATE: 2531204
Parameter
Units
92422047001
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
79
78
4-Bromofluorobenzene (S)
%
96
96
Toluene-d8 (S)
%
104
103
RPD Qualifiers
v3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 23

Pace Analytical Services, LLC
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QUALITY CONTROL DATA
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
QC Batch: 465021 Analysis Method: EPA 8260D Mod.
QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM
Associated Lab Samples: 92422047001, 92422047002, 92422047003
METHOD BLANK: 2529043
Matrix:
Water
Associated Lab Samples:
92422047001, 92422047002, 92422047003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
03/25/19 19:23
1,2-Dichloroethane-d4 (S)
%
92
50-150
03/25/19 19:23
Toluene-d8 (S)
%
98
50-150
03/25/19 19:23
LABORATORY CONTROL SAMPLE: 2529044
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 20.3 102 71-125
1,2-Dichloroethane-d4 (S) % 96 50-150
Toluene-d8 (S) % 98 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2529045
2529046
MS
MSD
92422048003 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 17.2
17.4 81
82
50-150 1
1,2-Dichloroethane-d4 (S)
%
97
92
50-150
Toluene-d8(S)
%
96
96
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 23

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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HOLBROOKS ROAD SURFACE WATER
Pace Project No.: 92422047
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/01 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 19 of 23

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HOLBROOKS ROAD SURFACE WATER
92422047
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92422047001
HRSW2
EPA 3010A
465869
EPA 6010D
466009
92422047002
HRSW3
EPA 3010A
465869
EPA 6010D
466009
92422047003
HRSW4
EPA 3010A
465869
EPA 6010D
466009
92422047001
HRSW2
EPA 3010A
465907
EPA 6020B
466015
92422047002
HRSW3
EPA 3010A
465907
EPA 6020B
466015
92422047003
HRSW4
EPA 3010A
465907
EPA 6020B
466015
92422047001
HRSW2
EPA 8260D
465536
92422047002
HRSW3
EPA 8260D
465536
92422047003
HRSW4
EPA 8260D
465536
92422047001
HRSW2
EPA 8260D Mod.
465021
92422047002
HRSW3
EPA 8260D Mod.
465021
92422047003
HRSW4
EPA 8260D Mod.
465021
Date: 04/01 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 23

aCEAnaiWiCc?J
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February7, 2018
Page 1 of 2
Document No.;
F•CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville 0 Eden❑ Greenwood ❑ Huntersville © Raleigh[] Mechanicsville[]
F Sample Condition GlientName: WO# : 92422047
i -Up-on Receipt Project Oil
1�-1 �. r,k ).0 r/1",,l a �:%-'"r 'try � I /; I.
Courier: ❑Fed Far ❑UP5 ' ❑USPS ❑Client II I II' III I I II III II III
❑ Commercial ❑Pace ❑Other; 92422047
Custody Seal Present? []Yes ❑K% Seals Intact? []Yes ❑No
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None/ ❑ Other
Therriiometey gZ i 04$ Type of Ice. ❑Wet ❑Blue
❑IR Gun 10.
Cooler Terrip ('C): Correction Factor: Add/Subtract ('C) 0.0
Cooler Temp Corrected ('C):
USDA Regulated Soil (j3 NIA, water sample)
Did samples originate in a quarantine zone within the United States; CA, NY, or SC (check maps)?
i—lva. 171u .
Date/Initials Person Examining Contents:
Biological Tissue Frozen?
[]Yes I]No []N/A
[]None
Temp should be above freezing to 6°C
05amples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source {internationally, .
includine Hawaii and Puerto Rico)? ❑Yes []NO
Cam ments/Discrepan cy;
Chain of Custody Present?
Yves
❑No
❑N/A
E.
Samples Arrived within Hold Time?
❑Yes
❑No
❑N/A
2.
Short Hold TirneAnalysls (02 hr.)?
❑Yes
[]NO
❑NJA
3.
Rush Turn Around Time Requested?
Dyes
❑No
❑N/A
4.
Sufficient Volume?
[]Yes
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Or/es
❑Yes
❑No
ON.
[:]N/A
❑N/A
6.
Containers Intact?
❑Ves
❑No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
[JNIA
B.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
[]Yes
[]No
❑N/A
9.
Head space in VOA Vials (>5-6mm)?
❑Yes
❑No
❑NIA
10.
Trip 131ank Present?
Trip Blank Custody Seals Present?
[]Yes
[]Yes
❑No
[]NO
[]NIA
[]N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Tlme: _
Project Manager SCURF Review: ¢
Project Manager SRF Review: `
Field Data Required? ❑Yes []NO
Date: l , i
t
Date:
Page 21 of 23

Document Name:
Sample Condition Upon Recei!
Document No.:
F-CAR-CS-033-Rev.06
Document Revised: February 7, 2018
Page 1 of 2
issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/9015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project!" WO# . 92 4 22047
PM: MWB Due Date: 04/03/19
CLIENT: 92-MECK CO
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adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm will be sent to the North Carolina OEHNR Certification Office ;i.e.
Out of hotd, incorrect preservative, out of temp, incorrect containers.
Page 22 of 23

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