MO-9448_40883_CA__IAR_20181126_Initial Abatement Action Report

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INITIAL ABATEMENT ACTION REPORT
GADO BUILDING
5318 MORRIS FIELD DRIVE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA 28208
PREPARED FOR:
CHARLOTTE DOUGLAS INTERNATIONAL AIRPORT
P.O. BOX 19066
CHARLOTTE, NORTH CAROLINA 28219
PREPARED BY:
WOOD ENVIRONMENT & INFRASTRUCTURE SOLUTIONS, INC.
2801 YORKMONT ROAD, SUITE 100
CHARLOTTE, NORTH CAROLINA 28208
NOVEMBER 26, 2018
WOOD PROJECT: 6228-18-0503

wood.
Wood Environment & Infrastructure Solutions, Inc.
2801 Yorkmont Road, Suite 100
Charlotte, North Carolina 28208
Licensures: NC Engineering F-1253, Geology C-247
T: 704-357-8600
www.woodpic.com
November 26, 2018
Ms. Trudy Beverly
North Carolina Department of Environmental Quality
Mooresville Regional Office
UST Section
610 East Center Avenue
Mooresville, North Carolina 28115
Subject: Initial Abatement Action Report
GADO Building
5318 Morris Field Drive
Charlotte, Mecklenburg County, North Carolina
Wood Project: 6228-18-0503
Facility ID: 00-0-0000033447
Dear Ms. Beverly:
On behalf of Charlotte -Douglas International Airport (CLT), (Tank Owner), Wood Environment &
Infrastructure Solutions, Inc. (Wood) is submitting the enclosed Initial Abatement Action Report for the
facility located at 5318 Morris Field Drive in Charlotte, Mecklenburg County, North Carolina (the Site).
The report was prepared in general accordance with the North Carolina Department of Environmental
Quality, UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases (March 1, 2007 version, Change 8, effective January 9, 2018). This report includes a description of
the field activities and the results obtained.
Sincerely,
Wood Environment & Infrastructure Solutions, Inc.
Leanna Muroski
Technical Professional
Enclosure
Robert C. Foster, LG
Associate Geologist
Registered, NC #1335
Mr. James P. McDorman, P.G., Environmental Compliance Coordinator, CLT
'Wood' is a trading name for John Wood Group PLC and its subsidiaries r

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
TABLE OF CONTENTS
TABLEOF CONTENTS.................................................................................................................... ii
A.
SITE INFORMATION........................................................................................................... 1
1.
Site Identification...................................................................................................................................1
2.
Information about Contacts Associated with the UST System.......................................................1
3.
Information about Release...................................................................................................................1
B.
SITE HISTORY AND CHARACTERIZATION........................................................................ 3
1.
UST Owner/Operator Information......................................................................................................3
2.
UST Information.....................................................................................................................................4
3.
Site Characterization.............................................................................................................................5
C.
UST CLOSURE REPORT.......................................................................................................6
1.
Preparations for Closure.......................................................................................................................6
2.
Closure Procedures................................................................................................................................6
D.
INITIAL RESPONSE AND ABATEMENT ACTION.............................................................. 8
E.
EXCAVATION OF CONTAMINATED SOIL.......................................................................... 9
1.
Determination of the Source and Extent of Soil Contamination...................................................9
2.
Excavation Process.................................................................................................................................9
F.
CONCLUSIONS..................................................................................................................10
FIGURES
Figure 1 Site Topo
Figure 2 Tank Location Map
Figure 3 Site Plan
TABLES
Table 1 Summary of Soil Analytical Results
APPENDICES
Appendix A Liquid and Soil Disposal Manifests
Appendix B Photographs
Appendix C UST-213 Form
Appendix D Laboratory Analytical Reports and Chain -of -Custody Forms

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
A. SITE INFORMATION
1. Site Identification
Date of Report: November 26, 2018
Facility I.D.: 00-0-0000033447 UST Incident Number: N/A Site Risk:
Site Name: GADO Building
Street Address: 5318 Morris Field Drive
City: Charlotte Zip Code: 28208 County: Mecklenburg
Description of Geographical Data Point: Middle of tank basin
Location Method: Google Maps
Latitude: 35.212160' Longitude:-80.932720'
2. Information about Contacts Associated with the UST System
UST Owner: Charlotte Douglas International Airport
Address: P.O. Box 19066, Charlotte, North Carolina 28219
Telephone: [phone]
UST Operator: Charlotte Douglas International Airport
Address: P.O. Box 19066, Charlotte, North Carolina 28219
Telephone: [phone]
Property Owner: City of Charlotte Real Estate Division
Address: 600 East Fourth Street, Charlotte, North Carolina 28202
Telephone: [phone]
Consultant: Wood Environment & Infrastructure Solutions, Inc.
Address: 2801 Yorkmont Road, Suite 100, Charlotte, North Carolina 28208
Telephone: [phone]
Analytical Laboratory: Con -test Analytical Laboratory State Certification No.: 25703
Address: 39 Spruce Street, East Longmeadow, MA 01028
Telephone: [phone]
3. Information about Release
Date Discovered: October 19, 2018
Estimated Quantity of Release: Unknown
Cause of Release: leaking UST
Source of Release: Underground Storage Tank

Initial Abatement Action Report — GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
Sizes and Contents of Tanks or Other Containment from which Release Occurred: One
approximate 1,400-gallon UST formerly used to store heating oil for a boiler.
I, Robert C. Foster, a Licensed Geologist for Wood Environment & Infrastructure Solutions, Inc., do certify
information cont� ned in this report is correct and accurate to the best of my knowledge.
� 6&61tt-�C' VW-NITZ�Inll, h
Please affix Seal a` O�o.�i,L,r (Date)
SEAL
1335 —
Wood EnvironmeFR Infrastructure �Igtions, Inc. is licensed to practice geology and engineering in
-'Qi
- .'
North Carolina. The,4,p oikli 60t r s C-247.
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2

Initial Abatement Action Report - GADO Building
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
B. SITE HISTORY AND CHARACTERIZATION
1. UST Owner/Operator Information
November 26, 2018
UST ID Number
1 1
Facility ID Number
00-0-0000033447
Name of Land Owner
Dates of Ownership
City of Charlotte Real Estate Division
Street Address
600 West Fourth Street
City
State
Zip
Telephone Number
Charlotte
North Carolina
28202
704-336-2291
Name of Tank Owner/Operator
Dates of Operation
Charlotte Douglas International Airport
1973 to 1990
Street Address
P.O. Box 19066
City
State
Zip
Telephone Number
Charlotte
North Carolina
28219
704-359-4789
Incident Number
Pending

Initial Abatement Action Report — GADO Building
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
2. UST Information
November 26, 2018
Description of
Was release
Associated
Status of
associated
UST ID
Current/Last
Previous
Capacity (in
Construction
Date Tank
Tank Dimensions
Piping and
UST
with the UST
Number
Contents
Contents
gallons)
Details
Installed
Pumps
System?
No pumps
Approximately
present. 1/2-
June 23,
1
Heating Oil
Heating Oil
Steel
4 feet by 15 feet
inch diameter
Removed
Yes
1,400
copper tubing
1973
product lines.

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
3. Site Characterization
The Site is comprised of a small portion of Mecklenburg County Tax Parcel 115-211-03 which
encompasses approximately 249 acres. The CLT Airport GADO Building and an adjacent auxiliary
building formerly located at 5318 Morris Field Drive in Charlotte, North Carolina were recently
demolished. The GADO Building encompassed approximately 6,600 square ft. with two stories
and a basement. The auxiliary building encompassed approximately 225 square ft. The buildings
were reportedly built in the 1950's. During demolition activities, Jones Grading and Fencing, Inc.
(Jones) encountered a buried Underground Storage Tank (UST). A Topographic Map is included
as Figure 1. An aerial photograph showing the location of the tank at the property is included
as Figure 2. The tank was reportedly installed in 1973 and was used to store heating oil for the
on -site boiler until about 1990 when the boiler was converted to natural gas.
The site is located within the Charlotte Belt of the Piedmont Physiographic Province consisting
of low rounded hills and long rolling northeast to the southwest trending ridges with incised
creek channels. Based on a review of the North Carolina Geologic Map, the site is underlain by
metamorphosed quartz diorite.
Based on the United States Geologic Survey (USGS) topographic map, the elevation at the Site
ranges from about 722 feet above mean sea level. Surface drainage patterns within the
Piedmont typically indicate the direction contaminants would be transported by surface or
groundwater. Based on our interpretation of the topographic map and on -site observations,
surface water on the Site would be expected to flow to the east.
The direction and movement of groundwater through soil is dependent on soil type and the
presence of relict structures and textures of the underlying rock. Fractures, faults, folds and
foliation planes affect the migration of groundwater in rock. Since no significant geologic
features were identified in or on the site, it is reasonable to assume that the direction of on -
surface groundwater flow under static conditions (no pumping interference) approximates the
surface topography of the site. Groundwater at the site would be expected to flow to the east
toward an unnamed tributary of Taggart Creek.
5

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
C. UST CLOSURE REPORT
Preparations for Closure
CLT personnel retained Jones to remove the UST and Wood to perform the UST Closure
Assessment. Because the tank contained liquid at the time of discovery, CLT also retained a
waste disposal company to mobilize a vacuum truck to the property and remove the liquids and
transport them to a permitted facility for disposal. Prior to removal of the tank, approximately
700 gallons of heating oil and petroleum contact water (PCW) was pumped from the tank into a
vacuum truck for off -site disposal by HAZ-MAT Environmental Services. The liquid disposal
manifest is included in Appendix A.
2. Closure Procedures
On October 19, 2018, Wood personnel met CLT and Jones personnel at the site to oversee the
removal of the tank. Jones personnel had removed overburden soil prior to Wood's arrival. The
tank had been covered by three feet of soil prior to discovery. Based on field screening, the
overburden soil did not appear to be affected with petroleum and was stockpiled separately for
later use. Prior to initiating the UST removal activities, Wood personnel used a RAE Systems
QRAE (2 Gas) meter to check the inside of the tank for flammable vapors. The lower explosive
limit (LEL) was measured within the UST using a RAE Systems QRAE 3 to verify safe removal.
Prior to removal, the UST was rendered inert by inserting dry ice into the tank. Based on this
information, Jones resumed removal of soil to further expose the top and sides of the UST.
Representative samples of soil from around the UST were collected and screened in the field for
volatile organic compounds (VOCs) using a RAE Systems MiniRAE 3000 equipped with a
photoionization detector (PID) while the UST was being exposed. Elevated PID readings were
noted in the soil as removal extended vertically to near the depth of the bottom of the tank.
On October 19, 2018, Wood personnel observed Jones removing the UST from the excavation.
As the tank was lifted from the excavation, pooled heating oil was noted on the soil beneath the
tank. In addition, corrosion holes were noted in the UST upon removal. Photographs taken by
Wood personnel during the excavation and removal activities are included in Appendix B. The
UST was transported by Jones to Southern Metals Company for disposal. The UST-2B UST
Closure Form is included in Appendix C.
UST closure soil samples were collected following the removal of the UST. Two soil samples (TB-
1 and TB-2) were collected from beneath the UST at a depth of nine feet below ground surface
0

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
(bgs). In addition, CLT personnel requested that Wood collect a sample from the stockpile
(Stockpile) for waste characterization purposes. The soil samples were collected manually by
Wood personnel directly from the trackhoe excavator bucket. To minimize the potential for
cross -contamination, a new pair of nitrile gloves was donned for the collection of each soil
sample. The soil samples (T13-1 and T13-2) were placed directly into laboratory -provided
containers and placed in a cooler on ice for delivery to Con -test Analytical Laboratory (Con -test),
a North Carolina -certified laboratory. The soil samples were analyzed for Total Petroleum
Hydrocarbons (TPH) diesel range organics (DRO) and gasoline range organics (GRO) via EPA
Method 8015C. In addition, the stockpile sample was analyzed for benzene, ethylbenzene,
toluene and xylenes (BETX) by EPA Method 826013. The samples were maintained under a chain -
of -custody protocol.
7

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
D. INITIAL RESPONSE AND ABATEMENT ACTION
CLT personnel requested that Wood personnel return to the site on October 22, 2018 to oversee
removal of petroleum -affected soil from the excavation. A representative of Wood observed soil
excavation and collected samples of soil from the excavator bucket and screened them in the
field for VOCs using a RAE Systems MiniRAE 3000 equipped with a PID. As the affected soil was
removed from the excavation, Jones personnel placed the soil on plastic sheeting for temporary
storage until disposal arrangements were complete. On October 22, 2018, Wood personnel
collected confirmation soil samples from the sidewalls (SW-1, SW-2, SW-3 and SW-4) and base
(TB-3) of the excavation for analysis. The sample locations are shown on Figure 3 and the
sample depths are provided on Table 1.
The soil samples were collected manually by Wood personnel directly from the excavator
bucket. To minimize the potential for cross -contamination, a new pair of nitrile gloves was
donned for the collection of each soil sample. The soil samples were placed directly into
laboratory -provided containers and placed in a cooler on ice for delivery to Con -test for analysis
including VOCs (EPA Method 8260B), semi -volatile organic compounds (SVOCs) by EPA Method
8270 and MADEP Volatile Petroleum Hydrocarbons (VPH) and Extractable Petroleum
Hydrocarbons (EPH).
Based on the analytical results (Table 1), CLT personnel requested that Wood personnel return
to the site on October 31 and November 1, 2018 to oversee additional removal of visibly -stained
petroleum -affected soil from the excavation. A representative of Wood observed soil excavation
and collected samples of soil from the excavator bucket and screened them in the field for VOCs
using a Foxboro TVA equipped with a flame ionization detector (FID). As the affected soil was
removed from the excavation, Jones personnel placed the soil on plastic sheeting for temporary
storage until disposal arrangements were complete. On November 1, 2018, Wood personnel
collected one additional confirmation soil sample from the base (TB-4-18, depth of 18 feet bgs)
of the excavation for analysis. Groundwater was noted seeping into the base of the excavation at
the depth of sample TB-4-18.
The soil sample was collected manually by Wood using the same methods described above. The
soil sample was placed directly into laboratory -provided containers and placed in a cooler on ice
for delivery to Con -test for analysis including VOCs (EPA Method 8260B), SVOCs by EPA Method
8270 and MADEP VPH and EPH.
M

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
E. EXCAVATION OF CONTAMINATED SOIL
1. Determination of the Source and Extent of Soil Contamination
The results of the analysis of the sidewall and base soil samples were evaluated to determine the
point at which soil excavation was terminated. The analysis of soil samples SW-1, SW-4 (depth of
10 feet bgs) and TB-4-18 (depth of 18 feet bgs) identified concentrations of petroleum
constituents that exceeded the Soil -to -Water Maximum Soil Contaminant Concentrations
(MSCCs) as shown on Table 1. None of the samples that reflect soil remaining in the excavation
contained concentrations of petroleum constituents that exceeded the Residential or
Industrial/Commercial MSCCs. The laboratory analytical reports and chain -of -custody forms are
included in Appendix D.
2. Excavation Process
The excavation process is described in Section D of this report. The excavated and stockpiled
soil was placed into trucks and transported to Republic Services landfill at 5105 Morehead Road
in Concord, North Carolina for disposal as non -hazardous waste. A total of 668.19 tons of soil
was transported to the landfill for disposal. As of the date of this report, the excavation
remained open. CLT is planning to retain services to perform backfilling of the excavation and
appropriate compaction testing.
9

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
F. CONCLUSIONS
The Site is comprised of a small portion of Mecklenburg County Tax Parcel 115-211-03 which
encompasses approximately 249 acres. The CLT Airport GADO Building and an adjacent auxiliary
building formerly located at 5318 Morris Field Drive in Charlotte, North Carolina were recently
demolished. A Topographic Map is included as Figure 1. An aerial photograph showing the
location of the tank at the property is included as Figure 2. A site plan showing the depth and
lateral extent of the tank excavation is included as Figure 3.
None of the samples that reflect soil remaining in the excavation exceeded the Residential or
Industrial/Commercial MSCCs. Because the analysis of soil samples SW-1, SW-4 (depth of 10
feet bgs) and TB-4-18 (depth of 18 feet bgs) identified concentrations of petroleum constituents
that exceeded the Soil -to -Water Maximum Soil Contaminant Concentrations (MSCCs), it will be
necessary to perform a Phase I Limited Site Assessment (LSA) to evaluate the groundwater
quality at the former tank location.
10

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
FIGURES

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of PREPARED BY: LM I DATE: 11/16/2018 1 CHECKED BY: RF I DATE: 11/16/2018 I PROJECT NO: 6228-18-0503 1 FIGURE NO:

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PREPARED BY: SS DATE: 11/16/2018 CHECKED BY: RF DATE: 11/16/2018 PROJECT No.: 6228-18-0503 FIGURE No.: 3
File Location: P:\6228 Environmental\jobs\2018\6228-18-0503 GADO Building UST Closure\Cad\GADO Bldg — Fig 3 — Site Plan.dwg

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
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Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
APPENDICES

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
APPENDIX A
LIQUID AND SOIL DISPOSAL MANIFESTS

ry��ar
1A�! ,I kr +1I 1
j i 11 11
��``
NONi H A C)U
qiiicm
EML WLA-roR LOGATI CIN
!*fr31►�E
0RJC,INA-nNG ADDRESS
MAILIING ADO RESS —
+ 'I# -if STATE—_ ZIF*
clrr
PHONE NO,
COINTACTNAM
0ES. OF WASTF;
0UCLj4_jaj AAL. Al.
fRIPTIO
7. PETROLEUA+IOONTA TWATER
- OFF -SPEC LIGHT OIL, DIESEL OR GAS
3. NON-HAZARt US LIQUIDS
4- SEDIMENTORS01-I0
5. 55- ALLON DRUM REMOVED - SOLID OR EMPTY
6. 56- ALLON DRUM REMOVED - LIQUID
7.
13,
i�
10. ARRIVAL TIME:
DEPARTU E TIME:
4 *F,LAft.,+ Vq,L
P "J 1`1"
I#W, 14" ,
dL�
YY[Y1iMti.6-14 rxr,tl°rls�r� --
1'4,11rf. FWMFII "ti AA WVh `
NAur
CITY
PRONE No
CONTACT NAMrz
ED
Ne
---`I "�oAxdT�Y- — - ---� i
4
GENERATOR'S ERTIFICATIOIN; I hereby certify that the above named material Is riot a hazardous waSte as defined Ly 40 CFR Pan 26'1 os a(�y apptilcabtie skate law, has t4�
described, classified and packaged, and is in proper corOion for transportation according to applicable regulations- fienerakorl usiomer shall r6mburse t#f -MAT M Teasanabi
and charges for handling, analyzing, loading, preparing, transporting. storing or caring for Donconfofming or -aRf spec waste. 5n iudinq casts of deconlami, gig afrd el a ing ci
Generator must nc)tify HAZ-MAT of any charges to,,the waste strearrr prior to shipment. 1. . .-r..
1g136M_ _ 3hIDr1'r
Generator Auth-orized ent Name -
—Section Ill.
R
HAZ,--MAT
ENVIRONMENTAL SERVICES
P.C). BOAC 37392 e CHARLOTTE, N.C. 28237
I. Driver hlameffitle
�. Phone o- c, Tack No.
lazardous Waste Transporter Permits
:PA NCO0481461 70
THAN,.}Sr{ ICV,K {j)CRSml`a}rL'nI plerPji-di- nxporICr I cv,
�':aeLs 1SrrLs rlr cu�rlPit LE IL-LL}
f. Address - .
h. Phone No.
j. Transporler of Permit Nos.
—� S#rapmeM Oats
Driwarsi mare
TRANSPORTER 11
Url�ar 5lgnalu�ti
;, r�fir 3'rr 1FIT I [' Il'�''i
4c`, on IV. • JL -LLJjL i 1 ih - t — -
Site Name'. e: z-M B vlr nmen al ervl
Ih sical ,address: 21Q Dalto AvenUe
gharlo.tie.N.C. 0
a. Pylons No.
b. Mailing Addfess:
1. Truck o. --
L
Discrepancy Indica#ion Spat I�� atruda a + 4 lIL�1�d'J � 31r I�1�V
NS �s to c ,* M al �s rr el ner ved fTwn aura IOMbUn been i and will be � �, � � �7� I l ot prope 690
�n�L l�U[%0j1 Rd Ce
re blend 'info a � asbe fuel four Qse in large irldAM hurrw. � asw vm a mefl systems a� tiled fc E F.A' OW00 • Inc�MtMel f
yelp into �e MUD sanita4on rawer system under permit IUP6012. (3) j4dg
I) Our Inntrimt syrn oxiats on a first in, fli t oul basks mid "ct sfukl be prowaod within seven d •
DATIE )Ni-H UAT
AGNA7'UREOF FACIUTYAGENT
-fkIOINAL t:INALT.S.i?. - VE LOV- 4i"=R f�ti

REPUBLIC"
SERVICES
4481214
NON —HAZARDOUS WASTE MANIFE;Coniners
1, Generator's US EPA ID Number Manifest Document Number
2. Page 1 of
3. Generator's Name and Mailing Address
5. Generating Location (if
4. Phone ( )
6. Phone ( )
].Transporter#t Company Name
6,US EPA ID Number
rter#1'a Phone
10. Transempr#2 Company Name
11. US EPA ID Number
Transport Phone
13. Designated TI6ID Facility Name and Site Address
14. US EPA ID Number
's Phone
GAII `D.Do moiB1 1111i. i. nl'^. 'Pi ,T.),i
AH 4L{f!
16. Waste Shipping Name and Description
1]. Republic Services Appmvel A add Ex,
ers
19. Total
Pa. Unit
Quantity
WWoI
r .r.
TypeObil-Nlfaror-.
ua$[nl
,i.I c ri.� iU:cb. Is
b
6
do
I
/�
�4
W
if
f�
^1
J
I
21. Additional Descriptions for Materials Listed Above --
22. Special Handling Instructions and Additional Information
23, GENERATORS CERTIFICATION: I hereby cehity that the above named material Is not a hazardous waste as defined by 40
state law, hasbeen
properly described classifiedantl packaged, antl is In proper condition for transportation according to applicable regulations; ANeatment residue ofapreviously
restricted hazardous waste subect to the Land Disposal ResMctions. I certfy and warrant that the waste has been treated e requirements of 40
Lanyicable
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261.
Printetl/rypetl Name
6ignaNre Monrh Oay sear
2 24.Transporter IN: Acknowledgement of Receipt ofMaterials _
Prinled?ypsd Name
Signature r- n4onln oay near
O
2 h 25. anr#2 sporte: Acknowledgementof Receipt of Materials
G Pr1nt irl'T pad Name - Signature r Monrh oay veer
It
26, Discrepancy Indication Space /r
r
J_
Fadldry Owns'' Operator Certification of receipt Cl waste materials Covered by this promise[ (except as noted in Item 19)
LL
L2].
N -
Prinied?ypetl Name ( 6lgnature y Oaf Yea.
F
TRANSPORTERdt1 NEOPMMMMW

tREPUBLIC
Zf SERVICES
NON -HAZARDOUS WASTE MANIFEST
4481215
1, Generator's US EPA 10 Number Manifest Document Number
2. Page 1 of
B. Generator'e Name and Malang Address
Glwfbtle Uuugrn6 Nlfy+p(l
SGaneratlng Location (if different) r /
Tilll pYbNivi M.W..
5i18 hkrNlBtlxW Dr.
Gharkrlte. W.262M
//'
1-h6110F1B. IVl. tBCNf1 :m al1ursv
'Ll .5%I l'
4. Phone( )
S. Phone( )
7, Transporter#1 Company Name
8. US EPA ID Number
9. Transporter #1's Phone
10. Transpoder#2 Company Name
11. US EPA ID Number
12. Transporter#2's Phone
13. Designated PSM Facility Name and Site Atltlress
14. US EPA ID Number
15. Facility's Phone
ll L®rlp9N 9I115 W rehiliW RO GLOL4l G. bill 211Y
%US iS4 JOW X g67
16, Waste Shipping Name and Description
17. Republic Services AppmvalAaad Exp.Date
1S. Containers
19, Total
20. Unit
Quantity
WtAmi
No.
Type
W Ni h4azermmun self
5010- a-i NJ) IW26,'19
�O
R .
b
w
21. Additional Descriptions for Materials Listed Above -"
22. Special Handling Insimctions and Additional Information
G
4kraW YJJ.S:i:)6
M. GENERATORS CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is in proper condition for transportation a000Ming to applicable regulations',
AND, if this waste Is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Reductions. I ci and warrant that the waste has been treated In accordance with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261.
Pamed hyped Name
Signature
Monm Day year
be 24. Transporter #1: Acknowledgement of Receipt of Materials
F Printed/Typed Name
Signature
Mouth Day Yen,
O
a
of25, Transporter #2: Acknowledgement of Receipt of Materials
2 Primedlryped Name
Signal is
Month Day Year
da i_. _
26. Discrepancy Indication Space
T
F
J
< 27. Fxclilty Owner or Operator'. Cepupation of receipt of waste materials covered by this manifest (except as noted'm
LL
Item 19)
o +a: a M al, lIli l,L-t n..r 7. _n w!-2Lu4
I
N
H Printed?ypetl Name /
Signature
Monm ay/ vAsr
TRANSPORTER#

REPUBLIC'
if SERVICES
NON -HAZARDOUS WASTE MANIFEST 4481,216
1. Generator's US EPA ID Number Manifest Document Number
2. Page 1 of
`
3. Gersho t(p9f� 55 ryrya E tl yy'ling Add e 5
�THi14�U LJO�)L n,i y!111_ea-il
5. Generating Local Iif different)
.
._,.:,.
,u.. _. i.li"...
4. Phone(
6Phonel 1
9 Irmorporterlfl Company Name
8. US EPAID Number
9. Transporter k's Phone
10. Transpoherk2 Company Name
11. US EPAID Number
12. Transponder k2's Phone
13. Deaignated TISIO Facility Name and Site Address
14, US EPAID Number
15. Facility's Phone
(NA, .S trtlflll 6 f LIS MCIF11EN6 m" f-coni. 4 2tiscry
,.I t t.,-
16. Waste Shipping Name and Description
17. Republic Services Approval Nand Ex, Data
18.Containers
19. Total
did Unit
peanut,
WWOI
V.
No.
Type
Q b.
0
C/
J
21. Additional Oescilpticns for Materials Listed Above
22. Spai HanGling Instructions antl Additional Information
di of .t.fil earl r
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste Ie a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I caddy and warrant that the waste has been treated in accordance with the requirements of 40
DEE 268 and Is n0 longer a hazardous .to a5 defined by 40 CFR 261,
PrintedlTyped Name
Signature mwm Day var
¢ 24. Transperterim Acknowledgement of Recelpl of Materials
IW— PrintedlTyped Name
Signature Month Oay Year
¢
6
Z25,Transporter A2: Acknowledgement of Receipt of Materials
6 Prfnte yped Name - Signature Monm onyUp vm/
26. Discrepancy Indication Space
>
F
J
Q20. Facility Owner or Operator Codification of receipt of waste materials covered by this manifest (except as noted In Item 19)
LL
N
F Pdnted/Typetl Name �
�
Signature I_ .Iwnrn � Yev
✓
�
1
TRANSPORTE13#1

���REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFEST = 4461217
1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of
3. Generator's Nams and Melling Address 5. Generating Location (if different)
4. Phone ( 1 6. Phone ( )
]. Transporter #1 Company Name
8,US EPA ID Number
9. Transpoher#1's Phone
1O. Transporter H2 Company Name
11. US EPA ID Number
12. Transporter#2's Phone
13. Designated TIS/D Facility Name and Site Address
141, US EPA ID Number
15. Facility's Phone
. ry Iso:11:. ;S:: lvl01 v tlt$reS lFit (. ..:.. .. ..... frh(,
16. waste Shipping Name and Description
17. Republic Services Approval #and Exp. Date
18. Containers
19. Total
20. Unit
Ouantiry
WWoI
No.
Type
O
6 b.
W
W
('J
21. Additional Descriptions far Materials Listed Above
22. Special Handling Instructions and Additional Information
23. GENERATOR'S CERTIFICATION: 1 hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is in proper condition for transportation accnrdlng to applicable regulations; AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I caddy and warrant that the waste has been treated in accordance with the requirements of 40
CFR 268 and Is no longer a hazardous waste as defined by 40 CFH 261,
PrintedRyped Name _ _,
Signature Monm oey veer
Q 24. Transporter#1 Acknowledgement of Receipt of Mandate.
i—
Printed/Fyped Name $gnaWle con. Day Yea/
Q
LL
Ol 25. Transporter#i Acknowledgement of Receipt of Materials -
2
PrintebRyped Name Signature Monm oey veer
F
26. Discrepancy Indication Space
F
J
G27. Facility Owner or Operator Certification of receipt of waste materials covered by this manifest (except as rated in Item 19)
LL
0
N
F Printod?yped Name Signature Monlh pay_ ear
GENERATOR'S COPY

90 'A REPUBLIC' > -� (� L �,
SERVICES --I'�
NON -HAZARDOUS WASTE MANIFEST= 44 8
218
1. Generator's US EPA ID Number Manifest Document Number
2. Page 1 of
3. Generator's No and Mailin Ail
5. Generating Location (if different)
a.wtlo uouyte�Anpo
'ax Ra Mur... on,
5318 MorrWil Dr
fharVil W. 2d2pR
l.I1tlt10i1B. 14G [C21:iT /D4 :1ti'I UI:Stl
/U4 aid I U lead
4. Phone l J
6. Phone( )
]. Transporter #1 Company Name
6. US EPA ID Number
9. Transpoder#1's Phone
f
1 D. Transxi42 Company amen
11. US EPA 10 Number
12. Tamperer#2's Phone
13. Designated TISID Facility Name and Slte Address
14. US EPA ID Number
15, Facility's Phone
M5Landfill51o%MGrshaod Rd GORcad,Ni 2aoZ7
104 d12.2004 x 351
16. Waste Snaking Name and Description
1]. Republic Services Appmval#antl Exp.Date
te.C.dMimers
19, Total
20. Unit
,.entity
WWoI
No.
Type
¢ Non FWH1ldON6 SOU
O
50iGleH1/91/ICr2blif
ad b.
ad
W
de
21. Addif at Descriptions for Materials Listed Above
22, Special Handling Instructions and Additional Information
OW acct tr-J.fSJkJ
23. GENERATOR'S CERTIFICATION: I thereby certify that the above named material is not a resources waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packages and Is in proper condition
for transportation according to applicable regulations; AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions.
I certify and warrant that the waste has been treated in accordance wtlb the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CPS 261.
Prietedneyped Name
SignisWfe uomn Cry Year
as 24.Transporter #i'. Acknowledgement of Receipt of Materials
w Punted?yped Name
Signature Monts pay Year
iT—
Z25 Transporter#2 Acknowledgement of Receipt of Materials
1
Printed/typed Name
ED
Signature tat pay Y r
�_. /
1 ��
26, Discrepancy ledicatido' pace
J
Q27 Facility Owner or Operator[ Certification of receipt of waste materials coveretl by Ibis manliest fexaept as noted In Item 19)
o"Ni LANDI III ; ,_o m , t ,..
N
F Printetl/fypetl Name ��
Signature MonlF key Year
t
� �—
TRANSPORTER#2

9WA REPUBLIC'
:' SERVICES
NON -HAZARDOUS WASTE MAN IFEST 448i219
1. Generator's US EPA IS Number Mani test Sediment Number
2. Page l of
3. Generator's Name antl Mailing Address
5. Generating Location (if different)
_p.no" Onuyill"ujioit
5'f id iiwrrisk Ef.
5318 Morrlg{lpld Dr,
ChaMld9, NC 2020R
Ghe1,10i 1I 'di I(w Win may
7,ael d6t U 130
4. Phone ( )
6-Phone ( )
1. Transporter 11 Company Name
6, US EPA ID Number
9. Transporter#1's Phone
10. Transporter#2 Company Name
11. USEPAIDNumber
12. Transport 42's Phone
13. Designated T/S/D Facility Name and Site Address
14. US EPA IO Number
15. Facilitys Phone
MA0 UntlfNl'1 bB IbretloYd Rd C:ViMgfd, NL 2do3S
11192-200A k ;f57
16. Waste Shipping Name and Desorption
1]. Republic Services Approval # and Ex, Sate
18. Containers
19. Total
2p. Unit
quantity
WWoI
No.
pe
a.
Non HBTArdoui Soli
5010.1&119i/ 101eryl9
b.
2
w
z
w
(9
/
21. Additional Descriptions for Materials Listed Above
22. Special Handing Instructions antl Additional Information
NN ecaslblaiba5
23. GENERATORS CERTIFICATION: I hereby certity that the above named material Is not a haurdous waste as defined by 40 CPU 261 or any applicable state law, has
been properly described classified and packaged, and is in proper condition for transportation awarding to applicable regulations; AND, if this waste Is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I certity and warrant that the waste has been treated In accordance with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 GFR 261,
Printed/Typed Name
Sgni Di Day year
24. Transporter dl: Acknowledgement of Receipt of Materials
F Printed?yped Name
Signature Moth Day t r
6 _
op 25. Transporter 42. Acknowledgement of Receipt of Materials
2
QPrated/Typed Name
Signature Mw0 Day year
F
26-Discrepancy Indication Space
Q21. Facllly Owner or Operator Gerti0da0on of receipt of waste materials covered by this menlfast (except as noted In Item 19)
O Gull LANItI-ILL
F Pdnted?ypad Name ^
Slid ture Monty Day Y r
TRANSPORTER#2 I ��i

REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFEST 4481220
1, Generator's US EPA ID Number Manilest Document Number
2, Page 1 of
3. General r s Name and Mailing Address 5, Genefafing L0pa11on (it different)
r o
funip" opowWY Allwrt FV,ze 0.MA lln t0 Ln
5318 A1DrrhReW CA GAa n\1rte. elk ZAe 0,,1
Ltma GE. taC- 2+}21ffl nar u_
4. Phone ( ) 6. Phone ( 1
>. Transporter Nl Company Name 8. US EPA ID Number A. Transporter G711',nc
10. Transporter N2 Companytiama
11. US EPA ID Number
12Transp0rer k2'e PM1pne
13. Designaled TlSA) Facility Name and Site Address
14. US EPA ID Number
15. Facility's Phone
t MLS LSi MR S l Ob MRr611B8d NO GOn"fia, NL 2B I
1114.7a, vassal % Al
16. Waste Shipping Name and Description
17. Republic Selvlces Approval"no Exp. Cate
t8. Gan\miners
1st. Total
20. Unit
Quantity
W1,V01
—
—
o.
Type
a,
Cc rVUR h1r1[B 3 iniguil0Y
SI114 ib-1Id /111T.'2Lv IR
O
Q b.
W
W
C0
a
21. Additional Descriptions for Materials Listed Above -
22. Special Handling Instructions and Additional Information
Idll ®I.iAA3.i.3J:iF!
23. GENERATOR'S CERTIFICATION: I hereby carify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is in proper condition for transportation aseeming to applicable regulations; AND, it this waste is a treatment residue of a
.
previously restricted hazardous waste subject t0 the Land Disposal Restrictions. I parity and warrant that the waste has been treated in accordance with the requirements of 40
CFR 268 and Is no longer a hazardous waste as defined by 40 OFR 261,
Printed/I'yped Name
Signature Mon. Day Yeai
J r i T
24. Transporter 91 Acknowledgement of Reaelpt of Materials
FW. Printedri Name
Signature Man. tray, Year
0
25. Transporter 02'. Acknowledgement of Receipt of Materials -
2
¢ Parted?yped Name
—
5G,❑6Wre Monts Oay Year
6. Discrepancy Indication Sliece
T
F
J
La 27. Facility Owner ar Operator: Degradation at receipt of waste materials covered by this moue t (ex¢epr as rabbis Item 19)
LL
� JMS L4NliriLL 6iidr FA(Iitr.H4AC) Hp t v , - , r_ ...,... e„
N
F Prin\etlRypetl Name �1/ Signature � Monm Oay Yee.
TRANSPORTER#2

���REPUBLIC`�/���! �)
SERVICES
NON -HAZARDOUS WASTE!MMANIFEST 4481221
T Generator's US EPA ID Number Manifest Document Number 2. Page 1 of
3. Generate, s Name and Malling Addriaks
5. Generating Locafon (If dlfferem)
i. Jar teryIm F
53fd Fdomisfleld far
,"..rout, l.'4.'Ri ..T-
4. Phone ( 1
6. Phone ( )
>. Transporter#1 Company Name
S. US EPA ID Number
9. Transporter #1'a Phone
10. Transporter#2 Company Name
11. US EPA ID Number
12. Transporter#2's Phone
13. Designated TlStD Facility Name and Site Address
14. US EPA ID Number
15. Facility's Phone
r. unsung 5LkRy Mafelxraa tea GAfr.Gld, pi im.—i
16. Waste Shipping Name and Description
17, Republic Semcas Approval# and Exp. Date
13.80ntainers
19, Told
20. Unit
Quantity
WWol
.r
. e ..
N0.
Type
a
rK,n IstneRra0tt4 Kvn
-Vftl Il, v_.i rfp<n 15
0
b.
w
of
\
Ca
l
1
21. AddlHDnel Descriptions for Materials Listed Above
22. Special Handling Instructions and Additional Information
can aruall fz iUS
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 Or any applicable state law, haz
been properly described classified and packaged and is in proper condition for transportation according to applicable regulations; AND, if this waste Is a treatment residue of a
previously restricted hazardous Waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements of 40
CFR 268 and Is no longer a Leapfrog waste as defined by 40 CFR 261.
PMteday ed Name
Signature Mont Oey Y r,
¢ 24. Transporter 01. Acknowledgement of Receipt of Materials
pu Pdntetl/TyPed Neme 3lgnwere Monty Oay Year
be
of25.Transporter ID: Acknowledgement of Receipt of Materials
< PdntedRyped Name I
Signature / col 0, Yee,
26. Dearer Indiee can Space
F
Q9. Facility Owner or Dperator: Certification of receipt of waste materials covered by this manifest (except as noted in Item 19)
w
N
PrintedRyped Name 1 _l
Signature rtaonm._ On
TRANSPORTER#t
N

REPUBLIC'
SERWCES
NON -HAZARDOUS WASTE MANIFEST 4 4 81 ^ ` 2
1. Generator's US EPA ID Number Manifest Document Number
2. Page 1 of
9. Generalllr%Mail A
6. Generating Location (t different)
r�?:1 it FMrff141Wb CF
Li KJ Kdaij, f*, :6,:YJ i'.I4 ¢.I rrt ul
4. Pbon6 ( )
6. Phone ( )
]. Transporter #1 Company Name
8, US EPA ID Number
9. Transporter A's Phone
10. Transporter #2 Company Name
11, US EPA ID Number
12. Transporter#2'c Phone
13. Deslgnated T/S/D Facility Name and Site Address
14. US EPA ID Number
15. Facility's Phone
- MS :Dltclui b1ty, (NIGfGhdRO I (.cmcolu. tail- z6DW 1
;..+: -, .
16, Waste Shipping Name and Descnption
17. Republic Services Approval #and Este Date
18. Containers
19. Total
20. Unit
Ouantiry
WWol
�•rvrcw
,a
No.
Type
ad 14U.; 1'N{s'alr4DL1 "416
Q
6 b.
W
M
W
C
i
21. Atltlitional Descriptions for Materials Listed Above
-
'j.
22. Special Handling Instructions and Additional Information
r
tail a,",l J401f
23. GENERATOR'S CERTIFICATION: I hereby certity that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state of has
been properly described classified and packaged, and Is in proper condition for transportation according to applicable regulations; AND, It this waste is a treatment residue of a
previously confirmed hazardous waste subject t0 the Lend Disposal Restrictions.
I certify and warrant hat He waste has been treated In accordance with the requirements of 40
CFR 268 and is n0 longer a hazardous waste as defined by 40 CFR 261.
,.
Printed/Typed Name _
Signature Month pay Yoar
24, Transporter Ill Acknowledgement of Receipt of Materials
f firmetl/Fyped Name
Signature Month Oay Year
Q
O
6
26. Transporter #2: Acknowletlge em nt of Receipt of Materials
Z
Printetl?yP tlName
Signature Madre oey ter
,('
E_ �� iJ _z/ 1 -
26 Discrepancy' Indication Space
- _
i
F
J_
2]. Facility Owner or Opzmtor'. Cedlflcation of receipt of waste materials covered by this manifest (except as noted In Item 19)
O
N
Printetlltypetl Name'
~ r
Signature _ ManN pay
1
r /
II
/
/
TRANSPORTE11#1

It?REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFEST= 4481223
L Generator's US EPA ID Number Manifest Document Number 2. Page 1 of
Generators a and MalmgAdress
L.hJr alb l.or a A IPDIt
5318 Moniallskl Dr
k,h rh011 NC 28208 nw e61 Vl:m
Phone (
Tamperer 41 Company Name
10. Tranepmter a2 cempacy Name
13. Designated T/S/D Facility Name and Site Address
Ma Landf111 5105 Morehead Rd Cahoot NC 28M7
NOR Hazardous &A
cherw", W. 28208
Ili J6101N
6. Phone ( )
IS EPA ID Number
9. Transport 41's Phane
US EPA ID Number
12. In ..punt 's Phone
US EPA ID Number
15. Facility's Phone
IOa782.1004 X 367
Republic Services Approval band Exp.Date
16. Containers
19. Toi:
Our
.
No
I Type
Ic"M 1aa
NJ
bNl acccY3a3858
23. GENERATOR'S CERTIFICATION: I hereby cedity that the shove named material Is not a mourners waste as defined by 40 CFR 261 or any applicable state law, has
been properly described classified and packaged, and Is In proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Formation, I cedify and warrant that the waste has been treated in accordance with the requirements of 49
CFR 263 and is no longer a hazardous waste as defined by 40 CFR 261,
Printed/rypel Name Signature mono No
ffiar
Q 24.Transporter #1: Acknowledgement of Receipt of Materials
f Prinied/fyped Name Signature -- fort oey—Year
2 25. Transporter#2: Acknowledgement of Receipt fMaterials -��-
Prinied/iypetl frommi Signature Men. Dey Year
1-
26. Di.rdpenhy Indication Space
f
J
LL2. Facility Owner or Operator: Cortifateriaie leatlon of receipt of waste mhavered by this memmot (except as noted in Item 19)
o CM5 LANUFiLL 31rm ii Inv 1;vk 1k, V_. .elux- III e,....,
w
F Printetl/fypetl Name ^ Signature McnrnT,Dar IY,Tr
TRANSPORTERR2

W REPUBLIC`
SERVICESREPUBLIC'
NON-HAZARDOUS WASTE MANIFEST=
4481224
1. Generators US EPA ID Number Meniteg Document Number2, Page 1 of
3. Gener"wia Name g
aDad"
5. GepeldtO yy�� ryryIl
Ktw 11 different)
tl Yaw MII(a>fl
Mpr
5318 AA0rF10111tl uF.
Chaplet t0, M. 2820N
GinarmllS, NL. 2EVOR /IM an ill.
)pal A6I Dl,1N
4. Phone ( 7
6. Phone ( J
]. Transporter #1 Company Name
6. US EPA ID Number
9. Transpmtar#t's Phone
10. Transporter#2 Company Name —�
11. US EPA IDNumber
12, Transporter#2'a Phone
14, US EPA ID Number
15. Facility's Phone
13. Designated T/SID Facility Name antl Site Atltlress
AA3 Lantlllu btd5 Abretreati fatl aancukG. fN(: 28Ue 7
I(rt. /Reltxla x 3s
16. Waste Shipping Name and Description
V. Republic Services Approval # and Exp. Date
18. Containers 19.
Total
20. Unit
Quantity
Stolen
No.
Type
a.
Q 1-1.—G1N(WUw 50N
$(11f}itl-IiVti 16126i IM
O
It b.
w
ad
C�,�
U
7)
21. Additional Descriptions far Materials Listed Above
22. Special Handling Instructions and Additional Information
Al accEfa335MA
23. GENERATOR'S CERTIFICATION: I hereby eedify that the above named material is not a hazardous waste be formed by 40 DER 261 or any applicable state law, has
been properly described, classlled and packaged, and is in tamper condition for transportation according to Callaway, regulations; AND, if this waste is a treatment residue of a
previously postponed hazardous waste correct to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements of 40
CUP 268 and is no longer a hazardous waste as defined by 40 DER 261.
Printatl?yped Name
Signature boom Day veer
24.➢ansporter Bt'. Acknowledgement of Receipt of Materials
PrintetlRypetl Name
6ignature Memo dry 'oar
04
_ _
Transeorter#2'. Acknowledgement of Ramuptef Materials - --�
Z25.
QPdnletl/Iyped Name
Signature Monitl pay Des
F `
28. Discrepancy Indication Spade
J
Q27. Facility Owner or Operate, Certification of receipt of waste materials covered by this manifest (except as noted in item 19)
LL
CMa iANl1GILL hnT Mk-rnL r:I tu: rn/li.kili,,, M. d4i IluLii ;-tea„ I no
�
N
F Printetl/rypetl Name
Signature
TRANSPORTER #2;
V

�Rii REPUBLIC"
C SERVICES
NON -HAZARDOUS WASTE MANIFEST 4481''J
1, Generator's US EPA ID Number Manif.d Document Number
2.Page1 of
3. Generator's Name and Mailing Address
5. Generating Location (if different)
Gni rbW Gouptas Airport
�e iAottisrrlo in
6316 MUIIKiii ik
CCnaRnl(b, fir, 28Zfl3
4. Phone( Charlotte, INC kW08 the and D'IJN .ao,
Phone( 1 /U..lbr irl 11
]. Transporter #1 Company Name
8.US EPA ID Number
9. Transporter #1's Phone
'J
10. Touchagar#2 Company ame
11. US EPA ID Number
12. Transporter#2's Phone
13. Designated TISID Facility Name and Site Address
14. US EPA ID Number
15. Facility's Phone
NIS LantliP151(di Martinelli Rd Comoro, I is 2a92I
; Is iu 2W4 A it
16. Waste Shipping Name and Description
9. Republic Services Approval#and Exp. Dale
18. Containers
19. The
20. Unit
Quantity
Will
No.
Type
print opttu
Rum nuav
o¢
6
b
W
2
W
f9
ezk
21.Addtlional Descriptions for Materials Listed At..
22. Special Handling Instructions and Additional Information
fill aWQr4&3M*
_
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of
previously restricted hazardous waste subject to the Land Disposal Restrictions. I merry and warrant that the waste has been treated In accordance with the requirements of 40
CFR 268 and is no longer a hazalance waste as defined by 40 CFR 261.
Rd
teall ped Name
signs re month day v r
¢ 24, Transporter #1'. Acknowledgement of Receipt of Materials
F Printed/ryped Name
Signature Mon. Day veer
g
M 25. Transporter 92. Acherbudedgement of Receipt of Materials
Printed/rypetl Name
Signatwe Mon. day Year
f-
26. Discrepancy Indication Space
F
J
Q 27. Facility Ownef of operator: Certireopen of receipt of waste materials covered by this manifest (except as noted In Item 19)
LL
(.MS IANUHLL 61 W MldtEY EALi t<(11. NV V it . rp., ; .. r r c-! U[-lUr+ ,.. .1-,
N
F Primemryped Name
Signature nth day Y
tE
TRANSPORTER#2 mmmiWifd

ICT
SERVICES
NON -HAZARDOUS WASTE MANIFEST 4481164
1, Generator's US EPA ID Number Manifest Document Number
2. Page l of
3. Generator's Name and Mailing Address 5. Generating Location if different)
C.Imi DIJA Dougil All Wig mcdotielo Ce,
6516 Mforrwwld br. c`.M1erRrtlp, MC 282M
4. Phone ( C'Re eitE. NL 4dj /W Ant 01as 6. Phone( ) 7+?t do I O136
7 Transporter 91 Company Name 6, US EPA ID Number 9. Transporter #1's Phone
c —
10. Transpoher #2 Company Name
11. US EPA ID Number
12. Transponer#2's Phone
13. Designated TISI) Facility Name and Site Address
14. US EPA ID Number
15, Facility's Phone
k Arts LOndfIN 5105 Mk refleed NO COrrl:ar0, NL 281
1G4.hk J0G4 r fb ,
18. Containers 19. Total 20, Unit
16. Waste Shipping Name and Description
17, Republic Services Approval # and Ex, Data
Quantity WWol
No. Type
Alp 1n bdow
Earn Detrw
a
a b
as
up
w
C�
tD
�
—L_
1
21. Atldhional Descriptions for thermals Ludd Above
22. Special Handling Instructions and Additional Information
did eDC4433SIS5
_
23. GENERATOR'S CERTIFICATION: I hereby cdi that the above named material is not a hazardous waste as defined by 40 CFR 2fi1 or any applicable state Is has
been properly described, classified and packaged, and Is in proper condition for transportation according to applicable regulations', AND, if this waste Is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I both, and warrant that the waste has been treated in accordance with the requirements of 40
CFR 268 and is no longer a hszardens waste az defined by 40 CFR 261.
Printed/Typed Name
Signjatu e Monlll lay on,
¢ 24.Transporter#1'. acknowledgement of Receipt at Materials
W "coned7y,graiLlsaoff,
Sighawre Month Day over
y
S
w 25. Transpo r ant of Receipt of Materials '
2
—.
2 Parini ?yped Name
Sgrlature Muntn Oey year
26. Discrepancy Indication Space
Y
F
J
Q27, Facility Owner or Operator Cedlfication of receipt of waste materials covered by Nis manifest (except asnoted in Item 19(
LL
GMSIANUF(LL51WMOREHEAGnf)C t4GLit, tie. tlul[i itw/U2-duu r.:ro�
N
h PrintetlRypetl Name
Signature -of ay
TRANSPORTER#2

REPUBLIC -
SERVICES
NON -HAZARDOUS WASTE MANIFEST= 44E1165
I Generator's US EPA 10 Number Manifest Document Number
2-Page l of
3. Generator's Name and Mailing Address
5. Generating Location (If different)
t ito"o{tb Lsto'gal'rn"! l
!, iP, vaon r'i, I V!
r;;tR Mnr+51ke4:i UP
4. Phone ( gyoll C, i 11. /11Ud 01 .31
6. Phone ( )
I. Transporter #1 Company Name I
8. US EPA ID Number
9. Transporter#t's Phone
ifs 4,
10. Transporter#2 Company Name i
11, US EPA ID Number
12. Transp0her#2's Phone
13, Designated T/S/O Facility Name and Site Address
14. US EPVD Number
15. Facility's Phone
I LtifWMI 61 U' 440errtr3l Do C,, g.r N.iI ol7
16. Waste Shipping Name and Description
17. Republic Services Approved #and Exp. Date
18. Containers
IF Total
20. Unit
Guandry
WWol
No.
Type
i C. o.
➢W G%(H' I
K
IyOtI P1n2SA WtlE :41t
�i}PJ-Itl-IiN/I}�vr_
to
ad
W
7
ad
21. Additional Descriptions for Materials Listed Above
22. Special Handling Instructions and Additional Information
r. " ad,,
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and Is in proper condition for transportation according t0 applicable regulations; AND, if this waste is a treatment residue of a
previously restricted hazardous wage subject W the Land Disposal Restrictions. I early and warrant that the waste has been treated In acescis ce With the peritoneums of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261.
Pnnterl/Fypetl Name
Signature Monty Day Y r
M 24. Transporterld Acknowledgement of Receipt of Materials
ad
Pdnted?yped Name .
S nature Mn rh Day Year
a
cknowl dg t of Receipt of Materials
of 25. Threasportsirl: Acknowledgement
+
2 Printad sed rl Monslt Day Y.
2, Discrepancy Increases Space
Y
C
J
u9. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except as noted in Item 19)
N
F PpMed/ryped Name ightfu rn Day
G-'
TRANSPORTER41

REPUBLIC'
D
SERVICES
NON -HAZARDOUS WASTE MANIFEST 44$1166
1. Generator's US EPA ID Number Manifest Document Number
2, Page 1 of
3. Generator's Name and Mailing Address
5. Generating Location (if dlfferbnt)
(.Mlblle hat(Qui ArtpOft
Oftb ,n
6818 trbnlalMll N.
Oiler es", NC 211%...,.
4. Phone ( q0tialle• NC 2&08 rEa zn Drab
6. Phone ( 1
7. Transpoder#1 Company Name
8. US EPA ID Number
9. Tmnsponir#1'a Phone
l l)`
10.1 nsporter#7Compd Name J
11, US EPA ID Number
12. Transporter #2's Phone
13. Designated T/SID Facility Name and Site Address
14, US EPA ID Number
15. FadlLLy's Phone
" Mai Lanst 6 Y06 MGtersi etf Rd "noccol. et 2&027
N4..IF2.<q14 X 361
16. Waste Shipping Name and Description
IT Republic Services Approval#and Exp. Date
18. Containers
19. more
20. Unit
Quantity
WWDI
No.
Type
dlN l(I(MIIW
I-W IIIIMOW
--
—
I
2
I
O
6 b.
ad
W
be
W
!J
21. Atltlitional Descriptiona for Materials Listed Above -
22. Special Handling Instructions and Additional Information
uW 1101"333669
t'
23. GENERATOR'S CERTIFICATION: I hereby pacify that the above named material is not a hazardous ..to as seemed by 40 CFR 261 or any applicable Mete law, has
been properly described, classified and packaged, bad is In proper condition for transportation according to applicable regulations) AND, It this waste is a treatment residue of
previously restricted hazardous waste subject to the Land Disposal Restrictions. I partly and warrant that the waste has been treated In dependence with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261.
PdntedRyped Nang
Signature - Monet Day Yon,
ar ;
24. Transponder #1: Acknowledgement of Hecelpt of Materials
CPrinted/Type Name
SignaWre Fbnm Day Year
O /
�ledg
M 25, Titter #2: meht of Receipt at Materials
2 Printed?yp/d NamB
& Mre
Monet pay Year
F' l �C
26. Discrepancy Indic ion Space -
J
Q9. Facility Owner or Operator'. Ceddicatioo of receipt of waste materials covered by this manifest (except as noted in item 19) -
LL
�_ lifrlJ UlfiilYl(L :Ii1k5 fVM1XlEfltitll t(II V./Y\ (il, tyl, Arnie rUrL%fI<-MW A.1Dr
N
F PriniatlRyped Name /
Signature /� Monet pay Ye
I
L
/
TRANSPORTER#2

C���A REPUBLIC"ys
1r A SERVICES
NON -HAZARDOUS WASTE MANIFEST 4481167
1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of
S. Generator's Neme antl Mailing Atldress
6_ Generating Location I different) _
�.nprkrue WlldtaN An):•oi t
whiddi Or
4. Phone ( f-iwaoGe. �.'. ehalb nw wr nl._,
6. Phone( )
7rter#1 Company Name
_ t
8, US EPA ID Number
S. Transponerllt's Phone
10, Transporter X2Company Name
11. US EPA ID Number
12. Transporter 41 Phone
13. Designated TISID Facility Name antl Site Atldress
14. US EFAd. Number
15. Facility's PM1one
M. Legal NfOIerNNtl F.d tiAnr.Lru, iVl. 1[t1117
IJA il:;i dLi A Jet
1fi. Waste Stripping Name antl Dascriplion
1]. Republic Services Approval# and Exp. Date
18. Containers
19, Teter
20. Unit
Quantity
Weal
No.
Type
O
a
1tl(+I1 1 Id211IWU6 bUl1
CUiJ I of rWGcii1
b.
w
up
S
p.
J
)
/
21. Additional Descriptions for Materials Listed Above
22 Special Handling Instructions and Atltlitionel Information
fors attx �Yib5n
23. GENERATOR'S CERTIFICATION: I hereby codify, that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste Is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I codify and warrant that the waste has been treated in aaordancs with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261.
PrinteorTyped Name
Signature Mrvrr6 pay Yaar
¢
24, Transporter #1: Acknowledgement of Receipt of Materials
PrictiallName
Signature...�-- Idanm pay v r
O
--.._
of25.
Transporter n: Acknowledgement of Pare of of Materials
a
¢
PrintedR pad Neme
V
SignaWre Monrn pay Year
F
i
26. Diserepasay indication Space
F
J
G27. Facility Owner or Operator Ceniflcation of receipt of waste materials covered by tM1ls manifest (except as notetl in Item 19)
LL
O
N
F Printetl?VPad Name 6l,nature� n, her Yea
I/Vt
TRANSPORTER#1

REPUBLIC'^
SERVICES
NON -HAZARDOUS WASTE MANIFEST M 4481i68
1, Generator's US EPA ID Number Manifest Document Number
2. Page 1 of
3. Generator's Name and Mailing Address
S. Generating Location (if different)
tenanted Lovifilaa ASl
Pf 10 hen of W 'A
6316 Monldlald Dr.
1.1.41sapa, W, 2WOa
4. Phone( gWr6 a, NC 2520s /(M:3N1Oim
6. Phone l ) /O"')Ial UI:f€1
T. Transporter #1 Company Name
S. US EPA Ip Number
9. Transporter #1'a Phone
Tc
_
10. Trransporcer Co ame J
11. US EPA ID Number
12. Transporter #2's Phone
13, Designated TIS/D Facility Name and Site Address
14, US EPA ID Number
15. Fadlity's Phone
i li Landfill 5105 Abfallead lid Conill NC 2"7
/Oq./ll 2534 x'36!
16. Waste Shipping Name and Description
17. Republic Services Approval A and Exp. Date
16. Containers
19. Total
20, Unit
Quantity
WWOI
No.
T pe
9Ad XI F✓
Yd it] Oydee
K
O
4 b
III
W
2
21. Additional Descriptions for Materials Listed Above
22. Special Handling Instructions and Additional Information
BW aml i.1365U
23, GENERATORS CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, It this waste is a treatment resitlue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I certity and warrant that the waste has been treated In accordance with the requirements of 40
CFR 266 and Is no longer a hazardous waste as defined by 40 GET 261,
Printetl/fypd Name
Signature,f Monm oay v.=:
24.Transporter#1: Acknowledgement of Receipt of Materials �.
to Printed yp tl Name Sign oay Yeer
�— /tyrervronm
pi
as 25. Trans orter#2: Ac owletlgemant of Rewip[of Matenals
2 Printed/typed Name
Signatme Monm pay ven:
F
26, Discrepancy Indication Space
Y
F
4 27. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except as noted in Item 19)
LL
GM5 LANDFILL Rich MCnitnHLAG RU s,,ACAfiRif Iw 2ixiY: AAEU52-[ li A.1Ri
As
F Prinled?yped Name )
Signature M nm Day vea:.
TRANSPORTER#2

5;W REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFEST,
I Generator's US EPA ID Number Maniteat Document Number 2. Page 1 of
_
3. Gene t N ntl M I g Atltlress 5 Ge e2ting LocaYon(t tlifferent)
¢sir A 1 CN t re"'14Ri be ?W2
4. Phone ( 1...... e. Phone
].Transporter at Company Name
B.US EPA ID Number
9. Transporter#1's Phone
10. Transporter#2 Company Name
11. US EPA ID Number
12. Transporter 42's Phone
13. Designated TISID Equably Name and Site Address
14. US EPAiD Number
15. Facillty's Phone
I. FRlI Fh O riiY MOURNell 411(_p:u Ct fib l,VeI
16. Waste Shipping Name antl Description
17. Republic Services Appmval#and Esp. Date
1B.Centainers
19. Total
20, Unit
Quantity
WWOI
Nc.
Type
_
is 'is
be
O
(vPh Kd2bfU(NiOtl
biilel NSf r4(r i4110 i9
b.
W
Up
W
L.
21. Additional Descriptions for Materiels Listed Above
22. Special Handling Instructions and Additional Information
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 SEE 261 or any applicable state law, has
been properly described, classified and packaged and is In proper condition for transportation according to applicable NAUiations; AND, if waste is a treatment residue of
previously restricted hazardous waste subject to the land Disposal Restrictions. I certify and warrant that the waste has been treated In accordance with the requirements of 40
CFF 268 and is no longer a hazardous waste de defined by 40 CFR 261.
Prinied?yped Name
Signature Monm oey Year
24.1ransporter8l: Acknowletlgement of Receipt of Materials
IW-
Printed/typed Name Signature - —" '-- Noah ady her
O_...�
I
b�mi__Lc ""--' 11 �'I
W
25.TransporterN2: Acknowletlgement of Receipt of Materials
Q
Prinied/trP dl�afne
Signature Per
M•(�/
'.. '�` f
/Y
rW'N� J
C
26. Discrepancy IndLCetion Space
F
J
Es
LL
27. Facility Owner or Operator'. Certification of receipt of waste materials covered by this manmet (except as noted in 119)
Es
N
F
Printetl/typed Name Signature M qey
IM 5Y
TF
TRANSPORTER41

C��REPUBLIC
SERVICES
NON -HAZARDOUS WASTE MANIFEST= 4481173
1. Generator's US EPA ID Number Manifest Document Number
2. Pass 1 of
3. Generator's Name and Mailing Address
5, Generating Location iif different)
0wrii DorgNa AflW
W 16 Mwff it Or.
Ill Mlnrrflllil Br.
Chor sal NC 20206
4. Phone ( Cp1aMW. NC 28206 /w Ant (If N
6, Phone ( ) 104 361 0139
]. Transporter #1 Company Name
6. US EPA ID Number
9. Transporter or's Phone
10. Tr`alispoddr 42 Dow my Nam
11. US EPA ID Number
12. Transpoder#2's Phone
13. Designated T/SID Facility Name and Site Add..
14, US EPA D Number
15, Facility's Phone
M$ Lignoll 5109 Murano w Rd Igor w, WC 2BOd 7
IN NA) 2004 X ae?
16.Containers 19, Total 20. Unit
16. Waste Shipping Name and Description
ITRepublic Services Applovel#and Exp. Date
Quantity wwol
No. Type
lim In Ill
Fri In below
It
0
a b.
w
w
izI
v
21, Additional Descriptions far Materials Uptetl Above
22. Special Handling Instructions and Additional Information
coal accI133:3659
23. GENERATOR'S CERTIFICATION: I hereby cedity that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable gate law, has
been properly described classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been hosted In accordance with the requirements of 40
CFR 266 and is no longer a hazardous waste as defined by 40 CFR 261.
Printed/Typed No a
Signature ,, Month Day rear
. 1. — ErJ
-.1 IJ
IL 24.Transporter %1: Acknowledgement of Receipt of Materials
W PrW[ed/ryped Name
0
SignaWre _ Moom pay veer
_
d 2
In 23.-ran arter e2:Acnowledgement of Receipt of Materials
QPre intd?yped Name
$,,note. Month pay Year
F
26. Discrepancy Indication Space
J
Q 2]. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except es noted In Item 19)
LL
GAS LANDFILL 5iub Mih26 ' L D cjy i )RR NN, del / r w-r --iiMe A Job
Vi
F Printemryped Name
Signature _ 7
Oa
7
TRANSPORTER#

`2 REPUBLIC'
Y SERVICES
NON -HAZARDOUS WASTE MANIFEST
4481174
1, Generator's US EPA ID Number
Manifest Document Number
2. Page 1 of
�3. Generator z Name and Maling Address
5G ailleg Location (if different)
r l AUdWx PXjIpR
Mot!mh 1./
53 1 AMr mw wrx
frae ING wt'.
a _ ._
'I'm J IJL-I J'l ur
L
4. Phan6( I
6 Phone ( )
].Transporter #1 Company Name
8. US EPA ID Number
9. Transporter or's
Phone
10. Transpoder#2 Company Name .i
11. US EPA ID Number
12. Transporter Asia Phone
13. Designated TIS/D Facility Name and Site Address
14. US EPA ID Number
15. Facility's PM1one
andlt, 151011AURstmp6 iiQ._mK.Oftl_ PIL, 80,7
,
)'..g
16. Waste Shipping Name and Description
17. Republic Services Approval # end Eep. Date
18. Containers
19. Total.
20. Unit
Quantity
wwal
No.
Type
aYi Is owns,nl
pl lWl.Yi
2
O IVQp N'ii2G1(N!rY JUN
ne I i I!:/ IIll l.Pttl
b
W
/
21, Additional Descriptloos for Materials Listed Above
Ito Special Handling Instrudlons antl Atltlitlonal Information
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous Waste as defined by 40 CFR 261 or any applicable state few, has
been properly described, classified and packaged. and Is In proper condition for trensporlation according to applicable regulations; AND, If this
waste Is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions, I hardly and warrant that the waste has been treated In accordance with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261.
Printetlllyped Name
Signature `
MwM Oay Year
_
C 24, Transporter #1'. Acknowledgement of Receipt of Materials _
F Pllntetl?yped Name
Signal are` -
Mon In Oay Year
K
2 25,Transporter 62', Acknowledgement of Receipt of Materials
F Pi Yp9tlrvame
$igadtpr¢
Month Day gear
J/ /
26, Discrepancy indication Specs
I / r /
r
C
J
LL27. Facility Owner or Operator Certification of receipt of waste materials covered by this manifest (except as noted in Item 19)
n
F Pnntetllrypetl Ndm¢ Signature
Monrh y
/
TRANSPORTER M
1

REPUBLIC
Z� SERVICES
UBL
NON -HAZARDOUS WASTE MANIFESTM
4481175
1. Genaraior's US EPA ID Number Manifest Document Number
2. Page 1 of
3. Generator's Name and Mailing Address
5. Generating Location (it different) / —
,.narNribDDugltuAlfpDll
63 id Mbrrafeb L.
4)18IAorrklMb d.
Ctwrlofc. NC 2111
4.Phanel (ts uitt Ul:fS
6. Phone l )
XA.ifir Uj Jy
]. Transporter#1 Company Name
8. US EPA ID Number
9. Transporter#1's Phone
ly
i 6. Trenspo ei#2 Com Name _1
11. US EPA 10 Number
12. Transporter 42's Phone
13. Designated Tl$ID Facility Name and Site Address
14, US EPA ID Number
15. Facility's Phone
V.S LartU(1115'105 AbreRBiU HO Cooled NC <1102i
rU4-ill 2Q04 k 361
16, Waste Shipping Name antl Description
17. Republic $ervle¢s Approval#and Exp, Date
18. Containers
19, Tend
26, unit
Quantity
vil
Na.
Type
III m f1Bl01Ar
r in In OAarw
O
m
_
ad
Z
ad
r
21. Additional Descriptions for Materials Listed Above
'1
22. Special Handling Instructions and Additional Information
_
ON iccL#333669
23. GENERATORS CERTIFICATION: I hereby c und, that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, class fled and packaged, and is in proper condition for transportation according to applicable regulations;
AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Ricandrions. I certify antl warrant that the waste has been treated in accordance with the requirements of 46
CFR 268 and Is no longer a hazardous waste as defined by 46 RFR 261.
Pi ated/ryped Name
Signature
)�
Monrh Oey Year
_ _Sl r�
do 24.Transporter Ill: Acknowledgement of Receipt of Materials
F Printod?ypad Name - - - Signaure
HbnM Dax ✓ r
as 25 Tra p had u2 Acknowledgement of Receipt of Materials
_
2 Printetlrtypetl Name
Signa�ur�--
yarn Day Year
1-
S
I
26, Discrepancy Indication space
a
I-
J
Q2. Facility Owner or Operator: Certification of receipt of waste materials covered by u11s manifest (except as noted in
LL
Item 19)
GM5 LANDFILL ndu AhD RD C)NI jw. 114¢ ?iro-; ern z us I .a,
N
F Firm ed?vped Name
Signature
M Day
V
TRANSPORTER R2

REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFESTM 4481203
1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 Of
3. Generator's Name and Malling Address Location (If different)
1.P101W110 UOUj Hdl,rtd
]5Generating
(.$1 F. IAorcllnuttl ...
GiIHrWtle.:�. r,a.3n i u i_35
4. Phone ( ) 6 phone ( J
]. Transpoder #1 Company Name
e. US EPA ID Number
9. Transporter #1'a Phone
10. Transporter 42 Company Name
11. US EPA 10 Number
12. Tmnspoder #2's PM1one
IS. Designated TIED Facility Name and Site Address
14. US EPAIDNumber
15. Facility's PM1one
{
M5 L6rfOi111 � IIYa MatarmaG Fti:<<i1✓.-Did, Wi. [iH±e i
.,, 2e d..:..
16 Waste Shipping Name and Descdream
17. Republic Services Appmval#and Exp. Date
18.Cma iners
19, Total
20. Unit
Readily
WWOI
No.
Type
Q
O
ah", i8ealyd iK SOM
;i,c, to-r,4?7
b.
2
W
w
c
21. Additional Descriptors for Materiels Listed Above
22. Special Handling Instructions and Additional Information -
23. GENERATOR'S CERTIFICATION: hereby codify that the above named material is not a hazardous waste as defined by 40 GFR 261 or any applicable state law, has
been properly described classified and packaged, and is in proper condition for transportation aocoming to applicable regulations: AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I cedlfy and warrant that the waste has been treated In accordance with the requirements
of 40
CFR 268 and Is no longer a hazardous waste as defined by 40 CFR 261,
Pnntaidayped Name —
Signature Monts Cry
real
24. Transpoder#1: Acknowledgement of Receipt of Materials
ad
R inted/ryped Name
Signature Monet Day
Year
O
2 25. Transporter#2: Acknowledgement of Receipt of Materials.—
MPrime pa �� IGA,�
SignaWre r - rn oey
L 7�
year
/017am 1,
4
26. Discrepancy defloston Space J
T
F
J
Q2). FacI11Yy Owner or Operator: Codification of receipt 0f waste materials covered by this manifest (except as noted in Item 19)
LL
N
F Pnntetl?yped Name 1 signature nro y
Year
J(
TRANSPORTER #1

REPUBLIC'
SERWCES \.
e
NON -HAZARDOUS WASTE MANIFEST= 4481204
1. Generator's US EPA ID Number
Manifest Document Number
2. Page 1 of
3_ Generators N and M 'I ng Address
5 Generating Location (If different)
. i r _-f vh Adve..
.,....
'6'8 M.... !silIl [a
i.;hpurlie. i-4r._ rca Jig ..� ,. r..,.
4. PM1one( )
6. Phone( )
]. Transporter#1 Company Name
S.US EPA ID Number
9. Transporter #1 a Phone
10. Transporter#2 Company Name _,
11. US EPAID Number
12. Tamagnpeir Phone
13. Designated I If Facility Name and Site Address
14, US EPA ID Number
15. Facility's Phone
Miss i bfir i 5 iUrb MGI Iwar Aul t_4.c5 Ol tvG etA%d i
16. Waste Shipping Name and Description
17. Republic Services Approval# and Up. Date
16. Containers
19. Thing
Si Unit
Country
wi
N0.
Type
wik, Up uslk �za
a d.
a
of
Z
of
_
/
t0
/l
�
!
1
2TAdditional Descriptions for Materials Listed Above - "- - 1
22. Special Handling lnstmctions and Additional Information
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, he.
been properly described classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of
previously restricted hazardous waste subject to the Land Disposal Restrictions. I supply and warrant that the waste has been treated in accordance with the requirements of 40
DFR 266 and Is no longer a hazardous waste as defined by 40 CFR 261.
Printetl?yped Name
sid
Signature Monts pay per
C 24. Transponder fill Acknowledgement of Receipt of Materials
F Printer ad Name Signature Monts pay Year
r C • '
poReceipt Oi Matebel5 -
2 25. Transponder Acknowledgementot
a Prinla E Name Signature ) Month pay Year,
for Discrepancy Indic tics Space
J
LL2. Facility Owner or Operator Comficatlon of receipt of waste materials covered by this manliest (except as noted In Item 19)
N
PdntatlRyPetl Name �SlgnalUre MonfM1 pay Yeer
F
TRANSPORTER#1
-,a4%po�iSi's

REPUBLIC--
SERVICES J
NON -HAZARDOUS WASTE MANIFEST IIW4481205
1. Generator's US EPA ID Number Manifest Document Number
2. Page 1 of
3. Generator's Name and Meiling Address
5. Generating Location (ii Oflereng
Chanel Wiggi Airpon
Os18 N7orkiiii. U,.
5318 MarrMll C1t.
Cip rinaa, W, 2il2U8
1-hatbW, NC 2a20b au odl u at,
iue .ka i u l3s
4. Phonol )
6. Phone( )
]. Transporter #1 Company Name
8. US EPA ID Number
9. Transporter#PS PM1one
10. Train poer#20ompa Name
11. US EPA ID Number
12. Transporter#2'a Phone
14. US EPA ID Number
15. Facility's PM1one
13. Designated TISID Facility Name and Site Address
- M51an515151(15 ManYKatl litl C.OfIC4rtl, POL, 25U37
IN 192."a x � t
16. Waste Shipping Name end Description
9, Republic Sony.. Approval # and E., data
18, Contain
19. Total
20. Unit
Quantity
Wood
No.
Type
bun rT r
If, lafni
a Non Flazanow Soft
5115-"17811 111 IS
b.
w
w
21. Additional Descriptions for Materials Listed Above
22, Spacial Handling Instructions and Additional Information
DW accl.t33d559
23, GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hezartlous waste as tlefinetl by 40 CFR 261 or any applicable state lase has
been properly described, diesel and packaged and Is In proper condition for transportation assuming to applicable regulations;AND, if this waste is a treatment residue of
previously restbcted hazardous waste sublet[ to the Land Disposal Restrictions. I certity and warren[ that the waste has been traatatl In accordance with the requirements of 40
PER 268 and is no longer a hazardous waste as defined by 40 CFR 261.
Prnle ib?yped No,.
Signature Monln Oay ¢ar
6 24. Transporter 6l: Acknowledgement of Receipt of Materials
w Printetl?yped Name
Signature Monts Day Year
6 ,..Q
1` IGG
N 28: hpor anster#2:Acknowledgement cl Receipt of Materials -
zQ
2 Printed[T/yped Name
Sture lgoa`\j
1 Monet ony Yaar
26. Discrepancy Indlcaticn Space
EJ
Q 27. Facility Owner or Operator. Generation of receipt of waste materials savored by this manliest (except as noted In Item 19)
LL
o GMS LAND -ILi 6106 MlikEiFAO ftU WNulH.u, w; i1W(i I(,w-tg,. Afµ x,.Dl
N
F Printed/Typed Nam
Signature 2 Monet Dey vear
TRANSPORTER#2

r��REPUBLIC
SERVICES REP ICES 1 sL�:,KY �I a -
NON -HAZARDOUS WASTE MANIFESTM
4481206
rIGerator's UPS ID Number Manifest Document Number) 2. Page 1 of
I
3. Generator's Name and Mailing Address
5. Generating Location (if different)
c,nign fM Lxul Ail
w IO Awnivieru ut
63'I8 Mordo%l1 Dr.
ClyrlDl NC ?l
L),tmrw. w, NC 28200 / W :wn u1'.w
I" Via 10131,
4. Phone (
6. Pbone ( )
7.Transpoder#1 Company Name
B. US EPA ID Number
9. Transaction#1's Phone
10. Transpoter #2 Company Name
J1, US EPA ID Number
12, Transporter #Ts Phone
13. Designated TIS/D Facility Name and SIte Address
14. US EPA ID Number
15, Facility's Phone
li WIWI)610d1 MORAnes" rid(AQngps .14L sl1
704,792-Iub4 XT67
16. Waste Shlaping Name and Description
17, Republic Services Approval# and Exp. Date
18. Containers 19.
Total
20. Unit
Quantity
VJiNOI
No.
Type
Nunes zalwo 504
501G IbI ill iW2bF IV
a b.
M
w
z
up
�-
c.
c Jc.
21. Additional Descriptions for Materials Listed Above
22. Special Handling Instructions and Additional Information _
pail Dun: Al
23, GENERArOH'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable slate law, bas
been properly described. clacadred and packaged and Is in proper condition for transportation according to applicable regulations', AND, if this waste Is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I caMy and warrant that the waste has been treated In accordance with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 4o CFR 261.
Printod?yped Name
Signature Mom, og- vvar
24. Transporter It, Acknowledgement of Receipt of Materials
CPrinted/Typ dName Signature _ .,a pay veer
f0e
an 25. Tr p b"i�F%ceipl of Materials
Pented?yped Name
Signature Monm oey vea.
F
26, Discrepancy Indication Space
T
F
J
G27, Facility Owner or Operator: Competition of receipt of waste materials coveretl by this manifest (except as noted in Item 19)
do
O GMSVINI 6106W.)RtEHIlI R11 lAhto0ll, l,, ho, b(-Ajue,a,
N
Printed?yped Name
Signature Monm oay near
TRANSPORTER#2

�aD REPUBLIC I `51 r Q 5 6�1 l
Z► SERVICES
NON -HAZARDOUS WASTE MANIFESTM
4481207
1, Generator's US EPA ID Number Manifest Document Number
2. Page 1 of
3. Generator's Name and Mailing Address
S. Generating licimmon (if different)
ChorloW Douplii Alrpart
w id Mprr15141d Cx.
I AbFrIMNId OF.
Chadod+. INC 28206
C�loii' NC 2&106 rue �d1 Jv:M1
764 361 013ei
a. Phone(
6. Phone ( )
7. Transporter#1 Company Name
8. US EPA ID Number
9. Transporter 41's Phone
-
I . rnspormr#2. CempanyName
11. USEPAIDNumber
12. Transporter#2's Phone
13. Designated TISID Facility Name and Sit- -Atltlress
14. US EPA 10 Number
15. Facility's Phone
Mi LiOdfdi 010E ►lnririiid Rd F Mtlfrd, W, 2Wd7
7UA. 74e.sesul A 4ai
16. Waste Shipping Name and Description
17. Republic Serviras Approval# and Ezp.0ate
13. Conta!nere 19.
Total
26. Unit
Quantity
Ail
No.
Type
111 11,
ad Non i-lizerces" tioll
ik]iwib-1'191'1 Ir)rta ly
a b.
Is
z
J
i
21. Additional Oesoriptions for Materials Listed Above
22. Special Handling Infatuations and Additional Information
hill icaf333E59
23. GENERATOR'S CERTIFICATION: hereby comity that the above named material is not a hazardous waste as defined by 40 OFR 261 or any applicable state law, has
been properly described, classified and packaged, and Is In proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I codify and Warrant that the waste has been treated in accordance with the requirements of 40
OFF 268 and is no longer a hazardous waste as defined by 40 CFR 261,
PrintedlTyp d Name
Sign@W M-sh Oay veer
,, ) � - J — T
7 _ . ,. � I I a
IL 24.Transporter #1: Acknowledgement of Receipt of Materials
W Printed/Typed Name
SgnaWre
Mam. Oey Year
al
— - _
LL
4porter42'.
_.
W 25. Acknowledgementof Receipt of Materials
RPrinWd?ypetl Name
Signature Ioay veer
F
26. Discrepancy indication Space
F
J
Q27, Facility Owner or Operetoc Cognomen of receipt of waste materials covered by this manifest (axcept as noted in Item 19)
LL
O ��LAIVtii-iLt.ytlid lM➢tEiit71D RG +UNw!<ii, rqG (ikui ruwioi-e: uti <..Wi
N
F Printetl/fypetlName �� l
Signature in Day vYR
toMMM
J
TRANSPORTER N2wmmiwil

�REPUBLIC' _ /ir`�7
DD SERVICES
a
NON -HAZARDOUS WASTE MANIFEST 4481208
1. Generator's US EPA ID Number Manifest Document Number 2. Pagel of
3. Generators Name and Mailing Address
5. Generating Location (if different)
Grwtlpib Lotsda as AR{wtl
01914 IVfolualm91d Lu
6319 Mor-jiff d Dr
rhaMaq, 1120209
G1w1IIl1iE•, Ni 2UUI5 .U4 w1 GlAe
%Uy abou V
4. Phone ( )
6, Phone ( )
].Transporter ell Company Name
8. US EPA ID Number
9. Transporter#1'a Phone
1
)
10. Transporteri Company surang,
11. US EPAID Number
12. Transporter#2's Phone
13. Designated T/S/D Facility Name and Site Address
14. US EPA ID Number
15. Facility's Phone
t Mile LanaVI151ot! f111DMn"G NO C:O9bOla, i 21111121
704 /BI.ltNl., x -Ac!
16, Waste Shipping Name and Description
T]. Republic Sewlbes Approval # and &p. Date
18. Oentamade
19. Total
2S Unit
puantiry
WWoI
-
o.
pe
--
a.
NOR 0 rtasardi Stall
601 u- U& 11971 10idnp19
a d.
w
w
_
21. Additional Decorations for Materials Listed Above
22. Special Handling Instructions and Additional Information
oN ectl.Y333fi6ti
23. GENERATOR'S CERTIFICATION: I hereby county that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described classified and packaged and is in proper condition for transportation according to applicable regulations; AND, If fiis waste is a treatment residue 0f a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated In accordance with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261,
PdntetlRypetl Name
Signs Iore
,all
Day
ear
C 24. Transporter #1: Acknowledgement of Receipt of Materials
Pr nted/ryped Name
SlgnaWre Menlh pay Yeer
o ,f -;
Nam_
.
0 25.Transporter#Acknowledgement 4. AcknowleReceipt of Materials
< PrintedRyped Name
Slynatwe MOMM1
Oay Year
F
26. Discrepancy Indication Space
r
C
J
3 27. Facility Owner or Operetac Certification of receipt of waste materials covered by fluid s manifest (except as noted in Item 19)
LL
c CMS UNNfI1161 W M1iFtILNFAu but uirtititiu, or, ?;vdu /o4..r n< rw4 n sp,
N
F PdntetlRyped Name
Signature Mont Oaa ycyr,
TRANSPORTER#2

���REPUBLIC"
SERVICES
NON -HAZARDOUS WASTE MANIFEST=
4481209
1. Generator's US EPA ID Number Manifest Document Number
2. Page i of
_
3. Generator's Name and Mailing Address S. Gene rating Location(if brdenl)
t 111,00ollo Douglas Purport Sd Ia Morimew ES
RIiA Mornaflyld DI CrMrblp, W. MOO
ChalgW P1L 26[0B r� Jti1 U1 Jet
704 A0 t ul dg
4. Phone ( 6. Phone ( J
]. Transporter #1 Company Name 6.US EPA ID Number
9. Trans porter #I one
T
I
10. Transporter#2 Compa
11, US EPA ID Number
12. Transactor 42. Phone
13. Designatetl LSID Facility Namaland Site Atltlress
14, US EPA ID Number
15. Facility's Phone
MS LaMNI 510& MGreread Rd C.arecoard, IVC Z8027
]Q<-/Sl 2GDC % 36i
16, Waste Shipping Name and Description
17. Republic Services Approval #and Up, Date
1S. Contalnem
19. Total
a. Unit
Quantity
Wwol
No
Type
O¢ Non Tograndll Boll
501u1&1757710/etalal
Q b.
Op
W ad
Z
/
c.
21. Atltlitional Descriptions for Materials Listed Above
-
22. Special Handling Instructions and Additional Information
bill ak"La
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as tlermed by 4 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is In proper condition for transportation according to applicable regulations;
AND, if this waste is a treatment esidue of
previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warren[ that the waste has
been treated in accordance with the requirements of 44)
CFR 263 and is no longer a hazamed, waste as defined by 49 CFR 261.
Printed/Typed Name
Sgnature
Mann usy Year
24,Transporter Ni'. Acknowledgement of Receipt of Materials
P
2 Priated/T d Name
Signature
I natu a -�
9
Mon16 Day Year
W 25.Transporter 42'. Acknowledgement of Receipt of Materials
QP(ntedl'yped Name Signature
Y Yaar ManrM1 Oa
I-
26-Debrecen, Indication Spaoe
J
R2]. Facility Owner or Operetor: Certification of receipt of waste materials covered by this manifest (except as noletl in
LL
Item i97
p .MBIAHOHLL 67UiM <i: u_A;ndrx., r rn e alF.,u �.Ir.v.
N
F PnntedRypetl Name �
Signature -,
_
Monm oay ear
TRANSPORTER#2

�REPUBLIC'
D SERWCES
NON -HAZARDOUS WASTE MANIFEST M 448i210
1. Generator's US EPA ID Number Manifest Document Number
2. Page f of
3. Generator'sName and Mailing Address
5, Carl Location (if different)
4hiu6ra lol u"s Ara l
wid MUYnerl Ur.
5318 MpnMNld Dr
CMrlone. NC 20i
LIAMi .Pill 2b2(iH rWf111a1 Mff
lure Jib, oftSy
4. Phone ( )
6. Phone ( 1
7. Transporter#1 Company Name
6. US EPA ID Number
9. Transporter Al's Phone
T �tA
10. Transporter#2 Company Name
11, US EPA ID Number
12, Transporter #2'1 Phone
13. Designated T/S/D Faculty Name and Site Address
14, US EPA ID Number
15. Faciliq's Phone
Mti Legal blob MDIYMid Rd Siff liAla, ei zdUZ9
]Of.]u2TD0A %267
16. Waste Shipping Name and DescHptlon
t]rRepublle Services Approval #and Exp, Date
18.6ontoners
19. Royal
20. Unit
Country
WWol
No.
Type
O Nan H®zeuci wall
SUIRD- &1]J/i 110,411
a b.
w
w
21, Additional Descriptions for Materials Listed Above
22. Special Handling Instructions and Additional Information
bia uU.Y3:i3dors
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged and Is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions, I Certify and warrant that the waste has been treated in accordance with the monochrome of 40
GFR 268 and Is no longer a hazardous waste as defined by 40 CFP 261,
PrintedRyped Name
Signature Month pay v r
Its 24. Transporter#1 Acknowledgement of Receipt of Materials
2 Primed/Typed Name
Signature _ -" _, Month Day leer
__..
O
6
2 25. haneporter k2'. Acknowletlgem6nt of Receipt of Materiels
Pdntedayped Name
Signature Mon,, pay Year
F
26, Discrepancy Indication Space
C
J
Q27. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except as noted in Item S)
LL
o Gill itN1]HLLSllra MUREHLAi7 HG GGM.rnul .xi_ rtavr >a4 nl,-item .cr,
N
F Pdntedlfyped Name ^-y--
Signature --, MunM pay Year
�v
t'
or
TRANSPORTER X2
21

t REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFEST= 4481211
1, Generator's US EPA Io Number Manifest Document Number
2. Page 1 of
3. Generator's Name and Melling Address
5, Generating Location (if different)
[.I Idoft the JOi so(UOrl
� Ib spolun lNµl Lrt,
S,Y1tyfkooafw Qf
CbehfbtN, pY'_- 2e1015
�.. be Gotle. Mt, e6206 k4 uvl 0kpi
NP1361 0139
.
4Phone ( 7
6. Phone ( )
J. Transporter 41 Company Name
S. US EPA ID Number
9. Transporter to's Phone
1
yr
10. Transporter 12 Company Name -
11. USEPAID Number
12, Transporter#2's Phone
13. Designated TIED Facility Name and Site Address
14. US EPA ID Number
15. Facility's Phone
I. i Laf (IN 816E MWOIh O HO -01ILuf0. hi 2811
]UA 152-..1(W 'I I,,
16. Waste Shipping Name and Description
17. Republic Services Approval# and Exp. Data
16. Containers
19, Total
20, Unit
Quantity
WtlVdI
No.
Typo
I In in prache
O effort HiMbdua OBSOfI
rsul(J-1. "lot, tblFbi6
Q b.
W
up
up
O
1
-D
21. Atltlitional Descriptions for Materials Listed Above -
22. Special Handling Instructions and Additional Information
bill accLS333i
23. GENERATORS CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has
been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations: AND, if this waste is a treatment residue of a
previously restricted hazardous waste subject to the Lead Disposal Restrictions. I codify and warrant that the waste has been treated in accordance with the requirements of 40
CFR 263 and Is ne longer o hazardous waste as defined by 40 CARD 261,
Pdntetlayped Name
Signed, to Month ... year
_
be 24. Transporter #i'. Acknowledgement of Receipt of Materials
ttPrintedayped Name
Signature Moron pay year
- e
d
ra 25, Transporter #2'. Acknowledgement of Receipt of Materials
Z
sis Pentedayped Nam.
_
SIgrIGY. o More pay or.,
//
I._
26, D(sorepency Indication Space
F
Demarcation of receipt of waste materials covered by this manifest (except as noted In Item 19)
MZ,,Ah rILL OLU h9UnL LAI, RUQIN601i0, ll 1ie/ irW-Ib<-]iuC,r jo,
LOperator.
t
Signature�l Monm oey veer
TRANSPORTER 0

a ��� REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFEST
44 1212
1. Generator's US EPA ID Number ManXe9 Document Number
2. Paget of
3. Generator's Name and Mailing Address
5, Generating Location (it different)
g313 MorM1Ml4 Dr.
Cixfrblk. W. 282%
1..N0f edbi H 262UB I119.ur, blue
iO4 36. (1136
4. Phone ( 1
S. Phone ( )
7. Transporter#1 Company Name
8,US EPA ID Number
9. Transporter #1's Phone
1
10. Transpoder#2 Com ny Name J
11. US EPA ID Number
12. Tmnspmler#2's Phone
10, Designotatl TISID Facility Name and Site Address
14. US EPA 10 Number
16. Facilltys PM1one
MS L.ardnll 511 Mofatrea6 NO t,.nnoOrb. IVi. 2B(/27
7N M "A X A67
18. Containers 1g. Total 20. Unit
16. Waste Shipping Name and Description
17. Republic Services Appmvel#and E,.Date
Daanliry "i
No. Type
m
o Non HararlbLN SM
SOiu18,11977 iW2briS
Q b
IN
w
/OCR
21. Additional Descriptions for Materials Listed Above
22, Special Handling Instructions and Additional Information
bill pcclLtd i3i
23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste ser defined by 40 CFR 261 or any applicable state law, has
been properly described classified and packaged, and is In proper condition for transpodati0n according to applicable regulations;
AND, it this waste is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I certily and warrant that the waste has
been treated in accordance with the requirements of 40
CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261.
Pdntedayped Name
Slgnat0le
Well Oay Year
_
24.Transporter#1-. Acknowledgementof Receiptaf Materals
of
P mb driyped Name Signal .��
'� Monm Day veer
f�-----�---'
i..�1.4Z-4-,—
Z 2117re p her #2'. Ack
rig t of Reco pt of Matenals
QPrinted/Typed Name
Signature
xxxi Day Year
26. iscrepancy Indication Space
i
F
J
Q27, Facility Owner or Operator; Correction of receipt of waste materiels coveretl by this manifest(except as noted in
LL
Item lBJ
p OM6 LArylI11LLp1lK`VUl(LIILHJ'nll4lANL.OrtILNr. v4'I. W-r JLdW4
N
F Printed?yped Name
Signature
MontM1 Day
TRANSPORTERN2

REPUBLIC'
SERVICES
NON -HAZARDOUS WASTE MANIFEST 4 I L 13
1. Generator's US EPA ID Number Manliest Document Number 2. Page 1 of
3. Generator's Namo and Melling Address 5. Generating Londn, (If different)
4. Phone l 6. Phone( )
]. Transpoder Nl Company Name 8, US EPA ID Number 9. Transporter Nl's Phone
10. Transporter U2 Company Name
11, US EPA ID Number
12. Transporter N2's PM1one
13. Designated TIS/D Facility Name and Site Addincess
14. US EPA ID Number
15. Facility's Phone
M:, i990 P1 a61ERBelU fin lcry t A !flb.:;
) g14 y ,h
13. Waste Shipping Name and Description
17. Republic Seroces Approval Nand Exp.Date
18. Containers
19. Total
20. Unit
Quantity
WWel
No.
pe
a.
Tandn iozeubus bake
O
aut.2 ro- 'u,I
a d.
as
ad
1
I
21. Additional Descriptions for Materials Listed Above
22. Special Handling Instructions and Additional Information
23. GENERATOR'S CERTIFICATION: I hereby comfy that the above named material is not a hazardous waste as defined by 40 Cl 261 or any applicable state law, has
been properly described classified and packaged, and Is in proper condition for transportation According to applicable regulations; AND, If this waste Is a treatment residue of a
previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated In accordance with the requirements of 40
DER 268 and Is no longer a hazardous waste as defined by 40 OFR 261,
Printetl/typed Name - _.,
Signature sk" Day year
as 24.TransporterN1'. Acknowletlgement of Receipt of Materials
F Pented/typed Name
Signature monm usy veer
0
i25, Transporter 02'. Acknowledgement of Receipt of Materials
QPrinted/Typed Name
Signature edi Pan Year
F
26. Discrepancy Indication Space
i
F
J
Q2]. Facility Owner or Operator: Combination of receipt of waste mansions covered by this manifest (except as noted in Item 19)
LL
N
F Prin[ed?yped Name Signature - 'f tAagrh Day Fg1 wr
r
L) V
TRANSPORTER#1

tr
Uj
z
W
r�
R
��Z AgFIJ v; � sT
HAZgRdpUB WAgTf� MphIIF � _�-
1. Generatork In; ePA ID MrmbM MWVVRI C?p(yxl+enl iJumpo,A p)(n 5
J`
3. ppeertlh•Ir's Mara snA ttlMllnp Address _ - flan t!f dlllurorlli
H0r III I11,WW LA
1►kw T%R. d N Nr 1 U i
Cj9p ' +
A Phom I 1 `' 7c� n ...:t Ajb rw dot WAV ----
— Wi-g Prone
�nsporW
. Transpadef
rraNameUS 6A tdN',AOFf8, Tran>tpp{1°rrrr2 Co R _~~~ _
�"ny NBrne _
11. US CPA ID NW4110t
_ 16. Facility
's phone
•_ Deslpnated 7rS]D Faniiry Name and $ItA Address
+6. B $hipping Name and Description
2T. Adrkr al oesrainm� for Marerfals t fisted Abova
54. UUS EpA iD Nllr"
fwi rez•tv.d x ��
18. Total 2d. Unit
17• Repubec Services Approval N and DP-
I) IS. Containers f}uant4 WtNoi
W. TYQe
F. ,n ice'''
' i �R.s snaAedaanar rnlarm�•�•
� g2 SpLYf3f ygndlrl�g rnsrrU
G�ry�gpTOri CS��R77FrCArlpH• I hereby cart+fY that the above named material is not a hazardous waste as defined by 40 CFR 251 or any appticarile stale law, has
!beerrF�perly desorid d' dassifred and paclraged, and is in proper condition for transportation according to applicable regulations; ANO, if this waste is a treatment residuo o{ a
prevrnuslyresrricrad hazard°us waste suBject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements o[ 46
CFR 268 and is no ranger a hazardous waste as defined by 40 CFR 261.
Signature
Month Day Year
Prrnfe ITd Name - _ Y
Transporter#i: Rck 0:lodgement Of Receipt of Materials
;Fe r hyped Nature
S � -
snsporter i#2: Acki 00edgernOnt of Receipt of Materials
5yped Name
apancy Indica
signature
]wrier or Operator, Certification of receipt of waste materials covered by this manifest texcept as noted in item 19)
ame f T T Signature
TRANSPORTER =L
Month
Month Day Yea
Day

REPUBLIC
SERVICES
NON -HAZARD
t. Generalorg US EPA lD Number _ DuS WASTE MANIFEST
Manifest Documanl Number -—to_
2- P9g®+ ---
3- Generators Name and Mallur4 Andress
M1k
1 b. Ganeralrnp LocnUon flf rldfernnli
C Phone
7. Pansportez st ComPany Name
Ir:
10
. Transporter *2�ny Name
13- Deslg odlea TYSID Fa d} .
1dY Name and Site Address
11 MS
U"X" StLilo tMDf6t541fif; rtdC.Dr+1CWIl, t51i 2A[J2i
"I Waste $hipping Name and basrr Wrenn
Orc. 4
it >x
t ❑
b.
z
ua
21. Addi '.J
22. Spoc al Hand.
for Materials Listed Aboua
e, phone t 1
EPA ID Number
11, US EPA ID Number
14, US EPA 10 Number
9. Transporler A1's phone
12. Transporter #2's Phone
15. Facillty's Phone
17. Rapubflc Sarvlces Rpproial u and Exp, Date 1a. Containers 19- Total 20, U-nit
Quantity W Wo1
No. Typo
�3• CE'f�WXArfON, t hereby Certify that the above reamed material is not a hazardous Waste as defined by 40 CFR 261 ar any applicable state
G'1: 1 .01 a law, has
been Properly described, ctassifred and packaged, and is in proper condition for transportation accardfng to applicable regulations; AS+117, it this waste is a treatment rasiaue of s
PrR 268ra restricted hazardous waste subject to the Land Disposaf Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements of 4
CFq 2 fig and is rfo longer a hazardous waste as defined by 40 CFIg 261-
Prirrted/ryped IV,.,,, Monett nay Y
� Signature
24- transporter
#7' An Prinreowledgement of Receipt of Materials
d/rY Nairle _ Month Day
'} �- Signature
rra
A°►'ter #2: Rcknowl�gemenr of Receipt of Materials
int8dt7- _
Yaar
f q Marne Si nature yI fNorlrh Day rear
!,•�, r ` s � ` 1 I
:"Ity Dwn re
Pod Nan7e
Of receipt of waste materials covered by this manifest (except as rioted in Item 19)
Slgnarure
TRANSPORTER #1
mVrlin uay Year

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
APPENDIX B
PHOTOGRAPHS

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina
Wood Project: 6228-18-0503
PHOTO 1:
,.
' View of UST prior to
removal.
Im
J
PHOTO 2:
Pooled petroleum
noted beneath tank
upon removal.

Initial Abatement Action Report - GADO Building
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina
Wood Project: 6228-18-0503
November 26, 2018
PHOTO 3:
Pooled petroleum
noted beneath tank
upon removal.
PHOTO 4:
UST being removed
from excavation.

Initial Abatement Action Report - GADO Building
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina
Wood Project: 6228-18-0503
` _i'
er
November 26, 2018
PHOTO 5:
Corrosion holes noted
in UST.
PHOTO 6:
Corrosion holes noted
in UST.

Initial Abatement Action Report - GADO Building
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina
Wood Project: 6228-18-0503
i ..,.
.. � _... �..R.. Wit- •� ,
1
November 26, 2018
PHOTO 7:
Petroleum pooled
beneath tank on soil.
PHOTO 8:
Corrosion hole
measurements.

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
APPENDIX C
UST-2B FORM

UST-2B
Site Investigation Report for Permanent Closure or Change -in -
ND
Service of
UN -REGISTERED UST
Return completed form to:
STATE USE ONLY:
NC DEQ / DWM / UST SECTION
Facility ID #
1646 MAIL SERVICE CENTER
RALEIGH, NC 27699-1646
ATTN: REGISTRATION & PERMITTING
Date Received
phone [phone] fax [phone] htti)://www.wastenotnG.org/
INSTRUCTIONS (READ THIS FIRST)
1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank
Closure and Initial Response and Abatement. The guidelines can be obtained at http://deg.nc.gov/abouUdivisions/waste-management/waste-
management-permit-quidance/underground-storage-tanks-section.
2. Permanent closure: Complete all sections of this form.
3. Change -in-service: Where UST systems will be converted from storing a regulated substance to a non -regulated substance, complete sections I,
II, III, IV, and VI.
4. For more than 5 un-registered UST systems, attach additional forms as needed.
5. Un-Registered USTs may be subject to unpaid fees and late penalties.
6. REGISTERED USTs use Form UST-2A.
I. OWNERSHIP OF TANKS
II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
Charlotte Douglas International Airport
Facilityy Name or Company
GAD O Building
Street Address
Facility ID # (If known)
5601 Wilkinson Boulevard
00-0-0000033447
City County
Street Address
Charlotte Mecklenburg
5318 Morris Field Drive
State North Carolina Zip Code 28208
City County Zip Code
Charlotte Mecklenburg 28208
Phone Number
Phone Number
704/560/9242
None
III. CONTACT PERSONNEL
Contact for Facility:
Job Title:
Phone #: [phone]
Mr. James McDorman
Env. Comp. Coord
Closure Contractor Name:
Closure Contractor Company:
Address:
Phone #
Nate Jones, Jr.
Jones Grading & Fencing, Inc.
1726 Toal Street
704/331-9225
Primary Consultant Name:
Primary Consultant Company:
Address:
Phone #
Robert Foster
Wood E & I Solutions
2801 Yorkmont Road
704-357-5530
IV. UST INFORMATION FOR UN -REGISTERED UST SYSTEMS
V. EXCAVATION CONDITION
REGISTERED LISTS use Form UST-2A.
Tank ID
Size in
Last
Last
Permanent
Method of Permanent Closure:
Change -in-
Notable
No.
Gallons
Contents
Use
Close Date
Indicate REMOVED or enter fill
Service
Waterin
Free product
odor or
visible soil
Date
material, such as foam!
Date
excavation
contaminatio
concrete/ sand
n
—Yes—F
No
Yes
No
Yes
No
1
1,400
Fuel oil
1990
10/19/2018
REMOVED
NA
❑
❑.
❑
❑.
❑
❑
❑
❑
❑
❑
❑
VI. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate
and complete.
Print name and official title of owner or owner's authorized representative
James McDorman, Enviornmental Compliance Coordinator
Signature
Date Signed
11 /27/2018
INORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastengtnc.orq/ 1/2016

Initial Abatement Action Report - GADO Building November 26, 2018
5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208
Wood Project: 6228-18-0503
APPENDIX D
LABORATORY ANALYTICAL REPORT AND CHAIN -OF -CUSTODY FORM

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
October 24, 2018
Rob Foster
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: 5318 Morris Field Drive
Client Job Number:
Project Number: 6228-18-0503
Laboratory Work Order Number: 18J1029
Enclosed are results of analyses for samples received by the laboratory on October 20, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 15

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
18J1029-01
18J1029-02
Sample Preparation Information
QC Data
Petroleum Hydrocarbons Analyses
B215272
B215425
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
7
9
10
10
10
10
11
12
13
Page 2 of 15

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100 REPORT DATE: 10/24/2018
Charlotte, NC 28208 PURCHASE ORDER NUMBER:
ATTN: Rob Foster
PROJECT NUMBER: 6228-18-0503
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18J1029
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 5318 Morris Field Drive
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
TB-1 18J1029-01 Soil SM 254OG
SW-846 8015C
TB-2 18J1029-02 Soil SM 2540G
SW-846 8015C
Page 3 of 15

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 8015B GRO elevated reporting limit for samples 18J1029-01+02 due to high concentrations of target compounds.
SW-846 8015C
Qualifications:
S-01
The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit required from high analyte
concentration and/or matrix interferences.
Analyte & Samples(s) Qualified:
2-Fluorobiphenyl
18J1029-01[TB-1],18J1029-02[TB-2]
SW-846 8015C
Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard.
Diesel Range Organics (C10-C28) is quantitated against a calibration made with a #2 fuel oil standard.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 4 of 15

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029
Date Received: 10/20/2018
Field Sample #: TB-1 Sampled: 10/19/2018 13:45
Sample ID: 18.11029-01
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) 620 61 59 mg/Kg dry 50 SW-846 8015C 10/22/18 10/22/18 18:22 EEH
Diesel Range Organics 15000 2100 760 mg/Kg dry 100 SW-846 8015C 10/20/18 10/22/18 13:04 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 108 70-130 10/22/18 18:22
2-Fluorobiphenyl * 40-140 S-01 10/22/18 13:04
Page 5 of 15

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029
Date Received: 10/20/2018
Field Sample #: TB-1 Sampled: 10/19/2018 13:45
Sample ID: 18.11029-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 78.3 % Wt 1
SM 2540G 10/21/18 10/22/18 12:00 KMG
Page 6 of 15

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029
Date Received: 10/20/2018
Field Sample #: TB-2 Sampled: 10/19/2018 13:50
Sample ID: 18.11029-02
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) 650 74 71 mg/Kg dry 50 SW-846 8015C 10/22/18 10/22/18 18:57 EEH
Diesel Range Organics 12000 2100 750 mg/Kg dry 100 SW-846 8015C 10/20/18 10/22/18 13:22 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 115 70-130 10/22/18 18:57
2-Fluorobiphenyl * 40-140 S-01 10/22/18 13:22
Page 7 of 15

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029
Date Received: 10/20/2018
Field Sample #: TB-2 Sampled: 10/19/2018 13:50
Sample ID: 18.11029-02
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 76.3 % Wt 1
SM 2540G 10/21/18 10/22/18 12:00 KMG
Page 8 of 15

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ` FAX [phone] " TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
18J1029-01 [TB-1]
B215295
10/21/18
18J1029-02 [TB-2]
B215295
10/21/18
Prep Method: SW-846 3546-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18J1029-01[TB-1]
B215272
15.2
1.00
10/20/18
18J1029-02 [TB-2]
B215272
15.7
1.00
10/20/18
Prep Method: SW-846 5035/5030B-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18J1029-01[TB-1]
B215425
6.70
6.40
10/22/18
18J1029-02 [TB-2]
B215425
5.70
6.40
10/22/18
Page 9 of 15

Table of Contents
icon-tes w .
ANALYTICAL LABORATORY
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215272 - SW-846 3546
Blank (B215272-BLK1)
Prepared: 10/20/18 Analyzed: 10/21/18
Diesel Range Organics
ND
8.3
mg/Kg wet
Surrogate:2-Fluorobiphenyl
LCS (B215272-BS1)
2.01
mg/Kg wet
3.33 60.3
Prepared: 10/20/18 Analyzed: 10/21/18
40-140
Diesel Range Organics
22.9
8.3
mg/Kg wet
33.3 68.8
40-140
Surrogate:2-Fluorobiphenyl
LCS Dup (B215272-BSD1)
1.86
mg/Kg wet
3.33 55.7
Prepared: 10/20/18 Analyzed: 10/21/18
40-140
Diesel Range Organics
25.6
8.3
mg/Kg wet
33.3 76.7
40-140 10.8
Surrogate:2-Fluorobiphenyl
Batch B215425 - SW-846 5035/5030B
2.09
mg/Kg wet
3.33 62.6
40-140
Blank (B215425-BLK1)
Prepared & Analyzed: 10/22/18
Gasoline Range Organics (GRO)
ND
1.0
mg/Kg wet
Surrogate: 1-Chloro-3-fluorobenzene
LCS (B215425-BSI)
16.8
µg/L
15.0 112
Prepared & Analyzed: 10/22/18
70-130
Gasoline Range Organics (GRO)
0.216
0.010
mg/Kg wet
0.250 86.5
80-120
Surrogate: 1-Chloro-3-fluorobenzene
LCS Dup (B215425-BSD1)
15.9
µg/L
15.0 106
Prepared & Analyzed: 10/22/18
70-130
Gasoline Range Organics (GRO)
0.236
0.010
mg/Kg wet
0.250 94.2
80-120 8.59 30
Surrogate: 1-Chloro-3-fluorobenzene
16.6
µg/L
15.0 ill
70-130
Page 10 of 15

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 * FAX [phone] " TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
fi Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
S-01 The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit
required from high analyte concentration and/or matrix interferences.
Page 11 of 15

icon-tes w .
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street ` East Longmeadow, MA 01028 ' FAX [phone] " TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8015C in Soil
Gasoline Range Organics (GRO) NY,VA,NH,NC
Diesel Range Organics NY,VA,NH,NC
The CON -TEST Environmental Laboratory operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA
Massachusetts DEP
M-MA100
06/30/2019
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2019
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI
Rhode Island Department of Health
LA000112
12/30/2018
NC
North Carolina Div. of Water Quality
652
12/31/2018
NJ
New Jersey DEP
MA007 NELAP
06/30/2019
FL
Florida Department of Health
E871027 NELAP
06/30/2019
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME
State of Maine
2011028
06/9/2019
VA
Commonwealth of Virginia
460217
12/14/2018
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW
North Carolina Department of Health
25703
07/31/2019
Page 12 of 15

Table of Contents
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10/20/2018 Track your package or shipment with FedEx Tracking
Table of Contents
Travel History
10/20/2012 - Saturday
1019i2018 - FriGay
TRACT( ANOTHER SHIPMENT
77352398130b �`t
Delivered
Saturday 10/20/2018 at 9:46 am
DELIVERED
Signed for by: R.PATRAIDAS
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
FROM
Charlotte, NC LIS
TO
EAST LONGMEADOW, MA US
Shipment Facts
9A6 am
Expand History V
3,04 pm
OUR COMPANY MORE FROM FEDEX
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Table of Contents
I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Relinquishing
Over Samples
J).oc# 277 Rev $ 2.07
Login Sample Receipt Checklist - (Rejection Criteria Listing - using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client MC7C5�'�Zve i
Received By Date
How were the samples In Cooler No Cooler
received? Direct from Sampling
time
On Ice_
Ambient
No Ice
Melted Ice
Were samples within
By Gun # Actual Temp - Cl
Temperature? 2-6°C
By Blank # Actual Temp -
Was Custody Seal Intact?
Were Samples Tampered with?
Was COC Relinquished ?
Does Chain Agree With Samples? i
Are there broken/leaking/loose caps on any samples? ---
Is COC in ink/ Legible? --T--
Were samples received within holding time? �—
Did COC include all Client
Analysis Sampler Name
pertinent Information? Project
ID's - - Collection Dates/Times
Are Sample labels filled out and legible?
Are there Lab to Filters?
��
Who was notified?
Are there Rushes?
T—
Are there Short Holds?
A
Is there enough Volume?
Is there Headspace where applicable?
Proper Media/Containers Used?
-�
Were trip blanks received?
Do all samples have the proper pH?
jam' Acid
Who was notified? I'm
Who was notified?
MS/M S D?
Is splitting sampled required?
On COC? ��
Base

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
October 25, 2018
Rob Foster
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: 5318 Morris Field Drive
Client Job Number:
Project Number: 6228-18-0503
Laboratory Work Order Number: 18JI I I I
Enclosed are results of analyses for samples received by the laboratory on October 23, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 16

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
18J1111-01
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/MS
B215524
Petroleum Hydrocarbons Analyses
B215447
B215565
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B215520
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
5
5
8
9
9
9
10
10
10
11
11
12
13
14
Page 2 of 16

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce StreetEast Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100 REPORT DATE: 10/25/2018
Charlotte, NC 28208 PURCHASE ORDER NUMBER:
ATTN: Rob Foster
PROJECT NUMBER: 6228-18-0503
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18J1111
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 5318 Morris Field Drive
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
Stockpile 18J1111-01 Soil SM 254OG
SW-846 8015C
SW-846 8260B
Page 3 of 16

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 8015B GRO elevated reporting limit for sample 18J1111-01 due to high concentrations of target compounds.
For method 8260B elevated reporting limit for sample 18J1111-01 due to high concentrations of non -target compounds.
SW-846 8015C
Qualifications
S-01
The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit required from high analyte
concentration and/or matrix interferences.
Analyze & Samples(s) Qualified:
2-Fluorobiphenyl
18J1111-01[Stockpile]
Qualifications:
RL-13
Elevated reporting limit due to high concentration of non -target compounds.
Analyte & Samples(s) Qualified:
18JI I 11-01 [Stockpile]
SW-846 8260B
SW-846 8015C
Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard.
Diesel Range Organics (C 10-C28) is quantitated against a calibration made with a #2 fuel oil standard.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 4 of 16

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1111
Date Received: 10/23/2018
Field Sample #: Stockpile Sampled: 10/22/2018 15:20
Sample ID: 18.11111-01
Samnle Matrix: Soil
Sample Flags: RL-13 Volatile Organic Compounds by GC/MS
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Benzene ND 0.79 0.095 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF
Ethylbenzene 3.8 0.79 0.10 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF
Toluene 1.8 0.79 0.13 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF
m+p Xylene 8.7 1.6 0.20 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF
o-Xylene 4.2 0.79 0.10 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 83.6 70-130 10/25/18 0:59
Toluene-d8 101 70-130 10/25/18 0:59
4-Bromofluorobenzene 98.2 70-130 10/25/18 0:59
Page 5 of 16

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1111
Date Received: 10/23/2018
Field Sample #: Stockpile Sampled: 10/22/2018 15:20
Samnle ID: 18J1111-01
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) 390 78 76 mg/Kg dry 50 SW-846 8015C 10/24/18 10/24/18 13:34 EEH
Diesel Range Organics 7300 1100 410 mg/Kg dry 100 SW-846 8015C 10/23/18 10/25/18 10:35 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 113 70-130 10/24/18 13:34
2-Fluorobiphenyl * 40-140 S-01 10/25/18 10:35
Page 6 of 16

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1111
Date Received: 10/23/2018
Field Sample #: Stockpile Sampled: 10/22/2018 15:20
Samnle ID: 18J1111-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.0 % Wt 1
SM 2540G 10/24/18 10/24/18 11:09 MJR
Page 7 of 16

Table of Contents
40 ,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID] Batch Date
18J 1111 -0 1 [Stockpile] B215520 10/24/18
Prep Method: SW-846 3546-SW-846 8015C
Lab Number [Field ID] Batch Initial [g] Final [mL] Date
18J 1111 -0 1 [Stockpile] B215447 30.3 1.00 10/23/18
Prep Method: SW-846 5035/5030B-SW-846 8015C
Lab Number [Field ID] Batch Initial [g] Final [mL] Date
18J1111-01[Stockpile] B215565 5.80 6.60 10/24/18
Prep Method: SW-846 5035-SW-846 8260B
Sample Methanol Methanol Final
Lab Number [Field ID] Batch Amount(g) Volume(mL) Aliquot(mL) Volume(mL) Date
18J 1111 -0 1 [Stockpile] B215524 5.65 6.53 0.1 50 10/24/18
Page 8 of 16

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215524 - SW-846 5035
Blank (B215524-BLK1) Prepared & Analyzed: 10/24/18
Benzene
ND
0.050
mg/Kg wet
Ethylbenzene
ND
0.050
mg/Kg wet
Toluene
ND
0.050
mg/Kg wet
m+p Xylene
ND
0.10
mg/Kg wet
o-Xylene
ND
0.050
mg/Kg wet
Surrogate:l,2-Dichloroethane-d4
Surrogate: Toluene-d8
Surrogate:4-Bromofluorobenzene
LCS (B215524-BS1)
0.0210
0.0251
0.0244
mg/Kg wet
mg/Kg wet
mg/Kg wet
0.0250 84.1
0.0250 100
0.0250 97.7
Prepared & Analyzed: 10/24/18
70-130
70-130
70-130
Benzene
0.0110
0.0011
mg/Kg wet
0.0113
97.4
70-130
Ethylbenzene
0.0123
0.0011
mg/Kg wet
0.0113
108
70-130
Toluene
0.0119
0.0011
mg/Kg wet
0.0113
105
70-130
m+p Xylene
0.0237
0.0023
mg/Kg wet
0.0227
104
70-130
o-Xylene
0.0119
0.0011
mg/Kg wet
0.0113
105
70-130
Surrogate: 1,2-Dichloroethane-d4
0.0233
mg/Kg wet
0.0283
82.4
70-130
Surrogate: Toluene-d8
0.0285
mg/Kg wet
0.0283
101
70-130
Surrogate:4-Bromofluorobenzene
0.0277
mg/Kg wet
0.0283
97.8
70-130
LCS Dup (B215524-BSD1)
Prepared & Analyzed: 10/24/18
Benzene
0.0111
0.0011
mg/Kg wet
0.0113
97.7
70-130
0.308
25
Ethylbenzene
0.0118
0.0011
mg/Kg wet
0.0113
104
70-130
3.58
25
Toluene
0.0118
0.0011
mg/Kg wet
0.0113
104
70-130
1.34
25
m+p Xylene
0.0230
0.0023
mg/Kg wet
0.0227
101
70-130
2.97
25
o-Xylene
0.0115
0.0011
mg/Kg wet
0.0113
102
70-130
3.19
25
Surrogate:l,2-Dichloroethane-d4 0.0238 mg/Kg wet 0.0283 84.1 70-130
Surrogate: Toluene-d8 0.0286 mg/Kg wet 0.0283 101 70-130
Surrogate:4-Bromofluorobenzene 0.0274 mg/Kg wet 0.0283 96.6 70-130
Page 9 of 16

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215447 - SW-846 3546
Blank (B215447-BLK1)
Prepared: 10/23/18 Analyzed: 10/25/18
Diesel Range Organics
3.2
8.3
mg/Kg wet
J
Surrogate:2-Fluorobiphenyl
LCS (B215447-BS1)
2.43
mg/Kg wet
3.33 72.9
Prepared: 10/23/18 Analyzed: 10/25/18
40-140
Diesel Range Organics
29.7
8.3
mg/Kg wet
33.3 89.2
40-140
Surrogate:2-Fluorobiphenyl
LCS Dup (B215447-BSD1)
2.68
mg/Kg wet
3.33 80.4
Prepared: 10/23/18 Analyzed: 10/25/18
40-140
Diesel Range Organics
28.0
8.3
mg/Kg wet
33.3 84.0
40-140 5.98
Surrogate:2-Fluorobiphenyl
Batch B215565 - SW-846 5035/5030B
2.45
mg/Kg wet
3.33 73.6
40-140
Blank (B215565-BLK1)
Prepared & Analyzed: 10/24/18
Gasoline Range Organics (GRO)
ND
1.0
mg/Kg wet
Surrogate: 1-Chloro-3-fluorobenzene
LCS (B215565-BSI)
17.3
µg/L
15.0 115
Prepared & Analyzed: 10/24/18
70-130
Gasoline Range Organics (GRO)
0.230
0.010
mg/Kg wet
0.250 92.0
80-120
Surrogate: 1-Chloro-3-fluorobenzene
LCS Dup (B215565-BSD1)
17.1
µg/L
15.0 114
Prepared & Analyzed: 10/24/18
70-130
Gasoline Range Organics (GRO)
0.226
0.010
mg/Kg wet
0.250 90.4
80-120 1.80 30
Surrogate: 1-Chloro-3-fluorobenzene
17.4
µg/L
15.0 116
70-130
Page 10 of 16

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215520 - % Solids
Duplicate (B215520-DUPI) Source: 18J1111-01 Prepared & Analyzed: 10/24/18
% Solids 72.2 % Wt 73.0 1.09 20
Page 11 of 16

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
fi Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
RL-13 Elevated reporting limit due to high concentration of non -target compounds.
S-01 The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit
required from high analyte concentration and/or matrix interferences.
Page 12 of 16

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8015C in Soil
Gasoline Range Organics (GRO) NY,VA,NH,NC
Diesel Range Organics NY,VA,NH,NC
SW-846 8260B in Soil
Benzene
NC
Ethylbenzene
NC
Toluene
NC
m+p Xylene
NC
o-Xylene
NC
SW-846 8260C in Soil
Benzene
CT,NH,ME,VA,NY
Ethylbenzene
CT,NH,ME,VA,NY
Toluene
CT,NH,ME,VA,NY
m+p Xylene
CT,NH,ME,VA,NY
o-Xylene
CT,NH,ME,VA,NY
The CON -TEST Environmental
Laboratory operates under the
following certifications and accreditation:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA
Massachusetts DEP
M-MA100
06/30/2019
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2019
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI
Rhode Island Department of Health
LA000112
12/30/2018
NC
North Carolina Div. of Water Quality
652
12/31/2018
NJ
New Jersey DEP
MA007 NELAP
06/30/2019
FL
Florida Department of Health
E871027 NELAP
06/30/2019
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME
State of Maine
2011028
06/9/2019
VA
Commonwealth of Virginia
460217
12/14/2018
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW
North Carolina Department of Health
25703
07/31/2019
Page 13 of 16

Table of Contents
10/23/2018 Track your package or shipment with Fedl Tracking
EI
,,
W :, ..
Delivered
Tuesday 10/23/2018 at 9.14- am
DELIVERED
Signed for by: B BECCA
GET STATUS UPDATES
OBTAIN PROOF OF DELIVERY
FROM TO
Charlotte. NC US LAST LCNGMEADOV%{ MA US
Multiple -piece Shipment
3 Piece shipment
TRACKING NUMBER SHIPPER CITY, STATE SHIP DATE STATUS DELIVERY DATE DESTINATIOWR£CIPIENT
CITY, STATE
7735373D1375 CHARLOTTE, NO 10/22/2018 l U/2WO'l8 EAST LONGMEADOW, MA
(master)
773537302393
CHARLOTTE, NO
10/22/2018
10/23/2018
EAST LONGMEADCW, MA
773537302485
(,HARLOTTE, NC
10/22/20'18 -
0I28/2018
LASI" LONGMEADOW, MA
Shipment Facts
TRACKING NUMBER
SERVICE
MASTER TRACKING NUMBER
77353730239
Fcedtx Standard OVemQhit
773537301375
WEIGHT
DIMENSIONS
DELIVERED TO
10 ihs / 454 kgs
13x10x9 in.
Shippsng/Receiving
TOTAL PIECES
TOTAL SHIPMENT WEIGHT
TERMS
3
10 Ill / 4.54 kgs
Third Party
PACKAGING
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Your Packaging
Deliver Weekday, Additioral Handling
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Page 15 of 16

Table of Contents
c�
I Have Not Confirmed Sample Container r
Numbers With Lab Staff Before Relinquishing
Over Samples
Login Sample Receipt Checklist - (Rejection Criteria Listing - using Acceptance Policy) Any False
§tatement will be brought to the attention of the Client - State True or False
Client VQ
Received By
Date
Time 0 (mod
How were the samples In Cooler -r No Cooler On Ice j No Ice
received? Direct from Sampling Ambient Melted Ice
Were samples within By Gun # S, Actual Temp -
Temperature? 2-6°C By Blank # Actual Temp -
Was Custody Seal Intact? N/V� Were Samples Tampered with? PJA
Was COC Relinquished ? i Does Chain Agree With Samples?
Are there broken/leaking/loose caps on any samples?
Is COC in ink/ Legible?
Did COC include all Client
--r
pertinent Information? Project
Are Sample labels filled out and legible?
Are there Lab to Filters?
Are there Rushes?
o'
Are there Short Holds?
Is there enough Volume?
Is there Headspace where applicable?
Proper Media/Containers Used?
T—
Were trip blanks received?
Do all samples have the proper pH?(�
Were samples received within holding time? -r
4nalysis Sampler Name T
ID's Collection Dates/Times
Who was notified?
Who was notified?
Who was notified?
MS/MSD?
Is splitting samples required?
On COC? !
Acid Base

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
October 31, 2018
Rob Foster
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: 5318 Morris Field Drive
Client Job Number:
Project Number: 6228-18-0503
Laboratory Work Order Number: 18J1112
Enclosed are results of analyses for samples received by the laboratory on October 22, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 78

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
18J1112-01
18J1112-02
18J1112-03
18J1112-04
18J1112-05
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/ 4S
B215551
B215584
Semivolatile Organic Compounds by GUMS
B215606
Petroleum Hydrocarbons Analyses - EPH
B215618
Petroleum Hydrocarbons Analyses - VPH
B215495
B215561
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
8
8
15
22
29
36
43
45
45
45
49
55
55
60
60
64
64
65
67
68
76
Page 2 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce StreetEast Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100 REPORT DATE: 10/31/2018
Charlotte, NC 28208 PURCHASE ORDER NUMBER:
ATTN: Rob Foster
PROJECT NUMBER: 6228-18-0503
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18J1112
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 5318 Morris Field Drive
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
SW-1 18J1112-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 254OG
SW-846 8260B
SW-846 8270D
SW-2 18J1112-02 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
SW-846 8260B
SW-846 8270D
SW-3 18J1112-03 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 254OG
SW-846 8260B
SW-846 8270D
SW-4 18J1112-04 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 254OG
SW-846 8260B
SW-846 8270D
TB-3 18J1112-05 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 254OG
SW-846 8260B
SW-846 8270D
Page 3 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only adjusted hydrocarbon ranges were requested and reported.
For method MA EPH, only hydrocarbon ranges were requested and reported.
For method 8260B elevated reporting limits for sample 18J1112-05 due to high concentrations of target compounds.
Page 4 of 78

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ANALYTICAL LABORATORY
Table of Contents
Qualifications
B
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
MADEP-EPH-04-1.1
Analyte is found in the associated laboratory blank as well as in the sample.
Analyte & Samples(s) Qualified:
n-Octadecane
B215618-BS1,B215618-BSD1
MS-22
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
within method specified criteria.
Analyte & Samples(s) Qualified:
n-Nonane
B215618-MS1
MADEP-VPH-Feb 2018 Rev 2.1
Qualifications:
O-01
Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered with methanol, but with
less than the method -specified amount.
Analyte & Samples(s) Qualified:
18J1112-01[SW-1]
RL-05
Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.
Analyte & Samples(s) Qualified:
C5-C8 Aliphatics
18J1112-05[TB-3]
SW-846 8260B
Qualifications:
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
Acetone
B215551-BSDI
Diisopropyl Ether (RIPE)
B215551-BSDI
Methyl tert-Butyl Ether (MTBE)
B215551-BSDI
Tetrahydrofuran
B215551-BS1
RL-11
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
18JI I 12-05[TB-3]
Qualifications:
R-05
SW-846 8270D
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
Benzidine
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18JI I12-04[SW-4], 18J1112-05[TB-3], B215606-BLK1, B215606-BSI, B215606-BSD1
Page 5 of 78

,con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
V-04
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria. Reported result is estimated.
Analyte & Samples(s) Qualified:
Benzidine
B215606-BLKI, B215606-BSI, B215606-BSD1
V-05
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
Aniline
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3]
Benzidine
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3], B215606-BLKI, B215606-BSI, B215606-BSD1
Hexachlorocyclopentadiene
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3]
V-06
Continuing calibration did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
4-Nitrophenol
B215606-BS1,B215606-BSD1
V-16
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported
result.
Analyte & Samples(s) Qualified:
Pentachloronitrobenzene
B215606-BLKI, B215606-BSI, B215606-BSD1
V-19
Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99.
Reported result is estimated.
Analyte & Samples(s) Qualified:
2,4-Dinitrophenol
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3]
V-20
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte & Samples(s) Qualified:
2,6-Dinitrotoluene
18J1112-01[SW-1], 18Jl112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3]
2-Nitroaniline
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3]
4-Nitrophenol
18JI112-01[SW-1], 18JI112-02[SW-2], 18JI112-03[SW-3], 18JI112-04[SW-4], 18JI112-05[TB-3], B215606-BLKI
Benzoic Acid
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3]
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
3-Nitroaniline
B215606-BLKI, B215606-BSI, B215606-BSDI
4-Chloroaniline
18J1112-01[SW-1], 18JI I12-02[SW-2], 18JI I12-03[SW-3], 18J1112-04[SW-4], 18JI I12-05[TB-3], B215606-BLKI, B215606-BSI, B215606-BSDI
4-Nitrophenol
B215606-BLKI, B215606-BSI, B215606-BSDI
Aniline
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18JI I12-04[SW-4], 18J1112-05[TB-3], B215606-BLKI, B215606-13SI, B215606-BSDI
Benzidine
18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18JI I12-04[SW-4], 18J1112-05[TB-3], B215606-BLKI, B215606-BSI, B215606-BSD1
Page 6 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028' FAX [phone] ` TEL. [phone]
MADEP-EPH-04-1.1
SPE cartridge contamination with non -petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-Feb 2018 Rev 2.1
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain -of -custody form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Project Manager
Page 7 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-1 Sampled: 10/22/2018 13:50
Sample ID: 18J1112-01
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0.12
0.028
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Acrylonitrile
ND
0.0071
0.0030
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0012
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Benzene
ND
0.0024
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Bromobenzene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Bromochloromethane
ND
0.0024
0.0017
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Bromodichloromethane
ND
0.0024
0.00071
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Bromoform
ND
0.0024
0.0017
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Bromomethane
ND
0.012
0.0050
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
2-Butanone (MEK)
ND
0.048
0.021
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
tert-Butyl Alcohol (TBA)
ND
0.048
0.025
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
n-Butylbenzene
0.0015
0.0024
0.00083
mg/Kg dry
1 J
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
sec-Butylbenzene
0.0015
0.0024
0.0012
mg/Kg dry
1 J
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
tert-Butylbenzene
ND
0.0024
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0012
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Carbon Disulfide
ND
0.0071
0.0051
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Carbon Tetrachloride
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Chlorobenzene
ND
0.0024
0.00083
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Chlorodibromomethane
ND
0.0012
0.00083
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Chloroethane
ND
0.024
0.0018
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Chloroform
ND
0.0048
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Chloromethane
ND
0.012
0.0076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
2-Chlorotoluene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
4-Chlorotoluene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0024
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2-Dibromoethane (EDB)
ND
0.0012
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Dibromomethane
ND
0.0024
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2-Dichlorobenzene
ND
0.0024
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,3-Dichlorobenzene
ND
0.0024
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,4-Dichlorobenzene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
trans-1,4-Dichloro-2-butene
ND
0.0048
0.0025
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.024
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,1-Dichloroethane
ND
0.0024
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2-Dichloroethane
ND
0.0024
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1, 1 -Dichloroethylene
ND
0.0048
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
cis-1,2-Dichloroethylene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
trans-1,2-Dichloroethylene
ND
0.0024
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2-Dichloropropane
ND
0.0024
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,3-Dichloropropane
ND
0.0012
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
2,2-Dichloropropane
ND
0.0024
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1, 1 -Dichloropropene
ND
0.0024
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
cis-1,3-Dichloropropene
ND
0.0012
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
trans-1,3-Dichloropropene
ND
0.0012
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Diethyl Ether
ND
0.024
0.0021
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
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Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-1 Sampled: 10/22/2018 13:50
Sample ID: 18J1112-01
Samnle Matrix: Soil
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.0012
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,4-Dioxane
ND
0.12
0.069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Ethylbenzene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Hexachlorobutadiene
ND
0.0024
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
2-Hexanone (MBK)
ND
0.024
0.013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Isopropylbenzene (Cumene)
ND
0.0024
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0048
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Methylene Chloride
ND
0.024
0.0084
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.024
0.0090
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Naphthalene
0.0080
0.0048
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
n-Propylbenzene
0.0011
0.0024
0.00083
mg/Kg dry
1 J
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Styrene
ND
0.0024
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0024
0.0021
mg/Kgdry
1
SW-8468260B
10/24/18
10/24/18 11:29
MFF
1,1,2,2-Tetrachloroethane
ND
0.0024
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Tetrachloroethylene
ND
0.0024
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Tetrahydrofuran
ND
0.012
0.0026
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Toluene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2,3-Trichlorobenzene
ND
0.0024
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2,4-Trichlorobenzene
ND
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,3,5-Trichlorobenzene
ND
0.0024
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1, 1, 1 -Trichloroethane
ND
0.0024
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,1,2-Trichloroethane
ND
0.0024
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Trichloroethylene
ND
0.0024
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Trichlorofluoromethane (Freon 11)
ND
0.012
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,2,3-Trichloropropane
ND
0.0024
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.012
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
(Freon 113)
1,2,4-Trimethylbenzene
0.0038
0.0024
0.00095
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
1,3,5-Trimethylbenzene
0.00075
0.0024
0.00071
mg/Kg dry
1 J
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Vinyl Chloride
ND
0.012
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
m+p Xylene
ND
0.0048
0.0020
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
o-Xylene
ND
0.0024
0.00083
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:29
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qua]
1,2-Dichloroethane-d4
106
70-130
10/24/18 11:29
Toluene-d8
103
70-130
10/24/18 11:29
4-Bromofluorobenzene
110
70-130
10/24/18 11:29
Page 9 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-1 Sampled: 10/22/2018 13:50
Samnle ID: 18J1112-01
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.23
0.069
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Acenaphthylene
ND
0.23
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Acetophenone
ND
0.46
0.091
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Aniline
ND
0.46
0.13
mg/Kg dry
1 V-05, V-34
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Anthracene
ND
0.23
0.067
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Benzidine
ND
0.90
0.58
mg/Kg dry
1 R-05, V-05, V-34
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Benzo(a)anthracene
ND
0.23
0.061
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Benzo(a)pyrene
ND
0.23
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Benzo(b)fluoranthene
ND
0.23
0.065
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Benzo(g,h,i)perylene
ND
0.23
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Benzo(k)fluoranthene
ND
0.23
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Benzoic Acid
ND
1.4
0.25
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Bis(2-chloroethoxy)methane
ND
0.46
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Bis(2-chloroethyl)ether
ND
0.46
0.091
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Bis(2-chloroisopropyl)ether
ND
0.46
0.099
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.46
0.18
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
4-Bromophenylphenylether
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Butylbenzylphthalate
ND
0.46
0.11
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Carbazole
ND
0.23
0.060
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
4-Chloroaniline
ND
0.90
0.11
mg/Kg dry
1 V-34
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
4-Chloro-3-methylphenol
ND
0.90
0.099
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2-Chloronaphthalene
ND
0.46
0.087
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2-Chlorophenol
ND
0.46
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
4-Chlorophenylphenylether
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Chrysene
ND
0.23
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Dibenz(a,h)anthracene
ND
0.23
0.14
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Dibenzofman
ND
0.46
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Di-n-butylphthalate
ND
0.46
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
1,2-Dichlorobenzene
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
1,3-Dichlorobenzene
ND
0.46
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
1,4-Dichlorobenzene
ND
0.46
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
3,3-Dichlorobenzidine
ND
0.23
0.071
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2,4-Dichlorophenol
ND
0.46
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Diethylphthalate
ND
0.46
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2,4-Dimethylphenol
ND
0.46
0.086
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Dimethylphthalate
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
4,6-Dinitro-2-methylphenol
ND
0.46
0.44
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2,4-Dinitrophenol
ND
0.90
0.26
mg/Kg dry
1 V-19
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2,4-Dinitrotoluene
ND
0.46
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2,6-Dinitrotoluene
ND
0.46
0.082
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Di-n-octylphthalate
ND
0.46
0.24
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.46
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Fluoranthene
ND
0.23
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Flumene
0.10
0.23
0.075
mg/Kg dry
1 J
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Page 10 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-1 Sampled: 10/22/2018 13:50
Samnle ID: 18J1112-01
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Hexachlorobutadiene
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Hexachlorocyclopentadiene
ND
0.46
0.098
mg/Kg dry
1
V-05
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Hexachloroethane
ND
0.46
0.092
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Indeno(1,2,3-cd)pyrene
ND
0.23
0.17
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Isophorone
ND
0.46
0.090
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
1-Methylnaphthalene
0.39
0.23
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2-Methylnaphthalene
0.66
0.23
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2-Methylphenol
ND
0.46
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
3/4-Methylphenol
ND
0.46
0.15
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Naphthalene
0.13
0.23
0.12
mg/Kg dry
1
J
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2-Nitroaniline
ND
0.46
0.077
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
3-Nitroaniline
ND
0.46
0.067
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
4-Nitroaniline
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Nitrobenzene
ND
0.46
0.087
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2-Nitrophenol
ND
0.46
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
4-Nitrophenol
ND
0.90
0.10
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
N-Nitrosodimethylamine
ND
0.46
0.29
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
N-Nitrosodiphenylamine
ND
0.46
0.095
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
N-Nitrosodi-n-propylamine
ND
0.46
0.095
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Pentachloronitrobenzene
ND
0.46
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Pentachlorophenol
ND
0.46
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Phenanthrene
0.22
0.23
0.12
mg/Kg dry
1
J
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Phenol
ND
0.46
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Pyrene
0.10
0.23
0.076
mg/Kg dry
1
J
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Pyridine
ND
0.46
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
1,2,4,5-Tetrachlorobenzene
ND
0.46
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
1,2,4-Trichlorobenzene
ND
0.46
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2,4,5-Trichlorophenol
ND
0.46
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
2,4,6-Trichlorophenol
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:06
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
63.3
30-130
10/29/18 18:06
Phenol-d6
71.1
30-130
10/29/18 18:06
Nitrobenzene-d5
63.8
30-130
10/29/18 18:06
2-Fluorobiphenyl
56.4
30-130
10/29/18 18:06
2,4,6-Tribromophenol
95.8
30-130
10/29/18 18:06
p-Terphenyl-dl4
69.6
30-130
10/29/18 18:06
Page 11 of 78

Table of Contents
40 icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-1 Sampled: 10/22/2018 13:50
Samnle ID: 18J1112-01
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C9-C18 Aliphatics 74 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW
C19-C36 Aliphatics 25 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW
Unadjusted C11-C22 Aromatics 57 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW
C11-C22 Aromatics 55 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD) 64.7 40-140 10/29/18 2:10
o-Terphenyl(OTP) 71.2 40-140 10/29/18 2:10
2-Bromonaphthalene 94.8 40-140 10/29/18 2:10
2-Fluorobiphenyl 106 40-140 10/29/18 2:10
Page 12 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-1 Sampled: 10/22/2018 13:50
Sample ID: 18J1112-01
Samnle Matrix: Soil
Sample Flags: 0-01 Petroleum Hydrocarbons Analyses - VPH
Soil/Methanol Preservation Ratio: 1.53
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C5-C8 Aliphatics
ND 13
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 21:21 EEH
Rev 2.1
C9-C12 Aliphatics
ND 13
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 21:21 EEH
Rev 2.1
C9-C10 Aromatics
15 13
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 21:21 EEH
Rev 2.1
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2,5-Dibromotoluene (FID)
105
70-130
10/24/18 21:21
2,5-Dibromotoluene (PID)
104
70-130
10/24/18 21:21
Page 13 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-1 Sampled: 10/22/2018 13:50
Samnle ID: 18J1112-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 73.1 % Wt 1
SM 2540G 10/27/18 10/28/18 15:28 BLM
Page 14 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-2 Sampled: 10/22/2018 14:05
Sample ID: 18J1112-02
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0.13
0.030
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Acrylonitrile
ND
0.0076
0.0032
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0013
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Benzene
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Bromobenzene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Bromochloromethane
ND
0.0025
0.0018
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Bromodichloromethane
ND
0.0025
0.00076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Bromoform
ND
0.0025
0.0018
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Bromomethane
ND
0.013
0.0053
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
2-Butanone (MEK)
ND
0.051
0.022
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
tert-Butyl Alcohol (TBA)
ND
0.051
0.027
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
n-Butylbenzene
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
sec-Butylbenzene
ND
0.0025
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
tert-Butylbenzene
ND
0.0025
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0013
0.00076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Carbon Disulfide
ND
0.0076
0.0055
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Carbon Tetrachloride
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Chlorobenzene
ND
0.0025
0.00089
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Chlorodibromomethane
ND
0.0013
0.00089
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Chloroethane
ND
0.025
0.0019
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Chloroform
ND
0.0051
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Chloromethane
ND
0.013
0.0081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
2-Chlorotoluene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
4-Chlorotoluene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0025
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2-Dibromoethane (EDB)
ND
0.0013
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Dibromomethane
ND
0.0025
0.00076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2-Dichlorobenzene
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,3-Dichlorobenzene
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,4-Dichlorobenzene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
trans-1,4-Dichloro-2-butene
ND
0.0051
0.0027
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.025
0.0017
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,1-Dichloroethane
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2-Dichloroethane
ND
0.0025
0.0017
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1, 1 -Dichloroethylene
ND
0.0051
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
cis-1,2-Dichloroethylene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
trans-1,2-Dichloroethylene
ND
0.0025
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2-Dichloropropane
ND
0.0025
0.0017
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,3-Dichloropropane
ND
0.0013
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
2,2-Dichloropropane
ND
0.0025
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1, 1 -Dichloropropene
ND
0.0025
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
cis-1,3-Dichloropropene
ND
0.0013
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
trans-1,3-Dichloropropene
ND
0.0013
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Diethyl Ether
ND
0.025
0.0023
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Page 15 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-2 Sampled: 10/22/2018 14:05
Sample ID: 18J1112-02
Samnle Matrix: Soil
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.0013
0.00076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,4-Dioxane
ND
0.13
0.073
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Ethylbenzene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Hexachlorobutadiene
ND
0.0025
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
2-Hexanone (MBK)
ND
0.025
0.014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Isopropylbenzene (Cumene)
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0051
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Methylene Chloride
ND
0.025
0.0090
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.025
0.0097
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Naphthalene
ND
0.0051
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
n-Propylbenzene
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Styrene
ND
0.0025
0.00076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0025
0.0023
mg/Kg dry
1
SW-8468260B
10/24/18
10/24/18 11:54
MFF
1,1,2,2-Tetrachloroethane
ND
0.0025
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Tetrachloroethylene
ND
0.0025
0.0017
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Tetrahydrofuran
ND
0.013
0.0028
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Toluene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2,3-Trichlorobenzene
ND
0.0025
0.00076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2,4-Trichlorobenzene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,3,5-Trichlorobenzene
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1, 1, 1 -Trichloroethane
ND
0.0025
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,1,2-Trichloroethane
ND
0.0025
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Trichloroethylene
ND
0.0025
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Trichlorofluoromethane (Freon 11)
ND
0.013
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,2,3-Trichloropropane
ND
0.0025
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.013
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0025
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
1,3,5-Trimethylbenzene
ND
0.0025
0.00076
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Vinyl Chloride
ND
0.013
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
m+p Xylene
ND
0.0051
0.0022
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
o-Xylene
ND
0.0025
0.00089
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 11:54
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qua]
1,2-Dichloroethane-d4
107
70-130
10/24/18 11:54
Toluene-d8
104
70-130
10/24/18 11:54
4-Bromofluorobenzene
109
70-130
10/24/18 11:54
Page 16 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-2 Sampled: 10/22/2018 14:05
Samnle ID: 18J1112-02
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.24
0.073
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Acenaphthylene
ND
0.24
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Acetophenone
ND
0.49
0.096
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Aniline
ND
0.49
0.14
mg/Kg dry
1 V-05, V-34
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Anthracene
ND
0.24
0.070
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Benzidine
ND
0.95
0.61
mg/Kg dry
1 R-05, V-05, V-34
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Benzo(a)anthracene
ND
0.24
0.065
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Benzo(a)pyrene
ND
0.24
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Benzo(b)fluoranthene
ND
0.24
0.069
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Benzo(g,h,i)perylene
ND
0.24
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Benzo(k)fluoranthene
ND
0.24
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Benzoic Acid
ND
1.4
0.26
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Bis(2-chloroethoxy)methane
ND
0.49
0.093
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Bis(2-chloroethyl)ether
ND
0.49
0.096
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Bis(2-chloroisopropyl)ether
ND
0.49
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.49
0.19
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
4-Bromophenylphenylether
ND
0.49
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Butylbenzylphthalate
ND
0.49
0.12
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Carbazole
ND
0.24
0.063
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
4-Chloroaniline
ND
0.95
0.11
mg/Kg dry
1 V-34
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
4-Chloro-3-methylphenol
ND
0.95
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2-Chloronaphthalene
ND
0.49
0.092
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2-Chlorophenol
ND
0.49
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
4-Chlorophenylphenylether
ND
0.49
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Chrysene
ND
0.24
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Dibenz(a,h)anthracene
ND
0.24
0.15
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Dibenzofman
ND
0.49
0.085
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Di-n-butylphthalate
ND
0.49
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
1,2-Dichlorobenzene
ND
0.49
0.086
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
1,3-Dichlorobenzene
ND
0.49
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
1,4-Dichlorobenzene
ND
0.49
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
3,3-Dichlorobenzidine
ND
0.24
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2,4-Dichlorophenol
ND
0.49
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Diethylphthalate
ND
0.49
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2,4-Dimethylphenol
ND
0.49
0.091
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Dimethylphthalate
ND
0.49
0.086
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
4,6-Dinitro-2-methylphenol
ND
0.49
0.46
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2,4-Dinitrophenol
ND
0.95
0.28
mg/Kg dry
1 V-19
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2,4-Dinitrotoluene
ND
0.49
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2,6-Dinitrotoluene
ND
0.49
0.086
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Di-n-octylphthalate
ND
0.49
0.26
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.49
0.079
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Fluoranthene
ND
0.24
0.081
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Flumene
ND
0.24
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Page 17 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-2 Sampled: 10/22/2018 14:05
Samnle ID: 18J1112-02
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.49
0.086
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Hexachlorobutadiene
ND
0.49
0.086
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Hexachlorocyclopentadiene
ND
0.49
0.10
mg/Kg dry
1
V-05
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Hexachloroethane
ND
0.49
0.098
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Indeno(1,2,3-cd)pyrene
ND
0.24
0.18
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Isophorone
ND
0.49
0.095
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
1-Methylnaphthalene
ND
0.24
0.093
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2-Methylnaphthalene
ND
0.24
0.085
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2-Methylphenol
ND
0.49
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
3/4-Methylphenol
ND
0.49
0.16
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Naphthalene
ND
0.24
0.13
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2-Nitroaniline
ND
0.49
0.082
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
3-Nitroaniline
ND
0.49
0.070
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
4-Nitroaniline
ND
0.49
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Nitrobenzene
ND
0.49
0.092
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2-Nitrophenol
ND
0.49
0.13
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
4-Nitrophenol
ND
0.95
0.11
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
N-Nitrosodimethylamine
ND
0.49
0.31
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
N-Nitrosodiphenylamine
ND
0.49
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
N-Nitrosodi-n-propylamine
ND
0.49
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Pentachloronitrobenzene
ND
0.49
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Pentachlorophenol
ND
0.49
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Phenanthrene
ND
0.24
0.13
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Phenol
ND
0.49
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Pyrene
ND
0.24
0.081
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Pyridine
ND
0.49
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
1,2,4,5-Tetrachlorobenzene
ND
0.49
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
1,2,4-Trichlorobenzene
ND
0.49
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2,4,5-Trichlorophenol
ND
0.49
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
2,4,6-Trichlorophenol
ND
0.49
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:32
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
58.7
30-130
10/29/18 18:32
Phenol-d6
64.6
30-130
10/29/18 18:32
Nitrobenzene-d5
59.2
30-130
10/29/18 18:32
2-Fluorobiphenyl
53.3
30-130
10/29/18 18:32
2,4,6-Tribromophenol
86.9
30-130
10/29/18 18:32
p-Terphenyl-dl4
65.9
30-130
10/29/18 18:32
Page 18 of 78

Table of Contents
40 icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-2 Sampled: 10/22/2018 14:05
Samnle ID: 18J1112-02
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C9-C18 Aliphatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW
C19-C36 Aliphatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW
Unadjusted C11-C22 Aromatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW
C11-C22 Aromatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD) 67.3 40-140 10/29/18 3:06
o-Terphenyl(OTP) 72.4 40-140 10/29/18 3:06
2-Bromonaphthalene 97.0 40-140 10/29/18 3:06
2-Fluorobiphenyl 103 40-140 10/29/18 3:06
Page 19 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-2 Sampled: 10/22/2018 14:05
Sample ID: 18J1112-02
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - VPH
Soil/Methanol Preservation Ratio: 1.00
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C5-C8 Aliphatics
ND 19
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 21:51 EEH
Rev 2.1
C9-C12 Aliphatics
ND 19
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 21:51 EEH
Rev 2.1
C9-C10 Aromatics
ND 19
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 21:51 EEH
Rev 2.1
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2,5-Dibromotoluene (FID)
114
70-130
10/24/18 21:51
2,5-Dibromotoluene (PID)
103
70-130
10/24/18 21:51
Page 20 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-2 Sampled: 10/22/2018 14:05
Samnle ID: 18J1112-02
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 68.2 % Wt 1
SM 2540G 10/27/18 10/28/18 15:28 BLM
Page 21 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-3 Sampled: 10/22/2018 14:25
Sample ID: 18J1112-03
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0.10
0.024
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Acrylonitrile
ND
0.0061
0.0025
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0010
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Benzene
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Bromobenzene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Bromochloromethane
ND
0.0020
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Bromodichloromethane
ND
0.0020
0.00061
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Bromoform
ND
0.0020
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Bromomethane
ND
0.010
0.0043
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
2-Butanone (MEK)
ND
0.041
0.018
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
tert-Butyl Alcohol (TBA)
ND
0.041
0.021
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
n-Butylbenzene
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
sec-Butylbenzene
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
tert-Butylbenzene
ND
0.0020
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0010
0.00061
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Carbon Disulfide
ND
0.0061
0.0044
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Carbon Tetrachloride
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Chlorobenzene
ND
0.0020
0.00071
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Chlorodibromomethane
ND
0.0010
0.00071
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Chloroethane
ND
0.020
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Chloroform
ND
0.0041
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Chloromethane
ND
0.010
0.0065
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
2-Chlorotoluene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
4-Chlorotoluene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0020
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2-Dibromoethane (EDB)
ND
0.0010
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Dibromomethane
ND
0.0020
0.00061
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2-Dichlorobenzene
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,3-Dichlorobenzene
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,4-Dichlorobenzene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
trans-1,4-Dichloro-2-butene
ND
0.0041
0.0021
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.020
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,1-Dichloroethane
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2-Dichloroethane
ND
0.0020
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1, 1 -Dichloroethylene
ND
0.0041
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
cis-1,2-Dichloroethylene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
trans-1,2-Dichloroethylene
ND
0.0020
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2-Dichloropropane
ND
0.0020
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,3-Dichloropropane
ND
0.0010
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
2,2-Dichloropropane
ND
0.0020
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1, 1 -Dichloropropene
ND
0.0020
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
cis-1,3-Dichloropropene
ND
0.0010
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
trans-1,3-Dichloropropene
ND
0.0010
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Diethyl Ether
ND
0.020
0.0018
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Page 22 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-3 Sampled: 10/22/2018 14:25
Sample ID: 18J1112-03
Samnle Matrix: Soil
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.0010
0.00061
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,4-Dioxane
ND
0.10
0.059
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Ethylbenzene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Hexachlorobutadiene
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
2-Hexanone (MBK)
ND
0.020
0.011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Isopropylbenzene (Cumene)
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0041
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Methylene Chloride
ND
0.020
0.0072
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.020
0.0077
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Naphthalene
ND
0.0041
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
n-Propylbenzene
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Styrene
ND
0.0020
0.00061
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0020
0.0018
mg/Kgdry
1
SW-8468260B
10/24/18
10/24/18 12:18
MFF
1,1,2,2-Tetrachloroethane
ND
0.0020
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Tetrachloroethylene
ND
0.0020
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Tetrahydrofuran
ND
0.010
0.0022
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Toluene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2,3-Trichlorobenzene
ND
0.0020
0.00061
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2,4-Trichlorobenzene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,3,5-Trichlorobenzene
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1, 1, 1 -Trichloroethane
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,1,2-Trichloroethane
ND
0.0020
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Trichloroethylene
ND
0.0020
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Trichlorofluoromethane (Freon 11)
ND
0.010
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,2,3-Trichloropropane
ND
0.0020
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.010
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0020
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
1,3,5-Trimethylbenzene
ND
0.0020
0.00061
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Vinyl Chloride
ND
0.010
0.0011
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
m+p Xylene
ND
0.0041
0.0017
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
o-Xylene
ND
0.0020
0.00071
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 12:18
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qua]
1,2-Dichloroethane-d4
107
70-130
10/24/18 12:18
Toluene-d8
105
70-130
10/24/18 12:18
4-Bromofluorobenzene
107
70-130
10/24/18 12:18
Page 23 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-3 Sampled: 10/22/2018 14:25
Samnle ID: 18J1112-03
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.22
0.067
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Acenaphthylene
ND
0.22
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Acetophenone
ND
0.45
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Aniline
ND
0.45
0.13
mg/Kg dry
1 V-05, V-34
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Anthracene
ND
0.22
0.064
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Benzidine
ND
0.87
0.56
mg/Kg dry
1 R-05, V-05, V-34
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Benzo(a)anthracene
ND
0.22
0.059
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Benzo(a)pyrene
ND
0.22
0.069
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Benzo(b)fluoranthene
ND
0.22
0.063
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Benzo(g,h,i)perylene
ND
0.22
0.098
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Benzo(k)fluoranthene
ND
0.22
0.069
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Benzoic Acid
ND
1.3
0.24
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Bis(2-chloroethoxy)methane
ND
0.45
0.085
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Bis(2-chloroethyl)ether
ND
0.45
0.088
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Bis(2-chloroisopropyl)ether
ND
0.45
0.096
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.45
0.17
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
4-Bromophenylphenylether
ND
0.45
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Butylbenzylphthalate
ND
0.45
0.11
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Carbazole
ND
0.22
0.058
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
4-Chloroaniline
ND
0.87
0.10
mg/Kg dry
1 V-34
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
4-Chloro-3-methylphenol
ND
0.87
0.096
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2-Chloronaphthalene
ND
0.45
0.084
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2-Chlorophenol
ND
0.45
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
4-Chlorophenylphenylether
ND
0.45
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Chrysene
ND
0.22
0.069
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Dibenz(a,h)anthracene
ND
0.22
0.14
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Dibenzofman
ND
0.45
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Di-n-butylphthalate
ND
0.45
0.097
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
1,2-Dichlorobenzene
ND
0.45
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
1,3-Dichlorobenzene
ND
0.45
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
1,4-Dichlorobenzene
ND
0.45
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
3,3-Dichlorobenzidine
ND
0.22
0.068
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2,4-Dichlorophenol
ND
0.45
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Diethylphthalate
ND
0.45
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2,4-Dimethylphenol
ND
0.45
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Dimethylphthalate
ND
0.45
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
4,6-Dinitro-2-methylphenol
ND
0.45
0.42
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2,4-Dinitrophenol
ND
0.87
0.25
mg/Kg dry
1 V-19
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2,4-Dinitrotoluene
ND
0.45
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2,6-Dinitrotoluene
ND
0.45
0.079
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Di-n-octylphthalate
ND
0.45
0.23
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.45
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Fluoranthene
ND
0.22
0.073
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Flumene
ND
0.22
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Page 24 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-3 Sampled: 10/22/2018 14:25
Samnle ID: 18J1112-03
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.45
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Hexachlorobutadiene
ND
0.45
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Hexachlorocyclopentadiene
ND
0.45
0.094
mg/Kg dry
1
V-05
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Hexachloroethane
ND
0.45
0.089
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Indeno(1,2,3-cd)pyrene
ND
0.22
0.16
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Isophorone
ND
0.45
0.087
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
1-Methylnaphthalene
ND
0.22
0.085
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2-Methylnaphthalene
ND
0.22
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2-Methylphenol
ND
0.45
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
3/4-Methylphenol
ND
0.45
0.14
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Naphthalene
ND
0.22
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2-Nitroaniline
ND
0.45
0.075
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
3-Nitroaniline
ND
0.45
0.064
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
4-Nitroaniline
ND
0.45
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Nitrobenzene
ND
0.45
0.084
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2-Nitrophenol
ND
0.45
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
4-Nitrophenol
ND
0.87
0.097
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
N-Nitrosodimethylamine
ND
0.45
0.28
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
N-Nitrosodiphenylamine
ND
0.45
0.092
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
N-Nitrosodi-n-propylamine
ND
0.45
0.092
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Pentachloronitrobenzene
ND
0.45
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Pentachlorophenol
ND
0.45
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Phenanthrene
ND
0.22
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Phenol
ND
0.45
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Pyrene
ND
0.22
0.073
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Pyridine
ND
0.45
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
1,2,4,5-Tetrachlorobenzene
ND
0.45
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
1,2,4-Trichlorobenzene
ND
0.45
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2,4,5-Trichlorophenol
ND
0.45
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
2,4,6-Trichlorophenol
ND
0.45
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 18:59
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
69.8
30-130
10/29/18 18:59
Phenol-d6
77.2
30-130
10/29/18 18:59
Nitrobenzene-d5
78.3
30-130
10/29/18 18:59
2-Fluorobiphenyl
59.7
30-130
10/29/18 18:59
2,4,6-Tribromophenol
100
30-130
10/29/18 18:59
p-Terphenyl-dl4
70.6
30-130
10/29/18 18:59
Page 25 of 78

Table of Contents
40 icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-3 Sampled: 10/22/2018 14:25
Samnle ID: 18J1112-03
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C9-C18 Aliphatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW
C19-C36 Aliphatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW
Unadjusted C11-C22 Aromatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW
C11-C22 Aromatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD) 71.6 40-140 10/29/18 3:24
o-Terphenyl(OTP) 78.5 40-140 10/29/18 3:24
2-Bromonaphthalene 97.9 40-140 10/29/18 3:24
2-Fluorobiphenyl 107 40-140 10/29/18 3:24
Page 26 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-3 Sampled: 10/22/2018 14:25
Sample ID: 18J1112-03
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - VPH
Soil/Methanol Preservation Ratio: 1.12
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C5-C8 Aliphatics
ND 15
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 22:20 EEH
Rev 2.1
C9-C12 Aliphatics
ND 15
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 22:20 EEH
Rev 2.1
C9-C10 Aromatics
ND 15
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/24/18 10/24/18 22:20 EEH
Rev 2.1
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2,5-Dibromotoluene (FID)
115
70-130
10/24/18 22:20
2,5-Dibromotoluene (PID)
103
70-130
10/24/18 22:20
Page 27 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-3 Sampled: 10/22/2018 14:25
Samnle ID: 18J1112-03
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 75.8 % Wt 1
SM 2540G 10/27/18 10/28/18 15:28 BLM
Page 28 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-4 Sampled: 10/22/2018 14:40
Sample ID: 18J1112-04
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0.12
0.027
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Acrylonitrile
ND
0.0069
0.0029
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0012
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Benzene
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Bromobenzene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Bromochloromethane
ND
0.0023
0.0016
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Bromodichloromethane
ND
0.0023
0.00069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Bromoform
ND
0.0023
0.0016
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Bromomethane
ND
0.012
0.0049
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
2-Butanone (MEK)
ND
0.046
0.020
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
tert-Butyl Alcohol (TBA)
ND
0.046
0.024
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
n-Butylbenzene
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
sec-Butylbenzene
ND
0.0023
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
tert-Butylbenzene
ND
0.0023
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0012
0.00069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Carbon Disulfide
ND
0.0069
0.0050
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Carbon Tetrachloride
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Chlorobenzene
ND
0.0023
0.00081
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Chlorodibromomethane
ND
0.0012
0.00081
mg/Kg dry
I
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Chloroethane
ND
0.023
0.0017
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Chloroform
ND
0.0046
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Chloromethane
ND
0.012
0.0074
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
2-Chlorotoluene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
4-Chlorotoluene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0023
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2-Dibromoethane (EDB)
ND
0.0012
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Dibromomethane
ND
0.0023
0.00069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2-Dichlorobenzene
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,3-Dichlorobenzene
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,4-Dichlorobenzene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
trans-1,4-Dichloro-2-butene
ND
0.0046
0.0024
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.023
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,1-Dichloroethane
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2-Dichloroethane
ND
0.0023
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1, 1 -Dichloroethylene
ND
0.0046
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
cis-1,2-Dichloroethylene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
trans-1,2-Dichloroethylene
ND
0.0023
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2-Dichloropropane
ND
0.0023
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,3-Dichloropropane
ND
0.0012
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
2,2-Dichloropropane
ND
0.0023
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1, 1 -Dichloropropene
ND
0.0023
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
cis-1,3-Dichloropropene
ND
0.0012
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
trans-1,3-Dichloropropene
ND
0.0012
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Diethyl Ether
ND
0.023
0.0021
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Page 29 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-4 Sampled: 10/22/2018 14:40
Sample ID: 18J1112-04
Samnle Matrix: Soil
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.0012
0.00069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,4-Dioxane
ND
0.12
0.067
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Ethylbenzene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Hexachlorobutadiene
ND
0.0023
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
2-Hexanone (MBK)
ND
0.023
0.013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Isopropylbenzene (Cumene)
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0046
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Methylene Chloride
ND
0.023
0.0082
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.023
0.0088
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Naphthalene
ND
0.0046
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
n-Propylbenzene
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Styrene
ND
0.0023
0.00069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0023
0.0021
mg/Kg dry
1
SW-8468260B
10/24/18
10/24/18 13:58
MFF
1,1,2,2-Tetrachloroethane
ND
0.0023
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Tetrachloroethylene
ND
0.0023
0.0015
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Tetrahydrofuran
ND
0.012
0.0025
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Toluene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2,3-Trichlorobenzene
ND
0.0023
0.00069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2,4-Trichlorobenzene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,3,5-Trichlorobenzene
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1, 1, 1 -Trichloroethane
ND
0.0023
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,1,2-Trichloroethane
ND
0.0023
0.0014
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Trichloroethylene
ND
0.0023
0.0012
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Trichlorofluoromethane (Freon 11)
ND
0.012
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,2,3-Trichloropropane
ND
0.0023
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.012
0.0010
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
0.0023
0.00092
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
1,3,5-Trimethylbenzene
ND
0.0023
0.00069
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Vinyl Chloride
ND
0.012
0.0013
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
m+p Xylene
ND
0.0046
0.0020
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
o-Xylene
ND
0.0023
0.00081
mg/Kg dry
1
SW-846 8260B
10/24/18
10/24/18 13:58
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qua]
1,2-Dichloroethane-d4
108
70-130
10/24/18 13:58
Toluene-d8
105
70-130
10/24/18 13:58
4-Bromofluorobenzene
106
70-130
10/24/18 13:58
Page 30 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-4 Sampled: 10/22/2018 14:40
Samnle ID: 18J1112-04
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
0.88
0.24
0.071
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Acenaphthylene
ND
0.24
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Acetophenone
ND
0.47
0.093
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Aniline
ND
0.47
0.13
mg/Kg dry
1 V-05, V-34
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Anthracene
0.31
0.24
0.068
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Benzidine
ND
0.91
0.59
mg/Kg dry
1 R-05, V-05, V-34
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Benzo(a)anthracene
ND
0.24
0.062
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Benzo(a)pyrene
ND
0.24
0.073
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Benzo(b)fluoranthene
ND
0.24
0.066
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Benzo(g,h,i)perylene
ND
0.24
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Benzo(k)fluoranthene
ND
0.24
0.073
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Benzoic Acid
ND
1.4
0.25
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Bis(2-chloroethoxy)methane
ND
0.47
0.090
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Bis(2-chloroethyl)ether
ND
0.47
0.093
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Bis(2-chloroisopropyl)ether
ND
0.47
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.47
0.18
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
4-Bromophenylphenylether
ND
0.47
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Butylbenzylphthalate
ND
0.47
0.11
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Carbazole
ND
0.24
0.061
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
4-Chloroaniline
ND
0.91
0.11
mg/Kg dry
1 V-34
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
4-Chloro-3-methylphenol
ND
0.91
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2-Chloronaphthalene
ND
0.47
0.089
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2-Chlorophenol
ND
0.47
0.084
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
4-Chlorophenylphenylether
ND
0.47
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Chrysene
ND
0.24
0.073
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Dibenz(a,h)anthracene
ND
0.24
0.14
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Dibenzofman
ND
0.47
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Di-n-butylphthalate
ND
0.47
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
1,2-Dichlorobenzene
ND
0.47
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
1,3-Dichlorobenzene
ND
0.47
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
1,4-Dichlorobenzene
ND
0.47
0.084
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
3,3-Dichlorobenzidine
ND
0.24
0.072
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2,4-Dichlorophenol
ND
0.47
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Diethylphthalate
ND
0.47
0.084
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2,4-Dimethylphenol
ND
0.47
0.087
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Dimethylphthalate
ND
0.47
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
4,6-Dinitro-2-methylphenol
ND
0.47
0.45
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2,4-Dinitrophenol
ND
0.91
0.27
mg/Kg dry
1 V-19
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2,4-Dinitrotoluene
ND
0.47
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2,6-Dinitrotoluene
ND
0.47
0.083
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Di-n-octylphthalate
ND
0.47
0.25
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.47
0.076
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Fluoranthene
0.27
0.24
0.078
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Flumene
1.9
0.24
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Page 31 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-4 Sampled: 10/22/2018 14:40
Samnle ID: 18J1112-04
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.47
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Hexachlorobutadiene
ND
0.47
0.083
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Hexachlorocyclopentadiene
ND
0.47
0.10
mg/Kg dry
1
V-05
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Hexachloroethane
ND
0.47
0.094
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Indeno(1,2,3-cd)pyrene
ND
0.24
0.17
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Isophorone
ND
0.47
0.091
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
1-Methylnaphthalene
9.4
1.2
0.45
mg/Kg dry
5
SW-846 8270D
10/24/18
10/30/18 15:32
BGL
2-Methylnaphthalene
15
1.2
0.41
mg/Kg dry
5
SW-846 8270D
10/24/18
10/30/18 15:32
BGL
2-Methylphenol
ND
0.47
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
3/4-Methylphenol
ND
0.47
0.15
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Naphthalene
2.8
0.24
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2-Nitroaniline
ND
0.47
0.079
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
3-Nitroaniline
ND
0.47
0.068
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
4-Nitroaniline
ND
0.47
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Nitrobenzene
ND
0.47
0.089
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2-Nitrophenol
ND
0.47
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
4-Nitrophenol
ND
0.91
0.10
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
N-Nitrosodimethylamine
ND
0.47
0.30
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
N-Nitrosodiphenylamine
ND
0.47
0.097
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
N-Nitrosodi-n-propylamine
ND
0.47
0.097
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Pentachloronitrobenzene
ND
0.47
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Pentachlorophenol
ND
0.47
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Phenanthrene
4.4
0.24
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Phenol
ND
0.47
0.080
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Pyrene
1.4
0.24
0.078
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Pyridine
ND
0.47
0.076
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
1,2,4,5-Tetachlorobenzene
ND
0.47
0.084
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
1,2,4-Trichlorobenzene
ND
0.47
0.084
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2,4,5-Trichlorophenol
ND
0.47
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
2,4,6-Trichlorophenol
ND
0.47
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:26
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
59.4
30-130
10/29/18 19:26
2-Fluorophenol
64.6
30-130
10/30/18 15:32
Phenol-d6
66.1
30-130
10/29/18 19:26
Phenol-d6
72.5
30-130
10/30/18 15:32
Nitrobenzene-d5
63.7
30-130
10/29/18 19:26
Nitrobenzene-d5
77.3
30-130
10/30/18 15:32
2-Fluorobiphenyl
43.9
30-130
10/29/18 19:26
2-Fluorobiphenyl
60.4
30-130
10/30/18 15:32
2,4,6-Tribromophenol
89.6
30-130
10/29/18 19:26
2,4,6-Tribromophenol
73.3
30-130
10/30/18 15:32
p-Terphenyl-dl4
77.9
30-130
10/29/18 19:26
p-Terphenyl-dl4
74.3
30-130
10/30/18 15:32
Page 32 of 78

Table of Contents
40 icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-4 Sampled: 10/22/2018 14:40
Samnle ID: 18J1112-04
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C9-C18 Aliphatics 17 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW
C19-C36 Aliphatics ND 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW
Unadjusted C11-C22 Aromatics ND 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW
C11-C22 Aromatics ND 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD) 76.0 40-140 10/29/18 3:43
o-Terphenyl(OTP) 80.4 40-140 10/29/18 3:43
2-Bromonaphthalene 97.3 40-140 10/29/18 3:43
2-Fluorobiphenyl 106 40-140 10/29/18 3:43
Page 33 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-4 Sampled: 10/22/2018 14:40
Sample ID: 18J1112-04
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - VPH
Soil/Methanol Preservation Ratio: 0.85
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C5-C8 Aliphatics
ND 20
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/23/18 10/25/18 20:08 EEH
Rev 2.1
C9-C12 Aliphatics
ND 20
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/23/18 10/25/18 20:08 EEH
Rev 2.1
C9-C10 Aromatics
ND 20
mg/Kg dry 1
MADEP-VPH-Feb 2018
10/23/18 10/25/18 20:08 EEH
Rev 2.1
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2,5-Dibromotoluene (FID)
82.9
70-130
10/25/18 20:08
2,5-Dibromotoluene (PID)
82.8
70-130
10/25/18 20:08
Page 34 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: SW-4 Sampled: 10/22/2018 14:40
Samnle ID: 18J1112-04
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 72.2 % Wt 1
SM 2540G 10/27/18 10/28/18 15:28 BLM
Page 35 of 78

Table of Contents
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ANALYTICAL LABORATORY
Project Location: 5318 Morris Field Drive
Date Received: 10/22/2018
Field Sample #: TB-3
Sample ID: 18J1112-05
Samnle Matrix: Soil
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Description:
Sampled: 10/22/2018 13:00
Work Order: 18J1112
Sample Flags: RL-11
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Acetone
ND
14
2.7
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Acrylonitrile
ND
1.4
0.16
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
tert-Amyl Methyl Ether (TAME)
ND
0.56
0.030
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Benzene
ND
0.28
0.033
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Bromobenzene
ND
0.28
0.042
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Bromochloromethane
ND
0.28
0.062
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Bromodichloromethane
ND
0.28
0.082
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Bromoform
ND
0.56
0.059
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Bromomethane
ND
0.56
0.26
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
2-Butanone (MEK)
ND
5.6
0.66
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
tert-Butyl Alcohol (TBA)
ND
5.6
0.61
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
n-Butylbenzene
1.8
0.28
0.042
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
sec-Butylbenzene
1.7
0.28
0.036
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
tert-Butylbenzene
ND
0.28
0.034
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
tert-Butyl Ethyl Ether (TBEE)
ND
0.14
0.027
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Carbon Disulfide
ND
0.84
0.28
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Carbon Tetrachloride
ND
0.28
0.069
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Chlorobenzene
ND
0.28
0.045
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Chlorodibromomethane
ND
0.14
0.029
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Chloroethane
ND
0.56
0.078
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Chloroform
ND
0.56
0.061
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Chloromethane
ND
0.56
0.15
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
2-Chlorotoluene
ND
0.28
0.033
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
4-Chlorotoluene
ND
0.28
0.039
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2-Dibromo-3-chloropropane (DBCP)
ND
1.4
0.10
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2-Dibromoethane (EDB)
ND
0.14
0.041
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Dibromomethane
ND
0.28
0.045
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2-Dichlorobenzene
ND
0.28
0.047
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,3-Dichlorobenzene
ND
0.28
0.047
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,4-Dichlorobenzene
ND
0.28
0.042
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
trans-1,4-Dichloro-2-butene
ND
0.56
0.087
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Dichlorodifluoromethane (Freon 12)
ND
0.56
0.079
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,1-Dichloroethane
ND
0.28
0.044
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2-Dichloroethane
ND
0.28
0.054
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1, 1 -Dichloroethylene
ND
0.28
0.059
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
cis-1,2-Dichloroethylene
ND
0.28
0.041
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
trans-1,2-Dichloroethylene
ND
0.28
0.042
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2-Dichloropropane
ND
0.28
0.036
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,3-Dichloropropane
ND
0.14
0.036
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
2,2-Dichloropropane
ND
0.28
0.059
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1, 1 -Dichloropropene
ND
0.56
0.036
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
cis-1,3-Dichloropropene
ND
0.14
0.033
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
trans-1,3-Dichloropropene
ND
0.14
0.031
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Diethyl Ether
ND
0.56
0.062
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Page 36 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: TB-3 Sampled: 10/22/2018 13:00
Sample ID: 18J1112-05
Samnle Matrix: Soil
Sample Flags: RL-11 Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.14
0.051
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,4-Dioxane
ND
14
7.4
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Ethylbenzene
0.93
0.28
0.036
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Hexachlorobutadiene
ND
0.28
0.16
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
2-Hexanone (MBK)
ND
2.8
0.42
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Isopropylbenzene (Cumene)
0.75
0.28
0.033
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
p-Isopropyltoluene (p-Cymene)
1.0
0.28
0.042
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Methyl tert-Butyl Ether (MTBE)
ND
0.28
0.025
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Methylene Chloride
ND
1.4
0.89
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
4-Methyl-2-pentanone (MIBK)
ND
2.8
0.41
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Naphthalene
7.8
0.56
0.034
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
n-Propylbenzene
1.5
0.28
0.036
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Styrene
ND
0.28
0.042
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1, 1, 1,2-Tetrachloroethane
ND
0.28
0.033
mg/Kgdry
4
SW-8468260B
10/24/18
10/27/18 11:45
EEH
1,1,2,2-Tetrachloroethane
ND
0.14
0.045
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Tetrachloroethylene
ND
0.28
0.076
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Tetrahydrofuran
ND
2.8
0.30
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Toluene
0.32
0.28
0.047
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2,3-Trichlorobenzene
ND
1.4
0.039
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2,4-Trichlorobenzene
ND
0.28
0.053
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,3,5-Trichlorobenzene
ND
0.28
0.047
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1, 1, 1 -Trichloroethane
ND
0.28
0.037
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,1,2-Trichloroethane
ND
0.28
0.066
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Trichloroethylene
ND
0.28
0.056
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Trichlorofluoromethane (Freon 11)
ND
0.56
0.041
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,2,3-Trichloropropane
ND
0.56
0.060
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.28
0.054
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
(Freon 113)
1,2,4-Trimethylbenzene
8.0
0.28
0.050
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
1,3,5-Trimethylbenzene
1.9
0.28
0.036
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Vinyl Chloride
ND
0.56
0.037
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
m+p Xylene
2.4
0.56
0.071
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
o-Xylene
1.1
0.28
0.037
mg/Kg dry
4
SW-846 8260B
10/24/18
10/27/18 11:45
EEH
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
92.6
70-130
10/27/18 11:45
Toluene-d8
101
70-130
10/27/18 11:45
4-Bromofluorobenzene
104
70-130
10/27/18 11:45
Page 37 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: TB-3 Sampled: 10/22/2018 13:00
Samnle ID: 18J1112-05
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.23
0.069
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Acenaphthylene
ND
0.23
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Acetophenone
ND
0.46
0.090
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Aniline
ND
0.46
0.13
mg/Kg dry
1 V-05, V-34
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Anthracene
ND
0.23
0.066
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Benzidine
ND
0.89
0.57
mg/Kg dry
1 R-05, V-05, V-34
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Benzo(a)anthracene
ND
0.23
0.061
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Benzo(a)pyrene
ND
0.23
0.071
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Benzo(b)fluoranthene
ND
0.23
0.065
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Benzo(g,h,i)perylene
ND
0.23
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Benzo(k)fluoranthene
ND
0.23
0.071
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Benzoic Acid
ND
1.3
0.24
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Bis(2-chloroethoxy)methane
ND
0.46
0.087
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Bis(2-chloroethyl)ether
ND
0.46
0.090
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Bis(2-chloroisopropyl)ether
ND
0.46
0.098
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.46
0.18
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
4-Bromophenylphenylether
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Butylbenzylphthalate
ND
0.46
0.11
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Carbazole
ND
0.23
0.059
mg/Kg dry
I
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
4-Chloroaniline
ND
0.89
0.10
mg/Kg dry
1 V-34
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
4-Chloro-3-methylphenol
ND
0.89
0.098
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2-Chloronaphthalene
ND
0.46
0.086
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2-Chlorophenol
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
4-Chlorophenylphenylether
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Chrysene
ND
0.23
0.071
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Dibenz(a,h)anthracene
ND
0.23
0.14
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Dibenzofman
ND
0.46
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Di-n-butylphthalate
ND
0.46
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
1,2-Dichlorobenzene
ND
0.46
0.081
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
1,3-Dichlorobenzene
ND
0.46
0.078
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
1,4-Dichlorobenzene
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
3,3-Dichlorobenzidine
ND
0.23
0.070
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2,4-Dichlorophenol
ND
0.46
0.078
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Diethylphthalate
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2,4-Dimethylphenol
ND
0.46
0.085
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Dimethylphthalate
ND
0.46
0.081
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
4,6-Dinitro-2-methylphenol
ND
0.46
0.43
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2,4-Dinitrophenol
ND
0.89
0.26
mg/Kg dry
1 V-19
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2,4-Dinitrotoluene
ND
0.46
0.074
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2,6-Dinitrotoluene
ND
0.46
0.081
mg/Kg dry
1 V-20
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Di-n-octylphthalate
ND
0.46
0.24
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.46
0.074
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Fluoranthene
ND
0.23
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Flumene
ND
0.23
0.074
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Page 38 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: TB-3 Sampled: 10/22/2018 13:00
Samnle ID: 18J1112-05
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.46
0.081
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Hexachlorobutadiene
ND
0.46
0.081
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Hexachlorocyclopentadiene
ND
0.46
0.097
mg/Kg dry
1
V-05
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Hexachloroethane
ND
0.46
0.092
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Indeno(1,2,3-cd)pyrene
ND
0.23
0.16
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Isophorone
ND
0.46
0.089
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
1-Methylnaphthalene
ND
0.23
0.087
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2-Methylnaphthalene
ND
0.23
0.079
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2-Methylphenol
ND
0.46
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
3/4-Methylphenol
ND
0.46
0.15
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Naphthalene
ND
0.23
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2-Nitroaniline
ND
0.46
0.077
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
3-Nitroaniline
ND
0.46
0.066
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
4-Nitroaniline
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Nitrobenzene
ND
0.46
0.086
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2-Nitrophenol
ND
0.46
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
4-Nitrophenol
ND
0.89
0.10
mg/Kg dry
1
V-20
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
N-Nitrosodimethylamine
ND
0.46
0.29
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
N-Nitrosodiphenylamine
ND
0.46
0.094
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
N-Nitrosodi-n-propylamine
ND
0.46
0.094
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Pentachloronitrobenzene
ND
0.46
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Pentachlorophenol
ND
0.46
0.11
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Phenanthrene
ND
0.23
0.12
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Phenol
ND
0.46
0.078
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Pyrene
ND
0.23
0.075
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Pyridine
ND
0.46
0.074
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
1,2,4,5-Tetrachlorobenzene
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
1,2,4-Trichlorobenzene
ND
0.46
0.082
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2,4,5-Trichlorophenol
ND
0.46
0.10
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
2,4,6-Trichlorophenol
ND
0.46
0.077
mg/Kg dry
1
SW-846 8270D
10/24/18
10/29/18 19:52
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
71.9
30-130
10/29/18 19:52
Phenol-d6
82.0
30-130
10/29/18 19:52
Nitrobenzene-d5
86.6
30-130
10/29/18 19:52
2-Fluorobiphenyl
59.3
30-130
10/29/18 19:52
2,4,6-Tribromophenol
97.0
30-130
10/29/18 19:52
p-Terphenyl-dl4
75.6
30-130
10/29/18 19:52
Page 39 of 78

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: TB-3 Sampled: 10/22/2018 13:00
Samnle ID: 18J1112-05
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C9-C18 Aliphatics 1400 140 mg/Kg dry 10 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:39 RMW
C19-C36 Aliphatics 360 68 mg/Kg dry 5 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:57 RMW
Unadjusted C11-C22 Aromatics 870 140 mg/Kg dry 10 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:39 RMW
C11-C22 Aromatics 830 140 mg/Kg dry 10 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:39 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD) 76.6 40-140 10/29/18 4:01
o-Terphenyl(OTP) 91.4 40-140 10/29/18 4:01
2-Bromonaphthalene 102 40-140 10/29/18 4:01
2-Fluorobiphenyl 108 40-140 10/29/18 4:01
Page 40 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: TB-3 Sampled: 10/22/2018 13:00
Sample ID: 18J1112-05
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - VPH
Soil/Methanol Preservation Ratio: 1.13
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C5-C8 Aliphatics
ND 160
mg/Kg dry 10
RL-05 MADEP-VPH-Feb 2018
10/23/18 10/26/18 2:59 EEH
Rev 2.1
C9-C12 Aliphatics
280 160
mg/Kg dry 10
MADEP-VPH-Feb 2018
10/23/18 10/26/18 2:59 EEH
Rev 2.1
C9-C10 Aromatics
440 160
mg/Kg dry 10
MADEP-VPH-Feb 2018
10/23/18 10/26/18 2:59 EEH
Rev 2.1
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2,5-Dibromotoluene (FID)
70.9
70-130
10/26/18 2:59
2,5-Dibromotoluene (PID)
81.0
70-130
10/26/18 2:59
Page 41 of 78

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112
Date Received: 10/22/2018
Field Sample #: TB-3 Sampled: 10/22/2018 13:00
Samnle ID: 18J1112-05
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 72.9 % Wt 1
SM 2540G 10/27/18 10/28/18 15:28 BLM
Page 42 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-MADEP-EPH-04-1.1
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18J1112-01 [SW-1]
B215618
20.6
2.00
10/24/18
18J1112-02 [SW-2]
B215618
20.1
2.00
10/24/18
18J1112-03 [SW-3]
B215618
20.5
2.00
10/24/18
18J1112-04 [SW-4]
B215618
20.3
2.00
10/24/18
18J1112-05 [TB-3]
B215618
20.3
2.00
10/24/18
Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18J1112-04 [SW-4]
B215495
4.30
6.20
10/23/18
18J1112-05 [TB-3]
B215495
5.70
6.50
10/23/18
Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]
Batch
Initial [g]
Final [mL[
Date
18J1112-01 [SW-1]
B215561
7.70
7.10
10/24/18
18J1112-02 [SW-2]
B215561
5.00
6.60
10/24/18
18J1112-03 [SW-3]
B215561
5.60
6.40
10/24/18
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
18J1112-01 [SW-1]
B215828
10/27/18
18J1112-02 [SW-2]
B215828
10/27/18
18J1112-03 [SW-3]
B215828
10/27/18
18J 1112-04 [SW-4]
B215828
10/27/18
18J1112-05 [TB-3]
B215828
10/27/18
Prep Method: SW-846 5035-SW-846 8260B
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18J1112-01[SW-1]
B215551
5.75
10.0
10/24/18
18J1112-02 [SW-2]
B215551
5.77
10.0
10/24/18
18J1112-03 [SW-3]
B215551
6.48
10.0
10/24/18
18J 1112-04 [SW-4]
B215551
5.99
10.0
10/24/18
Prep Method: SW-846 5035-SW-846 8260B
Sample
Methanol Methanol
Final
Lab Number [Field ID]
Batch
Amount(g)
Volume(mL) Aliquot(mL)
Volume(mL) Date
18J 1112-05 [TB-3]
B215584
6.71
6.82 0.25
50 10/24/18
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18J1112-01 [SW-1]
B215606
30.2
1.00
10/24/18
18J1112-02 [SW-2]
B215606
30.6
1.00
10/24/18
18J1112-03 [SW-3]
B215606
30.2
1.00
10/24/18
18J1112-04 [SW-4]
B215606
30.0
1.00
10/24/18
Page 43 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID] Batch Initial [g] Final [mL] Date
18J1112-04RE1 [SW-4] B215606 30.0 1.00 10/24/18
18J1112-05 [TB-3] B215606 30.6 1.00 10/24/18
Page 44 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215551 - SW-846 5035
Blank (B215551-BLK1) Prepared & Analyzed: 10/24/18
Acetone
ND
0.10
mg/Kg wet
Acrylonitrile
ND
0.0060
mg/Kg wet
tert-Amyl Methyl Ether (TAME)
ND
0.0010
mg/Kg wet
Benzene
ND
0.0020
mg/Kg wet
Bromobenzene
ND
0.0020
mg/Kg wet
Bromochloromethane
ND
0.0020
mg/Kg wet
Bromodichloromethane
ND
0.0020
mg/Kg wet
Bromoform
ND
0.0020
mg/Kg wet
Bromomethane
ND
0.010
mg/Kg wet
2-Butanone (MEK)
ND
0.040
mg/Kg wet
tert-Butyl Alcohol (TBA)
ND
0.040
mg/Kg wet
n-Butylbenzene
ND
0.0020
mg/Kg wet
sec-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butyl Ethyl Ether (TBEE)
ND
0.0010
mg/Kg wet
Carbon Disulfide
ND
0.0060
mg/Kg wet
Carbon Tetrachloride
ND
0.0020
mg/Kg wet
Chlorobenzene
ND
0.0020
mg/Kg wet
Chlorodibromomethane
ND
0.0010
mg/Kg wet
Chloroethane
ND
0.020
mg/Kg wet
Chloroform
ND
0.0040
mg/Kg wet
Chloromethane
ND
0.010
mg/Kg wet
2-Chlorotoluene
ND
0.0020
mg/Kg wet
4-Chlorotoluene
ND
0.0020
mg/Kg wet
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0020
mg/Kg wet
1,2-Dibromoethane (EDB)
ND
0.0010
mg/Kg wet
Dibromomethane
ND
0.0020
mg/Kg wet
1,2-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,3-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,4-Dichlorobenzene
ND
0.0020
mg/Kg wet
trans-1,4-Dichloro-2-butene
ND
0.0040
mg/Kg wet
Dichlorodifluoromethane (Freon 12)
ND
0.020
mg/Kg wet
1,1-Dichloroethane
ND
0.0020
mg/Kg wet
1,2-Dichloroethane
ND
0.0020
mg/Kg wet
1,1-Dichloroethylene
ND
0.0040
mg/Kg wet
cis-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
trans-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
1,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,3-Dichloropropane
ND
0.0010
mg/Kg wet
2,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,1-Dichloropropene
ND
0.0020
mg/Kg wet
cis-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
trans-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
Diethyl Ether
ND
0.020
mg/Kg wet
Diisopropyl Ether (RIPE)
ND
0.0010
mg/Kg wet
1,4-Dioxane
ND
0.10
mg/Kg wet
Ethylbenzene
ND
0.0020
mg/Kg wet
Hexachlorobutadiene
ND
0.0020
mg/Kg wet
2-Hexanone (MBK)
ND
0.020
mg/Kg wet
Isopropylbenzene (Cumene)
ND
0.0020
mg/Kg wet
p-Isopropyltoluene (p-Cymene)
ND
0.0020
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.0040
mg/Kg wet
Page 45 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215551 - SW-846 5035
Blank (B215551-BLK1)
Prepared & Analyzed: 10/24/18
Methylene Chloride
ND
0.020
mg/Kg wet
4-Methyl-2-pentanone (MIBK)
ND
0.020
mg/Kg wet
Naphthalene
ND
0.0040
mg/Kg wet
n-Propylbenzene
ND
0.0020
mg/Kg wet
Styrene
ND
0.0020
mg/Kg wet
1, 1, 1,2-Tetrachloroethane
ND
0.0020
mg/Kg wet
1,1,2,2-Tetrachloroethane
ND
0.0010
mg/Kg wet
Tetrachloroethylene
ND
0.0020
mg/Kg wet
Tetrahydrofuran
ND
0.010
mg/Kg wet
Toluene
ND
0.0020
mg/Kg wet
1,2,3-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,3,5-Trichlorobenzene
ND
0.0020
mg/Kg wet
1, 1, 1 -Trichloroethane
ND
0.0020
mg/Kg wet
1,1,2-Trichloroethane
ND
0.0020
mg/Kg wet
Trichloroethylene
ND
0.0020
mg/Kg wet
Trichlorofluoromethane (Freon 11)
ND
0.010
mg/Kg wet
1,2,3-Trichloropropane
ND
0.0020
mg/Kg wet
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.010
mg/Kg wet
113)
1,2,4-Trimethylbenzene
ND
0.0020
mg/Kg wet
1,3,5-Trimethylbenzene
ND
0.0020
mg/Kg wet
Vinyl Chloride
ND
0.010
mg/Kg wet
m+p Xylene
ND
0.0040
mg/Kg wet
o-Xylene
ND
0.0020
mg/Kg wet
Surrogate: 1,2-Dichloroethane-d4 0.0532 mg/Kg wet 0.0500 106 70-130
Surrogate: Toluene-d8 0.0515 mg/Kg wet 0.0500 103 70-130
Surrogate:4-Bromofluorobenzene 0.0529 mg/Kg wet 0.0500 106 70-130
LCS (B215551-BS1) Prepared & Analyzed: 10/24/18
Acetone
0.264
0.10
mg/Kg wet
0.200
132
70-160
Acrylonitrile
0.0226
0.0060
mg(Kgwet
0.0200
113
70-130
tert-Amyl Methyl Ether (TAME)
0.0256
0.0010
mg/Kg wet
0.0200
128
70-130
Benzene
0.0234
0.0020
mg/Kg wet
0.0200
117
70-130
Bromobenzene
0.0199
0.0020
mg/Kgwet
0.0200
99.4
70-130
Bromochloromethane
0.0218
0.0020
mg/Kg wet
0.0200
109
70-130
Bromodichloromethane
0.0213
0.0020
mg/Kg wet
0.0200
106
70-130
Bromoform
0.0209
0.0020
mg/Kgwet
0.0200
104
70-130
Bromomethane
0.0179
0.010
mg/Kg wet
0.0200
89.4
40-130
2-Butanone (MEK)
0.291
0.040
mg/Kg wet
0.200
145
70-160
tert-Butyl Alcohol (TBA)
0.188
0.040
mg/Kg wet
0.200
94.2
40-130
n-Butylbenzene
0.0172
0.0020
mg/Kg wet
0,0200
85.9
70-130
sec-Butylbenzene
0.0189
0.0020
mg/Kg wet
0.0200
94.5
70-130
tert-Butylbenzene
0.0189
0.0020
mg/Kgwet
0.0200
94.4
70-160
tert-Butyl Ethyl Ether (TBEE)
0.0256
0.0010
mg/Kg wet
0,0200
128
70-130
Carbon Disulfide
0.0242
0.0060
mg/Kg wet
0.0200
121
70-130
Carbon Tetrachloride
0.0250
0.0020
mg/Kg wet
0.0200
125
70-130
Chlorobenzene
0.0198
0.0020
mg/Kg wet
0,0200
99.2
70-130
Chlorodibromomethane
0.0241
0.0010
mg/Kg wet
0.0200
121
70-130
Chloroethane
0.0203
0.020
mg/Kgwet
0.0200
102
70-130
Chloroform
0.0235
0.0040
mg/Kg wet
0,0200
118
70-130
Chloromethane
0.0203
0.010
mg/Kg wet
0.0200
101
70-130
2-Chlorotoluene
0.0208
0.0020
mg/Kg wet
0.0200
104
70-130
t
t
t
t
t
Page 46 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215551 - SW-846 5035
LCS (B215551-BSI)
Prepared & Analyzed: 10/24/18
4-Chlorotoluene
0.0206
0.0020
mg/Kg wet
0.0200
103
70-130
1,2-Dibromo-3-chloropropane (DBCP)
0.0186
0.0020
mg/Kg wet
0.0200
93.2
70-130
1,2-Dibromoethane (EDB)
0.0221
0.0010
mg/Kg wet
0.0200
110
70-130
Dibromomethane
0.0190
0.0020
mg/Kg wet
0.0200
95.2
70-130
1,2-Dichlorobenzene
0.0187
0.0020
mg/Kg wet
0.0200
93.6
70-130
1,3-Dichlorobenzene
0.0193
0.0020
mg/Kg wet
0.0200
96.6
70-130
1,4-Dichlorobenzene
0.0186
0.0020
mg/Kg wet
0.0200
93.0
70-130
trans-1,4-Dichloro-2-butene
0.0166
0.0040
mg/Kg wet
0.0200
83.2
70-130
Dichlorodifluoromethane (Freon 12)
0.0205
0.020
mg/Kg wet
0.0200
102
40-160
1,1-Dichloroethane
0.0233
0.0020
mg/Kg wet
0.0200
117
70-130
1,2-Dichloroethane
0.0238
0.0020
mg/Kg wet
0.0200
119
70-130
1,1-Dichloroethylene
0.0239
0.0040
mg/Kg wet
0.0200
119
70-130
cis-1,2-Dichloroethylene
0.0229
0.0020
mg/Kg wet
0.0200
115
70-130
trans-1,2-Dichloroethylene
0.0240
0.0020
mg/Kg wet
0.0200
120
70-130
1,2-Dichloropropane
0.0219
0.0020
mg/Kg wet
0.0200
109
70-130
1,3-Dichloropropane
0.0226
0.0010
mg/Kg wet
0.0200
113
70-130
2,2-Dichloropropane
0.0191
0.0020
mg/Kg wet
0.0200
95.6
70-130
1,1-Dichloropropene
0.0239
0.0020
mg/Kg wet
0.0200
120
70-130
cis-1,3-Dichloropropene
0.0218
0.0010
mg/Kg wet
0.0200
109
70-130
trans-1,3-Dichloropropene
0.0219
0.0010
mg/Kg wet
0.0200
110
70-130
Diethyl Ether
0.0242
0.020
mg/Kg wet
0.0200
121
70-130
Diisopropyl Ether (DIPE)
0.0258
0.0010
mg/Kg wet
0.0200
129
70-130
1,4-Dioxane
0.209
0.10
mg/Kg wet
0.200
105
40-160
Ethylbenzene
0.0190
0.0020
mg/Kg wet
0.0200
94.9
70-130
Hexachlorobutadiene
0.0174
0.0020
mg/Kg wet
0.0200
87.2
70-160
2-Hexanone (MBK)
0.271
0.020
mg/Kg wet
0.200
136
70-160
Isopropylbenzene (Cumene)
0.0203
0.0020
mg/Kg wet
0.0200
102
70-130
p-Isopropyltoluene (p-Cymene)
0.0184
0.0020
mg/Kg wet
0.0200
91.8
70-130
Methyl tert-Butyl Ether (MTBE)
0.0261
0.0040
mg/Kg wet
0.0200
130
70-130
Methylene Chloride
0.0225
0.020
mg/Kg wet
0.0200
112
40-160
4-Methyl-2-pentanone (MIBK)
0.263
0.020
mg/Kg wet
0.200
131
70-160
Naphthalene
0.0158
0.0040
mg/Kg wet
0.0200
79.2
40-130
n-Propylbenzene
0.0200
0.0020
mg/Kg wet
0.0200
100
70-130
Styrene
0.0191
0.0020
mg/Kg wet
0.0200
95.3
70-130
1, 1, 1,2-Tetrachloroethane
0.0203
0.0020
mg/Kg wet
0.0200
102
70-130
1,1,2,2-Tetrachloroethane
0.0194
0.0010
mg/Kg wet
0.0200
97.1
70-130
Tetrachloroethylene
0.0256
0.0020
mg/Kg wet
0.0200
128
70-130
Tetrahydrofuran
0.0263
0.010
mg/Kg wet
0.0200
132 *
70-130
Toluene
0.0220
0.0020
mg/Kg wet
0.0200
110
70-130
1,2,3-Trichlorobenzene
0.0163
0.0020
mg/Kg wet
0.0200
81.5
70-130
1,2,4-Trichlorobenzene
0.0159
0.0020
mg/Kg wet
0.0200
79.5
70-130
1,3,5-Trichlorobenzene
0.0173
0.0020
mg/Kg wet
0.0200
86.4
70-130
1, 1, 1 -Trichloroethane
0.0243
0.0020
mg/Kg wet
0.0200
122
70-130
1,1,2-Trichloroethane
0.0220
0.0020
mg/Kg wet
0.0200
110
70-130
Trichloroethylene
0.0214
0.0020
mg/Kg wet
0.0200
107
70-130
Trichlorofluoromethane (Freon 11)
0.0236
0.010
mg/Kg wet
0.0200
118
70-130
1,2,3-Trichloropropane
0.0206
0.0020
mg/Kg wet
0.0200
103
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0241
0.010
mg/Kg wet
0.0200
121
70-130
113)
1,2,4-Trimethylbenzene
0.0177
0.0020
mg/Kg wet
0.0200
88.7
70-130
1,3,5-Trimethylbenzene
0.0193
0.0020
mg/Kg wet
0.0200
96.6
70-130
Vinyl Chloride
0.0202
0.010
mg/Kg wet
0,0200
101
40-130
f
t
t
f
t
t
L-07
Page 47 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215551 - SW-846 5035
LCS (B215551-BSI) Prepared & Analyzed: 10/24/18
m+p Xylene 0.0388 0.0040 mg/Kg wet 0.0400 96.9 70-130
o-Xylene 0.0199 0.0020 mg/Kg wet 0.0200 99.4 70-130
Surrogate:l,2-Dichloroethane-d4
Surrogate: Toluene-d8
Surrogate:4-Bromofluorobenzene
LCS Dup (B215551-BSDI)
0.0523
0.0518
0.0533
mg/Kg wet
mg/Kg wet
mg/Kg wet
0.0500 105
0.0500 104
0.0500 107
Prepared & Analyzed: 10/24/18
70-130
70-130
70-130
Acetone
0332
0.10
mg/Kg wet
0.200
166
* 70-160
22.8
Acrylonitrile
0.0231
0.0060
mg/Kg wet
0.0200
115
70-130
2.04
tert-Amyl Methyl Ether (TAME)
0.0259
0.0010
mg/Kg wet
0.0200
130
70-130
1.30
Benzene
0.0232
0.0020
mg/Kg wet
0.0200
116
70-130
1.01
Bromobenzene
0.0199
0.0020
mg/Kg wet
0.0200
99.7
70-130
0.301
Bromochloromethane
0.0233
0.0020
mg/Kg wet
0.0200
117
70-130
6.63
Bromodichloromethane
0.0216
0.0020
mg/Kg wet
0.0200
108
70-130
1.47
Bromoform
0.0212
0.0020
mg/Kg wet
0.0200
106
70-130
1.65
Bromomethane
0.0176
0.010
mg/Kg wet
0.0200
88.2
40-130
1.40
2-Butanone (MEK)
0.321
0.040
mg/Kg wet
0.200
160
70-160
9.79
tert-Butyl Alcohol (TBA)
0.208
0.040
mg/Kg wet
0.200
104
40-130
10.0
n-Butylbenzene
0.0166
0.0020
mg/Kg wet
0.0200
82.8
70-130
3.69
sec-Butylbenzene
0.0187
0.0020
mg/Kg wet
0.0200
93.3
70-130
1.28
tert-Butylbenzene
0.0184
0.0020
mg/Kg wet
0.0200
92.2
70-160
2.33
tert-Butyl Ethyl Ether (TBEE)
0.0257
0.0010
mg/Kg wet
0.0200
128
70-130
0.367
Carbon Disulfide
0.0232
0.0060
mg/Kg wet
0.0200
116
70-130
4.41
Carbon Tetrachloride
0.0252
0.0020
mg/Kg wet
0.0200
126
70-130
0.677
Chlorobenzene
0.0199
0.0020
mg/Kg wet
0.0200
99.7
70-130
0.452
Chlorodibromomethane
0.0247
0.0010
mg/Kg wet
0.0200
124
70-130
2.47
Chloroethane
0.0214
0.020
mg/Kg wet
0.0200
107
70-130
5.03
Chloroform
0.0240
0.0040
mg/Kg wet
0.0200
120
70-130
2.00
Chloromethane
0.0207
0.010
mg/Kg wet
0.0200
103
70-130
2.13
2-Chlorotoluene
0.0206
0.0020
mg/Kg wet
0.0200
103
70-130
0.928
4-Chlorotoluene
0.0199
0.0020
mg/Kg wet
0.0200
99.7
70-130
3.43
1,2-Dibromo-3-chloropropane (DBCP)
0.0200
0.0020
mg/Kg wet
0.0200
99.9
70-130
6.95
1,2-Dibromoethane (EDB)
0.0224
0.0010
mg/Kg wet
0.0200
112
70-130
1.64
Dibromomethane
0.0200
0.0020
mg/Kg wet
0.0200
99.9
70-130
4.84
1,2-Dichlorobenzene
0.0184
0.0020
mg/Kg wet
0.0200
92.0
70-130
1.74
1,3-Dichlorobenzene
0.0193
0.0020
mg/Kg wet
0.0200
96.5
70-130
0.0207
1,4-Dichlorobenzene
0.0183
0.0020
mg/Kg wet
0.0200
91.5
70-130
1.64
trans-1,4-Dichloro-2-butene
0.0163
0.0040
mg/Kg wet
0.0200
81.5
70-130
2.06
Dichlorodifluoromethane (Freon 12)
0.0204
0.020
mg/Kg wet
0.0200
102
40-160
0.352
1, 1 -Dichloroethane
0.0234
0.0020
mg/Kg wet
0.0200
117
70-130
0.445
1,2-Dichloroethane
0.0236
0.0020
mg/Kg wet
0.0200
118
70-130
0.608
1,1-Dichloroethylene
0.0234
0.0040
mg/Kg wet
0.0200
117
70-130
2.24
cis-1,2-Dichloroethylene
0.0229
0.0020
mg/Kg wet
0.0200
114
70-130
0.175
trans-1,2-Dichloroethylene
0.0237
0.0020
mg/Kg wet
0.0200
118
70-130
1.37
1,2-Dichloropropane
0.0220
0.0020
mg/Kg wet
0.0200
110
70-130
0.520
1,3-Dichloropropane
0.0228
0.0010
mg/Kg wet
0.0200
114
70-130
1.22
2,2-Dichloropropane
0.0188
0.0020
mg/Kg wet
0.0200
93.8
70-130
1.93
1,1-Dichloropropene
0.0238
0.0020
mg/Kg wet
0.0200
119
70-130
0.620
cis-1,3-Dichloropropene
0.0226
0.0010
mg/Kg wet
0.0200
113
70-130
3.75
trans-1,3-Dichloropropene
0.0222
0.0010
mg/Kg wet
0.0200
ill
70-130
1.21
Diethyl Ether
0.0259
0.020
mg/Kg wet
0.0200
130
70-130
6.96
Diisopropyl Ether (RIPE)
0.0263
0.0010
mg/Kg wet
0.0200
132
* 70-130
2.07
25 L-07 t
25
25
25
25
25
25
25
25 f
25 t
25 t
25
25
25 t
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25 t
25
25
25
25
25
25
25
25
25
25
25
25
25 L-07
Page 48 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215551 - SW-846 5035
LCS Dup (B215551-BSD1) Prepared & Analyzed: 10/24/18
1,4-Dioxane
0.263
0.10
mg/Kgwet
0.200
132
40-160
22.8
50
f #
Ethylbenzene
0.0186
0.0020
mg/Kg wet
0.0200
93.0
70-130
2.06
25
Hexachlorobutadiene
0.0176
0.0020
mg/Kg wet
0.0200
88.0
70-160
0.970
25
2-Hexanone (MBK)
0.288
0.020
mg/Kg wet
0.200
144
70-160
6.00
25
f
Isopropylbenzene (Cumene)
0.0200
0.0020
mg/Kg wet
0.0200
100
70-130
1.29
25
p-Isopropyltoluene (p-Cymene)
0.0181
0.0020
mg/Kg wet
0.0200
90.5
70-130
1.41
25
Methyl tert-Butyl Ether (MTBE)
0.0265
0.0040
mg/Kg wet
0.0200
133 *
70-130
1.81
25
L-07
Methylene Chloride
0.0207
0.020
mg/Kg wet
0.0200
104
40-160
8.29
25
t
4-Methyl-2-pentanone (MIBK)
0.275
0.020
mg/Kg wet
0.200
138
70-160
4.74
25
t
Naphthalene
0.0165
0.0040
mg/Kg wet
0.0200
82.5
40-130
4.12
25
f
n-Propylbenzene
0.0197
0.0020
mg/Kg wet
0.0200
98.5
70-130
1.62
25
Styrene
0.0187
0.0020
mg/Kg wet
0.0200
93.4
70-130
1.99
25
1, 1, 1,2-Tetrachloroethane
0.0202
0.0020
mg/Kg wet
0.0200
101
70-130
0.404
25
1,1,2,2-Tetrachloroethane
0.0202
0.0010
mg/Kg wet
0.0200
101
70-130
4.18
25
Tetrachloroethylene
0.0238
0.0020
mg/Kg wet
0.0200
119
70-130
7.30
25
Tetrahydrofuran
0.0255
0.010
mg/Kg wet
0.0200
128
70-130
3.10
25
Toluene
0.0218
0.0020
mg/Kg wet
0.0200
109
70-130
0.903
25
1,2,3-Trichlorobenzene
0.0166
0.0020
mg/Kg wet
0.0200
83.0
70-130
1.85
25
1,2,4-Trichlorobenzene
0.0156
0.0020
mg/Kg wet
0.0200
78.0
70-130
1.90
25
1,3,5-Trichlorobenzene
0.0171
0.0020
mg/Kg wet
0.0200
85.6
70-130
0.884
25
1, 1, 1 -Trichloroethane
0.0242
0.0020
mg/Kg wet
0.0200
121
70-130
0.775
25
1,1,2-Trichloroethane
0.0235
0.0020
mg/Kg wet
0.0200
118
70-130
6.78
25
Trichloroethylene
0.0216
0.0020
mg/Kg wet
0.0200
108
70-130
0.864
25
Trichlorofluoromethane (Freon 11)
0.0234
0.010
mg/Kg wet
0.0200
117
70-130
0.793
25
1,2,3-Trichloropropane
0.0213
0.0020
mg/Kg wet
0.0200
107
70-130
3.54
25
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0250
0.010
mg/Kg wet
0.0200
125
70-130
3.41
25
113)
1,2,4-Trimethylbenzene
0.0174
0.0020
mg/Kg wet
0.0200
87.1
70-130
1.84
25
1,3,5-Trimethylbenzene
0.0192
0.0020
mg/Kg wet
0.0200
96.0
70-130
0.706
25
Vinyl Chloride
0.0203
0.010
mg/Kg wet
0.0200
101
40-130
0.198
25
t
m+p Xylene
0.0386
0.0040
mg/Kg wet
0.0400
96.4
70-130
0.522
25
o-Xylene
0.0197
0.0020
mg/Kg wet
0.0200
98.5
70-130
0.859
25
Surrogate:l,2-Dichloroethane-d4
0.0535
mg/Kg wet
0.0500
107
70-130
Surrogate: Toluene-d8
0.0514
mg/Kg wet
0.0500
103
70-130
Surrogate:4-Bromofluorobenzene
0.0532
mg/Kg wet
0.0500
106
70-130
Batch B215584 - SW-846 5035
Blank (B215584-BLKI)
Prepared: 10/24/18 Analyzed: 10/27/18
Acetone
ND
2.5
mg/Kg wet
Acrylonitrile
ND
0.25
mg/Kg wet
tert-Amyl Methyl Ether (TAME)
ND
0.025
mg/Kg wet
Benzene
ND
0.050
mg/Kg wet
Bromobenzene
ND
0.050
mg/Kg wet
Bromochloromethane
ND
0.050
mg/Kg wet
Bromodichloromethane
ND
0.050
mg/Kg wet
Bromoform
ND
0.050
mg/Kg wet
Bromomethane
ND
0.10
mg/Kg wet
2-Butanone (MEK)
ND
1.0
mg/Kg wet
tert-Butyl Alcohol (TBA)
ND
1.0
mg/Kg wet
n-Butylbenzene
ND
0.050
mg/Kg wet
sec-Butylbenzene
ND
0.050
mg/Kg wet
tert-Butylbenzene
ND
0.050
mg/Kg wet
Page 49 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215584 - SW-846 5035
Blank (B215584-BLK1) Prepared: 10/24/18 Analyzed: 10/27/18
tert-Butyl Ethyl Ether (TBEE)
ND
0.025
mg/Kg wet
Carbon Disulfide
ND
0.15
mg/Kg wet
Carbon Tetrachloride
ND
0.050
mg/Kg wet
Chlorobenzene
ND
0.050
mg/Kg wet
Chlorodibromomethane
ND
0.025
mg/Kg wet
Chloroethane
ND
0.10
mg/Kg wet
Chloroform
ND
0.10
mg/Kg wet
Chloromethane
ND
0.10
mg/Kg wet
2-Chlorotoluene
ND
0.050
mg/Kg wet
4-Chlorotoluene
ND
0.050
mg/Kg wet
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.25
mg/Kg wet
1,2-Dibromoethane (EDB)
ND
0.025
mg/Kg wet
Dibromomethane
ND
0.050
mg/Kg wet
1,2-Dichlorobenzene
ND
0.050
mg/Kg wet
1,3-Dichlorobenzene
ND
0.050
mg/Kg wet
1,4-Dichlorobenzene
ND
0.050
mg/Kg wet
trans-1,4-Dichloro-2-butene
ND
0.10
mg/Kg wet
Dichlorodifluoromethane (Freon 12)
ND
0.10
mg/Kg wet
1,1-Dichloroethane
ND
0.050
mg/Kg wet
1,2-Dichloroethane
ND
0.050
mg/Kg wet
1,1-Dichloroethylene
ND
0.050
mg/Kg wet
cis-1,2-Dichloroethylene
ND
0.050
mg/Kg wet
trans-1,2-Dichloroethylene
ND
0.050
mg/Kg wet
1,2-Dichloropropane
ND
0.050
mg/Kg wet
1,3-Dichloropropane
ND
0.025
mg/Kg wet
2,2-Dichloropropane
ND
0.050
mg/Kg wet
1,1-Dichloropropene
ND
0.10
mg/Kg wet
cis-1,3-Dichloropropene
ND
0.025
mg/Kg wet
trans-1,3-Dichloropropene
ND
0.025
mg/Kg wet
Diethyl Ether
ND
0.10
mg/Kg wet
Diisopropyl Ether (RIPE)
ND
0.025
mg/Kg wet
1,4-Dioxane
ND
2.5
mg/Kg wet
Ethylbenzene
ND
0.050
mg/Kg wet
Hexachlorobutadiene
ND
0.050
mg/Kg wet
2-Hexanone (MBK)
ND
0.50
mg/Kg wet
Isopropylbenzene (Cumene)
ND
0.050
mg/Kg wet
p-Isopropyltoluene (p-Cymene)
ND
0.050
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.050
mg/Kg wet
Methylene Chloride
ND
0.25
mg/Kg wet
4-Methyl-2-pentanone (MIBK)
ND
0.50
mg/Kg wet
Naphthalene
ND
0.10
mg/Kg wet
n-Propylbenzene
ND
0.050
mg/Kg wet
Styrene
ND
0.050
mg/Kg wet
1, 1, 1,2-Tetrachloroethane
ND
0.050
mg/Kg wet
1,1,2,2-Tetrachloroethane
ND
0.025
mg/Kg wet
Tetrachloroethylene
ND
0.050
mg/Kg wet
Tetrahydrofuran
ND
0.50
mg/Kg wet
Toluene
ND
0.050
mg/Kg wet
1,2,3-Trichlorobenzene
ND
0.25
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.050
mg/Kg wet
1,3,5-Trichlorobenzene
ND
0.050
mg/Kg wet
1, 1, 1 -Trichloroethane
ND
0.050
mg/Kg wet
Page 50 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215584 - SW-846 5035
Blank (B215584-BLK1)
Prepared: 10/24/18 Analyzed: 10/27/18
1,1,2-Trichloroethane
ND
0.050
mg/Kg wet
Trichloroethylene
ND
0.050
mg/Kg wet
Trichlorofluoromethane (Freon 11)
ND
0.10
mg/Kg wet
1,2,3-Trichloropropane
ND
0.10
mg/Kg wet
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.050
mg/Kg wet
113)
1,2,4-Trimethylbenzene
ND
0.050
mg/Kg wet
1,3,5-Trimethylbenzene
ND
0.050
mg/Kg wet
Vinyl Chloride
ND
0.10
mg/Kg wet
m+p Xylene
ND
0.10
mg/Kg wet
o-Xylene
ND
0.050
mg/Kg wet
Surrogate:l,2-Dichloroethane-d4
0.0247
mg/Kg wet
0.0250 98.6 70-130
Surrogate: Toluene-d8
0.0246
mg/Kg wet
0.0250 98.3 70-130
Surrogate: 4-Bromofluorobenzene
0.0250
mg/Kg wet
0.0250 100 70-130
LCS (B215584-BSI)
Prepared: 10/24/18 Analyzed: 10/27/18
Acetone
0.155
0.057
mg/Kg wet
0.113
137
70-160
t
Acrylonitrile
0.0102
0.0057
mg/Kg wet
0,0113
90.1
70-130
tert-Amyl Methyl Ether (TAME)
0.0107
0.00057
mg/Kg wet
0.0113
94.1
70-130
Benzene
0.0108
0.0011
mg/Kgwet
0.0113
95.5
70-130
Bromobenzene
0.0112
0.0011
mg/Kg wet
0,0113
98.9
70-130
Bromochloromethane
0.0119
0.0011
mg/Kg wet
0.0113
105
70-130
Bromodichloromethane
0.0115
0.0011
mg/Kgwet
0.0113
102
70-130
Bromoform
0.00991
0.0011
mg/Kg wet
0,0113
87.4
70-130
Bromomethane
0.00564
0.0023
mg/Kg wet
0.0113
49.8
40-130
t
2-Butanone (MEK)
0.126
0.023
mg/Kg wet
0.113
111
70-160
t
tert-Butyl Alcohol (TBA)
0.0780
0.023
mg/Kg wet
0.113
68.8
40-130
t
n-Butylbenzene
0.0111
0.0011
mg/Kg wet
0.0113
97.7
70-130
sec-Butylbenzene
0.0116
0.0011
mg/Kgwet
0.0113
103
70-130
tert-Butylbenzene
0.0113
0.0011
mg/Kg wet
0,0113
100
70-160
t
tert-Butyl Ethyl Ether (TBEE)
0.0111
0.00057
mg/Kg wet
0.0113
97.9
70-130
Carbon Disulfide
0.0114
0.0034
mg/Kg wet
0.0113
100
70-130
Carbon Tetrachloride
0.0104
0.0011
mg/Kg wet
0,0113
91.6
70-130
Chlorobenzene
0.0117
0.0011
mg/Kg wet
0.0113
104
70-130
Chlorodibromomethane
0.0123
0.00057
mg/Kgwet
0.0113
108
70-130
Chloroethane
0.0101
0.0023
mg/Kg wet
0,0113
89.3
70-130
Chloroform
0.0113
0.0023
mg/Kg wet
0.0113
100
70-130
Chloromethane
0.0104
0.0023
mg/Kgwet
0.0113
91.4
70-130
2-Chlorotoluene
0.0113
0.0011
mg/Kg wet
0,0113
100
70-130
4-Chlorotoluene
0.0117
0.0011
mg/Kg wet
0.0113
103
70-130
1,2-Dibromo-3-chloropropane(DBCP)
0.00954
0.0057
mg/Kgwet
0.0113
84.2
70-130
1,2-Dibromoethane (EDB)
0.0114
0.00057
mg/Kg wet
0,0113
101
70-130
Dibromomethane
0.0123
0.0011
mg/Kg wet
0.0113
108
70-130
1,2-Dichlorobenzene
0.0118
0.0011
mg/Kgwet
0.0113
104
70-130
1,3-Dichlorobenzene
0.0119
0.0011
mg/Kg wet
0,0113
105
70-130
1,4-Dichlorobenzene
0.0113
0.0011
mg/Kg wet
0.0113
99.7
70-130
trans-1,4-Dichloro-2-butene
0.00975
0.0023
mg/Kgwet
0.0113
86.0
70-130
Dichlorodifluoromethane (Freon 12)
0.00811
0.0023
mg/Kg wet
0,0113
71.6
40-160
1,1-Dichloroethane
0.0112
0.0011
mg/Kg wet
0.0113
99.2
70-130
1,2-Dichloroethane
0.0114
0.0011
mg/Kgwet
0.0113
101
70-130
1,1-Dichloroethylene
0.0102
0.0011
mg/Kg wet
0,0113
90.4
70-130
cis-1,2-Dichloroethylene
0.0115
0.0011
mg/Kg wet
0.0113
101
70-130
trans-1,2-Dichloroethylene
0.0111
0.0011
mg/Kgwet
0.0113
97.6
70-130
Page 51 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215584 - SW-846 5035
LCS (B215584-BSI) Prepared: 10/24/18 Analyzed: 10/27/18
1,2-Dichloropropane
0.0109
0.0011
mg/Kg wet
0.0113
96.4
70-130
1,3-Dichloropropane
0.0109
0.00057
mg/Kg wet
0.0113
96.4
70-130
2,2-Dichloropropane
0.00804
0.0011
mg/Kg wet
0.0113
70.9
70-130
1,1-Dichloropropene
0.0106
0.0023
mg/Kg wet
0.0113
93.2
70-130
cis-1,3-Dichloropropene
0.0115
0.00057
mg/Kg wet
0.0113
102
70-130
trans-1,3-Dichloropropene
0.0122
0.00057
mg/Kg wet
0.0113
108
70-130
Diethyl Ether
0.0120
0.0023
mg/Kg wet
0.0113
106
70-130
Diisopropyl Ether (DIPE)
0.0112
0.00057
mg/Kg wet
0.0113
98.7
70-130
1,4-Dioxane
0.0972
0.057
mg/Kg wet
0.113
85.8
40-160
t
Ethylbenzene
0.0115
0.0011
mg/Kg wet
0.0113
102
70-130
Hexachlorobutadiene
0.0112
0.0011
mg/Kg wet
0.0113
98.6
70-160
2-Hexanone (MBK)
0.115
0.011
mg/Kg wet
0.113
102
70-160
t
Isopropylbenzene(Cumene)
0.0114
0.0011
mg/Kg wet
0.0113
101
70-130
p-Isopropyholuene (p-Cymene)
0.0109
0.0011
mg/Kg wet
0.0113
95.9
70-130
Methyl tert-Butyl Ether (MTBE)
0.0116
0.0011
mg/Kg wet
0.0113
102
70-130
Methylene Chloride
0.0109
0.0057
mg/Kg wet
0.0113
96.5
40-160
f
4-Methyl-2-pentanone (MIBK)
0.104
0.011
mg/Kg wet
0.113
91.5
70-160
t
Naphthalene
0.0100
0.0023
mg/Kg wet
0.0113
88.6
40-130
t
n-Propylbenzene
0.0115
0.0011
mg/Kg wet
0.0113
102
70-130
Styrene
0.0118
0.0011
mg/Kg wet
0.0113
104
70-130
1, 1, 1,2-Tetrachloroethane
0.0114
0.0011
mg/Kg wet
0.0113
101
70-130
1,1,2,2-Tetrachloroethane
0.0102
0.00057
mg/Kg wet
0.0113
90.0
70-130
Tetrachloroethylene
0.0111
0.0011
mg/Kg wet
0.0113
97.7
70-130
Tetrahydrofuran
0.0108
0.011
mg/Kg wet
0.0113
95.3
70-130
J
Toluene
0.0112
0.0011
mg/Kg wet
0.0113
99.0
70-130
1,2,3-Trichlorobenzene
0.0103
0.0057
mg/Kg wet
0.0113
91.0
70-130
1,2,4-Trichlorobenzene
0.00904
0.0011
mg/Kg wet
0.0113
79.8
70-130
1,3,5-Trichlorobenzene
0.0116
0.0011
mg/Kg wet
0.0113
102
70-130
1, 1, 1 -Trichloroethane
0.0110
0.0011
mg/Kg wet
0.0113
97.0
70-130
1,1,2-Trichloroethane
0.0113
0.0011
mg/Kg wet
0.0113
100
70-130
Trichloroethylene
0.0121
0.0011
mg/Kg wet
0.0113
107
70-130
Trichlorofluoromethane (Freon 11)
0.00886
0.0023
mg/Kg wet
0.0113
78.2
70-130
1,2,3-Trichloropropane
0.0107
0.0023
mg/Kg wet
0.0113
94.3
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.00961
0.0011
mg/Kg wet
0.0113
84.8
70-130
113)
1,2,4-Trimethylbenzene
0.0115
0.0011
mg/Kg wet
0.0113
101
70-130
1,3,5-Trimethylbenzene
0.0114
0.0011
mg/Kg wet
0,0113
100
70-130
Vinyl Chloride
0.0123
0.0023
mg/Kg wet
0.0113
108
40-130
t
m+p Xylene
0.0233
0.0023
mg/Kg wet
0.0227
103
70-130
o-Xylene
0.0119
0.0011
mg/Kg wet
0,0113
105
70-130
Surrogate: 1,2-Dichloroethane-d4 0.0280 mg/Kg wet 0.0283 98.8 70-130
Surrogate: Toluene-d8 0.0283 mg/Kg wet 0.0283 99.8 70-130
Surrogate:4-Bromofluorobenzene 0.0282 mg/Kg wet 0.0283 99.6 70-130
Page 52 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215584 - SW-846 5035
LCS Dup (B215584-BSD1)
Prepared: 10/24/18 Analyzed: 10/27/18
Acetone
0.134
0.057
mg/Kg wet
0.113
118
70-160
14.9
25
f
Acrylonitrile
0.0100
0.0057
mg/Kg wet
0.0113
88.4
70-130
1.90
25
tert-Amyl Methyl Ether (TAME)
0.0104
0.00057
mg/Kg wet
0.0113
92.0
70-130
2.26
25
Benzene
0.0105
0.0011
mg/Kg wet
0.0113
92.8
70-130
2.87
25
Bromobenzene
0.0114
0.0011
mg/Kg wet
0.0113
101
70-130
2.00
25
Bromochloromethane
0.0116
0.0011
mg/Kg wet
0.0113
103
70-130
2.50
25
Bromodichloromethane
0.0111
0.0011
mg/Kg wet
0.0113
98.2
70-130
3.60
25
Bromoform
0.0102
0.0011
mg/Kg wet
0.0113
90.0
70-130
2.93
25
Bromomethane
0.00658
0.0023
mg/Kg wet
0.0113
58.1
40-130
15.4
25
t
2-Butanone (MEK)
0.115
0.023
mg/Kg wet
0.113
101
70-160
9.30
25
f
tert-Butyl Alcohol (TBA)
0.0819
0.023
mg/Kg wet
0.113
72.2
40-130
4.88
25
t
n-Butylbenzene
0.0112
0.0011
mg/Kg wet
0.0113
98.5
70-130
0.815
25
sec-Butylbenzene
0.0117
0.0011
mg/Kg wet
0.0113
103
70-130
0.681
25
tert-Butylbenzene
0.0112
0.0011
mg/Kg wet
0.0113
99.2
70-160
0.803
25
t
tert-Butyl Ethyl Ether (TBEE)
0.0110
0.00057
mg/Kg wet
0.0113
97.3
70-130
0.615
25
Carbon Disulfide
0.0110
0.0034
mg/Kg wet
0.0113
96.7
70-130
3.75
25
Carbon Tetrachloride
0.0101
0.0011
mg/Kg wet
0.0113
89.0
70-130
2.88
25
Chlorobenzene
0.0115
0.0011
mg/Kg wet
0.0113
102
70-130
1.75
25
Chlorodibromomethane
0.0118
0.00057
mg/Kg wet
0.0113
104
70-130
4.15
25
Chloroethane
0.00957
0.0023
mg/Kg wet
0.0113
84.4
70-130
5.64
25
Chloroform
0.0108
0.0023
mg/Kg wet
0.0113
95.0
70-130
5.23
25
Chloromethane
0.00909
0.0023
mg/Kg wet
0.0113
80.2
70-130
13.1
25
2-Chlorotoluene
0.0119
0.0011
mg/Kg wet
0.0113
105
70-130
4.59
25
4-Chlorotoluene
0.0120
0.0011
mg/Kg wet
0.0113
106
70-130
2.67
25
1,2-Dibromo-3-chloropropane (DBCP)
0.0102
0.0057
mg/Kg wet
0.0113
90.1
70-130
6.77
25
1,2-Dibromoethane (EDB)
0.0114
0.00057
mg/Kg wet
0.0113
100
70-130
0.497
25
Dibromomethane
0.0124
0.0011
mg/Kg wet
0.0113
109
70-130
1.10
25
1,2-Dichlorobenzene
0.0116
0.0011
mg/Kg wet
0.0113
102
70-130
1.65
25
1,3-Dichlorobenzene
0.0117
0.0011
mg/Kg wet
0.0113
103
70-130
1.83
25
1,4-Dichlorobenzene
0.0112
0.0011
mg/Kg wet
0.0113
99.0
70-130
0.705
25
trans-1,4-Dichloro-2-butene
0.0104
0.0023
mg/Kg wet
0.0113
91.8
70-130
6.52
25
Dichlorodifluoromethane (Freon 12)
0.00784
0.0023
mg/Kg wet
0.0113
69.2
40-160
3.41
25
t
1,1-Dichloroethane
0.0108
0.0011
mg/Kg wet
0.0113
94.9
70-130
4.43
25
1,2-Dichloroethane
0.0112
0.0011
mg/Kg wet
0.0113
98.9
70-130
2.10
25
1,1-Dichloroethylene
0.00996
0.0011
mg/Kg wet
0.0113
87.9
70-130
2.80
25
cis-1,2-Dichloroethylene
0.0108
0.0011
mg/Kg wet
0.0113
94.9
70-130
6.62
25
trans-1,2-Dichloroethylene
0.0110
0.0011
mg/Kg wet
0.0113
97.2
70-130
0.411
25
1,2-Dichloropropane
0.0107
0.0011
mg/Kg wet
0.0113
94.5
70-130
1.99
25
1,3-Dichloropropane
0.0109
0.00057
mg/Kg wet
0.0113
96.2
70-130
0.208
25
2,2-Dichloropropane
0.00796
0.0011
mg/Kg wet
0.0113
70.2
70-130
0.992
25
1,1-Dichloropropene
0.0104
0.0023
mg/Kg wet
0.0113
91.5
70-130
1.84
25
cis-1,3-Dichloropropene
0.0110
0.00057
mg/Kg wet
0.0113
97.0
70-130
4.83
25
trans-1,3-Dichloropropene
0.0118
0.00057
mg/Kg wet
0.0113
104
70-130
3.31
25
Diethyl Ether
0.0117
0.0023
mg/Kg wet
0.0113
104
70-130
2.38
25
Diisopropyl Ether (RIPE)
0.0108
0.00057
mg/Kg wet
0.0113
95.4
70-130
3.40
25
1,4-Dioxane
0.103
0.057
mg/Kg wet
0.113
90.9
40-160
5.82
50
I:
Ethylbenzene
0.0116
0.0011
mg/Kg wet
0.0113
103
70-130
1.08
25
Hexachlorobutadiene
0.0114
0.0011
mg/Kg wet
0.0113
101
70-160
2.31
25
2-Hexanone (MBK)
0.113
0.011
mg/Kg wet
0.113
99.3
70-160
2.30
25
Isopropylbenzene (Cumene)
0.0117
0.0011
mg/Kg wet
0.0113
103
70-130
1.96
25
p-Isopropyltoluene (p-Cymene)
0.0109
0.0011
mg/Kg wet
0.0113
95.8
70-130
0.104
25
Methyl tert-Butyl Ether (MTBE)
0.0115
0.0011
mg/Kg wet
0.0113
102
70-130
0.686
25
Page 53 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215584 - SW-846 5035
LCS Dup (B215584-BSD1)
Prepared: 10/24/18 Analyzed: 10/27/18
Methylene Chloride
0.0106
0.0057
mg/Kg wet
0.0113
93.1
40-160
3.59
25 t
4-Methyl-2-pentanone (MIBK)
0.107
0.011
mg/Kg wet
0.113
94.3
70-160
2.96
25 f
Naphthalene
0.0106
0.0023
mg/Kg wet
0.0113
93.2
40-130
5.06
25 t
n-Propylbenzene
0.0116
0.0011
mg/Kg wet
0.0113
102
70-130
0.294
25
Styrene
0.0117
0.0011
mg/Kg wet
0.0113
103
70-130
0.675
25
1, 1, 1,2-Tetrachloroethane
0.0113
0.0011
mg/Kg wet
0.0113
100
70-130
0.598
25
1,1,2,2-Tetrachloroethane
0.0109
0.00057
mg/Kg wet
0.0113
96.5
70-130
6.97
25
Tetrachloroethylene
0.0112
0.0011
mg/Kg wet
0.0113
98.6
70-130
0.917
25
Tetrahydrofuran
0.0115
0.011
mg/Kg wet
0.0113
102
70-130
6.69
25
Toluene
0.0112
0.0011
mg/Kg wet
0.0113
99.2
70-130
0.202
25
1,2,3-Trichlorobenzene
0.0107
0.0057
mg/Kg wet
0.0113
94.8
70-130
4.09
25
1,2,4-Trichlorobenzene
0.00934
0.0011
mg/Kg wet
0.0113
82.4
70-130
3.21
25
1,3,5-Trichlorobenzene
0.0119
0.0011
mg/Kg wet
0.0113
105
70-130
2.22
25
1, 1, 1 -Trichloroethane
0.0105
0.0011
mg/Kg wet
0.0113
93.0
70-130
4.21
25
1,1,2-Trichloroethane
0.0115
0.0011
mg/Kg wet
0.0113
102
70-130
1.69
25
Trichloroethylene
0.0117
0.0011
mg/Kg wet
0.0113
103
70-130
3.71
25
Trichlorofluoromethane (Freon 11)
0.00876
0.0023
mg/Kg wet
0.0113
77.3
70-130
1.16
25
1,2,3-Trichloropropane
0.0111
0.0023
mg/Kg wet
0.0113
97.8
70-130
3.64
25
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.00910
0.0011
mg/Kg wet
0.0113
80.3
70-130
5.45
25
113)
1,2,4-Trimethylbenzene
0.0115
0.0011
mg/Kg wet
0.0113
102
70-130
0.493
25
1,3,5-Trimethylbenzene
0.0117
0.0011
mg/Kg wet
0,0113
103
70-130
2.36
25
Vinyl Chloride
0.0111
0.0023
mg/Kg wet
0.0113
98.0
40-130
9.80
25 t
m+p Xylene
0.0236
0.0023
mg/Kg wet
0.0227
104
70-130
1.21
25
o-Xylene
0.0122
0.0011
mg/Kg wet
0.0113
108
70-130
2.16
25
Surrogate: 1,2-Dichloroethane-d4
0.0270
mg/Kg wet
0.0283
95.4
70-130
Surrogate: Toluene-d8
0.0285
mg/Kg wet
0.0283
101
70-130
Surrogate:4-Bromofluorobenzene
0.0291
mg/Kg wet
0.0283
103
70-130
Page 54 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215606 - SW-846 3546
Blank (B215606-BLK1) Prepared: 10/24/18 Analyzed: 10/27/18
Acenaphthene
ND
0.17
mg/Kg wet
Acenaphthylene
ND
0.17
mg/Kg wet
Acetophenone
ND
0.34
mg/Kg wet
Aniline
ND
0.34
mg/Kg wet
Anthracene
ND
0.17
mg/Kg wet
Benzidine
ND
0.66
mg/Kg wet
Benzo(a)anthracene
ND
0.17
mg/Kg wet
Benzo(a)pyrene
ND
0.17
mg/Kg wet
Benzo(b)fluoranthene
ND
0.17
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.17
mg/Kg wet
Benzo(k)fluoranthene
ND
0.17
mg/Kg wet
Benzoic Acid
ND
1.0
mg/Kg wet
Bis(2-chloroethoxy)methane
ND
0.34
mg/Kg wet
Bis(2-chloroethyl)ether
ND
0.34
mg/Kg wet
Bis(2-chloroisopropyl)ether
ND
0.34
mg/Kg wet
Bis(2-Ethylhexyl)phthalate
ND
0.34
mg/Kg wet
4-Bromophenylphenylether
ND
0.34
mg/Kg wet
Butylbenzylphthalate
ND
0.34
mg/Kg wet
Carbazole
ND
0.17
mg/Kg wet
4-Chloroaniline
ND
0.66
mg/Kg wet
4-Chloro-3-methylphenol
ND
0.66
mg/Kg wet
2-Chloronaphthalene
ND
0.34
mg/Kg wet
2-Chlorophenol
ND
0.34
mg/Kg wet
4-Chlorophenylphenylether
ND
0.34
mg/Kg wet
Chrysene
ND
0.17
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.17
mg/Kg wet
Dibenzofuran
ND
0.34
mg/Kg wet
Di-n-butylphthalate
ND
0.34
mg/Kg wet
1,2-Dichlorobenzene
ND
0.34
mg/Kg wet
1,3-Dichlorobenzene
ND
0.34
mg/Kg wet
1,4-Dichlorobenzene
ND
0.34
mg/Kg wet
3,3-Dichlorobenzidine
ND
0.17
mg/Kg wet
2,4-Dichlorophenol
ND
0.34
mg/Kg wet
Diethylphthalate
ND
0.34
mg/Kg wet
2,4-Dimethylphenol
ND
0.34
mg/Kg wet
Dimethylphthalate
ND
0.34
mg/Kg wet
4,6-Dinitro-2-methylphenol
ND
0.34
mg/Kg wet
2,4-Dinitrophenol
ND
0.66
mg/Kg wet
2,4-Dinitrotoluene
ND
0.34
mg/Kg wet
2,6-Dinitrotoluene
ND
0.34
mg/Kg wet
Di-n-octylphthalate
ND
0.34
mg/Kg wet
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.34
mg/Kg wet
Fluoranthene
ND
0.17
mg/Kg wet
Fluorene
ND
0.17
mg/Kg wet
Hexachlorobenzene
ND
0.34
mg/Kg wet
Hexachlorobutadiene
ND
0.34
mg/Kg wet
Hexachlorocyclopentadiene
ND
0.34
mg/Kg wet
Hexachloroethane
ND
0.34
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.17
mg/Kg wet
Isophorone
ND
0.34
mg/Kg wet
1-Methylnaphthalene
ND
0.17
mg/Kg wet
2-Methylnaphthalene
ND
0.17
mg/Kg wet
V-34
V-05, V-34, R-05,
V-04
V-34
Page 55 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215606 - SW-846 3546
Blank (B215606-BLK1)
Prepared: 10/24/18 Analyzed: 10/27/18
2-Methylphenol
ND
0.34
mg/Kg wet
3/4-Methylphenol
ND
0.34
mg/Kg wet
Naphthalene
ND
0.17
mg/Kg wet
2-Nitroaniline
ND
0.34
mg/Kg wet
3-Nitroaniline
ND
0.34
mg/Kg wet
V-34
4-Nitroaniline
ND
0.34
mg/Kg wet
Nitrobenzene
ND
0.34
mg/Kg wet
2-Nitrophenol
ND
0.34
mg/Kg wet
4-Nitrophenol
ND
0.66
mg/Kg wet
V-20, V-34
N-Nitrosodimethylamine
ND
0.34
mg/Kg wet
N-Nitrosodiphenylamine
ND
0.34
mg/Kg wet
N-Nitrosodi-n-propylamine
ND
0.34
mg/Kg wet
Pentachloronitrobenzene
ND
0.34
mg/Kg wet
V-16
Pentachlorophenol
ND
0.34
mg/Kg wet
Phenanthrene
ND
0.17
mg/Kg wet
Phenol
ND
0.34
mg/Kg wet
Pyrene
ND
0.17
mg/Kg wet
Pyridine
ND
0.34
mg/Kg wet
1,2,4,5-Tetrachlorobenzene
ND
0.34
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.34
mg/Kg wet
2,4,5-Trichlorophenol
ND
0.34
mg/Kg wet
2,4,6-Trichlorophenol
ND
0.34
mg/Kg wet
Surrogate:2-Fluorophenol
5.09
mg/Kg wet
6.67
76.3
30-130
Surrogate: Phenol-d6
5.19
mg/Kg wet
6.67
77.8
30-130
Surrogate: Nitrobenzene-d5
2.51
mg/Kg wet
3.33
75.2
30-130
Surrogate:2-Fluorobiphenyl
2.06
mg/Kg wet
3.33
61.7
30-130
Surrogate: 2,4,6-Tribromophenol
5.25
mg/Kg wet
6.67
78.7
30-130
Surrogate: p-Terphenyl-dl4
2.32
mg/Kg wet
3.33
69.6
30-130
LCS (B215606-BSI)
Prepared: 10/24/18 Analyzed: 10/27/18
Acenaphthene
1.18
0.17
mg/Kg wet
1.67
70.9
40-140
Acenaphthylene
1.26
0.17
mg/Kg wet
1.67
75.8
40-140
Acetophenone
1.14
0.34
mg/Kg wet
1.67
68.4
40-140
Aniline
1.09
0.34
mg/Kg wet
1.67
65.5
10-140
V-34 f
Anthracene
1.20
0.17
mg/Kg wet
1.67
71.9
40-140
Benzidine
1.37
0.66
mg/Kg wet
1.67
82.2
40-140
R-05, V-04, V-05,
V-34
Benzo(a)anthracene
1.27
0.17
mg/Kg wet
1.67
76.3
40-140
Benzo(a)pyrene
1.25
0.17
mg/Kg wet
1.67
74.9
40-140
Benzo(b)fluoranthene
1.17
0.17
mg/Kg wet
1.67
70.0
40-140
Benzo(g,h,i)perylene
1.07
0.17
mg/Kg wet
1.67
64.2
40-140
Benzo(k)fluoranthene
1.19
0.17
mg/Kg wet
1.67
71.6
40-140
Benzoic Acid
0.579
1.0
mg/Kg wet
1.67
34.7
30-130
1
Bis(2-chloroethoxy)methane
1.34
0.34
mg/Kg wet
1.67
80.7
40-140
Bis(2-chloroethyl)ether
1.17
0.34
mg/Kg wet
1.67
70.1
40-140
Bis(2-chloroisopropyl)ether
1.25
0.34
mg/Kg wet
1.67
75.0
40-140
Bis(2-Ethylhexyl)phthalate
1.21
0.34
mg/Kg wet
1.67
72.6
40-140
4-Bromophenylphenylether
1.25
0.34
mg/Kg wet
1.67
75.0
40-140
Butylbenzylphthalate
1.29
0.34
mg/Kg wet
1.67
77.2
40-140
Carbazole
1.17
0.17
mg/Kg wet
1.67
69.9
40-140
4-Chloroaniline
1.12
0.66
mg/Kg wet
1.67
67.0
10-140
V-34
4-Chloro-3-methylphenol
1.25
0.66
mg/Kg wet
1.67
75.2
30-130
2-Chloronaphthalene
1.11
0.34
mg/Kg wet
1.67
66.4
40-140
Page 56 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215606 - SW-846 3546
LCS (B215606-BSI) Prepared: 10/24/18 Analyzed: 10/27/18
2-Chlorophenol
1.12
0.34
mg/Kg wet
1.67
67.3
30-130
4-Chlorophenylphenylether
1.31
0.34
mg/Kg wet
1.67
78.6
40-140
Chrysene
1.21
0.17
mg/Kg wet
1.67
72.3
40-140
Dibenz(a,h)anthracene
1.06
0.17
mg/Kg wet
1.67
63.3
40-140
Dibenzofuran
1.30
0.34
mg/Kg wet
1.67
78.0
40-140
Di-n-butylphthalate
1.21
0.34
mg/Kg wet
1.67
72.5
40-140
1,2-Dichlorobenzene
1.01
0.34
mg/Kg wet
1.67
60.3
40-140
1,3-Dichlorobenzene
0.962
0.34
mg/Kg wet
1.67
57.7
40-140
1,4-Dichlorobenzene
0.975
0.34
mg/Kg wet
1.67
58.5
40-140
3,3-Dichlorobenzidine
1.40
0.17
mg/Kg wet
1.67
84.2
20-140 t
2,4-Dichlorophenol
1.22
0.34
mg/Kg wet
1.67
73.2
30-130
Diethylphthalate
1.30
0.34
mg/Kg wet
1.67
78.0
40-140
2,4-Dimethylphenol
1.28
0.34
mg/Kg wet
1.67
76.9
30-130
Dimethylphthalate
1.33
0.34
mg/Kg wet
1.67
80.1
40-140
4,6-Dinitro-2-methylphenol
1.13
0.34
mg/Kg wet
1.67
67.9
30-130
2,4-Dinitrophenol
0.889
0.66
mg/Kg wet
1.67
53.3
30-130
2,4-Dinitrotoluene
1.30
0.34
mg/Kg wet
1.67
78.0
40-140
2,6-Dinitrotoluene
1.35
0.34
mg/Kg wet
1.67
81.1
40-140
Di-n-octylphthalate
1.16
0.34
mg/Kg wet
1.67
69.7
40-140
1,2-Diphenylhydrazine (as Azobenzene)
1.30
0.34
mg/Kg wet
1.67
78.0
40-140
Fluoranthene
1.17
0.17
mg/Kg wet
1.67
70.1
40-140
Fluorene
1.25
0.17
mg/Kg wet
1.67
75.1
40-140
Hexachlorobenzene
1.24
0.34
mg/Kg wet
1.67
74.7
40-140
Hexachlorobutadiene
1.11
0.34
mg/Kg wet
1.67
66.5
40-140
Hexachlorocyclopentadiene
1.09
0.34
mg/Kg wet
1.67
65.7
40-140
Hexachloroethane
1.04
0.34
mg/Kg wet
1.67
62.1
40-140
Indeno(1,2,3-cd)pyrene
1.07
0.17
mg/Kg wet
1.67
64.2
40-140
Isophorone
1.22
0.34
mg/Kg wet
1.67
73.3
40-140
1-Methylnaphthalene
1.06
0.17
mg/Kg wet
1.67
63.3
40-140
2-Methylnaphthalene
1.20
0.17
mg/Kg wet
1.67
71.8
40-140
2-Methylphenol
1.09
0.34
mg/Kg wet
1.67
65.4
30-130
3/4-Methylphenol
1.17
0.34
mg/Kg wet
1.67
70.3
30-130
Naphthalene
1.11
0.17
mg/Kg wet
1.67
66.4
40-140
2-Nitroaniline
1.32
0.34
mg/Kg wet
1.67
79.2
40-140
3-Nitroaniline
1.30
0.34
mg/Kg wet
1.67
77.8
30-140 V-34 t
4-Nitroaniline
1.33
0.34
mg/Kg wet
1.67
79.7
40-140
Nitrobenzene
1.12
0.34
mg/Kg wet
1.67
67.2
40-140
2-Nitrophenol
1.16
0.34
mg/Kg wet
1.67
69.8
30-130
4-Nitrophenol
1.37
0.66
mg/Kg wet
1.67
94.5
30-130 V-06,V-34
N-Nitrosodimethylarnme
0.955
0.34
mg/Kg wet
1.67
57.3
40-140
N-Nitrosodiphenylamine
1.49
0.34
mg/Kg wet
1.67
89.2
40-140
N-Nitrosodi-n-propylamine
1.14
0.34
mg/Kg wet
1.67
68.3
40-140
Pentachloronitrobenzene
1.27
0.34
mg/Kg wet
1.67
76.0
40-140 V-16
Pentachlorophenol
0.869
0.34
mg/Kg wet
1.67
52.1
30-130
Phenanthrene
1.21
0.17
mg/Kg wet
1.67
72.6
40-140
Phenol
1.24
0.34
mg/Kg wet
1.67
74.6
30-130
Pyrene
1.26
0.17
mg/Kg wet
1.67
75.5
40-140
Pyridine
0.659
0.34
mg/Kg wet
1.67
39.5
30-140
1,2,4,5-Tetrachlorobenzene
1.29
0.34
mg/Kg wet
1.67
77.3
40-140
1,2,4-Trichlorobenzene
1.09
0.34
mg/Kg wet
1.67
65.1
40-140
2,4,5-Trichlorophenol
1.33
0.34
mg/Kg wet
1.67
79.8
30-130
2,4,6-Trichlorophenol
1.34
0.34
mg/Kg wet
1.67
80.4
30-130
Page 57 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215606 - SW-846 3546
LCS (B215606-BSI) Prepared: 10/24/18 Analyzed: 10/27/18
Surrogate:2-Fluorophenol
4.94
mg/Kg wet
6.67
74.1
30-130
Surrogate: Phenol-d6
5.11
mg/Kg wet
6.67
76.7
30-130
Surrogate: Nitrobenzene-d5
2.50
mg/Kg wet
3.33
75.1
30-130
Surrogate:2-Fluorobiphenyl
2.29
mg/Kg wet
3.33
68.7
30-130
Surrogate: 2,4,6-Tribromophenol
5.87
mg/Kg wet
6.67
88.1
30-130
Surrogate:p-Terphenyl-dl4
2.57
mg/Kg wet
3.33
77.1
30-130
LCS Dup (B215606-BSD1)
Prepared: 10/24/18 Analyzed: 10/27/18
Acenaphthene
1.19
0.17
mg/Kg wet
1.67
71.3
Acenaphthylene
1.26
0.17
mg/Kg wet
1.67
75.4
Acetophenone
1.24
0.34
mg/Kg wet
1.67
74.6
Aniline
0.883
0.34
mg/Kg wet
1.67
53.0
Anthracene
1.19
0.17
mg/Kg wet
1.67
71.4
Benzidine
0.923
0.66
mg/Kg wet
1.67
55.4
Benzo(a)anthracene
1.26
0.17
mg/Kg wet
1.67
75.3
Benzo(a)pyrene
1.28
0.17
mg/Kg wet
1.67
77.0
Benzo(b)fluoranthene
1.17
0.17
mg/Kg wet
1.67
70.3
Benzo(g,h,i)perylene
1.02
0.17
mg/Kg wet
1.67
61.1
Benzo(k)fluoranthene
1.19
0.17
mg/Kg wet
1.67
71.3
Benzoic Acid
0.601
1.0
mg/Kg wet
1.67
36.1
Bis(2-chloroethoxy)methane
1.41
0.34
mg/Kg wet
1.67
84.7
Bis(2-chloroethyl)ether
1.33
0.34
mg/Kg wet
1.67
79.9
Bis(2-chloroisopropyl)ether
1.40
0.34
mg/Kg wet
1.67
84.2
Bis(2-Ethylhexyl)phthalate
1.19
0.34
mg/Kg wet
1.67
71.2
4-Bromophenylphenylether
1.26
0.34
mg/Kg wet
1.67
75.4
Butylbenzylphthalate
1.30
0.34
mg/Kg wet
1.67
77.8
Carbazole
1.16
0.17
mg/Kg wet
1.67
69.4
4-Chloroaniline
0.833
0.66
mg/Kg wet
1.67
50.0
4-Chloro-3-methylphenol
1.28
0.66
mg/Kg wet
1.67
76.8
2-Chloronaphthalene
1.25
0.34
mg/Kg wet
1.67
74.9
2-Chorophenol
1.27
0.34
mg/Kg wet
1.67
76.1
4-Chlorophenylphenylether
1.30
0.34
mg/Kg wet
1.67
77.9
Chrysene
1.18
0.17
mg/Kg wet
1.67
70.6
Dibenz(a,h)anthracene
1.03
0.17
mg/Kg wet
1.67
62.0
Dibenzofuran
1.29
0.34
mg/Kg wet
1.67
77.3
Di-n-butylphthalate
1.18
0.34
mg/Kg wet
1.67
70.6
1,2-Dichlorobenzene
1.14
0.34
mg/Kg wet
1.67
68.2
1,3-Dichlorobenzene
1.09
0.34
mg/Kg wet
1.67
65.3
1,4-Dichlorobenzene
1.11
0.34
mg/Kg wet
1.67
66.8
3,3-Dichlorobenzidine
1.08
0.17
mg/Kg wet
1.67
65.0
2,4-Dichlorophenol
1.22
0.34
mg/Kg wet
1.67
73.0
Diethylphthalate
1.30
0.34
mg/Kg wet
1.67
77.7
2,4-Dimethylphenol
1.36
0.34
mg/Kg wet
1.67
81.9
Dimethylphthalate
1.32
0.34
mg/Kg wet
1.67
79.3
4,6-Dinitro-2-methylphenol
1.08
0.34
mg/Kg wet
1.67
64.6
2,4-Dinitrophenol
0.814
0.66
mg/Kg wet
1.67
48.8
2,4-Dinitrotoluene
1.31
0.34
mg/Kg wet
1.67
78.8
2,6-Dinitrotoluene
1.37
0.34
mg/Kg wet
1.67
82.2
Di-n-octylphthalate
1.16
0.34
mg/Kg wet
1.67
69.7
1,2-Diphenylhydrazine (as Azobenzene)
1.26
0.34
mg/Kg wet
1.67
75.7
Fluoranthene
1.16
0.17
mg/Kg wet
1.67
69.7
Fluorene
1.27
0.17
mg/Kg wet
1.67
76.1
40-140
0.591
30
40-140
0.503
30
40-140
8.56
30
10-140
21.1
50
V-34
t $
40-140
0.698
30
40-140
39.0
* 30
R-05, V-04, V-05,
V-34
40-140
1.29
30
40-140
2.71
30
40-140
0.342
30
40-140
4.82
30
40-140
0.420
30
30-130
3.78
50
J
$
40-140
4.91
30
40-140
13.0
30
40-140
11.6
30
40-140
1.89
30
40-140
0.558
30
40-140
0.826
30
40-140
0.804
30
10-140
29.2
30
V-34
t
30-130
2.11
30
40-140
12.1
30
30-130
12.3
30
40-140
0.869
30
40-140
2.46
30
40-140
2.17
30
40-140
0.798
30
40-140
2.63
30
40-140
12.3
30
40-140
12.3
30
40-140
13.2
30
20-140
25.8
50
t #
30-130
0.301
30
40-140
0.359
30
30-130
6.27
30
40-140
0.928
30
30-130
4.92
30
30-130
8.81
30
40-140
0.995
30
40-140
1.35
30
40-140
0.00
30
40-140
2.99
30
40-140
0.658
30
40-140
1.27
30
Page 58 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215606 - SW-846 3546
LCS Dup (B215606-BSD1) Prepared: 10/24/18 Analyzed: 10/27/18
Hexachlorobenzene
1.26
0.34
mg/Kg wet
1.67
75.6
40-140
1.28
30
Hexachlorobutadiene
1.18
0.34
mg/Kg wet
1.67
70.7
40-140
6.12
30
Hexachlorocyclopentadiene
1.12
0.34
mg/Kg wet
1.67
66.9
40-140
1.87
30
Hexachloroethane
1.19
0.34
mg/Kg wet
1.67
71.4
40-140
14.0
30
Indeno(1,2,3-cd)pyrene
1.06
0.17
mg/Kg wet
1.67
63.3
40-140
1.35
30
Isophorone
1.27
0.34
mg/Kg wet
1.67
76.4
40-140
4.03
30
I-Methylnaphthalene
1.11
0.17
mg/Kg wet
1.67
66.4
40-140
4.78
30
2-Methylnaphthalene
1.26
0.17
mg/Kg wet
1.67
75.7
40-140
5.26
30
2-Methylphenol
1.19
0.34
mg/Kg wet
1.67
71.6
30-130
9.08
30
3/4-Methylphenol
1.23
0.34
mg/Kg wet
1.67
73.8
30-130
4.80
30
Naphthalene
1.15
0.17
mg/Kg wet
1.67
69.2
40-140
4.10
30
2-Nitroanihne
1.35
0.34
mg/Kg wet
1.67
81.0
40-140
2.22
30
3-Nitroaniline
1.13
0.34
mg/Kg wet
1.67
68.0
30-140
13.5
30 V-34 f
4-Nitroaniline
1.32
0.34
mg/Kg wet
1.67
79.3
40-140
0.478
30
Nitrobenzene
1.24
0.34
mg/Kg wet
1.67
74.4
40-140
10.2
30
2-Nitrophenol
1.20
0.34
mg/Kg wet
1.67
72.1
30-130
3.33
30
4-Nitrophenol
1.41
0.66
mg/Kg wet
1.67
84.4
30-130
11.2
50 V-06, V-34 $
N-Nitrosodimethylamine
1.17
0.34
mg/Kg wet
1.67
70.1
40-140
20.1
30
N-Nitrosodiphenylamine
1.43
0.34
mg/Kg wet
1.67
85.8
40-140
3.79
30
N-Nitrosodi-n-propylamine
1.22
0.34
mg/Kg wet
1.67
73.5
40-140
7.31
30
Pentachloronitrobenzene
1.20
0.34
mg/Kg wet
1.67
71.9
40-140
5.57
30 V-16
Pentachlorophenol
0.862
0.34
mg/Kg wet
1.67
51.7
30-130
0.809
30
Phenanthrene
1.21
0.17
mg/Kg wet
1.67
72.5
40-140
0.221
30
Phenol
1.30
0.34
mg/Kg wet
1.67
77.9
30-130
4.27
30
Pyrene
1.27
0.17
mg/Kg wet
1.67
75.9
40-140
0.528
30
Pyridine
0.828
0.34
mg/Kg wet
1.67
49.7
30-140
22.7
30 t
1,2,4,5-Tetrachlorobenzene
1.27
0.34
mg/Kg wet
1.67
76.4
40-140
1.17
30
1,2,4-Trichlorobenzene
1.17
0.34
mg/Kg wet
1.67
70.2
40-140
7.45
30
2,4,5-Trichlorophenol
1.34
0.34
mg/Kg wet
1.67
80.3
30-130
0.574
30
2,4,6-Trichlorophenol
1.31
0.34
mg/Kg wet
1.67
78.5
30-130
2.42
30
Surrogate:2-Fluorophenol
5.33
mg/Kg wet
6.67
80.0
30-130
Surrogate: Phenol-d6
5.36
mg/Kg wet
6.67
80.4
30-130
Surrogate: Nitrobenzene-d5
2.66
mg/Kg wet
3.33
79.9
30-130
Surrogate: 2-Fluorobiphenyl
2.19
mg/Kg wet
3.33
65.8
30-130
Surrogate: 2,4,6-Tribromophenol
5.84
mg/Kg wet
6.67
87.7
30-130
Surrogate: p-Terphenyl-dl4
2.53
mg/Kg wet
3.33
75.9
30-130
Page 59 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215618 - SW-846 3546
Blank (B215618-BLK1) Prepared: 10/24/18 Analyzed: 10/25/18
C9-C 18 Aliphatics
ND
10
mg/Kg wet
C19-C36 Aliphatics
ND
10
mg/Kg wet
Cl 1-C22 Aromatics
ND
10
mg/Kg wet
Acenaphthene
ND
0.10
mg/Kg wet
Acenaphthylene
ND
0.10
mg/Kg wet
Anthracene
ND
0.10
mg/Kg wet
Benzo(a)anthracene
ND
0.10
mg/Kg wet
Benzo(a)pyrene
ND
0.10
mg/Kg wet
Benzo(b)fluoranthene
ND
0.10
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.10
mg/Kg wet
Benzo(b)fluoranthene
ND
0.10
mg/Kg wet
Chrysene
ND
0.10
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.10
mg/Kg wet
Fluoranthene
ND
0.10
mg/Kg wet
Fluorene
ND
0.10
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.10
mg/Kg wet
2-Methylnaphthalene
ND
0.10
mg/Kg wet
Naphthalene
ND
0.10
mg/Kg wet
Phenanthrene
ND
0.10
mg/Kg wet
Pyrene
ND
0.10
mg/Kg wet
n-Decane
ND
0.10
mg/Kg wet
n-Docosane
ND
0.10
mg/Kg wet
n-Dodecane
ND
0.10
mg/Kg wet
n-Eicosane
ND
0.10
mg/Kg wet
n-Hexacosane
ND
0.10
mg/Kg wet
n-Hexadecane
ND
0.10
mg/Kg wet
n-Hexatriacontane
ND
0.10
mg/Kg wet
n-Nonadecane
ND
0.10
mg/Kg wet
n-Nonane
ND
0.10
mg/Kg wet
n-Octacosane
ND
0.10
mg/Kg wet
n-Octadecane
0.11
0.10
mg/Kg wet
n-Tetracosane
ND
0.10
mg/Kg wet
n-Tetradecane
ND
0.10
mg/Kg wet
n-Triacontane
ND
0.10
mg/Kg wet
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
Surrogate: Chlorooctadecane (COD)
4.16 mg/Kg wet
5.20 80.0 40-140
Surrogate: o-Terphenyl (OTP)
4.26 mg/Kg wet
5.00 85.2 40-140
Surrogate:2-Bromonaphthalene
4.31 mg/Kg wet
5.00 86.3 40-140
Surrogate: 2-Fluorobiphenyl
4.69 mg/Kg wet
5.00 93.8 40-140
LCS (B215618-BS1)
Prepared: 10/24/18 Analyzed: 10/25/18
C9-C 18 Aliphatics
24.2
10
mg/Kg wet
30.0
80.8
40-140
C19-C36Aliphatics
37.3
10
mg/Kg wet
40.0
93.1
40-140
Acenaphthene
3.69
0.10
mg/Kg wet
5.00
73.8
40-140
Acenaphthylene
3.44
0.10
mg/Kg wet
5.00
68.8
40-140
Anthracene
4.01
0.10
mg/Kg wet
5.00
80.2
40-140
Benzo(a)anthracene
3.96
0.10
mg/Kg wet
5.00
79.2
40-140
Benzo(a)pyrene
3.88
0.10
mg/Kg wet
5.00
77.7
40-140
Benzo(b)fluoranthene
4.04
0.10
mg/Kg wet
5.00
80.7
40-140
Benzo(g,h,i)perylene
3.87
0.10
mg/Kg wet
5.00
77.3
40-140
Benzo(k)fluoranthene
3.96
0.10
mg/Kg wet
5.00
79.2
40-140
Page 60 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215618 - SW-846 3546
LCS (B215618-BSI) Prepared: 10/24/18 Analyzed: 10/25/18
Chrysene
4.05
0.10
mg/Kg wet
5.00
81.0
40-140
Dibenz(a,h)anthracene
4.04
0.10
mg/Kg wet
5.00
80.7
40-140
Fluoranthene
4.10
0.10
mg/Kg wet
5.00
82.0
40-140
Fluorene
3.77
0.10
mg/Kg wet
5.00
75.4
40-140
Indeno(1,2,3-cd)pyrene
3.80
0.10
mg/Kg wet
5.00
76.1
40-140
2-Methylnaphthalene
3.20
0.10
mg/Kg wet
5.00
64.0
40-140
Naphthalene
3.25
0.10
mg/Kg wet
5.00
65.1
40-140
Phenanthrene
4.08
0.10
mg/Kg wet
5.00
81.5
40-140
Pyrene
4.12
0.10
mg/Kg wet
5.00
82.4
40-140
n-Decane
2.80
0.10
mg/Kg wet
5.00
56.1
40-140
n-Docosane
4.01
0.10
mg/Kg wet
5.00
80.3
40-140
n-Dodecane
3.27
0.10
mg/Kg wet
5.00
65.4
40-140
n-Eicosane
4.02
0.10
mg/Kg wet
5.00
80.5
40-140
n-Hexacosane
3.96
0.10
mg/Kg wet
5.00
79.3
40-140
n-Hexadecane
4.06
0.10
mg/Kg wet
5.00
81.2
40-140
n-Hexatriacontane
3.90
0.10
mg/Kg wet
5.00
77.9
40-140
n-Nonadecane
4.03
0.10
mg/Kg wet
5.00
80.5
40-140
n-Nonane
2.16
0.10
mg/Kg wet
5.00
43.1
30-140
n-Octacosane
3.87
0.10
mg/Kg wet
5.00
77.3
40-140
n-Octadecane
4.15
0.10
mg/Kg wet
5.00
83.0
40-140 B
n-Tetracosane
4.00
0.10
mg/Kg wet
5.00
80.1
40-140
n-Tetradecane
3.64
0.10
mg/Kg wet
5.00
72.8
40-140
n-Triacontane
3.90
0.10
mg/Kg wet
5.00
77.9
40-140
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
Surrogate: Chlorooctadecane (COD)
3.99
mg/Kg wet
5.20
76.6
40-140
Surrogate: o-Terphenyl (OTP)
4.07
mg/Kg wet
5.00
81.4
40-140
Surrogate: 2-Bromonaphthalene
4.10
mg/Kg wet
5.00
81.9
40-140
Surrogate:2-Fluorobiphenyl
4.63
mg/Kg wet
5.00
92.7
40-140
LCS Dup (B215618-BSD1)
Prepared: 10/24/18 Analyzed: 10/25/18
C9-C18Aliphatics
25.2
10
mg/Kg wet
30.0
83.9
40-140
3.75
C19-C36Aliphatics
39.9
10
mg/Kg wet
40.0
99.8
40-140
6.94
Acenaphthene
4.20
0.10
mg/Kg wet
5.00
84.0
40-140
12.9
Acenaphthylene
3.91
0.10
mg/Kg wet
5.00
78.2
40-140
12.8
Anthracene
4.47
0.10
mg/Kg wet
5.00
89.3
40-140
10.8
Benzo(a)anthracene
4.43
0.10
mg/Kg wet
5.00
88.5
40-140
11.1
Benzo(a)pyrene
4.34
0.10
mg/Kg wet
5.00
86.8
40-140
11.1
Benzo(b)fluoranthene
4.51
0.10
mg/Kg wet
5.00
90.2
40-140
11.1
Benzo(g,h,i)perylene
4.32
0.10
mg/Kg wet
5.00
86.5
40-140
11.2
Benzo(k)fluoranthene
4.42
0.10
mg/Kg wet
5.00
88.3
40-140
10.8
Chrysene
4.54
0.10
mg/Kg wet
5.00
90.8
40-140
11.4
Dibenz(a,h)anthracene
4.48
0.10
mg/Kg wet
5.00
89.5
40-140
10.3
Fluoranthene
4.56
0.10
mg/Kg wet
5.00
91.2
40-140
10.6
Fluorene
4.27
0.10
mg/Kg wet
5.00
85.4
40-140
12.4
Indeno(1,2,3-cd)pyrene
4.24
0.10
mg/Kg wet
5.00
84.7
40-140
10.8
2-Methylnaphthalene
3.62
0.10
mg/Kg wet
5.00
72.4
40-140
12.3
Naphthalene
3.63
0.10
mg/Kg wet
5.00
72.6
40-140
11.0
Phenanthrene
4.55
0.10
mg/Kg wet
5.00
91.0
40-140
11.0
Pyrene
4.38
0.10
mg/Kg wet
5.00
91.6
40-140
10.6
n-Decane
2.91
0.10
mg/Kg wet
5.00
58.1
40-140
3.60
n-Docosane
4.39
0.10
mg/Kg wet
5.00
87.8
40-140
8.90
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
Page 61 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215618 - SW-846 3546
LCS Dup (B215618-BSD1) Prepared: 10/24/18 Analyzed: 10/25/18
n-Dodecane
3.52
0.10
mg/Kg wet
5.00
70.5
40-140
7.50
25
n-Eicosane
4.54
0.10
mg/Kg wet
5.00
90.7
40-140
11.9
25
n-Hexacosane
4.34
0.10
mg/Kg wet
5.00
86.8
40-140
9.04
25
n-Hexadecane
4.43
0.10
mg/Kg wet
5.00
88.6
40-140
8.69
25
n-Hexatriacontane
4.22
0.10
mg/Kg wet
5.00
84.5
40-140
8.07
25
n-Nonadecane
4.39
0.10
mg/Kg wet
5.00
87.7
40-140
8.56
25
n-Nonane
2.12
0.10
mg/Kg wet
5.00
42.4
30-140
1.69
25
n-Octacosane
4.24
0.10
mg/Kg wet
5.00
84.7
40-140
9.09
25
n-Octadecane
4.49
0.10
mg/Kg wet
5.00
89.9
40-140
7.93
25 B
n-Tetracosane
4.38
0.10
mg/Kg wet
5.00
87.5
40-140
8.87
25
n-Tetradecane
4.00
0.10
mg/Kg wet
5.00
79.9
40-140
9.28
25
n-Triacontane
4.28
0.10
mg/Kg wet
5.00
85.6
40-140
9.39
25
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
Surrogate: Chlorooctadecane (COD)
4.42 mg/Kg wet
5.20 84.9 40-140
Surrogate: o-Terphenyl (OTP)
4.59 mg/Kg wet
5.00 91.7 40-140
Surrogate:2-Bromonaphthalene
4.52 mg/Kg wet
5.00 90.4 40-140
Surrogate:2-Fluorobiphenyl
5.02 mg/Kg wet
5.00 100 40-140
Matrix Spike (B215618-MS1)
Source: 18J1112-01
Prepared: 10/24/18 Analyzed: 10/29/18
C9-C18 Aliphatics
101
13
mg/Kg dry
40.4
74.3
65.2
40-140
C19-C36 Aliphatics
67.8
13
mg/Kg dry
53.9
24.8
79.7
40-140
Acenaphthene
3.18
0.13
mg/Kg dry
6.74
0.241
73.4
40-140
Acenaphthylene
4.45
0.13
mg/Kg dry
6.74
ND
66.1
40-140
Anthracene
5.40
0.13
mg/Kg dry
6.74
ND
80.1
40-140
Benzo(a)anthracene
3.25
0.13
mg/Kg dry
6.74
ND
77.9
40-140
Benzo(a)pyrene
5.18
0.13
mg/Kg dry
6.74
ND
76.9
40-140
Benzo(b)fluoranthene
5.36
0.13
mg/Kg dry
6.74
ND
79.6
40-140
Benzo(g,h,i)perylene
3.28
0.13
mg/Kg dry
6.74
ND
78.4
40-140
Benzo(k)fluoranthene
5.25
0.13
mg/Kg dry
6.74
ND
78.0
40-140
Chrysene
5.30
0.13
mg/Kg dry
6.74
ND
78.7
40-140
Dibenz(a,h)anthracene
3.21
0.13
mg/Kg dry
6.74
ND
77.3
40-140
Fluoranthene
5.56
0.13
mg/Kg dry
6.74
ND
82.5
40-140
Fluorene
5.37
0.13
mg/Kg dry
6.74
0.259
75.9
40-140
Indeno(1,2,3-cd)pyrene
4.99
0.13
mg/Kg dry
6.74
ND
74.1
40-140
2-Methylnaphthalene
4.80
0.13
mg/Kg dry
6.74
0.492
64.0
40-140
Naphthalene
4.50
0.13
mg/Kg dry
6.74
0.330
61.9
40-140
Phenanthrene
3.74
0.13
mg/Kg dry
6.74
0.285
81.0
40-140
Pyrene
5.62
0.13
mg/Kg dry
6.74
ND
83.4
40-140
n-Nonane
2.01
0.13
mg/Kg dry
6.74
ND
29.9
* 30-140 MS-22
Surrogate: Chlorooctadecane (COD)
5.04 mg/Kg dry 7.01 71.9 40-140
Surrogate: o-Terphenyl (OTP)
5.41 mg/Kg dry 6.74 80.3 40-140
Surrogate: 2-Bromonaphthalene
6.12 mg/Kg dry 6.74 90.8 40-140
Surrogate: 2-Fluorobiphenyl
6.92 mg/Kg dry 6.74 103 40-140
Page 62 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215618 - SW-846 3546
Matrix Spike Dup (B215618-MSD1) Source: 18J1112-01 Prepared: 10/24/18 Analyzed: 10/29/18
C9-C18 Aliphatics
111
14
mg/Kg dry
40.8
74.3
90.1
40-140
9.83
50
C19-C36 Aliphatics
71.0
14
mg/Kg dry
54.4
24.8
84.8
40-140
4.59
50
Acenaphthene
5.04
0.14
mg/Kg dry
6.80
0.241
70.5
40-140
2.88
50
Acenaphthylene
4.31
0.14
mg/Kg dry
6.80
ND
63.4
40-140
3.21
50
Anthracene
5.25
0.14
mg/Kg dry
6.80
ND
77.1
40-140
2.82
50
Benzo(a)anthracene
5.14
0.14
mg/Kg dry
6.80
ND
75.5
40-140
2.14
50
Benzo(a)pyrene
4.07
0.14
mg/Kg dry
6.80
ND
74.5
40-140
2.12
50
Benzo(k)fluoranthene
5.26
0.14
mg/Kg dry
6.80
ND
77.3
40-140
1.96
50
Benzo(g,h,i)perylene
5.17
0.14
mg/Kg dry
6.80
ND
76.0
40-140
2.17
50
Benzo(k)fluoranthene
4.07
0.14
mg/Kg dry
6.80
ND
74.6
40-140
3.48
50
Chrysene
5.17
0.14
mg/Kg dry
6.80
ND
76.0
40-140
2.54
50
Dibenz(a,h)anthracene
5.09
0.14
mg/Kg dry
6.80
ND
74.8
40-140
2.27
50
Fluoranthene
5.43
0.14
mg/Kg dry
6.80
ND
79.9
40-140
2.31
50
Fluorene
5.21
0.14
mg/Kg dry
6.80
0.259
72.7
40-140
3.11
50
Indeno(1,2,3-cd)pyrene
4.88
0.14
mg/Kg dry
6.80
ND
71.7
40-140
2.21
50
2-Methylnaphthalene
4.80
0.14
mg/Kg dry
6.80
0.492
63.2
40-140
0.172
50
Naphthalene
4.46
0.14
mg/Kg dry
6.80
0.330
60.7
40-140
0.862
50
Phenanthrene
5.55
0.14
mg/Kg dry
6.80
0.285
77.4
40-140
3.45
50
Pyrene
5.51
0.14
mg/Kg dry
6.80
ND
80.9
40-140
2.07
50
n-Nonane
2.09
0.14
mg/Kg dry
6.80
ND
30.8
30-140
3.87
50
Surrogate: Chlorooctadecane (COD)
5.17 mg/Kg dry 7.08 73.1 40-140
Surrogate: o-Terphenyl (OTP)
5.21 mg/Kg dry 6.80 76.6 40-140
Surrogate: 2-13romonaphthalene
6.17 mg/Kg dry 6.80 90.7 40-140
Surrogate:2-Fluorobiphenyl
6.89 mg/Kg dry 6.80 101 40-140
Page 63 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - VPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215495 - MA VPH
Blank (B215495-BLK1) Prepared: 10/23/18 Analyzed: 10/25/18
C5-C8 Aliphatics
ND
10
mg/Kg wet
C9-C12 Aliphatics
ND
10
mg/Kg wet
C9-C 10 Aromatics
ND
10
mg/Kg wet
Benzene
ND
0.050
mg/Kg wet
Butylcyclohexane
ND
0.050
mg/Kg wet
Decane
ND
0.050
mg/Kg wet
Ethylbenzene
ND
0.050
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.050
mg/Kg wet
2-Methylpentane
ND
0.050
mg/Kg wet
Naphthalene
ND
0.50
mg/Kg wet
Nonane
ND
0.050
mg/Kg wet
Pentane
ND
0.050
mg/Kg wet
Toluene
ND
0.050
mg/Kg wet
1,2,4-Trimethylbenzene
ND
0.050
mg/Kg wet
2,2,4-Trimethylpentane
ND
0.050
mg/Kg wet
m+p Xylene
ND
0.10
mg/Kg wet
o-Xylene
ND
0.050
mg/Kg wet
Surrogate:2,5-Dibromotoluene (FID) 35.8 µg/L 40.0 89.6 70-130
Surrogate:2,5-Dibromotoluene (PID) 33.9 µg/L 40.0 84.7 70-130
LCS (B215495-BS1) Prepared: 10/23/18 Analyzed: 10/25/18
C9-C 10 Aromatics
0.144
0.20
mg/Kg wet
70-130
Benzene
0.0964
0.0010
mg/Kg wet
0.100
96.4
70-130
Butylcyclohexane
0.0856
0.0010
mg/Kg wet
0.100
85.6
70-130
Decane
0.0867
0.0010
mg/Kg wet
0.100
86.7
70-130
Ethylbenzene
0.101
0.0010
mg/Kg wet
0.100
101
70-130
Methyl tert-Butyl Ether (MTBE)
0.0956
0.0010
mg/Kg wet
0.100
95.6
70-130
2-Methylpentane
0.101
0.0010
mg/Kgwet
0.100
101
70-130
Naphthalene
0.0916
0.010
mg/Kg wet
0.100
91.6
70-130
Nonane
0.0829
0.0010
mg/Kg wet
0.100
82.9
30-130
Pentane
0.0871
0.0010
mg/Kg wet
0.100
87.1
70-130
Toluene
0.0987
0.0010
mg/Kg wet
0.100
98.7
70-130
1,2,4-Trimethylbenzene
0.105
0.0010
mg/Kg wet
0.100
105
70-130
2,2,4-Trimethylpentane
0.101
0.0010
mg/Kg wet
0.100
101
70-130
m+p Xylene
0.206
0.0020
mg/Kg wet
0.200
103
70-130
o-Xylene
0.101
0.0010
mg/Kg wet
0.100
101
70-130
Surrogate: 2,5-Dibromotoluene (FID) 33.8 µg/L 40.0 84.6 70-130
Surrogate: 2,5-Dibromotoluene (PID) 30.1 µg/L 40.0 75.1 70-130
LCS Dup (B215495-BSD1) Prepared: 10/23/18 Analyzed: 10/25/18
C9-C 10 Aromatics
0.147
0.20
mg/Kg wet
70-130
1.89
Benzene
0.0977
0.0010
mg/Kg wet
0.100
97.7
70-130
1.35
Butylcyclohexane
0.0868
0.0010
mg/Kg wet
0.100
86.8
70-130
1.39
Decane
0.0883
0.0010
mg/Kg wet
0.100
88.3
70-130
1.83
Ethylbenzene
0.103
0.0010
mg/Kg wet
0.100
103
70-130
1.44
Methyl tert-Butyl Ether (MTBE)
0.0963
0.0010
mg/Kg wet
0.100
96.3
70-130
0.761
2-Methylpentane
0.102
0.0010
mg/Kg wet
0.100
102
70-130
1.06
Naphthalene
0.0968
0.010
mg/Kg wet
0.100
96.8
70-130
5.57
Nonane
0.0839
0.0010
mg/Kg wet
0.100
83.9
30-130
1.26
Pentane
0.0915
0.0010
mg/Kg wet
0.100
91.5
70-130
4.88
Toluene
0.100
0.0010
mg/Kg wet
0.100
100
70-130
1.49
1,2,4-Trimethylbenzene
0.106
0.0010
mg/Kg wet
0.100
106
70-130
1.45
25
25
25
25
25
25
25
25
25
25
25
25
Page 64 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - VPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215495 - MA VPH
LCS Dup (B215495-BSD1)
Prepared: 10/23/18 Analyzed: 10/25/18
2,2,4-Trimethylpentane
0.103
0.0010
mg/Kg wet
0.100
103
70-130 2.10 25
m+p Xylene
0.209
0.0020
mg/Kg wet
0.200
105
70-130 1.43 25
o-Xylene
0.103
0.0010
mg/Kg wet
0.loo
103
70-130 1.25 25
Surrogate: 2,5-Dibromotoluene (FID)
35.1
µg/L
40.0
87.8
70-130
Surrogate:2,5-Dibromotoluene (PID)
33.6
µg/L
40.0
84.0
70-130
Batch B215561 - MA VPH
Blank (11215561-BLKI)
Prepared & Analyzed: 10/24/18
C5-C8 Aliphatics
ND
10
mg/Kg wet
C9-C 12 Aliphatics
ND
10
mg/Kg wet
C9-C10 Aromatics
ND
10
mg/Kg wet
Benzene
ND
0.050
mg/Kg wet
Butylcyclohexane
ND
0.050
mg/Kg wet
Decane
ND
0.050
mg/Kg wet
Ethylbenzene
ND
0.050
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.050
mg/Kg wet
2-Methylpentane
ND
0.050
mg/Kg wet
Naphthalene
ND
0.50
mg/Kg wet
Nonane
ND
0.050
mg/Kg wet
Pentane
ND
0.050
mg/Kg wet
Toluene
ND
0.050
mg/Kg wet
1,2,4-Trimethylbenzene
ND
0.050
mg/Kg wet
2,2,4-Trimethylpentane
ND
0.050
mg/Kg wet
m+p Xylene
ND
0.10
mg/Kg wet
o-Xylene
ND
0.050
mg/Kg wet
Surrogate: 2,5-Dibromotoluene (FID)
44.3
µg/L
40.0
111
70-130
Surrogate:2,5-Dibromotoluene (PID)
40.5
µg/L
40.0
101
70-130
LCS (B215561-BS1)
Prepared & Analyzed: 10/24/18
C9-C10Aromatics
0.0798
0.20
mg/Kg wet
70-130
Benzene
0.0522
0.0010
mg/Kg wet
0.0500
104
70-130
Butylcyclohexane
0.0593
0.0010
mg/Kg wet
0.0500
119
70-130
Decane
0.0473
0.0010
mg/Kg wet
0.0500
94.7
70-130
Ethylbenzene
0.0547
0.0010
mg/Kg wet
0.0500
109
70-130
Methyl tert-Butyl Ether (MTBE)
0.0511
0.0010
mg/Kg wet
0.0500
102
70-130
2-Methylpentane
0.0533
0.0010
mg/Kg wet
0.0500
107
70-130
Naphthalene
0.0570
0.010
mg/Kgwet
0.0500
114
70-130
Nonane
0.0578
0.0010
mg/Kg wet
0.0500
116
30-130
Pentane
0.0462
0.0010
mg/Kg wet
0.0500
92.5
70-130
Toluene
0.0532
0.0010
mg/Kg wet
0.0500
106
70-130
1,2,4-Trimethylbenzene
0.0576
0.0010
mg/Kg wet
0.0500
115
70-130
2,2,4-Trimethylpentane
0.0532
0.0010
mg/Kg wet
0.0500
106
70-130
m+p Xylene
0.112
0.0020
mg/Kg wet
0.100
112
70-130
o-Xylene
0.0548
0.0010
mg/Kg wet
0.0500
110
70-130
Surrogate:2,5-Dibromotoluene (FID)
45.4
µg/L
40.0
114
70-130
Surrogate:2,5-Dibromotoluene (PID)
40.6
µg/L
40.0
102
70-130
Page 65 of 78

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - VPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B215561 - MA VPH
LCS Dup (B215561-BSD1) Prepared & Analyzed: 10/24/18
C9-C 10 Aromatics
0.0758
0.20
mg/Kg wet
70-130
5.10
25
Benzene
0.0500
0.0010
mg/Kg wet
0.0500
99.9
70-130
4.34
25
Butylcyclohexane
0.0570
0.0010
mg/Kg wet
0.0500
114
70-130
3.99
25
Decane
0.0446
0.0010
mg/Kg wet
0.0500
89.2
70-130
5.96
25
Ethylbenzene
0.0524
0.0010
mg/Kg wet
0.0500
105
70-130
4.31
25
Methyl tert-Butyl Ether (MTBE)
0.0499
0.0010
mg/Kg wet
0.0500
99.9
70-130
2.30
25
2-Methylpentane
0.0505
0.0010
mg/Kg wet
0.0500
101
70-130
5.40
25
Naphthalene
0.0567
0.010
mg/Kg wet
0.0500
113
70-130
0.586
25
Nonane
0.0554
0.0010
mg/Kg wet
0.0500
ill
30-130
4.16
25
Pentane
0.0439
0.0010
mg/Kg wet
0.0500
87.9
70-130
5.10
25
Toluene
0.0510
0.0010
mg/Kg wet
0.0500
102
70-130
4.22
25
1,2,4-Trimethylbenzene
0.0550
0.0010
mg/Kg wet
0.0500
110
70-130
4.60
25
2,2,4-Trimethylpentane
0.0512
0.0010
mg/Kg wet
0.0500
102
70-130
3.81
25
m+p Xylene
0.107
0.0020
mg/Kg wet
0.100
107
70-130
4.74
25
o-Xylene
0.0526
0.0010
mg/Kg wet
0.0500
105
70-130
4.19
25
Surrogate:2,5-Dibromotoluene (FID) 45.5 µg/L 40.0 114 70-130
Surrogate:2,5-Dibromotoluene (PID) 40.5 µg/L 40.0 101 70-130
Page 66 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*
QC result is outside of established limits.
fi
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
B Analyte is found in the associated laboratory blank as well as in the sample.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is within method specified criteria.
0-01 Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered
with methanol, but with less than the method -specified amount.
R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
RL-05 Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met.
RL-11 Elevated reporting limit due to high concentration of target compounds.
V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria. Reported result is estimated.
V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound.
V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound.
V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may
be associated with reported result.
V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with
correlation coefficient <0.99. Reported result is estimated.
V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
Page 67 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
MADEP-EPH-04-1.1 in Soil
C9-C18 Aliphatics
CT,NC,ME,NH-P
C19-06 Aliphatics
CT,NC,ME,NH-P
Unadjusted Cl1-C22 Aromatics
CT,NC,ME,NH-P
C11-C22 Aromatics
CT,NC,ME,NH-P
Acenaphthene
CT,NC,ME,NH-P
Acenaphthylene
CT,NC,ME,NH-P
Anthracene
CT,NC,ME,NH-P
Benzo(a)anthracene
CT,NC,ME,NH-P
Benzo(a)pyrene
CT,NC,ME,NH-P
Benzo(b)fluoranthene
CT,NC,ME,NH-P
Benzo(g,h,i)perylene
CT,NC,ME,NH-P
Benzo(k)fluoranthene
CT,NC,ME,NH-P
Chrysene
CT,NC,ME,NH-P
Dibenz(a,h)anthracene
CT,NC,ME,NH-P
Fluoranthene
CT,NC,ME,NH-P
Fluorene
CT,NC,ME
Indeno(1,2,3-cd)pyrene
CT,NC,ME NH-P
2-Methylnaphthalene
CT,NC,ME
Naphthalene
CT,NC,ME,NH-P
Phenanthrene
CT,NC,ME,NH-P
Pyrene
CT,NC,ME,NH-P
MADEP-VPH-Feb 1018 Rev 2.1 in Soil
C5-C8 Aliphatics
CT,NC,ME,NH-P
C9-C12 Aliphatics
CT,NC,ME,NH-P
C9-C10 Aromatics
CT,NC,ME,NH-P
Benzene
CT,NC,ME,NH-P
Ethylbenzene
CT,NC,ME,NH-P
Methyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-P
Naphthalene
CT,NC,ME,NH-P
Toluene
CT,NC,ME,NH-P
m+p Xylene
CT,NC,ME,NH-P
o-Xylene
CT,NC,ME,NH-P
SW-846 8260B in Soil
Acetone
NC
Acetone
NC
Acrylonitrile
NC
Acrylonitrile
NC
tert-Amyl Methyl Ether (TAME)
NC
tert-Amyl Methyl Ether (TAME)
NC
Benzene
NC
Benzene
NC
Bromobenzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Page 68 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8260B in Soil
Bromodichloromethane
NC
Bromoform
NC
Bromoform
NC
Bromomethane
NC
Bromomethane
NC
2-Butanone (MEK)
NC
2-Butanone (MEK)
NC
tert-Butyl Alcohol (TBA)
NC
tert-Butyl Alcohol (TBA)
NC
n-Butylbenzene
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
tert-Butylbenzene
NC
tert-Butyl Ethyl Ether (TBEE)
NC
tert-Butyl Ethyl Ether (TBEE)
NC
Carbon Disulfide
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroethane
NC
Chloroform
NC
Chloroform
NC
Chloromethane
NC
Chloromethane
NC
2-Chlorotoluene
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromo-3-chloropropane (DBCP)
NC
1,2-Dibromo-3-chloropropane (DBCP)
NC
1,2-Dibromoethane (EDB)
NC
1,2-Dibromoethane (EDB)
NC
Dibromomethane
NC
Dibromomethane
NC
1,2-Dichlorobenzene
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
Page 69 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8260B in Soil
trans-1,4-Dichloro-2-butene
NC
trans-1,4-Dichloro-2-butene
NC
Dichlorodifluoromethane (Freon 12)
NC
Dichlorodifluoromethane (Freon 12)
NC
1,1-Dichloroethane
NC
1,1-Dichloroethane
NC
1,2-Dichloroethane
NC
1,2-Dichloroethane
NC
1,1-Dichloroethylene
NC
1,1-Dichloroethylene
NC
cis-1,2-Dichloroethylene
NC
cis-1,2-Dichloroethylene
NC
trans-1,2-Dichloroethylene
NC
trans-1,2-Dichloroethylene
NC
1,2-Dichloropropane
NC
1,2-Dichloropropane
NC
1,3-Dichloropropane
NC
1,3-Dichloropropane
NC
2,2-Dichloropropane
NC
2,2-Dichloropropane
NC
1,1-Dichloropropene
NC
1,1-Dichloropropene
NC
cis- 1,3 -Dichloropropene
NC
cis- 1,3 -Dichloropropene
NC
trans- l,3-Dichloropropene
NC
trans- l,3-Dichloropropene
NC
Diethyl Ether
NC
Diethyl Ether
NC
Diisopropyl Ether (DIPE)
NC
Diisopropyl Ether (DIPE)
NC
1,4-Dioxane
NC
1,4-Dioxane
NC
Ethylbenzene
NC
Ethylbenzene
NC
Hexachlorobutadiene
NC
Hexachlorobutadiene
NC
2-Hexanone (MBK)
NC
2-Hexanone (MBK)
NC
Isopropylbenzene (Cumene)
NC
Isopropylbenzene (Cumene)
NC
p-Isopropyltoluene (p-Cymene)
NC
p-Isopropyltoluene (p-Cymene)
NC
Methyl tert-Butyl Ether (MTBE)
NC
Methyl tert-Butyl Ether (MTBE)
NC
Methylene Chloride
NC
Methylene Chloride
NC
4-Methyl-2-pentanone (MIBK)
NC
Page 70 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
SW-846 8260B in Soil
4-Methyl-2-pentanone (MIBK)
Naphthalene
Naphthalene
n-Propylbenzene
n-Propylbenzene
Styrene
Styrene
1, 1, 1,2-Tetrachloroethane
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
1,1, 2, 2-Tetrachloroethane
Tetrachloroethylene
Tetrachloroethylene
Tetrahydrofuran
Tetrahydrofuran
Toluene
Toluene
1,2,3-Trichlorobenzene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trichlorobenzene
1,3,5-Trichlorobenzene
1, 1, 1 -Trichloroethane
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
1,1,2-Trichloroethane
Trichloroethylene
Trichloroethylene
Trichlorofluoromethane (Freon 11)
Trichlorofluoromethane (Freon 11)
1,2,3-Trichloropropane
1,2,3-Trichloropropane
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1,2,4-Trimethylbenzene
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Chloride
Vinyl Chloride
m+p Xylene
m+p Xylene
o-Xylene
o-Xylene
SW-846 8270D in Soil
Certifications
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
Page 71 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Soil
Acenaphthene
CT,NY,NH,ME,NC,VA
Acenaphthylene
CT,NY,NH,ME,NC,VA
Acetophenone
NY,NH,ME,NC,VA
Aniline
NY,NH,ME,NC,VA
Anthracene
CT,NY,NH,ME,NC,VA
Benzidine
CT,NY,NH,ME,NC,VA
Benzo(a)anthracene
CT,NY,NH,ME,NC,VA
Benzo(a)pyrene
CT,NY,NH,ME,NC,VA
Benzo(b)fluoranthene
CT,NY,NH,ME,NC,VA
Benzo(g,h,i)perylene
CT,NY,NH,ME,NC,VA
Benzo(k)fluoranthene
CT,NY,NH,ME,NC,VA
Benzoic Acid
NY,NH,ME,NC,VA
Bis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VA
Bis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VA
Bis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VA
Bis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA
4-Bromophenylphenylether
CT,NY,NH,ME,NC,VA
Butylbenzylphthalate
CT,NY,NH,Nffi,NC,VA
Carbazole
NC
4-Chloroaniline
CT,NY,NH,ME,NC,VA
4-Chloro-3-methylphenol
CT,NY,NH,ME,NC,VA
2-Chloronaphthalene
CT,NY,NH,NC,VA
2-Chlorophenol
CT,NY,NH,ME,NC,VA
4-Chlorophenylphenylether
CT,NY NH,ME,NC,VA
Chrysene
CT,NY,NH,ME,NC,VA
Dibenz(a,h)anthracene
CT,NY,NH,ME,NC,VA
Dibenzofuran
CT,NY,NH,ME,NC,VA
Di-n-butylphthalate
CT,NY,NH,ME,NC,VA
1,2-Dichlorobenzene
NY,NH,ME,NC,VA
1,3-Dichlorobenzene
NY,NH,ME,NC,VA
1,4-Dichlorobenzene
NY,NH,ME,NC,VA
3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA
2,4-Dichlorophenol
CT,NY,NH,ME,NC,VA
Diethylphthalate
CT,NY,NH,ME,NC,VA
2,4-Dimethylphenol
CT,NY,NH,ME,NC,VA
Dimethylphthalate
CT,NY,NH,ME,NC,VA
4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA
2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VA
Di-n-octylphthalate
CT,NY,NH,ME,NC,VA
1,2-Diphenylhydrazine (as Azobenzene)
NY,NH,ME,NC,VA
Fluoranthene
CT,NY,NH,ME,NC,VA
Fluorene
NY,NH,ME,NC,VA
Hexachlorobenzene
CT,NY,NH,ME,NC,VA
Hexachlorobutadiene
CT,NY,NH,ME,NC,VA
Hexachlorocyclopentadiene
CT,NY,NH,ME,NC,VA
Page 72 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Soil
Hexachloroethane
CT,NY,NH,ME,NC,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA
Isophorone
CT,NY,NH,ME,NC,VA
1-Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NH,ME,NC,VA
2-Methylphenol
CT,NY,NH,ME,NC,VA
3/4-Methylphenol
CT,NY,NH,ME,NC,VA
Naphthalene
CT,NY,NH,ME,NC,VA
2-Nitroaniline
CT,NY,NH,ME,NC,VA
3-Nitroaniline
CT,NY,NH,ME,NC,VA
4-Nitroaniline
CT,NY,NH,ME,NC,VA
Nitrobenzene
CT,NY,NH,ME,NC,VA
2-Nitrophenol
CT,NY,NH,ME,NC,VA
4-Nitrophenol
CT,NY,NH,ME,NC,VA
N-Nitrosodimethylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodiphenylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodi-n-propylamine
CT,NY,NH,ME,NC,VA
Pentachloronitrobenzene
NY,NC
Pentachlorophenol
CT,NY,NH,ME,NC,VA
Phenanthrene
CT,NY,NH,ME,NC,VA
Phenol
CT,NY,NH,ME,NC,VA
Pyrene
CT,NY,NH,ME,NC,VA
Pyridine
CT,NY,NH,ME,NC,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA
2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA
2,4,6-Trichlorophenol
CT,NY,NH,ME,NC,VA
2-Fluorophenol
NC
SW-846 8270D in Water
Acenaphthene
CT,NY,NC,ME,NH,VA
Acenaphthylene
CT,NY,NC,ME,NH,VA
Acetophenone
NY,NC
Aniline
CT,NY,NC,ME,VA
Anthracene
CT,NY,NC,ME,NH,VA
Benzidine
CT,NY,NC,ME,NH,VA
Benzo(a)anthracene
CT,NY,NC,ME,NH,VA
Benzo(a)pyrene
CT,NY,NC,ME,NH,VA
Benzo(b)fluoranthene
CT,NY,NC,ME,NH,VA
Benzo(g,h,i)perylene
CT,NY,NC,ME,NH,VA
Benzo(k)fluoranthene
CT,NY,NC,ME,NH,VA
Benzoic Acid
NY,NC,ME,NH,VA
Bis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VA
Bis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA
4-Bromophenylphenylether
CT,NY,NC,ME,NH,VA
Page 73 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Water
Butylbenzylphthalate
CT,NY,NC,ME,NH,VA
Carbazole
NC
4-Chloroaniline
CT,NY,NC,ME,NH,VA
4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA
2-Chloronaphthalene
CT,NY,NC,ME,NH,VA
2-Chlorophenol
CT,NY,NC,ME,NH,VA
4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VA
Chrysene
CT,NY,NC,ME,NH,VA
Dibenz(a,h)anthracene
CT,NY,NC,ME,NH,VA
Dibenzofuran
CT,NY,NC,ME,NH,VA
Di-n-butylphthalate
CT,NY,NC,ME,NH,VA
1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA
3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA
2,4-Dichlorophenol
CT,NY,NC,ME,NH,VA
Diethylphthalate
CT,NY,NC,ME,NH,VA
2,4-Dimethylphenol
CT,NY,NC,ME,NH,VA
Dimethylphthalate
CT,NY,NC,ME,NH,VA
4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA
2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VA
Di-n-octylphthalate
CT,NY,NC,ME,NH,VA
1,2-Diphenylhydrazine(as Azobenzene)
NY,NC
Fluoranthene
CT,NY,NC,ME,NH,VA
Fluorene
NY,NC,ME,NH,VA
Hexachlorobenzene
CT,NY,NC,ME,NH,VA
Hexachlorobutadiene
CT,NY,NC,ME,NH,VA
Hexachlorocyclopentadiene
CT,NY,NC,ME,NH,VA
Hexachloroethane
CT,NY,NC,ME,NH,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VA
Isophorone
CT,NY,NC,ME,NH,VA
I -Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NC,ME,NH,VA
2-Methylphenol
CT,NY,NC,NH,VA
3/4-Methylphenol
CT,NY,NC,NH,VA
Naphthalene
CT,NY,NC,ME,NH,VA
2-Nitroaniline
CT,NY,NC,ME,NH,VA
3-Nitroaniline
CT,NY,NC,ME,NH,VA
4-Nitroaniline
CT,NY,NC,ME,NH,VA
Nitrobenzene
CT,NY,NC,ME,NH,VA
2-Nitrophenol
CT,NY,NC,ME,NH,VA
4-Nitrophenol
CT,NY,NC,ME,NH,VA
N-Nitrosodimethylamine
CT,NY,NC,ME,NH,VA
N-Nitrosodiphenylamine
CT,NY,NC,ME,NH,VA
N-Nitrosodi-n-propylamine
CT,NY,NC,ME,NH,VA
Page 74 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8270D in Water
Pentachloronitrobenzene
NC
Pentachlorophenol
CT,NY,NC,ME,NH,VA
Phenanthrene
CT,NY,NC,ME,NH,VA
Phenol
CT,NY,NC,ME,NH,VA
Pyrene
CT,NY,NC,ME,NH,VA
Pyridine
CT,NY,NC,ME,NH,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA
2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA
2,4,6-Trichlorophenol
CT,NY,NC,ME,NH,VA
2-Fluorophenol
NC
The CON -TEST Environmental Laboratory operates under the
following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA
Massachusetts DEP
M-MA100
06/30/2019
CT
Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY
New York State Department of Health
10899 NELAP
04/1/2019
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI
Rhode Island Department of Health
LA000112
12/30/2018
NC
North Carolina Div. of Water Quality
652
12/31/2018
NJ
New Jersey DEP
MA007 NELAP
06/30/2019
FL
Florida Department of Health
E871027 NELAP
06/30/2019
VT
Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME
State of Maine
2011028
06/9/2019
VA
Commonwealth of Virginia
460217
12/14/2018
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW
North Carolina Department of Health
25703
07/31/2019
Page 75 of 78

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Table of Contents
I Have Not Confirmed Sample ContainerC C3) n te S t
UIP
Numbers With Lab Staff Before Relinquishing
Over Samples
Doc�:277 ,Rev 5'2017
Login Sample Receipt Checklist: - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client WOA
Received By Zry Date 2 Time 91 q
On Ice
,-� ---
How were the samples
received? Direct from Sampling Ambient Melted Ice
Were samples within By Gun # Actual Temp -
Temperature? 2-WC By Blank # Actual Temp -
Was Custody Sea[ Intact? ( Were Samples Tampered with? l�
Was COC Relinquished ? fi Does Chain Agree With Samples?
Are there broken/leaking/loose caps on any samples? ` -
Is COC in ink/ Legible? i _ Were samples received within holding time? _ ti -
Did COC include all Client Analysis T` Sampler Name ---
pertinent Information? Project ID's t — Collection Dates/Times
Are Sample labels filled out and legible? t
Are there Lab to Filters?_ Who was notified?
Are there Rushes? �_ Who was notified?
Are there Short Holds? Who was notified?
Is there enough Volume?
Is there Headspace where applicable? MS/MSD?
Proper Media/Containers Used? Is splitting sampl required?
Were trip blanks received? On COC?
Do all samples have the proper pH? Acid Base
In Cooler
No Cooler
No Ice
78 of 78
In Cooler
No Cooler
No Ice
78 of 78

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
November 8, 2018
Rob Foster
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: 5318 Morris Field Drive
Client Job Number:
Project Number: 6228-18-0503
Laboratory Work Order Number: 18KO087
Enclosed are results of analyses for samples received by the laboratory on November 1, 2018. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 39

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
18K0087-01
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/ 4S
B216398
Semivolatile Organic Compounds by GUMS
B216342
Petroleum Hydrocarbons Analyses - EPH
B216348
Petroleum Hydrocarbons Analyses - VPH
B216531
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
3
4
7
7
14
15
15
15
20
20
25
25
28
28
30
31
37
Page 2 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce StreetEast Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
AMEC - Charlotte
2801 Yorkmont Rd, Suite 100 REPORT DATE: 11 /8/2018
Charlotte, NC 28208 PURCHASE ORDER NUMBER:
ATTN: Rob Foster
PROJECT NUMBER: 6228-18-0503
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18KO087
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report.
PROJECT LOCATION: 5318 Morris Field Drive
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
TB-4-18 18KO087-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-Feb
2018 Rev 2.1
SM 254OG
SW-846 8260B
SW-846 8270D
Page 3 of 39

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA EPH, only hydrocarbon ranges were requested and reported.
For method MA VPH, only adjusted hydrocarbon ranges were requested and reported.
Page 4 of 39

Table of Contents
40 ,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
MADEP-EPH-04-1.1
Qualifications:
L-07A
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
outside of control limits. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
n-Decane
B216348-BSD1
n-Nonane
B216348-BSD1
R-05
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
n-Decane
B216348-BLKI, B216348-BSI
n-Nonane
B216348-BLKI, B216348-BSI
SW-846 8260B
Qualifications:
L-07A
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
outside of control limits. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
Acetone
B216398-BS1
R-05
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
2-Butanone (MEK)
18K0087-01[TB-4-18], B216398-BLKI, B216398-BSI, B216398-BSDI
Acetone
18K0087-01 [TB-4-18], B216398-BLKI, B216398-BSI, B216398-BSDI
SW-846 8270D
Qualifications:
L-04
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
Hexachlorocyclopentadiene
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSD1
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
Pyridine
B216342-BSDI
Page 5 of 39

,con-testo
ANALYTICAL LABORATORY
Table of Contents
V-05
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
4-Chloroaniline
18K0087-01 [TB-4-18]
Aniline
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
Benzidine
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
Chrysene
18K0087-01 [TB-4-18]
Hexachlorocyclopentadiene
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSD1
Pyridine
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
V-06
Continuing calibration did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
2-Nitroaniline
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
4-Nitrophenol
18K0087-OI[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
V-19
Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99.
Reported result is estimated.
Analyte & Samples(s) Qualified:
2,4-Dinitrophenol
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
4-Chloroaniline
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
Aniline
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
Benzidine
18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI
MADEP-EPH-04-1.1
SPE cartridge contamination with non -petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-Feb 2018 Rev 2.1
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain -of -custody form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Director of Operations
Page 6 of 39

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087
Date Received: 11/1/2018
Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30
Sample ID: 18KO087-01
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0.11
0.026
mg/Kg dry
1 R-05
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Acrylonitrile
ND
0.0066
0.0027
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
tert-Amyl Methyl Ether (TAME)
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Benzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Bromobenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Bromochloromethane
ND
0.0022
0.0015
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Bromodichloromethane
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Bromoform
ND
0.0022
0.0015
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Bromomethane
ND
0.011
0.0046
mg/Kg dry
1
SW-846 8260B
11/5/18
1115118 15:57
MFF
2-Butanone (MEK)
ND
0.044
0.019
mg/Kg dry
1 R-05
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
tert-Butyl Alcohol (TBA)
ND
0.044
0.023
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
n-Butylbenzene
0.0019
0.0022
0.00077
mg/Kg dry
1 J
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
sec-Butylbenzene
0.0040
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
tert-Butylbenzene
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
0.0011
0.00066
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Carbon Disulfide
ND
0.0066
0.0047
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Carbon Tetrachloride
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Chlorobenzene
ND
0.0022
0.00077
mg/Kg dry
I
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Chlorodibromomethane
ND
0.0011
0.00077
mg/Kg dry
I
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Chloroethane
ND
0.022
0.0016
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Chloroform
ND
0.0044
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Chloromethane
ND
0.011
0.0070
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
2-Chlorotoluene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
4-Chlorotoluene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
1115118 15:57
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0022
0.0012
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,2-Dibromoethane (EDB)
ND
0.0011
0.0011
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Dibromomethane
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,2-Dichlorobenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,3-Dichlorobenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,4-Dichlorobenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
trans-1,4-Dichloro-2-butene
ND
0.0044
0.0023
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Dichlorodifluoromethane (Freon 12)
ND
0.022
0.0014
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,1-Dichloroethane
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,2-Dichloroethane
ND
0.0022
0.0014
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1, 1 -Dichloroethylene
ND
0.0044
0.0012
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
cis-1,2-Dichloroethylene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
trans-1,2-Dichloroethylene
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,2-Dichloropropane
ND
0.0022
0.0014
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,3-Dichloropropane
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
2,2-Dichloropropane
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1, 1 -Dichloropropene
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
cis-1,3-Dichloropropene
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
trans-1,3-Dichloropropene
ND
0.0011
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Diethyl Ether
ND
0.022
0.0020
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Page 7 of 39

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087
Date Received: 11/1/2018
Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30
Sample ID: 18KO087-01
Samnle Matrix: Soil
Volatile Organic Compounds by GC/MS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0.0011
0.00066
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,4-Dioxane
ND
0.11
0.063
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Ethylbenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Hexachlorobutadiene
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
2-Hexanone (MBK)
ND
0.022
0.012
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Isopropylbenzene (Cumene)
0.00077
0.0022
0.00077
mg/Kg dry
1
J
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
p-Isopropyltoluene (p-Cymene)
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
1115118 15:57
MFF
Methyl tert-Butyl Ether (MTBE)
ND
0.0044
0.00099
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Methylene Chloride
ND
0.022
0.0078
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
4-Methyl-2-pentanone (MIBK)
ND
0.022
0.0083
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Naphthalene
0.0081
0.0044
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
n-Propylbenzene
0.0012
0.0022
0.00077
mg/Kg dry
1
J
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Styrene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1, 1, 1,2-Tetrachloroethane
ND
0.0022
0.0020
mg/Kg dry
1
SW-8468260B
11/5/18
11/5/18 15:57
MFF
1,1,2,2-Tetrachloroethane
ND
0.0022
0.00099
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Tetrachloroethylene
ND
0.0022
0.0014
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Tetrahydrofuran
ND
0.011
0.0024
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Toluene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,2,3-Trichlorobenzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,2,4-Trichlorobenzene
ND
0.0022
0.00088
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,3,5-Trichlorobenzene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1, 1, 1 -Trichloroethane
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
11/5/18
1115118 15:57
MFF
1,1,2-Trichloroethane
ND
0.0022
0.0013
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Trichloroethylene
ND
0.0022
0.0011
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Trichlorofluoromethane (Freon 11)
ND
0.011
0.0012
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,2,3-Trichloropropane
ND
0.0022
0.0012
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
0.011
0.00099
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
(Freon 113)
1,2,4-Trimethylbenzene
0.0017
0.0022
0.00088
mg/Kg dry
1
J
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
1,3,5-Trimethylbenzene
ND
0.0022
0.00066
mg/Kg dry
1
SW-846 8260B
11/5/18
1115118 15:57
MFF
Vinyl Chloride
ND
0.011
0.0012
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
m+p Xylene
ND
0.0044
0.0019
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
o-Xylene
ND
0.0022
0.00077
mg/Kg dry
1
SW-846 8260B
11/5/18
11/5/18 15:57
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qaal
1,2-Dichloroethane-d4
102
70-130
11/5/18 15:57
Toluene-d8
95.8
70-130
11/5/18 15:57
4-Bromofluorobenzene
101
70-130
11/5/18 15:57
Page 8 of 39

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087
Date Received: 11/1/2018
Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30
Samnle ID: 18KO087-01
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0.48
0.14
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Acenaphthylene
ND
0.48
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Acetophenone
ND
0.95
0.19
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Aniline
ND
0.95
0.27
mg/Kg dry
1 V-05, V-34
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Anthracene
ND
0.48
0.14
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Benzidine
ND
1.8
1.2
mg/Kg dry
1 V-05, V-34
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Benzo(a)anthracene
ND
0.48
0.13
mg/Kg dry
I
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Benzo(a)pyrene
ND
0.48
0.15
mg/Kg dry
I
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Benzo(b)fluoranthene
ND
0.48
0.13
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Benzo(g,h,i)perylene
ND
0.48
0.21
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Benzo(k)fluoranthene
ND
0.48
0.15
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Benzoic Acid
ND
2.8
0.51
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Bis(2-chloroethoxy)methane
ND
0.95
0.18
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Bis(2-chloroethyl)ether
ND
0.95
0.19
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Bis(2-chloroisopropyl)ether
ND
0.95
0.20
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Bis(2-Ethylhexyl)phthalate
ND
0.95
0.37
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
4-Bromophenylphenylether
ND
0.95
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Butylbenzylphthalate
ND
0.95
0.23
mg/Kg dry
I
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Carbazole
ND
0.48
0.12
mg/Kg dry
I
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
4-Chloroaniline
ND
1.8
0.22
mg/Kg dry
1 V-05, V-34
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
4-Chloro-3-methylphenol
ND
1.8
0.20
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2-Chloronaphthalene
ND
0.95
0.18
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2-Chlorophenol
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
4-Chlorophenylphenylether
ND
0.95
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Chrysene
ND
0.48
0.15
mg/Kg dry
1 V-05
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Dibenz(a,h)anthracene
ND
0.48
0.29
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Dibenzofman
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Di-n-butylphthalate
ND
0.95
0.21
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
1,2-Dichlorobenzene
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
1,3-Dichlorobenzene
ND
0.95
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
1,4-Dichlorobenzene
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
3,3-Dichlorobenzidine
ND
0.48
0.15
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2,4-Dichlorophenol
ND
0.95
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Diethylphthalate
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2,4-Dimethylphenol
ND
0.95
0.18
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Dimethylphthalate
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
4,6-Dinitro-2-methylphenol
ND
0.95
0.90
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2,4-Dinitrophenol
ND
1.8
0.54
mg/Kg dry
1 V-19
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2,4-Dinitrotoluene
ND
0.95
0.15
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2,6-Dinitrotoluene
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Di-n-octylphthalate
ND
0.95
0.50
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.95
0.15
mg/Kg dry
I
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Fluoranthene
ND
0.48
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Flumene
ND
0.48
0.15
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Page 9 of 39

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087
Date Received: 11/1/2018
Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30
Samnle ID: 18KO087-01
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Hexachlorobutadiene
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Hexachlorocyclopentadiene
ND
0.95
0.20
mg/Kg dry
1
L-04, V-05
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Hexachloroethane
ND
0.95
0.19
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Indeno(1,2,3-cd)pyrene
ND
0.48
0.34
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Isophorone
ND
0.95
0.18
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
1-Methylnaphthalene
ND
0.48
0.18
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2-Methylnaphthalene
0.18
0.48
0.17
mg/Kg dry
1
J
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2-Methylphenol
ND
0.95
0.24
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
3/4-Methylphenol
ND
0.95
0.30
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Naphthalene
ND
0.48
0.24
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2-Nitroaniline
ND
0.95
0.16
mg/Kg dry
1
V-06
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
3-Nitroaniline
ND
0.95
0.14
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
4-Nitroaniline
ND
0.95
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Nitrobenzene
ND
0.95
0.18
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2-Nitrophenol
ND
0.95
0.25
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
4-Nitrophenol
ND
1.8
0.21
mg/Kg dry
1
V-06
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
N-Nitrosodimethylamine
ND
0.95
0.60
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
N-Nitrosodiphenylamine
ND
0.95
0.20
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
N-Nitrosodi-n-propylamine
ND
0.95
0.20
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Pentachloronitrobenzene
ND
0.95
0.23
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Pentachlorophenol
ND
0.95
0.23
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Phenanthrene
ND
0.48
0.25
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Phenol
ND
0.95
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Pyrene
ND
0.48
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Pyridine
ND
0.95
0.15
mg/Kg dry
1
V-05
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
1,2,4,5-Texachlorobenzene
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
1,2,4-Trichlorobenzene
ND
0.95
0.17
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2,4,5-Trichlorophenol
ND
0.95
0.22
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
2,4,6-Trichlorophenol
ND
0.95
0.16
mg/Kg dry
1
SW-846 8270D
11/3/18
11/6/18 15:39
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
58.0
30-130
11/6/18 15:39
Phenol-d6
62.9
30-130
11/6/18 15:39
Nitrobenzene-d5
62.8
30-130
11/6/18 15:39
2-Fluorobiphenyl
55.8
30-130
11/6/18 15:39
2,4,6-Tribromophenol
74.5
30-130
11/6/18 15:39
p-Terphenyl-dl4
56.3
30-130
11/6/18 15:39
Page 10 of 39

Table of Contents
40 icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087
Date Received: 11/1/2018
Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30
Samnle ID: 18KO087-01
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - EPH
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C9-C18 Aliphatics 130 14 mg/Kg dry 1 MADEP-EPH-04-1.1 11/4/18 11/7/18 1:08 RMW
C19-C36 Aliphatics 37 14 mg/Kg dry 1 MADEP-EPH-04-1.1 11/4/18 11/7/18 1:08 RMW
C11-C22 Aromatics 78 14 mg/Kg dry 1 MADEP-EPH-04-1.1 11/4/18 11/7/18 1:08 RMW
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD) 59.7 40-140 11/7/18 1:08
o-Terphenyl(OTP) 64.8 40-140 11/7/18 1:08
2-Bromonaphthalene 91.4 40-140 11/7/18 1:08
2-Fluorobiphenyl 107 40-140 11/7/18 1:08
Page 11 of 39

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087
Date Received: 11/1/2018
Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30
Sample ID: 18KO087-01
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses - VPH
Soil/Methanol Preservation Ratio: 1.19
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
C5-C8 Aliphatics
ND 16
mg/Kg dry 1
MADEP-VPH-Feb2018
11/6/18 11/7/18 17:07 EEH
Rev 2.1
C9-C12 Aliphatics
24 16
mg/Kg dry 1
MADEP-VPH-Feb 2018
11/6/18 11/7/18 17:07 EEH
Rev 2.1
C9-C10 Aromatics
31 16
mg/Kg dry 1
MADEP-VPH-Feb 2018
11/6/18 11/7/18 17:07 EEH
Rev 2.1
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2,5-Dibromotoluene(FID)
103
70-130
11/7/18 17:07
2,5-Dibromotoluene (PID)
116
70-130
11/7/18 17:07
Page 12 of 39

Table of Contents
icon-te w
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087
Date Received: 11/1/2018
Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30
Samnle ID: 18KO087-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 70.1 % Wt 1
SM 2540G 11/5/18 11/6/18 10:02 CJT
Page 13 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-MADEP-EPH-04-1.1
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18K0087-01 [TB-4-18]
B216348
20.0
2.00
11/04/18
Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18K0087-01[TB-4-18]
B216531
6.00
6.80
11/06/18
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
18K0087-01 [TB-4-18]
B216440
11/05/18
Prep Method: SW-846 5035-SW-846 8260B
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18K0087-01 [TB-4-18]
B216398
6.51
10.0
11/05/18
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18K0087-01 [TB-4-18]
B216342
15.3
1.00
11/03/18
Page 14 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216398 - SW-846 5035
Blank (B216398-BLK1)
Prepared & Analyzed: 11/05/18
Acetone
ND
0.10
mg/Kg wet R-05
Acrylonitrile
ND
0.0060
mg/Kg wet
tert-Amyl Methyl Ether (TAME)
ND
0.0010
mg/Kg wet
Benzene
ND
0.0020
mg/Kg wet
Bromobenzene
ND
0.0020
mg/Kg wet
Bromochloromethane
ND
0.0020
mg/Kg wet
Bromodichloromethane
ND
0.0020
mg/Kg wet
Bromoform
ND
0.0020
mg/Kg wet
Bromomethane
ND
0.010
mg/Kg wet
2-Butanone (MEK)
ND
0.040
mg/Kg wet R-05
tert-Butyl Alcohol (TBA)
ND
0.040
mg/Kg wet
n-Butylbenzene
ND
0.0020
mg/Kg wet
sec-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butylbenzene
ND
0.0020
mg/Kg wet
tert-Butyl Ethyl Ether (TBEE)
ND
0.0010
mg/Kg wet
Carbon Disulfide
ND
0.0060
mg/Kg wet
Carbon Tetrachloride
ND
0.0020
mg/Kg wet
Chlorobenzene
ND
0.0020
mg/Kg wet
Chlorodibromomethane
ND
0.0010
mg/Kg wet
Chloroethane
ND
0.020
mg/Kg wet
Chloroform
ND
0.0040
mg/Kg wet
Chloromethane
ND
0.010
mg/Kg wet
2-Chlorotoluene
ND
0.0020
mg/Kg wet
4-Chlorotoluene
ND
0.0020
mg/Kg wet
1,2-Dibromo-3-chloropropane (DBCP)
ND
0.0020
mg/Kg wet
1,2-Dibromoethane (EDB)
ND
0.0010
mg/Kg wet
Dibromomethane
ND
0.0020
mg/Kg wet
1,2-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,3-Dichlorobenzene
ND
0.0020
mg/Kg wet
1,4-Dichlorobenzene
ND
0.0020
mg/Kg wet
trans-1,4-Dichloro-2-butene
ND
0.0040
mg/Kg wet
Dichlorodifluoromethane (Freon 12)
ND
0.020
mg/Kg wet
1,1-Dichloroethane
ND
0.0020
mg/Kg wet
1,2-Dichloroethane
ND
0.0020
mg/Kg wet
1,1-Dichloroethylene
ND
0.0040
mg/Kg wet
cis-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
trans-1,2-Dichloroethylene
ND
0.0020
mg/Kg wet
1,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,3-Dichloropropane
ND
0.0010
mg/Kg wet
2,2-Dichloropropane
ND
0.0020
mg/Kg wet
1,1-Dichloropropene
ND
0.0020
mg/Kg wet
cis-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
trans-1,3-Dichloropropene
ND
0.0010
mg/Kg wet
Diethyl Ether
ND
0.020
mg/Kg wet
Diisopropyl Ether (RIPE)
ND
0.0010
mg/Kg wet
1,4-Dioxane
ND
0.10
mg/Kg wet
Ethylbenzene
ND
0.0020
mg/Kg wet
Hexachlorobutadiene
ND
0.0020
mg/Kg wet
2-Hexanone (MBK)
ND
0.020
mg/Kg wet
Isopropylbenzene (Cumene)
ND
0.0020
mg/Kg wet
p-Isopropyltoluene (p-Cymene)
ND
0.0020
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.0040
mg/Kg wet
Page 15 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
malyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216398 - SW-846 5035
Blank (B216398-BLK1)
Prepared & Analyzed: 11/05/18
Methylene Chloride
ND
0.020
mg/Kg wet
4-Methyl-2-pentanone (MIBK)
ND
0.020
mg/Kg wet
Naphthalene
ND
0.0040
mg/Kg wet
n-Propylbenzene
ND
0.0020
mg/Kg wet
Styrene
ND
0.0020
mg/Kg wet
1, 1, 1,2-Tetrachloroethane
ND
0.0020
mg/Kg wet
1,1,2,2-Tetrachloroethane
ND
0.0010
mg/Kg wet
Tetrachloroethylene
ND
0.0020
mg/Kg wet
Tetrahydrofuran
ND
0.010
mg/Kg wet
Toluene
ND
0.0020
mg/Kg wet
1,2,3-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.0020
mg/Kg wet
1,3,5-Trichlorobenzene
ND
0.0020
mg/Kg wet
1, 1, 1 -Trichloroethane
ND
0.0020
mg/Kg wet
1,1,2-Trichloroethane
ND
0.0020
mg/Kg wet
Trichloroethylene
ND
0.0020
mg/Kg wet
Trichlorofluoromethane (Freon 11)
ND
0.010
mg/Kg wet
1,2,3-Trichloropropane
ND
0.0020
mg/Kg wet
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0.010
mg/Kg wet
113)
1,2,4-Trimethylbenzene
ND
0.0020
mg/Kg wet
1,3,5-Trimethylbenzene
ND
0.0020
mg/Kg wet
Vinyl Chloride
ND
0.010
mg/Kg wet
m+p Xylene
ND
0.0040
mg/Kg wet
o-Xylene
ND
0.0020
mg/Kg wet
Surrogate: 1,2-Dichloroethane-d4
0.0522
mg/Kg wet
0.0500
104
70-130
Surrogate: Toluene-d8
0.0478
mg/Kg wet
0.0500
95.5
70-130
Surrogate:4-Bromofluorobenzene
0.0510
mg/Kg wet
0.0500
102
70-130
LCS (B216398-BS1)
Prepared & Analyzed: 11/05/18
Acetone
0.383
0.10
mg/Kg wet
0.200
191
* 70-160
R-05, L-07A t
Acrylonitrile
0.0194
0.0060
mg/Kg wet
0.0200
97.2
70-130
tert-Amyl Methyl Ether (TAME)
0.0205
0.0010
mg/Kg wet
0.0200
102
70-130
Benzene
0.0192
0.0020
mg/Kg wet
0.0200
95.8
70-130
Bromobenzene
0.0197
0.0020
mg/Kg wet
0.0200
98.5
70-130
Bromochloromethane
0.0221
0.0020
mg/Kg wet
0.0200
ill
70-130
Bromodichloromethane
0.0197
0.0020
mg/Kg wet
0.0200
98.7
70-130
Bromoform
0.0216
0.0020
mg/Kg wet
0.0200
108
70-130
Bromomethane
0.0120
0.010
mg/Kg wet
0.0200
60.1
40-130
t
2-Butanone (MEK)
0.308
0.040
mg/Kg wet
0.200
154
70-160
R-05 t
tert-Butyl Alcohol (TBA)
0.228
0.040
mg/Kg wet
0.200
114
40-130
t
n-Butylbenzene
0.0197
0.0020
mg/Kg wet
0,0200
98.5
70-130
sec-Butylbenzene
0.0196
0.0020
mg/Kg wet
0.0200
98.0
70-130
tert-Butylbenzene
0.0186
0.0020
mg/Kg wet
0.0200
92.9
70-160
t
tert-Butyl Ethyl Ether (TBEE)
0.0202
0.0010
mg/Kg wet
0,0200
101
70-130
Carbon Disulfide
0.0197
0.0060
mg/Kg wet
0.0200
98.3
70-130
Carbon Tetrachloride
0.0211
0.0020
mg/Kg wet
0.0200
105
70-130
Chlorobenzene
0.0203
0.0020
mg/Kg wet
0,0200
102
70-130
Chlorodibromomethane
0.0223
0.0010
mg/Kg wet
0.0200
Ill
70-130
Chloroethane
0.0175
0.020
mg/Kg wet
0.0200
87.7
70-130
.l
Chloroform
0.0200
0.0040
mg/Kg wet
0,0200
99.8
70-130
Chloromethane
0.0193
0.010
mg/Kg wet
0.0200
96.4
70-130
2-Chlorotoluene
0.0201
0.0020
mg/Kg wet
0.0200
101
70-130
Page 16 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216398 - SW-846 5035
LCS (B216398-BSI) Prepared & Analyzed: 11/05/18
4-Chlorotoluene
0.0206
0.0020
mg/Kg wet
0.0200
103
70-130
1,2-Dibromo-3-chloropropane (DBCP)
0.0252
0.0020
mg/Kg wet
0.0200
126
70-130
1,2-Dibromoethane (EDB)
0.0215
0.0010
mg/Kg wet
0.0200
107
70-130
Dibromomethane
0.0206
0.0020
mg/Kg wet
0.0200
103
70-130
1,2-Dichlorobenzene
0.0211
0.0020
mg/Kg wet
0.0200
106
70-130
1,3-Dichlorobenzene
0.0205
0.0020
mg/Kg wet
0.0200
103
70-130
1,4-Dichlorobenzene
0.0198
0.0020
mg/Kg wet
0.0200
99.1
70-130
trans-1,4-Dichloro-2-butene
0.0211
0.0040
mg/Kg wet
0.0200
105
70-130
Dichlorodifluoromethane(Freon 12)
0.0175
0.020
mg/Kg wet
0.0200
87.5
40-160
1,1-Dichloroethane
0.0200
0.0020
mg/Kg wet
0.0200
100
70-130
1,2-Dichloroethane
0.0210
0.0020
mg/Kg wet
0.0200
105
70-130
1,1-Dichloroethylene
0.0201
0.0040
mg/Kg wet
0.0200
101
70-130
cis-1,2-Dichloroethylene
0.0195
0.0020
mg/Kg wet
0.0200
97.5
70-130
trans-1,2-Dichloroethylene
0.0200
0.0020
mg/Kg wet
0.0200
100
70-130
1,2-Dichloropropane
0.0188
0.0020
mg/Kg wet
0.0200
94.2
70-130
1,3-Dichloropropane
0.0211
0.0010
mg/Kg wet
0.0200
105
70-130
2,2-Dichloropropane
0.0192
0.0020
mg/Kg wet
0.0200
95.9
70-130
1,1-Dichloropropene
0.0201
0.0020
mg/Kg wet
0.0200
101
70-130
cis-1,3-Dichloropropene
0.0204
0.0010
mg/Kg wet
0.0200
102
70-130
trans-1,3-Dichloropropene
0.0212
0.0010
mg/Kg wet
0.0200
106
70-130
Diethyl Ether
0.0201
0.020
mg/Kg wet
0.0200
100
70-130
Diisopropyl Ether (RIPE)
0.0201
0.0010
mg/Kg wet
0.0200
101
70-130
1,4-Dioxane
0.212
0.10
mg/Kg wet
0.200
106
40-160
Ethylbenzene
0.0194
0.0020
mg/Kg wet
0.0200
96.8
70-130
Hexachlorobutadiene
0.0210
0.0020
mg/Kg wet
0.0200
105
70-160
2-Hexanone (MBK)
0.265
0.020
mg/Kg wet
0.200
132
70-160
Isopropylbenzene (Cumene)
0.0195
0.0020
mg/Kg wet
0.0200
97.5
70-130
p-Isopropyltoluene (p-Cymene)
0.0186
0.0020
mg/Kg wet
0.0200
93.1
70-130
Methyl tert-Butyl Ether (MTBE)
0.0212
0.0040
mg/Kg wet
0.0200
106
70-130
Methylene Chloride
0.0212
0.020
mg/Kg wet
0.0200
106
40-160
4-Methyl-2-pentanone (MIBK)
0.225
0.020
mg/Kg wet
0.200
113
70-160
Naphthalene
0.0209
0.0040
mg/Kg wet
0.0200
104
40-130
n-Propylbenzene
0.0201
0.0020
mg/Kg wet
0.0200
101
70-130
Styrene
0.0201
0.0020
mg/Kg wet
0.0200
101
70-130
1, 1, 1,2-Tetrachloroethane
0.0203
0.0020
mg/Kg wet
0.0200
102
70-130
1,1,2,2-Tetrachloroethane
0.0218
0.0010
mg/Kg wet
0.0200
109
70-130
Tetrachloroethylene
0.0205
0.0020
mg/Kg wet
0.0200
103
70-130
Tetrahydrofuran
0.0198
0.010
mg/Kg wet
0.0200
98.8
70-130
Toluene
0.0184
0.0020
mg/Kg wet
0.0200
92.1
70-130
1,2,3-Trichlorobenzene
0.0220
0.0020
mg/Kg wet
0.0200
110
70-130
1,2,4-Trichlorobenzene
0.0233
0.0020
mg/Kg wet
0.0200
116
70-130
1,3,5-Trichlorobenzene
0.0226
0.0020
mg/Kg wet
0.0200
113
70-130
1, 1, 1 -Trichloroethane
0.0193
0.0020
mg/Kg wet
0.0200
96.7
70-130
1,1,2-Trichloroethane
0.0201
0.0020
mg/Kg wet
0.0200
100
70-130
Trichloroethylene
0.0197
0.0020
mg/Kg wet
0.0200
98.3
70-130
Trichlorofluoromethane (Freon 11)
0.0179
0.010
mg/Kg wet
0.0200
89.3
70-130
1,2,3-Trichloropropane
0.0222
0.0020
mg/Kg wet
0.0200
ill
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0194
0.010
mg/Kg wet
0.0200
97.0
70-130
113)
1,2,4-Trimethylbenzene
0.0188
0.0020
mg/Kg wet
0.0200
93.9
70-130
1,3,5-Trimethylbenzene
0.0199
0.0020
mg/Kg wet
0.0200
99.3
70-130
Vinyl Chloride
0.0179
0.010
mg/Kg wet
0,0200
89.3
40-130
J f
t
t
f
t
t
Page 17 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216398 - SW-846 5035
LCS (B216398-BSI)
Prepared & Analyzed: 11/05/18
m+p Xylene
0.0387
0.0040
mg/Kg wet
0.0400
96.6
70-130
o-Xylene
0.0192
0.0020
mg/Kg wet
0.0200
96.0
70-130
Surrogate:l,2-Dichloroethane-d4
0.0530
mg/Kg wet
0.0500
106
70-130
Surrogate: Toluene-d8
0.0482
mg/Kg wet
0.0500
96.5
70-130
Surrogate:4-Bromofluorobenzene
0.0506
mg/Kg wet
0.0500
101
70-130
LCS Dup (B216398-BSDI)
Prepared & Analyzed: 11/05/18
Acetone
0.245
0.10
mg/Kg wet
0.200
123
70-160
43.8 *
25
R-05 t
Acrylonitrile
0.0185
0.0060
mg/Kg wet
0.0200
92.4
70-130
5.06
25
tert-Amyl Methyl Ether (TAME)
0.0193
0.0010
mg/Kg wet
0.0200
96.4
70-130
6.04
25
Benzene
0.0186
0.0020
mg/Kg wet
0.0200
92.9
70-130
3.07
25
Bromobenzene
0.0179
0.0020
mg/Kg wet
0.0200
89.3
70-130
9.80
25
Bromochloromethane
0.0222
0.0020
mg/Kg wet
0.0200
111
70-130
0.361
25
Bromodichloromethane
0.0187
0.0020
mg/Kg wet
0.0200
93.6
70-130
5.30
25
Bromoform
0.0201
0.0020
mg/Kg wet
0.0200
101
70-130
7.09
25
Bromomethane
0.0139
0.010
mg/Kg wet
0.0200
69.7
40-130
14.8
25
f
2-Butanone (MEK)
0.225
0.040
mg/Kg wet
0.200
113
70-160
31.1 *
25
R-05 t
tert-Butyl Alcohol (TBA)
0.198
0.040
mg/Kg wet
0.200
99.0
40-130
13.9
25
t
n-Butylbenzene
0.0190
0.0020
mg/Kg wet
0.0200
94.8
70-130
3.83
25
sec-Butylbenzene
0.0194
0.0020
mg/Kg wet
0.0200
97.1
70-130
0.923
25
tert-Butylbenzene
0.0182
0.0020
mg/Kg wet
0.0200
90.8
70-160
2.29
25
t
tert-Butyl Ethyl Ether (TBEE)
0.0195
0.0010
mg/Kg wet
0.0200
97.3
70-130
3.93
25
Carbon Disulfide
0.0195
0.0060
mg/Kg wet
0.0200
97.5
70-130
0.817
25
Carbon Tetrachloride
0.0192
0.0020
mg/Kg wet
0.0200
95.9
70-130
9.34
25
Chlorobenzene
0.0198
0.0020
mg/Kg wet
0.0200
99.2
70-130
2.49
25
Chlorodibromomethane
0.0217
0.0010
mg/Kg wet
0.0200
109
70-130
2.45
25
Chloroethane
0.0177
0.020
mg/Kg wet
0.0200
88.6
70-130
1.02
25
J
Chloroform
0.0197
0.0040
mg/Kg wet
0.0200
98.3
70-130
1.51
25
Chloromethane
0.0186
0.010
mg/Kg wet
0.0200
93.2
70-130
3.38
25
2-Chlorotoluene
0.0193
0.0020
mg/Kg wet
0.0200
96.7
70-130
4.05
25
4-Chlorotoluene
0.0193
0.0020
mg/Kg wet
0.0200
96.7
70-130
6.21
25
1,2-Dibromo-3-chloropropane (DBCP)
0.0218
0.0020
mg/Kg wet
0.0200
109
70-130
14.2
25
1,2-Dibromoethane (EDB)
0.0214
0.0010
mg/Kg wet
0.0200
107
70-130
0.187
25
Dibromomethane
0.0202
0.0020
mg/Kg wet
0.0200
101
70-130
1.76
25
1,2-Dichlorobenzene
0.0202
0.0020
mg/Kg wet
0.0200
101
70-130
4.35
25
1,3-Dichlorobenzene
0.0196
0.0020
mg/Kg wet
0.0200
98.2
70-130
4.38
25
1,4-Dichlorobenzene
0.0185
0.0020
mg/Kg wet
0.0200
92.4
70-130
7.00
25
trans-1,4-Dichloro-2-butene
0.0193
0.0040
mg/Kg wet
0.0200
96.3
70-130
9.02
25
Dichlorodifluoromethane(Freon 12)
0.0187
0.020
mg/Kg wet
0.0200
93.4
40-160
6.52
25
J t
1, 1 -Dichloroethane
0.0203
0.0020
mg/Kg wet
0.0200
101
70-130
1.39
25
1,2-Dichloroethane
0.0203
0.0020
mg/Kg wet
0.0200
102
70-130
3.48
25
1,1-Dichloroethylene
0.0190
0.0040
mg/Kg wet
0.0200
94.9
70-130
5.83
25
cis-1,2-Dichloroethylene
0.0188
0.0020
mg/Kg wet
0.0200
94.0
70-130
3.66
25
trans-1,2-Dichloroethylene
0.0195
0.0020
mg/Kg wet
0.0200
97.5
70-130
2.73
25
1,2-Dichloropropane
0.0197
0.0020
mg/Kg wet
0.0200
98.3
70-130
4.26
25
1,3-Dichloropropane
0.0203
0.0010
mg/Kg wet
0.0200
102
70-130
3.68
25
2,2-Dichloropropane
0.0189
0.0020
mg/Kg wet
0.0200
94.6
70-130
1.36
25
1,1-Dichloropropene
0.0187
0.0020
mg/Kg wet
0.0200
93.3
70-130
7.53
25
cis-1,3-Dichloropropene
0.0202
0.0010
mg/Kg wet
0.0200
101
70-130
0.888
25
trans-1,3-Dichloropropene
0.0200
0.0010
mg/Kg wet
0.0200
99.8
70-130
5.84
25
Diethyl Ether
0.0201
0.020
mg/Kg wet
0.0200
100
70-130
0.00
25
Diisopropyl Ether (DIPE)
0.0199
0.0010
mg/Kg wet
0.0200
99.4
70-130
1.30
25
Page 18 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216398 - SW-846 5035
LCS Dup (B216398-BSD1)
Prepared & Analyzed: 11/05/18
1,4-Dioxane
0.208
0.10
mg/Kg wet
0.200
104
40-160
1.85
50
f #
Ethylbenzene
0.0182
0.0020
mg/Kg wet
0.0200
90.8
70-130
6.40
25
Hexachlorobutadiene
0.0204
0.0020
mg/Kg wet
0.0200
102
70-160
3.19
25
2-Hexanone (MBK)
0.219
0.020
mg/Kg wet
0.200
110
70-160
18.9
25
f
Isopropylbenzene (Cumene)
0.0190
0.0020
mg/Kg wet
0.0200
94.8
70-130
2.81
25
p-Isopropyltoluene (p-Cymene)
0.0184
0.0020
mg/Kg wet
0.0200
91.9
70-130
1.30
25
Methyl tert-Butyl Ether (MTBE)
0.0207
0.0040
mg/Kg wet
0.0200
104
70-130
2.58
25
Methylene Chloride
0.0204
0.020
mg/Kg wet
0.0200
102
40-160
4.13
25
t
4-Methyl-2-pentanone (MIBK)
0.213
0.020
mg/Kg wet
0.200
107
70-160
5.43
25
t
Naphthalene
0.0200
0.0040
mg/Kg wet
0.0200
99.9
40-130
4.50
25
f
n-Propylbenzene
0.0193
0.0020
mg/Kg wet
0.0200
96.3
70-130
4.47
25
Styrene
0.0181
0.0020
mg/Kg wet
0.0200
90.4
70-130
10.7
25
1, 1, 1,2-Tetrachloroethane
0.0192
0.0020
mg/Kgwet
0.0200
96.0
70-130
5.67
25
1,1,2,2-Tetrachloroethane
0.0198
0.0010
mg/Kg wet
0.0200
99.1
70-130
9.61
25
Tetrachloroethylene
0.0199
0.0020
mg/Kg wet
0.0200
99.7
70-130
2.87
25
Tetrahydrofuran
0.0199
0.010
mg/Kg wet
0.0200
99.5
70-130
0.706
25
Toluene
0.0182
0.0020
mg/Kg wet
0.0200
90.8
70-130
1.42
25
1,2,3-Trichlorobenzene
0.0198
0.0020
mg/Kg wet
0.0200
99.2
70-130
10.1
25
1,2,4-Trichlorobenzene
0.0221
0.0020
mg/Kg wet
0.0200
110
70-130
5.21
25
1,3,5-Trichlorobenzene
0.0201
0.0020
mg/Kg wet
0.0200
100
70-130
11.7
25
1, 1, 1 -Trichloroethane
0.0194
0.0020
mg/Kg wet
0.0200
97.0
70-130
0.310
25
1,1,2-Trichloroethane
0.0196
0.0020
mg/Kg wet
0.0200
98.2
70-130
2.32
25
Trichloroethylene
0.0191
0.0020
mg/Kg wet
0.0200
95.6
70-130
2.78
25
Trichlorofluoromethane (Freon 11)
0.0182
0.010
mg/Kg wet
0.0200
90.8
70-130
1.67
25
1,2,3-Trichloropropane
0.0207
0.0020
mg/Kgwet
0.0200
103
70-130
7.18
25
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
0.0187
0.010
mg/Kg wet
0.0200
93.4
70-130
3.78
25
113)
1,2,4-Trimethylbenzene
0.0178
0.0020
mg/Kg wet
0.0200
88.9
70-130
5.47
25
1,3,5-Trimethylbenzene
0.0187
0.0020
mg/Kg wet
0.0200
93.5
70-130
6.02
25
Vinyl Chloride
0.0184
0.010
mg/Kg wet
0.0200
91.8
40-130
2.76
25
t
m+p Xylene
0.0363
0.0040
mg/Kg wet
0.0400
90.8
70-130
6.19
25
o-Xylene
0.0188
0.0020
mg/Kg wet
0.0200
94.0
70-130
2.11
25
Surrogate:l,2-Dichloroethane-d4
0.0521
mg/Kg wet
0.0500
104
70-130
Surrogate: Toluene-d8
0.0492
mg/Kg wet
0.0500
98.4
70-130
Surrogate:4-Bromofluorobenzene
0.0500
mg/Kg wet
0.0500
100
70-130
Page 19 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216342 - SW-846 3546
Blank (B216342-BLK1) Prepared: 11/03/18 Analyzed: 11/05/18
Acenaphthene
ND
0.17
mg/Kg wet
Acenaphthylene
ND
0.17
mg/Kg wet
Acetophenone
ND
0.34
mg/Kg wet
Aniline
ND
0.34
mg/Kg wet
Anthracene
ND
0.17
mg/Kg wet
Benzidine
ND
0.66
mg/Kg wet
Benzo(a)anthracene
ND
0.17
mg/Kg wet
Benzo(a)pyrene
ND
0.17
mg/Kg wet
Benzo(b)fluoranthene
ND
0.17
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.17
mg/Kg wet
Benzo(b)fluoranthene
ND
0.17
mg/Kg wet
Benzoic Acid
ND
1.0
mg/Kg wet
Bis(2-chloroethoxy)methane
ND
0.34
mg/Kg wet
Bis(2-chloroethyl)ether
ND
0.34
mg/Kg wet
Bis(2-chloroisopropyl)ether
ND
0.34
mg/Kg wet
Bis(2-Ethylhexyl)phthalate
ND
0.34
mg/Kg wet
4-Bromophenylphenylether
ND
0.34
mg/Kg wet
Butylbenzylphthalate
ND
0.34
mg/Kg wet
Carbazole
ND
0.17
mg/Kg wet
4-Chloroaniline
ND
0.66
mg/Kg wet
4-Chloro-3-methylphenol
ND
0.66
mg/Kg wet
2-Chloronaphthalene
ND
0.34
mg/Kg wet
2-Chlorophenol
ND
0.34
mg/Kg wet
4-Chlorophenylphenylether
ND
0.34
mg/Kg wet
Chrysene
ND
0.17
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.17
mg/Kg wet
Dibenzofuran
ND
0.34
mg/Kg wet
Di-n-butylphthalate
ND
0.34
mg/Kg wet
1,2-Dichlorobenzene
ND
0.34
mg/Kg wet
1,3-Dichlorobenzene
ND
0.34
mg/Kg wet
1,4-Dichlorobenzene
ND
0.34
mg/Kg wet
3,3-Dichlorobenzidine
ND
0.17
mg/Kg wet
2,4-Dichlorophenol
ND
0.34
mg/Kg wet
Diethylphthalate
ND
0.34
mg/Kg wet
2,4-Dimethylphenol
ND
0.34
mg/Kg wet
Dimethylphthalate
ND
0.34
mg/Kg wet
4,6-Dinitro-2-methylphenol
ND
0.34
mg/Kg wet
2,4-Dinitrophenol
ND
0.66
mg/Kg wet
2,4-Dinitrotoluene
ND
0.34
mg/Kg wet
2,6-Dinitrotoluene
ND
0.34
mg/Kg wet
Di-n-octylphthalate
ND
0.34
mg/Kg wet
1,2-Diphenylhydrazine (as Azobenzene)
ND
0.34
mg/Kg wet
Fluoranthene
ND
0.17
mg/Kg wet
Fluorene
ND
0.17
mg/Kg wet
Hexachlorobenzene
ND
0.34
mg/Kg wet
Hexachlorobutadiene
ND
0.34
mg/Kg wet
Hexachlorocyclopentadiene
ND
0.34
mg/Kg wet
Hexachloroethane
ND
0.34
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.17
mg/Kg wet
Isophorone
ND
0.34
mg/Kg wet
1-Methylnaphthalene
ND
0.17
mg/Kg wet
2-Methylnaphthalene
ND
0.17
mg/Kg wet
V-05, V-34
V-05, V-34
V-34
V-19
L-04, V-05
Page 20 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216342 - SW-846 3546
Blank (B216342-BLK1)
Prepared: 11/03/18 Analyzed: 11/05/18
2-Methylphenol
ND
0.34
mg/Kg wet
3/4-Methylphenol
ND
0.34
mg/Kg wet
Naphthalene
ND
0.17
mg/Kg wet
2-Nitroaniline
ND
0.34
mg/Kg wet
V-06
3-Nitroaniline
ND
0.34
mg/Kg wet
4-Nitroaniline
ND
0.34
mg/Kg wet
Nitrobenzene
ND
0.34
mg/Kg wet
2-Nitrophenol
ND
0.34
mg/Kg wet
4-Nitrophenol
ND
0.66
mg/Kg wet
V-06
N-Nitrosodimethylamine
ND
0.34
mg/Kg wet
N-Nitrosodiphenylamine
ND
0.34
mg/Kg wet
N-Nitrosodi-n-propylamine
ND
0.34
mg/Kg wet
Pentachloronitrobenzene
ND
0.34
mg/Kg wet
Pentachlorophenol
ND
0.34
mg/Kg wet
Phenanthrene
ND
0.17
mg/Kg wet
Phenol
ND
0.34
mg/Kg wet
Pyrene
ND
0.17
mg/Kg wet
Pyridine
ND
0.34
mg/Kg wet
V-05
1,2,4,5-Tetrachlorobenzene
ND
0.34
mg/Kg wet
1,2,4-Trichlorobenzene
ND
0.34
mg/Kg wet
2,4,5-Trichlorophenol
ND
0.34
mg/Kg wet
2,4,6-Trichlorophenol
ND
0.34
mg/Kg wet
Surrogate:2-Fluorophenol
3.75
mg/Kg wet
6.67
56.2
30-130
Surrogate: Phenol-d6
4.24
mg/Kg wet
6.67
63.6
30-130
Surrogate: Nitrobenzene-d5
2.13
mg/Kg wet
3.33
64.0
30-130
Surrogate:2-Fluorobiphenyl
1.77
mg/Kg wet
3.33
53.1
30-130
Surrogate: 2,4,6-Tribromophenol
4.84
mg/Kg wet
6.67
72.5
30-130
Surrogate: p-Terphenyl-dl4
2.21
mg/Kg wet
3.33
66.4
30-130
LCS (B216342-BS1)
Prepared: 11/03/18 Analyzed: 11/05/18
Acenaphthene
0.927
0.17
mg/Kg wet
1.67
55.6
40-140
Acenaphthylene
1.01
0.17
mg/Kg wet
1.67
60.8
40-140
Acetophenone
0.955
0.34
mg/Kg wet
1.67
57.3
40-140
Aniline
0.649
0.34
mg/Kg wet
1.67
38.9
10-140
V-05, V-34 f
Anthracene
0.969
0.17
mg/Kg wet
1.67
58.1
40-140
Benzidine
0.766
0.66
mg/Kg wet
1.67
45.9
40-140
V-05,V-34
Benzo(a)anthracene
1.01
0.17
mg/Kg wet
1.67
60.5
40-140
Benzo(a)pyrene
1.11
0.17
mg/Kg wet
1.67
66.8
40-140
Benzo(b)fluoranthene
1.05
0.17
mg/Kg wet
1.67
62.9
40-140
Benzo(g,h,i)perylene
1.28
0.17
mg/Kg wet
1.67
76.8
40-140
Benzo(k)fluoranthene
1.05
0.17
mg/Kg wet
1.67
63.1
40-140
Benzoic Acid
1.12
1.0
mg/Kg wet
1.67
67.4
30-130
Bis(2-chloroethoxy)methane
1.03
0.34
mg/Kg wet
1.67
61.7
40-140
Bis(2-chloroethyl)ether
1.01
0.34
mg/Kg wet
1.67
60.7
40-140
Bis(2-chloroisopropyl)ether
1.19
0.34
mg/Kg wet
1.67
71.4
40-140
Bis(2-Ethylhexyl)phthalate
1.14
0.34
mg/Kg wet
1.67
68.3
40-140
4-Bromophenylphenylether
1.04
0.34
mg/Kg wet
1.67
62.4
40-140
Butylbenzylphthalate
1.09
0.34
mg/Kg wet
1.67
65.6
40-140
Carbazole
0.920
0.17
mg/Kg wet
1.67
55.2
40-140
4-Chloroaniline
0.655
0.66
mg/Kg wet
1.67
39.3
10-140
V-34, J t
4-Chloro-3-methylphenol
1.08
0.66
mg/Kg wet
1.67
64.6
30-130
2-Chloronaphthalene
0.859
0.34
mg/Kg wet
1.67
51.6
40-140
Page 21 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
\nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216342 - SW-846 3546
LCS (B216342-BS1)
Prepared: 11/03/18 Analyzed: 11/05/18
2-Chlorophenol
0.904
0.34
mg/Kg wet
1.67
54.2
30-130
4-Chlorophenylphenylether
1.08
0.34
mg/Kg wet
1.67
64.8
40-140
Chrysene
0.947
0.17
mg/Kg wet
1.67
56.8
40-140
Dibenz(a,h)anthracene
1.27
0.17
mg/Kg wet
1.67
76.3
40-140
Dibenzofuran
1.07
0.34
mg/Kg wet
1.67
64.1
40-140
Di-n-butylphthalate
1.02
0.34
mg/Kg wet
1.67
61.2
40-140
1,2-Dichlorobenzene
0.829
0.34
mg/Kg wet
1.67
49.8
40-140
1,3-Dichlorobenzene
0.780
0.34
mg/Kg wet
1.67
46.8
40-140
1,4-Dichlorobenzene
0.806
0.34
mg/Kg wet
1.67
48.3
40-140
3,3-Dichlorobenzidine
0.930
0.17
mg/Kg wet
1.67
55.8
20-140
t
2,4-Dichlorophenol
0.975
0.34
mg/Kg wet
1.67
58.5
30-130
Diethylphthalate
1.09
0.34
mg/Kg wet
1.67
65.3
40-140
2,4-Dimethylphenol
0.876
0.34
mg/Kg wet
1.67
52.6
30-130
Dimethylphthalate
1.08
0.34
mg/Kg wet
1.67
65.1
40-140
4,6-Dinitro-2-methylphenol
0.957
0.34
mg/Kg wet
1.67
57.4
30-130
2,4-Dinitrophenol
0.813
0.66
mg/Kg wet
1.67
48.8
30-130
V-19
2,4-Dinitrotoluene
1.12
0.34
mg/Kg wet
1.67
67.4
40-140
2,6-Dinitrotoluene
1.19
0.34
mg/Kg wet
1.67
71.2
40-140
Di-n-octylphthalate
1.27
0.34
mg/Kg wet
1.67
76.0
40-140
1,2-Diphenylhydrazine (as Azobenzene)
1.08
0.34
mg/Kg wet
1.67
64.5
40-140
Fluoranthene
0.964
0.17
mg/Kg wet
1.67
57.8
40-140
Fluorene
1.03
0.17
mg/Kg wet
1.67
61.6
40-140
Hexachlorobenzene
1.02
0.34
mg/Kg wet
1.67
61.4
40-140
Hexachlorobutadiene
0.880
0.34
mg/Kg wet
1.67
52.8
40-140
Hexachlorocyclopentadiene
0.554
0.34
mg/Kg wet
1.67
33.2 *
40-140
L-04, V-05
Hexachloroethane
0.833
0.34
mg/Kg wet
1.67
50.0
40-140
Indeno(1,2,3-cd)pyrene
1.36
0.17
mg/Kg wet
1.67
81.8
40-140
Isophorone
1.00
0.34
mg/Kg wet
1.67
60.2
40-140
1-Methylnaphthalene
0.874
0.17
mg/Kg wet
1.67
52.4
40-140
2-Methylnaphthalene
0.957
0.17
mg/Kg wet
1.67
57.4
40-140
2-Methylphenol
0.981
0.34
mg/Kg wet
1.67
58.9
30-130
3/4-Methylphenol
1.03
0.34
mg/Kg wet
1.67
61.6
30-130
Naphthalene
0.891
0.17
mg/Kg wet
1.67
53.5
40-140
2-Nitroaniline
1.23
0.34
mg/Kg wet
1.67
74.1
40-140
V-06
3-Nitroaniline
0.978
0.34
mg/Kg wet
1.67
58.7
30-140
t
4-Nitroaniline
1.06
0.34
mg/Kg wet
1.67
63.7
40-140
Nitrobenzene
0.979
0.34
mg/Kg wet
1.67
58.8
40-140
2-Nitrophenol
0.967
0.34
mg/Kg wet
1.67
58.0
30-130
4-Nitrophenol
1.32
0.66
mg/Kg wet
1.67
78.9
30-130
V-06
N-Nitrosodimethylamine
1.06
0.34
mg/Kg wet
1.67
63.4
40-140
N-Nitrosodiphenylamine
1.15
0.34
mg/Kg wet
1.67
68.8
40-140
N-Nitrosodi-n-propylamine
0.982
0.34
mg/Kg wet
1.67
58.9
40-140
Pentachloronitrobenzene
1.05
0.34
mg/Kg wet
1.67
63.0
40-140
Pentachlorophenol
0.671
0.34
mg/Kg wet
1.67
40.3
30-130
Phenanthrene
0.963
0.17
mg/Kg wet
1.67
57.8
40-140
Phenol
0.962
0.34
mg/Kg wet
1.67
57.7
30-130
Pyrene
1.06
0.17
mg/Kg wet
1.67
63.7
40-140
Pyridine
0.512
0.34
mg/Kg wet
1.67
30.7
30-140
V-05
1,2,4,5-Tetrachlorobenzene
0.984
0.34
mg/Kg wet
1.67
59.1
40-140
1,2,4-Trichlorobenzene
0.854
0.34
mg/Kg wet
1.67
51.3
40-140
2,4,5-Trichlorophenol
1.07
0.34
mg/Kg wet
1.67
64.0
30-130
2,4,6-Trichlorophenol
1.04
0.34
mg/Kg wet
1.67
62.7
30-130
Page 22 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216342 - SW-846 3546
LCS (B216342-BS1)
Prepared: 11/03/18 Analyzed: 11/05/18
Surrogate:2-Fluorophenol
3.68
mg/Kg wet
6.67
55.2
30-130
Surrogate: Phenol-d6
4.18
mg/Kg wet
6.67
62.6
30-130
Surrogate: Nitrobenzene-d5
2.12
mg/Kg wet
3.33
63.5
30-130
Surrogate:2-Fluorobiphenyl
1.79
mg/Kg wet
3.33
53.6
30-130
Surrogate: 2,4,6-Tribromophenol
5.32
mg/Kg wet
6.67
79.7
30-130
Surrogate:p-Terphenyl-dl4
2.23
mg/Kg wet
3.33
66.8
30-130
LCS Dup (B216342-BSD1)
Prepared: 11/03/18 Analyzed: 11/05/18
Acenaphthene
1.07
0.17
mg/Kg wet
1.67
63.9
40-140
13.9
30
Acenaphthylene
1.14
0.17
mg/Kg wet
1.67
68.2
40-140
11.4
30
Acetophenone
0.994
0.34
mg/Kg wet
1.67
59.6
40-140
4.00
30
Aniline
0.689
0.34
mg/Kg wet
1.67
41.4
10-140
6.03
50
V-05,V-34 f #
Anthracene
1.07
0.17
mg/Kg wet
1.67
64.1
40-140
9.81
30
Benzidine
0.891
0.66
mg/Kg wet
1.67
53.4
40-140
15.1
30
V-05,V-34
Benzo(a)anthracene
1.11
0.17
mg/Kg wet
1.67
66.7
40-140
9.87
30
Benzo(a)pyrene
1.25
0.17
mg/Kg wet
1.67
74.9
40-140
11.5
30
Benzo(b)fluoranthene
1.16
0.17
mg/Kg wet
1.67
69.8
40-140
10.3
30
Benzo(g,h,i)perylene
1.42
0.17
mg/Kg wet
1.67
85.1
40-140
10.2
30
Benzo(k)fluoranthene
1.15
0.17
mg/Kg wet
1.67
69.3
40-140
9.28
30
Benzoic Acid
1.18
1.0
mg/Kg wet
1.67
70.6
30-130
4.63
50
$
Bis(2-chloroethoxy)methane
1.13
0.34
mg/Kg wet
1.67
67.7
40-140
9.18
30
Bis(2-chloroethyl)ether
1.01
0.34
mg/Kg wet
1.67
60.7
40-140
0.0329
30
Bis(2-chloroisopropyl)ether
1.18
0.34
mg/Kg wet
1.67
70.8
40-140
0.844
30
Bis(2-Ethylhexyl)phthalate
1.26
0.34
mg/Kg wet
1.67
75.8
40-140
10.4
30
4-Bromophenylphenylether
1.05
0.34
mg/Kg wet
1.67
62.9
40-140
0.766
30
Butylbenzylphthalate
1.26
0.34
mg/Kg wet
1.67
75.7
40-140
14.4
30
Carbazole
1.02
0.17
mg/Kg wet
1.67
61.4
40-140
10.7
30
4-Chloroaniline
0.694
0.66
mg/Kg wet
1.67
41.7
10-140
5.78
30
V-34 t
4-Chloro-3-methylphenol
1.21
0.66
mg/Kg wet
1.67
72.5
30-130
11.5
30
2-Chloronaphthalene
0.971
0.34
mg/Kg wet
1.67
58.3
40-140
12.2
30
2-Chorophenol
0.932
0.34
mg/Kg wet
1.67
55.9
30-130
3.05
30
4-Chlorophenylphenylether
1.21
0.34
mg/Kg wet
1.67
72.8
40-140
11.5
30
Chrysene
1.03
0.17
mg/Kg wet
1.67
61.8
40-140
8.40
30
Dibenz(a,h)anthracene
1.41
0.17
mg/Kg wet
1.67
84.8
40-140
10.6
30
Dibenzofuran
1.17
0.34
mg/Kg wet
1.67
70.4
40-140
9.37
30
Di-n-butylphthalate
1.11
0.34
mg/Kg wet
1.67
66.4
40-140
8.12
30
1,2-Dichlorobenzene
0.809
0.34
mg/Kg wet
1.67
48.6
40-140
2.44
30
1,3-Dichlorobenzene
0.750
0.34
mg/Kg wet
1.67
45.0
40-140
3.97
30
1,4-Dichlorobenzene
0.740
0.34
mg/Kg wet
1.67
45.0
40-140
7.20
30
3,3-Dichlorobenzidine
1.00
0.17
mg/Kg wet
1.67
60.2
20-140
7.66
50
t #
2,4-Dichlorophenol
1.08
0.34
mg/Kg wet
1.67
64.6
30-130
9.98
30
Diethylphthalate
1.23
0.34
mg/Kg wet
1.67
73.9
40-140
12.3
30
2,4-Dimethylphenol
0.967
0.34
mg/Kg wet
1.67
58.0
30-130
9.91
30
Dimethylphthalate
1.23
0.34
mg/Kg wet
1.67
73.8
40-140
12.5
30
4,6-Dinitro-2-methylphenol
1.08
0.34
mg/Kg wet
1.67
64.8
30-130
12.0
30
2,4-Dinitrophenol
0.906
0.66
mg/Kg wet
1.67
54.3
30-130
10.7
30
V-19
2,4-Dinitrotoluene
1.26
0.34
mg/Kg wet
1.67
75.8
40-140
11.7
30
2,6-Dinitrotoluene
1.35
0.34
mg/Kg wet
1.67
81.2
40-140
13.1
30
Di-n-octylphthalate
1.39
0.34
mg/Kg wet
1.67
83.5
40-140
9.45
30
1,2-Diphenylhydrazine (as Azobenzene)
1.18
0.34
mg/Kg wet
1.67
70.7
40-140
9.08
30
Fluoranthene
1.08
0.17
mg/Kg wet
1.67
64.7
40-140
11.3
30
Fluorene
1.18
0.17
mg/Kg wet
1.67
70.8
40-140
13.9
30
Page 23 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216342 - SW-846 3546
LCS Dup (B216342-BSD1) Prepared: 11/03/18 Analyzed: 11/05/18
Hexachlorobenzene
1.04
0.34
mg/Kg wet
1.67
62.6
40-140
2.03
30
Hexachlorobutadiene
0.902
0.34
mg/Kg wet
1.67
54.1
40-140
2.47
30
Hexachlorocyclopentadiene
0.619
0.34
mg/Kg wet
1.67
37.1 *
40-140
11.0
30
L-04, V-05
Hexachloroethane
0.816
0.34
mg/Kg wet
1.67
49.0
40-140
2.02
30
Indeno(1,2,3-cd)pyrene
1.48
0.17
mg/Kg wet
1.67
88.8
40-140
8.21
30
Isophorone
1.08
0.34
mg/Kg wet
1.67
65.1
40-140
7.79
30
1-Methylnaphthalene
0.959
0.17
mg/Kg wet
1.67
57.5
40-140
9.31
30
2-Methylnaphthalene
1.06
0.17
mg/Kg wet
1.67
63.6
40-140
10.2
30
2-Methylphenol
1.06
0.34
mg/Kg wet
1.67
63.5
30-130
7.49
30
3/4-Methylphenol
1.11
0.34
mg/Kg wet
1.67
66.4
30-130
7.44
30
Naphthalene
0.925
0.17
mg/Kg wet
1.67
55.5
40-140
3.78
30
2-Nitroanihne
1.49
0.34
mg/Kg wet
1.67
89.2
40-140
18.5
30
V-06
3-Nitroaniline
1.08
0.34
mg/Kg wet
1.67
65.0
30-140
10.3
30
f
4-Nitroaniline
1.20
0.34
mg/Kg wet
1.67
71.8
40-140
12.0
30
Nitrobenzene
1.03
0.34
mg/Kg wet
1.67
61.8
40-140
5.04
30
2-Nitrophenol
1.06
0.34
mg/Kg wet
1.67
63.3
30-130
8.70
30
4-Nitrophenol
1.92
0.66
mg/Kg wet
1.67
91.1
30-130
14.3
50
V-06 $
N-Nitrosodimethylamine
1.01
0.34
mg/Kg wet
1.67
60.7
40-140
4.22
30
N-Nitrosodiphenylamine
1.25
0.34
mg/Kg wet
1.67
74.9
40-140
8.49
30
N-Nitrosodi-n-propylamine
1.07
0.34
mg/Kg wet
1.67
64.4
40-140
8.95
30
Pentachloronitrobenzene
1.06
0.34
mg/Kg wet
1.67
63.7
40-140
1.23
30
Pentachlorophenol
0.679
0.34
mg/Kg wet
1.67
40.7
30-130
1.09
30
Phenanthrene
1.06
0.17
mg/Kg wet
1.67
63.9
40-140
9.99
30
Phenol
1.01
0.34
mg/Kg wet
1.67
60.7
30-130
5.03
30
Pyrene
1.18
0.17
mg/Kg wet
1.67
70.9
40-140
10.6
30
Pyridine
0.473
0.34
mg/Kg wet
1.67
28.4 *
30-140
7.99
30
L-07, V-05 t
1,2,4,5-Tetrachlorobenzene
1.08
0.34
mg/Kg wet
1.67
65.0
40-140
9.51
30
1,2,4-Trichlorobenzene
0.887
0.34
mg/Kg wet
1.67
53.2
40-140
3.71
30
2,4,5-Trichlorophenol
1.22
0.34
mg/Kg wet
1.67
73.3
30-130
13.6
30
2,4,6-Trichlorophenol
1.18
0.34
mg/Kg wet
1.67
70.5
30-130
11.8
30
Surrogate:2-Fluorophenol
3.74
mg/Kg wet
6.67
56.2
30-130
Surrogate: Phenol-d6
4.38
mg/Kg wet
6.67
65.7
30-130
Surrogate: Nitrobenzene-d5
2.17
mg/Kg wet
3.33
65.2
30-130
Surrogate: 2-Fluorobiphenyl
2.01
mg/Kg wet
3.33
60.3
30-130
Surrogate:2,4,6-Tribromophenol
5.88
mg/Kg wet
6.67
88.2
30-130
Surrogate: p-Terphenyl-dl4
2.44
mg/Kg wet
3.33
73.3
30-130
Page 24 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216348 - SW-846 3546
Blank (B216348-BLK1) Prepared: 11/04/18 Analyzed: 11/05/18
C9-C 18 Aliphatics
ND
10
mg/Kg wet
C19-C36 Aliphatics
ND
10
mg/Kg wet
Cl 1-C22 Aromatics
ND
10
mg/Kg wet
Acenaphthene
ND
0.10
mg/Kg wet
Acenaphthylene
ND
0.10
mg/Kg wet
Anthracene
ND
0.10
mg/Kg wet
Benzo(a)anthracene
ND
0.10
mg/Kg wet
Benzo(a)pyrene
ND
0.10
mg/Kg wet
Benzo(b)fluoranthene
ND
0.10
mg/Kg wet
Benzo(g,h,i)perylene
ND
0.10
mg/Kg wet
Benzo(b)fluoranthene
ND
0.10
mg/Kg wet
Chrysene
ND
0.10
mg/Kg wet
Dibenz(a,h)anthracene
ND
0.10
mg/Kg wet
Fluoranthene
ND
0.10
mg/Kg wet
Fluorene
ND
0.10
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
0.10
mg/Kg wet
2-Methylnaphthalene
ND
0.10
mg/Kg wet
Naphthalene
ND
0.10
mg/Kg wet
Phenanthrene
ND
0.10
mg/Kg wet
Pyrene
ND
0.10
mg/Kg wet
n-Decane
ND
0.10
mg/Kg wet R-05
n-Docosane
ND
0.10
mg/Kg wet
n-Dodecane
ND
0.10
mg/Kg wet
n-Eicosane
ND
0.10
mg/Kg wet
n-Hexacosane
ND
0.10
mg/Kg wet
n-Hexadecane
ND
0.10
mg/Kg wet
n-Hexatriacontane
ND
0.10
mg/Kg wet
n-Nonadecane
ND
0.10
mg/Kg wet
n-Nonane
ND
0.10
mg/Kg wet R-05
n-Octacosane
ND
0.10
mg/Kg wet
n-Octadecane
ND
0.10
mg/Kg wet
n-Tetracosane
ND
0.10
mg/Kg wet
n-Tetradecane
ND
0.10
mg/Kg wet
n-Triacontane
ND
0.10
mg/Kg wet
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
Surrogate: Chlorooctadecane (COD)
3.83 mg/Kg wet
5.15 74.3 40-140
Surrogate: o-Terphenyl (OTP)
4.08 mg/Kg wet
5.00 81.6 40-140
Surrogate:2-Bromonaphthalene
5.59 mg/Kg wet
5.00 112 40-140
Surrogate: 2-Fluorobiphenyl
5.93 mg/Kg wet
5.00 119 40-140
LCS (B216348-BS1)
Prepared: 11/04/18 Analyzed: 11/05/18
C9-C 18 Aliphatics
21.6
10
mg/Kg wet
30.0
72.1
40-140
C19-C36Aliphatics
31.8
10
mg/Kg wet
40.0
79.6
40-140
Acenaphthene
3.41
0.10
mg/Kg wet
5.00
68.1
40-140
Acenaphthylene
3.20
0.10
mg/Kg wet
5.00
63.9
40-140
Anthracene
3.30
0.10
mg/Kg wet
5.00
66.0
40-140
Benzo(a)anthracene
3.22
0.10
mg/Kg wet
5.00
64.4
40-140
Benzo(a)pyrene
3.20
0.10
mg/Kg wet
5.00
64.0
40-140
Benzo(b)fluoranthene
3.30
0.10
mg/Kg wet
5.00
66.0
40-140
Benzo(g,h,i)perylene
3.21
0.10
mg/Kg wet
5.00
64.3
40-140
Benzo(k)fluoranthene
3.26
0.10
mg/Kg wet
5.00
65.2
40-140
Page 25 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
walyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216348 - SW-846 3546
LCS (B216348-BSI)
Prepared: 11/04/18 Analyzed: 11/05/18
Chrysene
3.32
0.10
mg/Kg wet
5.00
66.5
40-140
Dibenz(a,h)anthracene
3.37
0.10
mg/Kg wet
5.00
67.3
40-140
Fluoranthene
3.32
0.10
mg/Kg wet
5.00
66.4
40-140
Fluorene
3.32
0.10
mg/Kg wet
5.00
66.3
40-140
Indeno(1,2,3-cd)pyrene
3.14
0.10
mg/Kg wet
5.00
62.8
40-140
2-Methylnaphthalene
3.03
0.10
mg/Kg wet
5.00
60.6
40-140
Naphthalene
3.09
0.10
mg/Kg wet
5.00
61.9
40-140
Phenanthrene
3.39
0.10
mg/Kg wet
5.00
67.7
40-140
Pyrene
3.33
0.10
mg/Kg wet
5.00
66.5
40-140
n-Decane
2.60
0.10
mg/Kg wet
5.00
52.0
40-140 R-05
n-Docosane
3.32
0.10
mg/Kg wet
5.00
66.3
40-140
n-Dodecane
3.06
0.10
mg/Kg wet
5.00
61.2
40-140
n-Eicosane
3.30
0.10
mg/Kg wet
5.00
66.1
40-140
n-Hexacosane
3.26
0.10
mg/Kg wet
5.00
65.3
40-140
n-Hexadecane
3.48
0.10
mg/Kg wet
5.00
69.5
40-140
n-Hexatriacontane
3.16
0.10
mg/Kg wet
5.00
63.3
40-140
n-Nonadecane
3.33
0.10
mg/Kg wet
5.00
66.7
40-140
n-Nonane
1.94
0.10
mg/Kg wet
5.00
38.8
30-140 R-05
n-Octacosane
3.18
0.10
mg/Kg wet
5.00
63.7
40-140
n-Octadecane
3.44
0.10
mg/Kg wet
5.00
68.8
40-140
n-Tetracosane
3.30
0.10
mg/Kg wet
5.00
66.0
40-140
n-Tetradecane
3.36
0.10
mg/Kg wet
5.00
67.2
40-140
n-Triacontane
3.22
0.10
mg/Kg wet
5.00
64.3
40-140
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
Surrogate: Chlorooctadecane (COD)
3.34
mg/Kg wet
5.15
64.9
40-140
Surrogate: o-Terphenyl (OTP)
3.41
mg/Kg wet
5.00
68.2
40-140
Surrogate: 2-Bromonaphthalene
5.17
mg/Kg wet
5.00
103
40-140
Surrogate:2-Fluorobiphenyl
5.68
mg/Kg wet
5.00
114
40-140
LCS Dup (B216348-BSD1)
Prepared: 11/04/18 Analyzed: 11/05/18
C9-C18Aliphatics
19.2
10
mg/Kg wet
30.0
63.9
40-140
12.0
C19-C36Aliphatics
34.2
10
mg/Kg wet
40.0
85.6
40-140
7.24
Acenaphthene
3.03
0.10
mg/Kg wet
5.00
60.5
40-140
11.8
Acenaphthylene
2.82
0.10
mg/Kg wet
5.00
56.5
40-140
12.4
Anthracene
3.40
0.10
mg/Kg wet
5.00
70.0
40-140
5.87
Benzo(a)anthracene
3.63
0.10
mg/Kg wet
5.00
72.7
40-140
12.0
Benzo(a)pyrene
3.39
0.10
mg/Kg wet
5.00
71.7
40-140
11.3
Benzo(b)fluoranthene
3.73
0.10
mg/Kg wet
5.00
74.5
40-140
12.1
Benzo(g,h,i)perylene
3.35
0.10
mg/Kg wet
5.00
67.0
40-140
4.23
Benzo(k)fluoranthene
3.65
0.10
mg/Kg wet
5.00
72.9
40-140
11.1
Chrysene
3.71
0.10
mg/Kg wet
5.00
74.2
40-140
11.0
Dibenz(a,h)anthracene
3.65
0.10
mg/Kg wet
5.00
73.0
40-140
8.14
Fluoranthene
3.68
0.10
mg/Kg wet
5.00
73.6
40-140
10.4
Fluorene
3.06
0.10
mg/Kg wet
5.00
61.2
40-140
8.06
Indeno(1,2,3-cd)pyrene
3.50
0.10
mg/Kg wet
5.00
70.1
40-140
11.0
2-Methylnaphthalene
2.58
0.10
mg/Kg wet
5.00
51.6
40-140
16.0
Naphthalene
2.55
0.10
mg/Kg wet
5.00
51.0
40-140
19.3
Phenanthrene
3.42
0.10
mg/Kg wet
5.00
68.3
40-140
0.876
Pyrene
3.70
0.10
mg/Kg wet
5.00
74.1
40-140
10.7
n-Decane
1.90
0.10
mg/Kg wet
5.00
38.0
* 40-140
31.1
n-Docosane
3.67
0.10
mg/Kg wet
5.00
73.4
40-140
10.0
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25
25 L-07.A
25
Page 26 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - EPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216348 - SW-846 3546
LCS Dup (B216348-BSD1)
Prepared: 11/04/18 Analyzed: 11/05/18
n-Dodecane
2.45
0.10
mg/Kg wet
5.00
49.0
40-140
22.1
25
n-Eicosane
3.77
0.10
mg/Kg wet
5.00
75.4
40-140
13.1
25
n-Hexacosane
3.62
0.10
mg/Kg wet
5.00
72.4
40-140
10.3
25
n-Hexadecane
3.16
0.10
mg/Kg wet
5.00
63.2
40-140
9.54
25
n-Hexatriacontane
3.56
0.10
mg/Kg wet
5.00
71.3
40-140
11.9
25
n-Nonadecane
3.38
0.10
mg/Kg wet
5.00
71.5
40-140
7.03
25
n-Nonane
1.28
0.10
mg/Kg wet
5.00
25.6 *
30-140
40.9 *
25 L-07A
n-Octacosane
3.54
0.10
mg/Kg wet
5.00
70.8
40-140
10.5
25
n-Octadecane
3.55
0.10
mg/Kg wet
5.00
71.0
40-140
3.19
25
n-Tetracosane
3.65
0.10
mg/Kg wet
5.00
72.9
40-140
9.98
25
n-Tetradecane
2.86
0.10
mg/Kg wet
5.00
57.3
40-140
16.0
25
n-Triacontane
3.37
0.10
mg/Kg wet
5.00
71.5
40-140
10.5
25
Naphthalene -aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
2-Methylnaphthalene-aliphatic fraction
ND
0.10
mg/Kg wet
5.00
0-5
Surrogate: Chlorooctadecane (COD)
3.64
mg/Kg wet
5.15
70.6
40-140
Surrogate: o-Terphenyl (OTP)
3.55
mg/Kg wet
5.00
70.9
40-140
Surrogate:2-Bromonaphthalene
5.44
mg/Kg wet
5.00
109
40-140
Surrogate:2-Fluorobiphenyl
5.93
mg/Kg wet
5.00
119
40-140
Page 27 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - VPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216531 - MA VPH
Blank (B216531-BLK1) Prepared: 11/06/18 Analyzed: 11/07/18
C5-C8 Aliphatics
ND
10
mg/Kg wet
C9-C12 Aliphatics
ND
10
mg/Kg wet
C9-C 10 Aromatics
ND
10
mg/Kg wet
Benzene
ND
0.050
mg/Kg wet
Butylcyclohexane
ND
0.050
mg/Kg wet
Decane
ND
0.050
mg/Kg wet
Ethylbenzene
ND
0.050
mg/Kg wet
Methyl tert-Butyl Ether (MTBE)
ND
0.050
mg/Kg wet
2-Methylpentane
ND
0.050
mg/Kg wet
Naphthalene
ND
0.50
mg/Kg wet
Nonane
ND
0.050
mg/Kg wet
Pentane
ND
0.050
mg/Kg wet
Toluene
ND
0.050
mg/Kg wet
1,2,4-Trimethylbenzene
ND
0.050
mg/Kg wet
2,2,4-Trimethylpentane
ND
0.050
mg/Kg wet
m+p Xylene
ND
0.10
mg/Kg wet
o-Xylene
ND
0.050
mg/Kg wet
Surrogate:2,5-Dibromotoluene (FID) 41.1 µg/L 40.0 103 70-130
Surrogate:2,5-Dibromotoluene (PID) 37.9 µg/L 40.0 94.8 70-130
LCS (B216531-BS1) Prepared: 11/06/18 Analyzed: 11/07/18
C9-C 10 Aromatics
0.0700
0.20
mg/Kg wet
70-130
Benzene
0.0491
0.0010
mg/Kg wet
0.0500
98.3
70-130
Butylcyclohexane
0.0585
0.0010
mg/Kg wet
0.0500
117
70-130
Decane
0.0463
0.0010
mg/Kg wet
0.0500
92.6
70-130
Ethylbenzene
0.0499
0.0010
mg/Kg wet
0.0500
99.9
70-130
Methyl tert-Butyl Ether (MTBE)
0.0487
0.0010
mg/Kg wet
0.0500
97.5
70-130
2-Methylpentane
0.0548
0.0010
mg/Kgwet
0.0500
110
70-130
Naphthalene
0.0461
0.010
mg/Kg wet
0.0500
92.3
70-130
Nonane
0.0566
0.0010
mg/Kg wet
0.0500
113
30-130
Pentane
0.0530
0.0010
mg/Kg wet
0.0500
106
70-130
Toluene
0.0497
0.0010
mg/Kg wet
0.0500
99.5
70-130
1,2,4-Trimethylbenzene
0.0508
0.0010
mg/Kg wet
0.0500
102
70-130
2,2,4-Trimethylpentane
0.0524
0.0010
mg/Kg wet
0.0500
105
70-130
m+p Xylene
0.101
0.0020
mg/Kg wet
0.100
101
70-130
o-Xylene
0.0502
0.0010
mg/Kg wet
0.0500
100
70-130
Surrogate: 2,5-Dibromotoluene (FID) 41.8 µg/L 40.0 107 70-130
Surrogate:2,5-Dibromotoluene (PID) 41.9 µg/L 40.0 105 70-130
LCS Dup (B216531-BSD1) Prepared: 11/06/18 Analyzed: 11/07/18
C9-C 10 Aromatics
0.0692
0.20
mg/Kg wet
70-130
1.25
Benzene
0.0495
0.0010
mg/Kg wet
0.0500
99.0
70-130
0.698
Butylcyclohexane
0.0572
0.0010
mg/Kg wet
0.0500
114
70-130
2.23
Decane
0.0451
0.0010
mg/Kg wet
0.0500
90.2
70-130
2.55
Ethylbenzene
0.0504
0.0010
mg/Kg wet
0.0500
101
70-130
0.833
Methyl tert-Butyl Ether (MTBE)
0.0488
0.0010
mg/Kg wet
0.0500
97.6
70-130
0.195
2-Methylpentane
0.0555
0.0010
mg/Kg wet
0.0500
ill
70-130
1.22
Naphthalene
0.0455
0.010
mg/Kg wet
0.0500
91.1
70-130
1.32
Nonane
0.0560
0.0010
mg/Kg wet
0.0500
112
30-130
1.12
Pentane
0.0522
0.0010
mg/Kg wet
0.0500
104
70-130
1.51
Toluene
0.0500
0.0010
mg/Kg wet
0.0500
100
70-130
0.515
1,2,4-Trimethylbenzene
0.0508
0.0010
mg/Kg wet
0.0500
102
70-130
0.0315
25
25
25
25
25
25
25
25
25
25
25
25
Page 28 of 39

Table of Contents
,con -testy
ANALYTICAL LABORATORY
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - VPH - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B216531 - MA VPH
LCS Dup (B216531-BSD1) Prepared: 11/06/18 Analyzed: 11/07/18
2,2,4-Trimethylpentane 0.0519 0.0010 mg/Kg wet 0.0500 104 70-130 0.859 25
m+p Xylene 0.102 0.0020 mg/Kg wet 0.100 102 70-130 0.442 25
o-Xylene 0.0505 0.0010 mg/Kg wet 0.0500 101 70-130 0.544 25
Surrogate:2,5-Dibromotoluene (FID) 42.2 µg/L 40.0 106 70-130
Surrogate:2,5-Dibromotoluene (PID) 40.9 µg/L 40.0 102 70-130
Page 29 of 39

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits.
fi Wide recovery limits established for difficult compound.
$ Wide RPD limits established for difficult compound.
# Data exceeded client recommended or regulatory level
ND Not Detected
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07A Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for
this compound.
R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound.
V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound
V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with
correlation coefficient <0.99. Reported result is estimated.
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
Page 30 of 39

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
MADEP-EPH-04-1.1 in Soil
C9-C18 Aliphatics
CT,NC,ME,NH-P
C19-06 Aliphatics
CT,NC,ME,NH-P
C11-C22 Aromatics
CT,NC,ME,NH-P
Acenaphthene
CT,NC,ME,NH-P
Acenaphthylene
CT,NC,ME,NH-P
Anthracene
CT,NC,ME,NH-P
Benzo(a)anthracene
CT,NC,ME,NH-P
Benzo(a)pyrene
CT,NC,ME,NH-P
Benzo(b)fluoranthene
CT,NC,ME,NH-P
Benzo(g,h,i)perylene
CT,NC,ME,NH-P
Benzo(k)fluoranthene
CT,NC,ME,NH-P
Chrysene
CT,NC,ME,NH-P
Dibenz(a,h)anthracene
CT,NC,ME,NH-P
Fluoranthene
CT,NC,ME,NH-P
Fluorene
CT,NC,ME
Indeno(1,2,3-cd)pyrene
CT,NC,ME,NH-P
2-Methylnaphthalene
CT,NC,ME
Naphthalene
CT,NC,ME,NH-P
Phenanthrene
CT,NC,ME,NH-P
Pyrene
CT,NC,ME,NH-P
MADEP-VPH-Feb 1018 Rev 1.1 in Soil
C5-C8 Aliphatics
CT,NC,ME,NH-P
C9-C12 Aliphatics
CT,NC,ME,NH-P
C9-C10 Aromatics
CT,NC,ME,NH-P
Benzene
CT,NC,ME,NH-P
Ethylbenzene
CT,NC,ME,NH-P
Methyl tert-Butyl Ether (MTBE)
CT,NC,ME,NH-P
Naphthalene
CT,NC,ME,NH-P
Toluene
CT,NC,ME,NH-P
m+p Xylene
CT,NC,ME,NH-P
o-Xylene
CT,NC,ME,NH-P
SW-846 8260B in Soil
Acetone
NC
Acrylonitrile
NC
tert-Amyl Methyl Ether (TAME)
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Bromoform
NC
Bromomethane
NC
2-Butanone (MEK)
NC
tert-Butyl Alcohol (TBA)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
Page 31 of 39

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8260B in Soil
tert-Butyl Ethyl Ether (TBEE)
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromo-3-chloropropane (DBCP)
NC
1,2-Dibromoethane (EDB)
NC
Dibromomethane
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
trans-1,4-Dichloro-2-butene
NC
Dichlorodifluoromethane (Freon 12)
NC
1,1-Dichloroethane
NC
1,2-Dichloroethane
NC
1,1-Dichloroethylene
NC
cis-1,2-Dichloroethylene
NC
trans-1,2-Dichloroethylene
NC
1,2-Dichloropropane
NC
1,3-Dichloropropane
NC
2,2-Dichloropropane
NC
1,1-Dichloropropene
NC
cis- 1,3 -Dichloropropene
NC
trans- l,3-Dichloropropene
NC
Diethyl Ether
NC
Diisopropyl Ether (DIPE)
NC
1,4-Dioxane
NC
Ethylbenzene
NC
Hexachlombutadiene
NC
2-Hexanone (MBK)
NC
Isopropylbenzene (Cumene)
NC
p-Isopropyltoluene (p-Cymene)
NC
Methyl tert-Butyl Ether (MTBE)
NC
Methylene Chloride
NC
4-Methyl-2-pentanone (MIBK)
NC
Naphthalene
NC
n-Propylbenzene
NC
Styrene
NC
1, 1, 1,2-Tetrachloroethane
NC
1,1,2,2-Tetrachloroethane
NC
Tetrachloroethylene
NC
Tetrahydrofuran
NC
Page 32 of 39

MN
,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
SW-846 8260B in Soil
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trichlorobenzene
1, 1, 1 -Trichloroethane
1,1,2-Trichloroethane
Trichloroethylene
Trichlorofluoromethane (Freon 11)
1,2,3-Trichloropropane
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Chloride
m+p Xylene
o-Xylene
SW-846 8270D in Soil
Acenaphthene
Acenaphthylene
Acetophenone
Aniline
Anthracene
Benzidine
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
B is(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
Bis(2-chloroisopropyl)ether
Bis(2-Ethylhexyl)phthalate
4-Bromophenylphenylether
Butylbenzylphthalate
Carbazole
4-Chloroaniline
4-Chloro-3-methylphenol
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenylether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Di-n-butylphthalate
1,2-Dichlorobenzene
1,3-Dichlorobenzene
Certifications
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
NY,NH,ME,NC,VA
NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
NC
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
NY,NH,ME,NC,VA
NY,NH,ME,NC,VA
Page 33 of 39

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Soil
1,4-Dichlorobenzene
NY,NH,ME,NC,VA
3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA
2,4-Dichlorophenol
CT,NY,NH,ME,NC,VA
Diethylphthalate
CT,NY,NH,ME,NC,VA
2,4-Dimethylphenol
CT,NY,NH,ME,NC,VA
Dimethylphthalate
CT,NY,NH,ME,NC,VA
4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA
2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VA
Di-n-octylphthalate
CT,NY,NH,ME,NC,VA
1,2-Diphenylhydrazine (as Azobenzene)
NY,NH,ME,NC,VA
Fluoranthene
CT,NY,NH,ME,NC,VA
Fluorene
NY,NH,ME,NC,VA
Hexachlorobenzene
CT,NY,NH,ME,NC,VA
Hexachlorobutadiene
CT,NY,NH,ME,NC,VA
Hexachlorocyclopentadiene
CT,NY,NH,ME,NC,VA
Hexachloroethane
CT,NY,NH,ME,NC,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA
Isophorone
CT,NY,NH,ME,NC,VA
I -Methylnaphthalene
NC
2-Methy1naphthalene
CT,NY,NH,ME,NC,VA
2-Methylphenol
CT,NY,NH,ME,NC,VA
3/4-Methylphenol
CT,NY,NH,ME,NC,VA
Naphthalene
CT,NY,NH,ME,NC,VA
2-Nitroaniline
CT,NY,NH,ME,NC,VA
3-Nitroaniline
CT,NY,NH,ME,NC,VA
4-Nitroaniline
CT,NY,NH,ME,NC,VA
Nitrobenzene
CT,NY,NH,ME,NC,VA
2-Nitrophenol
CT,NY,NH,ME,NC,VA
4-Nitrophenol
CT,NY,NH,ME,NC,VA
N-Nitrosodimethylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodiphenylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodi-n-propylamine
CT,NY,NH,ME,NC,VA
Pentachloronitrobenzene
NY,NC
Pentachlorophenol
CT,NY,NH,ME,NC,VA
Phenanthrene
CT,NY,NH,ME,NC,VA
Phenol
CT,NY,NH,ME,NC,VA
Pyrene
CT,NY,NH,ME,NC,VA
Pyridine
CT,NY,NH,ME,NC,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA
2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA
2,4,6-Trichlorophenol
CT,NY,NH,ME,NC,VA
2-Fluorophenol
NC
SW-846 8270D in Water
Page 34 of 39

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Water
Acenaphthene
CT,NY,NC,ME,NH,VA
Acenaphthylene
CT,NY,NC,ME,NH,VA
Acetophenone
NY,NC
Aniline
CT,NY,NC,ME,VA
Anthracene
CT,NY,NC,ME,NH,VA
Benzidine
CT,NY,NC,ME,NH,VA
Benzo(a)anthracene
CT,NY,NC,ME,NH,VA
Benzo(a)pyrene
CT,NY,NC,ME,NH,VA
Benzo(b)fluoranthene
CT,NY,NC,ME,NH,VA
Benzo(g,h,i)perylene
CT,NY,NC,ME,NH,VA
Benzo(k)fluoranthene
CT,NY,NC,ME,NH,VA
Benzoic Acid
NY,NC,ME,NH,VA
Bis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VA
Bis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VA
Bis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA
4-Bromophenylphenylether
CT,NY,NC,ME,NH,VA
Butylbenzylphthalate
CT,NY,NC,ME,NH,VA
Carbazole
NC
4-Chloroaniline
CT,NY,NC,ME,NH,VA
4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA
2-Chloronaphthalene
CT,NY,NC,ME,NH,VA
2-Chlorophenol
CT,NY NC,ME,NH,VA
4-Chlorophenylphenylether
CT,NY NC,ME,NH,VA
Chrysene
CT,NY,NC,ME,NH,VA
Dibenz(a,h)anthracene
CT,NY,NC,ME,NH,VA
Dibenzofuran
CT,NY,NC,ME,NH,VA
Di-n-butylphthalate
CT,NY,NC,ME,NH,VA
1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA
1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA
3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA
2,4-Dichlorophenol
CT,NY,NC,ME,NH,VA
Diethylphthalate
CT,NY,NC,ME,NH,VA
2,4-Dimethylphenol
CT,NY,NC,ME,NH,VA
Dimethylphthalate
CT,NY,NC,ME,NH,VA
4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA
2,4-Dinitrotoluene
CT,NY,NC,ME,NH,VA
2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VA
Di-n-octylphthalate
CT,NY,NC,ME,NH,VA
1,2-Diphenylhydrazine (as Azobenzene)
NY,NC
Fluoranthene
CT,NY,NC,ME,NH,VA
Fluorene
NY,NC,ME,NH,VA
Hexachlorobenzene
CT,NY,NC,ME,NH,VA
Hexachlorobutadiene
CT,NY,NC,ME,NH,VA
Hexachlorocyclopentadiene
CT,NY,NC,ME,NH,VA
Page 35 of 39

,con -testy
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street' East Longmeadow, MA 01028 . FAX [phone] ` TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8270D in Water
Hexachlomethane
CT,NY,NC,ME,NH,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VA
Isophorone
CT,NY,NC,ME,NH,VA
1-Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NC,ME,NH,VA
2-Methylphenol
CT,NY,NC,NH,VA
3/4-Methylphenol
CT,NY,NC,NH,VA
Naphthalene
CT,NY,NC,ME,NH,VA
2-Nitmaniline
CT,NY,NC,ME,NH,VA
3-Nitroaniline
CT,NY,NC,ME,NH,VA
4-Nitroaniline
CT,NY,NC,ME,NH,VA
Nitrobenzene
CT,NY,NC,ME,NH,VA
2-Nitrophenol
CT,NY,NC,ME,NH,VA
4-Nitrophenol
CT,NY,NC,ME,NH,VA
N-Nitrosodimethylamine
CT,NY,NC,ME,NH,VA
N-Nitrosodiphenylamine
CT,NY,NC,ME,NH,VA
N-Nitrosodi-n-propylamine
CT,NY,NC,ME,NH,VA
Pentachloronitrobenzene
NC
Pentachlorophenol
CT,NY,NC,ME,NH,VA
Phenanthrene
CT,NY,NC,ME,NH,VA
Phenol
CT,NY,NC,ME,NH,VA
Pyrene
CT,NY,NC,ME,NH,VA
Pyridine
CT,NY,NC,ME,NH,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA
2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA
2,4,6-Trichlorophenol
CT,NY,NC,ME,NH,VA
2-Fluorophenol
NC
The CON -TEST Environmental Laboratory operates under the
following certifications and accreditations:
Code Description
Number
Expires
AIHA AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA Massachusetts DEP
M-MA100
06/30/2019
CT Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY New York State Department of Health
10899 NELAP
04/1/2019
NH-S New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI Rhode Island Department of Health
LA000112
12/30/2018
NC North Carolina Div. of Water Quality
652
12/31/2018
NJ New Jersey DEP
MA007 NELAP
06/30/2019
FL Florida Department of Health
E871027 NELAP
06/30/2019
VT Vermont Department of Health Lead Laboratory
LL015036
07/30/2019
ME State of Maine
2011028
06/9/2019
VA Commonwealth of Virginia
460217
12/14/2018
NH-P New Hampshire Environmental Lab
2557 NELAP
09/6/2019
VT-DW Vermont Department of Health Drinking Water
VT-255716
06/12/2019
NC-DW North Carolina Department of Health
25703
07/31/2019
Page 36 of 39

Table of Contents
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11/01/2018
11/02/2018
EAST LONGMEADOW, MA
773629234493
CHARLOTTE, NO
1W01/2018
11/02/2018
EAST LONGMEADOW, MA
Shipment Facts
https:llwww.fedex.comlappslfedextrackl?action=track&tracknurnbers=773629234379&locale=en_US&cntry_code=us Page 38 of 39

Table of Contents
Received By
How were the samples
received?
Date 1!
In Cooler -7— No Cooler
Direct from Sampling
Time
On Ice 1
Ambient
RI
No Ice
Melted Ice
Were samples within By Gun # Actual Temp - .
Temperature? 2-6°C T By Blank # Actual Temp -
Was Custody Sea] Intact? Aiy: - Were Samples Tampered with?
Was COC Relinquished ? T Does Chain Agree With Samples? �—
Are there broken/leaking/loose caps on any samples? I^
Is COC in inkl Legible? i—
Did COC include all Client i
pertinent Information? Project S
Are Sample labels filled out and legible? 7—
Are there Lab to Filters?
Are there Rushes? _ �=
Are there Short Holds?
Is there enough Volume? T
Is there Headspace where applicable?
Proper Media/Containers Used?
Were trip blanks received?
Do all samples have the proper pH? 1 V -
Were samples received within holding time? S
Analysis f Sampler Name
ID`s r{- Collection Dates/Times i
Who was notified?
Who was notified?
Who was notified?
MS/MSD?
Is splitting samples required?
On COC?
Acid Base

Beverly, Trudy
From:
McDorman, James <[e-mail]>
Sent:
Tuesday, March 26, 2019 8:42 AM
To:
Beverly, Trudy
Cc:
Foster, Rob
Subject:
[External] CLT-Former GADO Building
• I email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
�[e-mail]
Good morning Trudy,
Our consultant, Wood Environment & Infrastructure Solutions (Wood), submitted an Initial Abatement Action
Report (IAAR) back in November 2018. The IAAR was for an UST permanent closure, impacted soil excavation
and disposal. Checking in to see if you have any questions or require additional information concerning the
IAAR.
Thank you,
JAMES P MCDORMAN P.G. I ENVIRONMENTAL COMPLIANCE COORDINATOR
CHARLOTTE DOUGLAS INTERNATIONAL AIRPORT
m 704-560-9242
cltairport.com
Charlotte Douglas International Airport (CLT), a City of Charlotte department, welcomes more than 46 million
passengers annually. CLT is ranked among the top 10 busiest airports in the world, averaging 1,400 daily aircraft
operations. (ACI 2018 Preliminary rankings) CLT is served by seven major carriers, 15 regional carriers and three
foreign flag carriers with nonstop service to 174 destinations, including 36 international locations and 3 US territories.
(CLT Fast Facts)

Beverly, Trudy
From:
Sent:
To:
Beverly, Trudy
Tuesday, December 11, 2018 9:58 AM
'Foster, Rob'
Subject: RE: [External] GADO building Initial Abatement Action Report
Hey Rob,
Yes, the report was received on December 7tn
Trudy
er-a D� E Q7>
u.pr.�r+rt n �rw�eMwnr� uwiih�
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environment Quality
Underground Storage Tanks Section
Corrective Action Branch
Mooresville Regional Office
[phone] (Office)
Trudv.Beve rlv(@ncdenr.gov
Err Y mmwOvve to aW from this addre55 +s subject to the
h+o h Caidffa P)bkc Reco Fds Law aril may be dwk.)sed to third part+es-
Branch's Underground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-
management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https://deg.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps
File Review Procedures:
https://deg.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://edocs.deg.nc.gov/WasteManagement/Search.aspx
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/Electronic%20Document%20Submi
ttal%20Memo%20Update. pdf
https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%2Ofile%20names%20for%20
Laserfiche.docx
From: Foster, Rob [mailto:[e-mail]]
Sent: Tuesday, December 11, 2018 9:55 AM
To: Beverly, Trudy <[e-mail]>
Subject: [External] GADO building Initial Abatement Action Report
0 External email. Do not click links or open attachments unless verified. Send all suspicious email as an attachment to
Trudy,
We recently submitted by regular mail the report described above. I just wanted to verify you rec'd it.

Rob Foster
Rob Foster, LG
Associate Geologist — Charlotte, North Carolina
Environment & Infrastructure Solutions
Direct: [phone]
Mobile: [phone]
VoIP: #711-5530
Rob.foster(aD_woodplc.com
www.woodplc.com
wood
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