HomeMy WebLinkAbout17038_Goodyear_Tryon Place Soil and Soil Gas Summary Report 20180517
SOIL AND SOIL GAS SAMPLING REPORT
FORMER GOODYEAR SERVICE CENTER
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
BROWNFIELDS PROJECT No. 17038-13-060
ECS PROJECT NO. 49.5350
PREPARED FOR
CRESCENT SOUTH TRYON, LLC
MAY 17, 2018
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
1
TABLE OF CONTENTS
1.0 PROJECT INFORMATION ................................................................................................... 2
2.0 PREVIOUS INVESTIGATIONS ............................................................................................. 2
3.0 PROPOSED DEVELOPMENT ......................................................................................... 2
4.0 OBJECTIVE OF THE WORKPLAN ....................................................................................... 2
5.0 SAMPLE COLLECTION ........................................................................................................ 3
5.1 Soil Gas ............................................................................................................................ 3
5.2 Soil Samples ..................................................................................................................... 5
6.0 RESULTS ............................................................................................................................. 6
6.1 Soil Gas Analysis ............................................................................................................. 6
6.2 Soil Sample Analysis ........................................................................................................ 8
7.0 CONCLUSIONS .................................................................................................................... 9
FIGURES
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Preliminary Site Development Plan
Figure 4 Preliminary Site Development Plan with Sample Locations
TABLES
Table 1 Soil Gas Sample Results
Table 2 Soil Sample Results
APPENDICES
Appendix A Brownfields Survey Plat
Appendix B Exhibit C – Summary of Soil and Groundwater Contaminants
Appendix C Soil Gas Sample Laboratory Report
Appendix D Risk Calculators
Appendix E Soil Sample Laboratory Report
Appendix F Soil Gas Data Sheets
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
2
1.0 PROJECT INFORMATION
The site is currently comprised of four parcels identified as Mecklenburg Parcel ID Nos.
12512105, 12512103, 12512102, and 12512101 located in Charlotte, Mecklenburg County,
North Carolina. The parcels included in the Brownfields site are shown on Exhibit B – Draft
Survey Plat included as Appendix A. The four parcels together total approximately 3.5 acres
and are each owned by 601 South Tryon, LLC. The site was formerly developed with a parking
lot and three buildings; the Former Goodyear Service Center, a 27,000 square foot office
building, and a 45,000 square foot office building. These improvements have been demolished
in connection with the redevelopment of the property.
The location of the site is shown on Figures 1 and 2.
2.0 PREVIOUS INVESTIGATIONS
ECS conducted a soil and groundwater assessment of the Former Goodyear Service Center
property in October/November 2013. ECS also conducted an assessment of the former gasoline
station and former automobile dealership on the north side of the site along Tryon Street in
March 2014. Assessment activities included the collection of soil and groundwater samples to
evaluate the extent of contamination identified in the previous assessments. Arsenic, chromium
VI, and several poly-aromatic hydrocarbons (PAHs) were detected above the
commercial/industrial Inactive Hazardous Sites Branch’s Preliminary Soil Remediation Goals
(PSRGs). The results are summarized in Exhibit C of the Brownfields Agreement (Appendix B).
3.0 PROPOSED DEVELOPMENT
The redevelopment is anticipated to include an office tower with ground floor retail along South
Tryon Street, a hotel along Stonewall Street, a courtyard at the corner of Tryon and Stonewall
Streets, a multi-level parking deck across the balance of the site, and potentially multi-family
residential (See Figure 3).
4.0 OBJECTIVE OF THE WORKPLAN
The objective of the work plan was to determine if the previously detected tetrachloroethylene
(PCE) in the groundwater is creating a vapor intrusion concern for those areas of the future site
development that will be built slab on grade and to determine if the soil which has previously not
been analyzed and will be excavated as part of the future site development is impacted with
volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), and/or RCRA
metals. The soil gas and soil sampling was conducted in general accordance with the North
Carolina Division of Waste Management’s (NCDWM) Vapor Intrusion Guidance (April 2014) and
the NCDWM Inactive Hazardous Site Program’s Guidelines for Assessment and Cleanup
(October 2015). The work plan was approved by the Brownfields’ Manager on December 8,
2017.
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
3
5.0 SAMPLE COLLECTION
5.1 Soil Gas – October 2017 Sample Event
Two portions of the site are proposed to have slab on grade buildings. The proposed slabs are
anticipated to be close to the existing grade. Therefore, on October 15, 2017, ECS collected soil
gas samples from four locations within the proposed footprint of each space. Four exterior soil gas
samples were collected from a depth of 5 feet below grade on the northwest portion of the site
where the office tower/retail will be located. One sub-slab soil gas sample was collected from within
the current structure on the southeast portion of the site along with three exterior soil gas samples
where the hotel is proposed to be located. The approximate locations of the samples are shown on
Figure 4. In the approved work plan, ECS proposed using probe material and Summa canisters
supplied from H&P Mobile Laboratories (H&P); however, H&P was not able to provide the
materials in a timely manner, so ECS used in-house sampling materials and ordered the Summa
canisters from Con-Test Analytical Laboratory.
The borings for the exterior soil gas samples were created by driving a 2-inch O.D direct push
sampler to a depth of 5 feet below the ground surface (bgs) on October 14, 2017. The soil
collected in the macro core sampler was screened in the field with a photo-ionization detector
(PID). Once the boring reached termination depth of 5 feet, a soil gas probe consisting of a five
foot section of decontaminated ¼ O.D. stainless steel tube and stainless steel Swag-Lok fittings
and valve was lowered into the boring. Approximately one foot of clean coarse sand was
placed around the base of the probe. A seal consisting of three feet of bentonite powder was
hydrated with distilled water. The soil gas probe was allowed to stabilize for a minimum of four
hours before the soil gas sample was collected.
The interior sub-slab vapor sample was collected by drilling a 3/8-inch diameter hole through the
concrete slab of the current onsite structure and installing a soil gas probe consisting of
dedicated ¼ O.D. polyethylene tubing and stainless Swag-Lok fittings and valve through the
slab and approximately 2 inches into the under lying gravel stone base. Sand filled the boring to
approximately two inches above the end of the tubing and the remainder of the boring was filled
with bentonite powder and hydrated.
A dedicated syringe was used at each sample location and connected to the tubing to purge the
tubing. Three volumes of the tubing were purged prior to sample collection. Following purging,
the tubing was connected to a 400 ml Summa canister, which was used to collect the sample.
The Summa canister was fitted with a flow regulator. The flow rate for both purging and sample
collection was 0.2 liters per minute. The pressure in the canister was recorded before and after
sample collection. The purge volume, sample collection time, shut-in test results, and canister
vacuum readings prior to and after collection are summarized on the Soil Gas Field Sampling
Form, included in Appendix F.
The probes were removed and the holes filled cement grout following sample collection.
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
4
Leak Detection
Prior to collecting the soil and sub-slab vapor samples, laboratory grade helium gas was used
as a quality assurance control measure to confirm the integrity of the probe seal at each sample
location. A plastic cylinder (approximately 1.75 quarts) was placed and sealed over the
sampling point and purged with laboratory grade helium. The probe point tubing and tracer gas
tubing was placed through the cylinder wall via rubber grommets. The cylinder was placed on a
4-inch rubber gasket and held securely to the slab with a heavy weight. During the purging
stage, the cylinder was flooded with laboratory grade helium via the hose placed through the
cylinder wall. A Model MGD-2002 Multi-Gas Leak detector or similar was connected to the
probe tube and the air stream being purged was measured for helium. A helium concentration
of less than five percent helium was considered acceptable. If concentrations greater than five
percent helium were measured, the probe tube seal was reseated and the leak detection
process was repeated. The results of the helium field check are summarized on the Soil Gas
Field Sampling Form included in Appendix F.
Sample Analysis
Following sample collection, the canisters were labeled and maintained under chain-of-custody
protocol until delivered to Con-Test Analytical Laboratory in East Longmeadow, Massachusetts.
A Chain-of-Custody document was utilized throughout the collection and transportation of the
samples. Each sample was analyzed for the full list of VOCs using EPA Method TO-15. The
results were reported below risk screening levels and J flags were be reported.
Quality Control
One duplicate sample (DUP) of sample SG-6 was collected and analyzed for the same
compounds using EPA Method TO-15.
5.2 Soil Gas – January 2018 Sample Event
Following review of the initial results, the Brownfields Project Manager requested additional soil gas
samples be collected along the South Tryon Street portion of the site (replicate samples SG-1R
through SG-4R). On January 30, 2018, ECS collected samples from four locations within the
proposed footprint of the office building located along South Tryon Street. The approximate
locations of the samples are shown on Figure 4. Per the approved work plan, ECS used probe
material and Summa canisters supplied from H&P Mobile Laboratories (H&P).
The borings for the exterior soil gas samples were advanced using a decontaminated 2-inch
O.D. hand auger to a depth of 5 feet below the ground surface (bgs). The soil collected from
the hand auger was screened in the field with a photo-ionization detector (PID). Once the
boring reached termination depth, a sample probe consisting of dedicated Nylafow tubing and
air stone was lowered into the boring. A seal consisting of three feet of bentonite powder was
hydrated with distilled water. The soil gas probe was allowed to stabilize for a minimum of 24
hours before the soil gas sample was collected.
A dedicated syringe was used at each sample location and connected to the tubing to purge the
tubing. Three volumes of the tubing were purged prior to sample collection. Following purging,
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
5
the tubing was connected to a 1 liter Summa canister, which was used to collect the sample.
The Summa canister was fitted with a flow regulator. The flow rate for both purging and sample
collection was 0.2 liters per minute. The pressure in the canister was recorded before and after
sample collection. The purge volume, sample collection time, shut-in test results, and canister
vacuum readings prior to and after collection are summarized on the Soil Gas Field Sampling
Form, included in Appendix F.
On the day of the sampling, the weather was clear and temperature was in the mid-40s F.
The probes were removed and the holes filled with cement grout following sample collection.
Leak Detection
Prior to collecting the exterior soil gas samples, laboratory grade helium gas was used as a
quality assurance control measure to confirm the integrity of the probe seal at each sample
location. A plastic cylinder (approximately 1.75 quarts) was placed and sealed over the
sampling point and purged with laboratory grade helium. The probe point tubing and tracer gas
tubing was placed through the cylinder wall via rubber grommets. The cylinder was placed on a
4-inch rubber gasket and held securely to the slab with a heavy weight. During the purging
stage, the cylinder was flooded with laboratory grade helium via the hose placed through the
cylinder wall. A Model MGD-2002 Multi-Gas Leak detector or similar was connected to the
probe tube and the air stream being purged was measured for helium. A helium concentration
of less than five percent helium was considered acceptable. If concentrations greater than five
percent helium were measured, the probe tube seal was reseated and the leak detection
process was repeated. The results of the helium field check are summarized on the Soil Gas
Field Sampling Form included in Appendix F
Sample Analysis
Following sample collection, the canisters were labeled and maintained under chain-of-custody
until delivered to H&P Mobile Geochemistry Inc. in Carlsbad, California. A Chain-of-Custody
document was utilized throughout the collection and transportation of the samples. Each
sample was analyzed for the full list of VOCs using EPA Method TO-15. The results were
reported below risk screening levels and J flags were be reported.
Quality Control
One duplicate sample (DUP-R) of sample SG-1R was collected and analyzed for the same
compounds using EPA Method TO-15.
5.3 Soil Samples
ECS proposed collecting soil samples in the areas of future redevelopment/soil disturbance
where samples have not previously been collected (See Figure 5 redline area). The anticipated
depth to top of partially weathered rock; i.e. residuum, was 15 to 20 feet. The accessible areas
of the site were separated into seven sections and four borings were advanced in each section.
Twenty-eight (28) soil borings were advanced to a depth of 15 to 17 feet or direct-push
refusal/top of partially weathered rock. Samples were to be collected from shallow depths
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
6
(approximately 5 feet deep) and deeper depths in each boring (approximately 10 to 15 feet). As
such, ECS expected to collect up to 56 grab soil samples for analysis of VOCs, two samples
from each boring, and up to fourteen (14) composite samples for SVOCs and total RCRA
metals by compositing the shallow and deep soil samples from each boring in each of the seven
quadrants.
On October 14 and 15, 2017, ECS contracted with a North Carolina licensed drilling contractor to
drill the soil borings using direct push technology. The soil samples were classified in the field by
an ECS professional and screened for volatile organic vapors using a PID. The work plan
proposed collecting samples from a shallow depth (5 feet) and a deeper depth (between 10 and
15 feet) in each boring. However, the direct push rig encountered probe refusal at a depth of 5
feet in Area 4, so the samples were only collected from the bottom of the boring. The deeper
samples varied across the site, ranging in depths between 9 and 17 feet below grade. As such,
48 grab samples were collected and analyzed for VOCs using EPA Method 8260. Thirteen (13)
composite samples were analyzed for SVOCs using EPA Method 8270 and total RCRA metals
by EPA Methods 6010/7470/7471.
Two soil samples were also collected from the Goodyear portion of the site for disposal soil
profiling purposes (GP-1 and GP-2). The samples were analyzed for total petroleum
hydrocarbons using EPA Method 8045. The locations of the boring are shown on Figure 4.
Quality Control
One duplicate sample (SB-DUP) of sample SB2-2S was collected and analyzed for the same
compounds.
Once the samples were collected, the drilling contractor properly abandoned the borings.
6.0 RESULTS
6.1 Soil Gas Analysis – October 2017 Sample Event
On the day of the sampling, the weather was clear and temperature was in the mid to upper
50s. The results of the helium field check did not detect helium above 1 percent in the samples.
The shut in test did not detect breaches in the sample train, the PID did not detect organic
vapors above background, and there was no visual evidence of staining. Though eight of the
canister vacuums read zero in the field, the lab measured vacuums upon arrival. One of the
canisters (SG-1) still had vacuum upon sample completion, but read zero upon receipt by the
lab. This sample is considered invalid because it was possible contaminants were introduced
into the sample in transit to the laboratory. The results are summarized on the Soil Gas
Sampling Form, included in Appendix F.
Laboratory analysis of the eight soil gas samples and the duplicate (DUP) sample detected
tetrachloroethene (PCE) at concentrations ranging from 560 ug/m3 (SG-7) to 34,000 ug/m3
(DUP), which is above the Residential Vapor Intrusion Screening Level (VISL) of 278 ug/m3.
PCE was detected in the soil gas samples collected from SG-2, SG-6, and DUP at
concentrations above the Industrial VISL of 3,500 ug/m3. Trichloroethylene (TCE) was detected
in the samples collected from SG-1 through SG-6, SG-8, and DUP at concentrations ranging
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
7
from 18 ug/m3 (SG-1) to 350 ug/m3 (DUP) which is above the Residential VISL of 13.9 ug/m3.
TCE was detected in the samples collected from SG-6 and DUP at concentrations above the
Industrial VISL of 175 ug/m3. Ethyl Acetate was detected in the sample collected from SG-8 at a
concentration of 1,600 ug/m3, which is above the Residential VISL of 487 ug/m3 but below the
Industrial VISL of 6,130 ug/m3.
Various other VOCs were detected above the laboratory reporting limits and detection limits in
the samples, but at concentrations below their respective Residential VISLs.
Quality Control
One duplicate sample (DUP) was collected from SG-6 and analyzed for the same compounds
using EPA Method TO-15. The compounds detected in the duplicate sample were similar to
those detected in SG-6 and at similar concentrations.
The results are summarized in Table 1 and the laboratory report is included as Appendix C.
6.1 Soil Gas Analysis - January 2018 Sample Event
On the day of the sampling, the weather was clear and temperature was in the mid-40s F. The
results of the helium field check did not detect helium above one percent in the samples. The
shut in test did not detect breaches in the sample train. The PID did not detect organic vapors
above background and there was no visual evidence of staining. Each of the canisters still had
vacuum and arrived at the laboratory under similar vacuum indicating no loss of vacuum in
transit. The results are summarized on the Soil Gas Sampling Form, included in Appendix F.
Laboratory analysis of the four soil gas samples (SG-1R through SG-4R) detected various
VOCs above the laboratory reporting limits and detection limits in the samples, but at
concentrations below their respective Residential VISLs. The reporting limit for
hexachlorobutadiene is above the Residential VISL, but below the Non-residential VISL.
Quality Control
One duplicate sample (DUP-R) was collected from SG-1R and analyzed for the same
compounds using EPA Method TO-15. The compounds detected in the duplicate sample were
similar to those detected in SG-1R and at similar concentrations.
The results are summarized in Table 1 and the laboratory report is included as Appendix C.
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
8
Risk Calculators
The North Carolina Department of Environmental Quality Risk Calculator (August 2016) was
used on the October 2017 soil gas results from each soil gas sample location (the duplicate
sample (DUP) results were used instead of the SG-6 results, as they were generally a higher
concentration and therefore more conservative). Each constituent was placed in the calculator
(J values were put in as the estimated concentration). The vapor intrusion calculator was run
for resident and non-resident worker at each location. The Brownfields Project Manager also
ran a combined sample scenario where the data from the four samples collected under each
proposed building was included together in the risk calculator.
The calculators determined the vapor intrusion risk was exceeded for a resident at each of the
sample locations in the area of the proposed hotel except SG-7. Both the residence and non-
resident worker vapor intrusion risk was exceeded a SG-6/DUP. The combined risk calculator
also determined the risk was exceeded for the proposed hotel.
The remaining samples did not exceed non-resident worker vapor risk nor did the combined risk
calculator. The Summary of Risk Assessment Output sheets for each location and the combined
buildings are included in Appendix D.
Risk calculators were not used with respect to the soil gas results from the January 2018
sampling event, since no samples collected demonstrated soil gas exceeding residential
concentrations.
6.2 Soil Sample Analysis
Laboratory analysis of the shallow and deep soil samples did not detect VOCs at concentrations
above the laboratory reporting limit.
Laboratory analysis of the composite samples SB4-S, SB5-S, SB6-S, and SB7-S detected
benzo(a)pyrene at concentrations ranging from an estimated concentration of 0.14 mg/kg (SB7-
S) to 0.67 mg/kg (SB6-S) which are above the Residential Use Health-Based PSRG, but below
the Industrial Health-Based PSRG of 2.1 mg/kg.
Laboratory analysis of 12 of the 13 composite samples detected arsenic at concentrations
above the Residential Use Health-Based PSRG of 0.68 mg/kg. Arsenic was detected in SB4-S
at a concentration of 30 mg/kg, which is above the Industrial Health-Based PSRG of 3.0 mg/kg.
The remaining samples likely reflect naturally occurring concentrations of arsenic.
Various other metals and SVOCs were detected at concentrations above the laboratory
reporting limit but below the Residential Health-based PSRGs.
The TPH analysis detected diesel range TPH above the NCDEQ’s Station Action Level of 100
ppm.
A summary of the soil sample analytical results in included as Table 2 and the laboratory report
is included as Appendix E.
Soil and Soil Gas Sampling Report
Former Goodyear Service Center
Brownfields Project No. 17038-13-060
ECS Project No. 49-5350
May 17, 2018
9
7.0 CONCLUSIONS
Based on the results of the soil and soil gas assessment of the site, ECS has the following
conclusion:
The soil on the site needs to be handled and managed/disposed/reused in accordance
with the approved Environmental Management Plan (EMP).
Soil gas concentrations collected in the samples within the proposed hotel footprint on
October 15, 2017 documented exceedances of screening levels for residential and non-
resident worker risks. Soil gas concentrations collected in the samples collected on
January 31, 2018 did not exceed residential screening levels. The observed results in
both events are consistent with levels found throughout Uptown Charlotte.
Based on DWM’s Vapor Intrusion Guidance, vapor mitigation is not necessary under the
retail/office tower development proposed for the South Tryon Street portion of the
redevelopment. Vapor intrusion risk calculators indicate that a vapor mitigation system
will be needed under the hotel development proposed for the Stonewall Street portion of
the site.
FIGURES
FIGURE 1
SITE LOCATION MAP
FORMER GOODYEAR SERVICE CENTER
BROWNFIELDS PROJECT No. 17038-13-060
CHARLOTTE, MECKLENBURG COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-5350
SOURCE:
USGS TOPOGRAPHIC MAP:
CHARLOTTE EAST, DATED 1967
PHOTOREVISED 1988
NORTH CAROLINA QUADRANGLE
SCALE: 1” = 2,000’
SITE
LEGEND
1 – Former Charlotte Observer
2 – Duke Energy Building
3 – Harvey B. Gant Building
4 – Charlotte Convention Center
5 – Westin Charlotte Hotel
6 – JDM Building – Multi-Tenant Office
7 – Interstate 277
– Historical Gasoline Station Based on Sanborns
– Historical Auto Dealership Based on Sanborns
SOURCE:
GOOGLE EARTH
2012 AERIAL PHOTOGRAPH
(VIA THE INTERNET)
SCALE AS SHOWN
FIGURE 2
SITE MAP
FORMER GOODYEAR SERVICE CENTER
BROWNFIELDS PROJECT No. 17038-13-060
CHARLOTTE, MECKLENBURG COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-5350
1
6
5
4
3
2
7
SOURCE:
MECKLENBURG COUNTY GIS (POLARIS)
SCALE AS SHOWN
FIGURE 3
PRELIMINARY SITE DEVELOPMENT PLAN
FORMER GOODYEAR SERVICE CENTER
BROWNFIELDS PROJECT No. 17038-13-060
CHARLOTTE, MECKLENBURG COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-5350
MULTI LEVEL
BELOW GROUND PARKING –
EXCAVATION AREA
(RED OUTLINE)
PROPOSED SLAB-ON-GRADE
OFFICE BUILDING WITH
GROUND FLOOR RETAIL
(BLACK OUTLINE)
HOTEL
PROPOSED SLAB-
ON-GRADE
(BLUE OUTLINE)
COURTYARD
SOURCE:
MECKLENBURG COUNTY GIS (POLARIS)
SCALE AS SHOWN
FIGURE 4
PRELIMINARY SITE DEVELOPMENT PLAN
WITH SAMPLE LOCATIONS
FORMER GOODYEAR SERVICE CENTER
BROWNFIELDS PROJECT No. 17038-13-060
CHARLOTTE, MECKLENBURG COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-5350
Soil Sampling Area
Soil Sampling Location
Soil-Gas Sampling Location
Sub-Slab Vapor Sampling Location
Yellow border represents slab on grade
Blue border represents area to excavated
1
2
3
4
5
6
7
SB4-S
SB6-S/D
SB7-S/D
SB1-S/D
SB3-S/D
SB5-S/D
SB2-S/D
SG-1/1R
SG-2/2R
SG-3/3R
SG-4/4R
SG-5
SG-6
SG-8
SG-7
GP-1
GP-2
TABLES
TABLE 1: SUMMARY OF SOIL GAS ANALYTICAL RESULTS
TRYON PLACE, TRYON AND STONEWALL STREETS
Parameter
Sample ID SG-1 SG-2 SG-3 SG-4 SG-5 SG-6 SG-7 SG-8 DUP SG-1R SG-2R SG-3R SG-4R DUP-R
Collection Date
Acetone 45 J 50 22 J 42 J 81 < 52 24 J < 53 51 J 270 130 30 120 <24 220,000 2,700,000
Benzene 1.3 J 2.9 < 2.0 7.2 3.1 12 < 2.1 15 1.9 J 45 3.5 2.6 J 2.5 J 44 120 1,600
2-Butone (IMEK)10 J 13 J 4.0 J 8.9 J 19 J 11 J < 5.1 45 J 10 J 33 8.2 J 3.1 J 7.9 J 33 35,000 440,000
Carbon Disulfide 4.1 J 1.6 J < 20 6.5 J 15 J 120 < 20 < 17 4.7 J 370 2.6 J 10 4.0 J 340 4,900 61,000
Chloroform <3.1 <2.6 <3.1 <2.6 <3.4 <2.7 <3.1 <2.7 <3.1 <4.9 <4.9 1.3 J <4.9 1.3 J 41 530
Chloromethane < 2.6 < 2.2 1.2 J 1.1 J 3.9 8.2 < 2.7 1.4 J < 2.7 2.5 0.8 J 1.4 J 2.9 11 630 7,900
Cyclohexane < 2.2 < 1.8 < 2.2 71 < 2.4 26 < 2.2 8.1 < 2.2 68 <17 <17 <17 65 42,000 530,000
Dichlorodifluoromethane (F12)3.0 J 2.2 J < 3.1 2.4 J 2.6 J 2.3 J 2.5 J 2.5 J 3.1 J 8.6 2.2 J 2.7 J 2.1 J 7.1 700 8,800
cis-1,2-Dichloroethylene 13 42 13 10 20 120 6.2 22 240 <4.0 <4.0 <4.0 <4.0 <4.0 NS NS
trans-1,2-Dichloroethylene < 2.5 < 2.1 < 2.5 < 2.1 < 2.8 1.9 J < 2.6 < 2.2 3.4 <8.0 <8.0 <8.0 <8.0 <8.0 NS NS
Ethanol < 48 < 40 < 48 21 J 44 J < 41 < 49 110 < 49 40 95 26 92 39 NS NS
Ethyl acetate < 2.3 < 1.9 < 2.3 < 1.9 2.7 < 2.0 5.1 1,600 < 2.3 <18 <18 <18 5.4 J <18 490 6,100
Ethylbenzene < 2.8 46 3.6 4.2 < 3.0 4.3 < 2.8 3.8 < 2.8 20 QL-1H 2.4 QL-1H J 2.9 QL-1H J 3.0 QL-1H J 19 QL-1H 370 4,900
4-Ethyltoluene < 2.0 2.0 J < 3.1 1.9 J < 3.4 < 2.7 < 32.< 2.7 < 3.2 <5.0 2.3 J <5.0 <5.0 <5.0 NS NS
Heptane 1.9 J 1.9 J < 2.6 69 3.6 29 2.9 3.6 2.4 J 41 5.1 11 8.0 39 NS NS
Hexane 4.3 J 4.5 J < 90 47 J 7.7 J 49 4.3 J 25 J 4.9 J 130 4.6 14 1.6 J 120 4,900 61,000
Hexachlorobutadiene < 6.8 < 5.6 < 6.8 < 5.7 < 7.5 4.0 J,Z-01 < 6.9 < 5.9 < 6.9 <54 <54 <54 <54 <54 43 560
Isopropanol 2.2 J, Z-01 2.5 J, Z-01 < 62 Z-01 3.8 J, Z-01 5.6 J, Z-01 2.2 J, Z-01 2.5 J, Z-01 38 J, Z-01 2.8 J, Z-01 <25 13 J 4.8 J 25 J 8.7 J 1,400 18,000
Methylene chloride < 22 < 18 < 22 2.8 J 4.5 J 2.8 J 3.4 J 120 < 22 1.2 J <3.5 1.1 J 1.5 J 1.2 J 4,200 53,000
4-Methyl-2-pentanone (MIBK)< 2.6 < 2.2 < 2.6 < 2.2 < 2.9 < 2.2 < 2.6 8 < 2.8 5.4 J <8.3 <8.3 <8.3 6.9 J 21,000 260,000
Naphthalene 7.3 < 2.8 < 3.3 < 2.8 < 3.7 < 2.9 < 3.4 < 2.9 6.8 <5.3 <5.3 <5.3 4.5 J <5.3 21 260
Propene 31 J 30 J 6.6 J 66 25 J 290 9.5 J < 38 30 J 3900 13 31 20 4300 NS NS
Styrene < 2.7 L-03 3.0 L-03 < 2.7 L- 03 < 2.3 L- 03 2.2 L- 03 3.0 L- 03 2.7 L- 03 5.6 L- 03 < 2.7 L- 03 5.0 <4.3 <4.3 <4.3 5.3 7,000 88,000
Tetrachloroethylene 1,300 4,000 1,300 1,300 2,000 30,000 560 2,400 34,000 12 2.4 J <6.9 45 11 280 3,500
Toluene 3.5 7.4 2.6 4.6 6.3 9.8 2.2 J 140 3.4 110 50 69 110 110 35,000 440,000
Trichloroethylene 18 63 19 35 30 210 9.2 58 350 <5.5 <5.5 <5.5 3.8 J <5.5 14.0 180
1,1,1-Trichloroethane <3.5 <2.9 <3.5 <2.9 <3.8 <3.0 <3.5 <3.0 <3.5 <5.5 <5.5 <5.5 3.2 J <5.5 35,000 440,000
Trichlorofluoromethane (F11)<14 <12 <14 <12 <16 <12 <14 <12 <14 1.5 J <5.6 1.7 J 1.2 J 1.4 J NS NS
1,2,4-Trimethylbenzene < 3.1 3.4 < 3.1 < 2.6 < 3.4 3.8 < 3.2 2.0 J 3.3 <5.0 <5.0 3.2 J 4.3 J <5.0 420 5,300
1,3,5-Trimethylbenzene < 3.1 4.2 < 3.1 < 2.6 < 3.4 11 <3.2 2.1 J 14 <5.0 <5.0 <5.0 1.8 J <5.0 420 5,300
Vinyl acetate < 45 1.8 J < 45 < 38 < 49 < 39 < 45 < 39 < 45 <3.6 <3.6 <3.6 <3.6 <3.6 1,400 18,000
Vinyl chloride <1.6 <1.3 <1.6 <1.4 <1.8 3.0 <1.6 <1.4 5.8 1.6 J <2.6 <2.6 <2.6 1.8 J 56 2,800
m,p-Xylenes < 5.5 190 15 < 4.6 4.3 J 11 < 5.6 9.8 < 5.6 12 11 7.8 J 14 13 700 8,800
o-Xylenes < 2.8 61 5 2.3 J < 3.0 4.6 < 2.8 8.2 3.0 7.6 4.5 2.6 J 4.0 J 7.2 700 8,800
Notes:
Comparison Criteria = North Carolina DWM Soil Gas Screening Level (SGSL) from IHSB Levels
DWM Vapor Intrusion Screening dated February 2018
Results presented in micrograms per cubic meter (ug/m3)
Bold indicates a detection above the Residential SGSL
Italics indicates a detection above the Non-Residential SGSL
Z-01 = Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in house limits of 50-150%.
L-03 = Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side.
QL-1H = The LCS and/or LCSD recoveries fell above the established control specifications for this analyte. Any result for this compound is qualified and should be considered biased high.J =Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration
SGSL = Soil Gas Screening LevelDUP collected on 10/15/17 = Duplicate of SG-6
DUPR collected on 1/31/18 = Duplicate of SG-1R
ResidentialSGSL Non-ResidentialSGSL
Target Volatile Organic Compounds by TO-15
COMPARISON CRITERIAANALYTICAL RESULTS
1/31/1810/15/17
TABLE 2: SUMMARY OF SOIL ANALYTICAL RESULTS - VOCS Quadrants 1 through 4
Tryon PlaceEast Stonewall Street, Charlotte, North Carolina
Parameter
Sample ID SB1-1S SB1-1D SB1-2S SB1-2D SB1-3S SB1-3D SB1-4S SB2-1S SB2-2S SB-Dup SB2-3S SB2-3D SB2-4S SB2-4D SB3-1S SB3-1D SB3-2S SB3-2D SB3-3S SB3-3D SB3-4S SB3-4D SB4-1S SB4-2S SB4-3S SB4-4S
Collection Depth
(feet bgs)5 12 5 14 5 11 5 5 5 5 5 9 5 14 5 13 5 14 5 15 5 15 5 5 5 5
Collection Date 10/15/17 10/14/17
Volatile Organic Compounds
Acetone 0.052 <0.040 <0.038 <0.041 <0.039 <0.042 <0.0037 0.024 J 0.13 0.029J 0.029J <0.037 0.026 J <0.047 0.052 <0.044 0.049 <0.035 0.11 <0.036 0.08 <0.040 <0.040 0.075 0.11 <0.038 1,200 10,0000
Benzene <0.0027 <0.0024 <0.0023 <0.0025 <0.0023 <0.0025 <0.0022 <0.0027 <0.0026 <0.0024 <0.0025 <0.0022 <0.0021 <0.0028 <0.0021 <0.0026 <0.0028 <0.0021 <0.0028 <0.0022 <0.0022 <0.0024 <0.0024 0.0019 J <0.0028 <0.0023 1.2 5.4
Toluene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 0.0032 J <0.0046 <0.0038 820 820
2-Butanone <0.089 <0.080 <0.077 <0.082 <0.078 <0.084 <0.075 <0.089 <0.087 <0.081 <0.085 <0.075 <0.069 <0.094 <0.071 <0.087 <0.093 <0.070 <0.092 <0.072 <0.074 <0.079 <0.081 <0.088 <0.092 <0.076 5,500 28,000
1,2,4-Trimethylbenzene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 <0.0044 <0.0046 <0.0038 63 220
1,3,5-Trimethylbenzene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 <0.0044 <0.0046 <0.0038 56 180
4-Isopropyltoluene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 <0.0044 <0.0046 <0.0038 25 NS
m,p-Xylenes <0.0089 <0.0080 <0.0077 <0.0082 <0.0078 <0.0084 <0.0075 <0.0089 <0.0087 <0.0081 <0.0085 <0.0075 <0.0069 <0.0094 <0.0071 <0.0087 <0.0093 <0.0070 <0.0092 <0.0072 <0.0074 <0.0079 <0.0081 <0.0088 <0.0092 <0.0076 120 390
Methyl isobutyl ketone <0.044 <0.040 <0.038 <0.041 <0.039 <0.042 <0.037 <0.045 <0.043 <0.041 <0.042 <0.037 <0.034 <0.047 <0.035 <0.044 <0.046 <0.035 <0.046 <0.036 <0.037 <0.040 <0.040 <0.044 <0.046 <0.038 3,400 3,400
Naphthalene <0.0089 <0.0080 <0.0077 <0.0082 <0.0078 <0.0084 <0.0075 <0.0089 <0.0087 <0.0081 <0.0085 <0.0075 <0.0069 <0.0094 <0.0071 <0.0087 <0.0093 <0.0070 <0.0092 <0.0072 <0.0074 <0.0079 <0.0081 <0.0088 <0.0092 <0.0076 4.1 18
n-Butylbenzene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 <0.0044 <0.0046 <0.0038 110 110
n-Propylbenzene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 <0.0044 <0.0046 <0.0038 260 260
o-xylene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 <0.0044 <0.0046 <0.0038 140 430
Xylene, total <0.013 <0.012 <0.012 <0.012 <0.012 <0.013 <0.011 <0.013 <0.013 <0.012 <0.013 <0.011 <0.010 <0.014 <0.011 <0.013 <0.014 <0.011 <0.014 <0.011 <0.011 <0.012 <0.012 <0.013 <0.014 <0.011 120 260
sec-Butylbenzene <0.0044 <0.0040 <0.0038 <0.0041 <0.0039 <0.0042 <0.0037 <0.0045 <0.0043 <0.0041 <0.0042 <0.0037 <0.0034 <0.0047 <0.0035 <0.0044 <0.0046 <0.0035 <0.0046 <0.0036 <0.0037 <0.0040 <0.0040 <0.0044 <0.0046 <0.0038 150 150
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)Feet bgs = Feet below ground surface
Bold denotes concentration exceeds the Residential PSRG (February 2018)
J = Estimated concentration, below calibration range and above Method Detection LimitThe standard for trivalent chromium used for total chromium, as recent sampling determined that the chromium present was trivalent, not hexavalent.
SB-Dup is a duplicate sample of SB2-2S
Comparison CriteriaANALYTICAL RESULTS
Unrestricted Use Health Base-Based PSRG
Industrial Health-Based PSRG
1014/17 10/14/17 10/15/17
TABLE 2: SUMMARY OF SOIL ANALYTICAL RESULTS - VOCS Quadrants 1 through 4
Tryon Place
East Stonewall Street, Charlotte, North Carolina
Parameter
Sample ID SB5-1S SB5-1D SB5-2S SB5-3S SB5-4S SB5-4D SB6-1S SB6-1D SB6-2S SB6-2D SB6-3S SB6-3D SB6-4S SB6-4D SB7-1S SB7-1D SB7-2S SB7-2D SB7-3S SB7-3D SB7-4S SB7-4D
Collection Depth
(feet bgs)5 9 5 5 5 11 5 14 5 13 5 11 5 17 5 14 5 10 5 15 5 14
Collection Date
Volatile Organic Compounds
Acetone 0.062 <0.049 <0.042 0.062 0.064 0.022 J 0.15 0.18 0.036 <0.043 0.16 0.022 J 0.11 <0.043 0.041 <0.040 0.020 J <0.055 0.012 J <0.039 0.11 <0.051 1,200 10,0000
Benzene <0.0026 <0.0030 <0.0025 <0.0027 <0.0024 <0.0026 <0.0026 <0.0023 <0.0021 <0.0026 0.0020 J <0.0026 0.0028 <0.0026 <0.0021 <0.0024 <0.0022 <0.0033 <0.0023 <0.0023 <0.0026 <0.0031 1.2 5.4
Toluene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 <0.0038 <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 820 820
2-Butanone <0.086 <0.099 <0.084 <0.089 <0.079 <0.087 <0.088 <0.075 <0.089 <0.086 0.018 J <0.087 <0.090 <0.086 <0.070 <0.079 <0.073 <0.11 <0.078 <0.077 <0.086 <0.10 5,500 28,000
1,2,4-Trimethylbenzene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 0.010 A <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 63 220
1,3,5-Trimethylbenzene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 0.0044 A <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 56 180
4-Isopropyltoluene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 0.011 A <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 25 NS
m,p-Xylenes <0.0086 <0.0099 <0.0084 <0.0089 <0.0079 <0.0087 <0.0088 0.0018 A,J <0.0069 <0.0086 <0.0072 <0.0087 <0.0090 <0.0086 <0.0070 <0.0079 <0.0073 <0.011 <0.0078 <0.0077 <0.0086 <0.010 120 390
Methyl isobutyl ketone <0.043 <0.049 <0.042 <0.044 <0.039 <0.044 <0.044 0.0076 J <0.035 <0.043 <0.036 <0.044 <0.045 <0.043 <0.070 <0.040 <0.037 <0.055 <0.039 <0.039 <0.043 <0.051 3,400 3,400
Naphthalene <0.0086 <0.0099 <0.0084 <0.0089 <0.0079 <0.0087 <0.0088 0.0089 A <0.0069 <0.0086 <0.0072 <0.0087 <0.0090 <0.0086 <0.0070 <0.0079 <0.0073 <0.011 <0.0078 <0.0077 <0.0086 <0.010 4.1 18
n-Butylbenzene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 0.0065 A <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 110 110
n-Propylbenzene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 0.0039 A <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 260 260
o-xylene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 0.0030 A,J <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 140 430
Xylene, total <0.013 <0.015 <0.013 <0.013 <0.012 <0.013 <0.013 0.0048 A,J <0.010 <0.013 <0.011 <0.013 <0.013 <0.013 <0.010 <0.012 <0.011 <0.017 <0.012 <0.012 <0.013 <0.015 120 260
sec-Butylbenzene <0.0043 <0.0049 <0.0042 <0.0044 <0.0039 <0.0044 <0.0044 0.0061 A <0.0035 <0.0043 <0.0036 <0.0044 <0.0045 <0.0043 <0.0035 <0.0040 <0.0037 <0.0055 <0.0039 <0.0039 <0.0043 <0.0051 150 150
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
Feet bgs = Feet below ground surface
Bold denotes concentration exceeds the Residential PSRG February 2018)
J = Estimated concentration, below calibration range and above Method Detection Limit
A = Internal standard repsonse outside the QC limits. Analysis repeated without improvement. Reanalysis result reported.The standard for trivalent chromium used for total chromium, as recent sampling determined that the chromium present was trivalent, not hexavalent.
10/15/17 10/14/17
Unrestricted Use Health Base-Based PSRG
Industrial Health-
Based PSRG
Comparison Criteria
TABLE 2: SUMMARY OF SOIL ANALYTICAL RESULTS - VOCS Quadrants 1 through 4Tryon Place
East Stonewall Street, Charlotte, North Carolina
Parameter
Sample ID SB1-S SB1-D SB2-S SB2-D SB3-S SB3-D SB4-S SB5-S SB5-D SB6-S SB6-D SB7-S SB7-D
Collection Depth (feet bgs)5 11-14 5 9-14 5 13-15 5 5 9-11 5 11-17 5 10-15
Collection Date
Total Metals
Arsenic 0.58 1.30 1.10 0.71 2.70 1.40 30.00 1.50 1.10 4.60 1.60 5.50 2.80 0.68 3.0
Barium 27.00 36.00 46.00 370.00 53.00 40.00 110.00 66.00 62.00 200.00 51.00 55.00 56.00 3,100 47,000
Cadmium <0.29 <0.28 <0.30 <0.28 <0.29 <0.29 0.33 <0.29 <0.27 0.34 <0.28 0.37 <0.29 14 200
Chromium 28.00 10.00 39.00 130.00 20.00 200.00 21.00 31.00 31.00 46.00 14.00 24.00 63.00 23,000 350,000
Lead 9.00 6.70 8.90 3.10 33.00 4.90 82.00 9.80 4.00 180.00 6.10 61.00 7.30 400 800
Mercury <0.022 <0.021 <0.023 <0.021 0.18 <0.021 0.24 <0.023 <0.020 0.78 <0.023 0.27 <0.024 2.30 9.70
Selenium 0.57 0.61 1.20 0.75 0.88 0.62 1.20 1.10 0.73 0.64 0.93 1.30 0.94 78 1,200
Semivolatile Organic Compounds
1-Methylnaphthalene <0.38 <0.37 <0.40 <0.36 <0.38 <0.38 <0.36 <0.38 <0.35 0.13 J <0.37 <0.38 <0.38 18 73
2-Methylnaphthalene <0.38 <0.37 <0.40 <0.36 <0.38 <0.38 0.096 J <0.38 <0.35 0.16 J <0.37 <0.38 <0.38 48 600
Anthracene <0.38 <0.37 <0.40 <0.36 <0.38 <0.38 <0.36 <0.38 <0.35 0.11 J <0.37 <0.38 <0.38 3,600 45,000
Benz(a)anthracene <0.38 <0.37 <0.40 <0.36 <0.38 <0.38 0.25 J 0.13 J <0.35 0.55 <0.37 0.13 J <0.38 1.1 21
Benzo(a)pyrene <0.38 <0.37 <0.40 <0.36 0.11 J <0.38 0.31 J 0.15 J <0.35 0.67 <0.37 0.14 J <0.38 0.11 2.1
Benzo(b)fluoranthene <0.38 <0.37 <0.40 <0.36 0.17 J <0.38 0.44 0.24 J <0.35 0.88 <0.37 0.20 J <0.38 1.1 21
Benzo(k)fluoranthene <0.38 <0.37 <0.40 <0.36 ,0.37 <0.38 0.13 J <0.38 <0.35 0.26 J <0.37 <0.38 <0.38 11 210
Benzo(g,h,i)perylene <0.38 <0.37 <0.40 <0.36 0.096 J <0.38 <0.37 0.13 J <0.35 0.46 <0.37 <0.38 <0.38 NS NS
Chrysene <0.38 <0.37 <0.40 <0.36 0.10 J <0.38 0.28 J 0.19 J <0.35 0.60 <0.37 0.16 J <0.38 110 2,100
Dibenzo(a,h)anthracene <0.38 <0.37 <0.40 <0.36 <0.38 <0.38 <0.36 <0.38 <0.35 0.11 J <0.37 <0.38 <0.38 0.11 2.1
Fluoranthene <0.38 <0.37 <0.40 <0.36 0.16 J <0.38 0.42 0.39 <0.35 0.98 <0.37 0.23 J <0.38 480 6,000
Indeo(1,2,3-cd)pyrene <0.38 <0.37 <0.40 <0.36 0.097 J <0.38 0.26J 0.13 J <0.35 <0.37 <0.37 0.099 J <0.38 1.1 21
Naphthalene <0.38 <0.37 <0.40 <0.36 <0.38 <0.38 <0.36 <0.38 <0.35 0.14J <0.37 <0.38 <0.38 4.1 18
Phenanthrene <0.38 <0.37 <0.40 <0.36 <0.38 <0.38 0.25 J 0.15 J <0.35 0.37 <0.37 <0.38 <0.38 NS NS
Pyrene <0.38 <0.37 <0.40 <0.36 0.17 J <0.38 0.4 0.33 J <0.35 1.0 <0.37 0.22 J <0.38 360 4,500
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
Feet bgs = Feet below ground surfaceBold denotes concentration exceeds the residential PSRG (February 2018)
Underline denotes concentration exceeds the residential and commercial PSRG
J = Estimated concentration, below calibration range and above Method Detection Limit
The standard for trivalent chromium used for total chromium, as recent sampling determined that the chromium present was trivalent, not hexavalent.
Residential Use
Health Base-
Based PSRG
Industrial Health-
Based PSRG
10/15/17
Comparison Criteria
APPENDIX A
APPENDIX B
17038-13-060/Goodyear 2016-07-25
1
Exhibit C
The most recent environmental sampling at the Property reported in the Environmental
Reports occurred in August 2014.The following tables set forth, for contaminants present at the
Property above unrestricted use standards or screening levels, the concentration found at each
sample location, and the applicable standard or screening level. Screening levels and
groundwater standards are shown for reference only and are not set forth as cleanup levels for
purposes of this Agreement.
GROUNDWATER
Groundwater contaminants in micrograms per liter (the equivalent of parts per billion), the
standards or screening levels for which are contained in Title 15A of the North Carolina
Administrative Code, Subchapter 2L (2L), Rule .0202, (April 1 2013 version); or the 2L
Groundwater Interim Maximum Allowable Concentrations (“IMACs”, October 1, 2010 version):
Groundwater
Contaminant
Sample
Location
Date of
Sampling
Concentration
Exceeding Screening
Level (µg/L)
2L Standard
(µg/L)
Tetrachloroethylene TW-2 11/2/2013 3.4 0.7
Notes:
1. Screening limits displayed for non-carcinogens are for a hazard quotient equal to 0.2. Screening levels
displayed for carcinogens are for a 1.0E-5 lifetime incremental cancer risk (LICR).
SOIL
Soil contaminants in milligrams per kilogram (the equivalent of parts per million), the
screening levels for which are derived from the Preliminary Industrial Health- Based Soil
Remediation Goals of the Inactive Hazardous Sites Branch of DEQ’s Superfund Section (April
2016 version):
Soil
Contaminant
Sample
Location
Depth
(ft)
Date of Sampling Concentration
Exceeding
Screening Level
(mg/kg)
Industrial
Screening
Level1
(mg/kg)
Arsenic SB2 4-8 04/29/2006 4.3 3
Arsenic SB3 8-12 04/29/2006 7.1 3
Arsenic GP-1* 8-10 10/26/2013 6.7 3
Arsenic GP-2* 17-18 10/26/2013 5.5 3
Arsenic GP-3* 13-14 10/26/2013 7.3 3
Arsenic GP-4* 12-13 10/26/2013 4.5 3
Arsenic GP-1 12 10/22/2013 4.4 3
Arsenic GP-5 8 10/22/2013 4.0 3
Arsenic GP-6 8 10/22/2013 11 3
17038-13-060/Goodyear 2016-07-25
2
Soil
Contaminant
Sample
Location
Depth
(ft)
Date of Sampling Concentration
Exceeding
Screening Level
(mg/kg)
Industrial
Screening
Level1
(mg/kg)
Arsenic GP-7 16 10/22/2013 5.7 3
Arsenic GP-8 12 10/22/2013 3.7 3
Arsenic GP-10 8 10/22/2013 3.3 3
Arsenic GP-12 12 10/22/2013 3.2 3
Arsenic GP-13 8 10/22/2013 7.6 3
Arsenic GP-14 8 10/22/2013 4.3 3
Arsenic SB-01 2-4 03/13/2014 6.1 3
Arsenic SB-02 2-4 03/13/2014 5.75 3
Arsenic SB-03 2-4 03/13/2014 11.7 3
Arsenic SB-04 10-12 03/13/2014 6.04 3
Arsenic SB-05 10-12 03/13/2014 4.4 3
Arsenic SB-06 2-4 03/14/2014 3.75 3
Arsenic SB-07 2-4 03/13/2014 6.18 3
Arsenic SB-08 2-4 03/13/2014 7.39 3
Arsenic SB-09 2-4 03/13/2014 6.53 3
Arsenic SB-10 10-12 03/13/2014 4.28 3
Chromium VI GP-2 8 10/22/2013 6.87 6.3
Benzo(a)anthracene GP-6 8 10/22/2013 3.7 2.9
Benzo(a)anthracene GP-13 8 10/22/2013 5.0 2.9
Benzo(a)pyrene GP-6 8 10/22/2013 3.7 0.29
Benzo(a)pyrene GP-13 8 10/22/2013 5.6 0.29
Benzo(b)fluoranthene GP-6 8 10/22/2013 4.2 2.9
Benzo(b)fluoranthene GP-13 8 10/22/2013 6.4 2.9
Dibenzo(a,h)anthracene GP-6 8 10/22/2013 0.98 0.29
Dibenzo(a,h)anthracene GP-13 8 10/22/2013 0.97 0.29
Indeno(1,2,3-cd)pyrene GP-6 8 10/22/2013 3.1 2.9
Indeno(1,2,3-cd)pyrene GP-13 8 10/22/2013 4.8 2.9
1Screening levels displayed for non-carcinogens are for a hazard quotient equal to 0.2. Screening levels
displayed for carcinogens are for a 1.0E-6 lifetime incremental cancer risk.
*Boring locations on Goodyear Property installed by ECS Carolinas
APPENDIX C
16 May 2018
Enclosed is the analytical report for the above referenced project. The data herein applies to
samples as received by H&P Mobile Geochemistry, Inc. on 01-Feb-18 which were analyzed in
accordance with the attached Chain of Custody record(s).
The results for all sample analyses and required QA/QC analyses are presented in the following
sections and summarized in the documents:
•Sample Summary
•Case Narrative (if applicable)
•Sample Results
•Quality Control Summary
•Notes and Definitions / Appendix
•Chain of Custody
•Sampling Logs (if applicable)
Unless otherwise noted, I certify that all analyses were performed and reviewed in compliance with
our Quality Systems Manual and Standard Operating Procedures. This report shall not be
reproduced, except in full, without the written approval of H&P Mobile Geochemistry, Inc.
We at H&P Mobile Geochemistry, Inc. sincerely appreciate the opportunity to provide analytical
services to you on this project. If you have any questions or concerns regarding this analytical report,
please contact me at your convenience at 760-804-9678.
Sincerely,
Client Project: Tryon Place
H&P Project: ECS020118-11 Rev 2
Charlotte, NC 28217
1812 Center Park Drive, Suite D
ECS Southeast, LLP - Charlotte
Mr. Chris Orrell
Laboratory Director
Janis La Roux
Dear Mr. Chris Orrell:
Quality. Accuracy. Experience.2470 Impala Drive, Carlsbad, CA 92010 & Field Office - Signal Hill, CA
P 1.800.834.9888 / 760.804.9678 F 760.804.9159 W handpmg.com
MobileGeochemistry Inc.
H&P Mobile Geochemistry, Inc. is certified under the California ELAP and the National Environmental
Laboratory Accreditation Conference (NELAC). H&P is approved as an Environmental Testing Laboratory and
Mobile Laboratory in accordance with the DoD-ELAP Program and ISO/IEC 17025:2005 programs,
accreditation number 69070 for EPA Method TO-15, H&P Method TO-15, EPA Method 8260B and H&P 8260SV.
Page 1 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
SG-4R E802006-01 Vapor 31-Jan-18 01-Feb-18
SG-3R E802006-02 Vapor 31-Jan-18 01-Feb-18
SG-2R E802006-03 Vapor 31-Jan-18 01-Feb-18
SG-1R E802006-04 Vapor 31-Jan-18 01-Feb-18
Dup E802006-05 Vapor 31-Jan-18 01-Feb-18
Page 2 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-4R (E802006-01) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EPA TO-1507-Feb-18 07-Feb-18ug/m3 EB807111Propene8.7ND0.7
"""""Dichlorodifluoromethane (F12)J"5.01.22.1
"""""Chloromethane "2.10.62.9
""""""Dichlorotetrafluoroethane (F114)7.1ND1.8
""""""Vinyl chloride 2.6ND1.0
""""""Bromomethane 16ND1.2
""""""Chloroethane 8.0ND0.8
"""""Ethanol "191292
"""""Trichlorofluoromethane (F11)J"5.61.21.2
"""""Acetone "247.5120
"""""Isopropyl alcohol J"253.725
""""""1,1-Dichloroethene 4.0ND1.5
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND1.9
"""""Methylene chloride (Dichloromethane)J"3.51.01.5
"""""Carbon disulfide J"6.30.94.0
""""""trans-1,2-Dichloroethene 8.0ND1.0
""""""Vinyl acetate 3.6ND1.2
""""""1,1-Dichloroethane 4.1ND1.4
"""""2-Butanone (MEK)J"302.07.9
"""""n-Hexane J"3.61.41.6
""""""cis-1,2-Dichloroethene 4.0ND1.2
"""""Ethyl acetate J"181.15.4
""""""Chloroform 4.9ND1.3
"""""1,1,1-Trichloroethane J"5.51.23.2
""""""1,2-Dichloroethane (EDC)4.1ND1.3
"""""Benzene J"3.20.72.5
""""""Carbon tetrachloride 6.4ND1.2
""""""Cyclohexane 17ND0.7
"""""n-Heptane "4.12.18.0
"""""Trichloroethene J"5.51.53.8
""""""1,2-Dichloropropane 9.4ND1.5
""""""Bromodichloromethane 6.8ND1.6
""""""cis-1,3-Dichloropropene 4.6ND1.2
""""""4-Methyl-2-pentanone (MIBK)8.3ND3.2
""""""trans-1,3-Dichloropropene 4.6ND1.2
"""""Toluene "3.81.1110
Page 3 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-4R (E802006-01) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EPA TO-1507-Feb-18 07-Feb-18ug/m3 EB8071111,1,2-Trichloroethane 5.5ND1.3
""""""2-Hexanone (MBK)8.3ND5.4
""""""Dibromochloromethane 8.6ND1.6
"""""Tetrachloroethene "6.91.745
""""""1,2-Dibromoethane (EDB)7.8ND1.7
""""""1,1,1,2-Tetrachloroethane 7.0ND1.7
""""""Chlorobenzene 4.7ND1.2
"""""Ethylbenzene QL-1H, J"4.41.33.0
"""""m,p-Xylene "8.82.114
""""""Styrene 4.3ND1.5
"""""o-Xylene J"4.41.54.0
""""""Bromoform 10ND2.0
""""""1,1,2,2-Tetrachloroethane 7.0ND2.0
""""""4-Ethyltoluene 5.0ND1.6
"""""1,3,5-Trimethylbenzene J"5.01.71.8
"""""1,2,4-Trimethylbenzene J"5.02.04.3
""""""1,3-Dichlorobenzene 12ND1.9
""""""1,4-Dichlorobenzene 12ND2.0
""""""1,2-Dichlorobenzene 12ND2.2
"""""Naphthalene J"5.34.54.5
""""""1,2,4-Trichlorobenzene 38ND5.2
""""""Hexachlorobutadiene 54ND6.6
""""102 %76-134Surrogate: 1,2-Dichloroethane-d4
""""112 %78-125Surrogate: Toluene-d8
""""96.5 %77-127Surrogate: 4-Bromofluorobenzene
Page 4 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-3R (E802006-02) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EB80711 07-Feb-18 07-Feb-18ug/m3 1Propene EPA TO-158.70.731
"""""Dichlorodifluoromethane (F12)J"5.01.22.7
"""""Chloromethane J"2.10.61.4
""""""Dichlorotetrafluoroethane (F114)7.1ND1.8
""""""Vinyl chloride 2.6ND1.0
""""""Bromomethane 16ND1.2
""""""Chloroethane 8.0ND0.8
"""""Ethanol "191226
"""""Trichlorofluoromethane (F11)J"5.61.21.7
"""""Acetone "247.530
"""""Isopropyl alcohol J"253.74.8
""""""1,1-Dichloroethene 4.0ND1.5
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND1.9
"""""Methylene chloride (Dichloromethane)J"3.51.01.1
"""""Carbon disulfide "6.30.910
""""""trans-1,2-Dichloroethene 8.0ND1.0
""""""Vinyl acetate 3.6ND1.2
""""""1,1-Dichloroethane 4.1ND1.4
"""""2-Butanone (MEK)J"302.03.1
"""""n-Hexane "3.61.414
""""""cis-1,2-Dichloroethene 4.0ND1.2
""""""Ethyl acetate 18ND1.1
"""""Chloroform J"4.91.31.3
""""""1,1,1-Trichloroethane 5.5ND1.2
""""""1,2-Dichloroethane (EDC)4.1ND1.3
"""""Benzene J"3.20.72.6
""""""Carbon tetrachloride 6.4ND1.2
""""""Cyclohexane 17ND0.7
"""""n-Heptane "4.12.111
""""""Trichloroethene 5.5ND1.5
""""""1,2-Dichloropropane 9.4ND1.5
""""""Bromodichloromethane 6.8ND1.6
""""""cis-1,3-Dichloropropene 4.6ND1.2
""""""4-Methyl-2-pentanone (MIBK)8.3ND3.2
""""""trans-1,3-Dichloropropene 4.6ND1.2
"""""Toluene "3.81.169
Page 5 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-3R (E802006-02) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EPA TO-1507-Feb-18 07-Feb-18ug/m3 EB8071111,1,2-Trichloroethane 5.5ND1.3
""""""2-Hexanone (MBK)8.3ND5.4
""""""Dibromochloromethane 8.6ND1.6
""""""Tetrachloroethene 6.9ND1.7
""""""1,2-Dibromoethane (EDB)7.8ND1.7
""""""1,1,1,2-Tetrachloroethane 7.0ND1.7
""""""Chlorobenzene 4.7ND1.2
"""""Ethylbenzene QL-1H, J"4.41.32.9
"""""m,p-Xylene J"8.82.17.8
""""""Styrene 4.3ND1.5
"""""o-Xylene J"4.41.52.6
""""""Bromoform 10ND2.0
""""""1,1,2,2-Tetrachloroethane 7.0ND2.0
""""""4-Ethyltoluene 5.0ND1.6
""""""1,3,5-Trimethylbenzene 5.0ND1.7
"""""1,2,4-Trimethylbenzene J"5.02.03.2
""""""1,3-Dichlorobenzene 12ND1.9
""""""1,4-Dichlorobenzene 12ND2.0
""""""1,2-Dichlorobenzene 12ND2.2
""""""Naphthalene 5.3ND4.5
""""""1,2,4-Trichlorobenzene 38ND5.2
""""""Hexachlorobutadiene 54ND6.6
""""103 %76-134Surrogate: 1,2-Dichloroethane-d4
""""113 %78-125Surrogate: Toluene-d8
""""96.2 %77-127Surrogate: 4-Bromofluorobenzene
Page 6 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-2R (E802006-03) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EPA TO-1507-Feb-18 07-Feb-18ug/m3 EB807111Propene8.7ND0.7
"""""Dichlorodifluoromethane (F12)J"5.01.22.2
"""""Chloromethane J"2.10.60.8
""""""Dichlorotetrafluoroethane (F114)7.1ND1.8
""""""Vinyl chloride 2.6ND1.0
""""""Bromomethane 16ND1.2
""""""Chloroethane 8.0ND0.8
"""""Ethanol "191295
""""""Trichlorofluoromethane (F11)5.6ND1.2
"""""Acetone "247.5130
"""""Isopropyl alcohol J"253.713
""""""1,1-Dichloroethene 4.0ND1.5
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND1.9
""""""Methylene chloride (Dichloromethane)3.5ND1.0
"""""Carbon disulfide J"6.30.92.6
""""""trans-1,2-Dichloroethene 8.0ND1.0
""""""Vinyl acetate 3.6ND1.2
""""""1,1-Dichloroethane 4.1ND1.4
"""""2-Butanone (MEK)J"302.08.2
"""""n-Hexane "3.61.44.6
""""""cis-1,2-Dichloroethene 4.0ND1.2
""""""Ethyl acetate 18ND1.1
""""""Chloroform 4.9ND1.3
""""""1,1,1-Trichloroethane 5.5ND1.2
""""""1,2-Dichloroethane (EDC)4.1ND1.3
"""""Benzene "3.20.73.5
""""""Carbon tetrachloride 6.4ND1.2
""""""Cyclohexane 17ND0.7
"""""n-Heptane "4.12.15.1
""""""Trichloroethene 5.5ND1.5
""""""1,2-Dichloropropane 9.4ND1.5
""""""Bromodichloromethane 6.8ND1.6
""""""cis-1,3-Dichloropropene 4.6ND1.2
""""""4-Methyl-2-pentanone (MIBK)8.3ND3.2
""""""trans-1,3-Dichloropropene 4.6ND1.2
"""""Toluene "3.81.150
Page 7 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-2R (E802006-03) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EPA TO-1507-Feb-18 07-Feb-18ug/m3 EB8071111,1,2-Trichloroethane 5.5ND1.3
""""""2-Hexanone (MBK)8.3ND5.4
""""""Dibromochloromethane 8.6ND1.6
"""""Tetrachloroethene J"6.91.72.4
""""""1,2-Dibromoethane (EDB)7.8ND1.7
""""""1,1,1,2-Tetrachloroethane 7.0ND1.7
""""""Chlorobenzene 4.7ND1.2
"""""Ethylbenzene QL-1H, J"4.41.32.4
"""""m,p-Xylene "8.82.111
""""""Styrene 4.3ND1.5
"""""o-Xylene "4.41.54.5
""""""Bromoform 10ND2.0
""""""1,1,2,2-Tetrachloroethane 7.0ND2.0
"""""4-Ethyltoluene J"5.01.62.3
""""""1,3,5-Trimethylbenzene 5.0ND1.7
""""""1,2,4-Trimethylbenzene 5.0ND2.0
""""""1,3-Dichlorobenzene 12ND1.9
""""""1,4-Dichlorobenzene 12ND2.0
""""""1,2-Dichlorobenzene 12ND2.2
""""""Naphthalene 5.3ND4.5
""""""1,2,4-Trichlorobenzene 38ND5.2
""""""Hexachlorobutadiene 54ND6.6
""""103 %76-134Surrogate: 1,2-Dichloroethane-d4
""""90.5 %78-125Surrogate: Toluene-d8
""""96.1 %77-127Surrogate: 4-Bromofluorobenzene
Page 8 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-1R (E802006-04) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EB80711 07-Feb-18 07-Feb-18ug/m3 1Propene EEPA TO-158.70.73900
"""""Dichlorodifluoromethane (F12)"5.01.28.6
"""""Chloromethane "2.10.62.5
""""""Dichlorotetrafluoroethane (F114)7.1ND1.8
"""""Vinyl chloride J"2.61.01.6
""""""Bromomethane 16ND1.2
""""""Chloroethane 8.0ND0.8
"""""Ethanol "191240
"""""Trichlorofluoromethane (F11)J"5.61.21.5
"""""Acetone "247.5270
"""""Isopropyl alcohol J"253.77.6
""""""1,1-Dichloroethene 4.0ND1.5
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND1.9
"""""Methylene chloride (Dichloromethane)J"3.51.01.2
"""""Carbon disulfide "6.30.9370
""""""trans-1,2-Dichloroethene 8.0ND1.0
""""""Vinyl acetate 3.6ND1.2
""""""1,1-Dichloroethane 4.1ND1.4
"""""2-Butanone (MEK)"302.033
"""""n-Hexane "3.61.4130
""""""cis-1,2-Dichloroethene 4.0ND1.2
""""""Ethyl acetate 18ND1.1
""""""Chloroform 4.9ND1.3
""""""1,1,1-Trichloroethane 5.5ND1.2
""""""1,2-Dichloroethane (EDC)4.1ND1.3
"""""Benzene "3.20.745
""""""Carbon tetrachloride 6.4ND1.2
"""""Cyclohexane "170.768
"""""n-Heptane "4.12.141
""""""Trichloroethene 5.5ND1.5
""""""1,2-Dichloropropane 9.4ND1.5
""""""Bromodichloromethane 6.8ND1.6
""""""cis-1,3-Dichloropropene 4.6ND1.2
"""""4-Methyl-2-pentanone (MIBK)J"8.33.25.4
""""""trans-1,3-Dichloropropene 4.6ND1.2
"""""Toluene "3.81.1110
Page 9 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportSG-1R (E802006-04) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EPA TO-1507-Feb-18 07-Feb-18ug/m3 EB8071111,1,2-Trichloroethane 5.5ND1.3
""""""2-Hexanone (MBK)8.3ND5.4
""""""Dibromochloromethane 8.6ND1.6
"""""Tetrachloroethene "6.91.712
""""""1,2-Dibromoethane (EDB)7.8ND1.7
""""""1,1,1,2-Tetrachloroethane 7.0ND1.7
""""""Chlorobenzene 4.7ND1.2
"""""Ethylbenzene QL-1H"4.41.320
"""""m,p-Xylene "8.82.112
"""""Styrene "4.31.55.0
"""""o-Xylene "4.41.57.6
""""""Bromoform 10ND2.0
""""""1,1,2,2-Tetrachloroethane 7.0ND2.0
""""""4-Ethyltoluene 5.0ND1.6
""""""1,3,5-Trimethylbenzene 5.0ND1.7
""""""1,2,4-Trimethylbenzene 5.0ND2.0
""""""1,3-Dichlorobenzene 12ND1.9
""""""1,4-Dichlorobenzene 12ND2.0
""""""1,2-Dichlorobenzene 12ND2.2
""""""Naphthalene 5.3ND4.5
""""""1,2,4-Trichlorobenzene 38ND5.2
""""""Hexachlorobutadiene 54ND6.6
""""98.9 %76-134Surrogate: 1,2-Dichloroethane-d4
""""118 %78-125Surrogate: Toluene-d8
""""96.7 %77-127Surrogate: 4-Bromofluorobenzene
Page 10 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportDup (E802006-05) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EB80711 07-Feb-18 07-Feb-18ug/m3 1Propene EEPA TO-158.70.74300
"""""Dichlorodifluoromethane (F12)"5.01.27.1
"""""Chloromethane "2.10.611
""""""Dichlorotetrafluoroethane (F114)7.1ND1.8
"""""Vinyl chloride J"2.61.01.8
""""""Bromomethane 16ND1.2
""""""Chloroethane 8.0ND0.8
"""""Ethanol "191239
"""""Trichlorofluoromethane (F11)J"5.61.21.4
""""""Acetone 24ND7.5
"""""Isopropyl alcohol J"253.78.7
""""""1,1-Dichloroethene 4.0ND1.5
""""""1,1,2-Trichlorotrifluoroethane (F113)7.7ND1.9
"""""Methylene chloride (Dichloromethane)J"3.51.01.2
"""""Carbon disulfide "6.30.9340
""""""trans-1,2-Dichloroethene 8.0ND1.0
""""""Vinyl acetate 3.6ND1.2
""""""1,1-Dichloroethane 4.1ND1.4
"""""2-Butanone (MEK)"302.033
"""""n-Hexane "3.61.4120
""""""cis-1,2-Dichloroethene 4.0ND1.2
""""""Ethyl acetate 18ND1.1
"""""Chloroform J"4.91.31.3
""""""1,1,1-Trichloroethane 5.5ND1.2
""""""1,2-Dichloroethane (EDC)4.1ND1.3
"""""Benzene "3.20.744
""""""Carbon tetrachloride 6.4ND1.2
"""""Cyclohexane "170.765
"""""n-Heptane "4.12.139
""""""Trichloroethene 5.5ND1.5
""""""1,2-Dichloropropane 9.4ND1.5
""""""Bromodichloromethane 6.8ND1.6
""""""cis-1,3-Dichloropropene 4.6ND1.2
"""""4-Methyl-2-pentanone (MIBK)J"8.33.26.9
""""""trans-1,3-Dichloropropene 4.6ND1.2
"""""Toluene "3.81.1110
Page 11 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Volatile Organic Compounds by EPA TO-15
H&P Mobile Geochemistry, Inc.
Result Analyte Limit
Reporting
Units
Dilution
Batch Prepared Analyzed Method Notes FactorMDL
J- ReportDup (E802006-05) Vapor Sampled: 31-Jan-18 Received: 01-Feb-18
EPA TO-1507-Feb-18 07-Feb-18ug/m3 EB8071111,1,2-Trichloroethane 5.5ND1.3
""""""2-Hexanone (MBK)8.3ND5.4
""""""Dibromochloromethane 8.6ND1.6
"""""Tetrachloroethene "6.91.711
""""""1,2-Dibromoethane (EDB)7.8ND1.7
""""""1,1,1,2-Tetrachloroethane 7.0ND1.7
""""""Chlorobenzene 4.7ND1.2
"""""Ethylbenzene QL-1H"4.41.319
"""""m,p-Xylene "8.82.113
"""""Styrene "4.31.55.3
"""""o-Xylene "4.41.57.2
""""""Bromoform 10ND2.0
""""""1,1,2,2-Tetrachloroethane 7.0ND2.0
""""""4-Ethyltoluene 5.0ND1.6
""""""1,3,5-Trimethylbenzene 5.0ND1.7
""""""1,2,4-Trimethylbenzene 5.0ND2.0
""""""1,3-Dichlorobenzene 12ND1.9
""""""1,4-Dichlorobenzene 12ND2.0
""""""1,2-Dichlorobenzene 12ND2.2
""""""Naphthalene 5.3ND4.5
""""""1,2,4-Trichlorobenzene 38ND5.2
""""""Hexachlorobutadiene 54ND6.6
""""101 %76-134Surrogate: 1,2-Dichloroethane-d4
""""95.3 %78-125Surrogate: Toluene-d8
""""95.7 %77-127Surrogate: 4-Bromofluorobenzene
Page 12 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EB80711 - TO-15
Blank (EB80711-BLK1)Prepared & Analyzed: 06-Feb-18
Propene ug/m38.7ND
Dichlorodifluoromethane (F12)"5.0ND
Chloromethane "2.1ND
Dichlorotetrafluoroethane (F114)"7.1ND
Vinyl chloride "2.6ND
Bromomethane "16ND
Chloroethane "8.0ND
Ethanol "19ND
Trichlorofluoromethane (F11)"5.6ND
Acetone "24ND
Isopropyl alcohol "25ND
1,1-Dichloroethene "4.0ND
1,1,2-Trichlorotrifluoroethane (F113)"7.7ND
Methylene chloride (Dichloromethane)"3.5ND
Carbon disulfide "6.3ND
trans-1,2-Dichloroethene "8.0ND
Vinyl acetate "3.6ND
1,1-Dichloroethane "4.1ND
2-Butanone (MEK)"30ND
n-Hexane "3.6ND
cis-1,2-Dichloroethene "4.0ND
Ethyl acetate "18ND
Chloroform "4.9ND
1,1,1-Trichloroethane "5.5ND
1,2-Dichloroethane (EDC)"4.1ND
Benzene "3.2ND
Carbon tetrachloride "6.4ND
Cyclohexane "17ND
n-Heptane "4.1ND
Trichloroethene "5.5ND
1,2-Dichloropropane "9.4ND
Bromodichloromethane "6.8ND
cis-1,3-Dichloropropene "4.6ND
4-Methyl-2-pentanone (MIBK)"8.3ND
Page 13 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EB80711 - TO-15
Blank (EB80711-BLK1)Prepared & Analyzed: 06-Feb-18
trans-1,3-Dichloropropene ug/m34.6ND
Toluene "3.8ND
1,1,2-Trichloroethane "5.5ND
2-Hexanone (MBK)"8.3ND
Dibromochloromethane "8.6ND
Tetrachloroethene "6.9ND
1,2-Dibromoethane (EDB)"7.8ND
1,1,1,2-Tetrachloroethane "7.0ND
Chlorobenzene "4.7ND
Ethylbenzene "4.4ND
m,p-Xylene "8.8ND
Styrene "4.3ND
o-Xylene "4.4ND
Bromoform "10ND
1,1,2,2-Tetrachloroethane "7.0ND
4-Ethyltoluene "5.0ND
1,3,5-Trimethylbenzene "5.0ND
1,2,4-Trimethylbenzene "5.0ND
1,3-Dichlorobenzene "12ND
1,4-Dichlorobenzene "12ND
1,2-Dichlorobenzene "12ND
Naphthalene "5.3ND
1,2,4-Trichlorobenzene "38ND
Hexachlorobutadiene "54ND
"214 76-134Surrogate: 1,2-Dichloroethane-d4 101217
"207 78-125Surrogate: Toluene-d8 99.3206
"364 77-127Surrogate: 4-Bromofluorobenzene 97.5355
Page 14 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EB80711 - TO-15
LCS (EB80711-BS1)Prepared & Analyzed: 06-Feb-18
Dichlorodifluoromethane (F12)ug/m3 101 59-1281015.0100
Vinyl chloride "52.0 64-12796.62.650
Chloroethane "53.6 63-12789.88.048
Trichlorofluoromethane (F11)"113 62-12697.55.6110
1,1-Dichloroethene "80.8 61-1331034.083
1,1,2-Trichlorotrifluoroethane (F113)"155 66-1261027.7160
Methylene chloride (Dichloromethane)"70.8 62-11599.33.570
trans-1,2-Dichloroethene "80.8 67-12496.88.078
1,1-Dichloroethane "82.4 68-12695.94.179
cis-1,2-Dichloroethene "80.0 70-1211024.082
Chloroform "99.2 68-1231074.9110
1,1,1-Trichloroethane "111 68-1251025.5110
1,2-Dichloroethane (EDC)"82.4 65-1281024.184
Benzene "64.8 69-1191033.267
Carbon tetrachloride "128 68-13297.86.4130
Trichloroethene "110 71-1231035.5110
Toluene "76.8 66-1191013.877
1,1,2-Trichloroethane "111 73-1191025.5110
Tetrachloroethene "138 66-1241056.9140
1,1,1,2-Tetrachloroethane "140 67-1291107.0150
Ethylbenzene "88.4 QL-1H70-1241254.4110
m,p-Xylene "88.4 61-1341168.8100
o-Xylene "88.4 67-1251114.498
1,1,2,2-Tetrachloroethane "140 65-1271047.0150
"214 76-134Surrogate: 1,2-Dichloroethane-d4 104222
"207 78-125Surrogate: Toluene-d8 97.2201
"364 77-127Surrogate: 4-Bromofluorobenzene 97.6356
Page 15 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by EPA TO-15 - Quality Control
H&P Mobile Geochemistry, Inc.
Batch EB80711 - TO-15
LCS Dup (EB80711-BSD1)Prepared & Analyzed: 06-Feb-18
Dichlorodifluoromethane (F12)ug/m3 101 2559-128104 2.235.0100
Vinyl chloride "52.0 2564-12796.6 0.002.650
Chloroethane "53.6 2563-12790.0 0.1678.048
Trichlorofluoromethane (F11)"113 2562-12696.9 0.6155.6110
1,1-Dichloroethene "80.8 2561-133105 1.974.085
1,1,2-Trichlorotrifluoroethane (F113)"155 2566-126104 1.217.7160
Methylene chloride (Dichloromethane)"70.8 2562-11596.8 2.543.569
trans-1,2-Dichloroethene "80.8 2567-12496.7 0.1038.078
1,1-Dichloroethane "82.4 2568-12695.9 0.05204.179
cis-1,2-Dichloroethene "80.0 2570-121104 1.664.083
Chloroform "99.2 2568-123102 4.854.9100
1,1,1-Trichloroethane "111 2568-125101 0.5365.5110
1,2-Dichloroethane (EDC)"82.4 2565-128105 2.264.186
Benzene "64.8 2569-119105 2.023.268
Carbon tetrachloride "128 2568-13295.7 2.126.4120
Trichloroethene "110 2571-123104 0.7215.5110
Toluene "76.8 2566-119100 0.4453.877
1,1,2-Trichloroethane "111 2573-119101 0.8285.5110
Tetrachloroethene "138 2566-124104 0.4796.9140
1,1,1,2-Tetrachloroethane "140 2567-129111 0.2257.0150
Ethylbenzene "88.4 2570-124123 1.724.4110
m,p-Xylene "88.4 2561-134117 1.458.8100
o-Xylene "88.4 2567-125112 1.124.499
1,1,2,2-Tetrachloroethane "140 2565-127105 0.8557.0150
"214 76-134Surrogate: 1,2-Dichloroethane-d4 103220
"207 78-125Surrogate: Toluene-d8 114235
"364 77-127Surrogate: 4-Bromofluorobenzene 98.1358
Page 16 of 17
Project:
Project Number:
Project Manager:
Reported:
ECS Southeast, LLP - Charlotte
1812 Center Park Drive, Suite D
ECS020118-11 Rev 2
Tryon Place
Mr. Chris OrrellCharlotte, NC 28217 16-May-18 08:18
H&P Mobile
Geochemistry Inc.
2470 Impala Drive
Carlsbad, CA 92010
760-804-9678 Phone
760-804-9159 Fax
Notes and Definitions
QL-1H The LCS and/or LCSD recoveries fell above the established control specifications for this analyte. Any result for this compound
is qualified and should be considered biased high.
QL-1H The LCS and/or LCSD recoveries fell above the established control specifications for this analyte. Any result for this compound
is qualified and should be considered biased high.
J- Report This sample is reported to the MDL or LOD determined for this method. All confirmed hits above the listed MDL or LOD value
and below the RL/LOQ, will be flagged with a "J" result. If an MDL or LOD is not listed, the analyte is ND at the RL.
J Detected but below the RL/LOQ; therefore, result is an estimated concentration.
E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is
considered an estimate (CLP E-flag).
Percent Recovery
Relative Percent DifferenceRPD
%REC
Method Detection LimitMDL
Analyte NOT DETECTED at or above the reporting limitND
Leak Check CompoundLCC
Appendix
H&P Mobile Geochemistry, Inc. is approved as an Environmental Testing Laboratory and Mobile Laboratory in accordance with the DoD-ELAP Program
and ISO/IEC 17025:2005 programs through PJLA, accreditation number 69070 for EPA Method TO-15, H&P Method TO-15, EPA Method 8260B and
H&P 8260SV.
H&P is approved by the State of Arizona as an Environmental Testing Laboratory and Mobile Laboratory, certification numbers AZM758 and AZ0779.
H&P is approved by the State of California as an Environmental Laboratory and Mobile Laboratory in conformance with the Environmental Laboratory
Accreditation Program (ELAP) for the category of Volatile and Semi-Volatile Organic Chemistry of Hazardous Waste, certification numbers 2740, 2741,
2743, 2744, 2745, 2754 & 2930.
H&P is approved by the State of Florida Department of Health under the National Environmental Laboratory Accreditation Conference (NELAC)
certification number E871100.
The complete list of stationary and mobile laboratory certifications along with the fields of testing (FOTs) and analyte lists are available at
www.handpmg.com/about/certifications.
All soil results are reported in wet weight.
Page 17 of 17
Mobile
Geochemistry, Inc.
2470 Impala Drive, Carlsbad. CA 92010
& Field Office - Signal Hill, CA
W handpmg.com E info@handpmg.com
P 760.804.9678 F 760.804.9159
VAPOR / AIR Chain of Custody DATE:.
Page I of
Lab Client and Project Information Sample Receipt (Lab Use Only)
Lab Client/Consuitant n t-f .6 Ze.N.A.1+%,— .4—
PN2itic,t Name 4' ,. AtAa-
_ IWO' ••• . —", •
Date Rec'd: / 1 a Control It: gOtcps I
Lab Client Project Manager: c...4-,•,--t, 0,,,,,,k Project Location: C kux.ii-kA-1A--Ire., , 1....lti."
H&P Project # Ecs 02.011.rg-Il
Lab Client Address:,,,,,
'IS ---.0- C..cdon 'me- } >"ei:.. )).e , ,.;,,„,,,irt,',..,) Report E-Mail(s): i
•V5\•etbArk 1-g eQ-S v"Y\‘‘-€4'clr
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Lab Work Order # TOW-VIC,
Lab Client City, State, Zip:
1-e, Sample Intact Y Notes Below • No • See
, Phone Number.7r) t Y 7i-4.7-1I,1 Receipt Gauge ID: Sc o5 Temp: KT
Reporting Requirements Turnaround Time I Sampler Information Outside Lab:
W 5-7 day Stnd
Rush
Rush
Sampler(s):
C -, e)....,—/S\
Receipt Notes/Tracking #:
12155g501(00g
Lab PM Initials: 1614
911,standard Report • Level Ill • Level IV • 24-Hr Rush
0 Mobile Lab Signature: 1/it ..--A0k, Excel EDD • Other EDD: • 3-day
CA Geotracker Global ID: Date: 1 , 31 . li. • • 48-Hr • Other
Additional Instructions to Laboratory:tdlc( Tictiltds41ne
* Preferred VPC units (please choose one): -27 r2A)
Ekrzanoll E,1-Kilitce-fateu-cplavle
SOOVOUlell Tdoiet,:f-Dnee,F.Itfrrytt40
) . r 1
tleu A
1\10,4-141‘yi,b24421frc.Ferei V t f-1.0 Ac c. "pap
S' VOCs Standard Full List q 8260SV El TO-15 VOCs Short List! Project List q 8260SV q TO-15 Oxygenates q 8260SV q TO-15 Naphthalene IL1 8260SV q TO-15 TPHv as Gas 8260SVm q TO-15m Aromatic/Aliphatic Fractions q 8260SVm q TO-15m Leak Check Compound q DFA q IPA q He [Methane by EPA 8015m 4 Fixed Gases by ASTM D1945 q CO2 002 q N2 E pgil_ g4.1.giml 0 ppbv • ppmv
FIELD POINT
NAME
SAMPLE NAME (if applicable)
DATE TIME
mrn/ddlyy 24hr dock
SAMPLE TYPE
Indoor Air um, Ambient
Air AA), Subsiab (SS),
Soil vapor (S,i)
CONTAINER
SIZE & TYPE
400mLI11.161. Surma,
Tedlar, Tube, et.
Iff, „,...
E.(
li i,-- 8 Lab use only; Receipt Vac S (, -1-i P., i8iii.c 1:7,1.-7 ) 1,-1,01,...A— .--la \ ' 411 )4,
<,(,- 214. 1•7,1..77 I, Q)-)0 -5.0
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-7->k,..k,r) ,
_I _ —1-_,, ....1,--. ir ?) "q• g5
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ReZA,,,e, byqoloctiatv
Z. 1 I t t g t.: 14S F I'l
Appoved/Reliriquisned by: ainpany: Date: Time: Received by: Company: Date: Tore:
Approved/Relinquished by Company Date: Time: Received by: Company: Date- Time'
'Approval constit5n3s as to proceed with analysis and acceptance of conditions on tack Appendix Mt. Rev 523/2016. Effective 523/20/6
APPENDIX D
Summary of Risk Assessment Output Output Form 1A
Version Date: October 2017
Basis: June 2017 EPA RSL Table
Site ID: 17038-13-060
Exposure Unit ID: Worst Case S Tryon Building
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil Combined Pathways 0.0E+00 0.0E+00 NO
Groundwater Combined Pathways*0.0E+00 0.0E+00 NO
Soil Combined Pathways 0.0E+00 0.0E+00 NO
Groundwater Combined Pathways*0.0E+00 0.0E+00 NO
Construction Worker Soil Combined Pathways 0.0E+00 0.0E+00 NO
Soil Combined Pathways 0.0E+00 0.0E+00 NO
Surface Water Combined Pathways*0.0E+00 0.0E+00 NO
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 0.0E+00 0.0E+00 NO
Soil Gas to Indoor Air 5.4E-05 4.0E+00 YES
Indoor Air 0.0E+00 0.0E+00 NO
Groundwater to Indoor Air 0.0E+00 0.0E+00 NO
Soil Gas to Indoor Air 2.1E-06 3.2E-01 NO
Indoor Air 0.0E+00 0.0E+00 NO
Pathway Source
Source Soil NM
Source Groundwater NM
Source Soil NM
Source Groundwater NM
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed
the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a
risk-based closure.
Protection of Surface Water Exceedence of 2B at POE?
Exceedence of 2B at POE?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target POE Concentrations Exceeded?
Protection of Groundwater Use Exceedence of 2L at POE?
Exceedence of 2L at POE?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for
lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
PRIMARY CALCULATORS
Resident
Non-Residential Worker
User Defined
North Carolina DEQ Risk Calculator
Summary of Risk Assessment Output Output Form 1A
Version Date: October 2017
Basis: June 2017 EPA RSL Table
Site ID: 17038-13-060
Exposure Unit ID: Worst Case Stonewall Building
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil Combined Pathways 0.0E+00 0.0E+00 NO
Groundwater Combined Pathways*0.0E+00 0.0E+00 NO
Soil Combined Pathways 0.0E+00 0.0E+00 NO
Groundwater Combined Pathways*0.0E+00 0.0E+00 NO
Construction Worker Soil Combined Pathways 0.0E+00 0.0E+00 NO
Soil Combined Pathways 0.0E+00 0.0E+00 NO
Surface Water Combined Pathways*0.0E+00 0.0E+00 NO
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 0.0E+00 0.0E+00 NO
Soil Gas to Indoor Air 1.2E-04 3.0E+01 YES
Indoor Air 0.0E+00 0.0E+00 NO
Groundwater to Indoor Air 0.0E+00 0.0E+00 NO
Soil Gas to Indoor Air 8.8E-06 2.3E+00 YES
Indoor Air 0.0E+00 0.0E+00 NO
Pathway Source
Source Soil NM
Source Groundwater NM
Source Soil NM
Source Groundwater NM
PRIMARY CALCULATORS
Resident
Non-Residential Worker
User Defined
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed
the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a
risk-based closure.
Protection of Surface Water Exceedence of 2B at POE?
Exceedence of 2B at POE?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target POE Concentrations Exceeded?
Protection of Groundwater Use Exceedence of 2L at POE?
Exceedence of 2L at POE?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for
lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
APPENDIX E
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APPENDIX F