04001 W Morehead OAR 2000.11.03

•
November 3, 2000
Carter & Associates, Inc.
The Charlotte Plaza
201 South College Street, Suite 1510
Charlotte, North Carolina 28244
Attention: Mr. Lawrence Shaw
Reference: Soil and Groundwater Assessment Report
1310 West Morehead Property
Charlotte, North Carolina
S&ME Project No. 1354-99-750A
Dear Mr. Shaw:
RECE 16D
DEC 1 2000
SUPERFUND SECTION
S&ME, Inc. (S&ME) is pleased to submit this report of additional soil and groundwater
sampling performed at the referenced site (Figure 1) in accordance with our proposal 1354-9644-
00, dated August 28, 2000. This assessment was performed based on the results of the prior
assessments (reports dated September 22, 1999 and October 21, 1999) that showed the presence
of contaminants in the groundwater at the site at levels above the NCDENR 15A NCAC 2L
groundwater standards. The results of our assessment with conclusions are provided below.
GROUNDWATER AND SOIL SAMPLING ANALYSIS
Previous Sampling Results
Previous assessment at the site included soil and groundwater sampling from locations identified
as GP-1 through GP-5 and HA-1 on Figure 2. The results of those assessments are provided in
the tables included in Appendix I. The groundwater sampling results indicated the presence of
trichloroethene or TCE (58 micrograms per liter or µg/L) and bis(2-ethylhexyl)phthalate or
BEHP (35 µg/L) in sample GP-2 at concentrations above the NCDENR groundwater quality
standards of 2.8 and 3 µg/L, respectively. Groundwater sample (GP-2) was collected in the
southeast corner of the main building. This location was selected to evaluate groundwater
S&ME, Inc. Mailing address: [phone]
9751 Southern Pine Blvd. P.O. Box 7668 [phone] fax
Charlotte, North Carolina 28273 Charlotte, North Carolina 28241-7668 www.smeinc.com

Soil and Groundwater Assessment Report
West Morehead Street Pror-e: <<.
S&ME Project No. 1354-99-750A
_ November 3, 2000
quality in the apparent downgradient area of the main building. Groundwater is expected to flow
to the southeast, based on the surface topography of the area. Due to the presence of these
contaminants, S&ME proposed to collect two additional groundwater samples (GP-4 and GP-5)
from locations upgradient of the GP-2 sample. Due to the presence of TCE at an off -site location
to the northeast, S&ME presented the possibility that the TCE detected at the subject site may
have been from an offsite source. The upgradient sample (GP-4) was selected to evaluate if TCE
may be migrating onto the subject property from an off -site source. Groundwater samples were
collected on October 11, 1999, at locations GP-4 and GP-5 at depths of 37 and 35 feet below
land surface, respectively. No TCE or BEHP were detected in GP-4 or GP-5.
Chloroform was detected in groundwater samples GP-4 and GP-5 at concentrations of 24 µg/L
and 9.6 µg/L, respectively. The 15A NCAC 2L groundwater quality standard for chloroform is
0.19 µg/L. Based on the groundwater quality data and the anticipated groundwater flow
direction (southeast), the results of the additional groundwater analyses from GP-4 and GP-5 did
not suggest an off -site source for the TCE or BEHP that was detected in GP-2. Concentrations
of chloroform in GP-4 and GP-5 suggest that the chloroform may be from an off -site source.
Additional Groundwater S �mplin�
Five additional groundwater samples were collected at locations GP-6, GP-7, GP-8, GP-9, and
GP-10 at depths of approximately 5 feet below the groundwater table. The samples were then
placed on ice and shipped to S&ME's NCDENR-certified laboratory in Savannah, Georgia for
analysis according to EPA Method 624 for volatile organics.
The results from the groundwater analysis showed concentrations of chloroform in groundwater
samples GP-7, GP-8, and GP-9 at 5 µg/L. The NCAC 15 2L groundwater standard for
chloroform is 0.19 µg/L. The results from groundwater sample GP-8 also showed a
concentration of trichloroethene (TCE) at 23 µg/L. The NCAC 15 2L groundwater standard for
TCE is 2.8 µg/L. No other constituents were detected above the laboratory detection limits. A
summary of the groundwater analytical results is shown in Table 1 (attached). A copy of the
laboratory analytical report is attached.
Pa

Soil and Groundwater Assessment Report S&ME Project No. 1354-99-750A
West Morehead Street Property November _3.2000
Recent Soil Sampling Results
Eleven additional soil samples were collected at locations GP-6 through GP-16. Soil samples
were collected at depths of 3, 6, 9, and 12 feet for sample locations GP-6, GP-7, and GP-8. Soil
samples were collected at depths of 3 and 6 feet for sample locations GP-9 through GP-16. The
samples were screened in the field using a Toxic Vapor Analyzer (Foxboro TVA 1000). One
soil sample from each probe point was then selected for laboratory analysis according to EPA
Method 8260. Five soil samples from probe locations GP-9 through GP-16 were then selected
for laboratory analysis according to EPA Method 8260. The results are summarized in Table 2,
with the sample collection depth if feet below land surface indicated as the last number of the
sample ID. Soil samples GP-12-3, GP-13-6, and GP-16-3 had matrix interferences that made
quantification impossible, however, rough estimations of their quantities were included in the
laboratory report. Because of this, the decision was made to analyze soil samples GP-9-6, GP-
10-3, and GP-11-3.
Results of the soil samples showed concentrations of 2-butanone (MEK) at an estimated 0.006
milligrams per kilogram (mg/kg) in soil sample GP-14-3. Results for soil sample GP-16-3
showed concentrations of WE and 1,2-dibromo-3-chloropropane at 5.4 mg/kg (estimated,
outside of calibration range) and 0.005 mg/kg (estimated), respectively. None of the detected
constituents were reported at concentrations above the corresponding EPA Region III industrial
or residential risk -based concentrations. No other constituents were detected in the soil samples
at concentrations above the laboratory detection limits. A summary of the soil analytical results
is shown in Table 2. A copy of the laboratory analytical report is included in Appendix II. A
summary of the TVA readings is included in Table 3.
Groundwater Levels
Prior to groundwater sampling using the Geoprobe, the depth to groundwater in the probe holes
GP-8 through GP-10 was measured (Table 3). The depth to groundwater ranged from
approximately 11.2 to 17 feet. The data do not indicate a definitive groundwater flow direction
as would be predicted from the topography of the area. The soils encountered at the site consist
of a mixture of sand, silt and clay and are expected to have low hydraulic conductivity values.
3

Soil and Groundwater Assessment Report
West Morehead Street Pro[,en�_
S&ME Project No. 1354-99-750A
November 3. 2000
The groundwater levels measured in the probe holes may not represent actual depth to
groundwater due to the low permeable soils.
CONCLUSIONS
Trichloroethene was detected in soil (GP-16) at an estimated concentration of 5.4 mg/kg,
whereas the EPA Region III Risk -Based Concentrations (RBC) for Residential and Industrial
sites are 58 and 520 mg/kg, respectively. TCE was also detected in groundwater (GP-2 at 58
µg/L and GP-8 at 23 µg/L) at concentrations above the 15A NCAC 2L groundwater quality
standard of 2.8 µg/L. Based on the soil and groundwater sampling, the source is likely from an
on -site release along the former floor drains in the larger building.
Chloroform was detected in groundwater (GP-4, 5, 7, 8 and 9) at concentrations ranging from 5
to 24 µg/L, whereas the groundwater quality standard is 0.29 µg/L. The maximum concentration
was detected in the suspected upgradient portion of the site at GP-4. No chloroform was
detected in the soil. The source of chloroform is suspected to be from an off -site, upgradient
release.
Methyl ethyl ketone (or 2-butanone) was detected in the soil at GP-14 at a concentration of 0.006
mg/kg, which is below the EPA RBC for Residential and Industrial sites. 1,2-Dibromo-3-
chloropropane was detected in the soil at GP-16 at a concentration of 0.005 mg/kg, which is
below the EPA RBC for Residential and Industrial sites. These two chemicals were not detected
in the groundwater samples collected at the site.
4

Soil and Groundwater Assessment Report
West Morehead Street
CLOSURE
S&ME Project No. 1354-99-750A
November 3. 2000
S&ME appreciates the opportunity to be of service to you and hopes that this report fulfills your
needs. If you have any questions regarding the outlined scope of work, or if we may be of any
further assistance, please call.
Very truly yours,
S&ME, Inc.
Jana E. Churchwell, E.I. ',```���:8��.�a,,,to'r
Staff Professsional ,a CARpF
Al Quarles, L.G.
Senior Hydrogeolo
Z .ate\CE NS��
SEAL
1-133
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QU
Attachments: Table 1— Suroundwater Analytical Results
Table 2 — Summary of Soil Analytical Results
Table 3 — Summary of TVA and Groundwater Level Data
Figure 1 — Site Location Map
Figure 2 — Sample Location Map
Appendix I — Tables from the September 22, 1999 and
October 21, 1999 Assessments
Appendix II - Copy of Laboratory Analytical Results

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TABLE 3
Summary of TVA and Groundwater Level Data
West Morehead Property - Charlotte, NC
S&ME Project # 1354-99-750A
Location
ID
Depth (ft)
(ft)
TVA-PID
(ppm)
TVA-FID
(ppm)
DTW
(ft)
GP-6
3
8.1
0.8
17
6
0.2
0.4
9
0.2
0.0
12
0.2
0.0
GP-7
3
10.3
0.4
15.5
6
1.5
0.8
9
0.8
0.8
12
0.8
0.0
GP-8
3
5.8
1.5
6
5.1
0.9
9
4.0
2.0
12
3.1
2.3
GP-9
3
6.6
1.4
11.2
6
7.0
1.6
GP-10
3
4.4
1.0
15.5
6
5.1
1.1
GP-11
3
4.1
0.2
6
3.9
0.2
GP-12
3
4.8
0.3
6
5.3
0.2
GP-13
3
0.0
0.5
6
5.6
0.1
GP-14
3
5.8
1.3
6
4.1
1.1
GP-15
3
6.1
2.1
6
8.1
1.6
GP-16
3
2.0
3.2
6
1 3.3
1 1.1
Notes: ft - feet below surface
TVA - Foxboro Toxic Vapor Analyzer 1000
PID - Photo -Ionization Detector
FID - Flame Ionization Detector
DTW - Depth to Water measured in Geoprobe hole

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GRAPHIC SCALE
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PREVIOUS SAMPLE LOCATIONS
( IN FEET )
SAMPLE LOCATIONS
1. SOIL VAPOR SCREENING WITH TVA AT 3 AND 6 FOOT DEPTHS AT 8 LOCATIONS AND AT 9 AND 12 FOOT
DEPTHS AT 3 LOCATIONS
2.ONE SOIL SAMPLE AT 8 LOCATIONS BASED ON TVA MEASUREMENTS (EPA 8260)
3. SHALLOW GROUNDWATER SAMPLING AT 5 LOCATIONS: CIRCLED SOIL VAPOR LOCATION (EPA 624)
RESIDENTIAL
ASTE
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ts&ME
ENGINEERING • TESTING
ENVIRONMENTAL SERVICES
SAMPLE LOCATIONS
1310 WEST MOREHEAD ST
CHARLOTTE, NORTH CAROLINA
SCALE: DRAWN BY: CHECKED BY:
AS SHOWN WAQ
JOB NO. DATE: FIGURE NO.
1354-99-750 11 /3/00
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TABLE 1 (from October 21,1999 report)
SUMMARY OF SOIL AND GROUNDWATER QUALITY DATA
PH II ESA 1310 W. MOREHEAD STREET
CHARLOTTE, NORTH CAROLINA
S&ME PROJECT 1354-99-750
Groundwater
Sample ID
GP-1-W
GP-2-W
GP-4
GP-5 115A NCAC
Sample Date
9/l/99
9/l/99
10/11/99
10/11/99 2L
Sample Depth (ft)
39
41
37
35
Units
µg/L
µg/L
µg/L
µg/L i µg/L
Trichloroethene
---
58
---
--- 2.8
bis(2-ethylhexyl)phthalate
---
35
---
--- I 3
Chloroform
---
---
24
9.6 0.19
Notes:
µg/L : micrograms per liter
15A NCAC 2L : Groundwater Quality Standards
99-750-Tables.xls

•
Jana,
Here arc the results for all of your samples. The other samples GP 9-6, GP 10-3, and GP
11-3 have also been included. GP 13-6, GP 12-3, and GP 16-3 contained matrix
interferences that made quantification impossible. Rough estimations of their quantities
have been included. Significant levels of Trichloroethene were found in GP 16-3, but the
exact value could not be quantified due to the matrix interferences.
Thanks,
Stacy Savage
Lab Director
S&ME, Inc.
905 East 69th Street
Savannah, Georgia 31405
[phone]
[phone] fox
www.smeinc.com
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VOLATILE ORGANICS ANALYSIS DATA SHEET
GP-6
Lab Name: S&ME Mobile GC/MS_ _ Client: S&ME _
Project No 99750 Analyst: SS _ Project: C_HARL Group: SME1 _
Matrix: (soil/water) WATER Lab Sample ID: 99750-12 _
Sample wt/vol: 5,0 (glmi) ML Lab File ID: VOCSAMP6.D
Level: (low/med) LOW Date Received: 10/11/2000 _
% Moisture: not dec. _ Date Analyzed: 10/23/20_0_0_
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume K) Soil Aliquot Volume: ^- (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71.8
Dichlorodifluoromethane
f 5
U
74-87-3
Chloromethane
5
U
75-01-4 _—Vinyl
Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-69-4
Trichtorofluoromethane
5
U
67-64-1
Acetone
50
U
75-35-4
11-Dichtoroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Methylene Chloride
25
U
1634-04-4
Meth d t-But I Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13-1
Ac lonitrile
50
U
156-60-5
trans-12-Dichtoroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
1.1-Dichloroethane
5
U
78-93-3
2-Butanone MEi{
25
U
156-59-4
cis-12-Dichloroethene
5
U
67-66-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Tdchloroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-06.2
1,2-Dichloroethane
5
U
71-43-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichioro ro ane
5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
Dibromomethane
5
U
108-10-1
4-Meth 1-2- entanone MIB
25
U
10061-01-5
cis-1 3-Dichloro ro ene
5
U
108.88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
127-18-4
124-48-1
106-93-4
100-41-4
112-Tdchloroethane
Tetrachloroethene
Dibromochloromethane
12-D1bromoethane
Eth (benzene J
5
5
5
5
5
U
U
U
U
U
FORM I VOA
North Carolina Laboratory Certification No. 594
Legend — U= Undetectable E=Outside Calibration Range
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS _
Project No 99750 Analyst: SS
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 _ _ (g/ml) M
Level: (low/med) LOW
% Moisture: not dec.
GC Column: VOCOL ID: 0.25 _ (mm)
Soil Extract Volume _ (uL)
.. ---
EPA SAMPLE NO,
GP-6
Client: S&ME
Project: CHARL Group: SME1
Lab Sample ID: 99750-12
Lab File ID: VOCSAMP6.0
Date Received: 10111/2000
Date Analyzed: 10/23/2000
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L p
108-90-7
Chlorobenzene
5
U
630-20-6
1112-Tetrachloroethane
5
U
106-42-3
m+ X lane
5
U
95-47-6
o-X lens
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1 1 2 2-Tetrachloroethane
5
U
96-18-4
1 2,3-Trichloro ro ane
5
U
110.57-6
t-14-Dichloro-2-butene
50
U
108-86.1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
1 3-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chloro ro ane
25
U
91-20-3
Naphthalene I5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
Legend - U= Undetectable E=Outside Calibration Range
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VOLATILE ORGANICS ANALYSIS DATA SHEET LGP-7
Lab Name: S&ME Mobile GC/MS Client: S&ME
Project No 99750 Analyst: SS _ Project: CHARL Group: S_ME1 _
Matrix: (soil/water) WATER Lab Sample ID: 99750-10
Sample wUvol: 5.0 (g/mi) ML Lab File ID: VOCSAMP7.1)
Level: (low/med) LOW Date Received: 10/11/2000 _
% Moisture: not dec. _ Date Analyzed: 10/23/2000
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume K) Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
75-71-8
Dichlorodifluoromethane
5
U
74-87-3
Chloromethane
5
U
75-01-4
_
Vin I Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroelhane
5
U
75-69-4
Trichlorofluoromethane
5
U
67-84-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Methylene Chloride
25
U
1634-04-4
—Methyl t-But I Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13-1
Acrylonitrile
50
U
156-60-5
1 trans-12-Dichloroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
1 11-Dichloroethane
5
U
78-93-3
2-Bulanone ME
25
U
156-59-4
cis-l2-Dichloroethene
5
U
67-66-3
i Chloroform
5
74-97-5
Bromochloromethane
5
U
71-55-6
111-Trichloroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
71-43-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichloro ro ane
I 5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
Dibromomethane
5
U
108-10-1
4-Meth I-2- entanone MIB
25
U
10061-01-5
cis-1 3-Dichloro ro ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ra pane
5
U
591-78-6
2-Hexanone
25
U
1 79-00-5
1 1 2-Trichloroethane
5
U
1 127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106-93-4
12-Dibromoethane
5
U
100-41-4
Eth (benzene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
Legend - U= Undetectable E=Outside Calibration Range
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VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS Client: S&ME _
Project No 99750 _ Analyst: SS Project: CHARL Group: S_M_E1__ _
Matrix: (soil/water) WATER _ Lab Sample ID: 99750-10
Sample wt/vol: 5_0 (g/ml) ML Lab File ID: VOCSAMP7.13
Level: (law/med) LOW Date Received: 10/1112000 _
% Moisture: not dec. _ Date Analyzed: 10/23/2_000
GC Column: VOCOL ID: 0.25 (nun) Dilution Factor: 1.0
Soil Extract Volume _ , - (uL) Soil Aliquot Volume: _ _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-90-7
630-20-6
Chlorobenzene
12-Tetrachloroethane
E
5
5
106-42-3
X lens
5
AU
95-47-6
o-X lene
5
100-42-5
75-25-2
79-34-5
St rene
Bromaform
1 1 2 2-Tetrachloroethane
1 5
5
U
U
96-18-4
1 2 3-Trichloro propane
5
U
110-57-8
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
106-46-7
13-Dichlorobenzene
14-Dichiorobenzene
5
5
U
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chloro ro ane
25
U
91-20-31.
Naphthalene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
Legend - U= Undetectable E=Outside Calibration Range
90' d ZTO. ON 00:8T OO. ZO AON 8Z88- SS-ZT6-T : QI
8260
HdNNUMS-ONI `3WIIS

WENVIRQNMENrAL -SERVICES
c:NGINEERING - rr%IYNG
1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Project No 99750 Analyst: SS
Matrix: (soil/water) WATER
Sample wt/vol: 5.0 (g/ml) ML
Level: (low/med) LOW
% Moisture: not dec.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume (uL)
EPA SAMPLE NO.
GP-8
Client: S&ME
Project: CHARL Group: SME1 _
Lab Sample ID: 99750-6 _
Lab File ID: VOCSAMP2.D__
Date Received: 10/3/2000
Date Analyzed: 10/4/2000 _
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L p
75-71-8 Dichlorodlftuorometh_a_ ne
5
U
74-87-3
Chioromethane
5
U
75-01-4
Vinyl Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-69-4
Trichlorofluoromethane
5
U
67-64-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Meth lene Chloride
25
U
1634-04-4
_Methyl t-But I Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13-1
Acrylonitrile
50
156-60.5
trans-l2-Dichloroethene
5108-OS-4
!IU,
cetate
25
75-34-3hloroethane
5
U
78-93-3none
ME
25
U
15&59-4Dichloroethene
5
U
67-66-3orm
1H1.a2-D,ch
g
J
74-97-5chloromethane
5
U
71-55-6dchloroethane
5
U
58-23-5
Tetrachloride
5
U
107-06-2hloroethane
5
U
71-43-2
Benzene
5
U
79-01-6
Trichloroethene
23
78-87-5
1 2-Dichlororo ane
5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
Dibromomethane
5
U
108-10-1
4-Meth I-2- entanone MIB
25
U
10061-01-5
cis-1 3-Dichloro roene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Tdchloroethane
5
U
127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106-93-4
12-Dibromoethane
5
U
100-41-4
Eth (benzene
5
U
FORM I VOA
North Carolina Laboratory Cerdlication No. 594
Legend — U= Undetectable E=Outside Calibration Range
Zo'd ZTo-oN To:8T OO,ZO AON 82-88-2S2-ZT6-T:QI
8260
HdNNUAHS-MI `3W'8S

NV
NEE--aEISA1S&ME Mobile GC/MS
Project No 99750 Analyst: SS
Matrix: (soilfwater) WATER
Sample wt/vol: 5.0 (g/ml) ML
Level: (low/med) LOW
% Moisture: not dec.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume (uL)
Client: S&ME
Project: CHARL Group: SME1
Lab Sample ID: 99750-6
Lab File ID: VOCSAMP2.D
Date Received: 10/3/2000
Date Analyzed: 10/4/2000
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L _ Q
108-90-7
Chlorobenzene
5
U
630-20-6
1112-Tetrachloroethane
5
U
106-42-3
m+ X lane
5
U
95-47-6
o-X lene
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1 1 2 2-Tetrachloroethane
5
U
98-18-4
1 2 3-Trichloro ro ane
5
U
110-57-6
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
-4-Chlorotoluene
5
U
541-73-1 1
13-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chloro ro ane
25
U
91-20-3
Naphthalene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
Legend — U= Undetectable E=Outside Calibration Range
80-d ZTO•ON TO:st OO.ZO AON $2-88-5�SS�-zi6-i:al
8260
HUNNHAUS-3N I ` 3W'8S

l NGINFERI ESrINO ES
f:NGIN FEI7ING - rEB TINC
1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Project No 99750 _ Analyst: S_ S_
Matrix: (soillwater) WATER
Sample wt/vol: 5_0 (g/ml) M
Level: (lowlmed) LOW
% Moisture: not dec.
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume __ (uL)
EPA SAMPLE NO.
L_n_�
E Client: S&M
Project: CHARL Group: SME1 _
Lab Sample ID: 99750-2
Lab File ID: VOCSAMPI.D
Date Received: 10/3/2000
Date Analyzed: 10/4/2000
Dilution Factor: 1.0
Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UGIL q
75-71-8
Dichlorodifluoromethane
5
U
74-87-3
_
Chloromethane
5
U
75-01-4 --Vinyl
Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-69-4
Trichlorofluoromethane
5
U
67-64-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Methylene Chloride
25
U
1634-04-4
Methyl t-But I Ether (MTBE_1
25
U
75-15-0
on Disulfide
50
U
107-13-1
onitrile
50
U
156-60-5
-l2-Dichloroethene
5
U
108-05-4
Acetate
02-Butanone
25
U
75-34-3
ichloroethane
5
U
78-93-3
ME
25
U
156-59-4
cis-12-Dichloroethene
5
U
67-66-3
Chloroform
5
74-97-5
Bromochloromethane
5
U
71-55-6
111-Tdchloroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
71-43-2
79-01-6
Benzene
Trichloroethene
5
5
U
U
78-87-5
1 2-Dichloro ro ane
5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
108-10-1
Dibromomethane
4-Meth I-2- entanone MIBIS
5
25
U
U
10081-01-5
cis-1 3-Dichloro ro ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Tdchloroethane
5
U
127-18-4 Tetrachloroethene
5
U
124-48-1 f Dibromochloromethane
5
U
106-93-4 12-Dibromoethane
5
5
U
U
100-41-4 Eth (benzene
FORM I VOA
North Carolina Laboratory Certification No. 594
Legend — U= Undetectable E-Outside Calibration Range
60'd �TO'oN M 8T OO,ZO AON 8Z88-5�S£-ZT6-T:GI
8260
HUNNHAHS-ONI `3M

�yy £NVrrtdNMEN rAI_ SE7 VIGe,S
V ENGINEERING - T9.SnNG
1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
GP-8
Lab Name: SBME Mobile GC/MS Client: SBME _
Project No 99750 —_ Analyst: SS_—_ Project: C_HARL Group: SME1_
Matrix: (soil/water) WATER _ Lab Sample ID: 99750-2
Sample wt/vol: 5.0 (g/ml) ML Lab File ID: VOCSAMP1.D_ —
Level. (low/med) LOW _ Date Received: 10/3/2000
% Moisture: not dec. _ Date Analyzed: 10/41200.0__
GC Column: VOCOL ID: 0_25 (mm) Dilution Factor: 1.0
Soil Extract Volume (uL) Soil Aliquot Volume _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
108-90-7
Chlorobenzene
5
U
630-20-6
1112-Tetrachloroethane
5
U
106-42-3
m+ X lene
5
U
95-47-6
o-X lene
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1,12 2-Tetrachloroethane
5
U
96-18-4
1,2 3-Trichloro ro ane
5
U
110-57-6
1 t-14-Dichloro-2-butens
50
U
108-86.1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
13-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chloro ra ane
25
U
91-20-3
Naphthalene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
'Legend — U- Undetectable E=Outside Calibration Range
OT"d ZTO'ON 20:8T OO,ZO AON 8Z88-£S£-ZT6-T:QI
8260
HUNNUMS-ONI `3W'$S

V :;�,V7,1EER1 i-Z - 371v�-
1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS Client: S&ME L
GP-10
Project No 99750 Analyst: SS Project: CHARL Group: SME1
Matrix: (soil/water) WATER Lab Sample 10: 99750-8 _
Sample wt/vol: 5.0 (g/ml) ML Lab File ID: VOCSMP10.D _
Level: (low/med) LOW Date Received: 10/11/2000
% Moisture: not dec. _ _ Date Analyzed: 10/27/2000
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0 _
Soil Extract Volume _^- (uL) Soil Aliquot Volume: - — (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q
J_ 75-71-8
Dichlorodifluoromethane
5
U
' 74-87-3
Chloromethane
5
U
75-01-4
Vinyl Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroeihane
5
U
75-69-4
Trichlorofluoromethane
5
U
67-64-1
1 Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
i 75-09-2
Methylene Chloride
25
U
1634-04-4
Methyl t-But I Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13-1
Acrylonitrile
50
U
156-66-5
trans-i 2-Dichloroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
11-Dichloroethane
5
U
78-93-3
2-Butanone ME
25
U
156-59-4
cis-12-Dichloroethene
5
U
67-66-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Trichloroethane
5
U
58-23-5
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
71-43-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichloro roane
5
U
75-27-4
Bromodichloromethane
5
U
74-05-3
Dibromomethane
5
U
108-10-1
4-Meth I-2- entanone MIB
25
U
10061-01-5
cis-1 3-Dichioro ro ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichlororo ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Trichloroelhane
5
U
127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106-93-4
12-Dibromoethane
5
U
100-41-4
Eth lbenzene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
8260
Legend - U= Undetectable E=Outside Calibration Range
Ti•d LTO•oN b0:8l 00,N AON sZs8-.2s2-zT6-i:al
HUNNIJAUS-ZINI `3M

S&ME Mobile GC/MS up-lo
Project No 99750 Analyst: SS Project: CHARL Group: SME1
Matrix: (soil/water) WATER_ Lab Sample ID: 99750-8 _
Sample wt/vol: 5.0 (g/ml) ML Lab File ID: VOC_SMP10_.D
Level: (low/med) LOW Date Received: 10/11/2000 _
% Moisture: not dec. _ _ Date Analyzed: 10/27/2000 _
GC Column: VOCOL 10: 0.25 (mm) Dilution Factor. 1.0 _
Soil Extract Volume (uL) Soil Aliquot Volume: — (uL)'
CONCENTRATION UNITS:
CAS NO, COMPOUND (ug/L or ug/Kg) UG/L q
FORM I VOA 8260
North Carolina Laboratory Certification No. 594
Legend - U= Undetectable E=Outside Calibration Range
ZT'd ZTO'oN SO:ST OO,ZO OON 8Z8$-2S2-ZT6-T:QI
HUNNUMS-ONI `3W'8S

ME, INC-SAVANNAH ID:1-912-353-8878 OCT 31'00 14:14 No.007 P.02
1A
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME
Mobile GC/MS
Client: S&ME
GP 6-3
-- Project No 99750
Analyst: SS
Project: CHARL Group: SM_E7_
Matrix: (soil/water)
SOIL _
Lab Sample ID:
99750-11
Sample wt/vol:
5.0 _ (g/ml) G
Lab File ID:
VOCSAM28.13_
Level: (low(med)
LOW
Date Received:
10/9/2000_
Moisture: not dec.
0 _
Date Analyzed:
1_0/26/2000
GC Column: VOCOL _ ID: 0.25 (mm)
Dilution Factor:
_
1.0
Soil Extract Volume
__ (uL)
Soil Aliquot Volume:
_
(uL)
CONCENTRATION UNITS:
CAS NO.
75-71-8
COMPOUND
1
(ug/L or ug/Kg) UG/KG
_ Q
n
n
FORM I VOA 8260

S&ME
r^IP I
-'I
"7
INC-SAVANNAH ID:1-912-353-8878 OCT 31'00 14:15 No.007 P.03
1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET j
b Name: S&ME Mobile GC/MS Client: S&ME GP 6-3
oject No 99750 Analyst: SS _ Project: CHARL Group: SME1 _
itrix: (soil/water) SOIL Lab Sample ID: 99750-11
mple wt/vol: 5.0 _ (g/ml) G Lab File ID: VOCSAM2B.D
vel: (low/med) LOW Date Received: 10/9/2000
Moisture: not dec. 0 Date Analyzed: 10/26/2000
Column: VOCOL _ ID: 0.25 (mm) Dilution Factor: 1.0
it Extract Volume _ (uL) Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
FORM I VOA 8260

S&ME, INC-SAVANNAH ID:1-912-353-8878 OCT 31'00 14:16 N0.007 P.04
1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
GP-7-3
Lab Name: S&ME Mobile GC/MS Client: S&ME
Project No 99750 Analyst: SS Project: CHARL Group: SME1 _
Matrix: (soil/water) SOIL Lab Sample ID: 99750-9
Sample wt/vol: 5.0 (g/ml) G Lab File ID: VOCSAMI .D
Level: (1ow/med) LOW Date Received: 10/11/2000 _
% Moisture: not dec. 0 Date Analyzed: 10/26/2000
GC Column: VOCOL_ ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume (uL) Soil Aliquot Volume: - (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8
Dichlorodifluoromethane
5
U 1
74-87-3_
Chloromethane
5
U
75-01-4
Vinyl Chloride
5
U
74-83-9
Bromomethane
5
U 1
75-00-3
Chloroethane
5
U
75-69-4
Trichlorofluoromethane
5
U 1
67-64-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
1 Methylene Chloride
25
U
1634-04-4
Meth I 1-gut i Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13-1
Ac lonitrile
50
U
156-60-5
trans-12-Dichloroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
1.1-Dichloroethane
5
U
78-93-3
2-Butanone ME
25
U
156-59-4
cis-12-Dichloroethene
5
U
67-66-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Trichloroethane
5
U
56-23-5
Canyon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
71-43-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichiara ro ane
5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
Dibromomethane
5
U
108-10-1
4-Meth I-2- entanone MIBK
25
U
10061-01-5
cls-1 3-Dichloro ro ene
5
U
106-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichlororo ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Tdchloroethane
5
U
127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106-93-4
12-Dibromoethane
5
U
100-41-4
Eth (benzene
5
U
FORM I VOA 8260

S&ME, INC-SAVANNAH ID:1-912-353-8878 OCT 31'00 14:17 No.007 P.05
1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET OP-7-3
Lab Name: S&ME Mobile GC/MS Client: S&ME
Project No 99750 Analyst: SS — Project: CHARL Group: SME1_
Matrix: (soil/water) SOIL Lab Sample ID: 99750-9
G Lab File ID: VOCSAM1.D
Sample wt/vol: _5.0 (9/ml ) _. -- --
Level: (low/med) LOW Date Received: 10/11/2000
% Moisture: not dec. 0 Date Analyzed: 10/26/2000
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume K) Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG _ Q
FORM I VOA
8260

P EEi71�0�TI /4
1A EPA SAMPLE NO,
VOLATILE ORGANICS ANALYSIS DATA SHEET
•
Lab Name: SSME Mobile GC/MS
Client: GP8-6
S8M_E___
Project No 99750_ - Analyst: SS_
Project: CH_ARL Group: SME1_
Matrix: (soil/water) SOIL _
Lab Sample ID: 99750-5
Sample wt/vol: 5.0 (g/ml) G
Lab File ID: VOCSAMP4.0
Level: (low/med) LOW _
Date Received: 10/3/2000
% Moisture: not dec. 0 _ _
_
Dale Analyzed: 10/3/2000
GC Column: VOCOL_ ID: 0.25 (mm)
Dilution Factor: 1.0
Soil Extract Volume __ (uL)
Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG p
75-71-8 Dichlorodifluoromethane 5
T U
74-87-3 Chloromethane 5
U
_
75-01-4 Vin i Chloride
5
U
74-83-9 Bromomethane
5
U
Chloroethane
5
U
175-00-3
75-69-4 Trichlorofluoromethane
5
U
67-64-1 Acetone
50
U
75-35-4 11-Dichloroethene
5
U
74-88-4 lodomethane
25
U
75-09-2 Methylene Chloride
25
U
1634-04-4 -Methyl t-But I Ether MTBE
25
U
75-15-0 Carbon Disulfide
50
U
107-13-1 Acrylonitrile
50
U
156-60-5 trans 1 2-Dichloroethene
5
U
108-05-4 Vinyl Acetate
25
U
75-34-3 11-Dichloroethane
5
U
78-93-3 2-Butanone ME
25
U
156-59-4 cis-12-Dichloroethene
5
U
67-66-3 Chloroform
5
U
74-97-5 Bromochloromethane
5
U
71-55-6 111-Trichloroethane
5
U
56-23-5 Carbon Tetrachloride
5
U
107-06-2 12-Dichloroethane
5
U
71-43-2 Benzene
5
U
79-01-6 Trichloroethene
5
U
78-87-5 1 2-Dichlororo ane
5
U
75-27-4 Bromodichloromethane
5
U
74-95-3 Dibromomethane
5
U
108-10-1 4-Meth I-2- entanone MIB
25
U
10061-01-5 cis-1 3-Dichloro ro ene
108-88-3 Toluene
5
5
U
U
10061-02-6 trans-1 3-Dichlororo ene
5
U
591-78.6 2-Hexanone
79-00-5 112-Trichloroethane
127-18-4 Tetrachlaroethene
124-48-1 Dibrornochloromethane
106-93.4 12-Dibromoethane
25
5
5
5
5
U
U
U
U
U
100-41-4 Eth {benzene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
8260
Legend — U= Undetectable E=Outside Calibration Range
S�T'd 2-TO'oN SO:8T OO,ZO AON 8Z88-2S2—ZT6—T:QI
HdNNUMS-ONI ° 3W'8S

? V VIR ON MF.N 7AL S Kli VIC �'
:VGINF F_RINi. • TESTING 1A
VOLATILE ORGANICS ANAL
Lab Name: S&ME Mobile GC/MS
Project No 99750 __ Analyst: SS
Matrix: (soil/Water) SOIL
Sample wt/vol: 5_0 (g/ml) G
Level: (low/med) LOW
% Moisture: not dec. 0 —
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume _ _ (uL)
YSIS
EPA SAMPLE NO.
DATA SHEET
GP8-6
Client: S&ME
Project: CHARL Group:
SME1
Lab Sample ID:
99750-5
Lab File ID:
VOCSAMP4 _D
Date Received:
10/3/2000
Date Analyzed:
10/3/2000
Dilution Factor:
1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG p
108-90-7
Chlorobenzene
5
U
630-20-6
1 1 1 2-Tetrachloroethans
5
U
106-42-3
_
m+ X lene
5
U
95-47-6
o-X lene
5
U
10042-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
i 1 1 2 2-Tetrachloroethane
5
U
96-184
1.2 3-Trichlororo ane
5
U
110-57-6
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
13-Dichlorobenzene
5
U
10e-46-7
1 4-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chloro roane
25
U
91-20-3
Na hthalene
5
U
FORMIVOA
North Carolina Laboratory Certifleation No. 594
8260
Legend — U= Undetectable E=Outside Calibration Range
trT ' d ZT0' oN 90:8T 00, U f10N U88-5�Si-7,U-T : GI
HUNNUAUS-0NI ` 3W'8S

r� S&ME Mobile GC/MS
FNViIiONMFN
VVV LNCINEERINQ g,1
Project No 99750 _ Analyst: SS
Matrix: (soiUwater) SOIL
Sample wt/vol: 5.0 _ (g/ml) G _
Level: (low/med) LOW
% Moisture. not dec. 0
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume (uQ
GP9-6
Client: S&ME
-
Project: CHARL Group:
SME1
Lab Sample ID:
99750-1 _
Lab File ID:
VOCSAMP1.0___
Date Received:
10/3/2000
Date Analyzed:
10/3/2000
Dilution Factor.
1.0
Soil Aliquot Volume: _ (uL),
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8
1 Dichlorodifluorometh_an_ e
5
5
U
U
74-87-3
Chloromethane
75-01-4
Vinyl Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-69-4
Trichlorofluoromethane
5
U
87-64-1
Acetone
50
U
75-35-4
1 1-Dichloroethene
5
U
74-88-4
lodomethane
_
25
U
75-09-2
Methylene Chloride
25
U
1634-04-4
Methyl t-Butyl Ether MTBE
25
U
75-15-0
1 Carbon Disulfide
50
U
107-13-1
Acrylonitrile
50
U
156-60-5
trans-12-Dichloroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
11-Dichloroethane
5
U
78-93-3
2-Butanone ME
25
U
156-594
cis-12-Dichloroethene
5
U
67-66-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Trichloroethane
5
U
58-23-5 i
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
71-43-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichloro ro ane
5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
Dibromomethane
g
U
108-10-1
4-Methyl -entanone MIB
25
U
10061.01-5
cis-1 3-Dichloro roene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Trichloroethane
5
U
127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106.93-4
12-Dibromosthane
5
U
100-41-4
Eth ibenzene
5
U
North Carolina Laboratory Certification No. 594
FORM I VOA
8260
Legend - U= Undetectable
E=Outside Calibration Range
ST'd ZTO'oN Z0:8T OO,ZO AON 8Z88-2S2-ZT6-T:GI HdNNHAUS-ONI °3W'8S

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ENGINEERING
SA• L ''�-s rime; F.S
1A EPA SAMPLE NO,
VOLATILE ORGANICS ANALYSIS DATA SHEET
GP9-6
Lab Name: S&ME Mobile GC/MS Client: S&ME
Project No 99750 Analyst: SS _ Project: CHARL Group: SME1
Matrix: (soil/water) SOIL Lab Sample ID: 99750-1 _
Sample wi/vol: 5.0 (g/ml) G Lab File ID: VOCSAMPI .D
Level: (low/med) LOW Date Received: 10/3/2000
% Moisture: not dec. 0 _ Date Analyzed: 10/3/2000
GC Column: VOCOL _ ID: 0.25 (mm) Dilution Factor: 1.0�`_ `
Soil Extract Volume —_ (uQ Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG p
108-90-7
Chlorobenzene
5
U
630-20-6
1112-Tetrachloroethane
5
U
106-42-3
m+ X Iene
5
U
95-47-6
o-X lene
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1 1 2 2-Tetrachloroethane
5
U
96-18-4
1 2 3-Tdchloro ro ane
5
U
110-57-6
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
108-43-4 ' 4-Chlorotoluene
5
U
' 641-73-1 13-Dichlorobenzene
5
U
106-46-7 14-Dichlorobenzene
5
U
95-50-1 12-Dichlorobenzene
5
96-12-8 1 2-Dibromo-3-chloro ro ane
25
E
91-20-3 Na hthalene
5
U
,North Carolina Laboratory Certification No. 594
FORM I VOA
8260
Legend — U= Undetectable
E=Oufside Calibration Range
9T'd LTO'oN 80:8T 00,ZO AON 82-88-2S2-ZT6-T:QI HdNNUAHS-ONI `3W'8S

`} ENV/RGNMEN �- SERVICES
v CNGINECRING - rrSTING
1A
EPA SAMPLE NO,
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: SBME Mobile GC/MS
Client: S_&ME
GP14-3
Project No 99750
Analyst: SS
_ Project: CHARL_ Group: S_ME1
Matrix: (soil/wateO
SOIL
Lab Sample ID:
_
99750-4
Sample wt/vol:
5,0 (g/ml) G
_ Lab File ID:
_
VOCSAMP3.13_
Level: (low/med)
LOW _
Date Received:
10/3/2000
Moisture: not dec.
0 _
Date Analyzed:
10/3/2000
Y`
GC Column: VOCOL_ ID: 0.25 (mm)
Dilution Factor:
1.0
Soil Extract Volume
_- (uL)
_
Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8
Dichlorodifluoromethane
U —III
74-87-3
Chloromethane
5
r U
75-01-4
Vinyl Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-69-4
Trichlorofluoromethane
5
U
67-64-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Methylene Chloride
25
U
1634-04-4
1 Methyl t-Butyl Ether MTBE
25
U
i 75-15-0
1 Carbon Disulfide
50
U
107-13-1
Acrylonitrile
50
U
i 58-60-5
trans-1 2-Dichloroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
11-Dichloroethane
5
U
78-93-3
2-Butanone ME
6
J
156-59-4
cis-12-Dichloroelhene
5
U
67-66-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Trichloroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
3 71-43-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichloro ro ane
5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
Dibromomethane
5
U
108-10-1
4-Meth I-2- entanone MlB
25
U
10061-01-5
cis-1 3-Dichloro ra ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1,3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
.112-Trichloroethane
5
U
127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106-93-4
12-Dibromoethane
5
U
100-41-4
Eth (benzene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
I.egend - U- Undetectable E=Outside Calibration Range
ZT'd ZTO.ON 80:8T 00,ZO 6ON 8Z$8-�S£-ZT6-T:QI
8260
HUNNUAUS—DNI `3WIS

M� wa
6NVI RICNMEN IAl gNCINC-STING
ERIN6 - -riiNC
1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: SBME Mobile GC/MS
Project No 99750 Analyst: S_ S
Matrix: (soil/water) SOIL
Sample wt/vol: 6.0 _ (g/ml) G
Level: (low/med) LOW
% Moisture: not dec. 0
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume (uL)
EPA SAMPLE NO.
GP14-3
Client: SBME
Project: CHARL Group: SME1
Lab Sample ID: 99750-4 _
_ Lab File ID: VOCSAMP3.D_
Date Received: 10/3/2000
Date Analyzed: 10/3/2000
Dilution Factor: 1.0
Soil Aliquot Volume: _ _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG q
108.90-7
Chlorobenzene
5
U
630-20-6
1112-Tetrachloroethane
5
U
106-42-3
m+ X lene
5
U
95-47-6
o-X l sne
5
U
100-42-6
5
U
75-25-2
orm
5
U
79-34-5
96-18-4
Teirachloroethane
ichloro ro one
5
5
U
U
110-57-6
chloro-2-butene
24-Chlorotoluene
50
U
108-86-1
enzene
5
U
106-43-4
toluene
5
U
541-73-1
lorobenzene
5
U
106-46-7
95-50-1
lorobenzene
1.2-Dichlorobenzene
5
5
U
U
96-12-8
1 2-Dibromo-3-chloro ra ne
25
U
91-20-3 Naphthalene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
8260
Legend — U— Undetectable E—Outside Calibration Range
81 ' d ZTO' oN 60: 8T OO, ZO (1ON 8ZH-S�S�-ZZ6-T : QI
HUNNUMS-ONI `3W'8S

S5
ri'S TINGi
"�
1A
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Client: S&ME
GP1 ti-6
Project No 99750
_ ; Analyst: SS
Project: CHARL Group:
SME1
Matrix: (soil/water)
SOIL
Lab Sample ID:
99750-3 _
Sample wt/vol:
5.0 (g/ml) G
Lab File ID:
VOCSAMP2.13
Level: (low/mad)
LOW
Date Received:
10/3/2000
% Moisture: not dec.
0 _
Date Analyzed:
10/3/2000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor.
1.0
Soil Extract Volume
_ (ul-)
Soil Aliquot Volume: (uQ
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8
Dichlorodifluoromethane f
5
U
74-87-3
Chloromethane
5
U
75-01-4
Vinyl Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-69-4
Trichlorofluoromethane
5
U
67-84-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
175-09-2
Methylene Chloride
25
U
1e34-04-4
Meth I t-Butyl Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13-1
Ac lonitrile
50
U
156-60-5
trans-12-Dichloroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
11-131chloroethene
5
U
78-93-3
2-Butanone MEK
25
U
156-59-4
cis-l2-Dichloroethene
5
U
67-e8-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-e
111-Trichloroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
71-43-2
Benzene
5
U
79-01-8 1
Trichooroethene
5
U
78-87-5
1 2-Dichloro ro ane
5
U
75-27-4
Bromodichloromethane
5
U
74-95-3
Dibromomethane
5
U
108-10-1
4-Meth I-2- entanone MIB
25
U
10061-01-5
cis-1 3-Dichloro ro ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Trichloroethane
5
U
127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106-93-4 1
12-Dibromoethene
5
U
100-41-4
Eth Ibenzene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
8260
Legend — U= Undetectable E=Outside Calibration Range
6T' d ZTO' oN OT: 8T 00, �O AON 82-88-<M-ZT6-T : QI
HdNNUAUS-ONI `3M

1 A
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Client: SAME
Project No 99750
_ Analyst: SS
Project: C_H_ARL Group:
SME1
Matrix: (soil/water)
SOIL
Lab Sample ID:
99750-3 _
Sample wUvol:
5.0 (g/ml) G
_ Lab File ID:
VOCSAMP2.0
Level: (low/med)
LOW
Date Received:
10/3/2000
% Moisture: not dec.
0� —
Date Analyzed:
10/3/2000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor:
1.0
Soil Extract Volume
_ (ul-)
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
i 108-90-7
1 Chlorobenzene
5
U
630-20.6
1112-Tetrachloroethane
5
U
108.42.3
m+ X lene
5
U
95-47-6
o-X lens
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1 1 2 2-Tetrachloroethane
5
U
96-18-4
1 2 3-Trichloro ro ane
5
U
110-57-6
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
13-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
9e-12-8
1 2-Dibromo-3-chlororo one
25
U
91-20-3
Naphthalene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
8260
Legend — U= Undetectable E=Outside Calibration Range
OZ'd ZTO-aN TT:8T OO,ZO ACIN 8ZH-S�S�-ZT6-T:QI
HdNNUAUS-ONI `3M

raw �r W a
r7NVIRONMENrnt. f:RVICE6 1A
EN6INEERINC - rF.STINC
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: SBME Mobile GC/MS
Client: SBME
GP 16-3
Project No 99750 _ Analyst: SS
Project: CHARL Group:
SME1
Matrix: (saillwater) SOIL
Lab Sample ID:
99750-16 —_
Sample wt/vol: 5.0 (g/ml) G _
_ Lab File ID:
VOCSAM3X.D
Level: (low/med) LOW
Date Received:
10/2/2000
% Moisture: not dec. - 0
Date Analyzed:
10/26/2000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor:
1.0
Soil Extract Volume _ (uL)
Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG to
75-71-8
Dichlorodifluoromethane
5 U
74-87-3
Chloromethane
5 U
75-01-4
Vinyl Chloride
5 U
74-83-9
Bromomethane
5 U
75-00-3
Chloroethane
5 U
75-69-4
Tdchlorofiuoromethane
5 U
67-64-1
Acetone
50 U
75-35-4
11-Dichloroethene
5 U
74-88-4
lodomethane
25 U
75-09-2
Methylene Chloride
25 U
1634-04-4
Methyl t-But I Ether MTBE
25 U
75-15-0
i Carbon Disulfide
50 U
107-13-1
Acrylonitrile
50 U
156-60-5
trans-12-Dichloroethene
5 U
108-05-4
Vinyl Acetate
25 U
75-34-3
11-Dichloroethane
5 U
78-93-3
2-Butanone ME
25 U
156-59-4
cis-12-Dichloroethene
5 U
67-66-3
Chloroform
5 U
74-97-5
Bromochloromethane
5 U
71-55-6
111-Trichloroethane
5 U
56-23-5
Carbon Tetrachloride
5 U
107-06-2
12-Dichloroethane
5 U
71-43-2
Benzene
5 U
79-01-6
Trichloroethene
5400 E
78-87-5
1 2-Dichloro roane
5 U
75-27-4
Bromodichloromethene
5 U
74-95-3
Dibromomethane
5 U
108-10.1
4-Meth i-2- entanone M1B
25 U
10061-01-5
cis-1 3-Dichlororo ene
5 U
108-88-3
Toluene
5 U
10061-02-6
trans-1 3-Dichloro ro ene
5 U
591-78-6
2-Hexanone
25 U
79-00-5
112-Trichloroethane
5 U
127-18-4
Tetrachloroethene
5 U
124-48-1
Dibromochloromethane
5 U
106-93-4
12-Dibromoethane
5 U
j 100-41-4
Eth (benzene
5 U
FORMiVOA
,North Carolina Laboratory Certification No. 594
8260
Legend — U— Undetectable E=Outside Calibration Range
TZ'd ZTO'oN TT:8T OO,ZO AON 8Z88-!2S2-ZT6-1:QI
HUNNMUS-ONI ` 3M

v �NCIN EER- c- A�1 N��
1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
--
Client: S&ME
L=—J
Project No 99750
_ Analyst: SS
_ _
Project: CHARL_ Group: S_M_E1__
Matrix: (soil/water)
SOIL
Lab Sample ID:
_
99750-16
Sample wt/vol:
5.0 _- (g/ml) G
_ Lab File ID:
VOCS_AM3X.D
Level: (low/med)
LOW,Date
Received:
10/2/2000�
% Moisture: not dec.
0 _
Date Analyzed:
10/28/2000
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume _ _V (uL) Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
FORM I VOA 8260
North Carolina Laboratory Certification No. 594
Legend - U- Undetectable E-Outside Calibration Range
ZZ'd ZTO'ON ZT:8T 00,ZO ACIN 8z88-M-ZT6-T:GI
HdNN08S-ONI ' 3W'8S

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1 A
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME
Mobile GC/MS
Client: S&ME
GP 13-6
Project No 99750
Analyst: SS _
Project: CHARL Group;
SME1
Matrix: (soil/water)
SOIL
Lab Sample ID:
90750-13
Sample wt/vol:
5.0 (g/ml) G
Lab File ID:
VOCSAMP3.D
Level: (low/med)
LOW
Date Received:
10/11/2000
% Moisture: not dec.
0
Date Analyzed:
1012612000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor.
1.0
Soil Extract Volume
_- (uL)
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
75-71-8
Dichlorodifluoromethane
5
U
74-87-3
Chloromethane
5
U
75-01-4
Vin I Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-89-4
Trichlorofluoromethane
5
U
67-64-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Methylene Chloride
25
U
1634-04-4
Methyl t-Butyl Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13.1
Acrvionftdle
50
U
156-60-5
trans-12-Dichloroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
11-Dichloroethane
5
U
78-93-3
2-Butanone ME
25
U
156-59-4
cis-12-Dichloroethene
5
U
67-86-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Tdchicroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
71-43-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichloro ro pane
5
U
75-27-4
Bromodichloromethene
5
U
74-95-3
Dibromomethane
5
U
108-10-1
4-Meth I-2- entanone MIB
25
U
10061-01-5
cis-1 3-Dichloro ro ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Trichloroethane
5
U
127-18-4
Tetrachloroethene
5
U
124-48.1
Dibromochloramethane
5
U
106-934
12-Dibromoethane
5
U
100-41-4
Eth ibenzene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
8260
Legend — U= Undetectable E=Outside Calibration Range
2Z'cl �-TO'oN 2T:8T 00,ZO AON 8)88-2S£—ZT6-1:QI
HUNNHAUS—ONI `3W'8S

FNGINEERINGTA L.11YiRAlIG: S&ME Mobile GC/MS
Project No 99750 Analyst: SS
Matrix: (soiltwater) SOIL
Sample wt/vol: 5.0 - (g/ml) G
Level: (low/med) LOW
% Moisture: not dec. 0
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume (uL)
CAS NO. COMPOUND
Client: S&ME
Project: CHARL Group: SME1
Lab Sample ID: 99750-13
Lab File ID: VOCSAMP3.1)
Date Received: 10/11/2000
Date Analyzed: 10/26/2000
Dilution Factor: 1.0
Soil Aliquot Volume: (uL)-
CONCENTRATION UNITS:
(ug/L or ug/Kg) UG/KG Q
108-90-7
Chlorobenzene
5
f` U
830-20-6
1112-Tetrachloroethane
5
LU
106-42-3
m+ X lene
5
U I
95-47-6
o-X lene
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1 1 2 2-Tetrachloroethane
5
U
96-18-4
1 2 3-Tdchloro ro ane
5
U
110-57-6
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73.1
13-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
1 2-Dichlorobenzene
5
U
98-12-8
1 2-Dibromo-3-chloro ra ane
25
U
91-20-3
Naphthalene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
8260
Legend - U= Undetectable E=Outside Calibration Range
trZ'd ZTO'ON VT:8T OO,ZO AON 8Z88-£S2-ZT6-T:QI
HUNNUAUS-ONI `3W'8S

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FW0P lrER1*4r, ' r`"rlHc
1A
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Client: S&ME
GP 12-3
Project No 99750
Analyst: SS
Project: CHARL Group: SME_1
Matrix: (soiltwater)
SOIL
Lab Sample ID: 99750-14 _
Sample wt/vol:
5.0 (g/mI) G
Lab File ID: VOCSAMP4.13
Level: (low/med)
LOW
Date Received: 10/11/2000
% Moisture: not dec.
0
Date Analyzed: 10/26/2000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor: 1.0
Soil Extract Volume
(uL)
Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG q
75-71-8
Dichlorodifiuoromethane
5
U
74-87-3
Chloromethane
5
U
75-01-4
Vinyl Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
Chloroethane
5
U
75-69-4
Trichlorofluoromethane
5
U
67-64-1
Acetone
50
U
75-35-4
11-Dichioroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Methylene Chloride
25
U
1634-04-4
Meth I t-But l Ether MTBE
25
U
75-15-0
Carbon Disulfide
50
U
107-13-1
Ac lonitrile
50
U
156-60-5
trans-12-Dichioroethene
5
U
108-05-4
Vinyl Acetate
25
U
75-34-3
11-Oichloroethane
5
U
78-93-3
2-Butanone ME
25
U
156-59-4
cis-12-Dichioroethene
5
U
67-66-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Trichloroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-08-2
12-Dichloroethane
5
U
71-43-2
.Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
1 2-Dichloro ro ane
5
U
75-274
Bromodichloromethane
5
U
74-95-3
Dibromomethane
5
U
108-10.1
4-Meth I-2- entanone MIBK
25
U
10081-01-5
cis-1 3-Dichloro ro ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-8
2-Hexanone
25
U
79-00-5
112-Trichloroethane
5
U
127-18-4
Tetrachloroethene
5
U
12448-1
Dibromochloromethane
5
1 U
106-93-4
12-Oibromoethane
5
U
100-41-4
Eth (benzene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
8260
Legend — U= Undetectable E--Outside CaUbration Range
SZ'd ZTO'oN VT:8T OO,ZO AON 82-88-5�Si—ZT6—T.III
HUNNUAUS-3NI ` 3M

Y ..NGINKFR F_�Es
NG - �sTINc1A EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
GP 12-3
Lab Name: S&ME Mobile GC/MS
Client: S&ME
Project No 99750 Analyst: SS
Project: CHARL Group: SME1 _
Matrix: (soil/water) SOIL
Lab Sample ID: 99750-14 _
Sample wt/vol: 5.0 (g/ml) G
Lab File ID: VO_C_SAMP4.D_
Level: (low/med) LOW
Date Received: 10111/2000
% Moisture: not dec. 0
Date Analyzed: 10/26/2000~
GC Column: VOCOL - ID: 0.25 (mm)
Dilution Factor: 1.0
Soil Extract Volume __ (uQ
Soll Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-90-7
Chiorobenzene
5
U
630-20-6
1112-Tetra-chloroathane
5
U
106-42-3
m+ X lene
5
U
95-47-6
o-X lens
5
U
100-42-5
Styrene
5
U
U
75-25-2
Bromoform
5
79-34-5
1 1 2 2-Tetrachloroethane
5
U
96-18-4
1 2 3-Trichloro ro ane
5El
U
110-57-6
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
13-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chloro ro pane
25
U
91-20-3
Na hthalene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
8260
Legend - U- Undetectable E-Outside Calibration Range
9Z'd zTO'ON SZ:8I 00,N (10N 8188-2S2-ZI6-I.QI
HUNNUMS-DNI ` 3M

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V GNGINEE RINi - GCS TINO
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EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: SBME
Mobile GC/MS —
Client: S&ME
G P9-6
-
Project No 99750
_ Analyst: SS
Project: CHARL Group:
SME1
Matrix: (soll/water)
SOIL
Lab Sample ID:
_
99750-1
Sample wt/vol:
5.0 (g/ml) G
Lab File ID:
_
VOCSAMPI.D
Level: (low/med)
LOW
Date Received:
10/3/2000
% Moisture: not dec.
0_
Date Analyzed:
10/3/2000
GC Column: VOCOL ID: 0_25 (mm)
Dilution Factor:
1.0
Soil Extract Volume
(uL)
_
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG p
75-71-9 Dichlorodifluoromethane
5
U
74-87-3 Chloromethane
5
U
75-01-4 Vinyl Chloride
5
U
74-83-9 Bromomethane
5
U
75-00-3 Chloroethane
5
U
75-69-4 Tdchlorofluoromethane
5
U
67-64-1 Acetone
50
U
75-35-4 11-Dichloroethene
5
U
74-88-4 lodomethane
25
U
75-09-2 Meth lene Chloride
25
U
1634-04-4 Methyl Butyl Ether MTBE
25
U
75-15-0 Carbon Disulfide
50
U
107-13.1 Acrylonithle
50
U
156-60-5 trans-12-Dichloroethene
5
U
1 oa-05-4 Vinyl Acetate
25
U
75-34-3 11-Dichloroethene
5
U
78-93-3 2-Butanone ME
25
U
156-59-4 cis-l2-Dichloroethene
5
U
67-66-3 Chloroform
5
U
74-97-5 Bromochloromethane
5
U
71-55.6 111-Trichlomethene
5
U
56-23-5 Carbon Tetrachloride
5
U
107-06-2 12-Dichloroethane
5
U
71-43-2 Benzene
5
U
79-01-6 Tdchloroethene
5
U
78-87-5 1 2-Dichioro ro ane
5
U
75-27-4 Bromodichloromethane
5
U
74-95-3 Dibromomethane
5
U
108-10-1 4-Meth I-2- entanone MIB
25
U
10081-01-5 cis-1 3-Dichloro ro pene
5
U
108-88-3 Toluene
5
U
10061-02-6 trans-1 3-Dichlo ro ene
5
U
591-78-6 2-Hexanone
25
U
79-00-5 112-Trichloroethane
5
U
127-18-4 Tetrachloroethene
5
U
124-48-1 Dibromochloromethane
5
U
106-93-4 12-Dibromoethane
5
U
100-41-4 Eth (benzene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
8260
Legend - U= Undetectable E=Outside Calibration Range
zZ'd ZTO'oN 9T:8T OO,ZO AON 8Z88-£S2-ZT6-T:GI
HUNNUMS-ONI ` 3M

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V VINONMEN CAI. SERVICES
V4'INE[N�NG - IF -STING
1A
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: SBME Mobile GC/MS
Project No 99750 Analyst: SE
Matrix: (soil/water) SOIL
Sample wt/vol: 5.0 (g/ml) G
Level: (low/mad) LOW
% Moisture: not dec. 0
GC Column: VOCOL ID: 0.25 (mm)
Soil Extract Volume _ (uL)
EPA SAMPLE NO.
GP9-6
Client: SBME
Project: CHARL Group: SME1
Lab Sample ID: 99750-1
Lab File ID: VOCSAMPI.D
Date Received: 10/3/2000
Date Analyzed: 10/3/2000
Dilution Factor. 1.0
Soil Aliquot Volume: (uL)
CONCENTRATION UNITS.
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-90-7
Chlorobenzene
5
U
630-20-6
1.112-Tetrachloroethane
5
U
1 M42-3
m+ X lene
5
U
95-47-6
o-X lane
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1 1 2 2-Tetrachloroethane
5
U
96-18-4
1 2 3-Trichloro ro ane
5
U
110-57-6
t-14-Dichlora2-butene
50
U
106-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
13-Oichlorobenzene
5
U
106-46-7
14-Dlchlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chlororo ane
25
U
91-20-3
Na hthalene
5
1 U
FORMIVOA
North Carolina Laboratory Certification No. 594
8260
Legend — U= Undetectable E=Outside Calibration Range
27'd ZT0-oN 2T:8T OO,ZO hON U88-5�Si—ZT6—T:9I
HUNNUAUS—ONI ` 3WIS

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VV�NCINEERNG fF_S SING 1A
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Client: S&ME
�10-3
Project No 99750 Analyst: SS
_ Project: C_HARL Group: SME1
Matrix: (soil/water) SOIL
_
Lab Sample ID: 99750-7
Sample wt/vol: 5.0 (g/ml) G
Lab File ID: VOC10-3.D
Level: (low/med) LOW
Dale Received: 10/11/2000
% Moisture: not dec. 0 f
Date Analyzed: 11/2/2000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor: 1.0
Soil Extract Volume (uL)
Soil Aliquot Volume: _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG q
75-71-8
Dichlorodifluoromethane
5
U
74-87-3
Chloromethane
5
U
75-01-4
Vin I Chloride
5
U
74-83-9
Bromomethane
5
U
75-00-3
75-69-4
Chloroethane
Trichlorofluoromethane
5
5
U
U
67-64-1
Acetone
50
U
75-35-4
11-Dichloroethene
5
U
74-88-4
lodomethane
25
U
75-09-2
Meth lens Chloride
25
U
1634-04-4
Meth I t-But I Ether MTBE
25
U
75-15-0
107-13-1
Carbon Disulfide
I Acrylonitrlle
50
50
U
U
1 156-60-5
trans-12-Dichloroethene
5
U
108-05-4
75-34-3
Vin I Acetate
11-Dichloroethane
25
5
U
U
78-93-3
2-Butanone ME
25
U
156-59-4
cis-12-Dichloroe1hene
5
U
67-66-3
Chloroform
5
U
74-97-5
Bromochloromethane
5
U
71-55-6
111-Trichloroethane
5
U
56-23-5
Carbon Tetrachloride
5
U
107-06-2
12-Dichloroethane
5
U
7143-2
Benzene
5
U
79-01-6
Trichloroethene
5
U
78-87-5
75-27-4
1 2-Dichloro ro ane
Bromodichloromethane
5
5
U
U
74-95-3
108-10.1
Dibromomethane
4-Meth I-2- entanone MIB
5
25
U
U
10061-01-5
cis-1 3-Dichloro ro ene
5
U
108-88-3
Toluene
5
U
10061-02-6
trans-1 3-Dichloro ro ene
5
U
591-78-6
2-Hexanone
25
U
79-00-5
112-Trichloroethane
5
U
127-18-4
Tetrachloroethene
5
U
124-48-1
Dibromochloromethane
5
U
106-934
12-Dibromoethane
5
U
100-414
Eth ibenzene
5 1
U
FORM I VOA
North Carolina Laboratory Certification No. 594
Legend — U= Undetectable E=Outside Calibration Range
6Z'd ZTO'oN 8T:8T 00,ZO PION 8Z88-2S.2-ZT6-T:GI
8260
HUNNUAUS-0NI ° 3M

llA
'._NVIRONMEN rAES L SERVICES
` CNOINEERINo - rE9 rima 1A EPA SAMPLE NO.
i VOLATILE ORGANICS ANALYSIS DATA SHEET
- — —� GP 10-3
S
Lab Name: &ME Mobile GC/MS Client: S&ME
Project No 99750 Analyst: SS _ Project: CHARL Group: SME1
Matrix: (soil/water) SOIL Lab Sample ID: 99750-7
Sample wt/vol: 5.0 (g/ml) G Lab File ID: VOC10-3.D
Level: (low/med) LOW _ Date Received: 10111/2000
% Moisture: not dec. 0 Date Analyzed: 11/2./2000
GC Column: VOCOL ID: 0.25 (mm) Dilution Factor: 1.0
Soil Extract Volume (uL) Soil Aliquot Volume: _ _ (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-90-7
Chlorobenzene
5
U
630-26-e
1712-Tetrachloroethane
5
U
10e-42-3
1
m+ X lane
5
U
9547-6
o-X lene
5
U
100.42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
11,2,2-Tetrachloroethane
5
U
9e-18-4
1 2 3-Trichloro ro ane
5
U
110-57-6
t-14-Dichloro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1 __I
3-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
U
96-12-8
1 2-Dibromo-3-chloro ro ane
25
U
91-20-3
Naphthalene
5
U
FORM I VOA
North Carolina Laboratory Certification No. 594
Legend - U= Undetectable E=Outside Calibration Range
Oi'd ZTO'oN 8T:8T OO,ZO AON 8Z88-2S5�-7_T6-T:QI
8260
HdNNd(1aS-ONI `3W'BS

NGiNEERINC7-` �FSTING �g
1A
EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Client: S&ME _
GP11-3
Project No 99750
Analyst: SS
Project: CHARL Group:
SME1
Matrix: (soil/Water)
SOIL
Lab Sample ID:
_
99750-15
Sample wt/vol:
5.0 _ (g/ml) G
_ Lab File ID:
J
VOC11-3.D
Level: (low/med)
LOW
Date Received:
_
10/11/2000
% Moisture: not dec.
0 _
Date Analyzed:
11/1/2000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor:
1.0
Soil Extract Volume
(ul-)
Soil Aliquot Volume: - (uL)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG p
75-71-8 I Dichlorodifluoromethene 5
U
74-87-3 Chloromethane
5
U
75-01-4 Vinyl Chloride
5
U
74-83-8 Bromomethane
5
U
75-00-3 Chloroethane
5
U
75-69-4 Tdchlorofluoromethane
5
U
67-64-1 Acetone
50
U
75-35-4 11-Dichloroethene
5
U
74-88-4 lodomeihane
25
U
75-09-2 Methylene Chloride
25
U
1634-04-4 + Methyl t-But I Ether MTBE
25
U
75-15-0 Carbon Disulfide
50
U
107-13-1 AC lanitrile
50
U
158-60-5 trans-12-Dichloroethene
5
U
108-05-4 Vinyl Acetate
25
U
75-34-3 11-Dichloroethane
5
U
78-93-3 2-Butanone Mn-25
U
156-59-4 cis-12-Dichloroethene
5
U
e1-66-3 Chloroform
5
U
74-97-5 Bromochloromethane
5
U
71-65-6 111-Trichloroethane
5
U
56-23-5 Carbon Tetrachloride
5
U
107-06-2 12-Dichloroethane
5
U
71-43-2 Benzene
5
U
79-01-6 Trichloroethene
5
U
78-87-5 1 2-Dichloro ro ane
5
U
75-27-4 1 Bromodichloromethane
5
U
74-95-3 Dibromomethane
5
U
108-10-1 4-Meth I-2- entanone MIB
25
U
10061-01-5 cis-1 3-Dichloro ro ene
5
U
108-88-3 Toluene
5
U
10061-02-6 trans-1 3-Dichlororo ene
5
U
591-78-6 2-Hexanone
25
U
79-00-5 112-Ticchooroethane
5
U
127-18-4 Tetrachloroethene
5
U
124-48-1 Dibromochloromethane
5
U
106-93-4 12-Dibromoethane
5
U
100-41-4 Eth (benzene
5
U
FORMIVOA
North Carolina Laboratory Certification No. 594
Legend — U= undetectable E=Outside Calibration Range
T£'d ZTO'ON 6T:8T OO.ZO AON 8Z88-2S2-ZT6-T:QI
8260
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EPA SAMPLE NO.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: S&ME Mobile GC/MS
Client: S&ME
GP11-3
Project No 99750 Analyst: SS
_ Project: CHARL Group:
SME1
Matrix: (soiltwater) SOIL
Lab Sample ID:
99750-15
Sample wt/vol: 5;0 (g/ml) G
_ Lab File ID:
VOC11-3.1)
Level: (low/med) LOW
Date Received:
10/11/2000
% Moisture: not dea. 0
Date Analyzed:
11/1/2000
GC Column: VOCOL ID: 0.25 (mm)
Dilution Factor:
1.0
Soil Extract Volume _ K)
Soil Aliquot Volume: K)
CONCENTRATION UNITS:
CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q
108-90-7 ! Chlorobenzene
5
U
630-20-6 1112-Tetrachloroethane
5
U
106-42-3 m+ X lene
5
U
95-47-6
o-X Iene
5
U
100-42-5
Styrene
5
U
75-25-2
Bromoform
5
U
79-34-5
1 1 2 2-Tetrachloroethane
5
U
96-18-4
1 2 3-Trichloro propane
5
U
110-57-6
t-14-Dichioro-2-butene
50
U
108-86-1
Bromobenzene
5
U
106-43-4
4-Chlorotoluene
5
U
541-73-1
13-Dichlorobenzene
5
U
106-46-7
14-Dichlorobenzene
5
U
95-50-1
12-Dichlorobenzene
5
1 U
96-12-8
1 2-Dibromo-3-chloro propane
25
U
91-20-3
Naphthalene
5
1 U
FORMIVOA
North Carolina Laboratory Certiflcation No. 594
8260
Legend — U- Undetectable E=Outside Calibration Range
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