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HomeMy WebLinkAboutMO-9448_40883_CA__IAR_20181126_Initial Abatement Action Reportwood. INITIAL ABATEMENT ACTION REPORT GADO BUILDING 5318 MORRIS FIELD DRIVE CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA 28208 PREPARED FOR: CHARLOTTE DOUGLAS INTERNATIONAL AIRPORT P.O. BOX 19066 CHARLOTTE, NORTH CAROLINA 28219 PREPARED BY: WOOD ENVIRONMENT & INFRASTRUCTURE SOLUTIONS, INC. 2801 YORKMONT ROAD, SUITE 100 CHARLOTTE, NORTH CAROLINA 28208 NOVEMBER 26, 2018 WOOD PROJECT: 6228-18-0503 wood. Wood Environment & Infrastructure Solutions, Inc. 2801 Yorkmont Road, Suite 100 Charlotte, North Carolina 28208 Licensures: NC Engineering F-1253, Geology C-247 T: 704-357-8600 www.woodpic.com November 26, 2018 Ms. Trudy Beverly North Carolina Department of Environmental Quality Mooresville Regional Office UST Section 610 East Center Avenue Mooresville, North Carolina 28115 Subject: Initial Abatement Action Report GADO Building 5318 Morris Field Drive Charlotte, Mecklenburg County, North Carolina Wood Project: 6228-18-0503 Facility ID: 00-0-0000033447 Dear Ms. Beverly: On behalf of Charlotte -Douglas International Airport (CLT), (Tank Owner), Wood Environment & Infrastructure Solutions, Inc. (Wood) is submitting the enclosed Initial Abatement Action Report for the facility located at 5318 Morris Field Drive in Charlotte, Mecklenburg County, North Carolina (the Site). The report was prepared in general accordance with the North Carolina Department of Environmental Quality, UST Section Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases (March 1, 2007 version, Change 8, effective January 9, 2018). This report includes a description of the field activities and the results obtained. Sincerely, Wood Environment & Infrastructure Solutions, Inc. Leanna Muroski Technical Professional Enclosure Robert C. Foster, LG Associate Geologist Registered, NC #1335 Mr. James P. McDorman, P.G., Environmental Compliance Coordinator, CLT 'Wood' is a trading name for John Wood Group PLC and its subsidiaries r Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 TABLE OF CONTENTS TABLEOF CONTENTS.................................................................................................................... ii A. SITE INFORMATION........................................................................................................... 1 1. Site Identification...................................................................................................................................1 2. Information about Contacts Associated with the UST System.......................................................1 3. Information about Release...................................................................................................................1 B. SITE HISTORY AND CHARACTERIZATION........................................................................ 3 1. UST Owner/Operator Information......................................................................................................3 2. UST Information.....................................................................................................................................4 3. Site Characterization.............................................................................................................................5 C. UST CLOSURE REPORT.......................................................................................................6 1. Preparations for Closure.......................................................................................................................6 2. Closure Procedures................................................................................................................................6 D. INITIAL RESPONSE AND ABATEMENT ACTION.............................................................. 8 E. EXCAVATION OF CONTAMINATED SOIL.......................................................................... 9 1. Determination of the Source and Extent of Soil Contamination...................................................9 2. Excavation Process.................................................................................................................................9 F. CONCLUSIONS..................................................................................................................10 FIGURES Figure 1 Site Topo Figure 2 Tank Location Map Figure 3 Site Plan TABLES Table 1 Summary of Soil Analytical Results APPENDICES Appendix A Liquid and Soil Disposal Manifests Appendix B Photographs Appendix C UST-213 Form Appendix D Laboratory Analytical Reports and Chain -of -Custody Forms Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 A. SITE INFORMATION 1. Site Identification Date of Report: November 26, 2018 Facility I.D.: 00-0-0000033447 UST Incident Number: N/A Site Risk: Site Name: GADO Building Street Address: 5318 Morris Field Drive City: Charlotte Zip Code: 28208 County: Mecklenburg Description of Geographical Data Point: Middle of tank basin Location Method: Google Maps Latitude: 35.212160' Longitude:-80.932720' 2. Information about Contacts Associated with the UST System UST Owner: Charlotte Douglas International Airport Address: P.O. Box 19066, Charlotte, North Carolina 28219 Telephone: 704-359-4789 UST Operator: Charlotte Douglas International Airport Address: P.O. Box 19066, Charlotte, North Carolina 28219 Telephone: 704-359-4789 Property Owner: City of Charlotte Real Estate Division Address: 600 East Fourth Street, Charlotte, North Carolina 28202 Telephone: 704-336-2291 Consultant: Wood Environment & Infrastructure Solutions, Inc. Address: 2801 Yorkmont Road, Suite 100, Charlotte, North Carolina 28208 Telephone: 704-357-8600 Analytical Laboratory: Con -test Analytical Laboratory State Certification No.: 25703 Address: 39 Spruce Street, East Longmeadow, MA 01028 Telephone: 413-525-2332 3. Information about Release Date Discovered: October 19, 2018 Estimated Quantity of Release: Unknown Cause of Release: leaking UST Source of Release: Underground Storage Tank Initial Abatement Action Report — GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 Sizes and Contents of Tanks or Other Containment from which Release Occurred: One approximate 1,400-gallon UST formerly used to store heating oil for a boiler. I, Robert C. Foster, a Licensed Geologist for Wood Environment & Infrastructure Solutions, Inc., do certify information cont� ned in this report is correct and accurate to the best of my knowledge. � 6&61tt-�C' VW-NITZ�Inll, h Please affix Seal a` O�o.�i,L,r (Date) SEAL 1335 — Wood EnvironmeFR Infrastructure �Igtions, Inc. is licensed to practice geology and engineering in -'Qi - .' North Carolina. The,4,p oikli 60t r s C-247. JC 2 Initial Abatement Action Report - GADO Building 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 B. SITE HISTORY AND CHARACTERIZATION 1. UST Owner/Operator Information November 26, 2018 UST ID Number 1 1 Facility ID Number 00-0-0000033447 Name of Land Owner Dates of Ownership City of Charlotte Real Estate Division Street Address 600 West Fourth Street City State Zip Telephone Number Charlotte North Carolina 28202 704-336-2291 Name of Tank Owner/Operator Dates of Operation Charlotte Douglas International Airport 1973 to 1990 Street Address P.O. Box 19066 City State Zip Telephone Number Charlotte North Carolina 28219 704-359-4789 Incident Number Pending Initial Abatement Action Report — GADO Building 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 2. UST Information November 26, 2018 Description of Was release Associated Status of associated UST ID Current/Last Previous Capacity (in Construction Date Tank Tank Dimensions Piping and UST with the UST Number Contents Contents gallons) Details Installed Pumps System? No pumps Approximately present. 1/2- June 23, 1 Heating Oil Heating Oil Steel 4 feet by 15 feet inch diameter Removed Yes 1,400 copper tubing 1973 product lines. Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 3. Site Characterization The Site is comprised of a small portion of Mecklenburg County Tax Parcel 115-211-03 which encompasses approximately 249 acres. The CLT Airport GADO Building and an adjacent auxiliary building formerly located at 5318 Morris Field Drive in Charlotte, North Carolina were recently demolished. The GADO Building encompassed approximately 6,600 square ft. with two stories and a basement. The auxiliary building encompassed approximately 225 square ft. The buildings were reportedly built in the 1950's. During demolition activities, Jones Grading and Fencing, Inc. (Jones) encountered a buried Underground Storage Tank (UST). A Topographic Map is included as Figure 1. An aerial photograph showing the location of the tank at the property is included as Figure 2. The tank was reportedly installed in 1973 and was used to store heating oil for the on -site boiler until about 1990 when the boiler was converted to natural gas. The site is located within the Charlotte Belt of the Piedmont Physiographic Province consisting of low rounded hills and long rolling northeast to the southwest trending ridges with incised creek channels. Based on a review of the North Carolina Geologic Map, the site is underlain by metamorphosed quartz diorite. Based on the United States Geologic Survey (USGS) topographic map, the elevation at the Site ranges from about 722 feet above mean sea level. Surface drainage patterns within the Piedmont typically indicate the direction contaminants would be transported by surface or groundwater. Based on our interpretation of the topographic map and on -site observations, surface water on the Site would be expected to flow to the east. The direction and movement of groundwater through soil is dependent on soil type and the presence of relict structures and textures of the underlying rock. Fractures, faults, folds and foliation planes affect the migration of groundwater in rock. Since no significant geologic features were identified in or on the site, it is reasonable to assume that the direction of on - surface groundwater flow under static conditions (no pumping interference) approximates the surface topography of the site. Groundwater at the site would be expected to flow to the east toward an unnamed tributary of Taggart Creek. 5 Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 C. UST CLOSURE REPORT Preparations for Closure CLT personnel retained Jones to remove the UST and Wood to perform the UST Closure Assessment. Because the tank contained liquid at the time of discovery, CLT also retained a waste disposal company to mobilize a vacuum truck to the property and remove the liquids and transport them to a permitted facility for disposal. Prior to removal of the tank, approximately 700 gallons of heating oil and petroleum contact water (PCW) was pumped from the tank into a vacuum truck for off -site disposal by HAZ-MAT Environmental Services. The liquid disposal manifest is included in Appendix A. 2. Closure Procedures On October 19, 2018, Wood personnel met CLT and Jones personnel at the site to oversee the removal of the tank. Jones personnel had removed overburden soil prior to Wood's arrival. The tank had been covered by three feet of soil prior to discovery. Based on field screening, the overburden soil did not appear to be affected with petroleum and was stockpiled separately for later use. Prior to initiating the UST removal activities, Wood personnel used a RAE Systems QRAE (2 Gas) meter to check the inside of the tank for flammable vapors. The lower explosive limit (LEL) was measured within the UST using a RAE Systems QRAE 3 to verify safe removal. Prior to removal, the UST was rendered inert by inserting dry ice into the tank. Based on this information, Jones resumed removal of soil to further expose the top and sides of the UST. Representative samples of soil from around the UST were collected and screened in the field for volatile organic compounds (VOCs) using a RAE Systems MiniRAE 3000 equipped with a photoionization detector (PID) while the UST was being exposed. Elevated PID readings were noted in the soil as removal extended vertically to near the depth of the bottom of the tank. On October 19, 2018, Wood personnel observed Jones removing the UST from the excavation. As the tank was lifted from the excavation, pooled heating oil was noted on the soil beneath the tank. In addition, corrosion holes were noted in the UST upon removal. Photographs taken by Wood personnel during the excavation and removal activities are included in Appendix B. The UST was transported by Jones to Southern Metals Company for disposal. The UST-2B UST Closure Form is included in Appendix C. UST closure soil samples were collected following the removal of the UST. Two soil samples (TB- 1 and TB-2) were collected from beneath the UST at a depth of nine feet below ground surface 0 Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 (bgs). In addition, CLT personnel requested that Wood collect a sample from the stockpile (Stockpile) for waste characterization purposes. The soil samples were collected manually by Wood personnel directly from the trackhoe excavator bucket. To minimize the potential for cross -contamination, a new pair of nitrile gloves was donned for the collection of each soil sample. The soil samples (T13-1 and T13-2) were placed directly into laboratory -provided containers and placed in a cooler on ice for delivery to Con -test Analytical Laboratory (Con -test), a North Carolina -certified laboratory. The soil samples were analyzed for Total Petroleum Hydrocarbons (TPH) diesel range organics (DRO) and gasoline range organics (GRO) via EPA Method 8015C. In addition, the stockpile sample was analyzed for benzene, ethylbenzene, toluene and xylenes (BETX) by EPA Method 826013. The samples were maintained under a chain - of -custody protocol. 7 Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 D. INITIAL RESPONSE AND ABATEMENT ACTION CLT personnel requested that Wood personnel return to the site on October 22, 2018 to oversee removal of petroleum -affected soil from the excavation. A representative of Wood observed soil excavation and collected samples of soil from the excavator bucket and screened them in the field for VOCs using a RAE Systems MiniRAE 3000 equipped with a PID. As the affected soil was removed from the excavation, Jones personnel placed the soil on plastic sheeting for temporary storage until disposal arrangements were complete. On October 22, 2018, Wood personnel collected confirmation soil samples from the sidewalls (SW-1, SW-2, SW-3 and SW-4) and base (TB-3) of the excavation for analysis. The sample locations are shown on Figure 3 and the sample depths are provided on Table 1. The soil samples were collected manually by Wood personnel directly from the excavator bucket. To minimize the potential for cross -contamination, a new pair of nitrile gloves was donned for the collection of each soil sample. The soil samples were placed directly into laboratory -provided containers and placed in a cooler on ice for delivery to Con -test for analysis including VOCs (EPA Method 8260B), semi -volatile organic compounds (SVOCs) by EPA Method 8270 and MADEP Volatile Petroleum Hydrocarbons (VPH) and Extractable Petroleum Hydrocarbons (EPH). Based on the analytical results (Table 1), CLT personnel requested that Wood personnel return to the site on October 31 and November 1, 2018 to oversee additional removal of visibly -stained petroleum -affected soil from the excavation. A representative of Wood observed soil excavation and collected samples of soil from the excavator bucket and screened them in the field for VOCs using a Foxboro TVA equipped with a flame ionization detector (FID). As the affected soil was removed from the excavation, Jones personnel placed the soil on plastic sheeting for temporary storage until disposal arrangements were complete. On November 1, 2018, Wood personnel collected one additional confirmation soil sample from the base (TB-4-18, depth of 18 feet bgs) of the excavation for analysis. Groundwater was noted seeping into the base of the excavation at the depth of sample TB-4-18. The soil sample was collected manually by Wood using the same methods described above. The soil sample was placed directly into laboratory -provided containers and placed in a cooler on ice for delivery to Con -test for analysis including VOCs (EPA Method 8260B), SVOCs by EPA Method 8270 and MADEP VPH and EPH. M Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 E. EXCAVATION OF CONTAMINATED SOIL 1. Determination of the Source and Extent of Soil Contamination The results of the analysis of the sidewall and base soil samples were evaluated to determine the point at which soil excavation was terminated. The analysis of soil samples SW-1, SW-4 (depth of 10 feet bgs) and TB-4-18 (depth of 18 feet bgs) identified concentrations of petroleum constituents that exceeded the Soil -to -Water Maximum Soil Contaminant Concentrations (MSCCs) as shown on Table 1. None of the samples that reflect soil remaining in the excavation contained concentrations of petroleum constituents that exceeded the Residential or Industrial/Commercial MSCCs. The laboratory analytical reports and chain -of -custody forms are included in Appendix D. 2. Excavation Process The excavation process is described in Section D of this report. The excavated and stockpiled soil was placed into trucks and transported to Republic Services landfill at 5105 Morehead Road in Concord, North Carolina for disposal as non -hazardous waste. A total of 668.19 tons of soil was transported to the landfill for disposal. As of the date of this report, the excavation remained open. CLT is planning to retain services to perform backfilling of the excavation and appropriate compaction testing. 9 Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 F. CONCLUSIONS The Site is comprised of a small portion of Mecklenburg County Tax Parcel 115-211-03 which encompasses approximately 249 acres. The CLT Airport GADO Building and an adjacent auxiliary building formerly located at 5318 Morris Field Drive in Charlotte, North Carolina were recently demolished. A Topographic Map is included as Figure 1. An aerial photograph showing the location of the tank at the property is included as Figure 2. A site plan showing the depth and lateral extent of the tank excavation is included as Figure 3. None of the samples that reflect soil remaining in the excavation exceeded the Residential or Industrial/Commercial MSCCs. Because the analysis of soil samples SW-1, SW-4 (depth of 10 feet bgs) and TB-4-18 (depth of 18 feet bgs) identified concentrations of petroleum constituents that exceeded the Soil -to -Water Maximum Soil Contaminant Concentrations (MSCCs), it will be necessary to perform a Phase I Limited Site Assessment (LSA) to evaluate the groundwater quality at the former tank location. 10 Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 FIGURES [A IPA r' * of f S qW. i --iiY •• a �l J � L _ t y..� � e * i •' i I � F 0 500 1,000 2,000 F X Feetw. } f Copyriglta© 2013 National Geographic Society, i'cubeds o - SITE TOPO GADO Building woo5318 Morris Field Drive WD • Charlotte, North Carolina 2IL U W Q Area of Interest a 0 E PREPARED BY: LM DATE: 10/31/2018 CHECKED BY: RF DATE: 10/31/2018 PROJECT NO: 6228-18-0503 FIGURE NO: 1 �qw W.-* f iI ,a x E N x U c ci 0 10 20 40 21 Feet wood. MCLAk.graphic Inforr TANK LOCATION MAP GADO Building UST Closure Assessment 5318 Morris Field Drive Charlotte, North Carolina m Approximate Excavation Area Approximate Tank Location a E of PREPARED BY: LM I DATE: 11/16/2018 1 CHECKED BY: RF I DATE: 11/16/2018 I PROJECT NO: 6228-18-0503 1 FIGURE NO: CHAIN LINK FENCE APPROXIMATE EXTENT OF OUTER EXCAVATION (14 - 16 FEET DEEP) APPROXIMATE EXTENT OF INNER EXCAVATION (18 - 20 FEET DEEP) F- SW-2 TE�L_ 3 (14 FE SW-3 I TB- (18 FE I SW-4 UNDERGROUND STORAGE TANK (REMOVED) m ry U LL O Y U Q iW-1 m a LIGHT POLE m ry D U LL O w U Q LL O APPROX. LOCATION OF UST CLOSURE SITE PLAN ASSESMENT SOIL SAMPLE GADO BUILDING 5318 MORRIS FIELD DRIVE • APPROX. LOCATION OF CONFIRMATION CHARLOTTE, NORTH CAROLINA wood SOIL SAMPLE 77 PREPARED BY: SS DATE: 11/16/2018 CHECKED BY: RF DATE: 11/16/2018 PROJECT No.: 6228-18-0503 FIGURE No.: 3 File Location: P:\6228 Environmental\jobs\2018\6228-18-0503 GADO Building UST Closure\Cad\GADO Bldg — Fig 3 — Site Plan.dwg Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 TABLE J E N E U `j U o 0 W 0 v> 0 Ln 0 w 0 O 0 0 0 0 0 v 0 v 0 t0 O op 0 O O o O O M O v t0 v <O v <O ao N 0 O 0 O {p O M M M CO O O V 1� O at o ck p N N N Lo O f0 f0 f0 o 4 {'N7 N N a0 N N f0 N N N N a 2 a y � C G R C U O M t0 <O t0 OID p N N N 0 0 0 o M Q1 T T 01 p O W E N O O (n M w w w O r.- r O 7 to O N O M co a M Ql ar M o a - U Q N O O N' U) N D Ci 7 a-- D a R 00 w t w O0j N O O M C M N M wN ik Q d Y. o N Q Q Q Q Q Q Q co co Q Q Q Q Q Q Q Q Q Q Q Q Q Q O O O O N O Z Z Z Z Z Z Z M Z Z � Z Z Z Z Z Z Z Z Z Z Z Z Z M M n co pp Q) N_ N N N N N w w w w w p w w m ;oo _ Q O O O O O O O O O O O O O 7 7 7 GO 7 O O u r- Q Q m \ Q V p o a o 0 o p o o O V O V O V O V O V O O V O V O V y-, M Z Z F O O O O V V V o V V O h M 0 ry aD r o LO n O� M 0 O. u. co N M N co N co N M N co N M N co N M N (o O O O Q Q m F N V v r O O O o M O O O O O O O O O N V M Z Z p V V V V V V V V V o0 N O O) Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q O O colm 0 Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z � nj 00 O m O O) Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q Q O O 0 Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z Z N V N 7 O o N O o N O o N O o N O 0 N O o N O o N O o N O 0 N O o 7 O o ao0 M N N O V V N N N Q Q to v O O O O O O O O O O O O O O p� �j V V V V Z Z p v v v v v v v v v v v OD o 0 0 0 0 0 0 0 0 M N O 7 0 0 N 0 N 0 N 0 N 0 N 0 N 0 N 0 N 0 0 N N N N N N N N N N N N N N N N N N M Q Q fn p V 0 O V 0 O V 0 O V 0 O V 0 O V 0 O V 0 O V 0 o V 0 O V 0 O V 0 O V O V O V O V O V O V O V O V O V O V V V V V Z Z o Lo Ln U, Lo Lo U) Lo Lo 'o N? N M In 0 N 0 N 0 N 0 N 0 N o N o N o N o N o In o V N V N V N V N V N 7 N V N 7 N V N O D) O Lo Q Q > > fn p V O o V O o V O 0 V O o V O 0 V o o V 0 o V 0 o V 0 0 V 0 o V 0 o V 0 V o V 0 V 0 V o V 0 V 0 V 0 V o V V V V V Z Z � o 7 7 V 7 o 0 O �j C N U7 0 LL7 0 0 N 0 o N 0 0 N 0 0 N 0 0 7 0 o Cl) N Cl) N Cl)p N M o C p N N O M 7 v) Q Q to N p V p 0 O O O O O o o 0 o . 0 o O V O V O V O O O p c 0 n v I� N Z Z o o o V V V V O V N U fn C7 � 9 U H N T � () S] N 7 G a p c C E L L C7 O N N U 3 O a N Q` E m c m w o a U n o N u c u fn L O. R N _ a E O c N c N m C C 0 D 0 N f/1 m cc 01 o_ C d o _O ° v w° c v a� a a�i m o� 0 °� t ° r Q U — Q U m U m U m O o O R U H C N T >. .R. y N C N L3. L C T d R E a L d L �. L d 01 C O N L N L L 2 N E O E F f0 L C N C C ry N N Q W Q Q Q 01 C R y c L Y a > > a o N N H H n o f OQ a� U C m C> L T L ip Y w C N R N u o ao m a O N L O. m„ O 2o. O O. L.o o, 7 i0 C 47 _ E R N m R 0 2 0 L O- R N E N V L G. U to (J m U cn 2 0 N V m L N .L.. O cc Q Z v�i C C O O. W H �-- x VJ Q Q u- W N Z d d Q U Q U U U F (D O rn E E 0 0 d E 15 O o U a N m Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 APPENDICES Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 APPENDIX A LIQUID AND SOIL DISPOSAL MANIFESTS ry��ar 1A�! ,I kr +1I 1 j i 11 11 ��`` NONi H A C)U qiiicm EML WLA-roR LOGATI CIN !*fr31►�E 0RJC,INA-nNG ADDRESS MAILIING ADO RESS — + 'I# -if STATE—_ ZIF* clrr PHONE NO, COINTACTNAM 0ES. OF WASTF; 0UCLj4_jaj AAL. Al. fRIPTIO 7. PETROLEUA+IOONTA TWATER - OFF -SPEC LIGHT OIL, DIESEL OR GAS 3. NON-HAZARt US LIQUIDS 4- SEDIMENTORS01-I0 5. 55- ALLON DRUM REMOVED - SOLID OR EMPTY 6. 56- ALLON DRUM REMOVED - LIQUID 7. 13, i� 10. ARRIVAL TIME: DEPARTU E TIME: 4 *F,LAft.,+ Vq,L P "J 1`1" I#W, 14" , dL� YY[Y1iMti.6-14 rxr,tl°rls�r� -- 1'4,11rf. FWMFII "ti AA WVh ` NAur CITY PRONE No CONTACT NAMrz ED Ne ---`I "�oAxdT�Y- — - ---� i 4 GENERATOR'S ERTIFICATIOIN; I hereby certify that the above named material Is riot a hazardous waSte as defined Ly 40 CFR Pan 26'1 os a(�y apptilcabtie skate law, has t4� described, classified and packaged, and is in proper corOion for transportation according to applicable regulations- fienerakorl usiomer shall r6mburse t#f -MAT M Teasanabi and charges for handling, analyzing, loading, preparing, transporting. storing or caring for Donconfofming or -aRf spec waste. 5n iudinq casts of deconlami, gig afrd el a ing ci Generator must nc)tify HAZ-MAT of any charges to,,the waste strearrr prior to shipment. 1. . .-r.. 1g136M_ _ 3hIDr1'r Generator Auth-orized ent Name - —Section Ill. R HAZ,--MAT ENVIRONMENTAL SERVICES P.C). BOAC 37392 e CHARLOTTE, N.C. 28237 I. Driver hlameffitle �. Phone o- c, Tack No. lazardous Waste Transporter Permits :PA NCO0481461 70 THAN,.}Sr{ ICV,K {j)CRSml`a}rL'nI plerPji-di- nxporICr I cv, �':aeLs 1SrrLs rlr cu�rlPit LE IL-LL} f. Address - . h. Phone No. j. Transporler of Permit Nos. —� S#rapmeM Oats Driwarsi mare TRANSPORTER 11 Url�ar 5lgnalu�ti ;, r�fir 3'rr 1FIT I [' Il'�''i 4c`, on IV. • JL -LLJjL i 1 ih - t — - Site Name'. e: z-M B vlr nmen al ervl Ih sical ,address: 21Q Dalto AvenUe gharlo.tie.N.C. 0 a. Pylons No. b. Mailing Addfess: 1. Truck o. -- L Discrepancy Indica#ion Spat I�� atruda a + 4 lIL�1�d'J � 31r I�1�V NS �s to c ,* M al �s rr el ner ved fTwn aura IOMbUn been i and will be � �, � � �7� I l ot prope 690 �n�L l�U[%0j1 Rd Ce re blend 'info a � asbe fuel four Qse in large irldAM hurrw. � asw vm a mefl systems a� tiled fc E F.A' OW00 • Inc�MtMel f yelp into �e MUD sanita4on rawer system under permit IUP6012. (3) j4dg I) Our Inntrimt syrn oxiats on a first in, fli t oul basks mid "ct sfukl be prowaod within seven d • DATIE )Ni-H UAT AGNA7'UREOF FACIUTYAGENT -fkIOINAL t:INALT.S.i?. - VE LOV- 4i"=R f�ti REPUBLIC" SERVICES 4481214 NON —HAZARDOUS WASTE MANIFE;Coniners 1, Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generator's Name and Mailing Address 5. Generating Location (if 4. Phone ( ) 6. Phone ( ) ].Transporter#t Company Name 6,US EPA ID Number rter#1'a Phone 10. Transempr#2 Company Name 11. US EPA ID Number Transport Phone 13. Designated TI6ID Facility Name and Site Address 14. US EPA ID Number 's Phone GAII `D.Do moiB1 1111i. i. nl'^. 'Pi ,T.),i AH 4L{f! 16. Waste Shipping Name and Description 1]. Republic Services Appmvel A add Ex, ers 19. Total Pa. Unit Quantity WWoI r .r. TypeObil-Nlfaror-. ua$[nl ,i.I c ri.� iU:cb. Is b 6 do I /� �4 W if f� ^1 J I 21. Additional Descriptions for Materials Listed Above -- 22. Special Handling Instructions and Additional Information 23, GENERATORS CERTIFICATION: I hereby cehity that the above named material Is not a hazardous waste as defined by 40 state law, hasbeen properly described classifiedantl packaged, antl is In proper condition for transportation according to applicable regulations; ANeatment residue ofapreviously restricted hazardous waste subect to the Land Disposal ResMctions. I certfy and warrant that the waste has been treated e requirements of 40 Lanyicable CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261. Printetl/rypetl Name 6ignaNre Monrh Oay sear 2 24.Transporter IN: Acknowledgement of Receipt ofMaterials _ Prinled?ypsd Name Signature r- n4onln oay near O 2 h 25. anr#2 sporte: Acknowledgementof Receipt of Materials G Pr1nt irl'T pad Name - Signature r Monrh oay veer It 26, Discrepancy Indication Space /r r J_ Fadldry Owns'' Operator Certification of receipt Cl waste materials Covered by this promise[ (except as noted in Item 19) LL L2]. N - Prinied?ypetl Name ( 6lgnature y Oaf Yea. F TRANSPORTERdt1 NEOPMMMMW tREPUBLIC Zf SERVICES NON -HAZARDOUS WASTE MANIFEST 4481215 1, Generator's US EPA 10 Number Manifest Document Number 2. Page 1 of B. Generator'e Name and Malang Address Glwfbtle Uuugrn6 Nlfy+p(l SGaneratlng Location (if different) r / Tilll pYbNivi M.W.. 5i18 hkrNlBtlxW Dr. Gharkrlte. W.262M //' 1-h6110F1B. IVl. tBCNf1 :m al1ursv 'Ll .5%I l' 4. Phone( ) S. Phone( ) 7, Transporter#1 Company Name 8. US EPA ID Number 9. Transporter #1's Phone 10. Transpoder#2 Company Name 11. US EPA ID Number 12. Transporter#2's Phone 13. Designated PSM Facility Name and Site Atltlress 14. US EPA ID Number 15. Facility's Phone ll L®rlp9N 9I115 W rehiliW RO GLOL4l G. bill 211Y %US iS4 JOW X g67 16, Waste Shipping Name and Description 17. Republic Services AppmvalAaad Exp.Date 1S. Containers 19, Total 20. Unit Quantity WtAmi No. Type W Ni h4azermmun self 5010- a-i NJ) IW26,'19 �O R . b w 21. Additional Descriptions for Materials Listed Above -" 22. Special Handling Insimctions and Additional Information G 4kraW YJJ.S:i:)6 M. GENERATORS CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation a000Ming to applicable regulations', AND, if this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Reductions. I ci and warrant that the waste has been treated In accordance with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261. Pamed hyped Name Signature Monm Day year be 24. Transporter #1: Acknowledgement of Receipt of Materials F Printed/Typed Name Signature Mouth Day Yen, O a of25, Transporter #2: Acknowledgement of Receipt of Materials 2 Primedlryped Name Signal is Month Day Year da i_. _ 26. Discrepancy Indication Space T F J < 27. Fxclilty Owner or Operator'. Cepupation of receipt of waste materials covered by this manifest (except as noted'm LL Item 19) o +a: a M al, lIli l,L-t n..r 7. _n w!-2Lu4 I N H Printed?ypetl Name / Signature Monm ay/ vAsr TRANSPORTER# REPUBLIC' if SERVICES NON -HAZARDOUS WASTE MANIFEST 4481,216 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of ` 3. Gersho t(p9f� 55 ryrya E tl yy'ling Add e 5 �THi14�U LJO�)L n,i y!111_ea-il 5. Generating Local Iif different) . ._,.:,. ,u.. _. i.li"... 4. Phone( 6Phonel 1 9 Irmorporterlfl Company Name 8. US EPAID Number 9. Transporter k's Phone 10. Transpoherk2 Company Name 11. US EPAID Number 12. Transponder k2's Phone 13. Deaignated TISIO Facility Name and Site Address 14, US EPAID Number 15. Facility's Phone (NA, .S trtlflll 6 f LIS MCIF11EN6 m" f-coni. 4 2tiscry ,.I t t.,- 16. Waste Shipping Name and Description 17. Republic Services Approval Nand Ex, Data 18.Containers 19. Total did Unit peanut, WWOI V. No. Type Q b. 0 C/ J 21. Additional Oescilpticns for Materials Listed Above 22. Spai HanGling Instructions antl Additional Information di of .t.fil earl r 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste Ie a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I caddy and warrant that the waste has been treated in accordance with the requirements of 40 DEE 268 and Is n0 longer a hazardous .to a5 defined by 40 CFR 261, PrintedlTyped Name Signature mwm Day var ¢ 24. Transperterim Acknowledgement of Recelpl of Materials IW— PrintedlTyped Name Signature Month Oay Year ¢ 6 Z25,Transporter A2: Acknowledgement of Receipt of Materials 6 Prfnte yped Name - Signature Monm onyUp vm/ 26. Discrepancy Indication Space > F J Q20. Facility Owner or Operator Codification of receipt of waste materials covered by this manifest (except as noted In Item 19) LL N F Pdnted/Typetl Name � � Signature I_ .Iwnrn � Yev ✓ � 1 TRANSPORTE13#1 ���REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFEST = 4461217 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generator's Nams and Melling Address 5. Generating Location (if different) 4. Phone ( 1 6. Phone ( ) ]. Transporter #1 Company Name 8,US EPA ID Number 9. Transpoher#1's Phone 1O. Transporter H2 Company Name 11. US EPA ID Number 12. Transporter#2's Phone 13. Designated TIS/D Facility Name and Site Address 141, US EPA ID Number 15. Facility's Phone . ry Iso:11:. ;S:: lvl01 v tlt$reS lFit (. ..:.. .. ..... frh(, 16. waste Shipping Name and Description 17. Republic Services Approval #and Exp. Date 18. Containers 19. Total 20. Unit Ouantiry WWoI No. Type O 6 b. W W ('J 21. Additional Descriptions far Materials Listed Above 22. Special Handling Instructions and Additional Information 23. GENERATOR'S CERTIFICATION: 1 hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation accnrdlng to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I caddy and warrant that the waste has been treated in accordance with the requirements of 40 CFR 268 and Is no longer a hazardous waste as defined by 40 CFH 261, PrintedRyped Name _ _, Signature Monm oey veer Q 24. Transporter#1 Acknowledgement of Receipt of Mandate. i— Printed/Fyped Name $gnaWle con. Day Yea/ Q LL Ol 25. Transporter#i Acknowledgement of Receipt of Materials - 2 PrintebRyped Name Signature Monm oey veer F 26. Discrepancy Indication Space F J G27. Facility Owner or Operator Certification of receipt of waste materials covered by this manifest (except as rated in Item 19) LL 0 N F Printod?yped Name Signature Monlh pay_ ear GENERATOR'S COPY 90 'A REPUBLIC' > -� (� L �, SERVICES --I'� NON -HAZARDOUS WASTE MANIFEST= 44 8 218 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generator's No and Mailin Ail 5. Generating Location (if different) a.wtlo uouyte�Anpo 'ax Ra Mur... on, 5318 MorrWil Dr fharVil W. 2d2pR l.I1tlt10i1B. 14G [C21:iT /D4 :1ti'I UI:Stl /U4 aid I U lead 4. Phone l J 6. Phone( ) ]. Transporter #1 Company Name 6. US EPA ID Number 9. Transpoder#1's Phone f 1 D. Transxi42 Company amen 11. US EPA 10 Number 12. Tamperer#2's Phone 13. Designated TISID Facility Name and Slte Address 14. US EPA ID Number 15, Facility's Phone M5Landfill51o%MGrshaod Rd GORcad,Ni 2aoZ7 104 d12.2004 x 351 16. Waste Snaking Name and Description 1]. Republic Services Appmval#antl Exp.Date te.C.dMimers 19, Total 20. Unit ,.entity WWoI No. Type ¢ Non FWH1ldON6 SOU O 50iGleH1/91/ICr2blif ad b. ad W de 21. Addif at Descriptions for Materials Listed Above 22, Special Handling Instructions and Additional Information OW acct tr-J.fSJkJ 23. GENERATOR'S CERTIFICATION: I thereby certify that the above named material is not a resources waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packages and Is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance wtlb the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CPS 261. Prietedneyped Name SignisWfe uomn Cry Year as 24.Transporter #i'. Acknowledgement of Receipt of Materials w Punted?yped Name Signature Monts pay Year iT— Z25 Transporter#2 Acknowledgement of Receipt of Materials 1 Printed/typed Name ED Signature tat pay Y r �_. / 1 �� 26, Discrepancy ledicatido' pace J Q27 Facility Owner or Operator[ Certification of receipt of waste materials coveretl by Ibis manliest fexaept as noted In Item 19) o"Ni LANDI III ; ,_o m , t ,.. N F Printetl/fypetl Name �� Signature MonlF key Year t � �— TRANSPORTER#2 9WA REPUBLIC' :' SERVICES NON -HAZARDOUS WASTE MAN IFEST 448i219 1. Generator's US EPA IS Number Mani test Sediment Number 2. Page l of 3. Generator's Name antl Mailing Address 5. Generating Location (if different) _p.no" Onuyill"ujioit 5'f id iiwrrisk Ef. 5318 Morrlg{lpld Dr, ChaMld9, NC 2020R Ghe1,10i 1I 'di I(w Win may 7,ael d6t U 130 4. Phone ( ) 6-Phone ( ) 1. Transporter 11 Company Name 6, US EPA ID Number 9. Transporter#1's Phone 10. Transporter#2 Company Name 11. USEPAIDNumber 12. Transport 42's Phone 13. Designated T/S/D Facility Name and Site Address 14. US EPA IO Number 15. Facilitys Phone MA0 UntlfNl'1 bB IbretloYd Rd C:ViMgfd, NL 2do3S 11192-200A k ;f57 16. Waste Shipping Name and Desorption 1]. Republic Services Approval # and Ex, Sate 18. Containers 19. Total 2p. Unit quantity WWoI No. pe a. Non HBTArdoui Soli 5010.1&119i/ 101eryl9 b. 2 w z w (9 / 21. Additional Descriptions for Materials Listed Above 22. Special Handing Instructions antl Additional Information NN ecaslblaiba5 23. GENERATORS CERTIFICATION: I hereby certity that the above named material Is not a haurdous waste as defined by 40 CPU 261 or any applicable state law, has been properly described classified and packaged, and is in proper condition for transportation awarding to applicable regulations; AND, if this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certity and warrant that the waste has been treated In accordance with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 GFR 261, Printed/Typed Name Sgni Di Day year 24. Transporter dl: Acknowledgement of Receipt of Materials F Printed?yped Name Signature Moth Day t r 6 _ op 25. Transporter 42. Acknowledgement of Receipt of Materials 2 QPrated/Typed Name Signature Mw0 Day year F 26-Discrepancy Indication Space Q21. Facllly Owner or Operator Gerti0da0on of receipt of waste materials covered by this menlfast (except as noted In Item 19) O Gull LANItI-ILL F Pdnted?ypad Name ^ Slid ture Monty Day Y r TRANSPORTER#2 I ��i REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFEST 4481220 1, Generator's US EPA ID Number Manilest Document Number 2, Page 1 of 3. General r s Name and Mailing Address 5, Genefafing L0pa11on (it different) r o funip" opowWY Allwrt FV,ze 0.MA lln t0 Ln 5318 A1DrrhReW CA GAa n\1rte. elk ZAe 0,,1 Ltma GE. taC- 2+}21ffl nar u_ 4. Phone ( ) 6. Phone ( 1 >. Transporter Nl Company Name 8. US EPA ID Number A. Transporter G711',nc 10. Transporter N2 Companytiama 11. US EPA ID Number 12Transp0rer k2'e PM1pne 13. Designaled TlSA) Facility Name and Site Address 14. US EPA ID Number 15. Facility's Phone t MLS LSi MR S l Ob MRr611B8d NO GOn"fia, NL 2B I 1114.7a, vassal % Al 16. Waste Shipping Name and Description 17. Republic Selvlces Approval"no Exp. Cate t8. Gan\miners 1st. Total 20. Unit Quantity W1,V01 — — o. Type a, Cc rVUR h1r1[B 3 iniguil0Y SI114 ib-1Id /111T.'2Lv IR O Q b. W W C0 a 21. Additional Descriptions for Materials Listed Above - 22. Special Handling Instructions and Additional Information Idll ®I.iAA3.i.3J:iF! 23. GENERATOR'S CERTIFICATION: I hereby carify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation aseeming to applicable regulations; AND, it this waste is a treatment residue of a . previously restricted hazardous waste subject t0 the Land Disposal Restrictions. I parity and warrant that the waste has been treated in accordance with the requirements of 40 CFR 268 and Is no longer a hazardous waste as defined by 40 OFR 261, Printed/I'yped Name Signature Mon. Day Yeai J r i T 24. Transporter 91 Acknowledgement of Reaelpt of Materials FW. Printedri Name Signature Man. tray, Year 0 25. Transporter 02'. Acknowledgement of Receipt of Materials - 2 ¢ Parted?yped Name — 5G,❑6Wre Monts Oay Year 6. Discrepancy Indication Sliece T F J La 27. Facility Owner ar Operator: Degradation at receipt of waste materials covered by this moue t (ex¢epr as rabbis Item 19) LL � JMS L4NliriLL 6iidr FA(Iitr.H4AC) Hp t v , - , r_ ...,... e„ N F Prin\etlRypetl Name �1/ Signature � Monm Oay Yee. TRANSPORTER#2 ���REPUBLIC`�/���! �) SERVICES NON -HAZARDOUS WASTE!MMANIFEST 4481221 T Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generate, s Name and Malling Addriaks 5. Generating Locafon (If dlfferem) i. Jar teryIm F 53fd Fdomisfleld far ,"..rout, l.'4.'Ri ..T- 4. Phone ( 1 6. Phone ( ) >. Transporter#1 Company Name S. US EPA ID Number 9. Transporter #1'a Phone 10. Transporter#2 Company Name 11. US EPA ID Number 12. Transporter#2's Phone 13. Designated TlStD Facility Name and Site Address 14. US EPA ID Number 15. Facility's Phone r. unsung 5LkRy Mafelxraa tea GAfr.Gld, pi im.—i 16. Waste Shipping Name and Description 17, Republic Semcas Approval# and Exp. Date 13.80ntainers 19, Told 20. Unit Quantity WWol .r . e .. N0. Type a rK,n IstneRra0tt4 Kvn -Vftl Il, v_.i rfp<n 15 0 b. w of \ Ca l 1 21. AddlHDnel Descriptions for Materials Listed Above 22. Special Handling Instructions and Additional Information can aruall fz iUS 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 Or any applicable state law, haz been properly described classified and packaged and is in proper condition for transportation according to applicable regulations; AND, if this waste Is a treatment residue of a previously restricted hazardous Waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements of 40 CFR 268 and Is no longer a Leapfrog waste as defined by 40 CFR 261. PMteday ed Name Signature Mont Oey Y r, ¢ 24. Transporter 01. Acknowledgement of Receipt of Materials pu Pdntetl/TyPed Neme 3lgnwere Monty Oay Year be of25.Transporter ID: Acknowledgement of Receipt of Materials < PdntedRyped Name I Signature / col 0, Yee, 26. Dearer Indiee can Space F Q9. Facility Owner or Dperator: Certification of receipt of waste materials covered by this manifest (except as noted in Item 19) w N PrintedRyped Name 1 _l Signature rtaonm._ On TRANSPORTER#t N REPUBLIC' SERWCES NON -HAZARDOUS WASTE MANIFEST 4 4 81 ^ ` 2 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 9. Generalllr%Mail A 6. Generating Location (t different) r�?:1 it FMrff141Wb CF Li KJ Kdaij, f*, :6,:YJ i'.I4 ¢.I rrt ul 4. Pbon6 ( ) 6. Phone ( ) ]. Transporter #1 Company Name 8, US EPA ID Number 9. Transporter A's Phone 10. Transporter #2 Company Name 11, US EPA ID Number 12. Transporter#2'c Phone 13. Deslgnated T/S/D Facility Name and Site Address 14. US EPA ID Number 15. Facility's Phone - MS :Dltclui b1ty, (NIGfGhdRO I (.cmcolu. tail- z6DW 1 ;..+: -, . 16, Waste Shipping Name and Descnption 17. Republic Services Approval #and Este Date 18. Containers 19. Total 20. Unit Ouantiry WWol �•rvrcw ,a No. Type ad 14U.; 1'N{s'alr4DL1 "416 Q 6 b. W M W C i 21. Atltlitional Descriptions for Materials Listed Above - 'j. 22. Special Handling Instructions and Additional Information r tail a,",l J401f 23. GENERATOR'S CERTIFICATION: I hereby certity that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state of has been properly described classified and packaged, and Is in proper condition for transportation according to applicable regulations; AND, It this waste is a treatment residue of a previously confirmed hazardous waste subject t0 the Lend Disposal Restrictions. I certify and warrant hat He waste has been treated In accordance with the requirements of 40 CFR 268 and is n0 longer a hazardous waste as defined by 40 CFR 261. ,. Printed/Typed Name _ Signature Month pay Yoar 24, Transporter Ill Acknowledgement of Receipt of Materials f firmetl/Fyped Name Signature Month Oay Year Q O 6 26. Transporter #2: Acknowletlge em nt of Receipt of Materials Z Printetl?yP tlName Signature Madre oey ter ,(' E_ �� iJ _z/ 1 - 26 Discrepancy' Indication Space - _ i F J_ 2]. Facility Owner or Opzmtor'. Cedlflcation of receipt of waste materials covered by this manifest (except as noted In Item 19) O N Printetlltypetl Name' ~ r Signature _ ManN pay 1 r / II / / TRANSPORTE11#1 It?REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFEST= 4481223 L Generator's US EPA ID Number Manifest Document Number 2. Page 1 of Generators a and MalmgAdress L.hJr alb l.or a A IPDIt 5318 Moniallskl Dr k,h rh011 NC 28208 nw e61 Vl:m Phone ( Tamperer 41 Company Name 10. Tranepmter a2 cempacy Name 13. Designated T/S/D Facility Name and Site Address Ma Landf111 5105 Morehead Rd Cahoot NC 28M7 NOR Hazardous &A cherw", W. 28208 Ili J6101N 6. Phone ( ) IS EPA ID Number 9. Transport 41's Phane US EPA ID Number 12. In ..punt 's Phone US EPA ID Number 15. Facility's Phone IOa782.1004 X 367 Republic Services Approval band Exp.Date 16. Containers 19. Toi: Our . No I Type Ic"M 1aa NJ bNl acccY3a3858 23. GENERATOR'S CERTIFICATION: I hereby cedity that the shove named material Is not a mourners waste as defined by 40 CFR 261 or any applicable state law, has been properly described classified and packaged, and Is In proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Formation, I cedify and warrant that the waste has been treated in accordance with the requirements of 49 CFR 263 and is no longer a hazardous waste as defined by 40 CFR 261, Printed/rypel Name Signature mono No ffiar Q 24.Transporter #1: Acknowledgement of Receipt of Materials f Prinied/fyped Name Signature -- fort oey—Year 2 25. Transporter#2: Acknowledgement of Receipt fMaterials -��- Prinied/iypetl frommi Signature Men. Dey Year 1- 26. Di.rdpenhy Indication Space f J LL2. Facility Owner or Operator: Cortifateriaie leatlon of receipt of waste mhavered by this memmot (except as noted in Item 19) o CM5 LANUFiLL 31rm ii Inv 1;vk 1k, V_. .elux- III e,...., w F Printetl/fypetl Name ^ Signature McnrnT,Dar IY,Tr TRANSPORTERR2 W REPUBLIC` SERVICESREPUBLIC' NON-HAZARDOUS WASTE MANIFEST= 4481224 1. Generators US EPA ID Number Meniteg Document Number2, Page 1 of 3. Gener"wia Name g aDad" 5. GepeldtO yy�� ryryIl Ktw 11 different) tl Yaw MII(a>fl Mpr 5318 AA0rF10111tl uF. Chaplet t0, M. 2820N GinarmllS, NL. 2EVOR /IM an ill. )pal A6I Dl,1N 4. Phone ( 7 6. Phone ( J ]. Transporter #1 Company Name 6. US EPA ID Number 9. Transpmtar#t's Phone 10. Transporter#2 Company Name —� 11. US EPA IDNumber 12, Transporter#2'a Phone 14, US EPA ID Number 15. Facility's Phone 13. Designated T/SID Facility Name antl Site Atltlress AA3 Lantlllu btd5 Abretreati fatl aancukG. fN(: 28Ue 7 I(rt. /Reltxla x 3s 16. Waste Shipping Name and Description V. Republic Services Approval # and Exp. Date 18. Containers 19. Total 20. Unit Quantity Stolen No. Type a. Q 1-1.—G1N(WUw 50N $(11f}itl-IiVti 16126i IM O It b. w ad C�,� U 7) 21. Additional Descriptions far Materials Listed Above 22. Special Handling Instructions and Additional Information Al accEfa335MA 23. GENERATOR'S CERTIFICATION: I hereby eedify that the above named material is not a hazardous waste be formed by 40 DER 261 or any applicable state law, has been properly described, classlled and packaged, and is in tamper condition for transportation according to Callaway, regulations; AND, if this waste is a treatment residue of a previously postponed hazardous waste correct to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements of 40 CUP 268 and is no longer a hazardous waste as defined by 40 DER 261. Printatl?yped Name Signature boom Day veer 24.➢ansporter Bt'. Acknowledgement of Receipt of Materials PrintetlRypetl Name 6ignature Memo dry 'oar 04 _ _ Transeorter#2'. Acknowledgement of Ramuptef Materials - --� Z25. QPdnletl/Iyped Name Signature Monitl pay Des F ` 28. Discrepancy Indication Spade J Q27. Facility Owner or Operate, Certification of receipt of waste materials covered by this manifest (except as noted in item 19) LL CMa iANl1GILL hnT Mk-rnL r:I tu: rn/li.kili,,, M. d4i IluLii ;-tea„ I no � N F Printetl/rypetl Name Signature TRANSPORTER #2; V �Rii REPUBLIC" C SERVICES NON -HAZARDOUS WASTE MANIFEST 4481''J 1, Generator's US EPA ID Number Manif.d Document Number 2.Page1 of 3. Generator's Name and Mailing Address 5. Generating Location (if different) Gni rbW Gouptas Airport �e iAottisrrlo in 6316 MUIIKiii ik CCnaRnl(b, fir, 28Zfl3 4. Phone( Charlotte, INC kW08 the and D'IJN .ao, Phone( 1 /U..lbr irl 11 ]. Transporter #1 Company Name 8.US EPA ID Number 9. Transporter #1's Phone 'J 10. Touchagar#2 Company ame 11. US EPA ID Number 12. Transporter#2's Phone 13. Designated TISID Facility Name and Site Address 14. US EPA ID Number 15. Facility's Phone NIS LantliP151(di Martinelli Rd Comoro, I is 2a92I ; Is iu 2W4 A it 16. Waste Shipping Name and Description 9. Republic Services Approval#and Exp. Dale 18. Containers 19. The 20. Unit Quantity Will No. Type print opttu Rum nuav o¢ 6 b W 2 W f9 ezk 21.Addtlional Descriptions for Materials Listed At.. 22. Special Handling Instructions and Additional Information fill aWQr4&3M* _ 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of previously restricted hazardous waste subject to the Land Disposal Restrictions. I merry and warrant that the waste has been treated In accordance with the requirements of 40 CFR 268 and is no longer a hazalance waste as defined by 40 CFR 261. Rd teall ped Name signs re month day v r ¢ 24, Transporter #1'. Acknowledgement of Receipt of Materials F Printed/ryped Name Signature Mon. Day veer g M 25. Transporter 92. Acherbudedgement of Receipt of Materials Printed/rypetl Name Signatwe Mon. day Year f- 26. Discrepancy Indication Space F J Q 27. Facility Ownef of operator: Certireopen of receipt of waste materials covered by this manifest (except as noted In Item 19) LL (.MS IANUHLL 61 W MldtEY EALi t<(11. NV V it . rp., ; .. r r c-! U[-lUr+ ,.. .1-, N F Primemryped Name Signature nth day Y tE TRANSPORTER#2 mmmiWifd ICT SERVICES NON -HAZARDOUS WASTE MANIFEST 4481164 1, Generator's US EPA ID Number Manifest Document Number 2. Page l of 3. Generator's Name and Mailing Address 5. Generating Location if different) C.Imi DIJA Dougil All Wig mcdotielo Ce, 6516 Mforrwwld br. c`.M1erRrtlp, MC 282M 4. Phone ( C'Re eitE. NL 4dj /W Ant 01as 6. Phone( ) 7+?t do I O136 7 Transporter 91 Company Name 6, US EPA ID Number 9. Transporter #1's Phone c — 10. Transpoher #2 Company Name 11. US EPA ID Number 12. Transponer#2's Phone 13. Designated TISI) Facility Name and Site Address 14. US EPA ID Number 15, Facility's Phone k Arts LOndfIN 5105 Mk refleed NO COrrl:ar0, NL 281 1G4.hk J0G4 r fb , 18. Containers 19. Total 20, Unit 16. Waste Shipping Name and Description 17, Republic Services Approval # and Ex, Data Quantity WWol No. Type Alp 1n bdow Earn Detrw a a b as up w C� tD � —L_ 1 21. Atldhional Descriptions for thermals Ludd Above 22. Special Handling Instructions and Additional Information did eDC4433SIS5 _ 23. GENERATOR'S CERTIFICATION: I hereby cdi that the above named material is not a hazardous waste as defined by 40 CFR 2fi1 or any applicable state Is has been properly described, classified and packaged, and Is in proper condition for transportation according to applicable regulations', AND, if this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I both, and warrant that the waste has been treated in accordance with the requirements of 40 CFR 268 and is no longer a hszardens waste az defined by 40 CFR 261. Printed/Typed Name Signjatu e Monlll lay on, ¢ 24.Transporter#1'. acknowledgement of Receipt at Materials W "coned7y,graiLlsaoff, Sighawre Month Day over y S w 25. Transpo r ant of Receipt of Materials ' 2 —. 2 Parini ?yped Name Sgrlature Muntn Oey year 26. Discrepancy Indication Space Y F J Q27, Facility Owner or Operator Cedlfication of receipt of waste materials covered by Nis manifest (except asnoted in Item 19( LL GMSIANUF(LL51WMOREHEAGnf)C t4GLit, tie. tlul[i itw/U2-duu r.:ro� N h PrintetlRypetl Name Signature -of ay TRANSPORTER#2 REPUBLIC - SERVICES NON -HAZARDOUS WASTE MANIFEST= 44E1165 I Generator's US EPA 10 Number Manifest Document Number 2-Page l of 3. Generator's Name and Mailing Address 5. Generating Location (If different) t ito"o{tb Lsto'gal'rn"! l !, iP, vaon r'i, I V! r;;tR Mnr+51ke4:i UP 4. Phone ( gyoll C, i 11. /11Ud 01 .31 6. Phone ( ) I. Transporter #1 Company Name I 8. US EPA ID Number 9. Transporter#t's Phone ifs 4, 10. Transporter#2 Company Name i 11, US EPA ID Number 12. Transp0her#2's Phone 13, Designated T/S/O Facility Name and Site Address 14. US EPVD Number 15. Facility's Phone I LtifWMI 61 U' 440errtr3l Do C,, g.r N.iI ol7 16. Waste Shipping Name and Description 17. Republic Services Approved #and Exp. Date 18. Containers IF Total 20. Unit Guandry WWol No. Type i C. o. ➢W G%(H' I K IyOtI P1n2SA WtlE :41t �i}PJ-Itl-IiN/I}�vr_ to ad W 7 ad 21. Additional Descriptions for Materials Listed Above 22. Special Handling Instructions and Additional Information r. " ad,, 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and Is in proper condition for transportation according t0 applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous wage subject W the Land Disposal Restrictions. I early and warrant that the waste has been treated In acescis ce With the peritoneums of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261. Pnnterl/Fypetl Name Signature Monty Day Y r M 24. Transporterld Acknowledgement of Receipt of Materials ad Pdnted?yped Name . S nature Mn rh Day Year a cknowl dg t of Receipt of Materials of 25. Threasportsirl: Acknowledgement + 2 Printad sed rl Monslt Day Y. 2, Discrepancy Increases Space Y C J u9. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except as noted in Item 19) N F PpMed/ryped Name ightfu rn Day G-' TRANSPORTER41 REPUBLIC' D SERVICES NON -HAZARDOUS WASTE MANIFEST 44$1166 1. Generator's US EPA ID Number Manifest Document Number 2, Page 1 of 3. Generator's Name and Mailing Address 5. Generating Location (if dlfferbnt) (.Mlblle hat(Qui ArtpOft Oftb ,n 6818 trbnlalMll N. Oiler es", NC 211%...,. 4. Phone ( q0tialle• NC 2&08 rEa zn Drab 6. Phone ( 1 7. Transpoder#1 Company Name 8. US EPA ID Number 9. Tmnsponir#1'a Phone l l)` 10.1 nsporter#7Compd Name J 11, US EPA ID Number 12. Transporter #2's Phone 13. Designated T/SID Facility Name and Site Address 14, US EPA ID Number 15. FadlLLy's Phone " Mai Lanst 6 Y06 MGtersi etf Rd "noccol. et 2&027 N4..IF2.<q14 X 361 16. Waste Shipping Name and Description IT Republic Services Approval#and Exp. Date 18. Containers 19. more 20. Unit Quantity WWDI No. Type dlN l(I(MIIW I-W IIIIMOW -- — I 2 I O 6 b. ad W be W !J 21. Atltlitional Descriptiona for Materials Listed Above - 22. Special Handling Instructions and Additional Information uW 1101"333669 t' 23. GENERATOR'S CERTIFICATION: I hereby pacify that the above named material is not a hazardous ..to as seemed by 40 CFR 261 or any applicable Mete law, has been properly described, classified and packaged, bad is In proper condition for transportation according to applicable regulations) AND, It this waste is a treatment residue of previously restricted hazardous waste subject to the Land Disposal Restrictions. I partly and warrant that the waste has been treated In dependence with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261. PdntedRyped Nang Signature - Monet Day Yon, ar ; 24. Transponder #1: Acknowledgement of Hecelpt of Materials CPrinted/Type Name SignaWre Fbnm Day Year O / �ledg M 25, Titter #2: meht of Receipt at Materials 2 Printed?yp/d NamB & Mre Monet pay Year F' l �C 26. Discrepancy Indic ion Space - J Q9. Facility Owner or Operator'. Ceddicatioo of receipt of waste materials covered by this manifest (except as noted in item 19) - LL �_ lifrlJ UlfiilYl(L :Ii1k5 fVM1XlEfltitll t(II V./Y\ (il, tyl, Arnie rUrL%fI<-MW A.1Dr N F PriniatlRyped Name / Signature /� Monet pay Ye I L / TRANSPORTER#2 C���A REPUBLIC"ys 1r A SERVICES NON -HAZARDOUS WASTE MANIFEST 4481167 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of S. Generator's Neme antl Mailing Atldress 6_ Generating Location I different) _ �.nprkrue WlldtaN An):•oi t whiddi Or 4. Phone ( f-iwaoGe. �.'. ehalb nw wr nl._, 6. Phone( ) 7rter#1 Company Name _ t 8, US EPA ID Number S. Transponerllt's Phone 10, Transporter X2Company Name 11. US EPA ID Number 12. Transporter 41 Phone 13. Designated TISID Facility Name antl Site Atldress 14. US EFAd. Number 15. Facility's PM1one M. Legal NfOIerNNtl F.d tiAnr.Lru, iVl. 1[t1117 IJA il:;i dLi A Jet 1fi. Waste Stripping Name antl Dascriplion 1]. Republic Services Approval# and Exp. Date 18. Containers 19, Teter 20. Unit Quantity Weal No. Type O a 1tl(+I1 1 Id211IWU6 bUl1 CUiJ I of rWGcii1 b. w up S p. J ) / 21. Additional Descriptions for Materials Listed Above 22 Special Handling Instructions and Atltlitionel Information fors attx �Yib5n 23. GENERATOR'S CERTIFICATION: I hereby codify, that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I codify and warrant that the waste has been treated in aaordancs with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261. PrinteorTyped Name Signature Mrvrr6 pay Yaar ¢ 24, Transporter #1: Acknowledgement of Receipt of Materials PrictiallName Signature...�-- Idanm pay v r O --.._ of25. Transporter n: Acknowledgement of Pare of of Materials a ¢ PrintedR pad Neme V SignaWre Monrn pay Year F i 26. Diserepasay indication Space F J G27. Facility Owner or Operator Ceniflcation of receipt of waste materials covered by tM1ls manifest (except as notetl in Item 19) LL O N F Printetl?VPad Name 6l,nature� n, her Yea I/Vt TRANSPORTER#1 REPUBLIC'^ SERVICES NON -HAZARDOUS WASTE MANIFEST M 4481i68 1, Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generator's Name and Mailing Address S. Generating Location (if different) tenanted Lovifilaa ASl Pf 10 hen of W 'A 6316 Monldlald Dr. 1.1.41sapa, W, 2WOa 4. Phone( gWr6 a, NC 2520s /(M:3N1Oim 6. Phone l ) /O"')Ial UI:f€1 T. Transporter #1 Company Name S. US EPA Ip Number 9. Transporter #1'a Phone Tc _ 10. Trransporcer Co ame J 11. US EPA ID Number 12. Transporter #2's Phone 13, Designated TIS/D Facility Name and Site Address 14, US EPA ID Number 15. Fadlity's Phone i li Landfill 5105 Abfallead lid Conill NC 2"7 /Oq./ll 2534 x'36! 16. Waste Shipping Name and Description 17. Republic Services Approval A and Exp. Date 16. Containers 19. Total 20, Unit Quantity WWOI No. T pe 9Ad XI F✓ Yd it] Oydee K O 4 b III W 2 21. Additional Descriptions for Materials Listed Above 22. Special Handling Instructions and Additional Information BW aml i.1365U 23, GENERATORS CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, It this waste is a treatment resitlue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certity and warrant that the waste has been treated In accordance with the requirements of 40 CFR 266 and Is no longer a hazardous waste as defined by 40 GET 261, Printetl/fypd Name Signature,f Monm oay v.=: 24.Transporter#1: Acknowledgement of Receipt of Materials �. to Printed yp tl Name Sign oay Yeer �— /tyrervronm pi as 25. Trans orter#2: Ac owletlgemant of Rewip[of Matenals 2 Printed/typed Name Signatme Monm pay ven: F 26, Discrepancy Indication Space Y F 4 27. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except as noted in Item 19) LL GM5 LANDFILL Rich MCnitnHLAG RU s,,ACAfiRif Iw 2ixiY: AAEU52-[ li A.1Ri As F Prinled?yped Name ) Signature M nm Day vea:. TRANSPORTER#2 5;W REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFEST, I Generator's US EPA ID Number Maniteat Document Number 2. Page 1 of _ 3. Gene t N ntl M I g Atltlress 5 Ge e2ting LocaYon(t tlifferent) ¢sir A 1 CN t re"'14Ri be ?W2 4. Phone ( 1...... e. Phone ].Transporter at Company Name B.US EPA ID Number 9. Transporter#1's Phone 10. Transporter#2 Company Name 11. US EPA ID Number 12. Transporter 42's Phone 13. Designated TISID Equably Name and Site Address 14. US EPAiD Number 15. Facillty's Phone I. FRlI Fh O riiY MOURNell 411(_p:u Ct fib l,VeI 16. Waste Shipping Name antl Description 17. Republic Services Appmval#and Esp. Date 1B.Centainers 19. Total 20, Unit Quantity WWOI Nc. Type _ is 'is be O (vPh Kd2bfU(NiOtl biilel NSf r4(r i4110 i9 b. W Up W L. 21. Additional Descriptions for Materiels Listed Above 22. Special Handling Instructions and Additional Information 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 SEE 261 or any applicable state law, has been properly described, classified and packaged and is In proper condition for transportation according to applicable NAUiations; AND, if waste is a treatment residue of previously restricted hazardous waste subject to the land Disposal Restrictions. I certify and warrant that the waste has been treated In accordance with the requirements of 40 CFF 268 and is no longer a hazardous waste de defined by 40 CFR 261. Prinied?yped Name Signature Monm oey Year 24.1ransporter8l: Acknowletlgement of Receipt of Materials IW- Printed/typed Name Signature - —" '-- Noah ady her O_...� I b�mi__Lc ""--' 11 �'I W 25.TransporterN2: Acknowletlgement of Receipt of Materials Q Prinied/trP dl�afne Signature Per M•(�/ '.. '�` f /Y rW'N� J C 26. Discrepancy IndLCetion Space F J Es LL 27. Facility Owner or Operator'. Certification of receipt of waste materials covered by this manmet (except as noted in 119) Es N F Printetl/typed Name Signature M qey IM 5Y TF TRANSPORTER41 C��REPUBLIC SERVICES NON -HAZARDOUS WASTE MANIFEST= 4481173 1. Generator's US EPA ID Number Manifest Document Number 2. Pass 1 of 3. Generator's Name and Mailing Address 5, Generating Location iif different) 0wrii DorgNa AflW W 16 Mwff it Or. Ill Mlnrrflllil Br. Chor sal NC 20206 4. Phone ( Cp1aMW. NC 28206 /w Ant (If N 6, Phone ( ) 104 361 0139 ]. Transporter #1 Company Name 6. US EPA ID Number 9. Transporter or's Phone 10. Tr`alispoddr 42 Dow my Nam 11. US EPA ID Number 12. Transpoder#2's Phone 13. Designated T/SID Facility Name and Site Add.. 14, US EPA D Number 15, Facility's Phone M$ Lignoll 5109 Murano w Rd Igor w, WC 2BOd 7 IN NA) 2004 X ae? 16.Containers 19, Total 20. Unit 16. Waste Shipping Name and Description ITRepublic Services Applovel#and Exp. Date Quantity wwol No. Type lim In Ill Fri In below It 0 a b. w w izI v 21, Additional Descriptions far Materials Uptetl Above 22. Special Handling Instructions and Additional Information coal accI133:3659 23. GENERATOR'S CERTIFICATION: I hereby cedity that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable gate law, has been properly described classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been hosted In accordance with the requirements of 40 CFR 266 and is no longer a hazardous waste as defined by 40 CFR 261. Printed/Typed No a Signature ,, Month Day rear . 1. — ErJ -.1 IJ IL 24.Transporter %1: Acknowledgement of Receipt of Materials W PrW[ed/ryped Name 0 SignaWre _ Moom pay veer _ d 2 In 23.-ran arter e2:Acnowledgement of Receipt of Materials QPre intd?yped Name $,,note. Month pay Year F 26. Discrepancy Indication Space J Q 2]. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except es noted In Item 19) LL GAS LANDFILL 5iub Mih26 ' L D cjy i )RR NN, del / r w-r --iiMe A Job Vi F Printemryped Name Signature _ 7 Oa 7 TRANSPORTER# `2 REPUBLIC' Y SERVICES NON -HAZARDOUS WASTE MANIFEST 4481174 1, Generator's US EPA ID Number Manifest Document Number 2. Page 1 of �3. Generator z Name and Maling Address 5G ailleg Location (if different) r l AUdWx PXjIpR Mot!mh 1./ 53 1 AMr mw wrx frae ING wt'. a _ ._ 'I'm J IJL-I J'l ur L 4. Phan6( I 6 Phone ( ) ].Transporter #1 Company Name 8. US EPA ID Number 9. Transporter or's Phone 10. Transpoder#2 Company Name .i 11. US EPA ID Number 12. Transporter Asia Phone 13. Designated TIS/D Facility Name and Site Address 14. US EPA ID Number 15. Facility's PM1one andlt, 151011AURstmp6 iiQ._mK.Oftl_ PIL, 80,7 , )'..g 16. Waste Shipping Name and Description 17. Republic Services Approval # end Eep. Date 18. Containers 19. Total. 20. Unit Quantity wwal No. Type aYi Is owns,nl pl lWl.Yi 2 O IVQp N'ii2G1(N!rY JUN ne I i I!:/ IIll l.Pttl b W / 21, Additional Descriptloos for Materials Listed Above Ito Special Handling Instrudlons antl Atltlitlonal Information 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous Waste as defined by 40 CFR 261 or any applicable state few, has been properly described, classified and packaged. and Is In proper condition for trensporlation according to applicable regulations; AND, If this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions, I hardly and warrant that the waste has been treated In accordance with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261. Printetlllyped Name Signature ` MwM Oay Year _ C 24, Transporter #1'. Acknowledgement of Receipt of Materials _ F Pllntetl?yped Name Signal are` - Mon In Oay Year K 2 25,Transporter 62', Acknowledgement of Receipt of Materials F Pi Yp9tlrvame $igadtpr¢ Month Day gear J/ / 26, Discrepancy indication Specs I / r / r C J LL27. Facility Owner or Operator Certification of receipt of waste materials covered by this manifest (except as noted in Item 19) n F Pnntetllrypetl Ndm¢ Signature Monrh y / TRANSPORTER M 1 REPUBLIC Z� SERVICES UBL NON -HAZARDOUS WASTE MANIFESTM 4481175 1. Genaraior's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generator's Name and Mailing Address 5. Generating Location (it different) / — ,.narNribDDugltuAlfpDll 63 id Mbrrafeb L. 4)18IAorrklMb d. Ctwrlofc. NC 2111 4.Phanel (ts uitt Ul:fS 6. Phone l ) XA.ifir Uj Jy ]. Transporter#1 Company Name 8. US EPA ID Number 9. Transporter#1's Phone ly i 6. Trenspo ei#2 Com Name _1 11. US EPA 10 Number 12. Transporter 42's Phone 13. Designated Tl$ID Facility Name and Site Address 14, US EPA ID Number 15. Facility's Phone V.S LartU(1115'105 AbreRBiU HO Cooled NC <1102i rU4-ill 2Q04 k 361 16, Waste Shipping Name antl Description 17. Republic $ervle¢s Approval#and Exp, Date 18. Containers 19, Tend 26, unit Quantity vil Na. Type III m f1Bl01Ar r in In OAarw O m _ ad Z ad r 21. Additional Descriptions for Materials Listed Above '1 22. Special Handling Instructions and Additional Information _ ON iccL#333669 23. GENERATORS CERTIFICATION: I hereby c und, that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, class fled and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Ricandrions. I certify antl warrant that the waste has been treated in accordance with the requirements of 46 CFR 268 and Is no longer a hazardous waste as defined by 46 RFR 261. Pi ated/ryped Name Signature )� Monrh Oey Year _ _Sl r� do 24.Transporter Ill: Acknowledgement of Receipt of Materials F Printod?ypad Name - - - Signaure HbnM Dax ✓ r as 25 Tra p had u2 Acknowledgement of Receipt of Materials _ 2 Printetlrtypetl Name Signa�ur�-- yarn Day Year 1- S I 26, Discrepancy Indication space a I- J Q2. Facility Owner or Operator: Certification of receipt of waste materials covered by u11s manifest (except as noted in LL Item 19) GM5 LANDFILL ndu AhD RD C)NI jw. 114¢ ?iro-; ern z us I .a, N F Firm ed?vped Name Signature M Day V TRANSPORTER R2 REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFESTM 4481203 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 Of 3. Generator's Name and Malling Address Location (If different) 1.P101W110 UOUj Hdl,rtd ]5Generating (.$1 F. IAorcllnuttl ... GiIHrWtle.:�. r,a.3n i u i_35 4. Phone ( ) 6 phone ( J ]. Transpoder #1 Company Name e. US EPA ID Number 9. Transporter #1'a Phone 10. Transporter 42 Company Name 11. US EPA 10 Number 12. Tmnspoder #2's PM1one IS. Designated TIED Facility Name and Site Address 14. US EPAIDNumber 15. Facility's PM1one { M5 L6rfOi111 � IIYa MatarmaG Fti:<<i1✓.-Did, Wi. [iH±e i .,, 2e d..:.. 16 Waste Shipping Name and Descdream 17. Republic Services Appmval#and Exp. Date 18.Cma iners 19, Total 20. Unit Readily WWOI No. Type Q O ah", i8ealyd iK SOM ;i,c, to-r,4?7 b. 2 W w c 21. Additional Descriptors for Materiels Listed Above 22. Special Handling Instructions and Additional Information - 23. GENERATOR'S CERTIFICATION: hereby codify that the above named material is not a hazardous waste as defined by 40 GFR 261 or any applicable state law, has been properly described classified and packaged, and is in proper condition for transportation aocoming to applicable regulations: AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I cedlfy and warrant that the waste has been treated In accordance with the requirements of 40 CFR 268 and Is no longer a hazardous waste as defined by 40 CFR 261, Pnntaidayped Name — Signature Monts Cry real 24. Transpoder#1: Acknowledgement of Receipt of Materials ad R inted/ryped Name Signature Monet Day Year O 2 25. Transporter#2: Acknowledgement of Receipt of Materials.— MPrime pa �� IGA,� SignaWre r - rn oey L 7� year /017am 1, 4 26. Discrepancy defloston Space J T F J Q2). FacI11Yy Owner or Operator: Codification of receipt 0f waste materials covered by this manifest (except as noted in Item 19) LL N F Pnntetl?yped Name 1 signature nro y Year J( TRANSPORTER #1 REPUBLIC' SERWCES \. e NON -HAZARDOUS WASTE MANIFEST= 4481204 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3_ Generators N and M 'I ng Address 5 Generating Location (If different) . i r _-f vh Adve.. .,.... '6'8 M.... !silIl [a i.;hpurlie. i-4r._ rca Jig ..� ,. r..,. 4. PM1one( ) 6. Phone( ) ]. Transporter#1 Company Name S.US EPA ID Number 9. Transporter #1 a Phone 10. Transporter#2 Company Name _, 11. US EPAID Number 12. Tamagnpeir Phone 13. Designated I If Facility Name and Site Address 14, US EPA ID Number 15. Facility's Phone Miss i bfir i 5 iUrb MGI Iwar Aul t_4.c5 Ol tvG etA%d i 16. Waste Shipping Name and Description 17. Republic Services Approval# and Up. Date 16. Containers 19. Thing Si Unit Country wi N0. Type wik, Up uslk �za a d. a of Z of _ / t0 /l � ! 1 2TAdditional Descriptions for Materials Listed Above - "- - 1 22. Special Handling lnstmctions and Additional Information 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, he. been properly described classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of previously restricted hazardous waste subject to the Land Disposal Restrictions. I supply and warrant that the waste has been treated in accordance with the requirements of 40 DFR 266 and Is no longer a hazardous waste as defined by 40 CFR 261. Printetl?yped Name sid Signature Monts pay per C 24. Transponder fill Acknowledgement of Receipt of Materials F Printer ad Name Signature Monts pay Year r C • ' poReceipt Oi Matebel5 - 2 25. Transponder Acknowledgementot a Prinla E Name Signature ) Month pay Year, for Discrepancy Indic tics Space J LL2. Facility Owner or Operator Comficatlon of receipt of waste materials covered by this manliest (except as noted In Item 19) N PdntatlRyPetl Name �SlgnalUre MonfM1 pay Yeer F TRANSPORTER#1 -,a4%po�iSi's REPUBLIC-- SERVICES J NON -HAZARDOUS WASTE MANIFEST IIW4481205 1. Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generator's Name and Meiling Address 5. Generating Location (ii Oflereng Chanel Wiggi Airpon Os18 N7orkiiii. U,. 5318 MarrMll C1t. Cip rinaa, W, 2il2U8 1-hatbW, NC 2a20b au odl u at, iue .ka i u l3s 4. Phonol ) 6. Phone( ) ]. Transporter #1 Company Name 8. US EPA ID Number 9. Transporter#PS PM1one 10. Train poer#20ompa Name 11. US EPA ID Number 12. Transporter#2'a Phone 14. US EPA ID Number 15. Facility's PM1one 13. Designated TISID Facility Name and Site Address - M51an515151(15 ManYKatl litl C.OfIC4rtl, POL, 25U37 IN 192."a x � t 16. Waste Shipping Name end Description 9, Republic Sony.. Approval # and E., data 18, Contain 19. Total 20. Unit Quantity Wood No. Type bun rT r If, lafni a Non Flazanow Soft 5115-"17811 111 IS b. w w 21. Additional Descriptions for Materials Listed Above 22, Spacial Handling Instructions and Additional Information DW accl.t33d559 23, GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hezartlous waste as tlefinetl by 40 CFR 261 or any applicable state lase has been properly described, diesel and packaged and Is In proper condition for transportation assuming to applicable regulations;AND, if this waste is a treatment residue of previously restbcted hazardous waste sublet[ to the Land Disposal Restrictions. I certity and warren[ that the waste has been traatatl In accordance with the requirements of 40 PER 268 and is no longer a hazardous waste as defined by 40 CFR 261. Prnle ib?yped No,. Signature Monln Oay ¢ar 6 24. Transporter 6l: Acknowledgement of Receipt of Materials w Printetl?yped Name Signature Monts Day Year 6 ,..Q 1` IGG N 28: hpor anster#2:Acknowledgement cl Receipt of Materials - zQ 2 Printed[T/yped Name Sture lgoa`\j 1 Monet ony Yaar 26. Discrepancy Indlcaticn Space EJ Q 27. Facility Owner or Operator. Generation of receipt of waste materials savored by this manliest (except as noted In Item 19) LL o GMS LAND -ILi 6106 MlikEiFAO ftU WNulH.u, w; i1W(i I(,w-tg,. Afµ x,.Dl N F Printed/Typed Nam Signature 2 Monet Dey vear TRANSPORTER#2 r��REPUBLIC SERVICES REP ICES 1 sL�:,KY �I a - NON -HAZARDOUS WASTE MANIFESTM 4481206 rIGerator's UPS ID Number Manifest Document Number) 2. Page 1 of I 3. Generator's Name and Mailing Address 5. Generating Location (if different) c,nign fM Lxul Ail w IO Awnivieru ut 63'I8 Mordo%l1 Dr. ClyrlDl NC ?l L),tmrw. w, NC 28200 / W :wn u1'.w I" Via 10131, 4. Phone ( 6. Pbone ( ) 7.Transpoder#1 Company Name B. US EPA ID Number 9. Transaction#1's Phone 10. Transpoter #2 Company Name J1, US EPA ID Number 12, Transporter #Ts Phone 13. Designated TIS/D Facility Name and SIte Address 14. US EPA ID Number 15, Facility's Phone li WIWI)610d1 MORAnes" rid(AQngps .14L sl1 704,792-Iub4 XT67 16. Waste Shlaping Name and Description 17, Republic Services Approval# and Exp. Date 18. Containers 19. Total 20. Unit Quantity VJiNOI No. Type Nunes zalwo 504 501G IbI ill iW2bF IV a b. M w z up �- c. c Jc. 21. Additional Descriptions for Materials Listed Above 22. Special Handling Instructions and Additional Information _ pail Dun: Al 23, GENERArOH'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as defined by 40 CFR 261 or any applicable slate law, bas been properly described. clacadred and packaged and Is in proper condition for transportation according to applicable regulations', AND, if this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I caMy and warrant that the waste has been treated In accordance with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 4o CFR 261. Printod?yped Name Signature Mom, og- vvar 24. Transporter It, Acknowledgement of Receipt of Materials CPrinted/Typ dName Signature _ .,a pay veer f0e an 25. Tr p b"i�F%ceipl of Materials Pented?yped Name Signature Monm oey vea. F 26, Discrepancy Indication Space T F J G27, Facility Owner or Operator: Competition of receipt of waste materials coveretl by this manifest (except as noted in Item 19) do O GMSVINI 6106W.)RtEHIlI R11 lAhto0ll, l,, ho, b(-Ajue,a, N Printed?yped Name Signature Monm oay near TRANSPORTER#2 �aD REPUBLIC I `51 r Q 5 6�1 l Z► SERVICES NON -HAZARDOUS WASTE MANIFESTM 4481207 1, Generator's US EPA ID Number Manifest Document Number 2. Page 1 of 3. Generator's Name and Mailing Address S. Generating licimmon (if different) ChorloW Douplii Alrpart w id Mprr15141d Cx. I AbFrIMNId OF. Chadod+. INC 28206 C�loii' NC 2&106 rue �d1 Jv:M1 764 361 013ei a. Phone( 6. Phone ( ) 7. Transporter#1 Company Name 8. US EPA ID Number 9. Transporter 41's Phone - I . rnspormr#2. CempanyName 11. USEPAIDNumber 12. Transporter#2's Phone 13. Designated TISID Facility Name and Sit- -Atltlress 14. US EPA 10 Number 15. Facility's Phone Mi LiOdfdi 010E ►lnririiid Rd F Mtlfrd, W, 2Wd7 7UA. 74e.sesul A 4ai 16. Waste Shipping Name and Description 17. Republic Serviras Approval# and Ezp.0ate 13. Conta!nere 19. Total 26. Unit Quantity Ail No. Type 111 11, ad Non i-lizerces" tioll ik]iwib-1'191'1 Ir)rta ly a b. Is z J i 21. Additional Oesoriptions for Materials Listed Above 22. Special Handling Infatuations and Additional Information hill icaf333E59 23. GENERATOR'S CERTIFICATION: hereby comity that the above named material is not a hazardous waste as defined by 40 OFR 261 or any applicable state law, has been properly described, classified and packaged, and Is In proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I codify and Warrant that the waste has been treated in accordance with the requirements of 40 OFF 268 and is no longer a hazardous waste as defined by 40 CFR 261, PrintedlTyp d Name Sign@W M-sh Oay veer ,, ) � - J — T 7 _ . ,. � I I a IL 24.Transporter #1: Acknowledgement of Receipt of Materials W Printed/Typed Name SgnaWre Mam. Oey Year al — - _ LL 4porter42'. _. W 25. Acknowledgementof Receipt of Materials RPrinWd?ypetl Name Signature Ioay veer F 26. Discrepancy indication Space F J Q27, Facility Owner or Operetoc Cognomen of receipt of waste materials covered by this manifest (axcept as noted in Item 19) LL O ��LAIVtii-iLt.ytlid lM➢tEiit71D RG +UNw!<ii, rqG (ikui ruwioi-e: uti <..Wi N F Printetl/fypetlName �� l Signature in Day vYR toMMM J TRANSPORTER N2wmmiwil �REPUBLIC' _ /ir`�7 DD SERVICES a NON -HAZARDOUS WASTE MANIFEST 4481208 1. Generator's US EPA ID Number Manifest Document Number 2. Pagel of 3. Generators Name and Mailing Address 5. Generating Location (if different) Grwtlpib Lotsda as AR{wtl 01914 IVfolualm91d Lu 6319 Mor-jiff d Dr rhaMaq, 1120209 G1w1IIl1iE•, Ni 2UUI5 .U4 w1 GlAe %Uy abou V 4. Phone ( ) 6, Phone ( ) ].Transporter ell Company Name 8. US EPA ID Number 9. Transporter#1'a Phone 1 ) 10. Transporteri Company surang, 11. US EPAID Number 12. Transporter#2's Phone 13. Designated T/S/D Facility Name and Site Address 14. US EPA ID Number 15. Facility's Phone t Mile LanaVI151ot! f111DMn"G NO C:O9bOla, i 21111121 704 /BI.ltNl., x -Ac! 16, Waste Shipping Name and Description T]. Republic Sewlbes Approval # and &p. Date 18. Oentamade 19. Total 2S Unit puantiry WWoI - o. pe -- a. NOR 0 rtasardi Stall 601 u- U& 11971 10idnp19 a d. w w _ 21. Additional Decorations for Materials Listed Above 22. Special Handling Instructions and Additional Information oN ectl.Y333fi6ti 23. GENERATOR'S CERTIFICATION: I hereby county that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described classified and packaged and is in proper condition for transportation according to applicable regulations; AND, If fiis waste is a treatment residue 0f a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated In accordance with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261, PdntetlRypetl Name Signs Iore ,all Day ear C 24. Transporter #1: Acknowledgement of Receipt of Materials Pr nted/ryped Name SlgnaWre Menlh pay Yeer o ,f -; Nam_ . 0 25.Transporter#Acknowledgement 4. AcknowleReceipt of Materials < PrintedRyped Name Slynatwe MOMM1 Oay Year F 26. Discrepancy Indication Space r C J 3 27. Facility Owner or Operetac Certification of receipt of waste materials covered by fluid s manifest (except as noted in Item 19) LL c CMS UNNfI1161 W M1iFtILNFAu but uirtititiu, or, ?;vdu /o4..r n< rw4 n sp, N F PdntetlRyped Name Signature Mont Oaa ycyr, TRANSPORTER#2 ���REPUBLIC" SERVICES NON -HAZARDOUS WASTE MANIFEST= 4481209 1. Generator's US EPA ID Number Manifest Document Number 2. Page i of _ 3. Generator's Name and Mailing Address S. Gene rating Location(if brdenl) t 111,00ollo Douglas Purport Sd Ia Morimew ES RIiA Mornaflyld DI CrMrblp, W. MOO ChalgW P1L 26[0B r� Jti1 U1 Jet 704 A0 t ul dg 4. Phone ( 6. Phone ( J ]. Transporter #1 Company Name 6.US EPA ID Number 9. Trans porter #I one T I 10. Transporter#2 Compa 11, US EPA ID Number 12. Transactor 42. Phone 13. Designatetl LSID Facility Namaland Site Atltlress 14, US EPA ID Number 15. Facility's Phone MS LaMNI 510& MGreread Rd C.arecoard, IVC Z8027 ]Q<-/Sl 2GDC % 36i 16, Waste Shipping Name and Description 17. Republic Services Approval #and Up, Date 1S. Contalnem 19. Total a. Unit Quantity Wwol No Type O¢ Non Tograndll Boll 501u1&1757710/etalal Q b. Op W ad Z / c. 21. Atltlitional Descriptions for Materials Listed Above - 22. Special Handling Instructions and Additional Information bill ak"La 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material Is not a hazardous waste as tlermed by 4 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is In proper condition for transportation according to applicable regulations; AND, if this waste is a treatment esidue of previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warren[ that the waste has been treated in accordance with the requirements of 44) CFR 263 and is no longer a hazamed, waste as defined by 49 CFR 261. Printed/Typed Name Sgnature Mann usy Year 24,Transporter Ni'. Acknowledgement of Receipt of Materials P 2 Priated/T d Name Signature I natu a -� 9 Mon16 Day Year W 25.Transporter 42'. Acknowledgement of Receipt of Materials QP(ntedl'yped Name Signature Y Yaar ManrM1 Oa I- 26-Debrecen, Indication Spaoe J R2]. Facility Owner or Operetor: Certification of receipt of waste materials covered by this manifest (except as noletl in LL Item i97 p .MBIAHOHLL 67UiM <i: u_A;ndrx., r rn e alF.,u �.Ir.v. N F PnntedRypetl Name � Signature -, _ Monm oay ear TRANSPORTER#2 �REPUBLIC' D SERWCES NON -HAZARDOUS WASTE MANIFEST M 448i210 1. Generator's US EPA ID Number Manifest Document Number 2. Page f of 3. Generator'sName and Mailing Address 5, Carl Location (if different) 4hiu6ra lol u"s Ara l wid MUYnerl Ur. 5318 MpnMNld Dr CMrlone. NC 20i LIAMi .Pill 2b2(iH rWf111a1 Mff lure Jib, oftSy 4. Phone ( ) 6. Phone ( 1 7. Transporter#1 Company Name 6. US EPA ID Number 9. Transporter Al's Phone T �tA 10. Transporter#2 Company Name 11, US EPA ID Number 12, Transporter #2'1 Phone 13. Designated T/S/D Faculty Name and Site Address 14, US EPA ID Number 15. Faciliq's Phone Mti Legal blob MDIYMid Rd Siff liAla, ei zdUZ9 ]Of.]u2TD0A %267 16. Waste Shipping Name and DescHptlon t]rRepublle Services Approval #and Exp, Date 18.6ontoners 19. Royal 20. Unit Country WWol No. Type O Nan H®zeuci wall SUIRD- &1]J/i 110,411 a b. w w 21, Additional Descriptions for Materials Listed Above 22. Special Handling Instructions and Additional Information bia uU.Y3:i3dors 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged and Is in proper condition for transportation according to applicable regulations; AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions, I Certify and warrant that the waste has been treated in accordance with the monochrome of 40 GFR 268 and Is no longer a hazardous waste as defined by 40 CFP 261, PrintedRyped Name Signature Month pay v r Its 24. Transporter#1 Acknowledgement of Receipt of Materials 2 Primed/Typed Name Signature _ -" _, Month Day leer __.. O 6 2 25. haneporter k2'. Acknowletlgem6nt of Receipt of Materiels Pdntedayped Name Signature Mon,, pay Year F 26, Discrepancy Indication Space C J Q27. Facility Owner or Operator: Certification of receipt of waste materials covered by this manifest (except as noted in Item S) LL o Gill itN1]HLLSllra MUREHLAi7 HG GGM.rnul .xi_ rtavr >a4 nl,-item .cr, N F Pdntedlfyped Name ^-y-- Signature --, MunM pay Year �v t' or TRANSPORTER X2 21 t REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFEST= 4481211 1, Generator's US EPA Io Number Manifest Document Number 2. Page 1 of 3. Generator's Name and Melling Address 5, Generating Location (if different) [.I Idoft the JOi so(UOrl � Ib spolun lNµl Lrt, S,Y1tyfkooafw Qf CbehfbtN, pY'_- 2e1015 �.. be Gotle. Mt, e6206 k4 uvl 0kpi NP1361 0139 . 4Phone ( 7 6. Phone ( ) J. Transporter 41 Company Name S. US EPA ID Number 9. Transporter to's Phone 1 yr 10. Transporter 12 Company Name - 11. USEPAID Number 12, Transporter#2's Phone 13. Designated TIED Facility Name and Site Address 14. US EPA ID Number 15. Facility's Phone I. i Laf (IN 816E MWOIh O HO -01ILuf0. hi 2811 ]UA 152-..1(W 'I I,, 16. Waste Shipping Name and Description 17. Republic Services Approval# and Exp. Data 16. Containers 19, Total 20, Unit Quantity WtlVdI No. Typo I In in prache O effort HiMbdua OBSOfI rsul(J-1. "lot, tblFbi6 Q b. W up up O 1 -D 21. Atltlitional Descriptions for Materials Listed Above - 22. Special Handling Instructions and Additional Information bill accLS333i 23. GENERATORS CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR 261 or any applicable state law, has been properly described, classified and packaged, and is in proper condition for transportation according to applicable regulations: AND, if this waste is a treatment residue of a previously restricted hazardous waste subject to the Lead Disposal Restrictions. I codify and warrant that the waste has been treated in accordance with the requirements of 40 CFR 263 and Is ne longer o hazardous waste as defined by 40 CARD 261, Pdntetlayped Name Signed, to Month ... year _ be 24. Transporter #i'. Acknowledgement of Receipt of Materials ttPrintedayped Name Signature Moron pay year - e d ra 25, Transporter #2'. Acknowledgement of Receipt of Materials Z sis Pentedayped Nam. _ SIgrIGY. o More pay or., // I._ 26, D(sorepency Indication Space F Demarcation of receipt of waste materials covered by this manifest (except as noted In Item 19) MZ,,Ah rILL OLU h9UnL LAI, RUQIN601i0, ll 1ie/ irW-Ib<-]iuC,r jo, LOperator. t Signature�l Monm oey veer TRANSPORTER 0 a ��� REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFEST 44 1212 1. Generator's US EPA ID Number ManXe9 Document Number 2. Paget of 3. Generator's Name and Mailing Address 5, Generating Location (it different) g313 MorM1Ml4 Dr. Cixfrblk. W. 282% 1..N0f edbi H 262UB I119.ur, blue iO4 36. (1136 4. Phone ( 1 S. Phone ( ) 7. Transporter#1 Company Name 8,US EPA ID Number 9. Transporter #1's Phone 1 10. Transpoder#2 Com ny Name J 11. US EPA ID Number 12. Tmnspmler#2's Phone 10, Designotatl TISID Facility Name and Site Address 14. US EPA 10 Number 16. Facilltys PM1one MS L.ardnll 511 Mofatrea6 NO t,.nnoOrb. IVi. 2B(/27 7N M "A X A67 18. Containers 1g. Total 20. Unit 16. Waste Shipping Name and Description 17. Republic Services Appmvel#and E,.Date Daanliry "i No. Type m o Non HararlbLN SM SOiu18,11977 iW2briS Q b IN w /OCR 21. Additional Descriptions for Materials Listed Above 22, Special Handling Instructions and Additional Information bill pcclLtd i3i 23. GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste ser defined by 40 CFR 261 or any applicable state law, has been properly described classified and packaged, and is In proper condition for transpodati0n according to applicable regulations; AND, it this waste is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certily and warrant that the waste has been treated in accordance with the requirements of 40 CFR 268 and is no longer a hazardous waste as defined by 40 CFR 261. Pdntedayped Name Slgnat0le Well Oay Year _ 24.Transporter#1-. Acknowledgementof Receiptaf Materals of P mb driyped Name Signal .�� '� Monm Day veer f�-----�---' i..�1.4Z-4-,— Z 2117re p her #2'. Ack rig t of Reco pt of Matenals QPrinted/Typed Name Signature xxxi Day Year 26. iscrepancy Indication Space i F J Q27, Facility Owner or Operator; Correction of receipt of waste materiels coveretl by this manifest(except as noted in LL Item lBJ p OM6 LArylI11LLp1lK`VUl(LIILHJ'nll4lANL.OrtILNr. v4'I. W-r JLdW4 N F Printed?yped Name Signature MontM1 Day TRANSPORTERN2 REPUBLIC' SERVICES NON -HAZARDOUS WASTE MANIFEST 4 I L 13 1. Generator's US EPA ID Number Manliest Document Number 2. Page 1 of 3. Generator's Namo and Melling Address 5. Generating Londn, (If different) 4. Phone l 6. Phone( ) ]. Transpoder Nl Company Name 8, US EPA ID Number 9. Transporter Nl's Phone 10. Transporter U2 Company Name 11, US EPA ID Number 12. Transporter N2's PM1one 13. Designated TIS/D Facility Name and Site Addincess 14. US EPA ID Number 15. Facility's Phone M:, i990 P1 a61ERBelU fin lcry t A !flb.:; ) g14 y ,h 13. Waste Shipping Name and Description 17. Republic Seroces Approval Nand Exp.Date 18. Containers 19. Total 20. Unit Quantity WWel No. pe a. Tandn iozeubus bake O aut.2 ro- 'u,I a d. as ad 1 I 21. Additional Descriptions for Materials Listed Above 22. Special Handling Instructions and Additional Information 23. GENERATOR'S CERTIFICATION: I hereby comfy that the above named material is not a hazardous waste as defined by 40 Cl 261 or any applicable state law, has been properly described classified and packaged, and Is in proper condition for transportation According to applicable regulations; AND, If this waste Is a treatment residue of a previously restricted hazardous waste subject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated In accordance with the requirements of 40 DER 268 and Is no longer a hazardous waste as defined by 40 OFR 261, Printetl/typed Name - _., Signature sk" Day year as 24.TransporterN1'. Acknowletlgement of Receipt of Materials F Pented/typed Name Signature monm usy veer 0 i25, Transporter 02'. Acknowledgement of Receipt of Materials QPrinted/Typed Name Signature edi Pan Year F 26. Discrepancy Indication Space i F J Q2]. Facility Owner or Operator: Combination of receipt of waste mansions covered by this manifest (except as noted in Item 19) LL N F Prin[ed?yped Name Signature - 'f tAagrh Day Fg1 wr r L) V TRANSPORTER#1 tr Uj z W r� R ��Z AgFIJ v; � sT HAZgRdpUB WAgTf� MphIIF � _�- 1. Generatork In; ePA ID MrmbM MWVVRI C?p(yxl+enl iJumpo,A p)(n 5 J` 3. ppeertlh•Ir's Mara snA ttlMllnp Address _ - flan t!f dlllurorlli H0r III I11,WW LA 1►kw T%R. d N Nr 1 U i Cj9p ' + A Phom I 1 `' 7c� n ...:t Ajb rw dot WAV ---- — Wi-g Prone �nsporW . Transpadef rraNameUS 6A tdN',AOFf8, Tran>tpp{1°rrrr2 Co R _~~~ _ �"ny NBrne _ 11. US CPA ID NW4110t _ 16. Facility 's phone •_ Deslpnated 7rS]D Faniiry Name and $ItA Address +6. B $hipping Name and Description 2T. Adrkr al oesrainm� for Marerfals t fisted Abova 54. UUS EpA iD Nllr" fwi rez•tv.d x �� 18. Total 2d. Unit 17• Repubec Services Approval N and DP- I) IS. Containers f}uant4 WtNoi W. TYQe F. ,n ice''' ' i �R.s snaAedaanar rnlarm�•�• � g2 SpLYf3f ygndlrl�g rnsrrU G�ry�gpTOri CS��R77FrCArlpH• I hereby cart+fY that the above named material is not a hazardous waste as defined by 40 CFR 251 or any appticarile stale law, has !beerrF�perly desorid d' dassifred and paclraged, and is in proper condition for transportation according to applicable regulations; ANO, if this waste is a treatment residuo o{ a prevrnuslyresrricrad hazard°us waste suBject to the Land Disposal Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements o[ 46 CFR 268 and is no ranger a hazardous waste as defined by 40 CFR 261. Signature Month Day Year Prrnfe ITd Name - _ Y Transporter#i: Rck 0:lodgement Of Receipt of Materials ;Fe r hyped Nature S � - snsporter i#2: Acki 00edgernOnt of Receipt of Materials 5yped Name apancy Indica signature ]wrier or Operator, Certification of receipt of waste materials covered by this manifest texcept as noted in item 19) ame f T T Signature TRANSPORTER =L Month Month Day Yea Day REPUBLIC SERVICES NON -HAZARD t. Generalorg US EPA lD Number _ DuS WASTE MANIFEST Manifest Documanl Number -—to_ 2- P9g®+ --- 3- Generators Name and Mallur4 Andress M1k 1 b. Ganeralrnp LocnUon flf rldfernnli C Phone 7. Pansportez st ComPany Name Ir: 10 . Transporter *2�ny Name 13- Deslg odlea TYSID Fa d} . 1dY Name and Site Address 11 MS U"X" StLilo tMDf6t541fif; rtdC.Dr+1CWIl, t51i 2A[J2i "I Waste $hipping Name and basrr Wrenn Orc. 4 it >x t ❑ b. z ua 21. Addi '.J 22. Spoc al Hand. for Materials Listed Aboua e, phone t 1 EPA ID Number 11, US EPA ID Number 14, US EPA 10 Number 9. Transporler A1's phone 12. Transporter #2's Phone 15. Facillty's Phone 17. Rapubflc Sarvlces Rpproial u and Exp, Date 1a. Containers 19- Total 20, U-nit Quantity W Wo1 No. Typo �3• CE'f�WXArfON, t hereby Certify that the above reamed material is not a hazardous Waste as defined by 40 CFR 261 ar any applicable state G'1: 1 .01 a law, has been Properly described, ctassifred and packaged, and is in proper condition for transportation accardfng to applicable regulations; AS+117, it this waste is a treatment rasiaue of s PrR 268ra restricted hazardous waste subject to the Land Disposaf Restrictions. I certify and warrant that the waste has been treated in accordance with the requirements of 4 CFq 2 fig and is rfo longer a hazardous waste as defined by 40 CFIg 261- Prirrted/ryped IV,.,,, Monett nay Y � Signature 24- transporter #7' An Prinreowledgement of Receipt of Materials d/rY Nairle _ Month Day '} �- Signature rra A°►'ter #2: Rcknowl�gemenr of Receipt of Materials int8dt7- _ Yaar f q Marne Si nature yI fNorlrh Day rear !,•�, r ` s � ` 1 I :"Ity Dwn re Pod Nan7e Of receipt of waste materials covered by this manifest (except as rioted in Item 19) Slgnarure TRANSPORTER #1 mVrlin uay Year Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 APPENDIX B PHOTOGRAPHS Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina Wood Project: 6228-18-0503 PHOTO 1: ,. ' View of UST prior to removal. Im J PHOTO 2: Pooled petroleum noted beneath tank upon removal. Initial Abatement Action Report - GADO Building 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina Wood Project: 6228-18-0503 November 26, 2018 PHOTO 3: Pooled petroleum noted beneath tank upon removal. PHOTO 4: UST being removed from excavation. Initial Abatement Action Report - GADO Building 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina Wood Project: 6228-18-0503 ` _i' er November 26, 2018 PHOTO 5: Corrosion holes noted in UST. PHOTO 6: Corrosion holes noted in UST. Initial Abatement Action Report - GADO Building 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina Wood Project: 6228-18-0503 i ..,. .. � _... �..R.. Wit- •� , 1 November 26, 2018 PHOTO 7: Petroleum pooled beneath tank on soil. PHOTO 8: Corrosion hole measurements. Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 APPENDIX C UST-2B FORM UST-2B Site Investigation Report for Permanent Closure or Change -in - ND Service of UN -REGISTERED UST Return completed form to: STATE USE ONLY: NC DEQ / DWM / UST SECTION Facility ID # 1646 MAIL SERVICE CENTER RALEIGH, NC 27699-1646 ATTN: REGISTRATION & PERMITTING Date Received phone (919) 707-8171 fax (919) 715-1117 htti)://www.wastenotnG.org/ INSTRUCTIONS (READ THIS FIRST) 1. UST permanent closure or change in service must be completed in accordance with the latest version of the Guidelines for Site Checks, Tank Closure and Initial Response and Abatement. The guidelines can be obtained at http://deg.nc.gov/abouUdivisions/waste-management/waste- management-permit-quidance/underground-storage-tanks-section. 2. Permanent closure: Complete all sections of this form. 3. Change -in-service: Where UST systems will be converted from storing a regulated substance to a non -regulated substance, complete sections I, II, III, IV, and VI. 4. For more than 5 un-registered UST systems, attach additional forms as needed. 5. Un-Registered USTs may be subject to unpaid fees and late penalties. 6. REGISTERED USTs use Form UST-2A. I. OWNERSHIP OF TANKS II. LOCATION OF TANKS Owner Name (Corporation, Individual, Public Agency, or Other Entity) Charlotte Douglas International Airport Facilityy Name or Company GAD O Building Street Address Facility ID # (If known) 5601 Wilkinson Boulevard 00-0-0000033447 City County Street Address Charlotte Mecklenburg 5318 Morris Field Drive State North Carolina Zip Code 28208 City County Zip Code Charlotte Mecklenburg 28208 Phone Number Phone Number 704/560/9242 None III. CONTACT PERSONNEL Contact for Facility: Job Title: Phone #: 704/560-9242 Mr. James McDorman Env. Comp. Coord Closure Contractor Name: Closure Contractor Company: Address: Phone # Nate Jones, Jr. Jones Grading & Fencing, Inc. 1726 Toal Street 704/331-9225 Primary Consultant Name: Primary Consultant Company: Address: Phone # Robert Foster Wood E & I Solutions 2801 Yorkmont Road 704-357-5530 IV. UST INFORMATION FOR UN -REGISTERED UST SYSTEMS V. EXCAVATION CONDITION REGISTERED LISTS use Form UST-2A. Tank ID Size in Last Last Permanent Method of Permanent Closure: Change -in- Notable No. Gallons Contents Use Close Date Indicate REMOVED or enter fill Service Waterin Free product odor or visible soil Date material, such as foam! Date excavation contaminatio concrete/ sand n —Yes—F No Yes No Yes No 1 1,400 Fuel oil 1990 10/19/2018 REMOVED NA ❑ ❑. ❑ ❑. ❑ ❑ ❑ ❑ ❑ ❑ ❑ VI. CERTIFICATION I certify under penalty of law that I have personally examined and am familiar with the information submitted in this and all attached documents and that based on my inquiry of those individuals immediately responsible for obtaining the information, I believe that the submitted information is true accurate and complete. Print name and official title of owner or owner's authorized representative James McDorman, Enviornmental Compliance Coordinator Signature Date Signed 11 /27/2018 INORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION 1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE (919) 707-8171 FAX (919) 715-1117 http://www.wastengtnc.orq/ 1/2016 Initial Abatement Action Report - GADO Building November 26, 2018 5318 Morris Field Drive, Charlotte, Mecklenburg County, North Carolina 28208 Wood Project: 6228-18-0503 APPENDIX D LABORATORY ANALYTICAL REPORT AND CHAIN -OF -CUSTODY FORM icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 October 24, 2018 Rob Foster AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 Charlotte, NC 28208 Project Location: 5318 Morris Field Drive Client Job Number: Project Number: 6228-18-0503 Laboratory Work Order Number: 18J1029 Enclosed are results of analyses for samples received by the laboratory on October 20, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 15 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 18J1029-01 18J1029-02 Sample Preparation Information QC Data Petroleum Hydrocarbons Analyses B215272 B215425 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 5 5 7 9 10 10 10 10 11 12 13 Page 2 of 15 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 REPORT DATE: 10/24/2018 Charlotte, NC 28208 PURCHASE ORDER NUMBER: ATTN: Rob Foster PROJECT NUMBER: 6228-18-0503 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18J1029 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 5318 Morris Field Drive FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB TB-1 18J1029-01 Soil SM 254OG SW-846 8015C TB-2 18J1029-02 Soil SM 2540G SW-846 8015C Page 3 of 15 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method 8015B GRO elevated reporting limit for samples 18J1029-01+02 due to high concentrations of target compounds. SW-846 8015C Qualifications: S-01 The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit required from high analyte concentration and/or matrix interferences. Analyte & Samples(s) Qualified: 2-Fluorobiphenyl 18J1029-01[TB-1],18J1029-02[TB-2] SW-846 8015C Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard. Diesel Range Organics (C10-C28) is quantitated against a calibration made with a #2 fuel oil standard. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Tod E. Kopyscinski Laboratory Director Page 4 of 15 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029 Date Received: 10/20/2018 Field Sample #: TB-1 Sampled: 10/19/2018 13:45 Sample ID: 18.11029-01 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Gasoline Range Organics (GRO) 620 61 59 mg/Kg dry 50 SW-846 8015C 10/22/18 10/22/18 18:22 EEH Diesel Range Organics 15000 2100 760 mg/Kg dry 100 SW-846 8015C 10/20/18 10/22/18 13:04 RMW Surrogates % Recovery Recovery Limits Flag/Qual 1-Chloro-3-fluorobenzene 108 70-130 10/22/18 18:22 2-Fluorobiphenyl * 40-140 S-01 10/22/18 13:04 Page 5 of 15 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029 Date Received: 10/20/2018 Field Sample #: TB-1 Sampled: 10/19/2018 13:45 Sample ID: 18.11029-01 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 78.3 % Wt 1 SM 2540G 10/21/18 10/22/18 12:00 KMG Page 6 of 15 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029 Date Received: 10/20/2018 Field Sample #: TB-2 Sampled: 10/19/2018 13:50 Sample ID: 18.11029-02 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Gasoline Range Organics (GRO) 650 74 71 mg/Kg dry 50 SW-846 8015C 10/22/18 10/22/18 18:57 EEH Diesel Range Organics 12000 2100 750 mg/Kg dry 100 SW-846 8015C 10/20/18 10/22/18 13:22 RMW Surrogates % Recovery Recovery Limits Flag/Qual 1-Chloro-3-fluorobenzene 115 70-130 10/22/18 18:57 2-Fluorobiphenyl * 40-140 S-01 10/22/18 13:22 Page 7 of 15 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J 1029 Date Received: 10/20/2018 Field Sample #: TB-2 Sampled: 10/19/2018 13:50 Sample ID: 18.11029-02 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 76.3 % Wt 1 SM 2540G 10/21/18 10/22/18 12:00 KMG Page 8 of 15 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: % Solids-SM 2540G Lab Number [Field ID] Batch Date 18J1029-01 [TB-1] B215295 10/21/18 18J1029-02 [TB-2] B215295 10/21/18 Prep Method: SW-846 3546-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1029-01[TB-1] B215272 15.2 1.00 10/20/18 18J1029-02 [TB-2] B215272 15.7 1.00 10/20/18 Prep Method: SW-846 5035/5030B-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1029-01[TB-1] B215425 6.70 6.40 10/22/18 18J1029-02 [TB-2] B215425 5.70 6.40 10/22/18 Page 9 of 15 Table of Contents icon-tes w . ANALYTICAL LABORATORY 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215272 - SW-846 3546 Blank (B215272-BLK1) Prepared: 10/20/18 Analyzed: 10/21/18 Diesel Range Organics ND 8.3 mg/Kg wet Surrogate:2-Fluorobiphenyl LCS (B215272-BS1) 2.01 mg/Kg wet 3.33 60.3 Prepared: 10/20/18 Analyzed: 10/21/18 40-140 Diesel Range Organics 22.9 8.3 mg/Kg wet 33.3 68.8 40-140 Surrogate:2-Fluorobiphenyl LCS Dup (B215272-BSD1) 1.86 mg/Kg wet 3.33 55.7 Prepared: 10/20/18 Analyzed: 10/21/18 40-140 Diesel Range Organics 25.6 8.3 mg/Kg wet 33.3 76.7 40-140 10.8 Surrogate:2-Fluorobiphenyl Batch B215425 - SW-846 5035/5030B 2.09 mg/Kg wet 3.33 62.6 40-140 Blank (B215425-BLK1) Prepared & Analyzed: 10/22/18 Gasoline Range Organics (GRO) ND 1.0 mg/Kg wet Surrogate: 1-Chloro-3-fluorobenzene LCS (B215425-BSI) 16.8 µg/L 15.0 112 Prepared & Analyzed: 10/22/18 70-130 Gasoline Range Organics (GRO) 0.216 0.010 mg/Kg wet 0.250 86.5 80-120 Surrogate: 1-Chloro-3-fluorobenzene LCS Dup (B215425-BSD1) 15.9 µg/L 15.0 106 Prepared & Analyzed: 10/22/18 70-130 Gasoline Range Organics (GRO) 0.236 0.010 mg/Kg wet 0.250 94.2 80-120 8.59 30 Surrogate: 1-Chloro-3-fluorobenzene 16.6 µg/L 15.0 ill 70-130 Page 10 of 15 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 * FAX 413/525-6405 " TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. S-01 The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit required from high analyte concentration and/or matrix interferences. Page 11 of 15 icon-tes w . ANALYTICAL LABORATORY Table of Contents 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8015C in Soil Gasoline Range Organics (GRO) NY,VA,NH,NC Diesel Range Organics NY,VA,NH,NC The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2018 NC North Carolina Div. of Water Quality 652 12/31/2018 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2018 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 12 of 15 Table of Contents ice„• ?7.. 0 U S ix3 S 7F, DU iz. CC C CS C U yN - nOC :3 LN �'Q d LlO4 Vz sO cC¢LOcoO c!-0 c 11J 77II Q Ln V) 3n 0 -0 I it m X F� Y- ,i 'II i Q m s 11 II it II 11 Q C a V7 > cn C "0 ISOM a a o x �� [ .E E ` � N M i: � in .yVi ti v Ln p M LO 0 IA <tt c � c I� � GYl cn E � Gn m N CJ 7 T G C' C r C L� W C C C C E rt Pape 13 of 15 10/20/2018 Track your package or shipment with FedEx Tracking Table of Contents Travel History 10/20/2012 - Saturday 1019i2018 - FriGay TRACT( ANOTHER SHIPMENT 77352398130b �`t Delivered Saturday 10/20/2018 at 9:46 am DELIVERED Signed for by: R.PATRAIDAS GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM Charlotte, NC LIS TO EAST LONGMEADOW, MA US Shipment Facts 9A6 am Expand History V 3,04 pm OUR COMPANY MORE FROM FEDEX 'LC).ii 17edEx FedEx Won LFdEx CumpatiLde Our'roafcho Corperzii, RxSpcisA ifira' Deve3�per Rescx:rce Ceattcr Inac:."_r FedEx Cmos Boiucr r.:areef5 FOLLOW FEDEX Delivered FAST LONGMEADO'%Q, MA Shipment information sent to FedEx https:llwww.fedex.com/apps/fedextracki?action=track&tracknumbers=773523981306&locale=en_US&cntry_code=us Page 14 of 15 Table of Contents I Have Not Confirmed Sample Container Numbers With Lab Staff Before Relinquishing Over Samples J).oc# 277 Rev $ 2.07 Login Sample Receipt Checklist - (Rejection Criteria Listing - using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client MC7C5�'�Zve i Received By Date How were the samples In Cooler No Cooler received? Direct from Sampling time On Ice_ Ambient No Ice Melted Ice Were samples within By Gun # Actual Temp - Cl Temperature? 2-6°C By Blank # Actual Temp - Was Custody Seal Intact? Were Samples Tampered with? Was COC Relinquished ? Does Chain Agree With Samples? i Are there broken/leaking/loose caps on any samples? --- Is COC in ink/ Legible? --T-- Were samples received within holding time? �— Did COC include all Client Analysis Sampler Name pertinent Information? Project ID's - - Collection Dates/Times Are Sample labels filled out and legible? Are there Lab to Filters? �� Who was notified? Are there Rushes? T— Are there Short Holds? A Is there enough Volume? Is there Headspace where applicable? Proper Media/Containers Used? -� Were trip blanks received? Do all samples have the proper pH? jam' Acid Who was notified? I'm Who was notified? MS/M S D? Is splitting sampled required? On COC? �� Base ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 October 25, 2018 Rob Foster AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 Charlotte, NC 28208 Project Location: 5318 Morris Field Drive Client Job Number: Project Number: 6228-18-0503 Laboratory Work Order Number: 18JI I I I Enclosed are results of analyses for samples received by the laboratory on October 23, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 16 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 18J1111-01 Sample Preparation Information QC Data Volatile Organic Compounds by GC/MS B215524 Petroleum Hydrocarbons Analyses B215447 B215565 Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) B215520 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 5 5 8 9 9 9 10 10 10 11 11 12 13 14 Page 2 of 16 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce StreetEast Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 REPORT DATE: 10/25/2018 Charlotte, NC 28208 PURCHASE ORDER NUMBER: ATTN: Rob Foster PROJECT NUMBER: 6228-18-0503 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18J1111 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 5318 Morris Field Drive FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB Stockpile 18J1111-01 Soil SM 254OG SW-846 8015C SW-846 8260B Page 3 of 16 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method 8015B GRO elevated reporting limit for sample 18J1111-01 due to high concentrations of target compounds. For method 8260B elevated reporting limit for sample 18J1111-01 due to high concentrations of non -target compounds. SW-846 8015C Qualifications S-01 The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit required from high analyte concentration and/or matrix interferences. Analyze & Samples(s) Qualified: 2-Fluorobiphenyl 18J1111-01[Stockpile] Qualifications: RL-13 Elevated reporting limit due to high concentration of non -target compounds. Analyte & Samples(s) Qualified: 18JI I 11-01 [Stockpile] SW-846 8260B SW-846 8015C Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard. Diesel Range Organics (C 10-C28) is quantitated against a calibration made with a #2 fuel oil standard. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Project Manager Page 4 of 16 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1111 Date Received: 10/23/2018 Field Sample #: Stockpile Sampled: 10/22/2018 15:20 Sample ID: 18.11111-01 Samnle Matrix: Soil Sample Flags: RL-13 Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Benzene ND 0.79 0.095 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF Ethylbenzene 3.8 0.79 0.10 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF Toluene 1.8 0.79 0.13 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF m+p Xylene 8.7 1.6 0.20 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF o-Xylene 4.2 0.79 0.10 mg/Kg dry 10 SW-846 8260B 10/24/18 10/25/18 0:59 MFF Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 83.6 70-130 10/25/18 0:59 Toluene-d8 101 70-130 10/25/18 0:59 4-Bromofluorobenzene 98.2 70-130 10/25/18 0:59 Page 5 of 16 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1111 Date Received: 10/23/2018 Field Sample #: Stockpile Sampled: 10/22/2018 15:20 Samnle ID: 18J1111-01 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Gasoline Range Organics (GRO) 390 78 76 mg/Kg dry 50 SW-846 8015C 10/24/18 10/24/18 13:34 EEH Diesel Range Organics 7300 1100 410 mg/Kg dry 100 SW-846 8015C 10/23/18 10/25/18 10:35 RMW Surrogates % Recovery Recovery Limits Flag/Qual 1-Chloro-3-fluorobenzene 113 70-130 10/24/18 13:34 2-Fluorobiphenyl * 40-140 S-01 10/25/18 10:35 Page 6 of 16 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1111 Date Received: 10/23/2018 Field Sample #: Stockpile Sampled: 10/22/2018 15:20 Samnle ID: 18J1111-01 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 73.0 % Wt 1 SM 2540G 10/24/18 10/24/18 11:09 MJR Page 7 of 16 Table of Contents 40 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: % Solids-SM 2540G Lab Number [Field ID] Batch Date 18J 1111 -0 1 [Stockpile] B215520 10/24/18 Prep Method: SW-846 3546-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J 1111 -0 1 [Stockpile] B215447 30.3 1.00 10/23/18 Prep Method: SW-846 5035/5030B-SW-846 8015C Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1111-01[Stockpile] B215565 5.80 6.60 10/24/18 Prep Method: SW-846 5035-SW-846 8260B Sample Methanol Methanol Final Lab Number [Field ID] Batch Amount(g) Volume(mL) Aliquot(mL) Volume(mL) Date 18J 1111 -0 1 [Stockpile] B215524 5.65 6.53 0.1 50 10/24/18 Page 8 of 16 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215524 - SW-846 5035 Blank (B215524-BLK1) Prepared & Analyzed: 10/24/18 Benzene ND 0.050 mg/Kg wet Ethylbenzene ND 0.050 mg/Kg wet Toluene ND 0.050 mg/Kg wet m+p Xylene ND 0.10 mg/Kg wet o-Xylene ND 0.050 mg/Kg wet Surrogate:l,2-Dichloroethane-d4 Surrogate: Toluene-d8 Surrogate:4-Bromofluorobenzene LCS (B215524-BS1) 0.0210 0.0251 0.0244 mg/Kg wet mg/Kg wet mg/Kg wet 0.0250 84.1 0.0250 100 0.0250 97.7 Prepared & Analyzed: 10/24/18 70-130 70-130 70-130 Benzene 0.0110 0.0011 mg/Kg wet 0.0113 97.4 70-130 Ethylbenzene 0.0123 0.0011 mg/Kg wet 0.0113 108 70-130 Toluene 0.0119 0.0011 mg/Kg wet 0.0113 105 70-130 m+p Xylene 0.0237 0.0023 mg/Kg wet 0.0227 104 70-130 o-Xylene 0.0119 0.0011 mg/Kg wet 0.0113 105 70-130 Surrogate: 1,2-Dichloroethane-d4 0.0233 mg/Kg wet 0.0283 82.4 70-130 Surrogate: Toluene-d8 0.0285 mg/Kg wet 0.0283 101 70-130 Surrogate:4-Bromofluorobenzene 0.0277 mg/Kg wet 0.0283 97.8 70-130 LCS Dup (B215524-BSD1) Prepared & Analyzed: 10/24/18 Benzene 0.0111 0.0011 mg/Kg wet 0.0113 97.7 70-130 0.308 25 Ethylbenzene 0.0118 0.0011 mg/Kg wet 0.0113 104 70-130 3.58 25 Toluene 0.0118 0.0011 mg/Kg wet 0.0113 104 70-130 1.34 25 m+p Xylene 0.0230 0.0023 mg/Kg wet 0.0227 101 70-130 2.97 25 o-Xylene 0.0115 0.0011 mg/Kg wet 0.0113 102 70-130 3.19 25 Surrogate:l,2-Dichloroethane-d4 0.0238 mg/Kg wet 0.0283 84.1 70-130 Surrogate: Toluene-d8 0.0286 mg/Kg wet 0.0283 101 70-130 Surrogate:4-Bromofluorobenzene 0.0274 mg/Kg wet 0.0283 96.6 70-130 Page 9 of 16 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215447 - SW-846 3546 Blank (B215447-BLK1) Prepared: 10/23/18 Analyzed: 10/25/18 Diesel Range Organics 3.2 8.3 mg/Kg wet J Surrogate:2-Fluorobiphenyl LCS (B215447-BS1) 2.43 mg/Kg wet 3.33 72.9 Prepared: 10/23/18 Analyzed: 10/25/18 40-140 Diesel Range Organics 29.7 8.3 mg/Kg wet 33.3 89.2 40-140 Surrogate:2-Fluorobiphenyl LCS Dup (B215447-BSD1) 2.68 mg/Kg wet 3.33 80.4 Prepared: 10/23/18 Analyzed: 10/25/18 40-140 Diesel Range Organics 28.0 8.3 mg/Kg wet 33.3 84.0 40-140 5.98 Surrogate:2-Fluorobiphenyl Batch B215565 - SW-846 5035/5030B 2.45 mg/Kg wet 3.33 73.6 40-140 Blank (B215565-BLK1) Prepared & Analyzed: 10/24/18 Gasoline Range Organics (GRO) ND 1.0 mg/Kg wet Surrogate: 1-Chloro-3-fluorobenzene LCS (B215565-BSI) 17.3 µg/L 15.0 115 Prepared & Analyzed: 10/24/18 70-130 Gasoline Range Organics (GRO) 0.230 0.010 mg/Kg wet 0.250 92.0 80-120 Surrogate: 1-Chloro-3-fluorobenzene LCS Dup (B215565-BSD1) 17.1 µg/L 15.0 114 Prepared & Analyzed: 10/24/18 70-130 Gasoline Range Organics (GRO) 0.226 0.010 mg/Kg wet 0.250 90.4 80-120 1.80 30 Surrogate: 1-Chloro-3-fluorobenzene 17.4 µg/L 15.0 116 70-130 Page 10 of 16 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215520 - % Solids Duplicate (B215520-DUPI) Source: 18J1111-01 Prepared & Analyzed: 10/24/18 % Solids 72.2 % Wt 73.0 1.09 20 Page 11 of 16 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). RL-13 Elevated reporting limit due to high concentration of non -target compounds. S-01 The surrogate recovery for this sample is not available due to sample dilution below the surrogate reporting limit required from high analyte concentration and/or matrix interferences. Page 12 of 16 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8015C in Soil Gasoline Range Organics (GRO) NY,VA,NH,NC Diesel Range Organics NY,VA,NH,NC SW-846 8260B in Soil Benzene NC Ethylbenzene NC Toluene NC m+p Xylene NC o-Xylene NC SW-846 8260C in Soil Benzene CT,NH,ME,VA,NY Ethylbenzene CT,NH,ME,VA,NY Toluene CT,NH,ME,VA,NY m+p Xylene CT,NH,ME,VA,NY o-Xylene CT,NH,ME,VA,NY The CON -TEST Environmental Laboratory operates under the following certifications and accreditation: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2018 NC North Carolina Div. of Water Quality 652 12/31/2018 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2018 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 13 of 16 Table of Contents 10/23/2018 Track your package or shipment with Fedl Tracking EI ,, W :, .. Delivered Tuesday 10/23/2018 at 9.14- am DELIVERED Signed for by: B BECCA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO Charlotte. NC US LAST LCNGMEADOV%{ MA US Multiple -piece Shipment 3 Piece shipment TRACKING NUMBER SHIPPER CITY, STATE SHIP DATE STATUS DELIVERY DATE DESTINATIOWR£CIPIENT CITY, STATE 7735373D1375 CHARLOTTE, NO 10/22/2018 l U/2WO'l8 EAST LONGMEADOW, MA (master) 773537302393 CHARLOTTE, NO 10/22/2018 10/23/2018 EAST LONGMEADCW, MA 773537302485 (,HARLOTTE, NC 10/22/20'18 - 0I28/2018 LASI" LONGMEADOW, MA Shipment Facts TRACKING NUMBER SERVICE MASTER TRACKING NUMBER 77353730239 Fcedtx Standard OVemQhit 773537301375 WEIGHT DIMENSIONS DELIVERED TO 10 ihs / 454 kgs 13x10x9 in. Shippsng/Receiving TOTAL PIECES TOTAL SHIPMENT WEIGHT TERMS 3 10 Ill / 4.54 kgs Third Party PACKAGING SPECIAL HANDLING SECTION STANDARD TRANSIT Your Packaging Deliver Weekday, Additioral Handling 0 Surchirge 0/23/2018 by S:00 PM SHIP DATE ACTUAL DELIVERY L`� Tue. 10/23/2018 9.14 are Mon 10/22/2018 https://www.fedex. comlapps/fedextracki?action=track&tracknumbers=773537302393&locale=en_US&cntry_code=us Page 15 of 16 Table of Contents c� I Have Not Confirmed Sample Container r Numbers With Lab Staff Before Relinquishing Over Samples Login Sample Receipt Checklist - (Rejection Criteria Listing - using Acceptance Policy) Any False §tatement will be brought to the attention of the Client - State True or False Client VQ Received By Date Time 0 (mod How were the samples In Cooler -r No Cooler On Ice j No Ice received? Direct from Sampling Ambient Melted Ice Were samples within By Gun # S, Actual Temp - Temperature? 2-6°C By Blank # Actual Temp - Was Custody Seal Intact? N/V� Were Samples Tampered with? PJA Was COC Relinquished ? i Does Chain Agree With Samples? Are there broken/leaking/loose caps on any samples? Is COC in ink/ Legible? Did COC include all Client --r pertinent Information? Project Are Sample labels filled out and legible? Are there Lab to Filters? Are there Rushes? o' Are there Short Holds? Is there enough Volume? Is there Headspace where applicable? Proper Media/Containers Used? T— Were trip blanks received? Do all samples have the proper pH?(� Were samples received within holding time? -r 4nalysis Sampler Name T ID's Collection Dates/Times Who was notified? Who was notified? Who was notified? MS/MSD? Is splitting samples required? On COC? ! Acid Base ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 October 31, 2018 Rob Foster AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 Charlotte, NC 28208 Project Location: 5318 Morris Field Drive Client Job Number: Project Number: 6228-18-0503 Laboratory Work Order Number: 18J1112 Enclosed are results of analyses for samples received by the laboratory on October 22, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 78 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 18J1112-01 18J1112-02 18J1112-03 18J1112-04 18J1112-05 Sample Preparation Information QC Data Volatile Organic Compounds by GC/ 4S B215551 B215584 Semivolatile Organic Compounds by GUMS B215606 Petroleum Hydrocarbons Analyses - EPH B215618 Petroleum Hydrocarbons Analyses - VPH B215495 B215561 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 8 8 15 22 29 36 43 45 45 45 49 55 55 60 60 64 64 65 67 68 76 Page 2 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce StreetEast Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 REPORT DATE: 10/31/2018 Charlotte, NC 28208 PURCHASE ORDER NUMBER: ATTN: Rob Foster PROJECT NUMBER: 6228-18-0503 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18J1112 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 5318 Morris Field Drive FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB SW-1 18J1112-01 Soil MADEP-EPH-04-1.1 MADEP-VPH-Feb 2018 Rev 2.1 SM 254OG SW-846 8260B SW-846 8270D SW-2 18J1112-02 Soil MADEP-EPH-04-1.1 MADEP-VPH-Feb 2018 Rev 2.1 SM 2540G SW-846 8260B SW-846 8270D SW-3 18J1112-03 Soil MADEP-EPH-04-1.1 MADEP-VPH-Feb 2018 Rev 2.1 SM 254OG SW-846 8260B SW-846 8270D SW-4 18J1112-04 Soil MADEP-EPH-04-1.1 MADEP-VPH-Feb 2018 Rev 2.1 SM 254OG SW-846 8260B SW-846 8270D TB-3 18J1112-05 Soil MADEP-EPH-04-1.1 MADEP-VPH-Feb 2018 Rev 2.1 SM 254OG SW-846 8260B SW-846 8270D Page 3 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method MA VPH only adjusted hydrocarbon ranges were requested and reported. For method MA EPH, only hydrocarbon ranges were requested and reported. For method 8260B elevated reporting limits for sample 18J1112-05 due to high concentrations of target compounds. Page 4 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents Qualifications B 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 MADEP-EPH-04-1.1 Analyte is found in the associated laboratory blank as well as in the sample. Analyte & Samples(s) Qualified: n-Octadecane B215618-BS1,B215618-BSD1 MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is within method specified criteria. Analyte & Samples(s) Qualified: n-Nonane B215618-MS1 MADEP-VPH-Feb 2018 Rev 2.1 Qualifications: O-01 Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered with methanol, but with less than the method -specified amount. Analyte & Samples(s) Qualified: 18J1112-01[SW-1] RL-05 Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met. Analyte & Samples(s) Qualified: C5-C8 Aliphatics 18J1112-05[TB-3] SW-846 8260B Qualifications: L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Acetone B215551-BSDI Diisopropyl Ether (RIPE) B215551-BSDI Methyl tert-Butyl Ether (MTBE) B215551-BSDI Tetrahydrofuran B215551-BS1 RL-11 Elevated reporting limit due to high concentration of target compounds. Analyte & Samples(s) Qualified: 18JI I 12-05[TB-3] Qualifications: R-05 SW-846 8270D Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: Benzidine 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18JI I12-04[SW-4], 18J1112-05[TB-3], B215606-BLK1, B215606-BSI, B215606-BSD1 Page 5 of 78 ,con-testo ANALYTICAL LABORATORY Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Reported result is estimated. Analyte & Samples(s) Qualified: Benzidine B215606-BLKI, B215606-BSI, B215606-BSD1 V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Analyte & Samples(s) Qualified: Aniline 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3] Benzidine 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3], B215606-BLKI, B215606-BSI, B215606-BSD1 Hexachlorocyclopentadiene 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3] V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound. Analyte & Samples(s) Qualified: 4-Nitrophenol B215606-BS1,B215606-BSD1 V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. Analyte & Samples(s) Qualified: Pentachloronitrobenzene B215606-BLKI, B215606-BSI, B215606-BSD1 V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99. Reported result is estimated. Analyte & Samples(s) Qualified: 2,4-Dinitrophenol 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3] V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: 2,6-Dinitrotoluene 18J1112-01[SW-1], 18Jl112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3] 2-Nitroaniline 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3] 4-Nitrophenol 18JI112-01[SW-1], 18JI112-02[SW-2], 18JI112-03[SW-3], 18JI112-04[SW-4], 18JI112-05[TB-3], B215606-BLKI Benzoic Acid 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18J1112-04[SW-4], 18J1112-05[TB-3] V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: 3-Nitroaniline B215606-BLKI, B215606-BSI, B215606-BSDI 4-Chloroaniline 18J1112-01[SW-1], 18JI I12-02[SW-2], 18JI I12-03[SW-3], 18J1112-04[SW-4], 18JI I12-05[TB-3], B215606-BLKI, B215606-BSI, B215606-BSDI 4-Nitrophenol B215606-BLKI, B215606-BSI, B215606-BSDI Aniline 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18JI I12-04[SW-4], 18J1112-05[TB-3], B215606-BLKI, B215606-13SI, B215606-BSDI Benzidine 18J1112-01[SW-1], 18J1112-02[SW-2], 18J1112-03[SW-3], 18JI I12-04[SW-4], 18J1112-05[TB-3], B215606-BLKI, B215606-BSI, B215606-BSD1 Page 6 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028' FAX 413/525-6405 ` TEL. 413/525-2332 MADEP-EPH-04-1.1 SPE cartridge contamination with non -petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic range fraction in all samples in the batch. No significant modifications were made to the method. MADEP-VPH-Feb 2018 Rev 2.1 Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III. No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely covered by methanol in the proper containers specified on the chain -of -custody form unless specified in this narrative. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Lisa A. Worthington Project Manager Page 7 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-1 Sampled: 10/22/2018 13:50 Sample ID: 18J1112-01 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.12 0.028 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Acrylonitrile ND 0.0071 0.0030 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF tert-Amyl Methyl Ether (TAME) ND 0.0012 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Benzene ND 0.0024 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Bromobenzene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Bromochloromethane ND 0.0024 0.0017 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Bromodichloromethane ND 0.0024 0.00071 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 11:29 MFF Bromoform ND 0.0024 0.0017 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 11:29 MFF Bromomethane ND 0.012 0.0050 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 2-Butanone (MEK) ND 0.048 0.021 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF tert-Butyl Alcohol (TBA) ND 0.048 0.025 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF n-Butylbenzene 0.0015 0.0024 0.00083 mg/Kg dry 1 J SW-846 8260B 10/24/18 10/24/18 11:29 MFF sec-Butylbenzene 0.0015 0.0024 0.0012 mg/Kg dry 1 J SW-846 8260B 10/24/18 10/24/18 11:29 MFF tert-Butylbenzene ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0012 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Carbon Disulfide ND 0.0071 0.0051 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Carbon Tetrachloride ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Chlorobenzene ND 0.0024 0.00083 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 11:29 MFF Chlorodibromomethane ND 0.0012 0.00083 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 11:29 MFF Chloroethane ND 0.024 0.0018 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Chloroform ND 0.0048 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Chloromethane ND 0.012 0.0076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 2-Chlorotoluene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 4-Chlorotoluene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0024 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2-Dibromoethane (EDB) ND 0.0012 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Dibromomethane ND 0.0024 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2-Dichlorobenzene ND 0.0024 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,3-Dichlorobenzene ND 0.0024 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,4-Dichlorobenzene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF trans-1,4-Dichloro-2-butene ND 0.0048 0.0025 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Dichlorodifluoromethane (Freon 12) ND 0.024 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,1-Dichloroethane ND 0.0024 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2-Dichloroethane ND 0.0024 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1, 1 -Dichloroethylene ND 0.0048 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF cis-1,2-Dichloroethylene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF trans-1,2-Dichloroethylene ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2-Dichloropropane ND 0.0024 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,3-Dichloropropane ND 0.0012 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 2,2-Dichloropropane ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1, 1 -Dichloropropene ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF cis-1,3-Dichloropropene ND 0.0012 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF trans-1,3-Dichloropropene ND 0.0012 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Diethyl Ether ND 0.024 0.0021 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Page 8 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-1 Sampled: 10/22/2018 13:50 Sample ID: 18J1112-01 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0012 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,4-Dioxane ND 0.12 0.069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Ethylbenzene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Hexachlorobutadiene ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 2-Hexanone (MBK) ND 0.024 0.013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Isopropylbenzene (Cumene) ND 0.0024 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF p-Isopropyltoluene (p-Cymene) ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0048 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Methylene Chloride ND 0.024 0.0084 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 4-Methyl-2-pentanone (MIBK) ND 0.024 0.0090 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Naphthalene 0.0080 0.0048 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF n-Propylbenzene 0.0011 0.0024 0.00083 mg/Kg dry 1 J SW-846 8260B 10/24/18 10/24/18 11:29 MFF Styrene ND 0.0024 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0024 0.0021 mg/Kgdry 1 SW-8468260B 10/24/18 10/24/18 11:29 MFF 1,1,2,2-Tetrachloroethane ND 0.0024 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Tetrachloroethylene ND 0.0024 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Tetrahydrofuran ND 0.012 0.0026 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Toluene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2,3-Trichlorobenzene ND 0.0024 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2,4-Trichlorobenzene ND 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,3,5-Trichlorobenzene ND 0.0024 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1, 1, 1 -Trichloroethane ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,1,2-Trichloroethane ND 0.0024 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Trichloroethylene ND 0.0024 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Trichlorofluoromethane (Freon 11) ND 0.012 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,2,3-Trichloropropane ND 0.0024 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.012 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF (Freon 113) 1,2,4-Trimethylbenzene 0.0038 0.0024 0.00095 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF 1,3,5-Trimethylbenzene 0.00075 0.0024 0.00071 mg/Kg dry 1 J SW-846 8260B 10/24/18 10/24/18 11:29 MFF Vinyl Chloride ND 0.012 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF m+p Xylene ND 0.0048 0.0020 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF o-Xylene ND 0.0024 0.00083 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:29 MFF Surrogates % Recovery Recovery Limits Flag/Qua] 1,2-Dichloroethane-d4 106 70-130 10/24/18 11:29 Toluene-d8 103 70-130 10/24/18 11:29 4-Bromofluorobenzene 110 70-130 10/24/18 11:29 Page 9 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-1 Sampled: 10/22/2018 13:50 Samnle ID: 18J1112-01 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.23 0.069 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Acenaphthylene ND 0.23 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Acetophenone ND 0.46 0.091 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Aniline ND 0.46 0.13 mg/Kg dry 1 V-05, V-34 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Anthracene ND 0.23 0.067 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Benzidine ND 0.90 0.58 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Benzo(a)anthracene ND 0.23 0.061 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Benzo(a)pyrene ND 0.23 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Benzo(b)fluoranthene ND 0.23 0.065 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Benzo(g,h,i)perylene ND 0.23 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Benzo(k)fluoranthene ND 0.23 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Benzoic Acid ND 1.4 0.25 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Bis(2-chloroethoxy)methane ND 0.46 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Bis(2-chloroethyl)ether ND 0.46 0.091 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Bis(2-chloroisopropyl)ether ND 0.46 0.099 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Bis(2-Ethylhexyl)phthalate ND 0.46 0.18 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 4-Bromophenylphenylether ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Butylbenzylphthalate ND 0.46 0.11 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:06 BGL Carbazole ND 0.23 0.060 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:06 BGL 4-Chloroaniline ND 0.90 0.11 mg/Kg dry 1 V-34 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 4-Chloro-3-methylphenol ND 0.90 0.099 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2-Chloronaphthalene ND 0.46 0.087 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2-Chlorophenol ND 0.46 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 4-Chlorophenylphenylether ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Chrysene ND 0.23 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Dibenz(a,h)anthracene ND 0.23 0.14 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Dibenzofman ND 0.46 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Di-n-butylphthalate ND 0.46 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 1,2-Dichlorobenzene ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 1,3-Dichlorobenzene ND 0.46 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 1,4-Dichlorobenzene ND 0.46 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 3,3-Dichlorobenzidine ND 0.23 0.071 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2,4-Dichlorophenol ND 0.46 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Diethylphthalate ND 0.46 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2,4-Dimethylphenol ND 0.46 0.086 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Dimethylphthalate ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 4,6-Dinitro-2-methylphenol ND 0.46 0.44 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2,4-Dinitrophenol ND 0.90 0.26 mg/Kg dry 1 V-19 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2,4-Dinitrotoluene ND 0.46 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2,6-Dinitrotoluene ND 0.46 0.082 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Di-n-octylphthalate ND 0.46 0.24 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.46 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Fluoranthene ND 0.23 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Flumene 0.10 0.23 0.075 mg/Kg dry 1 J SW-846 8270D 10/24/18 10/29/18 18:06 BGL Page 10 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-1 Sampled: 10/22/2018 13:50 Samnle ID: 18J1112-01 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Hexachlorobutadiene ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Hexachlorocyclopentadiene ND 0.46 0.098 mg/Kg dry 1 V-05 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Hexachloroethane ND 0.46 0.092 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Indeno(1,2,3-cd)pyrene ND 0.23 0.17 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Isophorone ND 0.46 0.090 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 1-Methylnaphthalene 0.39 0.23 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2-Methylnaphthalene 0.66 0.23 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2-Methylphenol ND 0.46 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 3/4-Methylphenol ND 0.46 0.15 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Naphthalene 0.13 0.23 0.12 mg/Kg dry 1 J SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2-Nitroaniline ND 0.46 0.077 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 3-Nitroaniline ND 0.46 0.067 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 4-Nitroaniline ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Nitrobenzene ND 0.46 0.087 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2-Nitrophenol ND 0.46 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 4-Nitrophenol ND 0.90 0.10 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:06 BGL N-Nitrosodimethylamine ND 0.46 0.29 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL N-Nitrosodiphenylamine ND 0.46 0.095 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL N-Nitrosodi-n-propylamine ND 0.46 0.095 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Pentachloronitrobenzene ND 0.46 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Pentachlorophenol ND 0.46 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Phenanthrene 0.22 0.23 0.12 mg/Kg dry 1 J SW-846 8270D 10/24/18 10/29/18 18:06 BGL Phenol ND 0.46 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Pyrene 0.10 0.23 0.076 mg/Kg dry 1 J SW-846 8270D 10/24/18 10/29/18 18:06 BGL Pyridine ND 0.46 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 1,2,4,5-Tetrachlorobenzene ND 0.46 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 1,2,4-Trichlorobenzene ND 0.46 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2,4,5-Trichlorophenol ND 0.46 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL 2,4,6-Trichlorophenol ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:06 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 63.3 30-130 10/29/18 18:06 Phenol-d6 71.1 30-130 10/29/18 18:06 Nitrobenzene-d5 63.8 30-130 10/29/18 18:06 2-Fluorobiphenyl 56.4 30-130 10/29/18 18:06 2,4,6-Tribromophenol 95.8 30-130 10/29/18 18:06 p-Terphenyl-dl4 69.6 30-130 10/29/18 18:06 Page 11 of 78 Table of Contents 40 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-1 Sampled: 10/22/2018 13:50 Samnle ID: 18J1112-01 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C9-C18 Aliphatics 74 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW C19-C36 Aliphatics 25 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW Unadjusted C11-C22 Aromatics 57 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW C11-C22 Aromatics 55 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 2:10 RMW Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 64.7 40-140 10/29/18 2:10 o-Terphenyl(OTP) 71.2 40-140 10/29/18 2:10 2-Bromonaphthalene 94.8 40-140 10/29/18 2:10 2-Fluorobiphenyl 106 40-140 10/29/18 2:10 Page 12 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-1 Sampled: 10/22/2018 13:50 Sample ID: 18J1112-01 Samnle Matrix: Soil Sample Flags: 0-01 Petroleum Hydrocarbons Analyses - VPH Soil/Methanol Preservation Ratio: 1.53 Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C5-C8 Aliphatics ND 13 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 21:21 EEH Rev 2.1 C9-C12 Aliphatics ND 13 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 21:21 EEH Rev 2.1 C9-C10 Aromatics 15 13 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 21:21 EEH Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 105 70-130 10/24/18 21:21 2,5-Dibromotoluene (PID) 104 70-130 10/24/18 21:21 Page 13 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-1 Sampled: 10/22/2018 13:50 Samnle ID: 18J1112-01 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 73.1 % Wt 1 SM 2540G 10/27/18 10/28/18 15:28 BLM Page 14 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-2 Sampled: 10/22/2018 14:05 Sample ID: 18J1112-02 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.13 0.030 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Acrylonitrile ND 0.0076 0.0032 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF tert-Amyl Methyl Ether (TAME) ND 0.0013 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Benzene ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Bromobenzene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Bromochloromethane ND 0.0025 0.0018 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Bromodichloromethane ND 0.0025 0.00076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Bromoform ND 0.0025 0.0018 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Bromomethane ND 0.013 0.0053 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 2-Butanone (MEK) ND 0.051 0.022 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF tert-Butyl Alcohol (TBA) ND 0.051 0.027 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF n-Butylbenzene ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF sec-Butylbenzene ND 0.0025 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF tert-Butylbenzene ND 0.0025 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0013 0.00076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Carbon Disulfide ND 0.0076 0.0055 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Carbon Tetrachloride ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Chlorobenzene ND 0.0025 0.00089 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 11:54 MFF Chlorodibromomethane ND 0.0013 0.00089 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 11:54 MFF Chloroethane ND 0.025 0.0019 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Chloroform ND 0.0051 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Chloromethane ND 0.013 0.0081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 2-Chlorotoluene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 4-Chlorotoluene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0025 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2-Dibromoethane (EDB) ND 0.0013 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Dibromomethane ND 0.0025 0.00076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2-Dichlorobenzene ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,3-Dichlorobenzene ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,4-Dichlorobenzene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF trans-1,4-Dichloro-2-butene ND 0.0051 0.0027 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Dichlorodifluoromethane (Freon 12) ND 0.025 0.0017 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,1-Dichloroethane ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2-Dichloroethane ND 0.0025 0.0017 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1, 1 -Dichloroethylene ND 0.0051 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF cis-1,2-Dichloroethylene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF trans-1,2-Dichloroethylene ND 0.0025 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2-Dichloropropane ND 0.0025 0.0017 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,3-Dichloropropane ND 0.0013 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 2,2-Dichloropropane ND 0.0025 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1, 1 -Dichloropropene ND 0.0025 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF cis-1,3-Dichloropropene ND 0.0013 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF trans-1,3-Dichloropropene ND 0.0013 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Diethyl Ether ND 0.025 0.0023 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Page 15 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-2 Sampled: 10/22/2018 14:05 Sample ID: 18J1112-02 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0013 0.00076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,4-Dioxane ND 0.13 0.073 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Ethylbenzene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Hexachlorobutadiene ND 0.0025 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 2-Hexanone (MBK) ND 0.025 0.014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Isopropylbenzene (Cumene) ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF p-Isopropyltoluene (p-Cymene) ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0051 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Methylene Chloride ND 0.025 0.0090 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 4-Methyl-2-pentanone (MIBK) ND 0.025 0.0097 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Naphthalene ND 0.0051 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF n-Propylbenzene ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Styrene ND 0.0025 0.00076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0025 0.0023 mg/Kg dry 1 SW-8468260B 10/24/18 10/24/18 11:54 MFF 1,1,2,2-Tetrachloroethane ND 0.0025 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Tetrachloroethylene ND 0.0025 0.0017 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Tetrahydrofuran ND 0.013 0.0028 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Toluene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2,3-Trichlorobenzene ND 0.0025 0.00076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2,4-Trichlorobenzene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,3,5-Trichlorobenzene ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1, 1, 1 -Trichloroethane ND 0.0025 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,1,2-Trichloroethane ND 0.0025 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Trichloroethylene ND 0.0025 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Trichlorofluoromethane (Freon 11) ND 0.013 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,2,3-Trichloropropane ND 0.0025 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.013 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0025 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF 1,3,5-Trimethylbenzene ND 0.0025 0.00076 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Vinyl Chloride ND 0.013 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF m+p Xylene ND 0.0051 0.0022 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF o-Xylene ND 0.0025 0.00089 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 11:54 MFF Surrogates % Recovery Recovery Limits Flag/Qua] 1,2-Dichloroethane-d4 107 70-130 10/24/18 11:54 Toluene-d8 104 70-130 10/24/18 11:54 4-Bromofluorobenzene 109 70-130 10/24/18 11:54 Page 16 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-2 Sampled: 10/22/2018 14:05 Samnle ID: 18J1112-02 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.24 0.073 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Acenaphthylene ND 0.24 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Acetophenone ND 0.49 0.096 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Aniline ND 0.49 0.14 mg/Kg dry 1 V-05, V-34 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Anthracene ND 0.24 0.070 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Benzidine ND 0.95 0.61 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Benzo(a)anthracene ND 0.24 0.065 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Benzo(a)pyrene ND 0.24 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Benzo(b)fluoranthene ND 0.24 0.069 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Benzo(g,h,i)perylene ND 0.24 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Benzo(k)fluoranthene ND 0.24 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Benzoic Acid ND 1.4 0.26 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Bis(2-chloroethoxy)methane ND 0.49 0.093 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Bis(2-chloroethyl)ether ND 0.49 0.096 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Bis(2-chloroisopropyl)ether ND 0.49 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Bis(2-Ethylhexyl)phthalate ND 0.49 0.19 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 4-Bromophenylphenylether ND 0.49 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Butylbenzylphthalate ND 0.49 0.12 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:32 BGL Carbazole ND 0.24 0.063 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:32 BGL 4-Chloroaniline ND 0.95 0.11 mg/Kg dry 1 V-34 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 4-Chloro-3-methylphenol ND 0.95 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2-Chloronaphthalene ND 0.49 0.092 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2-Chlorophenol ND 0.49 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 4-Chlorophenylphenylether ND 0.49 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Chrysene ND 0.24 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Dibenz(a,h)anthracene ND 0.24 0.15 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Dibenzofman ND 0.49 0.085 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Di-n-butylphthalate ND 0.49 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 1,2-Dichlorobenzene ND 0.49 0.086 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 1,3-Dichlorobenzene ND 0.49 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 1,4-Dichlorobenzene ND 0.49 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 3,3-Dichlorobenzidine ND 0.24 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2,4-Dichlorophenol ND 0.49 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Diethylphthalate ND 0.49 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2,4-Dimethylphenol ND 0.49 0.091 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Dimethylphthalate ND 0.49 0.086 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 4,6-Dinitro-2-methylphenol ND 0.49 0.46 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2,4-Dinitrophenol ND 0.95 0.28 mg/Kg dry 1 V-19 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2,4-Dinitrotoluene ND 0.49 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2,6-Dinitrotoluene ND 0.49 0.086 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Di-n-octylphthalate ND 0.49 0.26 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.49 0.079 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:32 BGL Fluoranthene ND 0.24 0.081 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:32 BGL Flumene ND 0.24 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Page 17 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-2 Sampled: 10/22/2018 14:05 Samnle ID: 18J1112-02 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.49 0.086 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Hexachlorobutadiene ND 0.49 0.086 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Hexachlorocyclopentadiene ND 0.49 0.10 mg/Kg dry 1 V-05 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Hexachloroethane ND 0.49 0.098 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Indeno(1,2,3-cd)pyrene ND 0.24 0.18 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Isophorone ND 0.49 0.095 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 1-Methylnaphthalene ND 0.24 0.093 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2-Methylnaphthalene ND 0.24 0.085 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2-Methylphenol ND 0.49 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 3/4-Methylphenol ND 0.49 0.16 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Naphthalene ND 0.24 0.13 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2-Nitroaniline ND 0.49 0.082 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 3-Nitroaniline ND 0.49 0.070 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 4-Nitroaniline ND 0.49 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Nitrobenzene ND 0.49 0.092 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2-Nitrophenol ND 0.49 0.13 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 4-Nitrophenol ND 0.95 0.11 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:32 BGL N-Nitrosodimethylamine ND 0.49 0.31 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL N-Nitrosodiphenylamine ND 0.49 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL N-Nitrosodi-n-propylamine ND 0.49 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Pentachloronitrobenzene ND 0.49 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Pentachlorophenol ND 0.49 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Phenanthrene ND 0.24 0.13 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Phenol ND 0.49 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Pyrene ND 0.24 0.081 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Pyridine ND 0.49 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 1,2,4,5-Tetrachlorobenzene ND 0.49 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 1,2,4-Trichlorobenzene ND 0.49 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2,4,5-Trichlorophenol ND 0.49 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL 2,4,6-Trichlorophenol ND 0.49 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:32 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 58.7 30-130 10/29/18 18:32 Phenol-d6 64.6 30-130 10/29/18 18:32 Nitrobenzene-d5 59.2 30-130 10/29/18 18:32 2-Fluorobiphenyl 53.3 30-130 10/29/18 18:32 2,4,6-Tribromophenol 86.9 30-130 10/29/18 18:32 p-Terphenyl-dl4 65.9 30-130 10/29/18 18:32 Page 18 of 78 Table of Contents 40 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-2 Sampled: 10/22/2018 14:05 Samnle ID: 18J1112-02 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C9-C18 Aliphatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW C19-C36 Aliphatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW Unadjusted C11-C22 Aromatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW C11-C22 Aromatics ND 15 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:06 RMW Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 67.3 40-140 10/29/18 3:06 o-Terphenyl(OTP) 72.4 40-140 10/29/18 3:06 2-Bromonaphthalene 97.0 40-140 10/29/18 3:06 2-Fluorobiphenyl 103 40-140 10/29/18 3:06 Page 19 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-2 Sampled: 10/22/2018 14:05 Sample ID: 18J1112-02 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - VPH Soil/Methanol Preservation Ratio: 1.00 Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C5-C8 Aliphatics ND 19 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 21:51 EEH Rev 2.1 C9-C12 Aliphatics ND 19 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 21:51 EEH Rev 2.1 C9-C10 Aromatics ND 19 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 21:51 EEH Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 114 70-130 10/24/18 21:51 2,5-Dibromotoluene (PID) 103 70-130 10/24/18 21:51 Page 20 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-2 Sampled: 10/22/2018 14:05 Samnle ID: 18J1112-02 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 68.2 % Wt 1 SM 2540G 10/27/18 10/28/18 15:28 BLM Page 21 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-3 Sampled: 10/22/2018 14:25 Sample ID: 18J1112-03 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.10 0.024 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Acrylonitrile ND 0.0061 0.0025 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF tert-Amyl Methyl Ether (TAME) ND 0.0010 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Benzene ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Bromobenzene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Bromochloromethane ND 0.0020 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Bromodichloromethane ND 0.0020 0.00061 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Bromoform ND 0.0020 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Bromomethane ND 0.010 0.0043 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 2-Butanone (MEK) ND 0.041 0.018 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF tert-Butyl Alcohol (TBA) ND 0.041 0.021 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF n-Butylbenzene ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF sec-Butylbenzene ND 0.0020 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF tert-Butylbenzene ND 0.0020 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0010 0.00061 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Carbon Disulfide ND 0.0061 0.0044 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Carbon Tetrachloride ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Chlorobenzene ND 0.0020 0.00071 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 12:18 MFF Chlorodibromomethane ND 0.0010 0.00071 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 12:18 MFF Chloroethane ND 0.020 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Chloroform ND 0.0041 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Chloromethane ND 0.010 0.0065 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 2-Chlorotoluene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 4-Chlorotoluene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2-Dibromoethane (EDB) ND 0.0010 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Dibromomethane ND 0.0020 0.00061 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2-Dichlorobenzene ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,3-Dichlorobenzene ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,4-Dichlorobenzene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF trans-1,4-Dichloro-2-butene ND 0.0041 0.0021 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Dichlorodifluoromethane (Freon 12) ND 0.020 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,1-Dichloroethane ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2-Dichloroethane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1, 1 -Dichloroethylene ND 0.0041 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF cis-1,2-Dichloroethylene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF trans-1,2-Dichloroethylene ND 0.0020 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2-Dichloropropane ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,3-Dichloropropane ND 0.0010 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 2,2-Dichloropropane ND 0.0020 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1, 1 -Dichloropropene ND 0.0020 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF cis-1,3-Dichloropropene ND 0.0010 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF trans-1,3-Dichloropropene ND 0.0010 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Diethyl Ether ND 0.020 0.0018 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Page 22 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-3 Sampled: 10/22/2018 14:25 Sample ID: 18J1112-03 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0010 0.00061 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,4-Dioxane ND 0.10 0.059 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Ethylbenzene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Hexachlorobutadiene ND 0.0020 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 2-Hexanone (MBK) ND 0.020 0.011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Isopropylbenzene (Cumene) ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF p-Isopropyltoluene (p-Cymene) ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0041 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Methylene Chloride ND 0.020 0.0072 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 4-Methyl-2-pentanone (MIBK) ND 0.020 0.0077 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Naphthalene ND 0.0041 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF n-Propylbenzene ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Styrene ND 0.0020 0.00061 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0020 0.0018 mg/Kgdry 1 SW-8468260B 10/24/18 10/24/18 12:18 MFF 1,1,2,2-Tetrachloroethane ND 0.0020 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Tetrachloroethylene ND 0.0020 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Tetrahydrofuran ND 0.010 0.0022 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Toluene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2,3-Trichlorobenzene ND 0.0020 0.00061 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2,4-Trichlorobenzene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,3,5-Trichlorobenzene ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1, 1, 1 -Trichloroethane ND 0.0020 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,1,2-Trichloroethane ND 0.0020 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Trichloroethylene ND 0.0020 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Trichlorofluoromethane (Freon 11) ND 0.010 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,2,3-Trichloropropane ND 0.0020 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.010 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0020 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF 1,3,5-Trimethylbenzene ND 0.0020 0.00061 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Vinyl Chloride ND 0.010 0.0011 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF m+p Xylene ND 0.0041 0.0017 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF o-Xylene ND 0.0020 0.00071 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 12:18 MFF Surrogates % Recovery Recovery Limits Flag/Qua] 1,2-Dichloroethane-d4 107 70-130 10/24/18 12:18 Toluene-d8 105 70-130 10/24/18 12:18 4-Bromofluorobenzene 107 70-130 10/24/18 12:18 Page 23 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-3 Sampled: 10/22/2018 14:25 Samnle ID: 18J1112-03 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.22 0.067 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Acenaphthylene ND 0.22 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Acetophenone ND 0.45 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Aniline ND 0.45 0.13 mg/Kg dry 1 V-05, V-34 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Anthracene ND 0.22 0.064 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Benzidine ND 0.87 0.56 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Benzo(a)anthracene ND 0.22 0.059 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Benzo(a)pyrene ND 0.22 0.069 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Benzo(b)fluoranthene ND 0.22 0.063 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Benzo(g,h,i)perylene ND 0.22 0.098 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Benzo(k)fluoranthene ND 0.22 0.069 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Benzoic Acid ND 1.3 0.24 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Bis(2-chloroethoxy)methane ND 0.45 0.085 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Bis(2-chloroethyl)ether ND 0.45 0.088 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Bis(2-chloroisopropyl)ether ND 0.45 0.096 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Bis(2-Ethylhexyl)phthalate ND 0.45 0.17 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 4-Bromophenylphenylether ND 0.45 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Butylbenzylphthalate ND 0.45 0.11 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:59 BGL Carbazole ND 0.22 0.058 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 18:59 BGL 4-Chloroaniline ND 0.87 0.10 mg/Kg dry 1 V-34 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 4-Chloro-3-methylphenol ND 0.87 0.096 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2-Chloronaphthalene ND 0.45 0.084 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2-Chlorophenol ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 4-Chlorophenylphenylether ND 0.45 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Chrysene ND 0.22 0.069 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Dibenz(a,h)anthracene ND 0.22 0.14 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Dibenzofman ND 0.45 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Di-n-butylphthalate ND 0.45 0.097 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 1,2-Dichlorobenzene ND 0.45 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 1,3-Dichlorobenzene ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 1,4-Dichlorobenzene ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 3,3-Dichlorobenzidine ND 0.22 0.068 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2,4-Dichlorophenol ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Diethylphthalate ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2,4-Dimethylphenol ND 0.45 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Dimethylphthalate ND 0.45 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 4,6-Dinitro-2-methylphenol ND 0.45 0.42 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2,4-Dinitrophenol ND 0.87 0.25 mg/Kg dry 1 V-19 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2,4-Dinitrotoluene ND 0.45 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2,6-Dinitrotoluene ND 0.45 0.079 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Di-n-octylphthalate ND 0.45 0.23 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.45 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Fluoranthene ND 0.22 0.073 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Flumene ND 0.22 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Page 24 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-3 Sampled: 10/22/2018 14:25 Samnle ID: 18J1112-03 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.45 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Hexachlorobutadiene ND 0.45 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Hexachlorocyclopentadiene ND 0.45 0.094 mg/Kg dry 1 V-05 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Hexachloroethane ND 0.45 0.089 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Indeno(1,2,3-cd)pyrene ND 0.22 0.16 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Isophorone ND 0.45 0.087 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 1-Methylnaphthalene ND 0.22 0.085 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2-Methylnaphthalene ND 0.22 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2-Methylphenol ND 0.45 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 3/4-Methylphenol ND 0.45 0.14 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Naphthalene ND 0.22 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2-Nitroaniline ND 0.45 0.075 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 3-Nitroaniline ND 0.45 0.064 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 4-Nitroaniline ND 0.45 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Nitrobenzene ND 0.45 0.084 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2-Nitrophenol ND 0.45 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 4-Nitrophenol ND 0.87 0.097 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 18:59 BGL N-Nitrosodimethylamine ND 0.45 0.28 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL N-Nitrosodiphenylamine ND 0.45 0.092 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL N-Nitrosodi-n-propylamine ND 0.45 0.092 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Pentachloronitrobenzene ND 0.45 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Pentachlorophenol ND 0.45 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Phenanthrene ND 0.22 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Phenol ND 0.45 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Pyrene ND 0.22 0.073 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Pyridine ND 0.45 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 1,2,4,5-Tetrachlorobenzene ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 1,2,4-Trichlorobenzene ND 0.45 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2,4,5-Trichlorophenol ND 0.45 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL 2,4,6-Trichlorophenol ND 0.45 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 18:59 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 69.8 30-130 10/29/18 18:59 Phenol-d6 77.2 30-130 10/29/18 18:59 Nitrobenzene-d5 78.3 30-130 10/29/18 18:59 2-Fluorobiphenyl 59.7 30-130 10/29/18 18:59 2,4,6-Tribromophenol 100 30-130 10/29/18 18:59 p-Terphenyl-dl4 70.6 30-130 10/29/18 18:59 Page 25 of 78 Table of Contents 40 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-3 Sampled: 10/22/2018 14:25 Samnle ID: 18J1112-03 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C9-C18 Aliphatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW C19-C36 Aliphatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW Unadjusted C11-C22 Aromatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW C11-C22 Aromatics ND 13 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:24 RMW Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 71.6 40-140 10/29/18 3:24 o-Terphenyl(OTP) 78.5 40-140 10/29/18 3:24 2-Bromonaphthalene 97.9 40-140 10/29/18 3:24 2-Fluorobiphenyl 107 40-140 10/29/18 3:24 Page 26 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-3 Sampled: 10/22/2018 14:25 Sample ID: 18J1112-03 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - VPH Soil/Methanol Preservation Ratio: 1.12 Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C5-C8 Aliphatics ND 15 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 22:20 EEH Rev 2.1 C9-C12 Aliphatics ND 15 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 22:20 EEH Rev 2.1 C9-C10 Aromatics ND 15 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/24/18 10/24/18 22:20 EEH Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 115 70-130 10/24/18 22:20 2,5-Dibromotoluene (PID) 103 70-130 10/24/18 22:20 Page 27 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-3 Sampled: 10/22/2018 14:25 Samnle ID: 18J1112-03 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 75.8 % Wt 1 SM 2540G 10/27/18 10/28/18 15:28 BLM Page 28 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-4 Sampled: 10/22/2018 14:40 Sample ID: 18J1112-04 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.12 0.027 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Acrylonitrile ND 0.0069 0.0029 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF tert-Amyl Methyl Ether (TAME) ND 0.0012 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Benzene ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Bromobenzene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Bromochloromethane ND 0.0023 0.0016 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Bromodichloromethane ND 0.0023 0.00069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Bromoform ND 0.0023 0.0016 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Bromomethane ND 0.012 0.0049 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 2-Butanone (MEK) ND 0.046 0.020 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF tert-Butyl Alcohol (TBA) ND 0.046 0.024 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF n-Butylbenzene ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF sec-Butylbenzene ND 0.0023 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF tert-Butylbenzene ND 0.0023 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0012 0.00069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Carbon Disulfide ND 0.0069 0.0050 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Carbon Tetrachloride ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Chlorobenzene ND 0.0023 0.00081 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 13:58 MFF Chlorodibromomethane ND 0.0012 0.00081 mg/Kg dry I SW-846 8260B 10/24/18 10/24/18 13:58 MFF Chloroethane ND 0.023 0.0017 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Chloroform ND 0.0046 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Chloromethane ND 0.012 0.0074 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 2-Chlorotoluene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 4-Chlorotoluene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0023 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2-Dibromoethane (EDB) ND 0.0012 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Dibromomethane ND 0.0023 0.00069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2-Dichlorobenzene ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,3-Dichlorobenzene ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,4-Dichlorobenzene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF trans-1,4-Dichloro-2-butene ND 0.0046 0.0024 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Dichlorodifluoromethane (Freon 12) ND 0.023 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,1-Dichloroethane ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2-Dichloroethane ND 0.0023 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1, 1 -Dichloroethylene ND 0.0046 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF cis-1,2-Dichloroethylene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF trans-1,2-Dichloroethylene ND 0.0023 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2-Dichloropropane ND 0.0023 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,3-Dichloropropane ND 0.0012 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 2,2-Dichloropropane ND 0.0023 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1, 1 -Dichloropropene ND 0.0023 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF cis-1,3-Dichloropropene ND 0.0012 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF trans-1,3-Dichloropropene ND 0.0012 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Diethyl Ether ND 0.023 0.0021 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Page 29 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-4 Sampled: 10/22/2018 14:40 Sample ID: 18J1112-04 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0012 0.00069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,4-Dioxane ND 0.12 0.067 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Ethylbenzene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Hexachlorobutadiene ND 0.0023 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 2-Hexanone (MBK) ND 0.023 0.013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Isopropylbenzene (Cumene) ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF p-Isopropyltoluene (p-Cymene) ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0046 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Methylene Chloride ND 0.023 0.0082 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 4-Methyl-2-pentanone (MIBK) ND 0.023 0.0088 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Naphthalene ND 0.0046 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF n-Propylbenzene ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Styrene ND 0.0023 0.00069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0023 0.0021 mg/Kg dry 1 SW-8468260B 10/24/18 10/24/18 13:58 MFF 1,1,2,2-Tetrachloroethane ND 0.0023 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Tetrachloroethylene ND 0.0023 0.0015 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Tetrahydrofuran ND 0.012 0.0025 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Toluene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2,3-Trichlorobenzene ND 0.0023 0.00069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2,4-Trichlorobenzene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,3,5-Trichlorobenzene ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1, 1, 1 -Trichloroethane ND 0.0023 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,1,2-Trichloroethane ND 0.0023 0.0014 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Trichloroethylene ND 0.0023 0.0012 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Trichlorofluoromethane (Freon 11) ND 0.012 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,2,3-Trichloropropane ND 0.0023 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.012 0.0010 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF (Freon 113) 1,2,4-Trimethylbenzene ND 0.0023 0.00092 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF 1,3,5-Trimethylbenzene ND 0.0023 0.00069 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Vinyl Chloride ND 0.012 0.0013 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF m+p Xylene ND 0.0046 0.0020 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF o-Xylene ND 0.0023 0.00081 mg/Kg dry 1 SW-846 8260B 10/24/18 10/24/18 13:58 MFF Surrogates % Recovery Recovery Limits Flag/Qua] 1,2-Dichloroethane-d4 108 70-130 10/24/18 13:58 Toluene-d8 105 70-130 10/24/18 13:58 4-Bromofluorobenzene 106 70-130 10/24/18 13:58 Page 30 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-4 Sampled: 10/22/2018 14:40 Samnle ID: 18J1112-04 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene 0.88 0.24 0.071 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Acenaphthylene ND 0.24 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Acetophenone ND 0.47 0.093 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Aniline ND 0.47 0.13 mg/Kg dry 1 V-05, V-34 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Anthracene 0.31 0.24 0.068 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Benzidine ND 0.91 0.59 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Benzo(a)anthracene ND 0.24 0.062 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Benzo(a)pyrene ND 0.24 0.073 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Benzo(b)fluoranthene ND 0.24 0.066 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Benzo(g,h,i)perylene ND 0.24 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Benzo(k)fluoranthene ND 0.24 0.073 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Benzoic Acid ND 1.4 0.25 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Bis(2-chloroethoxy)methane ND 0.47 0.090 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Bis(2-chloroethyl)ether ND 0.47 0.093 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Bis(2-chloroisopropyl)ether ND 0.47 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Bis(2-Ethylhexyl)phthalate ND 0.47 0.18 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 4-Bromophenylphenylether ND 0.47 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Butylbenzylphthalate ND 0.47 0.11 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 19:26 BGL Carbazole ND 0.24 0.061 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 19:26 BGL 4-Chloroaniline ND 0.91 0.11 mg/Kg dry 1 V-34 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 4-Chloro-3-methylphenol ND 0.91 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2-Chloronaphthalene ND 0.47 0.089 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2-Chlorophenol ND 0.47 0.084 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 4-Chlorophenylphenylether ND 0.47 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Chrysene ND 0.24 0.073 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Dibenz(a,h)anthracene ND 0.24 0.14 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Dibenzofman ND 0.47 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Di-n-butylphthalate ND 0.47 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 1,2-Dichlorobenzene ND 0.47 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 1,3-Dichlorobenzene ND 0.47 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 1,4-Dichlorobenzene ND 0.47 0.084 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 3,3-Dichlorobenzidine ND 0.24 0.072 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2,4-Dichlorophenol ND 0.47 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Diethylphthalate ND 0.47 0.084 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2,4-Dimethylphenol ND 0.47 0.087 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Dimethylphthalate ND 0.47 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 4,6-Dinitro-2-methylphenol ND 0.47 0.45 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2,4-Dinitrophenol ND 0.91 0.27 mg/Kg dry 1 V-19 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2,4-Dinitrotoluene ND 0.47 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2,6-Dinitrotoluene ND 0.47 0.083 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Di-n-octylphthalate ND 0.47 0.25 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.47 0.076 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 19:26 BGL Fluoranthene 0.27 0.24 0.078 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 19:26 BGL Flumene 1.9 0.24 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Page 31 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-4 Sampled: 10/22/2018 14:40 Samnle ID: 18J1112-04 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.47 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Hexachlorobutadiene ND 0.47 0.083 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Hexachlorocyclopentadiene ND 0.47 0.10 mg/Kg dry 1 V-05 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Hexachloroethane ND 0.47 0.094 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Indeno(1,2,3-cd)pyrene ND 0.24 0.17 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Isophorone ND 0.47 0.091 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 1-Methylnaphthalene 9.4 1.2 0.45 mg/Kg dry 5 SW-846 8270D 10/24/18 10/30/18 15:32 BGL 2-Methylnaphthalene 15 1.2 0.41 mg/Kg dry 5 SW-846 8270D 10/24/18 10/30/18 15:32 BGL 2-Methylphenol ND 0.47 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 3/4-Methylphenol ND 0.47 0.15 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Naphthalene 2.8 0.24 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2-Nitroaniline ND 0.47 0.079 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 3-Nitroaniline ND 0.47 0.068 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 4-Nitroaniline ND 0.47 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Nitrobenzene ND 0.47 0.089 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2-Nitrophenol ND 0.47 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 4-Nitrophenol ND 0.91 0.10 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:26 BGL N-Nitrosodimethylamine ND 0.47 0.30 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL N-Nitrosodiphenylamine ND 0.47 0.097 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL N-Nitrosodi-n-propylamine ND 0.47 0.097 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Pentachloronitrobenzene ND 0.47 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Pentachlorophenol ND 0.47 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Phenanthrene 4.4 0.24 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Phenol ND 0.47 0.080 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Pyrene 1.4 0.24 0.078 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Pyridine ND 0.47 0.076 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 1,2,4,5-Tetachlorobenzene ND 0.47 0.084 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 1,2,4-Trichlorobenzene ND 0.47 0.084 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2,4,5-Trichlorophenol ND 0.47 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL 2,4,6-Trichlorophenol ND 0.47 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:26 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 59.4 30-130 10/29/18 19:26 2-Fluorophenol 64.6 30-130 10/30/18 15:32 Phenol-d6 66.1 30-130 10/29/18 19:26 Phenol-d6 72.5 30-130 10/30/18 15:32 Nitrobenzene-d5 63.7 30-130 10/29/18 19:26 Nitrobenzene-d5 77.3 30-130 10/30/18 15:32 2-Fluorobiphenyl 43.9 30-130 10/29/18 19:26 2-Fluorobiphenyl 60.4 30-130 10/30/18 15:32 2,4,6-Tribromophenol 89.6 30-130 10/29/18 19:26 2,4,6-Tribromophenol 73.3 30-130 10/30/18 15:32 p-Terphenyl-dl4 77.9 30-130 10/29/18 19:26 p-Terphenyl-dl4 74.3 30-130 10/30/18 15:32 Page 32 of 78 Table of Contents 40 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-4 Sampled: 10/22/2018 14:40 Samnle ID: 18J1112-04 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C9-C18 Aliphatics 17 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW C19-C36 Aliphatics ND 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW Unadjusted C11-C22 Aromatics ND 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW C11-C22 Aromatics ND 14 mg/Kg dry 1 MADEP-EPH-04-1.1 10/24/18 10/29/18 3:43 RMW Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 76.0 40-140 10/29/18 3:43 o-Terphenyl(OTP) 80.4 40-140 10/29/18 3:43 2-Bromonaphthalene 97.3 40-140 10/29/18 3:43 2-Fluorobiphenyl 106 40-140 10/29/18 3:43 Page 33 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-4 Sampled: 10/22/2018 14:40 Sample ID: 18J1112-04 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - VPH Soil/Methanol Preservation Ratio: 0.85 Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C5-C8 Aliphatics ND 20 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/23/18 10/25/18 20:08 EEH Rev 2.1 C9-C12 Aliphatics ND 20 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/23/18 10/25/18 20:08 EEH Rev 2.1 C9-C10 Aromatics ND 20 mg/Kg dry 1 MADEP-VPH-Feb 2018 10/23/18 10/25/18 20:08 EEH Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 82.9 70-130 10/25/18 20:08 2,5-Dibromotoluene (PID) 82.8 70-130 10/25/18 20:08 Page 34 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: SW-4 Sampled: 10/22/2018 14:40 Samnle ID: 18J1112-04 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 72.2 % Wt 1 SM 2540G 10/27/18 10/28/18 15:28 BLM Page 35 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY Project Location: 5318 Morris Field Drive Date Received: 10/22/2018 Field Sample #: TB-3 Sample ID: 18J1112-05 Samnle Matrix: Soil 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Sample Description: Sampled: 10/22/2018 13:00 Work Order: 18J1112 Sample Flags: RL-11 Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Acetone ND 14 2.7 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Acrylonitrile ND 1.4 0.16 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH tert-Amyl Methyl Ether (TAME) ND 0.56 0.030 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Benzene ND 0.28 0.033 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Bromobenzene ND 0.28 0.042 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Bromochloromethane ND 0.28 0.062 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Bromodichloromethane ND 0.28 0.082 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Bromoform ND 0.56 0.059 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Bromomethane ND 0.56 0.26 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 2-Butanone (MEK) ND 5.6 0.66 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH tert-Butyl Alcohol (TBA) ND 5.6 0.61 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH n-Butylbenzene 1.8 0.28 0.042 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH sec-Butylbenzene 1.7 0.28 0.036 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH tert-Butylbenzene ND 0.28 0.034 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH tert-Butyl Ethyl Ether (TBEE) ND 0.14 0.027 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Carbon Disulfide ND 0.84 0.28 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Carbon Tetrachloride ND 0.28 0.069 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Chlorobenzene ND 0.28 0.045 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Chlorodibromomethane ND 0.14 0.029 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Chloroethane ND 0.56 0.078 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Chloroform ND 0.56 0.061 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Chloromethane ND 0.56 0.15 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 2-Chlorotoluene ND 0.28 0.033 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 4-Chlorotoluene ND 0.28 0.039 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2-Dibromo-3-chloropropane (DBCP) ND 1.4 0.10 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2-Dibromoethane (EDB) ND 0.14 0.041 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Dibromomethane ND 0.28 0.045 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2-Dichlorobenzene ND 0.28 0.047 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,3-Dichlorobenzene ND 0.28 0.047 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,4-Dichlorobenzene ND 0.28 0.042 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH trans-1,4-Dichloro-2-butene ND 0.56 0.087 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Dichlorodifluoromethane (Freon 12) ND 0.56 0.079 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,1-Dichloroethane ND 0.28 0.044 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2-Dichloroethane ND 0.28 0.054 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1, 1 -Dichloroethylene ND 0.28 0.059 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH cis-1,2-Dichloroethylene ND 0.28 0.041 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH trans-1,2-Dichloroethylene ND 0.28 0.042 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2-Dichloropropane ND 0.28 0.036 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,3-Dichloropropane ND 0.14 0.036 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 2,2-Dichloropropane ND 0.28 0.059 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1, 1 -Dichloropropene ND 0.56 0.036 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH cis-1,3-Dichloropropene ND 0.14 0.033 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH trans-1,3-Dichloropropene ND 0.14 0.031 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Diethyl Ether ND 0.56 0.062 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Page 36 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: TB-3 Sampled: 10/22/2018 13:00 Sample ID: 18J1112-05 Samnle Matrix: Soil Sample Flags: RL-11 Volatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.14 0.051 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,4-Dioxane ND 14 7.4 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Ethylbenzene 0.93 0.28 0.036 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Hexachlorobutadiene ND 0.28 0.16 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 2-Hexanone (MBK) ND 2.8 0.42 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Isopropylbenzene (Cumene) 0.75 0.28 0.033 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH p-Isopropyltoluene (p-Cymene) 1.0 0.28 0.042 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Methyl tert-Butyl Ether (MTBE) ND 0.28 0.025 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Methylene Chloride ND 1.4 0.89 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 4-Methyl-2-pentanone (MIBK) ND 2.8 0.41 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Naphthalene 7.8 0.56 0.034 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH n-Propylbenzene 1.5 0.28 0.036 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Styrene ND 0.28 0.042 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1, 1, 1,2-Tetrachloroethane ND 0.28 0.033 mg/Kgdry 4 SW-8468260B 10/24/18 10/27/18 11:45 EEH 1,1,2,2-Tetrachloroethane ND 0.14 0.045 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Tetrachloroethylene ND 0.28 0.076 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Tetrahydrofuran ND 2.8 0.30 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Toluene 0.32 0.28 0.047 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2,3-Trichlorobenzene ND 1.4 0.039 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2,4-Trichlorobenzene ND 0.28 0.053 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,3,5-Trichlorobenzene ND 0.28 0.047 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1, 1, 1 -Trichloroethane ND 0.28 0.037 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,1,2-Trichloroethane ND 0.28 0.066 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Trichloroethylene ND 0.28 0.056 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Trichlorofluoromethane (Freon 11) ND 0.56 0.041 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,2,3-Trichloropropane ND 0.56 0.060 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.28 0.054 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH (Freon 113) 1,2,4-Trimethylbenzene 8.0 0.28 0.050 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH 1,3,5-Trimethylbenzene 1.9 0.28 0.036 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Vinyl Chloride ND 0.56 0.037 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH m+p Xylene 2.4 0.56 0.071 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH o-Xylene 1.1 0.28 0.037 mg/Kg dry 4 SW-846 8260B 10/24/18 10/27/18 11:45 EEH Surrogates % Recovery Recovery Limits Flag/Qual 1,2-Dichloroethane-d4 92.6 70-130 10/27/18 11:45 Toluene-d8 101 70-130 10/27/18 11:45 4-Bromofluorobenzene 104 70-130 10/27/18 11:45 Page 37 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: TB-3 Sampled: 10/22/2018 13:00 Samnle ID: 18J1112-05 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.23 0.069 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Acenaphthylene ND 0.23 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Acetophenone ND 0.46 0.090 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Aniline ND 0.46 0.13 mg/Kg dry 1 V-05, V-34 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Anthracene ND 0.23 0.066 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Benzidine ND 0.89 0.57 mg/Kg dry 1 R-05, V-05, V-34 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Benzo(a)anthracene ND 0.23 0.061 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Benzo(a)pyrene ND 0.23 0.071 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Benzo(b)fluoranthene ND 0.23 0.065 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Benzo(g,h,i)perylene ND 0.23 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Benzo(k)fluoranthene ND 0.23 0.071 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Benzoic Acid ND 1.3 0.24 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Bis(2-chloroethoxy)methane ND 0.46 0.087 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Bis(2-chloroethyl)ether ND 0.46 0.090 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Bis(2-chloroisopropyl)ether ND 0.46 0.098 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Bis(2-Ethylhexyl)phthalate ND 0.46 0.18 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 4-Bromophenylphenylether ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Butylbenzylphthalate ND 0.46 0.11 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 19:52 BGL Carbazole ND 0.23 0.059 mg/Kg dry I SW-846 8270D 10/24/18 10/29/18 19:52 BGL 4-Chloroaniline ND 0.89 0.10 mg/Kg dry 1 V-34 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 4-Chloro-3-methylphenol ND 0.89 0.098 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2-Chloronaphthalene ND 0.46 0.086 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2-Chlorophenol ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 4-Chlorophenylphenylether ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Chrysene ND 0.23 0.071 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Dibenz(a,h)anthracene ND 0.23 0.14 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Dibenzofman ND 0.46 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Di-n-butylphthalate ND 0.46 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 1,2-Dichlorobenzene ND 0.46 0.081 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 1,3-Dichlorobenzene ND 0.46 0.078 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 1,4-Dichlorobenzene ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 3,3-Dichlorobenzidine ND 0.23 0.070 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2,4-Dichlorophenol ND 0.46 0.078 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Diethylphthalate ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2,4-Dimethylphenol ND 0.46 0.085 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Dimethylphthalate ND 0.46 0.081 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 4,6-Dinitro-2-methylphenol ND 0.46 0.43 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2,4-Dinitrophenol ND 0.89 0.26 mg/Kg dry 1 V-19 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2,4-Dinitrotoluene ND 0.46 0.074 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2,6-Dinitrotoluene ND 0.46 0.081 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Di-n-octylphthalate ND 0.46 0.24 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.46 0.074 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Fluoranthene ND 0.23 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Flumene ND 0.23 0.074 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Page 38 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: TB-3 Sampled: 10/22/2018 13:00 Samnle ID: 18J1112-05 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.46 0.081 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Hexachlorobutadiene ND 0.46 0.081 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Hexachlorocyclopentadiene ND 0.46 0.097 mg/Kg dry 1 V-05 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Hexachloroethane ND 0.46 0.092 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Indeno(1,2,3-cd)pyrene ND 0.23 0.16 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Isophorone ND 0.46 0.089 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 1-Methylnaphthalene ND 0.23 0.087 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2-Methylnaphthalene ND 0.23 0.079 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2-Methylphenol ND 0.46 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 3/4-Methylphenol ND 0.46 0.15 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Naphthalene ND 0.23 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2-Nitroaniline ND 0.46 0.077 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 3-Nitroaniline ND 0.46 0.066 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 4-Nitroaniline ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Nitrobenzene ND 0.46 0.086 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2-Nitrophenol ND 0.46 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 4-Nitrophenol ND 0.89 0.10 mg/Kg dry 1 V-20 SW-846 8270D 10/24/18 10/29/18 19:52 BGL N-Nitrosodimethylamine ND 0.46 0.29 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL N-Nitrosodiphenylamine ND 0.46 0.094 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL N-Nitrosodi-n-propylamine ND 0.46 0.094 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Pentachloronitrobenzene ND 0.46 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Pentachlorophenol ND 0.46 0.11 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Phenanthrene ND 0.23 0.12 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Phenol ND 0.46 0.078 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Pyrene ND 0.23 0.075 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Pyridine ND 0.46 0.074 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 1,2,4,5-Tetrachlorobenzene ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 1,2,4-Trichlorobenzene ND 0.46 0.082 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2,4,5-Trichlorophenol ND 0.46 0.10 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL 2,4,6-Trichlorophenol ND 0.46 0.077 mg/Kg dry 1 SW-846 8270D 10/24/18 10/29/18 19:52 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 71.9 30-130 10/29/18 19:52 Phenol-d6 82.0 30-130 10/29/18 19:52 Nitrobenzene-d5 86.6 30-130 10/29/18 19:52 2-Fluorobiphenyl 59.3 30-130 10/29/18 19:52 2,4,6-Tribromophenol 97.0 30-130 10/29/18 19:52 p-Terphenyl-dl4 75.6 30-130 10/29/18 19:52 Page 39 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: TB-3 Sampled: 10/22/2018 13:00 Samnle ID: 18J1112-05 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C9-C18 Aliphatics 1400 140 mg/Kg dry 10 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:39 RMW C19-C36 Aliphatics 360 68 mg/Kg dry 5 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:57 RMW Unadjusted C11-C22 Aromatics 870 140 mg/Kg dry 10 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:39 RMW C11-C22 Aromatics 830 140 mg/Kg dry 10 MADEP-EPH-04-1.1 10/24/18 10/29/18 10:39 RMW Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 76.6 40-140 10/29/18 4:01 o-Terphenyl(OTP) 91.4 40-140 10/29/18 4:01 2-Bromonaphthalene 102 40-140 10/29/18 4:01 2-Fluorobiphenyl 108 40-140 10/29/18 4:01 Page 40 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: TB-3 Sampled: 10/22/2018 13:00 Sample ID: 18J1112-05 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - VPH Soil/Methanol Preservation Ratio: 1.13 Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C5-C8 Aliphatics ND 160 mg/Kg dry 10 RL-05 MADEP-VPH-Feb 2018 10/23/18 10/26/18 2:59 EEH Rev 2.1 C9-C12 Aliphatics 280 160 mg/Kg dry 10 MADEP-VPH-Feb 2018 10/23/18 10/26/18 2:59 EEH Rev 2.1 C9-C10 Aromatics 440 160 mg/Kg dry 10 MADEP-VPH-Feb 2018 10/23/18 10/26/18 2:59 EEH Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene (FID) 70.9 70-130 10/26/18 2:59 2,5-Dibromotoluene (PID) 81.0 70-130 10/26/18 2:59 Page 41 of 78 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18J1112 Date Received: 10/22/2018 Field Sample #: TB-3 Sampled: 10/22/2018 13:00 Samnle ID: 18J1112-05 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 72.9 % Wt 1 SM 2540G 10/27/18 10/28/18 15:28 BLM Page 42 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3546-MADEP-EPH-04-1.1 Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1112-01 [SW-1] B215618 20.6 2.00 10/24/18 18J1112-02 [SW-2] B215618 20.1 2.00 10/24/18 18J1112-03 [SW-3] B215618 20.5 2.00 10/24/18 18J1112-04 [SW-4] B215618 20.3 2.00 10/24/18 18J1112-05 [TB-3] B215618 20.3 2.00 10/24/18 Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1 Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1112-04 [SW-4] B215495 4.30 6.20 10/23/18 18J1112-05 [TB-3] B215495 5.70 6.50 10/23/18 Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1 Lab Number [Field ID] Batch Initial [g] Final [mL[ Date 18J1112-01 [SW-1] B215561 7.70 7.10 10/24/18 18J1112-02 [SW-2] B215561 5.00 6.60 10/24/18 18J1112-03 [SW-3] B215561 5.60 6.40 10/24/18 Prep Method: % Solids-SM 2540G Lab Number [Field ID] Batch Date 18J1112-01 [SW-1] B215828 10/27/18 18J1112-02 [SW-2] B215828 10/27/18 18J1112-03 [SW-3] B215828 10/27/18 18J 1112-04 [SW-4] B215828 10/27/18 18J1112-05 [TB-3] B215828 10/27/18 Prep Method: SW-846 5035-SW-846 8260B Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1112-01[SW-1] B215551 5.75 10.0 10/24/18 18J1112-02 [SW-2] B215551 5.77 10.0 10/24/18 18J1112-03 [SW-3] B215551 6.48 10.0 10/24/18 18J 1112-04 [SW-4] B215551 5.99 10.0 10/24/18 Prep Method: SW-846 5035-SW-846 8260B Sample Methanol Methanol Final Lab Number [Field ID] Batch Amount(g) Volume(mL) Aliquot(mL) Volume(mL) Date 18J 1112-05 [TB-3] B215584 6.71 6.82 0.25 50 10/24/18 Prep Method: SW-846 3546-SW-846 8270D Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1112-01 [SW-1] B215606 30.2 1.00 10/24/18 18J1112-02 [SW-2] B215606 30.6 1.00 10/24/18 18J1112-03 [SW-3] B215606 30.2 1.00 10/24/18 18J1112-04 [SW-4] B215606 30.0 1.00 10/24/18 Page 43 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3546-SW-846 8270D Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18J1112-04RE1 [SW-4] B215606 30.0 1.00 10/24/18 18J1112-05 [TB-3] B215606 30.6 1.00 10/24/18 Page 44 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215551 - SW-846 5035 Blank (B215551-BLK1) Prepared & Analyzed: 10/24/18 Acetone ND 0.10 mg/Kg wet Acrylonitrile ND 0.0060 mg/Kg wet tert-Amyl Methyl Ether (TAME) ND 0.0010 mg/Kg wet Benzene ND 0.0020 mg/Kg wet Bromobenzene ND 0.0020 mg/Kg wet Bromochloromethane ND 0.0020 mg/Kg wet Bromodichloromethane ND 0.0020 mg/Kg wet Bromoform ND 0.0020 mg/Kg wet Bromomethane ND 0.010 mg/Kg wet 2-Butanone (MEK) ND 0.040 mg/Kg wet tert-Butyl Alcohol (TBA) ND 0.040 mg/Kg wet n-Butylbenzene ND 0.0020 mg/Kg wet sec-Butylbenzene ND 0.0020 mg/Kg wet tert-Butylbenzene ND 0.0020 mg/Kg wet tert-Butyl Ethyl Ether (TBEE) ND 0.0010 mg/Kg wet Carbon Disulfide ND 0.0060 mg/Kg wet Carbon Tetrachloride ND 0.0020 mg/Kg wet Chlorobenzene ND 0.0020 mg/Kg wet Chlorodibromomethane ND 0.0010 mg/Kg wet Chloroethane ND 0.020 mg/Kg wet Chloroform ND 0.0040 mg/Kg wet Chloromethane ND 0.010 mg/Kg wet 2-Chlorotoluene ND 0.0020 mg/Kg wet 4-Chlorotoluene ND 0.0020 mg/Kg wet 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 mg/Kg wet 1,2-Dibromoethane (EDB) ND 0.0010 mg/Kg wet Dibromomethane ND 0.0020 mg/Kg wet 1,2-Dichlorobenzene ND 0.0020 mg/Kg wet 1,3-Dichlorobenzene ND 0.0020 mg/Kg wet 1,4-Dichlorobenzene ND 0.0020 mg/Kg wet trans-1,4-Dichloro-2-butene ND 0.0040 mg/Kg wet Dichlorodifluoromethane (Freon 12) ND 0.020 mg/Kg wet 1,1-Dichloroethane ND 0.0020 mg/Kg wet 1,2-Dichloroethane ND 0.0020 mg/Kg wet 1,1-Dichloroethylene ND 0.0040 mg/Kg wet cis-1,2-Dichloroethylene ND 0.0020 mg/Kg wet trans-1,2-Dichloroethylene ND 0.0020 mg/Kg wet 1,2-Dichloropropane ND 0.0020 mg/Kg wet 1,3-Dichloropropane ND 0.0010 mg/Kg wet 2,2-Dichloropropane ND 0.0020 mg/Kg wet 1,1-Dichloropropene ND 0.0020 mg/Kg wet cis-1,3-Dichloropropene ND 0.0010 mg/Kg wet trans-1,3-Dichloropropene ND 0.0010 mg/Kg wet Diethyl Ether ND 0.020 mg/Kg wet Diisopropyl Ether (RIPE) ND 0.0010 mg/Kg wet 1,4-Dioxane ND 0.10 mg/Kg wet Ethylbenzene ND 0.0020 mg/Kg wet Hexachlorobutadiene ND 0.0020 mg/Kg wet 2-Hexanone (MBK) ND 0.020 mg/Kg wet Isopropylbenzene (Cumene) ND 0.0020 mg/Kg wet p-Isopropyltoluene (p-Cymene) ND 0.0020 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.0040 mg/Kg wet Page 45 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215551 - SW-846 5035 Blank (B215551-BLK1) Prepared & Analyzed: 10/24/18 Methylene Chloride ND 0.020 mg/Kg wet 4-Methyl-2-pentanone (MIBK) ND 0.020 mg/Kg wet Naphthalene ND 0.0040 mg/Kg wet n-Propylbenzene ND 0.0020 mg/Kg wet Styrene ND 0.0020 mg/Kg wet 1, 1, 1,2-Tetrachloroethane ND 0.0020 mg/Kg wet 1,1,2,2-Tetrachloroethane ND 0.0010 mg/Kg wet Tetrachloroethylene ND 0.0020 mg/Kg wet Tetrahydrofuran ND 0.010 mg/Kg wet Toluene ND 0.0020 mg/Kg wet 1,2,3-Trichlorobenzene ND 0.0020 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.0020 mg/Kg wet 1,3,5-Trichlorobenzene ND 0.0020 mg/Kg wet 1, 1, 1 -Trichloroethane ND 0.0020 mg/Kg wet 1,1,2-Trichloroethane ND 0.0020 mg/Kg wet Trichloroethylene ND 0.0020 mg/Kg wet Trichlorofluoromethane (Freon 11) ND 0.010 mg/Kg wet 1,2,3-Trichloropropane ND 0.0020 mg/Kg wet 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.010 mg/Kg wet 113) 1,2,4-Trimethylbenzene ND 0.0020 mg/Kg wet 1,3,5-Trimethylbenzene ND 0.0020 mg/Kg wet Vinyl Chloride ND 0.010 mg/Kg wet m+p Xylene ND 0.0040 mg/Kg wet o-Xylene ND 0.0020 mg/Kg wet Surrogate: 1,2-Dichloroethane-d4 0.0532 mg/Kg wet 0.0500 106 70-130 Surrogate: Toluene-d8 0.0515 mg/Kg wet 0.0500 103 70-130 Surrogate:4-Bromofluorobenzene 0.0529 mg/Kg wet 0.0500 106 70-130 LCS (B215551-BS1) Prepared & Analyzed: 10/24/18 Acetone 0.264 0.10 mg/Kg wet 0.200 132 70-160 Acrylonitrile 0.0226 0.0060 mg(Kgwet 0.0200 113 70-130 tert-Amyl Methyl Ether (TAME) 0.0256 0.0010 mg/Kg wet 0.0200 128 70-130 Benzene 0.0234 0.0020 mg/Kg wet 0.0200 117 70-130 Bromobenzene 0.0199 0.0020 mg/Kgwet 0.0200 99.4 70-130 Bromochloromethane 0.0218 0.0020 mg/Kg wet 0.0200 109 70-130 Bromodichloromethane 0.0213 0.0020 mg/Kg wet 0.0200 106 70-130 Bromoform 0.0209 0.0020 mg/Kgwet 0.0200 104 70-130 Bromomethane 0.0179 0.010 mg/Kg wet 0.0200 89.4 40-130 2-Butanone (MEK) 0.291 0.040 mg/Kg wet 0.200 145 70-160 tert-Butyl Alcohol (TBA) 0.188 0.040 mg/Kg wet 0.200 94.2 40-130 n-Butylbenzene 0.0172 0.0020 mg/Kg wet 0,0200 85.9 70-130 sec-Butylbenzene 0.0189 0.0020 mg/Kg wet 0.0200 94.5 70-130 tert-Butylbenzene 0.0189 0.0020 mg/Kgwet 0.0200 94.4 70-160 tert-Butyl Ethyl Ether (TBEE) 0.0256 0.0010 mg/Kg wet 0,0200 128 70-130 Carbon Disulfide 0.0242 0.0060 mg/Kg wet 0.0200 121 70-130 Carbon Tetrachloride 0.0250 0.0020 mg/Kg wet 0.0200 125 70-130 Chlorobenzene 0.0198 0.0020 mg/Kg wet 0,0200 99.2 70-130 Chlorodibromomethane 0.0241 0.0010 mg/Kg wet 0.0200 121 70-130 Chloroethane 0.0203 0.020 mg/Kgwet 0.0200 102 70-130 Chloroform 0.0235 0.0040 mg/Kg wet 0,0200 118 70-130 Chloromethane 0.0203 0.010 mg/Kg wet 0.0200 101 70-130 2-Chlorotoluene 0.0208 0.0020 mg/Kg wet 0.0200 104 70-130 t t t t t Page 46 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215551 - SW-846 5035 LCS (B215551-BSI) Prepared & Analyzed: 10/24/18 4-Chlorotoluene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 1,2-Dibromo-3-chloropropane (DBCP) 0.0186 0.0020 mg/Kg wet 0.0200 93.2 70-130 1,2-Dibromoethane (EDB) 0.0221 0.0010 mg/Kg wet 0.0200 110 70-130 Dibromomethane 0.0190 0.0020 mg/Kg wet 0.0200 95.2 70-130 1,2-Dichlorobenzene 0.0187 0.0020 mg/Kg wet 0.0200 93.6 70-130 1,3-Dichlorobenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.6 70-130 1,4-Dichlorobenzene 0.0186 0.0020 mg/Kg wet 0.0200 93.0 70-130 trans-1,4-Dichloro-2-butene 0.0166 0.0040 mg/Kg wet 0.0200 83.2 70-130 Dichlorodifluoromethane (Freon 12) 0.0205 0.020 mg/Kg wet 0.0200 102 40-160 1,1-Dichloroethane 0.0233 0.0020 mg/Kg wet 0.0200 117 70-130 1,2-Dichloroethane 0.0238 0.0020 mg/Kg wet 0.0200 119 70-130 1,1-Dichloroethylene 0.0239 0.0040 mg/Kg wet 0.0200 119 70-130 cis-1,2-Dichloroethylene 0.0229 0.0020 mg/Kg wet 0.0200 115 70-130 trans-1,2-Dichloroethylene 0.0240 0.0020 mg/Kg wet 0.0200 120 70-130 1,2-Dichloropropane 0.0219 0.0020 mg/Kg wet 0.0200 109 70-130 1,3-Dichloropropane 0.0226 0.0010 mg/Kg wet 0.0200 113 70-130 2,2-Dichloropropane 0.0191 0.0020 mg/Kg wet 0.0200 95.6 70-130 1,1-Dichloropropene 0.0239 0.0020 mg/Kg wet 0.0200 120 70-130 cis-1,3-Dichloropropene 0.0218 0.0010 mg/Kg wet 0.0200 109 70-130 trans-1,3-Dichloropropene 0.0219 0.0010 mg/Kg wet 0.0200 110 70-130 Diethyl Ether 0.0242 0.020 mg/Kg wet 0.0200 121 70-130 Diisopropyl Ether (DIPE) 0.0258 0.0010 mg/Kg wet 0.0200 129 70-130 1,4-Dioxane 0.209 0.10 mg/Kg wet 0.200 105 40-160 Ethylbenzene 0.0190 0.0020 mg/Kg wet 0.0200 94.9 70-130 Hexachlorobutadiene 0.0174 0.0020 mg/Kg wet 0.0200 87.2 70-160 2-Hexanone (MBK) 0.271 0.020 mg/Kg wet 0.200 136 70-160 Isopropylbenzene (Cumene) 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 p-Isopropyltoluene (p-Cymene) 0.0184 0.0020 mg/Kg wet 0.0200 91.8 70-130 Methyl tert-Butyl Ether (MTBE) 0.0261 0.0040 mg/Kg wet 0.0200 130 70-130 Methylene Chloride 0.0225 0.020 mg/Kg wet 0.0200 112 40-160 4-Methyl-2-pentanone (MIBK) 0.263 0.020 mg/Kg wet 0.200 131 70-160 Naphthalene 0.0158 0.0040 mg/Kg wet 0.0200 79.2 40-130 n-Propylbenzene 0.0200 0.0020 mg/Kg wet 0.0200 100 70-130 Styrene 0.0191 0.0020 mg/Kg wet 0.0200 95.3 70-130 1, 1, 1,2-Tetrachloroethane 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 1,1,2,2-Tetrachloroethane 0.0194 0.0010 mg/Kg wet 0.0200 97.1 70-130 Tetrachloroethylene 0.0256 0.0020 mg/Kg wet 0.0200 128 70-130 Tetrahydrofuran 0.0263 0.010 mg/Kg wet 0.0200 132 * 70-130 Toluene 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 1,2,3-Trichlorobenzene 0.0163 0.0020 mg/Kg wet 0.0200 81.5 70-130 1,2,4-Trichlorobenzene 0.0159 0.0020 mg/Kg wet 0.0200 79.5 70-130 1,3,5-Trichlorobenzene 0.0173 0.0020 mg/Kg wet 0.0200 86.4 70-130 1, 1, 1 -Trichloroethane 0.0243 0.0020 mg/Kg wet 0.0200 122 70-130 1,1,2-Trichloroethane 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 Trichloroethylene 0.0214 0.0020 mg/Kg wet 0.0200 107 70-130 Trichlorofluoromethane (Freon 11) 0.0236 0.010 mg/Kg wet 0.0200 118 70-130 1,2,3-Trichloropropane 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0241 0.010 mg/Kg wet 0.0200 121 70-130 113) 1,2,4-Trimethylbenzene 0.0177 0.0020 mg/Kg wet 0.0200 88.7 70-130 1,3,5-Trimethylbenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.6 70-130 Vinyl Chloride 0.0202 0.010 mg/Kg wet 0,0200 101 40-130 f t t f t t L-07 Page 47 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215551 - SW-846 5035 LCS (B215551-BSI) Prepared & Analyzed: 10/24/18 m+p Xylene 0.0388 0.0040 mg/Kg wet 0.0400 96.9 70-130 o-Xylene 0.0199 0.0020 mg/Kg wet 0.0200 99.4 70-130 Surrogate:l,2-Dichloroethane-d4 Surrogate: Toluene-d8 Surrogate:4-Bromofluorobenzene LCS Dup (B215551-BSDI) 0.0523 0.0518 0.0533 mg/Kg wet mg/Kg wet mg/Kg wet 0.0500 105 0.0500 104 0.0500 107 Prepared & Analyzed: 10/24/18 70-130 70-130 70-130 Acetone 0332 0.10 mg/Kg wet 0.200 166 * 70-160 22.8 Acrylonitrile 0.0231 0.0060 mg/Kg wet 0.0200 115 70-130 2.04 tert-Amyl Methyl Ether (TAME) 0.0259 0.0010 mg/Kg wet 0.0200 130 70-130 1.30 Benzene 0.0232 0.0020 mg/Kg wet 0.0200 116 70-130 1.01 Bromobenzene 0.0199 0.0020 mg/Kg wet 0.0200 99.7 70-130 0.301 Bromochloromethane 0.0233 0.0020 mg/Kg wet 0.0200 117 70-130 6.63 Bromodichloromethane 0.0216 0.0020 mg/Kg wet 0.0200 108 70-130 1.47 Bromoform 0.0212 0.0020 mg/Kg wet 0.0200 106 70-130 1.65 Bromomethane 0.0176 0.010 mg/Kg wet 0.0200 88.2 40-130 1.40 2-Butanone (MEK) 0.321 0.040 mg/Kg wet 0.200 160 70-160 9.79 tert-Butyl Alcohol (TBA) 0.208 0.040 mg/Kg wet 0.200 104 40-130 10.0 n-Butylbenzene 0.0166 0.0020 mg/Kg wet 0.0200 82.8 70-130 3.69 sec-Butylbenzene 0.0187 0.0020 mg/Kg wet 0.0200 93.3 70-130 1.28 tert-Butylbenzene 0.0184 0.0020 mg/Kg wet 0.0200 92.2 70-160 2.33 tert-Butyl Ethyl Ether (TBEE) 0.0257 0.0010 mg/Kg wet 0.0200 128 70-130 0.367 Carbon Disulfide 0.0232 0.0060 mg/Kg wet 0.0200 116 70-130 4.41 Carbon Tetrachloride 0.0252 0.0020 mg/Kg wet 0.0200 126 70-130 0.677 Chlorobenzene 0.0199 0.0020 mg/Kg wet 0.0200 99.7 70-130 0.452 Chlorodibromomethane 0.0247 0.0010 mg/Kg wet 0.0200 124 70-130 2.47 Chloroethane 0.0214 0.020 mg/Kg wet 0.0200 107 70-130 5.03 Chloroform 0.0240 0.0040 mg/Kg wet 0.0200 120 70-130 2.00 Chloromethane 0.0207 0.010 mg/Kg wet 0.0200 103 70-130 2.13 2-Chlorotoluene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 0.928 4-Chlorotoluene 0.0199 0.0020 mg/Kg wet 0.0200 99.7 70-130 3.43 1,2-Dibromo-3-chloropropane (DBCP) 0.0200 0.0020 mg/Kg wet 0.0200 99.9 70-130 6.95 1,2-Dibromoethane (EDB) 0.0224 0.0010 mg/Kg wet 0.0200 112 70-130 1.64 Dibromomethane 0.0200 0.0020 mg/Kg wet 0.0200 99.9 70-130 4.84 1,2-Dichlorobenzene 0.0184 0.0020 mg/Kg wet 0.0200 92.0 70-130 1.74 1,3-Dichlorobenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.5 70-130 0.0207 1,4-Dichlorobenzene 0.0183 0.0020 mg/Kg wet 0.0200 91.5 70-130 1.64 trans-1,4-Dichloro-2-butene 0.0163 0.0040 mg/Kg wet 0.0200 81.5 70-130 2.06 Dichlorodifluoromethane (Freon 12) 0.0204 0.020 mg/Kg wet 0.0200 102 40-160 0.352 1, 1 -Dichloroethane 0.0234 0.0020 mg/Kg wet 0.0200 117 70-130 0.445 1,2-Dichloroethane 0.0236 0.0020 mg/Kg wet 0.0200 118 70-130 0.608 1,1-Dichloroethylene 0.0234 0.0040 mg/Kg wet 0.0200 117 70-130 2.24 cis-1,2-Dichloroethylene 0.0229 0.0020 mg/Kg wet 0.0200 114 70-130 0.175 trans-1,2-Dichloroethylene 0.0237 0.0020 mg/Kg wet 0.0200 118 70-130 1.37 1,2-Dichloropropane 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 0.520 1,3-Dichloropropane 0.0228 0.0010 mg/Kg wet 0.0200 114 70-130 1.22 2,2-Dichloropropane 0.0188 0.0020 mg/Kg wet 0.0200 93.8 70-130 1.93 1,1-Dichloropropene 0.0238 0.0020 mg/Kg wet 0.0200 119 70-130 0.620 cis-1,3-Dichloropropene 0.0226 0.0010 mg/Kg wet 0.0200 113 70-130 3.75 trans-1,3-Dichloropropene 0.0222 0.0010 mg/Kg wet 0.0200 ill 70-130 1.21 Diethyl Ether 0.0259 0.020 mg/Kg wet 0.0200 130 70-130 6.96 Diisopropyl Ether (RIPE) 0.0263 0.0010 mg/Kg wet 0.0200 132 * 70-130 2.07 25 L-07 t 25 25 25 25 25 25 25 25 f 25 t 25 t 25 25 25 t 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 t 25 25 25 25 25 25 25 25 25 25 25 25 25 L-07 Page 48 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215551 - SW-846 5035 LCS Dup (B215551-BSD1) Prepared & Analyzed: 10/24/18 1,4-Dioxane 0.263 0.10 mg/Kgwet 0.200 132 40-160 22.8 50 f # Ethylbenzene 0.0186 0.0020 mg/Kg wet 0.0200 93.0 70-130 2.06 25 Hexachlorobutadiene 0.0176 0.0020 mg/Kg wet 0.0200 88.0 70-160 0.970 25 2-Hexanone (MBK) 0.288 0.020 mg/Kg wet 0.200 144 70-160 6.00 25 f Isopropylbenzene (Cumene) 0.0200 0.0020 mg/Kg wet 0.0200 100 70-130 1.29 25 p-Isopropyltoluene (p-Cymene) 0.0181 0.0020 mg/Kg wet 0.0200 90.5 70-130 1.41 25 Methyl tert-Butyl Ether (MTBE) 0.0265 0.0040 mg/Kg wet 0.0200 133 * 70-130 1.81 25 L-07 Methylene Chloride 0.0207 0.020 mg/Kg wet 0.0200 104 40-160 8.29 25 t 4-Methyl-2-pentanone (MIBK) 0.275 0.020 mg/Kg wet 0.200 138 70-160 4.74 25 t Naphthalene 0.0165 0.0040 mg/Kg wet 0.0200 82.5 40-130 4.12 25 f n-Propylbenzene 0.0197 0.0020 mg/Kg wet 0.0200 98.5 70-130 1.62 25 Styrene 0.0187 0.0020 mg/Kg wet 0.0200 93.4 70-130 1.99 25 1, 1, 1,2-Tetrachloroethane 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 0.404 25 1,1,2,2-Tetrachloroethane 0.0202 0.0010 mg/Kg wet 0.0200 101 70-130 4.18 25 Tetrachloroethylene 0.0238 0.0020 mg/Kg wet 0.0200 119 70-130 7.30 25 Tetrahydrofuran 0.0255 0.010 mg/Kg wet 0.0200 128 70-130 3.10 25 Toluene 0.0218 0.0020 mg/Kg wet 0.0200 109 70-130 0.903 25 1,2,3-Trichlorobenzene 0.0166 0.0020 mg/Kg wet 0.0200 83.0 70-130 1.85 25 1,2,4-Trichlorobenzene 0.0156 0.0020 mg/Kg wet 0.0200 78.0 70-130 1.90 25 1,3,5-Trichlorobenzene 0.0171 0.0020 mg/Kg wet 0.0200 85.6 70-130 0.884 25 1, 1, 1 -Trichloroethane 0.0242 0.0020 mg/Kg wet 0.0200 121 70-130 0.775 25 1,1,2-Trichloroethane 0.0235 0.0020 mg/Kg wet 0.0200 118 70-130 6.78 25 Trichloroethylene 0.0216 0.0020 mg/Kg wet 0.0200 108 70-130 0.864 25 Trichlorofluoromethane (Freon 11) 0.0234 0.010 mg/Kg wet 0.0200 117 70-130 0.793 25 1,2,3-Trichloropropane 0.0213 0.0020 mg/Kg wet 0.0200 107 70-130 3.54 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0250 0.010 mg/Kg wet 0.0200 125 70-130 3.41 25 113) 1,2,4-Trimethylbenzene 0.0174 0.0020 mg/Kg wet 0.0200 87.1 70-130 1.84 25 1,3,5-Trimethylbenzene 0.0192 0.0020 mg/Kg wet 0.0200 96.0 70-130 0.706 25 Vinyl Chloride 0.0203 0.010 mg/Kg wet 0.0200 101 40-130 0.198 25 t m+p Xylene 0.0386 0.0040 mg/Kg wet 0.0400 96.4 70-130 0.522 25 o-Xylene 0.0197 0.0020 mg/Kg wet 0.0200 98.5 70-130 0.859 25 Surrogate:l,2-Dichloroethane-d4 0.0535 mg/Kg wet 0.0500 107 70-130 Surrogate: Toluene-d8 0.0514 mg/Kg wet 0.0500 103 70-130 Surrogate:4-Bromofluorobenzene 0.0532 mg/Kg wet 0.0500 106 70-130 Batch B215584 - SW-846 5035 Blank (B215584-BLKI) Prepared: 10/24/18 Analyzed: 10/27/18 Acetone ND 2.5 mg/Kg wet Acrylonitrile ND 0.25 mg/Kg wet tert-Amyl Methyl Ether (TAME) ND 0.025 mg/Kg wet Benzene ND 0.050 mg/Kg wet Bromobenzene ND 0.050 mg/Kg wet Bromochloromethane ND 0.050 mg/Kg wet Bromodichloromethane ND 0.050 mg/Kg wet Bromoform ND 0.050 mg/Kg wet Bromomethane ND 0.10 mg/Kg wet 2-Butanone (MEK) ND 1.0 mg/Kg wet tert-Butyl Alcohol (TBA) ND 1.0 mg/Kg wet n-Butylbenzene ND 0.050 mg/Kg wet sec-Butylbenzene ND 0.050 mg/Kg wet tert-Butylbenzene ND 0.050 mg/Kg wet Page 49 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215584 - SW-846 5035 Blank (B215584-BLK1) Prepared: 10/24/18 Analyzed: 10/27/18 tert-Butyl Ethyl Ether (TBEE) ND 0.025 mg/Kg wet Carbon Disulfide ND 0.15 mg/Kg wet Carbon Tetrachloride ND 0.050 mg/Kg wet Chlorobenzene ND 0.050 mg/Kg wet Chlorodibromomethane ND 0.025 mg/Kg wet Chloroethane ND 0.10 mg/Kg wet Chloroform ND 0.10 mg/Kg wet Chloromethane ND 0.10 mg/Kg wet 2-Chlorotoluene ND 0.050 mg/Kg wet 4-Chlorotoluene ND 0.050 mg/Kg wet 1,2-Dibromo-3-chloropropane (DBCP) ND 0.25 mg/Kg wet 1,2-Dibromoethane (EDB) ND 0.025 mg/Kg wet Dibromomethane ND 0.050 mg/Kg wet 1,2-Dichlorobenzene ND 0.050 mg/Kg wet 1,3-Dichlorobenzene ND 0.050 mg/Kg wet 1,4-Dichlorobenzene ND 0.050 mg/Kg wet trans-1,4-Dichloro-2-butene ND 0.10 mg/Kg wet Dichlorodifluoromethane (Freon 12) ND 0.10 mg/Kg wet 1,1-Dichloroethane ND 0.050 mg/Kg wet 1,2-Dichloroethane ND 0.050 mg/Kg wet 1,1-Dichloroethylene ND 0.050 mg/Kg wet cis-1,2-Dichloroethylene ND 0.050 mg/Kg wet trans-1,2-Dichloroethylene ND 0.050 mg/Kg wet 1,2-Dichloropropane ND 0.050 mg/Kg wet 1,3-Dichloropropane ND 0.025 mg/Kg wet 2,2-Dichloropropane ND 0.050 mg/Kg wet 1,1-Dichloropropene ND 0.10 mg/Kg wet cis-1,3-Dichloropropene ND 0.025 mg/Kg wet trans-1,3-Dichloropropene ND 0.025 mg/Kg wet Diethyl Ether ND 0.10 mg/Kg wet Diisopropyl Ether (RIPE) ND 0.025 mg/Kg wet 1,4-Dioxane ND 2.5 mg/Kg wet Ethylbenzene ND 0.050 mg/Kg wet Hexachlorobutadiene ND 0.050 mg/Kg wet 2-Hexanone (MBK) ND 0.50 mg/Kg wet Isopropylbenzene (Cumene) ND 0.050 mg/Kg wet p-Isopropyltoluene (p-Cymene) ND 0.050 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.050 mg/Kg wet Methylene Chloride ND 0.25 mg/Kg wet 4-Methyl-2-pentanone (MIBK) ND 0.50 mg/Kg wet Naphthalene ND 0.10 mg/Kg wet n-Propylbenzene ND 0.050 mg/Kg wet Styrene ND 0.050 mg/Kg wet 1, 1, 1,2-Tetrachloroethane ND 0.050 mg/Kg wet 1,1,2,2-Tetrachloroethane ND 0.025 mg/Kg wet Tetrachloroethylene ND 0.050 mg/Kg wet Tetrahydrofuran ND 0.50 mg/Kg wet Toluene ND 0.050 mg/Kg wet 1,2,3-Trichlorobenzene ND 0.25 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.050 mg/Kg wet 1,3,5-Trichlorobenzene ND 0.050 mg/Kg wet 1, 1, 1 -Trichloroethane ND 0.050 mg/Kg wet Page 50 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215584 - SW-846 5035 Blank (B215584-BLK1) Prepared: 10/24/18 Analyzed: 10/27/18 1,1,2-Trichloroethane ND 0.050 mg/Kg wet Trichloroethylene ND 0.050 mg/Kg wet Trichlorofluoromethane (Freon 11) ND 0.10 mg/Kg wet 1,2,3-Trichloropropane ND 0.10 mg/Kg wet 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.050 mg/Kg wet 113) 1,2,4-Trimethylbenzene ND 0.050 mg/Kg wet 1,3,5-Trimethylbenzene ND 0.050 mg/Kg wet Vinyl Chloride ND 0.10 mg/Kg wet m+p Xylene ND 0.10 mg/Kg wet o-Xylene ND 0.050 mg/Kg wet Surrogate:l,2-Dichloroethane-d4 0.0247 mg/Kg wet 0.0250 98.6 70-130 Surrogate: Toluene-d8 0.0246 mg/Kg wet 0.0250 98.3 70-130 Surrogate: 4-Bromofluorobenzene 0.0250 mg/Kg wet 0.0250 100 70-130 LCS (B215584-BSI) Prepared: 10/24/18 Analyzed: 10/27/18 Acetone 0.155 0.057 mg/Kg wet 0.113 137 70-160 t Acrylonitrile 0.0102 0.0057 mg/Kg wet 0,0113 90.1 70-130 tert-Amyl Methyl Ether (TAME) 0.0107 0.00057 mg/Kg wet 0.0113 94.1 70-130 Benzene 0.0108 0.0011 mg/Kgwet 0.0113 95.5 70-130 Bromobenzene 0.0112 0.0011 mg/Kg wet 0,0113 98.9 70-130 Bromochloromethane 0.0119 0.0011 mg/Kg wet 0.0113 105 70-130 Bromodichloromethane 0.0115 0.0011 mg/Kgwet 0.0113 102 70-130 Bromoform 0.00991 0.0011 mg/Kg wet 0,0113 87.4 70-130 Bromomethane 0.00564 0.0023 mg/Kg wet 0.0113 49.8 40-130 t 2-Butanone (MEK) 0.126 0.023 mg/Kg wet 0.113 111 70-160 t tert-Butyl Alcohol (TBA) 0.0780 0.023 mg/Kg wet 0.113 68.8 40-130 t n-Butylbenzene 0.0111 0.0011 mg/Kg wet 0.0113 97.7 70-130 sec-Butylbenzene 0.0116 0.0011 mg/Kgwet 0.0113 103 70-130 tert-Butylbenzene 0.0113 0.0011 mg/Kg wet 0,0113 100 70-160 t tert-Butyl Ethyl Ether (TBEE) 0.0111 0.00057 mg/Kg wet 0.0113 97.9 70-130 Carbon Disulfide 0.0114 0.0034 mg/Kg wet 0.0113 100 70-130 Carbon Tetrachloride 0.0104 0.0011 mg/Kg wet 0,0113 91.6 70-130 Chlorobenzene 0.0117 0.0011 mg/Kg wet 0.0113 104 70-130 Chlorodibromomethane 0.0123 0.00057 mg/Kgwet 0.0113 108 70-130 Chloroethane 0.0101 0.0023 mg/Kg wet 0,0113 89.3 70-130 Chloroform 0.0113 0.0023 mg/Kg wet 0.0113 100 70-130 Chloromethane 0.0104 0.0023 mg/Kgwet 0.0113 91.4 70-130 2-Chlorotoluene 0.0113 0.0011 mg/Kg wet 0,0113 100 70-130 4-Chlorotoluene 0.0117 0.0011 mg/Kg wet 0.0113 103 70-130 1,2-Dibromo-3-chloropropane(DBCP) 0.00954 0.0057 mg/Kgwet 0.0113 84.2 70-130 1,2-Dibromoethane (EDB) 0.0114 0.00057 mg/Kg wet 0,0113 101 70-130 Dibromomethane 0.0123 0.0011 mg/Kg wet 0.0113 108 70-130 1,2-Dichlorobenzene 0.0118 0.0011 mg/Kgwet 0.0113 104 70-130 1,3-Dichlorobenzene 0.0119 0.0011 mg/Kg wet 0,0113 105 70-130 1,4-Dichlorobenzene 0.0113 0.0011 mg/Kg wet 0.0113 99.7 70-130 trans-1,4-Dichloro-2-butene 0.00975 0.0023 mg/Kgwet 0.0113 86.0 70-130 Dichlorodifluoromethane (Freon 12) 0.00811 0.0023 mg/Kg wet 0,0113 71.6 40-160 1,1-Dichloroethane 0.0112 0.0011 mg/Kg wet 0.0113 99.2 70-130 1,2-Dichloroethane 0.0114 0.0011 mg/Kgwet 0.0113 101 70-130 1,1-Dichloroethylene 0.0102 0.0011 mg/Kg wet 0,0113 90.4 70-130 cis-1,2-Dichloroethylene 0.0115 0.0011 mg/Kg wet 0.0113 101 70-130 trans-1,2-Dichloroethylene 0.0111 0.0011 mg/Kgwet 0.0113 97.6 70-130 Page 51 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215584 - SW-846 5035 LCS (B215584-BSI) Prepared: 10/24/18 Analyzed: 10/27/18 1,2-Dichloropropane 0.0109 0.0011 mg/Kg wet 0.0113 96.4 70-130 1,3-Dichloropropane 0.0109 0.00057 mg/Kg wet 0.0113 96.4 70-130 2,2-Dichloropropane 0.00804 0.0011 mg/Kg wet 0.0113 70.9 70-130 1,1-Dichloropropene 0.0106 0.0023 mg/Kg wet 0.0113 93.2 70-130 cis-1,3-Dichloropropene 0.0115 0.00057 mg/Kg wet 0.0113 102 70-130 trans-1,3-Dichloropropene 0.0122 0.00057 mg/Kg wet 0.0113 108 70-130 Diethyl Ether 0.0120 0.0023 mg/Kg wet 0.0113 106 70-130 Diisopropyl Ether (DIPE) 0.0112 0.00057 mg/Kg wet 0.0113 98.7 70-130 1,4-Dioxane 0.0972 0.057 mg/Kg wet 0.113 85.8 40-160 t Ethylbenzene 0.0115 0.0011 mg/Kg wet 0.0113 102 70-130 Hexachlorobutadiene 0.0112 0.0011 mg/Kg wet 0.0113 98.6 70-160 2-Hexanone (MBK) 0.115 0.011 mg/Kg wet 0.113 102 70-160 t Isopropylbenzene(Cumene) 0.0114 0.0011 mg/Kg wet 0.0113 101 70-130 p-Isopropyholuene (p-Cymene) 0.0109 0.0011 mg/Kg wet 0.0113 95.9 70-130 Methyl tert-Butyl Ether (MTBE) 0.0116 0.0011 mg/Kg wet 0.0113 102 70-130 Methylene Chloride 0.0109 0.0057 mg/Kg wet 0.0113 96.5 40-160 f 4-Methyl-2-pentanone (MIBK) 0.104 0.011 mg/Kg wet 0.113 91.5 70-160 t Naphthalene 0.0100 0.0023 mg/Kg wet 0.0113 88.6 40-130 t n-Propylbenzene 0.0115 0.0011 mg/Kg wet 0.0113 102 70-130 Styrene 0.0118 0.0011 mg/Kg wet 0.0113 104 70-130 1, 1, 1,2-Tetrachloroethane 0.0114 0.0011 mg/Kg wet 0.0113 101 70-130 1,1,2,2-Tetrachloroethane 0.0102 0.00057 mg/Kg wet 0.0113 90.0 70-130 Tetrachloroethylene 0.0111 0.0011 mg/Kg wet 0.0113 97.7 70-130 Tetrahydrofuran 0.0108 0.011 mg/Kg wet 0.0113 95.3 70-130 J Toluene 0.0112 0.0011 mg/Kg wet 0.0113 99.0 70-130 1,2,3-Trichlorobenzene 0.0103 0.0057 mg/Kg wet 0.0113 91.0 70-130 1,2,4-Trichlorobenzene 0.00904 0.0011 mg/Kg wet 0.0113 79.8 70-130 1,3,5-Trichlorobenzene 0.0116 0.0011 mg/Kg wet 0.0113 102 70-130 1, 1, 1 -Trichloroethane 0.0110 0.0011 mg/Kg wet 0.0113 97.0 70-130 1,1,2-Trichloroethane 0.0113 0.0011 mg/Kg wet 0.0113 100 70-130 Trichloroethylene 0.0121 0.0011 mg/Kg wet 0.0113 107 70-130 Trichlorofluoromethane (Freon 11) 0.00886 0.0023 mg/Kg wet 0.0113 78.2 70-130 1,2,3-Trichloropropane 0.0107 0.0023 mg/Kg wet 0.0113 94.3 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.00961 0.0011 mg/Kg wet 0.0113 84.8 70-130 113) 1,2,4-Trimethylbenzene 0.0115 0.0011 mg/Kg wet 0.0113 101 70-130 1,3,5-Trimethylbenzene 0.0114 0.0011 mg/Kg wet 0,0113 100 70-130 Vinyl Chloride 0.0123 0.0023 mg/Kg wet 0.0113 108 40-130 t m+p Xylene 0.0233 0.0023 mg/Kg wet 0.0227 103 70-130 o-Xylene 0.0119 0.0011 mg/Kg wet 0,0113 105 70-130 Surrogate: 1,2-Dichloroethane-d4 0.0280 mg/Kg wet 0.0283 98.8 70-130 Surrogate: Toluene-d8 0.0283 mg/Kg wet 0.0283 99.8 70-130 Surrogate:4-Bromofluorobenzene 0.0282 mg/Kg wet 0.0283 99.6 70-130 Page 52 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215584 - SW-846 5035 LCS Dup (B215584-BSD1) Prepared: 10/24/18 Analyzed: 10/27/18 Acetone 0.134 0.057 mg/Kg wet 0.113 118 70-160 14.9 25 f Acrylonitrile 0.0100 0.0057 mg/Kg wet 0.0113 88.4 70-130 1.90 25 tert-Amyl Methyl Ether (TAME) 0.0104 0.00057 mg/Kg wet 0.0113 92.0 70-130 2.26 25 Benzene 0.0105 0.0011 mg/Kg wet 0.0113 92.8 70-130 2.87 25 Bromobenzene 0.0114 0.0011 mg/Kg wet 0.0113 101 70-130 2.00 25 Bromochloromethane 0.0116 0.0011 mg/Kg wet 0.0113 103 70-130 2.50 25 Bromodichloromethane 0.0111 0.0011 mg/Kg wet 0.0113 98.2 70-130 3.60 25 Bromoform 0.0102 0.0011 mg/Kg wet 0.0113 90.0 70-130 2.93 25 Bromomethane 0.00658 0.0023 mg/Kg wet 0.0113 58.1 40-130 15.4 25 t 2-Butanone (MEK) 0.115 0.023 mg/Kg wet 0.113 101 70-160 9.30 25 f tert-Butyl Alcohol (TBA) 0.0819 0.023 mg/Kg wet 0.113 72.2 40-130 4.88 25 t n-Butylbenzene 0.0112 0.0011 mg/Kg wet 0.0113 98.5 70-130 0.815 25 sec-Butylbenzene 0.0117 0.0011 mg/Kg wet 0.0113 103 70-130 0.681 25 tert-Butylbenzene 0.0112 0.0011 mg/Kg wet 0.0113 99.2 70-160 0.803 25 t tert-Butyl Ethyl Ether (TBEE) 0.0110 0.00057 mg/Kg wet 0.0113 97.3 70-130 0.615 25 Carbon Disulfide 0.0110 0.0034 mg/Kg wet 0.0113 96.7 70-130 3.75 25 Carbon Tetrachloride 0.0101 0.0011 mg/Kg wet 0.0113 89.0 70-130 2.88 25 Chlorobenzene 0.0115 0.0011 mg/Kg wet 0.0113 102 70-130 1.75 25 Chlorodibromomethane 0.0118 0.00057 mg/Kg wet 0.0113 104 70-130 4.15 25 Chloroethane 0.00957 0.0023 mg/Kg wet 0.0113 84.4 70-130 5.64 25 Chloroform 0.0108 0.0023 mg/Kg wet 0.0113 95.0 70-130 5.23 25 Chloromethane 0.00909 0.0023 mg/Kg wet 0.0113 80.2 70-130 13.1 25 2-Chlorotoluene 0.0119 0.0011 mg/Kg wet 0.0113 105 70-130 4.59 25 4-Chlorotoluene 0.0120 0.0011 mg/Kg wet 0.0113 106 70-130 2.67 25 1,2-Dibromo-3-chloropropane (DBCP) 0.0102 0.0057 mg/Kg wet 0.0113 90.1 70-130 6.77 25 1,2-Dibromoethane (EDB) 0.0114 0.00057 mg/Kg wet 0.0113 100 70-130 0.497 25 Dibromomethane 0.0124 0.0011 mg/Kg wet 0.0113 109 70-130 1.10 25 1,2-Dichlorobenzene 0.0116 0.0011 mg/Kg wet 0.0113 102 70-130 1.65 25 1,3-Dichlorobenzene 0.0117 0.0011 mg/Kg wet 0.0113 103 70-130 1.83 25 1,4-Dichlorobenzene 0.0112 0.0011 mg/Kg wet 0.0113 99.0 70-130 0.705 25 trans-1,4-Dichloro-2-butene 0.0104 0.0023 mg/Kg wet 0.0113 91.8 70-130 6.52 25 Dichlorodifluoromethane (Freon 12) 0.00784 0.0023 mg/Kg wet 0.0113 69.2 40-160 3.41 25 t 1,1-Dichloroethane 0.0108 0.0011 mg/Kg wet 0.0113 94.9 70-130 4.43 25 1,2-Dichloroethane 0.0112 0.0011 mg/Kg wet 0.0113 98.9 70-130 2.10 25 1,1-Dichloroethylene 0.00996 0.0011 mg/Kg wet 0.0113 87.9 70-130 2.80 25 cis-1,2-Dichloroethylene 0.0108 0.0011 mg/Kg wet 0.0113 94.9 70-130 6.62 25 trans-1,2-Dichloroethylene 0.0110 0.0011 mg/Kg wet 0.0113 97.2 70-130 0.411 25 1,2-Dichloropropane 0.0107 0.0011 mg/Kg wet 0.0113 94.5 70-130 1.99 25 1,3-Dichloropropane 0.0109 0.00057 mg/Kg wet 0.0113 96.2 70-130 0.208 25 2,2-Dichloropropane 0.00796 0.0011 mg/Kg wet 0.0113 70.2 70-130 0.992 25 1,1-Dichloropropene 0.0104 0.0023 mg/Kg wet 0.0113 91.5 70-130 1.84 25 cis-1,3-Dichloropropene 0.0110 0.00057 mg/Kg wet 0.0113 97.0 70-130 4.83 25 trans-1,3-Dichloropropene 0.0118 0.00057 mg/Kg wet 0.0113 104 70-130 3.31 25 Diethyl Ether 0.0117 0.0023 mg/Kg wet 0.0113 104 70-130 2.38 25 Diisopropyl Ether (RIPE) 0.0108 0.00057 mg/Kg wet 0.0113 95.4 70-130 3.40 25 1,4-Dioxane 0.103 0.057 mg/Kg wet 0.113 90.9 40-160 5.82 50 I: Ethylbenzene 0.0116 0.0011 mg/Kg wet 0.0113 103 70-130 1.08 25 Hexachlorobutadiene 0.0114 0.0011 mg/Kg wet 0.0113 101 70-160 2.31 25 2-Hexanone (MBK) 0.113 0.011 mg/Kg wet 0.113 99.3 70-160 2.30 25 Isopropylbenzene (Cumene) 0.0117 0.0011 mg/Kg wet 0.0113 103 70-130 1.96 25 p-Isopropyltoluene (p-Cymene) 0.0109 0.0011 mg/Kg wet 0.0113 95.8 70-130 0.104 25 Methyl tert-Butyl Ether (MTBE) 0.0115 0.0011 mg/Kg wet 0.0113 102 70-130 0.686 25 Page 53 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215584 - SW-846 5035 LCS Dup (B215584-BSD1) Prepared: 10/24/18 Analyzed: 10/27/18 Methylene Chloride 0.0106 0.0057 mg/Kg wet 0.0113 93.1 40-160 3.59 25 t 4-Methyl-2-pentanone (MIBK) 0.107 0.011 mg/Kg wet 0.113 94.3 70-160 2.96 25 f Naphthalene 0.0106 0.0023 mg/Kg wet 0.0113 93.2 40-130 5.06 25 t n-Propylbenzene 0.0116 0.0011 mg/Kg wet 0.0113 102 70-130 0.294 25 Styrene 0.0117 0.0011 mg/Kg wet 0.0113 103 70-130 0.675 25 1, 1, 1,2-Tetrachloroethane 0.0113 0.0011 mg/Kg wet 0.0113 100 70-130 0.598 25 1,1,2,2-Tetrachloroethane 0.0109 0.00057 mg/Kg wet 0.0113 96.5 70-130 6.97 25 Tetrachloroethylene 0.0112 0.0011 mg/Kg wet 0.0113 98.6 70-130 0.917 25 Tetrahydrofuran 0.0115 0.011 mg/Kg wet 0.0113 102 70-130 6.69 25 Toluene 0.0112 0.0011 mg/Kg wet 0.0113 99.2 70-130 0.202 25 1,2,3-Trichlorobenzene 0.0107 0.0057 mg/Kg wet 0.0113 94.8 70-130 4.09 25 1,2,4-Trichlorobenzene 0.00934 0.0011 mg/Kg wet 0.0113 82.4 70-130 3.21 25 1,3,5-Trichlorobenzene 0.0119 0.0011 mg/Kg wet 0.0113 105 70-130 2.22 25 1, 1, 1 -Trichloroethane 0.0105 0.0011 mg/Kg wet 0.0113 93.0 70-130 4.21 25 1,1,2-Trichloroethane 0.0115 0.0011 mg/Kg wet 0.0113 102 70-130 1.69 25 Trichloroethylene 0.0117 0.0011 mg/Kg wet 0.0113 103 70-130 3.71 25 Trichlorofluoromethane (Freon 11) 0.00876 0.0023 mg/Kg wet 0.0113 77.3 70-130 1.16 25 1,2,3-Trichloropropane 0.0111 0.0023 mg/Kg wet 0.0113 97.8 70-130 3.64 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.00910 0.0011 mg/Kg wet 0.0113 80.3 70-130 5.45 25 113) 1,2,4-Trimethylbenzene 0.0115 0.0011 mg/Kg wet 0.0113 102 70-130 0.493 25 1,3,5-Trimethylbenzene 0.0117 0.0011 mg/Kg wet 0,0113 103 70-130 2.36 25 Vinyl Chloride 0.0111 0.0023 mg/Kg wet 0.0113 98.0 40-130 9.80 25 t m+p Xylene 0.0236 0.0023 mg/Kg wet 0.0227 104 70-130 1.21 25 o-Xylene 0.0122 0.0011 mg/Kg wet 0.0113 108 70-130 2.16 25 Surrogate: 1,2-Dichloroethane-d4 0.0270 mg/Kg wet 0.0283 95.4 70-130 Surrogate: Toluene-d8 0.0285 mg/Kg wet 0.0283 101 70-130 Surrogate:4-Bromofluorobenzene 0.0291 mg/Kg wet 0.0283 103 70-130 Page 54 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215606 - SW-846 3546 Blank (B215606-BLK1) Prepared: 10/24/18 Analyzed: 10/27/18 Acenaphthene ND 0.17 mg/Kg wet Acenaphthylene ND 0.17 mg/Kg wet Acetophenone ND 0.34 mg/Kg wet Aniline ND 0.34 mg/Kg wet Anthracene ND 0.17 mg/Kg wet Benzidine ND 0.66 mg/Kg wet Benzo(a)anthracene ND 0.17 mg/Kg wet Benzo(a)pyrene ND 0.17 mg/Kg wet Benzo(b)fluoranthene ND 0.17 mg/Kg wet Benzo(g,h,i)perylene ND 0.17 mg/Kg wet Benzo(k)fluoranthene ND 0.17 mg/Kg wet Benzoic Acid ND 1.0 mg/Kg wet Bis(2-chloroethoxy)methane ND 0.34 mg/Kg wet Bis(2-chloroethyl)ether ND 0.34 mg/Kg wet Bis(2-chloroisopropyl)ether ND 0.34 mg/Kg wet Bis(2-Ethylhexyl)phthalate ND 0.34 mg/Kg wet 4-Bromophenylphenylether ND 0.34 mg/Kg wet Butylbenzylphthalate ND 0.34 mg/Kg wet Carbazole ND 0.17 mg/Kg wet 4-Chloroaniline ND 0.66 mg/Kg wet 4-Chloro-3-methylphenol ND 0.66 mg/Kg wet 2-Chloronaphthalene ND 0.34 mg/Kg wet 2-Chlorophenol ND 0.34 mg/Kg wet 4-Chlorophenylphenylether ND 0.34 mg/Kg wet Chrysene ND 0.17 mg/Kg wet Dibenz(a,h)anthracene ND 0.17 mg/Kg wet Dibenzofuran ND 0.34 mg/Kg wet Di-n-butylphthalate ND 0.34 mg/Kg wet 1,2-Dichlorobenzene ND 0.34 mg/Kg wet 1,3-Dichlorobenzene ND 0.34 mg/Kg wet 1,4-Dichlorobenzene ND 0.34 mg/Kg wet 3,3-Dichlorobenzidine ND 0.17 mg/Kg wet 2,4-Dichlorophenol ND 0.34 mg/Kg wet Diethylphthalate ND 0.34 mg/Kg wet 2,4-Dimethylphenol ND 0.34 mg/Kg wet Dimethylphthalate ND 0.34 mg/Kg wet 4,6-Dinitro-2-methylphenol ND 0.34 mg/Kg wet 2,4-Dinitrophenol ND 0.66 mg/Kg wet 2,4-Dinitrotoluene ND 0.34 mg/Kg wet 2,6-Dinitrotoluene ND 0.34 mg/Kg wet Di-n-octylphthalate ND 0.34 mg/Kg wet 1,2-Diphenylhydrazine (as Azobenzene) ND 0.34 mg/Kg wet Fluoranthene ND 0.17 mg/Kg wet Fluorene ND 0.17 mg/Kg wet Hexachlorobenzene ND 0.34 mg/Kg wet Hexachlorobutadiene ND 0.34 mg/Kg wet Hexachlorocyclopentadiene ND 0.34 mg/Kg wet Hexachloroethane ND 0.34 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.17 mg/Kg wet Isophorone ND 0.34 mg/Kg wet 1-Methylnaphthalene ND 0.17 mg/Kg wet 2-Methylnaphthalene ND 0.17 mg/Kg wet V-34 V-05, V-34, R-05, V-04 V-34 Page 55 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215606 - SW-846 3546 Blank (B215606-BLK1) Prepared: 10/24/18 Analyzed: 10/27/18 2-Methylphenol ND 0.34 mg/Kg wet 3/4-Methylphenol ND 0.34 mg/Kg wet Naphthalene ND 0.17 mg/Kg wet 2-Nitroaniline ND 0.34 mg/Kg wet 3-Nitroaniline ND 0.34 mg/Kg wet V-34 4-Nitroaniline ND 0.34 mg/Kg wet Nitrobenzene ND 0.34 mg/Kg wet 2-Nitrophenol ND 0.34 mg/Kg wet 4-Nitrophenol ND 0.66 mg/Kg wet V-20, V-34 N-Nitrosodimethylamine ND 0.34 mg/Kg wet N-Nitrosodiphenylamine ND 0.34 mg/Kg wet N-Nitrosodi-n-propylamine ND 0.34 mg/Kg wet Pentachloronitrobenzene ND 0.34 mg/Kg wet V-16 Pentachlorophenol ND 0.34 mg/Kg wet Phenanthrene ND 0.17 mg/Kg wet Phenol ND 0.34 mg/Kg wet Pyrene ND 0.17 mg/Kg wet Pyridine ND 0.34 mg/Kg wet 1,2,4,5-Tetrachlorobenzene ND 0.34 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.34 mg/Kg wet 2,4,5-Trichlorophenol ND 0.34 mg/Kg wet 2,4,6-Trichlorophenol ND 0.34 mg/Kg wet Surrogate:2-Fluorophenol 5.09 mg/Kg wet 6.67 76.3 30-130 Surrogate: Phenol-d6 5.19 mg/Kg wet 6.67 77.8 30-130 Surrogate: Nitrobenzene-d5 2.51 mg/Kg wet 3.33 75.2 30-130 Surrogate:2-Fluorobiphenyl 2.06 mg/Kg wet 3.33 61.7 30-130 Surrogate: 2,4,6-Tribromophenol 5.25 mg/Kg wet 6.67 78.7 30-130 Surrogate: p-Terphenyl-dl4 2.32 mg/Kg wet 3.33 69.6 30-130 LCS (B215606-BSI) Prepared: 10/24/18 Analyzed: 10/27/18 Acenaphthene 1.18 0.17 mg/Kg wet 1.67 70.9 40-140 Acenaphthylene 1.26 0.17 mg/Kg wet 1.67 75.8 40-140 Acetophenone 1.14 0.34 mg/Kg wet 1.67 68.4 40-140 Aniline 1.09 0.34 mg/Kg wet 1.67 65.5 10-140 V-34 f Anthracene 1.20 0.17 mg/Kg wet 1.67 71.9 40-140 Benzidine 1.37 0.66 mg/Kg wet 1.67 82.2 40-140 R-05, V-04, V-05, V-34 Benzo(a)anthracene 1.27 0.17 mg/Kg wet 1.67 76.3 40-140 Benzo(a)pyrene 1.25 0.17 mg/Kg wet 1.67 74.9 40-140 Benzo(b)fluoranthene 1.17 0.17 mg/Kg wet 1.67 70.0 40-140 Benzo(g,h,i)perylene 1.07 0.17 mg/Kg wet 1.67 64.2 40-140 Benzo(k)fluoranthene 1.19 0.17 mg/Kg wet 1.67 71.6 40-140 Benzoic Acid 0.579 1.0 mg/Kg wet 1.67 34.7 30-130 1 Bis(2-chloroethoxy)methane 1.34 0.34 mg/Kg wet 1.67 80.7 40-140 Bis(2-chloroethyl)ether 1.17 0.34 mg/Kg wet 1.67 70.1 40-140 Bis(2-chloroisopropyl)ether 1.25 0.34 mg/Kg wet 1.67 75.0 40-140 Bis(2-Ethylhexyl)phthalate 1.21 0.34 mg/Kg wet 1.67 72.6 40-140 4-Bromophenylphenylether 1.25 0.34 mg/Kg wet 1.67 75.0 40-140 Butylbenzylphthalate 1.29 0.34 mg/Kg wet 1.67 77.2 40-140 Carbazole 1.17 0.17 mg/Kg wet 1.67 69.9 40-140 4-Chloroaniline 1.12 0.66 mg/Kg wet 1.67 67.0 10-140 V-34 4-Chloro-3-methylphenol 1.25 0.66 mg/Kg wet 1.67 75.2 30-130 2-Chloronaphthalene 1.11 0.34 mg/Kg wet 1.67 66.4 40-140 Page 56 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215606 - SW-846 3546 LCS (B215606-BSI) Prepared: 10/24/18 Analyzed: 10/27/18 2-Chlorophenol 1.12 0.34 mg/Kg wet 1.67 67.3 30-130 4-Chlorophenylphenylether 1.31 0.34 mg/Kg wet 1.67 78.6 40-140 Chrysene 1.21 0.17 mg/Kg wet 1.67 72.3 40-140 Dibenz(a,h)anthracene 1.06 0.17 mg/Kg wet 1.67 63.3 40-140 Dibenzofuran 1.30 0.34 mg/Kg wet 1.67 78.0 40-140 Di-n-butylphthalate 1.21 0.34 mg/Kg wet 1.67 72.5 40-140 1,2-Dichlorobenzene 1.01 0.34 mg/Kg wet 1.67 60.3 40-140 1,3-Dichlorobenzene 0.962 0.34 mg/Kg wet 1.67 57.7 40-140 1,4-Dichlorobenzene 0.975 0.34 mg/Kg wet 1.67 58.5 40-140 3,3-Dichlorobenzidine 1.40 0.17 mg/Kg wet 1.67 84.2 20-140 t 2,4-Dichlorophenol 1.22 0.34 mg/Kg wet 1.67 73.2 30-130 Diethylphthalate 1.30 0.34 mg/Kg wet 1.67 78.0 40-140 2,4-Dimethylphenol 1.28 0.34 mg/Kg wet 1.67 76.9 30-130 Dimethylphthalate 1.33 0.34 mg/Kg wet 1.67 80.1 40-140 4,6-Dinitro-2-methylphenol 1.13 0.34 mg/Kg wet 1.67 67.9 30-130 2,4-Dinitrophenol 0.889 0.66 mg/Kg wet 1.67 53.3 30-130 2,4-Dinitrotoluene 1.30 0.34 mg/Kg wet 1.67 78.0 40-140 2,6-Dinitrotoluene 1.35 0.34 mg/Kg wet 1.67 81.1 40-140 Di-n-octylphthalate 1.16 0.34 mg/Kg wet 1.67 69.7 40-140 1,2-Diphenylhydrazine (as Azobenzene) 1.30 0.34 mg/Kg wet 1.67 78.0 40-140 Fluoranthene 1.17 0.17 mg/Kg wet 1.67 70.1 40-140 Fluorene 1.25 0.17 mg/Kg wet 1.67 75.1 40-140 Hexachlorobenzene 1.24 0.34 mg/Kg wet 1.67 74.7 40-140 Hexachlorobutadiene 1.11 0.34 mg/Kg wet 1.67 66.5 40-140 Hexachlorocyclopentadiene 1.09 0.34 mg/Kg wet 1.67 65.7 40-140 Hexachloroethane 1.04 0.34 mg/Kg wet 1.67 62.1 40-140 Indeno(1,2,3-cd)pyrene 1.07 0.17 mg/Kg wet 1.67 64.2 40-140 Isophorone 1.22 0.34 mg/Kg wet 1.67 73.3 40-140 1-Methylnaphthalene 1.06 0.17 mg/Kg wet 1.67 63.3 40-140 2-Methylnaphthalene 1.20 0.17 mg/Kg wet 1.67 71.8 40-140 2-Methylphenol 1.09 0.34 mg/Kg wet 1.67 65.4 30-130 3/4-Methylphenol 1.17 0.34 mg/Kg wet 1.67 70.3 30-130 Naphthalene 1.11 0.17 mg/Kg wet 1.67 66.4 40-140 2-Nitroaniline 1.32 0.34 mg/Kg wet 1.67 79.2 40-140 3-Nitroaniline 1.30 0.34 mg/Kg wet 1.67 77.8 30-140 V-34 t 4-Nitroaniline 1.33 0.34 mg/Kg wet 1.67 79.7 40-140 Nitrobenzene 1.12 0.34 mg/Kg wet 1.67 67.2 40-140 2-Nitrophenol 1.16 0.34 mg/Kg wet 1.67 69.8 30-130 4-Nitrophenol 1.37 0.66 mg/Kg wet 1.67 94.5 30-130 V-06,V-34 N-Nitrosodimethylarnme 0.955 0.34 mg/Kg wet 1.67 57.3 40-140 N-Nitrosodiphenylamine 1.49 0.34 mg/Kg wet 1.67 89.2 40-140 N-Nitrosodi-n-propylamine 1.14 0.34 mg/Kg wet 1.67 68.3 40-140 Pentachloronitrobenzene 1.27 0.34 mg/Kg wet 1.67 76.0 40-140 V-16 Pentachlorophenol 0.869 0.34 mg/Kg wet 1.67 52.1 30-130 Phenanthrene 1.21 0.17 mg/Kg wet 1.67 72.6 40-140 Phenol 1.24 0.34 mg/Kg wet 1.67 74.6 30-130 Pyrene 1.26 0.17 mg/Kg wet 1.67 75.5 40-140 Pyridine 0.659 0.34 mg/Kg wet 1.67 39.5 30-140 1,2,4,5-Tetrachlorobenzene 1.29 0.34 mg/Kg wet 1.67 77.3 40-140 1,2,4-Trichlorobenzene 1.09 0.34 mg/Kg wet 1.67 65.1 40-140 2,4,5-Trichlorophenol 1.33 0.34 mg/Kg wet 1.67 79.8 30-130 2,4,6-Trichlorophenol 1.34 0.34 mg/Kg wet 1.67 80.4 30-130 Page 57 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215606 - SW-846 3546 LCS (B215606-BSI) Prepared: 10/24/18 Analyzed: 10/27/18 Surrogate:2-Fluorophenol 4.94 mg/Kg wet 6.67 74.1 30-130 Surrogate: Phenol-d6 5.11 mg/Kg wet 6.67 76.7 30-130 Surrogate: Nitrobenzene-d5 2.50 mg/Kg wet 3.33 75.1 30-130 Surrogate:2-Fluorobiphenyl 2.29 mg/Kg wet 3.33 68.7 30-130 Surrogate: 2,4,6-Tribromophenol 5.87 mg/Kg wet 6.67 88.1 30-130 Surrogate:p-Terphenyl-dl4 2.57 mg/Kg wet 3.33 77.1 30-130 LCS Dup (B215606-BSD1) Prepared: 10/24/18 Analyzed: 10/27/18 Acenaphthene 1.19 0.17 mg/Kg wet 1.67 71.3 Acenaphthylene 1.26 0.17 mg/Kg wet 1.67 75.4 Acetophenone 1.24 0.34 mg/Kg wet 1.67 74.6 Aniline 0.883 0.34 mg/Kg wet 1.67 53.0 Anthracene 1.19 0.17 mg/Kg wet 1.67 71.4 Benzidine 0.923 0.66 mg/Kg wet 1.67 55.4 Benzo(a)anthracene 1.26 0.17 mg/Kg wet 1.67 75.3 Benzo(a)pyrene 1.28 0.17 mg/Kg wet 1.67 77.0 Benzo(b)fluoranthene 1.17 0.17 mg/Kg wet 1.67 70.3 Benzo(g,h,i)perylene 1.02 0.17 mg/Kg wet 1.67 61.1 Benzo(k)fluoranthene 1.19 0.17 mg/Kg wet 1.67 71.3 Benzoic Acid 0.601 1.0 mg/Kg wet 1.67 36.1 Bis(2-chloroethoxy)methane 1.41 0.34 mg/Kg wet 1.67 84.7 Bis(2-chloroethyl)ether 1.33 0.34 mg/Kg wet 1.67 79.9 Bis(2-chloroisopropyl)ether 1.40 0.34 mg/Kg wet 1.67 84.2 Bis(2-Ethylhexyl)phthalate 1.19 0.34 mg/Kg wet 1.67 71.2 4-Bromophenylphenylether 1.26 0.34 mg/Kg wet 1.67 75.4 Butylbenzylphthalate 1.30 0.34 mg/Kg wet 1.67 77.8 Carbazole 1.16 0.17 mg/Kg wet 1.67 69.4 4-Chloroaniline 0.833 0.66 mg/Kg wet 1.67 50.0 4-Chloro-3-methylphenol 1.28 0.66 mg/Kg wet 1.67 76.8 2-Chloronaphthalene 1.25 0.34 mg/Kg wet 1.67 74.9 2-Chorophenol 1.27 0.34 mg/Kg wet 1.67 76.1 4-Chlorophenylphenylether 1.30 0.34 mg/Kg wet 1.67 77.9 Chrysene 1.18 0.17 mg/Kg wet 1.67 70.6 Dibenz(a,h)anthracene 1.03 0.17 mg/Kg wet 1.67 62.0 Dibenzofuran 1.29 0.34 mg/Kg wet 1.67 77.3 Di-n-butylphthalate 1.18 0.34 mg/Kg wet 1.67 70.6 1,2-Dichlorobenzene 1.14 0.34 mg/Kg wet 1.67 68.2 1,3-Dichlorobenzene 1.09 0.34 mg/Kg wet 1.67 65.3 1,4-Dichlorobenzene 1.11 0.34 mg/Kg wet 1.67 66.8 3,3-Dichlorobenzidine 1.08 0.17 mg/Kg wet 1.67 65.0 2,4-Dichlorophenol 1.22 0.34 mg/Kg wet 1.67 73.0 Diethylphthalate 1.30 0.34 mg/Kg wet 1.67 77.7 2,4-Dimethylphenol 1.36 0.34 mg/Kg wet 1.67 81.9 Dimethylphthalate 1.32 0.34 mg/Kg wet 1.67 79.3 4,6-Dinitro-2-methylphenol 1.08 0.34 mg/Kg wet 1.67 64.6 2,4-Dinitrophenol 0.814 0.66 mg/Kg wet 1.67 48.8 2,4-Dinitrotoluene 1.31 0.34 mg/Kg wet 1.67 78.8 2,6-Dinitrotoluene 1.37 0.34 mg/Kg wet 1.67 82.2 Di-n-octylphthalate 1.16 0.34 mg/Kg wet 1.67 69.7 1,2-Diphenylhydrazine (as Azobenzene) 1.26 0.34 mg/Kg wet 1.67 75.7 Fluoranthene 1.16 0.17 mg/Kg wet 1.67 69.7 Fluorene 1.27 0.17 mg/Kg wet 1.67 76.1 40-140 0.591 30 40-140 0.503 30 40-140 8.56 30 10-140 21.1 50 V-34 t $ 40-140 0.698 30 40-140 39.0 * 30 R-05, V-04, V-05, V-34 40-140 1.29 30 40-140 2.71 30 40-140 0.342 30 40-140 4.82 30 40-140 0.420 30 30-130 3.78 50 J $ 40-140 4.91 30 40-140 13.0 30 40-140 11.6 30 40-140 1.89 30 40-140 0.558 30 40-140 0.826 30 40-140 0.804 30 10-140 29.2 30 V-34 t 30-130 2.11 30 40-140 12.1 30 30-130 12.3 30 40-140 0.869 30 40-140 2.46 30 40-140 2.17 30 40-140 0.798 30 40-140 2.63 30 40-140 12.3 30 40-140 12.3 30 40-140 13.2 30 20-140 25.8 50 t # 30-130 0.301 30 40-140 0.359 30 30-130 6.27 30 40-140 0.928 30 30-130 4.92 30 30-130 8.81 30 40-140 0.995 30 40-140 1.35 30 40-140 0.00 30 40-140 2.99 30 40-140 0.658 30 40-140 1.27 30 Page 58 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215606 - SW-846 3546 LCS Dup (B215606-BSD1) Prepared: 10/24/18 Analyzed: 10/27/18 Hexachlorobenzene 1.26 0.34 mg/Kg wet 1.67 75.6 40-140 1.28 30 Hexachlorobutadiene 1.18 0.34 mg/Kg wet 1.67 70.7 40-140 6.12 30 Hexachlorocyclopentadiene 1.12 0.34 mg/Kg wet 1.67 66.9 40-140 1.87 30 Hexachloroethane 1.19 0.34 mg/Kg wet 1.67 71.4 40-140 14.0 30 Indeno(1,2,3-cd)pyrene 1.06 0.17 mg/Kg wet 1.67 63.3 40-140 1.35 30 Isophorone 1.27 0.34 mg/Kg wet 1.67 76.4 40-140 4.03 30 I-Methylnaphthalene 1.11 0.17 mg/Kg wet 1.67 66.4 40-140 4.78 30 2-Methylnaphthalene 1.26 0.17 mg/Kg wet 1.67 75.7 40-140 5.26 30 2-Methylphenol 1.19 0.34 mg/Kg wet 1.67 71.6 30-130 9.08 30 3/4-Methylphenol 1.23 0.34 mg/Kg wet 1.67 73.8 30-130 4.80 30 Naphthalene 1.15 0.17 mg/Kg wet 1.67 69.2 40-140 4.10 30 2-Nitroanihne 1.35 0.34 mg/Kg wet 1.67 81.0 40-140 2.22 30 3-Nitroaniline 1.13 0.34 mg/Kg wet 1.67 68.0 30-140 13.5 30 V-34 f 4-Nitroaniline 1.32 0.34 mg/Kg wet 1.67 79.3 40-140 0.478 30 Nitrobenzene 1.24 0.34 mg/Kg wet 1.67 74.4 40-140 10.2 30 2-Nitrophenol 1.20 0.34 mg/Kg wet 1.67 72.1 30-130 3.33 30 4-Nitrophenol 1.41 0.66 mg/Kg wet 1.67 84.4 30-130 11.2 50 V-06, V-34 $ N-Nitrosodimethylamine 1.17 0.34 mg/Kg wet 1.67 70.1 40-140 20.1 30 N-Nitrosodiphenylamine 1.43 0.34 mg/Kg wet 1.67 85.8 40-140 3.79 30 N-Nitrosodi-n-propylamine 1.22 0.34 mg/Kg wet 1.67 73.5 40-140 7.31 30 Pentachloronitrobenzene 1.20 0.34 mg/Kg wet 1.67 71.9 40-140 5.57 30 V-16 Pentachlorophenol 0.862 0.34 mg/Kg wet 1.67 51.7 30-130 0.809 30 Phenanthrene 1.21 0.17 mg/Kg wet 1.67 72.5 40-140 0.221 30 Phenol 1.30 0.34 mg/Kg wet 1.67 77.9 30-130 4.27 30 Pyrene 1.27 0.17 mg/Kg wet 1.67 75.9 40-140 0.528 30 Pyridine 0.828 0.34 mg/Kg wet 1.67 49.7 30-140 22.7 30 t 1,2,4,5-Tetrachlorobenzene 1.27 0.34 mg/Kg wet 1.67 76.4 40-140 1.17 30 1,2,4-Trichlorobenzene 1.17 0.34 mg/Kg wet 1.67 70.2 40-140 7.45 30 2,4,5-Trichlorophenol 1.34 0.34 mg/Kg wet 1.67 80.3 30-130 0.574 30 2,4,6-Trichlorophenol 1.31 0.34 mg/Kg wet 1.67 78.5 30-130 2.42 30 Surrogate:2-Fluorophenol 5.33 mg/Kg wet 6.67 80.0 30-130 Surrogate: Phenol-d6 5.36 mg/Kg wet 6.67 80.4 30-130 Surrogate: Nitrobenzene-d5 2.66 mg/Kg wet 3.33 79.9 30-130 Surrogate: 2-Fluorobiphenyl 2.19 mg/Kg wet 3.33 65.8 30-130 Surrogate: 2,4,6-Tribromophenol 5.84 mg/Kg wet 6.67 87.7 30-130 Surrogate: p-Terphenyl-dl4 2.53 mg/Kg wet 3.33 75.9 30-130 Page 59 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215618 - SW-846 3546 Blank (B215618-BLK1) Prepared: 10/24/18 Analyzed: 10/25/18 C9-C 18 Aliphatics ND 10 mg/Kg wet C19-C36 Aliphatics ND 10 mg/Kg wet Cl 1-C22 Aromatics ND 10 mg/Kg wet Acenaphthene ND 0.10 mg/Kg wet Acenaphthylene ND 0.10 mg/Kg wet Anthracene ND 0.10 mg/Kg wet Benzo(a)anthracene ND 0.10 mg/Kg wet Benzo(a)pyrene ND 0.10 mg/Kg wet Benzo(b)fluoranthene ND 0.10 mg/Kg wet Benzo(g,h,i)perylene ND 0.10 mg/Kg wet Benzo(b)fluoranthene ND 0.10 mg/Kg wet Chrysene ND 0.10 mg/Kg wet Dibenz(a,h)anthracene ND 0.10 mg/Kg wet Fluoranthene ND 0.10 mg/Kg wet Fluorene ND 0.10 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.10 mg/Kg wet 2-Methylnaphthalene ND 0.10 mg/Kg wet Naphthalene ND 0.10 mg/Kg wet Phenanthrene ND 0.10 mg/Kg wet Pyrene ND 0.10 mg/Kg wet n-Decane ND 0.10 mg/Kg wet n-Docosane ND 0.10 mg/Kg wet n-Dodecane ND 0.10 mg/Kg wet n-Eicosane ND 0.10 mg/Kg wet n-Hexacosane ND 0.10 mg/Kg wet n-Hexadecane ND 0.10 mg/Kg wet n-Hexatriacontane ND 0.10 mg/Kg wet n-Nonadecane ND 0.10 mg/Kg wet n-Nonane ND 0.10 mg/Kg wet n-Octacosane ND 0.10 mg/Kg wet n-Octadecane 0.11 0.10 mg/Kg wet n-Tetracosane ND 0.10 mg/Kg wet n-Tetradecane ND 0.10 mg/Kg wet n-Triacontane ND 0.10 mg/Kg wet Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet Surrogate: Chlorooctadecane (COD) 4.16 mg/Kg wet 5.20 80.0 40-140 Surrogate: o-Terphenyl (OTP) 4.26 mg/Kg wet 5.00 85.2 40-140 Surrogate:2-Bromonaphthalene 4.31 mg/Kg wet 5.00 86.3 40-140 Surrogate: 2-Fluorobiphenyl 4.69 mg/Kg wet 5.00 93.8 40-140 LCS (B215618-BS1) Prepared: 10/24/18 Analyzed: 10/25/18 C9-C 18 Aliphatics 24.2 10 mg/Kg wet 30.0 80.8 40-140 C19-C36Aliphatics 37.3 10 mg/Kg wet 40.0 93.1 40-140 Acenaphthene 3.69 0.10 mg/Kg wet 5.00 73.8 40-140 Acenaphthylene 3.44 0.10 mg/Kg wet 5.00 68.8 40-140 Anthracene 4.01 0.10 mg/Kg wet 5.00 80.2 40-140 Benzo(a)anthracene 3.96 0.10 mg/Kg wet 5.00 79.2 40-140 Benzo(a)pyrene 3.88 0.10 mg/Kg wet 5.00 77.7 40-140 Benzo(b)fluoranthene 4.04 0.10 mg/Kg wet 5.00 80.7 40-140 Benzo(g,h,i)perylene 3.87 0.10 mg/Kg wet 5.00 77.3 40-140 Benzo(k)fluoranthene 3.96 0.10 mg/Kg wet 5.00 79.2 40-140 Page 60 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215618 - SW-846 3546 LCS (B215618-BSI) Prepared: 10/24/18 Analyzed: 10/25/18 Chrysene 4.05 0.10 mg/Kg wet 5.00 81.0 40-140 Dibenz(a,h)anthracene 4.04 0.10 mg/Kg wet 5.00 80.7 40-140 Fluoranthene 4.10 0.10 mg/Kg wet 5.00 82.0 40-140 Fluorene 3.77 0.10 mg/Kg wet 5.00 75.4 40-140 Indeno(1,2,3-cd)pyrene 3.80 0.10 mg/Kg wet 5.00 76.1 40-140 2-Methylnaphthalene 3.20 0.10 mg/Kg wet 5.00 64.0 40-140 Naphthalene 3.25 0.10 mg/Kg wet 5.00 65.1 40-140 Phenanthrene 4.08 0.10 mg/Kg wet 5.00 81.5 40-140 Pyrene 4.12 0.10 mg/Kg wet 5.00 82.4 40-140 n-Decane 2.80 0.10 mg/Kg wet 5.00 56.1 40-140 n-Docosane 4.01 0.10 mg/Kg wet 5.00 80.3 40-140 n-Dodecane 3.27 0.10 mg/Kg wet 5.00 65.4 40-140 n-Eicosane 4.02 0.10 mg/Kg wet 5.00 80.5 40-140 n-Hexacosane 3.96 0.10 mg/Kg wet 5.00 79.3 40-140 n-Hexadecane 4.06 0.10 mg/Kg wet 5.00 81.2 40-140 n-Hexatriacontane 3.90 0.10 mg/Kg wet 5.00 77.9 40-140 n-Nonadecane 4.03 0.10 mg/Kg wet 5.00 80.5 40-140 n-Nonane 2.16 0.10 mg/Kg wet 5.00 43.1 30-140 n-Octacosane 3.87 0.10 mg/Kg wet 5.00 77.3 40-140 n-Octadecane 4.15 0.10 mg/Kg wet 5.00 83.0 40-140 B n-Tetracosane 4.00 0.10 mg/Kg wet 5.00 80.1 40-140 n-Tetradecane 3.64 0.10 mg/Kg wet 5.00 72.8 40-140 n-Triacontane 3.90 0.10 mg/Kg wet 5.00 77.9 40-140 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 3.99 mg/Kg wet 5.20 76.6 40-140 Surrogate: o-Terphenyl (OTP) 4.07 mg/Kg wet 5.00 81.4 40-140 Surrogate: 2-Bromonaphthalene 4.10 mg/Kg wet 5.00 81.9 40-140 Surrogate:2-Fluorobiphenyl 4.63 mg/Kg wet 5.00 92.7 40-140 LCS Dup (B215618-BSD1) Prepared: 10/24/18 Analyzed: 10/25/18 C9-C18Aliphatics 25.2 10 mg/Kg wet 30.0 83.9 40-140 3.75 C19-C36Aliphatics 39.9 10 mg/Kg wet 40.0 99.8 40-140 6.94 Acenaphthene 4.20 0.10 mg/Kg wet 5.00 84.0 40-140 12.9 Acenaphthylene 3.91 0.10 mg/Kg wet 5.00 78.2 40-140 12.8 Anthracene 4.47 0.10 mg/Kg wet 5.00 89.3 40-140 10.8 Benzo(a)anthracene 4.43 0.10 mg/Kg wet 5.00 88.5 40-140 11.1 Benzo(a)pyrene 4.34 0.10 mg/Kg wet 5.00 86.8 40-140 11.1 Benzo(b)fluoranthene 4.51 0.10 mg/Kg wet 5.00 90.2 40-140 11.1 Benzo(g,h,i)perylene 4.32 0.10 mg/Kg wet 5.00 86.5 40-140 11.2 Benzo(k)fluoranthene 4.42 0.10 mg/Kg wet 5.00 88.3 40-140 10.8 Chrysene 4.54 0.10 mg/Kg wet 5.00 90.8 40-140 11.4 Dibenz(a,h)anthracene 4.48 0.10 mg/Kg wet 5.00 89.5 40-140 10.3 Fluoranthene 4.56 0.10 mg/Kg wet 5.00 91.2 40-140 10.6 Fluorene 4.27 0.10 mg/Kg wet 5.00 85.4 40-140 12.4 Indeno(1,2,3-cd)pyrene 4.24 0.10 mg/Kg wet 5.00 84.7 40-140 10.8 2-Methylnaphthalene 3.62 0.10 mg/Kg wet 5.00 72.4 40-140 12.3 Naphthalene 3.63 0.10 mg/Kg wet 5.00 72.6 40-140 11.0 Phenanthrene 4.55 0.10 mg/Kg wet 5.00 91.0 40-140 11.0 Pyrene 4.38 0.10 mg/Kg wet 5.00 91.6 40-140 10.6 n-Decane 2.91 0.10 mg/Kg wet 5.00 58.1 40-140 3.60 n-Docosane 4.39 0.10 mg/Kg wet 5.00 87.8 40-140 8.90 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 Page 61 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215618 - SW-846 3546 LCS Dup (B215618-BSD1) Prepared: 10/24/18 Analyzed: 10/25/18 n-Dodecane 3.52 0.10 mg/Kg wet 5.00 70.5 40-140 7.50 25 n-Eicosane 4.54 0.10 mg/Kg wet 5.00 90.7 40-140 11.9 25 n-Hexacosane 4.34 0.10 mg/Kg wet 5.00 86.8 40-140 9.04 25 n-Hexadecane 4.43 0.10 mg/Kg wet 5.00 88.6 40-140 8.69 25 n-Hexatriacontane 4.22 0.10 mg/Kg wet 5.00 84.5 40-140 8.07 25 n-Nonadecane 4.39 0.10 mg/Kg wet 5.00 87.7 40-140 8.56 25 n-Nonane 2.12 0.10 mg/Kg wet 5.00 42.4 30-140 1.69 25 n-Octacosane 4.24 0.10 mg/Kg wet 5.00 84.7 40-140 9.09 25 n-Octadecane 4.49 0.10 mg/Kg wet 5.00 89.9 40-140 7.93 25 B n-Tetracosane 4.38 0.10 mg/Kg wet 5.00 87.5 40-140 8.87 25 n-Tetradecane 4.00 0.10 mg/Kg wet 5.00 79.9 40-140 9.28 25 n-Triacontane 4.28 0.10 mg/Kg wet 5.00 85.6 40-140 9.39 25 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 4.42 mg/Kg wet 5.20 84.9 40-140 Surrogate: o-Terphenyl (OTP) 4.59 mg/Kg wet 5.00 91.7 40-140 Surrogate:2-Bromonaphthalene 4.52 mg/Kg wet 5.00 90.4 40-140 Surrogate:2-Fluorobiphenyl 5.02 mg/Kg wet 5.00 100 40-140 Matrix Spike (B215618-MS1) Source: 18J1112-01 Prepared: 10/24/18 Analyzed: 10/29/18 C9-C18 Aliphatics 101 13 mg/Kg dry 40.4 74.3 65.2 40-140 C19-C36 Aliphatics 67.8 13 mg/Kg dry 53.9 24.8 79.7 40-140 Acenaphthene 3.18 0.13 mg/Kg dry 6.74 0.241 73.4 40-140 Acenaphthylene 4.45 0.13 mg/Kg dry 6.74 ND 66.1 40-140 Anthracene 5.40 0.13 mg/Kg dry 6.74 ND 80.1 40-140 Benzo(a)anthracene 3.25 0.13 mg/Kg dry 6.74 ND 77.9 40-140 Benzo(a)pyrene 5.18 0.13 mg/Kg dry 6.74 ND 76.9 40-140 Benzo(b)fluoranthene 5.36 0.13 mg/Kg dry 6.74 ND 79.6 40-140 Benzo(g,h,i)perylene 3.28 0.13 mg/Kg dry 6.74 ND 78.4 40-140 Benzo(k)fluoranthene 5.25 0.13 mg/Kg dry 6.74 ND 78.0 40-140 Chrysene 5.30 0.13 mg/Kg dry 6.74 ND 78.7 40-140 Dibenz(a,h)anthracene 3.21 0.13 mg/Kg dry 6.74 ND 77.3 40-140 Fluoranthene 5.56 0.13 mg/Kg dry 6.74 ND 82.5 40-140 Fluorene 5.37 0.13 mg/Kg dry 6.74 0.259 75.9 40-140 Indeno(1,2,3-cd)pyrene 4.99 0.13 mg/Kg dry 6.74 ND 74.1 40-140 2-Methylnaphthalene 4.80 0.13 mg/Kg dry 6.74 0.492 64.0 40-140 Naphthalene 4.50 0.13 mg/Kg dry 6.74 0.330 61.9 40-140 Phenanthrene 3.74 0.13 mg/Kg dry 6.74 0.285 81.0 40-140 Pyrene 5.62 0.13 mg/Kg dry 6.74 ND 83.4 40-140 n-Nonane 2.01 0.13 mg/Kg dry 6.74 ND 29.9 * 30-140 MS-22 Surrogate: Chlorooctadecane (COD) 5.04 mg/Kg dry 7.01 71.9 40-140 Surrogate: o-Terphenyl (OTP) 5.41 mg/Kg dry 6.74 80.3 40-140 Surrogate: 2-Bromonaphthalene 6.12 mg/Kg dry 6.74 90.8 40-140 Surrogate: 2-Fluorobiphenyl 6.92 mg/Kg dry 6.74 103 40-140 Page 62 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215618 - SW-846 3546 Matrix Spike Dup (B215618-MSD1) Source: 18J1112-01 Prepared: 10/24/18 Analyzed: 10/29/18 C9-C18 Aliphatics 111 14 mg/Kg dry 40.8 74.3 90.1 40-140 9.83 50 C19-C36 Aliphatics 71.0 14 mg/Kg dry 54.4 24.8 84.8 40-140 4.59 50 Acenaphthene 5.04 0.14 mg/Kg dry 6.80 0.241 70.5 40-140 2.88 50 Acenaphthylene 4.31 0.14 mg/Kg dry 6.80 ND 63.4 40-140 3.21 50 Anthracene 5.25 0.14 mg/Kg dry 6.80 ND 77.1 40-140 2.82 50 Benzo(a)anthracene 5.14 0.14 mg/Kg dry 6.80 ND 75.5 40-140 2.14 50 Benzo(a)pyrene 4.07 0.14 mg/Kg dry 6.80 ND 74.5 40-140 2.12 50 Benzo(k)fluoranthene 5.26 0.14 mg/Kg dry 6.80 ND 77.3 40-140 1.96 50 Benzo(g,h,i)perylene 5.17 0.14 mg/Kg dry 6.80 ND 76.0 40-140 2.17 50 Benzo(k)fluoranthene 4.07 0.14 mg/Kg dry 6.80 ND 74.6 40-140 3.48 50 Chrysene 5.17 0.14 mg/Kg dry 6.80 ND 76.0 40-140 2.54 50 Dibenz(a,h)anthracene 5.09 0.14 mg/Kg dry 6.80 ND 74.8 40-140 2.27 50 Fluoranthene 5.43 0.14 mg/Kg dry 6.80 ND 79.9 40-140 2.31 50 Fluorene 5.21 0.14 mg/Kg dry 6.80 0.259 72.7 40-140 3.11 50 Indeno(1,2,3-cd)pyrene 4.88 0.14 mg/Kg dry 6.80 ND 71.7 40-140 2.21 50 2-Methylnaphthalene 4.80 0.14 mg/Kg dry 6.80 0.492 63.2 40-140 0.172 50 Naphthalene 4.46 0.14 mg/Kg dry 6.80 0.330 60.7 40-140 0.862 50 Phenanthrene 5.55 0.14 mg/Kg dry 6.80 0.285 77.4 40-140 3.45 50 Pyrene 5.51 0.14 mg/Kg dry 6.80 ND 80.9 40-140 2.07 50 n-Nonane 2.09 0.14 mg/Kg dry 6.80 ND 30.8 30-140 3.87 50 Surrogate: Chlorooctadecane (COD) 5.17 mg/Kg dry 7.08 73.1 40-140 Surrogate: o-Terphenyl (OTP) 5.21 mg/Kg dry 6.80 76.6 40-140 Surrogate: 2-13romonaphthalene 6.17 mg/Kg dry 6.80 90.7 40-140 Surrogate:2-Fluorobiphenyl 6.89 mg/Kg dry 6.80 101 40-140 Page 63 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215495 - MA VPH Blank (B215495-BLK1) Prepared: 10/23/18 Analyzed: 10/25/18 C5-C8 Aliphatics ND 10 mg/Kg wet C9-C12 Aliphatics ND 10 mg/Kg wet C9-C 10 Aromatics ND 10 mg/Kg wet Benzene ND 0.050 mg/Kg wet Butylcyclohexane ND 0.050 mg/Kg wet Decane ND 0.050 mg/Kg wet Ethylbenzene ND 0.050 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.050 mg/Kg wet 2-Methylpentane ND 0.050 mg/Kg wet Naphthalene ND 0.50 mg/Kg wet Nonane ND 0.050 mg/Kg wet Pentane ND 0.050 mg/Kg wet Toluene ND 0.050 mg/Kg wet 1,2,4-Trimethylbenzene ND 0.050 mg/Kg wet 2,2,4-Trimethylpentane ND 0.050 mg/Kg wet m+p Xylene ND 0.10 mg/Kg wet o-Xylene ND 0.050 mg/Kg wet Surrogate:2,5-Dibromotoluene (FID) 35.8 µg/L 40.0 89.6 70-130 Surrogate:2,5-Dibromotoluene (PID) 33.9 µg/L 40.0 84.7 70-130 LCS (B215495-BS1) Prepared: 10/23/18 Analyzed: 10/25/18 C9-C 10 Aromatics 0.144 0.20 mg/Kg wet 70-130 Benzene 0.0964 0.0010 mg/Kg wet 0.100 96.4 70-130 Butylcyclohexane 0.0856 0.0010 mg/Kg wet 0.100 85.6 70-130 Decane 0.0867 0.0010 mg/Kg wet 0.100 86.7 70-130 Ethylbenzene 0.101 0.0010 mg/Kg wet 0.100 101 70-130 Methyl tert-Butyl Ether (MTBE) 0.0956 0.0010 mg/Kg wet 0.100 95.6 70-130 2-Methylpentane 0.101 0.0010 mg/Kgwet 0.100 101 70-130 Naphthalene 0.0916 0.010 mg/Kg wet 0.100 91.6 70-130 Nonane 0.0829 0.0010 mg/Kg wet 0.100 82.9 30-130 Pentane 0.0871 0.0010 mg/Kg wet 0.100 87.1 70-130 Toluene 0.0987 0.0010 mg/Kg wet 0.100 98.7 70-130 1,2,4-Trimethylbenzene 0.105 0.0010 mg/Kg wet 0.100 105 70-130 2,2,4-Trimethylpentane 0.101 0.0010 mg/Kg wet 0.100 101 70-130 m+p Xylene 0.206 0.0020 mg/Kg wet 0.200 103 70-130 o-Xylene 0.101 0.0010 mg/Kg wet 0.100 101 70-130 Surrogate: 2,5-Dibromotoluene (FID) 33.8 µg/L 40.0 84.6 70-130 Surrogate: 2,5-Dibromotoluene (PID) 30.1 µg/L 40.0 75.1 70-130 LCS Dup (B215495-BSD1) Prepared: 10/23/18 Analyzed: 10/25/18 C9-C 10 Aromatics 0.147 0.20 mg/Kg wet 70-130 1.89 Benzene 0.0977 0.0010 mg/Kg wet 0.100 97.7 70-130 1.35 Butylcyclohexane 0.0868 0.0010 mg/Kg wet 0.100 86.8 70-130 1.39 Decane 0.0883 0.0010 mg/Kg wet 0.100 88.3 70-130 1.83 Ethylbenzene 0.103 0.0010 mg/Kg wet 0.100 103 70-130 1.44 Methyl tert-Butyl Ether (MTBE) 0.0963 0.0010 mg/Kg wet 0.100 96.3 70-130 0.761 2-Methylpentane 0.102 0.0010 mg/Kg wet 0.100 102 70-130 1.06 Naphthalene 0.0968 0.010 mg/Kg wet 0.100 96.8 70-130 5.57 Nonane 0.0839 0.0010 mg/Kg wet 0.100 83.9 30-130 1.26 Pentane 0.0915 0.0010 mg/Kg wet 0.100 91.5 70-130 4.88 Toluene 0.100 0.0010 mg/Kg wet 0.100 100 70-130 1.49 1,2,4-Trimethylbenzene 0.106 0.0010 mg/Kg wet 0.100 106 70-130 1.45 25 25 25 25 25 25 25 25 25 25 25 25 Page 64 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215495 - MA VPH LCS Dup (B215495-BSD1) Prepared: 10/23/18 Analyzed: 10/25/18 2,2,4-Trimethylpentane 0.103 0.0010 mg/Kg wet 0.100 103 70-130 2.10 25 m+p Xylene 0.209 0.0020 mg/Kg wet 0.200 105 70-130 1.43 25 o-Xylene 0.103 0.0010 mg/Kg wet 0.loo 103 70-130 1.25 25 Surrogate: 2,5-Dibromotoluene (FID) 35.1 µg/L 40.0 87.8 70-130 Surrogate:2,5-Dibromotoluene (PID) 33.6 µg/L 40.0 84.0 70-130 Batch B215561 - MA VPH Blank (11215561-BLKI) Prepared & Analyzed: 10/24/18 C5-C8 Aliphatics ND 10 mg/Kg wet C9-C 12 Aliphatics ND 10 mg/Kg wet C9-C10 Aromatics ND 10 mg/Kg wet Benzene ND 0.050 mg/Kg wet Butylcyclohexane ND 0.050 mg/Kg wet Decane ND 0.050 mg/Kg wet Ethylbenzene ND 0.050 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.050 mg/Kg wet 2-Methylpentane ND 0.050 mg/Kg wet Naphthalene ND 0.50 mg/Kg wet Nonane ND 0.050 mg/Kg wet Pentane ND 0.050 mg/Kg wet Toluene ND 0.050 mg/Kg wet 1,2,4-Trimethylbenzene ND 0.050 mg/Kg wet 2,2,4-Trimethylpentane ND 0.050 mg/Kg wet m+p Xylene ND 0.10 mg/Kg wet o-Xylene ND 0.050 mg/Kg wet Surrogate: 2,5-Dibromotoluene (FID) 44.3 µg/L 40.0 111 70-130 Surrogate:2,5-Dibromotoluene (PID) 40.5 µg/L 40.0 101 70-130 LCS (B215561-BS1) Prepared & Analyzed: 10/24/18 C9-C10Aromatics 0.0798 0.20 mg/Kg wet 70-130 Benzene 0.0522 0.0010 mg/Kg wet 0.0500 104 70-130 Butylcyclohexane 0.0593 0.0010 mg/Kg wet 0.0500 119 70-130 Decane 0.0473 0.0010 mg/Kg wet 0.0500 94.7 70-130 Ethylbenzene 0.0547 0.0010 mg/Kg wet 0.0500 109 70-130 Methyl tert-Butyl Ether (MTBE) 0.0511 0.0010 mg/Kg wet 0.0500 102 70-130 2-Methylpentane 0.0533 0.0010 mg/Kg wet 0.0500 107 70-130 Naphthalene 0.0570 0.010 mg/Kgwet 0.0500 114 70-130 Nonane 0.0578 0.0010 mg/Kg wet 0.0500 116 30-130 Pentane 0.0462 0.0010 mg/Kg wet 0.0500 92.5 70-130 Toluene 0.0532 0.0010 mg/Kg wet 0.0500 106 70-130 1,2,4-Trimethylbenzene 0.0576 0.0010 mg/Kg wet 0.0500 115 70-130 2,2,4-Trimethylpentane 0.0532 0.0010 mg/Kg wet 0.0500 106 70-130 m+p Xylene 0.112 0.0020 mg/Kg wet 0.100 112 70-130 o-Xylene 0.0548 0.0010 mg/Kg wet 0.0500 110 70-130 Surrogate:2,5-Dibromotoluene (FID) 45.4 µg/L 40.0 114 70-130 Surrogate:2,5-Dibromotoluene (PID) 40.6 µg/L 40.0 102 70-130 Page 65 of 78 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B215561 - MA VPH LCS Dup (B215561-BSD1) Prepared & Analyzed: 10/24/18 C9-C 10 Aromatics 0.0758 0.20 mg/Kg wet 70-130 5.10 25 Benzene 0.0500 0.0010 mg/Kg wet 0.0500 99.9 70-130 4.34 25 Butylcyclohexane 0.0570 0.0010 mg/Kg wet 0.0500 114 70-130 3.99 25 Decane 0.0446 0.0010 mg/Kg wet 0.0500 89.2 70-130 5.96 25 Ethylbenzene 0.0524 0.0010 mg/Kg wet 0.0500 105 70-130 4.31 25 Methyl tert-Butyl Ether (MTBE) 0.0499 0.0010 mg/Kg wet 0.0500 99.9 70-130 2.30 25 2-Methylpentane 0.0505 0.0010 mg/Kg wet 0.0500 101 70-130 5.40 25 Naphthalene 0.0567 0.010 mg/Kg wet 0.0500 113 70-130 0.586 25 Nonane 0.0554 0.0010 mg/Kg wet 0.0500 ill 30-130 4.16 25 Pentane 0.0439 0.0010 mg/Kg wet 0.0500 87.9 70-130 5.10 25 Toluene 0.0510 0.0010 mg/Kg wet 0.0500 102 70-130 4.22 25 1,2,4-Trimethylbenzene 0.0550 0.0010 mg/Kg wet 0.0500 110 70-130 4.60 25 2,2,4-Trimethylpentane 0.0512 0.0010 mg/Kg wet 0.0500 102 70-130 3.81 25 m+p Xylene 0.107 0.0020 mg/Kg wet 0.100 107 70-130 4.74 25 o-Xylene 0.0526 0.0010 mg/Kg wet 0.0500 105 70-130 4.19 25 Surrogate:2,5-Dibromotoluene (FID) 45.5 µg/L 40.0 114 70-130 Surrogate:2,5-Dibromotoluene (PID) 40.5 µg/L 40.0 101 70-130 Page 66 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. B Analyte is found in the associated laboratory blank as well as in the sample. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is within method specified criteria. 0-01 Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered with methanol, but with less than the method -specified amount. R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. RL-05 Elevated reporting limit due to high concentration of target compounds. MA CAM reporting limit not met. RL-11 Elevated reporting limit due to high concentration of target compounds. V-04 Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method specified criteria. Reported result is estimated. V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound. V-16 Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported result. V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99. Reported result is estimated. V-20 Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Page 67 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications MADEP-EPH-04-1.1 in Soil C9-C18 Aliphatics CT,NC,ME,NH-P C19-06 Aliphatics CT,NC,ME,NH-P Unadjusted Cl1-C22 Aromatics CT,NC,ME,NH-P C11-C22 Aromatics CT,NC,ME,NH-P Acenaphthene CT,NC,ME,NH-P Acenaphthylene CT,NC,ME,NH-P Anthracene CT,NC,ME,NH-P Benzo(a)anthracene CT,NC,ME,NH-P Benzo(a)pyrene CT,NC,ME,NH-P Benzo(b)fluoranthene CT,NC,ME,NH-P Benzo(g,h,i)perylene CT,NC,ME,NH-P Benzo(k)fluoranthene CT,NC,ME,NH-P Chrysene CT,NC,ME,NH-P Dibenz(a,h)anthracene CT,NC,ME,NH-P Fluoranthene CT,NC,ME,NH-P Fluorene CT,NC,ME Indeno(1,2,3-cd)pyrene CT,NC,ME NH-P 2-Methylnaphthalene CT,NC,ME Naphthalene CT,NC,ME,NH-P Phenanthrene CT,NC,ME,NH-P Pyrene CT,NC,ME,NH-P MADEP-VPH-Feb 1018 Rev 2.1 in Soil C5-C8 Aliphatics CT,NC,ME,NH-P C9-C12 Aliphatics CT,NC,ME,NH-P C9-C10 Aromatics CT,NC,ME,NH-P Benzene CT,NC,ME,NH-P Ethylbenzene CT,NC,ME,NH-P Methyl tert-Butyl Ether (MTBE) CT,NC,ME,NH-P Naphthalene CT,NC,ME,NH-P Toluene CT,NC,ME,NH-P m+p Xylene CT,NC,ME,NH-P o-Xylene CT,NC,ME,NH-P SW-846 8260B in Soil Acetone NC Acetone NC Acrylonitrile NC Acrylonitrile NC tert-Amyl Methyl Ether (TAME) NC tert-Amyl Methyl Ether (TAME) NC Benzene NC Benzene NC Bromobenzene NC Bromobenzene NC Bromochloromethane NC Bromochloromethane NC Bromodichloromethane NC Page 68 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8260B in Soil Bromodichloromethane NC Bromoform NC Bromoform NC Bromomethane NC Bromomethane NC 2-Butanone (MEK) NC 2-Butanone (MEK) NC tert-Butyl Alcohol (TBA) NC tert-Butyl Alcohol (TBA) NC n-Butylbenzene NC n-Butylbenzene NC sec-Butylbenzene NC sec-Butylbenzene NC tert-Butylbenzene NC tert-Butylbenzene NC tert-Butyl Ethyl Ether (TBEE) NC tert-Butyl Ethyl Ether (TBEE) NC Carbon Disulfide NC Carbon Disulfide NC Carbon Tetrachloride NC Carbon Tetrachloride NC Chlorobenzene NC Chlorobenzene NC Chlorodibromomethane NC Chlorodibromomethane NC Chloroethane NC Chloroethane NC Chloroform NC Chloroform NC Chloromethane NC Chloromethane NC 2-Chlorotoluene NC 2-Chlorotoluene NC 4-Chlorotoluene NC 4-Chlorotoluene NC 1,2-Dibromo-3-chloropropane (DBCP) NC 1,2-Dibromo-3-chloropropane (DBCP) NC 1,2-Dibromoethane (EDB) NC 1,2-Dibromoethane (EDB) NC Dibromomethane NC Dibromomethane NC 1,2-Dichlorobenzene NC 1,2-Dichlorobenzene NC 1,3-Dichlorobenzene NC 1,3-Dichlorobenzene NC 1,4-Dichlorobenzene NC 1,4-Dichlorobenzene NC Page 69 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8260B in Soil trans-1,4-Dichloro-2-butene NC trans-1,4-Dichloro-2-butene NC Dichlorodifluoromethane (Freon 12) NC Dichlorodifluoromethane (Freon 12) NC 1,1-Dichloroethane NC 1,1-Dichloroethane NC 1,2-Dichloroethane NC 1,2-Dichloroethane NC 1,1-Dichloroethylene NC 1,1-Dichloroethylene NC cis-1,2-Dichloroethylene NC cis-1,2-Dichloroethylene NC trans-1,2-Dichloroethylene NC trans-1,2-Dichloroethylene NC 1,2-Dichloropropane NC 1,2-Dichloropropane NC 1,3-Dichloropropane NC 1,3-Dichloropropane NC 2,2-Dichloropropane NC 2,2-Dichloropropane NC 1,1-Dichloropropene NC 1,1-Dichloropropene NC cis- 1,3 -Dichloropropene NC cis- 1,3 -Dichloropropene NC trans- l,3-Dichloropropene NC trans- l,3-Dichloropropene NC Diethyl Ether NC Diethyl Ether NC Diisopropyl Ether (DIPE) NC Diisopropyl Ether (DIPE) NC 1,4-Dioxane NC 1,4-Dioxane NC Ethylbenzene NC Ethylbenzene NC Hexachlorobutadiene NC Hexachlorobutadiene NC 2-Hexanone (MBK) NC 2-Hexanone (MBK) NC Isopropylbenzene (Cumene) NC Isopropylbenzene (Cumene) NC p-Isopropyltoluene (p-Cymene) NC p-Isopropyltoluene (p-Cymene) NC Methyl tert-Butyl Ether (MTBE) NC Methyl tert-Butyl Ether (MTBE) NC Methylene Chloride NC Methylene Chloride NC 4-Methyl-2-pentanone (MIBK) NC Page 70 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte SW-846 8260B in Soil 4-Methyl-2-pentanone (MIBK) Naphthalene Naphthalene n-Propylbenzene n-Propylbenzene Styrene Styrene 1, 1, 1,2-Tetrachloroethane 1, 1, 1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane 1,1, 2, 2-Tetrachloroethane Tetrachloroethylene Tetrachloroethylene Tetrahydrofuran Tetrahydrofuran Toluene Toluene 1,2,3-Trichlorobenzene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trichlorobenzene 1,3,5-Trichlorobenzene 1, 1, 1 -Trichloroethane 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichloroethylene Trichlorofluoromethane (Freon 11) Trichlorofluoromethane (Freon 11) 1,2,3-Trichloropropane 1,2,3-Trichloropropane 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Chloride Vinyl Chloride m+p Xylene m+p Xylene o-Xylene o-Xylene SW-846 8270D in Soil Certifications NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC Page 71 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Soil Acenaphthene CT,NY,NH,ME,NC,VA Acenaphthylene CT,NY,NH,ME,NC,VA Acetophenone NY,NH,ME,NC,VA Aniline NY,NH,ME,NC,VA Anthracene CT,NY,NH,ME,NC,VA Benzidine CT,NY,NH,ME,NC,VA Benzo(a)anthracene CT,NY,NH,ME,NC,VA Benzo(a)pyrene CT,NY,NH,ME,NC,VA Benzo(b)fluoranthene CT,NY,NH,ME,NC,VA Benzo(g,h,i)perylene CT,NY,NH,ME,NC,VA Benzo(k)fluoranthene CT,NY,NH,ME,NC,VA Benzoic Acid NY,NH,ME,NC,VA Bis(2-chloroethoxy)methane CT,NY,NH,ME,NC,VA Bis(2-chloroethyl)ether CT,NY,NH,ME,NC,VA Bis(2-chloroisopropyl)ether CT,NY,NH,ME,NC,VA Bis(2-Ethylhexyl)phthalate CT,NY,NH,ME,NC,VA 4-Bromophenylphenylether CT,NY,NH,ME,NC,VA Butylbenzylphthalate CT,NY,NH,Nffi,NC,VA Carbazole NC 4-Chloroaniline CT,NY,NH,ME,NC,VA 4-Chloro-3-methylphenol CT,NY,NH,ME,NC,VA 2-Chloronaphthalene CT,NY,NH,NC,VA 2-Chlorophenol CT,NY,NH,ME,NC,VA 4-Chlorophenylphenylether CT,NY NH,ME,NC,VA Chrysene CT,NY,NH,ME,NC,VA Dibenz(a,h)anthracene CT,NY,NH,ME,NC,VA Dibenzofuran CT,NY,NH,ME,NC,VA Di-n-butylphthalate CT,NY,NH,ME,NC,VA 1,2-Dichlorobenzene NY,NH,ME,NC,VA 1,3-Dichlorobenzene NY,NH,ME,NC,VA 1,4-Dichlorobenzene NY,NH,ME,NC,VA 3,3-Dichlorobenzidine CT,NY,NH,ME,NC,VA 2,4-Dichlorophenol CT,NY,NH,ME,NC,VA Diethylphthalate CT,NY,NH,ME,NC,VA 2,4-Dimethylphenol CT,NY,NH,ME,NC,VA Dimethylphthalate CT,NY,NH,ME,NC,VA 4,6-Dinitro-2-methylphenol CT,NY,NH,ME,NC,VA 2,4-Dinitrophenol CT,NY,NH,ME,NC,VA 2,4-Dinitrotoluene CT,NY,NH,ME,NC,VA 2,6-Dinitrotoluene CT,NY,NH,ME,NC,VA Di-n-octylphthalate CT,NY,NH,ME,NC,VA 1,2-Diphenylhydrazine (as Azobenzene) NY,NH,ME,NC,VA Fluoranthene CT,NY,NH,ME,NC,VA Fluorene NY,NH,ME,NC,VA Hexachlorobenzene CT,NY,NH,ME,NC,VA Hexachlorobutadiene CT,NY,NH,ME,NC,VA Hexachlorocyclopentadiene CT,NY,NH,ME,NC,VA Page 72 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Soil Hexachloroethane CT,NY,NH,ME,NC,VA Indeno(1,2,3-cd)pyrene CT,NY,NH,ME,NC,VA Isophorone CT,NY,NH,ME,NC,VA 1-Methylnaphthalene NC 2-Methylnaphthalene CT,NY,NH,ME,NC,VA 2-Methylphenol CT,NY,NH,ME,NC,VA 3/4-Methylphenol CT,NY,NH,ME,NC,VA Naphthalene CT,NY,NH,ME,NC,VA 2-Nitroaniline CT,NY,NH,ME,NC,VA 3-Nitroaniline CT,NY,NH,ME,NC,VA 4-Nitroaniline CT,NY,NH,ME,NC,VA Nitrobenzene CT,NY,NH,ME,NC,VA 2-Nitrophenol CT,NY,NH,ME,NC,VA 4-Nitrophenol CT,NY,NH,ME,NC,VA N-Nitrosodimethylamine CT,NY,NH,ME,NC,VA N-Nitrosodiphenylamine CT,NY,NH,ME,NC,VA N-Nitrosodi-n-propylamine CT,NY,NH,ME,NC,VA Pentachloronitrobenzene NY,NC Pentachlorophenol CT,NY,NH,ME,NC,VA Phenanthrene CT,NY,NH,ME,NC,VA Phenol CT,NY,NH,ME,NC,VA Pyrene CT,NY,NH,ME,NC,VA Pyridine CT,NY,NH,ME,NC,VA 1,2,4,5-Tetrachlorobenzene NY,NC 1,2,4-Trichlorobenzene CT,NY,NH,ME,NC,VA 2,4,5-Trichlorophenol CT,NY,NH,ME,NC,VA 2,4,6-Trichlorophenol CT,NY,NH,ME,NC,VA 2-Fluorophenol NC SW-846 8270D in Water Acenaphthene CT,NY,NC,ME,NH,VA Acenaphthylene CT,NY,NC,ME,NH,VA Acetophenone NY,NC Aniline CT,NY,NC,ME,VA Anthracene CT,NY,NC,ME,NH,VA Benzidine CT,NY,NC,ME,NH,VA Benzo(a)anthracene CT,NY,NC,ME,NH,VA Benzo(a)pyrene CT,NY,NC,ME,NH,VA Benzo(b)fluoranthene CT,NY,NC,ME,NH,VA Benzo(g,h,i)perylene CT,NY,NC,ME,NH,VA Benzo(k)fluoranthene CT,NY,NC,ME,NH,VA Benzoic Acid NY,NC,ME,NH,VA Bis(2-chloroethoxy)methane CT,NY,NC,ME,NH,VA Bis(2-chloroethyl)ether CT,NY,NC,ME,NH,VA Bis(2-chloroisopropyl)ether CT,NY,NC,ME,NH,VA Bis(2-Ethylhexyl)phthalate CT,NY,NC,ME,NH,VA 4-Bromophenylphenylether CT,NY,NC,ME,NH,VA Page 73 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Water Butylbenzylphthalate CT,NY,NC,ME,NH,VA Carbazole NC 4-Chloroaniline CT,NY,NC,ME,NH,VA 4-Chloro-3-methylphenol CT,NY,NC,ME,NH,VA 2-Chloronaphthalene CT,NY,NC,ME,NH,VA 2-Chlorophenol CT,NY,NC,ME,NH,VA 4-Chlorophenylphenylether CT,NY,NC,ME,NH,VA Chrysene CT,NY,NC,ME,NH,VA Dibenz(a,h)anthracene CT,NY,NC,ME,NH,VA Dibenzofuran CT,NY,NC,ME,NH,VA Di-n-butylphthalate CT,NY,NC,ME,NH,VA 1,2-Dichlorobenzene CT,NY,NC,ME,NH,VA 1,3-Dichlorobenzene CT,NY,NC,ME,NH,VA 1,4-Dichlorobenzene CT,NY,NC,ME,NH,VA 3,3-Dichlorobenzidine CT,NY,NC,ME,NH,VA 2,4-Dichlorophenol CT,NY,NC,ME,NH,VA Diethylphthalate CT,NY,NC,ME,NH,VA 2,4-Dimethylphenol CT,NY,NC,ME,NH,VA Dimethylphthalate CT,NY,NC,ME,NH,VA 4,6-Dinitro-2-methylphenol CT,NY,NC,ME,NH,VA 2,4-Dinitrophenol CT,NY,NC,ME,NH,VA 2,4-Dinitrotoluene CT,NY,NC,ME,NH,VA 2,6-Dinitrotoluene CT,NY,NC,ME,NH,VA Di-n-octylphthalate CT,NY,NC,ME,NH,VA 1,2-Diphenylhydrazine(as Azobenzene) NY,NC Fluoranthene CT,NY,NC,ME,NH,VA Fluorene NY,NC,ME,NH,VA Hexachlorobenzene CT,NY,NC,ME,NH,VA Hexachlorobutadiene CT,NY,NC,ME,NH,VA Hexachlorocyclopentadiene CT,NY,NC,ME,NH,VA Hexachloroethane CT,NY,NC,ME,NH,VA Indeno(1,2,3-cd)pyrene CT,NY,NC,ME,NH,VA Isophorone CT,NY,NC,ME,NH,VA I -Methylnaphthalene NC 2-Methylnaphthalene CT,NY,NC,ME,NH,VA 2-Methylphenol CT,NY,NC,NH,VA 3/4-Methylphenol CT,NY,NC,NH,VA Naphthalene CT,NY,NC,ME,NH,VA 2-Nitroaniline CT,NY,NC,ME,NH,VA 3-Nitroaniline CT,NY,NC,ME,NH,VA 4-Nitroaniline CT,NY,NC,ME,NH,VA Nitrobenzene CT,NY,NC,ME,NH,VA 2-Nitrophenol CT,NY,NC,ME,NH,VA 4-Nitrophenol CT,NY,NC,ME,NH,VA N-Nitrosodimethylamine CT,NY,NC,ME,NH,VA N-Nitrosodiphenylamine CT,NY,NC,ME,NH,VA N-Nitrosodi-n-propylamine CT,NY,NC,ME,NH,VA Page 74 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Water Pentachloronitrobenzene NC Pentachlorophenol CT,NY,NC,ME,NH,VA Phenanthrene CT,NY,NC,ME,NH,VA Phenol CT,NY,NC,ME,NH,VA Pyrene CT,NY,NC,ME,NH,VA Pyridine CT,NY,NC,ME,NH,VA 1,2,4,5-Tetrachlorobenzene NY,NC 1,2,4-Trichlorobenzene CT,NY,NC,ME,NH,VA 2,4,5-Trichlorophenol CT,NY,NC,ME,NH,VA 2,4,6-Trichlorophenol CT,NY,NC,ME,NH,VA 2-Fluorophenol NC The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2018 NC North Carolina Div. of Water Quality 652 12/31/2018 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2018 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 75 of 78 10/23/2018 Track your package or shipment with FedEx Tracking s°':" 773537302485 �' Delivered Tuesday 10/23/2018 at 9:14 am DELIVERED Signed for by. B BECCA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM TO Charlotte, NC US EAST LONGMEADOW, MA US Multiple -piece Shipment 3 Piece Shipment Table of Contents `iz TRACKING NUMBER SHIPPER CITY, STATE SHIP DATE STATUS DELIVERY DATE DESTINATIONJRECIPIENT CITY, STATE i735373U1375 CHARLOTTE, NC 10/22/2018 10,123/2018 EAST I_ONGtAEAIDOV4 MA (n�aster } 773537302393 CHARLOTTE, NC 10/22/2018 10/23/2018 EAST LONG MEADOW, MA 773S37302485 CHARLOTTE, NC 10/22/2C18 10./23/2018 EAST LONGMEADOW, MA Shipment Facts TRACKING NUMBER SERVICE MASTER TRACKING NUMBER 773537302485 FedEx Standard Overniet 773537301375 WEIGHT DIMENSIONS DELIVERED TO 10 Ibs 1f4.54 kgs 24x14x14 In. Shipping/Receiving TOTAL PIECES TOTAL SHIPMENT WEIGHT TERMS 10 lbs / 4.54 kgs l hird Parw PACKAGING SPECIAL HANDLING SECTION STANDARD TRANSIT Your Packaging Deliver Weekday, Additional HandJng 0 Surcharge 10/23/2018 by 3 00 prn SHIP DATE ACTUAL DELIVERY 0 TLJe 10/23/2018 9:14 any Man 10/22/2018 https:llwww.fedex.comlappslfedextrackl?action=track&tracknumbers=773537302485&locale=en_US&cntry_code=us I Page 77 of 78 Table of Contents I Have Not Confirmed Sample ContainerC C3) n te S t UIP Numbers With Lab Staff Before Relinquishing Over Samples Doc�:277 ,Rev 5'2017 Login Sample Receipt Checklist: - (Rejection Criteria Listing - Using Acceptance Policy) Any False Statement will be brought to the attention of the Client - State True or False Client WOA Received By Zry Date 2 Time 91 q On Ice ,-� --- How were the samples received? Direct from Sampling Ambient Melted Ice Were samples within By Gun # Actual Temp - Temperature? 2-WC By Blank # Actual Temp - Was Custody Sea[ Intact? ( Were Samples Tampered with? l� Was COC Relinquished ? fi Does Chain Agree With Samples? Are there broken/leaking/loose caps on any samples? ` - Is COC in ink/ Legible? i _ Were samples received within holding time? _ ti - Did COC include all Client Analysis T` Sampler Name --- pertinent Information? Project ID's t — Collection Dates/Times Are Sample labels filled out and legible? t Are there Lab to Filters?_ Who was notified? Are there Rushes? �_ Who was notified? Are there Short Holds? Who was notified? Is there enough Volume? Is there Headspace where applicable? MS/MSD? Proper Media/Containers Used? Is splitting sampl required? Were trip blanks received? On COC? Do all samples have the proper pH? Acid Base In Cooler No Cooler No Ice 78 of 78 In Cooler No Cooler No Ice 78 of 78 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 November 8, 2018 Rob Foster AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 Charlotte, NC 28208 Project Location: 5318 Morris Field Drive Client Job Number: Project Number: 6228-18-0503 Laboratory Work Order Number: 18KO087 Enclosed are results of analyses for samples received by the laboratory on November 1, 2018. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kerry K. McGee Project Manager Page 1 of 39 Table of Contents Table of Contents Sample Summary Case Narrative Sample Results 18K0087-01 Sample Preparation Information QC Data Volatile Organic Compounds by GC/ 4S B216398 Semivolatile Organic Compounds by GUMS B216342 Petroleum Hydrocarbons Analyses - EPH B216348 Petroleum Hydrocarbons Analyses - VPH B216531 Flag/Qualifier Summary Certifications Chain of Custody/Sample Receipt 3 4 7 7 14 15 15 15 20 20 25 25 28 28 30 31 37 Page 2 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce StreetEast Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 AMEC - Charlotte 2801 Yorkmont Rd, Suite 100 REPORT DATE: 11 /8/2018 Charlotte, NC 28208 PURCHASE ORDER NUMBER: ATTN: Rob Foster PROJECT NUMBER: 6228-18-0503 ANALYTICAL SUMMARY WORK ORDER NUMBER: 18KO087 The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report. PROJECT LOCATION: 5318 Morris Field Drive FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB TB-4-18 18KO087-01 Soil MADEP-EPH-04-1.1 MADEP-VPH-Feb 2018 Rev 2.1 SM 254OG SW-846 8260B SW-846 8270D Page 3 of 39 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. For method MA EPH, only hydrocarbon ranges were requested and reported. For method MA VPH, only adjusted hydrocarbon ranges were requested and reported. Page 4 of 39 Table of Contents 40 ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 MADEP-EPH-04-1.1 Qualifications: L-07A Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. Analyte & Samples(s) Qualified: n-Decane B216348-BSD1 n-Nonane B216348-BSD1 R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: n-Decane B216348-BLKI, B216348-BSI n-Nonane B216348-BLKI, B216348-BSI SW-846 8260B Qualifications: L-07A Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. Analyte & Samples(s) Qualified: Acetone B216398-BS1 R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. Analyte & Samples(s) Qualified: 2-Butanone (MEK) 18K0087-01[TB-4-18], B216398-BLKI, B216398-BSI, B216398-BSDI Acetone 18K0087-01 [TB-4-18], B216398-BLKI, B216398-BSI, B216398-BSDI SW-846 8270D Qualifications: L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Hexachlorocyclopentadiene 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSD1 L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. Analyte & Samples(s) Qualified: Pyridine B216342-BSDI Page 5 of 39 ,con-testo ANALYTICAL LABORATORY Table of Contents V-05 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Continuing calibration did not meet method specifications and was biased on the low side for this compound. Analyte & Samples(s) Qualified: 4-Chloroaniline 18K0087-01 [TB-4-18] Aniline 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI Benzidine 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI Chrysene 18K0087-01 [TB-4-18] Hexachlorocyclopentadiene 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSD1 Pyridine 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound. Analyte & Samples(s) Qualified: 2-Nitroaniline 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI 4-Nitrophenol 18K0087-OI[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99. Reported result is estimated. Analyte & Samples(s) Qualified: 2,4-Dinitrophenol 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Analyte & Samples(s) Qualified: 4-Chloroaniline 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI Aniline 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI Benzidine 18K0087-01[TB-4-18], B216342-BLKI, B216342-BSI, B216342-BSDI MADEP-EPH-04-1.1 SPE cartridge contamination with non -petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic range fraction in all samples in the batch. No significant modifications were made to the method. MADEP-VPH-Feb 2018 Rev 2.1 Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III. No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely covered by methanol in the proper containers specified on the chain -of -custody form unless specified in this narrative. The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. Daren J. Damboragian Director of Operations Page 6 of 39 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087 Date Received: 11/1/2018 Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30 Sample ID: 18KO087-01 Samnle Matrix: Soil Analyte Results RL Volatile Organic Compounds by GC/MS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acetone ND 0.11 0.026 mg/Kg dry 1 R-05 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Acrylonitrile ND 0.0066 0.0027 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF tert-Amyl Methyl Ether (TAME) ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Benzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Bromobenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Bromochloromethane ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Bromodichloromethane ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Bromoform ND 0.0022 0.0015 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Bromomethane ND 0.011 0.0046 mg/Kg dry 1 SW-846 8260B 11/5/18 1115118 15:57 MFF 2-Butanone (MEK) ND 0.044 0.019 mg/Kg dry 1 R-05 SW-846 8260B 11/5/18 11/5/18 15:57 MFF tert-Butyl Alcohol (TBA) ND 0.044 0.023 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF n-Butylbenzene 0.0019 0.0022 0.00077 mg/Kg dry 1 J SW-846 8260B 11/5/18 11/5/18 15:57 MFF sec-Butylbenzene 0.0040 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF tert-Butylbenzene ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF tert-Butyl Ethyl Ether (TBEE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Carbon Disulfide ND 0.0066 0.0047 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Carbon Tetrachloride ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Chlorobenzene ND 0.0022 0.00077 mg/Kg dry I SW-846 8260B 11/5/18 11/5/18 15:57 MFF Chlorodibromomethane ND 0.0011 0.00077 mg/Kg dry I SW-846 8260B 11/5/18 11/5/18 15:57 MFF Chloroethane ND 0.022 0.0016 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Chloroform ND 0.0044 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Chloromethane ND 0.011 0.0070 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 2-Chlorotoluene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 4-Chlorotoluene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 1115118 15:57 MFF 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,2-Dibromoethane (EDB) ND 0.0011 0.0011 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Dibromomethane ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,2-Dichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,3-Dichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,4-Dichlorobenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF trans-1,4-Dichloro-2-butene ND 0.0044 0.0023 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Dichlorodifluoromethane (Freon 12) ND 0.022 0.0014 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,1-Dichloroethane ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,2-Dichloroethane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1, 1 -Dichloroethylene ND 0.0044 0.0012 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF cis-1,2-Dichloroethylene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF trans-1,2-Dichloroethylene ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,2-Dichloropropane ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,3-Dichloropropane ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 2,2-Dichloropropane ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1, 1 -Dichloropropene ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF cis-1,3-Dichloropropene ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF trans-1,3-Dichloropropene ND 0.0011 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Diethyl Ether ND 0.022 0.0020 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Page 7 of 39 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087 Date Received: 11/1/2018 Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30 Sample ID: 18KO087-01 Samnle Matrix: Soil Volatile Organic Compounds by GC/MS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Diisopropyl Ether (DIPE) ND 0.0011 0.00066 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,4-Dioxane ND 0.11 0.063 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Ethylbenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Hexachlorobutadiene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 2-Hexanone (MBK) ND 0.022 0.012 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Isopropylbenzene (Cumene) 0.00077 0.0022 0.00077 mg/Kg dry 1 J SW-846 8260B 11/5/18 11/5/18 15:57 MFF p-Isopropyltoluene (p-Cymene) ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 1115118 15:57 MFF Methyl tert-Butyl Ether (MTBE) ND 0.0044 0.00099 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Methylene Chloride ND 0.022 0.0078 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 4-Methyl-2-pentanone (MIBK) ND 0.022 0.0083 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Naphthalene 0.0081 0.0044 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF n-Propylbenzene 0.0012 0.0022 0.00077 mg/Kg dry 1 J SW-846 8260B 11/5/18 11/5/18 15:57 MFF Styrene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1, 1, 1,2-Tetrachloroethane ND 0.0022 0.0020 mg/Kg dry 1 SW-8468260B 11/5/18 11/5/18 15:57 MFF 1,1,2,2-Tetrachloroethane ND 0.0022 0.00099 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Tetrachloroethylene ND 0.0022 0.0014 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Tetrahydrofuran ND 0.011 0.0024 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Toluene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,2,3-Trichlorobenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,2,4-Trichlorobenzene ND 0.0022 0.00088 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,3,5-Trichlorobenzene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1, 1, 1 -Trichloroethane ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 11/5/18 1115118 15:57 MFF 1,1,2-Trichloroethane ND 0.0022 0.0013 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Trichloroethylene ND 0.0022 0.0011 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Trichlorofluoromethane (Freon 11) ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,2,3-Trichloropropane ND 0.0022 0.0012 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,1,2-Trichloro-1,2,2-trifluoroethane ND 0.011 0.00099 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF (Freon 113) 1,2,4-Trimethylbenzene 0.0017 0.0022 0.00088 mg/Kg dry 1 J SW-846 8260B 11/5/18 11/5/18 15:57 MFF 1,3,5-Trimethylbenzene ND 0.0022 0.00066 mg/Kg dry 1 SW-846 8260B 11/5/18 1115118 15:57 MFF Vinyl Chloride ND 0.011 0.0012 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF m+p Xylene ND 0.0044 0.0019 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF o-Xylene ND 0.0022 0.00077 mg/Kg dry 1 SW-846 8260B 11/5/18 11/5/18 15:57 MFF Surrogates % Recovery Recovery Limits Flag/Qaal 1,2-Dichloroethane-d4 102 70-130 11/5/18 15:57 Toluene-d8 95.8 70-130 11/5/18 15:57 4-Bromofluorobenzene 101 70-130 11/5/18 15:57 Page 8 of 39 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087 Date Received: 11/1/2018 Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30 Samnle ID: 18KO087-01 Samnle Matrix: Soil Analyte Results RL Semivolatile Organic Compounds by GUMS DL Units Dilution Flag/Qual Method Date Prepared Date/Time Analyzed Analyst Acenaphthene ND 0.48 0.14 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Acenaphthylene ND 0.48 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Acetophenone ND 0.95 0.19 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Aniline ND 0.95 0.27 mg/Kg dry 1 V-05, V-34 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Anthracene ND 0.48 0.14 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Benzidine ND 1.8 1.2 mg/Kg dry 1 V-05, V-34 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Benzo(a)anthracene ND 0.48 0.13 mg/Kg dry I SW-846 8270D 11/3/18 11/6/18 15:39 BGL Benzo(a)pyrene ND 0.48 0.15 mg/Kg dry I SW-846 8270D 11/3/18 11/6/18 15:39 BGL Benzo(b)fluoranthene ND 0.48 0.13 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Benzo(g,h,i)perylene ND 0.48 0.21 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Benzo(k)fluoranthene ND 0.48 0.15 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Benzoic Acid ND 2.8 0.51 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Bis(2-chloroethoxy)methane ND 0.95 0.18 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Bis(2-chloroethyl)ether ND 0.95 0.19 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Bis(2-chloroisopropyl)ether ND 0.95 0.20 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Bis(2-Ethylhexyl)phthalate ND 0.95 0.37 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 4-Bromophenylphenylether ND 0.95 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Butylbenzylphthalate ND 0.95 0.23 mg/Kg dry I SW-846 8270D 11/3/18 11/6/18 15:39 BGL Carbazole ND 0.48 0.12 mg/Kg dry I SW-846 8270D 11/3/18 11/6/18 15:39 BGL 4-Chloroaniline ND 1.8 0.22 mg/Kg dry 1 V-05, V-34 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 4-Chloro-3-methylphenol ND 1.8 0.20 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2-Chloronaphthalene ND 0.95 0.18 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2-Chlorophenol ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 4-Chlorophenylphenylether ND 0.95 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Chrysene ND 0.48 0.15 mg/Kg dry 1 V-05 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Dibenz(a,h)anthracene ND 0.48 0.29 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Dibenzofman ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Di-n-butylphthalate ND 0.95 0.21 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 1,2-Dichlorobenzene ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 1,3-Dichlorobenzene ND 0.95 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 1,4-Dichlorobenzene ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 3,3-Dichlorobenzidine ND 0.48 0.15 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2,4-Dichlorophenol ND 0.95 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Diethylphthalate ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2,4-Dimethylphenol ND 0.95 0.18 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Dimethylphthalate ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 4,6-Dinitro-2-methylphenol ND 0.95 0.90 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2,4-Dinitrophenol ND 1.8 0.54 mg/Kg dry 1 V-19 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2,4-Dinitrotoluene ND 0.95 0.15 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2,6-Dinitrotoluene ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Di-n-octylphthalate ND 0.95 0.50 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 1,2-Diphenylhydrazine (as Azobenzene) ND 0.95 0.15 mg/Kg dry I SW-846 8270D 11/3/18 11/6/18 15:39 BGL Fluoranthene ND 0.48 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Flumene ND 0.48 0.15 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Page 9 of 39 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087 Date Received: 11/1/2018 Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30 Samnle ID: 18KO087-01 Samnle Matrix: Soil Semivolatile Organic Compounds by GUMS Date Date/Time Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst Hexachlorobenzene ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Hexachlorobutadiene ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Hexachlorocyclopentadiene ND 0.95 0.20 mg/Kg dry 1 L-04, V-05 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Hexachloroethane ND 0.95 0.19 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Indeno(1,2,3-cd)pyrene ND 0.48 0.34 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Isophorone ND 0.95 0.18 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 1-Methylnaphthalene ND 0.48 0.18 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2-Methylnaphthalene 0.18 0.48 0.17 mg/Kg dry 1 J SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2-Methylphenol ND 0.95 0.24 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 3/4-Methylphenol ND 0.95 0.30 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Naphthalene ND 0.48 0.24 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2-Nitroaniline ND 0.95 0.16 mg/Kg dry 1 V-06 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 3-Nitroaniline ND 0.95 0.14 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 4-Nitroaniline ND 0.95 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Nitrobenzene ND 0.95 0.18 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2-Nitrophenol ND 0.95 0.25 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 4-Nitrophenol ND 1.8 0.21 mg/Kg dry 1 V-06 SW-846 8270D 11/3/18 11/6/18 15:39 BGL N-Nitrosodimethylamine ND 0.95 0.60 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL N-Nitrosodiphenylamine ND 0.95 0.20 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL N-Nitrosodi-n-propylamine ND 0.95 0.20 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Pentachloronitrobenzene ND 0.95 0.23 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Pentachlorophenol ND 0.95 0.23 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Phenanthrene ND 0.48 0.25 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Phenol ND 0.95 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Pyrene ND 0.48 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Pyridine ND 0.95 0.15 mg/Kg dry 1 V-05 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 1,2,4,5-Texachlorobenzene ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 1,2,4-Trichlorobenzene ND 0.95 0.17 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2,4,5-Trichlorophenol ND 0.95 0.22 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL 2,4,6-Trichlorophenol ND 0.95 0.16 mg/Kg dry 1 SW-846 8270D 11/3/18 11/6/18 15:39 BGL Surrogates % Recovery Recovery Limits Flag/Qual 2-Fluorophenol 58.0 30-130 11/6/18 15:39 Phenol-d6 62.9 30-130 11/6/18 15:39 Nitrobenzene-d5 62.8 30-130 11/6/18 15:39 2-Fluorobiphenyl 55.8 30-130 11/6/18 15:39 2,4,6-Tribromophenol 74.5 30-130 11/6/18 15:39 p-Terphenyl-dl4 56.3 30-130 11/6/18 15:39 Page 10 of 39 Table of Contents 40 icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087 Date Received: 11/1/2018 Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30 Samnle ID: 18KO087-01 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - EPH Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C9-C18 Aliphatics 130 14 mg/Kg dry 1 MADEP-EPH-04-1.1 11/4/18 11/7/18 1:08 RMW C19-C36 Aliphatics 37 14 mg/Kg dry 1 MADEP-EPH-04-1.1 11/4/18 11/7/18 1:08 RMW C11-C22 Aromatics 78 14 mg/Kg dry 1 MADEP-EPH-04-1.1 11/4/18 11/7/18 1:08 RMW Surrogates % Recovery Recovery Limits Flag/Qual Chlorooctadecane (COD) 59.7 40-140 11/7/18 1:08 o-Terphenyl(OTP) 64.8 40-140 11/7/18 1:08 2-Bromonaphthalene 91.4 40-140 11/7/18 1:08 2-Fluorobiphenyl 107 40-140 11/7/18 1:08 Page 11 of 39 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087 Date Received: 11/1/2018 Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30 Sample ID: 18KO087-01 Samnle Matrix: Soil Petroleum Hydrocarbons Analyses - VPH Soil/Methanol Preservation Ratio: 1.19 Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst C5-C8 Aliphatics ND 16 mg/Kg dry 1 MADEP-VPH-Feb2018 11/6/18 11/7/18 17:07 EEH Rev 2.1 C9-C12 Aliphatics 24 16 mg/Kg dry 1 MADEP-VPH-Feb 2018 11/6/18 11/7/18 17:07 EEH Rev 2.1 C9-C10 Aromatics 31 16 mg/Kg dry 1 MADEP-VPH-Feb 2018 11/6/18 11/7/18 17:07 EEH Rev 2.1 Surrogates % Recovery Recovery Limits Flag/Qual 2,5-Dibromotoluene(FID) 103 70-130 11/7/18 17:07 2,5-Dibromotoluene (PID) 116 70-130 11/7/18 17:07 Page 12 of 39 Table of Contents icon-te w ANALYTICAL LABORATORY 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 Project Location: 5318 Morris Field Drive Sample Description: Work Order: 18KO087 Date Received: 11/1/2018 Field Sample #: TB-4-18 Sampled: 11/1/2018 11:30 Samnle ID: 18KO087-01 Samnle Matrix: Soil Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) Date Date/Time Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst % Solids 70.1 % Wt 1 SM 2540G 11/5/18 11/6/18 10:02 CJT Page 13 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 Sample Extraction Data Prep Method: SW-846 3546-MADEP-EPH-04-1.1 Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18K0087-01 [TB-4-18] B216348 20.0 2.00 11/04/18 Prep Method: MA VPH-MADEP-VPH-Feb 2018 Rev 2.1 Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18K0087-01[TB-4-18] B216531 6.00 6.80 11/06/18 Prep Method: % Solids-SM 2540G Lab Number [Field ID] Batch Date 18K0087-01 [TB-4-18] B216440 11/05/18 Prep Method: SW-846 5035-SW-846 8260B Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18K0087-01 [TB-4-18] B216398 6.51 10.0 11/05/18 Prep Method: SW-846 3546-SW-846 8270D Lab Number [Field ID] Batch Initial [g] Final [mL] Date 18K0087-01 [TB-4-18] B216342 15.3 1.00 11/03/18 Page 14 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216398 - SW-846 5035 Blank (B216398-BLK1) Prepared & Analyzed: 11/05/18 Acetone ND 0.10 mg/Kg wet R-05 Acrylonitrile ND 0.0060 mg/Kg wet tert-Amyl Methyl Ether (TAME) ND 0.0010 mg/Kg wet Benzene ND 0.0020 mg/Kg wet Bromobenzene ND 0.0020 mg/Kg wet Bromochloromethane ND 0.0020 mg/Kg wet Bromodichloromethane ND 0.0020 mg/Kg wet Bromoform ND 0.0020 mg/Kg wet Bromomethane ND 0.010 mg/Kg wet 2-Butanone (MEK) ND 0.040 mg/Kg wet R-05 tert-Butyl Alcohol (TBA) ND 0.040 mg/Kg wet n-Butylbenzene ND 0.0020 mg/Kg wet sec-Butylbenzene ND 0.0020 mg/Kg wet tert-Butylbenzene ND 0.0020 mg/Kg wet tert-Butyl Ethyl Ether (TBEE) ND 0.0010 mg/Kg wet Carbon Disulfide ND 0.0060 mg/Kg wet Carbon Tetrachloride ND 0.0020 mg/Kg wet Chlorobenzene ND 0.0020 mg/Kg wet Chlorodibromomethane ND 0.0010 mg/Kg wet Chloroethane ND 0.020 mg/Kg wet Chloroform ND 0.0040 mg/Kg wet Chloromethane ND 0.010 mg/Kg wet 2-Chlorotoluene ND 0.0020 mg/Kg wet 4-Chlorotoluene ND 0.0020 mg/Kg wet 1,2-Dibromo-3-chloropropane (DBCP) ND 0.0020 mg/Kg wet 1,2-Dibromoethane (EDB) ND 0.0010 mg/Kg wet Dibromomethane ND 0.0020 mg/Kg wet 1,2-Dichlorobenzene ND 0.0020 mg/Kg wet 1,3-Dichlorobenzene ND 0.0020 mg/Kg wet 1,4-Dichlorobenzene ND 0.0020 mg/Kg wet trans-1,4-Dichloro-2-butene ND 0.0040 mg/Kg wet Dichlorodifluoromethane (Freon 12) ND 0.020 mg/Kg wet 1,1-Dichloroethane ND 0.0020 mg/Kg wet 1,2-Dichloroethane ND 0.0020 mg/Kg wet 1,1-Dichloroethylene ND 0.0040 mg/Kg wet cis-1,2-Dichloroethylene ND 0.0020 mg/Kg wet trans-1,2-Dichloroethylene ND 0.0020 mg/Kg wet 1,2-Dichloropropane ND 0.0020 mg/Kg wet 1,3-Dichloropropane ND 0.0010 mg/Kg wet 2,2-Dichloropropane ND 0.0020 mg/Kg wet 1,1-Dichloropropene ND 0.0020 mg/Kg wet cis-1,3-Dichloropropene ND 0.0010 mg/Kg wet trans-1,3-Dichloropropene ND 0.0010 mg/Kg wet Diethyl Ether ND 0.020 mg/Kg wet Diisopropyl Ether (RIPE) ND 0.0010 mg/Kg wet 1,4-Dioxane ND 0.10 mg/Kg wet Ethylbenzene ND 0.0020 mg/Kg wet Hexachlorobutadiene ND 0.0020 mg/Kg wet 2-Hexanone (MBK) ND 0.020 mg/Kg wet Isopropylbenzene (Cumene) ND 0.0020 mg/Kg wet p-Isopropyltoluene (p-Cymene) ND 0.0020 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.0040 mg/Kg wet Page 15 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD malyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216398 - SW-846 5035 Blank (B216398-BLK1) Prepared & Analyzed: 11/05/18 Methylene Chloride ND 0.020 mg/Kg wet 4-Methyl-2-pentanone (MIBK) ND 0.020 mg/Kg wet Naphthalene ND 0.0040 mg/Kg wet n-Propylbenzene ND 0.0020 mg/Kg wet Styrene ND 0.0020 mg/Kg wet 1, 1, 1,2-Tetrachloroethane ND 0.0020 mg/Kg wet 1,1,2,2-Tetrachloroethane ND 0.0010 mg/Kg wet Tetrachloroethylene ND 0.0020 mg/Kg wet Tetrahydrofuran ND 0.010 mg/Kg wet Toluene ND 0.0020 mg/Kg wet 1,2,3-Trichlorobenzene ND 0.0020 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.0020 mg/Kg wet 1,3,5-Trichlorobenzene ND 0.0020 mg/Kg wet 1, 1, 1 -Trichloroethane ND 0.0020 mg/Kg wet 1,1,2-Trichloroethane ND 0.0020 mg/Kg wet Trichloroethylene ND 0.0020 mg/Kg wet Trichlorofluoromethane (Freon 11) ND 0.010 mg/Kg wet 1,2,3-Trichloropropane ND 0.0020 mg/Kg wet 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.010 mg/Kg wet 113) 1,2,4-Trimethylbenzene ND 0.0020 mg/Kg wet 1,3,5-Trimethylbenzene ND 0.0020 mg/Kg wet Vinyl Chloride ND 0.010 mg/Kg wet m+p Xylene ND 0.0040 mg/Kg wet o-Xylene ND 0.0020 mg/Kg wet Surrogate: 1,2-Dichloroethane-d4 0.0522 mg/Kg wet 0.0500 104 70-130 Surrogate: Toluene-d8 0.0478 mg/Kg wet 0.0500 95.5 70-130 Surrogate:4-Bromofluorobenzene 0.0510 mg/Kg wet 0.0500 102 70-130 LCS (B216398-BS1) Prepared & Analyzed: 11/05/18 Acetone 0.383 0.10 mg/Kg wet 0.200 191 * 70-160 R-05, L-07A t Acrylonitrile 0.0194 0.0060 mg/Kg wet 0.0200 97.2 70-130 tert-Amyl Methyl Ether (TAME) 0.0205 0.0010 mg/Kg wet 0.0200 102 70-130 Benzene 0.0192 0.0020 mg/Kg wet 0.0200 95.8 70-130 Bromobenzene 0.0197 0.0020 mg/Kg wet 0.0200 98.5 70-130 Bromochloromethane 0.0221 0.0020 mg/Kg wet 0.0200 ill 70-130 Bromodichloromethane 0.0197 0.0020 mg/Kg wet 0.0200 98.7 70-130 Bromoform 0.0216 0.0020 mg/Kg wet 0.0200 108 70-130 Bromomethane 0.0120 0.010 mg/Kg wet 0.0200 60.1 40-130 t 2-Butanone (MEK) 0.308 0.040 mg/Kg wet 0.200 154 70-160 R-05 t tert-Butyl Alcohol (TBA) 0.228 0.040 mg/Kg wet 0.200 114 40-130 t n-Butylbenzene 0.0197 0.0020 mg/Kg wet 0,0200 98.5 70-130 sec-Butylbenzene 0.0196 0.0020 mg/Kg wet 0.0200 98.0 70-130 tert-Butylbenzene 0.0186 0.0020 mg/Kg wet 0.0200 92.9 70-160 t tert-Butyl Ethyl Ether (TBEE) 0.0202 0.0010 mg/Kg wet 0,0200 101 70-130 Carbon Disulfide 0.0197 0.0060 mg/Kg wet 0.0200 98.3 70-130 Carbon Tetrachloride 0.0211 0.0020 mg/Kg wet 0.0200 105 70-130 Chlorobenzene 0.0203 0.0020 mg/Kg wet 0,0200 102 70-130 Chlorodibromomethane 0.0223 0.0010 mg/Kg wet 0.0200 Ill 70-130 Chloroethane 0.0175 0.020 mg/Kg wet 0.0200 87.7 70-130 .l Chloroform 0.0200 0.0040 mg/Kg wet 0,0200 99.8 70-130 Chloromethane 0.0193 0.010 mg/Kg wet 0.0200 96.4 70-130 2-Chlorotoluene 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 Page 16 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD .nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216398 - SW-846 5035 LCS (B216398-BSI) Prepared & Analyzed: 11/05/18 4-Chlorotoluene 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 1,2-Dibromo-3-chloropropane (DBCP) 0.0252 0.0020 mg/Kg wet 0.0200 126 70-130 1,2-Dibromoethane (EDB) 0.0215 0.0010 mg/Kg wet 0.0200 107 70-130 Dibromomethane 0.0206 0.0020 mg/Kg wet 0.0200 103 70-130 1,2-Dichlorobenzene 0.0211 0.0020 mg/Kg wet 0.0200 106 70-130 1,3-Dichlorobenzene 0.0205 0.0020 mg/Kg wet 0.0200 103 70-130 1,4-Dichlorobenzene 0.0198 0.0020 mg/Kg wet 0.0200 99.1 70-130 trans-1,4-Dichloro-2-butene 0.0211 0.0040 mg/Kg wet 0.0200 105 70-130 Dichlorodifluoromethane(Freon 12) 0.0175 0.020 mg/Kg wet 0.0200 87.5 40-160 1,1-Dichloroethane 0.0200 0.0020 mg/Kg wet 0.0200 100 70-130 1,2-Dichloroethane 0.0210 0.0020 mg/Kg wet 0.0200 105 70-130 1,1-Dichloroethylene 0.0201 0.0040 mg/Kg wet 0.0200 101 70-130 cis-1,2-Dichloroethylene 0.0195 0.0020 mg/Kg wet 0.0200 97.5 70-130 trans-1,2-Dichloroethylene 0.0200 0.0020 mg/Kg wet 0.0200 100 70-130 1,2-Dichloropropane 0.0188 0.0020 mg/Kg wet 0.0200 94.2 70-130 1,3-Dichloropropane 0.0211 0.0010 mg/Kg wet 0.0200 105 70-130 2,2-Dichloropropane 0.0192 0.0020 mg/Kg wet 0.0200 95.9 70-130 1,1-Dichloropropene 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 cis-1,3-Dichloropropene 0.0204 0.0010 mg/Kg wet 0.0200 102 70-130 trans-1,3-Dichloropropene 0.0212 0.0010 mg/Kg wet 0.0200 106 70-130 Diethyl Ether 0.0201 0.020 mg/Kg wet 0.0200 100 70-130 Diisopropyl Ether (RIPE) 0.0201 0.0010 mg/Kg wet 0.0200 101 70-130 1,4-Dioxane 0.212 0.10 mg/Kg wet 0.200 106 40-160 Ethylbenzene 0.0194 0.0020 mg/Kg wet 0.0200 96.8 70-130 Hexachlorobutadiene 0.0210 0.0020 mg/Kg wet 0.0200 105 70-160 2-Hexanone (MBK) 0.265 0.020 mg/Kg wet 0.200 132 70-160 Isopropylbenzene (Cumene) 0.0195 0.0020 mg/Kg wet 0.0200 97.5 70-130 p-Isopropyltoluene (p-Cymene) 0.0186 0.0020 mg/Kg wet 0.0200 93.1 70-130 Methyl tert-Butyl Ether (MTBE) 0.0212 0.0040 mg/Kg wet 0.0200 106 70-130 Methylene Chloride 0.0212 0.020 mg/Kg wet 0.0200 106 40-160 4-Methyl-2-pentanone (MIBK) 0.225 0.020 mg/Kg wet 0.200 113 70-160 Naphthalene 0.0209 0.0040 mg/Kg wet 0.0200 104 40-130 n-Propylbenzene 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 Styrene 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 1, 1, 1,2-Tetrachloroethane 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 1,1,2,2-Tetrachloroethane 0.0218 0.0010 mg/Kg wet 0.0200 109 70-130 Tetrachloroethylene 0.0205 0.0020 mg/Kg wet 0.0200 103 70-130 Tetrahydrofuran 0.0198 0.010 mg/Kg wet 0.0200 98.8 70-130 Toluene 0.0184 0.0020 mg/Kg wet 0.0200 92.1 70-130 1,2,3-Trichlorobenzene 0.0220 0.0020 mg/Kg wet 0.0200 110 70-130 1,2,4-Trichlorobenzene 0.0233 0.0020 mg/Kg wet 0.0200 116 70-130 1,3,5-Trichlorobenzene 0.0226 0.0020 mg/Kg wet 0.0200 113 70-130 1, 1, 1 -Trichloroethane 0.0193 0.0020 mg/Kg wet 0.0200 96.7 70-130 1,1,2-Trichloroethane 0.0201 0.0020 mg/Kg wet 0.0200 100 70-130 Trichloroethylene 0.0197 0.0020 mg/Kg wet 0.0200 98.3 70-130 Trichlorofluoromethane (Freon 11) 0.0179 0.010 mg/Kg wet 0.0200 89.3 70-130 1,2,3-Trichloropropane 0.0222 0.0020 mg/Kg wet 0.0200 ill 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0194 0.010 mg/Kg wet 0.0200 97.0 70-130 113) 1,2,4-Trimethylbenzene 0.0188 0.0020 mg/Kg wet 0.0200 93.9 70-130 1,3,5-Trimethylbenzene 0.0199 0.0020 mg/Kg wet 0.0200 99.3 70-130 Vinyl Chloride 0.0179 0.010 mg/Kg wet 0,0200 89.3 40-130 J f t t f t t Page 17 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216398 - SW-846 5035 LCS (B216398-BSI) Prepared & Analyzed: 11/05/18 m+p Xylene 0.0387 0.0040 mg/Kg wet 0.0400 96.6 70-130 o-Xylene 0.0192 0.0020 mg/Kg wet 0.0200 96.0 70-130 Surrogate:l,2-Dichloroethane-d4 0.0530 mg/Kg wet 0.0500 106 70-130 Surrogate: Toluene-d8 0.0482 mg/Kg wet 0.0500 96.5 70-130 Surrogate:4-Bromofluorobenzene 0.0506 mg/Kg wet 0.0500 101 70-130 LCS Dup (B216398-BSDI) Prepared & Analyzed: 11/05/18 Acetone 0.245 0.10 mg/Kg wet 0.200 123 70-160 43.8 * 25 R-05 t Acrylonitrile 0.0185 0.0060 mg/Kg wet 0.0200 92.4 70-130 5.06 25 tert-Amyl Methyl Ether (TAME) 0.0193 0.0010 mg/Kg wet 0.0200 96.4 70-130 6.04 25 Benzene 0.0186 0.0020 mg/Kg wet 0.0200 92.9 70-130 3.07 25 Bromobenzene 0.0179 0.0020 mg/Kg wet 0.0200 89.3 70-130 9.80 25 Bromochloromethane 0.0222 0.0020 mg/Kg wet 0.0200 111 70-130 0.361 25 Bromodichloromethane 0.0187 0.0020 mg/Kg wet 0.0200 93.6 70-130 5.30 25 Bromoform 0.0201 0.0020 mg/Kg wet 0.0200 101 70-130 7.09 25 Bromomethane 0.0139 0.010 mg/Kg wet 0.0200 69.7 40-130 14.8 25 f 2-Butanone (MEK) 0.225 0.040 mg/Kg wet 0.200 113 70-160 31.1 * 25 R-05 t tert-Butyl Alcohol (TBA) 0.198 0.040 mg/Kg wet 0.200 99.0 40-130 13.9 25 t n-Butylbenzene 0.0190 0.0020 mg/Kg wet 0.0200 94.8 70-130 3.83 25 sec-Butylbenzene 0.0194 0.0020 mg/Kg wet 0.0200 97.1 70-130 0.923 25 tert-Butylbenzene 0.0182 0.0020 mg/Kg wet 0.0200 90.8 70-160 2.29 25 t tert-Butyl Ethyl Ether (TBEE) 0.0195 0.0010 mg/Kg wet 0.0200 97.3 70-130 3.93 25 Carbon Disulfide 0.0195 0.0060 mg/Kg wet 0.0200 97.5 70-130 0.817 25 Carbon Tetrachloride 0.0192 0.0020 mg/Kg wet 0.0200 95.9 70-130 9.34 25 Chlorobenzene 0.0198 0.0020 mg/Kg wet 0.0200 99.2 70-130 2.49 25 Chlorodibromomethane 0.0217 0.0010 mg/Kg wet 0.0200 109 70-130 2.45 25 Chloroethane 0.0177 0.020 mg/Kg wet 0.0200 88.6 70-130 1.02 25 J Chloroform 0.0197 0.0040 mg/Kg wet 0.0200 98.3 70-130 1.51 25 Chloromethane 0.0186 0.010 mg/Kg wet 0.0200 93.2 70-130 3.38 25 2-Chlorotoluene 0.0193 0.0020 mg/Kg wet 0.0200 96.7 70-130 4.05 25 4-Chlorotoluene 0.0193 0.0020 mg/Kg wet 0.0200 96.7 70-130 6.21 25 1,2-Dibromo-3-chloropropane (DBCP) 0.0218 0.0020 mg/Kg wet 0.0200 109 70-130 14.2 25 1,2-Dibromoethane (EDB) 0.0214 0.0010 mg/Kg wet 0.0200 107 70-130 0.187 25 Dibromomethane 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 1.76 25 1,2-Dichlorobenzene 0.0202 0.0020 mg/Kg wet 0.0200 101 70-130 4.35 25 1,3-Dichlorobenzene 0.0196 0.0020 mg/Kg wet 0.0200 98.2 70-130 4.38 25 1,4-Dichlorobenzene 0.0185 0.0020 mg/Kg wet 0.0200 92.4 70-130 7.00 25 trans-1,4-Dichloro-2-butene 0.0193 0.0040 mg/Kg wet 0.0200 96.3 70-130 9.02 25 Dichlorodifluoromethane(Freon 12) 0.0187 0.020 mg/Kg wet 0.0200 93.4 40-160 6.52 25 J t 1, 1 -Dichloroethane 0.0203 0.0020 mg/Kg wet 0.0200 101 70-130 1.39 25 1,2-Dichloroethane 0.0203 0.0020 mg/Kg wet 0.0200 102 70-130 3.48 25 1,1-Dichloroethylene 0.0190 0.0040 mg/Kg wet 0.0200 94.9 70-130 5.83 25 cis-1,2-Dichloroethylene 0.0188 0.0020 mg/Kg wet 0.0200 94.0 70-130 3.66 25 trans-1,2-Dichloroethylene 0.0195 0.0020 mg/Kg wet 0.0200 97.5 70-130 2.73 25 1,2-Dichloropropane 0.0197 0.0020 mg/Kg wet 0.0200 98.3 70-130 4.26 25 1,3-Dichloropropane 0.0203 0.0010 mg/Kg wet 0.0200 102 70-130 3.68 25 2,2-Dichloropropane 0.0189 0.0020 mg/Kg wet 0.0200 94.6 70-130 1.36 25 1,1-Dichloropropene 0.0187 0.0020 mg/Kg wet 0.0200 93.3 70-130 7.53 25 cis-1,3-Dichloropropene 0.0202 0.0010 mg/Kg wet 0.0200 101 70-130 0.888 25 trans-1,3-Dichloropropene 0.0200 0.0010 mg/Kg wet 0.0200 99.8 70-130 5.84 25 Diethyl Ether 0.0201 0.020 mg/Kg wet 0.0200 100 70-130 0.00 25 Diisopropyl Ether (DIPE) 0.0199 0.0010 mg/Kg wet 0.0200 99.4 70-130 1.30 25 Page 18 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216398 - SW-846 5035 LCS Dup (B216398-BSD1) Prepared & Analyzed: 11/05/18 1,4-Dioxane 0.208 0.10 mg/Kg wet 0.200 104 40-160 1.85 50 f # Ethylbenzene 0.0182 0.0020 mg/Kg wet 0.0200 90.8 70-130 6.40 25 Hexachlorobutadiene 0.0204 0.0020 mg/Kg wet 0.0200 102 70-160 3.19 25 2-Hexanone (MBK) 0.219 0.020 mg/Kg wet 0.200 110 70-160 18.9 25 f Isopropylbenzene (Cumene) 0.0190 0.0020 mg/Kg wet 0.0200 94.8 70-130 2.81 25 p-Isopropyltoluene (p-Cymene) 0.0184 0.0020 mg/Kg wet 0.0200 91.9 70-130 1.30 25 Methyl tert-Butyl Ether (MTBE) 0.0207 0.0040 mg/Kg wet 0.0200 104 70-130 2.58 25 Methylene Chloride 0.0204 0.020 mg/Kg wet 0.0200 102 40-160 4.13 25 t 4-Methyl-2-pentanone (MIBK) 0.213 0.020 mg/Kg wet 0.200 107 70-160 5.43 25 t Naphthalene 0.0200 0.0040 mg/Kg wet 0.0200 99.9 40-130 4.50 25 f n-Propylbenzene 0.0193 0.0020 mg/Kg wet 0.0200 96.3 70-130 4.47 25 Styrene 0.0181 0.0020 mg/Kg wet 0.0200 90.4 70-130 10.7 25 1, 1, 1,2-Tetrachloroethane 0.0192 0.0020 mg/Kgwet 0.0200 96.0 70-130 5.67 25 1,1,2,2-Tetrachloroethane 0.0198 0.0010 mg/Kg wet 0.0200 99.1 70-130 9.61 25 Tetrachloroethylene 0.0199 0.0020 mg/Kg wet 0.0200 99.7 70-130 2.87 25 Tetrahydrofuran 0.0199 0.010 mg/Kg wet 0.0200 99.5 70-130 0.706 25 Toluene 0.0182 0.0020 mg/Kg wet 0.0200 90.8 70-130 1.42 25 1,2,3-Trichlorobenzene 0.0198 0.0020 mg/Kg wet 0.0200 99.2 70-130 10.1 25 1,2,4-Trichlorobenzene 0.0221 0.0020 mg/Kg wet 0.0200 110 70-130 5.21 25 1,3,5-Trichlorobenzene 0.0201 0.0020 mg/Kg wet 0.0200 100 70-130 11.7 25 1, 1, 1 -Trichloroethane 0.0194 0.0020 mg/Kg wet 0.0200 97.0 70-130 0.310 25 1,1,2-Trichloroethane 0.0196 0.0020 mg/Kg wet 0.0200 98.2 70-130 2.32 25 Trichloroethylene 0.0191 0.0020 mg/Kg wet 0.0200 95.6 70-130 2.78 25 Trichlorofluoromethane (Freon 11) 0.0182 0.010 mg/Kg wet 0.0200 90.8 70-130 1.67 25 1,2,3-Trichloropropane 0.0207 0.0020 mg/Kgwet 0.0200 103 70-130 7.18 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.0187 0.010 mg/Kg wet 0.0200 93.4 70-130 3.78 25 113) 1,2,4-Trimethylbenzene 0.0178 0.0020 mg/Kg wet 0.0200 88.9 70-130 5.47 25 1,3,5-Trimethylbenzene 0.0187 0.0020 mg/Kg wet 0.0200 93.5 70-130 6.02 25 Vinyl Chloride 0.0184 0.010 mg/Kg wet 0.0200 91.8 40-130 2.76 25 t m+p Xylene 0.0363 0.0040 mg/Kg wet 0.0400 90.8 70-130 6.19 25 o-Xylene 0.0188 0.0020 mg/Kg wet 0.0200 94.0 70-130 2.11 25 Surrogate:l,2-Dichloroethane-d4 0.0521 mg/Kg wet 0.0500 104 70-130 Surrogate: Toluene-d8 0.0492 mg/Kg wet 0.0500 98.4 70-130 Surrogate:4-Bromofluorobenzene 0.0500 mg/Kg wet 0.0500 100 70-130 Page 19 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216342 - SW-846 3546 Blank (B216342-BLK1) Prepared: 11/03/18 Analyzed: 11/05/18 Acenaphthene ND 0.17 mg/Kg wet Acenaphthylene ND 0.17 mg/Kg wet Acetophenone ND 0.34 mg/Kg wet Aniline ND 0.34 mg/Kg wet Anthracene ND 0.17 mg/Kg wet Benzidine ND 0.66 mg/Kg wet Benzo(a)anthracene ND 0.17 mg/Kg wet Benzo(a)pyrene ND 0.17 mg/Kg wet Benzo(b)fluoranthene ND 0.17 mg/Kg wet Benzo(g,h,i)perylene ND 0.17 mg/Kg wet Benzo(b)fluoranthene ND 0.17 mg/Kg wet Benzoic Acid ND 1.0 mg/Kg wet Bis(2-chloroethoxy)methane ND 0.34 mg/Kg wet Bis(2-chloroethyl)ether ND 0.34 mg/Kg wet Bis(2-chloroisopropyl)ether ND 0.34 mg/Kg wet Bis(2-Ethylhexyl)phthalate ND 0.34 mg/Kg wet 4-Bromophenylphenylether ND 0.34 mg/Kg wet Butylbenzylphthalate ND 0.34 mg/Kg wet Carbazole ND 0.17 mg/Kg wet 4-Chloroaniline ND 0.66 mg/Kg wet 4-Chloro-3-methylphenol ND 0.66 mg/Kg wet 2-Chloronaphthalene ND 0.34 mg/Kg wet 2-Chlorophenol ND 0.34 mg/Kg wet 4-Chlorophenylphenylether ND 0.34 mg/Kg wet Chrysene ND 0.17 mg/Kg wet Dibenz(a,h)anthracene ND 0.17 mg/Kg wet Dibenzofuran ND 0.34 mg/Kg wet Di-n-butylphthalate ND 0.34 mg/Kg wet 1,2-Dichlorobenzene ND 0.34 mg/Kg wet 1,3-Dichlorobenzene ND 0.34 mg/Kg wet 1,4-Dichlorobenzene ND 0.34 mg/Kg wet 3,3-Dichlorobenzidine ND 0.17 mg/Kg wet 2,4-Dichlorophenol ND 0.34 mg/Kg wet Diethylphthalate ND 0.34 mg/Kg wet 2,4-Dimethylphenol ND 0.34 mg/Kg wet Dimethylphthalate ND 0.34 mg/Kg wet 4,6-Dinitro-2-methylphenol ND 0.34 mg/Kg wet 2,4-Dinitrophenol ND 0.66 mg/Kg wet 2,4-Dinitrotoluene ND 0.34 mg/Kg wet 2,6-Dinitrotoluene ND 0.34 mg/Kg wet Di-n-octylphthalate ND 0.34 mg/Kg wet 1,2-Diphenylhydrazine (as Azobenzene) ND 0.34 mg/Kg wet Fluoranthene ND 0.17 mg/Kg wet Fluorene ND 0.17 mg/Kg wet Hexachlorobenzene ND 0.34 mg/Kg wet Hexachlorobutadiene ND 0.34 mg/Kg wet Hexachlorocyclopentadiene ND 0.34 mg/Kg wet Hexachloroethane ND 0.34 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.17 mg/Kg wet Isophorone ND 0.34 mg/Kg wet 1-Methylnaphthalene ND 0.17 mg/Kg wet 2-Methylnaphthalene ND 0.17 mg/Kg wet V-05, V-34 V-05, V-34 V-34 V-19 L-04, V-05 Page 20 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216342 - SW-846 3546 Blank (B216342-BLK1) Prepared: 11/03/18 Analyzed: 11/05/18 2-Methylphenol ND 0.34 mg/Kg wet 3/4-Methylphenol ND 0.34 mg/Kg wet Naphthalene ND 0.17 mg/Kg wet 2-Nitroaniline ND 0.34 mg/Kg wet V-06 3-Nitroaniline ND 0.34 mg/Kg wet 4-Nitroaniline ND 0.34 mg/Kg wet Nitrobenzene ND 0.34 mg/Kg wet 2-Nitrophenol ND 0.34 mg/Kg wet 4-Nitrophenol ND 0.66 mg/Kg wet V-06 N-Nitrosodimethylamine ND 0.34 mg/Kg wet N-Nitrosodiphenylamine ND 0.34 mg/Kg wet N-Nitrosodi-n-propylamine ND 0.34 mg/Kg wet Pentachloronitrobenzene ND 0.34 mg/Kg wet Pentachlorophenol ND 0.34 mg/Kg wet Phenanthrene ND 0.17 mg/Kg wet Phenol ND 0.34 mg/Kg wet Pyrene ND 0.17 mg/Kg wet Pyridine ND 0.34 mg/Kg wet V-05 1,2,4,5-Tetrachlorobenzene ND 0.34 mg/Kg wet 1,2,4-Trichlorobenzene ND 0.34 mg/Kg wet 2,4,5-Trichlorophenol ND 0.34 mg/Kg wet 2,4,6-Trichlorophenol ND 0.34 mg/Kg wet Surrogate:2-Fluorophenol 3.75 mg/Kg wet 6.67 56.2 30-130 Surrogate: Phenol-d6 4.24 mg/Kg wet 6.67 63.6 30-130 Surrogate: Nitrobenzene-d5 2.13 mg/Kg wet 3.33 64.0 30-130 Surrogate:2-Fluorobiphenyl 1.77 mg/Kg wet 3.33 53.1 30-130 Surrogate: 2,4,6-Tribromophenol 4.84 mg/Kg wet 6.67 72.5 30-130 Surrogate: p-Terphenyl-dl4 2.21 mg/Kg wet 3.33 66.4 30-130 LCS (B216342-BS1) Prepared: 11/03/18 Analyzed: 11/05/18 Acenaphthene 0.927 0.17 mg/Kg wet 1.67 55.6 40-140 Acenaphthylene 1.01 0.17 mg/Kg wet 1.67 60.8 40-140 Acetophenone 0.955 0.34 mg/Kg wet 1.67 57.3 40-140 Aniline 0.649 0.34 mg/Kg wet 1.67 38.9 10-140 V-05, V-34 f Anthracene 0.969 0.17 mg/Kg wet 1.67 58.1 40-140 Benzidine 0.766 0.66 mg/Kg wet 1.67 45.9 40-140 V-05,V-34 Benzo(a)anthracene 1.01 0.17 mg/Kg wet 1.67 60.5 40-140 Benzo(a)pyrene 1.11 0.17 mg/Kg wet 1.67 66.8 40-140 Benzo(b)fluoranthene 1.05 0.17 mg/Kg wet 1.67 62.9 40-140 Benzo(g,h,i)perylene 1.28 0.17 mg/Kg wet 1.67 76.8 40-140 Benzo(k)fluoranthene 1.05 0.17 mg/Kg wet 1.67 63.1 40-140 Benzoic Acid 1.12 1.0 mg/Kg wet 1.67 67.4 30-130 Bis(2-chloroethoxy)methane 1.03 0.34 mg/Kg wet 1.67 61.7 40-140 Bis(2-chloroethyl)ether 1.01 0.34 mg/Kg wet 1.67 60.7 40-140 Bis(2-chloroisopropyl)ether 1.19 0.34 mg/Kg wet 1.67 71.4 40-140 Bis(2-Ethylhexyl)phthalate 1.14 0.34 mg/Kg wet 1.67 68.3 40-140 4-Bromophenylphenylether 1.04 0.34 mg/Kg wet 1.67 62.4 40-140 Butylbenzylphthalate 1.09 0.34 mg/Kg wet 1.67 65.6 40-140 Carbazole 0.920 0.17 mg/Kg wet 1.67 55.2 40-140 4-Chloroaniline 0.655 0.66 mg/Kg wet 1.67 39.3 10-140 V-34, J t 4-Chloro-3-methylphenol 1.08 0.66 mg/Kg wet 1.67 64.6 30-130 2-Chloronaphthalene 0.859 0.34 mg/Kg wet 1.67 51.6 40-140 Page 21 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD \nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216342 - SW-846 3546 LCS (B216342-BS1) Prepared: 11/03/18 Analyzed: 11/05/18 2-Chlorophenol 0.904 0.34 mg/Kg wet 1.67 54.2 30-130 4-Chlorophenylphenylether 1.08 0.34 mg/Kg wet 1.67 64.8 40-140 Chrysene 0.947 0.17 mg/Kg wet 1.67 56.8 40-140 Dibenz(a,h)anthracene 1.27 0.17 mg/Kg wet 1.67 76.3 40-140 Dibenzofuran 1.07 0.34 mg/Kg wet 1.67 64.1 40-140 Di-n-butylphthalate 1.02 0.34 mg/Kg wet 1.67 61.2 40-140 1,2-Dichlorobenzene 0.829 0.34 mg/Kg wet 1.67 49.8 40-140 1,3-Dichlorobenzene 0.780 0.34 mg/Kg wet 1.67 46.8 40-140 1,4-Dichlorobenzene 0.806 0.34 mg/Kg wet 1.67 48.3 40-140 3,3-Dichlorobenzidine 0.930 0.17 mg/Kg wet 1.67 55.8 20-140 t 2,4-Dichlorophenol 0.975 0.34 mg/Kg wet 1.67 58.5 30-130 Diethylphthalate 1.09 0.34 mg/Kg wet 1.67 65.3 40-140 2,4-Dimethylphenol 0.876 0.34 mg/Kg wet 1.67 52.6 30-130 Dimethylphthalate 1.08 0.34 mg/Kg wet 1.67 65.1 40-140 4,6-Dinitro-2-methylphenol 0.957 0.34 mg/Kg wet 1.67 57.4 30-130 2,4-Dinitrophenol 0.813 0.66 mg/Kg wet 1.67 48.8 30-130 V-19 2,4-Dinitrotoluene 1.12 0.34 mg/Kg wet 1.67 67.4 40-140 2,6-Dinitrotoluene 1.19 0.34 mg/Kg wet 1.67 71.2 40-140 Di-n-octylphthalate 1.27 0.34 mg/Kg wet 1.67 76.0 40-140 1,2-Diphenylhydrazine (as Azobenzene) 1.08 0.34 mg/Kg wet 1.67 64.5 40-140 Fluoranthene 0.964 0.17 mg/Kg wet 1.67 57.8 40-140 Fluorene 1.03 0.17 mg/Kg wet 1.67 61.6 40-140 Hexachlorobenzene 1.02 0.34 mg/Kg wet 1.67 61.4 40-140 Hexachlorobutadiene 0.880 0.34 mg/Kg wet 1.67 52.8 40-140 Hexachlorocyclopentadiene 0.554 0.34 mg/Kg wet 1.67 33.2 * 40-140 L-04, V-05 Hexachloroethane 0.833 0.34 mg/Kg wet 1.67 50.0 40-140 Indeno(1,2,3-cd)pyrene 1.36 0.17 mg/Kg wet 1.67 81.8 40-140 Isophorone 1.00 0.34 mg/Kg wet 1.67 60.2 40-140 1-Methylnaphthalene 0.874 0.17 mg/Kg wet 1.67 52.4 40-140 2-Methylnaphthalene 0.957 0.17 mg/Kg wet 1.67 57.4 40-140 2-Methylphenol 0.981 0.34 mg/Kg wet 1.67 58.9 30-130 3/4-Methylphenol 1.03 0.34 mg/Kg wet 1.67 61.6 30-130 Naphthalene 0.891 0.17 mg/Kg wet 1.67 53.5 40-140 2-Nitroaniline 1.23 0.34 mg/Kg wet 1.67 74.1 40-140 V-06 3-Nitroaniline 0.978 0.34 mg/Kg wet 1.67 58.7 30-140 t 4-Nitroaniline 1.06 0.34 mg/Kg wet 1.67 63.7 40-140 Nitrobenzene 0.979 0.34 mg/Kg wet 1.67 58.8 40-140 2-Nitrophenol 0.967 0.34 mg/Kg wet 1.67 58.0 30-130 4-Nitrophenol 1.32 0.66 mg/Kg wet 1.67 78.9 30-130 V-06 N-Nitrosodimethylamine 1.06 0.34 mg/Kg wet 1.67 63.4 40-140 N-Nitrosodiphenylamine 1.15 0.34 mg/Kg wet 1.67 68.8 40-140 N-Nitrosodi-n-propylamine 0.982 0.34 mg/Kg wet 1.67 58.9 40-140 Pentachloronitrobenzene 1.05 0.34 mg/Kg wet 1.67 63.0 40-140 Pentachlorophenol 0.671 0.34 mg/Kg wet 1.67 40.3 30-130 Phenanthrene 0.963 0.17 mg/Kg wet 1.67 57.8 40-140 Phenol 0.962 0.34 mg/Kg wet 1.67 57.7 30-130 Pyrene 1.06 0.17 mg/Kg wet 1.67 63.7 40-140 Pyridine 0.512 0.34 mg/Kg wet 1.67 30.7 30-140 V-05 1,2,4,5-Tetrachlorobenzene 0.984 0.34 mg/Kg wet 1.67 59.1 40-140 1,2,4-Trichlorobenzene 0.854 0.34 mg/Kg wet 1.67 51.3 40-140 2,4,5-Trichlorophenol 1.07 0.34 mg/Kg wet 1.67 64.0 30-130 2,4,6-Trichlorophenol 1.04 0.34 mg/Kg wet 1.67 62.7 30-130 Page 22 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216342 - SW-846 3546 LCS (B216342-BS1) Prepared: 11/03/18 Analyzed: 11/05/18 Surrogate:2-Fluorophenol 3.68 mg/Kg wet 6.67 55.2 30-130 Surrogate: Phenol-d6 4.18 mg/Kg wet 6.67 62.6 30-130 Surrogate: Nitrobenzene-d5 2.12 mg/Kg wet 3.33 63.5 30-130 Surrogate:2-Fluorobiphenyl 1.79 mg/Kg wet 3.33 53.6 30-130 Surrogate: 2,4,6-Tribromophenol 5.32 mg/Kg wet 6.67 79.7 30-130 Surrogate:p-Terphenyl-dl4 2.23 mg/Kg wet 3.33 66.8 30-130 LCS Dup (B216342-BSD1) Prepared: 11/03/18 Analyzed: 11/05/18 Acenaphthene 1.07 0.17 mg/Kg wet 1.67 63.9 40-140 13.9 30 Acenaphthylene 1.14 0.17 mg/Kg wet 1.67 68.2 40-140 11.4 30 Acetophenone 0.994 0.34 mg/Kg wet 1.67 59.6 40-140 4.00 30 Aniline 0.689 0.34 mg/Kg wet 1.67 41.4 10-140 6.03 50 V-05,V-34 f # Anthracene 1.07 0.17 mg/Kg wet 1.67 64.1 40-140 9.81 30 Benzidine 0.891 0.66 mg/Kg wet 1.67 53.4 40-140 15.1 30 V-05,V-34 Benzo(a)anthracene 1.11 0.17 mg/Kg wet 1.67 66.7 40-140 9.87 30 Benzo(a)pyrene 1.25 0.17 mg/Kg wet 1.67 74.9 40-140 11.5 30 Benzo(b)fluoranthene 1.16 0.17 mg/Kg wet 1.67 69.8 40-140 10.3 30 Benzo(g,h,i)perylene 1.42 0.17 mg/Kg wet 1.67 85.1 40-140 10.2 30 Benzo(k)fluoranthene 1.15 0.17 mg/Kg wet 1.67 69.3 40-140 9.28 30 Benzoic Acid 1.18 1.0 mg/Kg wet 1.67 70.6 30-130 4.63 50 $ Bis(2-chloroethoxy)methane 1.13 0.34 mg/Kg wet 1.67 67.7 40-140 9.18 30 Bis(2-chloroethyl)ether 1.01 0.34 mg/Kg wet 1.67 60.7 40-140 0.0329 30 Bis(2-chloroisopropyl)ether 1.18 0.34 mg/Kg wet 1.67 70.8 40-140 0.844 30 Bis(2-Ethylhexyl)phthalate 1.26 0.34 mg/Kg wet 1.67 75.8 40-140 10.4 30 4-Bromophenylphenylether 1.05 0.34 mg/Kg wet 1.67 62.9 40-140 0.766 30 Butylbenzylphthalate 1.26 0.34 mg/Kg wet 1.67 75.7 40-140 14.4 30 Carbazole 1.02 0.17 mg/Kg wet 1.67 61.4 40-140 10.7 30 4-Chloroaniline 0.694 0.66 mg/Kg wet 1.67 41.7 10-140 5.78 30 V-34 t 4-Chloro-3-methylphenol 1.21 0.66 mg/Kg wet 1.67 72.5 30-130 11.5 30 2-Chloronaphthalene 0.971 0.34 mg/Kg wet 1.67 58.3 40-140 12.2 30 2-Chorophenol 0.932 0.34 mg/Kg wet 1.67 55.9 30-130 3.05 30 4-Chlorophenylphenylether 1.21 0.34 mg/Kg wet 1.67 72.8 40-140 11.5 30 Chrysene 1.03 0.17 mg/Kg wet 1.67 61.8 40-140 8.40 30 Dibenz(a,h)anthracene 1.41 0.17 mg/Kg wet 1.67 84.8 40-140 10.6 30 Dibenzofuran 1.17 0.34 mg/Kg wet 1.67 70.4 40-140 9.37 30 Di-n-butylphthalate 1.11 0.34 mg/Kg wet 1.67 66.4 40-140 8.12 30 1,2-Dichlorobenzene 0.809 0.34 mg/Kg wet 1.67 48.6 40-140 2.44 30 1,3-Dichlorobenzene 0.750 0.34 mg/Kg wet 1.67 45.0 40-140 3.97 30 1,4-Dichlorobenzene 0.740 0.34 mg/Kg wet 1.67 45.0 40-140 7.20 30 3,3-Dichlorobenzidine 1.00 0.17 mg/Kg wet 1.67 60.2 20-140 7.66 50 t # 2,4-Dichlorophenol 1.08 0.34 mg/Kg wet 1.67 64.6 30-130 9.98 30 Diethylphthalate 1.23 0.34 mg/Kg wet 1.67 73.9 40-140 12.3 30 2,4-Dimethylphenol 0.967 0.34 mg/Kg wet 1.67 58.0 30-130 9.91 30 Dimethylphthalate 1.23 0.34 mg/Kg wet 1.67 73.8 40-140 12.5 30 4,6-Dinitro-2-methylphenol 1.08 0.34 mg/Kg wet 1.67 64.8 30-130 12.0 30 2,4-Dinitrophenol 0.906 0.66 mg/Kg wet 1.67 54.3 30-130 10.7 30 V-19 2,4-Dinitrotoluene 1.26 0.34 mg/Kg wet 1.67 75.8 40-140 11.7 30 2,6-Dinitrotoluene 1.35 0.34 mg/Kg wet 1.67 81.2 40-140 13.1 30 Di-n-octylphthalate 1.39 0.34 mg/Kg wet 1.67 83.5 40-140 9.45 30 1,2-Diphenylhydrazine (as Azobenzene) 1.18 0.34 mg/Kg wet 1.67 70.7 40-140 9.08 30 Fluoranthene 1.08 0.17 mg/Kg wet 1.67 64.7 40-140 11.3 30 Fluorene 1.18 0.17 mg/Kg wet 1.67 70.8 40-140 13.9 30 Page 23 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216342 - SW-846 3546 LCS Dup (B216342-BSD1) Prepared: 11/03/18 Analyzed: 11/05/18 Hexachlorobenzene 1.04 0.34 mg/Kg wet 1.67 62.6 40-140 2.03 30 Hexachlorobutadiene 0.902 0.34 mg/Kg wet 1.67 54.1 40-140 2.47 30 Hexachlorocyclopentadiene 0.619 0.34 mg/Kg wet 1.67 37.1 * 40-140 11.0 30 L-04, V-05 Hexachloroethane 0.816 0.34 mg/Kg wet 1.67 49.0 40-140 2.02 30 Indeno(1,2,3-cd)pyrene 1.48 0.17 mg/Kg wet 1.67 88.8 40-140 8.21 30 Isophorone 1.08 0.34 mg/Kg wet 1.67 65.1 40-140 7.79 30 1-Methylnaphthalene 0.959 0.17 mg/Kg wet 1.67 57.5 40-140 9.31 30 2-Methylnaphthalene 1.06 0.17 mg/Kg wet 1.67 63.6 40-140 10.2 30 2-Methylphenol 1.06 0.34 mg/Kg wet 1.67 63.5 30-130 7.49 30 3/4-Methylphenol 1.11 0.34 mg/Kg wet 1.67 66.4 30-130 7.44 30 Naphthalene 0.925 0.17 mg/Kg wet 1.67 55.5 40-140 3.78 30 2-Nitroanihne 1.49 0.34 mg/Kg wet 1.67 89.2 40-140 18.5 30 V-06 3-Nitroaniline 1.08 0.34 mg/Kg wet 1.67 65.0 30-140 10.3 30 f 4-Nitroaniline 1.20 0.34 mg/Kg wet 1.67 71.8 40-140 12.0 30 Nitrobenzene 1.03 0.34 mg/Kg wet 1.67 61.8 40-140 5.04 30 2-Nitrophenol 1.06 0.34 mg/Kg wet 1.67 63.3 30-130 8.70 30 4-Nitrophenol 1.92 0.66 mg/Kg wet 1.67 91.1 30-130 14.3 50 V-06 $ N-Nitrosodimethylamine 1.01 0.34 mg/Kg wet 1.67 60.7 40-140 4.22 30 N-Nitrosodiphenylamine 1.25 0.34 mg/Kg wet 1.67 74.9 40-140 8.49 30 N-Nitrosodi-n-propylamine 1.07 0.34 mg/Kg wet 1.67 64.4 40-140 8.95 30 Pentachloronitrobenzene 1.06 0.34 mg/Kg wet 1.67 63.7 40-140 1.23 30 Pentachlorophenol 0.679 0.34 mg/Kg wet 1.67 40.7 30-130 1.09 30 Phenanthrene 1.06 0.17 mg/Kg wet 1.67 63.9 40-140 9.99 30 Phenol 1.01 0.34 mg/Kg wet 1.67 60.7 30-130 5.03 30 Pyrene 1.18 0.17 mg/Kg wet 1.67 70.9 40-140 10.6 30 Pyridine 0.473 0.34 mg/Kg wet 1.67 28.4 * 30-140 7.99 30 L-07, V-05 t 1,2,4,5-Tetrachlorobenzene 1.08 0.34 mg/Kg wet 1.67 65.0 40-140 9.51 30 1,2,4-Trichlorobenzene 0.887 0.34 mg/Kg wet 1.67 53.2 40-140 3.71 30 2,4,5-Trichlorophenol 1.22 0.34 mg/Kg wet 1.67 73.3 30-130 13.6 30 2,4,6-Trichlorophenol 1.18 0.34 mg/Kg wet 1.67 70.5 30-130 11.8 30 Surrogate:2-Fluorophenol 3.74 mg/Kg wet 6.67 56.2 30-130 Surrogate: Phenol-d6 4.38 mg/Kg wet 6.67 65.7 30-130 Surrogate: Nitrobenzene-d5 2.17 mg/Kg wet 3.33 65.2 30-130 Surrogate: 2-Fluorobiphenyl 2.01 mg/Kg wet 3.33 60.3 30-130 Surrogate:2,4,6-Tribromophenol 5.88 mg/Kg wet 6.67 88.2 30-130 Surrogate: p-Terphenyl-dl4 2.44 mg/Kg wet 3.33 73.3 30-130 Page 24 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216348 - SW-846 3546 Blank (B216348-BLK1) Prepared: 11/04/18 Analyzed: 11/05/18 C9-C 18 Aliphatics ND 10 mg/Kg wet C19-C36 Aliphatics ND 10 mg/Kg wet Cl 1-C22 Aromatics ND 10 mg/Kg wet Acenaphthene ND 0.10 mg/Kg wet Acenaphthylene ND 0.10 mg/Kg wet Anthracene ND 0.10 mg/Kg wet Benzo(a)anthracene ND 0.10 mg/Kg wet Benzo(a)pyrene ND 0.10 mg/Kg wet Benzo(b)fluoranthene ND 0.10 mg/Kg wet Benzo(g,h,i)perylene ND 0.10 mg/Kg wet Benzo(b)fluoranthene ND 0.10 mg/Kg wet Chrysene ND 0.10 mg/Kg wet Dibenz(a,h)anthracene ND 0.10 mg/Kg wet Fluoranthene ND 0.10 mg/Kg wet Fluorene ND 0.10 mg/Kg wet Indeno(1,2,3-cd)pyrene ND 0.10 mg/Kg wet 2-Methylnaphthalene ND 0.10 mg/Kg wet Naphthalene ND 0.10 mg/Kg wet Phenanthrene ND 0.10 mg/Kg wet Pyrene ND 0.10 mg/Kg wet n-Decane ND 0.10 mg/Kg wet R-05 n-Docosane ND 0.10 mg/Kg wet n-Dodecane ND 0.10 mg/Kg wet n-Eicosane ND 0.10 mg/Kg wet n-Hexacosane ND 0.10 mg/Kg wet n-Hexadecane ND 0.10 mg/Kg wet n-Hexatriacontane ND 0.10 mg/Kg wet n-Nonadecane ND 0.10 mg/Kg wet n-Nonane ND 0.10 mg/Kg wet R-05 n-Octacosane ND 0.10 mg/Kg wet n-Octadecane ND 0.10 mg/Kg wet n-Tetracosane ND 0.10 mg/Kg wet n-Tetradecane ND 0.10 mg/Kg wet n-Triacontane ND 0.10 mg/Kg wet Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet Surrogate: Chlorooctadecane (COD) 3.83 mg/Kg wet 5.15 74.3 40-140 Surrogate: o-Terphenyl (OTP) 4.08 mg/Kg wet 5.00 81.6 40-140 Surrogate:2-Bromonaphthalene 5.59 mg/Kg wet 5.00 112 40-140 Surrogate: 2-Fluorobiphenyl 5.93 mg/Kg wet 5.00 119 40-140 LCS (B216348-BS1) Prepared: 11/04/18 Analyzed: 11/05/18 C9-C 18 Aliphatics 21.6 10 mg/Kg wet 30.0 72.1 40-140 C19-C36Aliphatics 31.8 10 mg/Kg wet 40.0 79.6 40-140 Acenaphthene 3.41 0.10 mg/Kg wet 5.00 68.1 40-140 Acenaphthylene 3.20 0.10 mg/Kg wet 5.00 63.9 40-140 Anthracene 3.30 0.10 mg/Kg wet 5.00 66.0 40-140 Benzo(a)anthracene 3.22 0.10 mg/Kg wet 5.00 64.4 40-140 Benzo(a)pyrene 3.20 0.10 mg/Kg wet 5.00 64.0 40-140 Benzo(b)fluoranthene 3.30 0.10 mg/Kg wet 5.00 66.0 40-140 Benzo(g,h,i)perylene 3.21 0.10 mg/Kg wet 5.00 64.3 40-140 Benzo(k)fluoranthene 3.26 0.10 mg/Kg wet 5.00 65.2 40-140 Page 25 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD walyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216348 - SW-846 3546 LCS (B216348-BSI) Prepared: 11/04/18 Analyzed: 11/05/18 Chrysene 3.32 0.10 mg/Kg wet 5.00 66.5 40-140 Dibenz(a,h)anthracene 3.37 0.10 mg/Kg wet 5.00 67.3 40-140 Fluoranthene 3.32 0.10 mg/Kg wet 5.00 66.4 40-140 Fluorene 3.32 0.10 mg/Kg wet 5.00 66.3 40-140 Indeno(1,2,3-cd)pyrene 3.14 0.10 mg/Kg wet 5.00 62.8 40-140 2-Methylnaphthalene 3.03 0.10 mg/Kg wet 5.00 60.6 40-140 Naphthalene 3.09 0.10 mg/Kg wet 5.00 61.9 40-140 Phenanthrene 3.39 0.10 mg/Kg wet 5.00 67.7 40-140 Pyrene 3.33 0.10 mg/Kg wet 5.00 66.5 40-140 n-Decane 2.60 0.10 mg/Kg wet 5.00 52.0 40-140 R-05 n-Docosane 3.32 0.10 mg/Kg wet 5.00 66.3 40-140 n-Dodecane 3.06 0.10 mg/Kg wet 5.00 61.2 40-140 n-Eicosane 3.30 0.10 mg/Kg wet 5.00 66.1 40-140 n-Hexacosane 3.26 0.10 mg/Kg wet 5.00 65.3 40-140 n-Hexadecane 3.48 0.10 mg/Kg wet 5.00 69.5 40-140 n-Hexatriacontane 3.16 0.10 mg/Kg wet 5.00 63.3 40-140 n-Nonadecane 3.33 0.10 mg/Kg wet 5.00 66.7 40-140 n-Nonane 1.94 0.10 mg/Kg wet 5.00 38.8 30-140 R-05 n-Octacosane 3.18 0.10 mg/Kg wet 5.00 63.7 40-140 n-Octadecane 3.44 0.10 mg/Kg wet 5.00 68.8 40-140 n-Tetracosane 3.30 0.10 mg/Kg wet 5.00 66.0 40-140 n-Tetradecane 3.36 0.10 mg/Kg wet 5.00 67.2 40-140 n-Triacontane 3.22 0.10 mg/Kg wet 5.00 64.3 40-140 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 3.34 mg/Kg wet 5.15 64.9 40-140 Surrogate: o-Terphenyl (OTP) 3.41 mg/Kg wet 5.00 68.2 40-140 Surrogate: 2-Bromonaphthalene 5.17 mg/Kg wet 5.00 103 40-140 Surrogate:2-Fluorobiphenyl 5.68 mg/Kg wet 5.00 114 40-140 LCS Dup (B216348-BSD1) Prepared: 11/04/18 Analyzed: 11/05/18 C9-C18Aliphatics 19.2 10 mg/Kg wet 30.0 63.9 40-140 12.0 C19-C36Aliphatics 34.2 10 mg/Kg wet 40.0 85.6 40-140 7.24 Acenaphthene 3.03 0.10 mg/Kg wet 5.00 60.5 40-140 11.8 Acenaphthylene 2.82 0.10 mg/Kg wet 5.00 56.5 40-140 12.4 Anthracene 3.40 0.10 mg/Kg wet 5.00 70.0 40-140 5.87 Benzo(a)anthracene 3.63 0.10 mg/Kg wet 5.00 72.7 40-140 12.0 Benzo(a)pyrene 3.39 0.10 mg/Kg wet 5.00 71.7 40-140 11.3 Benzo(b)fluoranthene 3.73 0.10 mg/Kg wet 5.00 74.5 40-140 12.1 Benzo(g,h,i)perylene 3.35 0.10 mg/Kg wet 5.00 67.0 40-140 4.23 Benzo(k)fluoranthene 3.65 0.10 mg/Kg wet 5.00 72.9 40-140 11.1 Chrysene 3.71 0.10 mg/Kg wet 5.00 74.2 40-140 11.0 Dibenz(a,h)anthracene 3.65 0.10 mg/Kg wet 5.00 73.0 40-140 8.14 Fluoranthene 3.68 0.10 mg/Kg wet 5.00 73.6 40-140 10.4 Fluorene 3.06 0.10 mg/Kg wet 5.00 61.2 40-140 8.06 Indeno(1,2,3-cd)pyrene 3.50 0.10 mg/Kg wet 5.00 70.1 40-140 11.0 2-Methylnaphthalene 2.58 0.10 mg/Kg wet 5.00 51.6 40-140 16.0 Naphthalene 2.55 0.10 mg/Kg wet 5.00 51.0 40-140 19.3 Phenanthrene 3.42 0.10 mg/Kg wet 5.00 68.3 40-140 0.876 Pyrene 3.70 0.10 mg/Kg wet 5.00 74.1 40-140 10.7 n-Decane 1.90 0.10 mg/Kg wet 5.00 38.0 * 40-140 31.1 n-Docosane 3.67 0.10 mg/Kg wet 5.00 73.4 40-140 10.0 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 25 L-07.A 25 Page 26 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - EPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216348 - SW-846 3546 LCS Dup (B216348-BSD1) Prepared: 11/04/18 Analyzed: 11/05/18 n-Dodecane 2.45 0.10 mg/Kg wet 5.00 49.0 40-140 22.1 25 n-Eicosane 3.77 0.10 mg/Kg wet 5.00 75.4 40-140 13.1 25 n-Hexacosane 3.62 0.10 mg/Kg wet 5.00 72.4 40-140 10.3 25 n-Hexadecane 3.16 0.10 mg/Kg wet 5.00 63.2 40-140 9.54 25 n-Hexatriacontane 3.56 0.10 mg/Kg wet 5.00 71.3 40-140 11.9 25 n-Nonadecane 3.38 0.10 mg/Kg wet 5.00 71.5 40-140 7.03 25 n-Nonane 1.28 0.10 mg/Kg wet 5.00 25.6 * 30-140 40.9 * 25 L-07A n-Octacosane 3.54 0.10 mg/Kg wet 5.00 70.8 40-140 10.5 25 n-Octadecane 3.55 0.10 mg/Kg wet 5.00 71.0 40-140 3.19 25 n-Tetracosane 3.65 0.10 mg/Kg wet 5.00 72.9 40-140 9.98 25 n-Tetradecane 2.86 0.10 mg/Kg wet 5.00 57.3 40-140 16.0 25 n-Triacontane 3.37 0.10 mg/Kg wet 5.00 71.5 40-140 10.5 25 Naphthalene -aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 2-Methylnaphthalene-aliphatic fraction ND 0.10 mg/Kg wet 5.00 0-5 Surrogate: Chlorooctadecane (COD) 3.64 mg/Kg wet 5.15 70.6 40-140 Surrogate: o-Terphenyl (OTP) 3.55 mg/Kg wet 5.00 70.9 40-140 Surrogate:2-Bromonaphthalene 5.44 mg/Kg wet 5.00 109 40-140 Surrogate:2-Fluorobiphenyl 5.93 mg/Kg wet 5.00 119 40-140 Page 27 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216531 - MA VPH Blank (B216531-BLK1) Prepared: 11/06/18 Analyzed: 11/07/18 C5-C8 Aliphatics ND 10 mg/Kg wet C9-C12 Aliphatics ND 10 mg/Kg wet C9-C 10 Aromatics ND 10 mg/Kg wet Benzene ND 0.050 mg/Kg wet Butylcyclohexane ND 0.050 mg/Kg wet Decane ND 0.050 mg/Kg wet Ethylbenzene ND 0.050 mg/Kg wet Methyl tert-Butyl Ether (MTBE) ND 0.050 mg/Kg wet 2-Methylpentane ND 0.050 mg/Kg wet Naphthalene ND 0.50 mg/Kg wet Nonane ND 0.050 mg/Kg wet Pentane ND 0.050 mg/Kg wet Toluene ND 0.050 mg/Kg wet 1,2,4-Trimethylbenzene ND 0.050 mg/Kg wet 2,2,4-Trimethylpentane ND 0.050 mg/Kg wet m+p Xylene ND 0.10 mg/Kg wet o-Xylene ND 0.050 mg/Kg wet Surrogate:2,5-Dibromotoluene (FID) 41.1 µg/L 40.0 103 70-130 Surrogate:2,5-Dibromotoluene (PID) 37.9 µg/L 40.0 94.8 70-130 LCS (B216531-BS1) Prepared: 11/06/18 Analyzed: 11/07/18 C9-C 10 Aromatics 0.0700 0.20 mg/Kg wet 70-130 Benzene 0.0491 0.0010 mg/Kg wet 0.0500 98.3 70-130 Butylcyclohexane 0.0585 0.0010 mg/Kg wet 0.0500 117 70-130 Decane 0.0463 0.0010 mg/Kg wet 0.0500 92.6 70-130 Ethylbenzene 0.0499 0.0010 mg/Kg wet 0.0500 99.9 70-130 Methyl tert-Butyl Ether (MTBE) 0.0487 0.0010 mg/Kg wet 0.0500 97.5 70-130 2-Methylpentane 0.0548 0.0010 mg/Kgwet 0.0500 110 70-130 Naphthalene 0.0461 0.010 mg/Kg wet 0.0500 92.3 70-130 Nonane 0.0566 0.0010 mg/Kg wet 0.0500 113 30-130 Pentane 0.0530 0.0010 mg/Kg wet 0.0500 106 70-130 Toluene 0.0497 0.0010 mg/Kg wet 0.0500 99.5 70-130 1,2,4-Trimethylbenzene 0.0508 0.0010 mg/Kg wet 0.0500 102 70-130 2,2,4-Trimethylpentane 0.0524 0.0010 mg/Kg wet 0.0500 105 70-130 m+p Xylene 0.101 0.0020 mg/Kg wet 0.100 101 70-130 o-Xylene 0.0502 0.0010 mg/Kg wet 0.0500 100 70-130 Surrogate: 2,5-Dibromotoluene (FID) 41.8 µg/L 40.0 107 70-130 Surrogate:2,5-Dibromotoluene (PID) 41.9 µg/L 40.0 105 70-130 LCS Dup (B216531-BSD1) Prepared: 11/06/18 Analyzed: 11/07/18 C9-C 10 Aromatics 0.0692 0.20 mg/Kg wet 70-130 1.25 Benzene 0.0495 0.0010 mg/Kg wet 0.0500 99.0 70-130 0.698 Butylcyclohexane 0.0572 0.0010 mg/Kg wet 0.0500 114 70-130 2.23 Decane 0.0451 0.0010 mg/Kg wet 0.0500 90.2 70-130 2.55 Ethylbenzene 0.0504 0.0010 mg/Kg wet 0.0500 101 70-130 0.833 Methyl tert-Butyl Ether (MTBE) 0.0488 0.0010 mg/Kg wet 0.0500 97.6 70-130 0.195 2-Methylpentane 0.0555 0.0010 mg/Kg wet 0.0500 ill 70-130 1.22 Naphthalene 0.0455 0.010 mg/Kg wet 0.0500 91.1 70-130 1.32 Nonane 0.0560 0.0010 mg/Kg wet 0.0500 112 30-130 1.12 Pentane 0.0522 0.0010 mg/Kg wet 0.0500 104 70-130 1.51 Toluene 0.0500 0.0010 mg/Kg wet 0.0500 100 70-130 0.515 1,2,4-Trimethylbenzene 0.0508 0.0010 mg/Kg wet 0.0500 102 70-130 0.0315 25 25 25 25 25 25 25 25 25 25 25 25 Page 28 of 39 Table of Contents ,con -testy ANALYTICAL LABORATORY 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 QUALITY CONTROL Petroleum Hydrocarbons Analyses - VPH - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch B216531 - MA VPH LCS Dup (B216531-BSD1) Prepared: 11/06/18 Analyzed: 11/07/18 2,2,4-Trimethylpentane 0.0519 0.0010 mg/Kg wet 0.0500 104 70-130 0.859 25 m+p Xylene 0.102 0.0020 mg/Kg wet 0.100 102 70-130 0.442 25 o-Xylene 0.0505 0.0010 mg/Kg wet 0.0500 101 70-130 0.544 25 Surrogate:2,5-Dibromotoluene (FID) 42.2 µg/L 40.0 106 70-130 Surrogate:2,5-Dibromotoluene (PID) 40.9 µg/L 40.0 102 70-130 Page 29 of 39 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332 FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. fi Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level ND Not Detected RL Reporting Limit is at the level of quantitation (LOQ) DL Detection Limit is the lower limit of detection determined by the MDL study MCL Maximum Contaminant Level Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. No results have been blank subtracted unless specified in the case narrative section. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this compound is likely to be biased on the low side. L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD between the two LFB/LCS results is within method specified criteria. L-07A Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for this compound. R-05 Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this compound. V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound. V-06 Continuing calibration did not meet method specifications and was biased on the high side for this compound V-19 Initial calibration did not meet method specifications. Compound was calibrated using linear regression with correlation coefficient <0.99. Reported result is estimated. V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is estimated. Page 30 of 39 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications MADEP-EPH-04-1.1 in Soil C9-C18 Aliphatics CT,NC,ME,NH-P C19-06 Aliphatics CT,NC,ME,NH-P C11-C22 Aromatics CT,NC,ME,NH-P Acenaphthene CT,NC,ME,NH-P Acenaphthylene CT,NC,ME,NH-P Anthracene CT,NC,ME,NH-P Benzo(a)anthracene CT,NC,ME,NH-P Benzo(a)pyrene CT,NC,ME,NH-P Benzo(b)fluoranthene CT,NC,ME,NH-P Benzo(g,h,i)perylene CT,NC,ME,NH-P Benzo(k)fluoranthene CT,NC,ME,NH-P Chrysene CT,NC,ME,NH-P Dibenz(a,h)anthracene CT,NC,ME,NH-P Fluoranthene CT,NC,ME,NH-P Fluorene CT,NC,ME Indeno(1,2,3-cd)pyrene CT,NC,ME,NH-P 2-Methylnaphthalene CT,NC,ME Naphthalene CT,NC,ME,NH-P Phenanthrene CT,NC,ME,NH-P Pyrene CT,NC,ME,NH-P MADEP-VPH-Feb 1018 Rev 1.1 in Soil C5-C8 Aliphatics CT,NC,ME,NH-P C9-C12 Aliphatics CT,NC,ME,NH-P C9-C10 Aromatics CT,NC,ME,NH-P Benzene CT,NC,ME,NH-P Ethylbenzene CT,NC,ME,NH-P Methyl tert-Butyl Ether (MTBE) CT,NC,ME,NH-P Naphthalene CT,NC,ME,NH-P Toluene CT,NC,ME,NH-P m+p Xylene CT,NC,ME,NH-P o-Xylene CT,NC,ME,NH-P SW-846 8260B in Soil Acetone NC Acrylonitrile NC tert-Amyl Methyl Ether (TAME) NC Benzene NC Bromobenzene NC Bromochloromethane NC Bromodichloromethane NC Bromoform NC Bromomethane NC 2-Butanone (MEK) NC tert-Butyl Alcohol (TBA) NC n-Butylbenzene NC sec-Butylbenzene NC tert-Butylbenzene NC Page 31 of 39 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8260B in Soil tert-Butyl Ethyl Ether (TBEE) NC Carbon Disulfide NC Carbon Tetrachloride NC Chlorobenzene NC Chlorodibromomethane NC Chloroethane NC Chloroform NC Chloromethane NC 2-Chlorotoluene NC 4-Chlorotoluene NC 1,2-Dibromo-3-chloropropane (DBCP) NC 1,2-Dibromoethane (EDB) NC Dibromomethane NC 1,2-Dichlorobenzene NC 1,3-Dichlorobenzene NC 1,4-Dichlorobenzene NC trans-1,4-Dichloro-2-butene NC Dichlorodifluoromethane (Freon 12) NC 1,1-Dichloroethane NC 1,2-Dichloroethane NC 1,1-Dichloroethylene NC cis-1,2-Dichloroethylene NC trans-1,2-Dichloroethylene NC 1,2-Dichloropropane NC 1,3-Dichloropropane NC 2,2-Dichloropropane NC 1,1-Dichloropropene NC cis- 1,3 -Dichloropropene NC trans- l,3-Dichloropropene NC Diethyl Ether NC Diisopropyl Ether (DIPE) NC 1,4-Dioxane NC Ethylbenzene NC Hexachlombutadiene NC 2-Hexanone (MBK) NC Isopropylbenzene (Cumene) NC p-Isopropyltoluene (p-Cymene) NC Methyl tert-Butyl Ether (MTBE) NC Methylene Chloride NC 4-Methyl-2-pentanone (MIBK) NC Naphthalene NC n-Propylbenzene NC Styrene NC 1, 1, 1,2-Tetrachloroethane NC 1,1,2,2-Tetrachloroethane NC Tetrachloroethylene NC Tetrahydrofuran NC Page 32 of 39 MN ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte SW-846 8260B in Soil Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,3,5-Trichlorobenzene 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichlorofluoromethane (Freon 11) 1,2,3-Trichloropropane 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Chloride m+p Xylene o-Xylene SW-846 8270D in Soil Acenaphthene Acenaphthylene Acetophenone Aniline Anthracene Benzidine Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid B is(2-chloroethoxy)methane Bis(2-chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phthalate 4-Bromophenylphenylether Butylbenzylphthalate Carbazole 4-Chloroaniline 4-Chloro-3-methylphenol 2-Chloronaphthalene 2-Chlorophenol 4-Chlorophenylphenylether Chrysene Dibenz(a,h)anthracene Dibenzofuran Di-n-butylphthalate 1,2-Dichlorobenzene 1,3-Dichlorobenzene Certifications NC NC NC NC NC NC NC NC NC NC NC NC NC NC NC CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA NY,NH,ME,NC,VA NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA NC CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA CT,NY,NH,ME,NC,VA NY,NH,ME,NC,VA NY,NH,ME,NC,VA Page 33 of 39 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Soil 1,4-Dichlorobenzene NY,NH,ME,NC,VA 3,3-Dichlorobenzidine CT,NY,NH,ME,NC,VA 2,4-Dichlorophenol CT,NY,NH,ME,NC,VA Diethylphthalate CT,NY,NH,ME,NC,VA 2,4-Dimethylphenol CT,NY,NH,ME,NC,VA Dimethylphthalate CT,NY,NH,ME,NC,VA 4,6-Dinitro-2-methylphenol CT,NY,NH,ME,NC,VA 2,4-Dinitrophenol CT,NY,NH,ME,NC,VA 2,4-Dinitrotoluene CT,NY,NH,ME,NC,VA 2,6-Dinitrotoluene CT,NY,NH,ME,NC,VA Di-n-octylphthalate CT,NY,NH,ME,NC,VA 1,2-Diphenylhydrazine (as Azobenzene) NY,NH,ME,NC,VA Fluoranthene CT,NY,NH,ME,NC,VA Fluorene NY,NH,ME,NC,VA Hexachlorobenzene CT,NY,NH,ME,NC,VA Hexachlorobutadiene CT,NY,NH,ME,NC,VA Hexachlorocyclopentadiene CT,NY,NH,ME,NC,VA Hexachloroethane CT,NY,NH,ME,NC,VA Indeno(1,2,3-cd)pyrene CT,NY,NH,ME,NC,VA Isophorone CT,NY,NH,ME,NC,VA I -Methylnaphthalene NC 2-Methy1naphthalene CT,NY,NH,ME,NC,VA 2-Methylphenol CT,NY,NH,ME,NC,VA 3/4-Methylphenol CT,NY,NH,ME,NC,VA Naphthalene CT,NY,NH,ME,NC,VA 2-Nitroaniline CT,NY,NH,ME,NC,VA 3-Nitroaniline CT,NY,NH,ME,NC,VA 4-Nitroaniline CT,NY,NH,ME,NC,VA Nitrobenzene CT,NY,NH,ME,NC,VA 2-Nitrophenol CT,NY,NH,ME,NC,VA 4-Nitrophenol CT,NY,NH,ME,NC,VA N-Nitrosodimethylamine CT,NY,NH,ME,NC,VA N-Nitrosodiphenylamine CT,NY,NH,ME,NC,VA N-Nitrosodi-n-propylamine CT,NY,NH,ME,NC,VA Pentachloronitrobenzene NY,NC Pentachlorophenol CT,NY,NH,ME,NC,VA Phenanthrene CT,NY,NH,ME,NC,VA Phenol CT,NY,NH,ME,NC,VA Pyrene CT,NY,NH,ME,NC,VA Pyridine CT,NY,NH,ME,NC,VA 1,2,4,5-Tetrachlorobenzene NY,NC 1,2,4-Trichlorobenzene CT,NY,NH,ME,NC,VA 2,4,5-Trichlorophenol CT,NY,NH,ME,NC,VA 2,4,6-Trichlorophenol CT,NY,NH,ME,NC,VA 2-Fluorophenol NC SW-846 8270D in Water Page 34 of 39 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Water Acenaphthene CT,NY,NC,ME,NH,VA Acenaphthylene CT,NY,NC,ME,NH,VA Acetophenone NY,NC Aniline CT,NY,NC,ME,VA Anthracene CT,NY,NC,ME,NH,VA Benzidine CT,NY,NC,ME,NH,VA Benzo(a)anthracene CT,NY,NC,ME,NH,VA Benzo(a)pyrene CT,NY,NC,ME,NH,VA Benzo(b)fluoranthene CT,NY,NC,ME,NH,VA Benzo(g,h,i)perylene CT,NY,NC,ME,NH,VA Benzo(k)fluoranthene CT,NY,NC,ME,NH,VA Benzoic Acid NY,NC,ME,NH,VA Bis(2-chloroethoxy)methane CT,NY,NC,ME,NH,VA Bis(2-chloroethyl)ether CT,NY,NC,ME,NH,VA Bis(2-chloroisopropyl)ether CT,NY,NC,ME,NH,VA Bis(2-Ethylhexyl)phthalate CT,NY,NC,ME,NH,VA 4-Bromophenylphenylether CT,NY,NC,ME,NH,VA Butylbenzylphthalate CT,NY,NC,ME,NH,VA Carbazole NC 4-Chloroaniline CT,NY,NC,ME,NH,VA 4-Chloro-3-methylphenol CT,NY,NC,ME,NH,VA 2-Chloronaphthalene CT,NY,NC,ME,NH,VA 2-Chlorophenol CT,NY NC,ME,NH,VA 4-Chlorophenylphenylether CT,NY NC,ME,NH,VA Chrysene CT,NY,NC,ME,NH,VA Dibenz(a,h)anthracene CT,NY,NC,ME,NH,VA Dibenzofuran CT,NY,NC,ME,NH,VA Di-n-butylphthalate CT,NY,NC,ME,NH,VA 1,2-Dichlorobenzene CT,NY,NC,ME,NH,VA 1,3-Dichlorobenzene CT,NY,NC,ME,NH,VA 1,4-Dichlorobenzene CT,NY,NC,ME,NH,VA 3,3-Dichlorobenzidine CT,NY,NC,ME,NH,VA 2,4-Dichlorophenol CT,NY,NC,ME,NH,VA Diethylphthalate CT,NY,NC,ME,NH,VA 2,4-Dimethylphenol CT,NY,NC,ME,NH,VA Dimethylphthalate CT,NY,NC,ME,NH,VA 4,6-Dinitro-2-methylphenol CT,NY,NC,ME,NH,VA 2,4-Dinitrophenol CT,NY,NC,ME,NH,VA 2,4-Dinitrotoluene CT,NY,NC,ME,NH,VA 2,6-Dinitrotoluene CT,NY,NC,ME,NH,VA Di-n-octylphthalate CT,NY,NC,ME,NH,VA 1,2-Diphenylhydrazine (as Azobenzene) NY,NC Fluoranthene CT,NY,NC,ME,NH,VA Fluorene NY,NC,ME,NH,VA Hexachlorobenzene CT,NY,NC,ME,NH,VA Hexachlorobutadiene CT,NY,NC,ME,NH,VA Hexachlorocyclopentadiene CT,NY,NC,ME,NH,VA Page 35 of 39 ,con -testy ANALYTICAL LABORATORY Table of Contents 39 Spruce Street' East Longmeadow, MA 01028 . FAX 413/525-6405 ` TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte Certifications SW-846 8270D in Water Hexachlomethane CT,NY,NC,ME,NH,VA Indeno(1,2,3-cd)pyrene CT,NY,NC,ME,NH,VA Isophorone CT,NY,NC,ME,NH,VA 1-Methylnaphthalene NC 2-Methylnaphthalene CT,NY,NC,ME,NH,VA 2-Methylphenol CT,NY,NC,NH,VA 3/4-Methylphenol CT,NY,NC,NH,VA Naphthalene CT,NY,NC,ME,NH,VA 2-Nitmaniline CT,NY,NC,ME,NH,VA 3-Nitroaniline CT,NY,NC,ME,NH,VA 4-Nitroaniline CT,NY,NC,ME,NH,VA Nitrobenzene CT,NY,NC,ME,NH,VA 2-Nitrophenol CT,NY,NC,ME,NH,VA 4-Nitrophenol CT,NY,NC,ME,NH,VA N-Nitrosodimethylamine CT,NY,NC,ME,NH,VA N-Nitrosodiphenylamine CT,NY,NC,ME,NH,VA N-Nitrosodi-n-propylamine CT,NY,NC,ME,NH,VA Pentachloronitrobenzene NC Pentachlorophenol CT,NY,NC,ME,NH,VA Phenanthrene CT,NY,NC,ME,NH,VA Phenol CT,NY,NC,ME,NH,VA Pyrene CT,NY,NC,ME,NH,VA Pyridine CT,NY,NC,ME,NH,VA 1,2,4,5-Tetrachlorobenzene NY,NC 1,2,4-Trichlorobenzene CT,NY,NC,ME,NH,VA 2,4,5-Trichlorophenol CT,NY,NC,ME,NH,VA 2,4,6-Trichlorophenol CT,NY,NC,ME,NH,VA 2-Fluorophenol NC The CON -TEST Environmental Laboratory operates under the following certifications and accreditations: Code Description Number Expires AIHA AIHA-LAP, LLC - ISO17025:2005 100033 03/l/2020 MA Massachusetts DEP M-MA100 06/30/2019 CT Connecticut Department of Publilc Health PH-0567 09/30/2019 NY New York State Department of Health 10899 NELAP 04/1/2019 NH-S New Hampshire Environmental Lab 2516 NELAP 02/5/2019 RI Rhode Island Department of Health LA000112 12/30/2018 NC North Carolina Div. of Water Quality 652 12/31/2018 NJ New Jersey DEP MA007 NELAP 06/30/2019 FL Florida Department of Health E871027 NELAP 06/30/2019 VT Vermont Department of Health Lead Laboratory LL015036 07/30/2019 ME State of Maine 2011028 06/9/2019 VA Commonwealth of Virginia 460217 12/14/2018 NH-P New Hampshire Environmental Lab 2557 NELAP 09/6/2019 VT-DW Vermont Department of Health Drinking Water VT-255716 06/12/2019 NC-DW North Carolina Department of Health 25703 07/31/2019 Page 36 of 39 Table of Contents a d;m `� x o�Y z� w CL UEEE° c�m� a X "p .: co t.,., L -� O G7 Ci C] L_ - = O A� iv f-3 �_ .� _7 W N 'O >-< �' T7 T:1 T) C 'U sn ,�,� L E 1f5 ,py -`. j .d7' n7 a-+ tC .5= �-� ( + — Q1 +-' Q,3 L7. n :n G Z o if v} If m I€ tl ¢ n II O aY N 7 O q C7 O Q7 U S rn to to cA NO o c — c/j -� O Q3 1I[ C ¢ C7 a It 7 cn 1- O_ c }j It li Q II ' ii it !€ 7E -II ]y 3i II !E II 14 1[ I[ I7 I! Il .- C7 Gl¢yNNQ't7 :v ....i �NaiX -CDT m c[C9bVI> ❑ ®■ N <r vi O o E u. Q R 0 ? nv 2 a n 9 E != R .. O C C O 7 w - E E E E E C ' s Q � C r, Page 37 of 39 1112/2018 Track your package or shipment with FedEx Tracking Table of Contents 773629234379 Delivered Friday 11/02/2018 at 9:1 1 am DELIVERED Signed for by: B.BECCA GET STATUS UPDATES OBTAIN PROOF OF DELIVERY FROM To Charfotie, NC US EAST I.ONGV EADOW, MA US Multiple -piece Shipment 8 Piece shipment TRACKING NUMBER . SHIPPER CITY, STATE SHIP DATE STATUS DELIVERY DATE CITY, S AT] ONIREClPIENT CITY, STATIr 773629234287 CHARLOTTE, NO 11/01/2018 11/02/2018 EAST LONGMEADOW, MA (master) 773629233269 CHARLOTTE, NC 11/U1/2018 11/02/2018 EAST LONGMEADOW, MA 773629233637 CHARLOTTE, NC 11/U1/2018 11/02/2018 EAST LONGMEADOW, MA 773629234195 CHARLOTTE, NC 11/01/2018 11/02/2018 EAST LONGMLADOW, MA 773629234379 CHARLOTTE, NO 11/01/2018 11/02/2018 EAST LONGMEADOW, MA 773629234380 CHARLOTTE, NC 11/01/2018 11/02/2018 EAST LONGMEADOW, MA 773629234427 CHARLOTTE, NC 11/01/2018 11/02/2018 EAST LONGMEADOW, MA 773629234493 CHARLOTTE, NO 1W01/2018 11/02/2018 EAST LONGMEADOW, MA Shipment Facts https:llwww.fedex.comlappslfedextrackl?action=track&tracknurnbers=773629234379&locale=en_US&cntry_code=us Page 38 of 39 Table of Contents Received By How were the samples received? Date 1! In Cooler -7— No Cooler Direct from Sampling Time On Ice 1 Ambient RI No Ice Melted Ice Were samples within By Gun # Actual Temp - . Temperature? 2-6°C T By Blank # Actual Temp - Was Custody Sea] Intact? Aiy: - Were Samples Tampered with? Was COC Relinquished ? T Does Chain Agree With Samples? �— Are there broken/leaking/loose caps on any samples? I^ Is COC in inkl Legible? i— Did COC include all Client i pertinent Information? Project S Are Sample labels filled out and legible? 7— Are there Lab to Filters? Are there Rushes? _ �= Are there Short Holds? Is there enough Volume? T Is there Headspace where applicable? Proper Media/Containers Used? Were trip blanks received? Do all samples have the proper pH? 1 V - Were samples received within holding time? S Analysis f Sampler Name ID`s r{- Collection Dates/Times i Who was notified? Who was notified? Who was notified? MS/MSD? Is splitting samples required? On COC? Acid Base Beverly, Trudy From: McDorman, James <James.McDorman@cltairport.com> Sent: Tuesday, March 26, 2019 8:42 AM To: Beverly, Trudy Cc: Foster, Rob Subject: [External] CLT-Former GADO Building • I email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to �Wort.spam@nc.gov Good morning Trudy, Our consultant, Wood Environment & Infrastructure Solutions (Wood), submitted an Initial Abatement Action Report (IAAR) back in November 2018. The IAAR was for an UST permanent closure, impacted soil excavation and disposal. Checking in to see if you have any questions or require additional information concerning the IAAR. Thank you, JAMES P MCDORMAN P.G. I ENVIRONMENTAL COMPLIANCE COORDINATOR CHARLOTTE DOUGLAS INTERNATIONAL AIRPORT m 704-560-9242 cltairport.com Charlotte Douglas International Airport (CLT), a City of Charlotte department, welcomes more than 46 million passengers annually. CLT is ranked among the top 10 busiest airports in the world, averaging 1,400 daily aircraft operations. (ACI 2018 Preliminary rankings) CLT is served by seven major carriers, 15 regional carriers and three foreign flag carriers with nonstop service to 174 destinations, including 36 international locations and 3 US territories. (CLT Fast Facts) Beverly, Trudy From: Sent: To: Beverly, Trudy Tuesday, December 11, 2018 9:58 AM 'Foster, Rob' Subject: RE: [External] GADO building Initial Abatement Action Report Hey Rob, Yes, the report was received on December 7tn Trudy er-a D� E Q7> u.pr.�r+rt n �rw�eMwnr� uwiih� Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environment Quality Underground Storage Tanks Section Corrective Action Branch Mooresville Regional Office (704) 235-2182 (Office) Trudv.Beve rlv(@ncdenr.gov Err Y mmwOvve to aW from this addre55 +s subject to the h+o h Caidffa P)bkc Reco Fds Law aril may be dwk.)sed to third part+es- Branch's Underground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste- management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: https://deg.nc.gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-maps File Review Procedures: https://deg.nc.gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): https://edocs.deg.nc.gov/WasteManagement/Search.aspx Document Submittal & UST File Names for Laserfiche Policies: https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%20Action/Electronic%20Document%20Submi ttal%20Memo%20Update. pdf https://files.nc.gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%2Ofile%20names%20for%20 Laserfiche.docx From: Foster, Rob [mailto:rob.foster@woodplc.com] Sent: Tuesday, December 11, 2018 9:55 AM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Subject: [External] GADO building Initial Abatement Action Report 0 External email. Do not click links or open attachments unless verified. Send all suspicious email as an attachment to Trudy, We recently submitted by regular mail the report described above. I just wanted to verify you rec'd it. Rob Foster Rob Foster, LG Associate Geologist — Charlotte, North Carolina Environment & Infrastructure Solutions Direct: +1 (704) 357-5530 Mobile: +1 (704) 641-1141 VoIP: #711-5530 Rob.foster(aD_woodplc.com www.woodplc.com wood This message is the property of John Wood Group PLC and/or its subsidiaries and/or affiliates and is intended only for the named recipient(s). Its contents (including any attachments) may be confidential, legally privileged or otherwise protected from disclosure by law. Unauthorized use, copying, distribution or disclosure of any of it may be unlawful and is strictly prohibited. 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