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HomeMy WebLinkAboutMO-7444_36096_CA_RMR_20190108I` APEX January 8, 2019 Ms. Trudy Beverly Division of Waste Management Mooresville Regional Office Department of Environmental Quality 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 RE: Corrective Action Performance Report (July 1, 2018 to December 31, 2018) Pilot Travel Center #56 2825 Lane Street, Kannapolis, North Carolina Groundwater Incident Number: 36096 Risk Classification: High Dear Mr. Morris: Enclosed please find one copy of the Corrective Action Performance Report prepared by Apex Companies, LLC on behalf of Pilot Flying J for the referenced site. Should you have any questions regarding the enclosed, or if additional information is required, please feel free to contact me at (540) 563-4920. Best Regards, Robert S. Wagner Program Manager Enclosure Cc: Mr. Joey Cupp, Pilot Fling J Apex Companies, LLC • 7724 Garland Circle • Roanoke, VA 24019 T 540.563.4920 • F 540.563.4921 • apexcos.com I` APEX CORRECTIVE ACTION PERFORMANCE REPORT (July 1, 2018 to December 31, 2018) Pilot Station #56 2825 Lane Street Kannapolis, North Carolina Groundwater Incident Number: 36096 Risk Classification: High Facility ID 0-011084 Submitted To: Ms. Trudy Beverly Division of Waste Management 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 Prepared For: Mr. Joey Cupp Pilot Fling J 5508 Lonas Road Knoxville, Tennessee 37939 Prepared BY: Apex Companies, LLC 7724 Garland Circle Roanoke, Virginia 24019 January 8, 2019 Apex Project No.: 768490.030 Prepared By: Reviewed By: O�r- RO SEAL - � 1735 o OLOGN���,`�o' ` CKL EY Reviewed By: Kyle Hicks Robert S. Wagner Robert S. Williamson Environmental Scientist II Program Manager North Carolina Licensed Geologist #1735 Apex Companies, LLC • 7724 Garland Circle • Roanoke, VA 24019 T 540.563.4920 • F 540.563.4921 • apexcos.com A. SITE INFORMATION 1. Site Identification • Date of Report: January 8, 2019 • Facility Identification Number: 0-011084 • Site Name: Pilot Station #56 (site) • Site Street Address: 2825 Lane Street, Kannapolis, North Carolina. • Geographical Data Point: Store Building Google Earth Pro • Latitude 350 29' 53.20" N and Longitude -800 33' 39.54"W A site location map is included as Figure 1 to this report. 2. Information about Contacts Associated with the Underground Storage Tank (UST) System • UST Owner: Pilot Travel Centers, LLC 5508 Lonas Drive Knoxville, TN 37909 Phone: 865-588-7488 • UST Operator: Pilot Travel Centers, LLC 5508 Lonas Drive Knoxville, TN 37909 Phone: 865-588-7488 • Property Owner: Pilot Travel Centers, LLC 5508 Lonas Drive Knoxville, TN 37909 • Property Occupant: Pilot Travel Centers, LLC 2825 Lane Street Kannapolis, North Carolina • Consultant/Contractor: Apex Companies, LLC 7724 Garland Circle Roanoke, Virginia 24019 Phone: 540-563-4920 Facsimile: 540-563-4921 • Analytical Laboratory: ESC Lab Sciences 12065 Lebanon Road Mount Juliet, TN 37122 Phone: 800-767-5859 3. Information about Release • Date Discovered: June 13, 2006 • Estimated Quantity of Release: Unknown • Cause of Release: Unknown • Source of Release: Unknown • Size and Contents of UST System(s) from which release occurred: Unknown CA Performance Report (July 1 to Dec. 31, 2018) i January 8, 2019 Pilot # 56 Incident#36096 EXECUTIVE SUMMARY On behalf of Pilot Flying J (Pilot), Apex Companies, LLC (Apex) has completed system operation and maintenance (O&M) and groundwater monitoring activities associated with the soil and groundwater remediation system located at the Pilot Travel Center #56, a retail gasoline station. In accordance with North Carolina Department of Environmental Quality (NC DEQ) regulatory reporting requirements, Apex has prepared a Corrective Action Performance Report for the subject property located at 2825 Lane Street in Kannapolis, North Carolina. This report includes routine system O&M, system repairs, system monitoring, and semi-annual groundwater sampling for the period beginning July 1, 2018 and ending December 31, 2018. The site has been a working supplier of gasoline, diesel, and kerosene since at least 1984 and probably much earlier. From 1966 to 1972 the site was owned by the Humble Oil Company. In 1972 the property owner became Exxon Corporation via a name change. Aerial photographs obtained from Cabarrus County GIS department suggest that the site was a gas station by 1975. It operated as a Starvin Marvin from 1984 and then Speedway America until October 26, 2001, when Pilot Travel Centers, LLC purchased the property. The objective of the Corrective Action Plan (CAP) prepared by Apex, was to maintain groundwater quality conditions at the site below the applicable 2L Standards for benzene and meth tertbutyl ether (MTBE) while aggressively remediating source area groundwater and minor soil contamination. The corrective action approach to achieve the aforementioned goals for groundwater at the site consisted of an engineered air sparging and soil vapor extraction (SVE) system coupled with monitored natural attenuation. Air sparging will be effective to remove the volatile hydrocarbon constituents, including MTBE from the groundwater. SVE will capture volatile organic vapors from the subsurface and provide an increased pressure gradient to enhance the efficacy of the air sparging. The end of active remediation will be determined when asymptotic conditions are reached in dissolved hydrocarbon concentrations in groundwater or when the applicable 2L standards have been achieved, or risk can be reduced. CAP implementation at the site began in April 2012. Prior to CAP implementation seven monitoring wells (MW-11, MW-12, MW-19, MW-21, MW-23, MW-24, and DMW-3) were above the benzene 2L limit of 1.0 micrograms per liter (µg/L). The MTBE 2L limit of 20 µg/L was exceeded in eight monitoring wells (MW-11, MW-14, MW-17, MW-19, MW-21, MW-23, MW-24, and DMW-3) prior to CAP implementation. At the conclusion of 4' Quarter 2018 CAP implementation no monitoring wells exceeded the benzene 2L CAP endpoint and MW-14, MW-17, and DMW-3 exceeded the MTBE 2L CAP endpoint. Petroleum compounds have never been detected in any of the area potable water supplies and sentinel wells such as MW-21, MW-22, and MW-25 continue to indicate that the gasoline plume is confined to the original source zone identified and described in both the CSA and approved CAP. Based on the continued presence of MTBE above 2L groundwater quality standards in several monitoring wells, Apex recommends continued operation of the remediation system in accordance with the approved CAP. CA Performance Report (July 1 to Dec. 31, 2018) ii January 8, 2019 Pilot # 56 Incident#36096 TABLE OF CONTENTS 1.0 INTRODUCTION....................................................................................................................... 1 2.0 SITE HISTROY AND BACKGROUND..................................................................................... 1 3.0 REMEDIATION SYSTEM........................................................................................................... 3 4.0 GROUNDWATER MONITORING............................................................................................ 4 5.0 OPERATION AND MAINTENANCE........................................................................................ 5 6.0 CORRECTIVE ACTION PERFORMANCE REPORT SUMMARY .................................... 5 7.0 STATEMENTS AND CERTIFICATION................................................................................... 6 List of Figures Figure 1. Site Location Map Figure 2. Site Plan Figure 3. SVE System Layout Figure 4. Air Sparge System Layout Figure 5. MTBE Isoconcentration Map List of Tables Table 1. Groundwater Elevation Data Table 2. Summary of Groundwater Analytical Data Table 3. Operation and Maintenance Activities List of Appendices Appendix A Groundwater Laboratory Certificate of Analysis and Chain of Custody Appendix B Historical Groundwater Analytical Results Appendix C O&M Checklists CA Performance Report (July 1 to Dec. 31, 2018) iii January 8, 2019 Pilot # 56 Incident#36096 1.0 INTRODUCTION On behalf of Pilot Flying J (Pilot), Apex Companies, LLC (Apex) has completed system operation and maintenance (O&M) and groundwater monitoring activities associated with the soil and groundwater remediation system located at the Pilot Travel Center #56, a retail gasoline station. In accordance with North Carolina Department of Environmental Quality (NC DEQ) regulatory reporting requirements, Apex has prepared a Corrective Action Performance Report for the subject property located at 2825 Lane Street in Kannapolis, North Carolina (Figure 1). This report includes routine system O&M, system repairs, system monitoring, and semi-annual groundwater sampling for the period beginning July 1, 2018 and ending December 31, 2018. The remediation system was installed by Apex in accordance with the NC DEQ-approved Corrective Action Plan (CAP) to address the multiple -phase contaminants identified on the subject property. A description of the remediation system design and function is presented in Section 2.0. A site plan depicting pertinent features of the subject site and surrounding area is provided as Figure 2. This report for system O&M at the Pilot #56 facility is being submitted to Mr. Brett Morris of NC DEQ, on behalf of Pilot. 2.0 SITE HISTORY AND BACKGROUND The site has been a working supplier of gasoline, diesel, and kerosene since at least 1984 and probably much earlier. From 1966 to 1972 the site was owned by the Humble Oil Company. In 1972 the property owner became Exxon Corporation via a name change. Aerial photographs obtained from Cabarrus County GIS department suggest that the site was a gas station by 1975. It operated as a Starvin Marvin from 1984 and then Speedway America until October 26, 2001, when Pilot Travel Centers, LLC purchased the property. According to records reviewed by Apex, seven underground storage tanks (USTs) were closed by removal in May 1994. The UST Closure Report also documented that two 12,000- gallon USTs were removed from service in 1991. The report also documented that there were releases associated with both product lines and the southern UST tank basin. The release was assigned incident number 6379 by the North Carolina Department of Environment and Natural Resources (NCDENR). The site was redeveloped and subjected to active remediation. Following 18 months of active remediation, the incident was closed by NCDENR in 1998. In April 2006, a contractor mobilized to the site to gauge monitoring wells prior to abandonment on behalf of the responsible party for incident 6379. The contractor reportedly discovered light non -aqueous phase liquid (LNAPL) in RW-8 and MW-9. Follow-up investigation in the tank areas and product lines failed to determine a new source. NCDENR considered the LNAPL to be a new release and assigned incident number 36096. Several phases of assessment have occurred since 2006. A site check on the south side of the facility was performed which focused on soils around the new UST basin and the dispenser lines. A total of 22 soil samples were collected for total petroleum hydrocarbons (TPH) gasoline -range organics (GRO) analysis. Nine of the 22 soil samples were analyzed for TPH diesel -range organics (DRO) as well. Four soil samples were reported with GRO concentrations CA Performance Report (July 1 to Dec. 31, 2018) 1 January 8, 2019 Pilot #56 Incident#36096 above the NCDENR UST action level of 10 milligrams per kilogram (mg/kg) at the time of the investigation. DRO were detected in five of the soil samples above 10 mg/kg. A Phase II Limited Site Assessment was conducted and submitted, and the site was assigned a "High Risk" ranking by NCDENR. On February 20, 2009, NCDENR issued a Notice of Regulatory Requirements requesting a Comprehensive Site Assessment (CSA) for the site. A CSA was prepared for the site in December 2009 that delineated the dissolved -phase groundwater contamination vertically and horizontally. An additional round of sampling conducted in September 2010 confirmed the previous delineation. The dissolved -phase hydrocarbon plume did not extend beyond the site property line and the detected groundwater analytes did not exceed the gross contaminant levels (GCLs). The site is ranked `high risk' due to the presence of water supply wells located within a 1,000-foot radius of the source area. It is important to note that all the identified supply wells are located hydraulically cross -gradient of the site and over 425 ft from any exceedances of the North Carolina 15A NCAC 2L groundwater standards (2L). Repeated sampling and analysis of the water supply wells have never detected petroleum hydrocarbons in the samples collected. Furthermore, there are three shallow sentinel wells (MW-22, MW-26, and MW-27) between the source area and the water supply wells that currently and/or historically have met 2L standards. Silty sands dominate the lithology at the site. Shallow soil on site is disturbed and very heavily compacted. Bedrock was encountered at approximately 45 ft below land surface (bls) at DMW-2. Shallow groundwater is encountered at approximately 22 ft bls in the developed portion of the site and flows to the north-northwest. The contaminant of concern is unleaded gasoline. The two primary analytes of concern are meth tertbutyl ether (MTBE) and benzene. Historically there were other exceedances of the 2L standard, but there were no 2L exceedances in wells without having either benzene or MTBE present above 2L standards. The source area was presumed as south of the building, near MW- 24. At the time of CAP development the assumed dissolved groundwater contaminant plume in the south area was approximately 150 ft long by 60 ft wide and 30 ft deep (20 to 50 ft bls). Mass balance calculations indicated that the MTBE mass in the aquifer was approximately thirty gallons and the benzene mass was approximately one gallon. Based on the risk ranking for the site, corrective action objectives (CAOs) listed below were established for each site media by NCDENR. The status of the site in achieving the established CAOs are also noted. According to the North Carolina Administrative Code, (NCAC) 15A 2L .0407 soil must be cleaned up to MSCCs for soil to groundwater or residential standards, whichever is lower. The CAOs for residential soil were achieved prior to CAP implementation. The remediation design in the CAP addressed the nominal soil contamination in the southern area subsurface that remained above soil -to -groundwater standards. According to NCAC 15A 2L .0202, surface water must be remediated to NCAC, 15A 2B standards (213). The 2B standard for benzene was 70 µg/L. The CAOs for surface water at the site were achieved prior to CAP implementation and remedial measures were not carried forward in the CAP. According to NCAC 15A 2L .0202, groundwater at the site must be remediated to the applicable 2L Standards which are 1.0 µg/L and 20 µg/L for benzene and MTBE, respectively. CA Performance Report (July 1 to Dec. 31, 2018) 2 January 8, 2019 Pilot #56 Incident#36096 The objective of the CAP was to maintain groundwater quality conditions at the site below the applicable 2L Standards for benzene and MTBE while aggressively remediating source area groundwater and minor soil contamination. The corrective action approach to achieve the aforementioned goals for groundwater at the site consisted of an engineered air sparging and soil vapor extraction (SVE) system coupled with monitored natural attenuation. Air sparging will be effective to remove the volatile hydrocarbon constituents, including MTBE from the groundwater. SVE will capture volatile organic vapors from the subsurface and provide an increased pressure gradient to enhance the efficacy of the air sparging. The end of active remediation will be determined when asymptotic conditions are reached in dissolved hydrocarbon concentrations in groundwater or when the applicable 2L standards have been achieved, or risk can be reduced. A full description of the remediation system is provided below in Section 3.0. CAP implementation at the site began in April 2012. Prior to CAP implementation seven monitoring wells (MW-11, MW-12, MW-19, MW-21, MW-23, MW-24, and DMW-3) were above the benzene 2L limit of 1.0 µg/L. The MTBE 2L limit of 20 µg/L was exceeded in eight monitoring wells (MW-11, MW-14, MW-17, MW-19, MW-21, MW-23, MW-24, and DMW-3) prior to CAP implementation. On December 12, 2017 Apex met with Department of Transportation (DOT) staff and their consultant to inspect monitoring wells that were proposed for abandonment during a road construction project at the site. As a result of the construction project Apex turned off AS-5 supplying air to MW-18 pending abandonment by others. Additional wells requiring abandonment for the construction project were MW-3 and MW-19. At the conclusion of 2nd Quarter 2018 CAP implementation only MW-23 exceeded the benzene 2L CAP endpoint and MW-9, MW-23, and DMW-3 exceeded the MTBE 2L CAP endpoint. 3.0 REMEDIATION SYSTEM The SVE and air sparge remediation system at the Pilot #56 facility was successfully activated on April 18, 2012. The SVE system consists of a Roots Universal RAIV 36 blower (replaced February 2017) paired with a ten horsepower Baldor Electric motor. Together the system module is capable of a maximum extraction rate of 195 actual cubic feet per minute (ACFM) at a vacuum of 12.0 inches of mercury (in Hg). The air sparge system consists of a 15 horsepower "rotary screw" compressor capable of 44-cubic feet per minute (CFM) at 55.0 pounds per square inch (PSI). The complete system is housed in a mobile eight foot by 16 foot enclosed cargo trailer. The SVE manifold contains three "legs" capable of supplying a vacuum at recovery locations SVE-1 through SVE-3. The remediation system layout with SVE well locations is depicted on Figure 3. An air sparge manifold within the remediation system enclosure includes individual gate valves, pressure gauges, pressure regulators, flow meters, and check valves required to properly regulate air flow to allow for optimum treatment of the identified subsurface petroleum constituents at air sparge points AS-1 through AS-16. Activation activities included transportation of the turn -key system to the site and connection to the sub -gradient infrastructure and separately metered power from other site activities. The remediation system layout with air sparge well locations is depicted on Figure 4. CA Performance Report (July 1 to Dec. 31, 2018) 3 January 8, 2019 Pilot #56 Incident#36096 4,0 GROUNDWATER MONITORING During this phase, Apex performed a semi-annual groundwater monitoring event to assess water table elevations and current dissolved -phase contaminant levels. Pursuant to the NC DEQ-approved CAP, Apex performed monitoring and sampling at monitoring wells MW-9, MW-11, MW-12, MW-14, MW-17, MW-20, MW-21, MW-22, MW-23, MW-24, MW-25, and DMW-3. On December 20, 2018, Apex used a SolinstTM electronic interface probe to investigate for the presence of free product and to measure groundwater elevations. Free product was not detected in any of the groundwater monitoring wells gauged during this phase. Groundwater elevation data for the gauging event is presented in Table 1. Groundwater flow direction beneath the site is influenced by water table depression and mounding created by system operation at the recovery/sparge wells; thus, a water table gradient map is not included, but historical groundwater flow direction has been measured to the north-northwest. Monitoring/recovery/air sparge well locations are depicted on Figures 2, 3, and 4. Per NC DEQ directives, on December 20, 2018, Apex collected groundwater samples from twelve monitoring wells (MW-9, MW-11, MW-12, MW-14, MW-17, MW-20, MW-21, MW-22, MW-23, MW-24, MW-25, and DMW-3). Prior to sampling, Apex purged each well to remove suspended sediment from the water column and to collect samples representative of aquifer conditions. Each well was purged until a minimum of three well volumes had been displaced. Groundwater samples were collected using dedicated, disposable, high -density polyethylene bailers and were transferred directly into the appropriate sample containers immediately upon collection. The samples were stored on ice pending delivery to the laboratory. Disposable, latex gloves were used during all phases of sample collection. Groundwater samples were submitted to ESC Lab Sciences (ESC) in Mount Juliet, Tennessee for volatile organic compound (VOC) analysis via U.S. EPA SW-846 method 6200B. Strict sample security and chain -of -custody documentation were maintained during all phases of transport. Analytical results yielded petroleum compounds in seven of the twelve monitoring wells sampled, with a maximum MTBE concentration of 78.8 µg/L in monitoring well MW-17. A summary of current groundwater quality data is presented in Table 2. Chain -of -custody documentation and the laboratory Certificates of Analyses are included as Appendix A. Historical groundwater analytical results are provided in Appendix B. The dissolved -phase endpoint for benzene of 1.0 µg/L was not exceeded in any monitoring wells. The dissolved -phase endpoint for MTBE of 20 µg/L was exceeded in monitoring wells MW-14, MW-17 and DMW-3. An isoconcentration map for MTBE is provided as Figure 5. Per NC DEQ directives, on December 20, 2018, Apex also collected groundwater samples from six supply wells (5922, 5925, 5927, 5955 Turkey Road and 2847 and 2865 Lane Street). The supply well samples were collected from outdoor spigots after being purged for approximately ten minutes. Clean, disposable latex gloves were used during all phases of sample collection. The samples were labeled and stored on ice pending delivery to the laboratory. Supply well samples were submitted to ESC for VOC analysis via U.S. EPA SW-846 method 6200B. Strict sample security and chain -of -custody documentation were maintained during all phases of transport. Petroleum constituents were not detected in any of the supply well samples; however, tetrachloroethene at a concentration of 1.52 µg/L was detected in supply well SW- 5922, which was consistent with the previous sampling events. Tetrachloroethene is typically CA Performance Report (July 1 to Dec. 31, 2018) 4 January 8, 2019 Pilot #56 Incident#36096 associated with the use of solvents and could be the result of some recent plumbing repairs at the residence. Historically petroleum compounds have not been detected in any of the supply wells. The laboratory Certificate of Analysis and chain -of -custody records are provided as Appendix A. 5.0 OPERATION AND MAINTANENCE Per NC DEQ directives, Apex performed monthly site visits during this phase for routine O&M activities, system troubleshooting, system repairs, and system monitoring. The various maintenance activities included adding lubricating oil and coolant to the air sparge system air compressor, draining of moisture from the air compressor, greasing of all fittings associated with the SVE blower and motor, replacement of faulty components, and other maintenance activities to maintain system effectiveness. A tabular summary of the O&M dates and activities performed is presented in Table 3. Copies of the O&M checklists are included as Appendix C. During this phase, the SVE and air sparge system components achieved runtimes of 85% and 24%, respectively. The air sparge compressor has been set to turn on and off as needed to maintain proper flow rates at the manifold, so the runtime may not be reflective of the total delivery time to the air sparge wells. 6.0 CORRECTIVE ACTION PERFORMANCE REPORT SUMMARY Apex has completed CAP implementation activities associated with the Pilot #56 facility located in Kannapolis, North Carolina for the period beginning July 1, 2018 and ending December 31, 2018. System runtime remained consistent during this phase. At the conclusion of 4th Quarter 2018 CAP implementation no monitoring wells exceeded the benzene 2L CAP endpoint and only MW-14, MW-17, and DMW-3 exceeded the MTBE 2L CAP endpoint. Petroleum compounds have never been detected in any of the area potable water supplies and sentinel wells such as MW-21, MW-22, and MW-25 continue to indicate that the gasoline plume is confined to the original source zone identified and described in both the CSA and approved CAP. Based on the continued presence of MTBE above 2L groundwater quality standards in several monitoring wells, Apex recommends continued operation of the remediation system in accordance with the approved CAP. This report, prepared in accordance with NC DEQ- approved scope of work, is being submitted to Mr. Brett Morris of NC DEQ on behalf of Pilot. CA Performance Report (July 1 to Dec. 31, 2018) 5 January 8, 2019 Pilot #56 Incident#36096 7.0 STATEMENTS AND CERTIFICATION The following statements must be included at the closing of the document text, and must display the seal and signature of the certifying P.E. or L.G. in addition to the name and certification number of the company or corporation [See 15A NCAC 2L .0103(e).] 1 Enter the date the performance report was due. 01/15/19. Will this report be YES O submitted after the established due date? 2 Was any required information from the above template missing from this report? YES O IF the answer to question #1 or# 2 is "YES", please provide additional information in this cell to explain what was missing and why. Delay in preparation due to new format. 3 Has the operation of the installed active remediation system experienced any YES complications during this reporting period? (i.e., answer NO' if the system has been operational except for normal maintenance events, with no unscheduled shutdowns) 4 Have all issues that were responsible for causing these complications been resolved? YES O IF the answer to question #3 or #4 is "YES", please provide additional information in this cell describing the issue(s) and any troubleshooting and/or repair steps that have been taken (or are planned) to resolve the issue(s). g Will any of the proposed cleanup milestones under the schedule approved in the E5 NO Corrective Action Plan not be met? (within a reasonable margin of error) IF the answer to question 45 is "NO", skip to the certification under #8 below. IF the answer to question #5 is "YES", please generally describe in this cell the possible reason(s) and outline proposed remedies. (This should be described in more detail in the report text above.) While great progress has been made such as non-exceedance of Benzene 2L standard, some limitations to the existing equipment apply, as well as, task authorization approval for only one site visit per month to perform O&M activities. 6 Does any known or suspected source zone soil contamination or free product remain YES outside of the remediation system area of influence that could be inhibiting cleanup? 7 Has there been an unexpected increase in contaminant mass sufficient to suggest YES a potential new release from a separate onsite or offsite source? IF the answer to either question 46 or 47 is "YES", generally describe in this cell any actions recommended to further assess or clean up this known or suspected source. (This should be described in more detail in the report text above.) 8 Certification: Robert S. Williamson, a Licensed Geologist for Apex Companies, LLC, do certify that the information contained in this report is correct and accurate to the best of my knowledge. SEAL - ,o 1735 o °',,T/CKLEY `N; l' Apex Companies, LLC is licensed to practice Geology in North Carolina. The certification number of the company or corporation is C-519. CA Performance Report (July 1 to Dec. 31, 2018) 6 January 8, 2019 Pilot #56 Incident#36096 FIGURES FIGURE I Site Location Map Former Pilot #56 2825 Lane Street Kannapolis, Cabarrus County, North Carolina Lw rack �K f£ _ :✓ 'y Jam`' J fi• ,l 1� _• 011 L CC - wI w 1 - s•I ar�' :r 646 nj'rR•S l} r JI�t7.. ■ �t M fi5 •, • V: `. y] !\f~ @' �' �--,: y � 5 � �,� - , lf'�' � "tip • � Ali ti x ti ti �J Y.` h1d� —_ +■���� �_' J: � elf( l4646_ 4 1-7 ,.1` bet Ch ETC �--� • f � � f —� � ■ ' I Irrrr v 7724 Garland Circle CONCORD, NORTH CAROLINA Project: CAP Implementation Roanoke, VA 24019 Telephone: (540) 563-4920 Client: Pilot Flying J s Source: U.S.G.S. Topographic Map of the Concord Quadrangle, North Carolina, �Y 7.5 Minute Series (1991) Apex Job #: 768490.030 ALatitude: Scale: 1:24,000 Contour Interval: 10 Feet Vertical Datum: National Geodetic 035°on tude: N � Vertical Datum 1929 Date: January 2019 Longitude: Horizontal Datum: North American Daturn1927 080 33' 39.54" W e!'. W W-25 � •F IF -lit 4 MW-13 _ F 4 • x T* 1 �•�1 . RW-1 MW-1 DMW-2 }- -3 _ 9 Boo.; pMw-26 MW- 4#-�,DMW-3 M++21 MW 22 — - MW-4 i _ . 'BMW-24 04-IF-1 t; ' RW-6 My 2- si r MW-23 err. RW r MW-3 1 *MW-18 - } + '11iadorL�d MW-2 - Abandoned r MW-27-' Lost -MW-19 Lost -r - } 100' 0' 50, 100, 1P0 200' , 0. Legend GRAPHICS ALE MW-1 Monitoring Well DR.: DRY DATE: Jan 2019 CAP Implementation Incident #36096 =` ' 1--� J E 7� 1 APEX 7724 Garland Circle Roanoke, VA24019 Phone:540-563-4920 CK.:CLC APP'D.: RSW SCALE: 1" =10V APEX PROJ. NO.: 768490.030 www.apexcos.com Site Plan Pilot Station #56 2825 Lane Street Kannapolis, North Carolina FIGURE No. 2 A � a 0 LO a i >, L U Z o cv m J c cn EU= 3 L n > i y E 'A N N a)•,ter va O .Vr O (� N L c x W 3 p N O W~ Y p s`� A a UM i O Z �' =` 'p O o N Q Q o c M W 'ate _ , � on O W * e as .2 Z�v o i E 1 1 1� 8 m 1 1 b 1 1 e � 1 1 1 n yk FT] n 1 1 1 112s ,1 � 1 1 F 11 11 h , r LLLIII 1 1 11 11 it F F 1 1 1 1 1 1 11 11 1 11 hp n o N LM N O co a a a >% Z o LEU5 ui p U (a ` > � ca W C U o U) CD v v Q O y' = U a Q o o (D G] O W a o M on y Z�v o i E / I 1 IIIN IIIX e 8 m IIIN IIIn �t I�yJr T\ 111n IIIN IIIII \ h \ IIIII IIIII IIIN �jI[q�Ir � T ♦♦ \ � Illn g IIIN 3 \ ♦ � ` \ b ♦ ♦♦\ n \\ `yT�'IF♦ \ IIIH IIIII 11113i IIIII � ♦ ♦ ; ♦ \ yyy ♦ ♦ 1 \ S Ilm IIIII IIIII h � k ♦ O \ ♦ \ h I `�� ♦♦ \ 1 ♦ � ♦♦�♦ I IIIII p IIIII IIIII ` y`. \ [♦♦♦ \ 1 ` \ ♦♦♦ \ I IIIII F IIIII ♦ \ I IIIII R IIIII � \ 1}��` IIIII IIIII N i i 0 O O In n o In It) N O _I_ __ MW-7 A" WMW-25 N r T r r MW-13 i�r k i l � RW-1 29.6 - - + _ R BMW-9 78.8 � RW-2 DMW-2 M�12 4.28- -3+ W-26 MW-0� ` � � � DM- MW-21 I - 9 # +-ND MW-22 _ - - - MW-4 i MW-20 j _ of . , ND _ .. -�- 4.02, o. MW-24 t� RW-6ti ND � a .. �.. .: MW-23 �.• �. RW- 1+ _ ND r. Y Legend MW-1 Monitoring Well ND = Non -Detect in ug/L 100' 0' 50, 100, 1 P0 200' GRAPHIC SCALE 1"=100' CAP Implementation Incident #3609E TABLES Table 1. Groundwater Elevation Data Monitoring/ Recovery Well Location Date Relative Top of Casing Elevation' Depth to Water (feet) Relative Groundwater Elevation (feet) MW-9 12/20/18 750.11 18.60 731.51 MW-11 12/20/18 753.12 18.47 734.65 MW-12 12/20/18 751.34 17.98 733.36 MW-14 12/20/18 749.79 17.42 732.37 MW-17 12/20/18 748.69 17.92 730.77 MW-20 12/20/18 752.30 18.56 733.74 MW-21 12/20/18 753.08 18.12 734.96 MW-22 12/20/18 754.00 19.31 734.69 MW-23 12/20/18 753.27 19.18 734.09 MW-24 12/20/18 752.28 18.45 733.83 MW-25 12/20/18 745.90 18.95 726.95 DMW-3 12/20/18 752.19 18.67 733.52 ' Top of casing elevation based on assumed site datum from Concord USGS map of 740.00 feet. Table 2. Summary of Groundwater Analytical Data December 20, 2018 2L Parameter MW-9 MW-11 MW-12 MW-14 MW-17 MW-20 MW-21 MW-22 MW-23 MW-24 MW-25 DMW-3 Groundwater Standard' Benzene, (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 1.0 Toluene (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 600 Ethylbenzene (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 600 Xylenes (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 500 MTBE (µg/L) ND ND ND 29.63 78.8 4.02 ND ND ND ND ND 46.5 20 EDB (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 0.02 1,2-Dichloroethane ND ND ND ND ND ND ND ND ND ND ND ND 0.4 /I Styrene (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 70 Isopropylbenzene ND ND ND ND ND ND ND ND ND ND ND ND 70 /L Propylbenzene (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 70 1,3,5-Trimethylbenzene ND ND ND ND ND ND ND ND ND ND ND ND 400 (JAg/L) tert-Butylbenzene ND ND ND ND ND ND ND ND ND ND ND ND 70 /I, 1,2,4-Trimethylbenzene ND ND 1.59 ND ND ND ND ND 6.88 ND ND ND 400 /L n-Butylbenzene (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 70 sec-Butylbenzene ND ND ND ND ND ND ND ND 1.37 ND ND ND 70 (JAg/L) p-Isopropyltoluene ND ND ND ND ND ND ND ND ND ND ND ND 25 /L Naphthalene (µg/L) ND ND ND ND ND ND ND ND ND ND ND ND 6.0 Di -isopropyl ether I ND ND :ND ND ND 1.58 ND ND ND ND ND ND 70 DIPE /L 1 All parameters analyzed via U.S. EPA method 620013, reported in micrograms per liter (µg/L). 2 ND = Non -detect. 3 Bold = Level detected above 2L Standard for high risk sites. '2L Groundwater quality standards as defined in section 15A NCAC 02L .0202; reported in micrograms per liter (µg/L). Table 3. Operations and Maintenance Activities SVE/Air Sparge Date Activities Compressor Staff Hours 06/21/18 1 Last O&M visit during 2nd Quarter 2018. 43,201.0 / 21,925.4 JSC System non -operational upon arrival due to emergency stop. Changed oil in SVE. Reset E-stop and activated all 07/26/18 components. Replaced cracked Dwyer gauge on AS-1. 43,364.8 / 22,089.6 KAH Performed routine O&M activities. System fully operational upon departure. SVE fully operational upon arrival. Activated air sparge 08/22/18 compressor. Performed O&M activities. System fully 449010.2 / 20,476.0 KAH operational upon departure. SVE fully operational upon arrival. Activated air sparge 09/27/18 compressor. Performed O&M activities. Repaired Dwyer 44,875.5 / 20,597.5 KAH gauge on AS-4. System fully operational upon departure. SVE fully operational upon arrival. Activated air sparge 10/24/18 compressor. Performed routine O&M activities. System fully 45,524.1 / 22,692.7 KAH operational upon departure. SVE fully operational upon arrival. Activated air sparge 11/19/18 compressor. Performed routine O&M activities. System fully 46,149.5 / 22,859.9 KAH operational upon departure. SVE non -operational upon arrival due to sheared belt. Activated air sparge compressor. Replaced belt on SVE. 12/20/18 Performed routine O&M activities. Performed semi-annual 46,890.0/ 22,984.2 KAH sampling event of monitoring wells and supply wells. System fully operational upon departure. Total Hours' 3,689.0/ 1,058.8 ' Total hours from 06/21/18 to 12/20/18. APPENDIX A Laboratory Certificate of Analysis And Chain -of -Custody Documentation aceAnalytical o National Center for Testing & Innovation ANALYTICAL REPORT January 02, 2019 Apex Environmental Inc. - Roanke Va Sample Delivery Group: L1055594 Samples Received: 12/21/2018 Project Number: 768490-030 Description: Pilot 56 Report To: Robert Wagner 7724 Garland Circle Roanoke, VA 24019 Entire Report Reviewed By: Pam Langford Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. V Am moos P. TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Fn Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 6 Sr: Sample Results 7 FS SW-5922 L1055594-01 7 [Cn] SW-5925 L1055594-02 9 SW-5927 L1055594-03 11 FSr SW-5955 L1055594-04 13 SW-2865 L1055594-05 15 RC SW-2847 L1055594-06 17 �GI MW-21 L1055594-07 19 MW-22 L1055594-08 21 rAl MW-24 L1055594-09 23 MW-25 L1055594-10 25 FSC DMW-3 L1055594-11 27 MW-14 L1055594-12 29 MW-9 L1055594-13 31 MW-12 L1055594-14 33 MW-17 L1055594-15 35 MW-20 L1055594-16 37 MW-23 L1055594-17 39 MW-11 L1055594-18 41 Qc: Quality Control Summary 43 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 43 GI: Glossary of Terms 55 Al: Accreditations & Locations 56 Sc: Sample Chain of Custody 57 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 2 of 58 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time SW-5922 L1055594-01 GW Kyle Hicks 12/20/1814:15 12/21/1810:00 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215013 1 12/22/1816:11 12/22/1816:11 BMB Collected by Collected date/time Received date/time M SW-5925 L1055594-02 GW Kyle Hicks 12/20/1814:25 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst [Cn] date/time date/time Organic Compounds (GC/MS) by Method 6200E-1997 WG1215013 1 12/22/1816:31 12/22/1816:31 BMB FSrVolatile Collected by Collected date/time Received date/time 6QC SW-5927 L1055594-03 GW Kyle Hicks 12/20/1814:35 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst GI date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215013 1 12/22/1816:51 12/22/1816:51 BMB FAI Collected by Collected date/time Received date/time SW-5955 L1055594-04 GW Kyle Hicks 12/20/1814:40 12/21/1810:00 FSC Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215013 1 12/22/1817:11 12/22/1817:11 BMB Collected by Collected date/time Received date/time SW-2865 L1055594-05 GW Kyle Hicks 12/20/1814:50 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215013 1 12/22/1817:31 12/22/1817:31 BMB Collected by Collected date/time Received date/time SW-2847 L1055594-06 GW Kyle Hicks 12/20/1815:00 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1216990 1 12/29/1811:22 12/29/1811:22 JHH Collected by Collected date/time Received date/time MW-21 L1055594-07 GW Kyle Hicks 12/20/1812:35 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1216990 1 12/29/1811:42 12/29/1811:42 JHH Collected by Collected date/time Received date/time MW-22 L1055594-08 GW Kyle Hicks 12/20/1812:30 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200E-1997 WG1216990 1 12/29/1812:01 12/29/1812:01 JHH ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 3 of 58 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time MW-24 L1055594-09 GW Kyle Hicks 12/20/1812:05 12/21/1810:00 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1216990 1 12/29/1812:21 12/29/1812:21 JHH Collected by Collected date/time Received date/time M MW-25 L1055594-10 GW Kyle Hicks 12/20/1813:30 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst [Cn] date/time date/time Organic Compounds (GC/MS) by Method 6200E-1997 WG1216990 1 12/29/1812:41 12/29/1812:41 JHH FSrVolatile Collected by Collected date/time Received date/time 6QC DMW-3 L1055594-11 GW Kyle Hicks 12/20/1812:15 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst GI date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215938 1 12/26/1812:53 12/26/1812:53 TJJ FAI Collected by Collected date/time Received date/time MW-14 L1055594-12 GW Kyle Hicks 12/20/1813:10 12/21/1810:00 FSC Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215938 1 12/26/1813:13 12/26/1813:13 TJJ Collected by Collected date/time Received date/time MW-9 L1055594-13 GW Kyle Hicks 12/20/1813:35 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215938 1 12/26/1813:32 12/26/1813:32 TJJ Collected by Collected date/time Received date/time MW-12 L1055594-14 GW Kyle Hicks 12/20/1813:20 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215938 1 12/26/1813:52 12/26/1813:52 TJJ Collected by Collected date/time Received date/time MW-17 L1055594-15 GW Kyle Hicks 12/20/1813:40 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215938 1 12/26/1814:12 12/26/1814:12 TJJ Collected by Collected date/time Received date/time MW-20 L1055594-16 GW Kyle Hicks 12/20/1812:55 12/21/1810:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 6200E-1997 WG1215938 1 12/26/1814:32 12/26/1814:32 TJJ ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 4 of 58 MW-23 L1055594-17 GW SAMPLE SUMMARY Collected by Kyle Hicks Method Batch Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG1215938 MW-11 L1055594-18 GW Dilution Preparation date/time 1 12/26/1814:52 Collected by Kyle Hicks Method Batch Dilution Preparation date/time Volatile Organic Compounds (GC/MS) by Method 6200E-1997 WG1215938 1 12/26/1815:12 ONE LAB. NATIONWIDE. Collected date/time Received date/time 12/20/1812:00 12/21/1810:00 FP1 Analysis Analyst date/time FTC 12/26/18 14:52 TJJ Collected date/time Received date/time M 12/20/1812:40 12/21/1810:00 [�n] Analysis Analyst date/time TJJ FSr12/26/1815:12 RC F, FAI FSC ACCOUNT: PROJECT: SDG: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 DATE/TIME: PAGE: 01/02/19 09:23 5 of 58 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. Pam Langford Project Manager FP1 FTC FSS FSr 6 QC �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 6 of 58 SW-5922 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 14:15 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/22/201816:11 WG1215013 FTc Acrolein ND 50.0 1 12/22/201816:11 WG1215013 Acrylonitrile ND 10.0 1 12/22/201816:11 WG1215013 F Benzene ND 1.00 1 12/22/201816:11 WG1215013 Bromobenzene ND 1.00 1 12/22/201816:11 WG1215013 Bromodichloromethane ND 1.00 1 12/22/201816:11 WG1215013 4 Crl Bromoform ND 1.00 1 12/22/201816:11 WG1215013 Bromomethane ND 5.00 1 12/22/201816:11 WG1215013 n-Butylbenzene ND 1.00 1 12/22/201816:11 WG1215013 sec -Butyl benzene ND 1.00 1 12/22/201816:11 WG1215013 ter[-Butylbenzene ND 1.00 1 12/22/201816:11 WG1215013 Fc Carbon tetrachloride ND 1.00 1 12/22/201816:11 WG1215013 Chlorobenzene ND 1.00 1 12/22/201816:11 WG1215013 Fq Chlorodibromomethane ND 1.00 1 12/22/201816:11 WG1215013 Chloroethane ND 5.00 1 12/22/201816:11 WG1215013 Chloroform ND 5.00 1 12/22/201816:11 WG1215013 FAI Chloromethane ND 2.50 1 12/22/201816:11 WG1215013 2-Chlorotoluene ND 1.00 1 12/22/201816:11 WG1215013 F 4-Chlorotoluene ND 1.00 1 12/22/201816:11 WG1215013 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/22/201816:11 WG1215013 1,2-Dibromoethane ND 1.00 1 12/22/201816:11 WG1215013 Dibromomethane ND 1.00 1 12/22/201816:11 WG1215013 1,2-Dichlorobenzene ND 1.00 1 12/22/201816:11 WG1215013 1,3-Dichlorobenzene ND 1.00 1 12/22/201816:11 WG1215013 1,4-Dichlorobenzene ND 1.00 1 12/22/201816:11 WG1215013 Dichlorodifluoromethane ND 5.00 1 12/22/201816:11 WG1215013 1,1-Dichloroethane ND 1.00 1 12/22/201816:11 WG1215013 1,2-Dichloroethane ND 1.00 1 12/22/201816:11 WG1215013 1,1-Dichloroethene ND 1.00 1 12/22/201816:11 WG1215013 cis-1,2-Dichloroethene ND 1.00 1 12/22/201816:11 WG1215013 trans-1,2-Dichloroethene ND 1.00 1 12/22/201816:11 WG1215013 1,2-Dichloropropane ND 1.00 1 12/22/201816:11 WG1215013 1,1-Dichloropropene ND 1.00 1 12/22/201816:11 WG1215013 1,3-Dichloropropane ND 1.00 1 12/22/201816:11 WG1215013 2,2-Dichloropropane ND 1.00 1 12/22/201816:11 WG1215013 Di -isopropyl ether ND 1.00 1 12/22/201816:11 WG1215013 Ethylbenzene ND 1.00 1 12/22/201816:11 WG1215013 Hexachloro-1,3-butadiene ND 1.00 1 12/22/201816:11 WG1215013 Isopropylbenzene ND 1.00 1 12/22/201816:11 WG1215013 p-Isopropyltoluene ND 1.00 1 12/22/201816:11 WG1215013 2-Butanone (MEK) ND 10.0 1 12/22/201816:11 WG1215013 Methylene Chloride ND 5.00 1 12/22/201816:11 WG1215013 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/22/201816:11 WG1215013 Methyl tert-butyl ether ND 1.00 1 12/22/201816:11 WG1215013 Naphthalene ND 5.00 1 12/22/201816:11 WG1215013 n-Propylbenzene ND 1.00 1 12/22/201816:11 WG1215013 Styrene ND 1.00 1 12/22/201816:11 WG1215013 1,1,1,2-Tetrachloroethane ND 1.00 1 12/22/201816:11 WG1215013 1,1,2,2-Tetrachloroethane ND 1.00 1 12/22/201816:11 WG1215013 Tetrachloroethene 1.52 1.00 1 12/22/201816:11 WG1215013 Toluene ND 1.00 1 12/22/201816:11 WG1215013 1,2,3-Trichlorobenzene ND 1.00 1 12/22/201816:11 WG1215013 1,2,4-Trichlorobenzene ND 1.00 1 12/22/201816:11 WG1215013 1,1,1-Trichloroethane ND 1.00 1 12/22/201816:11 WG1215013 1,1,2-Trichloroethane ND 1.00 1 12/22/201816:11 WG1215013 Trichloroethene ND 1.00 1 12/22/201816:11 WG1215013 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 7 of 58 ONE LAB. NATIONWIDE. SW-5922 SAMPLE RESULTS - 01 Collected date/time: 12/20/18 14:15 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 98.9 (S) Dibromofluoromethane 102 (S) a, a, a-Trifluoroto/uene 97.0 (S) 4-Bromof/uorobenzene 102 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/22/201816:11 2.50 1 12/22/201816:11 1.00 1 12/22/201816:11 1.00 1 12/22/201816:11 1.00 1 12/22/201816:11 1.00 1 12/22/201816:11 2.00 1 12/22/201816:11 80.0-120 121221201816:11 75. 0-120 121221201816:11 80.0-120 121221201816:11 77. 0-126 121221201816:11 Batch WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 8 of 58 SW-5925 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 14:25 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/22/201816:31 WG1215013 FTc Acrolein ND 50.0 1 12/22/201816:31 WG1215013 Acrylonitrile ND 10.0 1 12/22/201816:31 WG1215013 F Benzene ND 1.00 1 12/22/201816:31 WG1215013 Bromobenzene ND 1.00 1 12/22/201816:31 WG1215013 Bromodichloromethane ND 1.00 1 12/22/201816:31 WG1215013 4 Crl Bromoform ND 1.00 1 12/22/201816:31 WG1215013 Bromomethane ND 5.00 1 12/22/201816:31 WG1215013 n-Butylbenzene ND 1.00 1 12/22/201816:31 WG1215013 sec -Butyl benzene ND 1.00 1 12/22/201816:31 WG1215013 ter[-Butylbenzene ND 1.00 1 12/22/201816:31 WG1215013 Fc Carbon tetrachloride ND 1.00 1 12/22/201816:31 WG1215013 Chlorobenzene ND 1.00 1 12/22/201816:31 WG1215013 Fq Chlorodibromomethane ND 1.00 1 12/22/201816:31 WG1215013 Chloroethane ND 5.00 1 12/22/201816:31 WG1215013 Chloroform ND 5.00 1 12/22/201816:31 WG1215013 FAI Chloromethane ND 2.50 1 12/22/201816:31 WG1215013 2-Chlorotoluene ND 1.00 1 12/22/201816:31 WG1215013 F 4-Chlorotoluene ND 1.00 1 12/22/201816:31 WG1215013 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/22/201816:31 WG1215013 1,2-Dibromoethane ND 1.00 1 12/22/201816:31 WG1215013 Dibromomethane ND 1.00 1 12/22/201816:31 WG1215013 1,2-Dichlorobenzene ND 1.00 1 12/22/201816:31 WG1215013 1,3-Dichlorobenzene ND 1.00 1 12/22/201816:31 WG1215013 1,4-Dichlorobenzene ND 1.00 1 12/22/201816:31 WG1215013 Dichlorodifluoromethane ND 5.00 1 12/22/201816:31 WG1215013 1,1-Dichloroethane ND 1.00 1 12/22/201816:31 WG1215013 1,2-Dichloroethane ND 1.00 1 12/22/201816:31 WG1215013 1,1-Dichloroethene ND 1.00 1 12/22/201816:31 WG1215013 cis-1,2-Dichloroethene ND 1.00 1 12/22/201816:31 WG1215013 trans-1,2-Dichloroethene ND 1.00 1 12/22/201816:31 WG1215013 1,2-Dichloropropane ND 1.00 1 12/22/201816:31 WG1215013 1,1-Dichloropropene ND 1.00 1 12/22/201816:31 WG1215013 1,3-Dichloropropane ND 1.00 1 12/22/201816:31 WG1215013 2,2-Dichloropropane ND 1.00 1 12/22/201816:31 WG1215013 Di -isopropyl ether ND 1.00 1 12/22/201816:31 WG1215013 Ethylbenzene ND 1.00 1 12/22/201816:31 WG1215013 Hexachloro-1,3-butadiene ND 1.00 1 12/22/201816:31 WG1215013 Isopropylbenzene ND 1.00 1 12/22/201816:31 WG1215013 p-Isopropyltoluene ND 1.00 1 12/22/201816:31 WG1215013 2-Butanone (MEK) ND 10.0 1 12/22/201816:31 WG1215013 Methylene Chloride ND 5.00 1 12/22/201816:31 WG1215013 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/22/201816:31 WG1215013 Methyl tert-butyl ether ND 1.00 1 12/22/201816:31 WG1215013 Naphthalene ND 5.00 1 12/22/201816:31 WG1215013 n-Propylbenzene ND 1.00 1 12/22/201816:31 WG1215013 Styrene ND 1.00 1 12/22/201816:31 WG1215013 1,1,1,2-Tetrachloroethane ND 1.00 1 12/22/201816:31 WG1215013 1,1,2,2-Tetrachloroethane ND 1.00 1 12/22/201816:31 WG1215013 Tetrachloroethene ND 1.00 1 12/22/201816:31 WG1215013 Toluene ND 1.00 1 12/22/201816:31 WG1215013 1,2,3-Trichlorobenzene ND 1.00 1 12/22/201816:31 WG1215013 1,2,4-Trichlorobenzene ND 1.00 1 12/22/201816:31 WG1215013 1,1,1-Trichloroethane ND 1.00 1 12/22/201816:31 WG1215013 1,1,2-Trichloroethane ND 1.00 1 12/22/201816:31 WG1215013 Trichloroethene ND 1.00 1 12/22/201816:31 WG1215013 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 9 of 58 ONE LAB. NATIONWIDE. SW-5925 SAMPLE RESULTS - 02 Collected date/time: 12/20/18 14:25 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 101 (S) Dibromofluoromethane 101 (S) a, a, a-Trifluoroto/uene 98.7 (S) 4-Bromof/uorobenzene 106 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/22/201816:31 2.50 1 12/22/201816:31 1.00 1 12/22/201816:31 1.00 1 12/22/201816:31 1.00 1 12/22/201816:31 1.00 1 12/22/201816:31 2.00 1 12/22/201816:31 80.0-120 12122120181631 75. 0-120 12122120181631 80.0-120 12122120181631 77. 0-126 12122120181631 Batch WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 10 of 58 SW-5927 SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 14:35 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/22/201816:51 WG1215013 FTc Acrolein ND 50.0 1 12/22/201816:51 WG1215013 Acrylonitrile ND 10.0 1 12/22/201816:51 WG1215013 F Benzene ND 1.00 1 12/22/201816:51 WG1215013 Bromobenzene ND 1.00 1 12/22/201816:51 WG1215013 Bromodichloromethane ND 1.00 1 12/22/201816:51 WG1215013 4 Crl Bromoform ND 1.00 1 12/22/201816:51 WG1215013 Bromomethane ND 5.00 1 12/22/201816:51 WG1215013 n-Butylbenzene ND 1.00 1 12/22/201816:51 WG1215013 sec -Butyl benzene ND 1.00 1 12/22/201816:51 WG1215013 ter[-Butylbenzene ND 1.00 1 12/22/201816:51 WG1215013 Fc Carbon tetrachloride ND 1.00 1 12/22/201816:51 WG1215013 Chlorobenzene ND 1.00 1 12/22/201816:51 WG1215013 Fq Chlorodibromomethane ND 1.00 1 12/22/201816:51 WG1215013 Chloroethane ND 5.00 1 12/22/201816:51 WG1215013 Chloroform ND 5.00 1 12/22/201816:51 WG1215013 FAI Chloromethane ND 2.50 1 12/22/201816:51 WG1215013 2-Chlorotoluene ND 1.00 1 12/22/201816:51 WG1215013 F 4-Chlorotoluene ND 1.00 1 12/22/201816:51 WG1215013 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/22/201816:51 WG1215013 1,2-Dibromoethane ND 1.00 1 12/22/201816:51 WG1215013 Dibromomethane ND 1.00 1 12/22/201816:51 WG1215013 1,2-Dichlorobenzene ND 1.00 1 12/22/201816:51 WG1215013 1,3-Dichlorobenzene ND 1.00 1 12/22/201816:51 WG1215013 1,4-Dichlorobenzene ND 1.00 1 12/22/201816:51 WG1215013 Dichlorodifluoromethane ND 5.00 1 12/22/201816:51 WG1215013 1,1-Dichloroethane ND 1.00 1 12/22/201816:51 WG1215013 1,2-Dichloroethane ND 1.00 1 12/22/201816:51 WG1215013 1,1-Dichloroethene ND 1.00 1 12/22/201816:51 WG1215013 cis-1,2-Dichloroethene ND 1.00 1 12/22/201816:51 WG1215013 trans-1,2-Dichloroethene ND 1.00 1 12/22/201816:51 WG1215013 1,2-Dichloropropane ND 1.00 1 12/22/201816:51 WG1215013 1,1-Dichloropropene ND 1.00 1 12/22/201816:51 WG1215013 1,3-Dichloropropane ND 1.00 1 12/22/201816:51 WG1215013 2,2-Dichloropropane ND 1.00 1 12/22/201816:51 WG1215013 Di -isopropyl ether ND 1.00 1 12/22/201816:51 WG1215013 Ethylbenzene ND 1.00 1 12/22/201816:51 WG1215013 Hexachloro-1,3-butadiene ND 1.00 1 12/22/201816:51 WG1215013 Isopropylbenzene ND 1.00 1 12/22/201816:51 WG1215013 p-Isopropyltoluene ND 1.00 1 12/22/201816:51 WG1215013 2-Butanone (MEK) ND 10.0 1 12/22/201816:51 WG1215013 Methylene Chloride ND 5.00 1 12/22/201816:51 WG1215013 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/22/201816:51 WG1215013 Methyl tert-butyl ether ND 1.00 1 12/22/201816:51 WG1215013 Naphthalene ND 5.00 1 12/22/201816:51 WG1215013 n-Propylbenzene ND 1.00 1 12/22/201816:51 WG1215013 Styrene ND 1.00 1 12/22/201816:51 WG1215013 1,1,1,2-Tetrachloroethane ND 1.00 1 12/22/201816:51 WG1215013 1,1,2,2-Tetrachloroethane ND 1.00 1 12/22/201816:51 WG1215013 Tetrachloroethene ND 1.00 1 12/22/201816:51 WG1215013 Toluene ND 1.00 1 12/22/201816:51 WG1215013 1,2,3-Trichlorobenzene ND 1.00 1 12/22/201816:51 WG1215013 1,2,4-Trichlorobenzene ND 1.00 1 12/22/201816:51 WG1215013 1,1,1-Trichloroethane ND 1.00 1 12/22/201816:51 WG1215013 1,1,2-Trichloroethane ND 1.00 1 12/22/201816:51 WG1215013 Trichloroethene ND 1.00 1 12/22/201816:51 WG1215013 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 11 of 58 ONE LAB. NATIONWIDE. SW-5927 SAMPLE RESULTS - 03 Collected date/time: 12/20/18 14:35 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 101 (S) Dibromofluoromethane 101 (S) a, a, a-Trifluoroto/uene 102 (S) 4-Bromof/uorobenzene 104 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/22/201816:51 2.50 1 12/22/201816:51 1.00 1 12/22/201816:51 1.00 1 12/22/201816:51 1.00 1 12/22/201816:51 1.00 1 12/22/201816:51 2.00 1 12/22/201816:51 80.0-120 121221201816:51 75. 0-120 1212212018 16:51 80.0-120 121221201816:51 77. 0-126 1212212018 16:51 Batch WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 Fp FTc FS Fn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 12 of 58 SW-5955 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 14:40 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/22/201817:11 WG1215013 FTc Acrolein ND 50.0 1 12/22/201817:11 WG1215013 Acrylonitrile ND 10.0 1 12/22/201817:11 WG1215013 F Benzene ND 1.00 1 12/22/201817:11 WG1215013 Bromobenzene ND 1.00 1 12/22/201817:11 WG1215013 Bromodichloromethane ND 1.00 1 12/22/201817:11 WG1215013 4 Crl Bromoform ND 1.00 1 12/22/201817:11 WG1215013 Bromomethane ND 5.00 1 12/22/201817:11 WG1215013 n-Butylbenzene ND 1.00 1 12/22/201817:11 WG1215013 sec -Butyl benzene ND 1.00 1 12/22/201817:11 WG1215013 ter[-Butylbenzene ND 1.00 1 12/22/201817:11 WG1215013 Fc Carbon tetrachloride ND 1.00 1 12/22/201817:11 WG1215013 Chlorobenzene ND 1.00 1 12/22/201817:11 WG1215013 Fq Chlorodibromomethane ND 1.00 1 12/22/201817:11 WG1215013 Chloroethane ND 5.00 1 12/22/201817:11 WG1215013 Chloroform ND 5.00 1 12/22/201817:11 WG1215013 FAI Chloromethane ND 2.50 1 12/22/201817:11 WG1215013 2-Chlorotoluene ND 1.00 1 12/22/201817:11 WG1215013 F 4-Chlorotoluene ND 1.00 1 12/22/201817:11 WG1215013 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/22/201817:11 WG1215013 1,2-Dibromoethane ND 1.00 1 12/22/201817:11 WG1215013 Dibromomethane ND 1.00 1 12/22/201817:11 WG1215013 1,2-Dichlorobenzene ND 1.00 1 12/22/201817:11 WG1215013 1,3-Dichlorobenzene ND 1.00 1 12/22/201817:11 WG1215013 1,4-Dichlorobenzene ND 1.00 1 12/22/201817:11 WG1215013 Dichlorodifluoromethane ND 5.00 1 12/22/201817:11 WG1215013 1,1-Dichloroethane ND 1.00 1 12/22/201817:11 WG1215013 1,2-Dichloroethane ND 1.00 1 12/22/201817:11 WG1215013 1,1-Dichloroethene ND 1.00 1 12/22/201817:11 WG1215013 cis-1,2-Dichloroethene ND 1.00 1 12/22/201817:11 WG1215013 trans-1,2-Dichloroethene ND 1.00 1 12/22/201817:11 WG1215013 1,2-Dichloropropane ND 1.00 1 12/22/201817:11 WG1215013 1,1-Dichloropropene ND 1.00 1 12/22/201817:11 WG1215013 1,3-Dichloropropane ND 1.00 1 12/22/201817:11 WG1215013 2,2-Dichloropropane ND 1.00 1 12/22/201817:11 WG1215013 Di -isopropyl ether ND 1.00 1 12/22/201817:11 WG1215013 Ethylbenzene ND 1.00 1 12/22/201817:11 WG1215013 Hexachloro-1,3-butadiene ND 1.00 1 12/22/201817:11 WG1215013 Isopropylbenzene ND 1.00 1 12/22/201817:11 WG1215013 p-Isopropyltoluene ND 1.00 1 12/22/201817:11 WG1215013 2-Butanone (MEK) ND 10.0 1 12/22/201817:11 WG1215013 Methylene Chloride ND 5.00 1 12/22/201817:11 WG1215013 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/22/201817:11 WG1215013 Methyl tert-butyl ether ND 1.00 1 12/22/201817:11 WG1215013 Naphthalene ND 5.00 1 12/22/201817:11 WG1215013 n-Propylbenzene ND 1.00 1 12/22/201817:11 WG1215013 Styrene ND 1.00 1 12/22/201817:11 WG1215013 1,1,1,2-Tetrachloroethane ND 1.00 1 12/22/201817:11 WG1215013 1,1,2,2-Tetrachloroethane ND 1.00 1 12/22/201817:11 WG1215013 Tetrachloroethene ND 1.00 1 12/22/201817:11 WG1215013 Toluene ND 1.00 1 12/22/201817:11 WG1215013 1,2,3-Trichlorobenzene ND 1.00 1 12/22/201817:11 WG1215013 1,2,4-Trichlorobenzene ND 1.00 1 12/22/201817:11 WG1215013 1,1,1-Trichloroethane ND 1.00 1 12/22/201817:11 WG1215013 1,1,2-Trichloroethane ND 1.00 1 12/22/201817:11 WG1215013 Trichloroethene ND 1.00 1 12/22/201817:11 WG1215013 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 13 of 58 ONE LAB. NATIONWIDE. SW-5955 SAMPLE RESULTS - 04 Collected date/time: 12/20/18 14:40 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 99.7 (S) Dibromofluoromethane 102 (S) a, a, a-Trifluoroto/uene 100 (S) 4-Bromof/uorobenzene 106 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/22/201817:11 2.50 1 12/22/201817:11 1.00 1 12/22/201817:11 1.00 1 12/22/201817:11 1.00 1 12/22/201817:11 1.00 1 12/22/201817:11 2.00 1 12/22/201817:11 80.0-120 121221201817.71 75. 0-120 121221201817.71 80.0-120 121221201817.71 77. 0-126 121221201817.71 Batch WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 Fp FTc FS Fn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 14 of 58 SW-2865 SAMPLE RESULTS - 05 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 14:50 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/22/201817:31 WG1215013 FTc Acrolein ND 50.0 1 12/22/201817:31 WG1215013 Acrylonitrile ND 10.0 1 12/22/201817:31 WG1215013 F Benzene ND 1.00 1 12/22/201817:31 WG1215013 Bromobenzene ND 1.00 1 12/22/201817:31 WG1215013 Bromodichloromethane ND 1.00 1 12/22/201817:31 WG1215013 4 Crl Bromoform ND 1.00 1 12/22/201817:31 WG1215013 Bromomethane ND 5.00 1 12/22/201817:31 WG1215013 n-Butylbenzene ND 1.00 1 12/22/201817:31 WG1215013 sec -Butyl benzene ND 1.00 1 12/22/201817:31 WG1215013 ter[-Butylbenzene ND 1.00 1 12/22/201817:31 WG1215013 Fc Carbon tetrachloride ND 1.00 1 12/22/201817:31 WG1215013 Chlorobenzene ND 1.00 1 12/22/201817:31 WG1215013 Fq Chlorodibromomethane ND 1.00 1 12/22/201817:31 WG1215013 Chloroethane ND 5.00 1 12/22/201817:31 WG1215013 Chloroform ND 5.00 1 12/22/201817:31 WG1215013 FAI Chloromethane ND 2.50 1 12/22/201817:31 WG1215013 2-Chlorotoluene ND 1.00 1 12/22/201817:31 WG1215013 F 4-Chlorotoluene ND 1.00 1 12/22/201817:31 WG1215013 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/22/201817:31 WG1215013 1,2-Dibromoethane ND 1.00 1 12/22/201817:31 WG1215013 Dibromomethane ND 1.00 1 12/22/201817:31 WG1215013 1,2-Dichlorobenzene ND 1.00 1 12/22/201817:31 WG1215013 1,3-Dichlorobenzene ND 1.00 1 12/22/201817:31 WG1215013 1,4-Dichlorobenzene ND 1.00 1 12/22/201817:31 WG1215013 Dichlorodifluoromethane ND 5.00 1 12/22/201817:31 WG1215013 1,1-Dichloroethane ND 1.00 1 12/22/201817:31 WG1215013 1,2-Dichloroethane ND 1.00 1 12/22/201817:31 WG1215013 1,1-Dichloroethene ND 1.00 1 12/22/201817:31 WG1215013 cis-1,2-Dichloroethene ND 1.00 1 12/22/201817:31 WG1215013 trans-1,2-Dichloroethene ND 1.00 1 12/22/201817:31 WG1215013 1,2-Dichloropropane ND 1.00 1 12/22/201817:31 WG1215013 1,1-Dichloropropene ND 1.00 1 12/22/201817:31 WG1215013 1,3-Dichloropropane ND 1.00 1 12/22/201817:31 WG1215013 2,2-Dichloropropane ND 1.00 1 12/22/201817:31 WG1215013 Di -isopropyl ether ND 1.00 1 12/22/201817:31 WG1215013 Ethylbenzene ND 1.00 1 12/22/201817:31 WG1215013 Hexachloro-1,3-butadiene ND 1.00 1 12/22/201817:31 WG1215013 Isopropylbenzene ND 1.00 1 12/22/201817:31 WG1215013 p-Isopropyltoluene ND 1.00 1 12/22/201817:31 WG1215013 2-Butanone (MEK) ND 10.0 1 12/22/201817:31 WG1215013 Methylene Chloride ND 5.00 1 12/22/201817:31 WG1215013 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/22/201817:31 WG1215013 Methyl tert-butyl ether ND 1.00 1 12/22/201817:31 WG1215013 Naphthalene ND 5.00 1 12/22/201817:31 WG1215013 n-Propylbenzene ND 1.00 1 12/22/201817:31 WG1215013 Styrene ND 1.00 1 12/22/201817:31 WG1215013 1,1,1,2-Tetrachloroethane ND 1.00 1 12/22/201817:31 WG1215013 1,1,2,2-Tetrachloroethane ND 1.00 1 12/22/201817:31 WG1215013 Tetrachloroethene ND 1.00 1 12/22/201817:31 WG1215013 Toluene ND 1.00 1 12/22/201817:31 WG1215013 1,2,3-Trichlorobenzene ND 1.00 1 12/22/201817:31 WG1215013 1,2,4-Trichlorobenzene ND 1.00 1 12/22/201817:31 WG1215013 1,1,1-Trichloroethane ND 1.00 1 12/22/201817:31 WG1215013 1,1,2-Trichloroethane ND 1.00 1 12/22/201817:31 WG1215013 Trichloroethene ND 1.00 1 12/22/201817:31 WG1215013 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 15 of 58 ONE LAB. NATIONWIDE. SW-2865 SAMPLE RESULTS - 05 Collected date/time: 12/20/18 14:50 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 97.7 (S) Dibromofluoromethane 100 (S) a, a, a-Trifluoroto/uene 101 (S) 4-Bromof/uorobenzene 106 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/22/201817:31 2.50 1 12/22/201817:31 1.00 1 12/22/201817:31 1.00 1 12/22/201817:31 1.00 1 12/22/201817:31 1.00 1 12/22/201817:31 2.00 1 12/22/201817:31 80.0-120 121221201817.31 75. 0-120 121221201817.31 80.0-120 121221201817.31 77. 0-126 121221201817.31 Batch WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 WG1215013 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 16 of 58 SW-2847 SAMPLE RESULTS - 06 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 15:00 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acetone ND 50.0 1 12/29/201811:22 WG1216990 FTc Acrolein ND J4 50.0 1 12/29/201811:22 WG1216990 Acrylonitrile ND 10.0 1 12/29/201811:22 WG1216990 F Benzene ND 1.00 1 12/29/201811:22 WG1216990 Bromobenzene ND 1.00 1 12/29/201811:22 WG1216990 Bromodichloromethane ND 1.00 1 12/29/201811:22 WG1216990 4 Crl Bromoform ND 1.00 1 12/29/201811:22 WG1216990 Bromomethane ND 5.00 1 12/29/201811:22 WG1216990 n-Butylbenzene ND 1.00 1 12/29/201811:22 WG1216990 sec -Butyl benzene ND 1.00 1 12/29/201811:22 WG1216990 ter[-Butylbenzene ND 1.00 1 12/29/201811:22 WG1216990 Fc Carbon tetrachloride ND 1.00 1 12/29/201811:22 WG1216990 Chlorobenzene ND 1.00 1 12/29/201811:22 WG1216990 Fq Chlorodibromomethane ND 1.00 1 12/29/201811:22 WG1216990 Chloroethane ND 5.00 1 12/29/201811:22 WG1216990 Chloroform ND 5.00 1 12/29/201811:22 WG1216990 FAI Chloromethane ND 2.50 1 12/29/201811:22 WG1216990 2-Chlorotoluene ND 1.00 1 12/29/201811:22 WG1216990 F 4-Chlorotoluene ND 1.00 1 12/29/201811:22 WG1216990 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/29/201811:22 WG1216990 1,2-Dibromoethane ND 1.00 1 12/29/201811:22 WG1216990 Dibromomethane ND 1.00 1 12/29/201811:22 WG1216990 1,2-Dichlorobenzene ND 1.00 1 12/29/201811:22 WG1216990 1,3-Dichlorobenzene ND 1.00 1 12/29/201811:22 WG1216990 1,4-Dichlorobenzene ND 1.00 1 12/29/201811:22 WG1216990 Dichlorodifluoromethane ND 5.00 1 12/29/201811:22 WG1216990 1,1-Dichloroethane ND 1.00 1 12/29/201811:22 WG1216990 1,2-Dichloroethane ND 1.00 1 12/29/201811:22 WG1216990 1,1-Dichloroethene ND 1.00 1 12/29/201811:22 WG1216990 cis-1,2-Dichloroethene ND 1.00 1 12/29/201811:22 WG1216990 trans-1,2-Dichloroethene ND 1.00 1 12/29/201811:22 WG1216990 1,2-Dichloropropane ND 1.00 1 12/29/201811:22 WG1216990 1,1-Dichloropropene ND 1.00 1 12/29/201811:22 WG1216990 1,3-Dichloropropane ND 1.00 1 12/29/201811:22 WG1216990 2,2-Dichloropropane ND 1.00 1 12/29/201811:22 WG1216990 Di -isopropyl ether ND 1.00 1 12/29/201811:22 WG1216990 Ethylbenzene ND 1.00 1 12/29/201811:22 WG1216990 Hexachloro-1,3-butadiene ND 1.00 1 12/29/201811:22 WG1216990 Isopropylbenzene ND 1.00 1 12/29/201811:22 WG1216990 p-Isopropyltoluene ND 1.00 1 12/29/201811:22 WG1216990 2-Butanone (MEK) ND 10.0 1 12/29/201811:22 WG1216990 Methylene Chloride ND 5.00 1 12/29/201811:22 WG1216990 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/29/201811:22 WG1216990 Methyl tert-butyl ether ND 1.00 1 12/29/201811:22 WG1216990 Naphthalene ND 5.00 1 12/29/201811:22 WG1216990 n-Propylbenzene ND 1.00 1 12/29/201811:22 WG1216990 Styrene ND 1.00 1 12/29/201811:22 WG1216990 1,1,1,2-Tetrachloroethane ND 1.00 1 12/29/201811:22 WG1216990 1,1,2,2-Tetrachloroethane ND 1.00 1 12/29/201811:22 WG1216990 Tetrachloroethene ND 1.00 1 12/29/201811:22 WG1216990 Toluene ND 1.00 1 12/29/201811:22 WG1216990 1,2,3-Trichlorobenzene ND 1.00 1 12/29/201811:22 WG1216990 1,2,4-Trichlorobenzene ND 1.00 1 12/29/201811:22 WG1216990 1,1,1-Trichloroethane ND 1.00 1 12/29/201811:22 WG1216990 1,1,2-Trichloroethane ND 1.00 1 12/29/201811:22 WG1216990 Trichloroethene ND 1.00 1 12/29/201811:22 WG1216990 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 17 of 58 ONE LAB. NATIONWIDE. SW-2847 SAMPLE RESULTS - 06 Collected date/time: 12/20/18 15:00 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 105 (S) Dibromofluoromethane 86.3 (S) a, a, a-Trifluoroto/uene 102 (S) 4-Bromof/uorobenzene 96.5 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/29/201811:22 2.50 1 12/29/201811:22 1.00 1 12/29/201811:22 1.00 1 12/29/201811:22 1.00 1 12/29/201811:22 1.00 1 12/29/201811:22 2.00 1 12/29/201811:22 80.0-120 121291201811:22 75. 0-120 121291201811:22 80.0-120 121291201811:22 77. 0-126 1212912018 11:22 Batch WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 18 of 58 MW-21 SAMPLE RESULTS - 07 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 12:35 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acetone ND 50.0 1 12/29/201811:42 WG1216990 FTc Acrolein ND J4 50.0 1 12/29/201811:42 WG1216990 Acrylonitrile ND 10.0 1 12/29/201811:42 WG1216990 F Benzene ND 1.00 1 12/29/201811:42 WG1216990 Bromobenzene ND 1.00 1 12/29/201811:42 WG1216990 Bromodichloromethane ND 1.00 1 12/29/201811:42 WG1216990 4 Crl Bromoform ND 1.00 1 12/29/201811:42 WG1216990 Bromomethane ND 5.00 1 12/29/201811:42 WG1216990 n-Butylbenzene ND 1.00 1 12/29/201811:42 WG1216990 sec -Butyl benzene ND 1.00 1 12/29/201811:42 WG1216990 ter[-Butylbenzene ND 1.00 1 12/29/201811:42 WG1216990 Fc Carbon tetrachloride ND 1.00 1 12/29/201811:42 WG1216990 Chlorobenzene ND 1.00 1 12/29/201811:42 WG1216990 Fq Chlorodibromomethane ND 1.00 1 12/29/201811:42 WG1216990 Chloroethane ND 5.00 1 12/29/201811:42 WG1216990 Chloroform ND 5.00 1 12/29/201811:42 WG1216990 FAI Chloromethane ND 2.50 1 12/29/201811:42 WG1216990 2-Chlorotoluene ND 1.00 1 12/29/201811:42 WG1216990 F 4-Chlorotoluene ND 1.00 1 12/29/201811:42 WG1216990 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/29/201811:42 WG1216990 1,2-Dibromoethane ND 1.00 1 12/29/201811:42 WG1216990 Dibromomethane ND 1.00 1 12/29/201811:42 WG1216990 1,2-Dichlorobenzene ND 1.00 1 12/29/201811:42 WG1216990 1,3-Dichlorobenzene ND 1.00 1 12/29/201811:42 WG1216990 1,4-Dichlorobenzene ND 1.00 1 12/29/201811:42 WG1216990 Dichlorodifluoromethane ND 5.00 1 12/29/201811:42 WG1216990 1,1-Dichloroethane ND 1.00 1 12/29/201811:42 WG1216990 1,2-Dichloroethane ND 1.00 1 12/29/201811:42 WG1216990 1,1-Dichloroethene ND 1.00 1 12/29/201811:42 WG1216990 cis-1,2-Dichloroethene ND 1.00 1 12/29/201811:42 WG1216990 trans-1,2-Dichloroethene ND 1.00 1 12/29/201811:42 WG1216990 1,2-Dichloropropane ND 1.00 1 12/29/201811:42 WG1216990 1,1-Dichloropropene ND 1.00 1 12/29/201811:42 WG1216990 1,3-Dichloropropane ND 1.00 1 12/29/201811:42 WG1216990 2,2-Dichloropropane ND 1.00 1 12/29/201811:42 WG1216990 Di -isopropyl ether ND 1.00 1 12/29/201811:42 WG1216990 Ethylbenzene ND 1.00 1 12/29/201811:42 WG1216990 Hexachloro-1,3-butadiene ND 1.00 1 12/29/201811:42 WG1216990 Isopropylbenzene ND 1.00 1 12/29/201811:42 WG1216990 p-Isopropyltoluene ND 1.00 1 12/29/201811:42 WG1216990 2-Butanone (MEK) ND 10.0 1 12/29/201811:42 WG1216990 Methylene Chloride ND 5.00 1 12/29/201811:42 WG1216990 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/29/201811:42 WG1216990 Methyl tert-butyl ether ND 1.00 1 12/29/201811:42 WG1216990 Naphthalene ND 5.00 1 12/29/201811:42 WG1216990 n-Propylbenzene ND 1.00 1 12/29/201811:42 WG1216990 Styrene ND 1.00 1 12/29/201811:42 WG1216990 1,1,1,2-Tetrachloroethane ND 1.00 1 12/29/201811:42 WG1216990 1,1,2,2-Tetrachloroethane ND 1.00 1 12/29/201811:42 WG1216990 Tetrachloroethene ND 1.00 1 12/29/201811:42 WG1216990 Toluene ND 1.00 1 12/29/201811:42 WG1216990 1,2,3-Trichlorobenzene ND 1.00 1 12/29/201811:42 WG1216990 1,2,4-Trichlorobenzene ND 1.00 1 12/29/201811:42 WG1216990 1,1,1-Trichloroethane ND 1.00 1 12/29/201811:42 WG1216990 1,1,2-Trichloroethane ND 1.00 1 12/29/201811:42 WG1216990 Trichloroethene ND 1.00 1 12/29/201811:42 WG1216990 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 19 of 58 ONE LAB. NATIONWIDE. MW-21 SAMPLE RESULTS - 07 Collected date/time: 12/20/18 12:35 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 105 (S) Dibromofluoromethane 85.0 (S) a, a, a-Trifluoroto/uene 103 (S) 4-Bromof/uorobenzene 97.8 Qualifier RDL Dilution Analysis ug/I date / time 5.00 1 12/29/201811:42 2.50 1 12/29/201811:42 1.00 1 12/29/201811:42 1.00 1 12/29/201811:42 1.00 1 12/29/201811:42 1.00 1 12/29/201811:42 2.00 1 12/29/201811:42 80.0-120 121291201811.42 75. 0-120 121291201811.42 80.0-120 121291201811.42 77. 0-126 1212912018 11.42 Batch WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 20 of 58 MW-22 SAMPLE RESULTS - 08 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 12:30 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/29/201812:01 WG1216990 FTc Acrolein ND J4 50.0 1 12/29/201812:01 WG1216990 Acrylonitrile ND 10.0 1 12/29/201812:01 WG1216990 F Benzene ND 1.00 1 12/29/201812:01 WG1216990 Bromobenzene ND 1.00 1 12/29/201812:01 WG1216990 Bromodichloromethane ND 1.00 1 12/29/201812:01 WG1216990 4 Crl Bromoform ND 1.00 1 12/29/201812:01 WG1216990 Bromomethane ND 5.00 1 12/29/201812:01 WG1216990 n-Butylbenzene ND 1.00 1 12/29/201812:01 WG1216990 sec -Butyl benzene ND 1.00 1 12/29/201812:01 WG1216990 ter[-Butylbenzene ND 1.00 1 12/29/201812:01 WG1216990 Fc Carbon tetrachloride ND 1.00 1 12/29/201812:01 WG1216990 Chlorobenzene ND 1.00 1 12/29/201812:01 WG1216990 Fq Chlorodibromomethane ND 1.00 1 12/29/201812:01 WG1216990 Chloroethane ND 5.00 1 12/29/201812:01 WG1216990 Chloroform ND 5.00 1 12/29/201812:01 WG1216990 FAI Chloromethane ND 2.50 1 12/29/201812:01 WG1216990 2-Chlorotoluene ND 1.00 1 12/29/201812:01 WG1216990 F 4-Chlorotoluene ND 1.00 1 12/29/201812:01 WG1216990 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/29/201812:01 WG1216990 1,2-Dibromoethane ND 1.00 1 12/29/201812:01 WG1216990 Dibromomethane ND 1.00 1 12/29/201812:01 WG1216990 1,2-Dichlorobenzene ND 1.00 1 12/29/201812:01 WG1216990 1,3-Dichlorobenzene ND 1.00 1 12/29/201812:01 WG1216990 1,4-Dichlorobenzene ND 1.00 1 12/29/201812:01 WG1216990 Dichlorodifluoromethane ND 5.00 1 12/29/201812:01 WG1216990 1,1-Dichloroethane ND 1.00 1 12/29/201812:01 WG1216990 1,2-Dichloroethane ND 1.00 1 12/29/201812:01 WG1216990 1,1-Dichloroethene ND 1.00 1 12/29/201812:01 WG1216990 cis-1,2-Dichloroethene ND 1.00 1 12/29/201812:01 WG1216990 trans-1,2-Dichloroethene ND 1.00 1 12/29/201812:01 WG1216990 1,2-Dichloropropane ND 1.00 1 12/29/201812:01 WG1216990 1,1-Dichloropropene ND 1.00 1 12/29/201812:01 WG1216990 1,3-Dichloropropane ND 1.00 1 12/29/201812:01 WG1216990 2,2-Dichloropropane ND 1.00 1 12/29/201812:01 WG1216990 Di -isopropyl ether ND 1.00 1 12/29/201812:01 WG1216990 Ethylbenzene ND 1.00 1 12/29/201812:01 WG1216990 Hexachloro-1,3-butadiene ND 1.00 1 12/29/201812:01 WG1216990 Isopropylbenzene ND 1.00 1 12/29/201812:01 WG1216990 p-Isopropyltoluene ND 1.00 1 12/29/201812:01 WG1216990 2-Butanone (MEK) ND 10.0 1 12/29/201812:01 WG1216990 Methylene Chloride ND 5.00 1 12/29/201812:01 WG1216990 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/29/201812:01 WG1216990 Methyl tert-butyl ether ND 1.00 1 12/29/201812:01 WG1216990 Naphthalene ND 5.00 1 12/29/201812:01 WG1216990 n-Propylbenzene ND 1.00 1 12/29/201812:01 WG1216990 Styrene ND 1.00 1 12/29/201812:01 WG1216990 1,1,1,2-Tetrachloroethane ND 1.00 1 12/29/201812:01 WG1216990 1,1,2,2-Tetrachloroethane ND 1.00 1 12/29/201812:01 WG1216990 Tetrachloroethene ND 1.00 1 12/29/201812:01 WG1216990 Toluene ND 1.00 1 12/29/201812:01 WG1216990 1,2,3-Trichlorobenzene ND 1.00 1 12/29/201812:01 WG1216990 1,2,4-Trichlorobenzene ND 1.00 1 12/29/201812:01 WG1216990 1,1,1-Trichloroethane ND 1.00 1 12/29/201812:01 WG1216990 1,1,2-Trichloroethane ND 1.00 1 12/29/201812:01 WG1216990 Trichloroethene ND 1.00 1 12/29/201812:01 WG1216990 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 21 of 58 ONE LAB. NATIONWIDE. MW-22 SAMPLE RESULTS - 08 Collected date/time: 12/20/18 12:30 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 107 (S) Dibromofluoromethane 84.0 (S) a, a, a-Trifluoroto/uene 106 (S) 4-Bromof/uorobenzene 96.4 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/29/201812:01 2.50 1 12/29/201812:01 1.00 1 12/29/201812:01 1.00 1 12/29/201812:01 1.00 1 12/29/201812:01 1.00 1 12/29/201812:01 2.00 1 12/29/201812:01 80.0-120 1212912018 12:01 75. 0-120 1212912018 12:01 80.0-120 1212912018 12:01 77. 0-126 1212912018 12:01 Batch WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 22 of 58 MW-24 SAMPLE RESULTS - 09 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 12:05 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acetone ND 50.0 1 12/29/201812:21 WG1216990 FTc Acrolein ND J4 50.0 1 12/29/201812:21 WG1216990 Acrylonitrile ND 10.0 1 12/29/201812:21 WG1216990 F Benzene ND 1.00 1 12/29/201812:21 WG1216990 Bromobenzene ND 1.00 1 12/29/201812:21 WG1216990 Bromodichloromethane ND 1.00 1 12/29/201812:21 WG1216990 4 Crl Bromoform ND 1.00 1 12/29/201812:21 WG1216990 Bromomethane ND 5.00 1 12/29/201812:21 WG1216990 n-Butylbenzene ND 1.00 1 12/29/201812:21 WG1216990 sec -Butyl benzene ND 1.00 1 12/29/201812:21 WG1216990 ter[-Butylbenzene ND 1.00 1 12/29/201812:21 WG1216990 Fc Carbon tetrachloride ND 1.00 1 12/29/201812:21 WG1216990 Chlorobenzene ND 1.00 1 12/29/201812:21 WG1216990 Fq Chlorodibromomethane ND 1.00 1 12/29/201812:21 WG1216990 Chloroethane ND 5.00 1 12/29/201812:21 WG1216990 Chloroform ND 5.00 1 12/29/201812:21 WG1216990 FAI Chloromethane ND 2.50 1 12/29/201812:21 WG1216990 2-Chlorotoluene ND 1.00 1 12/29/201812:21 WG1216990 F 4-Chlorotoluene ND 1.00 1 12/29/201812:21 WG1216990 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/29/201812:21 WG1216990 1,2-Dibromoethane ND 1.00 1 12/29/201812:21 WG1216990 Dibromomethane ND 1.00 1 12/29/201812:21 WG1216990 1,2-Dichlorobenzene ND 1.00 1 12/29/201812:21 WG1216990 1,3-Dichlorobenzene ND 1.00 1 12/29/201812:21 WG1216990 1,4-Dichlorobenzene ND 1.00 1 12/29/201812:21 WG1216990 Dichlorodifluoromethane ND 5.00 1 12/29/201812:21 WG1216990 1,1-Dichloroethane ND 1.00 1 12/29/201812:21 WG1216990 1,2-Dichloroethane ND 1.00 1 12/29/201812:21 WG1216990 1,1-Dichloroethene ND 1.00 1 12/29/201812:21 WG1216990 cis-1,2-Dichloroethene ND 1.00 1 12/29/201812:21 WG1216990 trans-1,2-Dichloroethene ND 1.00 1 12/29/201812:21 WG1216990 1,2-Dichloropropane ND 1.00 1 12/29/201812:21 WG1216990 1,1-Dichloropropene ND 1.00 1 12/29/201812:21 WG1216990 1,3-Dichloropropane ND 1.00 1 12/29/201812:21 WG1216990 2,2-Dichloropropane ND 1.00 1 12/29/201812:21 WG1216990 Di -isopropyl ether ND 1.00 1 12/29/201812:21 WG1216990 Ethylbenzene ND 1.00 1 12/29/201812:21 WG1216990 Hexachloro-1,3-butadiene ND 1.00 1 12/29/201812:21 WG1216990 Isopropylbenzene ND 1.00 1 12/29/201812:21 WG1216990 p-Isopropyltoluene ND 1.00 1 12/29/201812:21 WG1216990 2-Butanone (MEK) ND 10.0 1 12/29/201812:21 WG1216990 Methylene Chloride ND 5.00 1 12/29/201812:21 WG1216990 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/29/201812:21 WG1216990 Methyl tert-butyl ether ND 1.00 1 12/29/201812:21 WG1216990 Naphthalene ND 5.00 1 12/29/201812:21 WG1216990 n-Propylbenzene ND 1.00 1 12/29/201812:21 WG1216990 Styrene ND 1.00 1 12/29/201812:21 WG1216990 1,1,1,2-Tetrachloroethane ND 1.00 1 12/29/201812:21 WG1216990 1,1,2,2-Tetrachloroethane ND 1.00 1 12/29/201812:21 WG1216990 Tetrachloroethene ND 1.00 1 12/29/201812:21 WG1216990 Toluene ND 1.00 1 12/29/201812:21 WG1216990 1,2,3-Trichlorobenzene ND 1.00 1 12/29/201812:21 WG1216990 1,2,4-Trichlorobenzene ND 1.00 1 12/29/201812:21 WG1216990 1,1,1-Trichloroethane ND 1.00 1 12/29/201812:21 WG1216990 1,1,2-Trichloroethane ND 1.00 1 12/29/201812:21 WG1216990 Trichloroethene ND 1.00 1 12/29/201812:21 WG1216990 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 23 of 58 ONE LAB. NATIONWIDE. MW-24 SAMPLE RESULTS - 09 Collected date/time: 12/20/18 12:05 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 104 (S) Dibromofluoromethane 86.3 (S) a, a, a-Trifluoroto/uene 103 (S) 4-Bromof/uorobenzene 94.8 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/29/201812:21 2.50 1 12/29/201812:21 1.00 1 12/29/201812:21 1.00 1 12/29/201812:21 1.00 1 12/29/201812:21 1.00 1 12/29/201812:21 2.00 1 12/29/201812:21 80.0-120 121291201812:21 75. 0-120 121291201812:21 80.0-120 121291201812:21 77. 0-126 1212912018 12:21 Batch WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 24 of 58 MW-25 SAMPLE RESULTS - 10 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 13:30 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Acetone ND 50.0 1 12/29/201812:41 WG1216990 FTc Acrolein ND J4 50.0 1 12/29/201812:41 WG1216990 Acrylonitrile ND 10.0 1 12/29/201812:41 WG1216990 F Benzene ND 1.00 1 12/29/201812:41 WG1216990 Bromobenzene ND 1.00 1 12/29/201812:41 WG1216990 Bromodichloromethane ND 1.00 1 12/29/201812:41 WG1216990 4 Crl Bromoform ND 1.00 1 12/29/201812:41 WG1216990 Bromomethane ND 5.00 1 12/29/201812:41 WG1216990 n-Butylbenzene ND 1.00 1 12/29/201812:41 WG1216990 sec -Butyl benzene ND 1.00 1 12/29/201812:41 WG1216990 ter[-Butylbenzene ND 1.00 1 12/29/201812:41 WG1216990 Fc Carbon tetrachloride ND 1.00 1 12/29/201812:41 WG1216990 Chlorobenzene ND 1.00 1 12/29/201812:41 WG1216990 Fq Chlorodibromomethane ND 1.00 1 12/29/201812:41 WG1216990 Chloroethane ND 5.00 1 12/29/201812:41 WG1216990 Chloroform ND 5.00 1 12/29/201812:41 WG1216990 FAI Chloromethane ND 2.50 1 12/29/201812:41 WG1216990 2-Chlorotoluene ND 1.00 1 12/29/201812:41 WG1216990 F 4-Chlorotoluene ND 1.00 1 12/29/201812:41 WG1216990 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/29/201812:41 WG1216990 1,2-Dibromoethane ND 1.00 1 12/29/201812:41 WG1216990 Dibromomethane ND 1.00 1 12/29/201812:41 WG1216990 1,2-Dichlorobenzene ND 1.00 1 12/29/201812:41 WG1216990 1,3-Dichlorobenzene ND 1.00 1 12/29/201812:41 WG1216990 1,4-Dichlorobenzene ND 1.00 1 12/29/201812:41 WG1216990 Dichlorodifluoromethane ND 5.00 1 12/29/201812:41 WG1216990 1,1-Dichloroethane ND 1.00 1 12/29/201812:41 WG1216990 1,2-Dichloroethane ND 1.00 1 12/29/201812:41 WG1216990 1,1-Dichloroethene ND 1.00 1 12/29/201812:41 WG1216990 cis-1,2-Dichloroethene ND 1.00 1 12/29/201812:41 WG1216990 trans-1,2-Dichloroethene ND 1.00 1 12/29/201812:41 WG1216990 1,2-Dichloropropane ND 1.00 1 12/29/201812:41 WG1216990 1,1-Dichloropropene ND 1.00 1 12/29/201812:41 WG1216990 1,3-Dichloropropane ND 1.00 1 12/29/201812:41 WG1216990 2,2-Dichloropropane ND 1.00 1 12/29/201812:41 WG1216990 Di -isopropyl ether ND 1.00 1 12/29/201812:41 WG1216990 Ethylbenzene ND 1.00 1 12/29/201812:41 WG1216990 Hexachloro-1,3-butadiene ND 1.00 1 12/29/201812:41 WG1216990 Isopropylbenzene ND 1.00 1 12/29/201812:41 WG1216990 p-Isopropyltoluene ND 1.00 1 12/29/201812:41 WG1216990 2-Butanone (MEK) ND 10.0 1 12/29/201812:41 WG1216990 Methylene Chloride ND 5.00 1 12/29/201812:41 WG1216990 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/29/201812:41 WG1216990 Methyl tert-butyl ether ND 1.00 1 12/29/201812:41 WG1216990 Naphthalene ND 5.00 1 12/29/201812:41 WG1216990 n-Propylbenzene ND 1.00 1 12/29/201812:41 WG1216990 Styrene ND 1.00 1 12/29/201812:41 WG1216990 1,1,1,2-Tetrachloroethane ND 1.00 1 12/29/201812:41 WG1216990 1,1,2,2-Tetrachloroethane ND 1.00 1 12/29/201812:41 WG1216990 Tetrachloroethene ND 1.00 1 12/29/201812:41 WG1216990 Toluene ND 1.00 1 12/29/201812:41 WG1216990 1,2,3-Trichlorobenzene ND 1.00 1 12/29/201812:41 WG1216990 1,2,4-Trichlorobenzene ND 1.00 1 12/29/201812:41 WG1216990 1,1,1-Trichloroethane ND 1.00 1 12/29/201812:41 WG1216990 1,1,2-Trichloroethane ND 1.00 1 12/29/201812:41 WG1216990 Trichloroethene ND 1.00 1 12/29/201812:41 WG1216990 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 25 of 58 ONE LAB. NATIONWIDE. MW-25 SAMPLE RESULTS - 10 Collected date/time: 12/20/18 13:30 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 106 (S) Dibromofluoromethane 87.6 (S) a, a, a-Trifluoroto/uene 103 (S) 4-Bromof/uorobenzene 95.6 Qualifier RDL Dilution Analysis ug/I date / time 5.00 1 12/29/201812:41 2.50 1 12/29/201812:41 1.00 1 12/29/201812:41 1.00 1 12/29/201812:41 1.00 1 12/29/201812:41 1.00 1 12/29/201812:41 2.00 1 12/29/201812:41 80.0-120 121291201812.41 75. 0-120 121291201812.41 80.0-120 121291201812.41 77. 0-126 1212912018 12.41 Batch WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 WG1216990 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 26 of 58 DMW-3 SAMPLE RESULTS - 11 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 12:15 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201812:53 WG1215938 FTc Acrolein ND 50.0 1 12/26/201812:53 WG1215938 Acrylonitrile ND 10.0 1 12/26/201812:53 WG1215938 F Benzene ND 1.00 1 12/26/201812:53 WG1215938 Bromobenzene ND 1.00 1 12/26/201812:53 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201812:53 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201812:53 WG1215938 Bromomethane ND 5.00 1 12/26/201812:53 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201812:53 WG1215938 sec -Butyl benzene ND 1.00 1 12/26/201812:53 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201812:53 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201812:53 WG1215938 Chlorobenzene ND 1.00 1 12/26/201812:53 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201812:53 WG1215938 Chloroethane ND 5.00 1 12/26/201812:53 WG1215938 Chloroform ND 5.00 1 12/26/201812:53 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201812:53 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201812:53 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201812:53 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201812:53 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201812:53 WG1215938 Dibromomethane ND 1.00 1 12/26/201812:53 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201812:53 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201812:53 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201812:53 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201812:53 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201812:53 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201812:53 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201812:53 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201812:53 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201812:53 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201812:53 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201812:53 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201812:53 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201812:53 WG1215938 Di -isopropyl ether ND 1.00 1 12/26/201812:53 WG1215938 Ethylbenzene ND 1.00 1 12/26/201812:53 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201812:53 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201812:53 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201812:53 WG1215938 2-Butanone (MEK) ND 10.0 1 12/26/201812:53 WG1215938 Methylene Chloride ND 5.00 1 12/26/201812:53 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201812:53 WG1215938 Methyl tert-butyl ether 46.5 1.00 1 12/26/201812:53 WG1215938 Naphthalene ND 5.00 1 12/26/201812:53 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201812:53 WG1215938 Styrene ND 1.00 1 12/26/201812:53 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201812:53 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201812:53 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201812:53 WG1215938 Toluene ND 1.00 1 12/26/201812:53 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201812:53 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201812:53 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201812:53 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201812:53 WG1215938 Trichloroethene ND 1.00 1 12/26/201812:53 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 27 of 58 ONE LAB. NATIONWIDE. DMW-3 SAMPLE RESULTS - 11 Collected date/time: 12/20/18 12:15 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 104 (S) Dibromofluoromethane 95.2 (S) a, a, a-Trifluoroto/uene 100 (S) 4-Bromof/uorobenzene 93.0 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/26/201812:53 2.50 1 12/26/201812:53 1.00 1 12/26/201812:53 1.00 1 12/26/201812:53 1.00 1 12/26/201812:53 1.00 1 12/26/201812:53 2.00 1 12/26/201812:53 80.0-120 121261201812:53 75. 0-120 1212612018 12:53 80.0-120 121261201812:53 77. 0-126 1212612018 12:53 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 28 of 58 M W-14 SAMPLE RESULTS - 12 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 13:10 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201813:13 WG1215938 FTc Acrolein ND 50.0 1 12/26/201813:13 WG1215938 Acrylonitrile ND 10.0 1 12/26/201813:13 WG1215938 F Benzene ND 1.00 1 12/26/201813:13 WG1215938 Bromobenzene ND 1.00 1 12/26/201813:13 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201813:13 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201813:13 WG1215938 Bromomethane ND 5.00 1 12/26/201813:13 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201813:13 WG1215938 sec -Butyl benzene ND 1.00 1 12/26/201813:13 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201813:13 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201813:13 WG1215938 Chlorobenzene ND 1.00 1 12/26/201813:13 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201813:13 WG1215938 Chloroethane ND 5.00 1 12/26/201813:13 WG1215938 Chloroform ND 5.00 1 12/26/201813:13 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201813:13 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201813:13 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201813:13 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201813:13 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201813:13 WG1215938 Dibromomethane ND 1.00 1 12/26/201813:13 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201813:13 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201813:13 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201813:13 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201813:13 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201813:13 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201813:13 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201813:13 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201813:13 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201813:13 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201813:13 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201813:13 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201813:13 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201813:13 WG1215938 Di -isopropyl ether ND 1.00 1 12/26/201813:13 WG1215938 Ethylbenzene ND 1.00 1 12/26/201813:13 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201813:13 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201813:13 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201813:13 WG1215938 2-Butanone (MEK) ND 10.0 1 12/26/201813:13 WG1215938 Methylene Chloride ND 5.00 1 12/26/201813:13 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201813:13 WG1215938 Methyl tert-butyl ether 29.6 1.00 1 12/26/201813:13 WG1215938 Naphthalene ND 5.00 1 12/26/201813:13 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201813:13 WG1215938 Styrene ND 1.00 1 12/26/201813:13 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201813:13 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201813:13 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201813:13 WG1215938 Toluene ND 1.00 1 12/26/201813:13 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201813:13 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201813:13 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201813:13 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201813:13 WG1215938 Trichloroethene ND 1.00 1 12/26/201813:13 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 29 of 58 ONE LAB. NATIONWIDE. MW-14 SAMPLE RESULTS - 12 Collected date/time: 12/20/18 13:10 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 106 (S) Dibromofluoromethane 99.3 (S) a, a, a-Trifluoroto/uene 97.9 (S) 4-Bromof/uorobenzene 96.3 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/26/201813:13 2.50 1 12/26/201813:13 1.00 1 12/26/201813:13 1.00 1 12/26/201813:13 1.00 1 12/26/201813:13 1.00 1 12/26/201813:13 2.00 1 12/26/201813:13 80.0-120 121261201813.13 75. 0-120 121261201813.13 80.0-120 121261201813.13 77. 0-126 121261201813.13 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 30 of 58 MW-9 SAMPLE RESULTS - 13 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 13:35 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201813:32 WG1215938 FTc Acrolein ND 50.0 1 12/26/201813:32 WG1215938 Acrylonitrile ND 10.0 1 12/26/201813:32 WG1215938 F Benzene ND 1.00 1 12/26/201813:32 WG1215938 Bromobenzene ND 1.00 1 12/26/201813:32 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201813:32 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201813:32 WG1215938 Bromomethane ND 5.00 1 12/26/201813:32 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201813:32 WG1215938 sec -Butyl benzene ND 1.00 1 12/26/201813:32 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201813:32 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201813:32 WG1215938 Chlorobenzene ND 1.00 1 12/26/201813:32 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201813:32 WG1215938 Chloroethane ND 5.00 1 12/26/201813:32 WG1215938 Chloroform ND 5.00 1 12/26/201813:32 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201813:32 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201813:32 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201813:32 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201813:32 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201813:32 WG1215938 Dibromomethane ND 1.00 1 12/26/201813:32 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201813:32 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201813:32 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201813:32 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201813:32 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201813:32 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201813:32 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201813:32 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201813:32 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201813:32 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201813:32 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201813:32 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201813:32 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201813:32 WG1215938 Di -isopropyl ether ND 1.00 1 12/26/201813:32 WG1215938 Ethylbenzene ND 1.00 1 12/26/201813:32 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201813:32 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201813:32 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201813:32 WG1215938 2-Butanone (MEK) ND 10.0 1 12/26/201813:32 WG1215938 Methylene Chloride ND 5.00 1 12/26/201813:32 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201813:32 WG1215938 Methyl tert-butyl ether ND 1.00 1 12/26/201813:32 WG1215938 Naphthalene ND 5.00 1 12/26/201813:32 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201813:32 WG1215938 Styrene ND 1.00 1 12/26/201813:32 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201813:32 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201813:32 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201813:32 WG1215938 Toluene ND 1.00 1 12/26/201813:32 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201813:32 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201813:32 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201813:32 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201813:32 WG1215938 Trichloroethene ND 1.00 1 12/26/201813:32 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 31 of 58 ONE LAB. NATIONWIDE. MW-9 SAMPLE RESULTS - 13 Collected date/time: 12/20/18 13:35 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 105 (S) Dibromofluoromethane 99.7 (S) a, a, a-Trifluoroto/uene 98.2 (S) 4-Bromof/uorobenzene 94.1 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/26/201813:32 2.50 1 12/26/201813:32 1.00 1 12/26/201813:32 1.00 1 12/26/201813:32 1.00 1 12/26/201813:32 1.00 1 12/26/201813:32 2.00 1 12/26/201813:32 80.0-120 12/26/20181332 75. 0-120 12126120181332 80.0-120 12/26/20181332 77. 0-126 12126120181332 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 32 of 58 M W-12 SAMPLE RESULTS - 14 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 13:20 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201813:52 WG1215938 FTc Acrolein ND 50.0 1 12/26/201813:52 WG1215938 Acrylonitrile ND 10.0 1 12/26/201813:52 WG1215938 F Benzene ND 1.00 1 12/26/201813:52 WG1215938 Bromobenzene ND 1.00 1 12/26/201813:52 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201813:52 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201813:52 WG1215938 Bromomethane ND 5.00 1 12/26/201813:52 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201813:52 WG1215938 sec -Butyl benzene ND 1.00 1 12/26/201813:52 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201813:52 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201813:52 WG1215938 Chlorobenzene ND 1.00 1 12/26/201813:52 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201813:52 WG1215938 Chloroethane ND 5.00 1 12/26/201813:52 WG1215938 Chloroform ND 5.00 1 12/26/201813:52 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201813:52 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201813:52 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201813:52 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201813:52 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201813:52 WG1215938 Dibromomethane ND 1.00 1 12/26/201813:52 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201813:52 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201813:52 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201813:52 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201813:52 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201813:52 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201813:52 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201813:52 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201813:52 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201813:52 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201813:52 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201813:52 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201813:52 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201813:52 WG1215938 Di -isopropyl ether ND 1.00 1 12/26/201813:52 WG1215938 Ethylbenzene ND 1.00 1 12/26/201813:52 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201813:52 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201813:52 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201813:52 WG1215938 2-Butanone (MEK) ND 10.0 1 12/26/201813:52 WG1215938 Methylene Chloride ND 5.00 1 12/26/201813:52 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201813:52 WG1215938 Methyl tert-butyl ether ND 1.00 1 12/26/201813:52 WG1215938 Naphthalene ND 5.00 1 12/26/201813:52 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201813:52 WG1215938 Styrene ND 1.00 1 12/26/201813:52 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201813:52 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201813:52 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201813:52 WG1215938 Toluene ND 1.00 1 12/26/201813:52 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201813:52 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201813:52 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201813:52 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201813:52 WG1215938 Trichloroethene ND 1.00 1 12/26/201813:52 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 33 of 58 ONE LAB. NATIONWIDE. MW-12 SAMPLE RESULTS - 14 Collected date/time: 12/20/18 13:20 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene 1.59 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 104 (S) Dibromofluoromethane 97.4 (S) a, a, a-Trifluoroto/uene 95.7 (S) 4-Bromof/uorobenzene 95.3 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/26/201813:52 2.50 1 12/26/201813:52 1.00 1 12/26/201813:52 1.00 1 12/26/201813:52 1.00 1 12/26/201813:52 1.00 1 12/26/201813:52 2.00 1 12/26/201813:52 80.0-120 121261201813.52 75. 0-120 121261201813.52 80.0-120 121261201813.52 77. 0-126 1212612018 13.-52 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 34 of 58 M W-17 SAMPLE RESULTS - 15 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 13:40 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201814:12 WG1215938 FTc Acrolein ND 50.0 1 12/26/201814:12 WG1215938 Acrylonitrile ND 10.0 1 12/26/201814:12 WG1215938 F Benzene ND 1.00 1 12/26/201814:12 WG1215938 Bromobenzene ND 1.00 1 12/26/201814:12 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201814:12 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201814:12 WG1215938 Bromomethane ND 5.00 1 12/26/201814:12 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201814:12 WG1215938 sec -Butyl benzene ND 1.00 1 12/26/201814:12 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201814:12 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201814:12 WG1215938 Chlorobenzene ND 1.00 1 12/26/201814:12 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201814:12 WG1215938 Chloroethane ND 5.00 1 12/26/201814:12 WG1215938 Chloroform ND 5.00 1 12/26/201814:12 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201814:12 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201814:12 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201814:12 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201814:12 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201814:12 WG1215938 Dibromomethane ND 1.00 1 12/26/201814:12 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201814:12 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201814:12 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201814:12 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201814:12 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201814:12 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201814:12 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201814:12 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201814:12 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201814:12 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201814:12 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201814:12 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201814:12 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201814:12 WG1215938 Di -isopropyl ether ND 1.00 1 12/26/201814:12 WG1215938 Ethylbenzene ND 1.00 1 12/26/201814:12 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201814:12 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201814:12 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201814:12 WG1215938 2-Butanone (MEK) ND 10.0 1 12/26/201814:12 WG1215938 Methylene Chloride ND 5.00 1 12/26/201814:12 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201814:12 WG1215938 Methyl tert-butyl ether 78.8 1.00 1 12/26/201814:12 WG1215938 Naphthalene ND 5.00 1 12/26/201814:12 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201814:12 WG1215938 Styrene ND 1.00 1 12/26/201814:12 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201814:12 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201814:12 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201814:12 WG1215938 Toluene ND 1.00 1 12/26/201814:12 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201814:12 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201814:12 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201814:12 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201814:12 WG1215938 Trichloroethene ND 1.00 1 12/26/201814:12 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 35 of 58 ONE LAB. NATIONWIDE. MW-17 SAMPLE RESULTS - 15 Collected date/time: 12/20/18 13:40 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 106 (S) Dibromofluoromethane 97.3 (S) a, a, a-Trifluoroto/uene 96.2 (S) 4-Bromof/uorobenzene 94.3 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/26/201814:12 2.50 1 12/26/201814:12 1.00 1 12/26/201814:12 1.00 1 12/26/201814:12 1.00 1 12/26/201814:12 1.00 1 12/26/201814:12 2.00 1 12/26/201814:12 80.0-120 121261201814:12 75. 0-120 121261201814:12 80.0-120 121261201814:12 77. 0-126 121261201814:12 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 36 of 58 MW-20 SAMPLE RESULTS - 16 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 12:55 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201814:32 WG1215938 FTc Acrolein ND 50.0 1 12/26/201814:32 WG1215938 Acrylonitrile ND 10.0 1 12/26/201814:32 WG1215938 F Benzene ND 1.00 1 12/26/201814:32 WG1215938 Bromobenzene ND 1.00 1 12/26/201814:32 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201814:32 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201814:32 WG1215938 Bromomethane ND 5.00 1 12/26/201814:32 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201814:32 WG1215938 sec -Butyl benzene ND 1.00 1 12/26/201814:32 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201814:32 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201814:32 WG1215938 Chlorobenzene ND 1.00 1 12/26/201814:32 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201814:32 WG1215938 Chloroethane ND 5.00 1 12/26/201814:32 WG1215938 Chloroform ND 5.00 1 12/26/201814:32 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201814:32 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201814:32 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201814:32 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201814:32 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201814:32 WG1215938 Dibromomethane ND 1.00 1 12/26/201814:32 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201814:32 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201814:32 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201814:32 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201814:32 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201814:32 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201814:32 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201814:32 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201814:32 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201814:32 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201814:32 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201814:32 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201814:32 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201814:32 WG1215938 Di -isopropyl ether 1.58 1.00 1 12/26/201814:32 WG1215938 Ethylbenzene ND 1.00 1 12/26/201814:32 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201814:32 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201814:32 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201814:32 WG1215938 2-Butanone (MEK) ND 10.0 1 12/26/201814:32 WG1215938 Methylene Chloride ND 5.00 1 12/26/201814:32 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201814:32 WG1215938 Methyl tert-butyl ether 4.02 1.00 1 12/26/201814:32 WG1215938 Naphthalene ND 5.00 1 12/26/201814:32 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201814:32 WG1215938 Styrene ND 1.00 1 12/26/201814:32 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201814:32 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201814:32 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201814:32 WG1215938 Toluene ND 1.00 1 12/26/201814:32 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201814:32 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201814:32 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201814:32 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201814:32 WG1215938 Trichloroethene ND 1.00 1 12/26/201814:32 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 37 of 58 ONE LAB. NATIONWIDE. MW-20 SAMPLE RESULTS - 16 Collected date/time: 12/20/18 12:55 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 106 (S) Dibromofluoromethane 97.3 (S) a, a, a-Trifluoroto/uene 96.8 (S) 4-Bromof/uorobenzene 95.1 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/26/201814:32 2.50 1 12/26/201814:32 1.00 1 12/26/201814:32 1.00 1 12/26/201814:32 1.00 1 12/26/201814:32 1.00 1 12/26/201814:32 2.00 1 12/26/201814:32 80.0-120 12126120181432 75. 0-120 12126120181432 80.0-120 12126120181432 77. 0-126 12126120181432 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 38 of 58 MW-23 SAMPLE RESULTS - 17 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 12:00 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201814:52 WG1215938 FTc Acrolein ND 50.0 1 12/26/201814:52 WG1215938 Acrylonitrile ND 10.0 1 12/26/201814:52 WG1215938 F Benzene ND 1.00 1 12/26/201814:52 WG1215938 Bromobenzene ND 1.00 1 12/26/201814:52 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201814:52 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201814:52 WG1215938 Bromomethane ND 5.00 1 12/26/201814:52 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201814:52 WG1215938 sec -Butyl benzene 1.37 V3 1.00 1 12/26/201814:52 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201814:52 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201814:52 WG1215938 Chlorobenzene ND 1.00 1 12/26/201814:52 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201814:52 WG1215938 Chloroethane ND 5.00 1 12/26/201814:52 WG1215938 Chloroform ND 5.00 1 12/26/201814:52 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201814:52 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201814:52 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201814:52 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201814:52 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201814:52 WG1215938 Dibromomethane ND 1.00 1 12/26/201814:52 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201814:52 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201814:52 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201814:52 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201814:52 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201814:52 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201814:52 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201814:52 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201814:52 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201814:52 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201814:52 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201814:52 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201814:52 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201814:52 WG1215938 Di -isopropyl ether ND 1.00 1 12/26/201814:52 WG1215938 Ethylbenzene ND 1.00 1 12/26/201814:52 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201814:52 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201814:52 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201814:52 WG1215938 2-Butanone (MEK) ND 10.0 1 12/26/201814:52 WG1215938 Methylene Chloride ND 5.00 1 12/26/201814:52 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201814:52 WG1215938 Methyl tert-butyl ether ND 1.00 1 12/26/201814:52 WG1215938 Naphthalene ND 5.00 1 12/26/201814:52 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201814:52 WG1215938 Styrene ND 1.00 1 12/26/201814:52 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201814:52 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201814:52 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201814:52 WG1215938 Toluene ND 1.00 1 12/26/201814:52 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201814:52 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201814:52 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201814:52 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201814:52 WG1215938 Trichloroethene ND 1.00 1 12/26/201814:52 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 39 of 58 ONE LAB. NATIONWIDE. MW-23 SAMPLE RESULTS - 17 Collected date/time: 12/20/18 12:00 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Analyte Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Tri methyl ben zen e 1,3,5-Trim ethyl benzene Vinyl chloride o-Xylene m&p-Xylenes (S) Toluene-d8 (S) Dibromofluoromethane (S) a, a, a-Trifluoroto/uene (S) 4-Bromof/uorobenzene Result Qualifier RDL Dilution Analysis ug/I ug/I date / time ND 5.00 1 12/26/201814:52 ND 2.50 1 12/26/201814:52 6.88 V3 1.00 1 12/26/201814:52 ND 1.00 1 12/26/201814:52 ND 1.00 1 12/26/201814:52 1.57 1.00 1 12/26/201814:52 ND 2.00 1 12/26/201814:52 101 80.0-120 121261201814:52 103 75.0-120 121261201814:52 99.4 80.0-120 121261201814:52 98.0 77.0-126 121261201814:52 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 40 of 58 M W-11 SAMPLE RESULTS - 18 ONE LAB. NATIONWIDE. Collected date/time: 12/20/18 12:40 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 FP1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 12/26/201815:12 WG1215938 FTc Acrolein ND 50.0 1 12/26/201815:12 WG1215938 Acrylonitrile ND 10.0 1 12/26/201815:12 WG1215938 F Benzene ND 1.00 1 12/26/201815:12 WG1215938 Bromobenzene ND 1.00 1 12/26/201815:12 WG1215938 Bromodichloromethane ND 1.00 1 12/26/201815:12 WG1215938 4 Crl Bromoform ND 1.00 1 12/26/201815:12 WG1215938 Bromomethane ND 5.00 1 12/26/201815:12 WG1215938 n-Butylbenzene ND 1.00 1 12/26/201815:12 WG1215938 sec -Butyl benzene ND 1.00 1 12/26/201815:12 WG1215938 ter[-Butylbenzene ND 1.00 1 12/26/201815:12 WG1215938 Fc Carbon tetrachloride ND 1.00 1 12/26/201815:12 WG1215938 Chlorobenzene ND 1.00 1 12/26/201815:12 WG1215938 Fq Chlorodibromomethane ND 1.00 1 12/26/201815:12 WG1215938 Chloroethane ND 5.00 1 12/26/201815:12 WG1215938 Chloroform ND 5.00 1 12/26/201815:12 WG1215938 FAI Chloromethane ND 2.50 1 12/26/201815:12 WG1215938 2-Chlorotoluene ND 1.00 1 12/26/201815:12 WG1215938 F 4-Chlorotoluene ND 1.00 1 12/26/201815:12 WG1215938 1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/201815:12 WG1215938 1,2-Dibromoethane ND 1.00 1 12/26/201815:12 WG1215938 Dibromomethane ND 1.00 1 12/26/201815:12 WG1215938 1,2-Dichlorobenzene ND 1.00 1 12/26/201815:12 WG1215938 1,3-Dichlorobenzene ND 1.00 1 12/26/201815:12 WG1215938 1,4-Dichlorobenzene ND 1.00 1 12/26/201815:12 WG1215938 Dichlorodifluoromethane ND 5.00 1 12/26/201815:12 WG1215938 1,1-Dichloroethane ND 1.00 1 12/26/201815:12 WG1215938 1,2-Dichloroethane ND 1.00 1 12/26/201815:12 WG1215938 1,1-Dichloroethene ND 1.00 1 12/26/201815:12 WG1215938 cis-1,2-Dichloroethene ND 1.00 1 12/26/201815:12 WG1215938 trans-1,2-Dichloroethene ND 1.00 1 12/26/201815:12 WG1215938 1,2-Dichloropropane ND 1.00 1 12/26/201815:12 WG1215938 1,1-Dichloropropene ND 1.00 1 12/26/201815:12 WG1215938 1,3-Dichloropropane ND 1.00 1 12/26/201815:12 WG1215938 2,2-Dichloropropane ND 1.00 1 12/26/201815:12 WG1215938 Di -isopropyl ether ND 1.00 1 12/26/201815:12 WG1215938 Ethylbenzene ND 1.00 1 12/26/201815:12 WG1215938 Hexachloro-1,3-butadiene ND 1.00 1 12/26/201815:12 WG1215938 Isopropylbenzene ND 1.00 1 12/26/201815:12 WG1215938 p-Isopropyltoluene ND 1.00 1 12/26/201815:12 WG1215938 2-Butanone (MEK) 18.5 10.0 1 12/26/201815:12 WG1215938 Methylene Chloride ND 5.00 1 12/26/201815:12 WG1215938 4-Methyl-2-pentanone (MIBK) ND 10.0 1 12/26/201815:12 WG1215938 Methyl tert-butyl ether ND 1.00 1 12/26/201815:12 WG1215938 Naphthalene ND 5.00 1 12/26/201815:12 WG1215938 n-Propylbenzene ND 1.00 1 12/26/201815:12 WG1215938 Styrene ND 1.00 1 12/26/201815:12 WG1215938 1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/201815:12 WG1215938 1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/201815:12 WG1215938 Tetrachloroethene ND 1.00 1 12/26/201815:12 WG1215938 Toluene ND 1.00 1 12/26/201815:12 WG1215938 1,2,3-Trichlorobenzene ND 1.00 1 12/26/201815:12 WG1215938 1,2,4-Trichlorobenzene ND 1.00 1 12/26/201815:12 WG1215938 1,1,1-Trichloroethane ND 1.00 1 12/26/201815:12 WG1215938 1,1,2-Trichloroethane ND 1.00 1 12/26/201815:12 WG1215938 Trichloroethene ND 1.00 1 12/26/201815:12 WG1215938 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 41 of 58 ONE LAB. NATIONWIDE. MW-11 SAMPLE RESULTS - 18 Collected date/time: 12/20/18 12:40 L1055594 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Analyte ug/I Trichlorofluoromethane ND 1,2,3-Trichloropropane ND 1,2,4-Trimethyl ben zene ND 1,3,5-Trimethyl benzene ND Vinyl chloride ND o-Xylene ND m&p-Xylenes ND (S) Toluene-d8 103 (S) Dibromofluoromethane 97.5 (S) a, a, a-Trifluoroto/uene 97.1 (S) 4-Bromof/uorobenzene 95.9 Qualifier RDL ug/I Dilution Analysis date / time 5.00 1 12/26/201815:12 2.50 1 12/26/201815:12 1.00 1 12/26/201815:12 1.00 1 12/26/201815:12 1.00 1 12/26/201815:12 1.00 1 12/26/201815:12 2.00 1 12/26/201815:12 80.0-120 121261201815:12 75. 0-120 121261201815:12 80.0-120 121261201815:12 77. 0-126 121261201815:12 Batch WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 WG1215938 Fp FTc FS Fn N Fc F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 42 of 58 WG1215013 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 620OB-1997 1-1055594-01,02,03,04,05 Method Blank (MB) FP1(MB) R3371684-3 12/22/18 10:22 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I z TC Acetone U 10.0 50.0 Acrolein U 8.87 50.0 FSS Acrylonitrile U 1.87 10.0 Benzene U 0.331 1.00 Bromobenzene U 0.352 1.00 [Cn] Bromodichloromethane U 0.380 1.00 Bromoform U 0.469 1.00 FSr Bromomethane U 0.866 5.00 n-Butylbenzene U 0.361 1.00 sec -Butyl benzene U 0.365 1.00 tert-Butylbenzene U 0.399 1.00 Carbon tetrachloride U 0.379 1.00 GI Chlorobenzene U 0.348 1.00 Chlorodibromomethane U 0.327 1.00 Chloroethane U 0.453 5.00 FAI Chloroform U 0.324 5.00 Chloromethane U 0.276 2.50 FSC 2-Chlorotoluene U 0.375 1.00 4-Chlorotoluene U 0.351 1.00 1,2-Dibromo-3-Chloropropane U 1.33 5.00 1,2-Dibromoethane U 0.381 1.00 Dibromomethane U 0.346 1.00 1,2-Dichlorobenzene U 0.349 1.00 1,3-Dichlorobenzene U 0.220 1.00 1,4-Dichlorobenzene U 0.274 1.00 Dichlorodifluoromethane U 0.551 5.00 1,1-Dichloroethane U 0.259 1.00 1,2-Dichloroethane U 0.361 1.00 1,1-Dichloroethene U 0.398 1.00 cis-1,2-Dichloroethene U 0.260 1.00 trans-1,2-Dichloroethene U 0.396 1.00 1,2-Dichloropropane U 0.306 1.00 1,1-Dichloropropene U 0.352 1.00 1,3-Dichloropropane U 0.366 1.00 2,2-Dichloropropane U 0.321 1.00 Di -isopropyl ether U 0.320 1.00 Ethylbenzene U 0.384 1.00 Hexachloro-1,3-butadiene U 0.256 1.00 Isopropylbenzene U 0.326 1.00 p-Isopropyltoluene U 0.350 1.00 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 43 of 58 WG1215013 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 620OB-1997 1-1055594-01,02,03,04,05 Method Blank (MB) (MB) R3371684-3 12/22/18 10:22 MB Result Analyte ug/I 2-Butanone (MEK) U Methylene Chloride U 4-Methyl-2-pentanone (MIBK) U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,2,3-Trichlorobenzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl chloride U o-Xylene U m&p-Xylenes U (S) Toluene-d8 102 (S) Dibromofluoromethane 102 (S) a, a,o-Trifluoroto/uene 101 (S) 4-Bromof/uorobenzene 104 MB Qualifier MB MDL MB RDL ug/I ug/I 3.93 10.0 1.00 5.00 2.14 10.0 0.367 1.00 1.00 5.00 0.349 1.00 0.307 1.00 0.385 1.00 0.130 1.00 0.372 1.00 0.412 1.00 0.230 1.00 0.355 1.00 0.319 1.00 0.383 1.00 0.398 1.00 1.20 5.00 0.807 2.50 0.373 1.00 0.387 1.00 0.259 1.00 0.341 1.00 0.719 2.00 80.0-120 75.0-120 80.0-120 77.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3371684-1 12/22/18 09:04 • (LCSD) R3371684-2 12/22/18 09:23 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Acetone 125 106 107 Acrolein 125 95.7 98.0 Acrylonitrile 125 121 121 Benzene 25.0 23.8 24.3 Bromobenzene 25.0 26.5 27.0 Bromodichloromethane 25.0 23.7 23.7 ACCOUNT: Apex Environmental Inc. - Roanke Va LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 85.2 85.7 19.0-160 0.679 27 76.5 78.4 10.0-160 2.39 26 96.5 96.8 55.0-149 0.244 20 95.0 97.3 70.0-123 2.36 20 106 108 73.0-121 1.96 20 94.7 95.0 75.0-120 0.319 20 PROJECT: SDG: DATE/TIME: PAGE: 768490-030 L1055594 01/02/19 09:23 44 of 58 FP1 FTc FSS 4 Cn FSr �GI FAI [Sc WG1215013 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-01,02,03,04,05 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3371684-1 12/22/18 09:04 • (LCSD) R3371684-2 12/22/18 09:23 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Bromoform 25.0 27.1 26.5 Bromomethane 25.0 25.7 27.7 n-Butylbenzene 25.0 22.6 22.8 sec -Butyl benzene 25.0 24.6 24.7 tert-Butylbenzene 25.0 24.1 24.8 Carbon tetrachloride 25.0 22.1 22.6 Chlorobenzene 25.0 23.1 24.1 Chlorodibromomethane 25.0 23.5 23.0 Chloroethane 25.0 25.2 27.2 Chloroform 25.0 24.1 25.2 Chloromethane 25.0 23.2 25.2 2-Chlorotoluene 25.0 24.9 25.2 4-Chlorotoluene 25.0 25.8 25.6 1,2-Dibromo-3-Chloropropane 25.0 23.5 22.5 1,2-Dibromoethane 25.0 23.1 23.7 Dibromomethane 25.0 24.3 25.1 1,2-Dichlorobenzene 25.0 23.6 23.4 1,3-Dichlorobenzene 25.0 24.4 23.7 1,4-Dichlorobenzene 25.0 23.7 24.8 Dichlorodifluoromethane 25.0 29.0 31.5 1,1-Dichloroethane 25.0 24.4 26.1 1,2-Dichloroethane 25.0 24.6 25.1 1,1-Dichloroethene 25.0 24.7 25.6 cis-1,2-Dichloroethene 25.0 24.5 25.2 trans-1,2-Dichloroethene 25.0 24.0 24.4 1,2-Dichloropropane 25.0 26.2 25.4 1,1-Dichloropropene 25.0 25.4 25.6 1,3-Dichloropropane 25.0 24.7 25.4 2,2-Dichloropropane 25.0 21.8 23.8 Di -isopropyl ether 25.0 22.4 23.2 Ethylbenzene 25.0 23.1 23.5 Hexachloro-1,3-butadiene 25.0 19.6 20.7 Isopropylbenzene 25.0 26.7 26.6 p-Isopropyltoluene 25.0 23.3 23.5 2-Butanone (MEK) 125 118 120 Methylene Chloride 25.0 22.8 23.6 4-Methyl-2-pentanone (MIBK) 125 113 113 Methyl tert-butyl ether 25.0 24.0 25.4 Naphthalene 25.0 20.1 19.5 n-Propylbenzene 25.0 26.2 25.8 ACCOUNT: Apex Environmental Inc. - Roanke Va LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 108 106 68.0-132 2.16 20 103 111 10.0-160 7.28 25 90.6 91.0 73.0-125 0.492 20 98.4 98.7 75.0-125 0.331 20 96.4 99.3 76.0-124 2.97 20 88.6 90.4 68.0-126 2.05 20 92.4 96.2 80.0-121 3.99 20 93.8 92.2 77.0-125 1.80 20 101 109 47.0-150 7.67 20 96.4 101 73.0-120 4.59 20 92.8 101 41.0-142 8.38 20 99.7 101 76.0-123 1.17 20 103 102 75.0-122 0.632 20 93.9 89.8 58.0-134 4.40 20 92.3 94.6 80.0-122 2.53 20 97.3 100 80.0-120 3.17 20 94.3 93.7 79.0-121 0.646 20 97.4 94.9 79.0-120 2.67 20 94.6 99.4 79.0-120 4.88 20 116 126 51.0-149 8.22 20 97.5 104 70.0-126 6.62 20 98.3 100 70.0-128 2.14 20 98.8 102 71.0-124 3.36 20 98.0 101 73.0-120 2.89 20 96.0 97.8 73.0-120 1.80 20 105 101 77.0-125 3.12 20 102 102 74.0-126 0.502 20 98.7 101 80.0-120 2.77 20 87.1 95.2 58.0-130 8.88 20 89.7 92.6 58.0-138 3.26 20 92.3 93.9 79.0-123 1.70 20 78.5 82.9 54.0-138 5.35 20 107 106 76.0-127 0.722 20 93.3 94.1 76.0-125 0.845 20 94.2 95.7 44.0-160 1.58 20 91.4 94.2 67.0-120 3.05 20 90.4 90.4 68.0-142 0.0538 20 95.9 101 68.0-125 5.64 20 80.3 77.9 54.0-135 3.06 20 105 103 77.0-124 1.29 20 PROJECT: SDG: DATE/TIME: PAGE: 768490-030 L1055594 01/02/19 09:23 45 of 58 FP1 FTC FSS [Cn] FSr �GI FAI FSC WG1215013 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-01,02,03,04,05 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3371684-1 12/22/18 09:04 • (LCSD) R3371684-2 12/22/18 09:23 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % Styrene 25.0 27.4 27.1 109 108 73.0-130 0.972 20 1,1,1,2-Tetrachloroethane 25.0 22.0 22.8 88.1 91.2 75.0-125 3.48 20 1,1,2,2-Tetrachloroethane 25.0 25.0 25.1 99.9 100 65.0-130 0.512 20 Tetrachloroethene 25.0 21.8 22.9 87.1 91.6 72.0-132 5.06 20 Toluene 25.0 23.7 24.4 94.9 97.6 79.0-120 2.85 20 1,2,3-Trichlorobenzene 25.0 18.5 17.6 74.1 70.5 50.0-138 4.87 20 1,2,4-Trichlorobenzene 25.0 18.7 18.0 74.9 71.8 57.0-137 4.27 20 1,1,1-Trichloroethane 25.0 24.2 25.1 96.9 101 73.0-124 3.66 20 1,1,2-Trichloroethane 25.0 24.2 24.6 97.0 98.2 80.0-120 1.25 20 Trichloroethene 25.0 25.1 24.8 101 99.2 78.0-124 1.42 20 Trichlorofluoromethane 25.0 25.8 26.7 103 107 59.0-147 3.31 20 1,2,3-Trichloropropane 25.0 25.1 24.0 100 95.9 73.0-130 4.62 20 1,2,4-Trimethylbenzene 25.0 24.5 24.5 98.0 98.2 76.0-121 0.155 20 1,3,5-Trimethyl benzene 25.0 24.5 25.2 98.1 101 76.0-122 2.87 20 Vinyl chloride 25.0 26.2 28.5 105 114 67.0-131 8.43 20 o-Xylene 25.0 21.1 21.8 84.5 87.2 80.0-122 3.07 20 m&p-Xylenes 50.0 42.6 43.3 85.2 86.6 80.0-122 1.69 20 (S) Toluene-d8 103 104 80.0-120 (S) Dibromofluoromethane 98.6 101 75.0-120 (S) a, a, a-Trifluoroto/uene 98.1 97.4 80.0-120 (S) 4-Bromof/uorobenzene 112 112 77.0-126 ONE LAB. NATIONWIDE. FP1 FTC FSS 4 Cn FSr �GI FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 46 of 58 WG1215938 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-11,12,13,14,15,16,17,18 Method Blank (MB) FP1(MB) R3372064-3 12/26/1811:26 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I z TC Acetone U 10.0 50.0 Acrolein U 8.87 50.0 FSS Acrylonitrile U 1.87 10.0 Benzene U 0.331 1.00 Bromobenzene U 0.352 1.00 [Cn] Bromodichloromethane U 0.380 1.00 Bromoform U 0.469 1.00 FSr Bromomethane U 0.866 5.00 n-Butylbenzene U 0.361 1.00 sec -Butyl benzene U 0.365 1.00 tert-Butylbenzene U 0.399 1.00 Carbon tetrachloride U 0.379 1.00 GI Chlorobenzene U 0.348 1.00 Chlorodibromomethane U 0.327 1.00 Chloroethane U 0.453 5.00 FAI Chloroform U 0.324 5.00 Chloromethane U 0.276 2.50 FSC 2-Chlorotoluene U 0.375 1.00 4-Chlorotoluene U 0.351 1.00 1,2-Dibromo-3-Chloropropane U 1.33 5.00 1,2-Dibromoethane U 0.381 1.00 Dibromomethane U 0.346 1.00 1,2-Dichlorobenzene U 0.349 1.00 1,3-Dichlorobenzene U 0.220 1.00 1,4-Dichlorobenzene U 0.274 1.00 Dichlorodifluoromethane U 0.551 5.00 1,1-Dichloroethane U 0.259 1.00 1,2-Dichloroethane U 0.361 1.00 1,1-Dichloroethene U 0.398 1.00 cis-1,2-Dichloroethene U 0.260 1.00 trans-1,2-Dichloroethene U 0.396 1.00 1,2-Dichloropropane U 0.306 1.00 1,1-Dichloropropene U 0.352 1.00 1,3-Dichloropropane U 0.366 1.00 2,2-Dichloropropane U 0.321 1.00 Di -isopropyl ether U 0.320 1.00 Ethylbenzene U 0.384 1.00 Hexachloro-1,3-butadiene U 0.256 1.00 Isopropylbenzene U 0.326 1.00 p-Isopropyltoluene U 0.350 1.00 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 47 of 58 WG1215938 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-11,12,13,14,15,16,17,18 Method Blank (MB) (MB) R3372064-3 12/26/1811:26 MB Result Analyte ug/I 2-Butanone (MEK) U Methylene Chloride U 4-Methyl-2-pentanone (MIBK) U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,2,3-Trichlorobenzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl chloride U o-Xylene U m&p-Xylenes U (S) Toluene-d8 105 (S) Dibromofluoromethane 96.2 (S) a, a,o-Trifluoroto/uene 99.2 (S) 4-Bromof/uorobenzene 94.5 MB Qualifier MB MDL MB RDL ug/I ug/I 3.93 10.0 1.00 5.00 2.14 10.0 0.367 1.00 1.00 5.00 0.349 1.00 0.307 1.00 0.385 1.00 0.130 1.00 0.372 1.00 0.412 1.00 0.230 1.00 0.355 1.00 0.319 1.00 0.383 1.00 0.398 1.00 1.20 5.00 0.807 2.50 0.373 1.00 0.387 1.00 0.259 1.00 0.341 1.00 0.719 2.00 80.0-120 75.0-120 80.0-120 77.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3372064-1 12/26/1810:26 • (LCSD) R3372064-2 12/26/18 10:46 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Acetone 125 100 95.0 Acrolein 125 ill 121 Acrylonitrile 125 112 109 Benzene 25.0 22.8 23.3 Bromobenzene 25.0 22.1 22.9 Bromodichloromethane 25.0 20.8 21.0 ACCOUNT: Apex Environmental Inc. - Roanke Va LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 80.2 76.0 19.0-160 5.37 27 88.5 97.0 10.0-160 9.14 26 89.7 87.6 55.0-149 2.42 20 91.2 93.4 70.0-123 2.36 20 88.2 91.4 73.0-121 3.57 20 83.2 83.8 75.0-120 0.698 20 PROJECT: SDG: DATE/TIME: PAGE: 768490-030 L1055594 01/02/19 09:23 48 of 58 FP1 FTc FSS 4 Cn FSr �GI FAI [Sc WG1215938 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-11,12,13,14,15,16,17,18 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3372064-1 12/26/1810:26 • (LCSD) R3372064-2 12/26/18 10:46 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Bromoform 25.0 23.3 23.4 Bromomethane 25.0 26.9 25.9 n-Butylbenzene 25.0 24.4 24.9 sec -Butyl benzene 25.0 24.8 25.1 tert-Butylbenzene 25.0 23.6 24.7 Carbon tetrachloride 25.0 22.4 22.3 Chlorobenzene 25.0 25.1 25.7 Chlorodibromomethane 25.0 23.8 24.0 Chloroethane 25.0 25.4 26.2 Chloroform 25.0 22.4 22.3 Chloromethane 25.0 24.6 24.9 2-Chlorotoluene 25.0 24.7 24.8 4-Chlorotoluene 25.0 24.7 25.0 1,2-Dibromo-3-Chloropropane 25.0 20.3 20.8 1,2-Dibromoethane 25.0 24.1 25.2 Dibromomethane 25.0 21.5 21.9 1,2-Dichlorobenzene 25.0 23.2 23.4 1,3-Dichlorobenzene 25.0 23.9 24.5 1,4-Dichlorobenzene 25.0 25.5 25.3 Dichlorodifluoromethane 25.0 27.1 27.8 1,1-Dichloroethane 25.0 22.9 23.0 1,2-Dichloroethane 25.0 22.2 23.0 1,1-Dichloroethene 25.0 23.4 22.8 cis-1,2-Dichloroethene 25.0 22.2 22.3 trans-1,2-Dichloroethene 25.0 23.3 22.9 1,2-Dichloropropane 25.0 24.2 24.4 1,1-Dichloropropene 25.0 23.6 23.3 1,3-Dichloropropane 25.0 25.2 25.8 2,2-Dichloropropane 25.0 22.3 22.3 Di -isopropyl ether 25.0 22.7 22.4 Ethylbenzene 25.0 24.5 24.4 Hexachloro-1,3-butadiene 25.0 18.9 19.2 Isopropylbenzene 25.0 24.1 24.3 p-Isopropyltoluene 25.0 24.0 24.7 2-Butanone(MEK) 125 105 101 Methylene Chloride 25.0 23.0 23.1 4-Methyl-2-pentanone (MIBK) 125 115 116 Methyl tert-butyl ether 25.0 23.7 23.5 Naphthalene 25.0 17.6 17.7 n-Propylbenzene 25.0 22.8 23.3 ACCOUNT: Apex Environmental Inc. - Roanke Va LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 93.1 93.8 68.0-132 0.692 20 107 104 10.0-160 3.55 25 97.5 99.5 73.0-125 2.00 20 99.3 100 75.0-125 0.966 20 94.4 98.6 76.0-124 4.37 20 89.4 89.2 68.0-126 0.257 20 100 103 80.0-121 2.16 20 95.1 96.0 77.0-125 0.892 20 102 105 47.0-150 3.17 20 89.7 89.2 73.0-120 0.528 20 98.6 99.4 41.0-142 0.817 20 98.6 99.1 76.0-123 0.502 20 98.9 99.8 75.0-122 0.949 20 81.2 83.3 58.0-134 2.48 20 96.4 101 80.0-122 4.60 20 86.2 87.8 80.0-120 1.83 20 92.8 93.7 79.0-121 1.00 20 95.5 98.0 79.0-120 2.57 20 102 101 79.0-120 0.785 20 108 111 51.0-149 2.44 20 91.7 92.0 70.0-126 0.346 20 88.8 91.9 70.0-128 3.39 20 93.4 91.4 71.0-124 2.26 20 88.8 89.0 73.0-120 0.227 20 93.3 91.7 73.0-120 1.70 20 96.8 97.7 77.0-125 0.873 20 94.2 93.3 74.0-126 1.03 20 101 103 80.0-120 2.57 20 89.4 89.4 58.0-130 0.00157 20 90.7 89.6 58.0-138 1.16 20 98.0 97.5 79.0-123 0.437 20 75.8 76.9 54.0-138 1.55 20 96.3 97.1 76.0-127 0.805 20 96.2 98.6 76.0-125 2.54 20 83.8 80.8 44.0-160 3.61 20 92.2 92.2 67.0-120 0.0468 20 92.3 92.8 68.0-142 0.645 20 95.0 93.8 68.0-125 1.22 20 70.4 70.9 54.0-135 0.773 20 91.3 93.3 77.0-124 2.20 20 PROJECT: SDG: DATE/TIME: PAGE: 768490-030 L1055594 01/02/19 09:23 49 of 58 FP1 FTC FSS [Cn] FSr �GI FAI FSC WG1215938 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-11,12,13,14,15,16,17,18 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3372064-1 12/26/1810:26 • (LCSD) R3372064-2 12/26/18 10:46 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits Analyte ug/I ug/I ug/I % % % Styrene 25.0 23.1 24.0 92.4 96.1 73.0-130 1,1,1,2-Tetrachloroethane 25.0 23.0 23.1 92.0 92.3 75.0-125 1,1,2,2-Tetrachloroethane 25.0 22.2 22.1 88.8 88.4 65.0-130 Tetrachloroethene 25.0 25.3 25.5 101 102 72.0-132 Toluene 25.0 25.0 25.6 100 102 79.0-120 1,2,3-Trichlorobenzene 25.0 17.8 18.6 71.0 74.5 50.0-138 1,2,4-Trichlorobenzene 25.0 20.2 20.0 80.8 79.8 57.0-137 1,1,1-Trichloroethane 25.0 22.9 23.1 91.5 92.2 73.0-124 1,1,2-Trichloroethane 25.0 26.2 26.2 105 105 80.0-120 Trichloroethene 25.0 24.5 24.4 97.8 97.6 78.0-124 Trichlorofluoromethane 25.0 27.9 27.6 112 110 59.0-147 1,2,3-Trichloropropane 25.0 24.1 23.0 96.3 91.8 73.0-130 1,2,4-Trimethylbenzene 25.0 23.9 24.2 95.5 96.6 76.0-121 1,3,5-Trimethyl benzene 25.0 23.9 23.8 95.7 95.2 76.0-122 Vinyl chloride 25.0 25.9 25.7 104 103 67.0-131 o-Xylene 25.0 23.9 24.1 95.6 96.5 80.0-122 m&p-Xylenes 50.0 48.4 49.4 96.8 98.8 80.0-122 (S) Toluene-d8 105 106 80.0-120 (S) Dibromofluoromethane 96.1 96.6 75.0-120 (S) a, a, a-Trifluoroto/uene 98.2 95.6 80.0-120 (S) 4-Bromof/uorobenzene 90.4 90.5 77.0-126 LCS Qualifier FP1 LCSD Qualifier RPD RPD Limits FTC 3.86 20 0.275 20 FSS 0.461 20 0.910 20 2.33 20 rCn 4.75 20 1.25 20 FSr 0.811 20 0.321 20 0.198198 20 � 1.13 20 4.72 20 7G1 1.13 20 0.491 20 0.889 20 FAI 0.928 20 1.98 20 FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 50 of 58 WG1216990 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 620OB-1997 1-1055594-06,07,08,09,10 Method Blank (MB) (MB) R3372331-3 12/29/1810:08 MB Result Analyte ug/I MB Qualifier MB MDL MB RDL ug/I ug/I Acetone U 10.0 50.0 Acrolein U 8.87 50.0 Acrylonitrile U 1.87 10.0 Benzene U 0.331 1.00 Bromobenzene U 0.352 1.00 Bromodichloromethane U 0.380 1.00 Bromoform U 0.469 1.00 Bromomethane U 0.866 5.00 n-Butylbenzene U 0.361 1.00 sec -Butyl benzene U 0.365 1.00 tert-Butylbenzene U 0.399 1.00 Carbon tetrachloride U 0.379 1.00 Chlorobenzene U 0.348 1.00 Chlorodibromomethane U 0.327 1.00 Chloroethane U 0.453 5.00 Chloroform U 0.324 5.00 Chloromethane U 0.276 2.50 2-Chlorotoluene U 0.375 1.00 4-Chlorotoluene U 0.351 1.00 1,2-Dibromo-3-Chloropropane U 1.33 5.00 1,2-Dibromoethane U 0.381 1.00 Dibromomethane U 0.346 1.00 1,2-Dichlorobenzene U 0.349 1.00 1,3-Dichlorobenzene U 0.220 1.00 1,4-Dichlorobenzene U 0.274 1.00 Dichlorodifluoromethane U 0.551 5.00 1,1-Dichloroethane U 0.259 1.00 1,2-Dichloroethane U 0.361 1.00 1,1-Dichloroethene U 0.398 1.00 cis-1,2-Dichloroethene U 0.260 1.00 trans-1,2-Dichloroethene U 0.396 1.00 1,2-Dichloropropane U 0.306 1.00 1,1-Dichloropropene U 0.352 1.00 1,3-Dichloropropane U 0.366 1.00 2,2-Dichloropropane U 0.321 1.00 Di -isopropyl ether U 0.320 1.00 Ethylbenzene U 0.384 1.00 Hexachloro-1,3-butadiene U 0.256 1.00 Isopropylbenzene U 0.326 1.00 p-Isopropyltoluene U 0.350 1.00 ACCOUNT: Apex Environmental Inc. - Roanke Va PROJECT: SDG: DATE/TIME: PAGE: 768490-030 L1055594 01/02/19 09:23 51 of 58 FP1 FTC FSS [Cn] FSr �GI FAI FSC WG1216990 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 1-1055594-06,07,08,09,10 Method Blank (MB) (MB) R3372331-3 12/29/1810:08 MB Result Analyte ug/I 2-Butanone (MEK) U Methylene Chloride U 4-Methyl-2-pentanone (MIBK) U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,2,3-Trichlorobenzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl chloride U o-Xylene U m&p-Xylenes U (S) Toluene-d8 106 (S) Dibromofluoromethane 85.6 (S) a, a,o-Trifluoroto/uene 103 (S) 4-Bromof/uorobenzene 96.0 MB Qualifier MB MDL MB RDL ug/I ug/I 3.93 10.0 1.00 5.00 2.14 10.0 0.367 1.00 1.00 5.00 0.349 1.00 0.307 1.00 0.385 1.00 0.130 1.00 0.372 1.00 0.412 1.00 0.230 1.00 0.355 1.00 0.319 1.00 0.383 1.00 0.398 1.00 1.20 5.00 0.807 2.50 0.373 1.00 0.387 1.00 0.259 1.00 0.341 1.00 0.719 2.00 80.0-120 75.0-120 80.0-120 77.0-126 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3372331-1 12/29/18 09:10 • (LCSD) R3372331-2 12/29/18 09:29 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Acetone 125 122 121 Acrolein 125 252 268 Acrylonitrile 125 114 115 Benzene 25.0 21.2 21.5 Bromobenzene 25.0 24.0 24.5 Bromodichloromethane 25.0 23.5 23.5 ACCOUNT: Apex Environmental Inc. - Roanke Va ONE LAB. NATIONWIDE. LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 97.4 96.7 19.0-160 0.736 27 202 214 10.0-160 J4 J4 5.98 26 91.1 91.6 55.0-149 0.600 20 84.8 86.2 70.0-123 1.55 20 95.9 98.0 73.0-121 2.21 20 94.1 94.1 75.0-120 0.0402 20 PROJECT: SDG: DATE/TIME: PAGE: 768490-030 L1055594 01/02/19 09:23 52 of 58 FP1 FTc FSS 4 Cn FSr �GI FAI [Sc WG1216990 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-06,07,08,09,10 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3372331-1 12/29/18 09:10 • (LCSD) R3372331-2 12/29/18 09:29 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Bromoform 25.0 21.8 22.4 Bromomethane 25.0 21.4 21.5 n-Butylbenzene 25.0 26.7 27.3 sec -Butyl benzene 25.0 27.0 28.1 tert-Butylbenzene 25.0 26.2 27.5 Carbon tetrachloride 25.0 20.1 20.9 Chlorobenzene 25.0 26.7 26.7 Chlorodibromomethane 25.0 25.7 26.0 Chloroethane 25.0 22.8 24.9 Chloroform 25.0 21.1 21.6 Chloromethane 25.0 23.0 23.7 2-Chlorotoluene 25.0 25.1 25.9 4-Chlorotoluene 25.0 25.2 25.7 1,2-Dibromo-3-Chloropropane 25.0 21.0 21.8 1,2-Dibromoethane 25.0 25.4 25.7 Dibromomethane 25.0 23.5 23.5 1,2-Dichlorobenzene 25.0 23.9 24.3 1,3-Dichlorobenzene 25.0 25.9 26.5 1,4-Dichlorobenzene 25.0 25.1 25.8 Dichlorodifluoromethane 25.0 21.4 22.4 1,1-Dichloroethane 25.0 21.6 21.6 1,2-Dichloroethane 25.0 21.1 21.2 1,1-Dichloroethene 25.0 22.3 22.7 cis-1,2-Dichloroethene 25.0 21.7 21.7 trans-1,2-Dichloroethene 25.0 21.5 21.5 1,2-Dichloropropane 25.0 25.2 24.8 1,1-Dichloropropene 25.0 21.7 22.3 1,3-Dichloropropane 25.0 26.5 25.9 2,2-Dichloropropane 25.0 20.6 21.0 Di -isopropyl ether 25.0 22.6 22.6 Ethylbenzene 25.0 25.5 25.9 Hexachloro-1,3-butadiene 25.0 25.2 26.3 Isopropylbenzene 25.0 25.8 26.5 p-Isopropyltoluene 25.0 26.8 28.1 2-Butanone (MEK) 125 112 111 Methylene Chloride 25.0 21.2 21.3 4-Methyl-2-pentanone (MIBK) 125 135 131 Methyl tert-butyl ether 25.0 19.9 20.5 Naphthalene 25.0 21.8 22.9 n-Propylbenzene 25.0 25.4 26.4 ACCOUNT: Apex Environmental Inc. - Roanke Va LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 87.2 89.6 68.0-132 2.69 20 85.5 85.9 10.0-160 0.460 25 107 109 73.0-125 1.96 20 108 112 75.0-125 3.86 20 105 110 76.0-124 4.88 20 80.3 83.4 68.0-126 3.82 20 107 107 80.0-121 0.316 20 103 104 77.0-125 1.43 20 91.1 99.6 47.0-150 8.86 20 84.3 86.4 73.0-120 2.50 20 92.0 94.7 41.0-142 2.89 20 100 104 76.0-123 3.27 20 101 103 75.0-122 1.95 20 83.8 87.1 58.0-134 3.75 20 102 103 80.0-122 0.978 20 93.9 93.8 80.0-120 0.0410 20 95.5 97.2 79.0-121 1.80 20 104 106 79.0-120 2.14 20 100 103 79.0-120 2.96 20 85.5 89.4 51.0-149 4.54 20 86.4 86.6 70.0-126 0.228 20 84.6 84.6 70.0-128 0.0708 20 89.1 90.8 71.0-124 1.93 20 86.9 86.9 73.0-120 0.00976 20 85.8 86.2 73.0-120 0.413 20 101 99.4 77.0-125 1.42 20 86.6 89.1 74.0-126 2.77 20 106 104 80.0-120 2.28 20 82.5 84.0 58.0-130 1.87 20 90.3 90.4 58.0-138 0.119 20 102 104 79.0-123 1.56 20 101 105 54.0-138 4.20 20 103 106 76.0-127 2.59 20 107 112 76.0-125 4.65 20 89.5 89.0 44.0-160 0.560 20 84.8 85.4 67.0-120 0.655 20 108 105 68.0-142 2.81 20 79.8 81.9 68.0-125 2.60 20 87.2 91.5 54.0-135 4.84 20 102 105 77.0-124 3.71 20 PROJECT: SDG: DATE/TIME: PAGE: 768490-030 L1055594 01/02/19 09:23 53 of 58 FP1 FTC FSS [Cn] FSr �GI FAI FSC WG1216990 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1055594-06,07,08,09,10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) ONE LAB. NATIONWIDE. (LCS) R3372331-1 12/29/18 09:10 • (LCSD) R3372331-2 12/29/18 09:29 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % Styrene 25.0 25.5 26.3 102 105 73.0-130 3.21 20 1,1,1,2-Tetrachloroethane 25.0 26.7 26.8 107 107 75.0-125 0.285 20 1,1,2,2-Tetrachloroethane 25.0 25.6 26.1 102 104 65.0-130 1.77 20 Tetrachloroethene 25.0 27.0 27.6 108 110 72.0-132 2.35 20 Toluene 25.0 24.7 24.8 98.6 99.1 79.0-120 0.509 20 1,2,3-Trichlorobenzene 25.0 23.9 25.1 95.8 100 50.0-138 4.63 20 1,2,4-Trichlorobenzene 25.0 23.3 25.0 93.3 99.9 57.0-137 6.88 20 1,1,1-Trichloroethane 25.0 21.3 21.8 85.3 87.0 73.0-124 2.07 20 1,1,2-Trichloroethane 25.0 26.1 26.3 104 105 80.0-120 0.868 20 Trichloroethene 25.0 23.7 23.6 94.9 94.4 78.0-124 0.498 20 Trichlorofluoromethane 25.0 17.9 18.1 71.5 72.5 59.0-147 1.36 20 1,2,3-Trichloropropane 25.0 25.8 25.8 103 103 73.0-130 0.0702 20 1,2,4-Trimethylbenzene 25.0 25.5 25.9 102 104 76.0-121 1.75 20 1,3,5-Trimethyl benzene 25.0 25.9 26.6 104 106 76.0-122 2.67 20 Vinyl chloride 25.0 25.6 26.6 102 106 67.0-131 3.63 20 o-Xylene 25.0 25.9 25.9 104 104 80.0-122 0.191 20 m&p-Xylenes 50.0 53.5 53.4 107 107 80.0-122 0.112 20 (S) Toluene-d8 103 102 80.0-120 (S) Dibromofluoromethane 85.0 84.4 75.0-120 (S) a, a, a-Trifluoroto/uene 101 101 80.0-120 (S) 4-Bromof/uorobenzene 95.8 97.3 77.0-126 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 54 of 58 FP1 FTC FSS 4 Cn FSr �GI FAI FSC GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. FP1 FTC FSS [Cn] FSr 6 QC FAI FSC Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J4 The associated batch QC was outside the established quality control range for accuracy. V3 The internal standard exhibited poor recovery due to sample matrix interference. The analytical results will be biased high. BDL results will be unaffected. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 55 of 58 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T 104704245-17-14 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T ID T WI NY SD WY MI NV T NE IA OH T PA T f IL Ills WY vA UT T CA�� T KS MO KY W 11110 � NM O� AR N Sc T MS A`7L GA T TX * LA T AK T T q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: Apex Environmental Inc. - Roanke Va 768490-030 L1055594 01/02/19 09:23 ME PAGE: 56 of 58 3illing information. 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Time: Hold- Conditia l: r D N[F ri APPENDIX B Historical Groundwater Analytical Results Table 2.- Historical Groundwater and Surface Water Sampling Results Revision Date: 12/20/18 Incident Number and Name: # 36096 Pilot 056 Analytical Method (VOC by EPA 6200B) Contaminant of Concern: gasoline ���amamma�amamamamama ��ememme�emememememe ��amamma�amamamamama ��amammamamamamamama ���amamma®amam�mam®ma ��emem®®�eme�emem�me ��amamma�amamamamama ��amamma�amamamamama ��amammamamamamamama ��amammamamamamamama ��emem��®e�ememememe ��amamma�ama�amamama ��amamma�amamamamama ��am�mmamamamamamama ®��amamma®amamamamama ���memm®�eme�emem�me ��amamma®amamamamama ��amamma®amamamamama ��amamma®amamamamama ��amamma�amamamamama ��ememm®�eme�em®mime ��amamma�amamamamama ��amamma�amamamamama ��amammamamamamamama ��amamma�amamamamama ��amammamamamamamama ��amamma®amamamamama ��amammamamamamamama ��amamma�amamamam�ma ��amamma�amamamamama ��amammamamamamamama ��amamma�amamamamama ��amammamamamamamama ��amamma�amamamamama ��amamma�amamamamama ��a®ammmmmm�����mamm ��ama r r ®m�ammma��mama ��amammm�amamammmama ��amamma�a®amam��ama ��ammmma�amamamama�a ��amammamamamamama�a ��am�mm®��ma�amama�a ��amamma®ama�amam��a ��amamma�ama�amama�a ��ememm�meme�emem®me ��amamma�amamamam�ma ' ��amamma�amamamamama ��amamma�amamamam�ma ��emem�©meme�emememe ��amam�amamamamamama ��ama®mamamama®amama ��amammamamamamamama ��amammamamamamamama ��amamma©amamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��mmmmmamamammmammma ��0�0��0�0�0�0�0�0�0 ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��eme��®�emeoe�®��me ��amamma�amamamamama ��am®��a�amam®�a��ma ��am�m�a�amamamam�ma ��am�mmamama®amamama ��eme����e�e®���m�me ��amam�a�amamama��ma ��amamma�amamamamama ��amamma®amamamamama ��amamma®amamamamama ��amamma�amamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amamma�amamamamama ��amamma®amamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��ememme�emememememe ��amamma�amamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ���amammamamamamamama ®��amammamamamamamama ��emem®e�emememem®me ��amamma�amamamammma ��amamma�amamamamama ��amamma�amamamamama ��amamma�amamamamama ��amammamamamamamama ��amamma®amamamamama ��amamma�amamamam�ma ��amamma�amamamam�ma ��amamma�amamamamama ��amamma®amamamam�ma ��amamma�amamamam®ma ��amamma�amamamamama ��amammamamamamamama ��mmmmmmmmmmmmmmmmmm ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��mmmmmmmmmmmmmmmmmm ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��ememmememememememe ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamama�a ��amammamamamamama®a ��amammamamamamama®a ��amammamamamamama�a ��amammamamamamama®a ��ememmememememememe ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��ememmememememememe ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��mmmmmmmmmmmmmmmmmm ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��mmmmmmmmmm®mmmmmmm ��amammamamamamamama �miamammamamamamamama �miamammamamamamamama �miamammamamamamamama �miamammamamamamamama �miamammamamamamamama ��amammamamamamamama �miamammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ��amammamamamamamama ���mmmmmmmmmmmmmmmmmm o©��ommmm®m�mo�mmm — Not Detected NS: Not Sampled All results in ug/L APPENDIX C O&M Checklists PILOT # 56 KANAPOLIS, NC OPERATIONS AND MAINTENANCE CHECKLIST O&M Date: 07/26/18 Apex Job #: 768490.030 Apex Staff: KAH ALARM CONDITIONS Description p Check Alarm Conditions Conditions/Comments AWS High Level OK Emergency Stop ON INFLUENT MANIFOLD AND WELL HEADS Recovery Well ID Measurement Conditions/Comments Manifold (in Hg) Well Head (in Hg) SVE-1 13.5 NA SVE-2 29.0 NA SVE-3 9.5 NA SVE Header Influent (in hg) 8.0 SOIL VAPOR EXTRACTION (SVE) Description Measurement Conditions/Comments Vacuum (in Hg) 26.0 Temperature (°F) 190 Vent Stack Pressure (in H2O) 0.0 Flow Meter (in scfm) 110 Check Filter Clean Oil Level 3/4 full Changed oil SVE Hours 43,364.8 Check Fittings for Leaks None PHASE SEPARATOR (Knockout(KO)) Description Measurement Conditions/Comments Phase Separator Vacuum (in Hg) 8.0 Site Glass (clouding, scratched, etc.) Clear Check Fittings for Leaks None AIR SPARGE COMPRESSOR Description Measurement Conditions/Comments Air Compressor ON Air Compressor Hours 22,089.6 Air Compressor (psi) 50.0 Air Compressor Temperature 100.0 Air Compressor Regulator (psi) 50.0 Air Flow (scfin) 20.0 Drain Pressure Tank Yes AIR SPARGE WELLS Air Sparge Well Pressure (psi) Air Flow (scfm) AS-1 19.0 9.6 AS-2 18.0 5.2 AS-3 29.0 9.1 AS-4 30.0 3.4 AS-5 Off Off AS-6 Off Off AS-7 Off Off AS-8 Off Off AS-9 Off Off AS-10 Off Off AS-11 Off Off AS-12 Off Off AS-13 Off Off AS-14 Off Off AS-15 Off Off AS-16 Off Off SYSTEM BUILDING AND COMPONENTS Description Measurement Conditions/Comments General Condition of Building OK Heater (Operating Temperature) 500 Exhaust Ventilation Fan 500 Working Manifold OK Overhead Lighting Working Bulb needed in Compressor room Locks and Anchors Secure CONTROL PANEL (Building) Description Measurement Conditions/Comments Electric Meter Reading (kWh) 456,923 Electric Meter Reading (max kW) NA Breaker Box Secure Additional Comments and Notes: -Apex on site. Cloudy 85' -System non -operational upon arrival due to emergency stop. -Changed oil in the SVE. -Performed routine O&M activities -Repaired AS-1 Dwyer gauge union that was cracked. -System fully operational upon departure. -Apex off site. E PILOT # 56 KANAPOLIS, NC OPERATIONS AND MAINTENANCE CHECKLIST O&M Date: 08/22/18 Apex Job #: 768490.030 Apex Staff: KAH ALARM CONDITIONS Description p Check Alarm Conditions Conditions/Comments AWS High Level OK Emergency Stop OK INFLUENT MANIFOLD AND WELL HEADS Recovery Well ID Measurement Conditions/Comments Manifold (in Hg) Well Head (in Hg) SVE-1 14.0 NA SVE-2 29.5 NA SVE-3 10.0 NA SVE Header Influent (in hg) 9.0 SOIL VAPOR EXTRACTION (SVE) Description Measurement Conditions/Comments Vacuum (in Hg) 13.5 Temperature (°F) 185 Vent Stack Pressure (in H2O) 0.0 Flow Meter (in scfm) 90 Check Filter Clean Oil Level 3/4 full SVE Hours 44,010.2 Check Fittings for Leaks None PHASE SEPARATOR (Knockout(KO)) Description Measurement Conditions/Comments Phase Separator Vacuum (in Hg) 8.5 Drained water Site Glass (clouding, scratched, etc.) Clear Check Fittings for Leaks None AIR SPARGE COMPRESSOR Description Measurement Conditions/Comments Air Compressor OFF Turned back on Air Compressor Hours 22,476.0 Air Compressor (psi) 105 Air Compressor Temperature 90 Air Compressor Regulator (psi) 65 Air Flow (scfin) 16 Drain Pressure Tank Yes AIR SPARGE WELLS Air Sparge Well Pressure (psi) Air Flow (scfm) AS-1 26.0 9.2 AS-2 23.0 5.8 AS-3 38.0 4.4 AS-4 37.0 2.6 AS-5 Off Off AS-6 Off Off AS-7 Off Off AS-8 Off Off AS-9 Off Off AS-10 Off Off AS-11 Off Off AS-12 Off Off AS-13 Off Off AS-14 Off Off AS-15 Off Off AS-16 Off Off SYSTEM BUILDING AND COMPONENTS Description Measurement Conditions/Comments General Condition of Building OK Heater (Operating Temperature) 500 Exhaust Ventilation Fan 500 Working Manifold OK Overhead Lighting Working Bulb needed in Compressor room Locks and Anchors Secure CONTROL PANEL (Building) Description Measurement Conditions/Comments Electric Meter Reading (kWh) 465,863 Electric Meter Reading (max kW) NA Breaker Box Secure Additional Comments and Notes: -Apex on site. Sunny 850 -System operational upon arrival, but air sparge non -operational. -Reset compressor. -Performed routine O&M activities -System fully operational upon departure. -Apex off site. 2 PILOT # 56 KANAPOLIS, NC OPERATIONS AND MAINTENANCE CHECKLIST O&M Date: 09/27/18 Apex Job #: 768490.030 Apex Staff: KAH ALARM CONDITIONS Description p Check Alarm Conditions Conditions/Comments AWS High Level OK Emergency Stop OK INFLUENT MANIFOLD AND WELL HEADS Recovery Well ID Measurement Conditions/Comments Manifold (in Hg) Well Head (in Hg) SVE-1 14.0 NA SVE-2 29.5 NA SVE-3 10.0 NA SVE Header Influent (in hg) 9.0 SOIL VAPOR EXTRACTION (SVE) Description Measurement Conditions/Comments Vacuum (in Hg) 13.0 Temperature (°F) 195 Vent Stack Pressure (in H2O) 0.0 Flow Meter (in scfm) 95 Check Filter Clean Oil Level 3/4 full SVE Hours 44,875.5 Check Fittings for Leaks None PHASE SEPARATOR (Knockout(KO)) Description Measurement Conditions/Comments Phase Separator Vacuum (in Hg) 9.0 Drained water Site Glass (clouding, scratched, etc.) Clear Check Fittings for Leaks None AIR SPARGE COMPRESSOR Description Measurement Conditions/Comments Air Compressor OFF Turned back on Air Compressor Hours 22,597.5 Air Compressor (psi) 60 Air Compressor Temperature 100 Air Compressor Regulator (psi) 60 Air Flow (scfin) 121 Drain Pressure Tank Yes AIR SPARGE WELLS Air Sparge Well Pressure (psi) Air Flow (scfm) AS-1 24.0 11.2 AS-2 25.5 8.6 AS-3 25.0 13.0+ AS-4 24.0 2.6 AS-5 Off Off AS-6 Off Off AS-7 Off Off AS-8 Off Off AS-9 Off Off AS-10 Off Off AS-11 Off Off AS-12 Off Off AS-13 Off Off AS-14 Off Off AS-15 Off Off AS-16 Off Off SYSTEM BUILDING AND COMPONENTS Description Measurement Conditions/Comments General Condition of Building OK Heater (Operating Temperature) 500 Exhaust Ventilation Fan 500 Working Manifold OK Overhead Lighting Working Bulb needed in Compressor room Locks and Anchors Secure CONTROL PANEL (Building) Description Measurement Conditions/Comments Electric Meter Reading (kWh) 474,193 Electric Meter Reading (max kW) NA Breaker Box Secure Additional Comments and Notes: -Apex on site. Sunny 850 -System operational upon arrival, but air sparge non -operational. -Reset compressor. -Performed routine O&M activities. -Repaired Dwyer gauge on AS-4. -System fully operational upon departure. -Apex off site. 2 PILOT # 56 KANAPOLIS, NC OPERATIONS AND MAINTENANCE CHECKLIST O&M Date: 10/24/18 Apex Job #: 768490.030 Apex Staff: KAH ALARM CONDITIONS Description p Check Alarm Conditions Conditions/Comments AWS High Level OK Emergency Stop OK INFLUENT MANIFOLD AND WELL HEADS Recovery Well ID Measurement Conditions/Comments Manifold (in Hg) Well Head (in Hg) SVE-1 13.0 NA SVE-2 29.5 NA SVE-3 10.0 NA SVE Header Influent (in hg) 8.5 SOIL VAPOR EXTRACTION (SVE) Description Measurement Conditions/Comments Vacuum (in Hg) 11.5 Temperature (°F) 170 Vent Stack Pressure (in H2O) 0.0 Flow Meter (in scfm) 90 Check Filter Clean Oil Level 3/4 full SVE Hours 45,524.1 Check Fittings for Leaks None PHASE SEPARATOR (Knockout(KO)) Description Measurement Conditions/Comments Phase Separator Vacuum (in Hg) 8.5 Drained water Site Glass (clouding, scratched, etc.) Clear Check Fittings for Leaks None AIR SPARGE COMPRESSOR Description Measurement Conditions/Comments Air Compressor OFF Turned back on Air Compressor Hours 22,692.7 Air Compressor (psi) 65 Air Compressor Temperature 80 Air Compressor Regulator (psi) 60 Air Flow (scfin) 19 Drain Pressure Tank Yes AIR SPARGE WELLS Air Sparge Well Pressure (psi) Air Flow (scfm) AS-1 26.0 12.2 AS-2 26.0 8.4 AS-3 29.0 13.0+ AS-4 26.0 2.4 AS-5 Off Off AS-6 Off Off AS-7 Off Off AS-8 Off Off AS-9 Off Off AS-10 Off Off AS-11 Off Off AS-12 Off Off AS-13 Off Off AS-14 Off Off AS-15 Off Off AS-16 Off Off SYSTEM BUILDING AND COMPONENTS Description Measurement Conditions/Comments General Condition of Building OK Heater (Operating Temperature) 500 Exhaust Ventilation Fan 500 Working Manifold OK Overhead Lighting Working Bulb needed in Compressor room Locks and Anchors Secure CONTROL PANEL (Building) Description Measurement Conditions/Comments Electric Meter Reading (kWh) 480,203 Electric Meter Reading (max kW) NA Breaker Box Secure Additional Comments and Notes: -Apex on site. Sunny 750 -System operational upon arrival, but air sparge non -operational. -Reset compressor. -Performed routine O&M activities. -Check valve on knockout tank needs replacing upon next visit. -System fully operational upon departure. -Apex off site. 2 PILOT # 56 KANAPOLIS, NC OPERATIONS AND MAINTENANCE CHECKLIST O&M Date: 11/19/18 Apex Job #: 768490.030 Apex Staff: KAH ALARM CONDITIONS Description p Check Alarm Conditions Conditions/Comments AWS High Level OK Emergency Stop OK INFLUENT MANIFOLD AND WELL HEADS Recovery Well ID Measurement Conditions/Comments Manifold (in Hg) Well Head (in Hg) SVE-1 12.5 NA SVE-2 29.5 NA SVE-3 10.5 NA SVE Header Influent (in hg) 9.0 SOIL VAPOR EXTRACTION (SVE) Description Measurement Conditions/Comments Vacuum (in Hg) 11.5 Temperature (°F) 180 Vent Stack Pressure (in H2O) 0.0 Flow Meter (in scfm) 80 Check Filter Clean Oil Level 3/4 full Change next visit SVE Hours 46,149.5 Check Fittings for Leaks None PHASE SEPARATOR (Knockout(KO)) Description Measurement Conditions/Comments Phase Separator Vacuum (in Hg) 8.5 Drained water Site Glass (clouding, scratched, etc.) Clear Check Fittings for Leaks None AIR SPARGE COMPRESSOR Description Measurement Conditions/Comments Air Compressor OFF Turned back on Air Compressor Hours 22,859.9 Air Compressor (psi) 75 Air Compressor Temperature 72 Change oil next visit Air Compressor Regulator (psi) 65 Air Flow (scfin) 18 Drain Pressure Tank Yes AIR SPARGE WELLS Air Sparge Well Pressure (psi) Air Flow (scfm) AS-1 28.0 11.2 AS-2 28.5 8.6 AS-3 29.0 13.0+ AS-4 26.0 3.2 AS-5 Off Off AS-6 Off Off AS-7 Off Off AS-8 Off Off AS-9 Off Off AS-10 Off Off AS-11 Off Off AS-12 Off Off AS-13 Off Off AS-14 Off Off AS-15 Off Off AS-16 Off Off SYSTEM BUILDING AND COMPONENTS Description Measurement Conditions/Comments General Condition of Building OK Heater (Operating Temperature) 500 Exhaust Ventilation Fan 500 Working Manifold OK Overhead Lighting Working Bulb needed in Compressor room Locks and Anchors Secure CONTROL PANEL (Building) Description Measurement Conditions/Comments Electric Meter Reading (kWh) 486,606 Electric Meter Reading (max kW) NA Breaker Box Secure Additional Comments and Notes: -Apex on site. Sunny 65' -System operational upon arrival, but air sparge non -operational. -Reset compressor. -Performed routine O&M activities. -Check valve on knockout tank needs replacing upon next visit! -System fully operational upon departure. -Apex off site. 2 PILOT # 56 KANAPOLIS, NC OPERATIONS AND MAINTENANCE CHECKLIST O&M Date: 12/20/18 Apex Job #: 768490.030 Apex Staff: KAH ALARM CONDITIONS Description p Check Alarm Conditions Conditions/Comments AWS High Level OK Emergency Stop OK INFLUENT MANIFOLD AND WELL HEADS Recovery Well ID Measurement Conditions/Comments Manifold (in Hg) Well Head (in Hg) SVE-1 9.5 NA SVE-2 29.5 NA SVE-3 10.5 NA SVE Header Influent (in hg) 6.5 SOIL VAPOR EXTRACTION (SVE) Description Measurement Conditions/Comments Vacuum (in Hg) 5.5 Temperature (°F) 170 Vent Stack Pressure (in H2O) 0.0 Flow Meter (in scfm) 90 Check Filter Clean Oil Level 3/4 full Change next visit SVE Hours 46,890.0 Check Fittings for Leaks None PHASE SEPARATOR (Knockout(KO)) Description Measurement Conditions/Comments Phase Separator Vacuum (in Hg) 6.0 Drained water Site Glass (clouding, scratched, etc.) Clear Check Fittings for Leaks None AIR SPARGE COMPRESSOR Description Measurement Conditions/Comments Air Compressor OFF Turned back on Air Compressor Hours 22,984.2 Air Compressor (psi) 50 Air Compressor Temperature 68 Change oil next visit Air Compressor Regulator (psi) 45 Air Flow (scfin) 18 Drain Pressure Tank Yes AIR SPARGE WELLS Air Sparge Well Pressure (psi) Air Flow (scfm) AS-1 29.5 8.4 AS-2 29.5 8.6 AS-3 30.0 13.0+ AS-4 28.0 13.0+ AS-5 Off Off AS-6 Off Off AS-7 Off Off AS-8 Off Off AS-9 Off Off AS-10 Off Off AS-11 Off Off AS-12 Off Off AS-13 Off Off AS-14 Off Off AS-15 Off Off AS-16 Off Off SYSTEM BUILDING AND COMPONENTS Description Measurement Conditions/Comments General Condition of Building OK Heater (Operating Temperature) 500 Exhaust Ventilation Fan 500 Working Manifold OK Overhead Lighting Working Bulb needed in Compressor room Locks and Anchors Secure CONTROL PANEL (Building) Description Measurement Conditions/Comments Electric Meter Reading (kWh) 491,683 Electric Meter Reading (max kW) NA Breaker Box Secure Additional Comments and Notes: -Apex on site. Heavy rain 45' -System non -operational upon arrival due to compressor being off and belt broken on SVE. -Reset compressor. -Replaced belt on SVE. -Performed routine O&M activities. -Conducted quarterly sampling -Check valve on knockout tank needs replacing upon next visit! -System fully operational upon departure. -Collected OWS discharge sample. -Apex off site. L,