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6013_GreenwayNorthMeckCDLF_20190315_GWMonReport_FID1286609
SPRING 2018 SEMI-ANNUAL WATER QUALITY MONITORING REPORT CLOSED PHASE I C&D LANDFILL AREA GREENWAY WASTE SOLUTIONS AT NORTH MECK, LLC (FORMERLY NORTH MECKLENBURG C&D LANDFILL) 15300 HOLBROOKS ROAD HUNTERSVILLE, NORTH CAROLINA SOLID WASTE FACILITY PERMIT NO.60-13 Prepared For: GREENWAY WASTE SOLUTIONS AT NORTH MECK, LLC 19109 W. CATAWBA AVENUE CORNELIUS, NORTH CAROLINA 28031=5611 Prepared By: CIVIL &ENVIRONMENTAL CONSULTANTS, INC. 1900 CENTER PARK DRIVE, SUITE A CHARLOTTE NORTH CAROLINA 28217 �EC Project No. 111-370.001 July 16, 2018 Donald M. Cobb, P.G. Project Manager Scott L. Brown, P.E. Vice President ConSUItants, Inc. t,..a - ' � I900 Center Park Drive, Suite A I CNarbtte, NC 28217 � p: 980-224-6104 f: 980-224-8172 www.cecinc,com TABLE OF CONTENTS 1.0 PURPOSE...........................................................................................................................I 2.0 SITE DESCRIPTION AND BACKGROUND................................................................2 3.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES...............................................4 3.1 Well Water Level Gauging..................................................................................... 4 3.2 Well Purging........................................................................................................... 4 3.3 Groundwater Sample Collection............................................................................. 5 4.0 GROUNDWATER FLOW EVALUATION...................................................................6 5.0 WATER SAMPLE ANALYTICAL PARAMETERS....................................................7 6.0 SAMPLE ANALYTICAL DATA EVALUATION.........................................................8 6.1 Organic Analytes Detected at Concentrations Exceeding the 2L Standards .......... 8 6.2 Metal Analytes Detected at Concentrations Exceeding the 2L Standards .............. 9 6.3 Inorganic Leachate Indicator Parameters................................................................ 9 7.0 CONCLUSIONS AND RECOMMENDATIONS.........................................................10 7.1 Conclusions...........................................................................................................10 10.2 Recommendations.................................................................................................11 LIST OF FIGURES Figure 1 — Site Location Map Figure 2 — Site Map Figure 3 — Groundwater Potentiometric Map Figure 4 — Landfill Gas Extract System LIST OF TABLES Table 1 — History of Water Level Gauging Data and Well Construction Details Table 2 — Summary of Recent Site Groundwater Analytical Detections Table 3 — History of Site Groundwater Analytical Detections Table 4 - Summary of Vertical Hydraulic Gradients LIST OF APPENDICES Appendix A — Groundwater Sampling Field Logs Appendix B - Laboratory Analytical Data Reports Civil & Environmental Consultants, Inc. -i- Spring 2018 Water Quality Monitoring Report 1.0 PURPOSE On behalf of Greenway Waste Solutions at North Meck, LLC, Civil & Environmental Consultants, Inc. (CEC) has prepared this Spring 2018 Semi -Annual Water Quality Monitoring Report for the Closed Phase I Area at the subject landfill facility. This report describes the well gauging and field sampling activities, and provides a summary of the site groundwater conditions and acquired groundwater sample data. Civil & Environmental Consultants, Inc. _1- Spring 2018 Water Quality Monitoring Report 2.0 SITE DESCRIPTION AND BACKGROUND Greenway Waste Solutions at North Meek, LLC (GWS) operates the subject landfill under Solid Waste Facility Permit Number 60-13. The facility address is 15300 Holbrooks Road, Huntersville, North Carolina. The Closed Phase I C&D disposal area (Closed Phase I Area) is located in the southern portion of the site and is bounded by an unnamed tributary of Cane Creek to the north with other landfill disposal areas further to the north, private property to the west, and land owned by Mecklenburg County to the east. Adjacent land parcels to the south and southeast of the Closed Phase I Area are developed with single-family residences. Some adjacent parcels to the south and southeast have been purchased by GWS. Cane Creek lies south and southeast of the adjacent private properties on the south side of the closed landfill. The Closed Phase I Area comprises approximately 23.3 acres. Waste placement in this disposal area generally occurred during the years 1993 to 2002. It has been reported that the eastern and southern margins of this disposal area contain buried land -clearing debris approximately 30-40 feet wide and 20-30 feet deep. A Site Map is attached as Figure 1. Routine semi-annual groundwater monitoring has been conducted at the landfill since June 1996. The approximate locations of monitoring wells are shown on Figure 2. During the October 2012 monitoring event, VOCs were reported at concentrations exceeding the groundwater quality standards as defined by Title 15A North Carolina Administrative Code Subchapter 02L Groundwater Classifications and Standards (2L Standards) in MW-5. On a more consistent basis and concurrent with a change in the laboratory services provider (from Pace Analytical Services, Inc. to Shealy Environmental Services, Inc.) as of the April 2013 and for subsequent semi-annual monitoring events, VOCs (particularly vinyl chloride) were being reported in several detection well samples at concentrations exceeding the 2L Standards. As a consequence, the North Carolina Department of Environmental Quality (NCDEQ) — Solid Waste Section (SWS) required the permittee to implement a program of groundwater assessment monitoring and to perform a contaminant delineation investigation. Due to the proximity of a few private residential water supply wells (now inactive) downgradient of the landfill area, samples were collected from these wells. VOCs reported in the landfill Civil & Environmental Consultants, Inc. -2- Spring 2018 Water Quality Monitoring Report monitoring wells were also reported in the former Gilkerson residence well. The Gilkerson and other neighboring water supply wells were made inactive and these residences connected to a public water supply. GWS has purchased the former Gilkerson and Wright parcels. Civil & Environmental Consultants, Inc. -3- Spring 2018 Water Quality Monitoring Report 3.0 DESCRIPTION OF FIELD SAMPLING ACTIVITIES Field activities associated with the Spring 2018 semi-annual groundwater monitoring were conducted by CEC personnel from April 9 — 12, 2018. Project oversight was provided by an NC - licensed geologist. Well water levels were gauged, static well water was purged, and groundwater samples were collected from 23 monitoring wells including shallow wells MW-1, MW-4, MW- 4A, MW-5, MW-6, MW-7A, MW-8, MW-9, MW-10, MW-I IA, and MW-11B, and deeper wells MW-4D, MW-4D-1, MW-5D, MW-6D, MW-6D-1, MW-7, MW-7D, MW-8D, MW-10D, MW- 11, MW-11D-1, and MW-11D-2. MW-8 was not sampled for metals at this time; refer to Section 3.3 for further discussion. Also, groundwater samples were collected from three off -site inactive private water supply wells (former Gilkerson, Hammill, and Tinsley residential wells) situated adjacent to the southern perimeter of the Closed Phase I Area. The approximate locations of these monitoring points are shown on Figure 2. 3.1 WELL WATER LEVEL GAUGING Prior to well purging/sampling, the water level in each monitoring well was gauged using an electronic water level meter. The depth -to -groundwater was measured from a reference point on the top -of -casing and was recorded to the nearest 0.01-inch on the well sampling field log (see Appendix A). The water level probe was decontaminated between well measurements. 3.2 WELL PURGING To minimize sampling artifacts and validate certain metals and inorganic parameter data, CEC carefully monitored turbidity in the site monitoring wells during the well purge process. CEC made an effort to minimize turbidity prior to collecting well samples. Where the water table was shallow a peristaltic pump was utilized to purge the well at a low -flow rate until targeted analytical parameters were found to stabilize. During the well purge, specific conductance, pH, dissolved oxygen, turbidity and oxidation-reduction potential were frequently Civil & Environmental Consultants, Inc. -4- Spring 2018 Water Quality Monitoring Report measured with a YSI 556 Water Quality Meter in a flow -through cell to observe and document the chemical stability of the formation water entering the monitoring well. When parameter values indicated stable water chemistry as defined by USEPA Groundwater Sampling Guidelines for Superfund and RCRA Project Managers (EPA 542-S-02-001, May 2002), the well purge was considered complete and groundwater samples were then collected. Well purge data were recorded on the well sampling field logs provided in Appendix A. Where the water table was too deep to effectively use a low -flow peristaltic pump, a clean Monsoon submersible pump was employed to purge wells MW-4, MW-4A, MW-4D, MW-4D-1, MW-6, MW-6D, MW-6D-1, MW-7, MW-7A, MW-7D, , MW-8D, MW-IOD, and MW-I I until targeted analytical parameters stabilized. The submersible pump intake was maintained above each well screen provided that the well was adequately recharged during the well purge. The pump was decontaminated after every use and new tubing was attached for each well. 3.3 GROUNDWATER SAMPLE COLLECTION Following the above -described well purging procedures, groundwater samples were collected from each well employing either the same low -flow pumping protocols for the shallow wells or utilizing a submersible pump. Groundwater samples were collected in laboratory -supplied sample containers that were labeled and packed on ice in insulated coolers, which were then shipped overnight by FedEx to the selected analytical laboratory under chain -of -custody protocol. Due to high turbidity, monitoring well MW-8 was not sampled for metals during the initial round of water quality monitoring. This well is part of a Metals Alternative Source Demonstration currently ongoing at the site. As such, turbidity must be below 10 NTUs prior to sampling for metals. Elite Drilling attempted to redevelop MW-8 on June 7, 2018 but due to very high turbidity and slow recharge, the well was not successfully redeveloped. MW-8 will be replaced prior to the next sampling event in October 2018. Civil & Environmental Consultants, Inc. -5- Spring 2018 Water Quality Monitoring Report 4.0 GROUNDWATER FLOW EVALUATION A depth -to -water level measurement was performed relative to the top -of -well casing in each groundwater monitoring well prior to well purging. A water level elevation was calculated by subtracting the depth -to -water from the respective surveyed top -of -well casing elevation datum. Monitoring well gauging data are summarized in Table 1. Calculated water table elevations were used to prepare the Spring 2018 groundwater potentiometric map presented in Figure 3. Shallow groundwater movement across the Closed Phase I Area is radial; northward toward the tributary creek situated to the north and eastward or southward toward Cane Creek situated to the south. The "V"-shaped potentiometric contours in the vicinity of the tributary creek are indicative of shallow groundwater discharge from the Closed Phase I Area as well as from the adjacent Infill Area situated on the north side of the tributary creek. An upward vertical gradient was calculated for well clusters MW-5/5D and MW-10/10D located south of the tributary creek indicating groundwater recharge to the tributary in this site area. Also, upward vertical hydraulic gradients were calculated for well clusters MW-4A/4D and MW-8/8D that are located in the southern half of the Closed Phase I Area in the vicinity of Cane Creek. These data indicate local groundwater recharge to Cane Creek. A downward vertical gradient was determined for MW-7A/7D, located at the southeastern perimeter of the landfill and approximately 300 feet from Cane Creek. A downward vertical gradient was calculated for well clusters MW-11A/11D-1 and MW-11B/11D-2, which are located on the eastern perimeter of the Closed Phase I Area, upgradient from Cane Creek. A summary table for vertical hydraulic gradients is presented in Table 4. Civil & Environmental Consultants, Inc. -6- Spring 2018 Water Quality Monitoring Report 5.0 WATER SAMPLE ANALYTICAL PARAMETERS For the routine Spring 2018 semi-annual monitoring event, groundwater samples were collected from 23 monitoring wells and three water supply wells that were submitted to TestAmerica laboratory for analytical testing for the following parameters: Appendix I Volatile Organic Compounds (VOCs) plus Tetrahydrofuran (THF) [EPA 826013] Appendix I Metals [EPA 200.8] Monitoring well samples were also tested for leachate indicator parameters including the following list: Alkalinity [SM2320B] Manganese [EPA 200.8] Mercury [EPA 245.1 ] Sulfate [EPA 9056A] Calcium [EPA 200.8] Chloride [9056A] Iron [EPA 200.8] Total Dissolved Solids (TDS) [SM2540C] A quality control trip blank was analyzed for Appendix I VOCs plus tetrahydrofuran. In addition to routine semi-annual sample collection at the Closed Phase I Area, CEC personnel collected a split sample from well MW-5D that was submitted to Pace for VOC analyses. Civil & Environmental Consultants, Inc. -7- Spring 2018 Water Quality Monitoring Report 6.0 SAMPLE ANALYTICAL DATA EVALUATION Laboratory analytical data reports for the Spring 2018 semi-annual monitoring event are provided in Appendix B. Summaries of Appendix I VOCs, Appendix I metals, and inorganic analytes detected in the collected water samples at concentrations above their respective laboratory reporting limits are provided in Table 2. A historical summary of analytes detected in groundwater samples at concentrations above their respective laboratory reporting limits are provided in Table 3. 6.1 ORGANIC ANALYTES DETECTED AT CONCENTRATIONS EXCEEDING THE 2L STANDARDS For the Spring 2018 monitoring event, VC was detected at 1.7 µg/L in interior well MW-5, above the 2L Standard of 0.03 µg/L. Benzene was detected at 3.3 µg/L in interior well MW-IOD, above the 2L Standard of 1.0 µg/L. The sampled inactive water supply wells are located off -site to the south and southeast of the Closed Phase I Area. Trihalomethanes, including bromodichloromethane and dibromochloromethane, were detected in both the inactive Gilkerson and Tinsley supply wells at concentrations exceeding their 2L Standards. These compounds are commonly formed at relative low concentrations as a by-product of treating water with chlorine -based disinfectants and subsequent interaction with natural organics present in the water. Trihalomethanes have not been typically detected in the on -site groundwater samples. Tetrahydrofuran (THF) was detected at 12 µg/L in the Hammill well sample. Although the North Carolina Occupational and Environmental Epidemiology Branch previously established a health - based standard for THE of 700 µg/L, there is currently no 2L Standard due to the lack of historical toxicological data necessary to promulgate regulatory standards. THE was previously detected at 230 µg/L in the Hammill well sample in Fall 2017. Civil & Environmental Consultants, Inc. -8- Spring 2018 Water Quality Monitoring Report 6.2 METAL ANALYTES DETECTED AT CONCENTRATIONS EXCEEDING THE 2L STANDARDS As highlighted in Table 2, the laboratory test results for the monitoring event show that iron and manganese exceed the 2L Standards in the majority of the landfill monitoring well samples. Iron and manganese are naturally occurring metals in the local formation and can occur at elevated levels in reducing groundwater conditions such as those encountered at the subject landfill. Chromium, cobalt and vanadium were detected in several wells at concentrations exceeding their respective 2L Standards; however, the detected range of these analyte concentrations appears to be well within their naturally occurring levels. In MW-6, which is located on the eastern perimeter of the landfill, a number of metals were detected above their respective 2L standards; although periodically detected in the past, most such detections were below the 2L standards. Metals detected in exceedance of the standards include arsenic, barium, beryllium, cadmium, lead, as well as metals seen throughout the landfill like chromium, cobalt, manganese, vanadium and iron. 6.3 INORGANIC LEACHATE INDICATOR PARAMETERS The detections of inorganic parameters are summarized in Table 2. The levels of total dissolved solids (TDS) exceeded its 2L Standard of 500,000 µg/L in wells MW-5, MW-51), MW-6, MW- 61), MW-6D-1, MW-7, MW-81), MW-10, MW-IOD, MW-11 and the Hammill WSW. Chloride appears to be elevated in the majority of wells, and Sulfate exceeds the 2L standard of 250 mg/L in the Hammill WSW. Civil & Environmental Consultants, Inc. -9- Spring 2018 Water Quality Monitoring Report 7,0 CONCLUSIONS AND RECOMMENDATIONS 7.1 CONCLUSIONS Routine field activities associated with the Spring 2018 semi-annual groundwater monitoring were conducted by CEC personnel from April 9-12, 2018. Well water levels were gauged, static well water was purged, and groundwater samples were collected from 23 monitoring wells including shallow wells MW-1, MW-4, MW-4A, MW-5, MW-6, MW-7A, MW-8, MW-9, MW-10, MW- I IA, and MW-1113, and deeper wells MW-4D, MW-4D-1, MW-51), MW-61), MW-6D-1, MW-7, MW-71), MW-8D, MW-1OD, MW-11, MW-I ID-1, and MW-11D-2. Also, groundwater samples were collected from three off -site inactive private water supply wells (former Gilkerson, Hammill, and Tinsley residential wells) situated adjacent to the southern perimeter of the Closed Phase I Area. Vinyl chloride was detected above the 2L standard at 1.7 µg/L in interior well MW-51). Trihalomethanes, including bromodichloromethane and dibromochloromethane, detected in both inactive Gilkerson and Tinsley supply wells at concentrations exceeding their 2L Standards are commonly formed at relative low concentrations as a by-product of treating water with chlorine - based disinfectants and subsequent interaction with natural organics present in the water. Trihalomethanes have not been typically detected in the on -site groundwater samples. Iron and manganese exceeded the 2L Standards in the majority of the landfill monitoring well samples. Iron and manganese are naturally occurring metals in the local formation and can occur at elevated levels in reducing groundwater conditions such as those encountered at the subject landfill. Chromium, cobalt and vanadium were detected in several wells at concentrations exceeding their respective 2L Standards; however, the detected range of these analyte concentrations appears to be well within their naturally occurring levels The levels of total dissolved solids (TDS) exceeded its 2L Standard in wells MW-5, MW-51), MW-6, MW-6D, MW-6D-1, MW-7, MW-81), MW-10, MW-10D, MW-11 and the Hammill Civil & Environmental Consultants, Inc. -10- Spring 2018 Water Quality Monitoring Report WSW. Chloride appears to be elevated in the majority of wells, and Sulfate exceeds the 2L standard of 250 mg/L in the Hammill WSW. It is important to note that elevated TDS and chloride levels were observed in cross -gradient background well MW-81). Accordingly, CEC is currently evaluating available monitoring data for the closed Mecklenburg County Holbrooks Road Landfill facility, which lies adjacent and north of the subject landfill, to assess the potential for leachate migration beneath the subject landfill from this adjacent off -site MSW landfill. 10.2 RECOMMENDATIONS MW-6 demonstrated many metals above their respective 2L standards that have not been elevated continuously in the past. CEC suspects these detections may be caused by high turbidity in the monitoring well. The HF Scientific Turbidimeter measured a turbidity of 391.7 NTU after 20 minutes of purging MW-6. The well is scheduled to be re -developed prior to the upcoming Fall 2018 semi-annual event, in order to clear the well of suspended particles that may be effecting the metal concentrations. CEC predicts once the well is re -developed, the elevated detections of metal parameters will diminish. Please note that this will be the final report under the existing Water Quality Monitoring Plan. An updated Water Quality Monitoring Plan, prepared by CEC and dated April 19, 2018, was submitted to NC DEQ and approved in a letter dated April 20, 2018. This updated Water Quality Monitoring Plan will be followed beginning with the Fall 2018 semi-annual water quality monitoring event. Civil & Environmental Consultants, Inc. -11- Spring 2018 Water Quality Monitoring Report FIGURES Civil & Environmental Consultants, Inc. a 12NORTH ►hillinc 'hurch,Cem C REFERENCE U.S.G.S. 7.5' TOPOGRAPHIC MAP, CORNELIUS QUADRANGLE, NC DATED: 2016. C SCALE IN FEET 0 1000 20 ,=,= NOREEMECKLENBURG NWAY WASTE OLUUTIONS OF LANDFILL Civil & Environmental Consultants, Inc. NORTH MECK, LLC 1900 Center Park Drive - Suite A - Charlotte, NC 28217 Ph: 980.237.0373 - Fax: 980.237.0372 SITE LOCATION MAP www.cecinc.com DRAWN BY: PNP I CHECKED BY: EHS APPROVED BY: EHS FIGURE NO.: DATE: AUGUST 20171 DWG SCALE: 1 1000'1 PROJECT NO: 111-370.001 1 C T qLEGEND IL EXISTING STREAM CLOSED PHASE I AREA METHANE A hl;;6 MONITORING WELL � PROPERTY LINE - y INFILL • y- ' �' r T METHANE MONITORING BOUNDARY0� A M LANDFILL POINT OF COMPLIANCE LANDFILL REVIEW MW-1 GROUNDWATER • •' + MMW-3 r MW-16(i) LOCATION O r SW-lNF f . MMW-4(D iW-10 s SW-7 NEW SURFACE WATER SAMPLING • • ' • MW-2(i) REFERENCE TO INFILL AREA INFILL AREA Mw MW-11D(i) Mw-11(i) f X. MW-3(i) Z-5 / ` r �� av SSW-4 MMW-6 MW-4D i MW-4 iY®/ MW-11D-2 ti MW-5 SW-7 - - i J MW-5D �' OJ MW-11D-1 ~ r• MW-7D(i)4 MMW-8 SW-�' \ \ f OO O MW-11 MW-11A GW-2 1 _ MW-9D(t}-�,.� MW-7(i) SW-EFF W-1 SW-1 ® MW- - - - y MW-9(i) MMW-9- MW-8(i SW-2 MW-14(i) �MW-12D(i) +# MW-1OD -fir MW-13(i) MW-6 / • L _- GW-10 - MW_9 CLOSED PHASE I AREA MW-6D Mw\sD f :� - t [1i i i GREENWAY WASTE SOLUTIONS OF A AV AV NORTH MECK, LCC Civil & Environmental Consultants, Inc. NORTH MECKLENBURG LANDFILL 1900 Center Park Drive - Suite A - Charlotte, NC 28217 HUNTERSVILLE, NORTH CAROLINA REFERENCE Ph: 980.237.0373 - Fax: 980.237.0372 WATER QUALITY MONITORING LOCATION MAP SCALE IN FEET www.cecinc.com 1. AERIAL IMAGERY TAKEN FROM GOOGLE EARTH PRO. DRAWN BY: JKS/PAB CHECKED BY: EHS APPROVED BY: EHS FIGURE NO.: DATED OCTOBER 8, 2016 0 400 800 DATE: FEBRUARY 2018 1 DWG SCALE: 1" = 400' PROJECT NO: 111-370.0001 2 8 1 7 1 6 1 5 1 4 1 3 I� lei F E lei A \\\\\\\\ I ( r \ \ ( ��� 1 ��� \\\� \�ti \ /�/==-J " I / '/�\��/' /� /'���//��� ��_) I��\\ \\ \ill l\ \/ ,� /' /'/�'i/i'/��i���/%/�/i'"" '/i% /-'/r�i/i%// i�r�,�r/��///�-� \ I/�,�, f -i j'///'i//'/ii����= NOTES: \ 1111�1\ ' '(((��((( (( ({ / \ \ (� I �� \ \ l // i- ) // �/ I� l /��` I \\\ \1llllll\\ / // ///// /jj%///j ///r,///�// j///////� ////// \ 1 1 ///� -� �/ /'///// 1. 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COLONIAL PIPELINE 1 J \ // // I \ \ \ / / //, - \ / / / DO NOT EXCAVATE WITHIN v/ I /��i / // I ( , ) \ (\\ \\ \ \ i� \\\ \ 1 \ �-_ \- ��_ \ i' IIII i 1J I )�' r�i J )\\\\,\ \ \\\\ I I \ \ 1 I \ \\ THIS 100' GAS EASEMENT / I / , ! / l \�� ///�� \ ( \ \\ \ l \\ \\� \ � 1_ _-- IIII �// �J�/r � \\ \ \ / ` J \ J r (<< / ii \ \ \ /NF/LL EXPANS/ON I / / }�\\ \ \ / / /// �/ / �J ( ) (( ((\ \\\> > \\\ \ \ (/ - / / / 1' \ \ / \\ \ \ \\ l EW-214_/ / // / IIII/ / �J J ✓ /i/ji/ /i�i \ \\\ 1 / , AREA ACTIVE C&D _ I / / \\ - \\\\ � / - � /'�'/ ' // // �� )- (// T >�> , I I / // /�/� - \ I LANDFILL CELLS ` - �\ / /\\ \ \� _� - /i/ / / /, / " - �) I / / l \ I _ / / \ \ / /, / / / i // / \ �\\ \ \ L-\\ /// IIII /� j-� \\\\\\\ \ / I / , �� ) /C--/� ( / \\ � �� 1= % ' _ '- /' i / /// 2011;/// / �/ / I--- l� \ I) \\ /iii/�// // \ \\ \\\ \ I / ' \ 1 / , \\\\` / \�' %/ //%i ''"/�i / _ I I 1 / /// / / / \\\ \ \ \ \ ~� // - — // // / i / / / / // \ J \ \ / // // / //� \ l I \ \ / / � �- _ — / / / / / iii \ - / / \ \ /� \\\ / EW-202:/ / / / _ �\ - \ \ \ \ �„ I / //// ////�/ /// //- \\\ \���\�\� \ / I \ \\ \ \I / \ \\\\\( // � /� IIII/ -- / / /i % //� �/ �/ //%/ \! j \ \ \ \ / / -/ // / / - - / - / / / \\\\ I \ \\— I / / //// / // / \\\\ \\ \\ \�\ N � \ \\\ \ / \ \\ /�/i // �� /// /� / % / // // //,� \ /// /// / // \\\\\ \\\\ \\ \ \ \ \ \ \ / // — / \ \\ / / // / // / / \ \ \\\\ \\\ \\ \ l 1 ( \ I \ \ �� / //-- / / / / / /^ 1� 1 1 \ \ \ I /// /// / �/ / \\\\\\\ \\\\\\\ \\\\\ L I / \\\ \ l \ / / / \\\\\\ ��j/�/� /// / /� �// IIII i // / �/ I —��/ / \ 1 I I I \ \ \- 1 / //A/ / // / ////\ \\\\ \\ \ \ \ \\ \ \\ \� / // \�=�/i /� // EW-203 i- //� /�' // // ( / / / / I \ — \I / // / ///// \ \\ \ \\ \\\\ \ \\\ \\ I \ 1 / i/, I \ // / _/o%/ , /i/� /ji 1 11 I l \\ \\ \\ \IIII / // ///// // / / / // //� / //-\\\\�\\�\\\`\� �\�\\\� \\��\\ ` / \\\\\ \\I \\ \ / // I // �� / / / / j� 4" SDR 17 HDPE I 1 i _- 1 / / I I l \ \ \ I( l /I / // // / // / // \ \ \\ \ \ \ \\\ ( ���/ / // r // // // I ' / / / / / - / / / LATERAL PIPE / I I // j�� / \ \ \ 111 ( I// / /// // /// /// \ \\� \\\ \\\\\\\ \\\ \\\ \ \ \ \ \� / 1 //i IIII// � IIII// �/, TYP. \+J // / j \ l 1 \ \\ \ \-\ \ I I I IIII ll l / ll/l IIII% // �// 1 -\\\\.�- _\\.\�\��\\ \\ \ I \ \\ \ \ I \ -// / / / \\\ \\ 1 \// // IIII / // / / Ao / / /// ( )- �"� I,/��.. //// J \\ \ \\ \ I I / \\ \\\ , \ \\ \ \ \ / �/ IIII IIII /// // / / — = �� \ \ I I I I l / // // /// I EXISTING EXPANSION AREA 1 \\\\\\\ I \ \ \\ / IIII/ / / / / / -- /- t LANDFILL GAS HEADER ACCESS RISER \ I II I \ \ / / /i i // — -- / I/// \ \ \ � / \� - I 1 I // \\\ ) \ \ / / /�,-,/ //// � , \ \ I / / IIIII / / // l / / / CLOSED C&D LANDFILL CELLS \ / \ \ \\ \ \ / // / EW-204 ,, /i /i /// % % �� C401 — \ \ \ \ l l 1 1 / l l / l /// 1 \\ 8" HDPE 2% MIN. / \ \ \ / IIII PROTECTIVE ENCASEMENT FOR LANDFILL \ ll // I I I // / // \ \ \\ '- ///'/�f"', //' 'i'/�/'%%' eeo - '8�"�'B \\ \ / \ \\ APPROXIMATELY 485 LF -- \ \ / / //// // / // // / //i �/ % �- // GAS PIPES AT ROAD CROSSINGS- TYP. 5 _\ \ l l// I// / III IIII I / ll IIII / l/ / \ I I / \ \ \� \\ ' / \\ \ \\ / /j/� / // // / / // / -- 8 HDPE 2� MIN. / /// / I III I I I I 1 I11( 1 l I I \ \ \ \ HEADER PIPE \\\\ \\( !/ I / / /// /// �- APPROXIMATELY 836 LF , 6 8" BUT ISOLATION VALVE �/\ 1 I C400 i / // ////\ // Ill 111 I I I l I I I (, I I \ / / ) \ \ 1 \ I , \ ,'/" ,/ �/ / / / / j / TYP. _ ��\ \ \ // 1 \ / /1 \ // // / / , / /// //// IIII III 1 I I I EW-211 \\\ \- J �/ �� \ \ I '\\ / //) / '%i/ ,z - // / /// /, / (/ HEADER PIPE � / . 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'IIII /� \////i',/ / /�/ ///ii�'/ /'i'' / � / / l / / �\\ �l�\\\--^1 \\ /�,\\\\ \\\. \\ �\ \ ��\\-�,�,,/ii /�/�/����i/ii IIII IIII// // /� �/ / 1 / l/ f/ -� \ / /> \ \ \ C _ \ , /- �\/iiiiii / //�i I I�/�i�i/� /i'�iiiiii/i'i�///i' /l' / 1 I / /, / / / /� I ,�\\\ \ \\\ \ �: �✓ — \ .,/iii , / // /// /� / / / / / ///IIII\��1\\\l\�\uJ _/ ((\ \� \\���� — ✓�Lii'��'�'�/ 1/i/ii//��/i/ //�� // �� I 1 11 1 1 11\\ \1 ��� /- ��, /i �/ /i /'1 /IIII,// / „ //��ii��i /iiii //// / /// /z 1��1I \� i/ I 1\\ \\\ ��\\\�\\c-- /���/// j// ( %/j//� // IIII // / L----/ / / //// / // / / \\ l\ i \ \ 1 I \ \\ \\ \s--I, \ —) /i�/,i////,/�/�� //ice/�i� / iii // //i / �� :r- —_ / / \\\ / \ \ -�-% / / / /// / ////// /////j/%/ /// \/1-1 � l (11� /i //iii /i� /i/IIII/ ///i� 11 /-\\\\ � \ \\Z__ -„ / -----f I� ) �0\ � ;,%\�/////, //�//�/// /�/ /) /�/ 1 // /// II lII I 1 (/ / \� c/ice//ii/ii/// i /// f// / �\.��� \�\�� \ 1/ /�/ IIII / /i //�/ / �� %/ ) i I \ \�\ //// //// ///�/ / /�/1 , \�` - � \ � / /� ./%////�//� _ i ii / REFERENCE \ \ ---" — = - '� � I �,\A1�\ -�,� 1. EXISTING CONTOURS NORTH OF THE EXISTING CREEK PROVIDED BY PATTERSON LAND SURVEYING, PA DATED 2016. 2. EXISTING CONTOURS SOUTH OF THE EXISTING CREEK PROVIDED BY PATTERSON LAND SURVEYING. PA. DATED 2014. � � : ` — I \ \ \ /- / /// / ///////j // �\ m n — _ i/�/// /\ / %i �/ , IIII; / \1\ \ -\\ 11 'Ill&- /i%i/iiii' "\,�\\\ &. , 1, '000/ LEGEND EXISTING PROPERTY LINE EXISTING CONTOUR MAJOR EXISTING CONTOUR MINOR - - - EXISTING CREEK EXISTING LIMITS OF _ WASTE EXISTING PERIMETER METHANE MONITORING WELL PROPOSED LANDFILL GAS EXTRACTION WELLS PROPOSED LANDFILL GAS EXTRACTION WELLS RADIUS OF INFLUENCE 0 SCALE IN FEET 0 200 400 NORTH CAROLINA BOARD OF EXAMINERS FOR ENGINEERS AND SURVEYORS LICENSE NO. C-3035 0 or U W o CC z Ir O co 0 w in 0 w or 0 z 1—cj ^ T 4I N cQ Z cm rl °' o O ti m N 1 1 (U rn E ,-r a K o 111 � u- .9 4)� ID M I M § 1 > O -4 ��yyy 0 i � M 0 N "'' a 0) „i a) i W c a 4) U O .y O) T •rrj V W J Z L,L 0 0 J Z b a V JJJZ 0 C) It J � C) W � J ��Z> Q � J CC CC �e W a0vz Z G Z 0 3: 3: F- CC EL♦� V 0 W I � cn ~cf) 'QR V '^ V+ m Z < m 0 Y J O o w ti o o�- Q Q N x L) N II III: T J CC w a ;01.r11,1f,o,� ct f.'' II y i � �i:� `V-� � J Q Z M m p I s Q � w .� 0 C) > { SEAL � 0 0 0- ' o 0- r 9 4. . 'Z. , o a 0 j,' . -2-7-17 * DRAWING NO.: 1- 1 +410N.,--.e , , At To k1,%tj,% ,* C 300 SHEET 3 OF 6 A 5 4 TABLES Civil & Environmental Consultants, Inc. Table 1 Summary of Water Level Gauging Data Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Area Landfill CEC Project No. 111-370.001 Well ID Depths Screen 1 Interval TOC Elev. (ft) Fall a W.L. (TOC) Fall 2017 W.L. Elev. (ft) Spring 2018 W.L. (TOC) Spring 2018 W.L. Elev. (ft) MW-1 25 15-25 685.31 13.89 671.42 13.67 671.64 MW-4 42 32-42 717.55 35.42 682.13 36.49 681.06 MW-4A 44 34-44 711.63 33.01 678.62 33.18 678.45 MW-41) 100 85-100 711.30 32.55 678.75 32.81 678.49 MW-4D-1 135 120-135 NM 33.05 NM 33.22 NM MW-5 29 19-29 682.99 20.49 662.50 19.98 663.01 MW-51) 55 45-55 681.84 18.61 663.23 18.10 663.74 MW-6 67 57-67 738.25 58.44 679.81 58.78 679.47 MW-6D 95 80-95 737.90 58.71 679.19 58.40 679.50 MW-6D-1 160 145-160 NM 58.82 NM 58.65 NM MW-7 85 70-85 738.27 52.89 685.38 53.25 685.02 MW-7A 60 50-60 727.52 43.10 684.42 43.35 684.17 MW-71) 110 95-110 727.36 44.90 682.46 44.55 682.81 MW-8 80 70-80 764.39 68.41 695.98 68.57 695.82 MW-81) 122 107-122 768.20 72.00 696.20 71.90 696.30 MW-9 25 15-25 706.30 17.03 689.27 16.28 690.02 MW-10 25 15-25 696.81 17.88 678.93 17.29 679.52 MW-101) 65 55-65 726.77 42.83 683.94 41.55 685.22 MW-11 73 63-73 731.90 46.34 685.56 47.98 683.92 MW-11A 30 20-30 675.74 16.23 659.51 13.91 661.83 MW-1113 27 17-27 673.24 13.68 659.56 11.40 661.84 MW-11D-1 60 50-60 674.44 14.91 659.53 12.80 661.64 MW-11D-2 40 30-40 673.92 14.31 659.61 12.22 661.70 Notes: TOC= Top of Casing Elevation WL= Groundwater Level NM= Not Measured (1) Measured in feet below ground surface (2) Depth in feet relative to TOC elevation Table 2 Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent SUL SWSL MCL MW-1 M MW-5 MW-5D M MW-7A Laboratory- TA TA TA TA TA TA TA TA (DUP) P (split) TA TA TA TA TA Sample Date 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.16.18 Acetone 6000 l00 NS <5 2.7 J cn 2.6 J cn <5 <5 <5 <5 <5 <25 2.7 J cn <5 <5 <5 <5 Antimon ** 1 6 6 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 <3 Arsenic 10 10 10 0.97 J 0.82 J 0.75 J 3.5 3.4 0.32 J 0.67 J 14 0.63 J 4.8 0.83 J 0.69 J Barium 700 100 1 2000 33 430 180 180 74 240 210 1600 260 410 410 320 Benzene 1 1 5 <0.5 0.74 <0.5 <0.5 <0.5 0.67 0.99 0.85 <1 0.35 J 0.51 0.41 J <0.5 <0.5 Beryllium** 4 1 4 <1 <1 <1 <1 <1 <1 <1 6.1 <1 <1 <1 <1 Bromodichloromethane 0.6 1 NS <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Bromofnna 4 3 NS <1 <1 <1 <1 <1 <1 <1 <1 <1 <l <1 <1 <1 2-Butanone(MEK) 4,000 100 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Cadmium 2 1 5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3.1 <0.5 <0.5 <0.5 q2.1 Chloroethane 3000 10 NS <1 <1 <1 <1 <1 1 1.2 1.3 <1 <1 <1 <1 <1 Chlorofomr 70 5 70 <2 <2 <2 <2 <2 <2 <2 <2 <1 <2 <2 <2 <2 Chromium 10 10 100 <5 3.1 J 7.9 <5 7.6 <5 2.9 J 58 6.8 3.3 J 35 Cobalt** 1 10 NS 0.87 J 4.8 3.6 <1 <1 1.6 0.76 J 32 3.9 0.65 J 4.2 Copper 1,000 10 1,300 <2 <2 23 5.9 0.81 J 1.2 J 1.3 J 450 11 1.4 J 44 9.4 Carbon Disulfide 700 35 NS <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 Dibromochloromethane 0.4 3 NS <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1,1-Dichloroethane 6 5 NS <I <1 <1 1.9 <1 <1 1.9 1.8 1.7 <1 <1 <1 <1 <1 1,1-Dichloroethene 350 5 7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <l 1,4-13ichlorobeuzene 6 1 NS <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 cis-1,2-Dichloroethene 70 5 70 <1 <1 <1 <1 <1 <1 <1 <1 2.3 <1 <1 <1 <1 <1 Eth ]benzene 600 1 0.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 2-Hexanone NS 50 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 4-Meth 1-2- entanone NS 100 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Toluene 600 1 1000 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 <0.5 <0.5 <0.5 <0.5 <0.5 X lens 500 5 10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Lead 15 10 15 <0.5 1.1 6.5 1 0.22 J <0.5 <0.5 94 <0.5 <0.5 4.7 0.58 Manganese 50 50 NS 1600 730 94 460 270 410 780 5,000 7200 410 290 92 Mercury 1 0.2 2 <0.2 <0.2 0.26 <0.2 <0.2 <0.2 <0.2 0.81 <0.2 <0.2 0.53 0.35 Methylene Chloride 5 1 NS <5 <5 <5 <5 <5 <5 <5 <.:5 -=1 <5 <5 <5 <5 <5 Nickel l00 50 NS <2 4.9 9.7 0.68 J 3.5 2.4 9.7 42 19 2 17 8.6 Selenium 20 10 50 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 9.4 <2.5 <2.5 <2.5 <2.5 Silver 20 10 NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.49 J <0.5 <0.5 <0.5 <0.5 Tetrahydrofivan NS NS NS <10 <10 <10 <10 <10 <10 24 20 21.5 25 44 9.9 J <10 <10 Thallium** 0.2 5.5 2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 Tin 2000 100 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Vanadium** 0.3 25 NS <5 <5 14 <5 <5 <5 6 160 3.7J <5 19 11 Vinyl Chloride 0.03 1 2 <1 <1 <1 <1 <1 <1 1.7 1.4 1.7 <1 <1 <1 <1 <1 Zinc 1000 10 NS <10 40 90 12 <10 <10 <10 400 19 <10 30 13 Alkalinity NS NS NS 210,000 310,000 200,000 330,000 210,000 480,000 830,000 750,000 750,000 680,000 490,000 290,000 Iron 300 300 NS 6,000 1,600 5,600 2,200 1,000 240 230 76,000 780 6,500 7,300 3,200 Total Dissolved Solids 500,000 NS NS 270,000 410,000 250,000 360,000 260,000 720,000 1,300,000 870,000 890,000 730,000 620,000 400,000 Sulfate 250,000 250,000 NS 42,000 18,000 9,800 14,000 1,500 99,000 170,000 36,000 28,000 13,000 26,000 22,000 Chloride 250,000 NS NS 7,300 23,000 10,000 14,000-T 13,000 49,000 100,000 39,000 29,000 Fl 27,000 57,000 46,000 Notes: All units we in µg/L unless otherwised indicated NCDEQ Standard =15A NCAC 02L.0202 Groundwater Suds (Eff. 2013) * Interim Maximum Allowable Co xartration (Eff. 2013) Laboratories- Pace (P), Shealy (S), and Test America (TA) J - Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B-Compound was found in the blank and sample. cn= Refer to Case Narrative for further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS-Not Specified < "Report Limit' = Value is less that the Report Limit Table 2 Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-10 MW-IOD MW-11 MW-11A M Tinsley WSW Gilkerson WSW Hammill WSW Laborato '* TA TA TA TA TA TA TA TA TA TA TA TA TA TA Sample Date 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 4.10.18 Acetone 6000 100 NS <5 4.4 J cn <5 <5 <5 7.2 cn 15 <5 <5 <5 <5 <5 <5 <5 Antimon ** 1 6 6 <3 <3 <3 <3 <3 4.3 <3 <3 <3 <3 <3 <3 <3 Arsenic 10 10 10 0.29 J 0.34 J <l 1.2 2.3 0.58 J <1 <1 0.6 J 0.23 J <l <1 0.68 J Barium 700 1 100 2000 230 81 48 340 220 190 1 33 63 93 110 13 14 1 38 Benzene 1 1 5 <0.5 <0.5 <0.5 <0.5 0.42 J 3.3 0.42 J <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Beryllium** 4 1 4 <1 <I <1 <I <1 <1 <1 <1 <1 <1 <I <1 <1 Bromodichloromethane 0.6 1 NS <1 <l <l <1 <l <1 <1 <I <1 <1 <1 14 12 <1 Bromofomr 4 3 NS <1 <l <l <1 <1 <1 <1 <1 <1 <1 <1 <l 0.62 J <1 2-Butanone(MEK) 4,000 100 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Cadmium 2 1 5 <0.5 <0.5 <0.5 <0.5 1.6 0.34 J <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Chloroethane 3000 10 NS <1 <1 <1 <1 <1 <1 <1 <1 <1 <l <1 <1 <1 <1 Chloroform 70 5 70 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 37 31 <2 Chromium 10 10 100 <5 18 <5 <5 8.2 25 <5 <5 1.6 J <5 <5 1.5 J <5 Cobalt** 1 10 NS <1 1.2 <1 5.1 43 1.9 <1 <1 <1 0.75 J <1 <1 <1 Copper 1,000 10 1,300 <2 2.9 0.5 J <2 460 38 0.63 J 3.1 9.9 4.8 3.7 B 23 B 5.1 B Carbon Disulfide 700 35 NS <2 <2 <2 <2 <2 0.5 J <2 <2 <2 <2 <2 <2 <2 <2 Dibromochloromethane 0.4 3 NS <1 <l <1 <1 <l <1 <1 <1 <1 <1 <1 6 5.5 <1 1,1-Dichloroethane 6 5 NS <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1,1-Dichloroethene 350 5 7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <l <1 <1 <1 <1 114-Dichlorobenzene 6 1 NS <1 <1 <1 <1 <1 2 <1 <1 <1 <1 <1 <1 <1 <1 cis-1,2-Dichloroethene 70 5 70 <1 <l <l <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 Eth lbenzene 600 1 0.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2-Hexanone NS 50 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 4-Meth 1-2- entanone NS 100 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Toluene 600 1 1000 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Xylenes 500 5 10 <1 <l <1 <1 <1 <7 <1 <1 <1 <1 <1 <1 <1 <1 Lead 15 10 15 <0.5 0.23 J <0.5 <0.5 1.1 0.62 <0.5 <0.5 <0.5 0.34 J <0.5 7.4 0.32 J Manganese 50 50 NS 46 180 <2.5 4,600 17,000 1,400 3.9 7.6 5.1 42 1.8 J 28 88 Mercury 1 0.2 2 <0.2 <0.20 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 Methylene Chloride 5 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Nickel 100 50 NS <2 9.2 0.73 J 1.3 J 49 26 <2 <2 1.2 J 1.1 J <2 1.1 J 0.72 J Selenium 20 10 50 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 <2.5 Silver 20 10 NS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Tetrahydrofnnm NS NS NS <10 <10 <10 <10 9 J 97 6 J <10 <10 <10 <10 <10 <10 12 Thallium** 0.2 5.5 2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 <2 Tin 2000 100 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 2.1J Vanadium** 0.3 25 NS <5 6.3 3.4 J <5 8.7 5.9 <5 <5 2.9 J 2.3 J <5 <5 <5 Vinyl Chloride 0.03 1 2 <1 <I <I <1 <1 <1 <1 <1 <1 <I <1 <1 <1 <I Zinc 1000 10 NS <10 <10 <10 <10 11 15 <10 <10 32 13 1 <10 190 260 Alkalinity NS NS NS 350,000 300,000 410,000 47,000 630,000 1,700,000 680,000 23,000 36,000 300,000 53,000 22,000 23,000 93,000 Iron 300 300 NS 650 2,400 75 J 66,000 2,100 620 <100 <100 <100 <100 <100 1,500 B 210 B Total Dissolved Solids 500,000 NS NS 460,000 370,000 600,000 150,000 830,000 2,400,000 880,000 100,000 130,000 380,000 94,000 66,000 12Q,000 590,000 Sulfate 250,000 250,000 NS 28,000 43,000 15,000 16,000 340 13Q,000 68,000 12,000 18,000 35,000 17,000 8,400 8400 B 310,000 B Chloride 250,000 NS NS 48,000 12,000 82,000 22,000 47,000 200,000 35,000 3,800 4,500 25,000 5,400 8,300 8,800 5,600 Notes. All units are in pg/L unless otherwised indicated NCDEQ Standard = 15A NCAC 02L .0202 Groundwater Stds (Eff. 20E * Interim Maximum Allowable Concentration (Eff. 2013) Laboratories— Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted metlrod detection limit and below the adjusted reporting limit B-Compound was found m the blank and sample. cn= Refer to Case Narrative for further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009, NS- Not Specified < "Report Limit' = Value is less that the Report Limit Table 3 History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-1 Laboratory*** PR PR PR PR PR PR S S S S S S S S P P P P P P P P Sample Date 3.20.98 7.16.98 4.13.99 825.99 3.9.00 8.16.00 3.23.01 10.6.01 3.16.02 10.31.02 3.26.03 9.13.03 3.26.04 122.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.9.08 5.13.09 10.18.11 Acctonc 6000 100 NS <50 <50 <50 <50 <50 <50 <20 <20 <20 <20 <20 <20 <20 <20 <25 <25 <25 <25 <25 <25 <25 2.6 Antimony** 1 6 6 <6 Arsenic 10 10 10 <50 <10 <50 <10 <10 <10 18 <5 <5 <5 <5 <5 <10 <10 <5 <5 <5 <5 <5 <5 3.6 <10 Barium 700 1 100 2000 <100 <100 <100 680 100 73 59 75 53 51 45 55 45 59 43 250 46 53 43 59.2 40.2 25.2 Benzene 1 1 5 <5 <5 15 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 Beryllium** 4 1 4 <1 Bromodichlmomethane 0.6 1 NS 1 <5 1 <5 <5 1 <5 <5 1 <5 1 <5 <5 <5 <5 <5 1 <5 <5 1 <5 1 <5 <5 1 <5 1 <5 <5 1 <5 <5 <I Bromoform 4 3 NS <5 <5 <5 <5 <5 <5 <5 <5 1 <5 1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 2-Butanone(MEK) 4,000 100 NS <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <5 Cadmium 2 1 5 5 <5 <5 <5 <5 <1 <2 <2 <2 <2 <2 <2 <2 <2 <1 <1 <1 <1 <1 <1 <1 <1 Calcium NS NS NS Chlowethane 3000 10 NS <10 <10 <10 <10 <10 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 <1 Chloroform 70 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 Chromium 10 10 100 <5 <5 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <2 22 <2 <2 <5 0.57 <5 1 <10 Cobalt** 1 10 NS <10 Copper 1,000 10 1,300 1 1 1 1 1 1 11 <10 Carbon Disulfide 700 35 NS <50 <50 <50 <50 <50 <50 <5 <5 1 <5 1 <5 <5 <5 <5 <5 <10 <10 <10 I <10 I <10 <10 <10 <2 Dibromocliloromethane 0.4 3 NS <1 1,1-Dichloroethanc 6 5 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 1,1-Dichlorocthcnc 350 5 7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 1,4-Dichlorolh-cnc 6 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I cis-1,2-Dichloroethcnc 70 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <l Ethylbenzene 600 1 0.7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 1 <5 1 <1 2-Hexanone NS 50 NS 4-Methyl-2- entanone NS 100 NS Toluene 600 1 1000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 Xylenes 500 5 10 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <2 Lead 15 10 15 <15 <5 <15 <5 <5 <5 <3 <3 <3 <3 <3 <3 <3 <3 <5 6.8 <5 <5 <5 <5 <5 <10 Manganese 50 50 NS Mercury 1 0.2 2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.4 <0.4 <0.4 <0.4 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <10 <0.2 Methylene Chloride 5 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 Nickel 100 50 NS <50 Selenium 20 10 50 <10 <10 <10 <10 31 <10 <5 <5 <5 7.2 <5 <5 1 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 Sulfide NS 1,000 NS Silver 20 10 NS <18 <5 <18 <5 <5 <5 <5 <5 1 <5 <5 <5 <5 <5 <5 <2 1 <2 <2 1 <2 <5 <5 <5 <10 Tetrahydrofuran NS NS NS <10 Thallium** 0.2 5.5 2 <5.5 Tin 2000 100 NS Vanadium** 0.3 25 NS <25 Vinyl Chloride 0.03 1 2 <10 <10 <10 <10 <10 <10 <2 <2 <2 <2 <2 <2 <2 <2 <5 <5 <5 <5 1 <5 <5 <5 1 <1 Zinc 1000 1 10 NS <10 Alkalinity NS NS NS 348,000 Ammonia-N 1,500 NS NS Iron 300 300 NS Total Dissolved Solids 500,000 NS NS 353,000 Sulfate 250,000 250,000 NS 14,600 Carbon Dioxide NS NS NS Chloride 250,000 NS NS <5000 Notes: All units we in µg/L unless ofl-ised indicated NCDEQ Standard= 15A NCAC 02L .0202 Gusnal-ter Stds (Eff. 2013) * Interim Maximum Allowable Concentation (Eff. 2013) Labwatmies= Pace (P), Shealy (S), and Test America (TA) J = Estimated conc. above the adjusted method detection limit and below the adjusted reporting limit B=Compmwd was Imml in the blank and sample. n= Refer W Case Namative for fiuther detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL NICL MW-1 Cont. MW-4 Laboratory*** P P S S S S S S S P TA TA TA Sample Dale 4.12.12 1024.12 425.13 10.3.13 4.10.14 1023.14 424.15 1021.15 422.16 1027.16 428.17 10.10.17 4.10.18 3.2098 7.28.98 4.1399 825.99 3.9.00 8.16.00 3.23.01 lOb.01 3.16A2 Acetone 6000 100 NS <25 125 <20 <20 <20 <20 <20 2.6 <20 <25 5.1 <5 <5 750 <50 <50 <50 <50 <50 <20 <20 <20 Antimony** 1 6 6 <6 <6 <10 <10 <10 <10 <10 1.2 <5 <3 <3 <3 Arsenic 10 10 10 <10 13.1 12 <10 <10 <10 10 <26 2.6 <10 1.3 1 0.97 J <50 <10 <50 <10 <10 <10 14 <5 <5 Barium 700 1 100 2000 68 193 120 71 65 I10 77 460 81 66.4 67 370 33 <100 870 <100 110 <100 100 140 120 82 Benzene 1 1 5 <10 <10 <1 <1 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Beryllium** 4 1 4 <1 <I <4 <4 14 <4 <4 1.6 <1 <1 <1 <1 Bromodichloromethane 0.6 1 NS <1 <1 <t <t <1 <1 <1 <0.23 <1 <1 <1 <1 1 <5 1 <5 <5 <5 <5 <5 <5 <5 <5 Bromoform 4 3 NS <1 <1 <1 <1 <1 I <1 <1 <0.35 <1 <1 <1 <1 <5 <5 <5 <5 1 <5 <5 <5 <5 <5 2-Butamme(MEK) 4,000 100 NS <5 <5 <10 <10F<2 <10 <10 <18 <5 <5 <5 <5 <10 <10 <]0 <10 <10 <10 <10 <10 <10 Cadmium 2 1 5 <l <1 <2 <2 <2 <2 0.64 <2 <1 <0.5 <0.5 <0.5 5 <5 <5 <5 <5 <1 <2 <2 <2 Calcium NS NS NS 110,000 100,000 98,500 Chlormthane 3000 10 NS <1 <1 <2 <2 <2 <2 <0.28 <1 <1 <1 <1 <10 <10 <10 <10 <10 <10 <5 <5 <5 Chloroform 70 5 70 <1 <1 <1 <1 <1 <1 <0.21 <1 <2 <2 <2 <5 <5 <5 <5 <5 <5 <5 <5 <5 Chromium 10 10 100 <10 8.6 J <5 <5 <5 <5 20 <5 <5 <0.5 <0.5 <5 <5 <5 <50 <5 <5 <5 <5 <5 <5 Cobalt** 1 10 NS <10 <10 <25 <25 <25 <25 16 <25 <5 1.7 7.2 0.87 J Copper 1,000 10 1,300 <10 31.4 <5 <5 7.3 <5 67 5.1 <5 <2 0.68 <2 Carbon Disulfide 700 35 NS <2 <2 <1 <l <l <1 <0.45 <2 <2 <2F <50 <50 <50 <50 <50 <50 <5 <5 <5 Dibromochlommethane 0.4 3 NS <1 <1 <1 <1 <1 <1 <1 <0.23 <1 <1 <11,1-Dichlormthane 6 5 NS <l <t <I <1 <1 <1 <1 <0.19 <I <1 <I <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 l,l-Dichloroethenc 350 5 7 <1 <I <I <1 <1 <1 <1 <0.31 <I <1 <I <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 l,4-Dichlorobenzenc 6 1 NS <1 <1 <1 <1 <l <1 <l <0.19 <1 <1 <1 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 cis-1,2-Dichlormthme 70 5 70 <1 <1 <1 <I <1 <I <1 <0.2 <1 <I <1 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 Ethylbenzene 600 1 0.7 <l <1 <1 <l <1 <l <1 <0.21 <I <0.5 <0.5 <5 <5 <5 <5 <5 <5 <5 <5 <5 2-Hexanone NS 50 NS <5 <5 <54-Methyl-2-pentanone NS 100 NS <5 <5 <5 5 Toluene 600 1 1 1000 <l <1 <1 <1 <I <t L] <0.24 <l <0.5 <0.5 <065 <5 <5 <5 <5 <5 <5 15 <5 <5 Xylenes 500 5 10 <2 <2 <1 <1 <1 <1 1.3 <0.32 <1 <I <1 <I <5 <5 <5 <5 <5 <5 <5 <5 <5 Lead 15 10 15 <10 <10 <10 <10 <10 <10 <10 16 <10 <5 0.21 0.29 <0.5 <15 <5 <15 <5 <5 <5 <3 <3 <3 Manganese 50 50 NS 4,500 3,200 2,960 2,100 18,000 1600 Mercury 1 0.2 2 10.2 <0.2 <0.1 0.1 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 0.4 <0.2 <0.2 <0.1 <0.1 <0.1 Methylene Chloride 5 1 NS <1 <1 <1 <I <1 <1 <1 0.22 <I <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Nickel 100 50 NS <50 <50 <40 <40 <40 <40 <40 14 <40 <5 <2 <2 <2 Selenium 20 10 50 <10 <10 <10 <10 <10 <10 <10 <9.5 <10 <2.5 <2.5 <2.5 <10 <10 <10 <10 <10 <10 <5 <5 <5 Sulfide NS 1,000 NS <100 Silver 20 10 NS <10 <10 <5 <5 <5 <5 <5 <1.7 <5 <0.5 <0.5 <0.5 <18 <5 <19 <5 <5 --5 <5 <5 <5 Tetrahydrofuran NS NS NS <10 <10 <5 <5 <5 <5 <5 <0.57 <5 <10 <10 <10 <10 Thallium** 0.2 5.5 2 6.7 <5.5 6.7 <2 <2 <2 Tin 2000 100 NS <5 Vanadium** 0.3 25 NS 8.1 53.4 <50 <50 <50 <50 <50 71 7 <5 <5 <5 <5 Vinyl Chloride 0.03 1 2 <1 <1 <1 <1 1.5 <1 <1 <0.5 <1 <I 0.65 1.8 <10 <10 <10 <10 <10 <10 <2 <2 <2 Zinc 1000 10 NS 17.2 45.7 <20 20 43 31 <20 200 11 <10 <20 1 12 <10 Alkalinity NS NS NS 139,000,000 289,000 330,000 370,000 370,000 396,000 290,000 230,000 210,000 Ammonia-N 1,500 NS NS 1 860 700 720 Iron 300 300 NS 1 13,800 15,000 8,100 6,000 Total Dissolved Solids 500,000 NS NS 208,000 371,000 380,000 460,000 400,000 432,000 410,000 280,000 270,000 Sulfate 250,000 25Q000 NS 7,270 14,400 31,000 34,200 46,000 34,000 42,000 Carbon Dioxide NS NS NS 1 440,000 500,000 Chloride 250,000 NS NS 1 6,350 3,040 3,600 3,300 3,000 3,300 6,000 3,100 1 7,300 Not,: All units we in µg/L unless otherwised indicated NCDEQ Standard= ISA NCAC 02L .0202 Gumadwater Stds (Eff. 2013) * Interim Maximum Allawable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detectica limit and belaw the adjusted reporting limit B=Compound was faand in the blank and sample. n= Refer to Case Narrative for father detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL - coat. Laboratory - Sample Date 10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 1025.05 328.06 9.27.06 3.31.07 4.9.08 5.13.09 10.18.11 4.12.12 1024.12 425.13 10.3.13 4.10.14 1023.14 4.24.15 10.21.15 4.22.16 Acetone 6000 100 NS <20 120 <20 <20 <20 <25 <25 <25 <25 <25 <25 <25 5 <25 <25 <20 28 <20 <20 <20 5 <20 Antimony** 1 6 6 <6 <6 <6 <10 <10 <10 <10 <10 0.23 Arsenic 10 10 l0 <5 <5 <5 <10 <10 <5 <5 <5 <5 <5 <5 3.2 7.6 <10 <10 <10 <10 <10 <10 <10 1.9 5.6 Barium 700 100 2000 100 120 190 220 220 240 280 260 280 320 336 343 557 <100 527 620 620 650 610 650 550 660 Benzene 1 1 5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 <100 <1 <1 <1 <1 <1 <0.21 <1 Beryllium** 4 1 4 <1 <1 <10 <4 <4 <4 <4 <4 <0.12 Bromodichloromethane 0.6 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 1 <I <1 <I <1 <I <1 <I <1 <0.23 Bromofotm 4 3 NS 1 <5 1 <5 <5 <5 1 <5 1 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <1 <0.35 2-Butamme(MEK) 4,000 100 NS <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 I <10 <10 <5 <5 <1 <10 <10 <10 QO <10 Q8 Cadmium 2 1 5 <2 <2 <2 <2 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <5 <2 <2 <2 Calcium NS NS NS <1 550,000 71,000 Chloroethane 3000 10 NS <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 <1 <1 <2 <2 <2 <2 <2 <0.28 Chloroform 70 1 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <1 <0.21 Chromium 10 10 100 <5 <5 <5 <5 <5 <2 <2 <2 <2 <5 <5 0.4 <10 <10 <1 <5 <5 <5 <5 <5 0.87 6.1 Cobalt** I IO NS 10.2 <10 11.7 <25 <25 <25 <25 <25 18 19 Copper 1,000 IO 1,300 1 1 <10 I <10 <10 1 <5 5.9 <5 <5 <5 1.9 20 Carbon Disulfide 700 35 NS 1 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 <2 <2 <2 <1 <1 <1 <1 <1 1.7 Dibromochloromethane 0.4 3 NS I <l <1 <1 <1 <l I <1 <1 I <1 <0.23 l,l-Dichlormthane 6 5 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <I <0.19 <1 l,l-Dichloroethene 350 5 7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <1 0.45 <1 1,4-Dichlorobenzene 6 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <1 <0.19 <1 6s-1,2-Dichloroethene 70 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <1 <I <1 <I <1 <I <1 <0.2 <1 Ethylbenzene 600 1 0.7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <1 <I <1 <I <1 <I <1 <0.21 2-Hexanone NS 50 NS 4-Methyl-2-pentanone NS 100 NS Toluene 600 1 1000 1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <I <1 <1 <1 <0.24 Xylenes 500 5 10 <5 <5 <5 <5 <5 <5 15 <5 <5 <5 <5 <5 <2 <2 <2 1 <1 <1 <1 <1 <1 <0.32 Lead 15 10 15 <3 <3 <3 1 <3 <3 <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 <10 0.28 2.7 Manganese 50 50 NS 3,300 3,500 Mercury 1 0.2 2 <0.1 <0.1 <0.1 <0.4 <0.4 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.028 <0.1 Methylene Chloride 5 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <1 <I <1 <I <1 <I <1 <0.42 Nickel 100 50 NS 1 <50 <50 <50 140 <40 <40 <40 <40 8 15 Selem- 20 10 50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 I <10 <10 <10 <10 <10 <10 <10 <10 <10 <9.5 Sulfide NS 1,000 NS Silver 20 10 NS <5 <5 <5 <5 <5 <2 <2 <2 <2 <5 <5 <5 <10 <10 <10 <5 <5 <5 <5 <5 <1.7 Tetrahydrofuran NS NS NS <10 <10 <10 <5 <5 <5 <5 <5 <0.57 <5 Thallium** 0.2 5.5 2 <5.5 <5.5 <5.5 Ti. 2000 100 NS Vanadium** 0.3 25 NS <25 <25 <25 <50 <50 <50 <50 <50 1.9 20 Vinyl Chloride 0.03 1 2 <2 <2 <2 <2 <2 <5 <5 <5 <5 <5 <5 <5 <1 <t <1 3.5 7.1 6.8 7 2.7 1.2 <I Zinc 1000 10 NS I <10 <10 <10 <10 27 <20 <20 <20 140 <20 Alkalinity NS NS NS 1 332,000 <5000 1 306,000 390,000 320,000 390,000 Ammonia-N 1,500 NS NS 1 1,000 11000 Iron 300 300 NS Total Dissolved Solids 500,000 NS NS 427,000 <25,000 440,000 440,000 Sulfate 250,000 250,000 NS <5000 <5000 Carbon Dioxide NS NS NS =14,700 660,000 900,000 Chloride 250,000 NS NS 6,230 <5000 8,100 1 7,300 Notes: All units we in µg/L unless ofl-ised indicated NCDEQ Standard= 15A NCAC 02L .0202 Groundwater Stds (Eff. 2013) * Interim Masimom Allowable Conceatation (Eff. 2013) Laborstories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Comp-d was f d m the blank and sample. n= Refer to Case Narrative for father detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Sod. SWSL MCL = MW-4(cont.) W MW-4A MW-4D Laboratory*** Sample Date 10.27.16 5.1.17 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 MMMS 1023.14 424.15 1021.15 422.16 1027.16 10.27.16 5.1.17 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 41LL5 M21.15 Acctonc 6000 100 NS <25 15 5.8 5.7 2.7 J cn <20 <20 <20 <20 2.4 <20 <25 <2 15 <5 <5 2.6 J cn <20 <20 <20 <20 <16 Antimony** 1 6 6 <5 <3 <3 <3 <3 <10 <10 <10 <10 0.83 <5 <3 <3 <3 <3 <10 <10 <10 <10 0.19 Arsenic 10 10 10 <10 0.62 0.56 0.82 J <10 <10 <10 <10 0.37 <10 <10 0.43 0.3 0.75 J <10 <10 <10 <10 1.5 Barium 700 100 2000 241 440 410 430 270 120 83 110 110 68 246 160 170 180 86 89 140 110 140 Benzene 1 1 5 <1 1.1 0.32 1.1 0.74 <1 <1 <1 <1 <0.21 <1 <1 <0.4 0.35 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 Beryllium** 4 1 4 <l <1 <1 <1 14 <4 <4 <4 <0.12 <1 <I <1 <1 <4 <4 <4 <4 <0.12 Bromodichloromethane 0.6 1 NS <1 <I <1 <I <1 <l <1 <I <1 <0.23 <l <0.4 <I <1 <I <1 <I <I <l <1 1 <0.23 Bromoform 4 3 NS <1 <1 <1 <I <1 <1 <1 <1 <1 <0.35 <1 <0.4 <1 <1 <1 <1 <1 <1 <1 <1 <0.35 2-Butancte(MEK) 4,000 too NS <5 <5 <5 <5 <5 <10 <10 <10 <10 <18 <5 <2 <5 <5 <5 <5 <10 <10 <10 <10 <18 Cadmium 2 1 5 <1 <0.5 <0.5 <0.5 <2 <2 <2 <2 <0.044 0.12 <1 <0.5 <0.5 <0.5 <2 <2 <2 <2 <0.044 Calcium NS NS NS 34,700 34,000 14,000 42,400 84,000 Chloroethane 3000 10 NS <I <1 <I <1 <I <2 <2 <2 <2 <0.28 <1 <0.4 <1 <I <t <I <2 <2 <2 <2 <0.28 Chloroform 70 1 5 70 <1 <2 12 <2 <2 <1 <l <1 <1 <0.21 <1 <0.4 <2 <2 <2 <2 <1 <1 <1 <1 <0.21 Chromium 10 10 100 <5 8 2.6 3.1 J 27 <5 <5 <5 0.87 <5 9.9 2.3 10 7.9 <5 <5 8 <5 <6.3 Cobalt** 1 10 NS <5 6 4.9 4.8 <25 <25 <25 <25 0.7 <25 5.4 0.95 0.94 3.6 <25 <25 <25 <25 0.28 Copper 1,000 10 1,300 <5 3.8 1.6 <2 86 1 <5 <5 1 <5 1 5.3 3.7 102 6.3 6.4 23 <5 <5 16 <5 0.76 Carbon Disulfide 700 35 NS <2 <2 <2 <2 <2 <1 I <1 <1 <1 <0.45 <2 <0.4 <2 <2 <2 <2 <1 <1 <1 <1 <0.45 Dibromochloromedume 0.4 3 NS <1 <1 <1 <1 <1 <1 I <1 <1 <1 <0.23 <1 <0.4 <1 <1 <1 I <1 <1 <I <1 <I <0.23 1,1-Dichloroethane 6 5 NS <1 <1 <1 <1 <1 <1 <1 1.2 <1 0.83 <1 <1 0.61 0.64 0.54 0.75 <1 2.4 2.8 2.8 2.5 1.3 l,l-Dich1m,eth- 350 5 7 <1 <1 <1 <1 <1 <1 1.7 2.4 <1 1.8 1.4 <1 0.78 <1 <1 <1 <1 1.1 2.6 3.7 <1 1.4 1,4-Dichlorobenzcne 6 1 NS <1 <I <1 <I <1 <l <1 <l <1 <0.19 <1 <1 <0.4 <I <1 <I <1 <I <1 <l <1 <0.19 cis-1,2-Dichlorocthcne 70 1 5 70 <1 <1 <1 <1 <1 <l <1 <l <1 0.5 <1 <1 <0.4 <1 <1 <1 <I <1 <1 <1 <1 0.28 Ethylb-ame 600 1 1 0.7 <1 <0.5 <0.5 <0.5 <0.5 <1 <I <1 <1 <0.21 <1 <0.4 <0.5 <0.5 <0.5 <0.5 1.5 <1 <1 <I <0.21 2-Hexamme NS 50 NS <5 <5 <5 <5 <5 <5 <2 <5 <5 <5 <5 4-Methyl-2-pentamme NS 100 NS <5 <5 <5 <5 <5 1 1 1 <5 <2 <5 <5 <5 <5 Toluene 600 1 1000 <I <0.5 <0.5 <0.5 <0.5 <1 <I <1 3 <0.24 <1 <0.4 1 <0.5 1 <0.5 <0.5 <0.5 7.4 <l <1 <l 0.34 Xylenes 500 5 10 <I <1 <1 <1 I <I <1 I <I <1 3.9 <0.32 <1 <0.4 <1 <1 <t <1 8.1 <1 <I 1.1 <0.32 Lead 15 10 15 1 5.9 11 3.9 1.1 26 <10 <10 <10 0.94 <10 27.4 1.5 1.2 6.5 <10 <10 <10 <10 <0.15 Manganese 50 50 NS 1390 820 760 730 26 21 285 39 34 94 460 Mercury 1 0.2 2 <0.2 <0.2 <0.2 0.32 <0.1 <0.1 0.25 0.1 <0.1 <0.2 0.43 0.26 1 <0.1 0.32 0.48 <0.1 0.071 Methylene Chloride 5 1 NS <1 <5 <5 <5 <5 <l <1 <l <1 <0.42 <l <0.4 <5 <5 <5 <5 <l <1 <1 <1 <0.42 Nickel 100 50 NS <5 9.3 3.8 4.9 <40 <40 <40 <40 2.3 <40 18.6 3.6 6.5 9.7 <40 <40 <40 <40 6.6 Selenium 20 10 50 <10 <2.5 <2.5 <2.5 <10 <10 <10 <10 <9.5 <10 <2.5 <2.5 <2.5 <10 <10 I <10 <10 <9.5 Sulfide NS 1,000 NS <I00 <100 Silver 20 10 NS <5 <0.5 1 <0.5 <0.5 1 <5 <5 <5 <5 <1.7 <5 <0.5 1 <0.5 <0.5 <5 <5 <5 <5 <1.7 Tetrahydrofuran NS NS NS <10 <10 <10 <10 <10 <5 1 <5 <5 <5 <0.57 <5 <10 <1 <10 <10 <10 <10 <5 <5 <5 <5 <0.57 Thallium** 0.2 5.5 2 1 <5.4 I <2 <2 <2 <5.4 <2 <2 <2 Tin 2000 t00 NS <5 <5 Vanadium** 0.3 25 NS <5 2.5 <5 <5 68 <50 <50 <50 4.3 <50 55.4 5 3.5 1 14 1 <50 <50 <50 <50 <15 Vinyl Chloride 0.03 1 2 <1 14 <0.5 <0.5 <1 3.4 3.4 3.4 <1 1.2 2 <l 2 3.7 <0.5 <0.5 <1 4.7 6 6.9 1.7 0.65 Zinc 1000 1 10 NS 300 96 51 40 13 320 15 290 890 1200 257 39 16 90 <20 <20 45 <20 43 Alkalinity NS NS NS 253,000 312000 300,000 310,000 170,000 190,000 201,000 1 200,000 210,000 200,000 190,000 Ammonia-N 1,500 NS NS 140 1 170 <10 <100 1 820 Iron 300 300 NS 3,590 2,500 1,700 1,600 21,300 1 1,700 1 1,300 5,600 Total Dissolved Solids 500,000 NS NS 344,000 480,000 400,000 1 410,000 1 280,000 280,000 273,000 320,000 330,000 250,000 270,000 Sulfate 250,000 250,000 NS 11,900 20,000 10,000 18,000 10,800 11,000 12,000 9,800 Carbon Dioxide NS NS NS 380,000 620,000 1 210,000 Chloride 250,000 NS NS 1 16,300 1 21,000 19,000 23,000 8,200 8,400 9,700 10,000 1 1 11,000 10,000 8,400 Notes. All mots are in pg/L mless otherwised indicated NCDEQ Standard = l5A NCAC 02L .0202 Grom l-ter Std. (Eff. 2013) * Interim Maaimam Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compomd was fomd in the blank and sample. cn= Refer to Case Narrative for further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Masi- Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit' = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-4D (coat.) MW-4D-1 MW-5 Laboratory*** Sample Date S 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 4.10.18 10.23.14 424.15 10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 4.10.18 PR 3.20.98 PR 7.16.98 PR 4.13.99 PR 8.25.99 PR 3.9.00 PR 8.16.00 S 3.23.01 Acetone 6000 100 NS <20 <25 <5 15 <5 <5 <20 <20 9.1 <20 <25 <5 <5 <5 <5 <50 <50 <50 <50 <50 <50 <20 Antimony** 1 6 6 <5 <3 <3 <3 <3 <10 <10 0.56 <5 <3 13 <3 <3 Arsenic 10 10 l0 1.2 <10 0.64 0.48 3.5 <10 <10 1.5 1.7 <10 3.3 3.6 3.4 <50 <10 <50 <10 <10 <10 24 Barium 700 100 2000 110 56.2 50 47 180 30 31 32 45 49.8 62 68 74 <100 280 <100 300 280 200 170 Benzene 1 1 5 --1 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <0.21 <1 <1 0.46 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <5 Beryllium** 4 1 4 <1 <I <I <1 <4 <4 <0.12 <I <1 <1 <I Bromodichloromethane 0.6 1 NS <1 <I <1 <I <1 <I <1 <0.23 <I <1 <I <1 <I <5 <5 <5 <5 <5 <5 <5 Bromoform 4 3 NS <1 <1 <1 <1 <1 <1 <1 <0.35 <1 <1 <1 <1 <1 <5 <5 <5 15 <5 <5 <5 2-Butamne (MEK) 4,000 100 NS <5 <5 <5 <5 <5 <10 <10 <18 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 Cadmium 2 1 5 <2 <1 <0.5 <0.5 <0.5 <2 <2 <0.044 <2 <1 <0.5 <0.5 <0.5 14 14 <5 <5 <5 <1 <2 Calcium NS NS NS 70,000 35,900 37,000 44,000 42,400 Chloroethane 3000 10 NS <1 <1 <1 <1 <I <2 <2 <0.28 <1 <1 <1 <1 <1 <10 <10 <10 <10 <10 <10 <5 Chloroform 70 5 70 <1 <2 <2 <2 1 <2 1 <1 <1 <0.21 <1 <2 <2 43 <2 <5 <5 <5 <5 <5 <5 1 <5 Chromium 10 1 10 100 <5 <5 <0.5 <0.5 <5 <5 <5 0.93 <5 <5 5.8 <0.5 7.6 <5 18 <50 <5 6 <5 <5 Cobalt** 1 10 NS <2> - <5 <I <I <1 <25 <25 <2.6 <25 <5 2.2 9.5 <I Copper 1,000 10 1,300 1 1.3 <5 <2 1 <2 5.9 <5 <5 0.32 <5 <5 1.3 <2 0.81 J Carbon Disulfide 700 35 NS < <2 <2 <2 <2 9.6 1 <1 2.1 <2 <2 <2 <2 <2 <50 <50 <50 <50 <50 <50 <5 Dibromochloremethan, 0.4 3 NS <1 <1 <1 <I <1 <1 <1 <0.23 <1 <1 <1 0.76 <1 l,l-Dichloroethane 6 5 NS <1 <1 0.55 1.8 <l 1.9 <1 <1 1 <I <1 0.72 0.71 <1 <1 <5 <5 <5 <5 <5 <5 <5 l,l-Dichloroethene 350 5 7 Li <1 <1 <1 <1 <1 1.2 <1 1.5 1.1 <1 <1 <1 <1 <1 <5 <5 <5 <5 <5 <5 <5 1,4-DichImobenzene 6 1 NS <1 <1 <1 <1 <1 <1 <1 <1 <0.19 <1 <I <1 <I <1 <1 <5 <5 <5 <5 <5 <5 <5 cis-1,2-Diehl.mthene 70 5 70 <I <1 <I <1 <1 <1 <I <1 <0.2 <1 <I <1 <1 <1 <1 <5 <5 <5 <5 <5 <5 <5 Ethylbenzene 600 1 0.7 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <0.21 <1 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 1 15 1 <5 2-Hexanone NS 50 NS <5 <5 <5 <5 <5 0.8 <5 <5 <5 <0.5 <5 4-Methyl-2-pentanone NS 100 NS <5 <5 <5 <5 <5 0.81 <5 <5 <5 <5 1 <5 Toluene 600 1 1000 <t <0.5 <0.5 <0.5 <0.5 <I <l 0.66 <1 <0.5 <0.5 0.38 <0.5 <5 <5 <5 <5 <5 <5 <5 Xylenes 500 5 10 <1 <1 <1 <1 <1 1.2 0.43 <1 <1 <1 0.41 <1 <5 <5 1 <5 <5 <5 <5 <5 Lead 15 10 15 <10 <5 <0.5 0.17 1 <10 <10 <0.15 <10 <5 1.2 <0.5 0.22 J <15 <5 <15 <5 <5 <5 <3 Manganese 50 50 NS 410 210 280 260 460 30 180 194 210 250 270 Mercury 1 0.2 2 <0.1 <0.2 <0.2 <0.2 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 Methylene Chloride 5 1 NS <1 <5 <5 <5 <5 <1 <1 <0.42 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Nickel 100 50 NS <40 <5 <2 <2 0.68 J <40 <40 <6.3 <40 <5 3.6 2.3 3.5 Selenium 20 10 50 <10 <2.5 <2.5 <2.5 <10 <10 <9.5 <10 <2.5 <2.5 <2.5 <10 <10 <10 <10 <10 <10 1 <5 Sulfide NS 1,000 NS <100 <100 Silver 20 10 NS <5 <0.5 <0.5 <0.5 <5 <5 <L7 <5 <0.5 <0.5 <0.5 <18 1 <5 <18 <5 <5 <5 <5 Tetrahydrofuran NS NS NS - <10 <10 <10 <10 <10 <5 <5 <0.57 <5 <10 <10 <10 <10 <10 Thallium** 0.2 5.5 2 <5.4 <2 <2 <2 <5.4 <2 <2 <2 Ti. 2000 100 NS <5 <5 Vanadium** 0.3 25 NS -50 <5 <5 <5 1 <5 <50 <50 <15 <50 <5 <5 2.8 <5 Vinyl Chloride 0.03 1 2 0*85 <1 1.1 <0.5 <0.5 <1 1.2 <1 0.52 0.76 <I 2.1 <0,5 <0.5 <I <10 <10 <10 <10 <10 <10 <2 Zinc 1000 10 NS 44 72 8.7 11 12 <20 <20 9.8 11 <10 16 <20 <10 Alkalinity NS NS NS 180,000 132,000 140,000 140,000 330,000 150,000 190,000 1 187,000 200,000 210,000 210,000 Ammonia-N 1,500 NS NS <10 <100 74 <10 <100 Iron 300 300 NS 285 330 320 2,200 362 490 530 1,000 Total Dissolved Solids 500,000 NS NS 230,000 182,000 210,000 180,000 360,000 210,000 240,000 239,000 240,000 250,000 260,000 Sulfate 250,000 250,000 NS 8,100 8,500 7,800 14,000 5,300 3,000 1,300 1,500 Carbon Dioxide NS NS NS 210,000 140,000 190,000 Chloride 250,000 NS I NS 1 7,200 1 5,700 1 5,500 5,900 14,000 L3,000 12,000 12,300 13,000 8,900 13,000 Notes: All units me in µg/L unless otherwised indicated NCDEQ Standard= 15A NCAC 02L .0202 Gumadwater Stds (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compound was f d in the blank and sample. n= Refer to Case Narrative for further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-5 cunt. Laboratory*** S S S S S S S P P P P P P P P P P P S S S S Sample Date 10.6.01 3.16.02 10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.9.08 5.13.09 10.18.11 4.12.12 10.24.12 4.25.13 10.3.13 4.10.14 10.23.14 4.24.15 Acctonc 6000 100 NS 120 <20 <20 <20 <20 <20 <20 <25 <25 <25 <25 <25 <25 <25 3.8J <25 <25 <20 <20 <20 <20 <20 Antimony** 1 6 6 <6 <6 <6 <10 <10 <10 <10 <10 Arsenic 10 10 10 <5 <5 <5 <5 <5 <10 <10 <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 <10 Barium 700 1 100 2000 150 140 120 150 140 130 400 370 500 280 280 220 257 239 247 <100 1320 460 410 370 460 280 Benzene 1 1 5 15 <5 <5 <5 <5 <5 <5 <5 <5 <5 15 <5 0.44 0.53 <10 <10 0.53 J <1 <1 <1 <1 <1 Beryllium** 4 1 4 <1 <1 1 <4 <4 <4 <4 <4 Bromodichloromethane 0.6 1 NS 1 <5 1 <5 <5 11 <5 <5 <5 <5 <5 11 <5 <5 <5 1 <5 <5 1 <5 1 <1 <1 I <1 <1 <I <1 <I <1 Bromoform 4 3 NS <5 <5 <5 <5 <5 <5 1 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 I <1 <1 <1 2-Butanone(MEK) 4,000 L00 NS <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <5 <5 <5 <10 <10 <10 <10 <10 Cadmium 2 I 5 <2 <2 <2 <2 <2 <2 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <2 <2 <2 <2 Calcium NS NS NS Chloroethane 3000 10 NS <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 <1 <1 <1 <2 <2 <2 <2 <2 Chloroform 70 1 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <1 <1 <1 <1 <1 <1 I <1 Chromium IO 10 100 5.1 5.1 5.1 5.1 5.1 <5 <5 <2 43 <2 <2 <5 <5 <5 <10 <10 31.9 5.3 <5 <5 5.5 <5 Cobalt** 1 10 NS <10 <10 33.8 <25 <25 <25 <25 <25 Copper 1,000 10 1,300 1 1 1 11 1 1 1 27.3 <10 1 1130 160 110 63 140 11 Carbon Disulfide 700 35 NS <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 1 <2 <2 <2 <1 <1 I <1 <1 <l Dibromochloromethane 0.4 3 NS <1 <1 <1 <I <1 <I <1 <1 l,l-Dichloroethane 6 5 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 2.8 3.5 <1 <I 0.73J <I <1 <I <1 3.3 l,l-DichImuethene 350 5 7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <I <1 <l <1 <l <1 <1 1,4-Dichlorobenzene 6 1 NS <5 <5 <5 <5 <5 <5 <5 <5 15 <5 <5 <5 <5 0.39 <1 <1 <I <1 <1 <1 <1 <1 cis-1,2-Dichloroethene 70 1 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 1.9 2.1 2.1 1.8 1.9 1.9 Ethylbenzene 600 1 0.7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <1 2-Ilexamme, NS 50 NS 4-Methyl-2-pentamme NS I00 NS Toluene 600 I 1000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 I <1 <1 <1 <1 <1 Xylenes 500 5 10 <5 <5 <5 <5 <5 <5 1 <5 <5 <5 <5 <5 <5 <5 <5 <2 <2 <2 <1 <1 <1 <1 1.1 Lead 15 10 15 <3 <3 <3 <3 <3 <3 <3 <5 <5 <5 <5 <5 <5 <5 <10 <10 13.7 <10 <10 <10 <10 <10 Manganese 50 50 NS Mercury 1 0.2 2 <0.1 <0.1 <0.1 <0.1 <0.1 <0.4 <0.4 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 0.12 J <0.1 <0.1 <0.1 <0.1 <0.1 Methylene Chloride 5 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <1 <I <1 <I <1 <l I <1 Nickel 100 50 NS 1 <50 <50 24.3 J <40 <40 <40 <40 <40 Selenium 20 10 50 <5 <5 <5 5.2 8.8 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 Sulfide NS 1,000 NS Silver 20 10 NS <5 <5 <5 <5 <5 <5 <5 <2 <2 <2 <2 <5 <5 <5 <10 <10 <10 <5 <5 <5 <5 <5 Tetrahydrofuran NS NS NS <10 <10 <10 <5 <5 <5 <5 <5 Thallium** 0.2 5.5 2 1 1 <5.5 1 <5.5 1 <5.5 Tin 2000 I00 NS Vanadium** 0.3 25 NS 6.3 J <25 324 51 <50 <50 <50 <50 Vinyl Chloride 0.03 I 2 <2 <2 <2 <2 <2 <2 <2 <5 <5 <5 <5 <5 0.64 <5 <1 <I 0.95 J 4.6 7.5 6.4 8.6 3 Zinc 1000 1 10 NS 1 27.9 <10 327 49 31 26 55 <20 Alkalinity NS NS NS 1 1 343,000 <5000 232,000 230,000 Ammonia-N 1,500 NS NS Iron 300 300 NS Total Dissolved Solids 500,000 NS NS 344,000 <25,000 433,000 470,000 Sulfate 250,000 250,000 NS 14,600 <5000 1 114,000 100,000 Carbon Dioxide NS NS NS Chloride 250,000 NS NS <5000 <5000 1 26,800 25,000 Notes: All wits are in pg/L mless otherwised indicated NCDEQ Standard = l5A NCAC 02L .0202 Gmm l-ter Std. (Eff. 2013) * Interim Maairnum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compom l was fond in the blank and sample. cn= Refer to Case Narrative for further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maadmum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit' = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-5 (cons.) MW-5D Laboratory*** S S P TA TA TA TA S S S S S S P S (split) TA P (split) TA TA P (split) TA Sample Date 1021.15 422.16 10.27.16 427.17 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 1027.16 10.27.16 4.27.17 4.27.17 6.15.17 10.10.17 10.10.17 4.10.18 Acetone 6000 100 NS 2.2 <20 <25 <5 15 <5 <5 <20 <20 <20 <20 2.4 <20 <25 <2 <5 <25 <5 5.3 <25 <5 Antimony** 1 6 6 0.34 <5 <3 <3 <3 <3 <10 <10 <10 <10 0.28 <5 <3 <3 <3 <3 Arsenic 10 10 10 0.34 <10 <10 0.15 <1 0.32 J <10 <10 <10 <10 1 2.3 <10 0.27 0.49 0.67 J Barium 700 1 100 2000 310 310 254 230 240 240 280 320 320 320 290 750 260 230 240 210 Benzene 1 1 5 0.67 <1 <1 0.74 0.76 0.76 0.67 <1 1.1 <1 1.2 1.3 <1 <1 1.1 1.3 <1 0.97 0.7 <1 0.99 Beryllium** 4 1 4 <0.12 <1 <1 <1 <I <4 14 <4 <4 <0.12 <1 <I <I <1 Bromodichloromethane 0.6 1 NS <0.23 <I <1 <I <1 <I <1 <I <1 <I <0.23 <1 <0.4 <I <I I <1 <I <I <1 Bromoform 4 3 NS <0.35 <I <1 <I <1 <I <1 <1 <1 <I <0.35 <1 <0.4 <1 <I <1 <I <I <1 2-Butamme (MEK) 4,000 100 NS <18 <5 <5 <5 <5 <5 <10 <10 <10 <10 <18 <5 <2 <5 <5 <5 <5 <5 <5 Cadmium 2 1 5 110 <2 <1 <0.5 <0.5 <0.5 <2 <2 <2 <2 <0.044 0-31 <1 <0.5 <0.5 <0.5 Calcium NS NS NS 99,000 120,000 128,000 250,000 220,000 251,000 Chloroethane 3000 10 NS 1 <1 <1 1.5 1.7 1 2.5 2.5 2.5 2.2 2.1 1.4 1.3 1.1 1.6 1.8 1.6 1.7 1.2 Chloroform 70 1 5 70 <0.21 <1 <2 <2 <2 <2 <1 <1 <t <1 <0.21 <I <0.4 <2 <1 <2 <2 <1 <2 Chromium 10 t0 t00 0.93 <5 <5 <0.5 <0.5 <5 13 <5 <5 <5 1.2 9.7 <5 <0.5 <0.5 2.9 J Cobalt** 1 t0 NS 1.9 <25 <5 2.7 1.6 1.6 <25 <25 <25 <25 2.1 7.6 <5 0.71 1 0.89 0.76J Copper 1,000 to 1,300 1 21 1 49 34.4 5.4 1 1.2 1.2 J 28 19 7.2 5.8 5.2 290 <5 1.1 24 1.3 J Carbon Disulfide 700 35 NS <0.45 <2 <2 <2 <2 <2 <1 <I <1 <I <0.45 1 <2 <0.4 <2 1 <2 <2 <2 Dibromochloromethane 0.4 3 NS <0.23 <I <1 <I <1 <I <1 <I <1 <I <0.23 <1 <0.4 <1 <I <1 <I <I <1 t,l-Dichlormthane 6 5 NS 0.68 <1 <1 0.83 0.91 0.98 <1 3.6 3.3 1.9 2.9 2.8 2 1.9 2 1.7 2.1 2 1.6 1.7 1.9 l,l-Dichloroethene 350 5 7 <0.31 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.31 <1 <1 <0.4 <1 <1 <1 <1 <1 <1 1,4-Dichlorobenzene 6 1 NS 0.31 <1 <1 <1 <1 <1 <1 <t <1 <1 <1 0.44 <I <1 <0.4 <1 <I <1 <1 <1 <1 cis-1,2-Dichloroethene 70 1 5 70 1.9 1.4 2.1 1.9 2 <1 <I 6.5 5.4 3.1 4.3 3.8 2.5 2.8 <0.4 2.4 3.2 2.3 1 1.8 2.5 <1 Ethylbenzene 600 1 1 0.7 <0.21 <1 <0.5 <0.5 <0.5 <0.5 <1 <I <1 <1 <0.21 <1 <0.4 <0.5 <1 <0.5 <0.5 <1 <0.5 2-11exanone NS 50 NS <5 <5 1 <5 <5 <5 <0.26 <5 1 <2 <5 <5 <5 <5 <5 <5 4-Methyl-2-pentanone NS 100 NS I <5 <5 <5 <5 <5 0.69 <5 <2 <5 <5 <5 <5 <5 <5 Toluene 600 1 1000 1 <0.24 <I <0.5 <0.5 <0.5 <0.5 <1 <I <1 <1 0.65 <1 <0.4 <0.5 <1 <0.5 <0.5 <1 <0.5 Xylenes 500 5 10 <0.32 <1 <1 <1 <1 <1 <1 <1 <1 1.5 0.56 <1 <0.4 <1 <1 <1 <1 <1 <1 Lead 15 10 15 0.38 <5 0.22 <0.5 <0.5 <10 <10 <10 <10 <0.15 4.8 <5 0.26 <0.5 <0.5 Manganese 50 50 NS 290 310 416 490 370 410 800 1,200 620 670 740 780 Mercury 1 0.2 2 <0.028 <0.1 <0.2 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.028 <0.1 0.16 <0.2 <0.2 Methylene Chloride 5 1 NS 0.24 <I <5 <5 <5 <5 <1 <I <1 <I <0.42 <1 <0.4 <5 <2 <5 1 <5 <2 <5 Nickel 100 50 NS 3.5 <40 <5 1 2.4 1.2 2.4 <40 <40 <40 <40 9.8 IS 1 7.4 9.1 8.5 9.7 Selenium 20 10 50 1.4 1 <10 <2.5 <2.5 <2.5 <10 <10 <10 <10 4.1 <10 1 <2.5 <2.5 <2.5 Sulfide NS 1,000 NS <I00 <100 Silver 20 10 NS <1.7 <5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <1.7 <5 <0.5 <0.5 <0.5 Tetrahydrofuan NS NS NS 3.4 <5 <10 <10 <10 <10 <10 36 37 33 30 1 24 24 29.7 25 26 <10 24 15 23.4 24 Thallium** 0.2 5.5 2 <5.4 <2 <2 <2 <5.4 <2 <2 <2 Tin 2000 100 NS <5 <5 Vanadium** 0.3 25 NS 7.2 14 7.6 <5 <5 <5 <50 <50 <50 <50 7 110 6.1 5.5 3.2 1 6 Vinyl Chloride 0.03 1 2 2.1 3.3 <1 7.9 1.6 1.3 <1 12 13 3 6.2 6.6 5.5 2.1 6 7.2 2.4 2.5 1.8 2.4 1.7 Zinc 1000 10 NS 85 12 <10 1 <20 <20 <10 <20 <20 <20 <20 78 32 1 10 <20 <20 <10 Alkalinity NS NS NS 1 310,000 1 310,000 398,000 420,000 1 450,000 480,000 1 620,000 700,000 703,000 750,000 790,000 830,000 Ammonia-N 1,500 NS NS 96 <10 <I00 85 <10 <100 720 Iron 300 300 NS 2,800 550 210 240 161 Ito 160 230 Total Dissolved Solids 500,000 NS NS 590,000 450,000 612,000 730,000 690,000 721000 1,200,000 1,100,000 1,080,000 1,300,000 1,300,000 1,300,000 Sulfate 250,000 250,000 NS 80,700 92,000 100,000 99,000 145,000 170,000 190,000 17Q000 Carbon Dioxide NS NS NS 870,000 tom# 1,400,000 2,100,000 Chloride 250,000 NS NS 28,000 23,000 34,300 37,000 42,000 49,000 84,000 79,000 91,500 1 1 85,000 1 91,000 1 1 100,000 Not,: All units we in µg/L unless ofl-ised indicated NCDEQ Standard= 15A NCAC 02L .0202 Groandwater Stds (Eff. 2013) * Interim Maximum Allawable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and belaw the adjusted reporting limit B=Compound was f d in the blank and sample. n= Refer to Case N-tr a for further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent m®m®m®®®m®m®m®m®m®m®m®m®m „ Notes: All —its are in pg/L uuless othe—ised indicated NCDEQ Staudaul = 1SA NCAC 02L .0202 Gmmdwater Stds (Eff. 2013) • interim Mabmum Allowable Con autiou (Eff. 2013) Laboratud— Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjustedrep-ling limit B=Compom l was fond in the blank and sample. cu= Refer to Case Narrative fr further detail Bold /yellow values exceed the NCDEQ Staudaul Blue values exceed the Solid Waste Section Limit (SW SL) (Eff. 2011) Red values exceed the Mmtimum Couceatration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL M Laboratory*** Sample Date 5.13.09 10.18.11 4.12.12 1024.12 4.25.13 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.27.17 TA 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 Acctonc 6000 100 NS 7 2.7 J <25 <25 QO <20 <20 <20 <20 <16 <20 <25 <5 <5 <5 2.7 J - <20 <20 <20 <20 1.8 <20 Antimony** 1 6 6 <6 <6 <6 <6 <10 <10 <10 <10 <10 0.45 <5 <3 <3 <3 <3 <10 <10 <10 <10 0.52 Arsenic 10 10 10 2.7 <10 <10 <10 <10 <10 <10 <10 <10 1.2 <10 <10 0.77 3.8 14 <10 <10 <10 <10 1.3 <10 Barium 700 100 2000 20 2255 <100 288 310 320 300 320 300 290 270 265 190 220 1600 210 220 240 190 220 120 Benzene 1 1 5 <10 <10 <10 <10 <1 <1 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 0.35 J <1 <1 <1 <1 0.5 <1 Beryllium** 4 1 4 <1 <1 <I <1 <4 14 <4 <4 <4 <0.12 <1 <1 <1 6.1 <4 <4 <4 <4 <0.12 Bromodichloromethane 0.6 1 NS <1 <I <I <I <1 <I <1 <I <1 <0.23 <I <1 <I <1 <l <1 <1 <1 <1 <0.23 Bromoform 4 3 NS <1 <1 <1 <I <1 <I <1 <I <1 1.2 <1 <1 <1 <I <1 <1 <1 <1 <1 <0.35 2-Butanma,(MEK) 4,000 too NS <5 <5 <5 <5 <10 <10 <10 <10 <10 <18 <5 <5 <5 <5 <5 <10 <10 <10 <10 <18 Cadmium 2 1 5 <1 <1 <1 <1 <2 <2 <2 <2 <2 0.15 0.27 <1 0.25 <0.5 3.1 <2 2< <2 <2 <0.044 <2 Calcium NS NS NS 140,000 130,000 154,000 190,000 180,000 Chloroethane 3000 10 NS <1 <1 <1 <1 <2 <2 <2 <2 <2 <0.28 <1 <1 <1 <1 <1 <2 <2 <2 <2 <0.28 Chloroform 70 5 70 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.21 <1 <2 <2 <2 <2 <1 <1 <1 <1 <0.21 Chromium 10 10 100 <10 <10 <10 <10 <5 <5 <5 <5 <5 1.3 <5 <5 3.9 <0.5 58 <5 <5 <5 <5 <6.3 <5 Cobalt** 1 10 NS <10 <10 <10 <10 1 <25 <25 <25 <25 <25 0.5 <25 <5 1 0.86 2.7 32 <25 <25 <25 <25 1.8 <25 Copper 1,000 10 1,300 <10 <10 <10 1 9.6 J <5 10 11 20 1 6.5 6.8 5.9 1 6 8.5 3.2 450 1 11 <5 <5 1 <5 1.3 <5 Carbon Disulfide 700 35 NS <2 <2 <2 1 <2 <1 <1 <1 <1 <1 <0.45 1 <2 <2 <2 <2 <2 <1 <1 <1 <1 <0.45 Dibromochlormoodu ne 0.4 3 NS <I <1 <1 <1 <I <1 <I <1 <I <0.23 <1 <I <1 <I <1 <L <1 <1 <1 <0.23 l,l-Dichloroethane 6 5 NS <I <1 <1 <1 <1 <I <1 <t <1 <0.19 <1 <I <1 <I <1 <1 <1 <I <1 <1 <0.19 <I l,l-Dichloroeth- 350 5 7 <1 <I <I <I <1 <I <1 <1 <1 <0.31 <1 <1 <1 <1 <1 <1 <1 <I <1 <1 <0.31 <I 1,4-Dichlorobenzcne 6 1 NS <1 <1 <1 <I <1 <I <1 <1 <1 <0.19 <1 <1 <1 <1 <1 <1 <1 <1 <1 <7 <0.19 <1 cis-1,2-Dichlorocthcne 70 5 70 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.2 <1 Ethylbenzene 600 1 0.7 <I <1 <1 <1 <1 <1 <1 <1 <1 <0.21 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <I <1 <0.21 2-Hexamme NS 50 NS <0.26 <5 <5 <5 <5 <5 <0.26 4-Methyl-2-pentamme NS 100 NS 1 <5 <5 <5 <5 <5 <0.29 Toluene 600 1 1000 <I <1 <1 <1 <I <1 <I <1 <I 0.4 <1 <0.5 <0.5 1 <0.5 <0.5 <I <t <1 <1 0.4 Xylenes 500 5 10 <2 <2 <2 1 <2 <1 <I <1 <I 1.4 <0.32 <1 <1 <1 <1 <I <1 <1 <1 1.1 0.39 Lead 15 10 15 <10 <10 <10 <10 <10 <10 <10 <10 QO 0.29 <10 5.1 0.65 2.3 94 <10 <10 <10 <10 I <0.15 <10 Manganese 50 50 NS 150 25 3,510 170 1,500 5,000 1,600 1,300 Mercury 1 0.2 2 <0.2 <0.2 <0.2 <0.2 <0.1 0.17 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 0.81 <0.1 <0.1 <0.1 <0.1 <0.028 <0.1 Methylene Chloride 5 1 NS <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.42 <1 <5 <5 <5 <5 <1 <1 <1 <1 <0.42 Nickel 100 50 NS I <50 1 11.7 <50 13.1 J <40 <40 <40 <40 <40 12 15 <5 17 1 2.3 42 1 <40 <40 <40 <40 5.8 <40 Selenium 20 10 50 <10 <10 <10 <10 <10 <10 <10 <10 <10 1 1.7 <10 <2.5 1.5 9.4 <10 I <10 <10 <1 <9.5 Sulfide NS 1,000 NS I I <100 Silver 20 10 NS <I0 <10 <10 <10 <5 <5 <5 <5 <5 <L7 1 <5 <0.5 1 <0.5 0.49 J <5 <5 <5 <5 <1.7 Tetrahydrofuran NS NS NS <10 <10 <10 I <10 <5 <5 <5 <5 <5 <0.57 <5 34.8 <10 <10 I <10 25 18 25 27 33 2.9 7.2 Thallium** 0.2 5.5 2 <5.5 <5.5 <5.5 <5.5 <5A <2 <2 <2 Tin 2000 t00 NS <5 Vanadium** 0.3 25 NS <25 <25 <25 <25 <50 <50 <50 <50 <50 3.6 <50 <5 3.8 2.7 160 <50 <50 <50 <50 5.7 <50 Vinyl Chloride 0.03 1 2 <1 <I <1 <1 <1 29 1.6 <I <1 <0.5 <1 <1 0.7 <0.5 <0.5 <1 4.7 5.7 <1 1.8 1.5 2.7 Zinc 1000 1 10 NS I <10 1 26 <10 28 21 130 40 60 1 20 81 23 <10 20 16 400 20 25 <20 56 <20 Alkalinity NS NS NS 675,000 <5000 662,000 670,000 660,000 420,000 791,000 530,000 750,000 750,000 1 730,000 850200 Ammonia-N 1,500 NS NS 63 <10 <100 87 <10 Iron 300 300 NS 1 2,380 990 2,400 76,000 Total Dissolved Solids 500,000 NS NS 692,000 1 <25,000 773,000 700,000 870,000 490,000 942,000 1 720,000 910,000 870,000 910000 920000 Sulfate 250,000 250,000 NS 26,100J 1 <5000 31,300 17,000 43.700 30,000 1 1 38,000 36,000 Carbon Dioxide NS NS NS 900,000 500,000 1 1 i 1 990,000 ####### Chloride 250,000 NS NS 27,000 <5000 30,000 30,000 37,000 34,000 31,900 31,000 36,000 39,0009: 21,000 20,000 Notes. All mots are in pg/L mless otherwised indicated NCDEQ Standard = l5A NCAC 02L .0202 Gaum l-ter Std. (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compom l was fond in the blank and sample. cn= Refer to Case Narrative for fimther detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Masi- Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit' = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-6D (cont.) MW-6D-1 Laboratory*** Sample Date 10.27.16 MJA= 4.28.17 M&M 6.15.17 TA 10.10.17 T 4.10.18 1023.14 424.15 1021.15 422.16 1027.16 428.17 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 5.1.17 Acetone 6000 100 NS <25 6.7 <5 15 15 <20 <20 2.3 <20 <25 6.7 <5 <5 <5 <20 <20 <20 <20 <16 <20 <25 <5 Antimony** 1 6 6 <5 <3 <3 <3 <3 <10 <10 0.43 <5 <3 <3 <3 <3 <10 <10 <10 <10 1.7 <5 <3 Arsenic 10 10 10 <10 2 0.35 0.63 J <10 <10 L7 2.7 <10 2 2.7 4.8 <10 <10 <10 <10 0.67 <10 <10 0.43 Barium 700 100 2000 244 360 270 260 250 230 290 290 372 360 380 410 260 250 240 310 260 290 2 44 330 Benzene 1 1 5 <1 2.6 0.71 0.66 0.51 <1 <1 <0.21 <1 <1 2.6 1.7 1.4 0.41 J <1 <1 <1 <1 10.21 <1 <l 0.35 Beryllium- 4 1 4 <1 <1 <1 <1 <4 <4 <0.12 <1 <1 <1 <I <4 <4 <4 <4 <0.12 <1 <I Bromodichloromethane 0.6 1 NS <I <1 <1 <I <1 <I <1 <0.23 <I <1 <I <1 <I <1 <I <1 <I <0.23 <1 <I Bromoform 4 3 NS <I <l <1 <1 <1 <1 <1 <0.35 <I <1 <I <1 <I <1 <1 <1 1 <1 <0.35 1 <1 <l 2-Butamme(MEK) 4,000 100 NS <5 <5 <5 <5 <5 <10 <10 <18 <5 <5 <5 <5 <5 <10 <10 <10 <10 <18 <5 <5 Cadmium 2 1 5 <1 <0.5 <0.5 <0.5 <2 <2 0.13 <2 <1 <0.5 <0.5 <0.5 <2 <2 <2 <2 0.052 Q <I <0.5 Calcium NS NS NS 188,000 150,000 140,000 160,000 86,000 91,000 89,200 Chloroethane 3000 10 NS <1 <1 <I <1 <1 <2 <2 <0.28 <1 <I <1 <I <1 <2 <2 <2 <2 <0.28 <I <1 Chloroform 70 5 70 <1 <2 <2 <2 <2 <1 <1 <0.21 <1 <2 <2 <2 <2 1 <I <1 <I <1 <0.21 <1 <2 Chromium 10 t0 t00 <5 4.2 3.2 6.8 <5 <5 0.65 <5 17.3 4.2 <0.5 3.3 J <5 <5 <5 <5 0.67 <5 <5 18 Cobalt** 1 t0 NS <5 6.5 3.3 3.9 <25 1 <25 0.72 <25 <5 6.5 1 0.85 0.65 J <25 <25 <25 <25 1.4 <25 <5 67 Copper 1,000 10 1,300 1 7.5 2.2 3.5 11 <5 <5 0.85 1 <5 19.6 2.2 0.94 1.4 J 6.3 <5 <5 45 4.8 8.9 <5 26 Carbon Disulfide 700 35 NS <2 <2 <2 <2 <2 <1 <1 2.8 <2 <2 <2 <2 <2 <1 I <1 <1 I <1 <0.45 1 <2 <2 Dbromochloromethane 0.4 3 NS <1 <1 <1 <1 <1 <1 <I <0.23 <1 <1 <1 <I <1 <I <1 <I <1 <0.23 <1 <1 l,l-Dichloroethane 6 5 NS <1 <1 <I <1 <I <1 <I <0.19 <I <1 <I <1 <I <1 <I <1 <1 <1 <0.19 <I <1 l,l-Dichloroethene 350 5 7 <1 <1 <I <1 <I <1 <1 <0.31 <I <1 2.8 <I <1 <I <1 1.3 2.3 <1 2.6 2.4 <1 2.8 1,4-Dichlorobenzrnc 6 1 NS <I <1 <1 <1 <1 <1 <1 <0.19 <1 <1 <1 <I <1 <I <1 <1 <1 <1 <0.19 <1 <1 <1 cis-1,2-Diehlm.ethcne 70 5 70 <I <1 <1 <1 <1 <1 <1 <0.2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.2 <l <1 <l Ethylbenzene 600 1 0.7 <1 <0.5 <0.5 <0.5 <0.5 <I <1 <0.21 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <0.5 2-Hexanonc NS 50 NS <5 <5 <5 <5 <5 <0.26 <5 <5 <5 <5 <5 <0.26 <5 1 <5 4-Methyl-2-pentanone NS 1 100 NS 1 <5 <5 1 <5 <5 <5 <0.29 1 <5 <5 <5 <5 1 <5 <0.29 <5 <5 Toluene 600 1 1000 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 0.7 <1 <0.5 <0.5 <0.5 <0.5 <I <1 <I 1.1 0.66 <I <0.5 Xylenes 500 5 10 <1 <1 <I <1 <I <1 1.1 0.54 <1 <1 <1 <1 <t <1 <I <1 1.5 0.43 <1 <I Lead 15 10 15 <5 0.16 0.19 <0.5 <10 <I0 <I0 <5 0.16 <0.5 <0.5 <10 13 <10 <10 0.51 1. i <5 2.4 Manganese 50 50 NS 3,560 370 6,900 7200 370 480 355 370 300 410 190 200 88.9 160 Mercury 1 0.2 2 <0.2 <0.2 <0.2 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.028 <0.11 <0.2 Methylene Chloride 5 1 NS <l <5 <5 <5 <5 <1 <1 0.35 <1 <5 <5 <5 <5 <1 <I <1 <1 0.27 <1 <5 Nickel 100 50 NS 8.6 5 13 19 <40 <40 2.5 <40 12.1 5 2 2 <40 <40 <40 <40 1.9 <40 <5 12 Selenium 20 10 50 <10 <2.5 1.2 <2.5 <10 <10 1.2 <10 <2.5 1.3 <2.5 <10 <10 <10 <10 1.6 <10 <2.5 Sulfide NS 1,000 NS <100 I <100 <100 Silver 20 10 NS <5 <0.5 <0.5 <0.5 <5 <5 <1.7 <5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <1.7 <5 0.13 Tetrahydrofuran NS I NS NS 29.4 13 67 48 44 120 11 11 7 11.2 13 11 10 9.9 J <5 <5 <5 <5 <0.57 <5 <10 <10 Thallium** 0.2 5.5 2 <5.4 <2 <2 <2 <5.4 <2 <2 <2 <5.4 <2 Ti. 2000 100 NS <5 <5 Vanadium- 0.3 25 NS <5 <5 3.3 3.7 J <50 <50 1.8 <50 7.3 <0.5 7.3 1 <5 1 <50 <50 <50 <50 3.8 5.7 <5 13 Vinyl Chloride 0.03 1 2 <I 3.7 <0.5 1 <0.5 <1 3.8 <1 0.79 1.6 <1 3.7 <0.5 <0.5 <I 1.4 1.4 3.3 1.1 1.6 2.2 <1 9.3 Zinc 1000 t0 NS 30.3 <20 8.3 19 <20 <20 73 <20 <10 <20 <20 <10 <20 <20 48 32 73 16 <10 18 Alkalinity NS NS NS 1 953,000 1 620,000 780,000 750,000 1 500,000 570,000 1 637,000 1 620,000 650,000 680,000 310,000 1 390,000 376,000 400,000 Ammonia-N 1,500 NS NS 68 <10 140 190 <1 <I00 Iron 300 300 NS 480 780 5,330 2,100 3,300 6,500 180 3,900 Total Dissolved Solids 500,000 NS NS 960,000 890,000 600,000 620,000 666,000 750,000 700,000 730,000 470,000 490,000 485,000 550,000 Sulfate 250,000 250,000 NS =25,10024,'1000 28,000 28,000 11,000 13,000 13,000 33,200 25,000 Carbon Dioxide NS NS NS 490,000 590,000 370,000 540,000 Chloride 250,000 NS NS 27,000 29,000E1 1 25,000 25.000 29,600 24,000 1 25,000 1 27,000 1 44,000 44,000 55,600 51,000 Notes: All units are m µg/L unless ofl-ised indicated NCDEQ Standard= ISA NCAC 02L .0202 Groundwater Stds (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Labomtories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compound was limad m the blank and sample. n= Reter W Case Nwwtive for father detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL IV MW-7 (cont.) FF MW-7D Laboratory*** Sample Date 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 5.1.17 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.28.16 5.1.17 Acetone 6000 100 15 15 <5 <20 <20 <20 <20 <16 <20 <25 <5 <5 <5 <5 <20 <20 <20 <20 <16 <20 <25 <5 Antimony** 1 613 <3 <3 <10 <10 <10 <10 0.56 <5 <3 <3 <3 <3 <10 <10 <10 <10 0.21 <5 <3 Arsenic 10 10 t <1 0.831 <10 <10 <10 <10 0.45 <10 <10 0.28 0.86 0.691 <10 <10 <10 <10 0.29 <10 <10 <1 Barium 700 100 330 410 220 300 260 300 280 270 276 270 340 320 190 220 210 180 19 200 200 210 Benzene 1 1<0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <1 <0.5 Beryllium** 4 1 <1 <1 <4 <4 <4 <4 <O.12 <1 <1 <I <1 <4 <4 <4 <4 <O.12 <I <1 Bromodichlmmnethane 0.6 1 NS <I <1 <1 <1 <1 <1 <I <0.23 <1 <1 <1 <I <1 <I <1 <I <1 <0.23 <I <1 Bromolmrn 4 3 NS <I <1 <1 <1 <1 <1 1 <1 <0.35 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.35 <1 <1 2-Bumm- (MEK) 4,000 100 NS <5 <5 <5 <10 <10 <10 <10 <18 1 1 <5 <5 <5 <5 <5 <10 <10 <10 I <10 <18 1 <5 <5 Cadmium 2 1 5 <0.5 <0.5 <2 <2 <2 <2 <0.044 <2 <1 <0.5 <0.5 <0.5 <2 <2 <2 <2 <0.044 <2 <1 <0.5 Calcium NS NS NS 61,000 63,000 58,200 82,000 84,000 84,600 Chloroethane 3000 10 NS <1 <1 <1 <2 <2 <2 <2 <0.28 <1 <1 <1 <1 <1 12 <2 <2 <2 <0.28 <1 <1 Chloroform 70 5 70 <2 <2 <2 <1 <1 <I <1 0.23 <1 <2 <2 <2 <2 1 <1 <1 <1 <1 <0.21 <1 <2 Chromium 10 10 100 2A 35 <5 <5 <5 <5 <6.3 <5 <5 2.4 18 15 <5 <5 <5 <5 <6.3 <5 <5 <0.5 Cobalt** 1 I t0 NS 0.7 4.2 <25 <25 <25 <25 0.47 <25 <5 2.3 3.4 2.1 <25 <25 <25 <25 <2.6 <25 <5 <1 Copper 1,000 1 10 1,300 1 2 44 <5 <5 <5 7.8 1.6 1.4 <5 1.3 9.6 9.4 <5 <5 <5 <5 0.44 1.4 <5 <2 Carbon Disulfide 700 35 NS <2 <2 <2 <1 <l <1 <1 0.62 <2 <2 <2 <2 <2 <1 <1 <1 <1 1.8 <2 <2 Dbromochloromethane 0.4 3 NS <l <1 <1 <1 <1 <1 <1 1 <0.23 1 <1 <1 <1 <1 <1 <1 <1 <1 I <t 1 <0.23 <1 <I l,l-Dichloroethane 6 5 NS <1 <I <1 <I <1 <1 <1 <O.19 <I 2.2 <1 <1 <1 <1 <1 <1 <1 <0.19 <I <1 <1 l,l-Dichloroethene 350 5 7 <1 <1 <1 <1 <1 1.1 <1 1.4 1.9 <1 <1 <1 <I <1 <1 1.1 <1 1.5 1.9 <1 2 1,4-Dichlorobenzene 6 1 NS <I <1 <I <1 <I <1 <1 <0.19 <I <1 <I <1 <I <1 <I <1 <I <1 <0.19 <1 <I <1 cis-1,2-Dichloroethene 70 5 70 <I <1 <l <1 <1 <1 <1 <0.2 <1 <1 <1 <1 <1 <1 <I <1 <1 <1 <0.2 <1 <l <1 Ethylbenzene 600 1 0.7 <0.5 <0.5 <0.5 <1 <l <1 <1 <0.21 <1 <0.5 <0.5 <0.5 <0.5 -1 <1 <1 <1 <0.21 <1 <0.5 2-Hexanone NS 50 NS <5 <5 <5 <0.26 <5 <5 <5 <5 <5 <0.26 <5 <5 4-Methyl-2-pentanone NS 1 100 NS <5 <5 <5 <0.29 <5 <5 <5 <5 <5 <0.29 <5 <5 Toluene 600 1 1 1000 <0.5 <0.5 <0.5 <1 <I <t <1 0.5 <I <0.5 <0.5 <0.5 <0.5 <1 <1 <1 Ll 0.76 <1 <0.5 Xylenes 500 5 10 <1 <I <1 <I <I <I 1.6 0.38 <1 <1 <1 <1 <1 <1 <1 <1 1.4 0.5 <1 <1 Lead 15 10 15 0.2 4.7 <10 <10 <10 <10 <0.15 <10 <5 0.21 0.81 0.58 <10 <10 <10 <10 <O.15 <10 <5 0.22 Manganese 50 50 NS 130 290 200 65 64.4 47 120 92 170 83 90.7 50 Mercury 1 0.2 2 <0.2 0.53 <O.1 <0.1 <O.1 <0.1 0.21 <O.1 0.12 0.94 0.35 <O.1 <O.1 <O.1 <0.1 <0.028 <O.1 <0.2 Methylene Chloride 5 1 NS <5 <5 <5 <1 <l <1 <I <0.42 < <5 <5 <5 <5 <I <1 <1 <1 <0.42 <l <5 Nickel 100 50 NS 2 17 <40 <40 <40 <40 1.6 <40 <5 2.1 11 8.6 <40 140 <40 <40 1.1 <40 <5 <2 Selenium 20 10 50 13 <2.5 <10 <10 <10 <10 1.4 <10 <2.5 1.5 <2.5 <10 <10 <10 <10 <9.5 <10 <2.5 Sulfide NS 1,000 NS <100 <100 Silver 20 10 NS <0.5 <0.5 <5 <5 <5 <5 <1.7 1 <5 <0.5 <0.5 <0.5 <5 <5 <5 <5 <1.7 <5 <0.5 Tetrahydrofuran NS I NS NS <10 10 <10 <5 <5 <5 <5 <0.57 <5 <10 <10 <10 <10 <10 <5 <5 <5 <5 0.63 <5 <10 5.2 Thallium** 0.2 5.5 2 <2 <2 <5.4 <2 <2 <2 <5.4 <2 Tin 2000 100 NS <5 <5 Vanadium** 0.3 25 NS 1 <5 19 <50 <50 <50 <50 3.9 <50 7.5 5.2 1 15 11 <50 <50 <50 <50 <15 <50 <5 <5 Vinyl Chloride 0.03 1 2 <0.5 <0.5 <I <1 <l <1 <1 <0.5 <I <1 3.2 <0.5 <0.5 <1 <l 1.3 1.6 <1 0.64 1 1.1 1 <l 4 Zinc 1000 t0 NS <20 30 <20 <20 QO <20 74 <20 <10 <20 19 13 <20 <20 <20 QO 50 <20 <10 <20 Alkalinity NS NS NS 440,000 490,000 230,000 270,000 242,000 260,000 280,000 290,000 270,000 310,000 323,000 320,000 Ammonia-N 1,500 NS NS 1 53 <10 <100 73 <10 <100 Iron 300 300 NS 160 1 7,300 1 1,540 800 4,800 3,200 332 610 Total Dissolved Solids 500,000 NS NS 560,000 620,000 350,000 370,000 376,000 420,000 410,000 400,00(1 390,000 410,000 433,000 480,000 Sulfate 250,000 250,000 NS 35,000 26,000 21,100 20,000 22,000 22,000 23,100 27,000 Carbon Dioxide NS NS NS 350,000 460,000 310,000 400,000 Chloride 250,000 NS NS 47,000 57,000 30,000 32,000 37,500 36,000 38,000 46,000 35,000 35,000 48,500 1 42,000 Notes: All units are in µg/L unless otherwised indicated NCDEQ Standard= 15A NCAC 02L .0202 Groundwater Stds (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) 1= Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compound was faundm the blank and sample. n= Refer to Case Narrative for fiutlrer detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL M nt) MW-8D Laboratory*** Sample Date 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.28.16 4.28.17 6.15.17 10.11.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 J4.22.16W<2.16J4.28.17Acctonc 6000 100 NS <5 <5 <5 <20 <20 20 360 27 32 <25 8.9 <5 <5 4.4 J cn <20 QO <20 <20 <16 Antimony** 1 6 6 <3 <3 <3 <10 <10 <10 <10 3.1 <5 <3 <3 <3 <10 <10 <10 <10 0.21Arsenic 10 10 10 <1 0.29 J <10 <10 <10 <10 <26 <10 <10 2.9 1.5 <10 <10 <10 <10 0.52 0Barman 700 100 2000 220 230 230 200 57 45 150 37 130 140 140 140 91 91 34 72 55 115Benzene 1 1 5 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <1 Beryllium** 4 1 4 <1 <1 <4 <4 <4 <4 <0.12 <1 0.91 0.64 <4 <4 <4 <4 <0.12 <1Bromodichloromethane 0.6 1 NS <I <1 <I <1 <I <1 <I <0.23 <1 <I <1 <0.5 <1 <I <1 <1 <1 <0.23 <1Bromoform 4 3 NS <I <1 <1 <1 <1 <1 <1 <0.35 <1 <I <1 <1 <I <1 <1 <1 <0.35 <1 2-Butamme(MEK) 4,000 100 NS <5 <5 <5 <10 <10 <10 <10 <18 <5 <5 <5 <5 <10 <10 <10 <10 <18 <5 <5 Cadmium 2 1 5 <0,5 <0.5 <2 <2 <2 <2 <0.044 <2 <1 0.37 0.52 <0.5 <2 <2 <2 <2 <0.044 <2 <1 0.23 Calcium NS NS NS 57,000 43,000 47,800 85,000 85,000 119,000 Chloroethane 3000 10 NS <1 <1 <1 <2 <2 <2 <2 <0.28 <1 <1 <I I <1 <1 <2 <2 <2 <2 <0.28 <1 <1 Chloroform 70 5 70 <2 <2 <2 1 <1 <1 <1 <1 <0.21 <1 <2 <2 <2 1 <2 1 <1 <1 <1 <1 <0.21 <1 <2 Chromium 10 10 100 <0.5 <5 6.6 29 5.7 <5 16 <5 17.1 62 870 1 <5 <5 <5 <5 1.3 <5 <5 140 Cobalt** 1 t0 NS <1 <1 <25 <25 <25 27 45 6.4 48.4 38 37 <25 <25 <25 <25 1.4 <25 7.9 47 Copper 1,000 10 1,300 1 <2 <2 35 120 15 <5 60 2.1 47.1 100 110 38 <5 30 6.5 4.5 16.2 78 Carbon Disulfide 700 35 NS <2 <2 <2 <1 <I <1 <I 1 2.6 1 <2 <2 <2 <2 <2 <I <1 <1 <1 1 0.5 1 <2 1 <2 Dibromochloromethane 0.4 3 NS <l <1 <l <1 <l <1 <1 <0.23 <1 <1 <1 <1 <1 <1 I <1 <1 <1 <0.23 <1 <1 1,1-Dichloroethane 6 5 NS <l <1 <l <1 <l <1 <1 <0.19 <t <1 <1 <1 <1 <1 <1 <t <1 <t <0.19 4.2 <1 <1 l,l-Dichloroethene 350 5 7 <1 <1 <1 <1 <1 <1 <1 0.7 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.69 <1 <1 0.81 1,4-Dichlmobenzene 6 1 NS <1 <1 <1 <1 <I <1 <1 <0.19 <I <1 <I <1 I <I <1 <I <1 <I <1 <0.19 <1 <1 <I 6s-1,2-Dichloroethene 70 5 70 <I <1 <I <1 <1 <1 < <0.2 <1 <1 <1 <1 <1 <1 <l <1 <1 <1 <0.2 <1 <1 <l Ethylbenzene 600 1 0.7 <0.5 <0.5 <0.5 <1 <1 <1 <l <0.21 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <0.5 2-Hexanone NS 50 NS <5 <5 <5 1 <0.26 <5 1 <5 <5 <5 <5 <0.26 <5 <5 4-Methyl-2-pentanone NS 100 NS <5 <5 <5 1 <0.29 1 <5 <5 <5 <5 <5 <0.29 <5 <5 Toluene 600 1 1000 <0.5 <0.5 <0.5 <l <1 <I <1 <0.24 <1 <0.5 <0.5 <0.5 <0.5 <1 <I <1 <I 0.76 <I <0.5 Xylenes 500 5 10 <1 <I <1 <I <1 <I <1 <0.32 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.49 <1 <1 Lead 15 10 15 <0.5 <0.5 15 27 <10 <10 15 <10 7.4 <0.5 13 <10 <10 <10 <10 0.23 <10 <5 <0.5 Manganese 50 50 NS 48 46 4,400 2,400 4,280 3,100 4,300 81 130 254 670 Mercury 1 0.2 2 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 0.12 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 Methylene Chloride 5 1 NS <5 <5 <1 <1 <1 <1 <0.42 <1 <5 <5 <5 <5 <1 <1 <1 <1 0.38 <1 <5 Nickel 100 50 NS <2 <2 <40 <40 <40 <40 26 <40 228 46 470 <40 <40 <40 <40 2.9 <40 9.9 110 Selenium 20 10 50 <2.5 <2.5 <10 <10 <10 <10 <9.5 <10 <2.5 2.3 <10 <10 <10 <10 1.7 <10 1.6 Sulfide NS 1,000 NS <100 2.8 <100 Silver 20 10 NS <0.5 <0.5 <5 <5 <5 <5 <1.7 <5 0.34 <0.5 <5 <5 1 <5 <5 <1.7 <5 <0.5 Tetrahydrofaan NS NS NS <10 <10 <10 <5 1 <5 <5 <5 <0.57 <5 <10 <10 <10 <10 <10 <5 <5 <5 <5 <0.57 <5 <10 <10 Thallium** 0.2 5.5 2 <2 <2 1 1 6.1 <2 1 <2 6 <2 Ti. 2000 100 NS <5 Vanadium** 0.3 25 NS <5 <5 82 120 <50 <50 59 <50 511 77 72 <50 <50 <50 <50 4.2 <50 28 76 Vinyl Chloride 0.03 1 2 <0.5 <0.5 <1 <1 <1 1.1 <I <0.5 <1 <1 0.45 <0.5 <0.5 <1 1.6 1.7 2.1 <1 <0.5 0.66 <1 3.2 Zinc 1000 to NS <20 <10 71 180 28 <20 130 <20 537 88 79 <20 <20 <20 970 33 1.6 17.8 69 Alkalinity NS NS NS 340,000 350,000 250,000 260,000 1 280,000 <5000 290,000 300,000 250,000 280,000 355,000 <5000 Ammonia-N 1,500 NS NS 1 460 1,800 270 1 <50 <10 <100 Iron 300 300 NS 1 620 650 16,600 23,000 29,000 9,510 31,000 Total Dissolved Solids 500,000 NS NS 48Q,000 460,000 220,000 300,000 332,000 430,000 420,000 370,000 430,000 410,000 509,000 560,000 Sulfate 250,000 250,000 NS 26,000 28,000 50,200 41,000 46,000 43,000 14,700 17,000 Carbon Dioxide NS NS NS 290,000 440,000 240,000 280,000 Chloride 250,000 NS NS 40,000 48,000 1,100 6,400 9,000 1 10,000 1 1 12,000 1 12,000 1 1 55,000 53,000 77,200 71,000 Notes: All units me in µg/L unless cal-ised indicated NCDEQ Standard= 15A NCAC 02L .0202 Groundwater Stds (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Labomtories= Pace (P), Shealy (S), and Test America (TA) J = Estimated conc. above the adjusted method detection limit and below the adjusted reporting limit B=Compound was faundm the blank and sample. n= Refer to Case Narrative for father detail Bold /yellow values exceed the NCDEQ Shadard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-81) (cons.) MW-9 MW-10 Laboratory*** PR PR PR PR PR PR S S S Sample Date 6.15.17 10.11.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 4.10.18 3.20.98 7.16.98 4.13.99 8.25.99 3.9.00 8.16.00 3.23.01 10.6.01 3.16.02 Acctonc 6000 100 NS 15 15 <5 <20 <20 <20 <20 <16 <20 <25 <5 <5 <5 <50 <50 <50 <50 <50 <50 <20 <20 <20 Antimony** 1 6 6 <3 <3 <3 <10 <10 <10 <10 <O.17 <5 <3 <3 <3 Arsenic 10 10 10 0.15 0.34J <10 <10 <10 <10 0.37 <10 <10 <1 <1 <1 <50 <10 <50 <10 <10 <10 17 <5 <5 Barium 700 1 100 2000 110 81 250 110 210 210 70 65 49.7 42 54 48 <100 <100 <100 100 <100 72 97 120 46 Benzene 1 1 5 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Beryllium** 4 1 4 <1 <1 <4 <4 <4 <4 <O.12 <1 <1 <1 <1 Bromodichloromethane 0.6 1 NS <I <1 <1 <1 <I <1 <1 <0.23 <I <1 <I <1 <5 <5 <5 1 <5 11 <5 <5 <5 <5 1 <5 Bromoform 4 3 NS <1 <1 <1 <1 <1 <1 1 <1 <0.35 1 <1 <1 <1 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 2-Butamme(MEK) 4,000 100 NS <5 <5 <5 <10 <10 <10 1 <10 <18 15 <5 15 1 <5 1 <10 <10 <10 <10 <10 <10 <10 <10 <10 Cadmium 2 1 5 <0.5 <0.5 <2 <2 <2 <2 <0.044 <2 <1 75 <0.5 <0.5 6 <5 <5 <5 <5 <1 <2 <2 <2 Calcium NS NS NS 13,000 14,000 12,200 Chloroethane 3000 10 NS <::I <1 <1 <2 <2 <2 <2 <0.28 <1 <1 <1 <1 <10 <10 <10 <10 <10 <10 <5 <5 <5 Chloroform 70 1 5 70 <2 12 <2 <1 <1 <1 <1 <0.21 <1 <2 <2 <2 <5 <5 <5 <5 <5 15 <5 15 <5 Chromium 10 10 100 13 18 16 <5 12 15 1.7 15 <5 <0.5 <0.5 <5 <5 <5 <50 <5 <5 <5 <5 <5 <5 Cobalt** 1 10 NS 3.3 1.2 <25 <25 <25 <25 1.7 <25 <5 0.41 <1 <1 Copper 1,000 10 1,300 1 7.9 2.9 43 1 13 29 31 4.9 2.6 <5 0.92 <2 0.51 Carbon Disulfide 700 35 NS <2 <2 <2 <1 <1 <1 <1 <0.45 1 <2 <2 <2 <2 <50 1 <50 <50 <50 <50 <50 <5 <5 <5 Dibromochloromethane 0.4 3 NS <l <1 <1 <1 <1 <1 <I <0.23 <1 <I <1 <1 1,1-Dichloroethane 6 5 NS <l <1 <1 <1 <1 <l <I <0.19 <I <1 <I <1 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 1,1-Dichloroethene 350 5 7 <1 <1 <1 <1 <1 <1 <1 <0.31 <I <1 <1 <1 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 1,4-Dichlmobenzene 6 1 NS <I <1 <1 <1 <1 <1 <I <0.19 <1 <1 <1 <1 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 6s-1,2-Dichlaoethene 70 5 70 <1 <1 <I <1 <] <1 <1 <0.2 <1 <1 <1 <1 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 Ethylbenzene 600 1 0.7 <0.5 <0.5 <0.5 <1 <I <1 <l <0.21 <1 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <5 <5 <5 2-Hexanone NS 50 NS <5 <5 <5 <0.26 <5 <5 <5 <5 4-Methyl-2-pentanone NS 1 100 NS 15 <5 <5 1 <0.29 15 <5 <5 <5 Toluene 600 1 1 1000 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.24 1 <1 <0.5 <0.5 <0.5 <5 <5 <5 <5 <5 <5 <5R<5 <5 Xylenes 500 5 10 <1 <1 <1 <I <1 <I <1 <0.32 <1 <I <1 <I <5 <5 <5 <5 <5 <5 <5 <5 Lead 15 10 15 0.74 0.23 J <10 <10 <10 <10 0.54 <10 <5 0.32 <0.5 <0.5 <15 <5 <15 <5 <5 <5 <3 <3 Manganese 50 50 NS 260 ISO 60 34 6.2 30 1.9 <2.5 Mercury 1 0.22 <0.2 <0.20 <0.1 <O.1 <0.1 <O.1 <0.028 <0.1 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 Methylene Chloride 5 1 NS <5 <5 <5 <1 <1 <1 <1 <0.42 <1 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 Nickel 100 50 NS 12 9.2 <40 <40 <40 <40 2.4 <40 15 1 <2 0.73 J Selenium 20 10 50 <2.5 <2.5 <10 <10 <10 <10 <9.5 QO <2.5 <2.5 <2.5 <10 <10 <10 <10 <10 <10 <5 <5 1 <5 Sulfide NS 1,000 NS I <100 Silver 20 10 NS <0.5 <0.5 1 <5 <5 <5 <5 <147 <5 <0.5 <0.5 <0.5 <18 <5 <18 <5 <5 <5 <5 <5 Tetrahydrofuran NS NS NS <10 <10 <10 <5 <5 <5 <5 <0.57 <5 <10 <10 <10 <10 Thallium** 0.2 5.5 2 <2 <2 <5.4 <2 <2 <2 Ti. 2000 100 NS <5 Vanadium** 0.3 25 NS 11 6.3 58 <50 <50 50 63 <50 <5 3.2 2.2 3.4 J F<2 Vinyl Chloride 0.03 1 2 <0.5 <0.5 <1 <I <1 <1 <1 <0.5 <I <1 <0.5 <0.5 <l <10 <10 <10 <10 <10 <10 <2 <2 Zinc 1000 10 NS 16 <10 81 94 83 80 26 <20 <10 <20 <20 <10 Alkalinity NS NS NS 400,000 410,000 1 1 40,000 53,000 50,200 45,000 52,000 47,000 Ammonia-N 1,500 NS NS 1 300 <10 <100 Iron 300 300 NS 4,300 2,400 167 380 75 J Total Dissolved Solids 500000 NS NS 570,000 600,000 250,000 220,000 161,000 160,000 180,000 150,000 Sulfate 250!000 250,000 NS 15,000 15,000 18,500 18,000 15,000 16,000 Carbon Dioxide NS NS NS 100,000 320,000 Chloride 250,000 NS NS 82,000 82,000 14,000 30,000 18,600 9,000 24,000 22,000 Notes: All units are in µg/L unless otherwised indicated NCDEQ Standard= 15A NCAC 02L .0202 Groundwater Stds (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Labomtories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compound was faundm the blank and sample. n= Refer to Case Narrative for father detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL 1ICL MW-10 Cont. Laboratory*** S S S S S P P P P P P P P P P P S S S S S S Sample Date 10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 9.27.06 3.31.07 4.10.08 5.13.09 10.18.11 4.12.12 10.24.12 4.25.13 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 Acctonc 6000 100 NS <20 <2o <20 <20 <20 <25 <25 <25 <25 <25 <25 <25 2.6 <25 <25 <20 <20 <20 <20 <20 2.5 <20 Antimony** 1 6 6 <6 <6 <6 <6 <10 <10 <10 <10 <10 <0.17 Arsenic 10 10 10 <5 <5 <5 <10 <10 <5 <5 <5 <5 <5 <5 2.7 <10 <10 9.6 12 <10 13 <10 <10 5.1 1.2 Barium 700 1 100 2000 58 <25 100 82 91 96 460 130 48 110 96.7 73.9 110 <100 426 220 170 540 250 520 270 390 Benzene 1 1 5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <25 <1 <1 <1 <1 <0.21 <1 Beryllium** 4 1 4 <1 <1 <1 1.5 <1 <4 <4 <4 <4 0.13 Bromodichloromethane 0.6 1 NS 1 <5 1 <5 <5 1 <5 <5 1 <5 1 <5 <5 11 <5 <5 <5 1 <I <I <I <1 14 <1 <I <1 <I <0.23 Bromoform 4 3 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <I <I <1 <I <1 <I <1 <I <0.35 2-Butancte(MEK) 4,000 too NS <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <5 <5 <5 <5 <1 <10 <10 <10 <10 <18 Cadrmmn 2 1 5 <2 <2 <2 <2 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <2 <2 <2 <2 <0.044 <2 Calcium NS NS NS 50,000 100,000 Chloroethane 3000 10 NS <5 <5 <5 <5 <5 <IO <10 <10 <10 <10 <10 <1 <1 <1 <I <2 <2 <2 <2 <2 <0.28 Chloroform 70 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.21 Chromium 10 10 100 <5 <5 <5 <5 <5 <2 49 <2 <2 <5 <5 <10 <10 <10 33 <5 <5 <5 <5 <5 2.4 <5 Cobalt** 1 10 NS <10 6.4 <10 18 <25 <25 <25 <25 <25 6.9 <25 Copper 1,000 10 1,300 <10 <10 <10 65.5 <5 11 <5 <5 <5 5.1 1.4 Carbon Disulfide 700 35 NS <5 <5 <5 <5 <5 <10 <I <10 <10 <10 1.2 <2 <2 <2 <2 <l <1 <I <1 <1 0.48 Dibromochlormoodu ne 0.4 3 NS <l <I <l <1 <l <1 <1 <1 <1 <0.23 l,l-Dichloroethane 6 5 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.19 <1 1,1-Dichloroeth- 350 5 7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <I <1 <I <1 <0.31 <1 1,4-Dichlorobenzcne 6 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <I <1 <I <1 <0.19 <1 cis-1,2-Dichlorocthcne 70 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <I <1 <1 <1 <1 <1 <1 <1 <0.2 <1 Ethylbenzene 600 1 0.7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <I <l <I <I <1 <I <1 <I <0.21 2-Hexamme NS 50 NS <0.26 4-Methyl-2-pentamme NS 100 NS <0.29 Toluene 600 1 1000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <l <I <1 <1 <1 <1 <1 <0.24 Xylenes 500 5 10 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <2 <2 <2 <2 <1 <I <1 <I <1 <0.32 Lead 15 10 15 <3 <3 <3 <3 <3 <5 10 <5 <5 <5 <5 <10 <10 <10 31.1 <10 <10 <10 <10 I <10 1.9 <10 Manganese 50 50 NS 2,900 3,700 Mercury 1 0.2 2 <0.1 <0.1 <0.1 <0.4 <0.4 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 0.12 <0.1 <0.1 <0.1 <0.1 <0.1 <0.028 <0.1 Methylene Chloride 5 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <l <l <l <1 <l <1 <I <1 <l 0.19 Nickel 100 50 NS 1 <50 <50 <50 17 <40 <40 <40 <40 <40 2.3 <40 Selenium 20 10 50 <5 <5 <5 <5 <5 <5 <5 5.4 <5 15 4.3 4.2 <10 <10 <10 <10 <10 <10 <10 <10 <9.5 Sulfide NS 1,000 NS Silver 20 10 NS <5 <5 <5 <5 <5 <2 <2 <2 <2 <5 <5 <10 <10 I <10 <10 <5 <5 <5 <5 <5 <1.7 Tetrahydrofuran NS NS NS <10 <10 <10 <10 <5 <5 <5 <5 <5 0.86 <5 Thallium** 0.2 5.5 2 <5.5 <5.5 <5.5 <5.5 Tin 2000 100 NS Vanadium** 0.3 25 NS <25 7.1 <25 162 <50 <50 <50 <50 <50 12 <50 Vinyl Chloride 0.03 1 2 <2 <2 <2 <2 <2 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 2.2 5.3 7.2 6.7 3.1 0.8 <1 Zinc 1000 1 10 NS 14.6 <10 107 <20 <20 <20 <20 76 <20 Alkalinity NS NS NS 188,000 <5000 175,000 220,000 220,000 580,000 Ammonia-N 1,500 NS NS 1,500 1,500 Iron 300 300 NS Total Dissolved Solids 500,000 NS NS 244,000 <25,000 212,000 130,000 340,000 670,000 Sulfate 250,000 250,000 NS <5000 <5000 2,720 <1,000 Carbon Dioxide NS NS NS 1 320,000 ####### Chloride 250,000 NS NS 11,300 <5000 1 12,300 1 13,000 16,000 30,000 Notes: All mits are in pg/L mless otherwised indicated NCDEQ Standard = l5A NCAC 02L .0202 Gmm l-ter Std. (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compom l was fond in the blank and sample. cn= Refer to Case Narrative far further detail Bold /yellow values exceed the NCDEQ Staudard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit' = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL NM-10 cont. MW-10D MW-11 Laboratory*** P TA TA TA TA S S S S S S P S (split) TA TA TA TA PR PR PR PR Sample Date 10.27.16 5.1.17 6.15.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 10.27.16 5.1.17 6.15.17 10.11.17 4.10.18 3.20.98 7.16.98 4.13.99 8.25.99 Acctonc 6000 100 NS <25 <5 15 <5 15 <20 <20 <20 <20 4 <20 <25 <2 <5 <5 <5 7.2 cn <50 <50 <50 <50 Antimony** 1 6 6 <5 <3 <3 <3 <3 <10 <10 <10 <10 0.64 <5 <3 <3 <3 �3 Arsenic 10 10 10 <10 1.5 1.3 1.2 <10 <10 <10 <10 2.3 <10 <10 1A 1.6 2.3 <50 <10 <50 <10 Barium 700 100 2000 249 290 240 340 290 190 200 200 190 150 244 200 210 220 <100 <100 <100 150 Benzene 1 1 5 <1 0.41 <0.5 <0.5 0.42 J 3.1 2.7 2.9 2.5 1.3 2.5 2.9 2.9 3.2 3.3 3.2 33 <5 <5 <5 <5 Beryllium** 4 1 4 <1 <1 <1 <1 <4 14 <4 <4 <0.12 <I <1 <1 <I Bromodichloromethane 0.6 1 NS <1 <1 <1 <1 <1 <1 <I <1 <1 <0.23 <1 <0.4 <I <I <I <1 <5 <5 <5 <5 Bromoform 4 3 NS <1 <I <1 <t <1 <I <1 <I <1 <0.35 <1 <0.4 <1 <I <I <1 <5 <5 <5 <5 2-Butanma,(MEK) 4,000 100 NS <5 <5 <5 <5 <5 <10 <10 <10 <10 <18 <5 <2 <5 <5 <5 <5 <10 <10 <10 <10 Cadmium 2 I 5 <1 <0.5 <0.5 <0.5 <2 <2 <2 <2 <0.044 <2 <1 0.54 3.1 1,6 <5 <5 <5 <5 Calcium NS NS NS 61,600 380,000 420,000 392,000 Chloroethane 3000 10 NS <1 <1 <1 <1 <1 <2 <2 <2 <2 <0428 <1 <0.4 <I <1 <1 <1 <10 <10 <10 <10 Chloroform 70 5 70 <1 <2 <2 <2 <2 <l <1 <l <1 <0.21 <1 <0.4 <2 <2 <2 <2 <5 <5 <5 <5 Chromium to 10 100 <5 <0.5 <0.5 <5 <5 <5 <5 <5 3.8 <5 9.9 6 6.6 8.2 <5 <5 <50 <5 Cobalt** 1 10 NS <5 4.9 5 5.1 33 <25 26 26 24 25 36.4 38 49 43 Copper 1,000 10 1,300 <5 <2 1.3 <2 68 11 15 7 7.6 15 1,440 460 1,800 460 Carbon Disulfide 700 35 NS <2 <2 <2 <2 <2 <I <1 <I <1 <0.45 <2 <064 <2 <2 1 <2 0.5J <50 <50 <50 <50 Dibromochloromedume 0.4 3 NS <1 <1 <1 <1 <1 <I <1 <I <1 <0423 <1 <0.4 <I <I <I <1 l,l-Dichloroethane 6 5 NS <1 <I <1 <I <1 <1 <1 <1 <1 <0.19 <I <1 <0.4 <1 <I <I <1 <5 <5 <5 <5 1,1-Dich1moethenc 350 5 7 <1 <l <1 <I <1 <1 <1 <1 <1 <0.31 <l <1 <0.4 <1 <1 <I <1 <5 <5 <5 <5 1,4-Dichlorobenzene 6 1 NS <1 <1 <I <I <1 3 2.9 2.4 <I 0.91 1.6 1,9 <0.4 0,19 2.2 L8 2 <5 <5 <5 <5 cis-1,2-Dichloroethene 70 1 5 70 <I <1 <I <1 <I <1 <I <1 <1 <0.2 <I <1 <0.4 <1 <I <I <1 <5 <5 <5 <5 Ethylbenzene 600 1 0.7 <1 <065 <0.5 <0.5 <0.5 <I <1 <I <1 <0.21 <1 <064 <0.5 <0.5 <0.5 <045 <5 <5 <5 <5 2-Ilexanone NS 50 NS <5 <5 <5 1 <5 <5 <0.26 <5 <2 <5 <5 <5 <5 4-Methyl-2-pentamme NS 100 NS 1 <5 1 <5 <5 <5 <5 1 1 1 <0.29 <5 <2 <5 <5 <5 <5 Toluene 600 I 1000 <1 <0.5 <0.5 <0.5 <0.5 <1 <1 <1 3 <0.24 <1 <0.4 <0,5 <0,5 <0.5 <045 <5 <5 <5 Xylenes 500 5 10 <1 <1 <1 <1 <1 <1 <1 <1 4 <0.32 <1 <0.4 <1 <1 <1 <1 <5 <5 <5 <5 Lead 15 10 15 <5 <0.5 <0,5 <045 <10 <10 <10 <10 <10 1 <5 1 1.2 2.9 141 <15 <5 <15 <5 Manganese 50 50 NS 3,480 4,000 4,100 4,600 13,000 17,000 17,000 17000 1 17000 17,000 Mercury 1 0.2 2 <0.2 <0.2 <042 0413 <041 <0.1 <041 <0.028 <0.1 <0.2 0416 <042 <0.2 <0.2 0.2 <0.2 Methylene Chloride 5 1 NS <1 <5 <5 <5 <5 <1 <1 <I <1 <0442 <1 <0.4 <5 <5 7.5 <5 <5 <5 <5 <5 Nickel 100 50 NS <5 <2 <2 L3 J 51 43 <40 40 42 46 50.9 48 60 49 Selenium 20 10 50 <10 <2.5 <2.5 1 <2.5 <10 <10 <10 <10 1 849 <IO <15 1.2 <245 <10 <10 <10 <10 Sulfide NS 11000 NS <100 <100 Silver 20 10 NS <5 <0,5 <0,5 <0.5 <5 <5 <5 <5 <L7 <5 <0,5 0,12 <045 <18 <5 <18 <5 Tetrahydrofuran NS NS NS <10 7A <10 <10 9 J 120 110 91 85 61 54 81 64 76 77 79 97 Thallium** 0.2 5.5 2 <544 <2 <2 <2 1 5.9 <2 <2 Tin 2000 100 NS <5 1 <5 Vanadium** 03 25 NS 5.3 <5 <5 <5 <50 <50 <50 <50 5 <50 52.8 15 1 20 8.7 Vinyl Chloride 0.03 1 2 <1 6.1 <0.5 <0.5 <1 25 27 29 8.1 2.4 11 <1 7.5 18 1 <0.5 <0.5 I <1 <10 <10 <10 <10 Zinc 1000 10 NS <10 <20 <20 <10 37 <20 <20 <20 53 15 22.7 9.6 45 11 Alkalinity NS NS NS 360,000 500,000 380,000 630,000 1,600,000 1,500,000 1,610,000 1,700,000 1,700,000 1,700,000 Ammonia-N 1,500 NS NS 1,500 510 190 <100 Iron 300 300 NS 67,700 60,000 60,000 66,000 9,440 2,300 2,700 2,100 Total Dissolved Solids 500,000 NS NS 430,000 610,000 510,000 830,000 2,300,000 2,300,000 2,260,000 2,500,000 2,500,000 2,400,000 Sulfate 250,000 250,000 NS <2,000 700 780 340 216,000 190,000 140,000 130,000 Carbon Dioxide NS NS NS 2,000,000 2,100,000 Chloride 250,000 NS NS 23,800 32,000 25,000 47,000 in to 140,000 179,000 190,000 20Q,000 20Q000 Notes. All mots are in pg/L mless otherwised indicated NCDEQ Standard = l5A NCAC 02L .0202 Gmm l-ter Std. (Eff. 2013) * Interim Maairnum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compomd was fond in the blank and sample. cn= Refer to Case Narrative for further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maatimmn Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <Report Limit' = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meek Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-11 (cons.) Laboratory*** PR PR S S S S S S S S P P P P P P P P P S Sample Date 3.9.00 8.16.00 3.23.01 10.6.01 3.16.02 10.31.02 3.26.03 9.13.03 3.26.04 12.2.04 4.23.05 10.25.05 3.28.06 4.10.08 5.13.09 10.18.11 4.12.12 10.24.12 4.25.13 10.3.13 Acetone 6000 100 NS <50 <50 <20 QO <20 <20 <20 <20 <20 <20 <25 <25 <25 <25 <25 3.2 <25 <25 <20 <20 Antimony** 1 6 6 <6 <6 <6 <6 <10 <10 Arsenic 10 10 10 <10 <10 15 <5 <5 <5 <5 <5 <10 <10 <5 <5 <5 T <5 8.6 <10 <10 <10 <10 14 Barimn 700 100 2000 140 150 180 220 160 180 170 210 250 300 300 370 220 179 174 343 <100 244 140 270 Benzene 1 1 5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 0.9 <10 <10 <10 0.87 <1 1 Beryllium** 4 1 4 <I <1 <1 <1 <4 <4 Bromodichloromethanc 0.6 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 Bromoform 4 1 3 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 1 <5 <5 1 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 2-Butanone (MEK) 4,000 100 NS Qp <10 Qp <10 QO <10 Qp <10 Qp <10 <LO <10 <10 q0 <10 <10 <5 <5 <5 <5 <10 <10 Cadmium 2 1 5 <5 <1 <2 <2 <2 <2 <2 <2 <2 <2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 <2 Calcium NS NS NS Chloroethane 3000 to NS <10 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <1 <1 <1 <1 <2 <2 Chloroform 70 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 Chromium 10 IO 100 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <2 <2 <2 <2 <5 1.1 0.85 <10 <10 <10 <5 <5 Cobalt** 1 IO NS <10 <10 <10 <10 <25 <25 Copper 1,000 to 1,300 1 1 1 1 1 <10 <10 <10 <10 10 6.5 Carbon Disulfide 700 35 NS <50 <50 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 <2 <2 1 <2 <2 <1 <1 Dibromoehloromethanc 0.4 3 NS <1 <1 <1 <1 <1 <1 l,l-Dichloroethanc 6 5 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 0.54 <1 <I <1 <1 <I <I l,l-Dichloroethene 350 5 7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 1,4-Dichlorobenzenc 6 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 <1 <1 cis-1,2-Dichloroethme 70 5 70 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 <1 <1 I <1 <1 Ethylbenzenc 600 1 0.7 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <I <1 <1 <1 <1 <1 2-Hexanonc NS 50 NS 4-Methyl-2-pentanone NS 100 NS Toluene 600 1 1000 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <I <1 <1 <I <I Xylenes 500 5 10 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <2 <2 <2 <2 <1 <1 Lead 15 10 15 <5 <5 <3 <3 <3 <3 <3 <3 <3 <3 <5 <5 <5 <5 <5 <5 <10 <10 <10 <10 <10 <10 Manganese 50 50 NS Mercury 1 0.2 2 <0.2 <0.2 0.74 0.93 0.16 0.82 <0.4 <0.4 1 <4 0.48 0.95 0.71 2 0.27 <0.2 <0.2 <0.2 <0.2 <0.1 <0.1 Methylene Chloride 5 1 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <1 <1 I <1 <1 <1 <1 Nickel 100 50 NS <50 18.1 1 <50 16.4 140 <40 Selenium 20 10 50 <]0 <10 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 1 <10 <10 <10 <10 <10 <10 <10 <10 Sulfide NS 1,000 NS Silver 20 10 NS <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <2 <2 <2 <2 <5 1 <5 <10 <10 <10 <10 <5 <5 Tetrahydrofuran NS I NS NS <10 <10 <10 28.4 28 52 Thallium** 0.2 5.5 2 <5.5 <5.5 <5.5 <5.5 Tin 2000 100 NS Vanadium** 0.3 25 NS <25 <25 <25 <25 <50 <50 Vinyl Chloride 0.03 1 2 <10 <10 <2 <2 <2 <2 1 <2 <2 <2 <2 <5 <5 1 <5 <5 <5 <5 <1 <1 <1 <1 2.7 8.6 Zinc 1000 to NS <10 I <10 <10 <10 <20 Alkalinity NS NS NS 331,000 <5000 227,000 990,000 Ammonia-N 1,500 NS NS Iron 300 300 NS Total Dissolved Solids NS 382,000 <25,000 1,160,000 1,200,000,0 2500N 000Sulfate NS <5000 <5000 156,000 100,000 Carbon Dioxide NS NS NS Chloride 250,000 NS NS 6,180 <5000 59,700 49,000 Notes: All units we in µg/L unless ofl-ised indicated NCDEQ Standard= 15A NCAC 02L .0202 Groundwater Stds (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Labomtories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compound was fnmd in the blank and sample. n= Refer W Case Narrative for father detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL MW-11 (coat.) MW-1 Laboratory*** S S S S S P TA TA TA TA Sample Date 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.28.16 428.17 6.15.17 10.11.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 422.16 10.27.16 4.28.17 10.10.17 4.10.18 10.3.13 Acctonc 6000 100 NS <20 <20 <20 <16 <20 <25 7 6 <5 <5 <20 <20 <20 <20 <16 <20 <25 <5 <5 <5 <20 Antimony** 1 6 6 QO <10 <10 0.5 <5 <3 <3 <3 4.3 <10 QO <10 QO 0.34 <5 <3 <3 <3 <10 Arsenic 10 10 10 QO <10 <10 1.2 QO <10 0.83 0.52 0.58J <10 <10 <]0 <IO <26 <10 <10 <1 <1 <1 <10 Barium 700 100 2000 100 280 240 260 210 448 310 270 190 47 47 50 39 54 36 329 35 39 33 85 Benzene 1 1 5 <1 <1 1.2 0.62 <1 <1 1.1 0.7 0.9 0.42 J <1 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <1 Beryllium** 4 1 4 <4 <4 <4 <0.12 <I <1 <1 <1 <4 <4 <4 <4 <0.12 <1 <1 <1 <1 <4 Bromodichloromethanc 0.6 1 NS <7 <1 <7 <0.23 <I <I <I <1 <1 <1 <I <1 <1 <0.23 <I <1 <I <1 <I Bromoform 4 3 NS <1 <1 <1 <0.35 <I <I <I <1 <1 <1 <I <1 <1 <0.35 <I <1 <1 <1 <I 2-Butanone(MEK) 4,000 100 NS <10 <10 <10 <18 <5 <5 <5 <5 <5 <10 <10 <10 <10 <18 <5 <5 <5 <5 <10 Cadmium 2 1 5 <2 <2 <2 0.0047 0.8 <1 0.51 0.45 0.34 J <2 <2 <2 <2 <0.044 <2 <1 <0.5 <0.5 <0.5 <2 Calcium NS NS NS 270,000 160,000 290,000 13,000 8,300 138,000 Chloroethane 3000 to NS <2 <2 <2 <0.28 <1 <1 <1 <1 <1 <2 <2 <2 <2 <0.28 <1 <1 <1 <1 <2 Chloroform 70 5 70 <I <1 <1 <0.21 <I <2 <2 <2 <2 <1 <1 <1 <1 <0.21 <1 <2 <2 <2 <I Chromium 10 t0 100 <5 <5 <5 1.5 <5 22 17 51 25 <5 <5 <5 <5 <6.3 <5 <5 <0.5 <0.5 <5 <5 Cobalt** 1 10 NS <25 <25 <25 2 <25 8.9 6.2 3.1 1.9 <25 <25 <25 <25 <2.6 <25 <5 <1 <I <1 <25 Copper 1,000 to 1,300 1 14 32 1 42 1 14 45 1 203 89 1 36 1 38 <5 <5 <5 <5 0.82 <5 <5 13 0.71 0.63 J <5 Carbon Disulfide 700 35 NS <1 <1 <1 <0.45 <2 <2 <2 <2 <2 <1 I <I <1 <l <0.45 <2 <2 <2 <2 <1 Dibromochloromethaae 0.4 3 NS <1 <1 <1 <0.23 <l <l <I <1 <1 <1 <l <1 <l <0.23 <1 <1 <1 <1 <1 1,1-Dichlormthane 6 5 NS <1 <1 <1 <0.19 <1 <l <l <I <1 <1 <1 <l <1 <l <0.19 <1 <I <1 <1 <1 <1 l,l-Dichloroethem 350 5 7 <I <1 <I <0.31 <I <1 <1 <1 <1 <1 <1 <1 <1 <1 <0.31 <1 <I <1 <I <1 <I 1,4-Dichlorobenzenc 6 1 NS <1 <1 <I <0.19 <I <I <I <I <1 <1 <1 <1 <1 <l <0.19 <1 <I <1 <I <1 <I cis-1,2-Dichlmoethem 70 5 70 <1 <1 <I <0.2 <I <I <1 <I <1 <1 <1 <I <1 <l <0.2 <1 <1 <1 <1 <1 <I Ethylbenzene 600 1 0.7 <1 <1 <I <0.21 <I <0.5 <0.5 <0.5 <0.5 <1 <1 <1 <l <0.21 1 <1 <0.5 <0.5 <0.5 <I 2-Hexanone NS 50 NS 1 <0.26 1 <5 1 <5 <5 1 <5 <5 <0.26 <5 <5 <5 <5 4-Methyl-2-pentanone NS 100 1 NS <0.29 <5 <5 <5 <5 <5 <0.29 <5 <5 <5 <5 Toluene 600 1 1000 <1 <1 <1 0.29 <l <0.5 <0.5 <0.5 <0.5 <1 I <1 <1 <1 0.56 <1 <0.5 <0.5 <0.5 <1 Xylenes 500 5 10 <1 <1 <I <0.32 <l <1 <1 <1 <1 <1 <I <1 1.1 0.8 <t <1 <1 <1 <1 Lead 15 10 15 <10 <10 <10 0.4 <10 15.3 2.6 0.76 0.62 <10 <10 <10 <10 1 <0.15 <10 <5 2.4 <0.5 <0.5 <10 Manganese 50 50 NS 1,800 730 1,730 2,200 2,500 1,400 15 12 60.8 6.1 3.6 3.9 Mercury 1 0.2 2 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 <0.1 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 <0.1 Methylene Chloride 5 1 NS <1 <1 <1 <0.42 <1 <5 <5 <5 <5 <1 <l <1 <l <0.42 1 <I <5 <5 <5 <1 Nickel 100 50 NS <40 <40 <40 23 12 2044 31 53 26 <40 <40 <40 <40 <6.3 <40 <5 <2 <2 <2 <40 Selenium 20 1 10 50 <10 I <10 <10 2.7 <10 <2.5 1 <2.5 <2.5 <10 <10 <10 <10 <9.5 <10 <2.5 <2.5 <2.5 <10 Sulfide NS 1,000 NS <100 <100 Silver 20 10 NS 15 <5 <5 <1.7 <5 <0.5 <0.5 <0.5 <5 <5 <5 <5 77 <5 <0.5 <0.5 <0.5 <5 Tetrahydrofuran NS NS NS 23 28 30 22 9.4 28.9 20 16 17 6 J <5 <5 <5 <5 3.4 <5 QO <10 <10 <10 <5 Thallium** 0.2 5.5 2 <5.4 <2 <2 <2 <5.4 <2 <2 <2 Tin 2000 100 NS <5 <5 Vanadium** 0.3 25 NS <50 <50 <50 5.4 19 65.5 34 7 5.9 <50 <50 <50 <50 <15 <50 <5 <5 <5 <5 <50 Vinyl Chloride 0.03 1 2 9.2 12 2 1.9 <I <1 6.9 <0.5 <0.5 <1 3.7 <l <1 <l <0.5 <1 <1 <0.5 <0.5 1 <1 <1 Zinc 1000 10 NS <20 <20 1 <20 68 1 31 86.7 25 51 15 <20 <20 <20 1 <20 16 <20 <10 16 <20 <10 <20 Alkalinity NS NS NS 990,000 830,000 1,150,000 1,100,000 1 1,100,000 680,000 88,000 33,000 502,000 37,000 38,000 23,000 Ammonia-N 1,500 NS NS 160 <10 120 <10 <100 Iron 300 300 NS 33,000 5,600 750 620 164 <100 <100 Total Dissolved Solids 500,000 NS NS 1400 000 1,100,000 1,100,000 1,500,000 1,400,000 SSQ,000 240,000 110,000 657,000 140,000 120,000 100,000 Sulfate 250,000 250,000 NS 112,000 95,000 96,000 68,000 42,600 14,000 11,000 12,000 Carbon Dioxide NS NS NS 1,400,000 1,100,000 150,000 110,000 Chloride 250,000 NS NS 45,000 36,000 54,800 46,000 51,000 35,000 9,100 3,500 32,800 3,500 3,400 31800 Notes: All units we in µg/L unless otherwised indicated NCDEQ Standard= 15A NCAC 02L .0202 Groundwater Stds (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Labomtories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compound was found in the blank and sample. n= Refer to Case Narrative for fiafher detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit" = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL 1ICL MWAI -1 2 Laboratory*** Sample Date 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 4.10.18 10.3.13 4.10.14 10.23.14 4.24.15 10.21.15 4.22.16 10.27.16 4.28.17 10.10.17 4.10.18 10.3.13 4.10.14 S 10.23.14 Acctonc 6000 100 NS <20 <2o QO <16 <20 <25 <5 <5 <5 <20 <20 <20 <20 <16 <20 <25 <5 <5 <5 <20 <20 <20 Antimony** 1 6 6 <10 <10 <10 0.25 <5 <3 <3 <3 <10 <10 <10 <10 0.51 <5 <3 <3 <3 <10 <10 <10 Arsenic 10 10 10 <10 <I0 <10 <26 <I0 <10 <1 <1 <1 <10 <10 <10 <10 0.59 <10 <10 0.43 0.37 0.6 J <10 <10 <10 Barium 700 1 100 2000 85 85 100 200 88 84.4 70 85 63 130 130 130 96 74 110 85.2 92 94 93 120 150 56 Benzene 1 1 5 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <1 <1 <1 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <1 <1 <1 Beryllium** 4 1 4 <4 <4 <4 0.15 <1 <I <1 <1 <4 14 <4 <4 <0.12 <1 <1 <1 <1 <4 <4 <4 Bromodichloromethane 0.6 1 NS <1 <I <1 <0.23 <1 <1 <1 <1 <1 <1 <1 <1 <0.23 <1 <1 <1 <1 <1 <1 <1 Bromoform 4 3 NS <1 <1 <1 <0.35 <I <1 <I <1 <I <1 <1 <1 <0.35 <1 <I <1 <I I <1 <I <1 2-Butancte(MEK) 4,000 too NS <10 <10 <10 <18 <5 <5 <5 <5 <10 <10 <10 <10 <18 <5 <5 <5 <5 <10 <10 <10 Cadmium 2 1 5 <2 <2 <2 <0.044 <2 11,500 <0.5 <0.5 <0.5 <2 <2 <2 <2 0.044 <2 <1 <0.5 <0.5 <0.5 <2 <2 <2 Calcium NS NS NS 15,000 9,500 <100 57,000 13,000 70,600 Chloroethane 3000 10 NS <2 <2 <2 <0.28 <1 <1 <1 <1 <2 <2 <2 <2 <0.28 <1 <1 <1 <1 <2 <2 <2 Chloroform 70 1 5 70 <1 <I <1 <0.21 <1 <2 <2 <2 <1 <I <1 <I <0.21 <I <2 <2 <2 <1 <1 <l Chromium 10 10 100 <5 <5 <5 2.1 <5 <5 <0.5 <0.5 <5 7.6 <5 <5 <5 2.3 <5 <5 <0.5 <0.5 1.6 J <5 <5 <5 Cobalt** 1 10 NS <25 <25 <25 1.8 <25 <5 <1 <1 <1 <25 <25 <25 <25 <2.6 <25 <5 <I <1 <1 <25 <25 <25 Copper 1,000 10 1,300 <5 <5 <5 43 8.5 <5 3.4 3.8 3.1 5.9 20 20 10 27 4.3 8.1 1 9.6 9.7 9.9 7.8 <5 <5 Carbon Disulfide 700 35 NS <I <1 <I <0.45 <2 <2 <2 <2 <1 <1 <1 <1 <0.45 <2 <2 <2 <2 <1 <I <1 Dibromochlormoodu ne 0.4 3 NS <1 <1 <1 <0.23 <1 <1 <1 <1 <1 <1 <1 <1 <0.23 <1 <1 <I <1 <I <t <I l,l-Dichloroethane 6 5 NS <1 <I <1 <0.19 <I <1 <I <1 <I <1 <I <1 <I <0.19 <1 <1 <1 <I <1 <I <1 <I l,l-Dichloroeth- 350 5 7 <1 <1 <1 <0.31 <I <1 <1 <1 <1 <1 <1 <1 <1 <0.31 <1 <1 <1 <1 <1 <1 <1 <1 1,4-Dichlorobenzcne 6 1 NS <1 <1 <1 <0.19 <t <1 <1 <1 <1 <1 <1 <1 <1 <0.19 <1 <1 <I <1 <I <1 <I <1 cis-1,2-Dichlorocthcne 70 1 5 70 <I <1 <l <0.2 <1 <1 <1 <I <1 <1 <1 <I <1 <0.2 <I <1 <I <1 <1 <1 <I <1 Ethylbenzene 600 1 0.7 <I <1 <I <0.21 <1 <0.5 <0.5 <0.5 <1 <1 <I <1 <0.21 <1 <0.5 <0.5 <0.5 <1 <1 <1 2-Hexamme NS 50 NS <0.26 <5 <5 <5 <5 <0.26 <5 <5 <5 <5 4-Methyl-2-pentamme NS 100 NS <0.29 <5 <5 <5 <5 <0.29 <5 <5 <5 <5 Toluene 600 1 1000 <1 <1 <1 0.34 <1 <0.5 <0.5 <0.5 <1 <I <1 <1 0.33 <I <0.5 <0.5 <0.5 <I <1 <I Xylenes 500 5 10 <1 <I <1 0.52 <1 <I <1 <I <1 <I <1 <1 0.51 <I <1 <1 <1 <1 <1 <1 Lead 15 10 15 <10 <10 <10 0.84 <10 <5 0.24 <0.5 <0.5 <10 <10 <10 <10 0.27 <10 <5 <0.5 0.16 <0.5 <10 <10 <10 Manganese 50 50 NS 110 34 25 5.3 13 7.6 14 220 10.1 10 7.2 5.1 Mercury 1 0.2 2 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 0.14 <0.1 <0.1 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 1 <0.I <0.1 <0.I Methylene Chloride 5 1 NS <1 <1 <1 <0.42 <1 <5 <5 <5 <1 <1 <1 <1 <0.42 <1 <5 <5 <5 <1 <1 <1 Nickel 100 50 NS <40 <40 <40 1 2.1 <40 <5 <2 <2 <2 <40 <40 <40 <40 2 <40 <5 <2 <2 1.2J <40 <40 <40 Selenium 20 10 50 <10 <10 <10 <9.5 <10 <2.5 <2.5 <2.5 <10 <10 <10 <10 1 <10 <2.5 <2.5 <2.5 <10 <10 <10 Sulfide NS 1,000 NS <100 <100 Silver 20 10 NS <5 <5 <5 <1.7 <5 <0.5 <0.5 <0.5 1 <5 <5 <5 <5 <1.7 <5 <0.5 <0.5 <0.5 <5 <5 1 15 Tetrahydrofuran NS NS NS <5 <5 <5 <0.57 <5 <10 <10 <10 <10 8.4 <5 <5 <5 <0.57 <5 QO <10 <10 <10 15 <5 <5 Thallium** 0.2 5.5 2 <5.4 <2 <2 <2 <5.4 <2 <2 <2 Tin 2000 t00 NS <5 <5 Vanadium** 0.3 25 NS <50 <50 <50 17 <50 <5 <5 <5 <5 <50 <50 <50 <50 3.2 <50 <5 2.2 2.5 2.9J <50 <50 <50 Vinyl Chloride 0.03 1 2 <I <1 <1 <0.5 <1 <1 <0.5 <0.5 <1 4.5 29 2 1.4 1 <0.5 <I <1 <0.5 <0.5 <1 <1 <1 <1 Zinc 1000 1 10 NS <20 <20 <20 58 <20 <10 <20 <20 <10 <20 <20 <20 <20 26 <20 <10 19 20 32 <20 <20 <20 Alkalinity NS NS NS 65,000 39,000 46,900 48,000 50,000 36,000 280,000 280,000 268,000 280,000 290,000 300,000 Ammonia-N 1,500 NS NS 87 <10 I <100 150 <10 <100 Iron 300 300 NS 97.4 <100 57 <100 1 <50 1 <100 <100 Total Dissolved Solids 500,000 NS NS 670,000 110,000 131,000 140,000 110,000 130,000 400,000 360,000 386,000 410,000 400,000 380,000 Sulfate 250,000 250,000 NS 13,400 17,000 16,000 18,000 33,200 32,000 34,000 35,000 Carbon Dioxide NS NS NS 130,000 150,000 290,000 310,000 Chloride 250,000 NS NS 4,600 4,400 4,800 3,800 3,600 4,500 19,000 15,000 17,800 11,000 18,000 25,000 Notes: All mits are in pg/L mless otherwised indicated NCDEQ Standard = l5A NCAC 02L .0202 Gmm l-ter Std. (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compom l was fond in the blank and sample. cn= Refer to Case Narrative far further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified < "Report Limit' = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL D-2 (cunt.) Tinsley WSW (cont.) Gilkersan WSW Laboratory*** S S S P TA TA TA S S S P TA TA TA Sample Date 4.24. IL 10.21.15 4.22.16 10.27.16 4. 88.17 10.10.17 4.10.18 4.24.15 10.21.15 4.22.16 10.28.16 5.1.17 10.31.17 4.10.18 4.24.15 10.21.15 4.22.16 10.28.16 5.1.17 10.31.17 4.10.18 Acetone 6000 100 NS <20 <16 <20 Q5 <5 <5 <5 <20 <16 <20 <25 <5 <5 <5 <20 <16 <20 <25 <5 <5 <5 Antimony** 1 6 6 <10 <0.17 <5 <3 <3 <3 <10 <0.17 <5 <3 <3 <3 <10 <0.17 <5 <3 <3 <3 Arsenic 10 10 10 <10 <26 <10 <10 <1 <1 0.23 J <10 <26 <10 <10 0.54 0.19 <1 <10 <26 <10 <10 0.18 0.15 <1 Barium 700 100 2000 130 83 do 97.9 120 140 110 100 95 84 33 93 10 13 31 48 32 44.1 51 12 14 Benzene 1 I 5 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 <1 <0.21 <I <1 <0.5 <0.5 <0.5 Beryllium** 4 I 4 <4 <0.12 <I <1 <I <1 <4 <0.12 <1 <I <1 <1 <4 <0.12 <t <1 <l <1 Bromodichloromethanc 0.6 1 NS <1 <0.23 <1 <I <1 <I <1 <0.23 <l <1 14 14 <l <0.23 <I <1 14 12 Bromoform 4 3 NS <1 <0.35 <1 <I <1 <I <1 <0.35 <I <1 0.78 <1 <1 <0.35 <I <1 <I 0.62 J 2-Butanone(MEK) 4,000 L00 NS <10 <18 <5 <5 <5 <5 <10 <18 1 <5 <5 <5 <5 <10 <I8 <5 <5 <5 <5 Cadmium 2 I 5 <2 <0.044 <2 <1 <0.5 <0.5 <0.5 <2 <0.044 <2 <1 1 <0.5 <0.5 1 <0.5 1 <2 <0.044 1 <2 <1 <0.5 <0.5 <0.5 Calcium NS NS NS 14,000 13,000 12,600 63,000 62,000 98,100 1 22,000 23,000 21,200 Chloroethanc 3000 10 NS <2 <0.28 <1 <1 <1 <1 <2 <0.28 <1 <1 <1 <1 <2 <0.28 <1 <1 <1 <1 Chloroform 70 5 70 <1 <0.21 <1 <2 <2 <2 <I <0.21 <1 <2 42 37 <1 <0.21 <1 <2 41 31 Chromium 10 10 100 <5 <6.3 <5 <5 <0.5 <0.5 <5 <5 <6.3 <5 <5 <0.5 <0.5 <5 <5 1.5 <5 <5 <0.5 <0.5 L5 J Cobalt- 1 10 NS <25 0.53 <25 <5 1.2 0.32 0.75 J <25 0.32 <25 <5 <1 <1 <1 <25 2 <25 <5 2.2 <I <1 Copper 1,000 1 10 1,300 1 <5 1.5 4.7 <5 8.5 5 1 4.8 <5 0.44 4.1 202 1.1 4.1 3.7 B <5 7.6 <5 <5 1 13 18 23 B Carbon Disulfide 700 35 NS <1 <0.45 <2 <2K<55 <2 <1 <0.45 <2 <2 <2 <2 <I <0.45 <2 <2 <2 <2 Dibromochloromethanc 0.4 3 NS <1 <0.23 <1 <1 <1 <1 <0.23 <1 <1 6.9 6 <1 <0.23 <1 <1 7.6 5.5 l,l-Dichloroethanc 6 5 NS <1 <0.19 <1 <I <1 <1 <I <0.19 <1 <1 <1 <1 <I <1 <0.19 <I <1 <1 <1 <I l,l-Dichloroethenc 350 5 7 <1 <0.31 <1 <I <1 <1 <I <0.31 <I <1 <I <1g<5 <1 <0.31 <I <1 <I <1 <I 1,4-Dichlorobemene 6 1 NS <1 <0.19 <I <1 <1 <1 <1 <0.19 <1 <I <1 <1 <1 <0.19 <1 <1 <1 <1 <1 cis-1,2-Dichloroethenc 70 5 70 <1 <0.2 <I Q <7 <I <1 <0.2 <1 <I <1 <7 q <0.2 <1 <7 Q <I <1 Ethylb-ame 600 1 0.7 <1 <0.21 <1 <0.5 <0.5 <1 <0.21 <1 <0.5 <0.5 -1 <0.21 <1 <0.5 <0.5 <0.5 2-Hexanone NS 50 NS <0.26 <5 <5 <5 <0.26 <5 <5 <5 <0.26 <5 <5 <5 <5 4-Methyl-2-pentanone NS 100 NS <0.29 <5 <5 <5 <5 <0.29 <5 <5 <5 <0.29 <5 <5 <5 <5 Toluene 600 I 1000 <1 0.75 <0.5 <0.5 <0.5 <I <0.24 <1 <0.5 <0.5 <l <0.24 <1 <0.5 <0.5 <0.5 Xylenes 500 5 10 <1 L4 <1 <1 <1 <I <0.32 <1 <I <1 <1 <0.32 <1 <I <1 <1 Lead 15 10 15 <10 <0.15 <10<0.5 <0.5 0.34 J <10 <0.15 <10 88.6 <0.5 <0.5 <0.5 <10 0.38 <10 <5 0.54 5 7.4 Manganese 50 50 NS 98 290 99 73 42 120 25 54.3 40 1.6 L8 J 120 <10 21.4 98 16 28 Mercury 1 0.2 2 <0.1 <0.028 <0.1<0.2 K39.4 <0.2 <0.2 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 <0.1 0.14 0.12 <0.2 0.29 <0.2 Methylene Chloride 5 1 NS <1 <0.42 <5 <5 <5 <1 <0.42 <I <5 <5 <5 <1 <0.42 <1 <5 <5 <5 Nickel 100 50 NS <40 <6.3 <40 <2 l Li J <40 L4 <40 <5 <2 <2 <2 <40 1.9 <40 <5 1.5 1.5 1.1 J Selenium 20 10 50 <10 <9.5 <2.5 <2.5 <2.5 <10 <9.5 <10 <2.5 <2.5 <2.5 <10 <9.5 <10 <2.5 <2.5 <2.5 Sulfide NS 1,000 NS <100 <100 Silver 20 10 NS <5 <1.7 11 <5 <0.5 <0.5 <0.5 <5 1 <13 <5 <0.5 <0.5 <0.5 <5 Q9 <5 <0.5 <0.5 <0.5 Tetrahydrofuran NS NS NS <5 <0.57 <5 <10 <to <10 <10 <5 <0.57 <5 <10 <10 <10 <10 <5 <0.57 <5 QO <10 <10 <10 Thallium** 0.2 5.5 2 <5.1 <2 <2 <2 <5.4 <2 <2 <2 1 1 <5.4 <2 <2 <2 Tin 2000 100 NS <5 <5 1 <5 Vanadium- 0.3 25 NS <50 <15 <50 <5 <5 <5 2.3 J <50 1 <15 <50 <5 <5 <5 <5 <50 1 7.7 <50 <5 10 <5 Vinyl Chloride 0.03 I 2 <1 <0.5 <1 <1 <0.5 <0.5 <l <1 I <0.5 <1 <I <0.5 <0.5 <1 <I <0.5 0.93 <I 0.86 <1 Zinc 1000 10 NS QO 22 <20 <10 <20 9.2 13 24 33 <20 366 9.3 <20 <10 <20 20 <20 <10 15 32 190 Alkalinity NS NS NS 1 75,000 69,000 62,800 50,000 48,000 53,000 150,000 160,000 95,600 160,000 23,000 22,000 82,000 98,000 93,100 85,000 21,000 23,000 Ammonia-N 1,500 NS NS <50 <10 <I00 <50 <10 <100 74 <10 <100 Iron 300 300 NS 1 71 50 <100 311 200 <100 477 3,000 660 1,500 B Total Dissolved Solids 500,000 NS NS 190,000 170,000 145,000 130,000 100,000 94,000 320,000 320,000 550,000 380,000 66,000 66,000 140,000 170,000 155,000 160,000 62,000 120,000 Sulfate 250,000 250,000 NS 11,800 15,000 10,000 17,000 310,000 83,000 31,000 8,400 6,700 5,200 8,900 8400 B Carbon Dioxide NS NS NS 140,000 160,000 1 130,000 160,000 100,000 170,000 Chloride 250,000 NS NS 4,400 5,500 4,100 4,100 3,200 5,400 17,000 17,000 5,300 17,000 35,000 8,300 7,700 7,100 10,800 7,800 1 9,500 8,800 Notes. All -its are m pg/L mless otherwised m Heated NCDEQ Staudaul = 15A NCAC 02L .0202 Gmmdwater Stds (Eff. 2013) * Interim Mabmum Allowable Coacentratioo (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compomd was fond m the black and sample. cu= Refer to Case Narrative for further detail Bold /yellow values exceed the NCDEQ Staudaul Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Mmsimum Conceatratiou Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit' = Value is less that the Report Limit Table 3 (cont.) History of Site Groundwater and Private Wells Analytical Detections Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Constituent Std. SWSL MCL Hammill WSW Laboratory*** S S S P TA TA TA Sample Date 424.15 10.21.15 4.22.16 10.28.16 5.1.17 10.31.17 4.10.18 Acctonc 6000 100 NS <20 <16 <20 <25 7.4 6.5 <5 Antimony** 1 6 6 <10 0.2 <5 <3 <3 13 Arsenic 10 10 10 <10 5.3 4 <10 2.8 0.47 0.68 J Barium 700 1 100 2000 44 49 37 79.5 35 41 38 Benzene 1 1 5 <1 <0.21 <1 <1 <0.5 <0.5 <0.5 Beryllium** 4 1 4 <4 <0.12 <1 <1 <1 <I Bromodichloromethane 0.6 1 NS <1 1 <0.23 1 <1 I <1 <1 <1 Bromoform 4 3 NS <1 <0.35 <1 <1 <1 <1 2-Butanone(MEK) 4,000 100 NS <10 <18 <5 <5 22 <5 Cadmium 2 1 5 <2 <0.044 <2 <1 <0.5 <0.5 <0.5 Calcium NS NS NS 110,000 110,000 55,300 Chloroethane 3000 10 NS <2 <0.28 <1 <1 <1 <1 Chloroform 70 5 70 <1 <0.21 <1 <2 1 <2 <2 Chromium 10 10 100 <5 0.69 <5 <5 <0.5 <0.5 <5 Cobalt** 1 10 NS <25 0.43 <25 <5 <1 <1 <1 Copper 1,000 1 10 1 1,300 <5 1 4.7 8 32.8 4.4 4.3 5.1 B Carbon Disulfide 700 35 NS <1 <0.45 <2 <2 <2 <2 Dibromochloromethane 0.4 3 NS <1 <0.23 <I <1 <I <1 1,1-Dichloroethane 6 5 NS <I <0.19 <1 <1 <1 <1 <1 1,1-Dichloroedime 350 5 7 <1 <0.31 <1 <1 <1 <1 <1 1,4-Dichlorobenzene 6 1 NS <1 <0.19 <1 <1 <1 <1 <1 6s-1,2-Dichloroethene 70 5 70 <1 <0.2 <1 <1 <1 I <1 <1 Ethylbenzene 600 1 0.7 <1 <0.21 1 <1 <0.5 <0.5 <0.5 2-11exammi, NS 50 NS <0.26 <5 <5 <5 <5 4-Methyl-2-pentamne NS 1 100 1 NS <0.29 <5 <5 <5 <5 Toluene 600 1 1000 <1 0.43 <1 <0.5 <0.5 <0.5 Xylenes 500 5 10 <1 <0.32 <1 <I <1 <1 Lead 15 10 15 <10 0.7 <10 6 0.6 0.28 0.321 Manganese 50 50 NS 62 58 53 72 60 88 Mercury 1 0.2 2 <0.1 <0.028 <0.1 <0.2 <0.2 <0.2 Methylene Chloride 5 1 NS <1 1 0.34 1 <1 <5 1 <5 <5 Nickel 100 50 NS <40 2.5 <40 <5 <2 1 0.95 0.72 J Selenium 20 10 50 <10 <9.5 <10 <2.5 <2.5 <2.5 Sulfide NS 1 1,000 NS <100 Silver 20 10 NS <5 <1.7 <5 <0.5 <0.5 <0.5 Tetrahydrofumn NS NS NS <5 <0.57 26 <10 <10 230 12 Thallium** 0.2 5.5 2 <5.4 <2 <2 <2 Tin 2000 100 NS 2.1 J Vanadium** 0.3 25 NS <50 2.3 <50 <5 <5 <5 <5 Vinyl Chloride 0.03 1 2 <I <0.5 <1 <I <0.5 <0.5 <1 Zinc 1000 10 NS 53 25 14 27 33 490 260 Alkalinity NS NS NS 99,000 99,000 159,000 94,000 95,000 93,000 Ammonia-N 1,500 NS NS 310 <10 <100 Iron 300 300 NS 324 790 290 210 B Total Dissolved Solids 500,000 NS NS 510,000 570,000 308,000 600,000 600,000 590,000 Sulfate 250,000 250,000 NS 72,300 310,000 320, 1310,000 B Carbon Dioxide NS NS NS 92,000 96,000 Chloride 250,000 NS I NS 5,200 5,000 18,500 5,400 5,600 5,600 Notes: All wits are iu pg/L mless otherwised indicated NCDEQ Standard = 15A NCAC 02L .0202 Go mdwater Std. (Eff. 2013) * Interim Maximum Allowable Concentration (Eff. 2013) Laboratories= Pace (P), Shealy (S), and Test America (TA) J = Estimated cone. above the adjusted method detection limit and below the adjusted reporting limit B=Compomd was fond in the blank and sample. cn= Refer to Case Narrative far further detail Bold /yellow values exceed the NCDEQ Standard Blue values exceed the Solid Waste Section Limit (SWSL) (Eff. 2011) Red values exceed the Maximum Concentration Limit (MCL) (Eff. 2009) NS= Not Specified <'Report Limit' = Value is less that the Report Limit Table 4 Summary of Vertical Hydraulic Gradients Spring 2018 Semi -Annual Groundwater Monitoring North Meck Closed Phase I Area Landfill CEC Project No. 111-370.001 Screen Spring Spring GRD TOC TOS BOS Fall2017 Fall2017 Well ID i Depth Elev. Elev. i TOS i BOS Elev. Elev. Midpoint W.L. W.L. 2018 2018 VG Elev. W.L. W.L. (ft) (ft) (ft) (ft) (TOC)1 Elev. (ft) (ft) (TOC) Elev. (ft) MW-4A 44 711.93 711.63 34 44 677.93 667.93 672.93 33.01 678.62 33.18 678.45 0.001 MW-41) 100 711.72 711.30 85 100 626.72 611.72 619.22 32.55 678.75 32.81 678.49 MW-5 29 NM 682.99 19 29 663.99 653.99 658.99 20.49 662.50 19.98 663.01 0.027 MW-51) 55 679.22 681.84 45 55 636.84 626.84 631.84 18.61 663.23 18.10 663.74 MW-6 67 NM 738.25 57 67 -57 671.25 307.125 58.44 679.81 58.78 679.47 0.000 MW-6D 95 735.05 737.90 80 95 655.05 642.9 648.975 58.71 679.19 58.40 679.50 MW-7A 60 724.81 727.52 50 60 674.81 664.81 669.81 43.10 684.42 43.35 684.17 MW-7D 110 724.85 727.36 95 110 629.85 614.85 622.35 44.90 682.46 44.55 682.81 -0.029 MW-8 80 NM 764.39 70 80 694.39 684.39 689.39 68.41 695.98 68.57 695.82 0.0134 MW-8D 122 766.2 768.20 107 122 661.20 646.20 653.7 72.00 696.20 71.90 696.30 MW-10 25 694.93 696.81 15 25 679.93 669.93 674.93 17.88 678.93 17.29 679.52 0.51 MW-lOD 65 723.8 726.77 55 65 668.8 658.8 663.8 42.83 683.94 41.55 685.22 MW-11A 30 672.87 675.74 20 30 652.87 642.87 647.87 16.23 659.51 13.91 661.83 MW-11D-1 60 672.52 674.44 50 60 622.52 612.52 617.52 13.68 659.56 12.80 661.64 _0.006 MW-11B 27 670.77 673.24 17 27 653.77 643.77 648.77 14.91 659.53 11.40 661.84 MW-11D-2 40 671.04 673.92 30 40 641.04 631.04 636.04 14.31 659.61 12.22 661.70 -0.011 Notes: (1) Measured in feet below ground surface GRD = Ground TOC = Top -of -PVC Casing NM = Not Measured TOS = Top -of -Screen BOS = Bottom -of -Screen W.L. = Water Level VG = Vertical Gradient Vertical Gradien Shallow Well Water Level Elev. -Deep Well Water Level Elev. = - Shallow Well Screen Midpoint - Deep Well Screen Midpoint APPENDIX A Civil & Environmental Consultants, Inc. MAW �F V 4 w .ANY M IV Civil & Environmental Consultants, Inc. PROJECT J[/[ (C 1 05 c' JOB NlR48ER �I DATE SAMPLE LOCATION ID LI — LOCATION ACTIVITY START: r �C ,l END: WATER LEVEL / WELL DATA CASINGI ]MEASURED 1 3 TOP OF WELL WELL DEPTH FT I )HISTORICAL ( ; TOP Of PROT. CASING (FROM GROUND) P CASING/WELL DIfF. FT FT WELL MATERIAL: WELL LOCKED?: WELL DIA, 17 2 INCH - WATER LEVEL EQUIP. USED: WATER DEPTH F7 (c 7 FT [ 7 PVC C 7 C 7 YES C 7 4 INCH t 7 ELECT.COND.PROSE [ 7 55 17 NO L l 6 INCH 17 FLOAT ACTIVATED C ] 17 PRESS. TRANSDUCER [ 7 .16 GAL/FT (2 IN.) GAL/)1011 17 HEIGHT OF FT X C 7 .65 GAL/FT (4 IN.) o — J WELL INTEGRITY: YES NO - WATER COLUMN [ 7 1.5 GAL/FT (6 IN.) PROT, CASING SECURE C ] C 7 C ) _GAL/FT (_IN J TOTAL GAL PURGED CONCRETE COLLAR INTACT [ 7 C 1 OTHER EOUiPMENT DOCUNE NTATlON PURGING/SAMPLING EQUIP. USED: J 1F USED FOR: PURGING SAMPLING (J I] [l ➢ERISTALTIC EQUIPMENT 10 DECONTAMINATION FLUID$ USED: (J ALL TNAT APPLY AT LOGTI DN ( 7 ETHYL ALCOHOL [ 7 DEIONIZED WATER C ) TSP SOLUTION _. [ ) HEXANE [ 7 HNO3/D.I.WATER SOLUTION ( 7 POTABLE WATER ( 7 NONE C7 FI £LO ANRLTSI$ DATA AMBIENT AIR VOA PPM WELL NOUTN PPM HELD DATA COLLECTED C IIN-LINE I ]IN CONTAINER PURGE DATA TEMPERATURE, DEG C pM, WniLS SPECIFIC CONDUCTIVITY (u hes/cm. a 25 deB.c) OXIDATION-REDUCTION ,+/. my DISSOLVED OXYGEN, ppn L J,W LRkl, a SAMPLE COLLECTION REQUIREMENT iJ 2i REQUIRED AT TH15 LOCATION) J IF J.IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED Il CJ I NG C7 P% C J 1 V (] NOTES: p _ — Sw-�j'(Ln( � ��li T "h.�✓.e.v_ �.,ra� �a?e�:'<_. ��2� Uz, fie,% Civil & Environmental Consultants, Inc. PROJECT CLOSED JOB NUMBER III.. , � PATE SAMPLE LOCATION ID Mw q LOCATION ACTIVITY START: ��. �j END: WATER LEVEL / WELL DATA J III O I )MEASURED I J TOP OF WELL CASING STICK-UP FT CASING/WELL DIFF, WELL DEPTH C77 I )HISTORICAL 17 TOP OF PROT. CASING tFROM GRWNP) I) WELL MATERIAL: WELL LOCKED?: WELL DIA. 13 2 INCH WATER LEVEL EQUIP.. USED: WATER DEPTH JI b FT I I PVC I J 1 3 YES C J 4 INCH C 3 ELECT.C.QNbPROBE I ] SS 1 3 NO I ) 6 INCH 13 FLOAT ACTIVATED I ) I I PRESS. TRANSDUCER C 3 .16 GAL/FT (2IN.) GAL/VOL'. _ I J HEIGHT OF F7 X [ 3 .65 GAL/FT (4 IN.) _ WELL INTEGRITY: YES NO WATER COLUMN t 3 1.5 GAL/FT (6 1N.) PROT. CASING SECURE I I I ) 17 _GAL/FT {�-1 N.> TOTAL GAL PURGED CONCRETE COLLAR INTACT I 1 13 OTHER EQUIPMENT DOCUMENTATION �/ IF USED FOR: pEGONTAMINAT IDH FLUIDS USED: PURGING/SAMPLING EDULP. USED: PURGING SAMPLING EQUIPMENT ID (J ALL THAT APPLY AT LOCATION f 7 I7 PERISTALTIC PUMP t J ETHYL ALCOHOL C I Ik7 SUBMERSIBLE PUMP [ 7 DEIORIZED 'WATER C 3 't 1 BAILER 13 TV SOLUTION I I 17 PVC/SILICON TUBING I I HEXANE I) t I TEFLON/SILTC•ON TUBING I J HNOj/p:I.WATER SOLUTION 17 I I AIR LIFT I I POTABLE WATER [ ] t 3 NAND PUMP C I NONE I I _ IN -LINE FILTER 17 C 3 PRESS/VAC FILTER I J - CI 13 FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH 1 n PPM - FIELD DATA COLLECTED 1 IIN.-LINE 1 �•U t17'.K7 ��tOZ 1 )IN CONTAINER PURGE -DATA E ®. GALA a•i�vGAC @ �.•� GAL.o GAL a` GAL TEMPERATURE,PH� Units DEG C SPECIFIC CONDUCTIVITY(Lab DISSOLVED O OXIDATION -RFD mV DISSOLVED OXYGEN, _(j.,(p, g S �h SAMPLE COLLECTION REQUIREMENTS LJ IF REQUIRED AT THIS LOCATSDN) d IF SAMPLE OBSERVATIONS: I 7 TURBID T 7 COLORED C 7 CLOUDY [xl CLEAR I I ODOR ✓ IT FIELD PRESERVATION VOLUME SAMPLE SAI7PLE BOTTLE Ib'S ANALYTICAL PARAMETER FILTERED METNCO - REgUIR£D COLLECTED •jw%a47;c 1 3 [3 13 c i 01 :oa 0.94 t 3 NOTES: PR03ECT LEAUNIMANO Civil & Environmental Consultants, Inc. SAMPLE LOCATION ID AAvv Iqp( I JAB NLNBER ` I _3� O (� DATE L 1 LOCATION ACTIVITY START: �'L ; �� END: HATER LEVEL / NELL DATA C ]MEASURED I ) TOP OF WELL CASINO STICK-UP FT CASING/WELL RIFF. FT WELL DEPTH FT I )HISTORICAL 17 TAP OF PROT. CASING (PROM GROUND) 10 CI 33•1(� FT WATER DEPTH HEIGHT OF FT WATER COLUMN WELL MATERIAL: WELL LOCKED?: WELL DIA. C 7 2 INCH WATER LEVEL ERllIP.. USED; INCH [ I ELEC%CONDiPROBE I NCN [ I xLOAT ACTIVATED [ ) PRESS. TRANSDUCER [i NELL INTEGRITY-: YES NO PROT. CASING SECURE C I I 7 CONCRETE COLLAR INTACT C I I ] OTNER EQUIPMENT DOCUMENTATION J IF USED fOR: DECOWTAMINAT ION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID (./ ALL THAT APPLY AT LOCATION f 7 C) PERISTALTIC PUMP 17 ETHYL ALCOHOL I ] I I SUBMERSIBLE PUMP 7 —^ C ) DEIONIZED WATER C ) C J SAILER el TSP SOLUTION I I I ] PVCISILICON TUBING I ] HEXANE T J I) TEFLON/SILICON TUBING L I HNO3/I):LWATER SOLUTION C) C 3 AIR Lp FT I I POTABLE WATER C 7 [ I .HAND PUMP L I NONE I ] IN -LINE FILTER C ) C I ' PRESS/VAC FILTER [ ] t] CJ FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PPR FIELD DATA COLLECTED I IIN-LINE 17i)C I )IN CONTAINER I IV PURGE -DATA z CO GAL{a J .GAL a •7 GAL a GAL 0 GAL TEMPERATURE, DEG C pH, units SPECIFIC CONDUCTIVITY OXIDATION25 dON 9+/ OXIDATION: , REDUCTION,+/- my DISSOLVED OXYGEN, PPM l l!• O �••2/O {{"' l 'D R � J•10 -- I SAMPLE OBSERVATIONS: C ) TURBID i ) COLORED C 7 CLOUDY L 7 CLEAR C ] DOOR AYt'lJ Il •>'ib ZA-'rL'1�PL1 SAMPLE COLLECTION REQUIREMENTS (./ IF REQUIRED AT THIS LOCATION) 1 J IF 4 IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED ii zI I I r I] II II /",�lI" "lo [I II rI I) CI r I NOTES: V Civil & Environmental Consultants, Inc. PROJECT SOB NUMBER II -3�oQ1 DATE ' SAMPLE LOCATION ID Mvv�qD LOCATION ACTIVITY START: END: ^� WATER LEVEL / WELL DATA _ [ IMEASUREb 17 SOP OF WELL CASING STICK-UP FT CAS1NGyVELt DIFF. FT WELL DEPTH - FT 11 )HISTORICAL C I TOP OP.WT_ CASING (FROM GROUND) WELL MATERIAL: WELL LOCKED?: WELL DIA. L 12 INCH WATER LEVEL EQUIP.. USED: WATER DEPTH �2,5 FT 1 7 PVC 17 L 1 YES C J 4 INCH C J ELECT,COWO PROSE [ I SS L 7 NO 11 6 INCH C J FLOAT ACTIVATED I J C 7 PRESS, TRANSDUCER L 7 .16 GAL/FT (2IN.) GAL/VOL - [ J HEIGHT OF FT X [ I .65 GAL/FT (4 IN.) _ WELL INTEGRITY YES NO WATER COLUMN 1 7 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C J L J L J _GAL/FT I,__,_INJ TOTAL G914 PURGED CONCRETE COLLAR INTACT I J 1 J OTHER EOU]PMEBT DOCUMENTATION ,/ if USED FOR: I IDECONTAM INAT iDN FLUIDS USED. PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID ALL THAT APPLY AT LOCATION C 7 I PERISTALTIC PUMP 17 ETHYL ALCOHOL I I 17 SUBMERSIBLE PUMP C I bElON120 'WATER C 7 t J SAILER -- 17 TV SOLUTION C 7 i 7 PVC/SILICON TUBING C J HEXANE L I 1 J TEFLON/SILICON TUBING C I HNO3/1?:I.WATER SOLUTION L I i J AIR LIFT L J POTABLE WATER C I L I NAND PUMP L J NONE C J IN -LINE FILTER L I [ J PRESS/VAC FILTER C I, I7 it FIELD ANALYSIS DATA • AMBIENT AIR VOA PPM WELL MOUTH e^ PPM FIELD DATA COLLECTED C ITN -LINE �• n •eL 19 ••925 1 110 CONTAINER PURGE DATA a o-Jr GAL 0 .GAL a •h .GAL. a 2-- GAL a GAL TEMPERATURE, DEC C Units SPECIFIC CONDUCTIVITY Q 25 deg-c)DISSOL ED REDUCTION,+/- 4ND]SSOLVED 0%YGEN,ppm ,_J b 6T. �•y � _7.;1 +t(05(o ,pfi �(yp(UThOSIM, SAMPLE COLLECTION REQUIREMENTS f IF (,I IF REQUIRED AT TNIS LOCATION) ./ IF FIELD PRESERVATION VOLUHF SAMPLE SAMPLE BOTTLE Ib'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED II [1 v� [I TI II SAMPLE OBSERVATIONS: L I TURBID I I COLORED I I CLOUDY C 7 CLEAR { J ODOR Civil & Environmental Consultants, Inc. JOB NURSER II _ �� DATE ry I g PROJECT '--T—{-'-- SAMPLE LOCATION ID M �- ��'� - LOCATION, ACTIVITY START: IF y END: ; KQ 11 HATER LEVEL / WELL DATA [ ]MEASURED { ] TOP OF HELL GASING STICK -MP F7 GASINGyHELt DSFF, FT WELL DEPTH F77 I ]HISTORICAL CC I Top OF PROT. CASING (FROM GROUND) WELL MATERIAL: WELL LOCKED?: WELL DIA. C ] 2 INCH HATER LEVEL EQUIP.. USED: C '33, 22FT { ] I YES 17 4 INCH { ] ELECT. ACTIVATED ROBE HATER DEPTH PVC 17 ACTIATED L ] SS [ 7 NO I ] 6 INCH [ 7 FLOAT VATED 17 { I PRESS, TRANSDUCER 1 ] .16 GAL/FT (2 INGAC/VOL'' 17 WELL INTEGRITY:A�YES NO HEIGHT OF FT X { 1 .65 GALIFT (4 IN.) _ PROT. CASING SECURE C I 17 HATER COLUMN C 7 1.5 GAL/FT (6 IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT { ) I ] OTHER EQUIPMENT DOCUMENTATION �1 IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID 0 ALL THAT APPLY AT LOCATION [ j j] PERISTALTIC PUMP I ] ETHYL ALCOHOL ( ] [ ] SUBMERS IflLE PUMP 17 DEIORIZED "WATER C ) 1 ] BAILER C j TSP SOLUTION [ I [ I PVC/SILICON TUBING I I HEXANE { POTABLE 7 I ] TEFjLONISILICON TUBING C ) HATER .HATER i0LU710N j ] ( I AIR LIFT - C I POTAB C 9 C ] HARD PUMP I ] ROVE ( I 1N^LINE FILTER [ I [ 7 PRESS/VAC FILTER I ) I7 {7 FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PPH FIELD DATA COLLECTED I IN-CIN£ ] [ SIN CONTAINER � 13� 5 GAL Ca GAL SAMPLE OBSERVATIONS: PURGE DATA S E Q• GAL a GAL D 1.5 OAL.a L ] TURBID [ I COLORED TEMPERATURE, DEG C .—I•L�— is• I�j• b� [ 7 CLOUDY pH, uriixe T'ON UU 2 �f L ] CLEAR SPECI FHC CONDUCT IVITY--- 1 ✓' Y C 7 ODOR OXIDATION-REDUCTION;*f^ my b D]SSOLVED OXYGEN, ppm SAMPLE COLLECTION REQUIREMENTS Z1 IF SJ IK REQUIRED AT THIS LOCAT;DW) J IF FIELD PRESERYATIOH REq UHF �SAHP�ED SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED MET WOOIRED ( 7 f f f zl f r f via\�sOJm,Vl4& -ham 4 j l -'�0 ��� ay aim, Civil &Environmental Consultants, Inc. PROJECT J.f/'� ;" rr — ';, v j < JOB NUMBER SAMPLE LOCATION ID I J� Lj -- LOCATION ACTIVITY START: WATER LEVEL / WELL DATA [ ]MEASURED [ 7 TOP OF WELL CASING STICK-UP FT CASING/YELL DIFF. FT WELL DEPTH FT [ ]HISTORICAL I ) TOP OF PROT. CASING (FROM GROUND) fl r: WELL MATERIAL: WELL LOCKED?: WELL DIA. C 7 2 INCH � WATER LEVEL EQUIP. USED: WATER DEPTH iq _l FT [ J PVC C J C ] YES [ 14 INCH [ 7 ELECT.COND.PROBE [ J SS [ ] NO 1 16 INCH [ ) FLOAT ACTIVATED ( 7 ( I PRESS. TRANSDUCER [ 7 .16 GAL/FT (2 IN.> GAL/VOL [ I HEIGHT OF FT % [ ] .65 GAL/FT (4 IN = WELL INTEGRITY: YES NO WATER COLUMN ( 7 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C 7 C I [ 7 _GAL/FT ( IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT C 7 C 7 OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID ALL THAT APPLY AT LOCATION [ I [ 7 PERISTALTIC PUMP 17 ETHYL ALCOHOL (7 ( 7 SUBMERSIBLE PUMP [ 7 DEIONIZED WATER [ 7 [ ] RAILER [ I TSP SOLUTION [ 7 C J PVC/SILICON TUBING [ 7 HEXANE 1 7 [ 7 TEFLON/SILICON TUBING C ] HNO3/D.I.WATER SOLUTION [ I C 7 AIR LIFT I I POTABLE WATER C 7 [ J HAND PUMP C I NONE [ 7 IN•LINE FILTER C 7 C ] PRESS/VAC FILTER C I C7 [J FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PPM f1E10 DATA COLLECTED C N-LINE )I I ]IN CONTAINER PURGE DATA e, "a (-" 4AiIa �I`f �Nl a L-'a"L+. a �`�j"GAL a GAL SAMPLE OBSERVATIONS: ��/ q?� 17 TURBID iyl TEMPERATURE, DEG C J> 1 --- iLl. % p IN�t��' i'-I-CcG% [ 7 COLORED 7 1� PH, uni TS - !-> r 53 ,_(, S 1 /o-e�i '`'' {p_-jD-[`:(. I I CLOUDY SPECIFIC CONDUCTIVITY VO CLEAR 11c q (uanQs/cm. a 25 ae9.c) 16 C i l o Y ((�i I 1 o7 t] 000a -3LI(f OXIDATION-REDUCTION,+/- my DISSOLVED OXYGEN, Ppn33 � � D SAMPLE COLLECTION REQUIREMENTS (J If REQUIRED AT THIS LOCATION) J IF ,/ IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REWIRED COLLECTED I) [.7 [I CI CJ NOTES: f / AV I Civil & Environmental Consultants,' Inc. PROJECT �J /'� f `. �v JOB NUMBER SAMPLE LOCATION ID ��„'� LJ - j LOCATION ACTIVITY START: 3 S O END: WATER LEVEL / WELL DATA ( )MEASURED [ 7 TOP Of WELL CASING STICK•UD FT CASING/YELL DIf F. FT WELL DEPTH FT ( 7HISTORICAL L J TOP OF PROT. CASING (FROM GROUND) I WELL MATERIAL: WELL LOCKED?: WELL DIA. E 7 2 INCH WATER LEVEL EQUIP. USED: WATER DEPTH } .(J FT ( ] PVC [ 7 ( ) YES C J 4 INCH [ J ELECT.COND.PROSE L J SS t 7 NO t 2 6 INCH Z PRESS.ACTIVATED TRANSDUCER [ 3 .16 GAL/FT (2 INJ GALIVOL ( 7 HEIGHT OF F7 X [ ] .65 GAL/FT (4 IN.) = WELL INTEGRITY: YES NO WATER COLUMN C 7 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C 7 1 7 t ] GAL/FT (_IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT [ J C I -- OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EOVI P. USED: PURGING SAMPLING EQUIPMENT ID (J ALL THAT APPLY AT LOCATION ( 7 1 7 PERISTALTIC PUMP ( ] ETHYL ALCOHOL ( ) I ] SUBMERSIBLE PUMP L 7 DElONONLPATER [ ] ( J BAILER 17 TSP SOLUTION t ] 1 I PVC/SILICON TUBING [ J HEXANE I ] E ) TEFLON/SILICON TUBING L ] POTABLE .WATER SOLUTION P C 7 ! 7 AIR LIFT I J DTABLE WATER E J C] HAND PUMP C J NONE C J IN -LINE FILTER I ] ! 7 PRESS/VAC FILTER ( J C] [J FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED C ]IN -LONE [7IX CONTAINER PURGE DATA GAL SAMPLE OBSERVATIONS: ( ] TURBID TEMPERATURE, DEG C �' -� I,—(�/_�7�� / Li �' C ) ,COLORED - PH, Units C ]CLOUDY SPECIFIC CONDUCTIVITY L- - E4 CLEAR Cumhos/cm. a 25 IOH 0+/ `�� -- ' 17 ODOR OXIDATION-REDUCTION,+/- my DISSOLVED OXYGEN, Ppm , `! �i V S I: 7 3 SAMPLE COLLECTION REQUIREMENTS <J !i REQUIRED AT TN35 LOCATION) J 3F J 1F FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED [I I t 1 D't/ 7 f., C 7 NOTES: p lV/ 1 �! CC(%'LGA Lji 11A �F/A F 7AU Civil & Environmental Consultants, Inc. I� PROJECT � � JOB NUMBER `l` 3 •i%O' DATE SAMPLE LOCATION ID MVV - LOCATION ACTIVITY I START: WATER LEVEL / WELL DATA 111 I (MEASURED I J TOP OF WELL CASING STICK -tip FT - CASINGIWECL DIfF. FT WELL DEPTH I )HISTORICAL I I TOP OFPROT_ CASING <FROM GkOUNQ) i] p WELL MATERIAL: WELL LOCKED?: WELL DIA. C 12 INCH WATER LEVEL EQUIP.. USED; WATER DEPTH U F7 I) PVC [ 3 t 3 YES C 3 4 INCH C I ELECT. CORD aPROBE # 7 SS 13 NO t 3 6 INCH C 3 FLOAT ACTIVATED C ] [ ) PRESS. TRANSDUCER [ I .16 GAL/FT (2IN:) GAL/VOL # I HEIGHT OF FT X I I, .65 GAL/FT (4 IN.) _ WELL INTEGRITY: YES NO - WATER COLUMN 111.5 GAL/FT (6 IN PROT. CASING SECURE C ] I 3 I I _GAL/FT {�I N.) iOTAt GAL Pk1RGED CONCRETE COLLAR INTACT I I I ) OTHER EOUI PMENT DOCUMENTATION ,� IF USED FOR. DECONTAH INA7 iON FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING I EQUIPMENT IO (J ALL THAT APPLY AT LOCATION C I C 3 PERISTALTIC PUMP 13 ETHYL ALCOHOL [ ] I I S09HERSIBLE PUMP [ 7 OEIONIZED WRIER C 3 t I BAILER 13 TV SOLUTION 17 1 3 PVC/SILICON TUBING [ i HEXANE I ] [ 3 TEFLON/SIiiCON TUBING I I HNO3/I):1.WATER SOLUTION ' 1 3 1 7 AIR LIFT I I POTABLE WATER C 7 [ I MAND PUMP t 3 NONE I I IN -LINE FILTER I I # I PRESS/VAC FILTER 17 t3' iI FIELD ANALYSIS DATA AMBIENT AIR VOA PPM' WELL MCUTN -PPH FIELD DATA COLLECTED 17IR-LINE Iei: Ic; NO 16:'g0 I TIN CONTAINER PURGE DATA @ 0645' GAL is.GAL a 1.7 GAL. B 2 GAL fl - GAL TEMPERATURE, DEC C PH, units 1 SPECIFIC CONDUCTIVITY OXI DATI DN-REDUCTI ON,»/- mY OXIDATIONn a 25 dONI*/ DISSOLVED OXYGEN, ppm 21 ,N 6"� (o flab SAMPLE OBSERVATIONS: t ] TURBID [ ] COLORED t 7 CLOUDY L ] CLEAR # ] ODOR SAMPLE COLLECTION REOUI REMENFS (J 1f REQUIRED AT THIS LOCAT TON) �� �� 77 J If FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED HETROD REQUIRED COLLECTED I3 Il I / I L I i, [7 / I NOTES: ✓✓ Civil & Environmental Consultants, Inc. PROJECT IV"lL/ Q �tJ j�� SAMPLE LOCATION ID IV l' • — (0y) JOB NUMBER (I l PATE LOCATION ACTIVITY START: END: WATER LEVEL / WELL DATA 111 I ]MEASURED 1 ) TOP OF DELL CASING STICK-UP FT CASING/WELL DIFF. FT. WELL DEPTH 1 )HISTORICAL I ) TOP OF PROT. CASING (FROM GROUND) 11 WELL MATERIAL: �17ELL LOCKED?: WELL DIA. E 1 2 INCH - WATER LEVEL EQUIP.USED: WATER DEPTH 58. Q F7 17 PVC 13 13 YES. L 3 4 INCH C 3 ELECT.C.ONDiPROBE 13 SS f) NO 1 1 6 INCH C I FLOAT ACTIVATED 13 C I PRESS. TRANSDUCER L 7 .16 GAL/FT (21N:} GAL/VOL [) _ HEIGHT OF FT % ! 3 .65 CALM (4 IN.) o - WELL INTEGRITY: YES NO WATER COLUMN C 11.5 GAL/FT (6 IN.) PROT. CASING SECURE I I C 3 i ] iGAL/FT (_1N,) TOTAL GAL PURGEp CONCRETE COLLAR INTACT E I I I OTHER EQUIPMENT DOCUMENTATION ✓ IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT 10 (✓ ALL THAT APPLY AT LOCATION C 7 I3 PERISTALTIC PIMP I ] ETHYL ALCOHOL { I [ 7 SUBMERSIBLE PUMP 1 7 DEIORIZED ]CATER 1 ] 1 ) 13AILER 1 3 TSP SOLUTION I J C 3 PVC/SILICON TUBING I I HEXANE !) I J TEFLON/SILICON TUBING E J HNO3/P:I.WATER SOLUTION [ I 13 AIRS LIFT 1 3 POTABLE WATER C J 13 .NAND PUMP [ 3 NONE I I IN -LINE FILTER 1 I ! 3 PRESS/VAC FILTER I I [] !] FIELD ANALYSIS DATA - AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED I IIN-LINE - I 5 I IIN CONTAINER PURGE DATA O-°✓ GAGAL a I WL Q AL. a GAL a GAL TEMPERATURE, DEG C PH, units SPECIFIC , 2 25 IVITY (umioS/dm. a 25 deg.c) DISSOLVED -REDUCTION,+/- rtry DISSOLVED OXYGEN, PPm ---�'� (/, • Z Lr.y2 I ID • -1 F„•�r/ ITT S t�85 — y. O � -- _1 SAMPLE OBSERVATIONS: I J TURBID L ] COLORED 17 CLOUDY C ] CLEAR C 7 DOOR SAMPLE COLLECTION REQUIREMENTS � (✓ IF REQUIRED A7 THIS LOCATIONS ,( IF ✓ IT FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD - REQUIRED COLLECTED [ 7 r / r E3 r r NOTES: c Civil & Environmental Consultants, Inc. PROJECT NM W1/SLV JOB NUMBER [1t-37o.o©i PATE SAMPLE LOCATION ID rntA/- ��I LOCATION ACTIVITY START: �{,�(JQ END: WATER LEVEL / WELL DATA I )MEASURED 13 TOP OF WELL CASING STICK-UP FT CASING/WELL DIFF. - FT WELL DEPTHL�I I ]HISTORICAL I I TOP OF PRO% CASING (FROM GROUND) [I �� F7 WATER DEPTH Cy NEIGNT OF F7 WATER COLUMN EQUIPMENT DDCUHEHTATIDk PURG3 NG/SAMPLING EOU IP. USED: WELL MATERIAL: WELL LOCKED?: WELL DIA. C 1 2 INCH WATER LEVEL EQUIP,. USED: 13 PVC I J E) YES E 3 4 INCH E 3 ELECT,C,ONDiPROBE I I SS E J NO 11 6 INCH 13 FLOAT ACTIVATED 13. C I PRESS. TRANSDUCER I J ,tb PAL/FT (2 1H:) GAL/VDl' i I 465 GALIFT (4 IN..) _ C J 1.5 GAL/FT (6 IN.) i I _GAL/FT (�IN.) TOTAL GAL PURGED ,/ if USED FOR: PURGING SAMPLING I 1 I) PERISTALTIC PIMP I I T'FJ SUBMERSIBLE PUMP I J I ) BAI LER I ) I I PVC/SILICON TUBING I J I I TEFLON/SILICON-TUBING E 3 Cd AIR LIFT [ ) E 3 !LAND PUMP 13 IN -LINE FILTER I 1 PRESS/VAC FILTER tJ I1 [7 WELL INTEGRITY: YES NO PRDT. CASING SECURE 13 13 CONCRETE COLLAR INTACT 1 J 13 OTHER __ DECONTRMINAT iDN FLUIDS USED: EQUIPMENT 10 (J ALL THAT APPLY Al LOCATION I I ETHYL ALCOHOL I I DEIONIZED 'WATER I I TV SOLUTION I 1 HEXANE E 3 HNO3/D:LWATER SOLUTION 13 POTABLE WATER C 3 NONE I3 I7 fiELD ANALYSIS DATA AMBIENT AIR VOA PPH WELL MOUTH PPH FIELD DATA COLLECTED 13IN-LINE ' y ©d fj 6 [ I )IN CONTAINER PURGE DATA r� p: � GAL la I, C� .GAL a I • �i GAL. a a. o GAL a a.s GAL ph, mitURE, DEC C pH, tmiis SPECIFIC CONDUCTIVITY Cuar OXIDATION-REDUCTION,*/- my DISSOLVED OXYGEN, ppm DISSOLVED O GE deppm -f �ot - ,04 I1vol '7.O/40 a I 9 53� O ___L SAMPLE OBSERVATIONS: T 3 TURBID I 3 COLORED [ 7 CLOUDY [)tj CLEAR I j DOOR N lA. SAMPLE COLLECTION REOUI REMENTS (J IF REQUIRED AT THIS LOCATION) 4 If ✓ IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED [l T9 ✓ > / 13 C ] i / ! 13 I I I ] ! V [ J 13 GOD I I ! / ! NOTES: SOB NUMBER ' 1 RATE LOCATION ACTIVITY START: 1 0 d fj END: WATER LEVEL / WELL DATA C ]MEASURED I ] TOP OF WELL CASING STICK-UP FT CASING/WELL RIFF, F7 WELL DEPTH C ]HISTORICAL I J TOP OF PROT- CASING (FROM GROUND) CI 10 WELL MATERIAL: WATER DEPTHWELL LOCKED?: WELL DIA. [ 1 2 INCH WATER LEVEL EQUIP-. USED: ,Z� FT [ } PVC I I I ) YES t ) 4 INCH I I SS C I NO I J ELECT. ACTIVATED i J b INCH C I FLOAT ACTIVATED I J .16 GAL/FT (2IN:) GAL/VOL. I I I ] PRESS, TRANSDUCER HEIGHT OF FT I ] ,6S CALM(4 ]N.) _ C J X WATER COLUMN �� I J L5 GALL FT Lb IN,) WELL INTEGRITY: YES NO J GAL/FT PROT, CASING SECURE C I I] TOTAL GAL PURGED CONCRETE COLLAR INTACT I I I I OTHER EQUIPMENT DOCUMENTATION -J 1F USED FOR. DECONTAMINATION PURGING/SAMPLING EQUIP, USED: PURGING SAMPLING EQUIPMENT ID FLUIDS USED: . I J I -I PERISTALTIC PUMP I;/ ALL THAT APPLY AT LOCATION C ) I ) SUBMERSIBLE PUMP [ J ETHYL ALCOHOL C] I I BAILER I I DEl ONIZED 'WATER [ I I I PVC/SILICON TUBING I I TSP SOLUTION C) I I TEFLON/SILICON TOEING I I HEXANE. [ 7 L 3 AIR LIFT I I HNO3/II:I.WATER SOLUTION 1 I 13 NAND PUMP I I POTABLE WATER I I IN -LINE FILTER I I NONE L I PRESS/VAC FILTER L I (I II LI. FIELD ANALYSIS DATA • AMBIENT AIR VDA PPM WELL MOUTH PPM FIELD DATA COLLECTED { ITN-L1NE 0 ' I IIN CONTAINER PURGE DATA a Q•S GAL iJ V, O .GAL a J.L� GAL iJ oZ•O GAL 9 GAL- TEMPERATURE, _DEC C_ IFIIS SPECIFIC SPEClF7C CONDUCTIVITY OXIDATION-REDUCTION,+/- My {vhos/dm, 2S derrpm DISSOLVED OXYGEN, ( (q,d d •' � --�-�K- SAMPLE COLLECTION REQUIREMENTS t,l IF REQUIRED AT THIS LOCATION) J IF FIELD ANALYTICAL PARAMETER FILTERED 1 3 ;I (I L 1 1 �•Y/ � p 0� t3 it PROJECT I IV/ m � r/ /'I� � SAMPLE LOCATION ID F EEVV d If PRESERVATION _ ?/OLUME SAMPLE METH00 REgUI RED COLLECTED Il II {} [7 (I CT NOTES: c'iA rlY7V V'l/ `/ • � V g110IfS" SAMPLf BOTTLE ID'S SAMPLE OBSERVATIONS: C 7 TURBID I I COLORED [ 7 CLOUDY I7 CLEAR I ) ODOR PROJECTst��� SAMPLE LOCATION ID IY `�ti,/� NA7ER LEVEt / WELL DATA JDB NUMBER I .7.�n ODv� DATE D ✓I�rv� LOCATION ACTIVTTY START: END: L ]MEA"SURED L WELL DEPTH J TOP OF UELC CASING STICK-UP If� FT� U I ]HISTORICAL I I TOP OF PROT. CASING (FROM GROUND) J CASING/WELL RIFF. FT C) WATER DEPTH �(,I'A -�f FT WELL MATERIAL: WELL LOCKED?: WELL DIA. 17 4 INCH HATER LEVEL EQUIP.USED: INCH . 1 J.. 7✓I] [) C ^J YES 1 Ss k 1 I l SS I J NO i) 6 INCH I) FLOAT. ACTIVATED E 7 FLOAT ACTIVATED I ] .16 GAL/FT (2IN.) 17 C I PRESS. TRANSDUCER HEIGHT OF FT X I J .65 GAL/FT (4 IN.) = CAL/VOL - I I RATER COLUMN I ) 1.5 GAL/FT (6 IN.) WELL INTEGRITY: YES NO - I ] GAL/FT {IN,) TOTAL GAL PURGED CONCRETE COLLAR CINTACT I ) [ ] OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. -USED: PURGING SAMPLING I ) I I PERISTALTIC PUMP EQUIPMENT ID (✓ ALL THAT APPLY AT LOCATION [ 7 17 SUBMERSIBLE PUMP I I ETHYL ALCOHOL I] i I BAILER C I OEIONIZED WATER I ) "t7 PVC/SILICON TUBING -- I I TSP SOLUTION I I [ J TEFLON/SILICON-TUBING 11 HEXANE f} I I AIR LIFT L I HNQ3/p:I.WATER SOLUTION [ I [ i .NAND PUMP 17 POTABLE WATER I I _ IN -LINE FILTER C 7 NONE I I PRESS/VAC FILTER I I tJ Il t7 FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED I IIN-LINE �J I Ilk CONTAINER PURGE DATA GALJ@ "I GAL e Cj GAL CALSAMPLEOBSERVATIONS: TEHPERATURE, DEC C (7 C q ( i TUR&}ED PH, uilt5 '°---_L-LJ_ I I COLORED SPECIFIC CONDUCTIVITY C 7 CLOUDY (urhQslem. Z 25 deg•c) -� -,^h �I (�Gt�- d ] CLEAR OXIDATION-REDUCTION,*/- my -=L�-- I J DOOR DISSOLVED OXYGEN, -Ppm �77'�J. —--= �•srxa— . "SAMPLE COLLECTION REOVI REMENTS dd If REQUIRED AT THIS LOCATION) �! IF ANALYTFLAL PARAMETER J IF FIELD PRESERVATION • VOLUME SAMPLE SAMPLE BOTTLE ID'S FILTERED METHOD REQUIRED COLLECTED I 1 [ 17 1� I 11 tI O VT Avov NOTES: 'A? LAOAe nfj' � Civil & Environmental Consultants, Inc. PROJECT JOB NUMBER PATE SAMPLE LOCATION ID j;/�Ifv'_ LOCATION ACTIVITY START.: END: [LATER LEVEL / WELL DATA I ]MEASURED 17 TOP OF WELL CASING STICK-UP FT CASING/WELL DIFF. FT WELL DEPTH 17HISTOR]CAL [ J TDP OF PROT, CASING (fROlI GROUND) t7 10 WELL MATERIAL: WELL LOCKED?: WELL DIA. t 7 2 INCH - WATER LEVEL EQUIP.. USED: WATER DEPTH �LJ FT 17 PVC [ J 13 YES 1 3 4 INCH [ ] ELECT.CONDPkOBE [ I SS [ 3 NO [ 3 6 INCH [ J FLOAT ACTIVATED I I I I PRESS. TRANSDUCER I I .16 GAL/FT (2 IN:I GAL/VOL [ ] HEIGHT OF FT X I 1 .65 GAL/FT (4 IN.) _ WELL INTEGRITY; YES NO WATER COLUMN [ 1 1.5 GAL/FT (6 1)1.) PROT. CASING SECURE [ I I I 17 _GAL/FT („_IN,) TOTAL GAL PURGED CONCRETE COLLAR INTACT T I 17 OTHER EQUIPMENT DOCUMENTATION d IF USED .FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID (1 ALL THAT APPLY AT LOCATION 1 7 1'3 PERISTALTIC PUMP [ I ETHYL ALCOHOL [ I 17 SUBMERSIBLE PUMP 17 DEIONIZED WATER " C 3 I} aAt bER I I TSP SOLUTION [ 1 [ 3 PVC/SILICON TUBING I I HEXANE I I I TEFLON/SILICON TUBING t I HND3/D:I.WATER SOLUTION I-1 T I AIR LIFT - i I POTABLE WATER I I-- I I RAND PUFIP I I NONE I I _ IN -LINE FILTER 13 PRESS/VAC FILTER [ I FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED I IIN-LINE Oq: nQ•.� ha. 010 T 71N CONTAINER PURGE DATA c+ Q.•S GALIa �AL D Z. GAL. a� 2•S GAL a GAL TEMPERATURE, DEC C PH, tmiTs SPECIFIC CONDUCTIVITYiurffi OXIDATION-REDUCTION,* - MY DISSOLVED a 25 deg.c) OlS50WED OXYGEN, ppm _. __�. Lj ,q �Q_ h p, V O ---- O ---- - ---iJE SAMPLE COLLECTION REQUIREMENTS SJ IF RE9UIRED AT TH[5 LOCATION? �! Tf .1 1F FIELD PRESERVATION :VOLUME SAMPLE ANALYTICAL PARAMETER FILTERED METHOD ' REQUIRED *COLLECTED II I] I yam'/ [I 19 �y 4 II I I E3 ROTES: SAMPLE BOTTLE ID'S SAMPLE OBSERVATIONS: I J TURBID I ] COLORED T ] CLOUDY 17 CLEAR I ] OOOR PROJECT j y jv—r — 1 Mr ` SAMPLE LOCATION ID I WATER LEVEL / WELL DATA lV� VK JOB NUMBER lII_� .� PATE LOCATION ACTIVITY START: END: WELL DEPTH I ]MEASURED [ .3 TOP OF WELL CASING STICK-UP FT CASINGIWELL DIFF. FT _ I ]HISTORICAL t 7 TOP Of PROT. CASING iJ (FROM GROUND) HATER DEPTH // ryry,, StELL MATERIAL: HELL LOCKED?: WELL DIA. [ 3 2 INCH WATER LEVEL EQUIP. USED: IOV. FT 13 PVC I I I ) YES 13 4 INCH I I SS I I ND I J b INCH t 3 ELEC7.COND.,PROSE [ J t 3 FLOAT ACTIVATED [ 3 .16 GAL/FT (2 IN:) GAL/VOI,' I J PRESS. TRANSDUCER HEIGHT OF FT X ( 3 .65 GAL/FT (4 1N.) _ _ I 13 WATER COLUMN C 7 7.5 GAL/FT (6 14.) PROT4E1L 1NTEGRITY: YES NO I J , GAL/FT (__IN.) TOTAL GAL PURGED CONCRETE SING COLSECURE 1 3 I ] OTHER EQUIPMENT DOCUMENTATIUN ✓ If USED FORc DECONTAMINA7IpN FLUIDS USED: PURGINGJSAMPLINC EQUIP. USED: If SAMPLING I J r3 PERISTALTIC PUMP EQUIPMENT ID (J ALL THAT APPLY AT LOCATION 13 1 3 SUBMERSIBLE PUNp t 3 ETHYL ALCOHOL 13 I I BAILER ------= r 3 DEIONI2E0 'WATER r I I I QVC/SILICDN TUBING-- I J TSP SOLUTION 13 r 3 TEFLON/SILICON TUBING t J HEXANE ( 3 r 3 AIR LIFT I I HNO3/D.LWATER SOLUTION I 7 1 3 ,HAND PUMP - 13 POTABLE WATER ( 3 IN•LIHE FILTER �"--^' 13 NONE r J DRESSJVAC FILTER t J 11 !3 rI FIELD ANALYSIS DATA AMBIENT AIR VOA PURGE DATA G Q TEMPERATURE, DEC C pH, LmfIs SPECIFIC CONDUCTIVITY (unhOs/dm. @ 25 deg.c) OXIDATION-REDUCTION,+/- w DISSOLVED OXYGEN, ppm PM WELL HWTN PPH FIELD DATA COLLECTED (IrH-LINE II .jpk�' ( IIN CONTAINER a I CAL 2 Lo,' GAL.2 2- GAL a7GALSAHPLE OBSERVATIONS: vo•S IN•2 Dd'TURBID �o •R — tom', COLORED y� CLOUDY (oral CLEAR �2 1 1 WOR. SAMPLE COLLECTION RFOUI DEMENTS (.1 IF REQUIRED AT IRIS 1OCATION) ANALYTICAL PARAMETER 4 If FIELD PRESERVATION VOLUME .f IF S FILTERED METHOD AMPLE SAMPLE 80771E ID'S REQUIRED COLLECTED �Nm� L3 i I3 CA 0.3 �a !� J//� / ROTES: V V " -tJ� Nz o.c� �TDa gl(74f GO . o• h to : dc,/e(�„A �/ Civil & Environmental Consultants, Inc. PROJECT ��•I%/'a-�s'Ep JOB NUMBER I�I�.�Dl DATE tp f8 SAMPLE LOCATION SD mvm vvW LOCATION ACTIVTTY START: END: WATER LEVEL / WELL DATA CASINGr ]MEASURED t I TOP OF WELL WELL DEPTH L ]HIS ORICAL r 3 TOP OF PROT. CASING FROM AROUND) OASSNG/WELL DIEF. FT � FTC WELL MATERIAL: WELL LOCKED?: WELL D1A. 1 1 2 INCH WATER LEVEL EQUIP.. USED: WATER DEPTH �. F'f I ] PVC I ] I ) YES C ] 4 INCH C 3 ELECT.COnT%PROBE I] SS 1 3 NO I] 6 INCH C 3 FLOAT ACTIVATED I ] C I PRESS. TRANSDUCER C ] .16 GAL/FT (2IN..) GAL/VDL C 7 HEIGHT OF FT X L 1 .65 GAL/FT T4 IN.) _ '' - WELL INTEGRITY: YES NO WATER COLUMN I ] 1.5 GAL/FT K6 IN.PRDT. CASING SECURE 1 ] I ] I ] _GAL/FT t_IN J TOTAL GAL PURGED CONCRETE COLLAR INTACT I ] I I OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT I➢ IJ ALL THAT APPLY AT LOCATION I ] I PERISTALTIC PUMP 13 ETHYL ALCOHOL [ ] L ] SUBMERSIBLE PUMP_ C ] DEIONIZEO 'WATER C ] I I EAT UER I ] TSP SOLUTION L ] 13 PVC/SILICON TUBING I I HEXANE I I C ] TEFLONJSILICON THING I ] HNO3/D=i.WATER SOLUTION 13 13 AIR LIFT 1 3 POTABLE WATER I ] T ] HAND PUMP T 3 NONE I I IN -LINE FILTER C 3 1 3 % PRESS/VAC FILTER I3 11 FIELD ANALYSIS DATA AMBIENT AIR VDA PPM WELL MOUTH PPM FIELD DATA COLLECTED I IIN-LINE 5:I a- 15 L3;zp 25 1 )IN CONTAINER PURGE -DATA Q GAL I>a _GAL a (.� GAL. 2 Z GAL U GAL' TEMPERATURE, DEC; C^— PH, unfits SPECIFIC CONDUCTIVITY OXIDATION-REDUCTION,*/- mV_� OXIDATION-.h 2S dON,+/ DISSOLYED OXYGEN, ppmNOISE (O' O `-- �i�jp�- Z•O� 0. M —�KfSp SAMPLE COLLECTION REQUIREMENTS TJ IF REWIRED AT THIS LOCATION) .( IF J IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE IO'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED NOTES: SAMPLE OBSERVATIONS: T ] TURBID L ] COLORED C 7 CLOUDY 6 ] CLEAR I ] ODOR xr '. mo fnmff Civil & Environmental Consultants, Inc. PROJECT I ! ✓ nti V � — 6 � 01 c� c JOB NUMBER `--u-Y f DATE SAMPLE LOCATION ID I JV\ � - ''l LOCATION lON ACTIVITY START: q 6 `) EHD: Cj>S WATER LEVEL / WELL DATA CASINGt ]MEASURED t I TOP OF WELL WELL DEPTH F7 ( )HISTORICAL [ I TOP Of ROT. CASING (P fT CASING/WELL DIf F. (FROM GROUND)fT WELL MATERIAL: WELL LOCKED?: WELL DIA. C 1 2 INCH WATER LEVEL EQUIP. USED: WATER DEPTH '' fT [ J PVC C ) C J YES - [ 7 4 INCH C 7 ELECT.COND.PROBE C J SS C J NO C J 6 INCH C 7 FLOAT ACTIVATED C J C J PRESS. TRANSDUCER C 7 .16 GAL/FT (2 IN GAL/VOL [ 7 HEIGHT OF FT X C J .65 GAL/FT (4 IN.) = WELL INTEGRITY: YES NO WATER COLUMN C 7 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C 7 [ J C 7 _GAL/FT (_IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT C 7 C 7 OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: CURGINWSAMPLI HG EOU1 P. USED: PURGIXG SAMPLING C 7 [ 7 PERISTALTIC PUMP ( 7 C 1 SUBMERSIBLE PUMP ( ) ( I BAILER C 7 C 7 PVC/SILICON TUBING C 7 C 7 TEFLON/SILICON TUBING L 1 C 3 AIR LIFT C I C 7 HAND PUMP C 7 IN -LINE FILTER _ C I PRESS/VAC FILTER I I DECONTAMINATION FLUIDS USED: EQUIPMENT 7D (J ALL THAT APPLY AT LOCATION C 7 ETHYL ALCOHOL C 7 DEIONIZED WATER C 7 TSP SOLUTION C 7 HEXANE ( 7 HHO3/D.i.WATER SOLUTION C 7 POTABLE WATER C 7 NONE CJ FIELD ANALYSIS DATA ANB7ENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED [ 71N-U NE I )IN CONTAINER PURGE DATA D L i, � Gfj(,la (- GX1n a I 1- Ow � '12 L- GAb a GAL TEMPERATURE, DEG C PH, Unix$ SPECIFIC CONDUCTIVITY (urMos/cm- O 25 deg.c) OXIDATION -OXYGEN, ON,m/- DISSOLVED OXYGEN, ppm 13 - a 1 'J S'� 1 3- j 5 - I (?,;'^�- �>-]-O ., .! !A _ �? i.. / �/. ( SAMPLE OBSERVAiI OHS: ( ] TURBID C 7 COLORED J CLOUDT CLEAR I OR SAMPLE COLLECTION REQUIREMENTS (J lF AEWI0.ED AT THIS LOCATION) J IF J IF FIELD PRESERYAT iDN VOLUME SAMPLE SAMPLE BOTTLE 1D'S ANALYTICAL PARAMETER FILTERED METHOD REWIRED COLLECTED [7 C7 [] I C7 NOTES: } MOW � P/ / J �s ' Civil & Environmental Consultants, Inc. PROJECT /M t� F _ JOB NUMBER 13�o-on DATE 1 %la(I SAMPLE LOCATION ID I M L LOCATION ACTIVITY START: END: WATER LEVEL / WELLDATA ( ]MEASURED ( ) TOP Of WELL LASING STICK-UP FT CASING/YELL DIFF, FT WELL DEPTH FT 1 )HISTORICAL 1 I TOP OF PROT. CASING (FROM GROUND) 17 WELL MATERIAL: WELL LOCKED7: WELL DIA. I ] 2 INCH . WATER LEVEL EQUIP. USED: WATER DEPTH i- ,� FT ( ] PVC C 1 C ) YES [ 7 4 INCH I ) ELECT.COND.PROBE 17 SS C 7 NO C 7 6 INCH 17 FLOAT ACTIVATED ....—._ ( 7 17 PRESS. TRANSDUCER ( ) .16 GAL/PT (2 1N.1 GAL/VOL 17 HEIGHT OF FT X 1 7 .65 GAL/FT (4 IN.) _ WELL INTEGRITY: YES NO WATER COLUMN 17 1.5 GAL/FT (6 IN.) PROT. CASING SECURE C 7 [ 7 C 7 _GAL/FT SIN,) TOTAL GAL PURGED CONCRETE COLLAR INTACT 17 C ] OTHER EQUIPMENT DOCVMExTA710N J IF USED iDR: DECONTAX]NATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID (J ALL THAT APPLY AT LOCATION I ] 1 7 PERISTALTIC PUMP 17 ETHYL ALCOHOL I ) [ 7 SUBMERSIBLE PUMP 17 DEIONIZED WATER ( ] C 7 BAILER 17 TSP SOLUTION 17 I ] PVC/SILICON TUBING 17 NEXANE 17 I ] TEFLON/SILICON TUBING I ] HNO3/D.1.WATER SOLUTION [ 1 17 AIR LIFT 17 POTABLE WATER L 7 [ 7 HAND PUMP C J NONE C 7 _ IN -LINE FILTER I ] 17 PRESS/VAC FILTER C ] [] I7 FIELD ANALYSIS DATA AMBIENT AIR VOA PPX WELL MOUTH PPM FIELD DATA COLLECTED C ]IN -LINE I ]IN CONTAINER PURGE DATA a JJ Gxtj@ I� l,� L�f� a � L. 6NL a GAL a GAL SAMPLE OBSERVATIONS: 17 TURBID TEMPERATURE, DEG C Ci 3 I - l ) -"� R W COLORED PH, W its I) CLOUDY SPECIFIC CONDUCTIVITY 1 7 CLEAR (Lahos/cm. a 25 de6•0 �? 7 li �j `t (7 17 ODOR OXIDATION-REDUCTION,/- my -e31 -9-- DISSOLVED OXYGEN, OpA SAMPLE COLLECTION REQUIREMENTS (J IF REQUIRED AT THIS LOCATION) J IF J IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE 1D'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED - II I7 II L7 NOTES: S";� U� Civil & Environmental Consultants, Inc. PROJECT N1 " �� JOB NUMBER II _ .� DATE -1 p SAMPLE LOLAiTON ID �,W�®p LOCATION, ACTIVITY START: END: WATER LEYEt ! WELL DATA 17MEASUREb ( ] SOP OF DELL CASINO STICK-UP FT USING/HELL DIfF, FT WELL DEPTH FT I )HISTORICAL [ ) TOP OF WT. CASING (FROM GRCUND) I3 WELL MATf,RIAL& WELL LOCKED?: WELL DIA. 13 2 INCH WATER LEVEL EQUIP. USED: WATER DEPTH _ 5 F7 T C7 3 PVC 17 17 YES [ 3 4 INCH 1 7 ELE.CONDPROBE 1 7 SS { 7M0 CTIVATED 16 INCH ] PRESS. fWAT TRANSDUCER 1 3 .16 GAL/FT O2 IN, GAL/VOL - [ 7 HEIGHT OF FT X 1 3 .65 GAL/FT (4 IN.) _ - WELL INTEGRITY: YES NO WATER COLUMN C 7 1.5 GAL/FT L6 I).) PROT. CASING SECURE [ ] 13 I J GAL/FT (vIN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT I I I I OTHER _. EQUIPMENT DOCUHENTAT ION -/ If USED FOR: DECONTAMINkTIDN FLUIDS USED. PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING I EQUIPMENT ID IJ ALL THAT APPLY AT LOCATION 1 ] 13 PERISTALTIC PUMP - T 3 ETHYL ALCOHOL I I 17 SUBMERSIBLE PUMP 13 DEIONIZED WATER I I t I BAILER L] tSP SOLUTION 13 I 3 PVC/S3IICON TUBING [ 1 HEXANE 13 1 3 TEFLON/SILICON TUBING 13 MN03ID.I.WATER SOLUTION [ 3 I I AIR LIFT [ I POTABLE WATER C) I I .RAND PUMP L 3 NONE I I IN -LINE FILTER [ 3 I ] PRESS/VAC FILTER [ 7, I] 13 FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL HWTN PPM FIELD DATA COLLECTED I ]TN -LINE /t IU' I.110 lgzo 4'2iSN CONTAINER PURGE DATA BO�•S�GAt,ia &AL'�J� GAL. aD GAL a K+S GAL SAMPLE OBSERVATIONS: L 3 TURBID T 3 COLORED Ij� CLOUDY L 3 CLEAR 13 ODOR SAMPLE COLLEtTIDN REQUIREMENTS f If IJ IF REQUIRED AT THIS LOCATION? J IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED I7 I7 ! I ! L3 tee l S �I [7 f ! L7 I 7 •, l rr �y� � Q" L3 �Lk I3 fI J I NDT£s: could W��ISIG�W SAMPLE COLLEtTIDN REQUIREMENTS f If IJ IF REQUIRED AT THIS LOCATION? J IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED I7 I7 ! I ! L3 tee l S �I [7 f ! L7 I 7 •, l rr �y� � Q" L3 �Lk I3 fI J I NDT£s: could W��ISIG�W Civil & Environmental Consultants, Inc. PROJECT 7L 1 GJ D 106 NUMBER , PATE SAMPLE LOCATION ID I rn W 1 1 —�. LOCATION ACTIVTTY START: END: WATER LEYEL / HELL DATA L ]MEASURED ; I TOP OF WELL CASING STICK-UP FT CASING/WELL DIFF. FT WELL DEPTHFT I ]HISTORICAL C ) 715P OF PROT. CASING SFROM GROU9P) [7 WELL HFTERIAL: WELL LOCKED?: WELL OIA. [ 7 2 INCH WATER LEVEL EQUIP.. USED: FT 13 PVC I 1�1 7 YES 1 3 4 INCH C I ELECT.CONDPROBE WATER DEPTH, [ 3 SS C 3 NO t 3 6 INCH [ 7 FLOAT ACTIVATED ; I [ 3 PRESS. TRANSDUCER ; 3 .16 GAL/FT (2 IN.) GAL/VOL C 3 HEIGHT OF fT X I I .65 GAS/FT C4 ]N.) WELL INTEGRITY-: YES NO WATER COLUMN 17 1.5 GAL/FT (6 IN.) PROT. CASING SECURE I 1 13 I ] GAL/FT 1N.) TOTAL GAL PURGED CONCRETE COLLAR INTACT I 1 13 OTHER EQUIPMENT DOCUMENTATION j IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT 10 CJ ALL THAT APPLY AT LOCATION I j t3 PERISTALTIC PUMP 13 ETHYL ALCOHOL 13 1 3 SUBMERSIBLE PUMP T I DEIOKI2ED 'WATER 13 13 SAILER I j TSP SOLUTION I ] 13 PYC/SILICON TUBING C 7 HEXANE [ ] 1 7 TEFLON/SILICON-TUBING [ 3 HHQUP.I.WATER SOLUTION ' t 3 C 3 AIR LIFT - C 3 POTABLE WATER C 3 t 7 NAND PUMP t 3 NONE ] IN -LINE FILTER I I [ 7 PRESS/VAC FILTER I I, t7 I7 FIELD ANALYSIS DATA AMBIENT AIR VDA PPM WELL MOUTH PPM FIELD DATA COLLECTED I ITN. -LINE ' OJ 140.10 C IIN CONTAINER PURGE -DATA r, 6.•5*yy GAL a ��Q ..GAL 0 f •S GAL. a GAL 9 GAL as SAMPLE COLLECTION REQUIREMENTS it IF REQUIRED AT THIS LOCATION) .I IF J IT FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE IDIS ANALYTILAi PARAMETER TES: FILTERED METHOD REQUIRED (\Fi IQ° . I ba( 5 SAMPLE OBSERVATIONS: C 7 TURBID L 7 CDLORED [ J CLOUDY L I CLEAR [ 7 ODOR COLLECTED7 / / / COLLECTED7 / / / t t� lwwa� m �F M" / y � �nY Civil & Environmental Consultants, Ine. PROJECT I pJ AA L JOB NUMBER DATE SAMPLE LOCATION ID ? '�� LOCATION ACTIVITY START: END: WATER LEVEL / WELL DATA I ]MEASURED C I TOP OF WELL CASING STICK-UP FT CASING/WELL DIFF, FT WELL DEPTH FT C 3HISTORICAL 13 TOP OF PROT. CASING (FROM GROUND) 17 WELL MATERIAL: WELL LOCKED?: WELL DIA. C 7 2 INCH - WATER LEVEL EQUIP. USED: WATER DEPTH 3. o� FT C J PVC [ 7 C ] YES C 7 4 INCH 17 ELEC%COND.PROBE C ] SS [ 7 NO C 3 6 INCH 17 FLOAT ACTIVATED C 7 C ) PRESS. TRANSDUCER [ 7 .16 GAL/FT (2 1N-) GAL/VOL C J HEIGHT OF FT X C 1 .65 GAL/FT (4 IN.) c WELL INTEGRITY: YES NO WATER COLUMN [ 3 1.5 GAL/FT (6 IN,) PROT. CASING SECURE C 3 C ] [ ] _GAL/FT ( IN.) TOTAL GAL PURGED CONCRETE COLLAR INTACT t ] C 3 OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: PURGING/SAMPLING EDU1 P. USED: PURGING SAMPLING I ] [ ) PERISTALTIC PUMP ( ) [ ) SUBMERSIBLE PUMP t ) [ ] BAILER C J 13 PVC/SILICON TUBING C J C 3 TEFLON/SILICON TUBING t 1 [ 7 AIR LIFT C ] [ 7 HAND PUMP C 7 IN -LINE FILTER _ C ] PRESS/VAC FILTER DECONTAMINATION FLUIDS USED: EQUIPMENT ID (J ALL THAT APPLY AT LOCATION [ 7 ETHYL ALCOHOL I ] DEIONIZED WATER [ 7 TSP SOLUTION ( 7 HEXANE ( 3 HNO3/D.I.WATER SOLUTION [ 7 POTABLE WATER ( ) NONE C) FIELD ANALYSIS DATA AMBIENT AIR VOA PPX WELL MOUTH PPM FIELD DATA COLLECTED [ 7JN-LINE [ ]IN CONTAINER � PURGE DATA GAL ' SAMPLE OBSERVA710N5: TURBID SAMPLE COLLECTION REQUIREMENTS (V IF REQUIRED AT THIS LOCATION) J IF J IF FIELD PRESERVATION _ VOLUME SAMPLE. SAMPLE BOTTLE ID'S ANALYTICAL PARAMETER FILTERED METHOD REWIRED COLLECTED I) NOTES: Civil & Environmental Consultants, Inc. PROJECT C I e 5 r cQ JOB NUMBER 0 A 1- 3 -7 D DATE SAMPLE LOCATION ID Aq 1-! LOCATION ACTIVITY START: IU7 END: WATER LEVEL / WELL DATA [ )MEASURED I) TOP OF WELL CASING STICK-UP FT CASING/WELL DiFF. FT WELL DEPTH FT I )HISTORICAL 1 ) TOP OF PROT. CASING (FROM GROUND) C7 WELL MATERIAL: WELL LOCKED?: WELL DIA. 17 2 INCH WATER LEVEL EQUIP. USED: WATER DEPTH I PVC 17 C I YES I J 4 INCH I J ELECT.COND.PROSE C 7 SS I I NO L; 6 INCH j� FLOAT ACTIVATED ATRANSDUCER I I .76 GAL/FT (2 IN.) GAL/VOL C ] HEIGHT OF FT X I J .65 GALIFT (4 IN.) = WELL INTEGRITY: YES NO WATER COLUMN C 11.5 GALIFT (6 IN.) PROT. CASING SECURE C 7 I I I I GAL/FT (_IN,) TOTAL GAL PURGED CONCRETE COLLAR INTACT [ 7 C ] OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: DECONTAMINATION FLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ]D (J ALL THAT APPLY AT LOCATION I I 1 I PERISTALTIC PUMP 17 ETHYL ALCOHOL I ] 1 ] SUBMERSIBLE PUMP [ I DEIONIZED WATER [ I [ 7 BAILER C 7 TSP SOLUTION I J I) PVC/SILICON TUBING [ J HEXANE 1 I 1 J TEFLON/SILICON TUBING ( ] HNO3/D.I.WATER SOLUTION [ 7 I J AIR LIFT 1 I POTABLE WATER I J C I HAND PUMP C) MORE I J IN -LINE FILTER [ 7 C I PRESSIVAC FILTER I I C] tJ FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PDM FIELD DATA COLLECTED [ N-LINE ]I [ ]IN CONTAINER PURGE DATA 0A6 al �(...,. apt a :2 "2 C'BAk SAMPLE OSSERVATIONS: `j7' T I TURBID 7 j_ t 2,t I COLORED 3 ; 9 L,J CLOUDT jkT CLEAR DOOR 17 SAMPLE COLLECTION REOUI REHENTS ✓ IF (J IF REQUIRED AT THIS LOCATION) ✓ IF FIELD PRESERVATION _ VOLUME SAMPLE SAMPLE BOTTLE 10'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED I) 17 I I 17 C J [I I) I I I] IJ NOTES: Civil & Environmental Consultants, Inc. 4 PROJECT 1.v^., t- - G4. c ,_ Jt JOB NUMBER L-L'- DATE SAMPLE LOCATION ID ,� W: '� D , LOCATION ACTIVITY START: END: I,; - WATER LEVEL / WELL DATA CASINGr )MEASURED I TOP OF WELL WELL DEPTH FT I )HISTORICAL ` 3 TOP OF ROT. CASING (P FT CASING/DELL Dl Ff. FROM GROUND ) FT WELL MATERIAL: WELL LOCKED?: WELL DIA. [ 7 2 INCH - WATER LEVEL EQUIP. USED: WATER DEPTH {`} '� [: FT [ 7 PVC I 1 I 1 YES 17 4 INCH I I ELECT.COND.PROBE I) SS C 7 NO I J 6 INCH I l FLOAT ACTIVATED -••----- 17 17 PRESS. TRANSDUCER I I .16 GAL/FT (2 IN.) GAL/VOL - I J HEIGHT OF FT % 17 .65 GAL/FT (4 IN.) = WELL INTEGRITY: YES NO WATER COLUMN ( 3 1_5 GALIF7 (6 IN.) PROT. CASING SECURE C 3 C 7 C 1 _GAL/FT (_INJ TOTAL GAL PURGED CONCRETE COLLAR INTACT C 7 C I OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: DECONTAMINATION iLUIDS USED: PURGING/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT 1D (,/ ALL THAT APPLY AT LOCATION I ) [ 7 PERISTALTIC PUMP I ) ETHYL ALCOHOL 13 C 3 SUBMERSIBLE PUMP 17 DEIONIZED WATER I 1 [ 7 BAILER 17 TSP SOLUTION 13 1 J PVC/SILICON TUBING 1 7 HEXANE I 1 [ 3 TEFLON/SILICON TUBING 13 HNO3/D.I.WATER SOLUTION C 1 13 AIR LIFT 1 ) POTABLE WATER 17 [ 7 HAND PUMP I ) NONE C 3 IN -LINE FILTER I 1 17 PRESS/VAC FILTER 17 C7 I7 FIELD ANALYSIS DATA AMBIENT AIR VOA PPM WELL MOUTH PPM FIELD DATA COLLECTED 1]1N-LINE [ 71N CONTAINER PURGE DATAdA6'D BALa GAL a DAL TEMPERATURE, DEG C PH, MitS SPECIFIC CONDUCTIVITY (utdioi/cm. Q 25 de9•c> OXIDATION -OXYGEN, ON,m/• my DISSOLVED OXYGEN, ppm ( - 13 , (= �1 1 - 7 ��' 7-:�-j — 7- 5d jvI iv .- K�- ,> ==-�J SAMPLE COLLECTION REQUIREMENTS (J 1F REQUIRED AT THIS LOCATION) - J IF J IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE 1D'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED SAMPLE OBSERVATIONS* C ) TURBID C ) COLORED 17 CLOUDY jc7 CLEAR [ 7 ODOR [) NOTES: q V V Y 5 -i �y°I J 1Z� Civil & Environmental Consultants, Inc. PROJECT �, _ �,( d j P_ JOB NUMBER ,� DATE SAMPLE LOCATION ID GJ _ I ,.- LOCATION ACTIVITY START: L? 7 O END. WATER LEVEL / WELL DATA L )MEASURED ( 7 TOP OF WELL CASING STICK-UP FT CASING/HELL DIFF. fT WELL DEPTH E=FT I )HISTORICAL I ) TOP OF PROT. CASING (FROM GROUND) C7 WELL MATERIAL: WELL LOCKED?: WELL DIA. 17 2 INCH WATER LEVEL EQUIP. USED: WATER DEPTH -7s FT C 7 PVC 17 [ 3 YES [ ) 4 INCH ( 3 ELECT.COND.PROBE I] SS [ l NO t l 6 INCH I J FLOAT ACTIVATED C ] C 3 PRESS. TRANSDUCER C ] .16 GAL/FT (2 IN.) GAL/VOL I ) HEIGHT OF FT % ( 1 .65 GAL/FT (4 IN.) = WELL INTEGRITY: YES NO WATER COLUMN 17 1.5 GAL/FT 16 IN.) PROT. CASING SECURE C 7 C I 17 _GAL/FT (_IN.) TOTAL WL PURGED CONCRETE COLLAR INTACT [ 7 [ J OTHER EQUIPMENT DOCUMENTATION J IF USED FOR: DECONTAMINATION FLUIDS USED: PURG7NG/SAMPLING EQUIP. USED: PURGING SAMPLING EQUIPMENT ID (J ALL THAT APPLY AT LOCATION I J C ] PERISTALTIC PUMP 17 ETHYL ALCOHOL ( ] 17 SUBMERSIBLE PUMP 17 DEIONIZED WATER [ 7 17 BAILER I l TSP SOLUTION C] I J PVC/SILICON TUBING C 7 HEXANE I J 1 3 TEFLON/SILICON TUBING ( 3 HNO3/D.I.WATER SOLUTION C ] C ] AIR LIFT 17 POTABLE WATER [ ] C ] HAND P(04P 13 NONE 17 IN -LINE FILTER ( J [ 7 PRESS/VAC FILTER [ 7 [7 I] FIELD ANALYSIS DATA - AMBIENT AIR VOA ➢PM WELL MOUTH PPN FIELD DATA COLLECTED [ TIN -LINE - I 31N CONTAINER PURGE DATA la Ij /�L,ggygla L_ �:(D,.L a a 10-L. �ZGAt ' SAMPLE COLLECTION REQUIREMENTS (J IF REQUIRED AT THIS LOCATION) -1 IF FIELD PRESERVATION VOLUME SAMPLE SAMPLE BOTTLE 1D'S ANALYTICAL PARAMETER FILTERED METHOD REQUIRED COLLECTED L7 [ 7 ' _ I I7 [7 ©00 17 LI NOTES: SAMPLE OBSERVATIONS: I) TURBID I j G I CO i ] LORED I ) CLOUDY CLEAR 1 (� I 7 ODOR `7 APPENDIX B Civil & Environmental Consultants, Inc. TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Tel: (708)534-5200 TestAmerica Job ID: 500-143709-1 TestAmerica SDG: NCDEQ Solid Waste Facility = # 60-13 Client Project/Site: North Mecklenburg Landfill - Closed ror: Civil & Environmental Consultants Inc 1900 Center Park Drive Suite A Charlotte, North Carolina 28217 Attn: Mr. Ed Stephens A6%�/V 6W Authorized for release by: 51912018 5:02:16 PM Robin Kintz, Project Manager II (708)534-5200 robin.kintz@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 F Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Table of Contents CoverPage .............................................. 1 Table of Contents ......................................... 2 Definitions/Glossary....................................... 3 L Client Sample Results ...................................... 4 Lab Chronicle ............................................ 48 Certification Summary ...................................... 56 Method Summary ......................................... 57 Sample Summary ......................................... 58 Chain of Custody .......................................... 59 Receipt Checklists ......................................... 64 TestAmerica Chicago Page 2 of 64 5/9/2018 Definitions/Glossary Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Qualifiers GC/MS VOA Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. cn Refer to Case Narrative for further detail Metals Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. F1 MS and/or MSD Recovery is outside acceptance limits. General Chemistry C Qualifier Qualifier Description F1 MS and/or MSD Recovery is outside acceptance limits. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. tt Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Chicago Page 3 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW1 Lab Sample ID: 500-143709-1 Date Collected: 04/10/18 10:15 Matrix: Water Date Received: 04/12/18 09:10 F Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 19:03 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 19:03 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 19:03 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 19:03 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/18 19:03 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 19:03 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 19:03 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 19:03 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 19:03 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 19:03 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 19:03 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 19:03 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 19:03 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 19:03 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 19:03 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 19:03 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 19:03 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 19:03 1 Benzene <0.15 0.50 0.15 ug/L 04/18/18 19:03 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 19:03 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 19:03 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 19:03 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 19:03 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 19:03 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 19:03 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 19:03 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 19:03 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 19:03 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 19:03 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 19:03 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 19:03 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 19:03 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 19:03 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 19:03 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 19:03 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 19:03 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 19:03 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 19:03 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 19:03 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 19:03 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 19:03 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 19:03 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 19:03 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 19:03 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 19:03 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 19:03 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 19:03 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 19:03 1 0 TestAmerica Chicago Page 4 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW1 Lab Sample ID: 500-143709-1 Date Collected: 04/10/18 10:15 Matrix: Water Date Received: 04/12/18 09:10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 95 75- 126 04118118 19703 1 4-Bromofluorobenzene (Surr) 89 72 - 124 04118118 19:03 1 Dibromofluoromethane 93 75 - 120 04118118 19:03 1 Toluene-d8 (Surr) 93 75 - 120 04118118 19:03 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1811:39 1 Arsenic 0.97 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1811:39 1 Barium 33 2.5 0.73 ug/L 04/12/1815:45 04/13/1811:39 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1811:39 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1811:39 1 Chromium <1.1 5.0 1.1 ug/L 04/12/1815:45 04/13/1811:39 1 Cobalt 0.87 J 1.0 0.40 ug/L 04/12/1815:45 04/13/1811:39 1 Copper <0.50 2.0 0.50 ug/L 04/12/1815:45 04/13/1811:39 1 Iron 6000 100 47 ug/L 04/12/1815:45 04/13/1811:39 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1811:39 1 Manganese 1600 2.5 0.79 ug/L 04/12/1815:45 04/13/1811:39 1 Nickel <0.63 2.0 0.63 ug/L 04/12/1815:45 04/13/1811:39 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1811:39 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1811:39 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1811:39 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1811:39 1 Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1811:39 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1810:37 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 7300 200 170 ug/L 04/21/1812:58 1 Sulfate 42000 2000 950 ug/L 04/21/1813:11 10 Alkalinity 210000 5000 3700 ug/L 04/20/1814:32 1 Total Dissolved Solids 270000 10000 4300 ug/L 04/13/18 05:50 1 Client Sample ID: MW4 Lab Sample ID: 500-143709-2 Date Collected: 04/09/18 11:05 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/1819:29 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/1819:29 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/1819:29 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/1819:29 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/1819:29 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/1819:29 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/1819:29 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/1819:29 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/1819:29 1 TestAmerica Chicago Page 5 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW4 Lab Sample ID: 500-143709-2 Date Collected: 04/09/18 11:05 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 19:29 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 19:29 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 19:29 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 19:29 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 19:29 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 19:29 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 19:29 1 Acetone 2.7 J cn 5.0 1.7 ug/L 04/18/18 19:29 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 19:29 1 Benzene 0.74 0.50 0.15 ug/L 04/18/18 19:29 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 19:29 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 19:29 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 19:29 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 19:29 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 19:29 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 19:29 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 19:29 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 19:29 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 19:29 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 19:29 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 19:29 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 19:29 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 19:29 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 19:29 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 19:29 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 19:29 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 19:29 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 19:29 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 19:29 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 19:29 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 19:29 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 19:29 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 19:29 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 19:29 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 19:29 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 19:29 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 19:29 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 19:29 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 19:29 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 96 75- 126 04118118 19:29 1 4-Bromofluorobenzene (Surr) 89 72 - 124 04118118 19:29 1 Dibromofluoromethane 94 75 - 120 04118118 19:29 1 Toluene-d8 (Surr) 91 75 - 120 04118118 19:29 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1811:58 1 Arsenic 0.82 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1811:58 1 0 TestAmerica Chicago Page 6 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW4 Lab Sample ID: 500-143709-2 Date Collected: 04/09/18 11:05 Matrix: Water Date Received: 04/12/18 09:10 Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Barium 430 2.5 0.73 ug/L 04/12/1815:45 04/13/1811:58 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1811:58 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1811:58 1 Chromium 3.1 J 5.0 1.1 ug/L 04/12/1815:45 04/13/1811:58 1 Cobalt 4.8 1.0 0.40 ug/L 04/12/1815:45 04/13/1811:58 1 Copper <0.50 2.0 0.50 ug/L 04/12/1815:45 04/13/1811:58 1 Iron 1600 100 47 ug/L 04/12/1815:45 04/13/1811:58 1 Lead 1.1 0.50 0.19 ug/L 04/12/1815:45 04/13/1811:58 1 Manganese 730 2.5 0.79 ug/L 04/12/1815:45 04/13/1811:58 1 Nickel 4.9 2.0 0.63 ug/L 04/12/1815:45 04/13/1811:58 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1811:58 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1811:58 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1811:58 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1811:58 1 Zinc 40 10 6.9 ug/L 04/12/1815:45 04/13/1811:58 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 F1 0.20 0.098 ug/L 04/13/1812:05 04/16/1810:39 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 23000 1000 850 ug/L 04/21/1814:52 5 Sulfate 18000 400 190 ug/L 04/21/1814:40 2 Alkalinity 310000 5000 3700 ug/L 04/20/1814:43 1 Total Dissolved Solids 410000 10000 4300 ug/L 04/13/18 05:53 1 Client Sample ID: MW4A Date Collected: 04/09/18 12:10 Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: 500-143709-3 Matrix: Water Analyte Result Qualifier RL MDL Unit D 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 2-Hexanone <1.6 5.0 1.6 ug/L 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L Acetone 2.6 J cn 5.0 1.7 ug/L Prepared Analyzed Dil Fac 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 04/18/18 19:55 1 0 TestAmerica Chicago Page 7 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW4A Lab Sample ID: 500-143709-3 Date Collected: 04/09/18 12:10 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 19:55 1 Benzene <0.15 0.50 0.15 ug/L 04/18/18 19:55 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 19:55 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 19:55 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 19:55 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 19:55 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 19:55 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 19:55 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 19:55 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 19:55 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 19:55 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 19:55 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 19:55 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 19:55 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 19:55 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 19:55 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 19:55 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 19:55 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 19:55 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 19:55 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 19:55 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 19:55 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 19:55 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 19:55 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 19:55 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 19:55 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 19:55 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 19:55 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 19:55 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 19:55 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 19:55 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 95 75- 126 04118118 19:55 1 4-Bromofluorobenzene (Surr) 92 72 - 124 04118118 19:55 1 Dibromofluoromethane 94 75 - 120 04118118 19:55 1 Toluene-d8 (Surr) 92 75 - 120 04118118 19:55 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:01 1 Arsenic 0.75 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:01 1 Barium 180 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:01 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:01 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:01 1 Chromium 7.9 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:01 1 Cobalt 3.6 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:01 1 Copper 23 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:01 1 Iron 5600 100 47 ug/L 04/12/1815:45 04/13/1812:01 1 Lead 6.5 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:01 1 0 TestAmerica Chicago Page 8 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW4A Lab Sample ID: 500-143709-3 Date Collected: 04/09/18 12:10 Matrix: Water Date Received: 04/12/18 09:10 , Method: 6020B - Metals ICP/MS - ( ) Total Recoverable Continued (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Manganese 94 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:01 1 Nickel 9.7 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:01 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:01 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:01 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:01 1 Vanadium 14 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:01 1 E: Zinc 90 10 6.9 ug/L 04/12/1815:45 04/13/1812:01 1 Method: 7470A - Mercury (CVAA) F Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury 0.26 0.20 0.098 ug/L 04/13/1812:05 04/16/1810:46 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 10000 400 340 ug/L 04/21/1815:05 2 Sulfate 9800 400 190 ug/L 04/21/1815:05 2 Alkalinity 200000 5000 3700 ug/L 04/20/1814:49 1 Total Dissolved Solids 250000 10000 4300 ug/L 04/13/18 05:55 1 Client Sample ID: MW41) Lab Sample ID: 500-143709-4 Date Collected: 04/09/18 12:35 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 20:21 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 20:21 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 20:21 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 20:21 1 1,1-Dichloroethane 1.9 1.0 0.41 ug/L 04/18/18 20:21 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 20:21 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 20:21 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 20:21 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 20:21 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 20:21 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 20:21 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 20:21 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 20:21 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 20:21 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 20:21 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 20:21 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 20:21 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 20:21 1 Benzene <0.15 0.50 0.15 ug/L 04/18/18 20:21 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 20:21 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 20:21 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 20:21 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 20:21 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 20:21 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 20:21 1 TestAmerica Chicago Page 9 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW41) Lab Sample ID: 500-143709-4 Date Collected: 04/09/18 12:35 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 20:21 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 20:21 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 20:21 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 20:21 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 20:21 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 20:21 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 20:21 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 20:21 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 20:21 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 20:21 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 20:21 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 20:21 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 20:21 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 20:21 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 20:21 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 20:21 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 20:21 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 20:21 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 20:21 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 20:21 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 20:21 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 20:21 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 20:21 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 98 75- 126 04118118 20:21 1 4-Bromofluorobenzene (Surr) 91 72 - 124 04118118 20:21 1 Dibromofluoromethane 94 75 - 120 04118118 20:21 1 Toluene-d8 (Surr) 92 75 - 120 04118118 20:21 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:05 1 Arsenic 3.5 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:05 1 Barium 180 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:05 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:05 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:05 1 Chromium <1.1 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:05 1 Cobalt <0.40 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:05 1 Copper 5.9 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:05 1 Iron 2200 100 47 ug/L 04/12/1815:45 04/13/1812:05 1 Lead 1.0 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:05 1 Manganese 460 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:05 1 Nickel 0.68 J 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:05 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:05 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:05 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:05 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:05 1 Zinc 12 10 6.9 ug/L 04/12/1815:45 04/13/1812:05 1 0 TestAmerica Chicago Page 10 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW41) Lab Sample ID: 500-143709-4 Date Collected: 04/09/18 12:35 Matrix: Water Date Received: 04/12/18 09:10 , Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1810:56 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 14000 400 340 ug/L 04/21/1815:16 2 Sulfate 14000 400 190 ug/L 04/21/1815:18 2 Alkalinity 330000 5000 3700 ug/L 04/20/1814:57 1 Total Dissolved Solids 360000 10000 4300 ug/L 04/13/18 05:58 1 Client Sample ID: MW41)1 Lab Sample ID: 500-143709-5 Date Collected: 04/09/18 11:40 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 20:47 1 1,1, 1 -Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 20:47 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 20:47 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 20:47 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/18 20:47 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 20:47 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 20:47 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 20:47 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 20:47 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 20:47 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 20:47 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 20:47 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 20:47 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 20:47 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 20:47 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 20:47 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 20:47 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 20:47 1 Benzene <0.15 0.50 0.15 ug/L 04/18/18 20:47 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 20:47 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 20:47 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 20:47 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 20:47 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 20:47 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 20:47 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 20:47 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 20:47 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 20:47 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 20:47 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 20:47 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 20:47 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 20:47 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 20:47 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 20:47 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 20:47 1 TestAmerica Chicago Page 11 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW4D1 Lab Sample ID: 500-143709-5 Date Collected: 04/09/18 11:40 Matrix: Water Date Received: 04/12/18 09:10 , Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 20:47 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 20:47 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 20:47 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 20:47 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 20:47 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 20:47 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 20:47 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 20:47 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 20:47 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 20:47 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 20:47 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 20:47 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 20:47 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 99 75- 126 04118118 20:47 1 4-Bromofluorobenzene (Surr) 92 72 - 124 04118118 20:47 1 Dibromofluoromethane 97 75 - 120 04118118 20:47 1 Toluene-d8 (Surr) 93 75 - 120 04118118 20:47 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:16 1 Arsenic 3.4 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:16 1 Barium 74 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:16 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:16 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:16 1 Chromium 7.6 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:16 1 Cobalt <0.40 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:16 1 Copper 0.81 J 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:16 1 Iron 1000 100 47 ug/L 04/12/1815:45 04/13/1812:16 1 Lead 0.22 J 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:16 1 Manganese 270 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:16 1 Nickel 3.5 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:16 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:16 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:16 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:16 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:16 1 Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1812:16 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1810:57 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 13000 1000 850 ug/L 04/24/18 20:41 5 Sulfate 1500 200 95 ug/L 04/24/18 20:28 1 Alkalinity 210000 5000 3700 ug/L 04/20/1815:17 1 Total Dissolved Solids 260000 10000 4300 ug/L 04/13/18 06:53 1 TestAmerica Chicago Page 12 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW5 Lab Sample ID: 500-143709-6 Date Collected: 04/09/18 14:40 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 21:13 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 21:13 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 21:13 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 21:13 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/18 21:13 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 21:13 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 21:13 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 21:13 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 21:13 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 21:13 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 21:13 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 21:13 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 21:13 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 21:13 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 21:13 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 21:13 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 21:13 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 21:13 1 Benzene 0.67 0.50 0.15 ug/L 04/18/18 21:13 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 21:13 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 21:13 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 21:13 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 21:13 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 21:13 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 21:13 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 21:13 1 Chloroethane 1.0 1.0 0.51 ug/L 04/18/18 21:13 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 21:13 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 21:13 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 21:13 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 21:13 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 21:13 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 21:13 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 21:13 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 21:13 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 21:13 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 21:13 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 21:13 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 21:13 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 21:13 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 21:13 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 21:13 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 21:13 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 21:13 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 21:13 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 21:13 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 21:13 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 21:13 1 0 TestAmerica Chicago Page 13 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW5 Lab Sample ID: 500-143709-6 Date Collected: 04/09/18 14:40 Matrix: Water Date Received: 04/12/18 09:10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 100 75- 126 04118118 21713 1 4-Bromofluorobenzene (Surr) 89 72 - 124 04118118 21:13 1 Dibromofluoromethane 95 75 - 120 04118118 21:13 1 Toluene-d8 (Surr) 91 75 - 120 04118118 21:13 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:20 1 Arsenic 0.32 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:20 1 Barium 240 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:20 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:20 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:20 1 Chromium <1.1 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:20 1 Cobalt 1.6 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:20 1 Copper 1.2 J 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:20 1 Iron 240 100 47 ug/L 04/12/1815:45 04/13/1812:20 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:20 1 Manganese 410 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:20 1 Nickel 2.4 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:20 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:20 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:20 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:20 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:20 1 Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1812:20 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1810:59 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 49000 4000 3400 ug/L 04/24/18 20:53 20 Sulfate 99000 4000 1900 ug/L 04/24/18 20:53 20 Alkalinity 480000 5000 3700 ug/L 04/20/1815:26 1 Total Dissolved Solids 720000 10000 4300 ug/L 04/13/18 07:00 1 Client Sample ID: MWSD Lab Sample ID: 500-143709-7 Date Collected: 04/09/18 15:10 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/1821:39 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/1821:39 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/1821:39 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/1821:39 1 1,1-Dichloroethane 1.9 1.0 0.41 ug/L 04/18/18 21:39 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/1821:39 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/1821:39 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/1821:39 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/1821:39 1 TestAmerica Chicago Page 14 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MWSD Lab Sample ID: 500-143709-7 Date Collected: 04/09/18 15:10 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 21:39 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 21:39 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 21:39 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 21:39 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 21:39 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 21:39 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 21:39 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 21:39 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 21:39 1 Benzene 0.99 0.50 0.15 ug/L 04/18/18 21:39 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 21:39 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 21:39 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 21:39 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 21:39 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 21:39 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 21:39 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 21:39 1 Chloroethane 1.2 1.0 0.51 ug/L 04/18/18 21:39 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 21:39 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 21:39 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 21:39 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 21:39 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 21:39 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 21:39 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 21:39 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 21:39 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 21:39 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 21:39 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 21:39 1 Tetrahydrofuran 24 10 1.9 ug/L 04/18/18 21:39 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 21:39 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 21:39 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 21:39 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 21:39 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 21:39 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 21:39 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 21:39 1 Vinyl chloride 1.7 1.0 0.20 ug/L 04/18/18 21:39 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 21:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 102 75- 126 04118118 21:39 1 4-Bromofluorobenzene (Surr) 87 72 - 124 04118118 21:39 1 Dibromofluoromethane 93 75 - 120 04118118 21:39 1 Toluene-d8 (Surr) 96 75 - 120 04118118 21:39 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:24 1 Arsenic 0.67 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:24 1 0 TestAmerica Chicago Page 15 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MWSD Lab Sample ID: 500-143709-7 Date Collected: 04/09/18 15:10 Matrix: Water Date Received: 04/12/18 09:10 Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Barium 210 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:24 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:24 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:24 1 Chromium 2.9 J 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:24 1 Cobalt 0.76 J 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:24 1 Copper 1.3 J 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:24 1 Iron 230 100 47 ug/L 04/12/1815:45 04/13/1812:24 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:24 1 Manganese 780 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:24 1 Nickel 9.7 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:24 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:24 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:24 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:24 1 Vanadium 6.0 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:24 1 Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1812:24 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier Mercury <0.098 (General Chemistry Analyte Chloride Sulfate Alkalinity Total Dissolved Solids Client Sample ID: MW6 Date Collected: 04/09/18 15:50 Date Received: 04/12/18 09:10 RL MDL Unit D Prepared Analyzed Dil Fac 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:00 1 Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 100000 5000 4300 ug/L 04/24/18 21:31 25 170000 5000 2400 ug/L 04/24/18 21:31 25 830000 5000 3700 ug/L 04/20/1815:37 1 1300000 10000 4300 ug/L 04/13/18 07:06 1 Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: 500-143709-8 Matrix: Water Analyte Result Qualifier RL MDL Unit D 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 2-Hexanone <1.6 5.0 1.6 ug/L 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L Acetone 2.7 J cn 5.0 1.7 ug/L Prepared Analyzed Dil Fac 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 04/18/18 22:05 1 0 Page 16 of 64 TestAmerica Chicago 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW6 Lab Sample ID: 500-143709-8 Date Collected: 04/09/18 15:50 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 22:05 1 Benzene 0.35 J 0.50 0.15 ug/L 04/18/18 22:05 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 22:05 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 22:05 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 22:05 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 22:05 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 22:05 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 22:05 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 22:05 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 22:05 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 22:05 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 22:05 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 22:05 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 22:05 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 22:05 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 22:05 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 22:05 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 22:05 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 22:05 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 22:05 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 22:05 1 Tetrahydrofuran 25 10 1.9 ug/L 04/18/18 22:05 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 22:05 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 22:05 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 22:05 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 22:05 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 22:05 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 22:05 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 22:05 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 22:05 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 22:05 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 101 75- 126 04118118 22:05 1 4-Bromofluorobenzene (Surr) 89 72 - 124 04118118 22:05 1 Dibromofluoromethane 95 75 - 120 04118118 22:05 1 Toluene-d8 (Surr) 91 75 - 120 04118118 22:05 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:28 1 Arsenic 14 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:28 1 Barium 1600 13 3.7 ug/L 04/12/1815:45 04/13/1814:02 5 Beryllium 6.1 5.0 2.7 ug/L 04/12/1815:45 04/13/1814:02 5 Cadmium 3.1 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:28 1 Chromium 58 25 5.7 ug/L 04/12/1815:45 04/13/1814:02 5 Cobalt 32 5.0 2.0 ug/L 04/12/1815:45 04/13/1814:02 5 Copper 450 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:28 1 Iron 76000 500 230 ug/L 04/12/1815:45 04/13/1814:02 5 Lead 94 2.5 0.93 ug/L 04/12/1815:45 04/13/1814:02 5 0 TestAmerica Chicago Page 17 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW6 Lab Sample ID: 500-143709-8 Date Collected: 04/09/18 15:50 Matrix: Water Date Received: 04/12/18 09:10 , Method: 6020B - Metals ICP/MS - ( ) Total Recoverable Continued (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Manganese 5000 13 4.0 ug/L 04/12/1815:45 04/13/1814:02 5 Nickel 42 10 3.1 ug/L 04/12/1815:45 04/13/1814:02 5 Selenium 9.4 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:28 1 Silver 0.49 J 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:28 1 Thallium <2.9 10 2.9 ug/L 04/12/1815:45 04/13/1814:02 5 Vanadium 160 25 11 ug/L 04/12/1815:45 04/13/1814:02 5 Zinc 400 10 6.9 ug/L 04/12/1815:45 04/13/1812:28 1 Method: 7470A - Mercury (CVAA) C Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury 0.81 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:02 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 39000 2000 1700 ug/L 04/24/18 21:56 10 Sulfate 36000 2000 950 ug/L 04/24/18 21:56 10 Alkalinity 750000 5000 3700 ug/L 04/20/1815:48 1 Total Dissolved Solids 870000 10000 4300 ug/L 04/13/18 07:08 1 Client Sample ID: MW61) Lab Sample ID: 500-143709-9 Date Collected: 04/09/18 14:40 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 22:31 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 22:31 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 22:31 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 22:31 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/18 22:31 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 22:31 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 22:31 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 22:31 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 22:31 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 22:31 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 22:31 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 22:31 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 22:31 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 22:31 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 22:31 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 22:31 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 22:31 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 22:31 1 Benzene 0.51 0.50 0.15 ug/L 04/18/18 22:31 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 22:31 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 22:31 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 22:31 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 22:31 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 22:31 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 22:31 1 TestAmerica Chicago Page 18 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW61) Lab Sample ID: 500-143709-9 Date Collected: 04/09/18 14:40 Matrix: Water Date Received: 04/12/18 09:10 , Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 22:31 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 22:31 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 22:31 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 22:31 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 22:31 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 22:31 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 22:31 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 22:31 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 22:31 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 22:31 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 22:31 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 22:31 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 22:31 1 Tetrahydrofuran 44 10 1.9 ug/L 04/18/18 22:31 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 22:31 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 22:31 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 22:31 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 22:31 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 22:31 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 22:31 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 22:31 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 22:31 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 22:31 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 98 75- 126 04118118 22:31 1 4-Bromofluorobenzene (Surr) 93 72 - 124 04118118 22:31 1 Dibromofluoromethane 95 75 - 120 04118118 22:31 1 Toluene-d8 (Surr) 92 75 - 120 04118118 22:31 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:31 1 Arsenic 0.63 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:31 1 Barium 260 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:31 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:31 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:31 1 Chromium 6.8 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:31 1 Cobalt 3.9 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:31 1 Copper 11 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:31 1 Iron 780 100 47 ug/L 04/12/1815:45 04/13/1812:31 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:31 1 Manganese 7200 25 7.9 ug/L 04/12/1815:45 04/13/1814:10 10 Nickel 19 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:31 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:31 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:31 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:31 1 Vanadium 3.7 J 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:31 1 Zinc 19 10 6.9 ug/L 04/12/1815:45 04/13/1812:31 1 TestAmerica Chicago Page 19 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW61) Lab Sample ID: 500-143709-9 Date Collected: 04/09/18 14:40 Matrix: Water Date Received: 04/12/18 09:10 , Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:04 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 29000 F1 2000 1700 ug/L 04/24/18 22:09 10 Sulfate 28000 2000 950 ug/L 04/24/18 22:09 10 Alkalinity 750000 5000 3700 ug/L 04/20/1815:58 1 Total Dissolved Solids 890000 10000 4300 ug/L 04/13/18 07:11 1 Client Sample ID: MW61)1 Lab Sample ID: 500-143709-10 Date Collected: 04/09/18 15:15 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 22:57 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 22:57 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 22:57 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 22:57 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/18 22:57 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 22:57 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 22:57 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 22:57 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 22:57 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 22:57 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 22:57 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 22:57 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 22:57 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 22:57 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 22:57 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 22:57 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 22:57 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 22:57 1 Benzene 0.41 J 0.50 0.15 ug/L 04/18/18 22:57 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 22:57 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 22:57 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 22:57 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 22:57 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 22:57 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 22:57 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 22:57 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 22:57 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 22:57 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 22:57 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 22:57 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 22:57 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 22:57 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 22:57 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 22:57 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 22:57 1 TestAmerica Chicago Page 20 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW6D1 Lab Sample ID: 500-143709-10 Date Collected: 04/09/18 15:15 Matrix: Water Date Received: 04/12/18 09:10 , Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 22:57 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 22:57 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 22:57 1 Tetrahydrofuran 9.9 J 10 1.9 ug/L 04/18/18 22:57 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 22:57 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 22:57 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 22:57 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 22:57 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 22:57 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 22:57 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 22:57 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 22:57 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 22:57 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 98 75- 126 04118118 22:57 1 4-Bromofluorobenzene (Surr) 90 72 - 124 04118118 22:57 1 Dibromofluoromethane 95 75 - 120 04118118 22:57 1 Toluene-d8 (Surr) 93 75 - 120 04118118 22:57 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:35 1 Arsenic 4.8 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:35 1 Barium 410 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:35 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:35 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:35 1 Chromium 3.3 J 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:35 1 Cobalt 0.65 J 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:35 1 Copper 1.4 J 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:35 1 Iron 6500 100 47 ug/L 04/12/1815:45 04/13/1812:35 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:35 1 Manganese 410 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:35 1 Nickel 2.0 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:35 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:35 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:35 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:35 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:35 1 Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1812:35 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:05 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 27000 1000 850 ug/L 04/24/18 22:47 5 Sulfate 13000 1000 480 ug/L 04/24/18 22:47 5 Alkalinity 680000 5000 3700 ug/L 04/20/1816:12 1 Total Dissolved Solids 730000 10000 4300 ug/L 04/13/18 07:13 1 TestAmerica Chicago Page 21 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW7 Lab Sample ID: 500-143709-11 Date Collected: 04/10/18 10:25 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 23:23 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 23:23 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 23:23 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 23:23 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/18 23:23 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 23:23 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 23:23 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 23:23 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 23:23 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 23:23 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 23:23 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 23:23 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 23:23 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 23:23 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 23:23 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 23:23 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 23:23 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 23:23 1 Benzene <0.15 0.50 0.15 ug/L 04/18/18 23:23 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 23:23 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 23:23 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 23:23 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 23:23 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 23:23 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 23:23 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 23:23 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 23:23 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 23:23 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 23:23 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 23:23 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 23:23 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 23:23 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 23:23 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 23:23 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 23:23 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 23:23 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 23:23 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 23:23 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 23:23 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 23:23 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 23:23 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 23:23 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 23:23 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 23:23 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 23:23 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 23:23 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 23:23 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 23:23 1 0 TestAmerica Chicago Page 22 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW7 Lab Sample ID: 500-143709-11 Date Collected: 04/10/18 10:25 Matrix: Water Date Received: 04/12/18 09:10 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 96 75- 126 04118118 23723 1 4-Bromofluorobenzene (Surr) 91 72 - 124 04118118 23:23 1 Dibromofluoromethane 96 75 - 120 04118118 23:23 1 Toluene-d8 (Surr) 95 75 - 120 04118118 23:23 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:39 1 Arsenic 0.83 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:39 1 Barium 410 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:39 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:39 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:39 1 Chromium 35 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:39 1 Cobalt 4.2 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:39 1 Copper 44 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:39 1 Iron 7300 100 47 ug/L 04/12/1815:45 04/13/1812:39 1 Lead 4.7 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:39 1 Manganese 290 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:39 1 Nickel 17 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:39 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:39 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:39 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:39 1 Vanadium 19 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:39 1 Zinc 30 10 6.9 ug/L 04/12/1815:45 04/13/1812:39 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury 0.53 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:07 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 57000 2000 1700 ug/L 04/24/18 23:12 10 Sulfate 26000 2000 950 ug/L 04/24/18 23:12 10 Alkalinity 490000 5000 3700 ug/L 04/20/1816:21 1 Total Dissolved Solids 620000 10000 4300 ug/L 04/13/18 07:16 1 Client Sample ID: MW7A Lab Sample ID: 500-143709-12 Date Collected: 04/10/18 09:55 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/1823:49 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/1823:49 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/1823:49 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/1823:49 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/1823:49 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/1823:49 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/1823:49 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/1823:49 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/1823:49 1 TestAmerica Chicago Page 23 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW7A Lab Sample ID: 500-143709-12 Date Collected: 04/10/18 09:55 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 23:49 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 23:49 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 23:49 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 23:49 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 23:49 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 23:49 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 23:49 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 23:49 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 23:49 1 Benzene <0.15 0.50 0.15 ug/L 04/18/18 23:49 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 23:49 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 23:49 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 23:49 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 23:49 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 23:49 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 23:49 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 23:49 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 23:49 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 23:49 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 23:49 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 23:49 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 23:49 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 23:49 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 23:49 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 23:49 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 23:49 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 23:49 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 23:49 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 23:49 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 23:49 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 23:49 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 23:49 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 23:49 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 23:49 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 23:49 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 23:49 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 23:49 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 23:49 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 23:49 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 99 75- 126 04118118 23:49 1 4-Bromofluorobenzene (Surr) 88 72 - 124 04118118 23:49 1 Dibromofluoromethane 96 75 - 120 04118118 23:49 1 Toluene-d8 (Surr) 91 75 - 120 04118118 23:49 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:43 1 Arsenic 0.69 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:43 1 0 TestAmerica Chicago Page 24 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW7A Lab Sample ID: 500-143709-12 Date Collected: 04/10/18 09:55 Matrix: Water Date Received: 04/12/18 09:10 Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Barium 320 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:43 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:43 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:43 1 Chromium 15 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:43 1 Cobalt 2.1 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:43 1 Copper 9.4 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:43 1 Iron 3200 100 47 ug/L 04/12/1815:45 04/13/1812:43 1 Lead 0.58 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:43 1 Manganese 92 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:43 1 Nickel 8.6 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:43 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:43 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:43 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:43 1 Vanadium 11 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:43 1 Zinc 13 10 6.9 ug/L 04/12/1815:45 04/13/1812:43 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury 0.35 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:09 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 46000 2000 1700 ug/L 04/25/1815:20 10 Sulfate 22000 2000 950 ug/L 04/24/1819:55 10 Alkalinity 290000 5000 3700 ug/L 04/20/1816:29 1 Total Dissolved Solids 400000 10000 4300 ug/L 04/13/18 07:19 1 Client Sample ID: MW713 Date Collected: 04/10/18 09:30 Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: 500-143709-13 Matrix: Water Analyte Result Qualifier RL MDL Unit D 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 2-Hexanone <1.6 5.0 1.6 ug/L 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L Acetone <1.7 5.0 1.7 ug/L Prepared Analyzed Dil Fac 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 04/19/18 23:57 1 0 TestAmerica Chicago Page 25 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW71) Lab Sample ID: 500-143709-13 Date Collected: 04/10/18 09:30 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acrylonitrile <4.5 20 4.5 ug/L 04/19/18 23:57 1 Benzene <0.15 0.50 0.15 ug/L 04/19/18 23:57 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/19/18 23:57 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/19/18 23:57 1 Bromoform <0.48 1.0 0.48 ug/L 04/19/18 23:57 1 Bromomethane <0.80 2.0 0.80 ug/L 04/19/18 23:57 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/19/18 23:57 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/19/18 23:57 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/19/18 23:57 1 Chloroethane <0.51 1.0 0.51 ug/L 04/19/18 23:57 1 Chloroform <0.37 2.0 0.37 ug/L 04/19/18 23:57 1 Chloromethane <0.32 1.0 0.32 ug/L 04/19/18 23:57 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/19/18 23:57 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/19/18 23:57 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/19/18 23:57 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/19/18 23:57 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/19/18 23:57 1 lodomethane <0.66 2.5 0.66 ug/L 04/19/18 23:57 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/19/18 23:57 1 Styrene <0.39 1.0 0.39 ug/L 04/19/18 23:57 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/19/18 23:57 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/19/18 23:57 1 Toluene <0.15 0.50 0.15 ug/L 04/19/18 23:57 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/19/18 23:57 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/19/18 23:57 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/19/18 23:57 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/19/18 23:57 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/19/18 23:57 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/19/18 23:57 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/19/18 23:57 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/19/18 23:57 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 105 75- 126 04119118 23:57 1 4-Bromofluorobenzene (Surr) 92 72 - 124 04119118 23:57 1 Dibromofluoromethane 95 75 - 120 04119118 23:57 1 Toluene-d8 (Surr) 94 75 - 120 04119118 23:57 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:47 1 Arsenic 0.29 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:47 1 Barium 230 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:47 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:47 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:47 1 Chromium <1.1 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:47 1 Cobalt <0.40 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:47 1 Copper <0.50 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:47 1 Iron 650 100 47 ug/L 04/12/1815:45 04/13/1812:47 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:47 1 0 TestAmerica Chicago Page 26 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW7D Lab Sample ID: 500-143709-13 Date Collected: 04/10/18 09:30 Matrix: Water Date Received: 04/12/18 09:10 , Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Manganese 46 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:47 1 Nickel <0.63 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:47 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:47 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:47 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:47 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:47 1 E: Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1812:47 1 �Method: 7470A - Mercury (CVAA) F Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:10 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 48000 4000 3400 ug/L 04/25/1815:32 20 Sulfate 28000 1000 480 ug/L 04/24/18 20:07 5 Alkalinity 350000 5000 3700 ug/L 04/20/1816:36 1 Total Dissolved Solids 460000 10000 4300 ug/L 04/13/18 07:21 1 Client Sample ID: MW8 Date Collected: 04/10/18 11:20 Date Received: 04/12/18 09:10 Lab Sample ID: 500-143709-14 Matrix: Water Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/18 12:52 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/18 12:52 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/18 12:52 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/18 12:52 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/18 12:52 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/18 12:52 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/18 12:52 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/18 12:52 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/18 12:52 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/18 12:52 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/18 12:52 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/18 12:52 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/18 12:52 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 12:52 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/18 12:52 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 12:52 1 Acetone 4.4 J cn 5.0 1.7 ug/L 04/20/18 12:52 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 12:52 1 Benzene <0.15 0.50 0.15 ug/L 04/20/18 12:52 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 12:52 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 12:52 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 12:52 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 12:52 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 12:52 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 12:52 1 TestAmerica Chicago Page 27 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW8 Lab Sample ID: 500-143709-14 Date Collected: 04/10/18 11:20 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/1812:52 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 12:52 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 12:52 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 12:52 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 12:52 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 12:52 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 12:52 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 12:52 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 12:52 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 12:52 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 12:52 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 12:52 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 12:52 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/20/18 12:52 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 12:52 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 12:52 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 12:52 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 12:52 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 12:52 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 12:52 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 12:52 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 12:52 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 12:52 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 106 75- 126 04/20/18 12:52 1 4-Bromofluorobenzene (Surr) 94 72 - 124 04120118 12:52 1 Dibromofluoromethane 97 75 - 120 04120118 12:52 1 Toluene-d8 (Surr) 95 75 - 120 04120118 12:52 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 12000 1000 850 ug/L 04/26/18 09:52 5 Sulfate 43000 2000 950 ug/L 04/24/18 20:44 10 Alkalinity 300000 5000 3700 ug/L 04/20/1816:45 1 Total Dissolved Solids 370000 10000 4300 ug/L 04/13/18 07:24 1 Client Sample ID: MWBD Lab Sample ID: 500-143709-15 Date Collected: 04/10/18 13:25 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/1813:20 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/1813:20 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/1813:20 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/1813:20 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/1813:20 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/1813:20 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/1813:20 1 0 TestAmerica Chicago Page 28 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MWBD Lab Sample ID: 500-143709-15 Date Collected: 04/10/18 13:25 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/18 13:20 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/18 13:20 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/18 13:20 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/18 13:20 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/18 13:20 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/18 13:20 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 13:20 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/18 13:20 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 13:20 1 Acetone <1.7 5.0 1.7 ug/L 04/20/18 13:20 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 13:20 1 Benzene <0.15 0.50 0.15 ug/L 04/20/18 13:20 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 13:20 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 13:20 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 13:20 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 13:20 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 13:20 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 13:20 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 13:20 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 13:20 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 13:20 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 13:20 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 13:20 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 13:20 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 13:20 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 13:20 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 13:20 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 13:20 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 13:20 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 13:20 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 13:20 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/20/18 13:20 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 13:20 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 13:20 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 13:20 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 13:20 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 13:20 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 13:20 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 13:20 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 13:20 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 13:20 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 113 75- 126 04120118 13:20 1 4-Bromofluorobenzene (Surr) 95 72 - 124 04120118 13:20 1 Dibromofluoromethane 97 75- 120 04120118 13:20 1 Toluene-d8 (Surr) 94 75 - 120 04120118 13:20 1 0 TestAmerica Chicago Page 29 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MWBD Lab Sample ID: 500-143709-15 Date Collected: 04/10/18 13:25 Matrix: Water Date Received: 04/12/18 09:10 , Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1812:50 1 Arsenic 0.34 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1812:50 1 Barium 81 2.5 0.73 ug/L 04/12/1815:45 04/13/1812:50 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1812:50 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1812:50 1 Chromium 18 5.0 1.1 ug/L 04/12/1815:45 04/13/1812:50 1 Cobalt 1.2 1.0 0.40 ug/L 04/12/1815:45 04/13/1812:50 1 Copper 2.9 2.0 0.50 ug/L 04/12/1815:45 04/13/1812:50 1 Iron 2400 100 47 ug/L 04/12/1815:45 04/13/1812:50 1 Lead 0.23 J 0.50 0.19 ug/L 04/12/1815:45 04/13/1812:50 1 Manganese 180 2.5 0.79 ug/L 04/12/1815:45 04/13/1812:50 1 Nickel 9.2 2.0 0.63 ug/L 04/12/1815:45 04/13/1812:50 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1812:50 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1812:50 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1812:50 1 Vanadium 6.3 5.0 2.2 ug/L 04/12/1815:45 04/13/1812:50 1 Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1812:50 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:16 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 82000 5000 4300 ug/L 04/25/1815:45 25 Sulfate 15000 400 190 ug/L 04/24/18 20:57 2 Alkalinity 410000 5000 3700 ug/L 04/20/1816:53 1 Total Dissolved Solids 600000 10000 4300 ug/L 04/13/18 07:26 1 Client Sample ID: MW9 Lab Sample ID: 500-143709-16 Date Collected: 04/10/18 09:15 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/1813:48 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/1813:48 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/1813:48 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/1813:48 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/1813:48 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/1813:48 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/1813:48 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/1813:48 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/1813:48 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/1813:48 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/1813:48 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/1813:48 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/1813:48 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 13:48 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/1813:48 1 TestAmerica Chicago Page 30 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW9 Lab Sample ID: 500-143709-16 Date Collected: 04/10/18 09:15 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 13:48 1 Acetone <1.7 5.0 1.7 ug/L 04/20/18 13:48 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 13:48 1 Benzene <0.15 0.50 0.15 ug/L 04/20/18 13:48 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 13:48 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 13:48 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 13:48 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 13:48 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 13:48 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 13:48 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 13:48 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 13:48 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 13:48 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 13:48 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 13:48 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 13:48 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 13:48 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 13:48 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 13:48 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 13:48 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 13:48 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 13:48 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 13:48 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/20/18 13:48 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 13:48 1 trans- l,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 13:48 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 13:48 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 13:48 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 13:48 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 13:48 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 13:48 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 13:48 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 13:48 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 117 75- 126 04120118 13:48 1 4-Bromofluorobenzene (Surr) 94 72 - 124 04120118 13:48 1 Dibromofluoromethane 102 75 - 120 04120118 13:48 1 Toluene-d8 (Surr) 90 75 - 120 04120118 13:48 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1813:02 1 Arsenic <0.23 1.0 0.23 ug/L 04/12/1815:45 04/13/1813:02 1 Barium 48 2.5 0.73 ug/L 04/12/1815:45 04/13/1813:02 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1813:02 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1813:02 1 Chromium <1.1 5.0 1.1 ug/L 04/12/1815:45 04/13/1813:02 1 Cobalt <0.40 1.0 0.40 ug/L 04/12/1815:45 04/13/1813:02 1 Copper 0.50 J 2.0 0.50 ug/L 04/12/1815:45 04/13/1813:02 1 0 TestAmerica Chicago Page 31 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW9 Lab Sample ID: 500-143709-16 Date Collected: 04/10/18 09:15 Matrix: Water Date Received: 04/12/18 09:10 , Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Iron 75 J 100 47 ug/L 04/12/1815:45 04/13/1813:02 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1813:02 1 Manganese 3.0 2.5 0.79 ug/L 04/12/1815:45 04/13/1813:02 1 Nickel 0.73 J 2.0 0.63 ug/L 04/12/1815:45 04/13/1813:02 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1813:02 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1813:02 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1813:02 1 Vanadium 3.4 J 5.0 2.2 ug/L 04/12/1815:45 04/13/1813:02 1 Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1813:02 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:18 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 22000 1000 850 ug/L 04/25/1815:57 5 Sulfate 16000 400 190 ug/L 04/24/18 21:21 2 Alkalinity 47000 5000 3700 ug/L 04/23/1814:46 1 Total Dissolved Solids 150000 10000 4300 ug/L 04/13/18 07:29 1 Client Sample ID: MW10 Lab Sample ID: 500-143709-17 Date Collected: 04/10/18 09:50 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/18 14:16 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/18 14:16 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/18 14:16 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/18 14:16 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/18 14:16 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/18 14:16 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/18 14:16 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/18 14:16 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/18 14:16 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/18 14:16 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/18 14:16 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/18 14:16 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/18 14:16 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 14:16 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/18 14:16 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 14:16 1 Acetone <1.7 5.0 1.7 ug/L 04/20/18 14:16 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 14:16 1 Benzene 0.42 J 0.50 0.15 ug/L 04/20/18 14:16 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 14:16 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 14:16 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 14:16 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 14:16 1 TestAmerica Chicago Page 32 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW10 Lab Sample ID: 500-143709-17 Date Collected: 04/10/18 09:50 Matrix: Water Date Received: 04/12/18 09:10 , Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 14:16 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 14:16 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 14:16 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 14:16 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 14:16 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 14:16 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 14:16 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 14:16 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 14:16 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 14:16 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 14:16 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 14:16 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 14:16 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 14:16 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 14:16 1 Tetrahydrofuran 9.0 J 10 1.9 ug/L 04/20/18 14:16 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 14:16 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 14:16 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 14:16 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 14:16 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 14:16 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 14:16 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 14:16 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 14:16 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 14:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 115 75- 126 04120118 14:16 1 4-Bromofluorobenzene (Surr) 91 72 - 124 04120118 14:16 1 Dibromofluoromethane 100 75 - 120 04120118 14:16 1 Toluene-d8 (Surr) 92 75 - 120 04120118 14:16 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1813:05 1 Arsenic 1.2 1.0 0.23 ug/L 04/12/1815:45 04/13/1813:05 1 Barium 340 2.5 0.73 ug/L 04/12/1815:45 04/13/1813:05 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1813:05 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1813:05 1 Chromium <1.1 5.0 1.1 ug/L 04/12/1815:45 04/13/1813:05 1 Cobalt 5.1 1.0 0.40 ug/L 04/12/1815:45 04/13/1813:05 1 Copper <0.50 2.0 0.50 ug/L 04/12/1815:45 04/13/1813:05 1 Iron 66000 100 47 ug/L 04/12/1815:45 04/13/1813:05 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1813:05 1 Manganese 4600 2.5 0.79 ug/L 04/12/1815:45 04/13/1813:05 1 Nickel 1.3 J 2.0 0.63 ug/L 04/12/1815:45 04/13/1813:05 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1813:05 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1813:05 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1813:05 1 Vanadium <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1813:05 1 TestAmerica Chicago Page 33 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW10 Lab Sample ID: 500-143709-17 Date Collected: 04/10/18 09:50 Matrix: Water Date Received: 04/12/18 09:10 , Method: 6020B - Metals ICP/MS - Total Recoverable Continued ( ) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Zinc <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1813:05 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:19 1 General Chemistry C Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 47000 4000 3400 ug/L 04/25/1816:09 20 Sulfate 340 200 95 ug/L 04/24/18 22:11 1 Alkalinity 630000 5000 3700 ug/L 04/23/1814:11 1 Total Dissolved Solids 830000 10000 4300 ug/L 04/13/18 07:31 1 Client Sample ID: MW10D Date Collected: 04/10/18 14:25 Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: 500-143709-18 Matrix: Water Analyte Result Qualifier RL MDL Unit D 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 1,4-Dichlorobenzene 2.0 1.0 0.36 ug/L 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 2-Hexanone <1.6 5.0 1.6 ug/L 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L Acetone 7.2 cn 5.0 1.7 ug/L Acrylonitrile <4.5 20 4.5 ug/L Benzene 3.3 0.50 0.15 ug/L Bromochloromethane <0.43 1.0 0.43 ug/L Bromodichloromethane <0.37 1.0 0.37 ug/L Bromoform <0.48 1.0 0.48 ug/L Bromomethane <0.80 2.0 0.80 ug/L Carbon disulfide 0.50 J 2.0 0.45 ug/L Carbon tetrachloride <0.38 1.0 0.38 ug/L Chlorobenzene <0.39 1.0 0.39 ug/L Chloroethane <0.51 1.0 0.51 ug/L Chloroform <0.37 2.0 0.37 ug/L Chloromethane <0.32 1.0 0.32 ug/L cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L Prepared Analyzed Dil Fac 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 04/17/18 16:39 1 TestAmerica Chicago Page 34 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW10D Lab Sample ID: 500-143709-18 Date Collected: 04/10/18 14:25 Matrix: Water Date Received: 04/12/18 09:10 , Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Dibromochloromethane <0.49 1.0 0.49 ug/L 04/17/18 16:39 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/17/18 16:39 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/17/18 16:39 1 lodomethane <0.66 2.5 0.66 ug/L 04/17/18 16:39 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/17/18 16:39 1 Styrene <0.39 1.0 0.39 ug/L 04/17/18 16:39 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/17/18 16:39 1 Tetrahydrofuran 97 10 1.9 ug/L 04/17/18 16:39 1 Toluene <0.15 0.50 0.15 ug/L 04/17/18 16:39 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/17/18 16:39 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/17/18 16:39 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/17/18 16:39 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/17/18 16:39 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/17/18 16:39 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/17/18 16:39 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/17/18 16:39 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/17/18 16:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 101 75- 126 04117118 16:39 1 4-Bromofluorobenzene (Surr) 106 72 - 124 04117118 16:39 1 Dibromofluoromethane 95 75 - 120 04117118 16:39 1 Toluene-d8 (Surr) 94 75 - 120 04117118 16:39 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1813:09 1 Arsenic 2.3 1.0 0.23 ug/L 04/12/1815:45 04/13/1813:09 1 Barium 220 2.5 0.73 ug/L 04/12/1815:45 04/13/1813:09 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1813:09 1 Cadmium 1.6 0.50 0.17 ug/L 04/12/1815:45 04/13/1813:09 1 Chromium 8.2 5.0 1.1 ug/L 04/12/1815:45 04/13/1813:09 1 Cobalt 43 1.0 0.40 ug/L 04/12/1815:45 04/13/1813:09 1 Copper 460 2.0 0.50 ug/L 04/12/1815:45 04/13/1813:09 1 Iron 2100 100 47 ug/L 04/12/1815:45 04/13/1813:09 1 Lead 1.1 0.50 0.19 ug/L 04/12/1815:45 04/13/1813:09 1 Manganese 17000 25 7.9 ug/L 04/12/1815:45 04/13/1814:14 10 Nickel 49 2.0 0.63 ug/L 04/12/1815:45 04/13/1813:09 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1813:09 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1813:09 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1813:09 1 Vanadium 8.7 5.0 2.2 ug/L 04/12/1815:45 04/13/1813:09 1 Zinc 11 10 6.9 ug/L 04/12/1815:45 04/13/1813:09 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:21 1 TestAmerica Chicago Page 35 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW10D Lab Sample ID: 500-143709-18 Date Collected: 04/10/18 14:25 Matrix: Water Date Received: 04/12/18 09:10 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 200000 10000 8500 ug/L 04/25/1816:22 50 Sulfate 130000 10000 4800 ug/L 04/24/18 22:35 50 Alkalinity 1700000 5000 3700 ug/L 04/23/1814:37 1 Total Dissolved Solids 2400000 10000 4300 ug/L 04/13/18 07:34 1 Client Sample ID: MW11 Date Collected: 04/10/18 15:10 Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) 0 Lab Sample ID: 500-143709-19 Matrix: Water F Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/1814:44 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/18 14:44 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/18 14:44 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/18 14:44 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/18 14:44 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/18 14:44 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/18 14:44 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/18 14:44 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/18 14:44 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/18 14:44 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/18 14:44 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/18 14:44 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/18 14:44 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 14:44 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/18 14:44 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 14:44 1 Acetone <1.7 5.0 1.7 ug/L 04/20/18 14:44 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 14:44 1 Benzene 0.42 J 0.50 0.15 ug/L 04/20/18 14:44 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 14:44 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 14:44 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 14:44 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 14:44 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 14:44 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 14:44 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 14:44 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 14:44 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 14:44 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 14:44 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 14:44 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 14:44 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 14:44 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 14:44 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 14:44 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 14:44 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 14:44 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 14:44 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 14:44 1 Tetrahydrofuran 6.0 J 10 1.9 ug/L 04/20/18 14:44 1 TestAmerica Chicago Page 36 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 Lab Sample ID: 500-143709-19 Date Collected: 04/10/18 15:10 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Toluene <0.15 0.50 0.15 ug/L 04/20/18 14:44 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 14:44 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 14:44 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 14:44 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 14:44 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 14:44 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 14:44 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 14:44 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 14:44 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 117 75- 126 04120118 14:44 1 4-Bromofluorobenzene (Surr) 96 72 - 124 04120118 14:44 1 Dibromofluoromethane 98 75 - 120 04120118 14:44 1 Toluene-d8 (Surr) 93 75 - 120 04120118 14:44 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony 4.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1813:13 1 Arsenic 0.58 J 1.0 0.23 ug/L 04/12/1815:45 04/13/1813:13 1 Barium 190 2.5 0.73 ug/L 04/12/1815:45 04/13/1813:13 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1813:13 1 Cadmium 0.34 J 0.50 0.17 ug/L 04/12/1815:45 04/13/1813:13 1 Chromium 25 5.0 1.1 ug/L 04/12/1815:45 04/13/1813:13 1 Cobalt 1.9 1.0 0.40 ug/L 04/12/1815:45 04/13/1813:13 1 Copper 38 2.0 0.50 ug/L 04/12/1815:45 04/13/1813:13 1 Iron 620 100 47 ug/L 04/12/1815:45 04/13/1813:13 1 Lead 0.62 0.50 0.19 ug/L 04/12/1815:45 04/13/1813:13 1 Manganese 1400 2.5 0.79 ug/L 04/12/1815:45 04/13/1813:13 1 Nickel 26 2.0 0.63 ug/L 04/12/1815:45 04/13/1813:13 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1813:13 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1813:13 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1813:13 1 Vanadium 5.9 5.0 2.2 ug/L 04/12/1815:45 04/13/1813:13 1 Zinc 15 10 6.9 ug/L 04/12/1815:45 04/13/1813:13 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:22 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 35000 4000 3400 ug/L 04/25/1816:59 20 Sulfate 68000 4000 1900 ug/L 04/24/18 23:25 20 Alkalinity 680000 5000 3700 ug/L 04/23/1814:56 1 Total Dissolved Solids 880000 10000 4300 ug/L 04/13/18 07:37 1 0 TestAmerica Chicago Page 37 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11A Lab Sample ID: 500-143709-20 Date Collected: 04/09/18 12:30 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/18 15:13 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/18 15:13 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/18 15:13 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/18 15:13 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/18 15:13 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/18 15:13 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/18 15:13 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/18 15:13 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/18 15:13 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/18 15:13 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/18 15:13 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/18 15:13 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/18 15:13 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 15:13 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/18 15:13 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 15:13 1 Acetone <1.7 5.0 1.7 ug/L 04/20/18 15:13 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 15:13 1 Benzene <0.15 0.50 0.15 ug/L 04/20/18 15:13 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 15:13 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 15:13 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 15:13 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 15:13 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 15:13 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 15:13 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 15:13 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 15:13 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 15:13 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 15:13 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 15:13 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 15:13 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 15:13 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 15:13 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 15:13 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 15:13 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 15:13 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 15:13 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 15:13 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/20/18 15:13 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 15:13 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 15:13 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 15:13 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 15:13 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 15:13 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 15:13 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 15:13 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 15:13 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 15:13 1 0 TestAmerica Chicago Page 38 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11A Lab Sample ID: 500-143709-20 Date Collected: 04/09/18 12:30 Matrix: Water Date Received: 04/12/18 09:10 Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 111 75- 126 4-Bromofluorobenzene (Surr) 96 72 - 124 Dibromofluoromethane 96 75 - 120 Toluene-d8 (Surr) 94 75 - 120 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier Antimony <1.3 Arsenic <0.23 Barium 33 Beryllium <0.53 Cadmium <0.17 Chromium <1.1 Cobalt <0.40 Copper 0.63 J Iron <47 Lead <0.19 Manganese 3.9 Nickel <0.63 Selenium <0.98 Silver <0.12 Thallium <0.57 Vanadium <2.2 Zinc <6.9 Method: 7470A - Mercury (CVAA) Prepared Analyzed Dil Fac 04120118 15:13 1 04120118 15:13 1 04120118 15:13 1 04120118 15:13 1 0 RL MDL Unit D Prepared Analyzed Dil Fac 3.0 1.3 ug/L 04/12/1815:45 04/13/1813:17 1 1.0 0.23 ug/L 04/12/1815:45 04/13/1813:17 1 2.5 0.73 ug/L 04/12/1815:45 04/13/1813:17 1 1.0 0.53 ug/L 04/12/1815:45 04/13/1813:17 1 0.50 0.17 ug/L 04/12/1815:45 04/13/1813:17 1 5.0 1.1 ug/L 04/12/1815:45 04/13/1813:17 1 1.0 0.40 ug/L 04/12/1815:45 04/13/1813:17 1 2.0 0.50 ug/L 04/12/1815:45 04/13/1813:17 1 100 47 ug/L 04/12/1815:45 04/13/1813:17 1 0.50 0.19 ug/L 04/12/1815:45 04/13/1813:17 1 2.5 0.79 ug/L 04/12/1815:45 04/13/1813:17 1 2.0 0.63 ug/L 04/12/1815:45 04/13/1813:17 1 2.5 0.98 ug/L 04/12/1815:45 04/13/1813:17 1 0.50 0.12 ug/L 04/12/1815:45 04/13/1813:17 1 2.0 0.57 ug/L 04/12/1815:45 04/13/1813:17 1 5.0 2.2 ug/L 04/12/1815:45 04/13/1813:17 1 10 6.9 ug/L 04/12/1815:45 04/13/1813:17 1 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/1311812:05 04/1611811:24 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 3800 400 340 ug/L 04/25/1817:11 2 Sulfate 12000 400 190 ug/L 04/24/18 23:50 2 Alkalinity 23000 5000 3700 ug/L 04/20/1816:58 1 Total Dissolved Solids 100000 10000 4300 ug/L 04/13/18 07:39 1 Client Sample ID: MW11 B Lab Sample ID: 500-143709-21 Date Collected: 04/09/18 10:50 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/1815:41 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/1815:41 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/1815:41 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/1815:41 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/1815:41 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/1815:41 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/1815:41 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/1815:41 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/1815:41 1 Page 39 of 64 TestAmerica Chicago 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 B Lab Sample ID: 500-143709-21 Date Collected: 04/09/18 10:50 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/18 15:41 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/18 15:41 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/18 15:41 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/18 15:41 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 15:41 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/18 15:41 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 15:41 1 Acetone <1.7 5.0 1.7 ug/L 04/20/18 15:41 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 15:41 1 Benzene <0.15 0.50 0.15 ug/L 04/20/18 15:41 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 15:41 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 15:41 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 15:41 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 15:41 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 15:41 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 15:41 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 15:41 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 15:41 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 15:41 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 15:41 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 15:41 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 15:41 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 15:41 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 15:41 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 15:41 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 15:41 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 15:41 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 15:41 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 15:41 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/20/18 15:41 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 15:41 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 15:41 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 15:41 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 15:41 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 15:41 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 15:41 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 15:41 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 15:41 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 15:41 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 108 75- 126 04120118 15:41 1 4-Bromofluorobenzene (Surr) 94 72 - 124 04120118 15:41 1 Dibromofluoromethane 96 75 - 120 04120118 15:41 1 Toluene-d8 (Surr) 94 75 - 120 04120118 15:41 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:45 04/13/1813:20 1 Arsenic <0.23 1.0 0.23 ug/L 04/12/1815:45 04/13/1813:20 1 0 TestAmerica Chicago Page 40 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 B Lab Sample ID: 500-143709-21 Date Collected: 04/09/18 10:50 Matrix: Water Date Received: 04/12/18 09:10 Method: Analyte Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Thallium Vanadium Zinc 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 63 2.5 0.73 ug/L 04/12/1815:45 04/13/1813:20 1 <0.53 1.0 0.53 ug/L 04/12/1815:45 04/13/1813:20 1 <0.17 0.50 0.17 ug/L 04/12/1815:45 04/13/1813:20 1 <1.1 5.0 1.1 ug/L 04/12/1815:45 04/13/1813:20 1 <0.40 1.0 0.40 ug/L 04/12/1815:45 04/13/1813:20 1 3.1 2.0 0.50 ug/L 04/12/1815:45 04/13/1813:20 1 <47 100 47 ug/L 04/12/1815:45 04/13/1813:20 1 <0.19 0.50 0.19 ug/L 04/12/1815:45 04/13/1813:20 1 7.6 2.5 0.79 ug/L 04/12/1815:45 04/13/1813:20 1 <0.63 2.0 0.63 ug/L 04/12/1815:45 04/13/1813:20 1 <0.98 2.5 0.98 ug/L 04/12/1815:45 04/13/1813:20 1 <0.12 0.50 0.12 ug/L 04/12/1815:45 04/13/1813:20 1 <0.57 2.0 0.57 ug/L 04/12/1815:45 04/13/1813:20 1 <2.2 5.0 2.2 ug/L 04/12/1815:45 04/13/1813:20 1 <6.9 10 6.9 ug/L 04/12/1815:45 04/13/1813:20 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier Mercury <0.098 (General Chemistry Analyte Chloride Sulfate Alkalinity Total Dissolved Solids Client Sample ID: MW11 D1 Date Collected: 04/09/18 12:10 Date Received: 04/12/18 09:10 RL MDL Unit D Prepared Analyzed Dil Fac 0.20 0.098 ug/L 04/13/1812:05 04/16/1811:25 1 Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 4500 200 170 ug/L 04/25/1817:49 1 18000 400 190 ug/L 04/25/18 00:39 2 36000 5000 3700 ug/L 04/20/1817:04 1 130000 10000 4300 ug/L 04/13/18 07:42 1 Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: 500-143709-22 Matrix: Water Analyte Result Qualifier RL MDL Unit D 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 2-Hexanone <1.6 5.0 1.6 ug/L 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L Acetone <1.7 5.0 1.7 ug/L Prepared Analyzed Dil Fac 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 04/20/18 16:11 1 0 TestAmerica Chicago Page 41 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 D1 Lab Sample ID: 500-143709-22 Date Collected: 04/09/18 12:10 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 16:11 1 Benzene <0.15 0.50 0.15 ug/L 04/20/18 16:11 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 16:11 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 16:11 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 16:11 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 16:11 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 16:11 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 16:11 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 16:11 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 16:11 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 16:11 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 16:11 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 16:11 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 16:11 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 16:11 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 16:11 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 16:11 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 16:11 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 16:11 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 16:11 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 16:11 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/20/18 16:11 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 16:11 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 16:11 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 16:11 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 16:11 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 16:11 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 16:11 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 16:11 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 16:11 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 16:11 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 114 75- 126 04120118 16:11 1 4-Bromofluorobenzene (Surr) 94 72 - 124 04120118 16:11 1 Dibromofluoromethane 98 75 - 120 04120118 16:11 1 Toluene-d8 (Surr) 93 75 - 120 04120118 16:11 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:46 04/13/1813:32 1 Arsenic 0.60 J 1.0 0.23 ug/L 04/12/1815:46 04/13/1813:32 1 Barium 93 2.5 0.73 ug/L 04/12/1815:46 04/13/1813:32 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:46 04/13/1813:32 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:46 04/13/1813:32 1 Chromium 1.6 J 5.0 1.1 ug/L 04/12/1815:46 04/13/1813:32 1 Cobalt <0.40 1.0 0.40 ug/L 04/12/1815:46 04/13/1813:32 1 Copper 9.9 2.0 0.50 ug/L 04/12/1815:46 04/13/1813:32 1 Iron <47 100 47 ug/L 04/12/1815:46 04/13/1813:32 1 Lead <0.19 0.50 0.19 ug/L 04/12/1815:46 04/13/1813:32 1 0 TestAmerica Chicago Page 42 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 D1 Lab Sample ID: 500-143709-22 Date Collected: 04/09/18 12:10 Matrix: Water Date Received: 04/12/18 09:10 , Method: 6020B - Metals (ICP/MS) - Total Recoverable (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Manganese 5.1 2.5 0.79 ug/L 04/12/1815:46 04/13/1813:32 1 Nickel 1.2 J 2.0 0.63 ug/L 04/12/1815:46 04/13/1813:32 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:46 04/13/1813:32 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:46 04/13/1813:32 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:46 04/13/1813:32 1 Vanadium 2.9 J 5.0 2.2 ug/L 04/12/1815:46 04/13/1813:32 1 E: Zinc 32 10 6.9 ug/L 04/12/1815:46 04/13/1813:32 1 �Method: 7470A - Mercury (CVAA) F Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/18 12:05 04/16/18 09:19 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 25000 2000 1700 ug/L 04/26/1810:04 10 Sulfate 35000 2000 950 ug/L 04/25/18 01:04 10 Alkalinity 300000 5000 3700 ug/L 04/20/1817:11 1 Total Dissolved Solids 380000 10000 4300 ug/L 04/13/18 07:44 1 Client Sample ID: MW11 D2 Date Collected: 04/09/18 11:55 Date Received: 04/12/18 09:10 Lab Sample ID: 500-143709-23 Matrix: Water Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/20/18 16:39 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/20/18 16:39 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/20/18 16:39 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/20/18 16:39 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/20/18 16:39 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/20/18 16:39 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/20/18 16:39 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/20/18 16:39 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/20/18 16:39 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/20/18 16:39 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/20/18 16:39 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/20/18 16:39 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/20/18 16:39 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/20/18 16:39 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/20/18 16:39 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/20/18 16:39 1 Acetone <1.7 5.0 1.7 ug/L 04/20/18 16:39 1 Acrylonitrile <4.5 20 4.5 ug/L 04/20/18 16:39 1 Benzene <0.15 0.50 0.15 ug/L 04/20/18 16:39 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/20/18 16:39 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/20/18 16:39 1 Bromoform <0.48 1.0 0.48 ug/L 04/20/18 16:39 1 Bromomethane <0.80 2.0 0.80 ug/L 04/20/18 16:39 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/20/18 16:39 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/20/18 16:39 1 TestAmerica Chicago Page 43 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 D2 Lab Sample ID: 500-143709-23 Date Collected: 04/09/18 11:55 Matrix: Water Date Received: 04/12/18 09:10 , Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chlorobenzene <0.39 1.0 0.39 ug/L 04/20/18 16:39 1 Chloroethane <0.51 1.0 0.51 ug/L 04/20/18 16:39 1 Chloroform <0.37 2.0 0.37 ug/L 04/20/18 16:39 1 Chloromethane <0.32 1.0 0.32 ug/L 04/20/18 16:39 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/20/18 16:39 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/20/18 16:39 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/20/18 16:39 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/20/18 16:39 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/20/18 16:39 1 lodomethane <0.66 2.5 0.66 ug/L 04/20/18 16:39 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/20/18 16:39 1 Styrene <0.39 1.0 0.39 ug/L 04/20/18 16:39 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/20/18 16:39 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/20/18 16:39 1 Toluene <0.15 0.50 0.15 ug/L 04/20/18 16:39 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/20/18 16:39 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/20/18 16:39 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/20/18 16:39 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/20/18 16:39 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/20/18 16:39 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/20/18 16:39 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/20/18 16:39 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/20/18 16:39 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 109 75- 126 04120118 16:39 1 4-Bromofluorobenzene (Surr) 93 72 - 124 04120118 16:39 1 Dibromofluoromethane 97 75 - 120 04120118 16:39 1 Toluene-d8 (Surr) 93 75 - 120 04120118 16:39 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/12/1815:46 04/13/1813:59 1 Arsenic 0.23 J 1.0 0.23 ug/L 04/12/1815:46 04/13/1813:59 1 Barium 110 2.5 0.73 ug/L 04/12/1815:46 04/13/1813:59 1 Beryllium <0.53 1.0 0.53 ug/L 04/12/1815:46 04/13/1813:59 1 Cadmium <0.17 0.50 0.17 ug/L 04/12/1815:46 04/13/1813:59 1 Chromium <1.1 5.0 1.1 ug/L 04/12/1815:46 04/13/1813:59 1 Cobalt 0.75 J 1.0 0.40 ug/L 04/12/1815:46 04/13/1813:59 1 Copper 4.8 2.0 0.50 ug/L 04/12/1815:46 04/13/1813:59 1 Iron <47 100 47 ug/L 04/12/1815:46 04/13/1813:59 1 Lead 0.34 J 0.50 0.19 ug/L 04/12/1815:46 04/13/1813:59 1 Manganese 42 2.5 0.79 ug/L 04/12/1815:46 04/13/1813:59 1 Nickel 1.1 J 2.0 0.63 ug/L 04/12/1815:46 04/13/1813:59 1 Selenium <0.98 2.5 0.98 ug/L 04/12/1815:46 04/13/1813:59 1 Silver <0.12 0.50 0.12 ug/L 04/12/1815:46 04/13/1813:59 1 Thallium <0.57 2.0 0.57 ug/L 04/12/1815:46 04/13/1813:59 1 Vanadium 2.3 J 5.0 2.2 ug/L 04/12/1815:46 04/13/1813:59 1 Zinc 13 10 6.9 ug/L 04/12/1815:46 04/13/1813:59 1 TestAmerica Chicago Page 44 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 D2 Lab Sample ID: 500-143709-23 Date Collected: 04/09/18 11:55 Matrix: Water Date Received: 04/12/18 09:10 , Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/13/18 12:05 04/16/18 09:21 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 5400 400 340 ug/L 04/26/1810:17 2 Sulfate 17000 400 190 ug/L 04/25/18 01:16 2 Alkalinity 53000 5000 3700 ug/L 04/20/1817:17 1 Total Dissolved Solids 94000 10000 4300 ug/L 04/13/18 07:47 1 Client Sample ID: Duplicate Lab Sample ID: 500-143709-24 Date Collected: 04/09/18 00:00 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/1818:11 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 18:11 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 18:11 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 18:11 1 1,1-Dichloroethane 1.8 1.0 0.41 ug/L 04/18/18 18:11 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 18:11 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 18:11 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 18:11 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 18:11 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 18:11 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 18:11 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 18:11 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 18:11 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 18:11 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 18:11 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 18:11 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 18:11 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 18:11 1 Benzene 0.85 0.50 0.15 ug/L 04/18/18 18:11 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 18:11 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 18:11 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 18:11 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 18:11 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 18:11 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 18:11 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 18:11 1 Chloroethane 1.3 1.0 0.51 ug/L 04/18/18 18:11 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 18:11 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 18:11 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 18:11 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 18:11 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 18:11 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 18:11 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 18:11 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 18:11 1 TestAmerica Chicago Page 45 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: Duplicate Lab Sample ID: 500-143709-24 Date Collected: 04/09/18 00:00 Matrix: Water Date Received: 04/12/18 09:10 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Methylene Chloride <1.6 5.0 1.6 ug/L Styrene <0.39 1.0 0.39 ug/L Tetrachloroethene <0.37 1.0 0.37 ug/L Tetrahydrofuran 20 10 1.9 ug/L Toluene <0.15 0.50 0.15 ug/L trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L Trichloroethene <0.16 0.50 0.16 ug/L Trichlorofluoromethane <0.43 1.0 0.43 ug/L Vinyl acetate <0.91 2.0 0.91 ug/L Vinyl chloride 1.4 1.0 0.20 ug/L Xylenes, Total <0.22 1.0 0.22 ug/L Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 99 75- 126 4-Bromofluorobenzene (Surr) 90 72 - 124 Dibromofluoromethane 100 75 - 120 Toluene-d8 (Surr) 92 75 - 120 Client Sample ID: Trip Blank Date Collected: 04/09/18 00:00 Date Received: 04/12/18 09:10 Prepared Analyzed Dil Fac 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 04/18/18 18:11 1 Prepared Analyzed Dil Fac 04118118 18:11 1 04118118 18:11 1 04118118 18:11 1 04118118 18:11 1 Lab Sample ID: 500-143709-25 Matrix: Water Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 04/18/18 18:37 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 04/18/18 18:37 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 04/18/18 18:37 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 04/18/18 18:37 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 04/18/18 18:37 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 04/18/18 18:37 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 04/18/18 18:37 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 04/18/18 18:37 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 04/18/18 18:37 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 04/18/18 18:37 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 04/18/18 18:37 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 04/18/18 18:37 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 04/18/18 18:37 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 04/18/18 18:37 1 2-Hexanone <1.6 5.0 1.6 ug/L 04/18/18 18:37 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 04/18/18 18:37 1 Acetone <1.7 5.0 1.7 ug/L 04/18/18 18:37 1 Acrylonitrile <4.5 20 4.5 ug/L 04/18/18 18:37 1 Benzene <0.15 0.50 0.15 ug/L 04/18/18 18:37 1 Bromochloromethane <0.43 1.0 0.43 ug/L 04/18/18 18:37 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 04/18/18 18:37 1 Bromoform <0.48 1.0 0.48 ug/L 04/18/18 18:37 1 Bromomethane <0.80 2.0 0.80 ug/L 04/18/18 18:37 1 Carbon disulfide <0.45 2.0 0.45 ug/L 04/18/18 18:37 1 0 TestAmerica Chicago Page 46 of 64 5/9/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: Trip Blank Lab Sample ID: 500-143709-25 Date Collected: 04/09/18 00:00 Matrix: Water Date Received: 04/12/18 09:10 , Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Carbon tetrachloride <0.38 1.0 0.38 ug/L 04/18/18 18:37 1 Chlorobenzene <0.39 1.0 0.39 ug/L 04/18/18 18:37 1 Chloroethane <0.51 1.0 0.51 ug/L 04/18/18 18:37 1 Chloroform <0.37 2.0 0.37 ug/L 04/18/18 18:37 1 Chloromethane <0.32 1.0 0.32 ug/L 04/18/18 18:37 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 04/18/18 18:37 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 04/18/18 18:37 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 04/18/18 18:37 1 Dibromomethane <0.27 1.0 0.27 ug/L 04/18/18 18:37 1 Ethylbenzene <0.18 0.50 0.18 ug/L 04/18/18 18:37 1 lodomethane <0.66 2.5 0.66 ug/L 04/18/18 18:37 1 Methylene Chloride <1.6 5.0 1.6 ug/L 04/18/18 18:37 1 Styrene <0.39 1.0 0.39 ug/L 04/18/18 18:37 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 04/18/18 18:37 1 Tetrahydrofuran <1.9 10 1.9 ug/L 04/18/18 18:37 1 Toluene <0.15 0.50 0.15 ug/L 04/18/18 18:37 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 04/18/18 18:37 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 04/18/18 18:37 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 04/18/18 18:37 1 Trichloroethene <0.16 0.50 0.16 ug/L 04/18/18 18:37 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 04/18/18 18:37 1 Vinyl acetate <0.91 2.0 0.91 ug/L 04/18/18 18:37 1 Vinyl chloride <0.20 1.0 0.20 ug/L 04/18/18 18:37 1 Xylenes, Total <0.22 1.0 0.22 ug/L 04/18/18 18:37 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 97 75- 126 04118118 18:37 1 4-Bromofluorobenzene (Surr) 91 72 - 124 04118118 18:37 1 Dibromofluoromethane 96 75 - 120 04118118 18:37 1 Toluene-d8 (Surr) 93 75 - 120 04118118 18:37 1 TestAmerica Chicago Page 47 of 64 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed Client Sample ID: MW1 Date Collected: 04/10/18 10:15 Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Client Sample ID: MW4 Date Collected: 04/09/18 11:05 Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Client Sample ID: MW4A Date Collected: 04/09/18 12:10 Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020E Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Lab Sample ID: 500-143709-1 Matrix: Water Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428429 04/18/18 19:03 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 11:39 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 10:37 EEN TAL CHI 1 429118 04/21/18 12:58 EAT TAL CHI 10 429118 04/21/18 13:11 EAT TAL CHI 1 428854 04/20/18 14:32 SMO TAL CHI 1 427660 04/13/18 05:50 CLB TAL CHI Lab Sample ID: 500-143709-2 Matrix: Water Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428429 04/18/18 19:29 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 11:58 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 10:39 EEN TAL CHI 2 429118 04/21/18 14:40 EAT TAL CHI 5 429118 04/21/18 14:52 EAT TAL CHI 1 428854 04/20/18 14:43 SMO TAL CHI 1 427660 04/13/18 05:53 CLB TAL CHI Lab Sample ID: 500-143709-3 Matrix: Water Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428429 04/18/18 19:55 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 12:01 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 10:46 EEN TAL CHI 2 429118 04/21/18 15:05 EAT TAL CHI 1 428854 04/20/18 14:49 SMO TAL CHI 1 427660 04/13/18 05:55 CLB TAL CHI Page 48 of 64 TestAmerica Chicago 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed Client Sample ID: MW413 Date Collected: 04/09/18 12:35 Date Received: 04/12/18 09:10 TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Lab Sample ID: 500-143709-4 Matrix: Water Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428429 04/18/18 20:21 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 12:05 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 10:56 EEN TAL CHI Total/NA Analysis 9056A 2 429118 04/21/18 15:18 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 14:57 SMO TAL CHI Total/NA Analysis SM 2540C 1 427660 04/13/18 05:58 CLB TAL CHI Client Sample ID: MW41)1 Date Collected: 04/09/18 11:40 Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Client Sample ID: MW5 Date Collected: 04/09/18 14:40 Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020E Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Lab Sample ID: 500-143709-5 Matrix: Water Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428429 04/18/18 20:47 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 12:16 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 10:57 EEN TAL CHI 1 429308 04/24/18 20:28 EAT TAL CHI 5 429308 04/24/18 20:41 EAT TAL CHI 1 428854 04/20/18 15:17 SMO TAL CHI 1 427667 04/13/18 06:53 CLB TAL CHI Lab Sample ID: 500-143709-6 Matrix: Water Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428429 04/18/18 21:13 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 12:20 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 10:59 EEN TAL CHI 20 429308 04/24/18 20:53 EAT TAL CHI 1 428854 04/20/18 15:26 SMO TAL CHI 1 427667 04/13/18 07:00 CLB TAL CHI Page 49 of 64 TestAmerica Chicago 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW5D Lab Sample ID: 500-143709-7 Date Collected: 04/09/18 15:10 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428429 04/18/18 21:39 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 12:24 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 11:00 EEN TAL CHI Total/NA Analysis 9056A 25 429308 04/24/18 21:31 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 15:37 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:06 CLB TAL CHI Client Sample ID: MW6 Lab Sample ID: 500-143709-8 Date Collected: 04/09/18 15:50 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Client Sample ID: MW6D Date Collected: 04/09/18 14:40 Date Received: 04/12/18 09:10 Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428429 04/18/18 22:05 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 12:28 FXG TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 5 427928 04/13/18 14:02 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 11:02 EEN TAL CHI 10 429308 04/24/18 21:56 EAT TAL CHI 1 428854 04/20/18 15:48 SMO TAL CHI 1 427667 04/13/18 07:08 CLB TAL CHI Lab Sample ID: 500-143709-9 Matrix: Water Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Total/NA Analysis 8260B 1 428429 04/18/18 22:31 JJH Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE Total Recoverable Analysis 6020E 1 427928 04/13/18 12:31 FXG Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE Total Recoverable Analysis 6020B 10 427928 04/13/18 14:10 FXG Total/NA Prep 7470A 427754 04/13/18 12:05 EEN Total/NA Analysis 7470A 1 427959 04/16/1811:04 EEN Total/NA Analysis 9056A 10 429308 04/24/18 22:09 EAT Total/NA Analysis SM 2320B 1 428854 04/20/18 15:58 SMO Total/NA Analysis SM 2540C 1 427667 04/13/18 07:11 CLB Lab TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI Page 50 of 64 TestAmerica Chicago 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW6D1 Lab Sample ID: 500-143709-10 Date Collected: 04/09/18 15:15 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428429 04/18/18 22:57 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 12:35 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 11:05 EEN TAL CHI Total/NA Analysis 9056A 5 429308 04/24/18 22:47 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 16:12 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:13 CLB TAL CHI Client Sample ID: MW7 Lab Sample ID: 500-143709-11 Date Collected: 04/10/18 10:25 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Client Sample ID: MW7A Date Collected: 04/10/18 09:55 Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428429 04/18/18 23:23 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 12:39 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 11:07 EEN TAL CHI 10 429308 04/24/18 23:12 EAT TAL CHI 1 428854 04/20/18 16:21 SMO TAL CHI 1 427667 04/13/18 07:16 CLB TAL CHI Lab Sample ID: 500-143709-12 Matrix: Water Dilution Factor Batch Number Prepared or Analyzed Analyst Lab 1 428429 04/18/18 23:49 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 12:43 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 11:09 EEN TAL CHI 10 429319 04/24/18 19:55 EAT TAL CHI 10 429402 04/25/18 15:20 EAT TAL CHI 1 428854 04/20/18 16:29 SMO TAL CHI 1 427667 04/13/18 07:19 CLB TAL CHI TestAmerica Chicago Page 51 of 64 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc Project/Site: North Mecklenburg Landfill - Closed Client Sample ID: MW7D Date Collected: 04/10/18 09:30 Date Received: 04/12/18 09:10 TestAmerica Job ID: 500-143709-1 SDG: NCDEQ Solid Waste Facility = # 60-13 Lab Sample ID: 500-143709-13 Matrix: Water Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428546 04/19/18 23:57 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 12:47 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 11:10 EEN TAL CHI Total/NA Analysis 9056A 5 429319 04/24/18 20:07 EAT TAL CHI Total/NA Analysis 9056A 20 429402 04/25/18 15:32 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 16:36 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:21 CLB TAL CHI Client Sample ID: MW8 Lab Sample ID: 500-143709-14 Date Collected: 04/10/18 11:20 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428709 04/20/18 12:52 JJH TAL CHI Total/NA Analysis 9056A 10 429319 04/24/18 20:44 EAT TAL CHI Total/NA Analysis 9056A 5 429575 04/26/18 09:52 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 16:45 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:24 CLB TAL CHI Client Sample ID: MW8D Lab Sample ID: 500-143709-15 Date Collected: 04/10/18 13:25 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 428709 04/20/18 13:20 JJH TAL CHI 427587 04/12/18 15:45 BDE TAL CHI 1 427928 04/13/18 12:50 FXG TAL CHI 427754 04/13/18 12:05 EEN TAL CHI 1 427959 04/16/18 11:16 EEN TAL CHI 2 429319 04/24/18 20:57 EAT TAL CHI 25 429402 04/25/18 15:45 EAT TAL CHI 1 428854 04/20/18 16:53 SMO TAL CHI 1 427667 04/13/18 07:26 CLB TAL CHI Page 52 of 64 TestAmerica Chicago 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW9 Lab Sample ID: 500-143709-16 Date Collected: 04/10/18 09:15 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428709 04/20/18 13:48 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 13:02 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 11:18 EEN TAL CHI Total/NA Analysis 9056A 2 429319 04/24/18 21:21 EAT TAL CHI Total/NA Analysis 9056A 5 429402 04/25/18 15:57 EAT TAL CHI Total/NA Analysis SM 2320B 1 429134 04/23/18 14:46 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:29 CLB TAL CHI Client Sample ID: MW10 Lab Sample ID: 500-143709-17 Date Collected: 04/10/18 09:50 Matrix: Water Date Received: 04/12/18 09:10 Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428709 04/20/18 14:16 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 13:05 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 11:19 EEN TAL CHI Total/NA Analysis 9056A 1 429319 04/24/18 22:11 EAT TAL CHI Total/NA Analysis 9056A 20 429402 04/25/18 16:09 EAT TAL CHI Total/NA Analysis SM 2320B 1 429134 04/23/18 14:11 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:31 CLB TAL CHI Client Sample ID: MW1OD Date Collected: 04/10/18 14:25 Date Received: 04/12/18 09:10 Lab Sample ID: 500-143709-18 Matrix: Water Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Total/NA Analysis 8260B 1 428083 04/17/1816:39 PMF Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE Total Recoverable Analysis 6020B 1 427928 04/13/18 13:09 FXG Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE Total Recoverable Analysis 6020B 10 427928 04/13/18 14:14 FXG Total/NA Prep 7470A 427754 04/13/18 12:05 EEN Total/NA Analysis 7470A 1 427959 04/16/1811:21 EEN Total/NA Analysis 9056A 50 429319 04/24/18 22:35 EAT Total/NA Analysis 9056A 50 429402 04/25/1816:22 EAT Total/NA Analysis SM 2320B 1 429134 04/23/18 14:37 SMO Total/NA Analysis SM 2540C 1 427667 04/13/18 07:34 CLB Lab TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TestAmerica Chicago Page 53 of 64 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 Lab Sample ID: 500-143709-19 Date Collected: 04/10/18 15:10 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428709 04/20/18 14:44 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 13:13 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 11:22 EEN TAL CHI Total/NA Analysis 9056A 20 429319 04/24/18 23:25 EAT TAL CHI Total/NA Analysis 9056A 20 429402 04/25/18 16:59 EAT TAL CHI Total/NA Analysis SM 2320B 1 429134 04/23/18 14:56 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:37 CLB TAL CHI Client Sample ID: MW11A Lab Sample ID: 500-143709-20 Date Collected: 04/09/18 12:30 Matrix: Water Date Received: 04/12/18 09:10 Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428709 04/20/18 15:13 JJH TAL CHI Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 13:17 FXG TAL CHI Total/NA Prep 7470A 427754 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 11:24 EEN TAL CHI Total/NA Analysis 9056A 2 429319 04/24/18 23:50 EAT TAL CHI Total/NA Analysis 9056A 2 429402 04/25/18 17:11 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 16:58 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:39 CLB TAL CHI Client Sample ID: MW11B Date Collected: 04/09/18 10:50 Date Received: 04/12/18 09:10 Lab Sample ID: 500-143709-21 Matrix: Water Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Total/NA Analysis 8260B 1 428709 04/20/1815:41 JJH Total Recoverable Prep 3005A 427587 04/12/18 15:45 BDE Total Recoverable Analysis 6020B 1 427928 04/13/18 13:20 FXG Total/NA Prep 7470A 427754 04/13/18 12:05 EEN Total/NA Analysis 7470A 1 427959 04/16/1811:25 EEN Total/NA Analysis 9056A 2 429319 04/25/18 00:39 EAT Total/NA Analysis 9056A 1 429402 04/25/1817:49 EAT Total/NA Analysis SM 2320B 1 428854 04/20/18 17:04 SMO Total/NA Analysis SM 2540C 1 427667 04/13/18 07:42 CLB Lab TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TestAmerica Chicago Page 54 of 64 5/9/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Client Sample ID: MW11 D1 Lab Sample ID: 500-143709-22 Date Collected: 04/09/18 12:10 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428709 04/20/18 16:11 JJH TAL CHI Total Recoverable Prep 3005A 427588 04/12/18 15:46 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 13:32 FXG TAL CHI Total/NA Prep 7470A 427755 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 09:19 EEN TAL CHI Total/NA Analysis 9056A 10 429319 04/25/18 01:04 EAT TAL CHI Total/NA Analysis 9056A 10 429575 04/26/18 10:04 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 17:11 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:44 CLB TAL CHI Client Sample ID: MW11 D2 Lab Sample ID: 500-143709-23 Date Collected: 04/09/18 11:55 Matrix: Water Date Received: 04/12/18 09:10 Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428709 04/20/18 16:39 JJH TAL CHI Total Recoverable Prep 3005A 427588 04/12/18 15:46 BDE TAL CHI Total Recoverable Analysis 6020B 1 427928 04/13/18 13:59 FXG TAL CHI Total/NA Prep 7470A 427755 04/13/18 12:05 EEN TAL CHI Total/NA Analysis 7470A 1 427959 04/16/18 09:21 EEN TAL CHI Total/NA Analysis 9056A 2 429319 04/25/18 01:16 EAT TAL CHI Total/NA Analysis 9056A 2 429575 04/26/18 10:17 EAT TAL CHI Total/NA Analysis SM 2320B 1 428854 04/20/18 17:17 SMO TAL CHI Total/NA Analysis SM 2540C 1 427667 04/13/18 07:47 CLB TAL CHI Client Sample ID: Duplicate Lab Sample ID: 500-143709-24 Date Collected: 04/09/18 00:00 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428429 04/18/18 18:11 JJH TAL CHI Client Sample ID: Trip Blank Lab Sample ID: 500-143709-25 Date Collected: 04/09/18 00:00 Matrix: Water Date Received: 04/12/18 09:10 Batch Batch Dilution Batch Prepared Prep Type Type Method Run Factor Number or Analyzed Analyst Lab Total/NA Analysis 8260B 1 428429 04/18/18 18:37 JJH TAL CHI Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 TestAmerica Chicago Page 55 of 64 5/9/2018 Accreditation/Certification Summary C Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Laboratory: TestAmerica Chicago Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program EPA Region Identification Number Expiration Date North Carolina (WW/SW) State Program 4 291 12-31-18 The following analytes are included in this report, but accreditation/certification is not offered by the governing authority: Analysis Method Prep Method Matrix Analyte 8260E Water trans-1,4-Dichloro-2-butene TestAmerica Chicago Page 56 of 64 5/9/2018 Method Summary Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds (GC/MS) SW846 TAL CHI 6020B Metals (ICP/MS) SW846 TAL CHI 7470A Mercury (CVAA) SW846 TAL CHI 9056A Anions, Ion Chromatography SW846 TAL CHI SM 2320B Alkalinity SM TAL CHI SM 2540C Solids, Total Dissolved (TDS) SM TAL CHI 3005A Preparation, Total Recoverable or Dissolved Metals SW846 TAL CHI 5030B Purge and Trap SW846 TAL CHI 7470A Preparation, Mercury SW846 TAL CHI Protocol References: SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 ='Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 TestAmerica Chicago Page 57 of 64 5/9/2018 Sample Summary Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-143709-1 Project/Site: North Mecklenburg Landfill - Closed SDG: NCDEQ Solid Waste Facility = # 60-13 Lab Sample ID Client Sample ID Matrix Collected Received 500-143709-1 MW1 Water 04/10/18 10:15 04/12/18 09:10 500-143709-2 MW4 Water 04/09/18 11:05 04/12/18 09:10 500-143709-3 MW4A Water 04/09/18 12:10 04/12/18 09:10 500-143709-4 MW4D Water 04/09/18 12:35 04/12/18 09:10 500-143709-5 MW4D1 Water 04/09/18 11:40 04/12/18 09:10 500-143709-6 MW5 Water 04/09/18 14:40 04/12/18 09:10 500-143709-7 MW5D Water 04/09/18 15:10 04/12/18 09:10 500-143709-8 MW6 Water 04/09/18 15:50 04/12/18 09:10 500-143709-9 MW6D Water 04/09/18 14:40 04/12/18 09:10 500-143709-10 MW6D1 Water 04/09/18 15:15 04/12/18 09:10 500-143709-11 MW7 Water 04/10/18 10:25 04/12/18 09:10 500-143709-12 MW7A Water 04/10/18 09:55 04/12/18 09:10 500-143709-13 MW7D Water 04/10/18 09:30 04/12/18 09:10 500-143709-14 MW8 Water 04/10/18 11:20 04/12/18 09:10 500-143709-15 MW8D Water 04/10/18 13:25 04/12/18 09:10 500-143709-16 MW9 Water 04/10/18 09:15 04/12/18 09:10 500-143709-17 MW10 Water 04/10/18 09:50 04/12/18 09:10 500-143709-18 MW1 OD Water 04/10/18 14:25 04/12/18 09:10 500-143709-19 MW11 Water 04/10/18 15:10 04/12/18 09:10 500-143709-20 MW11A Water 04/09/18 12:30 04/12/18 09:10 500-143709-21 MW11 B Water 04/09/18 10:50 04/12/18 09:10 500-143709-22 MW11 D1 Water 04/09/18 12:10 04/12/18 09:10 500-143709-23 MW11 D2 Water 04/09/18 11:55 04/12/18 09:10 500-143709-24 Duplicate Water 04/09/18 00:00 04/12/18 09:10 500-143709-25 Trip Blank Water 04/09/18 00:00 04/12/18 09:10 TestAmerica Chicago Page 58 of 64 5/9/2018 TestAnnerica Chicago 2417 Bond Street University Park, IL 60484 Phnna (7nm 534_s9nn Fax.(7081 534-5911 Chain of Custody Record s-00--- /V 3 70 f TestAmenca Client Information Sampler: A J sL11 V t wr� fnN Lab PM: Kintz, Robin M Carrier Tracking No(s): COC No: 500-61781-29578.3 Client Contact: Mr. Ed Stephens Phone: ��' Z3 — o E-Mail: 1-bin. kintz@testamericafnc.com Page: Page 0 0 Company: Job #: f j Civil & Environmental Consultants Inc Analysis Requested Address: Due Date Requested: Preservation Codes: 1900 Center Park Drive Suite A gr=' =- =` _-' A - HCL M -Hexane B - NaOH N - None City: TAT Requested (days): Charlotte -- `F `c C- ZnAcetate 0-AsNa02 D - Nitric Acid P - Na204S State, Zip: NC, 28217 -` _", _ _ _ _-_.. _-- __- - -G--Amehlor E-NaHSO4 0-Na2SO3 F -MeOH R-Na2S203 -_ -- - S-H2SO4---_ _P_hone: --- --_- ---- ---- --- --- - -- 2S)a#'=. ---- --- ------ --- -=------_-�-------' 855-859-9932(Tel) Purchase Order not required _ o Z - =h _ - H-Ascorbic Acid T-TSP Dodecahydrate I - Ice U - Acetone Email: WO P. estephens@cecinc.com 'o 'tH".= m. y _ot z' =`=�� o � , o o- E c o a E m-d= a ._ - C- J - DI Water V - MCAA K -EDTA W - pH 4-5 L- EDA Z- other (specify) Project Name: Project #: NC North Mecklenburg Landfill 50013286 m =; -} d 0 d ❑ �, 4 Other: Site: o^ ti1/V SSOW#: a t N` 'NS in in o H a U o Matrix =_E 7G=gab) (W—ter, LE 4=E=_ N U Sample s=sona, 0—steroll, --- .LL - - w o M ,- Sample Identification Sample Date Time =rssue,n=alr m -_a= N . in Special Instructions/Note: - — =Preservation Cotle ;=, N__. A N•:' N B •' D. A - -- I \w-1 Lf 11 to.K Water X Water rw- A (rhh��� 'Y � r210 Water (rr W- v6� pp -1 d yy, �J}7 IPf� ° J Water ap�e6W- LID _ f h 1 :40 Water ^,1 q T9gp�z � 1' Q Water ''••,��� `-� SA� ��' I� Water rv' U .Y JAW - �� S Water s3 Mw-�'l Water ffl Mw" (017' I dS: l 5' Water �500-143709 COC Yoh P t0 8 (0 ' 2 i Water Possible Hazard Identification Sample Disposal (A fee may be assessed if samples are retained longer than 1 month) = Non -Hazard 0 Flammable kin Irritant Poison B Unknown Radiological = Return To Client 0 Disposal By Lab Archive For Deliverable Requested: 1, II, III, IV, Ot er (specify) Special Instructions/QC Requirements: �yMonths / Empty Kit Relinquished by: =' 7 i - Date: Time: Method of shipment: Relinquished by: - ,r ,...--' Datefrime: t t Company o R w by: Date ime m Company G%1, - , o1°� d % XS 1+1 L( it 14 ©b" Relinqui Date im : Company Received by: Date im Company TN- aow Relinquished -by: Date im' Company e Rece' d-b ' Date/Si e:_ Company__ Custody Seals Intact: Custody Seal No.: Cooler Temperature(s) eC and Other Remarks f •-67 - i ` d`% (,�`� r�`� i6`—D . A Yes A No Page 59 of 64 V Gl: UO/V4/LVIU 5/9/2018 L1 TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Phone (708)_534-5206 Fax (708) 534-5211 Chain of Custody Record .rep ' fs r e ,71 O - / �3 70 9 5TAm 1c am -ri-tE.-. LFAncrr fr. rtrvinor:r,^r:a:n:. TESTING Sampler: Lab PM: Carrier Tracing COC No: Client Information Kintz, Robin M 500-61781-29578.4 Client Contact: Mr. Ed Stephens Phone: E-Mail: robin.kintz@testamericainc.com Page: 2 Page 0 7 Company: Civil & Environmental Consultants Inc Analysis Requested Job #: ` r Y30 • 00 I Address: Due Date Requested:Preservation Codes: 1900 Center Park Drive Suite A A- HCL M -Hexane B- NaOH N -None City: TAT Requested (days): Charlotte -;._ =` _ �'- C - Zn Acetate O - AsNa02 D - Nitric Acid P - Na204S State, Zip: NC, 28217 = ��'• _ --_ E - NaHSO4 Q - Na2SO3 F -McOH R-Na2S203 Phone: PO #: _ 855-859-9932(Tel) Purchase Order not required o _ H- Ascorbic Acid T -TSP Dodecahydrate I - Ice U- Acetone Email: WO#: Z estephens@cecine.com o`o y r 4 v 0 E c °o. E w `m`- --�' J- DIWater v-MCAA K - EDTA W - pH 4-5 L- EDA Z- other (specify) Project Name: Project #: NC North Mecklenburg Landfill 50013286 -6 =0- `_mr _ =h v u a, p T «: ,a- __O.' Other: Site: SSOW#: -to tn m =.�_� .y Fin' ` u � in S 0 N 0 S m a � v"_"_ �_ � U o o - O' sZ1 Sample Matrix Type (w=wemr, � A� � o � R � v N az= Sample (C=comp, o=V,eer Sample Identification Sample Date Time G=grab) BT=Tlssue,A=Air) iz_4_ H ; ao m N -1°-' Special Instructions/Note: _ -_- Preservation Code - w � 1 l r 01''Ce Water 4116 it Water /o Water No 0 1^3d M.w-1l 411,10 Ile 15:10 =_ 01 � 1 -II 6 16 I1 1 1 Fml Possible Hazard Identification Sample Disposal (A fee may be assessed if samples are retained longer than 1 month) Non -Hazard Fla rfiable Skin Irritant Poison B Unknown Radiological Return To Client Disposal By Lab Archive For Months Deliverable Requested, III, IV, Other (specify) Special Instructions/QC Requirements: Empty Kit Relingtished Date: Time: Method of shipment: Relinq ish by: / DatefTime:7 pry Company/p /,�....,�� Rece' a y: Date ime Company Relinquis Date me / Com_pany Recewe by: Date/ im Company i3 liagJ s_h Clhy' — —1".t,[t me, Company--- Re cei Date Ti e — — Company --- Custody Seals Intact: Custody Seal No.: Cooler Temperature(s) eC and Other Remarks: A Yes A No Page 60 of 64 Ver:08/04/2016 5/9/2018 TestAmerica Chicago 2417 Bond Street University Park, IL 60484 - ---Phone (708) 534-5200 Fax (708) 534-5211 Vq� V1 Chain of Custody Record st Amef!c Client Information Sampler: Agustlna Cortina Lab PM: Kintz, Robin M 1 Tracking sorcy <8+� d' CDC No: 500-61781-29578.4 Client Contact: Mr. Ed Stephens Phone:980-237-0373 E-Mail: robin.kintz@testamericainc.com Page: Page 3 of 3 Company: Civil & Environmental Consultants Inc Analysis Requested Job #:111-370.001 Address: 1900 Center Park Drive Suite A Due Date Requested: " i = ' S Preservation Codes: A- HCL M -Hexane B - NaOH N - None C- ZnAcetate 0-AsNaO2 D- Nitric Acid P-Na204S E-NeHSO4 Q-Na2SO3 F- McOH R - Na2S203 �v-Am City: Charlotte TAT Requested (days): State, Zip: NC,28217 Phone: p0 #, Pur6hase -r erno requre -`- - —^�a m ,r 9r .! i; uai o N o > a E i °o o o ; °a E m N °o f a oo o0D ro c y t) o u'a' N 14 d o_ a • :, a; tp; �.. f°: H- Ascorbic Acid T- TSPDodecahydrate I -Ice U- Acetone J - DI Water V - MCAA K- EDTA W - pH 4-5 L-EDA Z- other(specify) Other: Email: estephens@cecinc.com WO#: Project Name: NC North Mecklenburg Landfill Project#: 50013286 Site: CLOSED SSOW#: % p li : Sample Identification Sample Date Sample Time Sample Type (C=comp, G= rab) Matrix (waweter, s•soaa 0- .i;;% eT.Ta.uo,A-Atr Special Instructions/Note: -x:.:•:; Preservattort.pode: MW-11D-2 4/9/18 11:55 water X X X Duplicate 419/18 water X �9. Possible Hazard Identification = Non -Hazard = Flammable Skin Irritant Poison B Unknown Radiological Sample Disposal (A fee maybe assessed if samples are retained longer than 1 month) = Retum To Client = Disposal By Lab Archive For Months Deliverable Requested: 1, 11, 111, IV, Other (specify) Special Instructions= Requirements: Empty Kit Relinquished by: JDate: Time: Method of shipment: Relinquished by: { /� . --`n �r Dateli ; �r II �� 0 ''�1� Company C c R c Iv d by: T- tti`1 Date a Im 11 54 Compan 1 V1 R i ut hed by., r Date tm I t t -o Company Received by: Date 'me �s< ,,� .a .n Company Relinquished by: Date el Company Receive Dater e: Company Custody Seals Intact: o Yes r1 No Custody Seal No.: , Cooler Tempemture(s) °C and Other Remadcs: Page 61 of 64 Ver:08/04/201b 5/9/2018 0M '#+d yLUyV6y IuIJ _ vr(I "uv 4 v T P T :sod SdW t aba sn-ii i tr8P'09 1H0INN3AO (nivaNVIS d00T'ddd z! - InHl s � , ssssaaajcicxx�g��.y/p��� 4{' Al 500-143709 Waybill .'j • vi,or VN ## NalsvW ### SEL ML 61,LL #Nai III111111] 111111111111111111111111111111111111111111111111111 1d�0 Od oozy -Kg (sot V8V0911 AWd A11SN3AINn 133HISGNOB l �VZ . Idl s 03H 31dWVS of 1N314id � = 9OZ89 ON 3AIW A110 N33no 9-0£8Z 1d11)I1WW MZ1l UV-•iJNCI'JV 6 31V0 dIHS i V9I,I.-Z6£ ("6 a T ORIGIN ID:PNUp (704) 392-1164 . SHIP DATE: 11APR18 CANDACE BONHAM ACTWGT. 40.00 LB TESTAMERIGA — — -CAD: 509604-31INET3980 2838-8 QUE�N CITY DRIVE CHARLOTTE NC 28208 BILL RECIPIENT UNITED STALES US ; To SAMPLE REC TAI 2417 BOND STREET UNIVERSITY PARK IL 60484 NV: Po, DEPT. _ s r �1111 -it I �� �� ' 1 1 1 I 1 T- ■ E►X „Ili THU -12 APR 3:OOP I `; MPS# 2 of 3 STANDARD OVERNIGHT I ; o2s3 7719 71217950 Mstr# 7719 7121 7397 ozol 60484 ��:Us a D NA JOTA • r< Page 62 of 64 5/9/2018 s ` M iN:ID'RNI- A ' (704) 39211�4 C nngqCEBOroHAM r TES ERICA - SHIP DATE: 11APR18 ' . 2838•B QUEEN CITY DRIVE ACTWGT: 40.0 CAD: 6096043A LB ? ET3980 ; CHARLOTTE NO 28208 UNITED STALES US BILLRECIPIE_ To SAMPLE REC TAI - 2417 BOND STREET; UNIVERSITY PARK IL 60484 (708)534-5200 NU: REF: P0: y III IIIiiriiia u � � r IFevFm. Express C EL I 1 k r Ij �'j r1 �� ¢•• � , I �'� x ;. 3 of 3 THU - ,12 PR 3-OOP E63 7719 7121 7960 STANDARD 0 ERNIGHT Mstr# 7719 7121 7397 0201 NAJOTAG0484 it �L s �RD yk I ; t i � r j • 0 �Al r � , Page 63 of 64 5/9/2018 Client: Civil & Environmental Consultants Inc Login Number: 143709 List Number: 1 Creator: Kelsey, Shawn M Question Login Sample Receipt Checklist Job Number: 500-143709-1 SDG Number: NCDEQ Solid Waste Facility = # 60-13 Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey True meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. True List Source: TestAmerica Chicago (0.9)(1.2)(0.5)c TestAmerica Chicago Page 64 of 64 5/9/2018 TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Tel: (708)534-5200 TestAmerica Job ID: 500-144127-1 Client Project/Site: NC North Mecklenburg Landfill - WSW roi Civil & Environmental Consultants Inc 1900 Center Park Drive Suite A Charlotte, North Carolina 28217 Attn: Matt Ginther Ahuc /V *W Authorized for release by: 71512018 9:06:51 AM Robin Kintz, Project Manager II (708)534-5200 robin.kintz@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW Table of Contents TestAmerica Job ID: 500-144127-1 CoverPage .............................................. 1 Table of Contents ......................................... 2 Case Narrative ........................................... 3 L Detection Summary ........................................ 4 Method Summary ......................................... 6 Sample Summary ......................................... 7 Client Sample Results ...................................... 8 E: Definitions ............................................... 17 QC Association ........................................... 18 F Surrogate Summary ....................................... 20 QC Sample Results ........................................ 21 Chronicle................................................ 27 Certification Summary ...................................... 28 Chain of Custody .......................................... 29 E: Receipt Checklists ......................................... 32 Page 2 of 32 TestAmerica Chicago 7/5/2018 Case Narrative C Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Job ID: 500-144127-1 Laboratory: TestAmerica Chicago Narrative Job Narrative 500-144127-1 Comments No additional comments. Receipt The samples were received on 4/20/2018 9:00 AM; the samples arrived in good condition, properly preserved and, where required, on ice The temperature of the cooler at receipt was 1.90 C. GC/MS VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica Chica o Page 3 of 32 7/5/20T8 Detection Summary Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW TestAmerica Job ID: 500-144127-1 Client Sample ID: Gilkerson WSW Lab Sample ID: 500-144127-1 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Bromodichloromethane 12 1.0 0.37 ug/L 1 8260B Total/NA Bromoform 0.62 J 1.0 0.48 ug/L 1 8260B Total/NA Chloroform 31 2.0 0.37 ug/L 1 8260B Total/NA Dibromochloromethane 5.5 1.0 0.49 ug/L 1 8260B Total/NA Barium 14 2.5 0.73 ug/L 1 6020B Total Recoverable Chromium 1.5 J 5.0 1.1 ug/L 1 6020B Total Recoverable Copper 23 B 2.0 0.50 ug/L 1 6020B Total Recoverable Iron 1500 B 100 47 ug/L 1 6020E Total Recoverable Lead 7.4 0.50 0.19 ug/L 1 6020B Total Recoverable Manganese 28 2.5 0.79 ug/L 1 6020B Total Recoverable Nickel 1.1 J 2.0 0.63 ug/L 1 6020B Total Recoverable Zinc 190 10 6.9 ug/L 1 6020B Total Recoverable Chloride 8800 400 340 ug/L 2 9056A Total/NA Sulfate 8400 B 400 190 ug/L 2 9056A Total/NA Alkalinity 23000 5000 3700 ug/L 1 SM 2320B Total/NA Total Dissolved Solids 120000 10000 4300 ug/L 1 SM 2540C Total/NA Client Sample ID: Tinsley WSW Lab Sample ID: 500-144127-2 E: Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Bromodichloromethane 14 1.0 0.37 ug/L 1 8260B Total/NA Chloroform 37 2.0 0.37 ug/L 1 8260B Total/NA Dibromochloromethane 6.0 1.0 0.49 ug/L 1 8260B Total/NA Barium 13 2.5 0.73 ug/L 1 6020B Total Recoverable Copper 3.7 B 2.0 0.50 ug/L 1 6020B Total Recoverable Manganese 1.8 J 2.5 0.79 ug/L 1 6020B Total Recoverable Chloride 8300 400 340 ug/L 2 9056A Total/NA Sulfate 8400 B 400 190 ug/L 2 9056A Total/NA Alkalinity 22000 5000 3700 ug/L 1 SM 2320B Total/NA Total Dissolved Solids 66000 10000 4300 ug/L 1 SM 2540C Total/NA Client Sample ID: Hammill WSW Lab Sample ID: 500-144127-3 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Tetrahydrofuran 12 10 1.9 ug/L 1 8260E Total/NA Arsenic 0.68 J 1.0 0.23 ug/L 1 6020B Total Recoverable Barium 38 2.5 0.73 ug/L 1 6020B Total Recoverable Copper 5.1 B 2.0 0.50 ug/L 1 6020B Total Recoverable Iron 210 B 100 47 ug/L 1 6020E Total Recoverable This Detection Summary does not include radiochemical test results. Page 4 of 32 TestAmerica Chicago 7/5/2018 Detection Summary Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW TestAmerica Job ID: 500-144127-1 Client Sample ID: Hammill WSW (Continued) Lab Sample ID: 500-144127-3 Analyte Result Qualifier RL MDL Unit Dil Fac D Method Prep Type Lead 0.32 J 0.50 0.19 ug/L 1 6020B Total Recoverable Manganese 88 2.5 0.79 ug/L 1 6020B Total Recoverable Nickel 0.72 J 2.0 0.63 ug/L 1 6020B Total Recoverable Tin 2.1 J 5.0 1.3 ug/L 1 6020B Total Recoverable Zinc 260 10 6.9 ug/L 1 6020B Total Recoverable Chloride 5600 200 170 ug/L 1 9056A Total/NA Sulfate 310000 B 10000 4800 ug/L 50 9056A Total/NA Alkalinity 93000 5000 3700 ug/L 1 SM 2320B Total/NA Total Dissolved Solids 590000 10000 4300 ug/L 1 SM 2540C Total/NA F This Detection Summary does not include radiochemical test results. TestAmerica Chicago Page 5 of 32 7/5/2018 Method Summary C Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Method Method Description Protocol Laboratory 8260B Volatile Organic Compounds (GC/MS) SW846 TAL CHI 6020B Metals (ICP/MS) SW846 TAL CHI 7470A Mercury (CVAA) SW846 TAL CHI 9056A Anions, Ion Chromatography SW846 TAL CHI SM 2320B Alkalinity SM TAL CHI SM 2540C Solids, Total Dissolved (TDS) SM TAL CHI 3005A Preparation, Total Recoverable or Dissolved Metals SW846 TAL CHI 5030B Purge and Trap SW846 TAL CHI 7470A Preparation, Mercury SW846 TAL CHI Protocol References: SM = "Standard Methods For The Examination Of Water And Wastewater" SW846 ='Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates. Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 TestAmerica Chicago Page 6 of 32 7/5/2018 Sample Summary Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW TestAmerica Job ID: 500-144127-1 Lab Sample ID Client Sample ID Matrix Collected Received 500-144127-1 Gilkerson WSW 500-144127-2 Tinsley WSW 500-144127-3 Hammill WSW Water Water Water 04/19/18 09:30 04/19/18 09:35 04/19/18 09:40 04/20/18 09:00 04/20/18 09:00 04/20/18 09:00 0 TestAmerica Chicago Page 7 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW TestAmerica Job ID: 500-144127-1 Client Sample ID: Gilkerson WSW Lab Sample ID: 500-144127-1 Date Collected: 04/19/18 09:30 Matrix: Water Date Received: 04/20/18 09:00 F Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 05/01/18 11:16 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 05/01/18 11:16 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 05/01/18 11:16 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 05/01/18 11:16 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 05/01/18 11:16 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 05/01/18 11:16 1 1,1-Dichloropropene <0.30 1.0 0.30 ug/L 05/01/18 11:16 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 05/01/18 11:16 1 1,2,4-Trichlorobenzene <0.34 1.0 0.34 ug/L 05/01/18 11:16 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 05/01/18 11:16 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 05/01/18 11:16 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 05/01/18 11:16 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 05/01/18 11:16 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 05/01/18 11:16 1 1,3-Dichlorobenzene <0.40 1.0 0.40 ug/L 05/01/18 11:16 1 1,3-Dichloropropane <0.36 1.0 0.36 ug/L 05/01/18 11:16 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 05/01/18 11:16 1 2,2-Dichloropropane <0.44 1.0 0.44 ug/L 05/01/18 11:16 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 05/01/18 11:16 1 2-Chloro-1,3-butadiene <0.23 1.0 0.23 ug/L 05/01/18 11:16 1 2-Hexanone <1.6 5.0 1.6 ug/L 05/01/18 11:16 1 3-Chloropropene <0.86 2.5 0.86 ug/L 05/01/18 11:16 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 05/01/18 11:16 1 Acetone <1.7 5.0 1.7 ug/L 05/01/18 11:16 1 Acetonitrile <4.2 10 4.2 ug/L 05/01/18 11:16 1 Acrolein <23 100 23 ug/L 05/01/18 11:16 1 Acrylonitrile <4.5 20 4.5 ug/L 05/01/18 11:16 1 Benzene <0.15 0.50 0.15 ug/L 05/01/18 11:16 1 Bromochloromethane <0.43 1.0 0.43 ug/L 05/01/18 11:16 1 Bromodichloromethane 12 1.0 0.37 ug/L 05/01/18 11:16 1 Bromoform 0.62 J 1.0 0.48 ug/L 05/01/18 11:16 1 Bromomethane <0.80 2.0 0.80 ug/L 05/01/18 11:16 1 Carbon disulfide <0.45 2.0 0.45 ug/L 05/01/18 11:16 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 05/01/18 11:16 1 Chlorobenzene <0.39 1.0 0.39 ug/L 05/01/18 11:16 1 Chloroethane <0.51 1.0 0.51 ug/L 05/01/18 11:16 1 Chloroform 31 2.0 0.37 ug/L 05/01/18 11:16 1 Chloromethane <0.32 1.0 0.32 ug/L 05/01/18 11:16 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 05/01/18 11:16 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 05/01/18 11:16 1 Dibromochloromethane 5.5 1.0 0.49 ug/L 05/01/18 11:16 1 Dibromomethane <0.27 1.0 0.27 ug/L 05/01/18 11:16 1 Dichlorodifluoromethane <0.67 2.0 0.67 ug/L 05/01/18 11:16 1 Ethyl methacrylate <0.53 2.5 0.53 ug/L 05/01/18 11:16 1 Ethylbenzene <0.18 0.50 0.18 ug/L 05/01/18 11:16 1 Hexachlorobutadiene <0.45 1.0 0.45 ug/L 05/01/18 11:16 1 lodomethane <0.66 2.5 0.66 ug/L 05/01/18 11:16 1 Isobutyl alcohol <36 100 36 ug/L 05/01/18 11:16 1 Methacrylonitrile <2.5 10 2.5 ug/L 05/01/18 11:16 1 TestAmerica Chicago Page 8 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Client Sample ID: Gilkerson WSW Lab Sample ID: 500-144127-1 Date Collected: 04/19/18 09:30 Matrix: Water Date Received: 04/20/18 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Methyl methacrylate <0.55 2.5 0.55 ug/L 05/01/18 11:16 1 Methylene Chloride <1.6 5.0 1.6 ug/L 05/01/18 11:16 1 Propionitrile <4.8 10 4.8 ug/L 05/01/18 11:16 1 Styrene <0.39 1.0 0.39 ug/L 05/01/18 11:16 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 05/01/18 11:16 1 Tetrahydrofuran <1.9 10 1.9 ug/L 05/01/18 11:16 1 Toluene <0.15 0.50 0.15 ug/L 05/01/18 11:16 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 05/01/18 11:16 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 05/01/18 11:16 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 05/01/18 11:16 1 Trichloroethene <0.16 0.50 0.16 ug/L 05/01/18 11:16 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 05/01/18 11:16 1 Vinyl acetate <0.91 2.0 0.91 ug/L 05/01/18 11:16 1 Vinyl chloride <0.20 1.0 0.20 ug/L 05/01/18 11:16 1 Xylenes, Total <0.22 1.0 0.22 ug/L 05/01/18 11:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 84 75- 126 05101118 11:16 1 4-Bromofluorobenzene (Surr) 112 72 - 124 05101118 11:16 1 Dibromofluoromethane 93 75 - 120 05101118 11:16 1 Toluene-d8 (Surr) 99 75 - 120 05101118 11:16 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/21/1815:25 04/24/1816:04 1 Arsenic <0.23 1.0 0.23 ug/L 04/21/1815:25 04/24/1816:04 1 Barium 14 2.5 0.73 ug/L 04/21/1815:25 04/24/1816:04 1 Beryllium <0.53 1.0 0.53 ug/L 04/21/1815:25 04/24/1816:04 1 Cadmium <0.17 0.50 0.17 ug/L 04/21/1815:25 04/24/1816:04 1 Chromium 1.5 J 5.0 1.1 ug/L 04/21/1815:25 04/24/1816:04 1 Cobalt <0.40 1.0 0.40 ug/L 04/21/1815:25 04/24/1816:04 1 Copper 23 B 2.0 0.50 ug/L 04/21/1815:25 04/24/1816:04 1 Iron 1500 B 100 47 ug/L 04/21/1815:25 04/24/1816:04 1 Lead 7.4 0.50 0.19 ug/L 04/21/1815:25 04/24/1816:04 1 Manganese 28 2.5 0.79 ug/L 04/21/1815:25 04/24/1816:04 1 Nickel 1.1 J 2.0 0.63 ug/L 04/21/1815:25 04/24/1816:04 1 Selenium <0.98 2.5 0.98 ug/L 04/21/1815:25 04/24/1816:04 1 Silver <0.12 0.50 0.12 ug/L 04/21/1815:25 04/24/1816:04 1 Thallium <0.57 2.0 0.57 ug/L 04/21/1815:25 04/24/1816:04 1 Tin <1.3 5.0 1.3 ug/L 04/21/1815:25 04/24/1816:04 1 Vanadium <2.2 5.0 2.2 ug/L 04/21/1815:25 04/24/1816:04 1 Zinc 190 10 6.9 ug/L 04/21/1815:25 04/24/1816:04 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/24/18 12:30 04/25/18 08:54 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 8800 400 340 ug/L 05/03/1816:42 2 TestAmerica Chicago Page 9 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Client Sample ID: Gilkerson WSW Lab Sample ID: 500-144127-1 Date Collected: 04/19/18 09:30 Matrix: Water Date Received: 04/20/18 09:00 General Chemistry (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Sulfate 8400 B 400 190 ug/L 05/03/1816:42 2 Alkalinity 23000 5000 3700 ug/L 04/26/1812:22 1 Total Dissolved Solids 120000 10000 4300 ug/L 04/24/18 06:46 1 F F TestAmerica Chicago Page 10 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW TestAmerica Job ID: 500-144127-1 Client Sample ID: Tinsley WSW Lab Sample ID: 500-144127-2 Date Collected: 04/19/18 09:35 Matrix: Water Date Received: 04/20/18 09:00 F Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 05/01/18 11:46 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 05/01/18 11:46 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 05/01/18 11:46 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 05/01/18 11:46 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 05/01/18 11:46 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 05/01/18 11:46 1 1,1-Dichloropropene <0.30 1.0 0.30 ug/L 05/01/18 11:46 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 05/01/18 11:46 1 1,2,4-Trichlorobenzene <0.34 1.0 0.34 ug/L 05/01/18 11:46 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 05/01/18 11:46 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 05/01/18 11:46 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 05/01/18 11:46 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 05/01/18 11:46 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 05/01/18 11:46 1 1,3-Dichlorobenzene <0.40 1.0 0.40 ug/L 05/01/18 11:46 1 1,3-Dichloropropane <0.36 1.0 0.36 ug/L 05/01/18 11:46 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 05/01/18 11:46 1 2,2-Dichloropropane <0.44 1.0 0.44 ug/L 05/01/18 11:46 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 05/01/18 11:46 1 2-Chloro-1,3-butadiene <0.23 1.0 0.23 ug/L 05/01/18 11:46 1 2-Hexanone <1.6 5.0 1.6 ug/L 05/01/18 11:46 1 3-Chloropropene <0.86 2.5 0.86 ug/L 05/01/18 11:46 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 05/01/18 11:46 1 Acetone <1.7 5.0 1.7 ug/L 05/01/18 11:46 1 Acetonitrile <4.2 10 4.2 ug/L 05/01/18 11:46 1 Acrolein <23 100 23 ug/L 05/01/18 11:46 1 Acrylonitrile <4.5 20 4.5 ug/L 05/01/18 11:46 1 Benzene <0.15 0.50 0.15 ug/L 05/01/18 11:46 1 Bromochloromethane <0.43 1.0 0.43 ug/L 05/01/18 11:46 1 Bromodichloromethane 14 1.0 0.37 ug/L 05/01/18 11:46 1 Bromoform <0.48 1.0 0.48 ug/L 05/01/18 11:46 1 Bromomethane <0.80 2.0 0.80 ug/L 05/01/18 11:46 1 Carbon disulfide <0.45 2.0 0.45 ug/L 05/01/18 11:46 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 05/01/18 11:46 1 Chlorobenzene <0.39 1.0 0.39 ug/L 05/01/18 11:46 1 Chloroethane <0.51 1.0 0.51 ug/L 05/01/18 11:46 1 Chloroform 37 2.0 0.37 ug/L 05/01/18 11:46 1 Chloromethane <0.32 1.0 0.32 ug/L 05/01/18 11:46 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 05/01/18 11:46 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 05/01/18 11:46 1 Dibromochloromethane 6.0 1.0 0.49 ug/L 05/01/18 11:46 1 Dibromomethane <0.27 1.0 0.27 ug/L 05/01/18 11:46 1 Dichlorodifluoromethane <0.67 2.0 0.67 ug/L 05/01/18 11:46 1 Ethyl methacrylate <0.53 2.5 0.53 ug/L 05/01/18 11:46 1 Ethylbenzene <0.18 0.50 0.18 ug/L 05/01/18 11:46 1 Hexachlorobutadiene <0.45 1.0 0.45 ug/L 05/01/18 11:46 1 lodomethane <0.66 2.5 0.66 ug/L 05/01/18 11:46 1 Isobutyl alcohol <36 100 36 ug/L 05/01/18 11:46 1 Methacrylonitrile <2.5 10 2.5 ug/L 05/01/18 11:46 1 TestAmerica Chicago Page 11 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Client Sample ID: Tinsley WSW Lab Sample ID: 500-144127-2 Date Collected: 04/19/18 09:35 Matrix: Water Date Received: 04/20/18 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Methyl methacrylate <0.55 2.5 0.55 ug/L 05/01/18 11:46 1 Methylene Chloride <1.6 5.0 1.6 ug/L 05/01/18 11:46 1 Propionitrile <4.8 10 4.8 ug/L 05/01/18 11:46 1 Styrene <0.39 1.0 0.39 ug/L 05/01/18 11:46 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 05/01/18 11:46 1 Tetrahydrofuran <1.9 10 1.9 ug/L 05/01/18 11:46 1 Toluene <0.15 0.50 0.15 ug/L 05/01/18 11:46 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 05/01/18 11:46 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 05/01/18 11:46 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 05/01/18 11:46 1 Trichloroethene <0.16 0.50 0.16 ug/L 05/01/18 11:46 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 05/01/18 11:46 1 Vinyl acetate <0.91 2.0 0.91 ug/L 05/01/18 11:46 1 Vinyl chloride <0.20 1.0 0.20 ug/L 05/01/18 11:46 1 Xylenes, Total <0.22 1.0 0.22 ug/L 05/01/18 11:46 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 82 75- 126 05101118 11:46 1 4-Bromofluorobenzene (Surr) 113 72 - 124 05101118 11:46 1 Dibromofluoromethane 93 75 - 120 05101118 11:46 1 Toluene-d8 (Surr) 98 75 - 120 05101118 11:46 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/21/1815:25 04/24/1816:08 1 Arsenic <0.23 1.0 0.23 ug/L 04/21/1815:25 04/24/1816:08 1 Barium 13 2.5 0.73 ug/L 04/21/1815:25 04/24/1816:08 1 Beryllium <0.53 1.0 0.53 ug/L 04/21/1815:25 04/24/1816:08 1 Cadmium <0.17 0.50 0.17 ug/L 04/21/1815:25 04/24/1816:08 1 Chromium <1.1 5.0 1.1 ug/L 04/21/1815:25 04/24/1816:08 1 Cobalt <0.40 1.0 0.40 ug/L 04/21/1815:25 04/24/1816:08 1 Copper 3.7 B 2.0 0.50 ug/L 04/21/1815:25 04/24/1816:08 1 Iron <47 100 47 ug/L 04/21/1815:25 04/24/1816:08 1 Lead <0.19 0.50 0.19 ug/L 04/21/1815:25 04/24/1816:08 1 Manganese 1.8 J 2.5 0.79 ug/L 04/21/1815:25 04/24/1816:08 1 Nickel <0.63 2.0 0.63 ug/L 04/21/1815:25 04/24/1816:08 1 Selenium <0.98 2.5 0.98 ug/L 04/21/1815:25 04/24/1816:08 1 Silver <0.12 0.50 0.12 ug/L 04/21/1815:25 04/24/1816:08 1 Thallium <0.57 2.0 0.57 ug/L 04/21/1815:25 04/24/1816:08 1 Tin <1.3 5.0 1.3 ug/L 04/21/1815:25 04/24/1816:08 1 Vanadium <2.2 5.0 2.2 ug/L 04/21/1815:25 04/24/1816:08 1 Zinc <6.9 10 6.9 ug/L 04/21/1815:25 04/24/1816:08 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/24/18 12:30 04/25/18 08:56 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 8300 400 340 ug/L 05/03/1817:20 2 TestAmerica Chicago Page 12 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW TestAmerica Job ID: 500-144127-1 Client Sample ID: Tinsley WSW Lab Sample ID: 500-144127-2 Date Collected: 04/19/18 09:35 Matrix: Water Date Received: 04/20/18 09:00 General Chemistry (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Sulfate 8400 B 400 196 ug/L 05/03/1817:20 2 Alkalinity 22000 5000 3700 ug/L 04/26/1812:32 1 Total Dissolved Solids 66000 10000 4300 ug/L 04/24/18 06:50 1 F F TestAmerica Chicago Page 13 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW TestAmerica Job ID: 500-144127-1 Client Sample ID: Hammill WSW Lab Sample ID: 500-144127-3 Date Collected: 04/19/18 09:40 Matrix: Water Date Received: 04/20/18 09:00 F Method: 8260B - Volatile Organic Compounds (GC/MS) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 05/01/18 12:16 1 1,1,1-Trichloroethane <0.38 1.0 0.38 ug/L 05/01/18 12:16 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 05/01/18 12:16 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 05/01/18 12:16 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 05/01/18 12:16 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 05/01/18 12:16 1 1,1-Dichloropropene <0.30 1.0 0.30 ug/L 05/01/18 12:16 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 05/01/18 12:16 1 1,2,4-Trichlorobenzene <0.34 1.0 0.34 ug/L 05/01/18 12:16 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 05/01/18 12:16 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 05/01/18 12:16 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 05/01/18 12:16 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 05/01/18 12:16 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 05/01/18 12:16 1 1,3-Dichlorobenzene <0.40 1.0 0.40 ug/L 05/01/18 12:16 1 1,3-Dichloropropane <0.36 1.0 0.36 ug/L 05/01/18 12:16 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 05/01/18 12:16 1 2,2-Dichloropropane <0.44 1.0 0.44 ug/L 05/01/18 12:16 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 05/01/18 12:16 1 2-Chloro-1,3-butadiene <0.23 1.0 0.23 ug/L 05/01/18 12:16 1 2-Hexanone <1.6 5.0 1.6 ug/L 05/01/18 12:16 1 3-Chloropropene <0.86 2.5 0.86 ug/L 05/01/18 12:16 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 05/01/18 12:16 1 Acetone <1.7 5.0 1.7 ug/L 05/01/18 12:16 1 Acetonitrile <4.2 10 4.2 ug/L 05/01/18 12:16 1 Acrolein <23 100 23 ug/L 05/01/18 12:16 1 Acrylonitrile <4.5 20 4.5 ug/L 05/01/18 12:16 1 Benzene <0.15 0.50 0.15 ug/L 05/01/18 12:16 1 Bromochloromethane <0.43 1.0 0.43 ug/L 05/01/18 12:16 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 05/01/18 12:16 1 Bromoform <0.48 1.0 0.48 ug/L 05/01/18 12:16 1 Bromomethane <0.80 2.0 0.80 ug/L 05/01/18 12:16 1 Carbon disulfide <0.45 2.0 0.45 ug/L 05/01/18 12:16 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 05/01/18 12:16 1 Chlorobenzene <0.39 1.0 0.39 ug/L 05/01/18 12:16 1 Chloroethane <0.51 1.0 0.51 ug/L 05/01/18 12:16 1 Chloroform <0.37 2.0 0.37 ug/L 05/01/18 12:16 1 Chloromethane <0.32 1.0 0.32 ug/L 05/01/18 12:16 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 05/01/18 12:16 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 05/01/18 12:16 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 05/01/18 12:16 1 Dibromomethane <0.27 1.0 0.27 ug/L 05/01/18 12:16 1 Dichlorodifluoromethane <0.67 2.0 0.67 ug/L 05/01/18 12:16 1 Ethyl methacrylate <0.53 2.5 0.53 ug/L 05/01/18 12:16 1 Ethylbenzene <0.18 0.50 0.18 ug/L 05/01/18 12:16 1 Hexachlorobutadiene <0.45 1.0 0.45 ug/L 05/01/18 12:16 1 lodomethane <0.66 2.5 0.66 ug/L 05/01/18 12:16 1 Isobutyl alcohol <36 100 36 ug/L 05/01/18 12:16 1 Methacrylonitrile <2.5 10 2.5 ug/L 05/01/18 12:16 1 TestAmerica Chicago Page 14 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Client Sample ID: Hammill WSW Lab Sample ID: 500-144127-3 Date Collected: 04/19/18 09:40 Matrix: Water Date Received: 04/20/18 09:00 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Methyl methacrylate <0.55 2.5 0.55 ug/L 05/01/18 12:16 1 Methylene Chloride <1.6 5.0 1.6 ug/L 05/01/18 12:16 1 Propionitrile <4.8 10 4.8 ug/L 05/01/18 12:16 1 Styrene <0.39 1.0 0.39 ug/L 05/01/18 12:16 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 05/01/18 12:16 1 Tetrahydrofuran 12 10 1.9 ug/L 05/01/18 12:16 1 Toluene <0.15 0.50 0.15 ug/L 05/01/18 12:16 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 05/01/18 12:16 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 05/01/18 12:16 1 trans- 1,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 05/01/18 12:16 1 Trichloroethene <0.16 0.50 0.16 ug/L 05/01/18 12:16 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 05/01/18 12:16 1 Vinyl acetate <0.91 2.0 0.91 ug/L 05/01/18 12:16 1 Vinyl chloride <0.20 1.0 0.20 ug/L 05/01/18 12:16 1 Xylenes, Total <0.22 1.0 0.22 ug/L 05/01/18 12:16 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 85 75- 126 05101118 12:16 1 4-Bromofluorobenzene (Surr) 114 72 - 124 05101118 12:16 1 Dibromofluoromethane 95 75 - 120 05101118 12:16 1 Toluene-d8 (Surr) 99 75 - 120 05101118 12:16 1 Method: 6020B - Metals (ICP/MS) - Total Recoverable Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Antimony <1.3 3.0 1.3 ug/L 04/21/1815:25 04/24/1816:11 1 Arsenic 0.68 J 1.0 0.23 ug/L 04/21/1815:25 04/24/1816:11 1 Barium 38 2.5 0.73 ug/L 04/21/1815:25 04/24/1816:11 1 Beryllium <0.53 1.0 0.53 ug/L 04/21/1815:25 04/24/1816:11 1 Cadmium <0.17 0.50 0.17 ug/L 04/21/1815:25 04/24/1816:11 1 Chromium <1.1 5.0 1.1 ug/L 04/21/1815:25 04/24/1816:11 1 Cobalt <0.40 1.0 0.40 ug/L 04/21/1815:25 04/24/1816:11 1 Copper 5.1 B 2.0 0.50 ug/L 04/21/1815:25 04/24/1816:11 1 Iron 210 B 100 47 ug/L 04/21/1815:25 04/24/1816:11 1 Lead 0.32 J 0.50 0.19 ug/L 04/21/1815:25 04/24/1816:11 1 Manganese 88 2.5 0.79 ug/L 04/21/1815:25 04/24/1816:11 1 Nickel 0.72 J 2.0 0.63 ug/L 04/21/1815:25 04/24/1816:11 1 Selenium <0.98 2.5 0.98 ug/L 04/21/1815:25 04/24/1816:11 1 Silver <0.12 0.50 0.12 ug/L 04/21/1815:25 04/24/1816:11 1 Thallium <0.57 2.0 0.57 ug/L 04/21/1815:25 04/24/1816:11 1 Tin 2.1 J 5.0 1.3 ug/L 04/21/1815:25 04/24/1816:11 1 Vanadium <2.2 5.0 2.2 ug/L 04/21/1815:25 04/24/1816:11 1 Zinc 260 10 6.9 ug/L 04/21/1815:25 04/24/1816:11 1 Method: 7470A - Mercury (CVAA) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Mercury <0.098 0.20 0.098 ug/L 04/24/18 12:30 04/25/18 08:58 1 General Chemistry Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chloride 5600 200 170 ug/L 05/03/1817:33 1 TestAmerica Chicago Page 15 of 32 7/5/2018 Client Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Client Sample ID: Hammill WSW Lab Sample ID: 500-144127-3 Date Collected: 04/19/18 09:40 Matrix: Water Date Received: 04/20/18 09:00 General Chemistry (Continued) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Sulfate 310000 B 10000 4800 ug/L 05/04/1812:51 50 Alkalinity 93000 5000 3700 ug/L 04/26/1812:38 1 Total Dissolved Solids 590000 10000 4300 ug/L 04/24/18 06:53 1 F F TestAmerica Chicago Page 16 of 32 7/5/2018 Definitions/Glossary Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Qualifiers GC/MS VOA Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Metals Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. B Compound was found in the blank and sample. General Chemistry Qualifier Qualifier Description B Compound was found in the blank and sample. J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. tt Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Chicago Page 17 of 32 7/5/2018 QC Association Summary Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW GC/MS VOA Analysis Batch: 430055 TestAmerica Job ID: 500-144127-1 Lab Sample ID Client Sample ID Prep Type Matrix Method 500-144127-1 Gilkerson WSW Total/NA Water 8260B 500-144127-2 Tinsley WSW Total/NA Water 8260B 500-144127-3 Hammill WSW Total/NA Water 8260B MB 500-430055/7 Method Blank Total/NA Water 8260B LCS 500-430055/5 Lab Control Sample Total/NA Water 8260B Prep Batch Metals Prep Batch: 428869 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 500-144127-1 Gilkerson WSW Total Recoverable Water 3005A 500-144127-2 Tinsley WSW Total Recoverable Water 3005A 500-144127-3 Hammill WSW Total Recoverable Water 3005A MB 500-428869/1-A Method Blank Total Recoverable Water 3005A LCS 500-428869/2-A Lab Control Sample Total Recoverable Water 3005A Prep Batch: 429180 Lab Sample ID Client Sample ID 500-144127-1 Gilkerson WSW 500-144127-2 Tinsley WSW 500-144127-3 Hammill WSW MB 500-429180/12-A Method Blank LCS 500-429180/13-A Lab Control Sample Analysis Batch: 429330 Prep Type Matrix Method Prep Batch C Total/NA Water 7470A Total/NA Water 7470A Total/NA Water 7470A Total/NA Water 7470A Total/NA Water 7470A Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 500-144127-1 Gilkerson WSW Total Recoverable Water 6020B 428869 500-144127-2 Tinsley WSW Total Recoverable Water 6020B 428869 500-144127-3 Hammill WSW Total Recoverable Water 6020B 428869 MB 500-428869/1-A Method Blank Total Recoverable Water 6020B 428869 LCS 500-428869/2-A Lab Control Sample Total Recoverable Water 6020B 428869 Analysis Batch: 429338 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 500-144127-1 Gilkerson WSW Total/NA Water 7470A 429180 500-144127-2 Tinsley WSW Total/NA Water 7470A 429180 500-144127-3 Hammill WSW Total/NA Water 7470A 429180 MB 500-429180/12-A Method Blank Total/NA Water 7470A 429180 LCS 500-429180/13-A Lab Control Sample Total/NA Water 7470A 429180 General Chemistry Analysis Batch: 429088 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 500-144127-1 Gilkerson WSW Total/NA Water SM 2540C 500-144127-2 Tinsley WSW Total/NA Water SM 2540C 500-144127-3 Hammill WSW Total/NA Water SM 2540C MB 500-429088/1 Method Blank Total/NA Water SM 2540C LCS 500-429088/2 Lab Control Sample Total/NA Water SM 2540C Page 18 of 32 TestAmerica Chicago 7/5/2018 QC Association Summary Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW General Chemistry (Continued) Analysis Batch: 429681 TestAmerica Job ID: 500-144127-1 Lab Sample ID Client Sample ID Prep Type Matrix Method 500-144127-1 Gilkerson WSW Total/NA Water SM 2320B 500-144127-2 Tinsley WSW Total/NA Water SM 2320B 500-144127-3 Hammill WSW Total/NA Water SM 2320B MB 500-429681/3 Method Blank Total/NA Water SM 2320B LCS 500-429681/4 Lab Control Sample Total/NA Water SM 2320B Analysis Batch: 430570 Lab Sample ID Client Sample ID Prep Type Matrix Method 500-144127-1 Gilkerson WSW Total/NA Water 9056A 500-144127-2 Tinsley WSW Total/NA Water 9056A 500-144127-3 Hammill WSW Total/NA Water 9056A MB 500-430570/20 Method Blank Total/NA Water 9056A LCS 500-430570/21 Lab Control Sample Total/NA Water 9056A Analysis Batch: 430780 Prep Batch Prep Batch 0 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 500-144127-3 Hammill WSW Total/NA Water 9056A MB 500-430780/8 Method Blank Total/NA Water 9056A LCS 500-430780/9 Lab Control Sample Total/NA Water 9056A TestAmerica Chicago Page 19 of 32 7/5/2018 Surrogate Summary Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW F TestAmerica Job ID: 500-144127-1 Method: 8260B - Volatile Organic Compounds (GC/MS) Matrix: Water Prep Type: Total/NA Percent Surrogate Recovery (Acceptance Limits) DCA BFB DBFM TOL Lab Sample ID Client Sample ID (75-126) (72-124) (75-120) (75-120) 500-144127-1 Gilkerson WSW 84 112 93 99 500-144127-2 Tinsley WSW 82 113 93 98 500-144127-3 Hammill WSW 85 114 95 99 LCS 500-430055/5 Lab Control Sample 81 112 88 101 MB 500-430055/7 Method Blank 87 111 95 98 Surrogate Legend DCA = 1,2-Dichloroethane-d4 (Surr) BFB = 4-Bromofluorobenzene (Surr) DBFM = Dibromofluoromethane TOL = Toluene-d8 (Surr) TestAmerica Chicago Page 20 of 32 7/5/2018 QC Sample Results C Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Method: 8260B - Volatile Organic Compounds (GC/MS) Lab Sample ID: MB 500-430055/7 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 430055 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,1,1,2-Tetrachloroethane <0.46 1.0 0.46 ug/L 05/01/18 10:46 1 1,1, 1 -Trichloroethane <0.38 1.0 0.38 ug/L 05/01/18 10:46 1 1,1,2,2-Tetrachloroethane <0.40 1.0 0.40 ug/L 05/01/18 10:46 1 1,1,2-Trichloroethane <0.35 1.0 0.35 ug/L 05/01/18 10:46 1 1,1-Dichloroethane <0.41 1.0 0.41 ug/L 05/01/18 10:46 1 1,1-Dichloroethene <0.39 1.0 0.39 ug/L 05/01/18 10:46 1 1,1-Dichloropropene <0.30 1.0 0.30 ug/L 05/01/18 10:46 1 1,2,3-Trichloropropane <0.41 1.0 0.41 ug/L 05/01/18 10:46 1 1,2,4-Trichlorobenzene <0.34 1.0 0.34 ug/L 05/01/18 10:46 1 1,2-Dibromo-3-Chloropropane <2.0 5.0 2.0 ug/L 05/01/18 10:46 1 1,2-Dibromoethane <0.39 1.0 0.39 ug/L 05/01/18 10:46 1 1,2-Dichlorobenzene <0.33 1.0 0.33 ug/L 05/01/18 10:46 1 1,2-Dichloroethane <0.39 1.0 0.39 ug/L 05/01/18 10:46 1 1,2-Dichloropropane <0.43 1.0 0.43 ug/L 05/01/18 10:46 1 1,3-Dichlorobenzene <0.40 1.0 0.40 ug/L 05/01/18 10:46 1 1,3-Dichloropropane <0.36 1.0 0.36 ug/L 05/01/18 10:46 1 1,4-Dichlorobenzene <0.36 1.0 0.36 ug/L 05/01/18 10:46 1 2,2-Dichloropropane <0.44 1.0 0.44 ug/L 05/01/18 10:46 1 2-Butanone (MEK) <2.1 5.0 2.1 ug/L 05/01/18 10:46 1 2-Chloro-1,3-butadiene <0.23 1.0 0.23 ug/L 05/01/18 10:46 1 2-Hexanone <1.6 5.0 1.6 ug/L 05/01/18 10:46 1 3-Chloropropene <0.86 2.5 0.86 ug/L 05/01/18 10:46 1 4-Methyl-2-pentanone (MIBK) <2.2 5.0 2.2 ug/L 05/01/18 10:46 1 Acetone <1.7 5.0 1.7 ug/L 05/01/18 10:46 1 Acetonitrile <4.2 10 4.2 ug/L 05/01/18 10:46 1 Acrolein <23 100 23 ug/L 05/01/18 10:46 1 Acrylonitrile <4.5 20 4.5 ug/L 05/01/18 10:46 1 Benzene <0.15 0.50 0.15 ug/L 05/01/18 10:46 1 Bromochloromethane <0.43 1.0 0.43 ug/L 05/01/18 10:46 1 Bromodichloromethane <0.37 1.0 0.37 ug/L 05/01/18 10:46 1 Bromoform <0.48 1.0 0.48 ug/L 05/01/18 10:46 1 Bromomethane <0.80 2.0 0.80 ug/L 05/01/18 10:46 1 Carbon disulfide <0.45 2.0 0.45 ug/L 05/01/18 10:46 1 Carbon tetrachloride <0.38 1.0 0.38 ug/L 05/01/18 10:46 1 Chlorobenzene <0.39 1.0 0.39 ug/L 05/01/18 10:46 1 Chloroethane <0.51 1.0 0.51 ug/L 05/01/18 10:46 1 Chloroform <0.37 2.0 0.37 ug/L 05/01/18 10:46 1 Chloromethane <0.32 1.0 0.32 ug/L 05/01/18 10:46 1 cis-1,2-Dichloroethene <0.41 1.0 0.41 ug/L 05/01/18 10:46 1 cis-1,3-Dichloropropene <0.42 1.0 0.42 ug/L 05/01/18 10:46 1 Dibromochloromethane <0.49 1.0 0.49 ug/L 05/01/18 10:46 1 Dibromomethane <0.27 1.0 0.27 ug/L 05/01/18 10:46 1 Dichlorodifluoromethane <0.67 2.0 0.67 ug/L 05/01/18 10:46 1 Ethyl methacrylate <0.53 2.5 0.53 ug/L 05/01/18 10:46 1 Ethylbenzene <0.18 0.50 0.18 ug/L 05/01/18 10:46 1 Hexachlorobutadiene <0.45 1.0 0.45 ug/L 05/01/18 10:46 1 lodomethane <0.66 2.5 0.66 ug/L 05/01/18 10:46 1 Isobutyl alcohol <36 100 36 ug/L 05/01/18 10:46 1 TestAmerica Chicago Page 21 of 32 7/5/2018 QC Sample Results Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: MB 500-43005517 Matrix: Water Analysis Batch: 430055 MB MB Analyte Result Qualifier RL MDL Unit Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac Methacrylonitrile <2.5 10 2.5 ug/L 05/01/18 10:46 1 Methyl methacrylate <0.55 2.5 0.55 ug/L 05/01/18 10:46 1 Methylene Chloride <1.6 5.0 1.6 ug/L 05/01/18 10:46 1 Propionitrile <4.8 10 4.8 ug/L 05/01/18 10:46 1 Styrene <0.39 1.0 0.39 ug/L 05/01/18 10:46 1 Tetrachloroethene <0.37 1.0 0.37 ug/L 05/01/18 10:46 1 Tetrahydrofuran <1.9 10 1.9 ug/L 05/01/18 10:46 1 Toluene <0.15 0.50 0.15 ug/L 05/01/18 10:46 1 trans- 1,2-Dichloroethene <0.35 1.0 0.35 ug/L 05/01/18 10:46 1 trans- 1,3-Dichloropropene <0.36 1.0 0.36 ug/L 05/01/18 10:46 1 trans- l,4-Dichloro-2-butene <1.2 5.0 1.2 ug/L 05/01/18 10:46 1 Trichloroethene <0.16 0.50 0.16 ug/L 05/01/18 10:46 1 Trichlorofluoromethane <0.43 1.0 0.43 ug/L 05/01/18 10:46 1 Vinyl acetate <0.91 2.0 0.91 ug/L 05/01/18 10:46 1 Vinyl chloride <0.20 1.0 0.20 ug/L 05/01/18 10:46 1 Xylenes, Total <0.22 1.0 0.22 ug/L 05/01/18 10:46 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 1,2-Dichloroethane-d4 (Surr) 87 75- 126 05101118 10:46 1 4-Bromofluorobenzene (Surr) 111 72 - 124 05101118 10:46 1 Dibromofluoromethane 95 75 - 120 05101118 10:46 1 Toluene-d8 (Surr) 98 75 - 120 05/01/18 10:46 1 Lab Sample ID: LCS 500-430055/5 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 430055 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 1,1,1,2-Tetrachloroethane 50.0 42.7 ug/L 85 70-125 1,1,1-Trichloroethane 50.0 40.5 ug/L 81 70-125 1,1,2,2-Tetrachloroethane 50.0 60.2 ug/L 120 67-127 1,1,2-Trichloroethane 50.0 52.9 ug/L 106 70-122 1,1-Dichloroethane 50.0 41.0 ug/L 82 70-125 1,1-Dichloroethene 50.0 46.3 ug/L 93 67-122 1,1-Dichloropropene 50.0 44.7 ug/L 89 70-121 1,2,3-Trichloropropane 50.0 56.1 ug/L 112 50-133 1,2,4-Trichlorobenzene 50.0 46.7 ug/L 93 66-127 1,2-Dibromo-3-Chloropropane 50.0 50.2 ug/L 100 56-123 1,2-Dibromoethane 50.0 51.4 ug/L 103 70-125 1,2-Dichlorobenzene 50.0 50.1 ug/L 100 70 -125 1,2-Dichloroethane 50.0 39.7 ug/L 79 68 -127 1,2-Dichloropropane 50.0 43.3 ug/L 87 67 -130 1,3-Dichlorobenzene 50.0 49.9 ug/L 100 70 -125 1,3-Dichloropropane 50.0 51.4 ug/L 103 62 -136 1,4-Dichlorobenzene 50.0 48.7 ug/L 97 70 -120 2,2-Dichloropropane 50.0 35.1 ug/L 70 58 -129 2-Butanone (MEK) 50.0 61.5 ug/L 123 53 -141 2-Hexanone 50.0 63.1 ug/L 126 56 -135 TestAmerica Chicago Page 22 of 32 7/5/2018 QC Sample Results Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCS 500-430055/5 Matrix: Water Analysis Batch: 430055 TestAmerica Job ID: 500-144127-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits 4-Methyl-2-pentanone (MIBK) 50.0 60.5 ug/L 121 56-133 Acetone 50.0 68.1 ug/L 136 40 -143 Benzene 50.0 44.7 ug/L 89 70-120 Bromochloromethane 50.0 42.3 ug/L 85 65 -122 Bromodichloromethane 50.0 44.0 ug/L 88 69 -120 Bromoform 50.0 41.3 ug/L 83 56 -132 Bromomethane 50.0 44.2 ug/L 88 40 -130 Carbon disulfide 50.0 44.6 ug/L 89 66 -120 Carbon tetrachloride 50.0 39.2 ug/L 78 65 -122 Chlorobenzene 50.0 48.0 ug/L 96 70 -120 Chloroethane 50.0 39.7 ug/L 79 45 -127 Chloroform 50.0 43.0 ug/L 86 70 -120 Chloromethane 50.0 36.8 ug/L 74 54 -147 cis-1,2-Dichloroethene 50.0 46.3 ug/L 93 70 -125 cis-1,3-Dichloropropene 50.0 47.3 ug/L 95 64 -127 Dibromochloromethane 50.0 45.1 ug/L 90 68 -125 Dibromomethane 50.0 44.4 ug/L 89 70 -120 Dichlorodifluoromethane 50.0 58.2 ug/L 116 40 -150 Ethylbenzene 50.0 51.1 ug/L 102 70 -120 Hexachlorobutadiene 50.0 44.2 ug/L 88 51 -150 lodomethane 50.0 40.4 ug/L 81 61 -136 m&p-Xylene 50.0 51.8 ug/L 104 70 -125 Methylene Chloride 50.0 46.3 ug/L 93 69 -125 o-Xylene 50.0 51.9 ug/L 104 70 -120 Styrene 50.0 51.6 ug/L 103 70 -120 Tetrachloroethene 50.0 43.1 ug/L 86 70 -128 Tetrahydrofuran 100 107 ug/L 107 59 -139 Toluene 50.0 51.7 ug/L 103 70 -125 trans- 1,2-Dichloroethene 50.0 45.9 ug/L 92 70-125 trans- 1,3-Dichloropropene 50.0 46.9 ug/L 94 62 -128 Trichloroethene 50.0 41.8 ug/L 84 70 -125 Trichlorofluoromethane 50.0 42.2 ug/L 84 70 -126 Vinyl acetate 50.0 43.3 ug/L 87 43 -133 Vinyl chloride 50.0 45.9 ug/L 92 64 -126 Xylenes, Total 100 104 ug/L 104 70 -125 LCS LCS Surrogate %Recovery Qualifier Limits 1,2-Dichloroethane-d4 (Surr) 81 75- 126 4-Bromofluorobenzene (Surr) 112 72 - 124 Dibromofluoromethane 88 75 - 120 Toluene-d8 (Surr) 101 75 - 120 TestAmerica Chicago Page 23 of 32 7/5/2018 QC Sample Results Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW Method: 6020B - Metals (ICP/MS) Lab Sample ID: MB 500-428869/1-A Matrix: Water Analysis Batch: 429330 Analyte Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Thallium Tin Vanadium Zinc MB MB Result Qualifier <1.3 <0.23 <0.73 <0.53 <0.17 <1.1 <0.40 0.551 J 89.3 J <0.19 <0.79 <0.63 <0.98 <0.12 <0.57 <1.3 <2.2 <6.9 Lab Sample ID: LCS 500-428869/2-A Matrix: Water Analysis Batch: 429330 TestAmerica Job ID: 500-144127-1 Client Sample ID: Method Blank Prep Type: Total Recoverable Prep Batch: 428869 RL MDL Unit D Prepared Analyzed Dil Fac 3.0 1.3 ug/L 04/21/1815:25 04/24/1815:56 1 1.0 0.23 ug/L 04/21/1815:25 04/24/1815:56 1 2.5 0.73 ug/L 04/21/1815:25 04/24/1815:56 1 1.0 0.53 ug/L 04/21/1815:25 04/24/1815:56 1 0.50 0.17 ug/L 04/21/1815:25 04/24/1815:56 1 5.0 1.1 ug/L 04/21/1815:25 04/24/1815:56 1 1.0 0.40 ug/L 04/21/1815:25 04/24/1815:56 1 2.0 0.50 ug/L 04/21/1815:25 04/24/1815:56 1 100 47 ug/L 04/21/1815:25 04/24/1815:56 1 0.50 0.19 ug/L 04/21/1815:25 04/24/1815:56 1 2.5 0.79 ug/L 04/21/1815:25 04/24/1815:56 1 2.0 0.63 ug/L 04/21/1815:25 04/24/1815:56 1 2.5 0.98 ug/L 04/21/1815:25 04/24/1815:56 1 0.50 0.12 ug/L 04/21/1815:25 04/24/1815:56 1 2.0 0.57 ug/L 04/21/1815:25 04/24/1815:56 1 5.0 1.3 ug/L 04/21/1815:25 04/24/1815:56 1 5.0 2.2 ug/L 04/21/1815:25 04/24/1815:56 1 10 6.9 ug/L 04/21/1815:25 04/24/1815:56 1 Spike LCS LCS Analyte Added Result Qualifier Uni Antimony 500 510 ug/ Arsenic 100 99.2 ug/ Barium 500 515 ug/ Beryllium 50.0 49.4 ug/ Cadmium 50.0 51.8 ug/ Chromium 200 212 ug/ Cobalt 500 527 ug/ Copper 250 261 ug/ Iron 1000 1080 ug/ Lead 100 110 ug/ Manganese 500 523 ug/ Nickel 500 536 ug/ Selenium 100 100 ug/ Silver 50.0 53.0 ug/ Thallium 100 109 ug/ Tin 1000 991 ug/ Vanadium 500 509 ug/ Zinc 500 517 ug/ Client Sample ID: Lab Control Sample Prep Type: Total Recoverable Prep Batch: 428869 %Rec. t D %Rec Limits L 102 80-120 L 99 80-120 L 103 80-120 L 99 80-120 L 104 80-120 L 106 80-120 L 105 80-120 L 104 80-120 L 108 80-120 L 110 80-120 L 105 80-120 L 107 80-120 L 100 80-120 L 106 80-120 L 109 80-120 L 99 80-120 L 102 80-120 L 103 80-120 Li Page 24 of 32 TestAmerica Chicago 7/5/2018 QC Sample Results C Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Method: 7470A - Mercury (CVAA) Lab Sample ID: MB 500-429180/12-A Matrix: Water Analysis Batch: 429338 MB MB Analyte Result Qualifier Mercury <0.098 Lab Sample ID: LCS 500-429180/13-A Matrix: Water Analysis Batch: 429338 Analyte Mercury Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 429180 RL MDL Unit D Prepared Analyzed Dil Fac 0.20 0.098 ug/L 04/24/18 12:30 04/25/18 08:25 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch:429180 Spike LCS LCS %Rec. Added Result Qualifier Unit D %Rec Limits - - - 2.00 1.92 ug/L 96 80-120 Method: 9056A - Anions, Ion Chromatography Lab Sample ID: MB 500-430570/20 Matrix: Water Analysis Batch: 430570 MB MB Analyte Result Qualifier Chloride <170 Sulfate 96.0 J Lab Sample ID: LCS 500-430570/21 Matrix: Water Analysis Batch: 430570 Client Sample ID: Method Blank m Prep Type: Total/NA RL MDL Unit D Prepared Analyzed Dil Fac C 200 170 ug/L 05/03/18 09:44 1 200 95 ug/L 05/03/18 09:44 1 Spike LCS LCS Analyte Added Result Qualifier Chloride 3000 2910 Sulfate 5000 4860 Lab Sample ID: MB 500-430780/8 Matrix: Water Analysis Batch: 430780 MB MB Analyte Result Qualifier Sulfate 107 J Lab Sample ID: LCS 500-430780/9 Matrix: Water Analysis Batch: 430780 Spike Analyte Added Sulfate 5000 Method: SM 2320B - Alkalinity FLab Sample ID: MB 500-429681/3 Matrix: Water Analysis Batch: 429681 MB MB Analyte Result Qualifier Alkalinity <3700 RL 200 RL 5000 MDL Unit 95 ug/L Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec. Unit D %Rec Limits ug/L 97 80 -120 ug/L 97 80 -120 Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 05/04/18 12:25 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS Result Qualifier Unit 4830 ug/L MDL Unit 3700 ug/L %Rec. D %Rec Limits 97 80-120 Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 04/26/18 11:10 1 Page 25 of 32 TestAmerica Chicago 7/5/2018 QC Sample Results Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW Lab Sample ID: LCS 500-429681/4 Matrix: Water Analysis Batch: 429681 Spike Analyte Added Alkalinity 100000 Method: SM 2540C - Solids, Total Dissolved (TDS) Lab Sample ID: MB 500-429088/1 Matrix: Water Analysis Batch: 429088 MB MB Analyte Result Qualifier RL Total Dissolved Solids <4300 10000 Lab Sample ID: LCS 500-429088/2 Matrix: Water Analysis Batch: 429088 F TestAmerica Job ID: 500-144127-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS %Rec. Result Qualifier Unit D %Rec Limits 104000 ug/L 104 85-115 Client Sample ID: Method Blank Prep Type: Total/NA F MDL Unit D Prepared Analyzed Dil Fac 4300 ug/L 04/24/18 06:02 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits Total Dissolved Solids 250000 282000 ug/L 113 80 -120 TestAmerica Chicago Page 26 of 32 7/5/2018 Lab Chronicle Client: Civil & Environmental Consultants Inc Project/Site: NC North Mecklenburg Landfill - WSW Client Sample ID: Gilkerson WSW Date Collected: 04/19/18 09:30 Date Received: 04/20/18 09:00 Batch Batch Prep Type Type Method Run Total/NA Analysis 8260B Total Recoverable Prep 3005A Total Recoverable Analysis 6020B Total/NA Prep 7470A Total/NA Analysis 7470A Total/NA Analysis 9056A Total/NA Analysis SM 2320B Total/NA Analysis SM 2540C Client Sample ID: Tinsley WSW Date Collected: 04/19/18 09:35 Date Received: 04/20/18 09:00 TestAmerica Job ID: 500-144127-1 Lab Sample ID: 500-144127-1 Matrix: Water Dilution Batch Prepared Factor Number or Analyzed Analyst Lab 1 430055 05/01/18 11:16 PMF TAL CHI 428869 04/21/18 15:25 BDE TAL CHI 1 429330 04/24/18 16:04 FXG TAL CHI 429180 04/24/18 12:30 EEN TAL CHI 1 429338 04/25/18 08:54 EEN TAL CHI 2 430570 05/03/18 16:42 EAT TAL CHI 1 429681 04/26/18 12:22 SMO TAL CHI 1 429088 04/24/18 06:46 CLB TAL CHI Lab Sample ID: 500-144127-2 Matrix: Water Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Lab Total/NA Analysis 8260B 1 430055 05/01/18 11:46 PMF TAL CHI Total Recoverable Prep 3005A 428869 04/21/18 15:25 BDE TAL CHI Total Recoverable Analysis 6020B 1 429330 04/24/18 16:08 FXG TAL CHI Total/NA Prep 7470A 429180 04/24/18 12:30 EEN TAL CHI Total/NA Analysis 7470A 1 429338 04/25/18 08:56 EEN TAL CHI Total/NA Analysis 9056A 2 430570 05/03/18 17:20 EAT TAL CHI Total/NA Analysis SM 2320B 1 429681 04/26/18 12:32 SMO TAL CHI Total/NA Analysis SM 2540C 1 429088 04/24/18 06:50 CLB TAL CHI Client Sample ID: Hammill WSW Lab Sample ID: 500-144127-3 Date Collected: 04/19/18 09:40 Matrix: Water Date Received: 04/20/18 09:00 Prep Type Batch Type Batch Method Dilution Run Factor Batch Number Prepared or Analyzed Analyst Total/NA Analysis 8260B 1 430055 05/01/1812:16 PMF Total Recoverable Prep 3005A 428869 04/21/18 15:25 BDE Total Recoverable Analysis 6020E 1 429330 04/24/18 16:11 FXG Total/NA Prep 7470A 429180 04/24/18 12:30 EEN Total/NA Analysis 7470A 1 429338 04/25/18 08:58 EEN Total/NA Analysis 9056A 1 430570 05/03/1817:33 EAT Total/NA Analysis 9056A 50 430780 05/04/1812:51 EAT Total/NA Analysis SM 2320B 1 429681 04/26/18 12:38 SMO Total/NA Analysis SM 2540C 1 429088 04/24/18 06:53 CLB Laboratory References: TAL CHI = TestAmerica Chicago, 2417 Bond Street, University Park, IL 60484, TEL (708)534-5200 Lab TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI TAL CHI Page 27 of 32 TestAmerica Chicago 7/5/2018 Accreditation/Certification Summary C Client: Civil & Environmental Consultants Inc TestAmerica Job ID: 500-144127-1 Project/Site: NC North Mecklenburg Landfill - WSW Laboratory: TestAmerica Chicago Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program EPA Region Identification Number Expiration Date North Carolina (WW/SW) State Program 4 291 12-31-18 The following analytes are included in this report, but accreditation/certification is not offered by the governing authority: Analysis Method Prep Method Matrix Analyte 8260E Water trans-1,4-Dichloro-2-butene TestAmerica Chicago Page 28 of 32 7/5/2018 5 C B co ID TestAmerica Chicago 2417 Bond Street University Park, IL 60484 Phone (708) 534-5200 Fax (708) 534-5211 Chain of Custody Record ` � I � Il l illl 191 �i ll Client Information Sampler: Lab PM: Kintz, Robin M Carrier Tracking No(s) COC No: 500-61784-29582.1 Client Contact: Mr. Ed Stephens Phone: E-Mail: robin.kintz@testamericalnc.com Page: a� y,. ,f Page 1 of 1 7(5G�� P Company: Civil & Environmental Consultants Inc Analysis Requested Job #: I �� Address: 1900 Center Park Drive Suite A Due Date Requested: o ? �" 't lG r ,rr ��:5 ;e:=, ;` z �i c N F + w a a v v > m o N co N N .' f 500-144127 COC -_ 3 19 r° Preservation Codes: A - HCL M - Hexane 6 - NaOH N - Noge C - Zn Acetate 0 - AsNaO2 D - Nitric Acid P - Na204S E-NaHSO4 Q-Na2SO3 F - McOH R - Na2S203 G - Amchlor S - H2SO4 H-Ascorbic Acid T- TSPDodecahydrate I - Ice U- Acetone J - DI Water V - MCAA K - EDTA W - pH 4-5 L - EDA Z - other (specify) Other: City: Charlotte TAT Requested (days): State, Zip: NC,28217 Phone: 855-859-9932(Tel) PO #: Purchase0rdernotrequired Email: Y DI= ettephens@cecino.com WO#: Project Name: NC North Mecklenburg Landfill Project #: 50013286 Site: SSOW#: Sample identification Sample Date Sample Time Sample Type (C=comp, G= rab) Matrix (w=water, s=:mia, o=wesremn, eT=TISSue,A=All Special Instructions/Note: Pr�.�XXD A , N , Q� I %N Water X 1�As�� Water X t. I �U' i 1 YV 1�� Vl Water X �G�t�%V1.1^G- Possible Hazard Identification = Non -Hazard = Flammable 'ft-Irritant Poison B Unknown Radiological Sample Disposal (A fee may be assessed if samples are retained longer than 1 month) Return To Client Disposal By Lab Archive For Months Deliverable Requested: I, II, III, IV, O116(specify) Special Instructions/QC Requirements: Empty Kit Relinquish y: Date: Time: Method of shipment: Relinquished by: Dateime: 3 ,3panys !/Rece d y: n Da :om Com Relinquished b Date/Time: Company RboflW by: Date/Time: Company Relinquished by: Dale/rime: Company Received by: Date/rime: Company Custody Seals Intact: A Yes A No Custody Seal No.: : �p Cooler Temperature(s) eC and Other Remarks__&A_= "I 0 Ver:08/04/2016 71014018 cl ry LZl VI 04 ORIGIN ID:PNVA (678) 866-9981 MATT GINTHER CIVIL ENTER PARK DR 1900 CENTER PARK DR STE A CHARLOTTE, NO 28217 UNITED STATES US 10 TEST AMERICA CHICAGO 2417 BOND ST SHIP DATE 19APR18 ACTWGT: 27.80 LB CAD: 006994797/SSFE1822 DIMS: 20x11x13 IN BILL THIRD PARTY a 03 UNIVERSITY PARK IL 60466 4708 834-6200 REF. -- POo DEP T' .III IIIIIIIII IIIIIIII I I IIII III I IIIIII II II'I I III Fed Ex Express a ilk o FRI - 20 APR 3:OOP TRK. 7g05 9593 5514 -02D 1 STANDARD OVERNIGHT NA JOTA IL-u60466 0RD 500-144127 Waybill Page 30 of 32 7/5/2018 TestAmerica THE LEADER IN ENVIRONMENTAL TESTING 2417 Bond Street, University Park, IL 60484 Phone: 708.534.5200 Fax: 708,534.5211 (optional) (optional) Report To Bill TO Contact: 1 5�-,aJ Contact: - Company: Il%le, , SDI MVvlr'ty`R Company: Address: 6.7 (or 2. V a 'Q 1r'Du orl WJ Address: Address: SQ,%el Ah- U-c- t �.1i1° y� g. Address: Phone: 'Itav - Phone: Fax: Fax: t:_�Aeil•�a.n'..i4. �.. � N.m _„ ivI']aiwa. D(,R/Qeforonnoft rX .7 '7'i �r�1"7 Chain of /Custody Record Lab Job #: ✓ �/� � � � Z 6. Chain of Custody Number: Page of Temperature °C of Cooler: Client Client Project # Preservative Preservative Key 1. HCL, Cool to 41 Project Name P iw Parameter t I� V' �' •— !� 2. H2SO4, Cool to 4° 3. HNO3, Cool to 41 4. NaOH, Cool to4° 5. NaOH/Zn, Cool to 41 NaHSO4 6. Cool to 4° 7. 8. None 9.Other Project Location/State Lab Project # Sampler Lab pM_ o 00 00 Sample ID P Sampling o � Comments Date Time c®7Fkke fb 'F%�5f, q. i f&•lg �Q 1 uw5 X X r r■ 500-14025 COC Turnaround Time Required (Business Days) Sample Disposal 1 Day _ 2 Days _ 5 Days _ 7 Days -k 10 Days _ 15 Days Other 1:1 Return to Client ❑ Disposal by Lab ❑ Archive for Months (A fee may be assessed if samples are retained longer than 1 month) � Requested Due Date 5t.. / Bi Relinquished By Company Date Time niiir t-Irti�/ Prih Received By S2 / Comperry ,� A , ' Date ,_ A J� ,� �L��°� f'-- Time_ _ A �� 14/YA' Relinquished By Companyf Date Time Received By Ymparly Date Time Relinquished By Company Date Time Received By Company Data Time Matrix Key Client Comments Lab Comments: WW - Wastewater SE - Sediment -� Ahris CK{ �} } (� j W-Water s0-Soil S - Soil L - Leachate SL - Sludge WI - Wipe - `�t �e M �a9tS� c,Lnr+ uAn 9 w` !(J trte eaP s MS - Miscellaneous DW - Drinking Water OL- Oil 0 - Other A-Alr Lab Courier Shipped I W ?' l6v1 '� Hand Delivered n 0 n Page 31 of 32 TAL-4124-5?/J?2O18 Client: Civil & Environmental Consultants Inc Login Number: 144127 List Number: 1 Creator: Sanchez, Ariel M Question Login Sample Receipt Checklist Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey True meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A 1.9 Job Number: 500-144127-1 List Source: TestAmerica Chicago TestAmerica Chicago Page 32 of 32 7/5/2018