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HomeMy WebLinkAboutMO-9434_40873_CA_IAR_20190201_Initial Abatement Action Reporthart hickman SMARTER ENVIRONMENTAL SOLUTIONS Via FedEx Overnight February 1, 2019 NC DEQ Division of Waste Management UST Section 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Attention: Ms. Beverly Trudy RE: IAA Report 2837 Cindy Lane Charlotte, NC H&H Job No. CHP-035 Dear Beverly, On behalf of The Housing Partnership, Hart & Hickman is submitting one hard copy of the Initial Abetment Action (IAA) Report for the above referenced property located in Charlotte, Mecklenburg County, North Carolina. An electronic copy of this report also is included on the enclosed CD. If you have any questions or comments, please do not hesitate to contact me. Sincerely, Hart & Hickman, PC Stephen R. Libbey, P.G. Project Manager Enclosures cc: Fred Dodson, Jr., The Housing Partnership (via email) 2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301 Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com 704.586.0007 main 919.847.4241 main Initial Abatement Action Report 2837 Cindy Lane Charlotte, North Carolina DEQ Incident No. TBD H&H Job No. CHP-035 February 1, 2019 hart .19 hickman SMARTER ENVIRONMENTAL SOLUTIONS C-1269 Engineering #C-245 Geology 2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301 Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com 704.586.0007 main 919.847.4241 main Initial Abatement Action Report A. Site Information 1. Site Identification Date of Report: February 1, 2019 Facility ID: NA UST Incident Number: TBD Site Narne: 2837 Cindy Lane Site Street Address: 2837 Cindy Lane City, Town: Charlotte Zip Code: 28269 County: Mecklenburg Description of Geographical Data Point: Former UST location Location Method: Goode Earth Latitude: 35' 17' 05"N Longitude: 80' 50' 33"W 2. Information about Contacts Associated with the Leaking UST System UST Owner: Unknown Address: Tel.: UST Operator: Unknown Address: Tel.: Property Owner: The Housing Partnership Address: 4601 Charlotte Park Drive Ste 350 Charlotte NC 28217 Tel.: (704) 342-0933 Property Occupant: Vacant Address: Tel.: Consultant/Contractor: Hart & Hickman PC Address: 2923 South Tryon Street, Suite 100, Charlotte, NC 28203 Tel.: (704) 586-0007 (Attn: Steve Libbey, PG) Analytical Laboratory: Prism Laboratories Inc. State Cert. No. 402 Address: 449 Springbrook Road, Charlotte, NC 28224 Tel.: (704) 529-6364 3. Information About Release Date Discovered: August 16.2018 Estimated Quantity of Release: Unknown Cause of Release: Unknown Source of Release: Heating Oil UST Sizes and contents of UST system: One 550-gallon heating oil UST 4. Certification I, Stephen Libbey, PG a LicensedllGFologist at Hart & Hickman, PC, do certify that the 111 information contained in this�f t and accurate to the best of my knowledge. EN SEAL , �Cf): 1656 %'y •Fo�oo�5• N Hart & Hickman, PC is licei%/�r�`�geology/engineering in North Carolina. The certification numbers of the coi � tf*+V�rNC 45/C-1269. 1 hart hickman SA\AAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil USTUAA.doc SMARTER ENVIRONMENTAL SOLUTIONS B. Site History and Characterization 1. UST Owner and Operator Information: UST ID Number UST-1 Facility ID Number N/A Name of Owner Dates of Ownership Unknown Street Address City State Zip Telephone Number Name of Operator Dates of Operation Unknown Street Address City State Zip Telephone Number 2 hart hickman SAAAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\IAA.doc SMARTER ENVIRONMENTAL SOLUTIONS 2. UST/AST Information: Was Approximate Description of Date release UST ID Current/Last Previous Capacity Construction Status of associated Tank Associated Piping and Tank Number Contents Contents (gallons) Details UST with the Dimensions Pumps Installed UST LUS:T-1 S stem? I Heating Oil I N/A 1 550 1 Steel 1 6' x 3.33' 1 N/A Unknown I Removed I Yes 3 S AAAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\IAA.doc hart 1 h I c k m a n SMARTER EWRONMENTAL SOLUTIONS 3. Non -UST spills at the site: No non -UST spills are known to have occurred at the site. 4. Description of release: The subject site is part of the Dillon Lakes Development Brownfields project. During Phase II Environmental Site Assessment (ESA) activities performed at the site in March 2018, H&H collected soil sample SB-1 from the north side of the UST and soil sample SB-2 from the south side of the UST (Figure 2). Laboratory analytical results indicated that gasoline -range TPH (TPH-GRO) was detected in the SB-1 at a concentration of 47.9 mg/kg which is below the DEQ action level of 50 mg/kg. Diesel -range total petroleum hydrocarbons (TPH-DRO) was also detected in SB-1 at a concentration of 567 mg/kg, which is above the DEQ action level of 100 mg/kg. TPH-GRO and TPH-DRO were not detected in soil sample SB-2 at concentrations above DEQ action levels. Phase II ESA laboratory analytical data are summarized in Table 1. 5. Site characteristics: The site is approximately 1.8 acres in area and formerly contained a 2,314 ft2 single-family residence and associated outbuildings. A site location map is presented as Figure 1, and a site map is presented as Figure 2. The subject property is located in the Piedmont Physiographic Province of North Carolina. According to the Geologic Map of North Carolina dated 1985, the subject property lies within the Charlotte Belt. In the site area, underlying bedrock is composed of granitic rock. The land surface of the area is generally characterized as gently sloping, which may become moderately steep where intersected by streams. In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed saprolite or residuum. The saprolite consists of unconsolidated clay, silt, and sand with lesser amounts of rock fragments. Due to the range of parent rock types and their variable susceptibility to weathering, the saprolite ranges widely in color, texture, and thickness. Generally, the saprolite is thickest near interstream divides and thins toward streambeds. In profile, the saprolite normally grades from clayey soils near the land surface to highly weathered rock above competent bedrock. The occurrence and movement of groundwater in the Piedmont is typically within two separate but interconnected water -bearing zones. A shallow water -bearing zone occurs within the saprolite, and a deeper water -bearing zone occurs within the underlying bedrock. The site is located at an approximate elevation of 790 ft above mean sea level. Topography in the source area generally slopes to the northwest (Figure 1). Based on topography, H&H anticipates that the groundwater flow direction at the site is to the northwest toward Dillon Lakes. Portions of Dillon Lakes have been 4 hart hickman SAAAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\IAA.doc SMARTER ENVIRONMENTAL SOLUTIONS permanently drained such that the nearest surface water is approximately 750 ft from the former UST. Visual observations during excavation activities and soil sample collection indicated that the soil surrounding UST system consists of brownish silty clays (saprolite). Groundwater and bedrock were not encountered in the excavation. Municipal water is available to the site and the areas surrounding the site. A formal water supply well survey was not performed. No obvious water supply wells were observed during area reconnaissance. 6. Initial abatement actions, assessment activities, and corrective actions performed to date: Prior to the 2018 assessment activities and January 2019 UST removal activities, no other known initial abatement actions, assessments, or corrective action activities were conducted at the site. In January 2019, H&H contracted with EVO Corporation (EVO) of Winston- Salem, NC to remove the heating oil UST at the site. Based on the 2018 Phase II ESA soil analytical results and as confirmed by field evidence of impacted soils at the time of closure, soil over -excavation activities were initiated following UST removal in accordance with DEQ guidance. The owner's goal was to obtain a No Further Action letter without a deed notice. The results of the soil over - excavation activities are discussed in Section D below. C. Site Check Report Not applicable. D. UST Closure Report following UST-12 format and Site Investigation Report for Permanent Closure or Change -in -Service of UST (UST-2 Form) 1. Preparations for closure including the steps taken to notify authorities, permits obtained and the steps taken to clean and purge the tanks: Prior to UST closure activities, H&H obtained a permit authorizing the UST removal from the City of Charlotte Fire Department. A copy of the permit is included in Appendix B. Prior to removal, residual fluids were removed from the tank. Then, the tank was triple -rinsed with a pressure washer and vacuum truck by EVO in accordance with Mecklenburg County requirements. Approximately 160 gallons of residual fluids and rinse water were removed from the UST. The non -hazardous material manifest for the residual fluids is included in Appendix C. 2. Closure procedures: Initially, soil was removed from the top and sides of the UST with a track hoe so that the tank could be removed from the ground. Soils encountered during the 5 hart hickman SAAAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\IAA.doc SMARTER ENVIRONMENTAL SOLUTIONS excavation were evaluated in the field for the presence of odors and staining, and for the presence of organic vapor readings with a PID. The PID was calibrated prior to its use against an isobutylene standard. Following removal, the UST was inspected for holes or other signs of structural damage. The UST was single -walled and constructed of steel. No evidence of structural damage was observed on the UST following removal. No surface or subsurface product piping was connected to the UST. 3. Note the amount of residual material pumped from the tank and describes the storage, sampling and disposal of the residual material and the disposal of the tank, pumps and piping: As stated above, EVO removed approximately 160 gallons of residual and rinse liquids from the UST. The fluid was disposed by EVO. The disposal certificate for the residual fluid is included in Appendix C. The UST was transported off -site by EVO for disposal at Foss Recycling in Winston-Salem, North Carolina. The tank disposal certificate is included in Appendix D. 4. Initial response actions and initial abatement actions: Initial response and abatement actions are discussed in the following section. 5. Soil excavation and Site Investigation activities: After removal of the UST, one closure soil sample was collected in accordance with DEQ guidelines. The closure sample was analyzed for TPH-GRO by EPA Method 5030/8015C and TPH-DRO by EPA Method 3550/8015C. The analytical results for the closure soil sample indicated the presence of TPH-DRO and TPH- GRO at concentrations of 380 mg/kg and 4,700 mg/kg, respectively. The detected concentrations exceed the DEQ action levels of 50 mg/kg and 100 mg/kg for TPH-GRO and TPH-DRO, respectively. Approximately 239 tons of impacted soils were excavated from the UST basin on January 3, 2019. The excavated soil was transported to EVO Corporation's treatment facility in Winston-Salem, NC for proper treatment and disposal. A copy of the certificate of disposal, non -hazardous waste manifests, and certified weight tickets for the excavated soil are provided in Appendix E. The dimensions of the UST basin excavation were approximately 19 ft long by 16 ft wide by 20 ft deep. Field screening indicated that more significant impacts were present in the center of the UST basin; therefore, additional impacted soil was removed from that area. The depth of the center of the basin was approximately 22 ft. The approximate extent of the excavation is depicted on Figure 3. 6 hart hickman SAAAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\IAA.doc SMARTER ENVIRONMENTAL SOLUTIONS Following soil over -excavation activities, four confirmation sidewall soil samples (SW -I though SW-4) and one confirmation base soil sample (B-1) were collected from the excavation. In accordance with DEQ guidance, the collected post - excavation soil samples were analyzed for volatile organic compounds (VOCs) by EPA Method 826013/5035A, semi-VOCs (SVOCs) by EPA Method 8270, and extractable petroleum hydrocarbons (EPH) and volatile petroleum hydrocarbons (VPH) using the Massachusetts Department of Environmental Protection (MADEP) Methods. The results of analyses of the post -excavation samples from the UST basin excavation indicated that post -excavation sidewall sample SW-3 contained concentrations of petroleum compounds slightly above the laboratory detection limits. However, the detected compounds did not exceed DEQ Soil -to - Groundwater or Residential Maximum Soil Contaminant Concentrations (MSCCs). Target compounds were not detected above the laboratory detection limits in the remaining samples. All soil samples were analyzed by a North Carolina certified laboratory. A chain - of -custody record was completed for samples collected and included sample description, date collected, time collected, matrix, sample container information, and analyses required. The chain -of -custody was signed by H&H prior to placement in an iced cooler for shipment to the laboratory. Prior to shipment, the cooler was closed with a seal indicating the H&H representative's signature and date such that a potential disturbance of the cooler contents could be detected by the laboratory. Soil sample results are presented in Table I and the sample locations are depicted on Figure 3. Laboratory analytical sheets are included in Appendix A. Following soil removal, the excavation was backfilled with clean imported backfill material. The imported backfill material consisted primarily of brown silty clays. E. Free Product Investigation and Recovery Report Not applicable. F. Groundwater and Surface Water Investigation Not applicable. G. Initial Response and Abatement Activities See Section B. H. Excavation of Contaminated Soil See Section D. 7 hart hickman SAAAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\IAA.doc SMARTER ENVIRONMENTAL SOLUTIONS I. Conclusions and Recommendations: In January 2019, one 550-gallon heating oil UST was removed from the site. Approximately 239 tons of impacted soils were excavated from the UST basin. Analytical results of post -excavation confirmation soil samples indicate that concentrations do not exceed DEQ MSCCs. Based upon the results of the UST closure activities, H&H recommends that DEQ issue a no further action (NFA) letter without deed notice for the heating oil UST. 8 hart hickman SAAAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\IAA.doc SMARTER ENVIRONMENTAL SOLUTIONS Table 1 Summary of Heating Oil UST Soil Sample Results 2827 Cindy Lane Charlotte, North Carolina H&H Job. No. CHP-035 5030/ 3550/ Analytical Method 8015C 8015C MADEP MADEP MADEP MADEP MADEP MADEP MADEP MADEP 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8260B 8270D ca U U U U U C C Contaminant of Concern t Q Q m m o o m m N N Q Q Q Q Q N Q U N N N 7 f9 co CV U O U N N N N C N N O O U 0 L6 C� C� .0 C6 U >, Q w Q U H O Q U N i Date Sample Incident = _ _ _ _ _ _ = E F0 2 00 m U 2 5 4 6 o .-L Sample ID Collected Source Area Depth (ft) Phase > > w w > w Q H c °vi � z N M X in Q °' SB-1 03/16/18 UST 8-9 ESA 47.9 <3.69 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SB-2 03/16/18 UST 7-8 ESA 567 3.86 J NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA UST-1 01/02/19 UST 6 CL 380 4,700 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA SW-1 01/03/19 UST 18 IA NA NA <5.6 <5.6 <31 BRL <31 <5.6 <12 BRL <0.0087 <0.0087 <0.0087 <0.0087 <0.017 <0.0087 <0.0087 <0.0087 <0.026 ALL BRL SW-2 01/03/19 UST 18 IA NA NA <6.9 <6.9 1 <31 BRL <31 1 <6.9 <12 BRL <0.0066 <0.0066 <0.0066 1 <0.0066 <0.013 <0.0066 1 <0.0066 <0.0066 <0.020 ALL BRL SW-3 01/03/19 UST 18 IA NA NA <6.2 18 <31 18 <31 <6.2 <13 BRL 0.011 0.019 0.0081 0.014 0.016 0.44 0.19 0.083 0.060 ALL BRL SW-4 01/03/19 UST 18 IA NA NA <6.1 <6.1 <31 BRL <31 <6.1 <13 BRL <0.0060 <0.0060 <0.0060 <0.0060 <0.012 <0.0060 <0.0060 <0.0060 <0.018 ALL BRL B-1 01/03/19 UST 22 IA NA NA <6.2 <6.2 <31 BRL <31 <6.2 <12 BRL <0.0061 <0.0061 <0.0061 <0.0061 <0.012 <0.0061 <0.0061 <0.0061 <0.0012 ALL BRL Action Level (mg/kg) 50 100 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS Soil to Ground Water MSCC (mg/kg) NS NS 68 NS 540 540 NS NS NS 31 1.7 3.3 3.4 1.7 0.16 8.5 8.3 0.12 4.6 6.6 Residential MSCC (mg/kg) NS NS 939 NS 1,500 1,500 31,000 NS NS 469 626 626 626 1,564 313 782 782 100 3,129 46 Industrial/Commercial MSCC (mg/kg) NS NS 24,528 NS 40,000 40,000 810,000 NS NS 12,264 16,350 16,350 16,350 40,880 8,176 20,440 20,440 l 4,000 81,760 410 Notes: Apart from VPH and EPH, only those compounds detected are shown. Concentrations are reported in milligrams per kilogram (mg/kg). UST = Underground Storage Tank Basin; ESA = Phase II Envriommnetal Site Assessment; CL = Closure Sample; IA = Initial Abatement Sample; TPH = Total Petroleum Hydrocarbons; GRO = Gasoline Range Organics; DRO = Diesel Range Organics; MADEP = Massachusetts Department of Environmental Protection; VPH = Volatile Petroleum Hydrocarbons; EPH = Extractable Petroleum Hydrocarbons; NA = Not Analyzed; NS = Not Specified; MSCC = Maximum Soil Contaminant Concentration; ND = Not Detected; BRL = Below Reporting Limits Table 1 (Page 1 of 1) S:\AAA-Master Projects\Charlotte Mecklenburg Housing Partnership - CHP\CHP-035 Cindy Lane Heating Oil UST\Tables\Soil Data pp 2/1/2019 Hart & Hickman, PC liL!illl*Y- HAM �- �'.,'� ' � .,'�##te�villel{,oiLdr` :� '�i � •�'�� 1 i � 5wf _,. l i fir* • # . y . �.*''. • * i 14!! �kl � � r �- }r } I � L� ! -I �1'' �L'*'i � Y-ter • �* - � -' eI\ * 3 ;�-- r '� Exp .IPI •mac_ �r I r- {I �i � F � • Ir � tilr4�+rIN$ J1w� � {'r * � ���J i .DLO I h _ •�- y �s .►•' ' _ } III' .�' - i +; y •- • xi } j `� � •1 i ��I� � r _off y1 ' II :• t� �._— 40( 780 APPROXIMATE w 0 2000 4000 SCALE IN FEET U.S.G.S. QUADRANGLE MAP DERITA, NORTH CAROLINA, 1996 QUADRANGLE 7.5 MINUTE SERIES (TOPOGRAPHIC) '-A � � � �j . � f� � ^k _ , IL. . If , 4 - f � s� . ' it dill HEATING ~ ! '•. 2EusI \ Kitt H�@��/ .. . ME. . AoEN - -LOC # - o,�� , � ¥ - , , . � � . ®• \. is N UST SAMPLE LOCATION MAP ST�EPROPERTY BOUNDARY DL ON LAKES PROPERTY �unRGauoSTORAGE TANK CINDY LANE CHARLOTTE NORTH CAROLINA L BORING LOCATION haft h|Ckman South 2hCa \ IOU z aim#> 80313$ Ir"PrImuelml SmAnxm �mc,cap #(-..clogy a mG:MATE o e 13DATE: 1- a @ REVISION NO.o ECALE IN FEET FJOB c Ss FIGURE ,2 _ SW-2 r I I I SW-3 I O $1 I OO ® I Qr SWA I UST11 41 r r I i I S W-1 I FORMER RESIDENCE LOCATION (2837 CINDY LANE) LEGEND FORMER RESIDENCE UNDERGROUND STORAGE -- TANK EXCAVATION FORMER UNDERGROUND --- STORAGE TANK POST -EXCAVATION CONFIRMATION SOIL SAMPLE 0 CLOSURE SOIL SAMPLE TING OIL UST a APPROXIMATE 10 20 SCALE IN FEET Appendix A Laboratory Analytical Reports 14 hart hickman SMARTER EWRONMENTAL SOLUTIONS TestAmerica ° THE LEADER IN ENVIRONMENTAL TESTING ANALYTICAL REPORT TestAmerica Laboratories, Inc. TestAmerica Nashville 2960 Foster Creighton Drive Nashville, TN 37204 Tel: (615)726-0177 TestAmerica Job ID: 490-148361-1 TestAmerica Sample Delivery Group: NVR-006 Client Project/Site: Dillion Lakes Property For: Hart & Hickman, PC 2923 S Tryon Street Suite 100 Charlotte, North Carolina 28203 Attn: Matt Ingalls Authorized for release by. 3/28/2018 4:46:46 PM Ken Hayes, Project Manager II (615)301-5035 ken.hayes@testamericainc.com The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property Table of Contents TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Cover Page .............................................. 1 Table of Contents ......................................... 2 Sample Summary ......................................... 3 Case Narrative ........................................... 4 Definitions............................................... 6 Client Sample Results ...................................... 7 QC Sample Results ........................................ 21 QC Association ........................................... 39 Chronicle................................................ 43 Method Summary ......................................... 45 Certification Summary ...................................... 46 Chain of Custody .......................................... 47 TestAmerica Nashville Page 2 of 48 3/28/2018 Sample Summary Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Lab Sample ID Client Sample ID Matrix Collected Received 490-148361-1 DPT-1 Soil (1-2) Solid 03/13/18 10:30 03/17/18 09:50 490-148361-2 DPT-2 soil (0.5-1.0) Solid 03/13/18 15:05 03/17/18 09:50 490-148361-3 DPT-3 soil (2-3) Solid 03/13/18 18:15 03/17/18 09:50 490-148361-4 SB-1 (8-9) Solid 03/16/18 18:15 03/17/18 09:50 490-148361-5 SB-2 (7-8) Solid 03/16/18 20:00 03/17/18 09:50 TestAmerica Nashville Page 3 of 48 3/28/2018 Case Narrative Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property Job ID: 490-148361-1 Laboratory: TestAmerica Nashville Narrative Comments No additional comments. Receipt The samples were received on 3/17/2018 9:50 AM; The temperature of the cooler at receipt was 3.11 C. TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Job Narrative 490-148361-1 the samples arrived in good condition, properly preserved and, where required, on ice. GC/MS VOA Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with analytical batch 490-502356. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC/MS Semi VOA Method 8270D: The continuing calibration verification (CCV) associated with batch 490-502850 recovered above the upper control limit for Phenol, N-Nitrosodi-n-propylamine and 4,6-Dinitro-2-methylphenol. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been reported. The following samples were impacted: DPT-1 Soil (1-2) (490-148361-1), DPT-2 soil (0.5-1.0) (490-148361-2) and DPT-3 soil (2-3) (490-148361-3). Method 8270D: Internal standard responses were outside of acceptance limits for the following sample: (490-148326-F-1-C MSD). The sample(s) shows evidence of matrix interference. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. GC Semi VOA Method 8015C: Surrogate recovery for the following sample was outside control limits: SIB-1 (8-9) (490-148361-4). Evidence of matrix interference is present; therefore, re -extraction and/or re -analysis was not performed. Method 8015C: The following sample was diluted due to the nature of the sample matrix: SB-1 (8-9) (490-148361-4). Elevated reporting limits (RLs) are provided. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Metals Method 6020B: The method blank for preparation batch 490-503276 and analytical batch 490-504079 contained Lead above the method detection limit (MDL). Associated samples were not re -analyzed because results were less than the reporting limit (RL). Method 6020B: The method blank for preparation batch 490-503276 and analytical batch 490-504079 contained Manganese above the reporting limit (RL). Associated sample were not re -extracted and/or re -analyzed because results were greater than 10X the value found in the method blank. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica Nashville Page 4 of 48 3/28/2018 Case Narrative Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property Job ID: 490-148361-1 (Contin Laboratory: TestAmerica Nashville (Continued) VOA Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Page 5 of 48 TestAmerica Nashville 3/28/2018 Definitions/Glossary Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property uualivers TestAmerica Job ID: 490-148361-1 SDG: NVR-006 GC/MS VOA Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. GUMS Semi VOA Qualifier Qualifier Description ISTD response or retention time outside acceptable limits GC Semi VOA Qualifier Qualifier Description X Surrogate is outside control limits J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Metals Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. B Compound was found in the blank and sample. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TestAmerica Nashville Page 6 of 48 3/28/2018 Client Sample Results Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property Client Sample ID: SB-1 (8-9) Date Collected: 03/16/18 18:15 Date Received: 03/17/18 09:50 TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Lab Sample ID: 490-148361-4 Matrix: Solid Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C6-CIO) 47.9 7.98 3.99 mg/Kg * 03/16/18 17:15 03/21/18 12:57 1 • Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac a,a,a-Trifluorotoluene 76 50- 150 03/16/18 17:15 03121118 12:57 1 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Diesel Range Organics [C10-C28] 567 27.1 13.5 mg/Kg 03/20/18 09:57 03/21/18 19:45 4 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac o-Terphenyl (Surr) 185 X 50 -150 03120118 09:57 03121118 19:45 4 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 71.2 0.1 0.1 % 03/19118 15:17 1 TestAmerica Nashville Page 19 of 48 3/28/2018 Client Sample Results Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property Client Sample ID: SB-2 (7-8) Date Collected: 03/16/18 20:00 Date Received: 03/17/18 09:50 TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Lab Sample ID: 490-148361-5 Matrix: Solid Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C6-C10) <3.69 7.37 3.69 mg/Kg 03/16/18 19:00 03/21/18 13:33 1 • Surrogate %Recovery Qualifier Limits Prepared Analyzed DU Fac a,a,a-Trifluorotoluene 75 50- 150 03/16/18 19:00 03121118 13:33 1 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Diesel Range Organics [C10-C28] 3.86 J 6.34 3.17 mg/Kg * 03/20/18 09:57 03/21/18 20:02 1 %Recovery Qualifier Limits Prepared Analyzed Dil Fac LSurrogate o-Terphenyl (Surr) 81 50 -150 03/20/18 09:57 03121118 20:02 1 General Chemistry Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac Percent Solids 78.9 0.1 0.1 % 03/19118 15:17 1 TestAmerica Nashville Page 20 of 48 3/28/2018 QC Sample Results Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-148326-F-1-B MS Matrix: Solid Analysis Batch: 502417 Analyte 2,6-Dinitrotoluene Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno[1,2,3-cd]pyrene Isophorone 1-Methylnaphthalene 2-Methylnaphthalene 2-Methylphenol 3 & 4 Methylphenol Naphthalene 2-Nitroaniline 3-Nitroaniline 4-Nitroaniline Nitrobenzene 2-Nitrophenol 4-Nitrophenol N-N itrosod i-n-propylamine n-Nitrosodiphenylamine(as diphenylamine) Pentachlorophenol Phenanthrene Phenol Pyrene 1,2,4-Trichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Surrogate 2-Fluorobiphenyl (Surr) 2-Fluorophenol (Surr) Nitrobenzene-d5 (Surr) Phenol-d5 (Surr) Terphenyl-d14 (Surr) 2,4,6-Tribromophenol (Surr) Sample Sample Result Qualifier Spike Added MS MS Result Qualifier Unit <0.262 1.98 1.734 mg/Kg <0.209 1.98 1.713 mg/Kg <0.0400 1.98 1.730 mg/Kg <0.0341 1.98 1.646 mg/Kg <0.294 1.98 1.785 mg/Kg <0.196 1.98 1.458 mg/Kg <0.176 1.98 0.8188 mg/Kg <0.213 1.98 1.298 mg/Kg <0.0341 1.98 1.515 mg/Kg <0.221 1.98 1.578 mg/Kg <0.0329 1.98 1.456 mg/Kg <0.0306 1.98 1.431 mg/Kg <0.254 1.98 1.676 mg/Kg <0.239 1.98 1.732 mg/Kg <0.0341 1.98 1.342 mg/Kg <0.243 1.98 1.654 mg/Kg <0.270 1.98 1.743 mg/Kg <0.280 1.98 1.835 mg/Kg <0.236 1.98 1.460 mg/Kg <0.286 1.98 1.454 mg/Kg <0.449 3.95 3.963 mg/Kg <0.228 1.98 1.792 mg/Kg <0.0623 1.68 1.342 mg/Kg Client Sample ID: Matrix Spike Prep Type: Total/NA Prep Batch: 502405 %Rec. D %Rec Limits 88 24-120 87 27-130 88 10-143 83 20-120 90 25-120 74 10-120 41 10-120 66 10-120 77 22-121 80 24-120 74 10-120 72 13-120 85 23-120 88 19-120 68 10-120 84 31 -120 88 31 -120 93 28-120 74 19-120 74 23-120 100 16-139 91 24-120 80 26-150 <0.313 3.95 3.782 mg/Kg # 96 19 -145 <0.0400 1.98 1.491 mg/Kg 75 21 -122 <0.239 1.98 1.867 mg/Kg 94 15 -120 <0.0400 1.98 1.388 mg/Kg 70 20 -123 <0.213 1.98 1.345 mg/Kg 68 14 -120 <0.256 1.98 1.618 mg/Kg 82 27 -120 <0.226 1.98 1.540 mg/Kg 78 24 -122 MS MS %Recovery Qualifier Limits 63 29-120 65 10-120 70 27-120 82 10-120 79 13-120 110 10-120 Lab Sample ID: 490-148326-F-1-C MSD Matrix: Solid Analysis Batch: 502417 Sample Sample Analyte Result Qualifier Acenaphthene <0.0376 Acenaphthylene <0.0341 Anthracene <0.0341 Spike MSD MSD Added Result Qualifier 1.97 1.488 1.97 1.642 1.97 1.650 Client Sample ID: Matrix Spike Duplicate Prep Type: Total/NA Prep Batch: 502405 %Rec. RPD Unit D %Rec Limits RPD Limit mg/Kg 3:� 76 19-120 6 50 mg/Kg 3:� 84 25-120 4 50 mg/Kg 3:� 84 28-125 8 49 TestAmerica Nashville Page 30 of 48 3/28/2018 QC Sample Results Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: 490-148326-F-1-C MSD Client Sample ID: Matrix Spike Duplicate Matrix: Solid Prep Type: Total/NA Analysis Batch: 502417 Prep Batch: 502405 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Benzo[a]anthracene <0.0353 1.97 1.684 mg/Kg 86 23 -120 10 50 Benzo[a]pyrene <0.0317 1.97 1.765 mg/Kg 90 15 -128 10 50 Benzo[b]fluoranthene <0.0329 1.97 1.873 mg/Kg 95 12 -133 15 50 Benzo[g,h,i]perylene <0.0388 1.97 1.590 mg/Kg 3:� 81 22.120 4 50 Benzo[k]fluoranthene <0.0317 1.97 1.759 mg/Kg # 89 28 -120 5 45 Bis(2-chloroethoxy)methane <0.235 1.97 1.491 mg/Kg # 76 24.120 3 50 Bis(2-chloroethyl)ether <0.250 1.97 1.605 . mg/Kg 0 82 22 -120 0 50 bis (2-chloroisopropyl) ether <0.233 1.97 1.476 . mg/Kg 75 20 -120 3 50 Bis(2-ethylhexyl) phthalate <0.243 1.97 1.477 mg/Kg 0 75 26 -120 1 50 4-Bromophenyl phenyl ether <0.241 1.97 1.702 mg/Kg 87 31 -120 6 37 Butyl benzyl phthalate <0.253 1.97 1.441 mg/Kg 73 24 -133 0 50 Carbazole <0.243 1.97 1.700 mg/Kg 87 25 -123 10 46 4-Chloroaniline <0.267 1.97 1.789 mg/Kg 91 26 -120 10 50 4-Chloro-3-methylphenol <0.197 1.97 2.016 mg/Kg 103 21 -120 13 49 2-Chloronaphthalene <0.246 1.97 1.350 mg/Kg 69 24 -120 1 50 2-Chlorophenol <0.224 1.97 1.470 mg/Kg 75 25 -120 3 50 4-Chlorophenyl phenyl ether <0.236 1.97 1.760 mg/Kg 90 26 -120 6 50 Chrysene <0.0435 1.97 1.707 mg/Kg 87 20 -120 9 49 Cresols <0.133 3.93 3.754 mg/Kg 96 10 - 200 10 50 Dibenz(a,h)anthracene <0.0376 1.97 1.677 mg/Kg # 85 12.128 6 50 Dibenzofuran <0.247 1.97 1.656 mg/Kg # 84 21 _ 120 7 50 1,2-Dichlorobenzene <0.223 1.97 1.376 mg/Kg 70 10 -120 1 50 1,3-Dichlorobenzene <0.223 1.97 1.300 mg/Kg 0 66 10 -120 2 50 1,4-Dichlorobenzene <0.230 1.97 1.320 mg/Kg 0 67 10 -120 0 50 3,3'-Dichlorobenzidine <0.240 1.97 1.246 mg/Kg 63 10 -120 11 50 2,4-Dichlorophenol <0.206 1.97 1.462 mg/Kg 74 17 -120 2 50 Diethyl phthalate <0.249 1.97 1.917 mg/Kg 98 29 -122 11 45 2,4-Dimethylphenol <0.394 1.97 1.469 mg/Kg 75 17 -120 3 50 Dimethyl phthalate <0.243 1.97 1.739 mg/Kg 88 30 -120 9 46 Di-n-butyl phthalate <0.248 1.97 1.743 mg/Kg 89 29 -126 8 49 4,6-Dinitro-2-methyl phenol <0.269 3.93 4.162 mg/Kg 106 10 -134 10 50 2,4-Dinitrophenol <0.295 3.93 3.985 mg/Kg 101 10 -150 15 50 2,4-Dinitrotoluene <0.244 1.97 2.199 mg/Kg 112 24 -121 13 50 2,6-Dinitrotoluene <0.262 1.97 1.875 mg/Kg 0 95 24.120 8 50 Di-n-octyl phthalate <0.209 1.97 1.768 mg/Kg 90 27.130 3 50 Fluoranthene <0.0400 1.97 1.956 mg/Kg 100 10 -143 12 50 Fluorene <0.0341 1.97 1.787 mg/Kg # 91 20 -120 8 50 Hexachlorobenzene <0.294 1.97 1.896 mg/Kg # 96 25 -120 6 50 Hexachlorobutadiene <0.196 1.97 1.396 mg/Kg 71 10 -120 4 50 Hexachlorocyclopentadiene <0.176 1.97 0.7147 mg/Kg 36 10 -120 14 50 Hexachloroethane <0.213 1.97 1.305 mg/Kg 66 10 -120 1 50 Indeno[1,2,3-cd]pyrene <0.0341 1.97 1.610 mg/Kg 82 22 -121 6 50 Isophorone <0.221 1.97 1.644 mg/Kg 84 24 -120 4 50 1-Methylnaphthalene <0.0329 1.97 1.529 mg/Kg 78 10 -120 5 50 2-Methylnaphthalene <0.0306 1.97 1.502 mg/Kg 76 13 -120 5 50 2-Methylphenol <0.254 1.97 1.812 mg/Kg 92 23 -120 8 50 3 & 4 Methylphenol <0.239 1.97 1.942 mg/Kg 99 19 -120 11 50 Naphthalene <0.0341 1.97 1.366 mg/Kg 69 10 -120 2 50 TestAmerica Nashville Page 31 of 48 3/28/2018 QC Sample Results Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Gasoline Range Organics) (Continued) — Lab Sample ID: MB 490-502838/9 Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 502838 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C6-CIO) <2.50 5.00 2.50 mg/Kg 03/21/18 12:16 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac a,a,a-Trifluorotoluene 75 L 50- 150 03121118 12:16 1 Lab Sample ID: LCS 490-502838/6 Client Sample ID: Lab Control Sample Matrix: Solid Prep Type: Total/NA Analysis Batch: 502838 Spike LCS LCS %Rec. Analyte Added Result Qualifier Unit D %Rec Limits GRO (C6-C10) 500 530.0 mg/Kg 106 70 -130 LCS LCS Surrogate %Recovery Qualifier Limits a,a,a-Trifluorotoluene 122 50 -150 Lab Sample ID: LCSD 490-502838/7 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 502838 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit GRO (C6-C10) 500 524.2 mg/Kg 105 70 -130 1 21 LCSD LCSD Surrogate %Recovery Qualifier Limits a, a, a-Trifluorotoluene 120 50 -150 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) Lab Sample ID: MB 490-502590/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 502818 Prep Batch: 502590 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Diesel Range Organics [C10-C28] <2.50 5.00 2.50 mg/Kg 03/20/18 09:56 03/21/18 02:16 1 MB MB Surrogate %Recovery Qualifier Limits o-Terphenyl (Surr) 87 50 - 150 Lab Sample ID: LCS 490-502590/2-A Matrix: Solid Analysis Batch: 502818 Spike LCS LCS Analyte Added Result Qualifier Diesel Range Organics 40.0 36.39 [C10-C28] Prepared Analyzed Dil Fac 03/20/18 09:56 03121118 02:16 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 502590 %Rec. Unit D %Rec Limits mg/Kg 91 54 -130 TestAmerica Nashville Page 33 of 48 3/28/2018 QC Sample Results Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Method: 8015C - Nonhalogenated Organics using GC/FID -Modified (Diesel Range Organics) (Continued) Lab Sample ID: LCS 490-502590/2-A Matrix: Solid Analysis Batch: 502818 LCS LCS Surrogate %Recovery Qualifier Limits o-Terphenyl (Surr) 71 50-150 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 502590 Lab Sample ID: 490-148361-5 MS Client Sample ID: SB-2 (7-8) Matrix: Solid Prep Type: Total/NA Analysis Batch: 502981 Prep Batch: 502590 Sample Sample Spike MS MS %Rec. Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits Diesel Range Organics 3.86 J 50.6 64.62 mg/Kg 120 10- 442 [C10-C28] MS MS Surrogate %Recovery Qualifier Limits o-Terphenyl (Surr) 82 50-150 Lab Sample ID: 490-148361-5 MSD Client Sample ID: SB-2 (7-8) Matrix: Solid Prep Type: Total/NA Analysis Batch: 502981 Prep Batch: 502590 Sample Sample Spike MSD MSD %Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Diesel Range Organics 3.86 J 50.0 70.32 mg/Kg 133 10 -142 8 47 [C10-C28] MSD MSD Surrogate %Recovery Qualifier Limits o-Terphenyl (Surr) 71 50-150 Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Lab Sample ID: MB 490-50252911-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 502846 Prep Batch: 502529 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac PCB-1016 <0.0100 0.0333 0.0100 mg/Kg 03/19/1817:09 03/21/1812:53 1 PCB-1221 <0.0100 0.0333 0.0100 mg/Kg 03/19/1817:09 03/21/1812:53 1 PCB-1232 <0.0100 0.0333 0.0100 mg/Kg 03/19/1817:09 03/21/1812:53 1 PCB-1242 a0.0100 0.0333 0.0100 mg/Kg 03/19/1817:09 03/21/1812:53 1 PCB-1248 <0.0100 0.0333 0.0100 mg/Kg 03/19/1817:09 03/21/1812:53 1 PCB-1254 <0.0100 0.0333 0.0100 mg/Kg 03/19/1817:09 03/21/1812:53 1 PCB-1260 <0.0100 0.0333 0.0100 mg/Kg 03/19/1817:09 03/21/1812:53 1 MB MB Surrogate %Recovery Qualifier DCB Decachlorobiphenyl (Surr) 83 Tetrachloro-m-xylene 64 Limits Prepared Analyzed Dil Fac 20 - 150 03119118 17: 09 03121118 12:53 1 19 - 147 03119118 17: 09 03121118 12:53 1 TestAmerica Nashville Page 34 of 48 3/28/2018 QC Association Summary Client: Hart & Hickman, PC Project/Site: Dillion Lakes Property General Chemistry Analysis Batch: 502498 TestAmerica Job ID: 490-148361-1 SDG: NVR-006 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-148361-1 DPT-1 Soil (1-2) Total/NA Solid Moisture 490-148361-2 DPT-2 soil (0.5-1.0) Total/NA Solid Moisture 490-148361-3 DPT-3 soil (2-3) Total/NA Solid Moisture 490-148361-4 SB-1 (8-9) Total/NA Solid Moisture 490-148361-5 SB-2 (7-8) Total/NA Solid Moisture 490-148337-E-7 DU Duplicate Total/NA Solid Moisture Prep Batch: 503252 Lab Sample ID 490-148361-1 490-148361-2 490-148361-3 MB 490-503252/1-A LCSI 490-503252/4-A LCSS 490-503252/2-A LCSSD 490-503252/3-A Analysis Batch: 503340 Client Sample ID DPT-1 Soil (1-2) DPT-2 soil (0.5-1.0) DPT-3 soil (2-3) Method Blank Lab Control Sample Lab Control Sample Lab Control Sample Dup Prep Type Matrix Method Total/NA Solid 3060A Total/NA Solid 3060A Total/NA Solid 3060A Total/NA Solid 3060A Total/NA Solid 3060A Total/NA Solid 3060A Total/NA Solid 3060A Prep Batch Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 490-148361-1 DPT-1 Soil (1-2) Total/NA Solid 7196A 503252 490-148361-2 DPT-2 soil (0.5-1.0) Total/NA Solid 7196A 503252 490-148361-3 DPT-3 soil (2-3) Total/NA Solid 7196A 503252 MB 490-503252/1-A Method Blank Total/NA Solid 7196A 503252 LCSI 490-503252/4-A Lab Control Sample Total/NA Solid 7196A 503252 LCSS 490-503252/2-A Lab Control Sample Total/NA Solid 7196A 503252 LCSSD 490-503252/3-A Lab Control Sample Dup Total/NA Solid 7196A 503252 0 Page 42 of 48 TestAmerica Nashville 3/28/2018 Accreditation/Certification Summary Client: Hart & Hickman, PC TestAmerica Job ID: 490-148361-1 Project/Site: Dillion Lakes Property SDG: NVR-006 Laboratory: TestAmerica Nashville Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. r- Authority Program EPA Region Identification Number Expiration Date North Carolina (WW/SW) State Program 4 387 12-31-18 The following analytes are included in this report, but accreditation/certification is not offered by the governing authority: Analysis Method Prep Method Matrix Analyte Moisture Solid Percent Solids TestAmerica Nashville Page 46 of 48 3/28/2018 TestAmedca THE L.EApER I E f+VIR(}N MEMi AL TE'. TIN r3 Nashville, TN COOLER RECEIPT FORM Charlotte 490-148361 Chain of Cusfady Cooler ReceivedlOpened On 311712018 C& 0950 40 Time Samples Removed From Cooler Time Samples Placed In Storage__—_ tc Hour Window} C L 1. Tracking # � {fast 4 digits, FedEx} Courier: FedEx IR Gun 10 17984353 pH Strip Lot Chlorine Strip Lot __64 2. Temperature of rep. sample or temp blank when opened: Degrees Celsius 3, If Item #2 temperature is 0DC or less, was the representative sample or temp blank frozen? YES 4. Were custody seals on outside of cooler? _ 1NO..ND ES N0... NA y If yes, how many and where' 5. Were the seals intact, signed, and dated correctly? S5.N0...NA 6. Were custody papers inside cooler? E ,NO,. NA I certif that I oj2ened the cooler and answered que5tions 1-6 intial 4;� _ 7. Were custody seals on containers: YES rCp and intact YES...NO. QD Were these signed and dated correctly? YES ... Nt 8. Packing mat'I used? blewr p Plastic bag Peanuts Vermiculite Foam Insert Paper Other None 9, Cooling process: A. Ice -pack Ice (direct contact) Dry Ice Other None 19, Did all contalners arrive in good condition (unbroken)? ,&..NO ... NA 11. Were all container labels complete (#, date, signed, pres., etc)7 4!9 .NO...NA 12. Did all container labels and tags agree with custody papers? �9.1NO...NA ee 13a. Were VOA via Is recivd7 DE...NO...NA b. Was there any observable headspace present in any VOA vial? YES...NO..WP 10 0 Larger than this, 14. Was there a Trip Blank in this cooler? YES(�,a.NA If multiple coolers, sequence # f certify that I unloaded the cooler and arswered questions 7-14 fin Val) 15a, On pres'd bottles, did pH test strips suggest preservation reached the correct pH level? YES ... NO� b. Did the bottle labels indicate that the correct preservatives were used CEESP...N0... NA 16. Was residual chlorine present? I certify that I checked for chlorine and pH as per SOP and answered questions 15-16 Ontiafl :;6�f 17. Were custody papers properly filled out (ink, signed, etc)? F ...NO...NA 18. Did you sign the custody papers in the appropriate place? NO...NA 19. Were correct containers used for the analysis requested? �..NO...NA 20. Was sufficient amount of sample sent in each container? I certify that I entered this project into LIMS and answered questions 17-20 (Intiall i cerUfv that I attached ial 21. Were there Non -Conformance issues at login? YE9.. O Was a NCM generated? YES.. B1S = Aroken in shipirim Cooler Receipt Form. doc LF- ) End of Fonn Page 47 of 48 NA Rc%ised 823. i7 I 3/28/2018 N CD W O OD W N fV O lestHmerica Charlotte 2838--8 Queen City Drive Charlotte, KC 28280 Phone: 704. 392. U64 Fax: Chain of Custody Record 2 5) 5 8 7 0 Regulatory Program: _I. Dry :.I \PD-5 J RCPA er; Al� ► ja 'L TestAmerlca TPE LEAOek EN Er.IVIIZQNIAENTAI TESTNG TestAmerica Laboratories, Inc. TAL-8210 (0713) Client Contact Project Managers Site Contact: �.y ❑ate: COC No: Company Name: yPoAm.Tel/Fax: Lab Contact• r Carrier: of c0cs Address: `j, A alysls Turnaround Time i m E N m = � 0 t ri �c7g �] v g c A o W e q Vj Y `' t "� SK - Sample CitylState/Zlp:L iudii CJIlPNt7AR DAYS [ WORMIG DAYS Far Lab 750Only: Wail[ -in Client Lab Sampling: Phone: 000-7 TAT ifdiiferentfrom Below ❑ 2 weeks y�� ❑ z, � : t k ❑ z days ❑ 1 day Fax: s Project Name !7i Site: Job/ SDG No.: P 0#ak& Sample Identification Sample Date Sample Time sample imp c�ae1 Matrix s of Con+- Sample Specific Notes: D FT—r Y,73119 i5--< G SXXI / y7 ds 400 Preservation Used: 1= Ice, 2= HU; 3= H.2SO' =HNO3; S- —Na QH;. ; Possible Hazard Identification: Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section [f the lab is to dispose of the sample. ample Disposal (A fee may be assessed it samples are retained longer than 1 month] L Return to Client ^ispp581 by lab L� A chive for _Months r—I Non riaxard Flammable J skin IrftM L Poison 8 nknown Special InstructionsfQC Requirements & Comments: �J Pwos ustody 5 is Intact: ❑ Yes Ho Custody Seal No.: oq erTamp. (C): bs erm 1 0.: by: � _ / i bReclir-i'q'Ished Ca pang D� rme: Received Compap r�� Date me: 2JI711 OEM by.Company: Date/Time: Received by: Comps y: crate" me: Relinquished by: Company: Datemme: Received in Laboratory by: Company: DatelTime: W S Asumumamma Case Narrative PRISM NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cert No. 37735 01/11/2019 Environmental Solutions SC Certification No. 99012 ,om `,. LABORATORIES, INC. Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Steve Libbey Project No.: CHP-035 2923 South Tryon St. Ste 100 Lab Submittal Date: 01/04/2019 Charlotte, NC 28203 Prism Work Order: 9010043 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a,j Angela D. Overcash VP Laboratory Services Reviewed By Terri W. Cole For Angela D. Overcash Project Manager Data Qualifiers Key Reference: CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. CVL CCV result is below the control limits. LCS recovery within the limits. Analyte not detected in the sample. No further action taken. DO Surrogates diluted out. L Parameter reported with possible low bias. LCS recovery below the QC limit. L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken. LH High LCS recovery. Analyte not detected in the sample(s). No further action taken. ILL Medium level analysis result below the RL. Low level analysis reported estimated above the calibration range. RLM Sample container suspected to have low methanol content. Results possibly biased high. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 46 Receipt Summary Full -Service Analytical R PRISMSample Environmental Solutions 01/11/2019 LABORATORIES INC. Prism Work Order: 9010043 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received UST-1 9010043-01 Solid 01/02/19 11:20 01/04/19 8:25 SW-1 9010043-02 Solid 01/03/19 15:10 01/04/19 8:25 SW-2 9010043-03 Solid 01/03/19 15:15 01/04/19 8:25 SW-3 9010043-04 Solid 01/03/19 15:20 01/04/19 8:25 SW-4 9010043-05 Solid 01/03/19 15:25 01/04/19 8:25 B-1 9010043-06 Solid 01/03/19 15:30 01/04/19 8:25 Samples were received in good condition at 3.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 46 Full -Service Analytical & �P R I S M Environmental Solutions �. LABORATORIES, INC. Summary of Detections 01/11/2019 Prism Work Order: 9010043 Prism ID Client ID Parameter Method Result Units 9010043-01 UST-1 Diesel Range Organics `8015C 4700 mg/kg dry 9010043-01 UST-1 Gasoline Range Organics '8015C 380 mg/kg dry 9010043-04 SW-3 1,2,4-Trimethylbenzene *8260B 0.44 LL mg/kg dry 9010043-04 SW-3 1,3,5-Trimethylbenzene `8260B 0.19 mg/kg dry 9010043-04 SW-3 4-Isopropyltoluene '8260B 0.083 mg/kg dry 9010043-04 SW-3 Isopropyl benzene (Cumene) *8260B 0.014 mg/kg dry 9010043-04 SW-3 m,p-Xylenes *8260B 0.032 mg/kg dry 9010043-04 SW-3 Naphthalene '8260B 0.016 mg/kg dry 9010043-04 SW-3 n-Propylbenzene "8260B 0.011 mg/kg dry 9010043-04 SW-3 o-Xylene *8260B 0.028 mg/kg dry 9010043-04 SW-3 sec -Butyl benzene `8260B 0.019 mg/kg dry 9010043-04 SW-3 tert-Butylbenzene '8260B 0.0081 mg/kg dry 9010043-04 SW-3 Xylenes, total *8260B 0.060 mg/kg dry 9010043-04 SW-3 C9-C12 Aliphatics `MADEP VPH 18 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 46 P R I S M Full -Service Analytical s Environmental Solutions LABORATORIES INC. Hart & Hickman (Charlotte) Attn: Steve Libbey 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: Cindy Lane UST, Charlotte, NC Project No.: CHP-035 Sample Matrix: Solid Laboratory Report 01 /11 /2019 Client Sample ID: UST-1 Prism Sample ID: 9010043-01 Prism Work Order: 9010043 Time Collected: 01/02/19 11:20 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 4700 mg/kg dry 420 110 50 *8015C 1/7/19 11:39 BGB P9A0072 Surrogate Recovery Control Limits o-Terphenyl 0 % 31-123 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 380 mg/kg dry 5.5 1.2 50 *8015C 1/8/19 10:09 ANGM P9A0090 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 105 % 50-137 General Chemistry Parameters % Solids 83.2 % by 0.100 0.100 1 *SM2540 G 1/8/19 14:30 TJY P9A0141 Weight This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 46 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 01 /11 /2019 Hart & Hickman (Charlotte) Attn: Steve Libbey 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: Cindy Lane UST, Charlotte, NC Project No.: CHP-035 Sample Matrix: Solid Client Sample ID: SW-1 Prism Sample ID: 9010043-02 Prism Work Order: 9010043 Time Collected: 01/03/19 15:10 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 31 3.9 1 *MADEP EPH 1/10/19 12:33 ZRC P9A0103 C19-C36 Aliphatics BRL mg/kg dry 31 6.8 1 *MADEP EPH 1/10/19 12:33 ZRC P9A0103 C11-C22 Aromatics BRL mg/kg dry 12 4.1 1 *MADEP EPH 1/10/19 12:33 ZRC P9A0103 Surrogate Recovery Control Limits 1-Chlorooctadecane 57 % 40-140 o-Terphenyl 73 % 40-140 2-Fluorobiphenyl 77 % 40-140 2-Bromonaphthalene 100 % 40-140 General Chemistry Parameters % Solids 78.3 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 *SM2540 G 1/8/19 14:30 TJY P9A0141 1,2,4-Trichlorobenzene BRL mg/kg dry 0.42 0.065 1 *8270D 1/10/19 17:57 JMV P9A0146 1,2-Dichlorobenzene BRL mg/kg dry 0.42 0.060 1 *8270D 1/10/19 17:57 JMV P9A0146 1,3-Dichlorobenzene BRL mg/kg dry 0.42 0.068 1 *8270D 1/10/19 17:57 JMV P9A0146 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.052 1 *8270D 1/10/19 17:57 JMV P9A0146 2,4,5-Trichlorophenol BRL mg/kg dry 0.42 0.068 1 *8270D 1/10/19 17:57 JMV P9A0146 2,4,6-Trichlorophenol BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 17:57 JMV P9A0146 2,4-Dichlorophenol BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 17:57 JMV P9A0146 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 17:57 JMV P9A0146 2,4-Dinitrophenol BRL mg/kg dry 0.42 0.16 1 *8270D 1/10/19 17:57 JMV P9A0146 2,4-Dinitrotoluene BRL mg/kg dry 0.42 0.080 1 *8270D 1/10/19 17:57 JMV P9A0146 2,6-Dinitrotoluene BRL mg/kg dry 0.42 0.076 1 *8270D 1/10/19 17:57 JMV P9A0146 2-Chloronaphthalene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 17:57 JMV P9A0146 2-Chlorophenol BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 17:57 JMV P9A0146 2-Methyl naphthalene BRL mg/kg dry 0.42 0.059 1 *8270D 1/10/19 17:57 JMV P9A0146 2-Methylphenol BRL mg/kg dry 0.42 0.064 1 *8270D 1/10/19 17:57 JMV P9A0146 2-Nitroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 17:57 JMV P9A0146 2-Nitrophenol BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 17:57 JMV P9A0146 3,3'-Dichlorobenzidine BRL mg/kg dry 0.42 0.034 1 *8270D 1/10/19 17:57 JMV P9A0146 3/4-Methyl phenol BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 17:57 JMV P9A0146 3-Nitroaniline BRL mg/kg dry 0.42 0.14 1 *8270D 1/10/19 17:57 JMV P9A0146 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.42 0.12 1 *8270D 1/10/19 17:57 JMV P9A0146 4-Bromophenyl phenyl ether BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 17:57 JMV P9A0146 4-Chloro-3-methylphenol BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 17:57 JMV P9A0146 4-Chloroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 17:57 JMV P9A0146 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 17:57 JMV P9A0146 4-Nitroaniline BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 17:57 JMV P9A0146 4-Nitrophenol BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 17:57 JMV P9A0146 Acenaphthene BRL mg/kg dry 0.42 0.046 1 *8270D 1/10/19 17:57 JMV P9A0146 Acenaphthylene BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 17:57 JMV P9A0146 Aniline BRL mg/kg dry 0.42 0.083 1 *8270D 1/10/19 17:57 JMV P9A0146 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 46 Laboratory Report ` Full -Service P R S M Analytical & / environmental Solutions LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-1 Attn: Steve Libbey NC Prism Sample ID: 9010043-02 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:10 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anthracene BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 17:57 JMV P9A0146 Azobenzene BRL mg/kg dry 0.42 0.054 1 *8270D 1/10/19 17:57 JMV P9A0146 Benzo(a)anthracene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 17:57 JMV P9A0146 Benzo(a)pyrene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 17:57 JMV P9A0146 Benzo(b)fluoranthene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 17:57 JMV P9A0146 Benzo(g,hJ)perylene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 17:57 JMV P9A0146 Benzo(k)fluoranthene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 17:57 JMV P9A0146 Benzoic Acid BRL mg/kg dry 0.42 0.19 1 *8270D 1/10/19 17:57 JMV P9A0146 Benzyl alcohol BRL mg/kg dry 0.42 0.031 1 *8270D 1/10/19 17:57 JMV P9A0146 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.42 0.045 1 *8270D 1/10/19 17:57 JMV P9A0146 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 17:57 JMV P9A0146 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.052 1 *8270D 1/10/19 17:57 JMV P9A0146 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.42 0.11 1 *8270D 1/10/19 17:57 JMV P9A0146 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.084 1 *8270D 1/10/19 17:57 JMV P9A0146 Chrysene BRL mg/kg dry 0.42 0.078 1 *8270D 1/10/19 17:57 JMV P9A0146 Dibenzo(a,h)anthracene BRL mg/kg dry 0.42 0.067 1 *8270D 1/10/19 17:57 JMV P9A0146 Dibenzofuran BRL mg/kg dry 0.42 0.055 1 *8270D 1/10/19 17:57 JMV P9A0146 Diethyl phthalate BRL mg/kg dry 0.42 0.086 1 *8270D 1/10/19 17:57 JMV P9A0146 Dimethyl phthalate BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 17:57 JMV P9A0146 Di-n-butyl phthalate BRL mg/kg dry 0.42 0.071 1 *8270D 1/10/19 17:57 JMV P9A0146 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.048 1 *8270D 1/10/19 17:57 JMV P9A0146 Fluoranthene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 17:57 JMV P9A0146 Fluorene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 17:57 JMV P9A0146 Hexachlorobenzene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 17:57 JMV P9A0146 Hexachlorobutadiene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 17:57 JMV P9A0146 Hexachlorocyclopentadiene BRL mg/kg dry 0.42 0.075 1 *8270D 1/10/19 17:57 JMV P9A0146 Hexachloroethane BRL mg/kg dry 0.42 0.063 1 *8270D 1/10/19 17:57 JMV P9A0146 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 17:57 JMV P9A0146 Isophorone BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 17:57 JMV P9A0146 Naphthalene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 17:57 JMV P9A0146 Nitrobenzene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 17:57 JMV P9A0146 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 17:57 JMV P9A0146 N-Nitrosodiphenylamine BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 17:57 JMV P9A0146 Pentachlorophenol BRL mg/kg dry 0.42 0.096 1 *8270D 1/10/19 17:57 JMV P9A0146 Phenanthrene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 17:57 JMV P9A0146 Phenol BRL mg/kg dry 0.42 0.038 1 *8270D 1/10/19 17:57 JMV P9A0146 Pyrene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 17:57 JMV P9A0146 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 93 % 37-131 2-Fluorobiphenyl 89 % 47-130 2-Fluorophenol 89 % 44-117 Nitrobenzene-d5 85 % 45-121 Phenol-d5 86 % 37-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 46 Laboratory Report ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-1 Attn: Steve Libbey NC Prism Sample ID: 9010043-02 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:10 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Terphenyl-d14 89 % 38-135 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0087 0.00071 1 *8260B 1/9/19 14:30 ANG P9A0133 1,1,1-Trichloroethane BRL mg/kg dry 0.0087 0.00042 1 *8260B 1/9/19 14:30 ANG P9A0133 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0087 0.00059 1 *8260B 1/9/19 14:30 ANG P9A0133 1,1,2-Trichloroethane BRL mg/kg dry 0.0087 0.00077 1 *8260B 1/9/19 14:30 ANG P9A0133 1,1-Dichloroethane BRL mg/kg dry 0.0087 0.00024 1 *8260B 1/9/19 14:30 ANG P9A0133 1,1-Dichloroethylene BRL mg/kg dry 0.0087 0.00038 1 *8260B 1/9/19 14:30 ANG P9A0133 1,1-Dichloropropylene BRL mg/kg dry 0.0087 0.00048 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0087 0.00049 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2,3-Trichloropropane BRL mg/kg dry 0.0087 0.0011 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0087 0.00065 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0087 0.00066 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2-Dibromoethane BRL mg/kg dry 0.0087 0.00035 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2-Dichlorobenzene BRL mg/kg dry 0.0087 0.00041 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2-Dichloroethane BRL mg/kg dry 0.0087 0.00052 1 *8260B 1/9/19 14:30 ANG P9A0133 1,2-Dichloropropane BRL mg/kg dry 0.0087 0.00054 1 *8260B 1/9/19 14:30 ANG P9A0133 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0087 0.00066 1 *8260B 1/9/19 14:30 ANG P9A0133 1,3-Dichlorobenzene BRL mg/kg dry 0.0087 0.00057 1 *8260B 1/9/19 14:30 ANG P9A0133 1,3-Dichloropropane BRL mg/kg dry 0.0087 0.00044 1 *8260B 1/9/19 14:30 ANG P9A0133 1,4-Dichlorobenzene BRL mg/kg dry 0.0087 0.00034 1 *8260B 1/9/19 14:30 ANG P9A0133 2,2-Dichloropropane BRL mg/kg dry 0.0087 0.00041 1 *8260B 1/9/19 14:30 ANG P9A0133 2-Chlorotoluene BRL mg/kg dry 0.0087 0.00045 1 *8260B 1/9/19 14:30 ANG P9A0133 4-Chlorotoluene BRL mg/kg dry 0.0087 0.00052 1 *8260B 1/9/19 14:30 ANG P9A0133 4-Isopropyltoluene BRL mg/kg dry 0.0087 0.00042 1 *8260B 1/9/19 14:30 ANG P9A0133 Acetone BRL mg/kg dry 0.087 0.0021 1 *8260B 1/9/19 14:30 ANG P9A0133 Benzene BRL mg/kg dry 0.0052 0.00050 1 *8260B 1/9/19 14:30 ANG P9A0133 Bromobenzene BRL mg/kg dry 0.0087 0.00072 1 *8260B 1/9/19 14:30 ANG P9A0133 Bromochloromethane BRL mg/kg dry 0.0087 0.00048 1 *8260B 1/9/19 14:30 ANG P9A0133 Bromodichloromethane BRL mg/kg dry 0.0087 0.00048 1 *8260B 1/9/19 14:30 ANG P9A0133 Bromoform BRL mg/kg dry 0.0087 0.00099 1 *8260B 1/9/19 14:30 ANG P9A0133 Bromomethane BRL CVL mg/kg dry 0.017 0.0011 1 *8260B 1/9/19 14:30 ANG P9A0133 Carbon Tetrachloride BRL mg/kg dry 0.0087 0.00043 1 *8260B 1/9/19 14:30 ANG P9A0133 Chlorobenzene BRL mg/kg dry 0.0087 0.00046 1 *8260B 1/9/19 14:30 ANG P9A0133 Chloroethane BRL mg/kg dry 0.017 0.00072 1 *8260B 1/9/19 14:30 ANG P9A0133 Chloroform BRL mg/kg dry 0.0087 0.00063 1 *8260B 1/9/19 14:30 ANG P9A0133 Chloromethane BRL CVL mg/kg dry 0.0087 0.00058 1 *8260B 1/9/19 14:30 ANG P9A0133 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0087 0.00037 1 *8260B 1/9/19 14:30 ANG P9A0133 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0087 0.00029 1 *8260B 1/9/19 14:30 ANG P9A0133 Dibromochloromethane BRL mg/kg dry 0.0087 0.00036 1 *8260B 1/9/19 14:30 ANG P9A0133 Dichlorodifluoromethane BRL mg/kg dry 0.0087 0.00039 1 *8260B 1/9/19 14:30 ANG P9A0133 Ethylbenzene BRL mg/kg dry 0.0087 0.00033 1 *8260B 1/9/19 14:30 ANG P9A0133 Isopropyl Ether BRL mg/kg dry 0.0087 0.00035 1 *8260B 1/9/19 14:30 ANG P9A0133 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 46 Laboratory Report ` Full -Service Analytical & / Environmental Solutions P R S M LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-1 Attn: Steve Libbey NC Prism Sample ID: 9010043-02 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:10 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Isopropylbenzene (Cumene) BRL mg/kg dry 0.0087 0.00051 1 *8260B 1/9/19 14:30 ANG P9A0133 m,p-Xylenes BRL mg/kg dry 0.017 0.00080 1 *8260B 1/9/19 14:30 ANG P9A0133 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.087 0.00078 1 *8260B 1/9/19 14:30 ANG P9A0133 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.17 0.00078 1 *8260B 1/9/19 14:30 ANG P9A0133 Methyl Isobutyl Ketone BRL mg/kg dry 0.087 0.00074 1 *8260B 1/9/19 14:30 ANG P9A0133 Methylene Chloride BRL mg/kg dry 0.017 0.00049 1 *8260B 1/9/19 14:30 ANG P9A0133 Methyl-tert-Butyl Ether BRL mg/kg dry 0.017 0.00028 1 *8260B 1/9/19 14:30 ANG P9A0133 Naphthalene BRL mg/kg dry 0.017 0.00027 1 *8260B 1/9/19 14:30 ANG P9A0133 n-Butylbenzene BRL mg/kg dry 0.0087 0.00044 1 *8260B 1/9/19 14:30 ANG P9A0133 n-Propylbenzene BRL mg/kg dry 0.0087 0.00052 1 *8260B 1/9/19 14:30 ANG P9A0133 o-Xylene BRL mg/kg dry 0.0087 0.00036 1 *8260B 1/9/19 14:30 ANG P9A0133 sec-Butylbenzene BRL mg/kg dry 0.0087 0.00042 1 *8260B 1/9/19 14:30 ANG P9A0133 Styrene BRL mg/kg dry 0.0087 0.00052 1 *8260B 1/9/19 14:30 ANG P9A0133 tert-Butylbenzene BRL mg/kg dry 0.0087 0.00029 1 *8260B 1/9/19 14:30 ANG P9A0133 Tetrachloroethylene BRL mg/kg dry 0.0087 0.00041 1 *8260B 1/9/19 14:30 ANG P9A0133 Toluene BRL mg/kg dry 0.0087 0.00050 1 *8260B 1/9/19 14:30 ANG P9A0133 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0087 0.00052 1 *8260B 1/9/19 14:30 ANG P9A0133 trans- 1,3-Dichloropropylene BRL mg/kg dry 0.0087 0.00046 1 *8260B 1/9/19 14:30 ANG P9A0133 Trichloroethylene BRL mg/kg dry 0.0087 0.00056 1 *8260B 1/9/19 14:30 ANG P9A0133 Trichlorofluoromethane BRL mg/kg dry 0.0087 0.00056 1 *8260B 1/9/19 14:30 ANG P9A0133 Vinyl acetate BRL CCV mg/kg dry 0.043 0.0012 1 *8260B 1/9/19 14:30 ANG P9A0133 Vinyl chloride BRL mg/kg dry 0.0087 0.00042 1 *8260B 1/9/19 14:30 ANG P9A0133 Xylenes, total BRL mg/kg dry 0.026 0.0016 1 *8260B 1/9/19 14:30 ANG P9A0133 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 104 % 84-123 Toluene-d8 87 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 5.6 0.18 100 *MADEP VPH 1/7/19 18:20 ANG/J P9A0082 C9-Cl2 Aliphatics BRL mg/kg dry 5.6 0.29 100 *MADEP VPH 1/7/19 18:20 ANG/J P9A0082 C9-C10 Aromatics BRL mg/kg dry 5.6 0.063 100 *MADEP VPH 1/7/19 18:20 ANG/J P9A0082 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 118 % 70-130 2,5-Dibromotoluene (FID) 129 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 46 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 01 /11 /2019 Hart & Hickman (Charlotte) Attn: Steve Libbey 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: Cindy Lane UST, Charlotte, NC Project No.: CHP-035 Sample Matrix: Solid Client Sample ID: SW-2 Prism Sample ID: 9010043-03 Prism Work Order: 9010043 Time Collected: 01/03/19 15:15 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 31 3.9 1 *MADEP EPH 1/10/19 13:10 ZRC P9A0103 C19-C36 Aliphatics BRL mg/kg dry 31 6.8 1 *MADEP EPH 1/10/19 13:10 ZRC P9A0103 C11-C22 Aromatics BRL mg/kg dry 12 4.1 1 *MADEP EPH 1/10/19 13:10 ZRC P9A0103 Surrogate Recovery Control Limits 1-Chlorooctadecane 64 % 40-140 o-Terphenyl 64 % 40-140 2-Fluorobiphenyl 80 % 40-140 2-Bromonaphthalene 104 % 40-140 General Chemistry Parameters % Solids 77.8 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 *SM2540 G 1/8/19 14:30 TJY P9A0141 1,2,4-Trichlorobenzene BRL mg/kg dry 0.42 0.065 1 *8270D 1/10/19 18:19 JMV P9A0146 1,2-Dichlorobenzene BRL mg/kg dry 0.42 0.060 1 *8270D 1/10/19 18:19 JMV P9A0146 1,3-Dichlorobenzene BRL mg/kg dry 0.42 0.068 1 *8270D 1/10/19 18:19 JMV P9A0146 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.052 1 *8270D 1/10/19 18:19 JMV P9A0146 2,4,5-Trichlorophenol BRL mg/kg dry 0.42 0.068 1 *8270D 1/10/19 18:19 JMV P9A0146 2,4,6-Trichlorophenol BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 18:19 JMV P9A0146 2,4-Dichlorophenol BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:19 JMV P9A0146 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:19 JMV P9A0146 2,4-Dinitrophenol BRL mg/kg dry 0.42 0.16 1 *8270D 1/10/19 18:19 JMV P9A0146 2,4-Dinitrotoluene BRL mg/kg dry 0.42 0.080 1 *8270D 1/10/19 18:19 JMV P9A0146 2,6-Dinitrotoluene BRL mg/kg dry 0.42 0.076 1 *8270D 1/10/19 18:19 JMV P9A0146 2-Chloronaphthalene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:19 JMV P9A0146 2-Chlorophenol BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 18:19 JMV P9A0146 2-Methyl naphthalene BRL mg/kg dry 0.42 0.059 1 *8270D 1/10/19 18:19 JMV P9A0146 2-Methylphenol BRL mg/kg dry 0.42 0.064 1 *8270D 1/10/19 18:19 JMV P9A0146 2-Nitroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:19 JMV P9A0146 2-Nitrophenol BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:19 JMV P9A0146 3,3'-Dichlorobenzidine BRL mg/kg dry 0.42 0.034 1 *8270D 1/10/19 18:19 JMV P9A0146 3/4-Methyl phenol BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 18:19 JMV P9A0146 3-Nitroaniline BRL mg/kg dry 0.42 0.14 1 *8270D 1/10/19 18:19 JMV P9A0146 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.42 0.12 1 *8270D 1/10/19 18:19 JMV P9A0146 4-Bromophenyl phenyl ether BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:19 JMV P9A0146 4-Chloro-3-methylphenol BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 18:19 JMV P9A0146 4-Chloroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:19 JMV P9A0146 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 18:19 JMV P9A0146 4-Nitroaniline BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 18:19 JMV P9A0146 4-Nitrophenol BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 18:19 JMV P9A0146 Acenaphthene BRL mg/kg dry 0.42 0.046 1 *8270D 1/10/19 18:19 JMV P9A0146 Acenaphthylene BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:19 JMV P9A0146 Aniline BRL mg/kg dry 0.42 0.083 1 *8270D 1/10/19 18:19 JMV P9A0146 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 46 Laboratory Report ` Full -Service P R S M Analytical & / environmental Solutions LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-2 Attn: Steve Libbey NC Prism Sample ID: 9010043-03 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:15 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anthracene BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 18:19 JMV P9A0146 Azobenzene BRL mg/kg dry 0.42 0.054 1 *8270D 1/10/19 18:19 JMV P9A0146 Benzo(a)anthracene BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 18:19 JMV P9A0146 Benzo(a)pyrene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:19 JMV P9A0146 Benzo(b)fluoranthene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 18:19 JMV P9A0146 Benzo(g,hJ)perylene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 18:19 JMV P9A0146 Benzo(k)fluoranthene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:19 JMV P9A0146 Benzoic Acid BRL mg/kg dry 0.42 0.19 1 *8270D 1/10/19 18:19 JMV P9A0146 Benzyl alcohol BRL mg/kg dry 0.42 0.031 1 *8270D 1/10/19 18:19 JMV P9A0146 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.42 0.044 1 *8270D 1/10/19 18:19 JMV P9A0146 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:19 JMV P9A0146 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.052 1 *8270D 1/10/19 18:19 JMV P9A0146 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.42 0.11 1 *8270D 1/10/19 18:19 JMV P9A0146 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.084 1 *8270D 1/10/19 18:19 JMV P9A0146 Chrysene BRL mg/kg dry 0.42 0.078 1 *8270D 1/10/19 18:19 JMV P9A0146 Dibenzo(a,h)anthracene BRL mg/kg dry 0.42 0.067 1 *8270D 1/10/19 18:19 JMV P9A0146 Dibenzofuran BRL mg/kg dry 0.42 0.055 1 *8270D 1/10/19 18:19 JMV P9A0146 Diethyl phthalate BRL mg/kg dry 0.42 0.086 1 *8270D 1/10/19 18:19 JMV P9A0146 Dimethyl phthalate BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 18:19 JMV P9A0146 Di-n-butyl phthalate BRL mg/kg dry 0.42 0.071 1 *8270D 1/10/19 18:19 JMV P9A0146 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.048 1 *8270D 1/10/19 18:19 JMV P9A0146 Fluoranthene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 18:19 JMV P9A0146 Fluorene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 18:19 JMV P9A0146 Hexachlorobenzene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:19 JMV P9A0146 Hexachlorobutadiene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 18:19 JMV P9A0146 Hexachlorocyclopentadiene BRL mg/kg dry 0.42 0.075 1 *8270D 1/10/19 18:19 JMV P9A0146 Hexachloroethane BRL mg/kg dry 0.42 0.063 1 *8270D 1/10/19 18:19 JMV P9A0146 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 18:19 JMV P9A0146 Isophorone BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 18:19 JMV P9A0146 Naphthalene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:19 JMV P9A0146 Nitrobenzene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:19 JMV P9A0146 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 18:19 JMV P9A0146 N-Nitrosodiphenylamine BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:19 JMV P9A0146 Pentachlorophenol BRL mg/kg dry 0.42 0.096 1 *8270D 1/10/19 18:19 JMV P9A0146 Phenanthrene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:19 JMV P9A0146 Phenol BRL mg/kg dry 0.42 0.038 1 *8270D 1/10/19 18:19 JMV P9A0146 Pyrene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 18:19 JMV P9A0146 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 90 % 37-131 2-Fluorobiphenyl 90 % 47-130 2-Fluorophenol 99 % 44-117 Nitrobenzene-d5 89 % 45-121 Phenol-d5 93 % 37-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 46 Laboratory Report ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-2 Attn: Steve Libbey NC Prism Sample ID: 9010043-03 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:15 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Terphenyl-d14 93 % 38-135 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0066 0.00055 1 *8260B 1/8/19 15:36 ANG P9A0127 1,1,1-Trichloroethane BRL mg/kg dry 0.0066 0.00032 1 *8260B 1/8/19 15:36 ANG P9A0127 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0066 0.00045 1 *8260B 1/8/19 15:36 ANG P9A0127 1,1,2-Trichloroethane BRL mg/kg dry 0.0066 0.00059 1 *8260B 1/8/19 15:36 ANG P9A0127 1,1-Dichloroethane BRL mg/kg dry 0.0066 0.00018 1 *8260B 1/8/19 15:36 ANG P9A0127 1,1-Dichloroethylene BRL mg/kg dry 0.0066 0.00029 1 *8260B 1/8/19 15:36 ANG P9A0127 1,1-Dichloropropylene BRL mg/kg dry 0.0066 0.00036 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0066 0.00038 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2,3-Trichloropropane BRL mg/kg dry 0.0066 0.00085 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0066 0.00049 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0066 0.00051 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2-Dibromoethane BRL mg/kg dry 0.0066 0.00027 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2-Dichlorobenzene BRL mg/kg dry 0.0066 0.00031 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2-Dichloroethane BRL mg/kg dry 0.0066 0.00040 1 *8260B 1/8/19 15:36 ANG P9A0127 1,2-Dichloropropane BRL mg/kg dry 0.0066 0.00041 1 *8260B 1/8/19 15:36 ANG P9A0127 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0066 0.00050 1 *8260B 1/8/19 15:36 ANG P9A0127 1,3-Dichlorobenzene BRL mg/kg dry 0.0066 0.00044 1 *8260B 1/8/19 15:36 ANG P9A0127 1,3-Dichloropropane BRL mg/kg dry 0.0066 0.00033 1 *8260B 1/8/19 15:36 ANG P9A0127 1,4-Dichlorobenzene BRL mg/kg dry 0.0066 0.00026 1 *8260B 1/8/19 15:36 ANG P9A0127 2,2-Dichloropropane BRL mg/kg dry 0.0066 0.00032 1 *8260B 1/8/19 15:36 ANG P9A0127 2-Chlorotoluene BRL mg/kg dry 0.0066 0.00034 1 *8260B 1/8/19 15:36 ANG P9A0127 4-Chlorotoluene BRL mg/kg dry 0.0066 0.00040 1 *8260B 1/8/19 15:36 ANG P9A0127 4-Isopropyltoluene BRL mg/kg dry 0.0066 0.00032 1 *8260B 1/8/19 15:36 ANG P9A0127 Acetone BRL mg/kg dry 0.066 0.0016 1 *8260B 1/8/19 15:36 ANG P9A0127 Benzene BRL mg/kg dry 0.0040 0.00039 1 *8260B 1/8/19 15:36 ANG P9A0127 Bromobenzene BRL mg/kg dry 0.0066 0.00055 1 *8260B 1/8/19 15:36 ANG P9A0127 Bromochloromethane BRL mg/kg dry 0.0066 0.00037 1 *8260B 1/8/19 15:36 ANG P9A0127 Bromodichloromethane BRL mg/kg dry 0.0066 0.00037 1 *8260B 1/8/19 15:36 ANG P9A0127 Bromoform BRL mg/kg dry 0.0066 0.00075 1 *8260B 1/8/19 15:36 ANG P9A0127 Bromomethane BRL mg/kg dry 0.013 0.00082 1 *8260B 1/8/19 15:36 ANG P9A0127 Carbon Tetrachloride BRL mg/kg dry 0.0066 0.00033 1 *8260B 1/8/19 15:36 ANG P9A0127 Chlorobenzene BRL mg/kg dry 0.0066 0.00035 1 *8260B 1/8/19 15:36 ANG P9A0127 Chloroethane BRL mg/kg dry 0.013 0.00055 1 *8260B 1/8/19 15:36 ANG P9A0127 Chloroform BRL mg/kg dry 0.0066 0.00048 1 *8260B 1/8/19 15:36 ANG P9A0127 Chloromethane BRL mg/kg dry 0.0066 0.00045 1 *8260B 1/8/19 15:36 ANG P9A0127 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0066 0.00028 1 *8260B 1/8/19 15:36 ANG P9A0127 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0066 0.00022 1 *8260B 1/8/19 15:36 ANG P9A0127 Dibromochloromethane BRL mg/kg dry 0.0066 0.00027 1 *8260B 1/8/19 15:36 ANG P9A0127 Dichlorodifluoromethane BRL mg/kg dry 0.0066 0.00030 1 *8260B 1/8/19 15:36 ANG P9A0127 Ethylbenzene BRL mg/kg dry 0.0066 0.00026 1 *8260B 1/8/19 15:36 ANG P9A0127 Isopropyl Ether BRL mg/kg dry 0.0066 0.00027 1 *8260B 1/8/19 15:36 ANG P9A0127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 46 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 01/11/2019 LABORATORIES INC. Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-2 Attn: Steve Libbey NC Prism Sample ID: 9010043-03 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:15 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Isopropylbenzene (Cumene) BRL mg/kg dry 0.0066 0.00039 1 *8260B 1/8/19 15:36 ANG P9A0127 m,p-Xylenes BRL mg/kg dry 0.013 0.00061 1 *8260B 1/8/19 15:36 ANG P9A0127 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.066 0.00060 1 *8260B 1/8/19 15:36 ANG P9A0127 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.13 0.00060 1 *8260B 1/8/19 15:36 ANG P9A0127 Methyl Isobutyl Ketone BRL mg/kg dry 0.066 0.00057 1 *8260B 1/8/19 15:36 ANG P9A0127 Methylene Chloride BRL mg/kg dry 0.013 0.00037 1 *8260B 1/8/19 15:36 ANG P9A0127 Methyl-tert-Butyl Ether BRL mg/kg dry 0.013 0.00021 1 *8260B 1/8/19 15:36 ANG P9A0127 Naphthalene BRL mg/kg dry 0.013 0.00021 1 *8260B 1/8/19 15:36 ANG P9A0127 n-Butylbenzene BRL mg/kg dry 0.0066 0.00034 1 *8260B 1/8/19 15:36 ANG P9A0127 n-Propylbenzene BRL mg/kg dry 0.0066 0.00039 1 *8260B 1/8/19 15:36 ANG P9A0127 o-Xylene BRL mg/kg dry 0.0066 0.00027 1 *8260B 1/8/19 15:36 ANG P9A0127 sec-Butylbenzene BRL mg/kg dry 0.0066 0.00032 1 *8260B 1/8/19 15:36 ANG P9A0127 Styrene BRL mg/kg dry 0.0066 0.00040 1 *8260B 1/8/19 15:36 ANG P9A0127 tert-Butylbenzene BRL mg/kg dry 0.0066 0.00022 1 *8260B 1/8/19 15:36 ANG P9A0127 Tetrachloroethylene BRL mg/kg dry 0.0066 0.00032 1 *8260B 1/8/19 15:36 ANG P9A0127 Toluene BRL mg/kg dry 0.0066 0.00038 1 *8260B 1/8/19 15:36 ANG P9A0127 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0066 0.00040 1 *8260B 1/8/19 15:36 ANG P9A0127 trans- 1,3-Dichloropropylene BRL mg/kg dry 0.0066 0.00035 1 *8260B 1/8/19 15:36 ANG P9A0127 Trichloroethylene BRL mg/kg dry 0.0066 0.00043 1 *8260B 1/8/19 15:36 ANG P9A0127 Trichlorofluoromethane BRL mg/kg dry 0.0066 0.00043 1 *8260B 1/8/19 15:36 ANG P9A0127 Vinyl acetate BRL CCV mg/kg dry 0.033 0.00091 1 *8260B 1/8/19 15:36 ANG P9A0127 Vinyl chloride BRL mg/kg dry 0.0066 0.00032 1 *8260B 1/8/19 15:36 ANG P9A0127 Xylenes, total BRL mg/kg dry 0.020 0.0012 1 *8260B 1/8/19 15:36 ANG P9A0127 Surrogate Recovery Control Limits 4-Bromofluorobenzene 100 % 70-130 Dibromofluoromethane 109 % 84-123 Toluene-d8 87 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 6.9 0.22 100 *MADEP VPH 1/7/19 16:28 ANG/J P9A0082 C9-Cl2 Aliphatics BRL mg/kg dry 6.9 0.36 100 *MADEP VPH 1/7/19 16:28 ANG/J P9A0082 C9-C10 Aromatics BRL mg/kg dry 6.9 0.078 100 *MADEP VPH 1/7/19 16:28 ANG/J P9A0082 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 121 % 70-130 2,5-Dibromotoluene (FID) 132 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 46 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 01 /11 /2019 Hart & Hickman (Charlotte) Attn: Steve Libbey 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: Cindy Lane UST, Charlotte, NC Project No.: CHP-035 Sample Matrix: Solid Client Sample ID: SW-3 Prism Sample ID: 9010043-04 Prism Work Order: 9010043 Time Collected: 01/03/19 15:20 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 31 3.9 1 *MADEP EPH 1/10/19 13:46 ZRC P9A0103 C19-C36 Aliphatics BRL mg/kg dry 31 6.8 1 *MADEP EPH 1/10/19 13:46 ZRC P9A0103 C11-C22 Aromatics BRL mg/kg dry 13 4.2 1 *MADEP EPH 1/10/19 13:46 ZRC P9A0103 Surrogate Recovery Control Limits 1-Chlorooctadecane 74 % 40-140 o-Terphenyl 72 % 40-140 2-Fluorobiphenyl 76 % 40-140 2-Bromonaphthalene 98 % 40-140 General Chemistry Parameters % Solids 77.5 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 *SM2540 G 1/8/19 14:30 TJY P9A0141 1,2,4-Trichlorobenzene BRL mg/kg dry 0.42 0.065 1 *8270D 1/10/19 18:42 JMV P9A0146 1,2-Dichlorobenzene BRL mg/kg dry 0.42 0.060 1 *8270D 1/10/19 18:42 JMV P9A0146 1,3-Dichlorobenzene BRL mg/kg dry 0.42 0.069 1 *8270D 1/10/19 18:42 JMV P9A0146 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.052 1 *8270D 1/10/19 18:42 JMV P9A0146 2,4,5-Trichlorophenol BRL mg/kg dry 0.42 0.068 1 *8270D 1/10/19 18:42 JMV P9A0146 2,4,6-Trichlorophenol BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 18:42 JMV P9A0146 2,4-Dichlorophenol BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:42 JMV P9A0146 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:42 JMV P9A0146 2,4-Dinitrophenol BRL mg/kg dry 0.42 0.16 1 *8270D 1/10/19 18:42 JMV P9A0146 2,4-Dinitrotoluene BRL mg/kg dry 0.42 0.080 1 *8270D 1/10/19 18:42 JMV P9A0146 2,6-Dinitrotoluene BRL mg/kg dry 0.42 0.076 1 *8270D 1/10/19 18:42 JMV P9A0146 2-Chloronaphthalene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:42 JMV P9A0146 2-Chlorophenol BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:42 JMV P9A0146 2-Methyl naphthalene BRL mg/kg dry 0.42 0.059 1 *8270D 1/10/19 18:42 JMV P9A0146 2-Methylphenol BRL mg/kg dry 0.42 0.064 1 *8270D 1/10/19 18:42 JMV P9A0146 2-Nitroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:42 JMV P9A0146 2-Nitrophenol BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:42 JMV P9A0146 3,3'-Dichlorobenzidine BRL mg/kg dry 0.42 0.034 1 *8270D 1/10/19 18:42 JMV P9A0146 3/4-Methyl phenol BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 18:42 JMV P9A0146 3-Nitroaniline BRL mg/kg dry 0.42 0.14 1 *8270D 1/10/19 18:42 JMV P9A0146 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.42 0.12 1 *8270D 1/10/19 18:42 JMV P9A0146 4-Bromophenyl phenyl ether BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:42 JMV P9A0146 4-Chloro-3-methylphenol BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 18:42 JMV P9A0146 4-Chloroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:42 JMV P9A0146 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 18:42 JMV P9A0146 4-Nitroaniline BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 18:42 JMV P9A0146 4-Nitrophenol BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 18:42 JMV P9A0146 Acenaphthene BRL mg/kg dry 0.42 0.046 1 *8270D 1/10/19 18:42 JMV P9A0146 Acenaphthylene BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:42 JMV P9A0146 Aniline BRL mg/kg dry 0.42 0.083 1 *8270D 1/10/19 18:42 JMV P9A0146 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 46 Laboratory Report ` Full -Service P R S M Analytical & / environmental Solutions LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-3 Attn: Steve Libbey NC Prism Sample ID: 9010043-04 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:20 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anthracene BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 18:42 JMV P9A0146 Azobenzene BRL mg/kg dry 0.42 0.054 1 *8270D 1/10/19 18:42 JMV P9A0146 Benzo(a)anthracene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:42 JMV P9A0146 Benzo(a)pyrene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:42 JMV P9A0146 Benzo(b)fluoranthene BRL mg/kg dry 0.42 0.059 1 *8270D 1/10/19 18:42 JMV P9A0146 Benzo(g,h,i)perylene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 18:42 JMV P9A0146 Benzo(k)fluoranthene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 18:42 JMV P9A0146 Benzoic Acid BRL mg/kg dry 0.42 0.19 1 *8270D 1/10/19 18:42 JMV P9A0146 Benzyl alcohol BRL mg/kg dry 0.42 0.031 1 *8270D 1/10/19 18:42 JMV P9A0146 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.42 0.045 1 *8270D 1/10/19 18:42 JMV P9A0146 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:42 JMV P9A0146 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.052 1 *8270D 1/10/19 18:42 JMV P9A0146 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.42 0.11 1 *8270D 1/10/19 18:42 JMV P9A0146 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.084 1 *8270D 1/10/19 18:42 JMV P9A0146 Chrysene BRL mg/kg dry 0.42 0.078 1 *8270D 1/10/19 18:42 JMV P9A0146 Dibenzo(a,h)anthracene BRL mg/kg dry 0.42 0.067 1 *8270D 1/10/19 18:42 JMV P9A0146 Dibenzofuran BRL mg/kg dry 0.42 0.055 1 *8270D 1/10/19 18:42 JMV P9A0146 Diethyl phthalate BRL mg/kg dry 0.42 0.086 1 *8270D 1/10/19 18:42 JMV P9A0146 Dimethyl phthalate BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 18:42 JMV P9A0146 Di-n-butyl phthalate BRL mg/kg dry 0.42 0.071 1 *8270D 1/10/19 18:42 JMV P9A0146 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:42 JMV P9A0146 Fluoranthene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 18:42 JMV P9A0146 Fluorene BRL mg/kg dry 0.42 0.062 1 *8270D 1/10/19 18:42 JMV P9A0146 Hexachlorobenzene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 18:42 JMV P9A0146 Hexachlorobutadiene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 18:42 JMV P9A0146 Hexachlorocyclopentadiene BRL mg/kg dry 0.42 0.075 1 *8270D 1/10/19 18:42 JMV P9A0146 Hexachloroethane BRL mg/kg dry 0.42 0.063 1 *8270D 1/10/19 18:42 JMV P9A0146 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 18:42 JMV P9A0146 Isophorone BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 18:42 JMV P9A0146 Naphthalene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:42 JMV P9A0146 Nitrobenzene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:42 JMV P9A0146 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 18:42 JMV P9A0146 N-Nitrosodiphenylamine BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 18:42 JMV P9A0146 Pentachlorophenol BRL mg/kg dry 0.42 0.096 1 *8270D 1/10/19 18:42 JMV P9A0146 Phenanthrene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 18:42 JMV P9A0146 Phenol BRL mg/kg dry 0.42 0.038 1 *8270D 1/10/19 18:42 JMV P9A0146 Pyrene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 18:42 JMV P9A0146 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 87 % 37-131 2-Fluorobiphenyl 85 % 47-130 2-Fluorophenol 85 % 44-117 Nitrobenzene-d5 80 % 45-121 Phenol-d5 81 % 37-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 46 Laboratory Report ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-3 Attn: Steve Libbey NC Prism Sample ID: 9010043-04 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:20 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Terphenyl-d14 88 % 38-135 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0071 0.00058 1 *8260B 1/8/19 19:45 ANG P9A0127 1,1,1-Trichloroethane BRL mg/kg dry 0.0071 0.00034 1 *8260B 1/8/19 19:45 ANG P9A0127 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0071 0.00048 1 *8260B 1/8/19 19:45 ANG P9A0127 1,1,2-Trichloroethane BRL mg/kg dry 0.0071 0.00063 1 *8260B 1/8/19 19:45 ANG P9A0127 1,1-Dichloroethane BRL mg/kg dry 0.0071 0.00020 1 *8260B 1/8/19 19:45 ANG P9A0127 1,1-Dichloroethylene BRL mg/kg dry 0.0071 0.00031 1 *8260B 1/8/19 19:45 ANG P9A0127 1,1-Dichloropropylene BRL mg/kg dry 0.0071 0.00039 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0071 0.00040 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2,3-Trichloropropane BRL mg/kg dry 0.0071 0.00090 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0071 0.00053 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2,4-Trimethyl benzene 0.44 LL mg/kg dry 0.0071 0.00054 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2-Dibromoethane BRL mg/kg dry 0.0071 0.00028 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2-Dichlorobenzene BRL mg/kg dry 0.0071 0.00033 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2-Dichloroethane BRL mg/kg dry 0.0071 0.00042 1 *8260B 1/8/19 19:45 ANG P9A0127 1,2-Dichloropropane BRL mg/kg dry 0.0071 0.00044 1 *8260B 1/8/19 19:45 ANG P9A0127 1,3,5-Trimethyl benzene 0.19 mg/kg dry 0.0071 0.00053 1 *8260B 1/8/19 19:45 ANG P9A0127 1,3-Dichlorobenzene BRL mg/kg dry 0.0071 0.00047 1 *8260B 1/8/19 19:45 ANG P9A0127 1,3-Dichloropropane BRL mg/kg dry 0.0071 0.00036 1 *8260B 1/8/19 19:45 ANG P9A0127 1,4-Dichlorobenzene BRL mg/kg dry 0.0071 0.00028 1 *8260B 1/8/19 19:45 ANG P9A0127 2,2-Dichloropropane BRL mg/kg dry 0.0071 0.00034 1 *8260B 1/8/19 19:45 ANG P9A0127 2-Chlorotoluene BRL mg/kg dry 0.0071 0.00037 1 *8260B 1/8/19 19:45 ANG P9A0127 4-Chlorotoluene BRL mg/kg dry 0.0071 0.00042 1 *8260B 1/8/19 19:45 ANG P9A0127 4-Isopropyltoluene 0.083 mg/kg dry 0.0071 0.00034 1 *8260B 1/8/19 19:45 ANG P9A0127 Acetone BRL mg/kg dry 0.071 0.0017 1 *8260B 1/8/19 19:45 ANG P9A0127 Benzene BRL mg/kg dry 0.0042 0.00041 1 *8260B 1/8/19 19:45 ANG P9A0127 Bromobenzene BRL mg/kg dry 0.0071 0.00059 1 *8260B 1/8/19 19:45 ANG P9A0127 Bromochloromethane BRL mg/kg dry 0.0071 0.00039 1 *8260B 1/8/19 19:45 ANG P9A0127 Bromodichloromethane BRL mg/kg dry 0.0071 0.00039 1 *8260B 1/8/19 19:45 ANG P9A0127 Bromoform BRL mg/kg dry 0.0071 0.00080 1 *8260B 1/8/19 19:45 ANG P9A0127 Bromomethane BRL mg/kg dry 0.014 0.00087 1 *8260B 1/8/19 19:45 ANG P9A0127 Carbon Tetrachloride BRL mg/kg dry 0.0071 0.00035 1 *8260B 1/8/19 19:45 ANG P9A0127 Chlorobenzene BRL mg/kg dry 0.0071 0.00038 1 *8260B 1/8/19 19:45 ANG P9A0127 Chloroethane BRL mg/kg dry 0.014 0.00059 1 *8260B 1/8/19 19:45 ANG P9A0127 Chloroform BRL mg/kg dry 0.0071 0.00051 1 *8260B 1/8/19 19:45 ANG P9A0127 Chloromethane BRL mg/kg dry 0.0071 0.00048 1 *8260B 1/8/19 19:45 ANG P9A0127 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0071 0.00030 1 *8260B 1/8/19 19:45 ANG P9A0127 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0071 0.00024 1 *8260B 1/8/19 19:45 ANG P9A0127 Dibromochloromethane BRL mg/kg dry 0.0071 0.00029 1 *8260B 1/8/19 19:45 ANG P9A0127 Dichlorodifluoromethane BRL mg/kg dry 0.0071 0.00032 1 *8260B 1/8/19 19:45 ANG P9A0127 Ethylbenzene BRL mg/kg dry 0.0071 0.00027 1 *8260B 1/8/19 19:45 ANG P9A0127 Isopropyl Ether BRL mg/kg dry 0.0071 0.00029 1 *8260B 1/8/19 19:45 ANG P9A0127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 46 Laboratory Report ` Full -Service Analytical & / Environmental Solutions P R S M LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-3 Attn: Steve Libbey NC Prism Sample ID: 9010043-04 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:20 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Isopropyl benzene (Cumene) 0.014 mg/kg dry 0.0071 0.00042 1 *8260B 1/8/19 19:45 ANG P9A0127 m,p-Xylenes 0.032 mg/kg dry 0.014 0.00065 1 *8260B 1/8/19 19:45 ANG P9A0127 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.071 0.00064 1 *8260B 1/8/19 19:45 ANG P9A0127 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.14 0.00064 1 *8260B 1/8/19 19:45 ANG P9A0127 Methyl Isobutyl Ketone BRL mg/kg dry 0.071 0.00060 1 *8260B 1/8/19 19:45 ANG P9A0127 Methylene Chloride BRL mg/kg dry 0.014 0.00040 1 *8260B 1/8/19 19:45 ANG P9A0127 Methyl-tert-Butyl Ether BRL mg/kg dry 0.014 0.00023 1 *8260B 1/8/19 19:45 ANG P9A0127 Naphthalene 0.016 mg/kg dry 0.014 0.00022 1 *8260B 118/19 19:45 ANG P9A0127 n-Butylbenzene BRL mg/kg dry 0.0071 0.00036 1 *8260B 1/8/19 19:45 ANG P9A0127 n-Propylbenzene 0.011 mg/kg dry 0.0071 0.00042 1 *8260B 1/8/19 19:45 ANG P9A0127 o-Xylene 0.028 mg/kg dry 0.0071 0.00029 1 *8260B 1/8/19 19:45 ANG P9A0127 sec-Butylbenzene 0.019 mg/kg dry 0.0071 0.00034 1 *8260B 1/8/19 19:45 ANG P9A0127 Styrene BRL mg/kg dry 0.0071 0.00043 1 *8260B 1/8/19 19:45 ANG P9A0127 tert-Butylbenzene 0.0081 mg/kg dry 0.0071 0.00024 1 *8260B 1/8119 19:45 ANG P9A0127 Tetrachloroethylene BRL mg/kg dry 0.0071 0.00034 1 *8260B 1/8/19 19:45 ANG P9A0127 Toluene BRL mg/kg dry 0.0071 0.00041 1 *8260B 1/8/19 19:45 ANG P9A0127 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0071 0.00042 1 *8260B 1/8/19 19:45 ANG P9A0127 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0071 0.00037 1 *8260B 1/8/19 19:45 ANG P9A0127 Trichloroethylene BRL mg/kg dry 0.0071 0.00046 1 *8260B 1/8/19 19:45 ANG P9A0127 Trichlorofluoromethane BRL mg/kg dry 0.0071 0.00046 1 *8260B 1/8/19 19:45 ANG P9A0127 Vinyl acetate BRL CCV mg/kg dry 0.035 0.00097 1 *8260B 1/8/19 19:45 ANG P9A0127 Vinyl chloride BRL mg/kg dry 0.0071 0.00034 1 *8260B 1/8/19 19:45 ANG P9A0127 Xylenes, total 0.060 mg/kg dry 0.021 0.0013 1 *8260B 1/8/19 19:45 ANG P9A0127 Surrogate Recovery Control Limits 4-Bromofluorobenzene 92 % 70-130 Dibromofluoromethane 101 % 84-123 Toluene-d8 95 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID C5-C8 Aliphatics BRL mg/kg dry 6.2 0.20 100 *MADEP VPH 1/7/19 16:56 ANG/J P9A0082 C9-C12 Aliphatics 18 mg/kg dry 6.2 0.33 100 *MADEP VPH 1/7/19 16:56 ANG/J P9A0082 C9-Cl0 Aromatics BRL mg/kg dry 6.2 0.070 100 *MADEP VPH 1/7/19 16:56 ANG/J P9A0082 Surrogate Recovery Control Limits 25-Dibromotoluene (PID) 123 % 70-130 2,5-Dibromotoluene (FID) 130 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 46 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 01 /11 /2019 Hart & Hickman (Charlotte) Attn: Steve Libbey 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: Cindy Lane UST, Charlotte, NC Project No.: CHP-035 Sample Matrix: Solid Client Sample ID: SW-4 Prism Sample ID: 9010043-05 Prism Work Order: 9010043 Time Collected: 01/03/19 15:25 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 31 3.9 1 *MADEP EPH 1/10/19 14:23 ZRC P9A0103 C19-C36 Aliphatics BRL mg/kg dry 31 6.8 1 *MADEP EPH 1/10/19 14:23 ZRC P9A0103 C11-C22 Aromatics BRL mg/kg dry 13 4.1 1 *MADEP EPH 1/10/19 14:23 ZRC P9A0103 Surrogate Recovery Control Limits 1-Chlorooctadecane 73 % 40-140 o-Terphenyl 87 % 40-140 2-Fluorobiphenyl 86 % 40-140 2-Bromonaphthalene 110 % 40-140 General Chemistry Parameters % Solids 77.9 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 *SM2540 G 1/8/19 14:30 TJY P9A0141 1,2,4-Trichlorobenzene BRL mg/kg dry 0.42 0.065 1 *8270D 1/10/19 19:05 JMV P9A0146 1,2-Dichlorobenzene BRL mg/kg dry 0.42 0.059 1 *8270D 1/10/19 19:05 JMV P9A0146 1,3-Dichlorobenzene BRL mg/kg dry 0.42 0.068 1 *8270D 1/10/19 19:05 JMV P9A0146 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 19:05 JMV P9A0146 2,4,5-Trichlorophenol BRL mg/kg dry 0.42 0.068 1 *8270D 1/10/19 19:05 JMV P9A0146 2,4,6-Trichlorophenol BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 19:05 JMV P9A0146 2,4-Dichlorophenol BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 19:05 JMV P9A0146 2,4-Dimethylphenol BRL mg/kg dry 0.42 0.048 1 *8270D 1/10/19 19:05 JMV P9A0146 2,4-Dinitrophenol BRL mg/kg dry 0.42 0.15 1 *8270D 1/10/19 19:05 JMV P9A0146 2,4-Dinitrotoluene BRL mg/kg dry 0.42 0.080 1 *8270D 1/10/19 19:05 JMV P9A0146 2,6-Dinitrotoluene BRL mg/kg dry 0.42 0.075 1 *8270D 1/10/19 19:05 JMV P9A0146 2-Chloronaphthalene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 19:05 JMV P9A0146 2-Chlorophenol BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 19:05 JMV P9A0146 2-Methyl naphthalene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 19:05 JMV P9A0146 2-Methylphenol BRL mg/kg dry 0.42 0.064 1 *8270D 1/10/19 19:05 JMV P9A0146 2-Nitroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 19:05 JMV P9A0146 2-Nitrophenol BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 19:05 JMV P9A0146 3,3'-Dichlorobenzidine BRL mg/kg dry 0.42 0.033 1 *8270D 1/10/19 19:05 JMV P9A0146 3/4-Methyl phenol BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 19:05 JMV P9A0146 3-Nitroaniline BRL mg/kg dry 0.42 0.13 1 *8270D 1/10/19 19:05 JMV P9A0146 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.42 0.11 1 *8270D 1/10/19 19:05 JMV P9A0146 4-Bromophenyl phenyl ether BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 19:05 JMV P9A0146 4-Chloro-3-methylphenol BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 19:05 JMV P9A0146 4-Chloroaniline BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 19:05 JMV P9A0146 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 19:05 JMV P9A0146 4-Nitroaniline BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 19:05 JMV P9A0146 4-Nitrophenol BRL mg/kg dry 0.42 0.10 1 *8270D 1/10/19 19:05 JMV P9A0146 Acenaphthene BRL mg/kg dry 0.42 0.046 1 *8270D 1/10/19 19:05 JMV P9A0146 Acenaphthylene BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 19:05 JMV P9A0146 Aniline BRL mg/kg dry 0.42 0.083 1 *8270D 1/10/19 19:05 JMV P9A0146 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 46 Laboratory Report ` Full -Service P R S M Analytical & / environmental Solutions LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-4 Attn: Steve Libbey NC Prism Sample ID: 9010043-05 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:25 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anthracene BRL mg/kg dry 0.42 0.047 1 *8270D 1/10/19 19:05 JMV P9A0146 Azobenzene BRL mg/kg dry 0.42 0.054 1 *8270D 1/10/19 19:05 JMV P9A0146 Benzo(a)anthracene BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 19:05 JMV P9A0146 Benzo(a)pyrene BRL mg/kg dry 0.42 0.050 1 *8270D 1/10/19 19:05 JMV P9A0146 Benzo(b)fluoranthene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 19:05 JMV P9A0146 Benzo(g,hJ)perylene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 19:05 JMV P9A0146 Benzo(k)fluoranthene BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 19:05 JMV P9A0146 Benzoic Acid BRL mg/kg dry 0.42 0.19 1 *8270D 1/10/19 19:05 JMV P9A0146 Benzyl alcohol BRL mg/kg dry 0.42 0.031 1 *8270D 1/10/19 19:05 JMV P9A0146 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.42 0.044 1 *8270D 1/10/19 19:05 JMV P9A0146 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 19:05 JMV P9A0146 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.051 1 *8270D 1/10/19 19:05 JMV P9A0146 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.42 0.11 1 *8270D 1/10/19 19:05 JMV P9A0146 Butyl benzyl phthalate BRL mg/kg dry 0.42 0.083 1 *8270D 1/10/19 19:05 JMV P9A0146 Chrysene BRL mg/kg dry 0.42 0.077 1 *8270D 1/10/19 19:05 JMV P9A0146 Dibenzo(a,h)anthracene BRL mg/kg dry 0.42 0.067 1 *8270D 1/10/19 19:05 JMV P9A0146 Dibenzofuran BRL mg/kg dry 0.42 0.055 1 *8270D 1/10/19 19:05 JMV P9A0146 Diethyl phthalate BRL mg/kg dry 0.42 0.085 1 *8270D 1/10/19 19:05 JMV P9A0146 Dimethyl phthalate BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 19:05 JMV P9A0146 Di-n-butyl phthalate BRL mg/kg dry 0.42 0.070 1 *8270D 1/10/19 19:05 JMV P9A0146 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.048 1 *8270D 1/10/19 19:05 JMV P9A0146 Fluoranthene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 19:05 JMV P9A0146 Fluorene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 19:05 JMV P9A0146 Hexachlorobenzene BRL mg/kg dry 0.42 0.066 1 *8270D 1/10/19 19:05 JMV P9A0146 Hexachlorobutadiene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 19:05 JMV P9A0146 Hexachlorocyclopentadiene BRL mg/kg dry 0.42 0.075 1 *8270D 1/10/19 19:05 JMV P9A0146 Hexachloroethane BRL mg/kg dry 0.42 0.062 1 *8270D 1/10/19 19:05 JMV P9A0146 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.42 0.058 1 *8270D 1/10/19 19:05 JMV P9A0146 Isophorone BRL mg/kg dry 0.42 0.040 1 *8270D 1/10/19 19:05 JMV P9A0146 Naphthalene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 19:05 JMV P9A0146 Nitrobenzene BRL mg/kg dry 0.42 0.057 1 *8270D 1/10/19 19:05 JMV P9A0146 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 19:05 JMV P9A0146 N-Nitrosodiphenylamine BRL mg/kg dry 0.42 0.049 1 *8270D 1/10/19 19:05 JMV P9A0146 Pentachlorophenol BRL mg/kg dry 0.42 0.095 1 *8270D 1/10/19 19:05 JMV P9A0146 Phenanthrene BRL mg/kg dry 0.42 0.056 1 *8270D 1/10/19 19:05 JMV P9A0146 Phenol BRL mg/kg dry 0.42 0.038 1 *8270D 1/10/19 19:05 JMV P9A0146 Pyrene BRL mg/kg dry 0.42 0.061 1 *8270D 1/10/19 19:05 JMV P9A0146 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 89 % 37-131 2-Fluorobiphenyl 87 % 47-130 2-Fluorophenol 85 % 44-117 Nitrobenzene-d5 80 % 45-121 Phenol-d5 83 % 37-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 46 Laboratory Report ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-4 Attn: Steve Libbey NC Prism Sample ID: 9010043-05 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:25 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Terphenyl-d14 87 % 38-135 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0060 0.00049 1 *8260B 1/8/19 16:03 ANG P9A0127 1,1,1-Trichloroethane BRL mg/kg dry 0.0060 0.00029 1 *8260B 1/8/19 16:03 ANG P9A0127 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0060 0.00041 1 *8260B 1/8/19 16:03 ANG P9A0127 1,1,2-Trichloroethane BRL mg/kg dry 0.0060 0.00053 1 *8260B 1/8/19 16:03 ANG P9A0127 1,1-Dichloroethane BRL mg/kg dry 0.0060 0.00017 1 *8260B 1/8/19 16:03 ANG P9A0127 1,1-Dichloroethylene BRL mg/kg dry 0.0060 0.00027 1 *8260B 1/8/19 16:03 ANG P9A0127 1,1-Dichloropropylene BRL mg/kg dry 0.0060 0.00033 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0060 0.00034 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2,3-Trichloropropane BRL mg/kg dry 0.0060 0.00077 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0060 0.00045 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0060 0.00046 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2-Dibromoethane BRL mg/kg dry 0.0060 0.00024 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2-Dichlorobenzene BRL mg/kg dry 0.0060 0.00028 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2-Dichloroethane BRL mg/kg dry 0.0060 0.00036 1 *8260B 1/8/19 16:03 ANG P9A0127 1,2-Dichloropropane BRL mg/kg dry 0.0060 0.00037 1 *8260B 1/8/19 16:03 ANG P9A0127 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0060 0.00045 1 *8260B 1/8/19 16:03 ANG P9A0127 1,3-Dichlorobenzene BRL mg/kg dry 0.0060 0.00040 1 *8260B 1/8/19 16:03 ANG P9A0127 1,3-Dichloropropane BRL mg/kg dry 0.0060 0.00030 1 *8260B 1/8/19 16:03 ANG P9A0127 1,4-Dichlorobenzene BRL mg/kg dry 0.0060 0.00024 1 *8260B 1/8/19 16:03 ANG P9A0127 2,2-Dichloropropane BRL mg/kg dry 0.0060 0.00029 1 *8260B 1/8/19 16:03 ANG P9A0127 2-Chlorotoluene BRL mg/kg dry 0.0060 0.00031 1 *8260B 1/8/19 16:03 ANG P9A0127 4-Chlorotoluene BRL mg/kg dry 0.0060 0.00036 1 *8260B 1/8/19 16:03 ANG P9A0127 4-Isopropyltoluene BRL mg/kg dry 0.0060 0.00029 1 *8260B 1/8/19 16:03 ANG P9A0127 Acetone BRL mg/kg dry 0.060 0.0015 1 *8260B 1/8/19 16:03 ANG P9A0127 Benzene BRL mg/kg dry 0.0036 0.00035 1 *8260B 1/8/19 16:03 ANG P9A0127 Bromobenzene BRL mg/kg dry 0.0060 0.00050 1 *8260B 1/8/19 16:03 ANG P9A0127 Bromochloromethane BRL mg/kg dry 0.0060 0.00033 1 *8260B 1/8/19 16:03 ANG P9A0127 Bromodichloromethane BRL mg/kg dry 0.0060 0.00033 1 *8260B 1/8/19 16:03 ANG P9A0127 Bromoform BRL mg/kg dry 0.0060 0.00068 1 *8260B 1/8/19 16:03 ANG P9A0127 Bromomethane BRL mg/kg dry 0.012 0.00074 1 *8260B 1/8/19 16:03 ANG P9A0127 Carbon Tetrachloride BRL mg/kg dry 0.0060 0.00030 1 *8260B 1/8/19 16:03 ANG P9A0127 Chlorobenzene BRL mg/kg dry 0.0060 0.00032 1 *8260B 1/8/19 16:03 ANG P9A0127 Chloroethane BRL mg/kg dry 0.012 0.00050 1 *8260B 1/8/19 16:03 ANG P9A0127 Chloroform BRL mg/kg dry 0.0060 0.00043 1 *8260B 1/8/19 16:03 ANG P9A0127 Chloromethane BRL mg/kg dry 0.0060 0.00040 1 *8260B 1/8/19 16:03 ANG P9A0127 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0060 0.00026 1 *8260B 1/8/19 16:03 ANG P9A0127 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0060 0.00020 1 *8260B 1/8/19 16:03 ANG P9A0127 Dibromochloromethane BRL mg/kg dry 0.0060 0.00025 1 *8260B 1/8/19 16:03 ANG P9A0127 Dichlorodifluoromethane BRL mg/kg dry 0.0060 0.00027 1 *8260B 1/8/19 16:03 ANG P9A0127 Ethylbenzene BRL mg/kg dry 0.0060 0.00023 1 *8260B 1/8/19 16:03 ANG P9A0127 Isopropyl Ether BRL mg/kg dry 0.0060 0.00024 1 *8260B 1/8/19 16:03 ANG P9A0127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 46 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 01/11/2019 LABORATORIES INC. Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: SW-4 Attn: Steve Libbey NC Prism Sample ID: 9010043-05 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:25 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Isopropylbenzene (Cumene) BRL mg/kg dry 0.0060 0.00036 1 *8260B 1/8/19 16:03 ANG P9A0127 m,p-Xylenes BRL mg/kg dry 0.012 0.00055 1 *8260B 1/8/19 16:03 ANG P9A0127 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.060 0.00054 1 *8260B 1/8/19 16:03 ANG P9A0127 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00054 1 *8260B 1/8/19 16:03 ANG P9A0127 Methyl Isobutyl Ketone BRL mg/kg dry 0.060 0.00051 1 *8260B 1/8/19 16:03 ANG P9A0127 Methylene Chloride BRL mg/kg dry 0.012 0.00034 1 *8260B 1/8/19 16:03 ANG P9A0127 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00019 1 *8260B 1/8/19 16:03 ANG P9A0127 Naphthalene BRL mg/kg dry 0.012 0.00019 1 *8260B 1/8/19 16:03 ANG P9A0127 n-Butylbenzene BRL mg/kg dry 0.0060 0.00031 1 *8260B 1/8/19 16:03 ANG P9A0127 n-Propylbenzene BRL mg/kg dry 0.0060 0.00036 1 *8260B 1/8/19 16:03 ANG P9A0127 o-Xylene BRL mg/kg dry 0.0060 0.00025 1 *8260B 1/8/19 16:03 ANG P9A0127 sec-Butylbenzene BRL mg/kg dry 0.0060 0.00029 1 *8260B 1/8/19 16:03 ANG P9A0127 Styrene BRL mg/kg dry 0.0060 0.00036 1 *8260B 1/8/19 16:03 ANG P9A0127 tert-Butylbenzene BRL mg/kg dry 0.0060 0.00020 1 *8260B 1/8/19 16:03 ANG P9A0127 Tetrachloroethylene BRL mg/kg dry 0.0060 0.00029 1 *8260B 1/8/19 16:03 ANG P9A0127 Toluene BRL mg/kg dry 0.0060 0.00034 1 *8260B 1/8/19 16:03 ANG P9A0127 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0060 0.00036 1 *8260B 1/8/19 16:03 ANG P9A0127 trans- 1,3-Dichloropropylene BRL mg/kg dry 0.0060 0.00032 1 *8260B 1/8/19 16:03 ANG P9A0127 Trichloroethylene BRL mg/kg dry 0.0060 0.00039 1 *8260B 1/8/19 16:03 ANG P9A0127 Trichlorofluoromethane BRL mg/kg dry 0.0060 0.00039 1 *8260B 1/8/19 16:03 ANG P9A0127 Vinyl acetate BRL CCV mg/kg dry 0.030 0.00082 1 *8260B 1/8/19 16:03 ANG P9A0127 Vinyl chloride BRL mg/kg dry 0.0060 0.00029 1 *8260B 1/8/19 16:03 ANG P9A0127 Xylenes, total BRL mg/kg dry 0.018 0.0011 1 *8260B 1/8/19 16:03 ANG P9A0127 Surrogate Recovery Control Limits 4-Bromofluorobenzene 99 % 70-130 Dibromofluoromethane 111 % 84-123 Toluene-d8 86 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 6.1 0.20 100 *MADEP VPH 1/7/19 17:24 ANG/J P9A0082 C9-Cl2 Aliphatics BRL mg/kg dry 6.1 0.32 100 *MADEP VPH 1/7/19 17:24 ANG/J P9A0082 C9-C10 Aromatics BRL mg/kg dry 6.1 0.068 100 *MADEP VPH 1/7/19 17:24 ANG/J P9A0082 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 126 % 70-130 2,5-Dibromotoluene (FID) 136 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 46 PR I S M Full -Service Analytical Environmental Solutions LABORATORIES INC. Laboratory Report 01 /11 /2019 Hart & Hickman (Charlotte) Attn: Steve Libbey 2923 South Tryon St. Ste 100 Charlotte, NC 28203 Project: Cindy Lane UST, Charlotte, NC Project No.: CHP-035 Sample Matrix: Solid Client Sample ID: B-1 Prism Sample ID: 9010043-06 Prism Work Order: 9010043 Time Collected: 01/03/19 15:30 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-Cl8 Aliphatics BRL mg/kg dry 31 3.8 1 *MADEP EPH 1/10/19 14:59 ZRC P9A0103 C19-C36 Aliphatics BRL mg/kg dry 31 6.6 1 *MADEP EPH 1/10/19 14:59 ZRC P9A0103 C11-C22 Aromatics BRL mg/kg dry 12 4.0 1 *MADEP EPH 1/10/19 14:59 ZRC P9A0103 Surrogate Recovery Control Limits 1-Chlorooctadecane 56 % 40-140 o-Terphenyl 74 % 40-140 2-Fluorobiphenyl 81 % 40-140 2-Bromonaphthalene 103 % 40-140 General Chemistry Parameters % Solids 77.0 Semivolatile Organic Compounds by GC/MS % by Weight 0.100 0.100 1 *SM2540 G 1/8/19 14:30 TJY P9A0141 1,2,4-Trichlorobenzene BRL mg/kg dry 0.43 0.066 1 *8270D 1/10/19 19:27 JMV P9A0146 1,2-Dichlorobenzene BRL mg/kg dry 0.43 0.061 1 *8270D 1/10/19 19:27 JMV P9A0146 1,3-Dichlorobenzene BRL mg/kg dry 0.43 0.069 1 *8270D 1/10/19 19:27 JMV P9A0146 1,4-Dichlorobenzene BRL mg/kg dry 0.43 0.052 1 *8270D 1/10/19 19:27 JMV P9A0146 2,4,5-Trichlorophenol BRL mg/kg dry 0.43 0.069 1 *8270D 1/10/19 19:27 JMV P9A0146 2,4,6-Trichlorophenol BRL mg/kg dry 0.43 0.048 1 *8270D 1/10/19 19:27 JMV P9A0146 2,4-Dichlorophenol BRL mg/kg dry 0.43 0.051 1 *8270D 1/10/19 19:27 JMV P9A0146 2,4-Dimethylphenol BRL mg/kg dry 0.43 0.049 1 *8270D 1/10/19 19:27 JMV P9A0146 2,4-Dinitrophenol BRL mg/kg dry 0.43 0.16 1 *8270D 1/10/19 19:27 JMV P9A0146 2,4-Dinitrotoluene BRL mg/kg dry 0.43 0.081 1 *8270D 1/10/19 19:27 JMV P9A0146 2,6-Dinitrotoluene BRL mg/kg dry 0.43 0.077 1 *8270D 1/10/19 19:27 JMV P9A0146 2-Chloronaphthalene BRL mg/kg dry 0.43 0.067 1 *8270D 1/10/19 19:27 JMV P9A0146 2-Chlorophenol BRL mg/kg dry 0.43 0.057 1 *8270D 1/10/19 19:27 JMV P9A0146 2-Methyl naphthalene BRL mg/kg dry 0.43 0.059 1 *8270D 1/10/19 19:27 JMV P9A0146 2-Methylphenol BRL mg/kg dry 0.43 0.065 1 *8270D 1/10/19 19:27 JMV P9A0146 2-Nitroaniline BRL mg/kg dry 0.43 0.067 1 *8270D 1/10/19 19:27 JMV P9A0146 2-Nitrophenol BRL mg/kg dry 0.43 0.052 1 *8270D 1/10/19 19:27 JMV P9A0146 3,3'-Dichlorobenzidine BRL mg/kg dry 0.43 0.034 1 *8270D 1/10/19 19:27 JMV P9A0146 3/4-Methyl phenol BRL mg/kg dry 0.43 0.051 1 *8270D 1/10/19 19:27 JMV P9A0146 3-Nitroaniline BRL mg/kg dry 0.43 0.14 1 *8270D 1/10/19 19:27 JMV P9A0146 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.43 0.12 1 *8270D 1/10/19 19:27 JMV P9A0146 4-Bromophenyl phenyl ether BRL mg/kg dry 0.43 0.058 1 *8270D 1/10/19 19:27 JMV P9A0146 4-Chloro-3-methylphenol BRL mg/kg dry 0.43 0.040 1 *8270D 1/10/19 19:27 JMV P9A0146 4-Chloroaniline BRL mg/kg dry 0.43 0.067 1 *8270D 1/10/19 19:27 JMV P9A0146 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.43 0.051 1 *8270D 1/10/19 19:27 JMV P9A0146 4-Nitroaniline BRL mg/kg dry 0.43 0.10 1 *8270D 1/10/19 19:27 JMV P9A0146 4-Nitrophenol BRL mg/kg dry 0.43 0.10 1 *8270D 1/10/19 19:27 JMV P9A0146 Acenaphthene BRL mg/kg dry 0.43 0.047 1 *8270D 1/10/19 19:27 JMV P9A0146 Acenaphthylene BRL mg/kg dry 0.43 0.050 1 *8270D 1/10/19 19:27 JMV P9A0146 Aniline BRL mg/kg dry 0.43 0.084 1 *8270D 1/10/19 19:27 JMV P9A0146 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 46 Laboratory Report ` Full -Service P R S M Analytical & / environmental Solutions LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: B-1 Attn: Steve Libbey NC Prism Sample ID: 9010043-06 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:30 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anthracene BRL mg/kg dry 0.43 0.048 1 *8270D 1/10/19 19:27 JMV P9A0146 Azobenzene BRL mg/kg dry 0.43 0.055 1 *8270D 1/10/19 19:27 JMV P9A0146 Benzo(a)anthracene BRL mg/kg dry 0.43 0.051 1 *8270D 1/10/19 19:27 JMV P9A0146 Benzo(a)pyrene BRL mg/kg dry 0.43 0.051 1 *8270D 1/10/19 19:27 JMV P9A0146 Benzo(b)fluoranthene BRL mg/kg dry 0.43 0.059 1 *8270D 1/10/19 19:27 JMV P9A0146 Benzo(g,hJ)perylene BRL mg/kg dry 0.43 0.057 1 *8270D 1/10/19 19:27 JMV P9A0146 Benzo(k)fluoranthene BRL mg/kg dry 0.43 0.052 1 *8270D 1/10/19 19:27 JMV P9A0146 Benzoic Acid BRL mg/kg dry 0.43 0.19 1 *8270D 1/10/19 19:27 JMV P9A0146 Benzyl alcohol BRL mg/kg dry 0.43 0.031 1 *8270D 1/10/19 19:27 JMV P9A0146 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.43 0.045 1 *8270D 1/10/19 19:27 JMV P9A0146 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.43 0.050 1 *8270D 1/10/19 19:27 JMV P9A0146 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.43 0.052 1 *8270D 1/10/19 19:27 JMV P9A0146 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.43 0.11 1 *8270D 1/10/19 19:27 JMV P9A0146 Butyl benzyl phthalate BRL mg/kg dry 0.43 0.085 1 *8270D 1/10/19 19:27 JMV P9A0146 Chrysene BRL mg/kg dry 0.43 0.079 1 *8270D 1/10/19 19:27 JMV P9A0146 Dibenzo(a,h)anthracene BRL mg/kg dry 0.43 0.068 1 *8270D 1/10/19 19:27 JMV P9A0146 Dibenzofuran BRL mg/kg dry 0.43 0.056 1 *8270D 1/10/19 19:27 JMV P9A0146 Diethyl phthalate BRL mg/kg dry 0.43 0.087 1 *8270D 1/10/19 19:27 JMV P9A0146 Dimethyl phthalate BRL mg/kg dry 0.43 0.058 1 *8270D 1/10/19 19:27 JMV P9A0146 Di-n-butyl phthalate BRL mg/kg dry 0.43 0.072 1 *8270D 1/10/19 19:27 JMV P9A0146 Di-n-octyl phthalate BRL mg/kg dry 0.43 0.049 1 *8270D 1/10/19 19:27 JMV P9A0146 Fluoranthene BRL mg/kg dry 0.43 0.057 1 *8270D 1/10/19 19:27 JMV P9A0146 Fluorene BRL mg/kg dry 0.43 0.062 1 *8270D 1/10/19 19:27 JMV P9A0146 Hexachlorobenzene BRL mg/kg dry 0.43 0.067 1 *8270D 1/10/19 19:27 JMV P9A0146 Hexachlorobutadiene BRL mg/kg dry 0.43 0.062 1 *8270D 1/10/19 19:27 JMV P9A0146 Hexachlorocyclopentadiene BRL mg/kg dry 0.43 0.076 1 *8270D 1/10/19 19:27 JMV P9A0146 Hexachloroethane BRL mg/kg dry 0.43 0.063 1 *8270D 1/10/19 19:27 JMV P9A0146 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.43 0.059 1 *8270D 1/10/19 19:27 JMV P9A0146 Isophorone BRL mg/kg dry 0.43 0.041 1 *8270D 1/10/19 19:27 JMV P9A0146 Naphthalene BRL mg/kg dry 0.43 0.058 1 *8270D 1/10/19 19:27 JMV P9A0146 Nitrobenzene BRL mg/kg dry 0.43 0.058 1 *8270D 1/10/19 19:27 JMV P9A0146 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.43 0.057 1 *8270D 1/10/19 19:27 JMV P9A0146 N-Nitrosodiphenylamine BRL mg/kg dry 0.43 0.050 1 *8270D 1/10/19 19:27 JMV P9A0146 Pentachlorophenol BRL mg/kg dry 0.43 0.097 1 *8270D 1/10/19 19:27 JMV P9A0146 Phenanthrene BRL mg/kg dry 0.43 0.058 1 *8270D 1/10/19 19:27 JMV P9A0146 Phenol BRL mg/kg dry 0.43 0.038 1 *8270D 1/10/19 19:27 JMV P9A0146 Pyrene BRL mg/kg dry 0.43 0.062 1 *8270D 1/10/19 19:27 JMV P9A0146 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 85 % 37-131 2-Fluorobiphenyl 86 % 47-130 2-Fluorophenol 83 % 44-117 Nitrobenzene-d5 80 % 45-121 Phenol-d5 81 % 37-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 46 Laboratory Report ` Full -Service Analytical & / environmental Solutions P R S M LABORATORIES INC. 01/11/2019 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: B-1 Attn: Steve Libbey NC Prism Sample ID: 9010043-06 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:30 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Terphenyl-d14 86 % 38-135 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0061 0.00051 1 *8260B 1/8/19 16:31 ANG P9A0127 1,1,1-Trichloroethane BRL mg/kg dry 0.0061 0.00030 1 *8260B 1/8/19 16:31 ANG P9A0127 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0061 0.00042 1 *8260B 1/8/19 16:31 ANG P9A0127 1,1,2-Trichloroethane BRL mg/kg dry 0.0061 0.00054 1 *8260B 1/8/19 16:31 ANG P9A0127 1,1-Dichloroethane BRL mg/kg dry 0.0061 0.00017 1 *8260B 1/8/19 16:31 ANG P9A0127 1,1-Dichloroethylene BRL mg/kg dry 0.0061 0.00027 1 *8260B 1/8/19 16:31 ANG P9A0127 1,1-Dichloropropylene BRL mg/kg dry 0.0061 0.00034 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0061 0.00035 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2,3-Trichloropropane BRL mg/kg dry 0.0061 0.00078 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0061 0.00046 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2,4-Trimethyl benzene BRL mg/kg dry 0.0061 0.00047 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2-Dibromoethane BRL mg/kg dry 0.0061 0.00025 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2-Dichlorobenzene BRL mg/kg dry 0.0061 0.00029 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2-Dichloroethane BRL mg/kg dry 0.0061 0.00037 1 *8260B 1/8/19 16:31 ANG P9A0127 1,2-Dichloropropane BRL mg/kg dry 0.0061 0.00038 1 *8260B 1/8/19 16:31 ANG P9A0127 1,3,5-Trimethyl benzene BRL mg/kg dry 0.0061 0.00046 1 *8260B 1/8/19 16:31 ANG P9A0127 1,3-Dichlorobenzene BRL mg/kg dry 0.0061 0.00041 1 *8260B 1/8/19 16:31 ANG P9A0127 1,3-Dichloropropane BRL mg/kg dry 0.0061 0.00031 1 *8260B 1/8/19 16:31 ANG P9A0127 1,4-Dichlorobenzene BRL mg/kg dry 0.0061 0.00024 1 *8260B 1/8/19 16:31 ANG P9A0127 2,2-Dichloropropane BRL mg/kg dry 0.0061 0.00029 1 *8260B 1/8/19 16:31 ANG P9A0127 2-Chlorotoluene BRL mg/kg dry 0.0061 0.00032 1 *8260B 1/8/19 16:31 ANG P9A0127 4-Chlorotoluene BRL mg/kg dry 0.0061 0.00037 1 *8260B 1/8/19 16:31 ANG P9A0127 4-Isopropyltoluene BRL mg/kg dry 0.0061 0.00030 1 *8260B 1/8/19 16:31 ANG P9A0127 Acetone BRL mg/kg dry 0.061 0.0015 1 *8260B 1/8/19 16:31 ANG P9A0127 Benzene BRL mg/kg dry 0.0037 0.00036 1 *8260B 1/8/19 16:31 ANG P9A0127 Bromobenzene BRL mg/kg dry 0.0061 0.00051 1 *8260B 1/8/19 16:31 ANG P9A0127 Bromochloromethane BRL mg/kg dry 0.0061 0.00034 1 *8260B 1/8/19 16:31 ANG P9A0127 Bromodichloromethane BRL mg/kg dry 0.0061 0.00034 1 *8260B 1/8/19 16:31 ANG P9A0127 Bromoform BRL mg/kg dry 0.0061 0.00070 1 *8260B 1/8/19 16:31 ANG P9A0127 Bromomethane BRL mg/kg dry 0.012 0.00076 1 *8260B 1/8/19 16:31 ANG P9A0127 Carbon Tetrachloride BRL mg/kg dry 0.0061 0.00031 1 *8260B 1/8/19 16:31 ANG P9A0127 Chlorobenzene BRL mg/kg dry 0.0061 0.00033 1 *8260B 1/8/19 16:31 ANG P9A0127 Chloroethane BRL mg/kg dry 0.012 0.00051 1 *8260B 1/8/19 16:31 ANG P9A0127 Chloroform BRL mg/kg dry 0.0061 0.00044 1 *8260B 1/8/19 16:31 ANG P9A0127 Chloromethane BRL mg/kg dry 0.0061 0.00041 1 *8260B 1/8/19 16:31 ANG P9A0127 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0061 0.00026 1 *8260B 1/8/19 16:31 ANG P9A0127 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0061 0.00021 1 *8260B 1/8/19 16:31 ANG P9A0127 Dibromochloromethane BRL mg/kg dry 0.0061 0.00025 1 *8260B 1/8/19 16:31 ANG P9A0127 Dichlorodifluoromethane BRL mg/kg dry 0.0061 0.00028 1 *8260B 1/8/19 16:31 ANG P9A0127 Ethylbenzene BRL mg/kg dry 0.0061 0.00024 1 *8260B 1/8/19 16:31 ANG P9A0127 Isopropyl Ether BRL mg/kg dry 0.0061 0.00025 1 *8260B 1/8/19 16:31 ANG P9A0127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 46 P R S M Laboratory Report ` Full -Service Analytical & / Environmental Solutions 01/11/2019 LABORATORIES INC. Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, Client Sample ID: B-1 Attn: Steve Libbey NC Prism Sample ID: 9010043-06 2923 South Tryon St. Ste 100 Project No.: CHP-035 Prism Work Order: 9010043 Charlotte, NC 28203 Sample Matrix: Solid Time Collected: 01/03/19 15:30 Time Submitted: 01/04/19 08:25 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Isopropylbenzene (Cumene) BRL mg/kg dry 0.0061 0.00036 1 *8260B 1/8/19 16:31 ANG P9A0127 m,p-Xylenes BRL mg/kg dry 0.012 0.00057 1 *8260B 1/8/19 16:31 ANG P9A0127 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.061 0.00056 1 *8260B 1/8/19 16:31 ANG P9A0127 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00056 1 *8260B 1/8/19 16:31 ANG P9A0127 Methyl Isobutyl Ketone BRL mg/kg dry 0.061 0.00052 1 *8260B 1/8/19 16:31 ANG P9A0127 Methylene Chloride BRL mg/kg dry 0.012 0.00035 1 *8260B 1/8/19 16:31 ANG P9A0127 Methyl-tert-Butyl Ether BRL mg/kg dry 0.012 0.00020 1 *8260B 1/8/19 16:31 ANG P9A0127 Naphthalene BRL mg/kg dry 0.012 0.00019 1 *8260B 1/8/19 16:31 ANG P9A0127 n-Butylbenzene BRL mg/kg dry 0.0061 0.00031 1 *8260B 1/8/19 16:31 ANG P9A0127 n-Propylbenzene BRL mg/kg dry 0.0061 0.00037 1 *8260B 1/8/19 16:31 ANG P9A0127 o-Xylene BRL mg/kg dry 0.0061 0.00025 1 *8260B 1/8/19 16:31 ANG P9A0127 sec-Butylbenzene BRL mg/kg dry 0.0061 0.00030 1 *8260B 1/8/19 16:31 ANG P9A0127 Styrene BRL mg/kg dry 0.0061 0.00037 1 *8260B 1/8/19 16:31 ANG P9A0127 tert-Butylbenzene BRL mg/kg dry 0.0061 0.00021 1 *8260B 1/8/19 16:31 ANG P9A0127 Tetrachloroethylene BRL mg/kg dry 0.0061 0.00029 1 *8260B 1/8/19 16:31 ANG P9A0127 Toluene BRL mg/kg dry 0.0061 0.00035 1 *8260B 1/8/19 16:31 ANG P9A0127 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0061 0.00037 1 *8260B 1/8/19 16:31 ANG P9A0127 trans- 1,3-Dichloropropylene BRL mg/kg dry 0.0061 0.00032 1 *8260B 1/8/19 16:31 ANG P9A0127 Trichloroethylene BRL mg/kg dry 0.0061 0.00040 1 *8260B 1/8/19 16:31 ANG P9A0127 Trichlorofluoromethane BRL mg/kg dry 0.0061 0.00040 1 *8260B 1/8/19 16:31 ANG P9A0127 Vinyl acetate BRL CCV mg/kg dry 0.031 0.00084 1 *8260B 1/8/19 16:31 ANG P9A0127 Vinyl chloride BRL mg/kg dry 0.0061 0.00030 1 *8260B 1/8/19 16:31 ANG P9A0127 Xylenes, total BRL mg/kg dry 0.018 0.0012 1 *8260B 1/8/19 16:31 ANG P9A0127 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 70-130 Dibromofluoromethane 111 % 84-123 Toluene-d8 87 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 6.2 0.20 100 *MADEP VPH 1/7/19 17:52 ANG/J P9A0082 C9-Cl2 Aliphatics BRL mg/kg dry 6.2 0.32 100 *MADEP VPH 1/7/19 17:52 ANG/J P9A0082 C9-C10 Aromatics BRL mg/kg dry 6.2 0.069 100 *MADEP VPH 1/7/19 17:52 ANG/J P9A0082 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 134 % 70-130 SR 2,5-Dibromotoluene (FID) 147 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 46 /r E P R I IS M Service Analytical Environmental Solutions LABORATORIES, INC. Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO127 - 5035 Blank (M0127-11311-K1) Prepared & Analyzed: 01/08/19 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO127 - 5035 Blank (P9A0127-BLK1) Prepared & Analyzed: 01/08/19 Methylene Chloride BRL 0.010 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans-1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans- 1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 50.6 ug/L 50.00 101 70-130 Surrogate: Dibromofluoromethane 52.3 ug/L 50.00 105 84-123 Surrogate: Toluene-d8 44.2 ug/L 50.00 88 76-129 LCS (P9A0127-BS1) Prepared & Analyzed: 01/08/19 1,1,1,2-Tetrachloroethane 0.0486 0.0050 mg/kg wet 0.05000 97 72-115 1,1,1-Trichloroethane 0.0522 0.0050 mg/kg wet 0.05000 104 67-131 1,1,2,2-Tetrachloroethane 0.0472 0.0050 mg/kg wet 0.05000 94 56-126 1,1,2-Trichloroethane 0.0487 0.0050 mg/kg wet 0.05000 97 70-133 1,1-Dichloroethane 0.0527 0.0050 mg/kg wet 0.05000 105 74-127 1,1-Dichloroethylene 0.0505 0.0050 mg/kg wet 0.05000 101 67-149 1,1-Dichloropropylene 0.0530 0.0050 mg/kg wet 0.05000 106 71-130 1,2,3-Trichlorobenzene 0.0462 0.0050 mg/kg wet 0.05000 92 68-130 1,2,3-Trichloropropane 0.0454 0.0050 mg/kg wet 0.05000 91 60-137 1,2,4-Trichlorobenzene 0.0462 0.0050 mg/kg wet 0.05000 92 66-125 1,2,4-Trimethyl benzene 0.0445 0.0050 mg/kg wet 0.05000 89 69-129 1,2-Dibromoethane 0.0499 0.0050 mg/kg wet 0.05000 100 70-132 1,2-Dichlorobenzene 0.0439 0.0050 mg/kg wet 0.05000 88 72-123 1,2-Dichloroethane 0.0552 0.0050 mg/kg wet 0.05000 110 68-128 1,2-Dichloropropane 0.0538 0.0050 mg/kg wet 0.05000 108 73-130 1,3,5-Trimethyl benzene 0.0448 0.0050 mg/kg wet 0.05000 90 69-128 1,3-Dichlorobenzene 0.0437 0.0050 mg/kg wet 0.05000 87 71-120 1,3-Dichloropropane 0.0490 0.0050 mg/kg wet 0.05000 98 75-124 1,4-Dichlorobenzene 0.0433 0.0050 mg/kg wet 0.05000 87 71-123 2,2-Dichloropropane 0.0539 0.0050 mg/kg wet 0.05000 108 50-142 2-Chlorotoluene 0.0442 0.0050 mg/kg wet 0.05000 88 67-124 4-Chlorotoluene 0.0443 0.0050 mg/kg wet 0.05000 89 71-126 4-Isopropyltoluene 0.0456 0.0050 mg/kg wet 0.05000 91 68-129 Acetone 0.116 0.050 mg/kg wet 0.1000 116 29-198 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 46 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO127 - 5035 LCS (P9A0127-BSI) Prepared & Analyzed: 01/08/19 Benzene 0.0536 0.0030 mg/kg wet 0.05000 107 74-127 Bromobenzene 0.0439 0.0050 mg/kg wet 0.05000 88 73-125 Bromochloromethane 0.0533 0.0050 mg/kg wet 0.05000 107 72-134 Bromodichloromethane 0.0550 0.0050 mg/kg wet 0.05000 110 75-122 Bromoform 0.0509 0.0050 mg/kg wet 0.05000 102 66-135 Bromomethane 0.0539 0.010 mg/kg wet 0.05000 108 20-180 Carbon Tetrachloride 0.0528 0.0050 mg/kg wet 0.05000 106 64-143 Chlorobenzene 0.0471 0.0050 mg/kg wet 0.05000 94 74-118 Chloroethane 0.0458 0.010 mg/kg wet 0.05000 92 33-149 Chloroform 0.0532 0.0050 mg/kg wet 0.05000 106 73-127 Chloromethane 0.0448 0.0050 mg/kg wet 0.05000 90 45-143 cis-1,2-Dichloroethylene 0.0529 0.0050 mg/kg wet 0.05000 106 76-134 cis-1,3-Dichloropropylene 0.0556 0.0050 mg/kg wet 0.05000 111 71-125 Dibromochloromethane 0.0492 0.0050 mg/kg wet 0.05000 98 73-122 Dichlorodifluoromethane 0.0369 0.0050 mg/kg wet 0.05000 74 26-146 Ethylbenzene 0.0473 0.0050 mg/kg wet 0.05000 95 74-128 Isopropyl Ether 0.0571 0.0050 mg/kg wet 0.05000 114 59-159 Isopropylbenzene (Cumene) 0.0445 0.0050 mg/kg wet 0.05000 89 68-126 m,p-Xylenes 0.0989 0.010 mg/kg wet 0.1000 99 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0572 0.050 mg/kg wet 0.05000 114 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0566 0.10 mg/kg wet 0.05000 113 63-149 Methyl Isobutyl Ketone 0.0611 0.050 mg/kg wet 0.05000 122 57-162 Methylene Chloride 0.0540 0.010 mg/kg wet 0.05000 108 74-129 Methyl-tert-Butyl Ether 0.0559 0.010 mg/kg wet 0.05000 112 70-130 Naphthalene 0.0477 0.010 mg/kg wet 0.05000 95 57-157 n-Butylbenzene 0.0461 0.0050 mg/kg wet 0.05000 92 65-135 n-Propylbenzene 0.0449 0.0050 mg/kg wet 0.05000 90 67-130 o-Xylene 0.0482 0.0050 mg/kg wet 0.05000 96 74-126 sec-Butylbenzene 0.0448 0.0050 mg/kg wet 0.05000 90 66-131 Styrene 0.0496 0.0050 mg/kg wet 0.05000 99 77-121 tert-Butyl benzene 0.0442 0.0050 mg/kg wet 0.05000 88 67-132 Tetrachloroethylene 0.0522 0.0050 mg/kg wet 0.05000 104 68-130 Toluene 0.0516 0.0050 mg/kg wet 0.05000 103 71-129 trans- 1,2-Dichloroethylene 0.0519 0.0050 mg/kg wet 0.05000 104 73-132 trans- 1,3-Dichloropropylene 0.0570 0.0050 mg/kg wet 0.05000 114 68-123 Trichloroethylene 0.0524 0.0050 mg/kg wet 0.05000 105 75-133 Trichlorofluoromethane 0.0489 0.0050 mg/kg wet 0.05000 98 44-146 Vinyl acetate 0.0919 0.025 mg/kg wet 0.05000 184 85-161 Vinyl chloride 0.0458 0.0050 mg/kg wet 0.05000 92 48-147 Xylenes, total 0.147 0.015 mg/kg wet 0.1500 98 74-126 Surrogate:4-Bromofluorobenzene 48.6 ug/L 50.00 97 70-130 Surrogate: Dibromofluoromethane 49.9 ug/L 50.00 100 84-123 Surrogate: Toluene-d8 44.2 ug/L 50.00 88 76-129 LH This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 46 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Attn: Steve Libbey 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9AO127 - 5035 Prism Work Order: 9010043 Time Submitted: 1/4/2019 8:25:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS Dup (P9AO127-BSD1) Prepared & Analyzed: 01/08/19 1,1,1,2-Tetrachloroethane 0.0456 0.0050 mg/kg wet 0.05000 91 72-115 6 20 1,1,1-Trichloroethane 0.0481 0.0050 mg/kg wet 0.05000 96 67-131 8 20 1,1,2,2-Tetrachloroethane 0.0459 0.0050 mg/kg wet 0.05000 92 56-126 3 20 1,1,2-Trichloroethane 0.0464 0.0050 mg/kg wet 0.05000 93 70-133 5 20 1,1-Dichloroethane 0.0493 0.0050 mg/kg wet 0.05000 99 74-127 7 20 1,1-Dichloroethylene 0.0467 0.0050 mg/kg wet 0.05000 93 67-149 8 20 1, 1 -Dichloropropylene 0.0485 0.0050 mg/kg wet 0.05000 97 71-130 9 20 1,2,3-Trichlorobenzene 0.0431 0.0050 mg/kg wet 0.05000 86 68-130 7 20 1,2,3-Trichloropropane 0.0445 0.0050 mg/kg wet 0.05000 89 60-137 2 20 1,2,4-Trichlorobenzene 0.0437 0.0050 mg/kg wet 0.05000 87 66-125 6 20 1,2,4-Trimethylbenzene 0.0427 0.0050 mg/kg wet 0.05000 85 69-129 4 20 1,2-Dibromoethane 0.0469 0.0050 mg/kg wet 0.05000 94 70-132 6 20 1,2-Dichlorobenzene 0.0422 0.0050 mg/kg wet 0.05000 84 72-123 4 20 1,2-Dichloroethane 0.0521 0.0050 mg/kg wet 0.05000 104 68-128 6 20 1,2-Dichloropropane 0.0514 0.0050 mg/kg wet 0.05000 103 73-130 5 20 1,3,5-Trimethylbenzene 0.0426 0.0050 mg/kg wet 0.05000 85 69-128 5 20 1,3-Dichlorobenzene 0.0420 0.0050 mg/kg wet 0.05000 84 71-120 4 20 1,3-Dichloropropane 0.0464 0.0050 mg/kg wet 0.05000 93 75-124 6 20 1,4-Dichlorobenzene 0.0414 0.0050 mg/kg wet 0.05000 83 71-123 4 20 2,2-Dichloropropane 0.0494 0.0050 mg/kg wet 0.05000 99 50-142 9 20 2-Chlorotoluene 0.0425 0.0050 mg/kg wet 0.05000 85 67-124 4 20 4-Chlorotoluene 0.0425 0.0050 mg/kg wet 0.05000 85 71-126 4 20 4-Isopropyltoluene 0.0432 0.0050 mg/kg wet 0.05000 86 68-129 5 20 Acetone 0.106 0.050 mg/kg wet 0.1000 106 29-198 9 20 Benzene 0.0505 0.0030 mg/kg wet 0.05000 101 74-127 6 20 Bromobenzene 0.0420 0.0050 mg/kg wet 0.05000 84 73-125 4 20 Bromochloromethane 0.0512 0.0050 mg/kg wet 0.05000 102 72-134 4 20 Bromodichloromethane 0.0524 0.0050 mg/kg wet 0.05000 105 75-122 5 20 Bromoform 0.0482 0.0050 mg/kg wet 0.05000 96 66-135 5 20 Bromomethane 0.0480 0.010 mg/kg wet 0.05000 96 20-180 12 20 Carbon Tetrachloride 0.0481 0.0050 mg/kg wet 0.05000 96 64-143 9 20 Chlorobenzene 0.0445 0.0050 mg/kg wet 0.05000 89 74-118 6 20 Chloroethane 0.0421 0.010 mg/kg wet 0.05000 84 33-149 8 20 Chloroform 0.0500 0.0050 mg/kg wet 0.05000 100 73-127 6 20 Chloromethane 0.0401 0.0050 mg/kg wet 0.05000 80 45-143 11 20 cis-1,2-Dichloroethylene 0.0498 0.0050 mg/kg wet 0.05000 100 76-134 6 20 cis-1,3-Dichloropropylene 0.0531 0.0050 mg/kg wet 0.05000 106 71-125 5 20 Dibromochloromethane 0.0468 0.0050 mg/kg wet 0.05000 94 73-122 5 20 Dichlorodifluoromethane 0.0335 0.0050 mg/kg wet 0.05000 67 26-146 10 20 Ethylbenzene 0.0442 0.0050 mg/kg wet 0.05000 88 74-128 7 20 Isopropyl Ether 0.0544 0.0050 mg/kg wet 0.05000 109 59-159 5 20 Isopropylbenzene (Cumene) 0.0424 0.0050 mg/kg wet 0.05000 85 68-126 5 20 m,p-Xylenes 0.0919 0.010 mg/kg wet 0.1000 92 75-124 7 20 Methyl Butyl Ketone (2-Hexanone) 0.0529 0.050 mg/kg wet 0.05000 106 61-157 8 20 Methyl Ethyl Ketone (2-Butanone) 0.0532 0.10 mg/kg wet 0.05000 106 63-149 6 20 Methyl Isobutyl Ketone 0.0574 0.050 mg/kg wet 0.05000 115 57-162 6 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO127 - 5035 LCS Dup (P9A0127-BSD1) Prepared & Analyzed: 01/08/19 Methylene Chloride 0.0512 0.010 mg/kg wet 0.05000 102 74-129 5 20 Methyl-tert-Butyl Ether 0.0562 0.010 mg/kg wet 0.05000 112 70-130 0.6 20 Naphthalene 0.0452 0.010 mg/kg wet 0.05000 90 57-157 5 20 n-Butylbenzene 0.0435 0.0050 mg/kg wet 0.05000 87 65-135 6 20 n-Propylbenzene 0.0426 0.0050 mg/kg wet 0.05000 85 67-130 5 20 o-Xylene 0.0455 0.0050 mg/kg wet 0.05000 91 74-126 6 20 sec-Butylbenzene 0.0423 0.0050 mg/kg wet 0.05000 85 66-131 6 20 Styrene 0.0463 0.0050 mg/kg wet 0.05000 93 77-121 7 20 tert-Butylbenzene 0.0421 0.0050 mg/kg wet 0.05000 84 67-132 5 20 Tetrachloroethylene 0.0481 0.0050 mg/kg wet 0.05000 96 68-130 8 20 Toluene 0.0487 0.0050 mg/kg wet 0.05000 97 71-129 6 20 trans-1,2-Dichloroethylene 0.0486 0.0050 mg/kg wet 0.05000 97 73-132 7 20 trans- 1,3-Dichloropropylene 0.0538 0.0050 mg/kg wet 0.05000 108 68-123 6 20 Trichloroethylene 0.0492 0.0050 mg/kg wet 0.05000 98 75-133 6 20 Trichlorofluoromethane 0.0448 0.0050 mg/kg wet 0.05000 90 44-146 9 20 Vinyl acetate 0.0888 0.025 mg/kg wet 0.05000 178 85-161 3 20 LH Vinyl chloride 0.0424 0.0050 mg/kg wet 0.05000 85 48-147 8 20 Xylenes, total 0.137 0.015 mg/kg wet 0.1500 92 74-126 7 20 Surrogate:4-Bromofluorobenzene 49.2 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 50.5 ug/L 50.00 101 84-123 Surrogate: Toluene-d8 44.5 ug/L 50.00 89 76-129 Batch P9AO133 - 5035 Blank (P9A0133-BLK1) Prepared & Analyzed: 01/09/19 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO133 - 5035 Blank (P9A0133-BLK1) Prepared & Analyzed: 01/09/19 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet Methylene Chloride BRL 0.010 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans-1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 50.3 ug/L 50.00 101 70-130 Surrogate: Dibromofluoromethane 50.4 ug/L 50.00 101 84-123 Surrogate: Toluene-d8 43.9 ug/L 50.00 88 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 46 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Attn: Steve Libbey 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9AO133 - 5035 Prism Work Order: 9010043 Time Submitted: 1/4/2019 8:25:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P9A0133-BSI) Prepared & Analyzed: 01/09/19 1,1,1,2-Tetrachloroethane 0.0499 0.0050 mg/kg wet 0.05000 100 72-115 1,1,1-Trichloroethane 0.0562 0.0050 mg/kg wet 0.05000 112 67-131 1,1,2,2-Tetrachloroethane 0.0492 0.0050 mg/kg wet 0.05000 98 56-126 1,1,2-Trichloroethane 0.0508 0.0050 mg/kg wet 0.05000 102 70-133 1,1-Dichloroethane 0.0551 0.0050 mg/kg wet 0.05000 110 74-127 1,1-Dichloroethylene 0.0546 0.0050 mg/kg wet 0.05000 109 67-149 1, 1 -Dichloropropylene 0.0579 0.0050 mg/kg wet 0.05000 116 71-130 1,2,3-Trichlorobenzene 0.0478 0.0050 mg/kg wet 0.05000 96 68-130 1,2,3-Trichloropropane 0.0470 0.0050 mg/kg wet 0.05000 94 60-137 1,2,4-Trichlorobenzene 0.0485 0.0050 mg/kg wet 0.05000 97 66-125 1,2,4-Trimethylbenzene 0.0475 0.0050 mg/kg wet 0.05000 95 69-129 1,2-Dibromoethane 0.0518 0.0050 mg/kg wet 0.05000 104 70-132 1,2-Dichlorobenzene 0.0459 0.0050 mg/kg wet 0.05000 92 72-123 1,2-Dichloroethane 0.0568 0.0050 mg/kg wet 0.05000 114 68-128 1,2-Dichloropropane 0.0563 0.0050 mg/kg wet 0.05000 113 73-130 1,3,5-Trimethylbenzene 0.0479 0.0050 mg/kg wet 0.05000 96 69-128 1,3-Dichlorobenzene 0.0461 0.0050 mg/kg wet 0.05000 92 71-120 1,3-Dichloropropane 0.0505 0.0050 mg/kg wet 0.05000 101 75-124 1,4-Dichlorobenzene 0.0454 0.0050 mg/kg wet 0.05000 91 71-123 2,2-Dichloropropane 0.0573 0.0050 mg/kg wet 0.05000 115 50-142 2-Chlorotoluene 0.0473 0.0050 mg/kg wet 0.05000 95 67-124 4-Chlorotoluene 0.0473 0.0050 mg/kg wet 0.05000 95 71-126 4-Isopropyltoluene 0.0490 0.0050 mg/kg wet 0.05000 98 68-129 Acetone 0.122 0.050 mg/kg wet 0.1000 122 29-198 Benzene 0.0562 0.0030 mg/kg wet 0.05000 112 74-127 Bromobenzene 0.0462 0.0050 mg/kg wet 0.05000 92 73-125 Bromochloromethane 0.0557 0.0050 mg/kg wet 0.05000 111 72-134 Bromodichloromethane 0.0570 0.0050 mg/kg wet 0.05000 114 75-122 Bromoform 0.0511 0.0050 mg/kg wet 0.05000 102 66-135 Bromomethane 0.0332 0.010 mg/kg wet 0.05000 66 20-180 Carbon Tetrachloride 0.0569 0.0050 mg/kg wet 0.05000 114 64-143 Chlorobenzene 0.0489 0.0050 mg/kg wet 0.05000 98 74-118 Chloroethane 0.0445 0.010 mg/kg wet 0.05000 89 33-149 Chloroform 0.0557 0.0050 mg/kg wet 0.05000 111 73-127 Chloromethane 0.0324 0.0050 mg/kg wet 0.05000 65 45-143 cis-1,2-Dichloroethylene 0.0558 0.0050 mg/kg wet 0.05000 112 76-134 cis-1,3-Dichloropropylene 0.0587 0.0050 mg/kg wet 0.05000 117 71-125 Dibromochloromethane 0.0510 0.0050 mg/kg wet 0.05000 102 73-122 Dichlorodifluoromethane 0.0369 0.0050 mg/kg wet 0.05000 74 26-146 Ethylbenzene 0.0497 0.0050 mg/kg wet 0.05000 99 74-128 Isopropyl Ether 0.0597 0.0050 mg/kg wet 0.05000 119 59-159 Isopropylbenzene (Cumene) 0.0485 0.0050 mg/kg wet 0.05000 97 68-126 m,p-Xylenes 0.104 0.010 mg/kg wet 0.1000 104 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0592 0.050 mg/kg wet 0.05000 118 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0582 0.10 mg/kg wet 0.05000 116 63-149 Methyl Isobutyl Ketone 0.0634 0.050 mg/kg wet 0.05000 127 57-162 LH This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 31 of 46 Level II QC Report P R I IS M Full -Service Analytical 1/11/19 Environmental Solutions LABORATORIES, INC. Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO133 - 5035 LCS (P9A0133-BS1) Prepared & Analyzed: 01/09/19 Methylene Chloride 0.0554 0.010 mg/kg wet 0.05000 111 74-129 Methyl-tert-Butyl Ether 0.0603 0.010 mg/kg wet 0.05000 121 70-130 Naphthalene 0.0509 0.010 mg/kg wet 0.05000 102 57-157 n-Butylbenzene 0.0496 0.0050 mg/kg wet 0.05000 99 65-135 n-Propylbenzene 0.0480 0.0050 mg/kg wet 0.05000 96 67-130 o-Xylene 0.0513 0.0050 mg/kg wet 0.05000 103 74-126 sec-Butylbenzene 0.0484 0.0050 mg/kg wet 0.05000 97 66-131 Styrene 0.0516 0.0050 mg/kg wet 0.05000 103 77-121 tert-Butyl benzene 0.0478 0.0050 mg/kg wet 0.05000 96 67-132 Tetrachloroethylene 0.0556 0.0050 mg/kg wet 0.05000 111 68-130 Toluene 0.0547 0.0050 mg/kg wet 0.05000 109 71-129 trans- 1,2-Dichloroethylene 0.0553 0.0050 mg/kg wet 0.05000 111 73-132 trans- 1,3-Dichloropropylene 0.0589 0.0050 mg/kg wet 0.05000 118 68-123 Trichloroethylene 0.0563 0.0050 mg/kg wet 0.05000 113 75-133 Trichlorofluoromethane 0.0474 0.0050 mg/kg wet 0.05000 95 44-146 Vinyl acetate 0.0882 0.025 mg/kg wet 0.05000 176 85-161 LH Vinyl chloride 0.0441 0.0050 mg/kg wet 0.05000 88 48-147 Xylenes, total 0.155 0.015 mg/kg wet 0.1500 103 74-126 Surrogate:4-Bromofluorobenzene 49.9 ug/L 50.00 100 70-130 Surrogate: Dibromofluoromethane 50.3 ug/L 50.00 101 84-123 Surrogate: Toluene-d8 44.9 ug/L 50.00 90 76-129 LCS Dup (P9AO133-BSD1) Prepared & Analyzed: 01/09/19 1,1,1,2-Tetrachloroethane 0.0480 0.0050 mg/kg wet 0.05000 96 72-115 4 20 1,1,1-Trichloroethane 0.0536 0.0050 mg/kg wet 0.05000 107 67-131 5 20 1,1,2,2-Tetrachloroethane 0.0473 0.0050 mg/kg wet 0.05000 95 56-126 4 20 1,1,2-Trichloroethane 0.0484 0.0050 mg/kg wet 0.05000 97 70-133 5 20 1,1-Dichloroethane 0.0534 0.0050 mg/kg wet 0.05000 107 74-127 3 20 1,1-Dichloroethylene 0.0514 0.0050 mg/kg wet 0.05000 103 67-149 6 20 1, 1 -Dichloropropylene 0.0544 0.0050 mg/kg wet 0.05000 109 71-130 6 20 1,2,3-Trichlorobenzene 0.0464 0.0050 mg/kg wet 0.05000 93 68-130 3 20 1,2,3-Trichloropropane 0.0460 0.0050 mg/kg wet 0.05000 92 60-137 2 20 1,2,4-Trichlorobenzene 0.0468 0.0050 mg/kg wet 0.05000 94 66-125 4 20 1,2,4-Trimethylbenzene 0.0458 0.0050 mg/kg wet 0.05000 92 69-129 4 20 1,2-Dibromoethane 0.0501 0.0050 mg/kg wet 0.05000 100 70-132 3 20 1,2-Dichlorobenzene 0.0451 0.0050 mg/kg wet 0.05000 90 72-123 2 20 1,2-Dichloroethane 0.0553 0.0050 mg/kg wet 0.05000 111 68-128 3 20 1,2-Dichloropropane 0.0549 0.0050 mg/kg wet 0.05000 110 73-130 2 20 1,3,5-Trimethylbenzene 0.0461 0.0050 mg/kg wet 0.05000 92 69-128 4 20 1,3-Dichlorobenzene 0.0449 0.0050 mg/kg wet 0.05000 90 71-120 3 20 1,3-Dichloropropane 0.0486 0.0050 mg/kg wet 0.05000 97 75-124 4 20 1,4-Dichlorobenzene 0.0441 0.0050 mg/kg wet 0.05000 88 71-123 3 20 2,2-Dichloropropane 0.0547 0.0050 mg/kg wet 0.05000 109 50-142 5 20 2-Chlorotoluene 0.0460 0.0050 mg/kg wet 0.05000 92 67-124 3 20 4-Chlorotoluene 0.0456 0.0050 mg/kg wet 0.05000 91 71-126 4 20 4-Isopropyltoluene 0.0467 0.0050 mg/kg wet 0.05000 93 68-129 5 20 Acetone 0.120 0.050 mg/kg wet 0.1000 120 29-198 1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 32 of 46 P R I IS M Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO133 - 5035 LCS Dup (P9A0133-BSD1) Prepared & Analyzed: 01/09/19 Benzene 0.0545 0.0030 mg/kg wet 0.05000 109 74-127 3 20 Bromobenzene 0.0450 0.0050 mg/kg wet 0.05000 90 73-125 2 20 Bromochloromethane 0.0545 0.0050 mg/kg wet 0.05000 109 72-134 2 20 Bromodichloromethane 0.0559 0.0050 mg/kg wet 0.05000 112 75-122 2 20 Bromoform 0.0495 0.0050 mg/kg wet 0.05000 99 66-135 3 20 Bromomethane 0.0317 0.010 mg/kg wet 0.05000 63 20-180 5 20 Carbon Tetrachloride 0.0532 0.0050 mg/kg wet 0.05000 106 64-143 7 20 Chlorobenzene 0.0470 0.0050 mg/kg wet 0.05000 94 74-118 4 20 Chloroethane 0.0434 0.010 mg/kg wet 0.05000 87 33-149 2 20 Chloroform 0.0538 0.0050 mg/kg wet 0.05000 108 73-127 3 20 Chloromethane 0.0353 0.0050 mg/kg wet 0.05000 71 45-143 9 20 LH cis-1,2-Dichloroethylene 0.0541 0.0050 mg/kg wet 0.05000 108 76-134 3 20 cis-1,3-Dichloropropylene 0.0571 0.0050 mg/kg wet 0.05000 114 71-125 3 20 Dibromochloromethane 0.0494 0.0050 mg/kg wet 0.05000 99 73-122 3 20 Dichlorodifluoromethane 0.0351 0.0050 mg/kg wet 0.05000 70 26-146 5 20 Ethylbenzene 0.0472 0.0050 mg/kg wet 0.05000 94 74-128 5 20 Isopropyl Ether 0.0584 0.0050 mg/kg wet 0.05000 117 59-159 2 20 Isopropylbenzene (Cumene) 0.0465 0.0050 mg/kg wet 0.05000 93 68-126 4 20 m,p-Xylenes 0.0987 0.010 mg/kg wet 0.1000 99 75-124 5 20 Methyl Butyl Ketone (2-Hexanone) 0.0561 0.050 mg/kg wet 0.05000 112 61-157 5 20 Methyl Ethyl Ketone (2-Butanone) 0.0565 0.10 mg/kg wet 0.05000 113 63-149 3 20 Methyl Isobutyl Ketone 0.0610 0.050 mg/kg wet 0.05000 122 57-162 4 20 Methylene Chloride 0.0544 0.010 mg/kg wet 0.05000 109 74-129 2 20 Methyl-tert-Butyl Ether 0.0565 0.010 mg/kg wet 0.05000 113 70-130 7 20 Naphthalene 0.0495 0.010 mg/kg wet 0.05000 99 57-157 3 20 n-Butylbenzene 0.0474 0.0050 mg/kg wet 0.05000 95 65-135 5 20 n-Propylbenzene 0.0461 0.0050 mg/kg wet 0.05000 92 67-130 4 20 o-Xylene 0.0486 0.0050 mg/kg wet 0.05000 97 74-126 5 20 sec-Butylbenzene 0.0462 0.0050 mg/kg wet 0.05000 92 66-131 5 20 Styrene 0.0495 0.0050 mg/kg wet 0.05000 99 77-121 4 20 tert-Butyl benzene 0.0460 0.0050 mg/kg wet 0.05000 92 67-132 4 20 Tetrachloroethylene 0.0528 0.0050 mg/kg wet 0.05000 106 68-130 5 20 Toluene 0.0526 0.0050 mg/kg wet 0.05000 105 71-129 4 20 trans- 1,2-Dichloroethylene 0.0526 0.0050 mg/kg wet 0.05000 105 73-132 5 20 trans- 1,3-Dichloropropylene 0.0570 0.0050 mg/kg wet 0.05000 114 68-123 3 20 Trichloroethylene 0.0545 0.0050 mg/kg wet 0.05000 109 75-133 3 20 Trichlorofluoromethane 0.0445 0.0050 mg/kg wet 0.05000 89 44-146 6 20 Vinyl acetate 0.0846 0.025 mg/kg wet 0.05000 169 85-161 4 20 LH Vinyl chloride 0.0420 0.0050 mg/kg wet 0.05000 84 48-147 5 20 Xylenes, total 0.147 0.015 mg/kg wet 0.1500 98 74-126 5 20 Surrogate:4-Bromofluorobenzene 49.9 ug/L 50.00 100 70-130 Surrogate: Dibromofluoromethane 51.0 ug/L 50.00 102 84-123 Surrogate: Toluene-d8 44.2 ug/L 50.00 88 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 33 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO146 - 3550C MS Blank (P9A0146-BLK1) Prepared & Analyzed: 01/10/19 1,2,4-Trichlorobenzene BRL 0.33 mg/kg wet 1,2-Dichlorobenzene BRL 0.33 mg/kg wet 1,3-Dichlorobenzene BRL 0.33 mg/kg wet 1,4-Dichlorobenzene BRL 0.33 mg/kg wet 2,4,5-Trichlorophenol BRL 0.33 mg/kg wet 2,4,6-Trichlorophenol BRL 0.33 mg/kg wet 2,4-Dichlorophenol BRL 0.33 mg/kg wet 2,4-Dimethylphenol BRL 0.33 mg/kg wet 2,4-Dinitrophenol BRL 0.33 mg/kg wet 2,4-Dinitrotoluene BRL 0.33 mg/kg wet 2,6-Dinitrotoluene BRL 0.33 mg/kg wet 2-Chloronaphthalene BRL 0.33 mg/kg wet 2-Chlorophenol BRL 0.33 mg/kg wet 2-Methyl naphthalene BRL 0.33 mg/kg wet 2-Methylphenol BRL 0.33 mg/kg wet 2-Nitroaniline BRL 0.33 mg/kg wet 2-Nitrophenol BRL 0.33 mg/kg wet 3,3'-Dichlorobenzidine BRL 0.33 mg/kg wet 3/4-Methyl phenol BRL 0.33 mg/kg wet 3-Nitroaniline BRL 0.33 mg/kg wet 4,6-Dinitro-2-methylphenol BRL 0.33 mg/kg wet 4-Bromophenyl phenyl ether BRL 0.33 mg/kg wet 4-Chloro-3-methylphenol BRL 0.33 mg/kg wet 4-Chloroaniline BRL 0.33 mg/kg wet 4-Chlorophenyl phenyl ether BRL 0.33 mg/kg wet 4-Nitroaniline BRL 0.33 mg/kg wet 4-Nitrophenol BRL 0.33 mg/kg wet Acenaphthene BRL 0.33 mg/kg wet Acenaphthylene BRL 0.33 mg/kg wet Aniline BRL 0.33 mg/kg wet Anthracene BRL 0.33 mg/kg wet Azobenzene BRL 0.33 mg/kg wet Benzo(a)anthracene BRL 0.33 mg/kg wet Benzo(a)pyrene BRL 0.33 mg/kg wet Benzo(b)fluoranthene BRL 0.33 mg/kg wet Benzo(g,h,i)perylene BRL 0.33 mg/kg wet Benzo(k)fluoranthene BRL 0.33 mg/kg wet Benzoic Acid BRL 0.33 mg/kg wet Benzyl alcohol BRL 0.33 mg/kg wet bis(2-Chloroethoxy)methane BRL 0.33 mg/kg wet Bis(2-Chloroethyl)ether BRL 0.33 mg/kg wet Bis(2-chloroisopropyl)ether BRL 0.33 mg/kg wet Bis(2-Ethylhexyl)phthalate BRL 0.33 mg/kg wet Butyl benzyl phthalate BRL 0.33 mg/kg wet Chrysene BRL 0.33 mg/kg wet Dibenzo(a,h)anthracene BRL 0.33 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 34 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Attn: Steve Libbey 2923 South Tryon St. Ste 100 Project No: CHP-035 Prism Work Order: 9010043 Time Submitted: 1/4/2019 8:25:OOAM Charlotte, NC 28203 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO146 - 3550C MS Blank (P9A0146-BLK1) Prepared & Analyzed: 01/10/19 Dibenzofuran BRL 0.33 mg/kg wet Diethyl phthalate BRL 0.33 mg/kg wet Dimethyl phthalate BRL 0.33 mg/kg wet Di-n-butyl phthalate BRL 0.33 mg/kg wet Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.33 mg/kg wet Fluorene BRL 0.33 mg/kg wet Hexachlorobenzene BRL 0.33 mg/kg wet Hexachlorobutadiene BRL 0.33 mg/kg wet Hexachlorocyclopentadiene BRL 0.33 mg/kg wet Hexachloroethane BRL 0.33 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.33 mg/kg wet Isophorone BRL 0.33 mg/kg wet Naphthalene BRL 0.33 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.33 mg/kg wet N-Nitrosodiphenylamine BRL 0.33 mg/kg wet Pentachlorophenol BRL 0.33 mg/kg wet Phenanthrene BRL 0.33 mg/kg wet Phenol BRL 0.33 mg/kg wet Pyrene BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tribromophenol 3.46 mg/kg wet 3.333 104 37-131 Surrogate: 2-Fluorobiphenyl 1.78 mg/kg wet 1.667 107 47-130 Surrogate: 2-Fluorophenol 3.68 mg/kg wet 3.333 110 44-117 Surrogate: Nitrobenzene-d5 1.48 mg/kg wet 1.667 89 45-121 Surrogate: Phenol-d5 3.48 mg/kg wet 3.333 104 37-127 Surrogate: Terphenyl-d14 1.73 mg/kg wet 1.667 104 38-135 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 35 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Attn: Steve Libbey 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9AO146 - 3550C MS Prism Work Order: 9010043 Time Submitted: 1/4/2019 8:25:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes LCS (P9A0146-BS1) Prepared & Analyzed: 01/10/19 1,2,4-Trichlorobenzene 1.32 0.33 mg/kg wet 1.667 79 54-110 1,2-Dichlorobenzene 1.42 0.33 mg/kg wet 1.667 85 53-107 1,3-Dichlorobenzene 1.38 0.33 mg/kg wet 1.667 83 52-108 1,4-Dichlorobenzene 1.40 0.33 mg/kg wet 1.667 84 52-108 2,4,5-Trichlorophenol 1.58 0.33 mg/kg wet 1.667 95 62-124 2,4,6-Trichlorophenol 1.59 0.33 mg/kg wet 1.667 95 62-120 2,4-Dichlorophenol 1.33 0.33 mg/kg wet 1.667 80 58-113 2,4-Dimethylphenol 1.83 0.33 mg/kg wet 1.667 110 59-110 2,4-Dinitrophenol 0.257 0.33 mg/kg wet 1.667 15 29-134 2,4-Dinitrotoluene 1.45 0.33 mg/kg wet 1.667 87 63-137 2,6-Dinitrotoluene 1.55 0.33 mg/kg wet 1.667 93 59-134 2-Chloronaphthalene 1.57 0.33 mg/kg wet 1.667 94 41-147 2-Chlorophenol 1.51 0.33 mg/kg wet 1.667 90 55-108 2-Methyl naphthalene 1.36 0.33 mg/kg wet 1.667 81 57-116 2-Methylphenol 1.58 0.33 mg/kg wet 1.667 95 56-111 2-Nitroaniline 1.58 0.33 mg/kg wet 1.667 95 62-125 2-Nitrophenol 1.21 0.33 mg/kg wet 1.667 73 58-112 3,3'-Dichlorobenzidine 1.90 0.33 mg/kg wet 1.667 114 51-161 3/4-Methyl phenol 1.42 0.33 mg/kg wet 1.667 85 56-111 3-Nitroaniline 1.55 0.33 mg/kg wet 1.667 93 65-136 4,6-Dinitro-2-methylphenol 0.853 0.33 mg/kg wet 1.667 51 46-148 4-Bromophenyl phenyl ether 1.59 0.33 mg/kg wet 1.667 96 58-137 4-Chloro-3-methylphenol 1.42 0.33 mg/kg wet 1.667 85 60-118 4-Chloroaniline 1.43 0.33 mg/kg wet 1.667 86 53-144 4-Chlorophenyl phenyl ether 1.62 0.33 mg/kg wet 1.667 97 59-131 4-Nitroaniline 1.70 0.33 mg/kg wet 1.667 102 62-143 4-Nitrophenol 1.48 0.33 mg/kg wet 1.667 89 48-148 Acenaphthene 1.54 0.33 mg/kg wet 1.667 93 62-118 Acenaphthylene 1.60 0.33 mg/kg wet 1.667 96 64-116 Aniline 1.78 0.33 mg/kg wet 1.667 107 24-190 Anthracene 1.71 0.33 mg/kg wet 1.667 103 71-132 Azobenzene 1.61 0.33 mg/kg wet 1.667 97 56-125 Benzo(a)anthracene 1.63 0.33 mg/kg wet 1.667 98 71-129 Benzo(a)pyrene 1.65 0.33 mg/kg wet 1.667 99 74-129 Benzo(b)fluoranthene 1.63 0.33 mg/kg wet 1.667 98 63-138 Benzo(g,h,i)perylene 1.70 0.33 mg/kg wet 1.667 102 41-154 Benzo(k)fluoranthene 1.73 0.33 mg/kg wet 1.667 104 62-145 Benzoic Acid BRL 0.33 mg/kg wet 1.667 10-83 Benzyl alcohol 1.49 0.33 mg/kg wet 1.667 89 55-112 bis(2-Chloroethoxy)methane 1.39 0.33 mg/kg wet 1.667 83 52-118 Bis(2-Chloroethyl)ether 1.50 0.33 mg/kg wet 1.667 90 50-116 Bis(2-chloroisopropyl)ether 1.46 0.33 mg/kg wet 1.667 88 48-119 Bis(2-Ethylhexyl)phthalate 1.64 0.33 mg/kg wet 1.667 99 62-135 Butyl benzyl phthalate 1.59 0.33 mg/kg wet 1.667 95 62-133 Chrysene 1.61 0.33 mg/kg wet 1.667 97 72-129 Dibenzo(a,h)anthracene 1.14 0.33 mg/kg wet 1.667 68 41-158 L L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 36 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO146 - 3550C MS LCS (PM0146-113SI) Prepared & Analyzed: 01/10/19 Dibenzofuran 1.56 0.33 mg/kg wet 1.667 93 64-115 Diethyl phthalate 1.64 0.33 mg/kg wet 1.667 99 73-120 Dimethyl phthalate 1.61 0.33 mg/kg wet 1.667 96 71-115 Di-n-butyl phthalate 1.67 0.33 mg/kg wet 1.667 100 68-127 Di-n-octyl phthalate 1.70 0.33 mg/kg wet 1.667 102 53-150 Fluoranthene 1.65 0.33 mg/kg wet 1.667 99 64-136 Fluorene 1.66 0.33 mg/kg wet 1.667 99 67-120 Hexachlorobenzene 1.52 0.33 mg/kg wet 1.667 91 63-134 Hexachlorobutadiene 1.42 0.33 mg/kg wet 1.667 85 55-112 Hexachlorocyclopentadiene 1.52 0.33 mg/kg wet 1.667 91 43-135 Hexachloroethane 1.35 0.33 mg/kg wet 1.667 81 49-113 Indeno(1,2,3-cd)pyrene 1.96 0.33 mg/kg wet 1.667 118 40-160 Isophorone 1.38 0.33 mg/kg wet 1.667 83 55-118 Naphthalene 1.36 0.33 mg/kg wet 1.667 82 62-111 Nitrobenzene 1.29 0.33 mg/kg wet 1.667 77 50-116 N-Nitroso-di-n-propylamine 1.36 0.33 mg/kg wet 1.667 82 53-113 N-Nitrosodiphenylamine 1.91 0.33 mg/kg wet 1.667 115 76-144 Pentachlorophenol 1.52 0.33 mg/kg wet 1.667 91 36-145 Phenanthrene 1.67 0.33 mg/kg wet 1.667 100 72-123 Phenol 1.51 0.33 mg/kg wet 1.667 90 56-108 Pyrene 1.61 0.33 mg/kg wet 1.667 97 51-141 Surrogate: 2,4,6-Tribromophenol 3.45 mg/kg wet 3.333 103 37-131 Surrogate: 2-Fluorobiphenyl 1.59 mg/kg wet 1.667 95 47-130 Surrogate: 2-Fluorophenol 3.14 mg/kg wet 3.333 94 44-117 Surrogate: Nitrobenzene-d5 1.30 mg/kg wet 1.667 78 45-121 Surrogate: Phenol-d5 3.07 mg/kg wet 3.333 92 37-127 Surrogate: Terphenyl-d14 1.57 mg/kg wet 1.667 94 38-135 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 37 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO146 - 3550C MS LCS Dup (P9AO146-BSD1) Prepared & Analyzed: 01/10/19 1,2,4-Trichlorobenzene 1.32 0.33 mg/kg wet 1.667 79 54-110 0.6 20 1,2-Dichlorobenzene 1.47 0.33 mg/kg wet 1.667 88 53-107 4 20 1,3-Dichlorobenzene 1.45 0.33 mg/kg wet 1.667 87 52-108 4 20 1,4-Dichlorobenzene 1.45 0.33 mg/kg wet 1.667 87 52-108 4 20 2,4,5-Trichlorophenol 1.57 0.33 mg/kg wet 1.667 94 62-124 0.1 20 2,4,6-Trichlorophenol 1.60 0.33 mg/kg wet 1.667 96 62-120 0.9 20 2,4-Dichlorophenol 1.36 0.33 mg/kg wet 1.667 82 58-113 3 20 2,4-Dimethylphenol 1.91 0.33 mg/kg wet 1.667 114 59-110 4 20 L2 2,4-Dinitrophenol 0.262 0.33 mg/kg wet 1.667 16 29-134 2 20 L 2,4-Dinitrotoluene 1.39 0.33 mg/kg wet 1.667 84 63-137 4 20 2,6-Dinitrotoluene 1.51 0.33 mg/kg wet 1.667 90 59-134 3 20 2-Chloronaphthalene 1.60 0.33 mg/kg wet 1.667 96 41-147 2 20 2-Chlorophenol 1.59 0.33 mg/kg wet 1.667 95 55-108 5 20 2-Methyl naphthalene 1.38 0.33 mg/kg wet 1.667 83 57-116 2 20 2-Methylphenol 1.67 0.33 mg/kg wet 1.667 100 56-111 6 20 2-Nitroaniline 1.64 0.33 mg/kg wet 1.667 99 62-125 4 20 2-Nitrophenol 1.22 0.33 mg/kg wet 1.667 73 58-112 0.3 20 3,3'-Dichlorobenzidine 1.88 0.33 mg/kg wet 1.667 113 51-161 0.9 20 3/4-Methyl phenol 1.44 0.33 mg/kg wet 1.667 87 56-111 2 20 3-Nitroaniline 1.50 0.33 mg/kg wet 1.667 90 65-136 3 20 4,6-Dinitro-2-methylphenol 0.820 0.33 mg/kg wet 1.667 49 46-148 4 20 4-Bromophenyl phenyl ether 1.55 0.33 mg/kg wet 1.667 93 58-137 3 20 4-Chloro-3-methylphenol 1.45 0.33 mg/kg wet 1.667 87 60-118 2 20 4-Chloroaniline 1.45 0.33 mg/kg wet 1.667 87 53-144 1 20 4-Chlorophenyl phenyl ether 1.60 0.33 mg/kg wet 1.667 96 59-131 2 20 4-Nitroaniline 1.77 0.33 mg/kg wet 1.667 106 62-143 4 20 4-Nitrophenol 1.45 0.33 mg/kg wet 1.667 87 48-148 2 20 Acenaphthene 1.55 0.33 mg/kg wet 1.667 93 62-118 0.3 20 Acenaphthylene 1.60 0.33 mg/kg wet 1.667 96 64-116 0 20 Aniline 1.88 0.33 mg/kg wet 1.667 113 24-190 5 20 Anthracene 1.65 0.33 mg/kg wet 1.667 99 71-132 4 20 Azobenzene 1.56 0.33 mg/kg wet 1.667 93 56-125 4 20 Benzo(a)anthracene 1.60 0.33 mg/kg wet 1.667 96 71-129 1 20 Benzo(a)pyrene 1.65 0.33 mg/kg wet 1.667 99 74-129 0.02 20 Benzo(b)fluoranthene 1.64 0.33 mg/kg wet 1.667 98 63-138 0.7 20 Benzo(g,h,i)perylene 1.67 0.33 mg/kg wet 1.667 100 41-154 2 20 Benzo(k)fluoranthene 1.70 0.33 mg/kg wet 1.667 102 62-145 1 20 Benzoic Acid BRL 0.33 mg/kg wet 1.667 10-83 20 L Benzyl alcohol 1.53 0.33 mg/kg wet 1.667 92 55-112 3 20 bis(2-Chloroethoxy)methane 1.42 0.33 mg/kg wet 1.667 85 52-118 2 20 Bis(2-Chloroethyl)ether 1.54 0.33 mg/kg wet 1.667 92 50-116 3 20 Bis(2-chloroisopropyl)ether 1.52 0.33 mg/kg wet 1.667 91 48-119 4 20 Bis(2-Ethylhexyl)phthalate 1.62 0.33 mg/kg wet 1.667 97 62-135 2 20 Butyl benzyl phthalate 1.55 0.33 mg/kg wet 1.667 93 62-133 2 20 Chrysene 1.61 0.33 mg/kg wet 1.667 96 72-129 0.5 20 Dibenzo(a,h)anthracene 1.10 0.33 mg/kg wet 1.667 66 41-158 3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 38 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO146 - 3550C MS LCS Dup (P9A0146-BSD1) Prepared & Analyzed: 01/10/19 Dibenzofuran 1.58 0.33 mg/kg wet 1.667 95 64-115 2 20 Diethyl phthalate 1.62 0.33 mg/kg wet 1.667 97 73-120 2 20 Dimethyl phthalate 1.60 0.33 mg/kg wet 1.667 96 71-115 0.3 20 Di-n-butyl phthalate 1.64 0.33 mg/kg wet 1.667 99 68-127 1 20 Di-n-octyl phthalate 1.70 0.33 mg/kg wet 1.667 102 53-150 0.1 20 Fluoranthene 1.60 0.33 mg/kg wet 1.667 96 64-136 3 20 Fluorene 1.65 0.33 mg/kg wet 1.667 99 67-120 0.3 20 Hexachlorobenzene 1.51 0.33 mg/kg wet 1.667 90 63-134 0.9 20 Hexachlorobutadiene 1.44 0.33 mg/kg wet 1.667 86 55-112 1 20 Hexachlorocyclopentadiene 1.52 0.33 mg/kg wet 1.667 91 43-135 0.1 20 Hexachloroethane 1.40 0.33 mg/kg wet 1.667 84 49-113 4 20 Indeno(1,2,3-cd)pyrene 1.96 0.33 mg/kg wet 1.667 118 40-160 0.07 20 Isophorone 1.38 0.33 mg/kg wet 1.667 83 55-118 0.3 20 Naphthalene 1.38 0.33 mg/kg wet 1.667 83 62-111 1 20 Nitrobenzene 1.29 0.33 mg/kg wet 1.667 78 50-116 0.4 20 N-Nitroso-di-n-propylamine 1.43 0.33 mg/kg wet 1.667 86 53-113 5 20 N-Nitrosodiphenylamine 1.92 0.33 mg/kg wet 1.667 115 76-144 0.2 20 Pentachlorophenol 1.62 0.33 mg/kg wet 1.667 97 36-145 6 20 Phenanthrene 1.62 0.33 mg/kg wet 1.667 97 72-123 3 20 Phenol 1.55 0.33 mg/kg wet 1.667 93 56-108 3 20 Pyrene 1.60 0.33 mg/kg wet 1.667 96 51-141 0.9 20 Surrogate: 2,4,6-Tribromophenol 3.33 mg/kg wet 3.333 100 37-131 Surrogate: 2-Fluorobiphenyl 1.56 mg/kg wet 1.667 94 47-130 Surrogate: 2-Fluorophenol 3.20 mg/kg wet 3.333 96 44-117 Surrogate: Nitrobenzene-d5 1.23 mg/kg wet 1.667 74 45-121 Surrogate: Phenol-d5 3.08 mg/kg wet 3.333 93 37-127 Surrogate: Terphenyl-d14 1.51 mg/kg wet 1.667 91 38-135 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 39 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO082 - MADEP VPH (S) Blank (P9A0082-BLK1) Prepared & Analyzed: 01/07/19 C5-C8 Aliphatics BRL 5.0 mg/kg wet C9-Cl2 Aliphatics BRL 5.0 mg/kg wet C9-Cl0 Aromatics BRL 5.0 mg/kg wet Surrogate: 2,5-Dibromotoluene (PID) 9410 ug/L 10000 94 70-130 Surrogate: 2,5-Dibromotoluene (FID) 10400 ug/L 10000 104 70-130 LCS (PM0082-13SI) Prepared & Analyzed: 01/07/19 C5-C8 Aliphatics 30.0 5.0 mg/kg wet 32.00 94 70-130 C9-Cl0 Aromatics 9.75 5.0 mg/kg wet 10.67 91 70-130 C9-Cl2 Aliphatic 35.3 5.0 mg/kg wet 32.00 110 70-130 Surrogate: 2,5-Dibromotoluene (PID) 9210 ug/L 10000 92 70-130 Surrogate: 2,5-Dibromotoluene (FID) 10200 ug/L 10000 102 70-130 LCS Dup (P9A0082-BSD1) Prepared & Analyzed: 01/07/19 C5-C8 Aliphatics 30.3 5.0 mg/kg wet 32.00 95 70-130 1 50 C9-Cl0 Aromatics 9.31 5.0 mg/kg wet 10.67 87 70-130 5 50 C9-Cl2 Aliphatic 34.4 5.0 mg/kg wet 32.00 107 70-130 2 50 Surrogate: 2,5-Dibromotoluene (PID) 9290 ug/L 10000 93 70-130 Surrogate: 2,5-Dibromotoluene (FID) 10300 ug/L 10000 103 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 40 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Attn: Steve Libbey 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Gasoline Range Organics by GC/FID - Quality Control Level II QC Report 1/11/19 Prism Work Order: 9010043 Time Submitted: 1/4/2019 8:25:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO090 - 5035 Blank (P9A0090-BLK1) Prepared & Analyzed: 01/07/19 Gasoline Range Organics BRL 5.0 mg/kg wet Surrogate: a,a,a-Trifluorotoluene 5.00 mg/kg 5.000 100 50-137 LCS (PM0090-113SI) Prepared & Analyzed: 01/07/19 Gasoline Range Organics 48.9 5.0 mg/kg wet 50.00 98 41-138 Surrogate: a,a,a-Trifluorotoluene 5.15 mg/kg 5.000 103 50-137 LCS Dup (P9AO090-BSD1) Prepared & Analyzed: 01/07/19 Gasoline Range Organics 52.7 5.0 mg/kg wet 50.00 105 41-138 7 20 Surrogate: a,a,a-Trifluorotoluene 5.15 mg/kg 5.000 103 50-137 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 41 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Level II QC Report 1/11/19 Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Prism Work Order: 9010043 Attn: Steve Libbey Time Submitted: 1/4/2019 8:25:OOAM 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Extractable Petroleum Hydrocarbons by GC/FID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9A0103 - 3550C GC Blank (P9A0103-BLK1) Prepared: 01/08/19 Analyzed: 01/09/19 C9-Cl8 Aliphatics BRL 25 mg/kg wet C19-C36 Aliphatics BRL 25 mg/kg wet C11-C22 Aromatics BRL 9.9 mg/kg wet Surrogate: 1-Chlorooctadecane 1.45 mg/kg wet 1.980 73 40-140 Surrogate: o-Terphenyl 1.61 mg/kg wet 1.980 81 40-140 Surrogate: 2-Fluorobiphenyl 3.12 mg/kg wet 3.960 79 40-140 Surrogate: 2-Bromonaphthalene 4.01 mg/kg wet 3.960 101 40-140 LCS (PM0103-13SI) Prepared: 01/08/19 Analyzed: 01/09/19 C9-Cl8 Aliphatics 47.5 24 mg/kg wet 58.65 81 40-140 C19-C36 Aliphatics 76.8 24 mg/kg wet 78.20 98 40-140 C11-C22 Aromatics 204 9.8 mg/kg wet 166.2 123 40-140 Surrogate: 1-Chlorooctadecane 1.40 mg/kg wet 1.955 72 40-140 Surrogate: o-Terphenyl 2.05 mg/kg wet 1.955 105 40-140 Surrogate: 2-Fluorobiphenyl 3.53 mg/kg wet 3.910 90 40-140 Surrogate: 2-Bromonaphthalene 4.56 mg/kg wet 3.910 117 40-140 LCS Dup (P9A0103-BSD1) Prepared: 01/08/19 Analyzed: 01/09/19 C9-Cl8 Aliphatics 53.6 25 mg/kg wet 59.41 90 40-140 12 50 C19-C36 Aliphatics 85.9 25 mg/kg wet 79.21 108 40-140 11 50 C11-C22 Aromatics 217 9.9 mg/kg wet 168.3 129 40-140 6 50 Surrogate: 1-Chlorooctadecane 1.63 mg/kg wet 1.980 82 40-140 Surrogate: o-Terphenyl 1.99 mg/kg wet 1.980 101 40-140 Surrogate: 2-Fluorobiphenyl 3.36 mg/kg wet 3.960 85 40-140 Surrogate: 2-Bromonaphthalene 4.29 mg/kg wet 3.960 108 40-140 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 42 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Hart & Hickman (Charlotte) Project: Cindy Lane UST, Charlotte, NC Attn: Steve Libbey 2923 South Tryon St. Ste 100 Project No: CHP-035 Charlotte, NC 28203 Diesel Range Organics by GC/FID - Quality Control Level II QC Report 1/11/19 Prism Work Order: 9010043 Time Submitted: 1/4/2019 8:25:OOAM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9AO072 - 3546 Blank (P9A0072-BLK1) Prepared & Analyzed: 01/04/19 Diesel Range Organics BRL 7.0 mg/kg wet Surrogate: o-Terphenyl 0.932 mg/kg wet 1.333 70 31-123 LCS (PM0072-113SI) Prepared & Analyzed: 01/04/19 Diesel Range Organics 70.4 7.0 mg/kg wet 66.67 106 46-126 Surrogate: o-Terphenyl 1.14 mg/kg wet 1.333 86 31-123 LCS Dup (P9AO072-BSD1) Prepared & Analyzed: 01/04/19 Diesel Range Organics 65.5 7.0 mg/kg wet 66.67 98 46-126 7 20 Surrogate: o-Terphenyl 1.08 mg/kg wet 1.333 81 31-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 43 of 46 P R 1 S M Full -Service Analytical s Environmental Solutions LABORATOR, Hart & Hickman (Charlotte) Attn: Steve Libbey 2923 South Tryon St. Ste 100 Charlotte, NC 28203 General Chemistry Parameters - Quality Control Analyte Batch P9AO141 - NO PREP Project: Cindy Lane UST, Charlotte, NC Project No: CHP-035 Level II QC Report 1/11/19 Prism Work Order: 9010043 Time Submitted: 1/4/2019 8:25:OOAM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Duplicate (P9A0141-DUP1) Source: 9010043-02 Prepared & Analyzed: 01/08/19 % Solids 78.1 0.100 % by Weight 78.3 0.3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 44 of 46 Sample Extraction Data Prep Method: 3546 Lab Number Batch Initial Final Date/Time 9010043-01 P9A0072 30.05 g 1 mL 01/04/19 12:05 Prep Method: 3550C GC Lab Number Batch Initial Final Date/Time 9010043-02 P9A0103 10.24 g 2 mL 01/09/19 9:20 9010043-03 P9A0103 10.32 g 2 mL 01/09/19 9:20 9010043-04 P9A0103 10.26 g 2 mL 01/09/19 9:20 9010043-05 P9A0103 10.21 g 2 mL 01/09/19 9:20 9010043-06 P9A0103 10.6 g 2 mL 01/09/19 9:20 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 9010043-01 P9A0090 5.45 g 5 mL 01/07/19 14:57 Prep Method: 3550C MS Lab Number Batch Initial Final DatelTime 9010043-02 P9A0146 30.03 g 1 mL 01/10/19 13:20 9010043-03 P9A0146 30.26 g 1 mL 01/10/19 13:20 9010043-04 P9A0146 30.31 g 1 mL 01/10/19 13:20 9010043-05 P9A0146 30.38 g 1 mL 01/10/19 13:20 9010043-06 P9A0146 30.15 g 1 mL 01/10/19 13:20 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 9010043-02 P9A0133 3.68 g 5 mL 01/09/19 8:41 9010043-03 P9A0127 4.84 g 5 mL 01/08/19 8:53 9010043-04 P9A0127 4.56 g 5 mL 01/08/19 8:53 9010043-05 P9A0127 5.35 g 5 mL 01/08/19 8:53 9010043-06 P9A0127 5.28 g 5 mL 01/08/19 8:53 Prep Method: MADEP VPH (S) Lab Number Batch Initial Final Date/Time 9010043-02 P9A0082 17.14 g 16 mL 01/07/19 10:14 9010043-03 P9A0082 13.91 g 16 mL 01/07/19 10:14 9010043-04 P9A0082 15.5 g 16 mL 01/07/19 10:14 9010043-05 P9A0082 15.75 g 16 mL 01/07/19 10:14 9010043-06 P9A0082 15.8 g 16 mL 01/07/19 10:14 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 45 of 46 ,u 0) 3 c cn Cm m; F CL v c cn Uj � C O ? U) m0 �=r D7 � 30 0 �. y �a m N (Do � C M O. cn m m _» 3 CT a co m � � to m N w � o Z 0I 1 K 0 m m a y N � CD -I- D m A m m mn fG W y m m N N m S y ma rr M m CD N �. a 7 y Mcr ri. < m m O C pl 7 m ID N cp m Y R a o' N O 3 3 CD y ll� Cr VI v\ C� 113 NJ Q 1J\ O O a 3 v r m r. p mm 0Z �i •D O z 0 0 rp rD 0m I m m p 0 =30 c1m_i 3 Nm m p cA p�02? 10- x �. X p m A m M 0m . ,. z 0 a m xln 17•Ixlx xI,/,I-�,I4I-,4 X Tp,� Dr O Z e �Cr M a X l(n Q G Q O C� . z Cn S U, � cncnmm-0 m m O 3 0 X M 0 a s m 3 O 0 3 m m a0 a n .. .. m a c° o O T o� �. a0 m V � fa 3 IBC �' y 0— z 'm ° r m _ ur z y o n X A 3 �''o 8 0)0 N `L l x n f A � ni 4 ID ^i ¢ "0 Kd n A( N r ?m o m n N Q ^ N z 3 2 crt b N CD r. h V' t �► 9 c N to� w D 0) V in m O M � N S7o w M m <OD D �rn 33 ° n N fn D z m � ec ocean p m Vmi m 9 lfl g (D m d O M m<m m m pNui° O a m 0 0 <mcrm m u nm m m Z z D A 0 ❑ ❑ 3moo C m m 5 3 a O p W CD m c F w A cr N M O Z .c' ❑ m RCN O vi n O n m cD A ry cu ocminx a m ri m~ m 'c r rn i m o c F w 11 ryryLi � m m]?cCL 0 W n �v� v� y C, ;3 a aK Q � N N W W m Z D j m m O y sw 3 °r 1 -aM m _ n d 31 M A = C o r Sao a C 3 m G 0 AZ _ n C) I O0 m X o z ti p D m ch I 3 r z T 1' z 6) O Z m D m M Z n Co O ° z IC) r m r D a a ID N W T le I 0 � ° m m A . m m 2 O O 7 D o z �^ a) Da3 a x am) '� r s Z r� I nAO � F 0 n X� tam Z O i m f' m m H 3 ID z m w Q r y n m �■ m m O r m Z 9 C m o `° a m m z 0 Paae 46 of 46 1 Appendix B UST Removal Permit hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Charlotte Fire Department 500 Dalton Avenue Charlotte, NC 28206 HART HICKMAN 2923 S TRYON ST CHARLOTTE, NC 28203 OCCUPANT AND LOCATION FOR WHICH PERMIT IS VALID. PRIVATE RESIDENCE 2837 S—T-R'ti'0 ST C.14,1114 �Atut Charlotte NC #Error PERMIT FOR: 16 Tank Instal/Removal PERMIT CONDITIONS: 1. THIS PERMIT SHALL BE POSTED ON PREMISES FOR WHICH ISSUED. 2. ANY CHANGE IN THIS PERMIT SHALL REQUIRE PRIOR APPROVAL OF THE FIRE MARSHAL 3. - THE ISSUANCE OF A PERMIT OR APPROVAL OF PLANS SHALL NOT BE DEEMED OR CONSTRUED TO BE A PERMIT FOR AN APPROVAL OF ANY VIOLATION OF ANY OF THE PROVISIONS OF THE BUILDINGS AND FIRE CODES. 4. THE LOCATION CAN BE INSPECTED AT ANY TIME BY THE CHARLOTTE FIRE DEPARTMENT. VALID FROM: 01/02/2019 VALID THROUGH: 01/02/2019 PERMIT NUMBER: 2019-154973632 /ez� Jonathan Leonard, Deputy Fire Marshal Appendix C Certificate of Disposal and Non -Hazardous Waste Manifest — Residual Liquids hart hickman P. SMARTER ENVIRONMENTAL SOLUTIONS CORP0RATIQN 1703 Vargra� street Win -Sa , .7 :%on ...feMNC 2710 Ph 336-725-5844 fax 338-726-6244 Evo Corporation does hereby qertify that 16Q gallons of non -hazardous contaminated water received on' 1/2/ 019 from; Generator., The Housing Partnership Originating at; 2837 Cindy Lane Charlotte, NC EC Waste ID #: 011908 has been disposed of by Evo Corporation in a manner approved by the North Carolina Department of Enviroiimcntql Quality. i Signature Thomas W. Hammett CEO Evo corporation EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST -Load # Manifest No. 11247 GENERATOR INFORMATION 1 The Housing Partnership 7n4_RR'7- ini Generator: oPhone: Site Address: 2837 Cindy L City/State: Chax .at#e NC Contact: Steve Ta*ldwv Gross Weight (lbs): Empty Weight (lbs): Net Weight (lbs): MATERIAL DESCRIPTION / QUANTITY / WEIGHT Material: Water Contaminant: Heating Oil Quantity I j „(D Tons Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Cio Transporter: c�orratn ,Phone: _-'7- Truck #: Contact: Tinitir T)iiafii-x- As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and 1 hereby receive this material for delivery to the facility designate. Driver Signature: Date: - FACILITY INFORMATION Evo, Corporation 1'703- Va�rgrave Street Winston-Salem NC Evo Project #: (11 1[8 Phone: Contact: 1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment andArAsposal in gmapirrnthat has been authorized by the late Qf North Carolina. Facility Siqnature: Date: vvn€ieiraciury uanaryrinvoice Evo Corporation, 2U68 Appendix D Tank Disposal Certificate hart hickman SMARTER ENVIRONMENTAL SOLUTIONS Tank Owner: The Housing Partnership Site Address: 2837 Cindy Lane Charlotte, NC Description of Tanks: Tank Size of Tank Number 550 Gallons Transporter: Evo Corporation EC Project 4: 011908 Disposal Certification: Contents #2 Fuel Oil C 0 FZ P 0 RAt 10 N 1703 Hargrave. Street Winston-Salem, NC 27107 ph 336-725-5844 fax 336-7,25-62.44 Evo Corporation does hereby certify that the above named storagq lan.k',was, transported to Foss Recycling, 3459 Thomasville Road, Winston. SqIeni NC proper disposal and recycling, Signature Appendix E Certificate of Disposal, Non -Hazardous Waste Manifests, and Weight Tickets - Impacted Soil 14 hart hickman SMARTER ENVIRONMENTAL SOLUTIONS C'ORP0RA,TION 1703 Vargrave Street Winston-Salem, NO 27107 ph 33&725-5U4 fax 336-725-6244 CERTIFICATE OF DISPOSAL Evo Corporation does hereby certify that 23925 tons of non -hazardous contaminated material received on 1/2/2019 and 1/3/2019 from: Generator: The Housing Partnership Originating at: 2837 Cindy Lane Charlotte, NC EC Wash ID #; 011908 has been disposed of by Evo Corporation in a manner approved by the North Carolina Department of Environmental Quality. Fj Signature Thomas W. Hammett CEO Evo Corporation EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 11248 GENERATOR INFORMATION The. Houses .part n.ershipa '704 -887- i Generator: Phone: Site Address: 283TCau4t Ln City/State: Charlotte NC Contact: Steve Libl Gross Weight (Ibs): Empty Weight (Ibs): Net Weight (lbs): Quantity MATERIAL DESCRIPTION / QUANTITY / WEIGHT 3 3 A.,11-70 Material: soil". Contaminant: He.atina Oil Tons Drums Pails Sacs Yards Other: 1. TRANSPORTER INFORMATION Transporter: EVC Truck Phone: 336-725-5W Contact: Tmy Fisher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and 1 hereby receive this material for delivery to the facility designate. Driver Signature: �,12 4&Z Date: % 67 FACILITY INFORMATION Evo Project #: 011908 Evo Corporation 1703 Vargrave Street Phone: Wilton -Salem NC Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina, Facility Signature: Date: White/Facility Canary/Invoice Pink/Carrier Evo Corporation, 2008 EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 112 4 GENERATOR INFORMATION Generator: wPhone: Site Address: Z83TCiudy Ln . City/State: $Y Contact: Steve Lgbey MATERIAL DESCRIPTION / QUANTITY / WEIGHT Gross Weight (ibs): 7 7 606 Material:' Empty Weight (Ibs): 13 Contaminant: Net Weight (Ibs):J_E�o Quantity 1cf1 Tans Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: Evo.Corporation Phone: 336-725-5844 Truck #: _f� ��� Contact: Tonv Dicer As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: Date: FACILITY INFORMATION By Co ration! inn on -slalom NC Evo Project #: 0111068 Phone: Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facili re: U Date: 1 ` z ` r✓ Evo Corparation, 2008 ility nvo EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 112 5 0 GENERATOR INFORMATION Generator: The Homing Partnership Phone: 704--88 7- Site Address: 2837 Cindy Ln — City/State: Charlotte RC Contact: Steve. L ALbey_ Gross Weight (lbs): Empty Weight (lbs): Net Weight (lbs): Quantity MATERIAL DESCRIPTION I QUANTITY / WEIGHT 7c6 .330VO 3 V. (JL 0 l 7- 2 3 Material: soil Contaminant: Hpating CAR ons Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter:rotgt . Truck Phone: 336-725-58 Contact: Tony Dishell As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: ! lay_ Date: FACILITY INFORMATION 1Evo Corporation. 1-703 Vargrave Street Winston-Salem NC Evo Project #: 011908 Phone: Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facil re: Date: ! ` z I I White/Facility Canary/lnvo Eve Corporation, 2008 EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 11251 GENERATOR INFORMATION fi'Hc;a P' i Generator: Site Address City/State: +Charlotte_ e t 'a J. hone: Contact: Steve Lffibe� MATERIAL DESCRIPTION / QUANTITY / WEIGHT G Gross Weight (lbs): _ �W Empty Weight (Ibs): .3311Zo Net Weight (lbs): 39' 7(0 Material: SO , Contaminant: Quantity ons Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: Phone:: 3367 2.5 5 Truck #: 3 / Contact: lion.*.Maher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: Date: FACILITY INFORMATION Evo. Corporation. 1703 Vargrave Street Winston-Salem NC Evo Project #: 011 Offl Phone: . Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and�qr jisposal in aver that has been authorized by the State 9f North Carolina, Facilitv Sionature: Date: White/Facility. Can Evo Corporation, 2008 EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 11 252 GENERATOR INFORMATION The Houses Partnership 704-887- 06 Generator: Phone: Site Address: 2837 +Cindy Ln City/State: Chazlotte NC Contact: Steve Libber I MATERIAL DESCRIPTION / QUANTITY / WEIGHT Gross Weight (lbs): 6a�� Material: soil Empty Weight (lbs): 33080 Contaminant: Heating:Oil Net Weight (lbs): 9&200 Quantity (To Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: c� Co rat on Phone: 336-725-58 - Truck #: V.5 C,nntact- Timnv As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Si natur __?� Date: FACILITY INFORMATION 1F'V0 Corporation 1703 Vargrave Street Winston-Salem KC Evo Project #: 011908 Phone: Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/(# dj�posa[ i� Qthat has been authorized by tie State of North Carolina. Facilitv Signature: Date: White/Facility Evo Corporation, 2008 EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 11253 GENERATOR INFORMATION Th H P nel hi 704-887-4606 Generator: Phone: Site Address: ,3? iUdV Lam. Clhatt+� =�C City/State: , .; Contact: Steve Mbey MATERIAL DESCRIPTION /QUANTITY 1 WEIGHT Gross Weight (lbs): ie"'�4w Material: Empty Weight (lbs): Net Weight (lbs): sail . Contaminant:3,:% 36G9 Quantity f C, � P on > Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: EV0. ccwporat Phone: 336-725-59 . Truck #: Zf Z_ Contact: 7i`an-Y Didwr As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: f f Date: r FACILITY INFORMATION Bvo +Cv ►raltion :. 170 �Ttreet''- wingtoli- ftlem NBC" � � • -X it V11 4� Phone: Contact: i certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facilitv Sianature: V Date: 1 — 3 — ac Spa Corporation, 2008 er EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 11254 GENERATOR INFORMATION The Housing Partnership 704-887- i06 Generator: Phone: Site Address 837 Cindy La City/State: Chax otte NC. Contact: Steve L rev ' MATERIAL DESCRIPTION / QUANTITY / WEIGHT Gross Weight (lbs):.-�q-I o --- Material: soil Empty Weight (lbs): 3 5 0 90_ Contaminant: Head Oil Net Weight (Ibs): 37 3 j O Quantity l �. 6(� Ton Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: Evc Co p►r� _ . Phone: 336-725-5844 Truck #: oZ - .3! Contact: Tonv Dishier As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: Date: Z.3 f FACILITY INFORMATION Evo Corporation 1703 Vargrave Street Winston-Salem NC Phone: Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Sianature: Date: I -- q -. White/Facility Evo Corporation, 2008 Y O CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 11255 GENERATOR INFORMATION 704 Generator: Phone: Site Address: 2837 Cindy Ln City/State: Charlotte Ne Contact: Steve ffibey MATERIAL. DESCRIPTION / QUANTITY / WEIGHT j Gross Weight (lbs): �, 3k, Empty Weight (lbs): _ -� 2 rT` d Net Weight (lbs): Quantity I d'ZD9 Material` Contaminant: :.: eating.0it one Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: /Eyo corpolatgcn Truck #: Phone: 1 336-725-58 Contact: fiofly DiBher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: Date: FACILITY INFORMATION Evo Coyporati+tl►n 170.3 Vaxgrave Street inston--Salem. NC Evo Project #: 011 goo —A Phone: Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature:', U 'r Date: ( -- ility Canary/Invo Evo Corporation, 2008 EVO CORPORATION 1703 Vargrave Street, Wiis#on-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 112 5 GENERATOR INFORMATION The Houses Partrxership 7OC887-4606 Generator: Phone: Site Address: 2837 Cindy Ln City/State: Charlotte NC Contact: Steve L be MATERIAL DESCRIPTION / QUANTITY / WEIGHT Gross Weight (lbs): 60 Material: �'�'� Empty Weight (Ibs): 3,3 QcZ_ Contaminant: Heating 0:9 Net Weight {Ibs}: QuantityL1 ons Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: 1..V0 Catltioll Truck #: Phone: 336-725-58 Contact: Tony Disher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Sian Date: / FACILITY INFORMATION I Evo Project #: 011908 Evo Corporation 1703 Va�rgratve StreetPhone: Winston-Salem IBC Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina Facilitv Si re: Date: I ) Evo Corporation, 2008 er EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. . GENERATOR INFORMATION 257 Generator: Phone: Site Address:„+i�at L �C�ici+�tte. I.fhey City/State: �� ` Contact:Steve _ MATERIAL DESCRIPTION / QUANTITY / WEIGHT Gross Weight ([bs}: 7f ?U Material:``'II' . Empty Weight (lbs): 000 Contaminant; t on Net Weight (Ibs): f'eel d `Quantity .3 �fons)Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter: r+a `+a r� .. ., ... '>.. Phone: 336-725E-58 - Truck #: Contact: 7Conv Disher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: ,,�,;, Date: FACILITY INFORMATION i Evo Project #: 01190 vd., ?%r veStrt Phone: .. *tb Sal. We'.Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina Facilitv Signature: Date: � --3 --1 Lo Corporation, 2008 Pin EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. 11258 GENERATOR INFORMATION The H i Partnership Generator: Phone: .704-887-4-606 Site Address: 2837 Ciucly Lam: City/State: chwiotte xc Contact: Steve Libbe r MATERIAL DESCRIPTION / QUANTITY / WEIGHT Gross Weight (lbs): 7 13 `1U Material: Empty Weight (lbs): 2 I��O""o Net Weight (lbs): 411 G po Quantity Contaminant: Jgeating Oil To s Drums Pails Sacs Yards Other: TRANSPORTER lr.rr INFORMATION Transporter. " Vle'y►rg�tn Truck #: �r Phone: 336-725-5844 Contact: Tony D:asher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. Driver Signature: / i Date: FACILITY INFORMATION �z VZ Eva Project 11208 Evo corporation 1703 Va rgrave Street Phone: Winston -Sale. NC Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facility Signature: Date: I _ q — ,�; VITIF Evo Corporation, 2008 EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST Load # Manifest No. GENERATOR INFORMATION 704 Generator: Phone: Site Address: City/State: 1mir�t+'�C . ,Contact:1tr MATERIAL DESCRIPTION / QUANTITY / WEIGHT Gross Weight (lbs): �? Empty Weight (lbs): � Net Weight (lbs): ?' T40 Quantity Material:` Contaminant: Hea;OU X01s Drums Pails Sacs Yards Other: TRANSPORTER INFORMATION Transporter:JP0.5844 ..Phone. Truck #: Contact: Tanv T)itahP7r As the transporter, I certify that the materials described above .being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. , Driver Signature: Date: % FACILITY INFORMATION By Co m m: : 1?U3 V 8 reet Whitk6l.-Saleni e ProjectEvo Ong Phone: Contact: I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Facilitv Signature: r Date: Ti Eva Corporation, 2008 ity 0 47219971 TICKET NUMBER As Il CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. 13OX 630 WALCOT , IA 52773 (563)2154-6263 www.catscale.com IHE_!AT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies is that we back up our guarantee with cash.* WEIGH WHAT WE SAY OR WE PAY® ~ If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will Immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine if our scale Is wrong, OR (2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness If we believe our scale was correct. IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext. 7 (Tali Free) or visit www.catscWeguarantse.com for Instructions. 3) IMMEDIATELY send a copy of the cltation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department. * The four weights shown below are separate weights. The GROSS WEIGHT Is the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. DATE: 1-0 2 --19 11:59 47219971 SCALE: LOCATION: PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT& MEASURE NORTH CAROLINA WEIGH NUMBER 9v'7-1 STOMER COPY 1709 LOVES I 85 EXIT 71 SALISBURY NC STEER AXLE 9 9 6 O 1 b DRIVEAXLE �- 7 eS C�o 1 b TRAILER AXLE 2786C> 1 b GROSS WEIGHT 5 eS 5 8 0 1 b This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law. LOVE'S TRAVEL. STOP #507 1105 PEELER RD., SUITE 100 LIVESTOCK, PRodt'&C L, MW Y, 13",1j nCLE WEIGHeQ FREIGHT ALL KINDS COMPANY EVO TRACTOR # Zip 33i TRAILER # WEIGHMASTER OR TICKET # OF FEE $11 . 50 WEIGHER SIGNATURE �^- FULL $ WEIGH /171 ALLAN (IF REWEtGH) O CAT scalar qeg' 317 47219988 TICKET NUMBER SCALE CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOTT, IA 52773 (563)284-6263 www.ratsrale.com THE CAT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies Is that we back up our guarantee with cash o WEIGH WHAT WE SAY OR WE PAYO If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine If our scale is wrong, OR (2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness if we believe our scale was correct. IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-677-CATSCALE, ext 7 (Toll Free) or visit www.catscaleguarantse.com for Instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Atin: Guarantee Department, *The four weights shown below are separate weights. The GROSS WEIGHT Is the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. DATE: 1-02--19 15:58 47219988 SCALE: LOCATION: PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT & MEASURE IMPRINT SEAL HERE (IFAPPLICABLE) WEIGH NUMBER 9971 1709 LOVES 185 EXIT 71 SALISBURY NC STEER AXLE DRIVEAXLE TRAILER AXLE * GROSS WEIGHT Ci'9b0 1 b 292:;R0 1 b 337Ead 1 b '72c?.4KD 1 to This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as.,R �3�aw. ... e s ,-J6L10 WEIGHMASTER LICENSE QTIRES JUNE 30, 2010 KEVIN GARNEY 3W LIVESTOCK, PRODUCE, PFtOPE�,$��t$iVEtGHED FREIGHT ALL KINDS EV O 215 331 NY COMPATRACTOR TRAILER k WEIGHMASTER OR FEE WEIGHER SIGNATURE FRILL $111+#EIG 47219971 Z • �� IFREWEIGHJ ALXCCOY i STONIER COPY 0CAT Scalaeaeg306311117 47220023 TICKET NUMBER ®e II CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOTT IA 52773 (563) 284.6263 www.catscafe.com THE CAT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies Is that we back up our guarantee with cash WEIGH WHAT WE SAY OR WE PAYS ' If you get an overweight fine from the state A-= one of our CAT Scales showed a legal weight, we will immediately check our scale and we will: (1) Reimburse you for the cost of the overwelght fine if our scale is wrong, OR (2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness If we believe our scale was correcL IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Past bond and request a court date. 2) Cali CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, ext. 7 (Toll Free) or visit www.caLsaaguarantee.com for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department. *The four weights shown below are separate weights. The GROSS WEIGHT Is the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. DATE: 1-03-19 12:32 SCALE: 47220023 LOCATION: PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT & MEASURE NORTH CAROIjNA V1 1709 LOVES I 85 EXIT 71 SALISBURY NC DRIVE AXLE 3 1- 7 E3 Ca 1 b TRAII ER AXLE 3 7 6 0 0 1 b GROSS WEIGHT 7 9 9 8 O l b This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy welghmaster, and when properly signed and sealed shalt be prime facia evidence of the accuracy of the weight shown as prescribed by law. 11V � Q LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, ORAFMCI E WEIGHED FREIGHT ALL KINDS COMPANY EVO TRACTOR # 215 331 TRAILER # ^IGH NUMBER WEIGHMASiEROR TO(ETSOF `:;2 _-S FEE $11.50 WEIGHER SIGNATURE FULL $ WEIGH ONN LY (IFREWEIGH) 0 CAT scale* Reg 3U63 11117 �47220033 TICKET NUMBER CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOiT IA 52773 563)284-6263 Www.catscale.com S THE CAT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies is that we back up our guarantee with cash c WEIGH WHAT WE SAY OR WE PAY® If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will Immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine If our scale Is wrong, OR (2) A representative of CAT Scale Company will appear In court WITH the driver as an expert witness If we believe our scale was correct. IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext 7 (Tall Free) or visit www.catscaleguarantee.com for Instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department The four weights shown below are separate weights. The GROSS WEIGHT Is the CERTIFIED WEIGHT" and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. DATE: 1-03-19 15:33 SCALE: 1709 47220033 LOCATION: LOVES PUBLIC WEIGHMASTER'S CERTIFICATE OF I B 5 EXIT 71 WEIGHT & MEASURE SAL I SBURY NC ! J t C. R�: tFdA WEIGH NUMBER ao23 STOMER COPY STEER AXLE l 4 C7 8 O l b DRIVE AXLE 3 3 2 O UU l b TRAILER AXLE 3 -q- 0 8 0 l b GROSS WEIGHT '% 7 3 & C7 1 b This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law. PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED FREIGHT "ALL KINDS COMPANY EV D TRACTOR # 215 TRAILER # 331 WEIGHMASTER OR 4EH TICKET It OF7220023 FEE $2.00 WEIGHER SIGNATURE FULL$WEIGH � MCCOY (IFREWEIGH) CAT SMISO Reg W6311117 47219975 TICKET NUMBER PAT. SCALE CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOTT IA 52773 (563)284-6263 �(www.catscale.com THE CAT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies Is that we back up our guarantee with cash C WEIGH WHAT WE SAY OR WE PAYO If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will Immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine if our scale is wrung, OR (2) A representative of CAT Scale Company will appear In court WITH the driver as an expert witness if we believe our scale was correct. IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, ext. 7 (Toll Free) or visit www.r-atscaleguarantee.com for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn. Guarantee Department. •The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIC3HT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale, tv_ DATE: 1-02-19 13:17 SCALE: 47219975 LOCATION: PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT & MEASURE NORTH u%ROLINA PUBLIC YEIGHK*TEF -- . -No Jt1NE 30, L HERE PLIC (I APABLE) WEIGH NUMBER c .77 9 7 5 1709 LOVES I B5 EXIT 71 SALISBURY NC STEER AXLE 1. a CD 4 © 1 b DRIVE AXLE a 2 3�22 O 1 b TRAILER AXLE 2 5 1 E3 O 1 b GROSS WEIGHT &? 5 4 Co 1 b This Is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy weighmaster, and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescrfbed by law. i /I'M5 -317 UVESTOCit, PRODUCE, PROPERTY. COMMODITY, OR ARTICLE WEIGHED FREIGHT ALL KINDS COMPANY EVO TRp,OOR # 216 317 ,rRAJtER # WEIGHMASTER OR �-� TICKED' # OF FEE 1 . 50 WEIGHER SIGNATURE FULL$ WEIGH 001, PENNY W I LSON (IF REWEIGH) STOMER COPY 0GAT Scale+Reg 306311/17 54843388 TICKET NUMBER ►. J® Il CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOTT IA 52773 (563)264-6263 www.catscale.com THE CAT S9ALE QUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies is that we back up our guarantee with cash.0 WEIGH WHAT WE SAY OR WE PAY® If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will immediately check our scale and we will: ' (1) Reimburse you for the cost of the overweight fine If our scale Is wrong, OR (2) A representative of CAT Scale Company will appear in court Wthe driver as an expert witness iii-1, If we believe our scale was correct. iF YOU SHOULD GET AN OVERWEIGHT FiNE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1.877-CATSCALE, ext. 7 (Toil Free) or visit www.catscaleguarantee.com for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department. DATE: 1? : 12 SCALE: li4843388 LOCATION: PUBLIC WEIGHMASTER'S CERTiFICATE OF WEIGHT & MEASURE WEICI-i NUMBER �3-3'!�N4S STOMER COPY 'The four weights shown below are separate weights. The GROSS WEIGHTIs the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. STEER AXLE vC51 a 4D �_ C DRIVE AXLE :�-p C, e-Z!, .La} (D � �-: 6`�5 TRAILER AXLE �D 7 t+ (7) -0 A- f:) PILOT TRAVEL OENTEFP T 85 EXIT 71 . GROSS WEIGHT S iLISPURY Nr. This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy welghmaster, and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law. alb ol1yoF �c COMPANY Elfin FEE $ i 1 cr1 PROPERTY. COMMODITY, OR ARTICLE WEIGHED WEIGHMASTER OR WEIGHER SIGNATU # pt -•'"TRAILER# R� TICKET # OF FULL $ WEIGH (!F REWEFGH} O CAT Scales Reg 3067 7/t8 54843408 TICKET NUMBER As n CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY PO. BOX 630 WALCOTT, IA 52773 (563) 284-6263 www,caL%cale.com THE CAT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companles is that we back up our guarantee with cash c WEIGH WHAT WE SAY OR WE PAY® If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will immediately check our scale and we will: (1) Reimburse you for the cost of the overweight flne if our scale Is wrong, OR (2) A representative of CAT Scale Company will appear In court WITH the driver as an expert witness if we believe our scale was correct: IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GETTHE PROBLEM RESOLVED. 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, eat. 7 (Toll Free) or visit www.catscaleguarantee.com for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department. DATE: 16 - 3. SCALE: LOCATION: PlktrbiVASA CASTER'S CERTIFICATE OF WEIGHT& MEASURE i The four weights shown below are separate weights. The GROSS WEIGHT Is the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. STEER AXLE DRIVE AXLE 61? 5 TRAILER AXLE PILOT TRAVEL CENTf" PS T 8 5 E X I T .-7t ' GROSS WEIGHT S 7XkZ3'okd k I fr—. is"f o c rtify 1C the following described merchandise was weighed, counted, or measured by a public or deputy welghmaster, and when properly signed and sealed she[[ be prima facia evidence of the accuracy of the weight shown as prescribed by law. 0� IS/ 0/ li�oe JVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED COMPANY TRACTOR # _TRAILER # r- r 1 -` _ WEIGHMASTER OR MWFULL TICKET # OF f`41[EIGH UMBER FEE WEIGHER SIGNATURE $WEIGH t r' OF REWEIGH) 3TOMER COPY f-: M`,'' _ PAR -f; f.1O 0CAT Scale#Reg 30677tie 18434?7 .CKET NUMBER AID A ERTIFIED UTOMATED RUCK CALE T SCAM COMPANY ). BOX 630 \LCOTT, IA 52T73 33) 284-6263 vw.catscale.com The CAT Scala Company guarantees that our scales will give an accurate weigh. What makes . e us different from other scale companies is that we back up our guarantee with cash WEIGH WHAT WE SAY OR WE PAY® * , et an overweight line from the state AFTO. one of our CAT Scales showed a legal weight, we will 1f you g Immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine 11 our scale is wrong, OR a (2) A representative of CAT Scale Company will appear in court WITH the driver as an expert witness it we believe our scale was correct. IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. a day at i-gTl-CAText. 7 (Toll Free) or visit www.catscaleguarantee.com 2} Calf CAT Scale Company direct 24 hours for instructions. our name, company, address, and phone number to 3} IMMEDIATELY s copy of the citation, CAT Department ale Tcket, y CAT Scale Company GHT s the * The d four was weighed sshown below E a full length ptatfire onntscafe�Ail weights are guarani eedi by CAT Scale. WEIGHT an DATE: 410 r ' ' SCALE: .L+P-4'2437 LOCATION: PUBLIC WEIGHMASTER`S CERTIFICATE OF ,pgQtANkASURE �XPiKE JUig �,q2 81 �STILLQ t l�y� sec �l�i1Fr� IMPRIAlT SEAL HERE (IF A LE) 4,E?.'--tH NfjhJBER TOMER COPY STEER AXLE DRIVE AXLE x-E 61, ear C� t=` q ` TRAILER AXLE PILOT mF;r' VET CENTE PS sx F d T T ? ? " GROSS WEIGHT t3 .! '? tD tD rpu'billic s is rodeeuthat the wefghmaster�and hendescribed p openly signed land seateda war. ishalidbe prima facia evidecounted, or nce of the p Y ",cv of the weight shown as prescribed by law. C�1r 011 � 06' Tr;NT ALL CK, UVESTOPRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED it a,r s vI-y OR �` LER ` COMPANY nL ET OF WEIGHMASTER OR LL 1 E WEIGHER SIGNATURE Y � # r (IF REVVEIGI4 `�-- .2 Clf c L��T� c"'.- i'T _ L O CAT Scales Reg 3067 7/18 54843461 TICKET NUMBER hk Ae 11 CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOTT,, IA 52773 (563)284-6263 www,catscale.com THE CAT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies Is that we back up our guarantee with cash o WEIGH WHAT WE SAY OR WE PAYS If you gat an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine If our scale Is wrong, OR (2) A representative of CAT Scale Company wll appear In court WITH the driver as an expert witness if we believe our scale was correct. IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department. The four weights shown below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. DATE: -p:S- 13 - S c" SCALE: 484.3461 LOCATION: PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT & MEASURE NORTH CAROLINA, PUBLIC WEIGHMASTER 'C�i�WMS UOF& 30, 2 It YLIVA LI.R, ") 42 2P nl in i 7R cor+ WEIGH NUMBER 6 4 S PILOT TRAVEL CENTE:PIC r 81S EXIT 771 SALISDURY NC STEER AXLE DRIVEAXLE TRAILER AXLE '2—, 3. =-'3 L- AD --L ' GROSS WEIGHT '7 C"a L,_ 1- 4L, 1 This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy walghmaster, and when properly signed and sealed shall be prima facla evidence of the accuracy of the weight shown as prescribed by law. ate bii�o� LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE COMPANY EVO WEIGHMASTER OR FEE WEIGHER SIGNATURE I . SO rr }f �' TRAILER # -- TICKET # OF FULL$ WEIGH (IF REWEIGH) STOMER COPY " %---- 0 CAT SCOA F4g 3W 7/18 54843436 TICKET NUMBER 'AaD F1 CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCO17 IA 52773 (563)284-6263 www.r-atscale.com THE CATNALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies is that we back up our guarantee with cash c WEIGH WHAT WE SAY OR WE PAYe If you get an overweight fine from the state AEjgR one of our CAT Scales showed a legal welghL we will Immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine If our scale Is wrong, OR (2) A representative of CAT Scale Company will appear In court WITH the driver as an expert witness if we believe our scale was correct. IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department. *The four weights shown below are separate weights. The GROSS WE102HTIs the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. DATE: 10 C 11. SCALE: =4843436 LOCATION: PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT & MEASURE NOMCMOLWA IBLIC WFIGHMR33ER 8g WETI_-'H NUMDEP L+ 13 -631 STOMER COPY 69S PILM- TRAVEL CENTERS SALISEP IPY N STEER AXLE ,� 7 .tif `x :1 L-- DRIVE AXLE TRAILER AXLE �a ' -1-3 -�• OD 1 L-- ' GROSS WFJGHT 7 Jl_ `3 L-�- rD -L U, This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy welghmaster, and when properly signed and sealed shall be prima facla evidence of the accuracy of the weight shown as prescribed by law. UVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE WEIGHED COMPANY WEIGHMASTER OR FEE 11 WEIGHER SIGNATU TRAILER# �c TICKET# OF FULL $ WE O CAT Scstee Reg 3067 71113 54843454 TICKET NUMBER (` 'A0 Fl CERTIFIED AUTOMATED TRUCK SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOTT, IA 52773 (563) 284-6263 www.catscale.com THE CAT SCALE GUARANTEE The CAT Scale Company guarantees that our scales will give an accurate weight. What makes us different from other scale companies Is that we back up our guarantee with cash c WEIGH WHAT WE SAY OR WE PAY0 14 If you get an overweight fine from the state AFTER one of our CAT Scales showed a legal weight, we will Immediately check our scale and we will: (1) Reimburse you for the cost of the overweight fine if our scale Is wrong, OR (2) A representative of CAT Scale Company will appear In court W1TH the driver as an expert witness If we believe our scale was correct. IF YOU SHOULD GETAN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CAT-SCALE, ext. 7 (Toll Free) or visit www.catscaleguarantee.com for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your name, company, address, and phone number to CAT Scale Company Attn: Guarantee Department. *The four weights shovm below are separate weights. The GROSS WEIGHT is the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights are guaranteed by CAT Scale. DATE: f 3 " 2 SCALE: 54843454 LOCATION. - PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT & MEASURE SUC V�e tAA u�� A G�STIL1 .. _ IMPRINT SEAL WEZ 13H NUMBER _i� L-4-:23 4!!�� PILOT TRAVEL, CENTERS I. 8S EXIT 71 SAL 1SPIJRY NF' STEER AXLE DRIVEAXLE a't C' a �' C't Cr _L t: _ TRAILER AXLE ' GROSS WEIGHT 'L� . IN L-q. -�2 13 y. t2, This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy welghmaster, and when properly signed and seated shall be prime facla evidence of the accuracy of the weight shown as prescribed by law. 5�1_ orb Sop .,�// LIVESTOCK, PRODUCE, PROPERTY, COMMODITY, OR ARTICLE EVO WEIGHMASTER OR FIE WEIGHER SIGNATURE Syi_k.1T�i Rf~ICI-IT ALL t='INDS )� TAAlLERB Sao TICKETNOF FULL $ WEIGH t i + (IF REWEIGH) STOMER COPY 0cnTscaW6ReQ30677r1e ON THE CAT SCALE C UA13A 54845 � The CAT scale Corr, ny guaraantees th"ur scaws+ wlll glvdsi a welght.What makes TICKET NUMBER us different from other scale companies is that we back up our guarantee with cash. WEIGH WHAT WE SA, R WE PAY® If you get an overweight fine from the state A E one of o r AT Scales showed a legal weight, we will • . immediately check our scale and we will: (1) Reimburse you forthe cost of the overweight fine if our scale Is wrong, OR 1 (2) A representative of CAT Scale Company will appear In court WITH the driver as an expert witness If we believe our scale was correct. I CERTIFIED IF YOU SHOULD GET AN OVERWEIGHT FINE, YOU SHOULD DO THE FOLLOWING TO GET THE PROBLEM RESOLVED: 1) Post bond and request a court date. 2) Call CAT Scale Company direct 24 hours a day at 1-877-CATSCAI E, ext.7-(Toll Free) or visit www.catsraleduarantsaicom AUTOMATED for instructions. 3) IMMEDIATELY send a copy of the citation, CAT Scale Ticket, your {lame, company, address, and phone number to TRUCK CAT Scale Company Attn: Guarantee Department..P. SCALE CAT SCALE COMPANY P.O. BOX 630 WALCOTT lA 52773 (563) 294-6263 www.catscale.com DATE: MEN SCALE: a LOCATION: PUBUCWEIGHMASTER`S CERTIFICATE OF WEIGHT& MEASURE "The four weights shown below are separate weights. he GROSS WEIGHT Is the CERTIFIED WEIGHT and was weighed on a full length platform scale. All weights -are guaranteed by CAT Scale. STEER AXLE DRIVE AXLE TRAILER AXLE ` GROSS WEIGHT This Is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy Welghmaster, and when properly signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed bylaw. P Cal LIVESTOCK, PRODUCE, PROPERTY, COMMODr7Y, OR ARTICLE WEIGH r C TRAILER # WEIGHMASTER OR TICKET# OF FEE WEIGHER SIGNATURE FULL$ WEIGH _ (€F REWEIGH) JSTOMER COPY OCAT SMWOReg 30877118