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SOIL AND GROUNDWATER ASSESSMENT REPORT
ATCO PROPERTY
2806 PATTERSON STREET
GREENSBORO, GUILFORD COUNTY, NORTH CAROLINA
ECS PROJECT 09.25395
PREPARED FOR:
JE CAPITAL, LLC
GREENSBORO, NORTH CAROLINA
MAY 15, 2015
9i
ECS CAROLINAS, LLP
"Setting the Standard for Service"
Geotechnicai • Construction Materials • Environmental • Facilities NC Registered Engineering Fi rm F- 1078
May 15, 2015
Mr. Eddie Krusch
JE Capital, LLC
P. O. Box 1195
Greensboro, North Carolina 27402
Reference: Soil and Groundwater Assessment Report
ATCO Property
2806 Patterson Street
Greensboro, Guilford County, North Carolina
ECS Project 09.25395
Dear Mr. Krusch:
As authorized by your acceptance of our Proposal 09.22984-P dated April 17, 2015, ECS
Carolinas, LLP (ECS) has completed our Limited Soil and Groundwater Assessment Report for
the above referenced site. Included in this report is a description of the field activities, the results
obtained, and our conclusions and recommendations.
We appreciate the opportunity to provide our services to you. If there are questions regarding
this report, or a need for further information, please contact us at (336) 856-7150.
Respectfully Submitted,
ECS CAROLINAS, LLP
RakrEnvironmental
Cavallier
SeProject Manager
Jo n M. Stewart, P.G.
•-Sief Geologist
4811 Koger Blvd., Greensboro, NC 27407 • T. 336-856-7150 • F: 336-856-7160 • www.ecsiimited.com
ECS Capitol Services, PLLC • ECS Carolinas, LLP • ECS Central, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLC • ECS Texas, LLP
TABLE OF CONTENTS
1.0 PROJECT INFORMATION...........................................................................................................1
2.0 FIELD ACTIVITIES.......................................................................................................................2
2.1 Soil Assessment................................................................................................................. 2
2.2 Groundwater Assessment................................................................................................... 2
3.0 LABORATORY ANALYSIS...........................................................................................................3
3.2 Groundwater Sample Analysis............................................................................................ 3
4.0 CONCLUSIONS...........................................................................................................................3
5.0 RECOMMENDATIONS................................................................................................................3
FIGURES
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Soil Sample Location Map — Diesel and Gasoline USTs
Figure 3A Soil Sample Location Map — Heating Oil UST
Figure 4 Groundwater Sample Location Map
TABLES
Table 1 Summary of Soil Analytical Results
Table 2 Summary of Groundwater Analytical Results
APPENDIX
Appendix A Laboratory Data Sheets and Chain of Custody Records
Soil and Groundwater Assessment Report
ATCO Property
2806 Patterson Street
Greensboro, Guilford County, North Carolina
ECS Project 09.25395
May 15, 2015
1.0 PROJECT INFORMATION
The site is the former ATCO Rubber Products, Inc. (ATCO) facility located at 2806 Patterson
Street in Greensboro, Guilford County, North Carolina (Figure 1 and Figure 2). Based on the
records search, site reconnaissance and interviews, the building was originally constructed as a
potato chip manufacturing facility. The potato chip manufacturing business operated at the site
until the early 1980s. The building was reportedly vacant for several years. In the mid-1980s,
ATCO moved into the building. There was is no evidence that hazardous chemicals have been
utilized at the site by ATCO during flexible ductwork production.
The subject site is currently occupied by two buildings which were recently used to manufacture
flexible ductwork and as a warehouse. A portion of the main building is currently used as an
used automobile sales business. An old boiler is located in a room on the southeast side of the
main building. The building boiler is no longer in use. It appears that the boiler last operated on
natural gas; however, there is a copper line running from the boiler to the outside of the building
indicating the use of fuel oil.
There was no evidence that underground storage tanks (USTs) were registered at the subject
site with the North Carolina Department of Environment and Natural Resources (NCDENR).
However, our review of records at the Greensboro Safety and Fire Prevention Bureau identified
documentation of several petroleum USTs that were previously located at the site. During our
site reconnaissance, an area north of the building contained a concrete area, adjacent to the
asphalt pavement. This area is believed to be the former location of a diesel UST. A second
UST was believed to be located near the northwest corner of the warehouse and a third UST
believed to be a heating oil UST is located south of the warehouse, near the former boiler room.
The site is located in a light industrial/commercial area of Greensboro. The site is bound on the
north by the Norfolk Southern railway property, on the east by light industrial/commercial
properties, on the south by a light industrial/commercial building and Patterson Street and on
the west by South Holden Road.
Two properties (former Chemical & Solvent, Inc. and former Ashland Chemical) that previously
contained chemical manufacturing/storage facilities are located on adjoining properties east of
the site. Based on proximity, the releases form these properties are considered RECs of the site.
Releases are identified at the Norfolk Southern railway property north of the site. Based on
proximity and groundwater flow direction inferred from the surface topography, releases at this
property could impact the property.
ECS was contracted by Mr. Eddie Krusch to conduct a soil and groundwater assessment at the
site to determine if the identified RECs could have impacted the site. Project information is
based on a conversation between Mr. Krusch and Mr. Randy Cavallier of ECS, the previous
Phase I ESA, and a recent site visit.
Soil and Groundwater Assessment Report
ATCO Property
2806 Patterson Street
Greensboro, Guilford County, North Carolina
ECS Project 09.25395
May 15, 2015
2.0 FIELD ACTIVITIES
2.1 Soil Assessment
On April 28, 2015, nine soil borings were drilled at the site to assess whether the suspect USTs
had had a release. Soil borings UST-1 A, UST-1 B and UST-1 C were drilled in the vicinity of the
concrete patched area on the northern portion of the site (suspected former diesel UST location).
Soil borings UST-2A, UST-213, UST-2C, and UST-2D were drilled in the vicinity of a second
concrete patched area (suspected gasoline UST location) and soil borings UST-3A and UST-313
were drilled in the vicinity of the suspected fuel oil UST. The approximate locations of the soil
borings are shown on Figure 3 and Figure 3A.
ECS proposed drilling the borings to a depth of 15 feet below the ground surface (bgs); however,
groundwater was detected at a depth of approximately 11 to 12 feet bgs, so the borings were
terminated at 10 feet bgs.
The soil borings were drilled using a track -mounted Geoprobe® drill rig. The Geoprobe® is
capable of driving various forms of soil and groundwater sampling probes into the ground to
depths equivalent to auger refusal. The Geoprobe® subcontractor used for this project was 3D
Environmental Investigations, LLC (3D). The field activities were observed by an ECS
professional. Prior to initiating the first boring and between each subsequent boring, the
Geoprobe® down -hole equipment was decontaminated with a high-pressure steam cleaner.
Soil samples were collected continuously from the ground surface to the termination depth of
each boring. The soil from each boring was screened for relative levels of volatile organic
vapors using the probe of a Thermo Model 2020 flame ionization detector (FID). To screen the
samples, the soil from the borings was placed in resealable plastic bags and placed in a warm
location for approximately ten minutes to allow the headspace in the bag to equilibrate with the
soil. The probe of the FID was then inserted into the bag and the reading recorded. The soil
sample from each boring with the highest reading on the FID was submitted for chemical
analysis. Because the purpose of the assessment was to determine presence or absence of
contamination, one sample from the gasoline UST area and one sample from the heating oil
UST area were not submitted for analysis, since field conditions indicated the presence of a
release.
The sampler, wearing a new pair of nitrile gloves, placed the samples in laboratory prepared
containers. Each container was labeled and placed in a cooler containing ice to maintain the
samples at approximately 4° Celsius. The samples were transported to Research and
Analytical Laboratories (R&A) in Kernersville, North Carolina to be analyzed for diesel range
and gasoline range total petroleum hydrocarbons (TPH) EPA Methods 8015/3550 and
8015/5035, respectively. Chain of Custody Records were maintained and included in Appendix
A.
2.2 Groundwater Assessment
To determine if the groundwater beneath the site has been impacted from the USTs and off -site
sources, four groundwater samples (GW-1 through GW-4) were collected at the site (Figure 4).
The groundwater samples were collected by pushing a groundwater -sampling probe to the desired
2
Soil and Groundwater Assessment Report
ATCO Property
2806 Patterson Street
Greensboro, Guilford County, North Carolina
ECS Project 09.25395
May 15, 2015
depth (generally five feet below the water table) and pulling back on the probe, exposing the
sampling screen. A piece of dedicated polyethylene tubing was inserted down the probe to the
depth of the screen. The tubing was connected to a peristaltic pump that was used to collect the
sample. The groundwater samples were submitted to R&A and analyzed for volatile organic
compounds (VOCs) and semi -volatile organic compounds (SVOCs) using Standard Method
6200B and EPA Method 625BNA, respectively. Upon completion of groundwater sampling
activities, the temporary monitoring points were properly abandoned. A Chain of Custody
Record was maintained and is included in Appendix A.
3.0 LABORATORY ANALYSIS
3.1 Soil Sample Results
Laboratory analysis of soil samples UST-2A, UST-213, and UST-313 detected gasoline and diesel
range TPH above the North Carolina Department of Environment and Natural Resources
(NCDENR), State Action Level of 10 parts per million (ppm). The laboratory analytical results
are summarized in Table 1. The laboratory data sheets are included in Appendix A.
3.2 Groundwater Sample Analysis
Laboratory analysis of the samples GW-1, GW-2 and GW-4 detected 1,2-dichloropropane at
concentrations that exceed the North Carolina 2L Groundwater Quality Standard (NC2LGWQS).
Laboratory analysis of the samples GW-3 and GW-4 detected tetrachloroethene (PCE) at
concentrations that exceed the NC2LGWQS. Ten additional VOCs were detected in sample
GW-4 at concentrations that exceed their respective NC2LGWQS. The laboratory analytical
results are summarized in Table 2. The laboratory data sheets are included in Appendix A.
4.0 CONCLUSIONS
Based on the results of the limited soil and groundwater assessment, it is ECS's opinion that
soil in the vicinity of the former gasoline UST and the heating oil UST have been impacted from
releases or spills of petroleum products associated with the USTs. It is our opinion that the
hydrocarbons detected in the groundwater are associated with releases from the off -site
sources.
5.0 RECOMMENDATIONS
Based on the laboratory analytical results of the samples collected during the recent soil and
groundwater assessment, ECS understands that a reporting obligation exists. ECS
recommended that a copy of the report be provided to the property owner and that they consult
legal counsel regarding their reporting obligation.
3
Soil and Groundwater Assessment Report
ATCO Property
2806 Patterson Street
Greensboro, Guilford County, North Carolina
ECS Project 09.25395
May 15, 2015
6.0 QUALIFICATIONS
The activities and evaluative approaches used in this assessment are consistent with those
normally employed in limited environmental assessment projects of this type. Our evaluation of
site conditions has been based on our understanding of the site project information and the data
obtained during our field activities on the date the samples were collected and from a limited
number of sample locations. This report was prepared for the express use of JE Capital, LLC.
Use of this report by any other individual or company implies their acceptance to the General
Conditions of Service of the original contract.
4
FIGURES
Hamiton Lakes ~ `. ; ,
- z to 'mount For St
se H
- Urlyl�r
/ I y
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= - • east
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r'
r RM 7 • � mil`
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-�% ••. } i ° V f -.I f' '...� '' f `i.` /� � 1, �( \�t 7 u , . � fP
Y' i �... � , / ` r �b I 1 � •' •! 1 d its L' 4,� r • ' / � � f \�
i \ Souib"
} �I+ 1 Z_ ' �6Y •• \, \ rdt+ r, _ •� .. - r * . , -„� ` ,.. -•c;� Y a Ch,
• • e>s �i � r � Y r ' Pd k "� 'F� '!t •i-�-��9TT�f'�f�.----=�v� � { . �_
SOURCE: w Eg FIGURE 1
USGS TOPOGRAPHIC MAP S SITE LOCATION MAP
GREENSBORO, NC QUADRANGLE ATCO PROPERTY
DATED 1951 AND REVISED 1994 2806 PATTERSON STREET
GREENSBORO, NORTH CAROLINA
SCALE 1"=2,000' �T ECS PROJECT NO. 09.25395
}
Q77
AKLAND AV
See Figure 3 Pal,..�•
See Figure 3A
-mow- # —
R
fir!
1! r
f
*1.r
' • !!
MAN( Lt RD
a
T T
FIGURE 2
SOURCE:
S SITE MAP
GUILFORD COUNTY GIS ATCO PROPERTY
AERIAL PHOTOGRAPH, DATED 2010 2806 PATTERSON STREET
GREENSBORO, NORTH CAROLINA
SCALE: 1 " = 200'
TM ECS PROJECT NO. 09.25395
0,
r ,`
x
,r`L ', V Rai •'� �� y�• ' � w,I
- ✓ i
41:5 T r
1 r
Ilk
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i
w Eg SOURCE: FIGURE 4
GROUNDWATER SAMPLE LOCATION MAP
GUILFORD COUNTY GIS ATCO PROPERTY
AERIAL PHOTOGRAPH, DATED 2010 2806 PATTERSON STREET
GREENSBORO, NORTH CAROLINA
SCALE: NOT TO SCALE
ECS PROJECT NO. 09.25395
Fence Former Diesel UST Excavation (Concrete)
----------- \ - -------------------- -------------------
UST-1 A
• UST-1 C
_._._._._._.-._.� _._
UST-1 B
UST-2B1
' UST-2A ±
UST-2C •
i
Former Gasoline UST Excavation • i
UST-2D
±
i
Grass
N
SOURCE: FIGURE 3
ECS FIELD NOTES s SOIL SAMPLE LOCATION MAP
AND DRAWINGS ATCO PROPERTY
2806 PATTERSON STREET
LLP GREENSBORO, NORTH CAROLINA
SCALE: 1 INCH = 10 FEET
ICIAR(OLLUH kls ECS PROJECT NO. 09.25395
Warehouse
Building
UST-3B
•
- - - - - - - - - - -
I
Vent Pipe 0
UST-3A 10,000 Gallon Fuel Oil UST
Main— — — — — — — — — — — --
Building
Debris
N
SOURCE: FIGURE 3A
ECS FIELD NOTES s SOIL SAMPLE LOCATION MAP
AND DRAWINGS ATCO PROPERTY
2806 PATTERSON STREET
LLP GREENSBORO, NORTH CAROLINA
SCALE: 1 INCH = 10 FEET
ICIAR(OLLUM/I&IS1 ECS PROJECT NO. 09.25395
TABLES
ATCO Property
Greensboro, North Carolina
TABLE 1: SUMMARY OF SOIL ANALYTICAL RESULTS
ECS Project 09.25395
Parameter
SOIL SAMPLING
Comparison
Criteria
Sample Location
Former Diesel UST
Former Gasoline UST
Heating Oil UST
Sample ID
UST-1 A
UST-1 B
UST-1 C
UST-2A
UST-213
UST-2C
UST-211)
UST-3A
UST-313
StateAction
Collection Depth (feet
b g)
10
5
10
5
5
10
5
10
10
Collection Date
4/28/15
Total Petroleum Hydrocarbons by EPA Method 8015 following 3550/5035 Preparations
GRO
BQL
338
169
NA
BQL
56.4
10
DRO
BQL
BQL
BQL
2,210
654
NA
NA
BQL
447
10
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
Feet bgs = Feet below ground surface
GRO = Gasoline Range Organics
DRO = Diesel Range Organics
BQL = Compound not detected at a concentration above the method quantitation limit
Bold = concentration exceeds Action Level
NA = Sample not submitted for analysis
ATCO Property
Greensboro, North Carolina
ECS Project 09.25395
TABLE 2: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Parameter
ANALYTICAL RESULTS
NC2LGWQS
GCL
Location
GW-1
GW-2
GW-3
GW-4
Date Sampled
4/28/15
Volatile Organic Compounds By EPA Method 8260
Benzene
BQL
BQL
BQL
477
1
5,000
Chloroform
BQL
BQL
BQL
2_B7
70
70,000
Cis 1,2-Dichloroethene
BQL
BQL
BQL
574
60
60,000
Trans 1,2-Dichloroethene
BQL
BQL
BQL
9 Fq
100
100,000
1,2-Dichlorobenzene
BQL
BQL
BQL
42.0
20
20,000
1,3-Dichlorobenzene
BQL
BQL
BQL
1.21
200
61,500
1,4-Dichlorobenzene
BQL
BQL
BQL
7.94
6
6,000
1,1-Dichloroethane
BQL
BQL
BQL
124
6
6,000
1,2-Dichloroethane
BQL
BQL
BQL
9.08
0.4
400
1,1-Dichloroethene
BQL
BQL
BQL
964
7
7,000
1,2-Dichloropropane
2.67
2.85
BQL
1.06
0.6
600
Isopropyl Ether (IPE)
U��
BQL
BQL
V...,
70
70,000
I-Propylbenzene
BQL
BQL
BQL
46
70
70,000
Naphthalene
BQL
BQL
3.13
1.57
6.0
6,000
Sec-Butylbenzene
BQL
BQL
0.71
BQL
70
8,500
Tetrachloroethene
BQL
BQL
1.45
68.5
0.7
700
Toluene
BQL
BQL
BQL
45
600
260,000
Trans 1,2-Dichloroethene
BQL
BQL
BQL
2.63
100
100,000
Trichloroethene
BQL
BQL
BQL
117
3
3,000
1,2,4-Trichlorobenzene
BQL
BQL
BQL
0.92
70
70,000
1,1,1-Trichloroethane
BQL
BQL
BQL
).6
200
200,000
1,1,2-Trichloroethane
BQL
BQL
BQL
23.9
0.6
600
Vinyl Chloride
BQL
BQL
BQL
2.27
0.03
30
Total Xylenes
BQL
BQL
BQL
64.0
500
500
Semi -Volatile Organic Compounds By EPA Method 8270BNA
1,2-Dichlorobenzene
I BQL
I BQL
I BQL
33.2
20
20,000
Notes:
Concentrations are presented in micrograms per liter, analagous to parts per billion
NC2LGWQS= 15 A NCAC 2L.0202 Water Quality Standard
GCL = Gross Contaminant Level
Bold = Concentration exceeds the NC2LGWQS
BQL = Below the reporting limit of the method of analysis
APPENDIX A
(Laboratory Data Sheets and Chain of Custody Records)
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RESEARCH & ANALyTICAt
LAbORATORIES, INC.
AnaWal/Process Cortsultotlone
Chemical Ail dysts jor Selected Parameters and Sampling Location IdendJied as Patterson
1, VoletQeOrganics
Quantitation
(.,W-1
GW-2
GW-s
GWA
EPA Method 82t50 B
Llrnli
Pruamda:r
"
UMN
t"At)
1R1FJt)
LUM
Aiaaac
75
BQL
BQL
BQL
BQL
Acrolcin
501
BQL
BQL
BQL
BQL
Aayimikile
100
BQL
BQL
BQL
BQL
Bin
0 5
BQL
I5Q1,
BQL
47,
Dtw^ -
0.5
BQL
BQL
BQL
BQL
Bromochlmamghmie
C +
Bizl.
BQL
UQL
BQL
Smmetihloaoorrtf`.me
0.5
BQL
k1Q1.
BQL
BQL
Bromofm]n
1.0
BQL
BQL
BQL
BQL
Bmniw=dwc
1.0
BQL
BQL
BQL
BQL
2-Butmo¢e
35
HQS
BQL
LIQ3,
BQL
Carbon Dmdfide
5.0
BQL
BQL
BQL
BQL
Carbon Tcaaeblondo
05
BQL
BQL
BQL
BQL
Chlaobarme
0.5
BQL
BQL
BQL
BQL.
Chloroodume
1.9
BQL
BQL
BA�L
BQL
2-0doroethyl vinyl ether
5.0
BQL
BQL
BQL
BQL
Chloroform
0.5
BOL.
BQL
BQL
2.67
CLH. q .&+ -.e
1.0
BQL
BQL
BQL
2-Qdoromtueae
0.5
BQJ-
BQL
BQL.
BQL
4 Cldorna.-jrnr
0.5
BQI-
BQL
BQL
BQL
Cis-1,2-Diddoroetlfau
0 5
BQL
U(U[-
BQL
5.74
Cis-1,3-Dichlmopropene
05
BQL
BQL
BQL
BQL
1.2-Ihkolro-S.Cld¢opvpone?!}IIfd�}
5.0
BQL
BQL
1HQ1.
9Q1,
1,2-Dibtonrocthax (EDB)
0.5
BQL
BQL
BQL
BQL
ELwar^sch�oramelhox
0.5
BQL
BQL
BQL
BQL
Ltk:urrtmrihmrc
0.5
BQL
HQ1.
BQL
BQL
1,2-DiehlorobeKene
0.5
BQL
F1Q1.
BQL
ILO
1,3-Diclilmbentta
r `.
BQL
BQL
BQL
1.21
1,1-Dichlorobmmre
0.5
BQL
BQL
BQL
734
1,1-Dicblorodhene
0.5
BQL
BQL
BQL
124
1,2-Diehloroethane
0.5
BQL
BQL
BQL
4-41111
1,1-Dicb1oroatl ma
0.5
BQL
BQL
BQL
9M
DiddoroBoummahmw
0.5
BQL
BQL
9i?L,
31Qi.
1,2-DicItlotapropena
0.5
2.67
3M
i.
3 A6
0-Diddorvpropmm
0.5
HQ2
BQL
BQL
BQL
2,2-Dieblomprvpmw
0.5
fiQ3.
BQL
BQL
BQL
1,1-Dic6lmopropma
0.5
BQl.
H-x I
BQL
BQ1,
Ethyl Bermme
R5
BQL
BQL
BQL
BQL
2-Hasanaee
5.0
BQL
BQL
BQL
BQL
IPE
AS
BQL
BQL
BQL
030
1-Propy@mzme
0.5
BQL
BQL
BQL
1.46
4-Medryl-2-Partmone
5.0
BQL
BQL
Hf%Vl,
BQL
Methyl Iodide
1.0
BQL
BQL
BQL
BQL
Mahy2®a Chloride
5.0
BQL
BQL
9Qi-
BQL
"ME
0.5
BQL
RQi.
BQL
00L
NapWWeue
0.5
BQL
BQL
3.13
1.57
N-Bulylbm teae
0.5
BQL
1101.
13QL
n1ji .
N-Prapylb®me
0.5
BQL
BQL
BQL
BQL
P-bowopyltolune
0.5
HQL
BQL
BQL
BQL
See-BuWbcu=
0.5
BQL
BQL
R71
BQL
SiyC
0.3
BQL
BQL
BQL
BQL
Tert-Butyl6etuara
0.5
100L
BQL
BQL
BQL
1,1,1,2-Tatra ltlorocthara
D 4
BQI-
BQL
BQL
BQL
1,1,2,2-TentWorceadu a
0.5
HQ1.
BQL
BQL
GQL
'ria'rw?.ircaedxe
0.5
BQL
BQL
1.45
M5
Toluene
0.5
BQL
BQL
BQL
1.44
Trars-1,2-Dicbloroethmm
0.5
BQL
BQL
BQL
r.ba
Ttars-0-Diebloropropenc
0.5
BQL
BQL
BQL
BQL
Trap-1,4-Dichloro-2-butene
5 0
BQL
BQL
BQL
BQL
1,2,3 Triddorebmzme
0.5
BQL,
BQL
BQL
BQL
1,2,4-Triahlorobmmu
415
BQL
BQL
BQL
0-92
l,l,l-Trirbloroah®a
0.5
BQL
BQL
BQL
10A
1,1,2-Tricidaroethaoe
0.5
BQL
Hs r7
HQI .
23.9
Triddoroethme
0.5
BQL
BQL
BQL
117
TriddoruP,rormwlic;
0.5
BQL
BQL
BQL
BQL
1,2,3Trichloropn4w
0.5
BQL
BQL
BQL
BQI.
1,2,44rhuethylbeazaoa
0.5
BQL
BQI.
BQL
BQL
1,3,5-Trimahylbamme
u '-
BQL
11Qi
BQL
BQL
Vinyl Acetate
1.0
BQL
BQL
SOL
BQL
Vinyl Cblcrida
f3 `
BQL
BQL
F3Q1
2.27
ToW Xylem
I 0
BQL
BQL
BQL
64.0
Dilution Faaror
I
I
i
I
Sample Number
3594-01
3594-02
3584-03
3594.04
Sample Date
0428/15
0429115
04/29/15
0428/15
Sample Time (hn)
1100
1130
1220
1330
Date Analyzed
04/30/15
04/30/15
04/30/15
04/30/15
Time Analyzed
1541
1613
1645
1717
Surrogate Recovery (DBFM)
Range (70-130%)
103%
102%
109%
104%
Surrogate Recovery (Toluene-d8)
Range (70-130%)
98%
98%
98%
123%
Surrogate Recovery (4-BFB)
Range (70-1301/6)
93%
96%
93%
93%
BQL - &low QmodMdw Limit ppb - Pub Per bM-
RESEARCh & ANA1yTiCAL
LABORATORIES, INC.
Analytical/Process Consultations
Chemical Analysis for Selected Parameters and Sampling Location Identified as Pagerson
�,�'(Irolltras. LIPFraka[. rol�rcted.��r�p.,#QI _ -
II, Semi-VolatileOMBuics
Quamtlltation
GW-2
(;W.3
G'W4 a
EPA Method 8270 BNA
haft
PyrsmgU
&W
b-2h1)
t224)
(22bl
4-Chloro-3-methylphoW
10.0
BQL
BQL
BQL
2-0lorophmol
10,0
BQL
6QL
E [QL.
2,4-DicLioropheool
10.0
BQL
BQL
BQL
2,4-1)i nedylphemol
10.0
BQL
0Q1.
BQL
2,4-DWtrophmo1
50.0
BQL
Bt tl,
BQL
2-Methyl-4,64khropheaol
50.0
BQL
BQL
BQL
2-Nitropbmol
10.0
BQL
BQL
BQL
4-Nitrop6mol
50.0
BQL
BQL
BQL
Pcmtuhlorophcaol
50.0
BQL
9Q1.
BQL
19Mm1
10.0
BQL
BQL
BQL
2,4,6-Trichlorophemo1
10.0
BQL
BQL
BQL
&WWM m
10.0
BQL
HQ1.
BQL
Apmzpb ft1cflc
10.0
BQL
BQL
BOL
AMP E
10.0
BQL
BQL
BQL
HeU&M
50.0
8QL
BQL
BQL
OgP*MPMditU g
10.0
HQL
BQL
BQL
Be1z4!4a1M=C
10.0
BQL
BQL
BQL
benw*)Oufthurthmc
10.0
BQL
BOL
BQL
Betat(gbd)pray'leee
10.0
BQL
BQL
BQL
Boteo(O T^ M&�
10.0
BQL
BQL
BQL
B--A butyl ph&Bb to
10,0
BQL
BQL
BQL
BI�2chltlhiktitJWyime�r�r.
10.0
BQL
13rl .
BQL
Bis(2-ddomdhy4)Cthc+
10.0
WiL
HQL
BQL
Bis(2-ch1oroisttpw"1)cthcr
10.0
LIQt.
i1Q1.
BQL
Bis(2-c&ybhezyl)phth&l-
10.0
BQL
BQL
BQL
4-Hromophemyl pbemyl ether
10.0
BQL
BQL
BQL
2-ChlmomephdWeme
10.0
BQL
BQL
BQL
4-Chloroph®yl phemyl ether
10.0
BQL
BQL
BQL
i2nywe
10.0
BQL
BQL
BQL
Dibe=0 hjtmlt rz=nc
10.0
BQL
BQL
BQL
1,2-Dichlorobeni me
10.0
1JQL
BQL
33.2
1,3-Dichlorobmeemc
10.0
BQL
BQL
BQL
l,4-Dkh1orobmuae
10.0
BQL
BQL
BQL
3,3-DichlorobeaMinc
20.0
0Q1.
BQL
BQL
Diethyl phthalate
10.0
13QL
BQL
BQL
Dimethyl phthmleu
10.0
BQL
BQL
BQL
DI-N-BOA phthalate
10.0
BQL
BQL
BQL
2,4-Ditrimotmlucac
10.0
BQL
BQL
BQL
2,6-OWUntotune
10.0
BQL
BQL
BQ1,
Di-N-Ouyl phth-I
10.0
BQL
BQL
UQq-
1.2-DiphenyMydnizice
50.0
BQL
BQL
BQL
fl: rmrd=
10.0
BQL
BQL
BQL
FLu
10.0
BQL
BQL
BQL
Hw=Morobmrmo
10.0
BQL
BQL
BQL
Hexarhlombun dkme
10.0
BQL
BQL
Aql,
�Itrdoe�e
10.0
BQL
Hql .
BQL
HaoeehGoroeO��e
10.0
BQL
BQL
BQL
Imdmo(1,2,3-od) pyreme
10.0
BQL
BQL
BQL
Isophacae
10.0
BQL
BQL
BQL
Naphtheleme
10.0
BQL
BQL
BQL
Nmo
10.0
BQL
BQL
BQL
N-Niuosodimethylemime
10.0
BQL
BQL
BQL
N-nimosodi-m�brume
10.0
BQL
BQL
BQL
N-NimosodkphmybMine
10.0
F3gl .
BQL
BQL
Phm"locnp
10.0
L3{ZL
BQL
BQL
Fyraee
10.0
BQJ.
VQL.
BQL
1,2,4-Triddorobenzmo
10.0
IIQI .
BQL
BQL
2-MethyhtaphthOwe
10.0
13UL
BQL
BQL
1-Me1hyhmphdWcoe
10.0
BQL
BQL
OM
Muctiam Facinr
I
I
I
Sample Number
3584-02
3584-03
3584-04
Sample Date
04/28/15
04/28/15
04/28/15
Sample Time (bra)
1130
1220
1330
Date Ertratxed
04/30/15
04/30/15
04/30/15
Date Analyzed
05/04/15
05/04/15
05/04/15
Time Analyzed
0236
0304
0333
Surrogate Recovery
Range
(2-FlmorophenoQ
(21-110%)
39%
42%
46%
(Phemol-d6) (10-I 10%) 26% 29% 36%
(Nltrobenzeae-d5) (35-114%) 82% 87% 83%
(2,4,6-Tribromophenol) (10-123%) 85% 73% 79%
(2-FtuoroblphenyQ (43-116%) 82% 69% 95%
(4-Terpheny"14) (33-141%) 69% 63% 65%
BNA - Bsse Namd Acid lictramblm ppb - pats per btmw
pl;.
it
0
I
dos _5!H'H ')dV
4 � \
o
u
cc f
— 7—�
2
IL
. [CIL:let ,
cc
co) d m M
N
W CO o )
to CU
M
r.Tu O
H a
\� I.
cc C9
Z06Z'ON 0 );Iuao Aaa,ans uiys id0�:� MZ '66 �dy
RESEARCh & ANA[yTICAI
LABORATORIES, INC.
Analytical/Process Consultations
Four (4) water and seven (7) soil samples were received in good condition on
29 April 2015. The samples were analyzed without difficulties unless noted below.
Sidney L. Champion
Director of Laboratory Services
5-5-[5
Date
P.O. Box 473 • 106 Short Street • Kernersville, North Carolina 27284. 336-996-2841 • Fax 336-996-0326
www.randalabs.com
QA/QC Summary
Method: ZOOB 5/10 20/ 0 001000 PPB C
FILE NAME: W C0430
CLIENT: ECS CAROLINAS(PROJECT:
PATTERSON
Sample ID:
3584 - 01- 04
INSTUMENT:
MS-2
Page 1 of 2
Extraction Method
NIA
Date Extracted
N/A
Weight Extracted
25ML
Final Extract Volume
25ML
Date Anglyzed
04/30/15
% Surrogate Recovery
99
97
94
Acceptance Range
(70-130)
(70-130)
(70-130)
LCS
Acceptance
Range
MS
MSD
RPD
QC
LIMITS
Compound
MDL
Method
LCS %
% Rec.
% Rec.
RPD
% REC
u
Blank
Recovery
DICHLORODIFLUOROMETHANE
0.12
ND
84
70-130
CHL-OROMETHANE
0.07
ND
72
70-130
VINYL CHLORIDE
0.11
NV
96
70-130
BROMOMETHANE
0.18
ND
77
70-130
CHLOROETHANE
0.11
ND
95
70-130
TRICHLOROFLUOROMETHANE
0.09
ND
100
70-130
ACETONE
1.18
ND
90
70-130
ACRYLONITRILE
12.38
ND
110
70-130
2-BUTANONE
0.88
ND
88
70-130
IJ-DICHLOROETHENE
0.09
ND
99
70-130
102
110
7
14
70-130
METHYL IODIDE
0.19
ND
84
70-130
CARBON DISULFIDE
0.45
ND
100
70-130
MEniYLENECHLORIDE
0.57
ND
97
70-130
TRANS-1,2-DICHLOROETHENE
0.10
ND
97
70-130
I,1-DICHLOROETHANE
0.17
ND
101
70-130
ISOPROPYLETHER(IPE)
0.12
ND
96
70-130
M> TIM-TRT-Burn ETHERO.ME)
0.16
N D
88
70-130
VINYL ACETATE
0.24
ND
84
70-130
CIS-1,2-DICHLOROETHENE
0.09
ND
95
70-130
,2-DICHLOROPROPANE
0.09
ND
99
70-130
BROMOCHLOROMETHANE
0.12
ND
87
70-130
CHLOROFORM
0.05
ND
96
70-130
1.1.1-TRICHLOROETHANE
0.12
ND
103
70-130
CARBON TETRACHLORIDE
0.10
ND
104
70- 1 3 0
l,l-DICHLOROPROPENE
0.12
ND
102
70-130
BENZENE
0.05
ND
99
70-130
100
lI}2
2
11
70-130
ETHYLACETATE
0.35
ND
88
70-130
1,2-DICHLOROETHANE
0.09
ND
97
70-00
TRICHLOROETHENE(TCE)
0.12
ND
101
70-130
98
100
2
14
70-130
11,2-DICHLOROPROPANE
0.10
ND
99
70-130
DIBROMOETHANE
0.25
ND
96
70-130
COMMENTS:
QA/QC Summary
Method: QW&MMOLUMMIM0 PP
FILE NAME: W C0430
Page 2 of 2
CLIENT: ECS CAROLINASPROJECT: PATTERSO
SAMPLE ID:
3584 - 01- 04
LCS
Acceptr
ange
MS
MSD
RPD
QC LIMITS
Compound
MDL
Method
LCS %
RPD
% REC
ug/L
Blank
Recovery
% Rec.
% Rec.
BROMODICHLOROMETHANE
0,07
ND
101
70-130
4-METHYL-2-PENTANONE
1.01
ND
95
70-130
CIS-1,3-DICHLOROPROPENE
0.10
j ND
99
70-130
TOLUENE
0.26
1 ND
90
70-130
87
90
3
13
70-130
TRANS-1,3-DICKOROPROPENE
0.12
ND
96
70-130
1,1,2-TRICHLOROETHANE
0.20
ND
92
70-130
TETRACHLOROETHENE(PCE)
0.17
ND
102
70-130
•HEXANONE
1.42
ND
95
70-130
DIBROMOCHLOROMETHANE
0.07
ND
93
70-130
1,3-DICHLOROPROPANE
0.13
ND
98
70-130
1,2-DI13ROMOETHANE(EDB)
0.15
ND
90
70-130
CHLOROBENZENE
0.10
ND
96
70-130
97
96
1
13
70-130
1,1,1,2-TETRACHLOROETHANE
0.10
ND
95
70-130
EMYL9ENZENE
0.07
ND
98
70-130
TOTAL XYLENES(M&P, 0)
0.29
ND
95
70-130
STYUNE
0.04
ND
98
70-130
BROMOFORM
0.29
ND
91
70-130
ISOPROPYLBENZENE
0.08
ND
98
70-130
BROMOBENZENE
0.07
ND
92
70-130
1,2,3-TRICHLOROPROPANE
0,11
ND
90
70-130
rR,ANS-1,4-DICHLORO-2-BUTENE
0,52
ND
90
70-130
N-PROPYLBENZENE
0.08
ND
99
70-130
2-CHLOROTOLUENE
0.10
ND
98
70-130
4-CHLOROTOLUENE
0.09
ND
98
70-130
1,3,5-TRQNETHYLBENZENE
0.07
ND
98
70-130
TERT-BUTYLBENZENE
0.08
ND
96
70-130
1,2,4-TRIMETHYLBENZENE
0.07
ND
96
70-130
SEC-BUTYLBENZENE
0.12
ND
100
70-130
1,3-DICHLOROBENZENE
0.12
ND
93
70-130
1,1,2,2-TETRACHLOROETHANE
0.08
ND
96
70-130
P-ISOPROPYLTOLUENE
0.09
ND
102
70-130
1,4-DICHLOROBENZENE
0.08
ND
98
70-130
1,2-DICHLOROBENZENE
0.09
ND
97
70-130
N-BUTYLBENZENE
0.10
ND
99
70-130
1,2-DIBR0M0.3-0WR0PR0PANE(DPCP)
0.49
ND
94
70-130
1,2,4-TRICHLOROBENZENE
0.47
ND
95
70-130
f4AYRTHALENE
0.18
ND
93
70-130
11,2,3-TRICHLOROBENZENE
0.18
ND
94
70-130
COMMENTS:
QA/QC Summary
Method: 625 100/200 PPB QCJ IFILE NAME: WLC0503-MS1
Page 1 of 2
CLIENT:ECS (PROJECT:PATTERSOl1�
SAMPLE ID:
3584-02-04
INSTRUMENT:MS-1
Extraction Method
3510
Date Extracted
OU30115
Weight Extracted
1L
Final Extract Volume
1M1.
-
Date Analyzed
OSM/15
% Surrogate Recovery
60
36
73
81
1 67
69
Acceptance Range
(5 - 77)
(7 - 64)
(29 -149)
(12 -123)
(10 -133)
(20 -133)
LCS
Range
MS
MSD
RPD
QC LIMITS
Compound
MDL
Method
LCS %
%Rec.
%Rec.
UG/L
Blank
Recoveryg
RPD
/o REC
�N-Nitrosodimcthylamine
0.970
ND
60
8-104
Bis(2-c1loroethy1)ether
0.430
ND
80
45-111
rt]enai
0.460
ND
43
D-76
27
26
1
42
12-110
2-Chlorophenol
0.300
ND
79
30-107
65
67
3
40
27-123
1,3-Dichlorobenzene
0.250
ND
68
48-90
1,4-Dichlorobonzene
0.200
ND
70
50-90
51
50
2
28
36-97
1,2-Dichlorobenzene
0.100
ND
68
50-93
Bis(2-chloroisopropyl)ether
0.380
ND
70
50-107
N-nitrosodi-n-propylamine
0.500
ND
68
47-111
74
67
10
38
41-116
HexachloroW=e
0.220
ND
66
36-90
2-Nitrophenot
0.670
ND
76
33-110
2,4-Dimethylphenol
1,550
ND
71
43-100
Nitrobenzene
0.500
ND
71
46-112
Isophorone
0.510
ND
67
50-104
Bis(2-chloroethoxy)methane
0.420
ND
62
49-105
2,4-Dichlorcphenol
0.540
ND
76
33-108
1,2,4-Trichlorobenzene
0.560
ND
66
47-95
66
64
3
28
39-90
4-Chloro-3-methylphenol
1.830
ND
72
44-107
85
74
14
42
23-97
Naphthalene
0,710
ND
75
50-96
Hexachlorobutadiene
0.770
ND
62
24-100
2,4,6-Trichlorophenol
0.540
ND
79
22-124
2-Methyl4,6-Dinitrophenol
3.250
ND
86
16-115
4-Nitrophenol
6.670
ND
42
1-69
22
21
8
50
10-80
Hexachlorocyclopentadiene
0.970
ND
52
16-85
N/A
a
= Data Not Available " - FAILED
QA/QC Summary
Method: 625 100/200 PPB
FILE NAME: WLC0503-MSI
Page 2 of 2
CLIENT:ECS (PROJECT:PATTERSOi
LCS
Acceptr
ange
C LIMITS
Compound
MDL
Method
LCS %
MS
MSD
�2PD
UG/L
Blank
Recovery
% Rec.
% Rec.
2-Chloronaphthalene
0.420
ND
76
51-100
RPD
0
/oREC
Dimethyl phthalate
0.400
ND
76
47-107
Acenaphthylene
0.150
ND
75
49-100
2,6-Dinitrotoluene
0.670
ND
82
49-106
Acenaphthene
0.280
ND
80
48-102
71
55
25
31
46-118
2,4-Dinitrotolume
0.670
ND
70
50-106
69
63
10
38
24-96
Diethyl phthalate
0.820
ND
79
49-107
4-Chlorophenyl phenyl ether
0.730
ND
86
43-112
2,4-Dinitrophenol
4.190
ND
68
D-118
Pwtachlorophenol
5.220
ND
89
15-123
17
15
16
50
9-103
N Nitrosadiphenylamine
1.150
ND
82
35-121
4-Bromophenyl phenyl ether
0.670
ND
81
48-107
~
Hexachlorobenzene
0.390
ND
76
50-102
PhMMOOM
0.280
ND
83
42-105
Antivacene
0.200
ND
72
44-104
Di-N-Butyl phthalate
0.650
ND
1 79
44-111
Benzidine
3.370
ND
I
D48
�>Yne
1.920
ND
79
39-107
69
63
'
31
26-127
Beryl butyl phthalate
1.220
ND
79
39-116
Baua(0)OWhMmm
0.380
ND
80
36-114
3,3-Dichlcrobenzidinc
5.050
ND
25
6-52
Chrysene
0.700
ND
80
45-99
Bis(2-ethyl-hexyl)phthalate
1.140
ND
77
30-134
Di-N-Octyl phthalate
0.740
ND
89
37-131
Benzo(b)lluoradhene
0.770
ND
87
49-107
Benzo(k)fluoranthene
0.600
ND
79
37-112
Berm(a)pyr-e
0.430
ND
80
49-105
Indeno(1,2,3-ed)pyrene
1.210
ND
48
38-122
Dibenzo(a,h)anthmme
1.680
ND
53
43-118
Benzo(g,h,i)Mlene
1.780
ND
43
42-119
N/A
= Data Not Available " = FAILED
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