14007_Bllom Industrial Lagoon Sampling Map-lab rpt 20091210

December 10, 2009
LIMS USE: FR - LAURA MINOR
LIMS OBJECT ID: 9257863
9257863
Project:
Pace Project No.:
RE:
Ms. Laura Minor
Resolve Environmental Services
410 E. Franklin Street
Monroe, NC 28112
BLOOMSBURG MILLS
Dear Ms. Minor:
Enclosed are the analytical results for sample(s) received by the laboratory on November 18, 2009.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
cc:Ms. Laura Minor, Resolve Environmental Services
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Ormond Beach Certification IDs8 East Tower Circle Ormond Beach, FL 32174Alabama Certification #: 41320
Virginia Certification #: 00432Texas Certification: FL NELAC ReciprocityTennessee Certification #: TN02974Puerto Rico Certification #: FL01264Pennsylvania Certification #: 68-547
North Carolina Certification #: 12710New York Certification #: 11608New Jersey Certification #: FL765New Hampshire Certification #: 2958Nevada Certification: FL NELAC Reciprocity
Montana Certification #: Cert 0074Mississippi Certification: FL NELAC Reciprocity
Michigan Certification #: 9911Massachusetts Certification #: M-FL1264
Maine Certification #: FL1264Louisiana Certification #: LA090012Kentucky Certification #: 90050Kansas Certification #: E-10383Hawaii Certification: FL NELAC Reciprocity
Guam Certification: FL NELAC ReciprocityGeorgia Certification #: 955Florida Certification #: E83079Connecticut Certification #: PH 0216Colorado Certification: FL NELAC Reciprocity
Arizona Certification #: AZ0735Wyoming Certification: FL NELAC Reciprocity
Charlotte Certification IDs9800 Kincey Ave. - Ste 100 Huntersville, NC 28078Connecticut Certification #: PH-0104
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784
South Carolina Certification #: 990060001South Carolina Drinking Water Cert. #: 990060003
Tennessee Certification #: 04010Virginia Certification #: 00213West Virginia Certification #: 357
Asheville Certification IDs
Florida/NELAP Certification #: E87648Connecticut Certification #: PH-0106Massachusetts Certification #: M-NC030
New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578
South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Tennessee Certification #: 2980
Virginia Certification #: 00072West Virginia Certification #: 356
2225 Riverside Dr. Asheville, NC 28804Louisiana/LELAP Certification #: 03095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9257863001 GP-1-0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863002 GP-1-3'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863003 GP-2-0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863004 GP-2-1'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863005 GP-3 0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863006 GP-3 2'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863007 GP-4 0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863008 GP-4 4.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863009 GP-5 0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CTNM
9257863010 GP-6 0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9257863011 GP-6 2'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9257863012 GP-7 0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9257863013 GP-7 1.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9257863014 GP-8 0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CJEA
9257863015 GP-8 2'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CKDF
9257863016 GP-9 0.5'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9257863017 GP-9 3'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
EPA 8270 72 PASI-OEAO
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9257863018 GP-10 3'EPA 6010 7 PASI-AJMW
EPA 7470 1 PASI-ASHB
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-0.5'Lab ID:9257863001 Collected:11/17/09 11:13 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 17:21 7440-38-212/09/09 12:300.025
Barium 0.16 mg/L 1 12/09/09 17:21 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 17:21 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 17:21 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 17:21 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 17:21 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 17:21 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:03 7439-97-6 M012/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 14:19 83-32-911/21/09 13:0232.8
Acenaphthylene ND ug/kg 1 12/03/09 14:19 208-96-811/21/09 13:0232.8
Anthracene ND ug/kg 1 12/03/09 14:19 120-12-711/21/09 13:0232.8
Benzo(a)anthracene ND ug/kg 1 12/03/09 14:19 56-55-311/21/09 13:0232.8
Benzo(a)pyrene ND ug/kg 1 12/03/09 14:19 50-32-811/21/09 13:0232.8
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 14:19 205-99-211/21/09 13:0232.8
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 14:19 191-24-211/21/09 13:0232.8
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 14:19 207-08-911/21/09 13:0232.8
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 14:19 101-55-311/21/09 13:02169
Butylbenzylphthalate ND ug/kg 1 12/03/09 14:19 85-68-711/21/09 13:02169
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 14:19 59-50-7 L211/21/09 13:02666
4-Chloroaniline ND ug/kg 1 12/03/09 14:19 106-47-811/21/09 13:02169
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 14:19 111-91-1 L211/21/09 13:02169
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 14:19 111-44-4 L211/21/09 13:02169
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 14:19 108-60-111/21/09 13:02169
2-Chloronaphthalene ND ug/kg 1 12/03/09 14:19 91-58-711/21/09 13:02169
2-Chlorophenol ND ug/kg 1 12/03/09 14:19 95-57-811/21/09 13:02169
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 14:19 7005-72-311/21/09 13:02169
Chrysene ND ug/kg 1 12/03/09 14:19 218-01-911/21/09 13:0232.8
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 14:19 53-70-311/21/09 13:0232.8
Dibenzofuran ND ug/kg 1 12/03/09 14:19 132-64-911/21/09 13:02169
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 14:19 95-50-111/21/09 13:02169
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 14:19 541-73-111/21/09 13:02169
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 14:19 106-46-711/21/09 13:02169
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 14:19 91-94-111/21/09 13:02666
2,4-Dichlorophenol ND ug/kg 1 12/03/09 14:19 120-83-211/21/09 13:02169
Diethylphthalate ND ug/kg 1 12/03/09 14:19 84-66-211/21/09 13:02169
2,4-Dimethylphenol ND ug/kg 1 12/03/09 14:19 105-67-9 L211/21/09 13:02169
Dimethylphthalate ND ug/kg 1 12/03/09 14:19 131-11-311/21/09 13:02169
Di-n-butylphthalate ND ug/kg 1 12/03/09 14:19 84-74-211/21/09 13:02169
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 14:19 534-52-111/21/09 13:02666
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 6 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-0.5'Lab ID:9257863001 Collected:11/17/09 11:13 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 14:19 51-28-511/21/09 13:02666
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 14:19 121-14-211/21/09 13:02169
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 14:19 606-20-211/21/09 13:02169
Di-n-octylphthalate ND ug/kg 1 12/03/09 14:19 117-84-011/21/09 13:02169
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 14:19 122-66-711/21/09 13:02169
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 14:19 117-81-711/21/09 13:02169
Fluoranthene ND ug/kg 1 12/03/09 14:19 206-44-011/21/09 13:0232.8
Fluorene ND ug/kg 1 12/03/09 14:19 86-73-711/21/09 13:0232.8
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 14:19 87-68-311/21/09 13:02169
Hexachlorobenzene ND ug/kg 1 12/03/09 14:19 118-74-111/21/09 13:02169
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 14:19 77-47-411/21/09 13:02666
Hexachloroethane ND ug/kg 1 12/03/09 14:19 67-72-1 L211/21/09 13:02169
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 14:19 193-39-511/21/09 13:0232.8
Isophorone ND ug/kg 1 12/03/09 14:19 78-59-1 L211/21/09 13:02169
1-Methylnaphthalene ND ug/kg 1 12/03/09 14:19 90-12-011/21/09 13:0232.8
2-Methylnaphthalene 34.9 ug/kg 1 12/03/09 14:19 91-57-611/21/09 13:0232.8
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 14:19 95-48-7 L211/21/09 13:02169
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 14:1911/21/09 13:02169
Naphthalene ND ug/kg 1 12/03/09 14:19 91-20-311/21/09 13:0232.8
2-Nitroaniline ND ug/kg 1 12/03/09 14:19 88-74-411/21/09 13:02169
3-Nitroaniline ND ug/kg 1 12/03/09 14:19 99-09-2 L211/21/09 13:02169
4-Nitroaniline ND ug/kg 1 12/03/09 14:19 100-01-611/21/09 13:02169
Nitrobenzene ND ug/kg 1 12/03/09 14:19 98-95-3 L211/21/09 13:02169
2-Nitrophenol ND ug/kg 1 12/03/09 14:19 88-75-511/21/09 13:02169
4-Nitrophenol ND ug/kg 1 12/03/09 14:19 100-02-711/21/09 13:02169
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 14:19 62-75-9 L211/21/09 13:02169
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 14:19 621-64-7 L211/21/09 13:02169
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 14:19 86-30-611/21/09 13:02169
Pentachlorophenol ND ug/kg 1 12/03/09 14:19 87-86-511/21/09 13:02666
Phenanthrene ND ug/kg 1 12/03/09 14:19 85-01-811/21/09 13:0232.8
Phenol ND ug/kg 1 12/03/09 14:19 108-95-2 L211/21/09 13:02169
Pyrene ND ug/kg 1 12/03/09 14:19 129-00-011/21/09 13:0232.8
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 14:19 120-82-111/21/09 13:02169
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 14:19 95-95-411/21/09 13:02169
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 14:19 88-06-211/21/09 13:02169
Nitrobenzene-d5 (S)34 %1 12/03/09 14:19 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)44 %1 12/03/09 14:19 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)57 %1 12/03/09 14:19 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)28 %1 12/03/09 14:19 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)27 %1 12/03/09 14:19 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)51 %1 12/03/09 14:19 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 18:18 67-64-1101
Benzene 9.5 ug/kg 1 11/19/09 18:18 71-43-25.0
Bromobenzene ND ug/kg 1 11/19/09 18:18 108-86-15.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 7 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-0.5'Lab ID:9257863001 Collected:11/17/09 11:13 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 18:18 74-97-55.0
Bromodichloromethane ND ug/kg 1 11/19/09 18:18 75-27-45.0
Bromoform ND ug/kg 1 11/19/09 18:18 75-25-25.0
Bromomethane ND ug/kg 1 11/19/09 18:18 74-83-910.1
2-Butanone (MEK)ND ug/kg 1 11/19/09 18:18 78-93-3101
n-Butylbenzene ND ug/kg 1 11/19/09 18:18 104-51-85.0
sec-Butylbenzene ND ug/kg 1 11/19/09 18:18 135-98-85.0
tert-Butylbenzene ND ug/kg 1 11/19/09 18:18 98-06-65.0
Carbon tetrachloride ND ug/kg 1 11/19/09 18:18 56-23-55.0
Chlorobenzene 110 ug/kg 1 11/19/09 18:18 108-90-75.0
Chloroethane ND ug/kg 1 11/19/09 18:18 75-00-310.1
Chloroform ND ug/kg 1 11/19/09 18:18 67-66-35.0
Chloromethane ND ug/kg 1 11/19/09 18:18 74-87-310.1
2-Chlorotoluene 29.6 ug/kg 1 11/19/09 18:18 95-49-85.0
4-Chlorotoluene ND ug/kg 1 11/19/09 18:18 106-43-45.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 18:18 96-12-85.0
Dibromochloromethane ND ug/kg 1 11/19/09 18:18 124-48-15.0
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 18:18 106-93-45.0
Dibromomethane ND ug/kg 1 11/19/09 18:18 74-95-35.0
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 18:18 95-50-15.0
1,3-Dichlorobenzene 6.8 ug/kg 1 11/19/09 18:18 541-73-15.0
1,4-Dichlorobenzene 24.9 ug/kg 1 11/19/09 18:18 106-46-75.0
Dichlorodifluoromethane ND ug/kg 1 11/19/09 18:18 75-71-810.1
1,1-Dichloroethane ND ug/kg 1 11/19/09 18:18 75-34-35.0
1,2-Dichloroethane ND ug/kg 1 11/19/09 18:18 107-06-25.0
1,1-Dichloroethene ND ug/kg 1 11/19/09 18:18 75-35-45.0
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 18:18 156-59-25.0
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 18:18 156-60-55.0
1,2-Dichloropropane ND ug/kg 1 11/19/09 18:18 78-87-55.0
1,3-Dichloropropane ND ug/kg 1 11/19/09 18:18 142-28-95.0
2,2-Dichloropropane ND ug/kg 1 11/19/09 18:18 594-20-75.0
1,1-Dichloropropene ND ug/kg 1 11/19/09 18:18 563-58-65.0
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 18:18 10061-01-55.0
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 18:18 10061-02-65.0
Diisopropyl ether ND ug/kg 1 11/19/09 18:18 108-20-35.0
Ethylbenzene ND ug/kg 1 11/19/09 18:18 100-41-45.0
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 18:18 87-68-35.0
2-Hexanone ND ug/kg 1 11/19/09 18:18 591-78-650.3
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 18:18 98-82-85.0
p-Isopropyltoluene ND ug/kg 1 11/19/09 18:18 99-87-65.0
Methylene Chloride ND ug/kg 1 11/19/09 18:18 75-09-220.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 18:18 108-10-150.3
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 18:18 1634-04-45.0
Naphthalene ND ug/kg 1 11/19/09 18:18 91-20-35.0
n-Propylbenzene ND ug/kg 1 11/19/09 18:18 103-65-15.0
Styrene ND ug/kg 1 11/19/09 18:18 100-42-55.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 8 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-0.5'Lab ID:9257863001 Collected:11/17/09 11:13 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 18:18 630-20-65.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 18:18 79-34-55.0
Tetrachloroethene ND ug/kg 1 11/19/09 18:18 127-18-45.0
Toluene 10.4 ug/kg 1 11/19/09 18:18 108-88-35.0
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 18:18 87-61-65.0
1,2,4-Trichlorobenzene ND ug/kg 1 11/19/09 18:18 120-82-15.0
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 18:18 71-55-65.0
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 18:18 79-00-55.0
Trichloroethene ND ug/kg 1 11/19/09 18:18 79-01-65.0
Trichlorofluoromethane ND ug/kg 1 11/19/09 18:18 75-69-45.0
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 18:18 96-18-45.0
1,2,4-Trimethylbenzene 5.3 ug/kg 1 11/19/09 18:18 95-63-65.0
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 18:18 108-67-85.0
Vinyl acetate ND ug/kg 1 11/19/09 18:18 108-05-450.3
Vinyl chloride ND ug/kg 1 11/19/09 18:18 75-01-410.1
Xylene (Total)ND ug/kg 1 11/19/09 18:18 1330-20-710.1
m&p-Xylene ND ug/kg 1 11/19/09 18:18 1330-20-710.1
o-Xylene ND ug/kg 1 11/19/09 18:18 95-47-65.0
Dibromofluoromethane (S)108 %1 11/19/09 18:18 1868-53-779-116
Toluene-d8 (S)102 %1 11/19/09 18:18 2037-26-588-110
4-Bromofluorobenzene (S)100 %1 11/19/09 18:18 460-00-474-115
1,2-Dichloroethane-d4 (S)104 %1 11/19/09 18:18 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 19.5 %1 11/19/09 13:350.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 9 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-3'Lab ID:9257863002 Collected:11/17/09 11:15 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 17:29 7440-38-212/09/09 12:300.025
Barium 0.074 mg/L 1 12/09/09 17:29 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 17:29 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 17:29 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 17:29 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 17:29 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 17:29 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:08 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 14:49 83-32-9 R111/21/09 13:0232.5
Acenaphthylene ND ug/kg 1 12/03/09 14:49 208-96-8 R111/21/09 13:0232.5
Anthracene ND ug/kg 1 12/03/09 14:49 120-12-7 R111/21/09 13:0232.5
Benzo(a)anthracene ND ug/kg 1 12/03/09 14:49 56-55-3 R111/21/09 13:0232.5
Benzo(a)pyrene ND ug/kg 1 12/03/09 14:49 50-32-8 R111/21/09 13:0232.5
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 14:49 205-99-2 R111/21/09 13:0232.5
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 14:49 191-24-2 R111/21/09 13:0232.5
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 14:49 207-08-9 R111/21/09 13:0232.5
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 14:49 101-55-3 M0,R111/21/09 13:02167
Butylbenzylphthalate ND ug/kg 1 12/03/09 14:49 85-68-7 M0,R111/21/09 13:02167
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 14:49 59-50-7 L2,M011/21/09 13:02659
4-Chloroaniline ND ug/kg 1 12/03/09 14:49 106-47-8 M0,R111/21/09 13:02167
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 14:49 111-91-1 L2,M0,
R111/21/09 13:02167
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 14:49 111-44-4 L2,M0,
R1
11/21/09 13:02167
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 14:49 108-60-1 M0,R111/21/09 13:02167
2-Chloronaphthalene ND ug/kg 1 12/03/09 14:49 91-58-7 M0,R111/21/09 13:02167
2-Chlorophenol ND ug/kg 1 12/03/09 14:49 95-57-8 M0,R111/21/09 13:02167
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 14:49 7005-72-3 M0,R111/21/09 13:02167
Chrysene ND ug/kg 1 12/03/09 14:49 218-01-9 R111/21/09 13:0232.5
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 14:49 53-70-3 R111/21/09 13:0232.5
Dibenzofuran ND ug/kg 1 12/03/09 14:49 132-64-9 M0,R111/21/09 13:02167
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 14:49 95-50-1 M0,R111/21/09 13:02167
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 14:49 541-73-1 M0,R111/21/09 13:02167
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 14:49 106-46-7 M0,R111/21/09 13:02167
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 14:49 91-94-1 M011/21/09 13:02659
2,4-Dichlorophenol ND ug/kg 1 12/03/09 14:49 120-83-2 M0,R111/21/09 13:02167
Diethylphthalate ND ug/kg 1 12/03/09 14:49 84-66-2 M0,R111/21/09 13:02167
2,4-Dimethylphenol ND ug/kg 1 12/03/09 14:49 105-67-9 L2,M0,
R111/21/09 13:02167
Dimethylphthalate ND ug/kg 1 12/03/09 14:49 131-11-3 M0,R111/21/09 13:02167
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 10 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-3'Lab ID:9257863002 Collected:11/17/09 11:15 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Di-n-butylphthalate ND ug/kg 1 12/03/09 14:49 84-74-2 M0,R111/21/09 13:02167
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 14:49 534-52-1 M011/21/09 13:02659
2,4-Dinitrophenol ND ug/kg 1 12/03/09 14:49 51-28-5 M011/21/09 13:02659
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 14:49 121-14-2 M0,R111/21/09 13:02167
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 14:49 606-20-2 M0,R111/21/09 13:02167
Di-n-octylphthalate ND ug/kg 1 12/03/09 14:49 117-84-0 M0,R111/21/09 13:02167
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 14:49 122-66-7 R111/21/09 13:02167
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 14:49 117-81-7 R111/21/09 13:02167
Fluoranthene ND ug/kg 1 12/03/09 14:49 206-44-0 R111/21/09 13:0232.5
Fluorene ND ug/kg 1 12/03/09 14:49 86-73-7 R111/21/09 13:0232.5
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 14:49 87-68-3 R111/21/09 13:02167
Hexachlorobenzene ND ug/kg 1 12/03/09 14:49 118-74-1 M0,R111/21/09 13:02167
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 14:49 77-47-4 M011/21/09 13:02659
Hexachloroethane ND ug/kg 1 12/03/09 14:49 67-72-1 L2,M0,
R1
11/21/09 13:02167
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 14:49 193-39-5 R111/21/09 13:0232.5
Isophorone ND ug/kg 1 12/03/09 14:49 78-59-1 L2,M0,
R111/21/09 13:02167
1-Methylnaphthalene ND ug/kg 1 12/03/09 14:49 90-12-0 R111/21/09 13:0232.5
2-Methylnaphthalene ND ug/kg 1 12/03/09 14:49 91-57-6 R111/21/09 13:0232.5
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 14:49 95-48-7 L2,M0,
R111/21/09 13:02167
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 14:49 M0,R111/21/09 13:02167
Naphthalene ND ug/kg 1 12/03/09 14:49 91-20-3 R111/21/09 13:0232.5
2-Nitroaniline ND ug/kg 1 12/03/09 14:49 88-74-4 M0,R111/21/09 13:02167
3-Nitroaniline ND ug/kg 1 12/03/09 14:49 99-09-2 L2,M0,
R1
11/21/09 13:02167
4-Nitroaniline ND ug/kg 1 12/03/09 14:49 100-01-6 M0,R111/21/09 13:02167
Nitrobenzene ND ug/kg 1 12/03/09 14:49 98-95-3 L2,M0,
R111/21/09 13:02167
2-Nitrophenol ND ug/kg 1 12/03/09 14:49 88-75-5 M0,R111/21/09 13:02167
4-Nitrophenol ND ug/kg 1 12/03/09 14:49 100-02-7 R111/21/09 13:02167
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 14:49 62-75-9 L2,M0,
R111/21/09 13:02167
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 14:49 621-64-7 L2,M0,
R111/21/09 13:02167
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 14:49 86-30-6 M0,R111/21/09 13:02167
Pentachlorophenol ND ug/kg 1 12/03/09 14:49 87-86-5 M011/21/09 13:02659
Phenanthrene ND ug/kg 1 12/03/09 14:49 85-01-8 R111/21/09 13:0232.5
Phenol ND ug/kg 1 12/03/09 14:49 108-95-2 L2,M0,
R111/21/09 13:02167
Pyrene ND ug/kg 1 12/03/09 14:49 129-00-0 R111/21/09 13:0232.5
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 14:49 120-82-1 M0,R111/21/09 13:02167
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 14:49 95-95-4 M0,R111/21/09 13:02167
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 14:49 88-06-2 M0,R111/21/09 13:02167
Nitrobenzene-d5 (S)41 %1 12/03/09 14:49 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)58 %1 12/03/09 14:49 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)59 %1 12/03/09 14:49 1718-51-011/21/09 13:0210-123
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 11 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-3'Lab ID:9257863002 Collected:11/17/09 11:15 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Phenol-d6 (S)40 %1 12/03/09 14:49 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)39 %1 12/03/09 14:49 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)49 %1 12/03/09 14:49 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 18:37 67-64-196.3
Benzene 25.9 ug/kg 1 11/19/09 18:37 71-43-24.8
Bromobenzene ND ug/kg 1 11/19/09 18:37 108-86-14.8
Bromochloromethane ND ug/kg 1 11/19/09 18:37 74-97-54.8
Bromodichloromethane ND ug/kg 1 11/19/09 18:37 75-27-44.8
Bromoform ND ug/kg 1 11/19/09 18:37 75-25-24.8
Bromomethane ND ug/kg 1 11/19/09 18:37 74-83-99.6
2-Butanone (MEK)ND ug/kg 1 11/19/09 18:37 78-93-396.3
n-Butylbenzene ND ug/kg 1 11/19/09 18:37 104-51-84.8
sec-Butylbenzene ND ug/kg 1 11/19/09 18:37 135-98-84.8
tert-Butylbenzene ND ug/kg 1 11/19/09 18:37 98-06-64.8
Carbon tetrachloride ND ug/kg 1 11/19/09 18:37 56-23-54.8
Chlorobenzene 63.0 ug/kg 1 11/19/09 18:37 108-90-74.8
Chloroethane ND ug/kg 1 11/19/09 18:37 75-00-39.6
Chloroform ND ug/kg 1 11/19/09 18:37 67-66-34.8
Chloromethane ND ug/kg 1 11/19/09 18:37 74-87-39.6
2-Chlorotoluene 5.2 ug/kg 1 11/19/09 18:37 95-49-84.8
4-Chlorotoluene ND ug/kg 1 11/19/09 18:37 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 18:37 96-12-84.8
Dibromochloromethane ND ug/kg 1 11/19/09 18:37 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 18:37 106-93-44.8
Dibromomethane ND ug/kg 1 11/19/09 18:37 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 18:37 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 11/19/09 18:37 541-73-14.8
1,4-Dichlorobenzene 5.9 ug/kg 1 11/19/09 18:37 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 11/19/09 18:37 75-71-89.6
1,1-Dichloroethane ND ug/kg 1 11/19/09 18:37 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 11/19/09 18:37 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 11/19/09 18:37 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 18:37 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 18:37 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 11/19/09 18:37 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 11/19/09 18:37 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 11/19/09 18:37 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 11/19/09 18:37 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 18:37 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 18:37 10061-02-64.8
Diisopropyl ether ND ug/kg 1 11/19/09 18:37 108-20-34.8
Ethylbenzene ND ug/kg 1 11/19/09 18:37 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 18:37 87-68-34.8
2-Hexanone ND ug/kg 1 11/19/09 18:37 591-78-648.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 12 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-1-3'Lab ID:9257863002 Collected:11/17/09 11:15 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 18:37 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 11/19/09 18:37 99-87-64.8
Methylene Chloride ND ug/kg 1 11/19/09 18:37 75-09-219.3
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 18:37 108-10-148.1
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 18:37 1634-04-44.8
Naphthalene ND ug/kg 1 11/19/09 18:37 91-20-34.8
n-Propylbenzene ND ug/kg 1 11/19/09 18:37 103-65-14.8
Styrene ND ug/kg 1 11/19/09 18:37 100-42-54.8
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 18:37 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 18:37 79-34-54.8
Tetrachloroethene ND ug/kg 1 11/19/09 18:37 127-18-44.8
Toluene ND ug/kg 1 11/19/09 18:37 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 18:37 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 11/19/09 18:37 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 18:37 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 18:37 79-00-54.8
Trichloroethene ND ug/kg 1 11/19/09 18:37 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 11/19/09 18:37 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 18:37 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 18:37 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 18:37 108-67-84.8
Vinyl acetate ND ug/kg 1 11/19/09 18:37 108-05-448.1
Vinyl chloride ND ug/kg 1 11/19/09 18:37 75-01-49.6
Xylene (Total)ND ug/kg 1 11/19/09 18:37 1330-20-79.6
m&p-Xylene ND ug/kg 1 11/19/09 18:37 1330-20-79.6
o-Xylene ND ug/kg 1 11/19/09 18:37 95-47-64.8
Dibromofluoromethane (S)99 %1 11/19/09 18:37 1868-53-779-116
Toluene-d8 (S)102 %1 11/19/09 18:37 2037-26-588-110
4-Bromofluorobenzene (S)100 %1 11/19/09 18:37 460-00-474-115
1,2-Dichloroethane-d4 (S)98 %1 11/19/09 18:37 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.7 %1 11/19/09 13:360.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 13 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-0.5'Lab ID:9257863003 Collected:11/17/09 11:20 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 17:35 7440-38-212/09/09 12:300.025
Barium 0.18 mg/L 1 12/09/09 17:35 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 17:35 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 17:35 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 17:35 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 17:35 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 17:35 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:13 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 16:18 83-32-911/21/09 13:0232.7
Acenaphthylene ND ug/kg 1 12/03/09 16:18 208-96-811/21/09 13:0232.7
Anthracene ND ug/kg 1 12/03/09 16:18 120-12-711/21/09 13:0232.7
Benzo(a)anthracene ND ug/kg 1 12/03/09 16:18 56-55-311/21/09 13:0232.7
Benzo(a)pyrene ND ug/kg 1 12/03/09 16:18 50-32-811/21/09 13:0232.7
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 16:18 205-99-211/21/09 13:0232.7
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 16:18 191-24-211/21/09 13:0232.7
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 16:18 207-08-911/21/09 13:0232.7
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 16:18 101-55-311/21/09 13:02168
Butylbenzylphthalate ND ug/kg 1 12/03/09 16:18 85-68-711/21/09 13:02168
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 16:18 59-50-7 L211/21/09 13:02663
4-Chloroaniline ND ug/kg 1 12/03/09 16:18 106-47-811/21/09 13:02168
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 16:18 111-91-1 L211/21/09 13:02168
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 16:18 111-44-4 L211/21/09 13:02168
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 16:18 108-60-111/21/09 13:02168
2-Chloronaphthalene ND ug/kg 1 12/03/09 16:18 91-58-711/21/09 13:02168
2-Chlorophenol ND ug/kg 1 12/03/09 16:18 95-57-811/21/09 13:02168
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 16:18 7005-72-311/21/09 13:02168
Chrysene ND ug/kg 1 12/03/09 16:18 218-01-911/21/09 13:0232.7
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 16:18 53-70-311/21/09 13:0232.7
Dibenzofuran ND ug/kg 1 12/03/09 16:18 132-64-911/21/09 13:02168
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 16:18 95-50-111/21/09 13:02168
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 16:18 541-73-111/21/09 13:02168
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 16:18 106-46-711/21/09 13:02168
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 16:18 91-94-111/21/09 13:02663
2,4-Dichlorophenol ND ug/kg 1 12/03/09 16:18 120-83-211/21/09 13:02168
Diethylphthalate ND ug/kg 1 12/03/09 16:18 84-66-211/21/09 13:02168
2,4-Dimethylphenol ND ug/kg 1 12/03/09 16:18 105-67-9 L211/21/09 13:02168
Dimethylphthalate ND ug/kg 1 12/03/09 16:18 131-11-311/21/09 13:02168
Di-n-butylphthalate ND ug/kg 1 12/03/09 16:18 84-74-211/21/09 13:02168
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 16:18 534-52-111/21/09 13:02663
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 14 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-0.5'Lab ID:9257863003 Collected:11/17/09 11:20 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 16:18 51-28-511/21/09 13:02663
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 16:18 121-14-211/21/09 13:02168
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 16:18 606-20-211/21/09 13:02168
Di-n-octylphthalate ND ug/kg 1 12/03/09 16:18 117-84-011/21/09 13:02168
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 16:18 122-66-711/21/09 13:02168
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 16:18 117-81-711/21/09 13:02168
Fluoranthene ND ug/kg 1 12/03/09 16:18 206-44-011/21/09 13:0232.7
Fluorene ND ug/kg 1 12/03/09 16:18 86-73-711/21/09 13:0232.7
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 16:18 87-68-311/21/09 13:02168
Hexachlorobenzene ND ug/kg 1 12/03/09 16:18 118-74-111/21/09 13:02168
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 16:18 77-47-411/21/09 13:02663
Hexachloroethane ND ug/kg 1 12/03/09 16:18 67-72-1 L211/21/09 13:02168
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 16:18 193-39-511/21/09 13:0232.7
Isophorone ND ug/kg 1 12/03/09 16:18 78-59-1 L211/21/09 13:02168
1-Methylnaphthalene ND ug/kg 1 12/03/09 16:18 90-12-011/21/09 13:0232.7
2-Methylnaphthalene 32.7 ug/kg 1 12/03/09 16:18 91-57-611/21/09 13:0232.7
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 16:18 95-48-7 L211/21/09 13:02168
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 16:1811/21/09 13:02168
Naphthalene ND ug/kg 1 12/03/09 16:18 91-20-311/21/09 13:0232.7
2-Nitroaniline ND ug/kg 1 12/03/09 16:18 88-74-411/21/09 13:02168
3-Nitroaniline ND ug/kg 1 12/03/09 16:18 99-09-2 L211/21/09 13:02168
4-Nitroaniline ND ug/kg 1 12/03/09 16:18 100-01-611/21/09 13:02168
Nitrobenzene ND ug/kg 1 12/03/09 16:18 98-95-3 L211/21/09 13:02168
2-Nitrophenol ND ug/kg 1 12/03/09 16:18 88-75-511/21/09 13:02168
4-Nitrophenol ND ug/kg 1 12/03/09 16:18 100-02-711/21/09 13:02168
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 16:18 62-75-9 L211/21/09 13:02168
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 16:18 621-64-7 L211/21/09 13:02168
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 16:18 86-30-611/21/09 13:02168
Pentachlorophenol ND ug/kg 1 12/03/09 16:18 87-86-511/21/09 13:02663
Phenanthrene ND ug/kg 1 12/03/09 16:18 85-01-811/21/09 13:0232.7
Phenol ND ug/kg 1 12/03/09 16:18 108-95-2 L211/21/09 13:02168
Pyrene ND ug/kg 1 12/03/09 16:18 129-00-011/21/09 13:0232.7
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 16:18 120-82-111/21/09 13:02168
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 16:18 95-95-411/21/09 13:02168
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 16:18 88-06-211/21/09 13:02168
Nitrobenzene-d5 (S)39 %1 12/03/09 16:18 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)51 %1 12/03/09 16:18 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)63 %1 12/03/09 16:18 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)34 %1 12/03/09 16:18 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)31 %1 12/03/09 16:18 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)64 %1 12/03/09 16:18 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 50 11/19/09 23:10 67-64-14640
Benzene 324 ug/kg 50 11/19/09 23:10 71-43-2232
Bromobenzene ND ug/kg 50 11/19/09 23:10 108-86-1232
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 15 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-0.5'Lab ID:9257863003 Collected:11/17/09 11:20 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 50 11/19/09 23:10 74-97-5232
Bromodichloromethane ND ug/kg 50 11/19/09 23:10 75-27-4232
Bromoform ND ug/kg 50 11/19/09 23:10 75-25-2232
Bromomethane ND ug/kg 50 11/19/09 23:10 74-83-9464
2-Butanone (MEK)ND ug/kg 50 11/19/09 23:10 78-93-34640
n-Butylbenzene 278 ug/kg 50 11/19/09 23:10 104-51-8232
sec-Butylbenzene ND ug/kg 50 11/19/09 23:10 135-98-8232
tert-Butylbenzene ND ug/kg 50 11/19/09 23:10 98-06-6232
Carbon tetrachloride ND ug/kg 50 11/19/09 23:10 56-23-5232
Chlorobenzene 2910 ug/kg 50 11/19/09 23:10 108-90-7232
Chloroethane ND ug/kg 50 11/19/09 23:10 75-00-3464
Chloroform ND ug/kg 50 11/19/09 23:10 67-66-3232
Chloromethane ND ug/kg 50 11/19/09 23:10 74-87-3464
2-Chlorotoluene 1900 ug/kg 50 11/19/09 23:10 95-49-8232
4-Chlorotoluene ND ug/kg 50 11/19/09 23:10 106-43-4232
1,2-Dibromo-3-chloropropane ND ug/kg 50 11/19/09 23:10 96-12-8232
Dibromochloromethane ND ug/kg 50 11/19/09 23:10 124-48-1232
1,2-Dibromoethane (EDB)ND ug/kg 50 11/19/09 23:10 106-93-4232
Dibromomethane ND ug/kg 50 11/19/09 23:10 74-95-3232
1,2-Dichlorobenzene ND ug/kg 50 11/19/09 23:10 95-50-1232
1,3-Dichlorobenzene 502 ug/kg 50 11/19/09 23:10 541-73-1232
1,4-Dichlorobenzene 1830 ug/kg 50 11/19/09 23:10 106-46-7232
Dichlorodifluoromethane ND ug/kg 50 11/19/09 23:10 75-71-8464
1,1-Dichloroethane ND ug/kg 50 11/19/09 23:10 75-34-3232
1,2-Dichloroethane ND ug/kg 50 11/19/09 23:10 107-06-2232
1,1-Dichloroethene ND ug/kg 50 11/19/09 23:10 75-35-4232
cis-1,2-Dichloroethene ND ug/kg 50 11/19/09 23:10 156-59-2232
trans-1,2-Dichloroethene ND ug/kg 50 11/19/09 23:10 156-60-5232
1,2-Dichloropropane ND ug/kg 50 11/19/09 23:10 78-87-5232
1,3-Dichloropropane ND ug/kg 50 11/19/09 23:10 142-28-9232
2,2-Dichloropropane ND ug/kg 50 11/19/09 23:10 594-20-7232
1,1-Dichloropropene ND ug/kg 50 11/19/09 23:10 563-58-6232
cis-1,3-Dichloropropene ND ug/kg 50 11/19/09 23:10 10061-01-5232
trans-1,3-Dichloropropene ND ug/kg 50 11/19/09 23:10 10061-02-6232
Diisopropyl ether ND ug/kg 50 11/19/09 23:10 108-20-3232
Ethylbenzene ND ug/kg 50 11/19/09 23:10 100-41-4232
Hexachloro-1,3-butadiene ND ug/kg 50 11/19/09 23:10 87-68-3232
2-Hexanone ND ug/kg 50 11/19/09 23:10 591-78-62320
Isopropylbenzene (Cumene)ND ug/kg 50 11/19/09 23:10 98-82-8232
p-Isopropyltoluene ND ug/kg 50 11/19/09 23:10 99-87-6232
Methylene Chloride ND ug/kg 50 11/19/09 23:10 75-09-2929
4-Methyl-2-pentanone (MIBK)ND ug/kg 50 11/19/09 23:10 108-10-12320
Methyl-tert-butyl ether ND ug/kg 50 11/19/09 23:10 1634-04-4232
Naphthalene 388 ug/kg 50 11/19/09 23:10 91-20-3232
n-Propylbenzene ND ug/kg 50 11/19/09 23:10 103-65-1232
Styrene ND ug/kg 50 11/19/09 23:10 100-42-5232
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 16 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-0.5'Lab ID:9257863003 Collected:11/17/09 11:20 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 50 11/19/09 23:10 630-20-6232
1,1,2,2-Tetrachloroethane ND ug/kg 50 11/19/09 23:10 79-34-5232
Tetrachloroethene ND ug/kg 50 11/19/09 23:10 127-18-4232
Toluene 484 ug/kg 50 11/19/09 23:10 108-88-3232
1,2,3-Trichlorobenzene ND ug/kg 50 11/19/09 23:10 87-61-6232
1,2,4-Trichlorobenzene 330 ug/kg 50 11/19/09 23:10 120-82-1232
1,1,1-Trichloroethane ND ug/kg 50 11/19/09 23:10 71-55-6232
1,1,2-Trichloroethane ND ug/kg 50 11/19/09 23:10 79-00-5232
Trichloroethene ND ug/kg 50 11/19/09 23:10 79-01-6232
Trichlorofluoromethane ND ug/kg 50 11/19/09 23:10 75-69-4232
1,2,3-Trichloropropane ND ug/kg 50 11/19/09 23:10 96-18-4232
1,2,4-Trimethylbenzene 476 ug/kg 50 11/19/09 23:10 95-63-6232
1,3,5-Trimethylbenzene 271 ug/kg 50 11/19/09 23:10 108-67-8232
Vinyl acetate ND ug/kg 50 11/19/09 23:10 108-05-42320
Vinyl chloride ND ug/kg 50 11/19/09 23:10 75-01-4464
Xylene (Total)ND ug/kg 50 11/19/09 23:10 1330-20-7464
m&p-Xylene ND ug/kg 50 11/19/09 23:10 1330-20-7464
o-Xylene ND ug/kg 50 11/19/09 23:10 95-47-6232
Dibromofluoromethane (S)98 %50 11/19/09 23:10 1868-53-7 D379-116
Toluene-d8 (S)101 %50 11/19/09 23:10 2037-26-588-110
4-Bromofluorobenzene (S)97 %50 11/19/09 23:10 460-00-474-115
1,2-Dichloroethane-d4 (S)104 %50 11/19/09 23:10 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.0 %1 11/19/09 13:360.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 17 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-1'Lab ID:9257863004 Collected:11/17/09 11:24 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 17:39 7440-38-212/09/09 12:300.025
Barium 0.064 mg/L 1 12/09/09 17:39 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 17:39 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 17:39 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 17:39 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 17:39 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 17:39 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:16 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 16:47 83-32-911/21/09 13:0232.9
Acenaphthylene ND ug/kg 1 12/03/09 16:47 208-96-811/21/09 13:0232.9
Anthracene ND ug/kg 1 12/03/09 16:47 120-12-711/21/09 13:0232.9
Benzo(a)anthracene ND ug/kg 1 12/03/09 16:47 56-55-311/21/09 13:0232.9
Benzo(a)pyrene ND ug/kg 1 12/03/09 16:47 50-32-811/21/09 13:0232.9
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 16:47 205-99-211/21/09 13:0232.9
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 16:47 191-24-211/21/09 13:0232.9
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 16:47 207-08-911/21/09 13:0232.9
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 16:47 101-55-311/21/09 13:02169
Butylbenzylphthalate ND ug/kg 1 12/03/09 16:47 85-68-711/21/09 13:02169
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 16:47 59-50-7 L211/21/09 13:02668
4-Chloroaniline ND ug/kg 1 12/03/09 16:47 106-47-811/21/09 13:02169
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 16:47 111-91-1 L211/21/09 13:02169
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 16:47 111-44-4 L211/21/09 13:02169
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 16:47 108-60-111/21/09 13:02169
2-Chloronaphthalene ND ug/kg 1 12/03/09 16:47 91-58-711/21/09 13:02169
2-Chlorophenol ND ug/kg 1 12/03/09 16:47 95-57-811/21/09 13:02169
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 16:47 7005-72-311/21/09 13:02169
Chrysene ND ug/kg 1 12/03/09 16:47 218-01-911/21/09 13:0232.9
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 16:47 53-70-311/21/09 13:0232.9
Dibenzofuran ND ug/kg 1 12/03/09 16:47 132-64-911/21/09 13:02169
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 16:47 95-50-111/21/09 13:02169
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 16:47 541-73-111/21/09 13:02169
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 16:47 106-46-711/21/09 13:02169
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 16:47 91-94-111/21/09 13:02668
2,4-Dichlorophenol ND ug/kg 1 12/03/09 16:47 120-83-211/21/09 13:02169
Diethylphthalate ND ug/kg 1 12/03/09 16:47 84-66-211/21/09 13:02169
2,4-Dimethylphenol ND ug/kg 1 12/03/09 16:47 105-67-9 L211/21/09 13:02169
Dimethylphthalate ND ug/kg 1 12/03/09 16:47 131-11-311/21/09 13:02169
Di-n-butylphthalate ND ug/kg 1 12/03/09 16:47 84-74-211/21/09 13:02169
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 16:47 534-52-111/21/09 13:02668
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 18 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-1'Lab ID:9257863004 Collected:11/17/09 11:24 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 16:47 51-28-511/21/09 13:02668
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 16:47 121-14-211/21/09 13:02169
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 16:47 606-20-211/21/09 13:02169
Di-n-octylphthalate ND ug/kg 1 12/03/09 16:47 117-84-011/21/09 13:02169
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 16:47 122-66-711/21/09 13:02169
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 16:47 117-81-711/21/09 13:02169
Fluoranthene ND ug/kg 1 12/03/09 16:47 206-44-011/21/09 13:0232.9
Fluorene ND ug/kg 1 12/03/09 16:47 86-73-711/21/09 13:0232.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 16:47 87-68-311/21/09 13:02169
Hexachlorobenzene ND ug/kg 1 12/03/09 16:47 118-74-111/21/09 13:02169
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 16:47 77-47-411/21/09 13:02668
Hexachloroethane ND ug/kg 1 12/03/09 16:47 67-72-1 L211/21/09 13:02169
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 16:47 193-39-511/21/09 13:0232.9
Isophorone ND ug/kg 1 12/03/09 16:47 78-59-1 L211/21/09 13:02169
1-Methylnaphthalene ND ug/kg 1 12/03/09 16:47 90-12-011/21/09 13:0232.9
2-Methylnaphthalene ND ug/kg 1 12/03/09 16:47 91-57-611/21/09 13:0232.9
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 16:47 95-48-7 L211/21/09 13:02169
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 16:4711/21/09 13:02169
Naphthalene ND ug/kg 1 12/03/09 16:47 91-20-311/21/09 13:0232.9
2-Nitroaniline ND ug/kg 1 12/03/09 16:47 88-74-411/21/09 13:02169
3-Nitroaniline ND ug/kg 1 12/03/09 16:47 99-09-2 L211/21/09 13:02169
4-Nitroaniline ND ug/kg 1 12/03/09 16:47 100-01-611/21/09 13:02169
Nitrobenzene ND ug/kg 1 12/03/09 16:47 98-95-3 L211/21/09 13:02169
2-Nitrophenol ND ug/kg 1 12/03/09 16:47 88-75-511/21/09 13:02169
4-Nitrophenol ND ug/kg 1 12/03/09 16:47 100-02-711/21/09 13:02169
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 16:47 62-75-9 L211/21/09 13:02169
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 16:47 621-64-7 L211/21/09 13:02169
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 16:47 86-30-611/21/09 13:02169
Pentachlorophenol ND ug/kg 1 12/03/09 16:47 87-86-511/21/09 13:02668
Phenanthrene ND ug/kg 1 12/03/09 16:47 85-01-811/21/09 13:0232.9
Phenol ND ug/kg 1 12/03/09 16:47 108-95-2 L211/21/09 13:02169
Pyrene ND ug/kg 1 12/03/09 16:47 129-00-011/21/09 13:0232.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 16:47 120-82-111/21/09 13:02169
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 16:47 95-95-411/21/09 13:02169
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 16:47 88-06-211/21/09 13:02169
Nitrobenzene-d5 (S)45 %1 12/03/09 16:47 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)56 %1 12/03/09 16:47 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)80 %1 12/03/09 16:47 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)40 %1 12/03/09 16:47 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)41 %1 12/03/09 16:47 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)56 %1 12/03/09 16:47 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 18:55 67-64-1138
Benzene ND ug/kg 1 11/19/09 18:55 71-43-26.9
Bromobenzene ND ug/kg 1 11/19/09 18:55 108-86-16.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 19 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-1'Lab ID:9257863004 Collected:11/17/09 11:24 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 18:55 74-97-56.9
Bromodichloromethane ND ug/kg 1 11/19/09 18:55 75-27-46.9
Bromoform ND ug/kg 1 11/19/09 18:55 75-25-26.9
Bromomethane ND ug/kg 1 11/19/09 18:55 74-83-913.8
2-Butanone (MEK)ND ug/kg 1 11/19/09 18:55 78-93-3138
n-Butylbenzene ND ug/kg 1 11/19/09 18:55 104-51-86.9
sec-Butylbenzene ND ug/kg 1 11/19/09 18:55 135-98-86.9
tert-Butylbenzene ND ug/kg 1 11/19/09 18:55 98-06-66.9
Carbon tetrachloride ND ug/kg 1 11/19/09 18:55 56-23-56.9
Chlorobenzene ND ug/kg 1 11/19/09 18:55 108-90-76.9
Chloroethane ND ug/kg 1 11/19/09 18:55 75-00-313.8
Chloroform ND ug/kg 1 11/19/09 18:55 67-66-36.9
Chloromethane ND ug/kg 1 11/19/09 18:55 74-87-313.8
2-Chlorotoluene ND ug/kg 1 11/19/09 18:55 95-49-86.9
4-Chlorotoluene ND ug/kg 1 11/19/09 18:55 106-43-46.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 18:55 96-12-86.9
Dibromochloromethane ND ug/kg 1 11/19/09 18:55 124-48-16.9
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 18:55 106-93-46.9
Dibromomethane ND ug/kg 1 11/19/09 18:55 74-95-36.9
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 18:55 95-50-16.9
1,3-Dichlorobenzene ND ug/kg 1 11/19/09 18:55 541-73-16.9
1,4-Dichlorobenzene ND ug/kg 1 11/19/09 18:55 106-46-76.9
Dichlorodifluoromethane ND ug/kg 1 11/19/09 18:55 75-71-813.8
1,1-Dichloroethane ND ug/kg 1 11/19/09 18:55 75-34-36.9
1,2-Dichloroethane ND ug/kg 1 11/19/09 18:55 107-06-26.9
1,1-Dichloroethene ND ug/kg 1 11/19/09 18:55 75-35-46.9
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 18:55 156-59-26.9
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 18:55 156-60-56.9
1,2-Dichloropropane ND ug/kg 1 11/19/09 18:55 78-87-56.9
1,3-Dichloropropane ND ug/kg 1 11/19/09 18:55 142-28-96.9
2,2-Dichloropropane ND ug/kg 1 11/19/09 18:55 594-20-76.9
1,1-Dichloropropene ND ug/kg 1 11/19/09 18:55 563-58-66.9
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 18:55 10061-01-56.9
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 18:55 10061-02-66.9
Diisopropyl ether ND ug/kg 1 11/19/09 18:55 108-20-36.9
Ethylbenzene ND ug/kg 1 11/19/09 18:55 100-41-46.9
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 18:55 87-68-36.9
2-Hexanone ND ug/kg 1 11/19/09 18:55 591-78-668.8
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 18:55 98-82-86.9
p-Isopropyltoluene ND ug/kg 1 11/19/09 18:55 99-87-66.9
Methylene Chloride ND ug/kg 1 11/19/09 18:55 75-09-227.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 18:55 108-10-168.8
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 18:55 1634-04-46.9
Naphthalene ND ug/kg 1 11/19/09 18:55 91-20-36.9
n-Propylbenzene ND ug/kg 1 11/19/09 18:55 103-65-16.9
Styrene ND ug/kg 1 11/19/09 18:55 100-42-56.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 20 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-2-1'Lab ID:9257863004 Collected:11/17/09 11:24 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 18:55 630-20-66.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 18:55 79-34-56.9
Tetrachloroethene ND ug/kg 1 11/19/09 18:55 127-18-46.9
Toluene ND ug/kg 1 11/19/09 18:55 108-88-36.9
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 18:55 87-61-66.9
1,2,4-Trichlorobenzene ND ug/kg 1 11/19/09 18:55 120-82-16.9
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 18:55 71-55-66.9
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 18:55 79-00-56.9
Trichloroethene ND ug/kg 1 11/19/09 18:55 79-01-66.9
Trichlorofluoromethane ND ug/kg 1 11/19/09 18:55 75-69-46.9
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 18:55 96-18-46.9
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 18:55 95-63-66.9
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 18:55 108-67-86.9
Vinyl acetate ND ug/kg 1 11/19/09 18:55 108-05-468.8
Vinyl chloride ND ug/kg 1 11/19/09 18:55 75-01-413.8
Xylene (Total)ND ug/kg 1 11/19/09 18:55 1330-20-713.8
m&p-Xylene ND ug/kg 1 11/19/09 18:55 1330-20-713.8
o-Xylene ND ug/kg 1 11/19/09 18:55 95-47-66.9
Dibromofluoromethane (S)109 %1 11/19/09 18:55 1868-53-779-116
Toluene-d8 (S)96 %1 11/19/09 18:55 2037-26-588-110
4-Bromofluorobenzene (S)99 %1 11/19/09 18:55 460-00-474-115
1,2-Dichloroethane-d4 (S)107 %1 11/19/09 18:55 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 4.9 %1 11/19/09 13:360.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 21 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 0.5'Lab ID:9257863005 Collected:11/17/09 11:35 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 17:43 7440-38-212/09/09 12:300.025
Barium 0.14 mg/L 1 12/09/09 17:43 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 17:43 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 17:43 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 17:43 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 17:43 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 17:43 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:18 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 17:17 83-32-911/21/09 13:0232.5
Acenaphthylene ND ug/kg 1 12/03/09 17:17 208-96-811/21/09 13:0232.5
Anthracene ND ug/kg 1 12/03/09 17:17 120-12-711/21/09 13:0232.5
Benzo(a)anthracene ND ug/kg 1 12/03/09 17:17 56-55-311/21/09 13:0232.5
Benzo(a)pyrene ND ug/kg 1 12/03/09 17:17 50-32-811/21/09 13:0232.5
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 17:17 205-99-211/21/09 13:0232.5
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 17:17 191-24-211/21/09 13:0232.5
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 17:17 207-08-911/21/09 13:0232.5
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 17:17 101-55-311/21/09 13:02167
Butylbenzylphthalate ND ug/kg 1 12/03/09 17:17 85-68-711/21/09 13:02167
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 17:17 59-50-7 L211/21/09 13:02659
4-Chloroaniline ND ug/kg 1 12/03/09 17:17 106-47-811/21/09 13:02167
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 17:17 111-91-1 L211/21/09 13:02167
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 17:17 111-44-4 L211/21/09 13:02167
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 17:17 108-60-111/21/09 13:02167
2-Chloronaphthalene ND ug/kg 1 12/03/09 17:17 91-58-711/21/09 13:02167
2-Chlorophenol ND ug/kg 1 12/03/09 17:17 95-57-811/21/09 13:02167
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 17:17 7005-72-311/21/09 13:02167
Chrysene ND ug/kg 1 12/03/09 17:17 218-01-911/21/09 13:0232.5
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 17:17 53-70-311/21/09 13:0232.5
Dibenzofuran ND ug/kg 1 12/03/09 17:17 132-64-911/21/09 13:02167
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 17:17 95-50-111/21/09 13:02167
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 17:17 541-73-111/21/09 13:02167
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 17:17 106-46-711/21/09 13:02167
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 17:17 91-94-111/21/09 13:02659
2,4-Dichlorophenol ND ug/kg 1 12/03/09 17:17 120-83-211/21/09 13:02167
Diethylphthalate ND ug/kg 1 12/03/09 17:17 84-66-211/21/09 13:02167
2,4-Dimethylphenol ND ug/kg 1 12/03/09 17:17 105-67-9 L211/21/09 13:02167
Dimethylphthalate ND ug/kg 1 12/03/09 17:17 131-11-311/21/09 13:02167
Di-n-butylphthalate ND ug/kg 1 12/03/09 17:17 84-74-211/21/09 13:02167
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 17:17 534-52-111/21/09 13:02659
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 22 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 0.5'Lab ID:9257863005 Collected:11/17/09 11:35 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 17:17 51-28-511/21/09 13:02659
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 17:17 121-14-211/21/09 13:02167
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 17:17 606-20-211/21/09 13:02167
Di-n-octylphthalate ND ug/kg 1 12/03/09 17:17 117-84-011/21/09 13:02167
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 17:17 122-66-711/21/09 13:02167
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 17:17 117-81-711/21/09 13:02167
Fluoranthene ND ug/kg 1 12/03/09 17:17 206-44-011/21/09 13:0232.5
Fluorene ND ug/kg 1 12/03/09 17:17 86-73-711/21/09 13:0232.5
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 17:17 87-68-311/21/09 13:02167
Hexachlorobenzene ND ug/kg 1 12/03/09 17:17 118-74-111/21/09 13:02167
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 17:17 77-47-411/21/09 13:02659
Hexachloroethane ND ug/kg 1 12/03/09 17:17 67-72-1 L211/21/09 13:02167
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 17:17 193-39-511/21/09 13:0232.5
Isophorone ND ug/kg 1 12/03/09 17:17 78-59-1 L211/21/09 13:02167
1-Methylnaphthalene ND ug/kg 1 12/03/09 17:17 90-12-011/21/09 13:0232.5
2-Methylnaphthalene ND ug/kg 1 12/03/09 17:17 91-57-611/21/09 13:0232.5
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 17:17 95-48-7 L211/21/09 13:02167
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 17:1711/21/09 13:02167
Naphthalene ND ug/kg 1 12/03/09 17:17 91-20-311/21/09 13:0232.5
2-Nitroaniline ND ug/kg 1 12/03/09 17:17 88-74-411/21/09 13:02167
3-Nitroaniline ND ug/kg 1 12/03/09 17:17 99-09-2 L211/21/09 13:02167
4-Nitroaniline ND ug/kg 1 12/03/09 17:17 100-01-611/21/09 13:02167
Nitrobenzene ND ug/kg 1 12/03/09 17:17 98-95-3 L211/21/09 13:02167
2-Nitrophenol ND ug/kg 1 12/03/09 17:17 88-75-511/21/09 13:02167
4-Nitrophenol ND ug/kg 1 12/03/09 17:17 100-02-711/21/09 13:02167
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 17:17 62-75-9 L211/21/09 13:02167
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 17:17 621-64-7 L211/21/09 13:02167
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 17:17 86-30-611/21/09 13:02167
Pentachlorophenol ND ug/kg 1 12/03/09 17:17 87-86-511/21/09 13:02659
Phenanthrene ND ug/kg 1 12/03/09 17:17 85-01-811/21/09 13:0232.5
Phenol ND ug/kg 1 12/03/09 17:17 108-95-2 L211/21/09 13:02167
Pyrene ND ug/kg 1 12/03/09 17:17 129-00-011/21/09 13:0232.5
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 17:17 120-82-111/21/09 13:02167
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 17:17 95-95-411/21/09 13:02167
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 17:17 88-06-211/21/09 13:02167
Nitrobenzene-d5 (S)35 %1 12/03/09 17:17 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)50 %1 12/03/09 17:17 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)67 %1 12/03/09 17:17 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)31 %1 12/03/09 17:17 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)32 %1 12/03/09 17:17 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)69 %1 12/03/09 17:17 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 19:13 67-64-191.0
Benzene 6.8 ug/kg 1 11/19/09 19:13 71-43-24.5
Bromobenzene ND ug/kg 1 11/19/09 19:13 108-86-14.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 23 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 0.5'Lab ID:9257863005 Collected:11/17/09 11:35 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 19:13 74-97-54.5
Bromodichloromethane ND ug/kg 1 11/19/09 19:13 75-27-44.5
Bromoform ND ug/kg 1 11/19/09 19:13 75-25-24.5
Bromomethane ND ug/kg 1 11/19/09 19:13 74-83-99.1
2-Butanone (MEK)ND ug/kg 1 11/19/09 19:13 78-93-391.0
n-Butylbenzene ND ug/kg 1 11/19/09 19:13 104-51-84.5
sec-Butylbenzene ND ug/kg 1 11/19/09 19:13 135-98-84.5
tert-Butylbenzene ND ug/kg 1 11/19/09 19:13 98-06-64.5
Carbon tetrachloride ND ug/kg 1 11/19/09 19:13 56-23-54.5
Chlorobenzene 110 ug/kg 1 11/19/09 19:13 108-90-74.5
Chloroethane ND ug/kg 1 11/19/09 19:13 75-00-39.1
Chloroform ND ug/kg 1 11/19/09 19:13 67-66-34.5
Chloromethane ND ug/kg 1 11/19/09 19:13 74-87-39.1
2-Chlorotoluene 80.4 ug/kg 1 11/19/09 19:13 95-49-84.5
4-Chlorotoluene ND ug/kg 1 11/19/09 19:13 106-43-44.5
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 19:13 96-12-84.5
Dibromochloromethane ND ug/kg 1 11/19/09 19:13 124-48-14.5
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 19:13 106-93-44.5
Dibromomethane ND ug/kg 1 11/19/09 19:13 74-95-34.5
1,2-Dichlorobenzene 4.7 ug/kg 1 11/19/09 19:13 95-50-14.5
1,3-Dichlorobenzene 14.6 ug/kg 1 11/19/09 19:13 541-73-14.5
1,4-Dichlorobenzene 51.7 ug/kg 1 11/19/09 19:13 106-46-74.5
Dichlorodifluoromethane ND ug/kg 1 11/19/09 19:13 75-71-89.1
1,1-Dichloroethane ND ug/kg 1 11/19/09 19:13 75-34-34.5
1,2-Dichloroethane ND ug/kg 1 11/19/09 19:13 107-06-24.5
1,1-Dichloroethene ND ug/kg 1 11/19/09 19:13 75-35-44.5
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 19:13 156-59-24.5
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 19:13 156-60-54.5
1,2-Dichloropropane ND ug/kg 1 11/19/09 19:13 78-87-54.5
1,3-Dichloropropane ND ug/kg 1 11/19/09 19:13 142-28-94.5
2,2-Dichloropropane ND ug/kg 1 11/19/09 19:13 594-20-74.5
1,1-Dichloropropene ND ug/kg 1 11/19/09 19:13 563-58-64.5
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 19:13 10061-01-54.5
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 19:13 10061-02-64.5
Diisopropyl ether ND ug/kg 1 11/19/09 19:13 108-20-34.5
Ethylbenzene ND ug/kg 1 11/19/09 19:13 100-41-44.5
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 19:13 87-68-34.5
2-Hexanone ND ug/kg 1 11/19/09 19:13 591-78-645.5
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 19:13 98-82-84.5
p-Isopropyltoluene ND ug/kg 1 11/19/09 19:13 99-87-64.5
Methylene Chloride ND ug/kg 1 11/19/09 19:13 75-09-218.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 19:13 108-10-145.5
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 19:13 1634-04-44.5
Naphthalene 10.2 ug/kg 1 11/19/09 19:13 91-20-34.5
n-Propylbenzene ND ug/kg 1 11/19/09 19:13 103-65-14.5
Styrene ND ug/kg 1 11/19/09 19:13 100-42-54.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 24 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 0.5'Lab ID:9257863005 Collected:11/17/09 11:35 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 19:13 630-20-64.5
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 19:13 79-34-54.5
Tetrachloroethene 52.5 ug/kg 1 11/19/09 19:13 127-18-44.5
Toluene 5.7 ug/kg 1 11/19/09 19:13 108-88-34.5
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 19:13 87-61-64.5
1,2,4-Trichlorobenzene 18.1 ug/kg 1 11/19/09 19:13 120-82-14.5
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 19:13 71-55-64.5
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 19:13 79-00-54.5
Trichloroethene ND ug/kg 1 11/19/09 19:13 79-01-64.5
Trichlorofluoromethane ND ug/kg 1 11/19/09 19:13 75-69-44.5
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 19:13 96-18-44.5
1,2,4-Trimethylbenzene 9.6 ug/kg 1 11/19/09 19:13 95-63-64.5
1,3,5-Trimethylbenzene 4.7 ug/kg 1 11/19/09 19:13 108-67-84.5
Vinyl acetate ND ug/kg 1 11/19/09 19:13 108-05-445.5
Vinyl chloride ND ug/kg 1 11/19/09 19:13 75-01-49.1
Xylene (Total)ND ug/kg 1 11/19/09 19:13 1330-20-79.1
m&p-Xylene ND ug/kg 1 11/19/09 19:13 1330-20-79.1
o-Xylene ND ug/kg 1 11/19/09 19:13 95-47-64.5
Dibromofluoromethane (S)111 %1 11/19/09 19:13 1868-53-779-116
Toluene-d8 (S)96 %1 11/19/09 19:13 2037-26-588-110
4-Bromofluorobenzene (S)95 %1 11/19/09 19:13 460-00-474-115
1,2-Dichloroethane-d4 (S)110 %1 11/19/09 19:13 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.8 %1 11/19/09 13:360.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 25 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 2'Lab ID:9257863006 Collected:11/17/09 11:42 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 17:46 7440-38-212/09/09 12:300.025
Barium 0.087 mg/L 1 12/09/09 17:46 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 17:46 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 17:46 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 17:46 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 17:46 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 17:46 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:21 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 17:47 83-32-911/21/09 13:0232.2
Acenaphthylene ND ug/kg 1 12/03/09 17:47 208-96-811/21/09 13:0232.2
Anthracene ND ug/kg 1 12/03/09 17:47 120-12-711/21/09 13:0232.2
Benzo(a)anthracene ND ug/kg 1 12/03/09 17:47 56-55-311/21/09 13:0232.2
Benzo(a)pyrene ND ug/kg 1 12/03/09 17:47 50-32-811/21/09 13:0232.2
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 17:47 205-99-211/21/09 13:0232.2
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 17:47 191-24-211/21/09 13:0232.2
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 17:47 207-08-911/21/09 13:0232.2
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 17:47 101-55-311/21/09 13:02166
Butylbenzylphthalate ND ug/kg 1 12/03/09 17:47 85-68-711/21/09 13:02166
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 17:47 59-50-7 L211/21/09 13:02655
4-Chloroaniline ND ug/kg 1 12/03/09 17:47 106-47-811/21/09 13:02166
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 17:47 111-91-1 L211/21/09 13:02166
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 17:47 111-44-4 L211/21/09 13:02166
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 17:47 108-60-111/21/09 13:02166
2-Chloronaphthalene ND ug/kg 1 12/03/09 17:47 91-58-711/21/09 13:02166
2-Chlorophenol ND ug/kg 1 12/03/09 17:47 95-57-811/21/09 13:02166
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 17:47 7005-72-311/21/09 13:02166
Chrysene ND ug/kg 1 12/03/09 17:47 218-01-911/21/09 13:0232.2
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 17:47 53-70-311/21/09 13:0232.2
Dibenzofuran ND ug/kg 1 12/03/09 17:47 132-64-911/21/09 13:02166
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 17:47 95-50-111/21/09 13:02166
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 17:47 541-73-111/21/09 13:02166
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 17:47 106-46-711/21/09 13:02166
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 17:47 91-94-111/21/09 13:02655
2,4-Dichlorophenol ND ug/kg 1 12/03/09 17:47 120-83-211/21/09 13:02166
Diethylphthalate ND ug/kg 1 12/03/09 17:47 84-66-211/21/09 13:02166
2,4-Dimethylphenol ND ug/kg 1 12/03/09 17:47 105-67-9 L211/21/09 13:02166
Dimethylphthalate ND ug/kg 1 12/03/09 17:47 131-11-311/21/09 13:02166
Di-n-butylphthalate ND ug/kg 1 12/03/09 17:47 84-74-211/21/09 13:02166
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 17:47 534-52-111/21/09 13:02655
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 26 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 2'Lab ID:9257863006 Collected:11/17/09 11:42 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 17:47 51-28-511/21/09 13:02655
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 17:47 121-14-211/21/09 13:02166
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 17:47 606-20-211/21/09 13:02166
Di-n-octylphthalate ND ug/kg 1 12/03/09 17:47 117-84-011/21/09 13:02166
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 17:47 122-66-711/21/09 13:02166
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 17:47 117-81-711/21/09 13:02166
Fluoranthene ND ug/kg 1 12/03/09 17:47 206-44-011/21/09 13:0232.2
Fluorene ND ug/kg 1 12/03/09 17:47 86-73-711/21/09 13:0232.2
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 17:47 87-68-311/21/09 13:02166
Hexachlorobenzene ND ug/kg 1 12/03/09 17:47 118-74-111/21/09 13:02166
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 17:47 77-47-411/21/09 13:02655
Hexachloroethane ND ug/kg 1 12/03/09 17:47 67-72-1 L211/21/09 13:02166
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 17:47 193-39-511/21/09 13:0232.2
Isophorone ND ug/kg 1 12/03/09 17:47 78-59-1 L211/21/09 13:02166
1-Methylnaphthalene ND ug/kg 1 12/03/09 17:47 90-12-011/21/09 13:0232.2
2-Methylnaphthalene ND ug/kg 1 12/03/09 17:47 91-57-611/21/09 13:0232.2
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 17:47 95-48-7 L211/21/09 13:02166
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 17:4711/21/09 13:02166
Naphthalene ND ug/kg 1 12/03/09 17:47 91-20-311/21/09 13:0232.2
2-Nitroaniline ND ug/kg 1 12/03/09 17:47 88-74-411/21/09 13:02166
3-Nitroaniline ND ug/kg 1 12/03/09 17:47 99-09-2 L211/21/09 13:02166
4-Nitroaniline ND ug/kg 1 12/03/09 17:47 100-01-611/21/09 13:02166
Nitrobenzene ND ug/kg 1 12/03/09 17:47 98-95-3 L211/21/09 13:02166
2-Nitrophenol ND ug/kg 1 12/03/09 17:47 88-75-511/21/09 13:02166
4-Nitrophenol ND ug/kg 1 12/03/09 17:47 100-02-711/21/09 13:02166
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 17:47 62-75-9 L211/21/09 13:02166
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 17:47 621-64-7 L211/21/09 13:02166
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 17:47 86-30-611/21/09 13:02166
Pentachlorophenol ND ug/kg 1 12/03/09 17:47 87-86-511/21/09 13:02655
Phenanthrene ND ug/kg 1 12/03/09 17:47 85-01-811/21/09 13:0232.2
Phenol ND ug/kg 1 12/03/09 17:47 108-95-2 L211/21/09 13:02166
Pyrene ND ug/kg 1 12/03/09 17:47 129-00-011/21/09 13:0232.2
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 17:47 120-82-111/21/09 13:02166
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 17:47 95-95-411/21/09 13:02166
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 17:47 88-06-211/21/09 13:02166
Nitrobenzene-d5 (S)37 %1 12/03/09 17:47 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)47 %1 12/03/09 17:47 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)64 %1 12/03/09 17:47 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)32 %1 12/03/09 17:47 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)35 %1 12/03/09 17:47 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)43 %1 12/03/09 17:47 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 22:34 67-64-188.8
Benzene ND ug/kg 1 11/19/09 22:34 71-43-24.4
Bromobenzene ND ug/kg 1 11/19/09 22:34 108-86-14.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 27 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 2'Lab ID:9257863006 Collected:11/17/09 11:42 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 22:34 74-97-54.4
Bromodichloromethane ND ug/kg 1 11/19/09 22:34 75-27-44.4
Bromoform ND ug/kg 1 11/19/09 22:34 75-25-24.4
Bromomethane ND ug/kg 1 11/19/09 22:34 74-83-98.9
2-Butanone (MEK)ND ug/kg 1 11/19/09 22:34 78-93-388.8
n-Butylbenzene ND ug/kg 1 11/19/09 22:34 104-51-84.4
sec-Butylbenzene ND ug/kg 1 11/19/09 22:34 135-98-84.4
tert-Butylbenzene ND ug/kg 1 11/19/09 22:34 98-06-64.4
Carbon tetrachloride ND ug/kg 1 11/19/09 22:34 56-23-54.4
Chlorobenzene 64.4 ug/kg 1 11/19/09 22:34 108-90-74.4
Chloroethane ND ug/kg 1 11/19/09 22:34 75-00-38.9
Chloroform ND ug/kg 1 11/19/09 22:34 67-66-34.4
Chloromethane ND ug/kg 1 11/19/09 22:34 74-87-38.9
2-Chlorotoluene ND ug/kg 1 11/19/09 22:34 95-49-84.4
4-Chlorotoluene ND ug/kg 1 11/19/09 22:34 106-43-44.4
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 22:34 96-12-84.4
Dibromochloromethane ND ug/kg 1 11/19/09 22:34 124-48-14.4
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 22:34 106-93-44.4
Dibromomethane ND ug/kg 1 11/19/09 22:34 74-95-34.4
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 22:34 95-50-14.4
1,3-Dichlorobenzene ND ug/kg 1 11/19/09 22:34 541-73-14.4
1,4-Dichlorobenzene ND ug/kg 1 11/19/09 22:34 106-46-74.4
Dichlorodifluoromethane ND ug/kg 1 11/19/09 22:34 75-71-88.9
1,1-Dichloroethane ND ug/kg 1 11/19/09 22:34 75-34-34.4
1,2-Dichloroethane ND ug/kg 1 11/19/09 22:34 107-06-24.4
1,1-Dichloroethene ND ug/kg 1 11/19/09 22:34 75-35-44.4
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 22:34 156-59-24.4
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 22:34 156-60-54.4
1,2-Dichloropropane ND ug/kg 1 11/19/09 22:34 78-87-54.4
1,3-Dichloropropane ND ug/kg 1 11/19/09 22:34 142-28-94.4
2,2-Dichloropropane ND ug/kg 1 11/19/09 22:34 594-20-74.4
1,1-Dichloropropene ND ug/kg 1 11/19/09 22:34 563-58-64.4
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 22:34 10061-01-54.4
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 22:34 10061-02-64.4
Diisopropyl ether ND ug/kg 1 11/19/09 22:34 108-20-34.4
Ethylbenzene ND ug/kg 1 11/19/09 22:34 100-41-44.4
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 22:34 87-68-34.4
2-Hexanone ND ug/kg 1 11/19/09 22:34 591-78-644.4
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 22:34 98-82-84.4
p-Isopropyltoluene ND ug/kg 1 11/19/09 22:34 99-87-64.4
Methylene Chloride ND ug/kg 1 11/19/09 22:34 75-09-217.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 22:34 108-10-144.4
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 22:34 1634-04-44.4
Naphthalene ND ug/kg 1 11/19/09 22:34 91-20-34.4
n-Propylbenzene ND ug/kg 1 11/19/09 22:34 103-65-14.4
Styrene ND ug/kg 1 11/19/09 22:34 100-42-54.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 28 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-3 2'Lab ID:9257863006 Collected:11/17/09 11:42 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 22:34 630-20-64.4
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 22:34 79-34-54.4
Tetrachloroethene ND ug/kg 1 11/19/09 22:34 127-18-44.4
Toluene ND ug/kg 1 11/19/09 22:34 108-88-34.4
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 22:34 87-61-64.4
1,2,4-Trichlorobenzene ND ug/kg 1 11/19/09 22:34 120-82-14.4
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 22:34 71-55-64.4
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 22:34 79-00-54.4
Trichloroethene ND ug/kg 1 11/19/09 22:34 79-01-64.4
Trichlorofluoromethane ND ug/kg 1 11/19/09 22:34 75-69-44.4
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 22:34 96-18-44.4
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 22:34 95-63-64.4
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 22:34 108-67-84.4
Vinyl acetate ND ug/kg 1 11/19/09 22:34 108-05-444.4
Vinyl chloride ND ug/kg 1 11/19/09 22:34 75-01-48.9
Xylene (Total)ND ug/kg 1 11/19/09 22:34 1330-20-78.9
m&p-Xylene ND ug/kg 1 11/19/09 22:34 1330-20-78.9
o-Xylene ND ug/kg 1 11/19/09 22:34 95-47-64.4
Dibromofluoromethane (S)102 %1 11/19/09 22:34 1868-53-779-116
Toluene-d8 (S)105 %1 11/19/09 22:34 2037-26-588-110
4-Bromofluorobenzene (S)95 %1 11/19/09 22:34 460-00-474-115
1,2-Dichloroethane-d4 (S)107 %1 11/19/09 22:34 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10.2 %1 11/19/09 13:480.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 29 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 0.5'Lab ID:9257863007 Collected:11/17/09 12:09 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:00 7440-38-212/09/09 12:300.025
Barium 0.078 mg/L 1 12/09/09 18:00 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:00 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:00 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:00 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:00 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:00 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:23 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 18:16 83-32-911/21/09 13:0232.5
Acenaphthylene ND ug/kg 1 12/03/09 18:16 208-96-811/21/09 13:0232.5
Anthracene ND ug/kg 1 12/03/09 18:16 120-12-711/21/09 13:0232.5
Benzo(a)anthracene ND ug/kg 1 12/03/09 18:16 56-55-311/21/09 13:0232.5
Benzo(a)pyrene ND ug/kg 1 12/03/09 18:16 50-32-811/21/09 13:0232.5
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 18:16 205-99-211/21/09 13:0232.5
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 18:16 191-24-211/21/09 13:0232.5
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 18:16 207-08-911/21/09 13:0232.5
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 18:16 101-55-311/21/09 13:02167
Butylbenzylphthalate ND ug/kg 1 12/03/09 18:16 85-68-711/21/09 13:02167
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 18:16 59-50-7 L211/21/09 13:02659
4-Chloroaniline ND ug/kg 1 12/03/09 18:16 106-47-811/21/09 13:02167
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 18:16 111-91-1 L211/21/09 13:02167
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 18:16 111-44-4 L211/21/09 13:02167
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 18:16 108-60-111/21/09 13:02167
2-Chloronaphthalene ND ug/kg 1 12/03/09 18:16 91-58-711/21/09 13:02167
2-Chlorophenol ND ug/kg 1 12/03/09 18:16 95-57-811/21/09 13:02167
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 18:16 7005-72-311/21/09 13:02167
Chrysene ND ug/kg 1 12/03/09 18:16 218-01-911/21/09 13:0232.5
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 18:16 53-70-311/21/09 13:0232.5
Dibenzofuran ND ug/kg 1 12/03/09 18:16 132-64-911/21/09 13:02167
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 18:16 95-50-111/21/09 13:02167
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 18:16 541-73-111/21/09 13:02167
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 18:16 106-46-711/21/09 13:02167
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 18:16 91-94-111/21/09 13:02659
2,4-Dichlorophenol ND ug/kg 1 12/03/09 18:16 120-83-211/21/09 13:02167
Diethylphthalate ND ug/kg 1 12/03/09 18:16 84-66-211/21/09 13:02167
2,4-Dimethylphenol ND ug/kg 1 12/03/09 18:16 105-67-9 L211/21/09 13:02167
Dimethylphthalate ND ug/kg 1 12/03/09 18:16 131-11-311/21/09 13:02167
Di-n-butylphthalate ND ug/kg 1 12/03/09 18:16 84-74-211/21/09 13:02167
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 18:16 534-52-111/21/09 13:02659
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 30 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 0.5'Lab ID:9257863007 Collected:11/17/09 12:09 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 18:16 51-28-511/21/09 13:02659
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 18:16 121-14-211/21/09 13:02167
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 18:16 606-20-211/21/09 13:02167
Di-n-octylphthalate ND ug/kg 1 12/03/09 18:16 117-84-011/21/09 13:02167
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 18:16 122-66-711/21/09 13:02167
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 18:16 117-81-711/21/09 13:02167
Fluoranthene ND ug/kg 1 12/03/09 18:16 206-44-011/21/09 13:0232.5
Fluorene ND ug/kg 1 12/03/09 18:16 86-73-711/21/09 13:0232.5
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 18:16 87-68-311/21/09 13:02167
Hexachlorobenzene ND ug/kg 1 12/03/09 18:16 118-74-111/21/09 13:02167
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 18:16 77-47-411/21/09 13:02659
Hexachloroethane ND ug/kg 1 12/03/09 18:16 67-72-1 L211/21/09 13:02167
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 18:16 193-39-511/21/09 13:0232.5
Isophorone ND ug/kg 1 12/03/09 18:16 78-59-1 L211/21/09 13:02167
1-Methylnaphthalene ND ug/kg 1 12/03/09 18:16 90-12-011/21/09 13:0232.5
2-Methylnaphthalene ND ug/kg 1 12/03/09 18:16 91-57-611/21/09 13:0232.5
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 18:16 95-48-7 L211/21/09 13:02167
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 18:1611/21/09 13:02167
Naphthalene ND ug/kg 1 12/03/09 18:16 91-20-311/21/09 13:0232.5
2-Nitroaniline ND ug/kg 1 12/03/09 18:16 88-74-411/21/09 13:02167
3-Nitroaniline ND ug/kg 1 12/03/09 18:16 99-09-2 L211/21/09 13:02167
4-Nitroaniline ND ug/kg 1 12/03/09 18:16 100-01-611/21/09 13:02167
Nitrobenzene ND ug/kg 1 12/03/09 18:16 98-95-3 L211/21/09 13:02167
2-Nitrophenol ND ug/kg 1 12/03/09 18:16 88-75-511/21/09 13:02167
4-Nitrophenol ND ug/kg 1 12/03/09 18:16 100-02-711/21/09 13:02167
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 18:16 62-75-9 L211/21/09 13:02167
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 18:16 621-64-7 L211/21/09 13:02167
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 18:16 86-30-611/21/09 13:02167
Pentachlorophenol ND ug/kg 1 12/03/09 18:16 87-86-511/21/09 13:02659
Phenanthrene ND ug/kg 1 12/03/09 18:16 85-01-811/21/09 13:0232.5
Phenol ND ug/kg 1 12/03/09 18:16 108-95-2 L211/21/09 13:02167
Pyrene ND ug/kg 1 12/03/09 18:16 129-00-011/21/09 13:0232.5
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 18:16 120-82-111/21/09 13:02167
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 18:16 95-95-411/21/09 13:02167
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 18:16 88-06-211/21/09 13:02167
Nitrobenzene-d5 (S)33 %1 12/03/09 18:16 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)42 %1 12/03/09 18:16 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)53 %1 12/03/09 18:16 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)28 %1 12/03/09 18:16 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)28 %1 12/03/09 18:16 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)49 %1 12/03/09 18:16 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 19:31 67-64-193.9
Benzene ND ug/kg 1 11/19/09 19:31 71-43-24.7
Bromobenzene ND ug/kg 1 11/19/09 19:31 108-86-14.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 31 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 0.5'Lab ID:9257863007 Collected:11/17/09 12:09 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 19:31 74-97-54.7
Bromodichloromethane ND ug/kg 1 11/19/09 19:31 75-27-44.7
Bromoform ND ug/kg 1 11/19/09 19:31 75-25-24.7
Bromomethane ND ug/kg 1 11/19/09 19:31 74-83-99.4
2-Butanone (MEK)ND ug/kg 1 11/19/09 19:31 78-93-393.9
n-Butylbenzene ND ug/kg 1 11/19/09 19:31 104-51-84.7
sec-Butylbenzene ND ug/kg 1 11/19/09 19:31 135-98-84.7
tert-Butylbenzene ND ug/kg 1 11/19/09 19:31 98-06-64.7
Carbon tetrachloride ND ug/kg 1 11/19/09 19:31 56-23-54.7
Chlorobenzene 102 ug/kg 1 11/19/09 19:31 108-90-74.7
Chloroethane ND ug/kg 1 11/19/09 19:31 75-00-39.4
Chloroform ND ug/kg 1 11/19/09 19:31 67-66-34.7
Chloromethane ND ug/kg 1 11/19/09 19:31 74-87-39.4
2-Chlorotoluene 4.9 ug/kg 1 11/19/09 19:31 95-49-84.7
4-Chlorotoluene ND ug/kg 1 11/19/09 19:31 106-43-44.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 19:31 96-12-84.7
Dibromochloromethane ND ug/kg 1 11/19/09 19:31 124-48-14.7
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 19:31 106-93-44.7
Dibromomethane ND ug/kg 1 11/19/09 19:31 74-95-34.7
1,2-Dichlorobenzene 9.6 ug/kg 1 11/19/09 19:31 95-50-14.7
1,3-Dichlorobenzene 15.3 ug/kg 1 11/19/09 19:31 541-73-14.7
1,4-Dichlorobenzene 90.0 ug/kg 1 11/19/09 19:31 106-46-74.7
Dichlorodifluoromethane ND ug/kg 1 11/19/09 19:31 75-71-89.4
1,1-Dichloroethane ND ug/kg 1 11/19/09 19:31 75-34-34.7
1,2-Dichloroethane ND ug/kg 1 11/19/09 19:31 107-06-24.7
1,1-Dichloroethene ND ug/kg 1 11/19/09 19:31 75-35-44.7
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 19:31 156-59-24.7
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 19:31 156-60-54.7
1,2-Dichloropropane ND ug/kg 1 11/19/09 19:31 78-87-54.7
1,3-Dichloropropane ND ug/kg 1 11/19/09 19:31 142-28-94.7
2,2-Dichloropropane ND ug/kg 1 11/19/09 19:31 594-20-74.7
1,1-Dichloropropene ND ug/kg 1 11/19/09 19:31 563-58-64.7
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 19:31 10061-01-54.7
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 19:31 10061-02-64.7
Diisopropyl ether ND ug/kg 1 11/19/09 19:31 108-20-34.7
Ethylbenzene ND ug/kg 1 11/19/09 19:31 100-41-44.7
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 19:31 87-68-34.7
2-Hexanone ND ug/kg 1 11/19/09 19:31 591-78-646.9
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 19:31 98-82-84.7
p-Isopropyltoluene ND ug/kg 1 11/19/09 19:31 99-87-64.7
Methylene Chloride ND ug/kg 1 11/19/09 19:31 75-09-218.8
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 19:31 108-10-146.9
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 19:31 1634-04-44.7
Naphthalene ND ug/kg 1 11/19/09 19:31 91-20-34.7
n-Propylbenzene ND ug/kg 1 11/19/09 19:31 103-65-14.7
Styrene ND ug/kg 1 11/19/09 19:31 100-42-54.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 32 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 0.5'Lab ID:9257863007 Collected:11/17/09 12:09 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 19:31 630-20-64.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 19:31 79-34-54.7
Tetrachloroethene ND ug/kg 1 11/19/09 19:31 127-18-44.7
Toluene ND ug/kg 1 11/19/09 19:31 108-88-34.7
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 19:31 87-61-64.7
1,2,4-Trichlorobenzene 9.4 ug/kg 1 11/19/09 19:31 120-82-14.7
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 19:31 71-55-64.7
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 19:31 79-00-54.7
Trichloroethene ND ug/kg 1 11/19/09 19:31 79-01-64.7
Trichlorofluoromethane ND ug/kg 1 11/19/09 19:31 75-69-44.7
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 19:31 96-18-44.7
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 19:31 95-63-64.7
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 19:31 108-67-84.7
Vinyl acetate ND ug/kg 1 11/19/09 19:31 108-05-446.9
Vinyl chloride ND ug/kg 1 11/19/09 19:31 75-01-49.4
Xylene (Total)ND ug/kg 1 11/19/09 19:31 1330-20-79.4
m&p-Xylene ND ug/kg 1 11/19/09 19:31 1330-20-79.4
o-Xylene ND ug/kg 1 11/19/09 19:31 95-47-64.7
Dibromofluoromethane (S)104 %1 11/19/09 19:31 1868-53-779-116
Toluene-d8 (S)98 %1 11/19/09 19:31 2037-26-588-110
4-Bromofluorobenzene (S)98 %1 11/19/09 19:31 460-00-474-115
1,2-Dichloroethane-d4 (S)106 %1 11/19/09 19:31 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 24.2 %1 11/19/09 13:480.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 33 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 4.5'Lab ID:9257863008 Collected:11/17/09 12:17 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:03 7440-38-212/09/09 12:300.025
Barium 0.15 mg/L 1 12/09/09 18:03 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:03 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:03 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:03 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:03 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:03 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:26 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 18:46 83-32-911/21/09 13:0232.9
Acenaphthylene ND ug/kg 1 12/03/09 18:46 208-96-811/21/09 13:0232.9
Anthracene ND ug/kg 1 12/03/09 18:46 120-12-711/21/09 13:0232.9
Benzo(a)anthracene ND ug/kg 1 12/03/09 18:46 56-55-311/21/09 13:0232.9
Benzo(a)pyrene ND ug/kg 1 12/03/09 18:46 50-32-811/21/09 13:0232.9
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 18:46 205-99-211/21/09 13:0232.9
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 18:46 191-24-211/21/09 13:0232.9
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 18:46 207-08-911/21/09 13:0232.9
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 18:46 101-55-311/21/09 13:02169
Butylbenzylphthalate ND ug/kg 1 12/03/09 18:46 85-68-711/21/09 13:02169
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 18:46 59-50-7 L211/21/09 13:02668
4-Chloroaniline ND ug/kg 1 12/03/09 18:46 106-47-811/21/09 13:02169
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 18:46 111-91-1 L211/21/09 13:02169
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 18:46 111-44-4 L211/21/09 13:02169
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 18:46 108-60-111/21/09 13:02169
2-Chloronaphthalene ND ug/kg 1 12/03/09 18:46 91-58-711/21/09 13:02169
2-Chlorophenol ND ug/kg 1 12/03/09 18:46 95-57-811/21/09 13:02169
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 18:46 7005-72-311/21/09 13:02169
Chrysene ND ug/kg 1 12/03/09 18:46 218-01-911/21/09 13:0232.9
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 18:46 53-70-311/21/09 13:0232.9
Dibenzofuran ND ug/kg 1 12/03/09 18:46 132-64-911/21/09 13:02169
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 18:46 95-50-111/21/09 13:02169
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 18:46 541-73-111/21/09 13:02169
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 18:46 106-46-711/21/09 13:02169
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 18:46 91-94-111/21/09 13:02668
2,4-Dichlorophenol ND ug/kg 1 12/03/09 18:46 120-83-211/21/09 13:02169
Diethylphthalate ND ug/kg 1 12/03/09 18:46 84-66-211/21/09 13:02169
2,4-Dimethylphenol ND ug/kg 1 12/03/09 18:46 105-67-9 L211/21/09 13:02169
Dimethylphthalate ND ug/kg 1 12/03/09 18:46 131-11-311/21/09 13:02169
Di-n-butylphthalate ND ug/kg 1 12/03/09 18:46 84-74-211/21/09 13:02169
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 18:46 534-52-111/21/09 13:02668
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 34 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 4.5'Lab ID:9257863008 Collected:11/17/09 12:17 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 18:46 51-28-511/21/09 13:02668
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 18:46 121-14-211/21/09 13:02169
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 18:46 606-20-211/21/09 13:02169
Di-n-octylphthalate ND ug/kg 1 12/03/09 18:46 117-84-011/21/09 13:02169
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 18:46 122-66-711/21/09 13:02169
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 18:46 117-81-711/21/09 13:02169
Fluoranthene ND ug/kg 1 12/03/09 18:46 206-44-011/21/09 13:0232.9
Fluorene ND ug/kg 1 12/03/09 18:46 86-73-711/21/09 13:0232.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 18:46 87-68-311/21/09 13:02169
Hexachlorobenzene ND ug/kg 1 12/03/09 18:46 118-74-111/21/09 13:02169
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 18:46 77-47-411/21/09 13:02668
Hexachloroethane ND ug/kg 1 12/03/09 18:46 67-72-1 L211/21/09 13:02169
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 18:46 193-39-511/21/09 13:0232.9
Isophorone ND ug/kg 1 12/03/09 18:46 78-59-1 L211/21/09 13:02169
1-Methylnaphthalene ND ug/kg 1 12/03/09 18:46 90-12-011/21/09 13:0232.9
2-Methylnaphthalene ND ug/kg 1 12/03/09 18:46 91-57-611/21/09 13:0232.9
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 18:46 95-48-7 L211/21/09 13:02169
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 18:4611/21/09 13:02169
Naphthalene ND ug/kg 1 12/03/09 18:46 91-20-311/21/09 13:0232.9
2-Nitroaniline ND ug/kg 1 12/03/09 18:46 88-74-411/21/09 13:02169
3-Nitroaniline ND ug/kg 1 12/03/09 18:46 99-09-2 L211/21/09 13:02169
4-Nitroaniline ND ug/kg 1 12/03/09 18:46 100-01-611/21/09 13:02169
Nitrobenzene ND ug/kg 1 12/03/09 18:46 98-95-3 L211/21/09 13:02169
2-Nitrophenol ND ug/kg 1 12/03/09 18:46 88-75-511/21/09 13:02169
4-Nitrophenol ND ug/kg 1 12/03/09 18:46 100-02-711/21/09 13:02169
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 18:46 62-75-9 L211/21/09 13:02169
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 18:46 621-64-7 L211/21/09 13:02169
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 18:46 86-30-611/21/09 13:02169
Pentachlorophenol ND ug/kg 1 12/03/09 18:46 87-86-511/21/09 13:02668
Phenanthrene ND ug/kg 1 12/03/09 18:46 85-01-811/21/09 13:0232.9
Phenol ND ug/kg 1 12/03/09 18:46 108-95-2 L211/21/09 13:02169
Pyrene ND ug/kg 1 12/03/09 18:46 129-00-011/21/09 13:0232.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 18:46 120-82-111/21/09 13:02169
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 18:46 95-95-411/21/09 13:02169
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 18:46 88-06-211/21/09 13:02169
Nitrobenzene-d5 (S)37 %1 12/03/09 18:46 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)46 %1 12/03/09 18:46 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)43 %1 12/03/09 18:46 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)34 %1 12/03/09 18:46 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)33 %1 12/03/09 18:46 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)35 %1 12/03/09 18:46 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/20/09 14:04 67-64-1125
Benzene ND ug/kg 1 11/20/09 14:04 71-43-26.2
Bromobenzene ND ug/kg 1 11/20/09 14:04 108-86-16.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 35 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 4.5'Lab ID:9257863008 Collected:11/17/09 12:17 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/20/09 14:04 74-97-56.2
Bromodichloromethane ND ug/kg 1 11/20/09 14:04 75-27-46.2
Bromoform ND ug/kg 1 11/20/09 14:04 75-25-26.2
Bromomethane ND ug/kg 1 11/20/09 14:04 74-83-912.5
2-Butanone (MEK)ND ug/kg 1 11/20/09 14:04 78-93-3125
n-Butylbenzene ND ug/kg 1 11/20/09 14:04 104-51-86.2
sec-Butylbenzene ND ug/kg 1 11/20/09 14:04 135-98-86.2
tert-Butylbenzene ND ug/kg 1 11/20/09 14:04 98-06-66.2
Carbon tetrachloride ND ug/kg 1 11/20/09 14:04 56-23-56.2
Chlorobenzene 15.8 ug/kg 1 11/20/09 14:04 108-90-76.2
Chloroethane ND ug/kg 1 11/20/09 14:04 75-00-312.5
Chloroform ND ug/kg 1 11/20/09 14:04 67-66-36.2
Chloromethane ND ug/kg 1 11/20/09 14:04 74-87-312.5
2-Chlorotoluene ND ug/kg 1 11/20/09 14:04 95-49-86.2
4-Chlorotoluene ND ug/kg 1 11/20/09 14:04 106-43-46.2
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/20/09 14:04 96-12-86.2
Dibromochloromethane ND ug/kg 1 11/20/09 14:04 124-48-16.2
1,2-Dibromoethane (EDB)ND ug/kg 1 11/20/09 14:04 106-93-46.2
Dibromomethane ND ug/kg 1 11/20/09 14:04 74-95-36.2
1,2-Dichlorobenzene ND ug/kg 1 11/20/09 14:04 95-50-16.2
1,3-Dichlorobenzene ND ug/kg 1 11/20/09 14:04 541-73-16.2
1,4-Dichlorobenzene 26.1 ug/kg 1 11/20/09 14:04 106-46-76.2
Dichlorodifluoromethane ND ug/kg 1 11/20/09 14:04 75-71-812.5
1,1-Dichloroethane ND ug/kg 1 11/20/09 14:04 75-34-36.2
1,2-Dichloroethane ND ug/kg 1 11/20/09 14:04 107-06-26.2
1,1-Dichloroethene ND ug/kg 1 11/20/09 14:04 75-35-46.2
cis-1,2-Dichloroethene ND ug/kg 1 11/20/09 14:04 156-59-26.2
trans-1,2-Dichloroethene ND ug/kg 1 11/20/09 14:04 156-60-56.2
1,2-Dichloropropane ND ug/kg 1 11/20/09 14:04 78-87-56.2
1,3-Dichloropropane ND ug/kg 1 11/20/09 14:04 142-28-96.2
2,2-Dichloropropane ND ug/kg 1 11/20/09 14:04 594-20-76.2
1,1-Dichloropropene ND ug/kg 1 11/20/09 14:04 563-58-66.2
cis-1,3-Dichloropropene ND ug/kg 1 11/20/09 14:04 10061-01-56.2
trans-1,3-Dichloropropene ND ug/kg 1 11/20/09 14:04 10061-02-66.2
Diisopropyl ether ND ug/kg 1 11/20/09 14:04 108-20-36.2
Ethylbenzene ND ug/kg 1 11/20/09 14:04 100-41-46.2
Hexachloro-1,3-butadiene ND ug/kg 1 11/20/09 14:04 87-68-36.2
2-Hexanone ND ug/kg 1 11/20/09 14:04 591-78-662.5
Isopropylbenzene (Cumene)ND ug/kg 1 11/20/09 14:04 98-82-86.2
p-Isopropyltoluene ND ug/kg 1 11/20/09 14:04 99-87-66.2
Methylene Chloride ND ug/kg 1 11/20/09 14:04 75-09-225.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/20/09 14:04 108-10-162.5
Methyl-tert-butyl ether ND ug/kg 1 11/20/09 14:04 1634-04-46.2
Naphthalene ND ug/kg 1 11/20/09 14:04 91-20-36.2
n-Propylbenzene ND ug/kg 1 11/20/09 14:04 103-65-16.2
Styrene ND ug/kg 1 11/20/09 14:04 100-42-56.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 36 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-4 4.5'Lab ID:9257863008 Collected:11/17/09 12:17 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/20/09 14:04 630-20-66.2
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/20/09 14:04 79-34-56.2
Tetrachloroethene ND ug/kg 1 11/20/09 14:04 127-18-46.2
Toluene ND ug/kg 1 11/20/09 14:04 108-88-36.2
1,2,3-Trichlorobenzene ND ug/kg 1 11/20/09 14:04 87-61-66.2
1,2,4-Trichlorobenzene ND ug/kg 1 11/20/09 14:04 120-82-16.2
1,1,1-Trichloroethane ND ug/kg 1 11/20/09 14:04 71-55-66.2
1,1,2-Trichloroethane ND ug/kg 1 11/20/09 14:04 79-00-56.2
Trichloroethene ND ug/kg 1 11/20/09 14:04 79-01-66.2
Trichlorofluoromethane ND ug/kg 1 11/20/09 14:04 75-69-46.2
1,2,3-Trichloropropane ND ug/kg 1 11/20/09 14:04 96-18-46.2
1,2,4-Trimethylbenzene ND ug/kg 1 11/20/09 14:04 95-63-66.2
1,3,5-Trimethylbenzene ND ug/kg 1 11/20/09 14:04 108-67-86.2
Vinyl acetate ND ug/kg 1 11/20/09 14:04 108-05-462.5
Vinyl chloride ND ug/kg 1 11/20/09 14:04 75-01-412.5
Xylene (Total)ND ug/kg 1 11/20/09 14:04 1330-20-712.5
m&p-Xylene ND ug/kg 1 11/20/09 14:04 1330-20-712.5
o-Xylene ND ug/kg 1 11/20/09 14:04 95-47-66.2
Dibromofluoromethane (S)107 %1 11/20/09 14:04 1868-53-779-116
Toluene-d8 (S)105 %1 11/20/09 14:04 2037-26-588-110
4-Bromofluorobenzene (S)100 %1 11/20/09 14:04 460-00-474-115
1,2-Dichloroethane-d4 (S)110 %1 11/20/09 14:04 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 22.3 %1 11/19/09 13:480.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 37 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-5 0.5'Lab ID:9257863009 Collected:11/17/09 12:34 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:07 7440-38-212/09/09 12:300.025
Barium 0.14 mg/L 1 12/09/09 18:07 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:07 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:07 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:07 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:07 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:07 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:33 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 19:15 83-32-911/21/09 13:0232.5
Acenaphthylene ND ug/kg 1 12/03/09 19:15 208-96-811/21/09 13:0232.5
Anthracene ND ug/kg 1 12/03/09 19:15 120-12-711/21/09 13:0232.5
Benzo(a)anthracene ND ug/kg 1 12/03/09 19:15 56-55-311/21/09 13:0232.5
Benzo(a)pyrene ND ug/kg 1 12/03/09 19:15 50-32-811/21/09 13:0232.5
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 19:15 205-99-211/21/09 13:0232.5
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 19:15 191-24-211/21/09 13:0232.5
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 19:15 207-08-911/21/09 13:0232.5
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 19:15 101-55-311/21/09 13:02167
Butylbenzylphthalate ND ug/kg 1 12/03/09 19:15 85-68-711/21/09 13:02167
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 19:15 59-50-7 L211/21/09 13:02659
4-Chloroaniline ND ug/kg 1 12/03/09 19:15 106-47-811/21/09 13:02167
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 19:15 111-91-1 L211/21/09 13:02167
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 19:15 111-44-4 L211/21/09 13:02167
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 19:15 108-60-111/21/09 13:02167
2-Chloronaphthalene ND ug/kg 1 12/03/09 19:15 91-58-711/21/09 13:02167
2-Chlorophenol ND ug/kg 1 12/03/09 19:15 95-57-811/21/09 13:02167
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 19:15 7005-72-311/21/09 13:02167
Chrysene ND ug/kg 1 12/03/09 19:15 218-01-911/21/09 13:0232.5
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 19:15 53-70-311/21/09 13:0232.5
Dibenzofuran ND ug/kg 1 12/03/09 19:15 132-64-911/21/09 13:02167
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 19:15 95-50-111/21/09 13:02167
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 19:15 541-73-111/21/09 13:02167
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 19:15 106-46-711/21/09 13:02167
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 19:15 91-94-111/21/09 13:02659
2,4-Dichlorophenol ND ug/kg 1 12/03/09 19:15 120-83-211/21/09 13:02167
Diethylphthalate ND ug/kg 1 12/03/09 19:15 84-66-211/21/09 13:02167
2,4-Dimethylphenol ND ug/kg 1 12/03/09 19:15 105-67-9 L211/21/09 13:02167
Dimethylphthalate ND ug/kg 1 12/03/09 19:15 131-11-311/21/09 13:02167
Di-n-butylphthalate ND ug/kg 1 12/03/09 19:15 84-74-211/21/09 13:02167
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 19:15 534-52-111/21/09 13:02659
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 38 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-5 0.5'Lab ID:9257863009 Collected:11/17/09 12:34 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 19:15 51-28-511/21/09 13:02659
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 19:15 121-14-211/21/09 13:02167
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 19:15 606-20-211/21/09 13:02167
Di-n-octylphthalate ND ug/kg 1 12/03/09 19:15 117-84-011/21/09 13:02167
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 19:15 122-66-711/21/09 13:02167
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 19:15 117-81-711/21/09 13:02167
Fluoranthene ND ug/kg 1 12/03/09 19:15 206-44-011/21/09 13:0232.5
Fluorene ND ug/kg 1 12/03/09 19:15 86-73-711/21/09 13:0232.5
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 19:15 87-68-311/21/09 13:02167
Hexachlorobenzene ND ug/kg 1 12/03/09 19:15 118-74-111/21/09 13:02167
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 19:15 77-47-411/21/09 13:02659
Hexachloroethane ND ug/kg 1 12/03/09 19:15 67-72-1 L211/21/09 13:02167
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 19:15 193-39-511/21/09 13:0232.5
Isophorone ND ug/kg 1 12/03/09 19:15 78-59-1 L211/21/09 13:02167
1-Methylnaphthalene ND ug/kg 1 12/03/09 19:15 90-12-011/21/09 13:0232.5
2-Methylnaphthalene ND ug/kg 1 12/03/09 19:15 91-57-611/21/09 13:0232.5
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 19:15 95-48-7 L211/21/09 13:02167
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 19:1511/21/09 13:02167
Naphthalene ND ug/kg 1 12/03/09 19:15 91-20-311/21/09 13:0232.5
2-Nitroaniline ND ug/kg 1 12/03/09 19:15 88-74-411/21/09 13:02167
3-Nitroaniline ND ug/kg 1 12/03/09 19:15 99-09-2 L211/21/09 13:02167
4-Nitroaniline ND ug/kg 1 12/03/09 19:15 100-01-611/21/09 13:02167
Nitrobenzene ND ug/kg 1 12/03/09 19:15 98-95-3 L211/21/09 13:02167
2-Nitrophenol ND ug/kg 1 12/03/09 19:15 88-75-511/21/09 13:02167
4-Nitrophenol ND ug/kg 1 12/03/09 19:15 100-02-711/21/09 13:02167
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 19:15 62-75-9 L211/21/09 13:02167
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 19:15 621-64-7 L211/21/09 13:02167
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 19:15 86-30-611/21/09 13:02167
Pentachlorophenol ND ug/kg 1 12/03/09 19:15 87-86-511/21/09 13:02659
Phenanthrene ND ug/kg 1 12/03/09 19:15 85-01-811/21/09 13:0232.5
Phenol ND ug/kg 1 12/03/09 19:15 108-95-2 L211/21/09 13:02167
Pyrene ND ug/kg 1 12/03/09 19:15 129-00-011/21/09 13:0232.5
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 19:15 120-82-111/21/09 13:02167
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 19:15 95-95-411/21/09 13:02167
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 19:15 88-06-211/21/09 13:02167
Nitrobenzene-d5 (S)33 %1 12/03/09 19:15 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)46 %1 12/03/09 19:15 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)66 %1 12/03/09 19:15 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)31 %1 12/03/09 19:15 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)32 %1 12/03/09 19:15 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)45 %1 12/03/09 19:15 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 50 11/19/09 23:47 67-64-14560
Benzene ND ug/kg 50 11/19/09 23:47 71-43-2228
Bromobenzene ND ug/kg 50 11/19/09 23:47 108-86-1228
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 39 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-5 0.5'Lab ID:9257863009 Collected:11/17/09 12:34 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 50 11/19/09 23:47 74-97-5228
Bromodichloromethane ND ug/kg 50 11/19/09 23:47 75-27-4228
Bromoform ND ug/kg 50 11/19/09 23:47 75-25-2228
Bromomethane ND ug/kg 50 11/19/09 23:47 74-83-9456
2-Butanone (MEK)ND ug/kg 50 11/19/09 23:47 78-93-34560
n-Butylbenzene ND ug/kg 50 11/19/09 23:47 104-51-8228
sec-Butylbenzene ND ug/kg 50 11/19/09 23:47 135-98-8228
tert-Butylbenzene ND ug/kg 50 11/19/09 23:47 98-06-6228
Carbon tetrachloride ND ug/kg 50 11/19/09 23:47 56-23-5228
Chlorobenzene 1840 ug/kg 50 11/19/09 23:47 108-90-7228
Chloroethane ND ug/kg 50 11/19/09 23:47 75-00-3456
Chloroform ND ug/kg 50 11/19/09 23:47 67-66-3228
Chloromethane ND ug/kg 50 11/19/09 23:47 74-87-3456
2-Chlorotoluene 1120 ug/kg 50 11/19/09 23:47 95-49-8228
4-Chlorotoluene ND ug/kg 50 11/19/09 23:47 106-43-4228
1,2-Dibromo-3-chloropropane ND ug/kg 50 11/19/09 23:47 96-12-8228
Dibromochloromethane ND ug/kg 50 11/19/09 23:47 124-48-1228
1,2-Dibromoethane (EDB)ND ug/kg 50 11/19/09 23:47 106-93-4228
Dibromomethane ND ug/kg 50 11/19/09 23:47 74-95-3228
1,2-Dichlorobenzene ND ug/kg 50 11/19/09 23:47 95-50-1228
1,3-Dichlorobenzene 284 ug/kg 50 11/19/09 23:47 541-73-1228
1,4-Dichlorobenzene 850 ug/kg 50 11/19/09 23:47 106-46-7228
Dichlorodifluoromethane ND ug/kg 50 11/19/09 23:47 75-71-8456
1,1-Dichloroethane ND ug/kg 50 11/19/09 23:47 75-34-3228
1,2-Dichloroethane ND ug/kg 50 11/19/09 23:47 107-06-2228
1,1-Dichloroethene ND ug/kg 50 11/19/09 23:47 75-35-4228
cis-1,2-Dichloroethene ND ug/kg 50 11/19/09 23:47 156-59-2228
trans-1,2-Dichloroethene ND ug/kg 50 11/19/09 23:47 156-60-5228
1,2-Dichloropropane ND ug/kg 50 11/19/09 23:47 78-87-5228
1,3-Dichloropropane ND ug/kg 50 11/19/09 23:47 142-28-9228
2,2-Dichloropropane ND ug/kg 50 11/19/09 23:47 594-20-7228
1,1-Dichloropropene ND ug/kg 50 11/19/09 23:47 563-58-6228
cis-1,3-Dichloropropene ND ug/kg 50 11/19/09 23:47 10061-01-5228
trans-1,3-Dichloropropene ND ug/kg 50 11/19/09 23:47 10061-02-6228
Diisopropyl ether ND ug/kg 50 11/19/09 23:47 108-20-3228
Ethylbenzene ND ug/kg 50 11/19/09 23:47 100-41-4228
Hexachloro-1,3-butadiene ND ug/kg 50 11/19/09 23:47 87-68-3228
2-Hexanone ND ug/kg 50 11/19/09 23:47 591-78-62280
Isopropylbenzene (Cumene)ND ug/kg 50 11/19/09 23:47 98-82-8228
p-Isopropyltoluene ND ug/kg 50 11/19/09 23:47 99-87-6228
Methylene Chloride ND ug/kg 50 11/19/09 23:47 75-09-2913
4-Methyl-2-pentanone (MIBK)ND ug/kg 50 11/19/09 23:47 108-10-12280
Methyl-tert-butyl ether ND ug/kg 50 11/19/09 23:47 1634-04-4228
Naphthalene ND ug/kg 50 11/19/09 23:47 91-20-3228
n-Propylbenzene ND ug/kg 50 11/19/09 23:47 103-65-1228
Styrene ND ug/kg 50 11/19/09 23:47 100-42-5228
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 40 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-5 0.5'Lab ID:9257863009 Collected:11/17/09 12:34 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 50 11/19/09 23:47 630-20-6228
1,1,2,2-Tetrachloroethane ND ug/kg 50 11/19/09 23:47 79-34-5228
Tetrachloroethene ND ug/kg 50 11/19/09 23:47 127-18-4228
Toluene ND ug/kg 50 11/19/09 23:47 108-88-3228
1,2,3-Trichlorobenzene ND ug/kg 50 11/19/09 23:47 87-61-6228
1,2,4-Trichlorobenzene ND ug/kg 50 11/19/09 23:47 120-82-1228
1,1,1-Trichloroethane ND ug/kg 50 11/19/09 23:47 71-55-6228
1,1,2-Trichloroethane ND ug/kg 50 11/19/09 23:47 79-00-5228
Trichloroethene ND ug/kg 50 11/19/09 23:47 79-01-6228
Trichlorofluoromethane ND ug/kg 50 11/19/09 23:47 75-69-4228
1,2,3-Trichloropropane ND ug/kg 50 11/19/09 23:47 96-18-4228
1,2,4-Trimethylbenzene ND ug/kg 50 11/19/09 23:47 95-63-6228
1,3,5-Trimethylbenzene ND ug/kg 50 11/19/09 23:47 108-67-8228
Vinyl acetate ND ug/kg 50 11/19/09 23:47 108-05-42280
Vinyl chloride ND ug/kg 50 11/19/09 23:47 75-01-4456
Xylene (Total)ND ug/kg 50 11/19/09 23:47 1330-20-7456
m&p-Xylene ND ug/kg 50 11/19/09 23:47 1330-20-7456
o-Xylene ND ug/kg 50 11/19/09 23:47 95-47-6228
Dibromofluoromethane (S)99 %50 11/19/09 23:47 1868-53-7 D379-116
Toluene-d8 (S)102 %50 11/19/09 23:47 2037-26-588-110
4-Bromofluorobenzene (S)98 %50 11/19/09 23:47 460-00-474-115
1,2-Dichloroethane-d4 (S)100 %50 11/19/09 23:47 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.1 %1 11/19/09 13:490.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 41 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 0.5'Lab ID:9257863010 Collected:11/17/09 12:50 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:10 7440-38-212/09/09 12:300.025
Barium 0.19 mg/L 1 12/09/09 18:10 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:10 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:10 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:10 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:10 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:10 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:36 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 19:45 83-32-911/21/09 13:0232.5
Acenaphthylene ND ug/kg 1 12/03/09 19:45 208-96-811/21/09 13:0232.5
Anthracene ND ug/kg 1 12/03/09 19:45 120-12-711/21/09 13:0232.5
Benzo(a)anthracene ND ug/kg 1 12/03/09 19:45 56-55-311/21/09 13:0232.5
Benzo(a)pyrene ND ug/kg 1 12/03/09 19:45 50-32-811/21/09 13:0232.5
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 19:45 205-99-211/21/09 13:0232.5
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 19:45 191-24-211/21/09 13:0232.5
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 19:45 207-08-911/21/09 13:0232.5
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 19:45 101-55-311/21/09 13:02167
Butylbenzylphthalate ND ug/kg 1 12/03/09 19:45 85-68-711/21/09 13:02167
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 19:45 59-50-7 L211/21/09 13:02659
4-Chloroaniline ND ug/kg 1 12/03/09 19:45 106-47-811/21/09 13:02167
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 19:45 111-91-1 L211/21/09 13:02167
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 19:45 111-44-4 L211/21/09 13:02167
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 19:45 108-60-111/21/09 13:02167
2-Chloronaphthalene ND ug/kg 1 12/03/09 19:45 91-58-711/21/09 13:02167
2-Chlorophenol ND ug/kg 1 12/03/09 19:45 95-57-811/21/09 13:02167
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 19:45 7005-72-311/21/09 13:02167
Chrysene ND ug/kg 1 12/03/09 19:45 218-01-911/21/09 13:0232.5
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 19:45 53-70-311/21/09 13:0232.5
Dibenzofuran ND ug/kg 1 12/03/09 19:45 132-64-911/21/09 13:02167
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 19:45 95-50-111/21/09 13:02167
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 19:45 541-73-111/21/09 13:02167
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 19:45 106-46-711/21/09 13:02167
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 19:45 91-94-111/21/09 13:02659
2,4-Dichlorophenol ND ug/kg 1 12/03/09 19:45 120-83-211/21/09 13:02167
Diethylphthalate ND ug/kg 1 12/03/09 19:45 84-66-211/21/09 13:02167
2,4-Dimethylphenol ND ug/kg 1 12/03/09 19:45 105-67-9 L211/21/09 13:02167
Dimethylphthalate ND ug/kg 1 12/03/09 19:45 131-11-311/21/09 13:02167
Di-n-butylphthalate ND ug/kg 1 12/03/09 19:45 84-74-211/21/09 13:02167
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 19:45 534-52-111/21/09 13:02659
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 42 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 0.5'Lab ID:9257863010 Collected:11/17/09 12:50 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 19:45 51-28-511/21/09 13:02659
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 19:45 121-14-211/21/09 13:02167
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 19:45 606-20-211/21/09 13:02167
Di-n-octylphthalate ND ug/kg 1 12/03/09 19:45 117-84-011/21/09 13:02167
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 19:45 122-66-711/21/09 13:02167
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 19:45 117-81-711/21/09 13:02167
Fluoranthene ND ug/kg 1 12/03/09 19:45 206-44-011/21/09 13:0232.5
Fluorene ND ug/kg 1 12/03/09 19:45 86-73-711/21/09 13:0232.5
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 19:45 87-68-311/21/09 13:02167
Hexachlorobenzene ND ug/kg 1 12/03/09 19:45 118-74-111/21/09 13:02167
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 19:45 77-47-411/21/09 13:02659
Hexachloroethane ND ug/kg 1 12/03/09 19:45 67-72-1 L211/21/09 13:02167
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 19:45 193-39-511/21/09 13:0232.5
Isophorone ND ug/kg 1 12/03/09 19:45 78-59-1 L211/21/09 13:02167
1-Methylnaphthalene ND ug/kg 1 12/03/09 19:45 90-12-011/21/09 13:0232.5
2-Methylnaphthalene ND ug/kg 1 12/03/09 19:45 91-57-611/21/09 13:0232.5
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 19:45 95-48-7 L211/21/09 13:02167
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 19:4511/21/09 13:02167
Naphthalene ND ug/kg 1 12/03/09 19:45 91-20-311/21/09 13:0232.5
2-Nitroaniline ND ug/kg 1 12/03/09 19:45 88-74-411/21/09 13:02167
3-Nitroaniline ND ug/kg 1 12/03/09 19:45 99-09-2 L211/21/09 13:02167
4-Nitroaniline ND ug/kg 1 12/03/09 19:45 100-01-611/21/09 13:02167
Nitrobenzene ND ug/kg 1 12/03/09 19:45 98-95-3 L211/21/09 13:02167
2-Nitrophenol ND ug/kg 1 12/03/09 19:45 88-75-511/21/09 13:02167
4-Nitrophenol ND ug/kg 1 12/03/09 19:45 100-02-711/21/09 13:02167
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 19:45 62-75-9 L211/21/09 13:02167
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 19:45 621-64-7 L211/21/09 13:02167
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 19:45 86-30-611/21/09 13:02167
Pentachlorophenol ND ug/kg 1 12/03/09 19:45 87-86-511/21/09 13:02659
Phenanthrene ND ug/kg 1 12/03/09 19:45 85-01-811/21/09 13:0232.5
Phenol ND ug/kg 1 12/03/09 19:45 108-95-2 L211/21/09 13:02167
Pyrene ND ug/kg 1 12/03/09 19:45 129-00-011/21/09 13:0232.5
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 19:45 120-82-111/21/09 13:02167
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 19:45 95-95-411/21/09 13:02167
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 19:45 88-06-211/21/09 13:02167
Nitrobenzene-d5 (S)36 %1 12/03/09 19:45 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)42 %1 12/03/09 19:45 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)73 %1 12/03/09 19:45 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)29 %1 12/03/09 19:45 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)30 %1 12/03/09 19:45 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)56 %1 12/03/09 19:45 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 22:52 67-64-1100
Benzene ND ug/kg 1 11/19/09 22:52 71-43-25.0
Bromobenzene ND ug/kg 1 11/19/09 22:52 108-86-15.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 43 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 0.5'Lab ID:9257863010 Collected:11/17/09 12:50 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 22:52 74-97-55.0
Bromodichloromethane ND ug/kg 1 11/19/09 22:52 75-27-45.0
Bromoform ND ug/kg 1 11/19/09 22:52 75-25-25.0
Bromomethane ND ug/kg 1 11/19/09 22:52 74-83-910
2-Butanone (MEK)ND ug/kg 1 11/19/09 22:52 78-93-3100
n-Butylbenzene ND ug/kg 1 11/19/09 22:52 104-51-85.0
sec-Butylbenzene ND ug/kg 1 11/19/09 22:52 135-98-85.0
tert-Butylbenzene ND ug/kg 1 11/19/09 22:52 98-06-65.0
Carbon tetrachloride ND ug/kg 1 11/19/09 22:52 56-23-55.0
Chlorobenzene 11.9 ug/kg 1 11/19/09 22:52 108-90-75.0
Chloroethane ND ug/kg 1 11/19/09 22:52 75-00-310
Chloroform ND ug/kg 1 11/19/09 22:52 67-66-35.0
Chloromethane ND ug/kg 1 11/19/09 22:52 74-87-310
2-Chlorotoluene ND ug/kg 1 11/19/09 22:52 95-49-85.0
4-Chlorotoluene ND ug/kg 1 11/19/09 22:52 106-43-45.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 22:52 96-12-85.0
Dibromochloromethane ND ug/kg 1 11/19/09 22:52 124-48-15.0
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 22:52 106-93-45.0
Dibromomethane ND ug/kg 1 11/19/09 22:52 74-95-35.0
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 22:52 95-50-15.0
1,3-Dichlorobenzene ND ug/kg 1 11/19/09 22:52 541-73-15.0
1,4-Dichlorobenzene 15.3 ug/kg 1 11/19/09 22:52 106-46-75.0
Dichlorodifluoromethane ND ug/kg 1 11/19/09 22:52 75-71-810
1,1-Dichloroethane ND ug/kg 1 11/19/09 22:52 75-34-35.0
1,2-Dichloroethane ND ug/kg 1 11/19/09 22:52 107-06-25.0
1,1-Dichloroethene ND ug/kg 1 11/19/09 22:52 75-35-45.0
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 22:52 156-59-25.0
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 22:52 156-60-55.0
1,2-Dichloropropane ND ug/kg 1 11/19/09 22:52 78-87-55.0
1,3-Dichloropropane ND ug/kg 1 11/19/09 22:52 142-28-95.0
2,2-Dichloropropane ND ug/kg 1 11/19/09 22:52 594-20-75.0
1,1-Dichloropropene ND ug/kg 1 11/19/09 22:52 563-58-65.0
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 22:52 10061-01-55.0
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 22:52 10061-02-65.0
Diisopropyl ether ND ug/kg 1 11/19/09 22:52 108-20-35.0
Ethylbenzene ND ug/kg 1 11/19/09 22:52 100-41-45.0
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 22:52 87-68-35.0
2-Hexanone ND ug/kg 1 11/19/09 22:52 591-78-650.0
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 22:52 98-82-85.0
p-Isopropyltoluene ND ug/kg 1 11/19/09 22:52 99-87-65.0
Methylene Chloride ND ug/kg 1 11/19/09 22:52 75-09-220.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 22:52 108-10-150.0
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 22:52 1634-04-45.0
Naphthalene ND ug/kg 1 11/19/09 22:52 91-20-35.0
n-Propylbenzene ND ug/kg 1 11/19/09 22:52 103-65-15.0
Styrene ND ug/kg 1 11/19/09 22:52 100-42-55.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 44 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 0.5'Lab ID:9257863010 Collected:11/17/09 12:50 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 22:52 630-20-65.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 22:52 79-34-55.0
Tetrachloroethene ND ug/kg 1 11/19/09 22:52 127-18-45.0
Toluene ND ug/kg 1 11/19/09 22:52 108-88-35.0
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 22:52 87-61-65.0
1,2,4-Trichlorobenzene 10.2 ug/kg 1 11/19/09 22:52 120-82-15.0
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 22:52 71-55-65.0
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 22:52 79-00-55.0
Trichloroethene ND ug/kg 1 11/19/09 22:52 79-01-65.0
Trichlorofluoromethane ND ug/kg 1 11/19/09 22:52 75-69-45.0
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 22:52 96-18-45.0
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 22:52 95-63-65.0
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 22:52 108-67-85.0
Vinyl acetate ND ug/kg 1 11/19/09 22:52 108-05-450.0
Vinyl chloride ND ug/kg 1 11/19/09 22:52 75-01-410
Xylene (Total)ND ug/kg 1 11/19/09 22:52 1330-20-710
m&p-Xylene ND ug/kg 1 11/19/09 22:52 1330-20-710
o-Xylene ND ug/kg 1 11/19/09 22:52 95-47-65.0
Dibromofluoromethane (S)99 %1 11/19/09 22:52 1868-53-779-116
Toluene-d8 (S)104 %1 11/19/09 22:52 2037-26-588-110
4-Bromofluorobenzene (S)98 %1 11/19/09 22:52 460-00-474-115
1,2-Dichloroethane-d4 (S)99 %1 11/19/09 22:52 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 23.8 %1 11/23/09 09:040.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 45 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 2'Lab ID:9257863011 Collected:11/17/09 12:55 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:14 7440-38-212/09/09 12:300.025
Barium 0.14 mg/L 1 12/09/09 18:14 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:14 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:14 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:14 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:14 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:14 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:38 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 20:15 83-32-911/21/09 13:0232.9
Acenaphthylene ND ug/kg 1 12/03/09 20:15 208-96-811/21/09 13:0232.9
Anthracene ND ug/kg 1 12/03/09 20:15 120-12-711/21/09 13:0232.9
Benzo(a)anthracene ND ug/kg 1 12/03/09 20:15 56-55-311/21/09 13:0232.9
Benzo(a)pyrene ND ug/kg 1 12/03/09 20:15 50-32-811/21/09 13:0232.9
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 20:15 205-99-211/21/09 13:0232.9
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 20:15 191-24-211/21/09 13:0232.9
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 20:15 207-08-911/21/09 13:0232.9
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 20:15 101-55-311/21/09 13:02169
Butylbenzylphthalate ND ug/kg 1 12/03/09 20:15 85-68-711/21/09 13:02169
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 20:15 59-50-7 L211/21/09 13:02668
4-Chloroaniline ND ug/kg 1 12/03/09 20:15 106-47-811/21/09 13:02169
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 20:15 111-91-1 L211/21/09 13:02169
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 20:15 111-44-4 L211/21/09 13:02169
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 20:15 108-60-111/21/09 13:02169
2-Chloronaphthalene ND ug/kg 1 12/03/09 20:15 91-58-711/21/09 13:02169
2-Chlorophenol ND ug/kg 1 12/03/09 20:15 95-57-811/21/09 13:02169
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 20:15 7005-72-311/21/09 13:02169
Chrysene ND ug/kg 1 12/03/09 20:15 218-01-911/21/09 13:0232.9
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 20:15 53-70-311/21/09 13:0232.9
Dibenzofuran ND ug/kg 1 12/03/09 20:15 132-64-911/21/09 13:02169
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 20:15 95-50-111/21/09 13:02169
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 20:15 541-73-111/21/09 13:02169
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 20:15 106-46-711/21/09 13:02169
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 20:15 91-94-111/21/09 13:02668
2,4-Dichlorophenol ND ug/kg 1 12/03/09 20:15 120-83-211/21/09 13:02169
Diethylphthalate ND ug/kg 1 12/03/09 20:15 84-66-211/21/09 13:02169
2,4-Dimethylphenol ND ug/kg 1 12/03/09 20:15 105-67-9 L211/21/09 13:02169
Dimethylphthalate ND ug/kg 1 12/03/09 20:15 131-11-311/21/09 13:02169
Di-n-butylphthalate ND ug/kg 1 12/03/09 20:15 84-74-211/21/09 13:02169
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 20:15 534-52-111/21/09 13:02668
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 46 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 2'Lab ID:9257863011 Collected:11/17/09 12:55 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 20:15 51-28-511/21/09 13:02668
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 20:15 121-14-211/21/09 13:02169
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 20:15 606-20-211/21/09 13:02169
Di-n-octylphthalate ND ug/kg 1 12/03/09 20:15 117-84-011/21/09 13:02169
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 20:15 122-66-711/21/09 13:02169
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 20:15 117-81-711/21/09 13:02169
Fluoranthene ND ug/kg 1 12/03/09 20:15 206-44-011/21/09 13:0232.9
Fluorene ND ug/kg 1 12/03/09 20:15 86-73-711/21/09 13:0232.9
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 20:15 87-68-311/21/09 13:02169
Hexachlorobenzene ND ug/kg 1 12/03/09 20:15 118-74-111/21/09 13:02169
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 20:15 77-47-411/21/09 13:02668
Hexachloroethane ND ug/kg 1 12/03/09 20:15 67-72-1 L211/21/09 13:02169
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 20:15 193-39-511/21/09 13:0232.9
Isophorone ND ug/kg 1 12/03/09 20:15 78-59-1 L211/21/09 13:02169
1-Methylnaphthalene ND ug/kg 1 12/03/09 20:15 90-12-011/21/09 13:0232.9
2-Methylnaphthalene ND ug/kg 1 12/03/09 20:15 91-57-611/21/09 13:0232.9
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 20:15 95-48-7 L211/21/09 13:02169
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 20:1511/21/09 13:02169
Naphthalene ND ug/kg 1 12/03/09 20:15 91-20-311/21/09 13:0232.9
2-Nitroaniline ND ug/kg 1 12/03/09 20:15 88-74-411/21/09 13:02169
3-Nitroaniline ND ug/kg 1 12/03/09 20:15 99-09-2 L211/21/09 13:02169
4-Nitroaniline ND ug/kg 1 12/03/09 20:15 100-01-611/21/09 13:02169
Nitrobenzene ND ug/kg 1 12/03/09 20:15 98-95-3 L211/21/09 13:02169
2-Nitrophenol ND ug/kg 1 12/03/09 20:15 88-75-511/21/09 13:02169
4-Nitrophenol ND ug/kg 1 12/03/09 20:15 100-02-711/21/09 13:02169
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 20:15 62-75-9 L211/21/09 13:02169
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 20:15 621-64-7 L211/21/09 13:02169
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 20:15 86-30-611/21/09 13:02169
Pentachlorophenol ND ug/kg 1 12/03/09 20:15 87-86-511/21/09 13:02668
Phenanthrene ND ug/kg 1 12/03/09 20:15 85-01-811/21/09 13:0232.9
Phenol ND ug/kg 1 12/03/09 20:15 108-95-2 L211/21/09 13:02169
Pyrene ND ug/kg 1 12/03/09 20:15 129-00-011/21/09 13:0232.9
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 20:15 120-82-111/21/09 13:02169
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 20:15 95-95-411/21/09 13:02169
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 20:15 88-06-211/21/09 13:02169
Nitrobenzene-d5 (S)51 %1 12/03/09 20:15 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)69 %1 12/03/09 20:15 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)87 %1 12/03/09 20:15 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)49 %1 12/03/09 20:15 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)47 %1 12/03/09 20:15 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)68 %1 12/03/09 20:15 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 19:50 67-64-179.6
Benzene ND ug/kg 1 11/19/09 19:50 71-43-24.0
Bromobenzene ND ug/kg 1 11/19/09 19:50 108-86-14.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 47 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 2'Lab ID:9257863011 Collected:11/17/09 12:55 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 19:50 74-97-54.0
Bromodichloromethane ND ug/kg 1 11/19/09 19:50 75-27-44.0
Bromoform ND ug/kg 1 11/19/09 19:50 75-25-24.0
Bromomethane ND ug/kg 1 11/19/09 19:50 74-83-98.0
2-Butanone (MEK)ND ug/kg 1 11/19/09 19:50 78-93-379.6
n-Butylbenzene ND ug/kg 1 11/19/09 19:50 104-51-84.0
sec-Butylbenzene ND ug/kg 1 11/19/09 19:50 135-98-84.0
tert-Butylbenzene ND ug/kg 1 11/19/09 19:50 98-06-64.0
Carbon tetrachloride ND ug/kg 1 11/19/09 19:50 56-23-54.0
Chlorobenzene 8.9 ug/kg 1 11/19/09 19:50 108-90-74.0
Chloroethane ND ug/kg 1 11/19/09 19:50 75-00-38.0
Chloroform ND ug/kg 1 11/19/09 19:50 67-66-34.0
Chloromethane ND ug/kg 1 11/19/09 19:50 74-87-38.0
2-Chlorotoluene ND ug/kg 1 11/19/09 19:50 95-49-84.0
4-Chlorotoluene ND ug/kg 1 11/19/09 19:50 106-43-44.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 19:50 96-12-84.0
Dibromochloromethane ND ug/kg 1 11/19/09 19:50 124-48-14.0
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 19:50 106-93-44.0
Dibromomethane ND ug/kg 1 11/19/09 19:50 74-95-34.0
1,2-Dichlorobenzene 4.6 ug/kg 1 11/19/09 19:50 95-50-14.0
1,3-Dichlorobenzene 5.3 ug/kg 1 11/19/09 19:50 541-73-14.0
1,4-Dichlorobenzene 19.7 ug/kg 1 11/19/09 19:50 106-46-74.0
Dichlorodifluoromethane ND ug/kg 1 11/19/09 19:50 75-71-88.0
1,1-Dichloroethane ND ug/kg 1 11/19/09 19:50 75-34-34.0
1,2-Dichloroethane ND ug/kg 1 11/19/09 19:50 107-06-24.0
1,1-Dichloroethene ND ug/kg 1 11/19/09 19:50 75-35-44.0
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 19:50 156-59-24.0
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 19:50 156-60-54.0
1,2-Dichloropropane ND ug/kg 1 11/19/09 19:50 78-87-54.0
1,3-Dichloropropane ND ug/kg 1 11/19/09 19:50 142-28-94.0
2,2-Dichloropropane ND ug/kg 1 11/19/09 19:50 594-20-74.0
1,1-Dichloropropene ND ug/kg 1 11/19/09 19:50 563-58-64.0
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 19:50 10061-01-54.0
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 19:50 10061-02-64.0
Diisopropyl ether ND ug/kg 1 11/19/09 19:50 108-20-34.0
Ethylbenzene ND ug/kg 1 11/19/09 19:50 100-41-44.0
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 19:50 87-68-34.0
2-Hexanone ND ug/kg 1 11/19/09 19:50 591-78-639.8
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 19:50 98-82-84.0
p-Isopropyltoluene ND ug/kg 1 11/19/09 19:50 99-87-64.0
Methylene Chloride ND ug/kg 1 11/19/09 19:50 75-09-215.9
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 19:50 108-10-139.8
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 19:50 1634-04-44.0
Naphthalene ND ug/kg 1 11/19/09 19:50 91-20-34.0
n-Propylbenzene ND ug/kg 1 11/19/09 19:50 103-65-14.0
Styrene ND ug/kg 1 11/19/09 19:50 100-42-54.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 48 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-6 2'Lab ID:9257863011 Collected:11/17/09 12:55 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 19:50 630-20-64.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 19:50 79-34-54.0
Tetrachloroethene ND ug/kg 1 11/19/09 19:50 127-18-44.0
Toluene ND ug/kg 1 11/19/09 19:50 108-88-34.0
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 19:50 87-61-64.0
1,2,4-Trichlorobenzene 9.1 ug/kg 1 11/19/09 19:50 120-82-14.0
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 19:50 71-55-64.0
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 19:50 79-00-54.0
Trichloroethene ND ug/kg 1 11/19/09 19:50 79-01-64.0
Trichlorofluoromethane ND ug/kg 1 11/19/09 19:50 75-69-44.0
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 19:50 96-18-44.0
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 19:50 95-63-64.0
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 19:50 108-67-84.0
Vinyl acetate ND ug/kg 1 11/19/09 19:50 108-05-439.8
Vinyl chloride ND ug/kg 1 11/19/09 19:50 75-01-48.0
Xylene (Total)ND ug/kg 1 11/19/09 19:50 1330-20-78.0
m&p-Xylene ND ug/kg 1 11/19/09 19:50 1330-20-78.0
o-Xylene ND ug/kg 1 11/19/09 19:50 95-47-64.0
Dibromofluoromethane (S)110 %1 11/19/09 19:50 1868-53-779-116
Toluene-d8 (S)102 %1 11/19/09 19:50 2037-26-588-110
4-Bromofluorobenzene (S)94 %1 11/19/09 19:50 460-00-474-115
1,2-Dichloroethane-d4 (S)105 %1 11/19/09 19:50 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 11.0 %1 11/23/09 09:040.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 49 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 0.5'Lab ID:9257863012 Collected:11/17/09 13:07 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:17 7440-38-212/09/09 12:300.025
Barium 0.11 mg/L 1 12/09/09 18:17 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:17 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:17 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:17 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:17 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:17 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:41 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 20:44 83-32-911/21/09 13:0232.4
Acenaphthylene ND ug/kg 1 12/03/09 20:44 208-96-811/21/09 13:0232.4
Anthracene ND ug/kg 1 12/03/09 20:44 120-12-711/21/09 13:0232.4
Benzo(a)anthracene ND ug/kg 1 12/03/09 20:44 56-55-311/21/09 13:0232.4
Benzo(a)pyrene ND ug/kg 1 12/03/09 20:44 50-32-811/21/09 13:0232.4
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 20:44 205-99-211/21/09 13:0232.4
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 20:44 191-24-211/21/09 13:0232.4
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 20:44 207-08-911/21/09 13:0232.4
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 20:44 101-55-311/21/09 13:02167
Butylbenzylphthalate ND ug/kg 1 12/03/09 20:44 85-68-711/21/09 13:02167
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 20:44 59-50-7 L211/21/09 13:02657
4-Chloroaniline ND ug/kg 1 12/03/09 20:44 106-47-811/21/09 13:02167
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 20:44 111-91-1 L211/21/09 13:02167
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 20:44 111-44-4 L211/21/09 13:02167
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 20:44 108-60-111/21/09 13:02167
2-Chloronaphthalene ND ug/kg 1 12/03/09 20:44 91-58-711/21/09 13:02167
2-Chlorophenol ND ug/kg 1 12/03/09 20:44 95-57-811/21/09 13:02167
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 20:44 7005-72-311/21/09 13:02167
Chrysene ND ug/kg 1 12/03/09 20:44 218-01-911/21/09 13:0232.4
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 20:44 53-70-311/21/09 13:0232.4
Dibenzofuran ND ug/kg 1 12/03/09 20:44 132-64-911/21/09 13:02167
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 20:44 95-50-111/21/09 13:02167
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 20:44 541-73-111/21/09 13:02167
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 20:44 106-46-711/21/09 13:02167
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 20:44 91-94-111/21/09 13:02657
2,4-Dichlorophenol ND ug/kg 1 12/03/09 20:44 120-83-211/21/09 13:02167
Diethylphthalate ND ug/kg 1 12/03/09 20:44 84-66-211/21/09 13:02167
2,4-Dimethylphenol ND ug/kg 1 12/03/09 20:44 105-67-9 L211/21/09 13:02167
Dimethylphthalate ND ug/kg 1 12/03/09 20:44 131-11-311/21/09 13:02167
Di-n-butylphthalate ND ug/kg 1 12/03/09 20:44 84-74-211/21/09 13:02167
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 20:44 534-52-111/21/09 13:02657
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 50 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 0.5'Lab ID:9257863012 Collected:11/17/09 13:07 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 20:44 51-28-511/21/09 13:02657
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 20:44 121-14-211/21/09 13:02167
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 20:44 606-20-211/21/09 13:02167
Di-n-octylphthalate ND ug/kg 1 12/03/09 20:44 117-84-011/21/09 13:02167
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 20:44 122-66-711/21/09 13:02167
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 20:44 117-81-711/21/09 13:02167
Fluoranthene ND ug/kg 1 12/03/09 20:44 206-44-011/21/09 13:0232.4
Fluorene ND ug/kg 1 12/03/09 20:44 86-73-711/21/09 13:0232.4
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 20:44 87-68-311/21/09 13:02167
Hexachlorobenzene ND ug/kg 1 12/03/09 20:44 118-74-111/21/09 13:02167
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 20:44 77-47-411/21/09 13:02657
Hexachloroethane ND ug/kg 1 12/03/09 20:44 67-72-1 L211/21/09 13:02167
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 20:44 193-39-511/21/09 13:0232.4
Isophorone ND ug/kg 1 12/03/09 20:44 78-59-1 L211/21/09 13:02167
1-Methylnaphthalene ND ug/kg 1 12/03/09 20:44 90-12-011/21/09 13:0232.4
2-Methylnaphthalene ND ug/kg 1 12/03/09 20:44 91-57-611/21/09 13:0232.4
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 20:44 95-48-7 L211/21/09 13:02167
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 20:4411/21/09 13:02167
Naphthalene ND ug/kg 1 12/03/09 20:44 91-20-311/21/09 13:0232.4
2-Nitroaniline ND ug/kg 1 12/03/09 20:44 88-74-411/21/09 13:02167
3-Nitroaniline ND ug/kg 1 12/03/09 20:44 99-09-2 L211/21/09 13:02167
4-Nitroaniline ND ug/kg 1 12/03/09 20:44 100-01-611/21/09 13:02167
Nitrobenzene ND ug/kg 1 12/03/09 20:44 98-95-3 L211/21/09 13:02167
2-Nitrophenol ND ug/kg 1 12/03/09 20:44 88-75-511/21/09 13:02167
4-Nitrophenol ND ug/kg 1 12/03/09 20:44 100-02-711/21/09 13:02167
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 20:44 62-75-9 L211/21/09 13:02167
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 20:44 621-64-7 L211/21/09 13:02167
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 20:44 86-30-611/21/09 13:02167
Pentachlorophenol ND ug/kg 1 12/03/09 20:44 87-86-511/21/09 13:02657
Phenanthrene ND ug/kg 1 12/03/09 20:44 85-01-811/21/09 13:0232.4
Phenol ND ug/kg 1 12/03/09 20:44 108-95-2 L211/21/09 13:02167
Pyrene ND ug/kg 1 12/03/09 20:44 129-00-011/21/09 13:0232.4
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 20:44 120-82-111/21/09 13:02167
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 20:44 95-95-411/21/09 13:02167
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 20:44 88-06-211/21/09 13:02167
Nitrobenzene-d5 (S)53 %1 12/03/09 20:44 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)66 %1 12/03/09 20:44 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)68 %1 12/03/09 20:44 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)44 %1 12/03/09 20:44 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)51 %1 12/03/09 20:44 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)58 %1 12/03/09 20:44 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 20:08 67-64-195.9
Benzene ND ug/kg 1 11/19/09 20:08 71-43-24.8
Bromobenzene ND ug/kg 1 11/19/09 20:08 108-86-14.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 51 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 0.5'Lab ID:9257863012 Collected:11/17/09 13:07 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 20:08 74-97-54.8
Bromodichloromethane ND ug/kg 1 11/19/09 20:08 75-27-44.8
Bromoform ND ug/kg 1 11/19/09 20:08 75-25-24.8
Bromomethane ND ug/kg 1 11/19/09 20:08 74-83-99.6
2-Butanone (MEK)ND ug/kg 1 11/19/09 20:08 78-93-395.9
n-Butylbenzene ND ug/kg 1 11/19/09 20:08 104-51-84.8
sec-Butylbenzene ND ug/kg 1 11/19/09 20:08 135-98-84.8
tert-Butylbenzene ND ug/kg 1 11/19/09 20:08 98-06-64.8
Carbon tetrachloride ND ug/kg 1 11/19/09 20:08 56-23-54.8
Chlorobenzene ND ug/kg 1 11/19/09 20:08 108-90-74.8
Chloroethane ND ug/kg 1 11/19/09 20:08 75-00-39.6
Chloroform ND ug/kg 1 11/19/09 20:08 67-66-34.8
Chloromethane ND ug/kg 1 11/19/09 20:08 74-87-39.6
2-Chlorotoluene ND ug/kg 1 11/19/09 20:08 95-49-84.8
4-Chlorotoluene ND ug/kg 1 11/19/09 20:08 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 20:08 96-12-84.8
Dibromochloromethane ND ug/kg 1 11/19/09 20:08 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 20:08 106-93-44.8
Dibromomethane ND ug/kg 1 11/19/09 20:08 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 20:08 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 11/19/09 20:08 541-73-14.8
1,4-Dichlorobenzene ND ug/kg 1 11/19/09 20:08 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 11/19/09 20:08 75-71-89.6
1,1-Dichloroethane ND ug/kg 1 11/19/09 20:08 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 11/19/09 20:08 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 11/19/09 20:08 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 20:08 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 20:08 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 11/19/09 20:08 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 11/19/09 20:08 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 11/19/09 20:08 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 11/19/09 20:08 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 20:08 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 20:08 10061-02-64.8
Diisopropyl ether ND ug/kg 1 11/19/09 20:08 108-20-34.8
Ethylbenzene ND ug/kg 1 11/19/09 20:08 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 20:08 87-68-34.8
2-Hexanone ND ug/kg 1 11/19/09 20:08 591-78-648.0
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 20:08 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 11/19/09 20:08 99-87-64.8
Methylene Chloride ND ug/kg 1 11/19/09 20:08 75-09-219.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 20:08 108-10-148.0
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 20:08 1634-04-44.8
Naphthalene ND ug/kg 1 11/19/09 20:08 91-20-34.8
n-Propylbenzene ND ug/kg 1 11/19/09 20:08 103-65-14.8
Styrene ND ug/kg 1 11/19/09 20:08 100-42-54.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 52 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 0.5'Lab ID:9257863012 Collected:11/17/09 13:07 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 20:08 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 20:08 79-34-54.8
Tetrachloroethene ND ug/kg 1 11/19/09 20:08 127-18-44.8
Toluene ND ug/kg 1 11/19/09 20:08 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 20:08 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 11/19/09 20:08 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 20:08 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 20:08 79-00-54.8
Trichloroethene ND ug/kg 1 11/19/09 20:08 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 11/19/09 20:08 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 20:08 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 20:08 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 20:08 108-67-84.8
Vinyl acetate ND ug/kg 1 11/19/09 20:08 108-05-448.0
Vinyl chloride ND ug/kg 1 11/19/09 20:08 75-01-49.6
Xylene (Total)ND ug/kg 1 11/19/09 20:08 1330-20-79.6
m&p-Xylene ND ug/kg 1 11/19/09 20:08 1330-20-79.6
o-Xylene ND ug/kg 1 11/19/09 20:08 95-47-64.8
Dibromofluoromethane (S)108 %1 11/19/09 20:08 1868-53-779-116
Toluene-d8 (S)100 %1 11/19/09 20:08 2037-26-588-110
4-Bromofluorobenzene (S)101 %1 11/19/09 20:08 460-00-474-115
1,2-Dichloroethane-d4 (S)109 %1 11/19/09 20:08 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.0 %1 11/23/09 09:050.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 53 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 1.5'Lab ID:9257863013 Collected:11/17/09 13:11 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:20 7440-38-212/09/09 12:300.025
Barium 0.17 mg/L 1 12/09/09 18:20 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:20 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:20 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:20 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:20 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:20 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:43 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 21:14 83-32-911/21/09 13:0233.0
Acenaphthylene ND ug/kg 1 12/03/09 21:14 208-96-811/21/09 13:0233.0
Anthracene ND ug/kg 1 12/03/09 21:14 120-12-711/21/09 13:0233.0
Benzo(a)anthracene ND ug/kg 1 12/03/09 21:14 56-55-311/21/09 13:0233.0
Benzo(a)pyrene ND ug/kg 1 12/03/09 21:14 50-32-811/21/09 13:0233.0
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 21:14 205-99-211/21/09 13:0233.0
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 21:14 191-24-211/21/09 13:0233.0
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 21:14 207-08-911/21/09 13:0233.0
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 21:14 101-55-311/21/09 13:02170
Butylbenzylphthalate ND ug/kg 1 12/03/09 21:14 85-68-711/21/09 13:02170
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 21:14 59-50-7 L211/21/09 13:02670
4-Chloroaniline ND ug/kg 1 12/03/09 21:14 106-47-811/21/09 13:02170
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 21:14 111-91-1 L211/21/09 13:02170
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 21:14 111-44-4 L211/21/09 13:02170
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 21:14 108-60-111/21/09 13:02170
2-Chloronaphthalene ND ug/kg 1 12/03/09 21:14 91-58-711/21/09 13:02170
2-Chlorophenol ND ug/kg 1 12/03/09 21:14 95-57-811/21/09 13:02170
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 21:14 7005-72-311/21/09 13:02170
Chrysene ND ug/kg 1 12/03/09 21:14 218-01-911/21/09 13:0233.0
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 21:14 53-70-311/21/09 13:0233.0
Dibenzofuran ND ug/kg 1 12/03/09 21:14 132-64-911/21/09 13:02170
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 21:14 95-50-111/21/09 13:02170
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 21:14 541-73-111/21/09 13:02170
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 21:14 106-46-711/21/09 13:02170
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 21:14 91-94-111/21/09 13:02670
2,4-Dichlorophenol ND ug/kg 1 12/03/09 21:14 120-83-211/21/09 13:02170
Diethylphthalate ND ug/kg 1 12/03/09 21:14 84-66-211/21/09 13:02170
2,4-Dimethylphenol ND ug/kg 1 12/03/09 21:14 105-67-9 L211/21/09 13:02170
Dimethylphthalate ND ug/kg 1 12/03/09 21:14 131-11-311/21/09 13:02170
Di-n-butylphthalate ND ug/kg 1 12/03/09 21:14 84-74-211/21/09 13:02170
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 21:14 534-52-111/21/09 13:02670
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 54 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 1.5'Lab ID:9257863013 Collected:11/17/09 13:11 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 21:14 51-28-511/21/09 13:02670
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 21:14 121-14-211/21/09 13:02170
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 21:14 606-20-211/21/09 13:02170
Di-n-octylphthalate ND ug/kg 1 12/03/09 21:14 117-84-011/21/09 13:02170
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 21:14 122-66-711/21/09 13:02170
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 21:14 117-81-711/21/09 13:02170
Fluoranthene ND ug/kg 1 12/03/09 21:14 206-44-011/21/09 13:0233.0
Fluorene ND ug/kg 1 12/03/09 21:14 86-73-711/21/09 13:0233.0
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 21:14 87-68-311/21/09 13:02170
Hexachlorobenzene ND ug/kg 1 12/03/09 21:14 118-74-111/21/09 13:02170
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 21:14 77-47-411/21/09 13:02670
Hexachloroethane ND ug/kg 1 12/03/09 21:14 67-72-1 L211/21/09 13:02170
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 21:14 193-39-511/21/09 13:0233.0
Isophorone ND ug/kg 1 12/03/09 21:14 78-59-1 L211/21/09 13:02170
1-Methylnaphthalene ND ug/kg 1 12/03/09 21:14 90-12-011/21/09 13:0233.0
2-Methylnaphthalene ND ug/kg 1 12/03/09 21:14 91-57-611/21/09 13:0233.0
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 21:14 95-48-7 L211/21/09 13:02170
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 21:1411/21/09 13:02170
Naphthalene ND ug/kg 1 12/03/09 21:14 91-20-311/21/09 13:0233.0
2-Nitroaniline ND ug/kg 1 12/03/09 21:14 88-74-411/21/09 13:02170
3-Nitroaniline ND ug/kg 1 12/03/09 21:14 99-09-2 L211/21/09 13:02170
4-Nitroaniline ND ug/kg 1 12/03/09 21:14 100-01-611/21/09 13:02170
Nitrobenzene ND ug/kg 1 12/03/09 21:14 98-95-3 L211/21/09 13:02170
2-Nitrophenol ND ug/kg 1 12/03/09 21:14 88-75-511/21/09 13:02170
4-Nitrophenol ND ug/kg 1 12/03/09 21:14 100-02-711/21/09 13:02170
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 21:14 62-75-9 L211/21/09 13:02170
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 21:14 621-64-7 L211/21/09 13:02170
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 21:14 86-30-611/21/09 13:02170
Pentachlorophenol ND ug/kg 1 12/03/09 21:14 87-86-511/21/09 13:02670
Phenanthrene ND ug/kg 1 12/03/09 21:14 85-01-811/21/09 13:0233.0
Phenol ND ug/kg 1 12/03/09 21:14 108-95-2 L211/21/09 13:02170
Pyrene ND ug/kg 1 12/03/09 21:14 129-00-011/21/09 13:0233.0
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 21:14 120-82-111/21/09 13:02170
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 21:14 95-95-411/21/09 13:02170
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 21:14 88-06-211/21/09 13:02170
Nitrobenzene-d5 (S)45 %1 12/03/09 21:14 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)55 %1 12/03/09 21:14 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)55 %1 12/03/09 21:14 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)37 %1 12/03/09 21:14 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)44 %1 12/03/09 21:14 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)53 %1 12/03/09 21:14 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 20:26 67-64-1113
Benzene ND ug/kg 1 11/19/09 20:26 71-43-25.7
Bromobenzene ND ug/kg 1 11/19/09 20:26 108-86-15.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 55 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 1.5'Lab ID:9257863013 Collected:11/17/09 13:11 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 20:26 74-97-55.7
Bromodichloromethane ND ug/kg 1 11/19/09 20:26 75-27-45.7
Bromoform ND ug/kg 1 11/19/09 20:26 75-25-25.7
Bromomethane ND ug/kg 1 11/19/09 20:26 74-83-911.3
2-Butanone (MEK)ND ug/kg 1 11/19/09 20:26 78-93-3113
n-Butylbenzene ND ug/kg 1 11/19/09 20:26 104-51-85.7
sec-Butylbenzene ND ug/kg 1 11/19/09 20:26 135-98-85.7
tert-Butylbenzene ND ug/kg 1 11/19/09 20:26 98-06-65.7
Carbon tetrachloride ND ug/kg 1 11/19/09 20:26 56-23-55.7
Chlorobenzene 17.3 ug/kg 1 11/19/09 20:26 108-90-75.7
Chloroethane ND ug/kg 1 11/19/09 20:26 75-00-311.3
Chloroform ND ug/kg 1 11/19/09 20:26 67-66-35.7
Chloromethane ND ug/kg 1 11/19/09 20:26 74-87-311.3
2-Chlorotoluene ND ug/kg 1 11/19/09 20:26 95-49-85.7
4-Chlorotoluene ND ug/kg 1 11/19/09 20:26 106-43-45.7
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 20:26 96-12-85.7
Dibromochloromethane ND ug/kg 1 11/19/09 20:26 124-48-15.7
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 20:26 106-93-45.7
Dibromomethane ND ug/kg 1 11/19/09 20:26 74-95-35.7
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 20:26 95-50-15.7
1,3-Dichlorobenzene ND ug/kg 1 11/19/09 20:26 541-73-15.7
1,4-Dichlorobenzene 13.0 ug/kg 1 11/19/09 20:26 106-46-75.7
Dichlorodifluoromethane ND ug/kg 1 11/19/09 20:26 75-71-811.3
1,1-Dichloroethane ND ug/kg 1 11/19/09 20:26 75-34-35.7
1,2-Dichloroethane ND ug/kg 1 11/19/09 20:26 107-06-25.7
1,1-Dichloroethene ND ug/kg 1 11/19/09 20:26 75-35-45.7
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 20:26 156-59-25.7
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 20:26 156-60-55.7
1,2-Dichloropropane ND ug/kg 1 11/19/09 20:26 78-87-55.7
1,3-Dichloropropane ND ug/kg 1 11/19/09 20:26 142-28-95.7
2,2-Dichloropropane ND ug/kg 1 11/19/09 20:26 594-20-75.7
1,1-Dichloropropene ND ug/kg 1 11/19/09 20:26 563-58-65.7
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 20:26 10061-01-55.7
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 20:26 10061-02-65.7
Diisopropyl ether ND ug/kg 1 11/19/09 20:26 108-20-35.7
Ethylbenzene ND ug/kg 1 11/19/09 20:26 100-41-45.7
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 20:26 87-68-35.7
2-Hexanone ND ug/kg 1 11/19/09 20:26 591-78-656.5
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 20:26 98-82-85.7
p-Isopropyltoluene ND ug/kg 1 11/19/09 20:26 99-87-65.7
Methylene Chloride ND ug/kg 1 11/19/09 20:26 75-09-222.6
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 20:26 108-10-156.5
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 20:26 1634-04-45.7
Naphthalene ND ug/kg 1 11/19/09 20:26 91-20-35.7
n-Propylbenzene ND ug/kg 1 11/19/09 20:26 103-65-15.7
Styrene ND ug/kg 1 11/19/09 20:26 100-42-55.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 56 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-7 1.5'Lab ID:9257863013 Collected:11/17/09 13:11 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 20:26 630-20-65.7
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 20:26 79-34-55.7
Tetrachloroethene ND ug/kg 1 11/19/09 20:26 127-18-45.7
Toluene ND ug/kg 1 11/19/09 20:26 108-88-35.7
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 20:26 87-61-65.7
1,2,4-Trichlorobenzene ND ug/kg 1 11/19/09 20:26 120-82-15.7
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 20:26 71-55-65.7
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 20:26 79-00-55.7
Trichloroethene ND ug/kg 1 11/19/09 20:26 79-01-65.7
Trichlorofluoromethane ND ug/kg 1 11/19/09 20:26 75-69-45.7
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 20:26 96-18-45.7
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 20:26 95-63-65.7
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 20:26 108-67-85.7
Vinyl acetate ND ug/kg 1 11/19/09 20:26 108-05-456.5
Vinyl chloride ND ug/kg 1 11/19/09 20:26 75-01-411.3
Xylene (Total)ND ug/kg 1 11/19/09 20:26 1330-20-711.3
m&p-Xylene ND ug/kg 1 11/19/09 20:26 1330-20-711.3
o-Xylene ND ug/kg 1 11/19/09 20:26 95-47-65.7
Dibromofluoromethane (S)110 %1 11/19/09 20:26 1868-53-779-116
Toluene-d8 (S)102 %1 11/19/09 20:26 2037-26-588-110
4-Bromofluorobenzene (S)99 %1 11/19/09 20:26 460-00-474-115
1,2-Dichloroethane-d4 (S)105 %1 11/19/09 20:26 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.6 %1 11/23/09 09:050.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 57 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 0.5'Lab ID:9257863014 Collected:11/17/09 13:16 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:24 7440-38-212/09/09 12:300.025
Barium 0.15 mg/L 1 12/09/09 18:24 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:24 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:24 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:24 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:24 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:24 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:46 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 21:43 83-32-911/21/09 13:0232.8
Acenaphthylene ND ug/kg 1 12/03/09 21:43 208-96-811/21/09 13:0232.8
Anthracene ND ug/kg 1 12/03/09 21:43 120-12-711/21/09 13:0232.8
Benzo(a)anthracene ND ug/kg 1 12/03/09 21:43 56-55-311/21/09 13:0232.8
Benzo(a)pyrene ND ug/kg 1 12/03/09 21:43 50-32-811/21/09 13:0232.8
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 21:43 205-99-211/21/09 13:0232.8
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 21:43 191-24-211/21/09 13:0232.8
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 21:43 207-08-911/21/09 13:0232.8
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 21:43 101-55-311/21/09 13:02169
Butylbenzylphthalate ND ug/kg 1 12/03/09 21:43 85-68-711/21/09 13:02169
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 21:43 59-50-7 L211/21/09 13:02666
4-Chloroaniline ND ug/kg 1 12/03/09 21:43 106-47-811/21/09 13:02169
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 21:43 111-91-1 L211/21/09 13:02169
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 21:43 111-44-4 L211/21/09 13:02169
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 21:43 108-60-111/21/09 13:02169
2-Chloronaphthalene ND ug/kg 1 12/03/09 21:43 91-58-711/21/09 13:02169
2-Chlorophenol ND ug/kg 1 12/03/09 21:43 95-57-811/21/09 13:02169
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 21:43 7005-72-311/21/09 13:02169
Chrysene ND ug/kg 1 12/03/09 21:43 218-01-911/21/09 13:0232.8
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 21:43 53-70-311/21/09 13:0232.8
Dibenzofuran ND ug/kg 1 12/03/09 21:43 132-64-911/21/09 13:02169
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 21:43 95-50-111/21/09 13:02169
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 21:43 541-73-111/21/09 13:02169
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 21:43 106-46-711/21/09 13:02169
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 21:43 91-94-111/21/09 13:02666
2,4-Dichlorophenol ND ug/kg 1 12/03/09 21:43 120-83-211/21/09 13:02169
Diethylphthalate ND ug/kg 1 12/03/09 21:43 84-66-211/21/09 13:02169
2,4-Dimethylphenol ND ug/kg 1 12/03/09 21:43 105-67-9 L211/21/09 13:02169
Dimethylphthalate ND ug/kg 1 12/03/09 21:43 131-11-311/21/09 13:02169
Di-n-butylphthalate ND ug/kg 1 12/03/09 21:43 84-74-211/21/09 13:02169
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 21:43 534-52-111/21/09 13:02666
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 58 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 0.5'Lab ID:9257863014 Collected:11/17/09 13:16 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 21:43 51-28-511/21/09 13:02666
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 21:43 121-14-211/21/09 13:02169
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 21:43 606-20-211/21/09 13:02169
Di-n-octylphthalate ND ug/kg 1 12/03/09 21:43 117-84-011/21/09 13:02169
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 21:43 122-66-711/21/09 13:02169
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 21:43 117-81-711/21/09 13:02169
Fluoranthene ND ug/kg 1 12/03/09 21:43 206-44-011/21/09 13:0232.8
Fluorene ND ug/kg 1 12/03/09 21:43 86-73-711/21/09 13:0232.8
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 21:43 87-68-311/21/09 13:02169
Hexachlorobenzene ND ug/kg 1 12/03/09 21:43 118-74-111/21/09 13:02169
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 21:43 77-47-411/21/09 13:02666
Hexachloroethane ND ug/kg 1 12/03/09 21:43 67-72-1 L211/21/09 13:02169
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 21:43 193-39-511/21/09 13:0232.8
Isophorone ND ug/kg 1 12/03/09 21:43 78-59-1 L211/21/09 13:02169
1-Methylnaphthalene ND ug/kg 1 12/03/09 21:43 90-12-011/21/09 13:0232.8
2-Methylnaphthalene ND ug/kg 1 12/03/09 21:43 91-57-611/21/09 13:0232.8
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 21:43 95-48-7 L211/21/09 13:02169
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 21:4311/21/09 13:02169
Naphthalene ND ug/kg 1 12/03/09 21:43 91-20-311/21/09 13:0232.8
2-Nitroaniline ND ug/kg 1 12/03/09 21:43 88-74-411/21/09 13:02169
3-Nitroaniline ND ug/kg 1 12/03/09 21:43 99-09-2 L211/21/09 13:02169
4-Nitroaniline ND ug/kg 1 12/03/09 21:43 100-01-611/21/09 13:02169
Nitrobenzene ND ug/kg 1 12/03/09 21:43 98-95-3 L211/21/09 13:02169
2-Nitrophenol ND ug/kg 1 12/03/09 21:43 88-75-511/21/09 13:02169
4-Nitrophenol ND ug/kg 1 12/03/09 21:43 100-02-711/21/09 13:02169
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 21:43 62-75-9 L211/21/09 13:02169
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 21:43 621-64-7 L211/21/09 13:02169
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 21:43 86-30-611/21/09 13:02169
Pentachlorophenol ND ug/kg 1 12/03/09 21:43 87-86-511/21/09 13:02666
Phenanthrene ND ug/kg 1 12/03/09 21:43 85-01-811/21/09 13:0232.8
Phenol ND ug/kg 1 12/03/09 21:43 108-95-2 L211/21/09 13:02169
Pyrene ND ug/kg 1 12/03/09 21:43 129-00-011/21/09 13:0232.8
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 21:43 120-82-111/21/09 13:02169
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 21:43 95-95-411/21/09 13:02169
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 21:43 88-06-211/21/09 13:02169
Nitrobenzene-d5 (S)42 %1 12/03/09 21:43 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)55 %1 12/03/09 21:43 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)69 %1 12/03/09 21:43 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)33 %1 12/03/09 21:43 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)39 %1 12/03/09 21:43 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)53 %1 12/03/09 21:43 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/19/09 20:44 67-64-179.8
Benzene ND ug/kg 1 11/19/09 20:44 71-43-24.0
Bromobenzene ND ug/kg 1 11/19/09 20:44 108-86-14.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 59 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 0.5'Lab ID:9257863014 Collected:11/17/09 13:16 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/19/09 20:44 74-97-54.0
Bromodichloromethane ND ug/kg 1 11/19/09 20:44 75-27-44.0
Bromoform ND ug/kg 1 11/19/09 20:44 75-25-24.0
Bromomethane ND ug/kg 1 11/19/09 20:44 74-83-98.0
2-Butanone (MEK)ND ug/kg 1 11/19/09 20:44 78-93-379.8
n-Butylbenzene ND ug/kg 1 11/19/09 20:44 104-51-84.0
sec-Butylbenzene ND ug/kg 1 11/19/09 20:44 135-98-84.0
tert-Butylbenzene ND ug/kg 1 11/19/09 20:44 98-06-64.0
Carbon tetrachloride ND ug/kg 1 11/19/09 20:44 56-23-54.0
Chlorobenzene 28.5 ug/kg 1 11/19/09 20:44 108-90-74.0
Chloroethane ND ug/kg 1 11/19/09 20:44 75-00-38.0
Chloroform ND ug/kg 1 11/19/09 20:44 67-66-34.0
Chloromethane ND ug/kg 1 11/19/09 20:44 74-87-38.0
2-Chlorotoluene ND ug/kg 1 11/19/09 20:44 95-49-84.0
4-Chlorotoluene ND ug/kg 1 11/19/09 20:44 106-43-44.0
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/19/09 20:44 96-12-84.0
Dibromochloromethane ND ug/kg 1 11/19/09 20:44 124-48-14.0
1,2-Dibromoethane (EDB)ND ug/kg 1 11/19/09 20:44 106-93-44.0
Dibromomethane ND ug/kg 1 11/19/09 20:44 74-95-34.0
1,2-Dichlorobenzene ND ug/kg 1 11/19/09 20:44 95-50-14.0
1,3-Dichlorobenzene ND ug/kg 1 11/19/09 20:44 541-73-14.0
1,4-Dichlorobenzene 5.3 ug/kg 1 11/19/09 20:44 106-46-74.0
Dichlorodifluoromethane ND ug/kg 1 11/19/09 20:44 75-71-88.0
1,1-Dichloroethane ND ug/kg 1 11/19/09 20:44 75-34-34.0
1,2-Dichloroethane ND ug/kg 1 11/19/09 20:44 107-06-24.0
1,1-Dichloroethene ND ug/kg 1 11/19/09 20:44 75-35-44.0
cis-1,2-Dichloroethene ND ug/kg 1 11/19/09 20:44 156-59-24.0
trans-1,2-Dichloroethene ND ug/kg 1 11/19/09 20:44 156-60-54.0
1,2-Dichloropropane ND ug/kg 1 11/19/09 20:44 78-87-54.0
1,3-Dichloropropane ND ug/kg 1 11/19/09 20:44 142-28-94.0
2,2-Dichloropropane ND ug/kg 1 11/19/09 20:44 594-20-74.0
1,1-Dichloropropene ND ug/kg 1 11/19/09 20:44 563-58-64.0
cis-1,3-Dichloropropene ND ug/kg 1 11/19/09 20:44 10061-01-54.0
trans-1,3-Dichloropropene ND ug/kg 1 11/19/09 20:44 10061-02-64.0
Diisopropyl ether ND ug/kg 1 11/19/09 20:44 108-20-34.0
Ethylbenzene ND ug/kg 1 11/19/09 20:44 100-41-44.0
Hexachloro-1,3-butadiene ND ug/kg 1 11/19/09 20:44 87-68-34.0
2-Hexanone ND ug/kg 1 11/19/09 20:44 591-78-639.9
Isopropylbenzene (Cumene)ND ug/kg 1 11/19/09 20:44 98-82-84.0
p-Isopropyltoluene ND ug/kg 1 11/19/09 20:44 99-87-64.0
Methylene Chloride ND ug/kg 1 11/19/09 20:44 75-09-216.0
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/19/09 20:44 108-10-139.9
Methyl-tert-butyl ether ND ug/kg 1 11/19/09 20:44 1634-04-44.0
Naphthalene ND ug/kg 1 11/19/09 20:44 91-20-34.0
n-Propylbenzene ND ug/kg 1 11/19/09 20:44 103-65-14.0
Styrene ND ug/kg 1 11/19/09 20:44 100-42-54.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 60 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 0.5'Lab ID:9257863014 Collected:11/17/09 13:16 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/19/09 20:44 630-20-64.0
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/19/09 20:44 79-34-54.0
Tetrachloroethene ND ug/kg 1 11/19/09 20:44 127-18-44.0
Toluene ND ug/kg 1 11/19/09 20:44 108-88-34.0
1,2,3-Trichlorobenzene ND ug/kg 1 11/19/09 20:44 87-61-64.0
1,2,4-Trichlorobenzene ND ug/kg 1 11/19/09 20:44 120-82-14.0
1,1,1-Trichloroethane ND ug/kg 1 11/19/09 20:44 71-55-64.0
1,1,2-Trichloroethane ND ug/kg 1 11/19/09 20:44 79-00-54.0
Trichloroethene ND ug/kg 1 11/19/09 20:44 79-01-64.0
Trichlorofluoromethane ND ug/kg 1 11/19/09 20:44 75-69-44.0
1,2,3-Trichloropropane ND ug/kg 1 11/19/09 20:44 96-18-44.0
1,2,4-Trimethylbenzene ND ug/kg 1 11/19/09 20:44 95-63-64.0
1,3,5-Trimethylbenzene ND ug/kg 1 11/19/09 20:44 108-67-84.0
Vinyl acetate ND ug/kg 1 11/19/09 20:44 108-05-439.9
Vinyl chloride ND ug/kg 1 11/19/09 20:44 75-01-48.0
Xylene (Total)ND ug/kg 1 11/19/09 20:44 1330-20-78.0
m&p-Xylene ND ug/kg 1 11/19/09 20:44 1330-20-78.0
o-Xylene ND ug/kg 1 11/19/09 20:44 95-47-64.0
Dibromofluoromethane (S)104 %1 11/19/09 20:44 1868-53-779-116
Toluene-d8 (S)98 %1 11/19/09 20:44 2037-26-588-110
4-Bromofluorobenzene (S)101 %1 11/19/09 20:44 460-00-474-115
1,2-Dichloroethane-d4 (S)98 %1 11/19/09 20:44 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.9 %1 11/23/09 09:050.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 61 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 2'Lab ID:9257863015 Collected:11/17/09 13:21 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:27 7440-38-212/09/09 12:300.025
Barium 0.11 mg/L 1 12/09/09 18:27 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:27 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:27 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:27 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:27 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:27 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:48 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 22:13 83-32-911/21/09 13:0232.7
Acenaphthylene ND ug/kg 1 12/03/09 22:13 208-96-811/21/09 13:0232.7
Anthracene ND ug/kg 1 12/03/09 22:13 120-12-711/21/09 13:0232.7
Benzo(a)anthracene ND ug/kg 1 12/03/09 22:13 56-55-311/21/09 13:0232.7
Benzo(a)pyrene ND ug/kg 1 12/03/09 22:13 50-32-811/21/09 13:0232.7
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 22:13 205-99-211/21/09 13:0232.7
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 22:13 191-24-211/21/09 13:0232.7
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 22:13 207-08-911/21/09 13:0232.7
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 22:13 101-55-311/21/09 13:02168
Butylbenzylphthalate ND ug/kg 1 12/03/09 22:13 85-68-711/21/09 13:02168
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 22:13 59-50-7 L211/21/09 13:02663
4-Chloroaniline ND ug/kg 1 12/03/09 22:13 106-47-811/21/09 13:02168
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 22:13 111-91-1 L211/21/09 13:02168
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 22:13 111-44-4 L211/21/09 13:02168
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 22:13 108-60-111/21/09 13:02168
2-Chloronaphthalene ND ug/kg 1 12/03/09 22:13 91-58-711/21/09 13:02168
2-Chlorophenol ND ug/kg 1 12/03/09 22:13 95-57-811/21/09 13:02168
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 22:13 7005-72-311/21/09 13:02168
Chrysene ND ug/kg 1 12/03/09 22:13 218-01-911/21/09 13:0232.7
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 22:13 53-70-311/21/09 13:0232.7
Dibenzofuran ND ug/kg 1 12/03/09 22:13 132-64-911/21/09 13:02168
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 22:13 95-50-111/21/09 13:02168
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 22:13 541-73-111/21/09 13:02168
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 22:13 106-46-711/21/09 13:02168
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 22:13 91-94-111/21/09 13:02663
2,4-Dichlorophenol ND ug/kg 1 12/03/09 22:13 120-83-211/21/09 13:02168
Diethylphthalate ND ug/kg 1 12/03/09 22:13 84-66-211/21/09 13:02168
2,4-Dimethylphenol ND ug/kg 1 12/03/09 22:13 105-67-9 L211/21/09 13:02168
Dimethylphthalate ND ug/kg 1 12/03/09 22:13 131-11-311/21/09 13:02168
Di-n-butylphthalate ND ug/kg 1 12/03/09 22:13 84-74-211/21/09 13:02168
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 22:13 534-52-111/21/09 13:02663
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 62 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 2'Lab ID:9257863015 Collected:11/17/09 13:21 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 22:13 51-28-511/21/09 13:02663
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 22:13 121-14-211/21/09 13:02168
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 22:13 606-20-211/21/09 13:02168
Di-n-octylphthalate ND ug/kg 1 12/03/09 22:13 117-84-011/21/09 13:02168
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 22:13 122-66-711/21/09 13:02168
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 22:13 117-81-711/21/09 13:02168
Fluoranthene ND ug/kg 1 12/03/09 22:13 206-44-011/21/09 13:0232.7
Fluorene ND ug/kg 1 12/03/09 22:13 86-73-711/21/09 13:0232.7
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 22:13 87-68-311/21/09 13:02168
Hexachlorobenzene ND ug/kg 1 12/03/09 22:13 118-74-111/21/09 13:02168
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 22:13 77-47-411/21/09 13:02663
Hexachloroethane ND ug/kg 1 12/03/09 22:13 67-72-1 L211/21/09 13:02168
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 22:13 193-39-511/21/09 13:0232.7
Isophorone ND ug/kg 1 12/03/09 22:13 78-59-1 L211/21/09 13:02168
1-Methylnaphthalene ND ug/kg 1 12/03/09 22:13 90-12-011/21/09 13:0232.7
2-Methylnaphthalene ND ug/kg 1 12/03/09 22:13 91-57-611/21/09 13:0232.7
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 22:13 95-48-7 L211/21/09 13:02168
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 22:1311/21/09 13:02168
Naphthalene ND ug/kg 1 12/03/09 22:13 91-20-311/21/09 13:0232.7
2-Nitroaniline ND ug/kg 1 12/03/09 22:13 88-74-411/21/09 13:02168
3-Nitroaniline ND ug/kg 1 12/03/09 22:13 99-09-2 L211/21/09 13:02168
4-Nitroaniline ND ug/kg 1 12/03/09 22:13 100-01-611/21/09 13:02168
Nitrobenzene ND ug/kg 1 12/03/09 22:13 98-95-3 L211/21/09 13:02168
2-Nitrophenol ND ug/kg 1 12/03/09 22:13 88-75-511/21/09 13:02168
4-Nitrophenol ND ug/kg 1 12/03/09 22:13 100-02-711/21/09 13:02168
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 22:13 62-75-9 L211/21/09 13:02168
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 22:13 621-64-7 L211/21/09 13:02168
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 22:13 86-30-611/21/09 13:02168
Pentachlorophenol ND ug/kg 1 12/03/09 22:13 87-86-511/21/09 13:02663
Phenanthrene ND ug/kg 1 12/03/09 22:13 85-01-811/21/09 13:0232.7
Phenol ND ug/kg 1 12/03/09 22:13 108-95-2 L211/21/09 13:02168
Pyrene ND ug/kg 1 12/03/09 22:13 129-00-011/21/09 13:0232.7
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 22:13 120-82-111/21/09 13:02168
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 22:13 95-95-411/21/09 13:02168
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 22:13 88-06-211/21/09 13:02168
Nitrobenzene-d5 (S)48 %1 12/03/09 22:13 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)66 %1 12/03/09 22:13 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)70 %1 12/03/09 22:13 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)41 %1 12/03/09 22:13 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)48 %1 12/03/09 22:13 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)60 %1 12/03/09 22:13 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/30/09 19:34 67-64-195.3
Benzene ND ug/kg 1 11/30/09 19:34 71-43-24.8
Bromobenzene ND ug/kg 1 11/30/09 19:34 108-86-14.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 63 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 2'Lab ID:9257863015 Collected:11/17/09 13:21 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/30/09 19:34 74-97-54.8
Bromodichloromethane ND ug/kg 1 11/30/09 19:34 75-27-44.8
Bromoform ND ug/kg 1 11/30/09 19:34 75-25-24.8
Bromomethane ND ug/kg 1 11/30/09 19:34 74-83-99.5
2-Butanone (MEK)ND ug/kg 1 11/30/09 19:34 78-93-395.3
n-Butylbenzene ND ug/kg 1 11/30/09 19:34 104-51-84.8
sec-Butylbenzene ND ug/kg 1 11/30/09 19:34 135-98-84.8
tert-Butylbenzene ND ug/kg 1 11/30/09 19:34 98-06-64.8
Carbon tetrachloride ND ug/kg 1 11/30/09 19:34 56-23-54.8
Chlorobenzene 51.9 ug/kg 1 11/30/09 19:34 108-90-74.8
Chloroethane ND ug/kg 1 11/30/09 19:34 75-00-39.5
Chloroform ND ug/kg 1 11/30/09 19:34 67-66-34.8
Chloromethane ND ug/kg 1 11/30/09 19:34 74-87-39.5
2-Chlorotoluene ND ug/kg 1 11/30/09 19:34 95-49-84.8
4-Chlorotoluene ND ug/kg 1 11/30/09 19:34 106-43-44.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/30/09 19:34 96-12-84.8
Dibromochloromethane ND ug/kg 1 11/30/09 19:34 124-48-14.8
1,2-Dibromoethane (EDB)ND ug/kg 1 11/30/09 19:34 106-93-44.8
Dibromomethane ND ug/kg 1 11/30/09 19:34 74-95-34.8
1,2-Dichlorobenzene ND ug/kg 1 11/30/09 19:34 95-50-14.8
1,3-Dichlorobenzene ND ug/kg 1 11/30/09 19:34 541-73-14.8
1,4-Dichlorobenzene 7.0 ug/kg 1 11/30/09 19:34 106-46-74.8
Dichlorodifluoromethane ND ug/kg 1 11/30/09 19:34 75-71-89.5
1,1-Dichloroethane ND ug/kg 1 11/30/09 19:34 75-34-34.8
1,2-Dichloroethane ND ug/kg 1 11/30/09 19:34 107-06-24.8
1,1-Dichloroethene ND ug/kg 1 11/30/09 19:34 75-35-44.8
cis-1,2-Dichloroethene ND ug/kg 1 11/30/09 19:34 156-59-24.8
trans-1,2-Dichloroethene ND ug/kg 1 11/30/09 19:34 156-60-54.8
1,2-Dichloropropane ND ug/kg 1 11/30/09 19:34 78-87-54.8
1,3-Dichloropropane ND ug/kg 1 11/30/09 19:34 142-28-94.8
2,2-Dichloropropane ND ug/kg 1 11/30/09 19:34 594-20-74.8
1,1-Dichloropropene ND ug/kg 1 11/30/09 19:34 563-58-64.8
cis-1,3-Dichloropropene ND ug/kg 1 11/30/09 19:34 10061-01-54.8
trans-1,3-Dichloropropene ND ug/kg 1 11/30/09 19:34 10061-02-64.8
Diisopropyl ether ND ug/kg 1 11/30/09 19:34 108-20-34.8
Ethylbenzene ND ug/kg 1 11/30/09 19:34 100-41-44.8
Hexachloro-1,3-butadiene ND ug/kg 1 11/30/09 19:34 87-68-34.8
2-Hexanone ND ug/kg 1 11/30/09 19:34 591-78-647.6
Isopropylbenzene (Cumene)ND ug/kg 1 11/30/09 19:34 98-82-84.8
p-Isopropyltoluene ND ug/kg 1 11/30/09 19:34 99-87-64.8
Methylene Chloride ND ug/kg 1 11/30/09 19:34 75-09-219.1
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/30/09 19:34 108-10-147.6
Methyl-tert-butyl ether ND ug/kg 1 11/30/09 19:34 1634-04-44.8
Naphthalene ND ug/kg 1 11/30/09 19:34 91-20-34.8
n-Propylbenzene ND ug/kg 1 11/30/09 19:34 103-65-14.8
Styrene ND ug/kg 1 11/30/09 19:34 100-42-54.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 64 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-8 2'Lab ID:9257863015 Collected:11/17/09 13:21 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/30/09 19:34 630-20-64.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/30/09 19:34 79-34-54.8
Tetrachloroethene ND ug/kg 1 11/30/09 19:34 127-18-44.8
Toluene ND ug/kg 1 11/30/09 19:34 108-88-34.8
1,2,3-Trichlorobenzene ND ug/kg 1 11/30/09 19:34 87-61-64.8
1,2,4-Trichlorobenzene ND ug/kg 1 11/30/09 19:34 120-82-14.8
1,1,1-Trichloroethane ND ug/kg 1 11/30/09 19:34 71-55-64.8
1,1,2-Trichloroethane ND ug/kg 1 11/30/09 19:34 79-00-54.8
Trichloroethene ND ug/kg 1 11/30/09 19:34 79-01-64.8
Trichlorofluoromethane ND ug/kg 1 11/30/09 19:34 75-69-44.8
1,2,3-Trichloropropane ND ug/kg 1 11/30/09 19:34 96-18-44.8
1,2,4-Trimethylbenzene ND ug/kg 1 11/30/09 19:34 95-63-64.8
1,3,5-Trimethylbenzene ND ug/kg 1 11/30/09 19:34 108-67-84.8
Vinyl acetate ND ug/kg 1 11/30/09 19:34 108-05-447.6
Vinyl chloride ND ug/kg 1 11/30/09 19:34 75-01-49.5
Xylene (Total)ND ug/kg 1 11/30/09 19:34 1330-20-79.5
m&p-Xylene ND ug/kg 1 11/30/09 19:34 1330-20-79.5
o-Xylene ND ug/kg 1 11/30/09 19:34 95-47-64.8
Dibromofluoromethane (S)107 %1 11/30/09 19:34 1868-53-779-116
Toluene-d8 (S)101 %1 11/30/09 19:34 2037-26-588-110
4-Bromofluorobenzene (S)105 %1 11/30/09 19:34 460-00-474-115
1,2-Dichloroethane-d4 (S)89 %1 11/30/09 19:34 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.0 %1 11/23/09 14:270.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 65 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 0.5'Lab ID:9257863016 Collected:11/17/09 13:36 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:30 7440-38-212/09/09 12:300.025
Barium 0.23 mg/L 1 12/09/09 18:30 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:30 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:30 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:30 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:30 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:30 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:51 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 22:43 83-32-911/21/09 13:0232.7
Acenaphthylene ND ug/kg 1 12/03/09 22:43 208-96-811/21/09 13:0232.7
Anthracene ND ug/kg 1 12/03/09 22:43 120-12-711/21/09 13:0232.7
Benzo(a)anthracene ND ug/kg 1 12/03/09 22:43 56-55-311/21/09 13:0232.7
Benzo(a)pyrene ND ug/kg 1 12/03/09 22:43 50-32-811/21/09 13:0232.7
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 22:43 205-99-211/21/09 13:0232.7
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 22:43 191-24-211/21/09 13:0232.7
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 22:43 207-08-911/21/09 13:0232.7
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 22:43 101-55-311/21/09 13:02168
Butylbenzylphthalate ND ug/kg 1 12/03/09 22:43 85-68-711/21/09 13:02168
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 22:43 59-50-7 L211/21/09 13:02663
4-Chloroaniline ND ug/kg 1 12/03/09 22:43 106-47-811/21/09 13:02168
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 22:43 111-91-1 L211/21/09 13:02168
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 22:43 111-44-4 L211/21/09 13:02168
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 22:43 108-60-111/21/09 13:02168
2-Chloronaphthalene ND ug/kg 1 12/03/09 22:43 91-58-711/21/09 13:02168
2-Chlorophenol ND ug/kg 1 12/03/09 22:43 95-57-811/21/09 13:02168
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 22:43 7005-72-311/21/09 13:02168
Chrysene ND ug/kg 1 12/03/09 22:43 218-01-911/21/09 13:0232.7
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 22:43 53-70-311/21/09 13:0232.7
Dibenzofuran ND ug/kg 1 12/03/09 22:43 132-64-911/21/09 13:02168
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 22:43 95-50-111/21/09 13:02168
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 22:43 541-73-111/21/09 13:02168
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 22:43 106-46-711/21/09 13:02168
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 22:43 91-94-111/21/09 13:02663
2,4-Dichlorophenol ND ug/kg 1 12/03/09 22:43 120-83-211/21/09 13:02168
Diethylphthalate ND ug/kg 1 12/03/09 22:43 84-66-211/21/09 13:02168
2,4-Dimethylphenol ND ug/kg 1 12/03/09 22:43 105-67-9 L211/21/09 13:02168
Dimethylphthalate ND ug/kg 1 12/03/09 22:43 131-11-311/21/09 13:02168
Di-n-butylphthalate ND ug/kg 1 12/03/09 22:43 84-74-211/21/09 13:02168
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 22:43 534-52-111/21/09 13:02663
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 66 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 0.5'Lab ID:9257863016 Collected:11/17/09 13:36 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 22:43 51-28-511/21/09 13:02663
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 22:43 121-14-211/21/09 13:02168
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 22:43 606-20-211/21/09 13:02168
Di-n-octylphthalate ND ug/kg 1 12/03/09 22:43 117-84-011/21/09 13:02168
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 22:43 122-66-711/21/09 13:02168
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 22:43 117-81-711/21/09 13:02168
Fluoranthene ND ug/kg 1 12/03/09 22:43 206-44-011/21/09 13:0232.7
Fluorene ND ug/kg 1 12/03/09 22:43 86-73-711/21/09 13:0232.7
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 22:43 87-68-311/21/09 13:02168
Hexachlorobenzene ND ug/kg 1 12/03/09 22:43 118-74-111/21/09 13:02168
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 22:43 77-47-411/21/09 13:02663
Hexachloroethane ND ug/kg 1 12/03/09 22:43 67-72-1 L211/21/09 13:02168
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 22:43 193-39-511/21/09 13:0232.7
Isophorone ND ug/kg 1 12/03/09 22:43 78-59-1 L211/21/09 13:02168
1-Methylnaphthalene ND ug/kg 1 12/03/09 22:43 90-12-011/21/09 13:0232.7
2-Methylnaphthalene ND ug/kg 1 12/03/09 22:43 91-57-611/21/09 13:0232.7
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 22:43 95-48-7 L211/21/09 13:02168
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 22:4311/21/09 13:02168
Naphthalene ND ug/kg 1 12/03/09 22:43 91-20-311/21/09 13:0232.7
2-Nitroaniline ND ug/kg 1 12/03/09 22:43 88-74-411/21/09 13:02168
3-Nitroaniline ND ug/kg 1 12/03/09 22:43 99-09-2 L211/21/09 13:02168
4-Nitroaniline ND ug/kg 1 12/03/09 22:43 100-01-611/21/09 13:02168
Nitrobenzene ND ug/kg 1 12/03/09 22:43 98-95-3 L211/21/09 13:02168
2-Nitrophenol ND ug/kg 1 12/03/09 22:43 88-75-511/21/09 13:02168
4-Nitrophenol ND ug/kg 1 12/03/09 22:43 100-02-711/21/09 13:02168
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 22:43 62-75-9 L211/21/09 13:02168
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 22:43 621-64-7 L211/21/09 13:02168
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 22:43 86-30-611/21/09 13:02168
Pentachlorophenol ND ug/kg 1 12/03/09 22:43 87-86-511/21/09 13:02663
Phenanthrene ND ug/kg 1 12/03/09 22:43 85-01-811/21/09 13:0232.7
Phenol ND ug/kg 1 12/03/09 22:43 108-95-2 IS,L211/21/09 13:02168
Pyrene ND ug/kg 1 12/03/09 22:43 129-00-011/21/09 13:0232.7
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 22:43 120-82-111/21/09 13:02168
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 22:43 95-95-411/21/09 13:02168
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 22:43 88-06-211/21/09 13:02168
Nitrobenzene-d5 (S)56 %1 12/03/09 22:43 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)71 %1 12/03/09 22:43 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)76 %1 12/03/09 22:43 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)43 %1 12/03/09 22:43 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)45 %1 12/03/09 22:43 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)68 %1 12/03/09 22:43 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/30/09 16:13 67-64-178.0
Benzene 12.3 ug/kg 1 11/30/09 16:13 71-43-23.9
Bromobenzene ND ug/kg 1 11/30/09 16:13 108-86-13.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 67 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 0.5'Lab ID:9257863016 Collected:11/17/09 13:36 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/30/09 16:13 74-97-53.9
Bromodichloromethane ND ug/kg 1 11/30/09 16:13 75-27-43.9
Bromoform ND ug/kg 1 11/30/09 16:13 75-25-23.9
Bromomethane ND ug/kg 1 11/30/09 16:13 74-83-97.8
2-Butanone (MEK)ND ug/kg 1 11/30/09 16:13 78-93-378.0
n-Butylbenzene ND ug/kg 1 11/30/09 16:13 104-51-83.9
sec-Butylbenzene ND ug/kg 1 11/30/09 16:13 135-98-83.9
tert-Butylbenzene ND ug/kg 1 11/30/09 16:13 98-06-63.9
Carbon tetrachloride ND ug/kg 1 11/30/09 16:13 56-23-53.9
Chlorobenzene 221 ug/kg 1 11/30/09 16:13 108-90-7 E3.9
Chloroethane ND ug/kg 1 11/30/09 16:13 75-00-37.8
Chloroform ND ug/kg 1 11/30/09 16:13 67-66-33.9
Chloromethane ND ug/kg 1 11/30/09 16:13 74-87-37.8
2-Chlorotoluene 15.1 ug/kg 1 11/30/09 16:13 95-49-83.9
4-Chlorotoluene ND ug/kg 1 11/30/09 16:13 106-43-43.9
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/30/09 16:13 96-12-83.9
Dibromochloromethane ND ug/kg 1 11/30/09 16:13 124-48-13.9
1,2-Dibromoethane (EDB)ND ug/kg 1 11/30/09 16:13 106-93-43.9
Dibromomethane ND ug/kg 1 11/30/09 16:13 74-95-33.9
1,2-Dichlorobenzene ND ug/kg 1 11/30/09 16:13 95-50-13.9
1,3-Dichlorobenzene ND ug/kg 1 11/30/09 16:13 541-73-13.9
1,4-Dichlorobenzene ND ug/kg 1 11/30/09 16:13 106-46-73.9
Dichlorodifluoromethane ND ug/kg 1 11/30/09 16:13 75-71-87.8
1,1-Dichloroethane ND ug/kg 1 11/30/09 16:13 75-34-33.9
1,2-Dichloroethane ND ug/kg 1 11/30/09 16:13 107-06-23.9
1,1-Dichloroethene ND ug/kg 1 11/30/09 16:13 75-35-43.9
cis-1,2-Dichloroethene ND ug/kg 1 11/30/09 16:13 156-59-23.9
trans-1,2-Dichloroethene ND ug/kg 1 11/30/09 16:13 156-60-53.9
1,2-Dichloropropane ND ug/kg 1 11/30/09 16:13 78-87-53.9
1,3-Dichloropropane ND ug/kg 1 11/30/09 16:13 142-28-93.9
2,2-Dichloropropane ND ug/kg 1 11/30/09 16:13 594-20-73.9
1,1-Dichloropropene ND ug/kg 1 11/30/09 16:13 563-58-63.9
cis-1,3-Dichloropropene ND ug/kg 1 11/30/09 16:13 10061-01-53.9
trans-1,3-Dichloropropene ND ug/kg 1 11/30/09 16:13 10061-02-63.9
Diisopropyl ether ND ug/kg 1 11/30/09 16:13 108-20-33.9
Ethylbenzene ND ug/kg 1 11/30/09 16:13 100-41-43.9
Hexachloro-1,3-butadiene ND ug/kg 1 11/30/09 16:13 87-68-33.9
2-Hexanone ND ug/kg 1 11/30/09 16:13 591-78-639.0
Isopropylbenzene (Cumene)ND ug/kg 1 11/30/09 16:13 98-82-83.9
p-Isopropyltoluene ND ug/kg 1 11/30/09 16:13 99-87-63.9
Methylene Chloride ND ug/kg 1 11/30/09 16:13 75-09-215.6
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/30/09 16:13 108-10-139.0
Methyl-tert-butyl ether ND ug/kg 1 11/30/09 16:13 1634-04-43.9
Naphthalene ND ug/kg 1 11/30/09 16:13 91-20-33.9
n-Propylbenzene ND ug/kg 1 11/30/09 16:13 103-65-13.9
Styrene ND ug/kg 1 11/30/09 16:13 100-42-53.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 68 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 0.5'Lab ID:9257863016 Collected:11/17/09 13:36 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/30/09 16:13 630-20-63.9
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/30/09 16:13 79-34-53.9
Tetrachloroethene ND ug/kg 1 11/30/09 16:13 127-18-43.9
Toluene ND ug/kg 1 11/30/09 16:13 108-88-33.9
1,2,3-Trichlorobenzene ND ug/kg 1 11/30/09 16:13 87-61-63.9
1,2,4-Trichlorobenzene ND ug/kg 1 11/30/09 16:13 120-82-13.9
1,1,1-Trichloroethane ND ug/kg 1 11/30/09 16:13 71-55-63.9
1,1,2-Trichloroethane ND ug/kg 1 11/30/09 16:13 79-00-53.9
Trichloroethene ND ug/kg 1 11/30/09 16:13 79-01-63.9
Trichlorofluoromethane ND ug/kg 1 11/30/09 16:13 75-69-43.9
1,2,3-Trichloropropane ND ug/kg 1 11/30/09 16:13 96-18-43.9
1,2,4-Trimethylbenzene ND ug/kg 1 11/30/09 16:13 95-63-63.9
1,3,5-Trimethylbenzene ND ug/kg 1 11/30/09 16:13 108-67-83.9
Vinyl acetate ND ug/kg 1 11/30/09 16:13 108-05-439.0
Vinyl chloride ND ug/kg 1 11/30/09 16:13 75-01-47.8
Xylene (Total)ND ug/kg 1 11/30/09 16:13 1330-20-77.8
m&p-Xylene ND ug/kg 1 11/30/09 16:13 1330-20-77.8
o-Xylene ND ug/kg 1 11/30/09 16:13 95-47-63.9
Dibromofluoromethane (S)99 %1 11/30/09 16:13 1868-53-779-116
Toluene-d8 (S)99 %1 11/30/09 16:13 2037-26-588-110
4-Bromofluorobenzene (S)99 %1 11/30/09 16:13 460-00-474-115
1,2-Dichloroethane-d4 (S)79 %1 11/30/09 16:13 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 12.6 %1 11/23/09 14:270.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 69 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 3'Lab ID:9257863017 Collected:11/17/09 13:43 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Arsenic ND mg/L 1 12/09/09 18:44 7440-38-212/09/09 12:300.025
Barium 0.15 mg/L 1 12/09/09 18:44 7440-39-312/09/09 12:300.025
Cadmium ND mg/L 1 12/09/09 18:44 7440-43-912/09/09 12:300.0050
Chromium ND mg/L 1 12/09/09 18:44 7440-47-312/09/09 12:300.025
Lead ND mg/L 1 12/09/09 18:44 7439-92-112/09/09 12:300.025
Selenium ND mg/L 1 12/09/09 18:44 7782-49-212/09/09 12:300.050
Silver ND mg/L 1 12/09/09 18:44 7440-22-412/09/09 12:300.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/08/09 17:00
Mercury ND ug/L 1 12/09/09 15:53 7439-97-612/09/09 11:300.20
8270 MSSV Full List Microwave Analytical Method: EPA 8270
Acenaphthene ND ug/kg 1 12/03/09 23:12 83-32-911/21/09 13:0233.0
Acenaphthylene ND ug/kg 1 12/03/09 23:12 208-96-811/21/09 13:0233.0
Anthracene ND ug/kg 1 12/03/09 23:12 120-12-711/21/09 13:0233.0
Benzo(a)anthracene ND ug/kg 1 12/03/09 23:12 56-55-311/21/09 13:0233.0
Benzo(a)pyrene ND ug/kg 1 12/03/09 23:12 50-32-811/21/09 13:0233.0
Benzo(b)fluoranthene ND ug/kg 1 12/03/09 23:12 205-99-211/21/09 13:0233.0
Benzo(g,h,i)perylene ND ug/kg 1 12/03/09 23:12 191-24-211/21/09 13:0233.0
Benzo(k)fluoranthene ND ug/kg 1 12/03/09 23:12 207-08-911/21/09 13:0233.0
4-Bromophenylphenyl ether ND ug/kg 1 12/03/09 23:12 101-55-311/21/09 13:02170
Butylbenzylphthalate ND ug/kg 1 12/03/09 23:12 85-68-711/21/09 13:02170
4-Chloro-3-methylphenol ND ug/kg 1 12/03/09 23:12 59-50-7 L211/21/09 13:02670
4-Chloroaniline ND ug/kg 1 12/03/09 23:12 106-47-811/21/09 13:02170
bis(2-Chloroethoxy)methane ND ug/kg 1 12/03/09 23:12 111-91-1 L211/21/09 13:02170
bis(2-Chloroethyl) ether ND ug/kg 1 12/03/09 23:12 111-44-4 L211/21/09 13:02170
bis(2-Chloroisopropyl) ether ND ug/kg 1 12/03/09 23:12 108-60-111/21/09 13:02170
2-Chloronaphthalene ND ug/kg 1 12/03/09 23:12 91-58-711/21/09 13:02170
2-Chlorophenol ND ug/kg 1 12/03/09 23:12 95-57-811/21/09 13:02170
4-Chlorophenylphenyl ether ND ug/kg 1 12/03/09 23:12 7005-72-311/21/09 13:02170
Chrysene ND ug/kg 1 12/03/09 23:12 218-01-911/21/09 13:0233.0
Dibenz(a,h)anthracene ND ug/kg 1 12/03/09 23:12 53-70-311/21/09 13:0233.0
Dibenzofuran ND ug/kg 1 12/03/09 23:12 132-64-911/21/09 13:02170
1,2-Dichlorobenzene ND ug/kg 1 12/03/09 23:12 95-50-111/21/09 13:02170
1,3-Dichlorobenzene ND ug/kg 1 12/03/09 23:12 541-73-111/21/09 13:02170
1,4-Dichlorobenzene ND ug/kg 1 12/03/09 23:12 106-46-711/21/09 13:02170
3,3'-Dichlorobenzidine ND ug/kg 1 12/03/09 23:12 91-94-111/21/09 13:02670
2,4-Dichlorophenol ND ug/kg 1 12/03/09 23:12 120-83-211/21/09 13:02170
Diethylphthalate ND ug/kg 1 12/03/09 23:12 84-66-211/21/09 13:02170
2,4-Dimethylphenol ND ug/kg 1 12/03/09 23:12 105-67-9 L211/21/09 13:02170
Dimethylphthalate ND ug/kg 1 12/03/09 23:12 131-11-311/21/09 13:02170
Di-n-butylphthalate ND ug/kg 1 12/03/09 23:12 84-74-211/21/09 13:02170
4,6-Dinitro-2-methylphenol ND ug/kg 1 12/03/09 23:12 534-52-111/21/09 13:02670
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 70 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 3'Lab ID:9257863017 Collected:11/17/09 13:43 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8270 MSSV Full List Microwave Analytical Method: EPA 8270
2,4-Dinitrophenol ND ug/kg 1 12/03/09 23:12 51-28-511/21/09 13:02670
2,4-Dinitrotoluene ND ug/kg 1 12/03/09 23:12 121-14-211/21/09 13:02170
2,6-Dinitrotoluene ND ug/kg 1 12/03/09 23:12 606-20-211/21/09 13:02170
Di-n-octylphthalate ND ug/kg 1 12/03/09 23:12 117-84-011/21/09 13:02170
1,2-Diphenylhydrazine ND ug/kg 1 12/03/09 23:12 122-66-711/21/09 13:02170
bis(2-Ethylhexyl)phthalate ND ug/kg 1 12/03/09 23:12 117-81-711/21/09 13:02170
Fluoranthene ND ug/kg 1 12/03/09 23:12 206-44-011/21/09 13:0233.0
Fluorene ND ug/kg 1 12/03/09 23:12 86-73-711/21/09 13:0233.0
Hexachloro-1,3-butadiene ND ug/kg 1 12/03/09 23:12 87-68-311/21/09 13:02170
Hexachlorobenzene ND ug/kg 1 12/03/09 23:12 118-74-111/21/09 13:02170
Hexachlorocyclopentadiene ND ug/kg 1 12/03/09 23:12 77-47-411/21/09 13:02670
Hexachloroethane ND ug/kg 1 12/03/09 23:12 67-72-1 L211/21/09 13:02170
Indeno(1,2,3-cd)pyrene ND ug/kg 1 12/03/09 23:12 193-39-511/21/09 13:0233.0
Isophorone ND ug/kg 1 12/03/09 23:12 78-59-1 L211/21/09 13:02170
1-Methylnaphthalene ND ug/kg 1 12/03/09 23:12 90-12-011/21/09 13:0233.0
2-Methylnaphthalene ND ug/kg 1 12/03/09 23:12 91-57-611/21/09 13:0233.0
2-Methylphenol(o-Cresol)ND ug/kg 1 12/03/09 23:12 95-48-7 L211/21/09 13:02170
3&4-Methylphenol(m&p Cresol)ND ug/kg 1 12/03/09 23:1211/21/09 13:02170
Naphthalene ND ug/kg 1 12/03/09 23:12 91-20-311/21/09 13:0233.0
2-Nitroaniline ND ug/kg 1 12/03/09 23:12 88-74-411/21/09 13:02170
3-Nitroaniline ND ug/kg 1 12/03/09 23:12 99-09-2 L211/21/09 13:02170
4-Nitroaniline ND ug/kg 1 12/03/09 23:12 100-01-611/21/09 13:02170
Nitrobenzene ND ug/kg 1 12/03/09 23:12 98-95-3 L211/21/09 13:02170
2-Nitrophenol ND ug/kg 1 12/03/09 23:12 88-75-511/21/09 13:02170
4-Nitrophenol ND ug/kg 1 12/03/09 23:12 100-02-711/21/09 13:02170
N-Nitrosodimethylamine ND ug/kg 1 12/03/09 23:12 62-75-9 L211/21/09 13:02170
N-Nitroso-di-n-propylamine ND ug/kg 1 12/03/09 23:12 621-64-7 L211/21/09 13:02170
N-Nitrosodiphenylamine ND ug/kg 1 12/03/09 23:12 86-30-611/21/09 13:02170
Pentachlorophenol ND ug/kg 1 12/03/09 23:12 87-86-511/21/09 13:02670
Phenanthrene ND ug/kg 1 12/03/09 23:12 85-01-811/21/09 13:0233.0
Phenol ND ug/kg 1 12/03/09 23:12 108-95-2 L211/21/09 13:02170
Pyrene ND ug/kg 1 12/03/09 23:12 129-00-011/21/09 13:0233.0
1,2,4-Trichlorobenzene ND ug/kg 1 12/03/09 23:12 120-82-111/21/09 13:02170
2,4,5-Trichlorophenol ND ug/kg 1 12/03/09 23:12 95-95-411/21/09 13:02170
2,4,6-Trichlorophenol ND ug/kg 1 12/03/09 23:12 88-06-211/21/09 13:02170
Nitrobenzene-d5 (S)50 %1 12/03/09 23:12 4165-60-011/21/09 13:0210-110
2-Fluorobiphenyl (S)63 %1 12/03/09 23:12 321-60-811/21/09 13:0218-110
Terphenyl-d14 (S)83 %1 12/03/09 23:12 1718-51-011/21/09 13:0210-123
Phenol-d6 (S)41 %1 12/03/09 23:12 13127-88-311/21/09 13:0210-110
2-Fluorophenol (S)47 %1 12/03/09 23:12 367-12-411/21/09 13:0218-110
2,4,6-Tribromophenol (S)63 %1 12/03/09 23:12 118-79-611/21/09 13:0210-110
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND ug/kg 1 11/30/09 16:31 67-64-175.9
Benzene 20.4 ug/kg 1 11/30/09 16:31 71-43-23.8
Bromobenzene ND ug/kg 1 11/30/09 16:31 108-86-13.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 71 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 3'Lab ID:9257863017 Collected:11/17/09 13:43 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Bromochloromethane ND ug/kg 1 11/30/09 16:31 74-97-53.8
Bromodichloromethane ND ug/kg 1 11/30/09 16:31 75-27-43.8
Bromoform ND ug/kg 1 11/30/09 16:31 75-25-23.8
Bromomethane ND ug/kg 1 11/30/09 16:31 74-83-97.6
2-Butanone (MEK)ND ug/kg 1 11/30/09 16:31 78-93-375.9
n-Butylbenzene ND ug/kg 1 11/30/09 16:31 104-51-83.8
sec-Butylbenzene ND ug/kg 1 11/30/09 16:31 135-98-83.8
tert-Butylbenzene ND ug/kg 1 11/30/09 16:31 98-06-63.8
Carbon tetrachloride ND ug/kg 1 11/30/09 16:31 56-23-53.8
Chlorobenzene 59.8 ug/kg 1 11/30/09 16:31 108-90-73.8
Chloroethane ND ug/kg 1 11/30/09 16:31 75-00-37.6
Chloroform ND ug/kg 1 11/30/09 16:31 67-66-33.8
Chloromethane ND ug/kg 1 11/30/09 16:31 74-87-37.6
2-Chlorotoluene ND ug/kg 1 11/30/09 16:31 95-49-83.8
4-Chlorotoluene ND ug/kg 1 11/30/09 16:31 106-43-43.8
1,2-Dibromo-3-chloropropane ND ug/kg 1 11/30/09 16:31 96-12-83.8
Dibromochloromethane ND ug/kg 1 11/30/09 16:31 124-48-13.8
1,2-Dibromoethane (EDB)ND ug/kg 1 11/30/09 16:31 106-93-43.8
Dibromomethane ND ug/kg 1 11/30/09 16:31 74-95-33.8
1,2-Dichlorobenzene ND ug/kg 1 11/30/09 16:31 95-50-13.8
1,3-Dichlorobenzene ND ug/kg 1 11/30/09 16:31 541-73-13.8
1,4-Dichlorobenzene ND ug/kg 1 11/30/09 16:31 106-46-73.8
Dichlorodifluoromethane ND ug/kg 1 11/30/09 16:31 75-71-87.6
1,1-Dichloroethane ND ug/kg 1 11/30/09 16:31 75-34-33.8
1,2-Dichloroethane ND ug/kg 1 11/30/09 16:31 107-06-23.8
1,1-Dichloroethene ND ug/kg 1 11/30/09 16:31 75-35-43.8
cis-1,2-Dichloroethene ND ug/kg 1 11/30/09 16:31 156-59-23.8
trans-1,2-Dichloroethene ND ug/kg 1 11/30/09 16:31 156-60-53.8
1,2-Dichloropropane ND ug/kg 1 11/30/09 16:31 78-87-53.8
1,3-Dichloropropane ND ug/kg 1 11/30/09 16:31 142-28-93.8
2,2-Dichloropropane ND ug/kg 1 11/30/09 16:31 594-20-73.8
1,1-Dichloropropene ND ug/kg 1 11/30/09 16:31 563-58-63.8
cis-1,3-Dichloropropene ND ug/kg 1 11/30/09 16:31 10061-01-53.8
trans-1,3-Dichloropropene ND ug/kg 1 11/30/09 16:31 10061-02-63.8
Diisopropyl ether ND ug/kg 1 11/30/09 16:31 108-20-33.8
Ethylbenzene ND ug/kg 1 11/30/09 16:31 100-41-43.8
Hexachloro-1,3-butadiene ND ug/kg 1 11/30/09 16:31 87-68-33.8
2-Hexanone ND ug/kg 1 11/30/09 16:31 591-78-637.9
Isopropylbenzene (Cumene)ND ug/kg 1 11/30/09 16:31 98-82-83.8
p-Isopropyltoluene ND ug/kg 1 11/30/09 16:31 99-87-63.8
Methylene Chloride ND ug/kg 1 11/30/09 16:31 75-09-215.2
4-Methyl-2-pentanone (MIBK)ND ug/kg 1 11/30/09 16:31 108-10-137.9
Methyl-tert-butyl ether ND ug/kg 1 11/30/09 16:31 1634-04-43.8
Naphthalene ND ug/kg 1 11/30/09 16:31 91-20-33.8
n-Propylbenzene ND ug/kg 1 11/30/09 16:31 103-65-13.8
Styrene ND ug/kg 1 11/30/09 16:31 100-42-53.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 72 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-9 3'Lab ID:9257863017 Collected:11/17/09 13:43 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
1,1,1,2-Tetrachloroethane ND ug/kg 1 11/30/09 16:31 630-20-63.8
1,1,2,2-Tetrachloroethane ND ug/kg 1 11/30/09 16:31 79-34-53.8
Tetrachloroethene ND ug/kg 1 11/30/09 16:31 127-18-43.8
Toluene ND ug/kg 1 11/30/09 16:31 108-88-33.8
1,2,3-Trichlorobenzene ND ug/kg 1 11/30/09 16:31 87-61-63.8
1,2,4-Trichlorobenzene ND ug/kg 1 11/30/09 16:31 120-82-13.8
1,1,1-Trichloroethane ND ug/kg 1 11/30/09 16:31 71-55-63.8
1,1,2-Trichloroethane ND ug/kg 1 11/30/09 16:31 79-00-53.8
Trichloroethene ND ug/kg 1 11/30/09 16:31 79-01-63.8
Trichlorofluoromethane ND ug/kg 1 11/30/09 16:31 75-69-43.8
1,2,3-Trichloropropane ND ug/kg 1 11/30/09 16:31 96-18-43.8
1,2,4-Trimethylbenzene ND ug/kg 1 11/30/09 16:31 95-63-63.8
1,3,5-Trimethylbenzene ND ug/kg 1 11/30/09 16:31 108-67-83.8
Vinyl acetate ND ug/kg 1 11/30/09 16:31 108-05-437.9
Vinyl chloride ND ug/kg 1 11/30/09 16:31 75-01-47.6
Xylene (Total)ND ug/kg 1 11/30/09 16:31 1330-20-77.6
m&p-Xylene ND ug/kg 1 11/30/09 16:31 1330-20-77.6
o-Xylene ND ug/kg 1 11/30/09 16:31 95-47-63.8
Dibromofluoromethane (S)99 %1 11/30/09 16:31 1868-53-779-116
Toluene-d8 (S)99 %1 11/30/09 16:31 2037-26-588-110
4-Bromofluorobenzene (S)105 %1 11/30/09 16:31 460-00-474-115
1,2-Dichloroethane-d4 (S)80 %1 11/30/09 16:31 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.1 %1 11/23/09 14:270.10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 73 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Sample:GP-10 3'Lab ID:9257863018 Collected:11/17/09 00:00 Received:11/18/09 17:19 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 12/02/09 16:35
Arsenic ND mg/L 1 12/04/09 02:46 7440-38-212/03/09 13:500.025
Barium 0.21 mg/L 1 12/04/09 02:46 7440-39-312/03/09 13:500.025
Cadmium ND mg/L 1 12/04/09 02:46 7440-43-912/03/09 13:500.0050
Chromium ND mg/L 1 12/04/09 02:46 7440-47-312/03/09 13:500.025
Lead 0.034 mg/L 1 12/04/09 02:46 7439-92-112/03/09 13:500.025
Selenium ND mg/L 1 12/04/09 02:46 7782-49-212/03/09 13:500.050
Silver ND mg/L 1 12/04/09 02:46 7440-22-412/03/09 13:500.025
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 12/02/09 16:35
Mercury ND ug/L 1 12/04/09 12:59 7439-97-612/03/09 15:100.20
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 19.7 %1 11/23/09 14:270.10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 74 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/5474
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:9257863018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:374303
Associated Lab Samples:9257863018
Matrix:Water
Analyzed
Arsenic mg/L ND 0.025 12/04/09 02:30
Barium mg/L ND 0.025 12/04/09 02:30
Cadmium mg/L ND 0.0050 12/04/09 02:30
Chromium mg/L ND 0.025 12/04/09 02:30
Lead mg/L ND 0.025 12/04/09 02:30
Selenium mg/L ND 0.050 12/04/09 02:30
Silver mg/L ND 0.025 12/04/09 02:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
374304LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.62.5 102 80-120
Barium mg/L 2.32.5 91 80-120
Cadmium mg/L 2.22.5 90 80-120
Chromium mg/L 2.32.5 92 80-120
Lead mg/L 2.22.5 87 80-120
Selenium mg/L 2.62.5 105 80-120
Silver mg/L 1.21.2 99 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
374306MATRIX SPIKE SAMPLE:
MSSpike
Result
9258330001
Arsenic mg/L 2.52.5 99 75-125ND
Barium mg/L 2.42.5 87 75-125232 ug/L
Cadmium mg/L 2.22.5 86 75-125ND
Chromium mg/L 2.22.5 90 75-125ND
Lead mg/L 2.12.5 83 75-125ND
Selenium mg/L 2.52.5 100 75-125ND
Silver mg/L 1.21.2 95 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
9257760001
374305SAMPLE DUPLICATE:
Arsenic mg/L NDND
Barium mg/L .015JND
Cadmium mg/L NDND
Chromium mg/L NDND
Lead mg/L NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 75 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Dup
Result QualifiersRPDResult
9257760001
374305SAMPLE DUPLICATE:
Selenium mg/L NDND
Silver mg/L .0041JND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 76 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/5507
EPA 3010
EPA 6010
6010 MET TCLP
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005, 9257863006, 9257863007, 9257863008,
9257863009, 9257863010, 9257863011, 9257863012, 9257863013, 9257863014, 9257863015, 9257863016,
9257863017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:376658
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005, 9257863006, 9257863007, 9257863008,
9257863009, 9257863010, 9257863011, 9257863012, 9257863013, 9257863014, 9257863015, 9257863016,
9257863017
Matrix:Water
Analyzed
Arsenic mg/L ND 0.025 12/09/09 17:14
Barium mg/L ND 0.025 12/09/09 17:14
Cadmium mg/L ND 0.0050 12/09/09 17:14
Chromium mg/L ND 0.025 12/09/09 17:14
Lead mg/L ND 0.025 12/09/09 17:14
Selenium mg/L ND 0.050 12/09/09 17:14
Silver mg/L ND 0.025 12/09/09 17:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
376659LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 2.62.5 105 80-120
Barium mg/L 2.22.5 88 80-120
Cadmium mg/L 2.32.5 94 80-120
Chromium mg/L 2.42.5 95 80-120
Lead mg/L 2.22.5 89 80-120
Selenium mg/L 2.62.5 104 80-120
Silver mg/L 1.21.2 96 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
376660MATRIX SPIKE SAMPLE:
MSSpike
Result
9257863001
Arsenic mg/L 2.42.5 96 75-125ND
Barium mg/L 2.22.5 80 75-1250.16
Cadmium mg/L 2.22.5 86 75-125ND
Chromium mg/L 2.22.5 89 75-125ND
Lead mg/L 2.02.5 82 75-125ND
Selenium mg/L 2.42.5 95 75-125ND
Silver mg/L 1.11.2 88 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
9257863002
376661SAMPLE DUPLICATE:
Arsenic mg/L NDND
Barium mg/L 0.072 30.074
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 77 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Dup
Result QualifiersRPDResult
9257863002
376661SAMPLE DUPLICATE:
Cadmium mg/L NDND
Chromium mg/L NDND
Lead mg/L NDND
Selenium mg/L NDND
Silver mg/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 78 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/2539
EPA 7470
EPA 7470
7470 Mercury TCLP
Associated Lab Samples:9257863018
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:374290
Associated Lab Samples:9257863018
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 12/04/09 12:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
374291LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.62.5 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
374299MATRIX SPIKE SAMPLE:
MSSpike
Result
9258330001
Mercury ug/L 1.9 M02.5 70 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
9257863018
374293SAMPLE DUPLICATE:
Mercury ug/L .16JND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 79 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MERP/2548
EPA 7470
EPA 7470
7470 Mercury TCLP
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005, 9257863006, 9257863007, 9257863008,
9257863009, 9257863010, 9257863011, 9257863012, 9257863013, 9257863014, 9257863015, 9257863016,
9257863017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:376638
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005, 9257863006, 9257863007, 9257863008,
9257863009, 9257863010, 9257863011, 9257863012, 9257863013, 9257863014, 9257863015, 9257863016,
9257863017
Matrix:Water
Analyzed
Mercury ug/L ND 0.20 12/09/09 14:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
376639LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.12.5 84 80-120
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
376640MATRIX SPIKE SAMPLE:
MSSpike
Result
9257863001
Mercury ug/L 1.7 M02.5 66 75-125ND
Parameter Units
Dup
Result QualifiersRPDResult
9257863002
376641SAMPLE DUPLICATE:
Mercury ug/L NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 80 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSSV/1388
EPA 8270
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005, 9257863006, 9257863007, 9257863008,
9257863009, 9257863010, 9257863011, 9257863012, 9257863013, 9257863014, 9257863015, 9257863016,
9257863017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:21287
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005, 9257863006, 9257863007, 9257863008,
9257863009, 9257863010, 9257863011, 9257863012, 9257863013, 9257863014, 9257863015, 9257863016,
9257863017
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene ug/kg ND 167 12/03/09 13:20
1,2-Dichlorobenzene ug/kg ND 167 12/03/09 13:20
1,2-Diphenylhydrazine ug/kg ND 167 12/03/09 13:20
1,3-Dichlorobenzene ug/kg ND 167 12/03/09 13:20
1,4-Dichlorobenzene ug/kg ND 167 12/03/09 13:20
1-Methylnaphthalene ug/kg ND 32.5 12/03/09 13:20
2,4,5-Trichlorophenol ug/kg ND 167 12/03/09 13:20
2,4,6-Trichlorophenol ug/kg ND 167 12/03/09 13:20
2,4-Dichlorophenol ug/kg ND 167 12/03/09 13:20
2,4-Dimethylphenol ug/kg ND 167 12/03/09 13:20
2,4-Dinitrophenol ug/kg ND 659 12/03/09 13:20
2,4-Dinitrotoluene ug/kg ND 167 12/03/09 13:20
2,6-Dinitrotoluene ug/kg ND 167 12/03/09 13:20
2-Chloronaphthalene ug/kg ND 167 12/03/09 13:20
2-Chlorophenol ug/kg ND 167 12/03/09 13:20
2-Methylnaphthalene ug/kg ND 32.5 12/03/09 13:20
2-Methylphenol(o-Cresol)ug/kg ND 167 12/03/09 13:20
2-Nitroaniline ug/kg ND 167 12/03/09 13:20
2-Nitrophenol ug/kg ND 167 12/03/09 13:20
3&4-Methylphenol(m&p Cresol)ug/kg ND 167 12/03/09 13:20
3,3'-Dichlorobenzidine ug/kg ND 659 12/03/09 13:20
3-Nitroaniline ug/kg ND 167 12/03/09 13:20
4,6-Dinitro-2-methylphenol ug/kg ND 659 12/03/09 13:20
4-Bromophenylphenyl ether ug/kg ND 167 12/03/09 13:20
4-Chloro-3-methylphenol ug/kg ND 659 12/03/09 13:20
4-Chloroaniline ug/kg ND 167 12/03/09 13:20
4-Chlorophenylphenyl ether ug/kg ND 167 12/03/09 13:20
4-Nitroaniline ug/kg ND 167 12/03/09 13:20
4-Nitrophenol ug/kg ND 167 12/03/09 13:20
Acenaphthene ug/kg ND 32.5 12/03/09 13:20
Acenaphthylene ug/kg ND 32.5 12/03/09 13:20
Anthracene ug/kg ND 32.5 12/03/09 13:20
Benzo(a)anthracene ug/kg ND 32.5 12/03/09 13:20
Benzo(a)pyrene ug/kg ND 32.5 12/03/09 13:20
Benzo(b)fluoranthene ug/kg ND 32.5 12/03/09 13:20
Benzo(g,h,i)perylene ug/kg ND 32.5 12/03/09 13:20
Benzo(k)fluoranthene ug/kg ND 32.5 12/03/09 13:20
bis(2-Chloroethoxy)methane ug/kg ND 167 12/03/09 13:20
bis(2-Chloroethyl) ether ug/kg ND 167 12/03/09 13:20
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 81 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:21287
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005, 9257863006, 9257863007, 9257863008,
9257863009, 9257863010, 9257863011, 9257863012, 9257863013, 9257863014, 9257863015, 9257863016,
9257863017
Matrix:Solid
Analyzed
bis(2-Chloroisopropyl) ether ug/kg ND 167 12/03/09 13:20
bis(2-Ethylhexyl)phthalate ug/kg ND 167 12/03/09 13:20
Butylbenzylphthalate ug/kg ND 167 12/03/09 13:20
Chrysene ug/kg ND 32.5 12/03/09 13:20
Di-n-butylphthalate ug/kg ND 167 12/03/09 13:20
Di-n-octylphthalate ug/kg ND 167 12/03/09 13:20
Dibenz(a,h)anthracene ug/kg ND 32.5 12/03/09 13:20
Dibenzofuran ug/kg ND 167 12/03/09 13:20
Diethylphthalate ug/kg ND 167 12/03/09 13:20
Dimethylphthalate ug/kg ND 167 12/03/09 13:20
Fluoranthene ug/kg ND 32.5 12/03/09 13:20
Fluorene ug/kg ND 32.5 12/03/09 13:20
Hexachloro-1,3-butadiene ug/kg ND 167 12/03/09 13:20
Hexachlorobenzene ug/kg ND 167 12/03/09 13:20
Hexachlorocyclopentadiene ug/kg ND 659 12/03/09 13:20
Hexachloroethane ug/kg ND 167 12/03/09 13:20
Indeno(1,2,3-cd)pyrene ug/kg ND 32.5 12/03/09 13:20
Isophorone ug/kg ND 167 12/03/09 13:20
N-Nitroso-di-n-propylamine ug/kg ND 167 12/03/09 13:20
N-Nitrosodimethylamine ug/kg ND 167 12/03/09 13:20
N-Nitrosodiphenylamine ug/kg ND 167 12/03/09 13:20
Naphthalene ug/kg ND 32.5 12/03/09 13:20
Nitrobenzene ug/kg ND 167 12/03/09 13:20
Pentachlorophenol ug/kg ND 659 12/03/09 13:20
Phenanthrene ug/kg ND 32.5 12/03/09 13:20
Phenol ug/kg ND 167 12/03/09 13:20
Pyrene ug/kg ND 32.5 12/03/09 13:20
2,4,6-Tribromophenol (S)%58 10-110 12/03/09 13:20
2-Fluorobiphenyl (S)%59 18-110 12/03/09 13:20
2-Fluorophenol (S)%45 18-110 12/03/09 13:20
Nitrobenzene-d5 (S)%48 10-110 12/03/09 13:20
Phenol-d6 (S)%43 10-110 12/03/09 13:20
Terphenyl-d14 (S)%68 10-123 12/03/09 13:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
21288LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10301660 62 55.2-104.2
1,2-Dichlorobenzene ug/kg 8471660 51 46.8-80.1
1,2-Diphenylhydrazine ug/kg 9391660 57
1,3-Dichlorobenzene ug/kg 8671660 52 46.4-80.6
1,4-Dichlorobenzene ug/kg 8561660 52 37.4-86.7
1-Methylnaphthalene ug/kg 10301660 62 20.7-121.7
2,4,5-Trichlorophenol ug/kg 12201660 73 58.1-101.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 82 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
21288LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/kg 12001660 73 46.2-106
2,4-Dichlorophenol ug/kg 10901660 65 47.1-102
2,4-Dimethylphenol ug/kg 900 L216605454.1-109.9
2,4-Dinitrophenol ug/kg 10801660 65 57.6-108
2,4-Dinitrotoluene ug/kg 14801660 89 62.7-99.2
2,6-Dinitrotoluene ug/kg 13201660 79 53.2-110.8
2-Chloronaphthalene ug/kg 9451660 57 49.8-101
2-Chlorophenol ug/kg 8581660 52 48.2-85.3
2-Methylnaphthalene ug/kg 9821660 59 20.9-121.3
2-Methylphenol(o-Cresol)ug/kg 855 L216605153.2-93.1
2-Nitroaniline ug/kg 11601660 70 64.2-102.8
2-Nitrophenol ug/kg 10001660 60 35-142.5
3&4-Methylphenol(m&p Cresol)ug/kg 9201660 55 50.1-87
3,3'-Dichlorobenzidine ug/kg 13501660 81 51.7-91.9
3-Nitroaniline ug/kg 1030 L216606264.9-102.5
4,6-Dinitro-2-methylphenol ug/kg 13801660 83 49.2-104.9
4-Bromophenylphenyl ether ug/kg 12901660 78 61-96.5
4-Chloro-3-methylphenol ug/kg 1010 L216606163.4-98.7
4-Chloroaniline ug/kg 10101660 61 54.8-90.6
4-Chlorophenylphenyl ether ug/kg 11901660 72 55.1-97.6
4-Nitroaniline ug/kg 14201660 85 48.6-95.1
4-Nitrophenol ug/kg 13401660 81 27.1-112
Acenaphthene ug/kg 10301660 62 22-124.1
Acenaphthylene ug/kg 10201660 62 22.7-127.8
Anthracene ug/kg 12901660 78 23.8-117
Benzo(a)anthracene ug/kg 13001660 78 25.7-125
Benzo(a)pyrene ug/kg 13801660 83 25.5-126.9
Benzo(b)fluoranthene ug/kg 13101660 79 24.9-132.8
Benzo(g,h,i)perylene ug/kg 13301660 80 28.1-134.9
Benzo(k)fluoranthene ug/kg 14601660 88 30.1-135.6
bis(2-Chloroethoxy)methane ug/kg 790 L216604851-93.2
bis(2-Chloroethyl) ether ug/kg 580 L216603550.3-86.8
bis(2-Chloroisopropyl) ether ug/kg 7731660 47 43.1-87.3
bis(2-Ethylhexyl)phthalate ug/kg 12401660 75 10-238.8
Butylbenzylphthalate ug/kg 12101660 73 55.5-116
Chrysene ug/kg 12701660 77 25.9-129.8
Di-n-butylphthalate ug/kg 12401660 75 63.2-102.6
Di-n-octylphthalate ug/kg 12601660 76 56.5-119.9
Dibenz(a,h)anthracene ug/kg 13301660 80 28.1-136
Dibenzofuran ug/kg 11001660 66 44-89.3
Diethylphthalate ug/kg 12601660 76 64.9-94.9
Dimethylphthalate ug/kg 12201660 73 55.3-94.5
Fluoranthene ug/kg 13401660 81 27.6-129.1
Fluorene ug/kg 12101660 73 22.1-134.4
Hexachloro-1,3-butadiene ug/kg 10501660 63 23.8-97.1
Hexachlorobenzene ug/kg 13001660 78 43.5-98.2
Hexachlorocyclopentadiene ug/kg 8371660 50 37.1-91.2
Hexachloroethane ug/kg 771 L216604650.9-110.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 83 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
21288LABORATORY CONTROL SAMPLE:
LCSSpike
Indeno(1,2,3-cd)pyrene ug/kg 13301660 80 27.4-134
Isophorone ug/kg 813 L216604954.7-91.2
N-Nitroso-di-n-propylamine ug/kg 846 L216605160.7-96.7
N-Nitrosodimethylamine ug/kg 467 L216602850.7-89.6
N-Nitrosodiphenylamine ug/kg 12101660 73 53.8-112.6
Naphthalene ug/kg 9571660 58 19.8-116.2
Nitrobenzene ug/kg 840 L216605154.6-87.7
Pentachlorophenol ug/kg 14201660 85 35.6-133.1
Phenanthrene ug/kg 12901660 78 27.7-128.9
Phenol ug/kg 723 L216604449.3-102.8
Pyrene ug/kg 13501660 81 27.7-128.9
2,4,6-Tribromophenol (S)%75 10-110
2-Fluorobiphenyl (S)%59 18-110
2-Fluorophenol (S)%45 18-110
Nitrobenzene-d5 (S)%49 10-110
Phenol-d6 (S)%43 10-110
Terphenyl-d14 (S)%82 10-123
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
21289MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9257863002
21290
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg M0,R116203555.2-10460 521630ND571972
1,2-Dichlorobenzene ug/kg M0,R116203046.8-80.48 471630ND486788
1,2-Diphenylhydrazine ug/kg R116202649641630ND417807
1,3-Dichlorobenzene ug/kg M0,R116203146.4-80.49 451630ND504795
1,4-Dichlorobenzene ug/kg M0,R116203237.4-86.49 431630ND524807
1-Methylnaphthalene ug/kg R116203220.7-12155 541630ND517900
2,4,5-Trichlorophenol ug/kg M0,R116203658.1-10170 641630ND5921150
2,4,6-Trichlorophenol ug/kg M0,R116203646.2-10668 611630ND5921110
2,4-Dichlorophenol ug/kg M0,R116203447.1-10260 561630ND552985
2,4-Dimethylphenol ug/kg M0,R116202454.1-10951 741630ND384832
2,4-Dinitrophenol ug/kg M016202557.6-108371630ND405J608J
2,4-Dinitrotoluene ug/kg M0,R116204562.7-99.73 491630ND7251190
2,6-Dinitrotoluene ug/kg M0,R116203953.2-11070 571630ND6381140
2-Chloronaphthalene ug/kg M0,R116203249.8-10158 591630ND515950
2-Chlorophenol ug/kg M0,R116202948.2-85.47 481630ND474775
2-Methylnaphthalene ug/kg R116203220.9-12155 531630ND523901
2-Methylphenol(o-Cresol)ug/kg M0,R116202353.2-93.44 621630ND380719
2-Nitroaniline ug/kg M0,R116203664.2-10263 541630ND5901020
2-Nitrophenol ug/kg M0,R116203135-142.555 571630ND495893
3&4-Methylphenol(m&pCresol)ug/kg M0,R116202650.1-8751 661630ND420839
3,3'-Dichlorobenzidine ug/kg M016203451.7-91.661630ND557J1080
3-Nitroaniline ug/kg M0,R116203164.9-10256 601630ND495918
4,6-Dinitro-2-methylphenol ug/kg M016202949.2-104541630ND471J880
4-Bromophenylphenyl ether ug/kg M0,R116204161-96.569 521630ND6661130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 84 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
21289MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9257863002
21290
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
4-Chloro-3-methylphenol ug/kg M016203063.4-98.571630ND492J930
4-Chloroaniline ug/kg M0,R116202854.8-90.54 651630ND454888
4-Chlorophenylphenyl ether ug/kg M0,R116203655.1-97.67 601630ND5881100
4-Nitroaniline ug/kg M0,R116203948.6-95.76 641630ND6411240
4-Nitrophenol ug/kg R116204027.1-11272 581630ND6501180
Acenaphthene ug/kg R116203122-124.159 631630ND498960
Acenaphthylene ug/kg R116203222.7-12759 591630ND521956
Anthracene ug/kg R116203523.8-11767 641630ND5691100
Benzo(a)anthracene ug/kg R116203825.7-12566 541630ND6151080
Benzo(a)pyrene ug/kg R116203925.5-12669 571630ND6251130
Benzo(b)fluoranthene ug/kg R116203924.9-13268 541630ND6371110
Benzo(g,h,i)perylene ug/kg R116203528.1-13466 611630ND5721080
Benzo(k)fluoranthene ug/kg R116204130.1-13571 551630ND6581160
bis(2-Chloroethoxy)methane ug/kg M0,R116202451-93.244 601630ND383712
bis(2-Chloroethyl) ether ug/kg M0,R116202150.3-86.34 471630ND344554
bis(2-Chloroisopropyl) ether ug/kg M0,R116202943.1-87.45 431630ND478742
bis(2-Ethylhexyl)phthalate ug/kg R116203410-238.862 581630ND5581010
Butylbenzylphthalate ug/kg M0,R116203455.5-11662 581630ND5591020
Chrysene ug/kg R116203725.9-12965 561630ND5951060
Di-n-butylphthalate ug/kg M0,R116203463.2-10262 581630ND5531010
Di-n-octylphthalate ug/kg M0,R116203556.5-11963 581630ND5691030
Dibenz(a,h)anthracene ug/kg R116203728.1-13668 601630ND6001110
Dibenzofuran ug/kg M0,R116203444-89.362 601630ND5491020
Diethylphthalate ug/kg M0,R116203864.9-94.67 561630ND6111090
Dimethylphthalate ug/kg M0,R116203655.3-94.65 561630ND5921060
Fluoranthene ug/kg R116203727.6-12964 541630ND6051050
Fluorene ug/kg R116203622.1-13469 631630ND5831120
Hexachloro-1,3-butadiene ug/kg R116203723.8-97.64 551630ND5971050
Hexachlorobenzene ug/kg M0,R116203843.5-98.69 581630ND6231130
Hexachlorocyclopentadiene ug/kg M016203037.1-91.521630ND493J847
Hexachloroethane ug/kg M0,R116203150.9-11049 471630ND499802
Indeno(1,2,3-cd)pyrene ug/kg R116203827.4-13468 581630ND6171120
Isophorone ug/kg M0,R116202454.7-91.41 541630ND389677
N-Nitroso-di-n-propylamine ug/kg M0,R116202360.7-96.47 681630ND376767
N-Nitrosodimethylamine ug/kg M0,R116201850.7-89.33 581630ND293531
N-Nitrosodiphenylamine ug/kg M0,R116203453.8-11263 611630ND5501030
Naphthalene ug/kg R116202919.8-11653 591630ND467859
Nitrobenzene ug/kg M0,R116202754.6-87.43 481630ND433704
Pentachlorophenol ug/kg M016201935.6-133541630ND312J882
Phenanthrene ug/kg R116203727.7-12865 561630ND5991070
Phenol ug/kg M0,R116202149.3-10240 631630ND344660
Pyrene ug/kg R116203727.7-12868 591630ND6031100
2,4,6-Tribromophenol (S)%33 10-11062
2-Fluorobiphenyl (S)%32 18-11057
2-Fluorophenol (S)%22 18-11039
Nitrobenzene-d5 (S)%25 10-11044
Phenol-d6 (S)%23 10-11043
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 85 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
21289MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9257863002
21290
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Terphenyl-d14 (S)%37 10-12368
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 86 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/9097
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9257863001, 9257863002, 9257863004, 9257863005, 9257863007, 9257863011, 9257863012, 9257863013,
9257863014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:368812
Associated Lab Samples:9257863001, 9257863002, 9257863004, 9257863005, 9257863007, 9257863011, 9257863012, 9257863013,
9257863014
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 11/19/09 14:02
1,1,1-Trichloroethane ug/kg ND 5.0 11/19/09 14:02
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 11/19/09 14:02
1,1,2-Trichloroethane ug/kg ND 5.0 11/19/09 14:02
1,1-Dichloroethane ug/kg ND 5.0 11/19/09 14:02
1,1-Dichloroethene ug/kg ND 5.0 11/19/09 14:02
1,1-Dichloropropene ug/kg ND 5.0 11/19/09 14:02
1,2,3-Trichlorobenzene ug/kg ND 5.0 11/19/09 14:02
1,2,3-Trichloropropane ug/kg ND 5.0 11/19/09 14:02
1,2,4-Trichlorobenzene ug/kg ND 5.0 11/19/09 14:02
1,2,4-Trimethylbenzene ug/kg ND 5.0 11/19/09 14:02
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 11/19/09 14:02
1,2-Dibromoethane (EDB)ug/kg ND 5.0 11/19/09 14:02
1,2-Dichlorobenzene ug/kg ND 5.0 11/19/09 14:02
1,2-Dichloroethane ug/kg ND 5.0 11/19/09 14:02
1,2-Dichloropropane ug/kg ND 5.0 11/19/09 14:02
1,3,5-Trimethylbenzene ug/kg ND 5.0 11/19/09 14:02
1,3-Dichlorobenzene ug/kg ND 5.0 11/19/09 14:02
1,3-Dichloropropane ug/kg ND 5.0 11/19/09 14:02
1,4-Dichlorobenzene ug/kg ND 5.0 11/19/09 14:02
2,2-Dichloropropane ug/kg ND 5.0 11/19/09 14:02
2-Butanone (MEK)ug/kg ND 100 11/19/09 14:02
2-Chlorotoluene ug/kg ND 5.0 11/19/09 14:02
2-Hexanone ug/kg ND 50.0 11/19/09 14:02
4-Chlorotoluene ug/kg ND 5.0 11/19/09 14:02
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 11/19/09 14:02
Acetone ug/kg ND 100 11/19/09 14:02
Benzene ug/kg ND 5.0 11/19/09 14:02
Bromobenzene ug/kg ND 5.0 11/19/09 14:02
Bromochloromethane ug/kg ND 5.0 11/19/09 14:02
Bromodichloromethane ug/kg ND 5.0 11/19/09 14:02
Bromoform ug/kg ND 5.0 11/19/09 14:02
Bromomethane ug/kg ND 10.0 11/19/09 14:02
Carbon tetrachloride ug/kg ND 5.0 11/19/09 14:02
Chlorobenzene ug/kg ND 5.0 11/19/09 14:02
Chloroethane ug/kg ND 10.0 11/19/09 14:02
Chloroform ug/kg ND 5.0 11/19/09 14:02
Chloromethane ug/kg ND 10.0 11/19/09 14:02
cis-1,2-Dichloroethene ug/kg ND 5.0 11/19/09 14:02
cis-1,3-Dichloropropene ug/kg ND 5.0 11/19/09 14:02
Dibromochloromethane ug/kg ND 5.0 11/19/09 14:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 87 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:368812
Associated Lab Samples:9257863001, 9257863002, 9257863004, 9257863005, 9257863007, 9257863011, 9257863012, 9257863013,
9257863014
Matrix:Solid
Analyzed
Dibromomethane ug/kg ND 5.0 11/19/09 14:02
Dichlorodifluoromethane ug/kg ND 10.0 11/19/09 14:02
Diisopropyl ether ug/kg ND 5.0 11/19/09 14:02
Ethylbenzene ug/kg ND 5.0 11/19/09 14:02
Hexachloro-1,3-butadiene ug/kg ND 5.0 11/19/09 14:02
Isopropylbenzene (Cumene)ug/kg ND 5.0 11/19/09 14:02
m&p-Xylene ug/kg ND 10.0 11/19/09 14:02
Methyl-tert-butyl ether ug/kg ND 5.0 11/19/09 14:02
Methylene Chloride ug/kg ND 20.0 11/19/09 14:02
n-Butylbenzene ug/kg ND 5.0 11/19/09 14:02
n-Propylbenzene ug/kg ND 5.0 11/19/09 14:02
Naphthalene ug/kg ND 5.0 11/19/09 14:02
o-Xylene ug/kg ND 5.0 11/19/09 14:02
p-Isopropyltoluene ug/kg ND 5.0 11/19/09 14:02
sec-Butylbenzene ug/kg ND 5.0 11/19/09 14:02
Styrene ug/kg ND 5.0 11/19/09 14:02
tert-Butylbenzene ug/kg ND 5.0 11/19/09 14:02
Tetrachloroethene ug/kg ND 5.0 11/19/09 14:02
Toluene ug/kg ND 5.0 11/19/09 14:02
trans-1,2-Dichloroethene ug/kg ND 5.0 11/19/09 14:02
trans-1,3-Dichloropropene ug/kg ND 5.0 11/19/09 14:02
Trichloroethene ug/kg ND 5.0 11/19/09 14:02
Trichlorofluoromethane ug/kg ND 5.0 11/19/09 14:02
Vinyl acetate ug/kg ND 50.0 11/19/09 14:02
Vinyl chloride ug/kg ND 10.0 11/19/09 14:02
Xylene (Total)ug/kg ND 10.0 11/19/09 14:02
1,2-Dichloroethane-d4 (S)%105 69-121 11/19/09 14:02
4-Bromofluorobenzene (S)%96 74-115 11/19/09 14:02
Dibromofluoromethane (S)%102 79-116 11/19/09 14:02
Toluene-d8 (S)%100 88-110 11/19/09 14:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
368813LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 58.350 117 75-137
1,1,1-Trichloroethane ug/kg 68.550 137 70-140
1,1,2,2-Tetrachloroethane ug/kg 61.550 123 74-133
1,1,2-Trichloroethane ug/kg 62.050 124 79-129
1,1-Dichloroethane ug/kg 73.2 L35014672-139
1,1-Dichloroethene ug/kg 57.150 114 69-154
1,1-Dichloropropene ug/kg 59.450 119 74-138
1,2,3-Trichlorobenzene ug/kg 55.950 112 71-150
1,2,3-Trichloropropane ug/kg 59.450 119 74-135
1,2,4-Trichlorobenzene ug/kg 55.550 111 68-150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 88 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
368813LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 59.150 118 70-130
1,2-Dibromo-3-chloropropane ug/kg 63.250 126 65-146
1,2-Dibromoethane (EDB)ug/kg 60.750 121 77-136
1,2-Dichlorobenzene ug/kg 60.050 120 75-141
1,2-Dichloroethane ug/kg 60.750 121 74-134
1,2-Dichloropropane ug/kg 60.850 122 77-138
1,3,5-Trimethylbenzene ug/kg 57.550 115 65-128
1,3-Dichlorobenzene ug/kg 58.850 118 76-133
1,3-Dichloropropane ug/kg 59.650 119 79-132
1,4-Dichlorobenzene ug/kg 58.250 116 75-137
2,2-Dichloropropane ug/kg 71.0 L35014273-137
2-Butanone (MEK)ug/kg 136100 136 61-138
2-Chlorotoluene ug/kg 58.450 117 73-138
2-Hexanone ug/kg 115100 115 58-159
4-Chlorotoluene ug/kg 61.250 122 75-136
4-Methyl-2-pentanone (MIBK)ug/kg 129100 129 74-139
Acetone ug/kg 136100 136 58-150
Benzene ug/kg 61.050 122 71-140
Bromobenzene ug/kg 58.650 117 72-144
Bromochloromethane ug/kg 67.6 L35013578-133
Bromodichloromethane ug/kg 58.850 118 78-133
Bromoform ug/kg 54.450 109 74-132
Bromomethane ug/kg 73.950 148 63-184
Carbon tetrachloride ug/kg 76.7 L35015373-143
Chlorobenzene ug/kg 58.850 118 77-137
Chloroethane ug/kg 59.050 118 68-146
Chloroform ug/kg 61.350 123 75-137
Chloromethane ug/kg 59.050 118 54-143
cis-1,2-Dichloroethene ug/kg 60.250 120 71-143
cis-1,3-Dichloropropene ug/kg 60.150 120 76-133
Dibromochloromethane ug/kg 58.950 118 77-131
Dibromomethane ug/kg 65.350 131 63-184
Dichlorodifluoromethane ug/kg 58.550 117 36-173
Diisopropyl ether ug/kg 56.250 112 68-144
Ethylbenzene ug/kg 59.050 118 69-141
Hexachloro-1,3-butadiene ug/kg 56.050 112 70-152
Isopropylbenzene (Cumene)ug/kg 58.550 117 77-143
m&p-Xylene ug/kg 118100 118 72-138
Methyl-tert-butyl ether ug/kg 59.250 118 2-138
Methylene Chloride ug/kg 57.350 115 69-136
n-Butylbenzene ug/kg 58.650 117 65-128
n-Propylbenzene ug/kg 59.250 118 72-139
Naphthalene ug/kg 58.050 116 61-138
o-Xylene ug/kg 60.950 122 74-137
p-Isopropyltoluene ug/kg 57.750 115 66-128
sec-Butylbenzene ug/kg 59.650 119 72-140
Styrene ug/kg 53.050 106 76-137
tert-Butylbenzene ug/kg 59.750 119 68-141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 89 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
368813LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 58.250 116 72-136
Toluene ug/kg 58.350 117 69-139
trans-1,2-Dichloroethene ug/kg 54.150 108 72-144
trans-1,3-Dichloropropene ug/kg 60.950 122 73-135
Trichloroethene ug/kg 58.250 116 75-136
Trichlorofluoromethane ug/kg 57.850 116 69-144
Vinyl acetate ug/kg 114100 114 50-150
Vinyl chloride ug/kg 59.050 118 61-145
Xylene (Total)ug/kg 179150 119 73-138
1,2-Dichloroethane-d4 (S)%103 69-121
4-Bromofluorobenzene (S)%98 74-115
Dibromofluoromethane (S)%101 79-116
Toluene-d8 (S)%100 88-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
369434MATRIX SPIKE SAMPLE:
MSSpike
Result
9257758003
1,1-Dichloroethene ug/kg 57.961.3 94 33-158ND
Benzene ug/kg 54.561.3 89 46-143ND
Chlorobenzene ug/kg 50.661.3 83 29-159ND
Toluene ug/kg 53.161.3 87 38-145ND
Trichloroethene ug/kg 53.161.3 87 70-130ND
1,2-Dichloroethane-d4 (S)%109 69-121
4-Bromofluorobenzene (S)%97 74-115
Dibromofluoromethane (S)%104 79-116
Toluene-d8 (S)%101 88-110
Parameter Units
Dup
Result QualifiersRPDResult
9257774002
369433SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 90 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Dup
Result QualifiersRPDResult
9257774002
369433SAMPLE DUPLICATE:
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 91 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Dup
Result QualifiersRPDResult
9257774002
369433SAMPLE DUPLICATE:
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%102 6106
4-Bromofluorobenzene (S)%104 696
Dibromofluoromethane (S)%105 4108
Toluene-d8 (S)%107 2103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 92 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/9098
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9257863003, 9257863006, 9257863008, 9257863009, 9257863010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:368816
Associated Lab Samples:9257863003, 9257863006, 9257863008, 9257863009, 9257863010
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 11/19/09 13:44
1,1,1-Trichloroethane ug/kg ND 5.0 11/19/09 13:44
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 11/19/09 13:44
1,1,2-Trichloroethane ug/kg ND 5.0 11/19/09 13:44
1,1-Dichloroethane ug/kg ND 5.0 11/19/09 13:44
1,1-Dichloroethene ug/kg ND 5.0 11/19/09 13:44
1,1-Dichloropropene ug/kg ND 5.0 11/19/09 13:44
1,2,3-Trichlorobenzene ug/kg ND 5.0 11/19/09 13:44
1,2,3-Trichloropropane ug/kg ND 5.0 11/19/09 13:44
1,2,4-Trichlorobenzene ug/kg ND 5.0 11/19/09 13:44
1,2,4-Trimethylbenzene ug/kg ND 5.0 11/19/09 13:44
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 11/19/09 13:44
1,2-Dibromoethane (EDB)ug/kg ND 5.0 11/19/09 13:44
1,2-Dichlorobenzene ug/kg ND 5.0 11/19/09 13:44
1,2-Dichloroethane ug/kg ND 5.0 11/19/09 13:44
1,2-Dichloropropane ug/kg ND 5.0 11/19/09 13:44
1,3,5-Trimethylbenzene ug/kg ND 5.0 11/19/09 13:44
1,3-Dichlorobenzene ug/kg ND 5.0 11/19/09 13:44
1,3-Dichloropropane ug/kg ND 5.0 11/19/09 13:44
1,4-Dichlorobenzene ug/kg ND 5.0 11/19/09 13:44
2,2-Dichloropropane ug/kg ND 5.0 11/19/09 13:44
2-Butanone (MEK)ug/kg ND 100 11/19/09 13:44
2-Chlorotoluene ug/kg ND 5.0 11/19/09 13:44
2-Hexanone ug/kg ND 50.0 11/19/09 13:44
4-Chlorotoluene ug/kg ND 5.0 11/19/09 13:44
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 11/19/09 13:44
Acetone ug/kg ND 100 11/19/09 13:44
Benzene ug/kg ND 5.0 11/19/09 13:44
Bromobenzene ug/kg ND 5.0 11/19/09 13:44
Bromochloromethane ug/kg ND 5.0 11/19/09 13:44
Bromodichloromethane ug/kg ND 5.0 11/19/09 13:44
Bromoform ug/kg ND 5.0 11/19/09 13:44
Bromomethane ug/kg ND 10.0 11/19/09 13:44
Carbon tetrachloride ug/kg ND 5.0 11/19/09 13:44
Chlorobenzene ug/kg ND 5.0 11/19/09 13:44
Chloroethane ug/kg ND 10.0 11/19/09 13:44
Chloroform ug/kg ND 5.0 11/19/09 13:44
Chloromethane ug/kg ND 10.0 11/19/09 13:44
cis-1,2-Dichloroethene ug/kg ND 5.0 11/19/09 13:44
cis-1,3-Dichloropropene ug/kg ND 5.0 11/19/09 13:44
Dibromochloromethane ug/kg ND 5.0 11/19/09 13:44
Dibromomethane ug/kg ND 5.0 11/19/09 13:44
Dichlorodifluoromethane ug/kg ND 10.0 11/19/09 13:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 93 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:368816
Associated Lab Samples:9257863003, 9257863006, 9257863008, 9257863009, 9257863010
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 11/19/09 13:44
Ethylbenzene ug/kg ND 5.0 11/19/09 13:44
Hexachloro-1,3-butadiene ug/kg ND 5.0 11/19/09 13:44
Isopropylbenzene (Cumene)ug/kg ND 5.0 11/19/09 13:44
m&p-Xylene ug/kg ND 10.0 11/19/09 13:44
Methyl-tert-butyl ether ug/kg ND 5.0 11/19/09 13:44
Methylene Chloride ug/kg ND 20.0 11/19/09 13:44
n-Butylbenzene ug/kg ND 5.0 11/19/09 13:44
n-Propylbenzene ug/kg ND 5.0 11/19/09 13:44
Naphthalene ug/kg ND 5.0 11/19/09 13:44
o-Xylene ug/kg ND 5.0 11/19/09 13:44
p-Isopropyltoluene ug/kg ND 5.0 11/19/09 13:44
sec-Butylbenzene ug/kg ND 5.0 11/19/09 13:44
Styrene ug/kg ND 5.0 11/19/09 13:44
tert-Butylbenzene ug/kg ND 5.0 11/19/09 13:44
Tetrachloroethene ug/kg ND 5.0 11/19/09 13:44
Toluene ug/kg ND 5.0 11/19/09 13:44
trans-1,2-Dichloroethene ug/kg ND 5.0 11/19/09 13:44
trans-1,3-Dichloropropene ug/kg ND 5.0 11/19/09 13:44
Trichloroethene ug/kg ND 5.0 11/19/09 13:44
Trichlorofluoromethane ug/kg ND 5.0 11/19/09 13:44
Vinyl acetate ug/kg ND 50.0 11/19/09 13:44
Vinyl chloride ug/kg ND 10.0 11/19/09 13:44
Xylene (Total)ug/kg ND 10.0 11/19/09 13:44
1,2-Dichloroethane-d4 (S)%107 69-121 11/19/09 13:44
4-Bromofluorobenzene (S)%98 74-115 11/19/09 13:44
Dibromofluoromethane (S)%104 79-116 11/19/09 13:44
Toluene-d8 (S)%102 88-110 11/19/09 13:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
368817LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 63.450 127 75-137
1,1,1-Trichloroethane ug/kg 71.3 L35014370-140
1,1,2,2-Tetrachloroethane ug/kg 65.150 130 74-133
1,1,2-Trichloroethane ug/kg 63.750 127 79-129
1,1-Dichloroethane ug/kg 77.3 L35015572-139
1,1-Dichloroethene ug/kg 61.950 124 69-154
1,1-Dichloropropene ug/kg 62.950 126 74-138
1,2,3-Trichlorobenzene ug/kg 62.250 124 71-150
1,2,3-Trichloropropane ug/kg 63.350 127 74-135
1,2,4-Trichlorobenzene ug/kg 61.750 123 68-150
1,2,4-Trimethylbenzene ug/kg 63.650 127 70-130
1,2-Dibromo-3-chloropropane ug/kg 66.450 133 65-146
1,2-Dibromoethane (EDB)ug/kg 64.850 130 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 94 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
368817LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 63.850 128 75-141
1,2-Dichloroethane ug/kg 64.850 130 74-134
1,2-Dichloropropane ug/kg 64.950 130 77-138
1,3,5-Trimethylbenzene ug/kg 60.550 121 65-128
1,3-Dichlorobenzene ug/kg 63.150 126 76-133
1,3-Dichloropropane ug/kg 62.150 124 79-132
1,4-Dichlorobenzene ug/kg 62.050 124 75-137
2,2-Dichloropropane ug/kg 74.8 L35015073-137
2-Butanone (MEK)ug/kg 136100 136 61-138
2-Chlorotoluene ug/kg 62.050 124 73-138
2-Hexanone ug/kg 120100 120 58-159
4-Chlorotoluene ug/kg 64.950 130 75-136
4-Methyl-2-pentanone (MIBK)ug/kg 135100 135 74-139
Acetone ug/kg 133100 133 58-150
Benzene ug/kg 64.850 130 71-140
Bromobenzene ug/kg 62.950 126 72-144
Bromochloromethane ug/kg 69.7 L35013978-133
Bromodichloromethane ug/kg 62.950 126 78-133
Bromoform ug/kg 57.450 115 74-132
Bromomethane ug/kg 83.350 167 63-184
Carbon tetrachloride ug/kg 69.950 140 73-143
Chlorobenzene ug/kg 63.450 127 77-137
Chloroethane ug/kg 64.850 130 68-146
Chloroform ug/kg 64.850 130 75-137
Chloromethane ug/kg 65.450 131 54-143
cis-1,2-Dichloroethene ug/kg 63.150 126 71-143
cis-1,3-Dichloropropene ug/kg 66.250 132 76-133
Dibromochloromethane ug/kg 62.350 125 77-131
Dibromomethane ug/kg 68.850 138 63-184
Dichlorodifluoromethane ug/kg 65.350 131 36-173
Diisopropyl ether ug/kg 59.650 119 68-144
Ethylbenzene ug/kg 63.650 127 69-141
Hexachloro-1,3-butadiene ug/kg 60.750 121 70-152
Isopropylbenzene (Cumene)ug/kg 63.350 127 77-143
m&p-Xylene ug/kg 127100 127 72-138
Methyl-tert-butyl ether ug/kg 61.850 124 2-138
Methylene Chloride ug/kg 61.450 123 69-136
n-Butylbenzene ug/kg 63.150 126 65-128
n-Propylbenzene ug/kg 63.150 126 72-139
Naphthalene ug/kg 63.950 128 61-138
o-Xylene ug/kg 64.050 128 74-137
p-Isopropyltoluene ug/kg 62.350 125 66-128
sec-Butylbenzene ug/kg 63.750 127 72-140
Styrene ug/kg 57.050 114 76-137
tert-Butylbenzene ug/kg 63.050 126 68-141
Tetrachloroethene ug/kg 62.750 125 72-136
Toluene ug/kg 62.550 125 69-139
trans-1,2-Dichloroethene ug/kg 57.150 114 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 95 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
368817LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 65.250 130 73-135
Trichloroethene ug/kg 62.850 126 75-136
Trichlorofluoromethane ug/kg 62.450 125 69-144
Vinyl acetate ug/kg 113100 113 50-150
Vinyl chloride ug/kg 66.350 133 61-145
Xylene (Total)ug/kg 191150 127 73-138
1,2-Dichloroethane-d4 (S)%100 69-121
4-Bromofluorobenzene (S)%98 74-115
Dibromofluoromethane (S)%101 79-116
Toluene-d8 (S)%100 88-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 96 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/9131
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9257863015, 9257863016, 9257863017
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:370482
Associated Lab Samples:9257863015, 9257863016, 9257863017
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 11/30/09 10:08
1,1,1-Trichloroethane ug/kg ND 5.0 11/30/09 10:08
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 11/30/09 10:08
1,1,2-Trichloroethane ug/kg ND 5.0 11/30/09 10:08
1,1-Dichloroethane ug/kg ND 5.0 11/30/09 10:08
1,1-Dichloroethene ug/kg ND 5.0 11/30/09 10:08
1,1-Dichloropropene ug/kg ND 5.0 11/30/09 10:08
1,2,3-Trichlorobenzene ug/kg ND 5.0 11/30/09 10:08
1,2,3-Trichloropropane ug/kg ND 5.0 11/30/09 10:08
1,2,4-Trichlorobenzene ug/kg ND 5.0 11/30/09 10:08
1,2,4-Trimethylbenzene ug/kg ND 5.0 11/30/09 10:08
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 11/30/09 10:08
1,2-Dibromoethane (EDB)ug/kg ND 5.0 11/30/09 10:08
1,2-Dichlorobenzene ug/kg ND 5.0 11/30/09 10:08
1,2-Dichloroethane ug/kg ND 5.0 11/30/09 10:08
1,2-Dichloropropane ug/kg ND 5.0 11/30/09 10:08
1,3,5-Trimethylbenzene ug/kg ND 5.0 11/30/09 10:08
1,3-Dichlorobenzene ug/kg ND 5.0 11/30/09 10:08
1,3-Dichloropropane ug/kg ND 5.0 11/30/09 10:08
1,4-Dichlorobenzene ug/kg ND 5.0 11/30/09 10:08
2,2-Dichloropropane ug/kg ND 5.0 11/30/09 10:08
2-Butanone (MEK)ug/kg ND 100 11/30/09 10:08
2-Chlorotoluene ug/kg ND 5.0 11/30/09 10:08
2-Hexanone ug/kg ND 50.0 11/30/09 10:08
4-Chlorotoluene ug/kg ND 5.0 11/30/09 10:08
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 11/30/09 10:08
Acetone ug/kg ND 100 11/30/09 10:08
Benzene ug/kg ND 5.0 11/30/09 10:08
Bromobenzene ug/kg ND 5.0 11/30/09 10:08
Bromochloromethane ug/kg ND 5.0 11/30/09 10:08
Bromodichloromethane ug/kg ND 5.0 11/30/09 10:08
Bromoform ug/kg ND 5.0 11/30/09 10:08
Bromomethane ug/kg ND 10.0 11/30/09 10:08
Carbon tetrachloride ug/kg ND 5.0 11/30/09 10:08
Chlorobenzene ug/kg ND 5.0 11/30/09 10:08
Chloroethane ug/kg ND 10.0 11/30/09 10:08
Chloroform ug/kg ND 5.0 11/30/09 10:08
Chloromethane ug/kg ND 10.0 11/30/09 10:08
cis-1,2-Dichloroethene ug/kg ND 5.0 11/30/09 10:08
cis-1,3-Dichloropropene ug/kg ND 5.0 11/30/09 10:08
Dibromochloromethane ug/kg ND 5.0 11/30/09 10:08
Dibromomethane ug/kg ND 5.0 11/30/09 10:08
Dichlorodifluoromethane ug/kg ND 10.0 11/30/09 10:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 97 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:370482
Associated Lab Samples:9257863015, 9257863016, 9257863017
Matrix:Solid
Analyzed
Diisopropyl ether ug/kg ND 5.0 11/30/09 10:08
Ethylbenzene ug/kg ND 5.0 11/30/09 10:08
Hexachloro-1,3-butadiene ug/kg ND 5.0 11/30/09 10:08
Isopropylbenzene (Cumene)ug/kg ND 5.0 11/30/09 10:08
m&p-Xylene ug/kg ND 10.0 11/30/09 10:08
Methyl-tert-butyl ether ug/kg ND 5.0 11/30/09 10:08
Methylene Chloride ug/kg ND 20.0 11/30/09 10:08
n-Butylbenzene ug/kg ND 5.0 11/30/09 10:08
n-Propylbenzene ug/kg ND 5.0 11/30/09 10:08
Naphthalene ug/kg ND 5.0 11/30/09 10:08
o-Xylene ug/kg ND 5.0 11/30/09 10:08
p-Isopropyltoluene ug/kg ND 5.0 11/30/09 10:08
sec-Butylbenzene ug/kg ND 5.0 11/30/09 10:08
Styrene ug/kg ND 5.0 11/30/09 10:08
tert-Butylbenzene ug/kg ND 5.0 11/30/09 10:08
Tetrachloroethene ug/kg ND 5.0 11/30/09 10:08
Toluene ug/kg ND 5.0 11/30/09 10:08
trans-1,2-Dichloroethene ug/kg ND 5.0 11/30/09 10:08
trans-1,3-Dichloropropene ug/kg ND 5.0 11/30/09 10:08
Trichloroethene ug/kg ND 5.0 11/30/09 10:08
Trichlorofluoromethane ug/kg ND 5.0 11/30/09 10:08
Vinyl acetate ug/kg ND 50.0 11/30/09 10:08
Vinyl chloride ug/kg ND 10.0 11/30/09 10:08
Xylene (Total)ug/kg ND 10.0 11/30/09 10:08
1,2-Dichloroethane-d4 (S)%90 69-121 11/30/09 10:08
4-Bromofluorobenzene (S)%108 74-115 11/30/09 10:08
Dibromofluoromethane (S)%101 79-116 11/30/09 10:08
Toluene-d8 (S)%101 88-110 11/30/09 10:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
370483LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 53.050 106 75-137
1,1,1-Trichloroethane ug/kg 46.050 92 70-140
1,1,2,2-Tetrachloroethane ug/kg 55.150 110 74-133
1,1,2-Trichloroethane ug/kg 50.650 101 79-129
1,1-Dichloroethane ug/kg 52.350 105 72-139
1,1-Dichloroethene ug/kg 46.050 92 69-154
1,1-Dichloropropene ug/kg 51.450 103 74-138
1,2,3-Trichlorobenzene ug/kg 55.750 111 71-150
1,2,3-Trichloropropane ug/kg 53.250 106 74-135
1,2,4-Trichlorobenzene ug/kg 59.850 120 68-150
1,2,4-Trimethylbenzene ug/kg 55.850 112 70-130
1,2-Dibromo-3-chloropropane ug/kg 48.750 97 65-146
1,2-Dibromoethane (EDB)ug/kg 55.150 110 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 98 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
370483LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/kg 53.250 106 75-141
1,2-Dichloroethane ug/kg 47.250 94 74-134
1,2-Dichloropropane ug/kg 49.750 99 77-138
1,3,5-Trimethylbenzene ug/kg 53.950 108 65-128
1,3-Dichlorobenzene ug/kg 53.050 106 76-133
1,3-Dichloropropane ug/kg 54.250 108 79-132
1,4-Dichlorobenzene ug/kg 50.350 101 75-137
2,2-Dichloropropane ug/kg 49.450 99 73-137
2-Butanone (MEK)ug/kg 103100 103 61-138
2-Chlorotoluene ug/kg 50.950 102 73-138
2-Hexanone ug/kg 106100 106 58-159
4-Chlorotoluene ug/kg 53.950 108 75-136
4-Methyl-2-pentanone (MIBK)ug/kg 100100 100 74-139
Acetone ug/kg 93.8J100 94 58-150
Benzene ug/kg 51.650 103 71-140
Bromobenzene ug/kg 50.350 101 72-144
Bromochloromethane ug/kg 48.650 97 78-133
Bromodichloromethane ug/kg 46.650 93 78-133
Bromoform ug/kg 54.150 108 74-132
Bromomethane ug/kg 54.750 109 63-184
Carbon tetrachloride ug/kg 50.450 101 73-143
Chlorobenzene ug/kg 51.650 103 77-137
Chloroethane ug/kg 45.950 92 68-146
Chloroform ug/kg 47.950 96 75-137
Chloromethane ug/kg 48.650 97 54-143
cis-1,2-Dichloroethene ug/kg 51.850 104 71-143
cis-1,3-Dichloropropene ug/kg 52.750 105 76-133
Dibromochloromethane ug/kg 50.350 101 77-131
Dibromomethane ug/kg 51.950 104 63-184
Dichlorodifluoromethane ug/kg 44.750 89 36-173
Diisopropyl ether ug/kg 46.550 93 68-144
Ethylbenzene ug/kg 53.350 107 69-141
Hexachloro-1,3-butadiene ug/kg 53.350 107 70-152
Isopropylbenzene (Cumene)ug/kg 52.950 106 77-143
m&p-Xylene ug/kg 111100 111 72-138
Methyl-tert-butyl ether ug/kg 43.350 87 2-138
Methylene Chloride ug/kg 48.150 96 69-136
n-Butylbenzene ug/kg 55.250 110 65-128
n-Propylbenzene ug/kg 54.550 109 72-139
Naphthalene ug/kg 61.850 124 61-138
o-Xylene ug/kg 57.350 115 74-137
p-Isopropyltoluene ug/kg 56.250 112 66-128
sec-Butylbenzene ug/kg 55.150 110 72-140
Styrene ug/kg 50.850 102 76-137
tert-Butylbenzene ug/kg 55.250 110 68-141
Tetrachloroethene ug/kg 54.350 109 72-136
Toluene ug/kg 49.350 99 69-139
trans-1,2-Dichloroethene ug/kg 41.350 83 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 99 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
370483LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene ug/kg 53.050 106 73-135
Trichloroethene ug/kg 53.250 106 75-136
Trichlorofluoromethane ug/kg 44.450 89 69-144
Vinyl acetate ug/kg 193 L310019350-150
Vinyl chloride ug/kg 52.350 105 61-145
Xylene (Total)ug/kg 168150 112 73-138
1,2-Dichloroethane-d4 (S)%89 69-121
4-Bromofluorobenzene (S)%106 74-115
Dibromofluoromethane (S)%93 79-116
Toluene-d8 (S)%95 88-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
372783MATRIX SPIKE SAMPLE:
MSSpike
Result
9257863015
1,1-Dichloroethene ug/kg 56.151.2 110 33-158ND
Benzene ug/kg 57.951.2 110 46-143ND
Chlorobenzene ug/kg 10751.2 108 29-15951.9
Toluene ug/kg 53.751.2 105 38-145ND
Trichloroethene ug/kg 54.051.2 106 70-130ND
1,2-Dichloroethane-d4 (S)%100 69-121
4-Bromofluorobenzene (S)%95 74-115
Dibromofluoromethane (S)%100 79-116
Toluene-d8 (S)%100 88-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 100 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2890
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9257863001, 9257863002, 9257863003, 9257863004, 9257863005
Parameter Units
Dup
Result QualifiersRPDResult
9257805001
368670SAMPLE DUPLICATE:
Percent Moisture %20.1 1117.9
Parameter Units
Dup
Result QualifiersRPDResult
9257863004
368671SAMPLE DUPLICATE:
Percent Moisture %5.3 84.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 101 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2891
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9257863006, 9257863007, 9257863008, 9257863009
Parameter Units
Dup
Result QualifiersRPDResult
9257690001
368707SAMPLE DUPLICATE:
Percent Moisture %22.0 022.0
Parameter Units
Dup
Result QualifiersRPDResult
9257863009
368708SAMPLE DUPLICATE:
Percent Moisture %18.7 917.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 102 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2895
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9257863010, 9257863011, 9257863012, 9257863013, 9257863014
Parameter Units
Dup
Result QualifiersRPDResult
9258044001
369634SAMPLE DUPLICATE:
Percent Moisture %10.9 1012.0
Parameter Units
Dup
Result QualifiersRPDResult
9257863014
369635SAMPLE DUPLICATE:
Percent Moisture %14.8 114.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 103 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/2897
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9257863015, 9257863016, 9257863017, 9257863018
Parameter Units
Dup
Result QualifiersRPDResult
9257948001
370243SAMPLE DUPLICATE:
Percent Moisture %27.5 226.9
Parameter Units
Dup
Result QualifiersRPDResult
9258102001
370244SAMPLE DUPLICATE:
Percent Moisture %15.0 1113.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 104 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9257863
BLOOMSBURG MILLS
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
Pace Analytical Services - Ormond BeachPASI-O
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte concentration exceeded the calibration range. The reported result is estimated.E
The internal standard response is below criteria. Results may be biased high.IS
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 12/10/2009 02:46 PM Page 105 of 105
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]