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HomeMy WebLinkAboutMO-9406_40849_CA_LSA_20190205_LSATM PHASE I LIMITED SITE ASSESSMENT REPORT FORMER CHARLOTTE CORRECTIONAL CENTER 4101 MEADOW OAK DRIVE CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA ECS PROJECT 49-6535-L PREPARED FOR: MR. ADAM DUERR EXETER 4100 MEADOW OAK, LLC 6285 BARFIELD ROAD, SUITE 225 ATLANTA, GEORGIA 30328 FEBRUARY 5, 2019 ECS SOUTHEAST, LLP "Setting the Standard for Service" - Geotechnical - Construction Materials - Environmental - Facilities NC Registered Fzngineernng Firm F•1078 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 February 5, 2019 Trudy Beverly, LG Hydrogeologist NCDEQ - Division of Waste Management Underground Storage Tanks Section — Corrective Action Branch Mooresville Regional Office 610 East Center Ave., Suite 301 Mooresville, NC 28115 Submitted via email (Trudy.Beverly@ncdenr.gov) and Federal Express Overnight Delivery Reference: Phase I Limited Site Assessment Report, Notice of Residual Petroleum, and Request for No Further Action 4101 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina NCDEQ Incident No. 40849 ECS Project No. 49-6535-L (Meadow Oaks Industrial) Dear Ms. Beverly: ECS Southeast, LLP (ECS) prepared this correspondence and the attached Phase I Limited Site Assessment (Phase I LSA) Report on behalf of its client, Exeter 4100 Meadow Oak, LLC. A CD with the report in PDF format is also attached. The Phase I LSA was prepared in response to a Notice of Regulatory Requirements (NORR) issued to Exeter 4100 Meadow Oak, LLC by the North Carolina Department of Environmental Quality (NCDEQ). It should be noted that Exeter 4100 Meadow Oak, LLC did not own or operate the underground storage tank (UST) which is the source of the release at this site. As such, Exeter 4100 Meadow Oak, LLC is not the responsible party and completed the Phase I ESA as a voluntary action. The analytical results in the Phase I LSA Report indicate maximum soil contaminant concentrations (MSCCs) were exceeded for the leaching from soil to groundwater exposure scenario in a sample collected at a depth of 15 feet below ground surface, but no MSCCs were exceeded in a sample collected at 25 feet bgs. It should be noted that analyses of one sidewall sample collected in October 2018 following removal of the UST and over -excavation of approximately 50 tons of impacted soil indicated that MSCCs for the leaching from soil to groundwater exposure and residential exposure scenarios were exceeded. The analytical results in the Phase I LSA Report did not indicate the presence of volatile organic compounds (VOCs) or semi -volatile organic compounds (SVOCs) above laboratory detection limits in a groundwater sample collected from a monitoring well constructed at the location of the former underground storage tank (UST). TICS from the EPA Method 625.1 chromatograph were noted but no groundwater standards apply to TICs. ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC - ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com FebruaryECS SOUTHEAST, LLP During the Phase I LSA, site conditions which would trigger a high or an intermediate risk classification for the site were not noted. An out -of -service water supply well was noted approximately 380 feet west and crossgradient from the UST. No other water supply wells were noted during the site and area reconnaissance. Eleven water well questionnaires were forwarded by certified mail to property owners within 500 feet of the subject site. Three questionnaires were retuned and both indicated water supply wells were not present on their respective properties. One questionnaire was returned as undeliverable. If additional completed questionnaires are received, ECS will forward them to you. ECS understands that its client, Exeter 4100 Meadow Oak, LLC, is negotiating with the State of North Carolina regarding acquisition of the subject site. ECS understand that Exeter 4100 Meadow Oak, LLC intends to utilize the site for industrial/commercial purposes. ECS, on behalf of Exeter 4100 Meadow Oak, LLC, respectfully request that NCDEQ review the attached report and issue a notice of no further action required (NFA Notice) with respect to the 10,000-gallon heating oil UST. ECS understands that NCDEQ will likely require that a Notice of Residual Petroleum (NORP) be completed and filed with the Mecklenburg County Register of Deeds and the NORP will restrict the use of the property to industrial/commercial purposes and will also prohibit the use of groundwater as a source of water supply. A completed NORP which has been signed by the owner of the property is attached and includes these restrictions. Thank you for your attention to this matter. If you have questions or comments, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP �� P x4tv- Joseph P. Nestor, P.G., P.E. Senior Environmental Project Manager 6nestor@ecslimited.com 704-280-7422 Attachments: Phase I Limited Site Assessment Report Notice of Residual Petroleum CD with Report in PDF Format Matthew H. McDuffie, P.G. Principal Geologist mmcduffie@ecslimited.com 704-378-9003 ECS Project No. 49:6535-L Page 12 Ecte E01- NOTICE OF RESIDUAL PETROLEUM Exeter Meadow Oak, Incident Number: 40849, 4101 Meadow Oak Drive, Charlotte, Mecklenburg County, North Carolina Current Property Owner's Deed: Book 605 Page 143 The property that is the subject of this Notice (hereinafter referred to as the "Site") contains residual petroleum and is an Underground Storage Tank (UST) incident under North Carolina's Statutes and Regulations, which consist of N.C.G.S. 143-215.94 and regulations adopted thereunder. This Notice is part of a remedial action for the Site that has been approved by the Secretary (or his/her delegate) of the North Carolina Department of Environment Quality (or its successor in function), as authorized by N.C.G.S. Section 143B-279.9 and 143B-279.11. The North Carolina Department of Environment Quality shall hereinafter be referred to as "DEQ". NOTICE Petroleum product was released and/or discharged at the Site. Petroleum constituents remain on the site, but are not a danger to public health and the environment, provided that the restrictions described herein, and any other measures required by DEQ pursuant to N.C.G.S. Sections 143B- 279.9 and 143B-279.11, are strictly complied with. This "Notice of Residual Petroleum" is composed of a description of the property, the location of the residual petroleum and the land use restrictions on the Site. The Notice has been approved and notarized by DEQ pursuant to N.C.G.S. Sections 143B-279.9 and 143B-279.11 and has/shall be recorded at the Mecklenburg County Register of Deeds' office Book Page Any map or plat required by DEQ has been/shall be recorded at the Mecklenburg County Register of Deeds' office Book , Page , and has been/shall be incorporated into the Notice by this reference. 1 of 4 Source Proper The State of North Carolina is the owner in fee simple of all or a portion of the Site, which is located in the County of Mecklenburg, State of North Carolina, and is known and legally described as: BEING ALL OF LOT 35 IN BLOCK 4 AS SHOWN ON MAP OF CLAIREBORNE WOODS, MAP 4 SUBDIVISION WHICH IS RECORDED IN MAP BOOK 24, AT PAGE 509 IN THE MECKLENBURG COUNTY PUBLIC REGISTRY, REFERENCE TO SAID MAP BEING HEREBY MADE FOR A PARTICULAR DESCRIPTION THEREOF. PERPETUAL LAND USE RESTRICTIONS Soil: The Site shall be used for industrial/commercial use only. Industrial/commercial use means a use where exposure to soil contamination is limited in time and does not involve exposure to children or other sensitive populations such as the elderly or sick. The real property shall not be developed or utilized for residential purposes including but not limited to: primary or secondary residences (permanent or temporary), schools, daycare centers, nursing homes, playgrounds, parks, recreation areas and/or picnic areas. Groundwater: Groundwater from the site is prohibited from use as a water supply. Water supply wells of any kind shall not be installed or operated on the site. ENFORCEMENT The above land use restriction(s) shall be enforced by any owner, operator, or other party responsible for the Site. The above land use restriction(s) may also be enforced by DEQ through any of the remedies provided by law or by means of a civil action, and may also be enforced by any unit of local government having jurisdiction over any part of the Site. Any attempt to cancel this Notice without the approval of DEQ (or its successor in function) shall be subject to enforcement by DEQ to the full extent of the law. Failure by any party required or authorized to enforce any of the above restriction(s) shall in no event be deemed a waiver of the right to do so thereafter as to the same violation or as to one occurring prior or subsequent thereto. 2of4 IN WITNESS WHEREOF. Tim Walton has caused tlii.q Notig to be executed pursuant la N.C.G.S. Sections t438-?79.9 and 14313-279.1 1. this �'tlay of "-a .2012- State of North' ]Carolina, Dept. of Administration By: � UjaZ7 P, , Title: Director, State Property Office 1 Signatory's name typed or printed: //;Pl PJ41, 7`VIU NORTH CAR LIMA Cr COUNTY (Name of county in. which acknowledgment was taken) I certify that the following person personally a eared liefore in; this day, acknowledging to me that he or she signed the foregoing document: 4/+F Date: (Official Seal) expires / 13012 Z tsi;;jurtr ) N0111r4. it'r.ddi r� (Printed or aped name of Notary Public) Notary Public My commission 3 of 4 Approved for the purposes of N.C.G.S. 143B-279.11 (Signature of Regional Supervisor) Regional Supervisor (Printed name of Regional Supervisor) Mooresville Regional Office UST Section Division of Waste Management Department of Environment Quality NORTH CAROLINA COUNTY (Name of county in which acknowledgment was taken) I certify that the following person(s) personally appeared before me this day, each acknowledging to me that he or she signed the foregoing document: (fidl printed name of Regional supervisor) Date: (Official Seal) expires: (signature of Nolary Public) printed or typed name of Notary Public) Notary Public My commission 4of4 t Ef 9-S ECS SOUTHEAST, LLP "Setting the Standard for Service" 1:r Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F•1073 NC Registered Geologists Firm C-406 SC Regis Eered Engmeenng Firm 3239 February 5, 2019 Mr. Adam Duerr Exeter 4100 Meadow Oak, LLC 6285 Barfield Road, Suite 225 Atlanta, Georgia 30328 Reference: Phase I Limited Site Assessment Report Former Charlotte Correctional Center 4101 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L Dear Mr. Duerr: As authorized by your acceptance of ECS Proposal 49: 12672P dated December 20, 2018 and authorized on January 3, 2019 , ECS Southeast, LLP (ECS) has completed the Phase I Limited Site Assessment Report for the above referenced site. Included in this report is a description of the field activities, the results obtained, and our conclusions and recommendations. ECS appreciates the opportunity to provide our environmental consulting services to you on this project. If you have any questions concerning this report or this project, please contact us. Sincerely, ECS SOUTHEAST, LLP Matthew H. M`Duffie, P.G. Principal Geologist MMcDuffie@ecslimited.com 704-525-5152 )014� .. AtfF7 Joseph P. Nestor, P. G., P.E. Senior Environmental Project Manager anestor@ecslimited.com 704-280-7422 ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 Site Name and Location: Facility ID#: Latitude and Longitude: Date of Report: Land Use Category: SITE INFORMATION Former Charlotte Correctional Center 4101 Meadow Oaks Drive Charlotte, Mecklenburg County, North Carolina 00-0-0000030621 35.193087' North, 80.921219' West February 5, 2019 Commercial UST System Owner: NC Department of Public Safety Central Engineering Attn: Jeffery O'Brian 4216 Mail Service Center Raleigh, North Carolina 28699-4216 (Information obtained from NCDEQ Registered Tank Database) Land Owner: NC State Highway and Public Works Commission 1119 East Sugar Creek Road Charlotte North Carolina 28205 (Information obtained from NCDEQ Registered Tank Database) Alternative Contact UST System Owner and Land Owner: NC Department of Administration State Property Office Attn: Joy M. Wayman, Real Property Agent Mail Service Center 1321 Raleigh, NC 27699-1321 Consultant: ECS Southeast, LLP Attention: Joseph P. Nestor, P.G., P.E. 1812 Center Park Drive; Suite D Charlotte, North Carolina 28217 (704) 280-7422 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 Laboratory: Pace Analytical Services, LLC 9800 Kincey Avenue; Suite 100 Huntersville, North Carolina 28409 (704) 875-9092 North Carolina Wastewater Certificate #12 Release Information: The UST system at the referenced site included one 10,000-gallon heating oil underground storage tank (UST). The North Carolina Department of Environmental Quality (NCDEQ) Registered Tanks Database (found on line at https://deg.nc.gov/about/divisions/waste- management/ust/databases) indicates that a 5,000-gallon heating oil UST was installed in 1964 and was temporarily closed. Evidence of a release was discovered during a Phase II Environmental Site Assessment (Phase II ESA) performed in April and May 2018 as part of due diligence for a potential real estate transaction. Four soil borings (SB-1 through SB-4) were advanced around the UST on April 23, 2018 and samples were collected and analyzed for total petroleum hydrocarbons (TPH) as gasoline range organics (GRO) and diesel range organics (DRO) by ultraviolet fluorescence (UVF). The analyses for samples from boring SB- 3 collected from 5 to 10 feet below ground surface (bgs) indicated the presence of TPH-GRO and TPH- DRO at concentrations above NCDEQ action levels. On September 7, 2018, ECS Geotechnical personnel noticed apparent petroleum hydrocarbons odors in a geotechnical boring (B-24) located approximately 100 feet northeast of the UST. ECS submitted a sample from geotechnical boring B-24 for laboratory analysis which detected concentrations of semi -volatile organic compounds (VOCs) and semi -volatile organic compounds (SVOCs) in excess of maximum soil contaminant concentrations (MSCCs) for the leaching form soil to groundwater. On September 21, 2018, a 10,000-gallon UST was removed from the site. (Note that the NCDEQ Registered Tanks Database indicated that a 5,000-gallon UST was present.) Field screening of soil with a photoionization detector (PID), visual observations of stained soil, and petroleum odors exuded from soil indicated a petroleum release had occurred. Approximately 50 tons of petroleum -impacted soil was excavated and removed from the site for offsite treatment/disposal. Analysis of samples collected from sidewalls of the resulting excavation indicated that soil remaining in place contained petroleum constituents in excess of MSCCs for the leaching form soil to groundwater and/or residential exposure scenarios. Phase i Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 Seal and Signature of Certifying Licensed Geologist I, Joseph P. Nestor, a Licensed Geologist for ECS Southeast, LLP, do certify that the information contained in this report is correct and accurate to the best of my knowledge. .0 ,,%1110111i r"Op, E SR 1q P. Joseph P. Nestor, P.G�.,�1J.�L1�� North Carolina Geologist License 1027 ECS Southeast, LLP is permitted to practice geology/engineering in North Carolina. The certification number of the corporation is C-406 for geology. Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 TABLE OF CONTENTS 1.0 BACKGROUND............................................................................................................................ 1 2.0 RISK CHARACTERIZATION........................................................................................................... 3 3.0 RECEPTOR INFORMATION.......................................................................................................... 6 4.0 SITE GEOLOGY AND HYDROGEOLOGY......................................................................................... 7 5.0 FIELD ACTIVITIES........................................................................................................................ 8 6.0 LABORATORY ANALYTICAL RESULTS........................................................................................... 9 7.0 CONCLUSIONS...........................................................................................................................11 8.0 RECOMMENDATIONS................................................................................................................11 9.0 QUALIFICATIONS.......................................................................................................................11 10.0 REFERENCES............................................................................................................................12 FIGURES Figure 1 Site Location Map Figure 2 Site Map Figure 3 Parcel Identification Map Figure 4 Sample Location Map TABLES Table 1 UST Information Table 2 Site and Adjacent Property Ownership Table 3 Summary of Soil Analytical Results for VOCs and SVOCs by EPA Methods 8260 and 8270D Table 4 Summary of Soil Analytical Results for Aliphatic and Aromatic Fractions by MADEP Method Table 5 Summary of Groundwater Analytical Results for VOCs and SVOCs by Standard Method 6200B and EPA Method 625.1 Table 6 Summary of Groundwater Analytical Results for Aliphatic and Aromatic Fractions by MADEP Method APPENDICIES Appendix A Notice of Regulatory Requirements — November 9, 2018 Appendix B Water Supply Well Questionnaires and Tracking Information Appendix C Boring Log Appendix D Laboratory Data Sheets and Chain of Custody Records Appendix E NCDEQ Well Construction Permit and Well Construction Record Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 1.0 BACKGROUND 1.1 Site History The site is the former Charlotte Correctional Center located at 4101 Meadow Oaks Drive in Charlotte, Mecklenburg County, North Carolina on Parcel Identification Number (PIN) 14326112 (Figure 1 and Figure 2). The site is approximately 46.81 acres in size. ECS understands that the site was last utilized as a correctional facility and is owned by the North Carolina State Highway and Public Works Commission. The site is presently unoccupied and vacant. A No. 2 fuel oil UST with nominal capacity of 10,000 gallons was located on -site adjacent to a boiler house with a partial basement. ECS understands that this UST was used to provide heating oil for consumptive use on the premises where stored. ECS understands that this UST is considered by the North Carolina Department of Environmental Quality (NCDEQ) to be a non - regulated, commercial UST. Evidence of a release was discovered during a Phase II Environmental Site Assessment (Phase II ESA) performed by ECS in April and May 2018 as part of due diligence for a potential real estate transaction (ECS Project No. 49:6535-B). Four soil borings (SB-1 through SB-4) were advanced around the UST on April 23, 2018 and samples were collected and analyzed for total petroleum hydrocarbons (TPH) as gasoline range organics (GRO) and diesel range organics (DRO) by ultraviolet fluorescence (UVF). The analyses for samples from boring SB-3 collected from 5 to 10 feet below ground surface (bgs) indicated the presence of TPH-GRO and TPH-DRO at concentrations of 3,149 and 24,639 milligrams per kilogram (mg/kg), respectively. Boring SB-3 was on the east side of the UST near the southwest corner of the boiler house. The analytical results for samples associated with the other three borings were below laboratory detection limits. On September 7, 2018, ECS Geotechnical personnel noticed apparent petroleum hydrocarbons odors in a geotechnical boring (B-24) located approximately 100 feet northeast of the UST. ECS screened samples from this boring with a photoionization detector (PID) and selected the sample with the highest PID reading for laboratory analysis. Laboratory analytical results for the soil sample collected from boring B- 24 at a depth of 8.5 to 10.0 feet bgs indicated concentrations of several VOCs and SVOCs. The concentrations of 1-methylnaphthalene (10.9 mg/kg), 2-methyl naphthalene (13.7 mg/kg), naphthalene (5.27 mg/kg as a SVOC), isopropylbenzene (2.23 mg/kg), and naphthalene (9.78 mg/kg as a VOC) exceed MSCCs for the leaching from soil to groundwater exposure scenario. Several other VOCs and SVOCs associated with this sample were detected at concentrations below MSCCs for the various exposure scenarios. On September 21, 2018, a 10,000-gallon UST was removed from the site. (Note that the NCDEQ Registered Tanks Database indicated that a 5,000-gallon UST was present and not a 10,000-gallon UST.) Field screening of soil with a photoionization detector (PID), visual observations of stained soil, and petroleum odors exuded from soil indicated a petroleum release had occurred. Approximately 50 tons of petroleum -impacted soil was excavated and removed from the site for offsite treatment/disposal. Samples were collected from the base and sidewalls of the resulting excavation. The sample from the base of the excavation was designated B-1. The samples from the four sidewalls were designated N-1, E-1, S-1, and W-1 and were associated with the north, east, south, and west sidewalls, respectively. Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 Laboratory analytical results of soil samples B-1 and S-1 did not indicate targeted constituents above the laboratory reporting limits. Laboratory analytical results of soil sample N-1 indicated concentrations of several VOCs and SVOCs. The concentrations of p-isopropyltoluene (2.23 milligrams per kilogram [mg/kg]) and naphthalene (0.732 mg/kg) exceed maximum soil contaminant concentrations (MSCCs) established be the NCDEQ UST Section for the leaching from soil to groundwater exposure scenario. The VOC, 1,3,5- trimethyl benzene, was detected at 0.345 mg/kg which is below MSCCs for the various exposure scenarios. The concentration of aromatic hydrocarbons containing 9 to 22 carbon atoms (C9 — C22 Aromatics) (137 mg/kg) associated with sample N-1 exceeded the MSCC for the leaching from soil to groundwater exposure scenario. Laboratory analytical results of soil sample E-1 detected concentrations of several VOCs and SVOCs. The concentrations of 1-methylnaphthalene (31.3 mg/kg), 2-methylnaphthalene (44.8 mg/kg), p isopropyltoluene (2.39 mg/kg), and naphthalene (5.34 mg/kg) exceed MSCCs for the leaching from soil to groundwater exposure scenario. Several other VOCs and SVOCs associated with sample E-1 were detected at concentrations below MSCCs for the various exposure scenarios. The concentration of C9 — C22 Aromatics (2,174 mg/kg) associated with sample E-1 exceeds the MSCCs for the leaching from soil to groundwater and residential exposure scenarios. The concentration of aliphatic hydrocarbons containing 9 to 18 carbon atoms (C9 — C18 Aliphatics) (5,137 mg/kg) associated with sample E-1 exceeds the MSCCs for the leaching from soil to groundwater and residential exposure scenarios. Laboratory analytical results of soil sample W-1 detected concentrations of several VOCs and SVOCs. The concentrations of these VOCs and SVOCs did not exceed MSCCs established for the three exposure scenarios. The concentration of aromatic hydrocarbons containing 9 to 22 carbon atoms (C9 — C22 Aromatics) exceeds the MSCC for the leaching from soil to groundwater exposure scenario. On November 9, 2018, NCDEQ issued a Notice of Regulatory Requirements (NORR) in which it indicated a Limited Site Assessment was required for this site. A copy of the NORR is included as Appendix A 1.2 UST Information One 10,000-gallon heating oil UST was located at the site. The UST measured approximately 10 feet in diameter and 17 feet in length. The heating oil tank supplied fuel to the boiler in the boiler house located immediately adjacent to the UST. ECS understands that this UST was used to provide heating oil for consumptive use on the premises where stored. ECS understands that this UST is considered by the NCDEQ to be a non -regulated, commercial UST. UST information is summarized on Table 1. 1.3 Future Use of Property The subject property has been marketed for sale by the State of North Carolina. ECS understands that Exeter 4100 Meadow Oak, LLC is in negotiations with the State of North Carolina to purchase the property for redevelopment for industrial/commercial purposes. 2 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 2.0 RISK CHARACTERIZATION The answers in the following questionnaire are intended to provide data for the assignment of the risk classification for the site. Limited Site Assessment Risk Classification and Land Use Form Part I - Groundwater/Surface Water/Vapor Impacts High Risk 1. Has the discharge or release contaminated any water supply well including any used for non - drinking purposes? NO 2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the discharge or release? NO 3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial cooling, filling swimming pools) located within 250 feet of the source area of the release or discharge? NO An out -of service water supply well is located approximately 380 feet west and crossgradient of the UST. 4. Does the groundwater within 500 feet of the source area of the discharge or release have the potential for future use in that there is no other source of water supply other than the groundwater? NO The site is within the city limits of Charlotte and municipal water is available. 5. Do vapors from the discharge or release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to public health, public safety, or the environment? NO 6. Are there any other factors that would cause the discharge or release to pose an imminent danger to public health, public safety, or the environment? NO 3 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 Intermediate Risk 7. Is a surface water body located within 500 feet of the source area of the discharge or release? NO The closest water body to the area of the release is an unnamed tributary to Taggart Creek and is located approximately 730 feet north of the UST. 8. Is the source area of the discharge or release located within a designated wellhead protection area as defined in 42 USC 300h-7(e)? NO 9. Is the discharge or release located in the Coastal Plain Physiographic region as designated on a map entitled "Geology of North Carolina" published by the Department in 1985? NO 10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels established by the Department? NO Part II - Land Use Property Containing Source Area of Discharge or Release 1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO Vacant prison buildings, including sleeping quarters, and other structures are present and unoccupied. These facilities have not been utilized since 2011. 2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? NO 3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? NO Vacant prison buildings and other structures are present and unoccupied. The site is being considered for redevelopment as an industrial property. 4. Can children visit the property? YES 5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel, or both)? NO Access to portions of the site are restricted by fences and razor wire. The UST was located outside the fence. 4 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 6. Does pavement, buildings, or other structures cap the contaminated soil? NO 7. What is the zoning status of the property? The property is presently zoned residential (R-22MF) 8. Is the use of the property likely to change in the next 20 years? YES 4100 Meadow Oak, LLC is in negotiations with the State of North Carolina to purchase the property for redevelopment for industrial/commercial purposes. Property Surrounding Source Area of Discharge or Release 9. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or temporary)? Approximately 600 feet to the southeast. (Double Tree Inn) 10. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? The Veterans Administration Health Care Center is located approximately Z300 feet northeast of the subject site. 11. What is the zoning status of properties in the surrounding area? The property located immediately north of the subject site is zoned industrial (1-1). Properties located immediately to the east of the subject property across the Billy Graham Parkway are zoned industrial (1-1[CD]). The property located immediately to the southwest of the subject property across West Tyvola Road is zoned commercial (0-2[CD]). And properties located immediately to the southwest and west of the subject property are zoned industrial (I-1 and 1-2). 12. Briefly characterize the use and activities of the land in the surrounding area. The area surrounding the site is near the Charlotte -Douglas Airport and used for commercial and industrial purposes. 5 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 3.0 RECEPTOR INFORMATION 3.1 Water Supply Wells Visual evidence of water supply wells, such as well houses or "fake" rocks, was not observed within 1,500 feet of the source area during the site reconnaissance. On January 10, 2019 ECS forwarded water supply well questionnaires by via certified mail (return -receipt -requested) to eleven property owners within 500 feet of the site (Table 2 and Figure 3). Three questionnaires were completed and returned. One questionnaire was returned as undeliverable as addressed. The respondents indicated that water supply wells were not present on their properties. The completed water supply well questionnaires and tracking information are included in Appendix C. 3.2 Public Water Supplies Information obtained from the area receptor survey indicates that the Charlotte -Mecklenburg Utility Department provides municipal water to the area. Water meters and fire hydrants were observed in the survey area. 3.3 Surface Water As determined from the Mecklenburg County Geographic Information System (GIS), an eastward flowing steam roughly bisects the subject site. This stream flows into Taggarts Creek approximately 330 feet east of the subject site. Surface water runoff originating in the vicinity of the UST appears to flow in a northwesterly direction towards the tributary to Taggarts Creek. 3.4 Wellhead Protection Areas There are no designated wellhead protection areas as defined by 42 USC 300h-7(e) located within 1,500 feet of the site. 3.5 Subsurface Structures There are no subsurface structures other than buried utilities located in the vicinity of the release. Groundwater was measured approximately 28 feet bgs; therefore the utilities should not intercept the groundwater or act as a pathway for vapors. 3.6 Land Use The site is currently vacant. C.1 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 3.7 Property Owners and Occupants The names and addresses of the property owners of the site and adjoining properties are included in Table 2. A portion of the Mecklenburg County GIS map with adjacent property locations is presented as Figure 3. 4.0 SITE GEOLOGY AND HYDROGEOLOGY The Geologic Map of North Carolina (Brown, 1985) describes the bedrock geology in the vicinity of the subject property as "granitic rock" and is further described as locally pinkinsh gray, massive to weakly foliated; contains hornblende". The map code on the Geologic Map of North Carolina for the bedrock at the subject property is DOg indicated the bedrock at the subject property was formed in the Devonian Period (380 to 410 million years before present). The subject site lies within the Piedmont physiographic province. Daniels and Dahlen (2002) describe the geology and hydrogeology of the Piedmont and Blue Ridge physiographic provinces as follows: a complex, two-part, regolith-fractured crystalline rock aquifer system. Thickness of the regolith throughout the study area is highly variable and ranges from 0 to more than 150 feet. The regolith consists of an unconsolidated or semi - consolidated mixture of clay and fragmental material ranging in grain size from silt to boulders. Because porosities range from 35 to 55 percent, the regolith provides the bulk of the water storage within the Blue Ridge and Piedmont ground -water system. At the base of the regolith is the transition zone where saprolite grades into unweathered bedrock. The transition zone has been identified as a potential conduit for rapid ground -water flow. If this is the case, the transition zone also may serve as a conduit for rapid movement of contaminants to nearby wells or to streams with channels that cut into or through the transition zone. How rapidly a contaminant moves through the system largely may be a function of the characteristics of the transition zone." 7 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 5.0 FIELD ACTIVITIES 5.1 Soil Sampling On January 15, 2019, soil samples were collected at the location of monitoring well MW-1 by hydraulically driving a five-foot long, 1.5-inch diameter soil sampling probe into the subsurface using a track mounted Geoprobe® drill rig. Continuous soil samples were collected from grade to 35 feet the ground surface (bgs) using a soil sampling probe lined with a dedicated disposable clear plastic tube. After the soil sampling probe was driven, the clear plastic tube filled with soil was removed from the probe and cut open to expose the soil. ECS visually classified the soil collected from the boring and screened the soil samples for relative levels of volatile organic vapors using a flame ionization detector (FID). Appendix C includes a boring log. Soil samples were collected from 15 and 25 feet bgs and these samples were designated MW-1-15 and MW-1-25, respectively. Soil samples were not collected from above 15 feet bgs because this material was fill which was imported and placed after the UST was removed in October 2018. The drill rig and tools were decontaminated using a high-pressure steam cleaner and municipal water prior to the collection of soil samples. ECS placed samples into containers provided by Pace Analytical Services, LLC (Pace). Each container was labeled and placed in a cooler containing ice to maintain the samples at approximately 4° Celsius. The samples were then delivered to Pace in Huntersville, North Carolina to be analyzed for volatile organic compounds (VOCs) using EPA Method 8260, for semi -volatile organic compounds (SVOCs) using EPA Method 8270, and volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH) using the Massachusetts Department of Environmental Protection (MADEP) Method. A Chain of Custody Record was maintained and is included in Appendix D. 5.2 Monitoring Well Construction On January 15, 2019, ECS observed the installation of monitoring well MW-1 (Figure 4) using a track mounted Geoprobe® drill rig equipped with 4.25 inch hollow -stem augers. The drill rig and tools were decontaminated using a high-pressure steam cleaner and municipal water prior to the installation of the well. A borehole was drilled to a depth of 40 feet bgs. The diameter of the borehole was approximately 9 inches. Following the drilling of the borehole, the well was constructed with 2-inch I.D. schedule 40 PVC flushed -threaded casing and screen. The PVC screen and casing were lowered to the bottom of the borehole. A 15-foot length of slotted well screen with machined 0.010-inch slot widths and threaded bottom plug were installed at the bottom of the well. A solid section of PVC casing was placed above the screened interval and extended to a point approximately 0.25 foot below the ground surface. The annular space around the well was filled with washed fine filter sand to approximately 2 feet above the top of the screen. A minimum 2-foot thick seal of bentonite pellets was placed immediately above the sand pack. The remaining borehole was filled with Portland concrete grout. The top of the well casing was equipped with a lockable, water -tight manhole cover and well plug. L:3 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 Following completion of the well, the driller developed the well remove fines. Development was performed by over pumping the well the water level was drawn down to the pump intake and then allowing the well to recharge and repeating this process. At least three well volumes were evacuated during development. Appendix E includes the NCDEQ Well Construction Permit and the NCDEQ Well Construction Record. 5.3 Groundwater Sampling and Analysis Prior to sampling, the monitoring well was purged using an electric submersible variable speed sampling pump (Proactive Environmental Products, Stainless steel 12 volt Monsoon Model with Power Booster II LCD Controller). A new length of polyethylene tubing was connected to the pump and the pump was lowered to within 1 foot of the bottom of the well. ECS removed a minimum of three well volumes before reducing the flow rate and collecting samples. ECS directed groundwater being discharged from the tubing directly into containers provided by Pace. Each container was labeled and placed in a cooler containing ice to maintain the samples at approximately 4° Celsius. The samples were then delivered to Pace in Huntersville, North Carolina to be analyzed for VOCs using Standard Method 6200B, for SVOCs using EPA Method 625, and VPH and EPH using the MADEP Method. In addition, ECS requested that Pace tentatively identify and estimate concentrations of compounds for the ten highest non -target target peaks on the chromatograph for the EPA 625 analyses. These compounds are referred to as tentatively identified compounds (TICS). A Chain of Custody Record was maintained and is included in Appendix E. 6.0 LABORATORY ANALYTICAL RESULTS 6.1 Analytical Results for Soil Samples Laboratory results for soil samples are summarized in Tables 3 and 4. Table 3 summarizes results for VOC and SVOC analyses by EPA Methods 8260 and 8270, respectively. Table 4 summarizes results for VPH and EPH analyses by the MADEP Method. Table 4 also provides information regarding the concentrations of various aliphatic and aromatic hydrocarbon fractions. Laboratory analysis of soil sample MW1-15 detected the following VOCs at the indicated concentrations: sec -butyl benzene (0.0127 milligrams per kilogram [mg/kg]), isopropylbenzene (0.0065 mg/kg), p-isopropyltoluenetoluene (0.0277 mg/kg), methylene chloride (0.0321 mg/kg), naphthalene (0.112 mg/kg), n-propylbenzene (0.0074 mg/kg), 1,2,4- trimethyl benzene (0.0831 mg/kg), and 1,3,5- tri methyl benzene (0.296 mg/kg). Laboratory analysis of soil sample MW1-15 detected the following SVOCs at the indicated concentrations: 1-methylnaphthalene (12.3 mg/kg) and 2-methylnaphthalene (9.46 mg/kg). As shown in Table 3, the detected concentration of methylene chloride, 1- methylnaphthalene, and 2-methylnaphthalene exceed the maximum soil contaminant concentration (MSCC) established by the NCDEQ for the leaching from soil to groundwater exposure scenario. It should be noted that methylene chloride is not typically associated with petroleum and is considered by EPA to be a common laboratory contaminant and was flagged as such by the laboratory. 9 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 Various hydrocarbon fractions were detected in sample MW-1-15 through VPH and EPH analyses by the MADEP Method. As shown in Table 4, the concentration of aliphatic hydrocarbons in the C9 to C18 range as determined by analyses for both VPH and EPH associated with sample MW-1-15 was 530.3 mg/kg. The concentration of aromatic hydrocarbons in the C9 to C22 range as determined by analyses for both VPH and EPH associated with sample MW-1-15 was 307.1 mg/kg. Laboratory analysis of soil sample MW1-25 detected the following VOCs at the indicated concentrations: n-butylbenzene (0.0085 mg/kg), sec -butyl benzene (0.0067 mg/kg), ethylbenzene (0.0059 mg/kg), isopropylbenzene (0.0055 mg/kg), p-isopropyltoluenetoluene (0.0147 mg/kg), naphthalene (0.0359 mg/kg), n-propylbenzene (0.0085 mg/kg), 1,2,4- trim ethyl benzene (0.0535 mg/kg), and 1,3,5-trimethylbenzene (0.0133 mg/kg). As shown in Table 3, the detected concentrations do not exceed MSCCs established by the NCDEQ for the various exposure scenario. Various hydrocarbon fractions were detected in sample MW-1-25 through VPH and EPH analyses by the MADEP Method. As shown in Table 4, the concentration of aliphatic hydrocarbons in the C5 to C8 range as determined by analyses for VPH was 8.2 mg/kg. The concentration of aliphatic hydrocarbons in the C9 to C18 range as determined by analyses for both VPH and EPH associated with sample MW-1- 15 was equal to or greater than 18.2 mg/kg but less than 31.8 mg/kg. The concentration of aromatic hydrocarbons in the C9 to C22 range as determined by analyses for both VPH and EPH associated with sample MW-1-25 was equal to or greater than 17.6 mg/kg but less than 21.2 mg/kg. 6.2 Analytical Results for Groundwater Samples Laboratory results for groundwater samples are summarized in Tables 5 and 6. Table 5 summarizes results for VOC and SVOC analyses by Standard Method 6200B and EPA Method 625.1, respectively. Table 6 summarizes results for VPH and EPH analyses by the MADEP Method. Table 6 also provides information regarding the concentrations of various aliphatic and aromatic hydrocarbon fractions. Laboratory analysis of groundwater sample MW-1 did not detect either VOCs or SVOCs as analyzed by Standard Method 6200B and EPA Method 625.1, respectively. Ten non -target peaks were noted on the EPA Method 625.1 chromatograph for SVOCs and were reported by the laboratory. Nine of the peaks were reported as tentatively identified compounds (TICS) and the remaining peak was reported as unknown. The laboratory results included in Appendix E contains a TICS report. Laboratory analysis of groundwater sample MW-1 did not detect either aromatic or aliphatic hydrocarbon fractions as either VPH or EPH as analyzed by MADEP. 10 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 7.0 CONCLUSIONS Based on the results of the LSA, ECS concludes the following: • The subject property is currently vacant and unoccupied. • The subject property is being considered for purchase by Exeter 4100 Meadow Oak, LLC for redevelopment for industrial/commercial purposes. • Laboratory analysis of soil samples collected during UST Closure activities performed in September 2018 detected targeted compounds at concentrations above MSCCs for the leaching from soil to groundwater and/or residential exposure scenarios but less than MSCCs for the industrial/commercial exposure scenario. • Laboratory analysis of soil samples collected in January 2019 as part of the Phase I LSA detected targeted compounds at concentrations above MSCCs for the leaching from soil to groundwater exposure scenario but less than MSCCs for either the residential or industrial/commercial exposure scenarios. • Laboratory analysis of the groundwater sample collected from MW-1 in January 2019 as part of the Phase I LSA did not detect target analytes for analyses performed by Standard Method 6200B or EPA Method 625.1. • Laboratory analysis of the groundwater sample collected from MW-1 in January 2019 as part of the Phase I LSA did not detect target VPH or EPH analytes for analyses performed by the MADEP Method. • An out -of -service water supply well is located approximately 380 feet crossgradient from the location of the former UST. No other water supply wells were identified within 1,000 feet of the subject property. Municipal water service is available in the area. • No conditions which would trigger and intermediate of high risk calcification for the subject property were identified during the Phase I LSA. 8.0 RECOMMENDATIONS ECS recommends the following: • A copy of this Phase I LSA report be submitted to the NCDEQ, Mooresville Regional Office along with a request for issuance of a No Further Action Required Notice. • A Notice of Residual Petroleum be submitted to the NCDEQ, Mooresville Regional Office. • A copy of this report be provided to the current owner of the subject property and that the owner consult with its legal counsel regarding possible notification requirements. 9.0 QUALIFICATIONS The activities and evaluative approaches used in this assessment are consistent with those normally employed in assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information and the data obtained during our field activities. 11 Phase 1 Limited Site Assessment Report Former Charlotte Correctional Center 4100 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina Facility ID No. 00-0-0000030621 ECS Project 49-6535-L February 5, 2019 10.0 REFERENCES Brown, Philip M. et al, 1985, Geologic Map of North Carolina, North Carolina Department of Natural Resources and Community Development, scale 1:500,000. Daniel, Charles C. and Paul R. Dahlen, 2002, Preliminary Hydrogeologic Assessment and Study Plan for a Regional Ground -Water Resource Investigation of the Blue Ridge and Piedmont Provinces of North Carolina, United States Geological Survey Water -Resources Investigation Report 2002-4105. 12 FIGURES llf I A 152 f % SIT E Th e �rt Institute crf Clott e kii % 3GO m SOURCE: FIGURE 1 SITE LOCATION MAP USGS TOPOGRAPHIC MAP MEADOW OAK INDUSTRIAL CHARLOTTE WEST, NC 4101 MEADOW OAK DRIVE CHARLOTTE, MECKLENBURG COUNTY, NORTH 2016 CAROLINA ECS PROJECT NO. 49-6535-L j N. { IL 1200 ft OUT -OF -SERVICE WATER SUPPLY WELL i IL FORMER 1'IF 10,000-GALL Ot f UST M11107 ct / I" 1430 4-12 4 d4604.12a V, 1431, 10 14304125 14-K6112 SUBJECT SITE 500-FO RADIUS 1,000-FO T RADIUS IL 1430al.a; FORMER OCA ON 03 107 • OF 10,000 ALL ST 14326109 M 1 3031 41 ------- 30 -3199 143 1430319e Alt 401111V112 14326116 1 4a2 M273 01 A q1M 143272.03 0. 0.0175.035 0.07 Miles 14326117 ) E "*0, --1 i . I I I I - i . I I I J .1 1� S 14327204.. ThiF map or report is prepared forthe inventory of real 1pis pertywithin Mecklenburg County and o.o.mpiled from recorded deeds, plats, tax maps, surveys, planimetric maps, and other public records and data reme ntio n d public primary information should be consulted Users of this map or report are hereby notified that the a ' for ve rifi cation. Mecklenburg County and it mapping .ntracto.assume no legal responsibility for the information contained herein. NOTES: Radii shown are approximate and are centered on the former 10,000-gallon UST. Parcel numbers are shown. The subject property is on Parcel No. 14326112 and is outlined in green. SOURCE: N FIGURE 3 PARCEL IDENTIFICATION MAP MECKLENBURG COUNTY MEADOW OAK INDUSTRIAL GEOGRAPHIC INFORMATION SYSTEM 4101 MEADOW OAK DRIVE CHARLOTTE, MECKLENBURG COUNTY, NORTH FEBRUARY 4, 2019 CAROLINA SCALE AS SHOWN ECS PROJECT NO. 49-6535-L 4 f. LEGEND '+ - it O Approximate Soil and Groundwater - Sample Location Approximate UST Location SOURCE: ;N FIGURE 4 �F SAMPLE LOCATION MAP s GOOGLE EARTH MEADOW OAK INDUSTRIAL 2018 4101 MEADOW OAK DRIVE CHARLOTTE, MECKLENBURG COUNTY, NORTH SCALE AS SHOWN CAROLINA ECS PROJECT NO. 49-6535-1 TABLES TABLE 1: UST INFORMATION Former Charlotte Correctional Center 4101 Meadow Oaks Drive Charlotte, Mecklenburg County, North Carolina ECS Project No. 49-6535-L UST ID Last Previous Capacity Construction Tank Installation Status Release Number Contents Contents (in Gallons) Details Dimensions Date 10 feet 0 by 17 RemoRemo Removed 1 Heating Oil Heating Oil 10,000 Single Wall Steel 1964 Yes feet length 0 Notes: The NCDEQ Tanks Database indicates a 5,000-galIon single wall steel tank is present at Facility ID No. 00-0-0000030621 at 4100 Meadow Oaks Drive and this UST was temporarily closed. The UST which was removed on Sepatember 21, 2018 was a 10,000-gallon (nominal) UST. TABLE 2: SITE AND ADJACENT PROPERTY OWNERSHIP Former Charlotte Correctional Center 4101 Meadow Oaks Drive Charlotte, North Carolina Parcel ID Figure 3 Mecklenburg County PIN Owner Owner's Address Direction from Site Site 14326112 NC State Highway & Public Works Commission 1119 East Sugar Creek Road Charlotte, North Carolina 28205 Not Applicable 14304122 Naman Cascade, LLC c/o Naman Hotels PO Box4540 East Florence, South Carolina 29502 14304123 Lakepointe Corporate Center Associates, LLC c/o Childress Klein Properties, Inc. 301 S College Street Charlotte NC 28202 East 14304124 Lakepointe Corporate Center Associates, LLC c/o Childress Klein Properties, Inc. 301 S College Street East Charlotte NC 28202 14311110 City of Charlotte Property Management 600 East 4th Street West Charlotte NC 28202 14311109 BIFIN LTD c/o Biesse America, Inc. 4110 Meadow Oak Drive West Charlotte NC 28208 14326110 BIFIN LTD c/o Biesse America, Inc. 4110 Meadow Oak Drive Charlotte NC 28208 Southwest 14326111 BIFIN LTD c/o Biesse America, Inc. 4110 Meadow Oak Drive Southwest Charlotte NC 28208 14326114 Spratt Legacy Partners, LLC PO Box 43586 Charlotte NC 28215 Southwest 14327301 Cole of Charlotte NC, LLC c/o Ryan PO Box 4900, Dept 604 South Scottsdale, AZ 85261 14327302 Cole of Charlotte NC, LLC c/o Ryan PO Box 4900, Dept 604 Southeast Scottsdale, AZ 85261 TABLE 3: SUMMARY OF SOIL ANALYTICAL RESULTS FOR VOCS AND SVOCS EPA METHODS 8260 AND 8270D Former Charlotte Correctional Center 4101 Meadow Oaks Drive Charlotte, North Carolina ECS Project No. 49-6535-L Parameter ANALYTICAL RESULTS COMPARISION CRITERIA Sample ID MW1-15 MW1-25 MAXIMUM SOIL CONTAMINANT CONCENTRATIONS FOR VARIOUS EXPOSURE SCENARIOS (mg/kg) Collection Date 1/15/19 SOIL TO GROUNDWATER RESIDENTIAL INDUSTRIAL/COMMERCIAL Volatile Organic Compounds by EPA Method 8260 n-Butylbenzene 0.0085 4.3 626 16,350 sec-Butylbenzene 0.0127 0.0067 3.3 626 16,350 Ethylbenzene 0.0059 4.9 1,560 40,000 Isopropyl benzene (Cumene) 0.0065 0.0055 1.7 1,564 40,880 p-Isopropyltoluene 0.0277 0.0147 0.12 100 4,000 Methylene Chloride 0.0321 ).0212 0.02 85 763 Naphthalene 0.112 0.0359 0.16 313 8,176 n-Propylbenzene 0.0074 0.0085 1.7 626 16,350 1,2,4-Trimethyl benzene 1 0.0831 1 0.0535 8.5 782 20,440 1,3,5-Trimethyl benzene 1 0.0296 0.0133 8.3 782 20,440 Semivolatile Organic Compounds by EPA Method 8270D 1-Methylnaphthalene 12.3 0.004 20 100 2-Methylna hthalene 9.46 3.6 63 1,635 Notes: Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm) BRL = Below Laboratory Reporting Limit PSRG = Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (February 2018) Bold denotes concentration exceeds the IH! the Soil -to -Water Maximum Contaminant Concentration Underline denotes concentration exceeds the IHSB Industrial/Commercial PSRG Italics denotes concentration exceeds the IHSB Protection of Groundwater PSRG NS = No Standard J = Detected but below the Reporting Limit; therefore, result is an estiamted concentration VOCS - Volatile Orgainc Compounds SVOCS - Semi -Volatile Orgainc Compounds TABLE 4: SUMMARY OF SOIL ANALYTICAL RESULTS FOR ALIPHATIC AND AROMATIC FRACTIONS BY MADEP METHOD PROJECT: MEADOW OAK INDUSTRIAL ECS PROJECT NO: 49-6535-L SOIL SAMPLE: MW1-15 MAXIMUM SOIL CONTAMINANT CONCENTRATIONS (MSCCs) 1 DEPTH OF COLLECTION: 15 FOOT FOR VARIOUS EXPOSURE SCENARIOS DATE OF COLLECTION: 01/15/2019 (mg/kg) CONCENTRATION SUM OF DETECTED BY VPH AND EPH TOXICOLOGICALLY DEFINED HYDROCARBON ANALYTICAL HYDROCARBON ANALYTICAL LABORATORY CONCENTRATIONS FRACTION FRACTION METHOD (mg/kg) (mg/kg) SOIL TO GROUND WATER RESIDENTIAL INDUSTRIAL/COMMERCIAL C5 - C8 ALIPHATICS C5 - C8 ALIPHATICS VPH <3.5 <3.5 68 939 24,528 C9 - C18 ALIPHATICS C9 - C12 ALIPHATICS VPH 49.3 530.3 540 1,500 40,000 C9 - C18 ALIPHATICS EPH 481 C19 - C36 ALIPHATICS C19 - C36 ALIPHATICS EPH <144 <144 CONSIDERED IMMOBILE 31,000 810,000 C9 - C22 AROMATICS C9 - C10 AROMATICS VPH 25.1 307.1 31 469 12,264 C11 - C22 AROMATICS EPH 282 SOIL SAMPLE: MW1-25 MAXIMUM SOIL CONTAMINANT CONCENTRATIONS (MSCCs) DEPTH OF COLLECTION: 15 FOOT FOR VARIOUS EXPOSURE SCENARIOS DATE OF COLLECTION: 01/15/2019 (mg/kg) CONCENTRATION SUM OF DETECTED BY VPH AND EPH TOXICOLOGICALLY DEFINED HYDROCARBON ANALYTICAL HYDROCARBON ANALYTICAL LABORATORY CONCENTRATIONS FRACTION FRACTION METHOD (mg/kg) (mg/kg) SOIL TO GROUND WATER RESIDENTIAL INDUSTRIAL/COMMERCIAL C5 - C8 ALIPHATICS C5 - C8 ALIPHATICS VPH 8.2 8.2 68 939 24,528 > OR = 18.2 C9 - C18 ALIPHATICS C9 - C12 ALIPHATICS VPH 18.2 BUT 540 1,500 40,000 C9 - C18 ALIPHATICS EPH <13.6 <31.8 C19 - C36 ALIPHATICS C19 - C36 ALIPHATICS EPH <13.6 <13.6 CONSIDERED IMMOBILE 31,000 810,000 > OR = 17.6 C9 - C22 AROMATICS C9 - C10 AROMATICS VPH 7.6 BUT 31 469 12,264 C11 - C22 AROMATICS EPH <13.6 <21.2 SAMPLES ANALYZED BY THE MASSACHUSETTS DEPARTMENT OF ENVIRONEMNTAL PROTECTION (MADEP) METHOD mg/kg - MILLIGRAMS PER KILOGRAM VPH -VOLATILE PETROLEUM HYDROCARBONS. EPH - EXTRACTABLE PETROLEUM HYDROCARBONS. BOLD TEXT INDICATES MSCC FOR SOIL TO GROUNDWATER EXPOSURE SCENARIO WAS EXCEEDED. MADEP - MASSACHUSETTS DEPARTMENT OF ENVIRONEMNTAL PROTECTION TABLE 5: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS FOR VOCS AND SVOCS BY STANDARD METHOD 6200B AND EPA METHOD 625.1 Former Charlotte Correctional Center 4101 Meadow Oaks Drive Charlotte, North Carolina ECS Project No. 49-6535-L Parameter ANALYTICAL RESULTS Sample ID MW-1 Collection Date 1/18/19 Volatile Organic Compounds by Standard Method 6200B No Volatile Organic Compounds by Standard Method 6200B Semi -Volatile Organic Compounds by EPA Method 625.1 No Semi -Volatile Organic Compounds by EPA Method 625.1 TABLE 6: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS FOR ALIPHATIC AND AROMATIC FRACTIONS Former Charlotte Correctional Center 4101 Meadow Oaks Drive Charlotte, North Carolina ECS Project No. 49-6535-L SAMPLE ID: MW-1 DATE COLLECTED: 01/18/2019 NORTH CAROLINA REGULATORY LIMITS CONCENTRATION SUM OF GROSS DETECTED BY VPH AND EPH 15A NCAC 2L CONTAMINANT TOXICOLOGICALLY DEFINED HYDROCARBON ANALYTICAL HYDROCARBON ANALYTICAL LABORATORY CONCENTRATIONS STANDARD LEVEL FRACTION FRACTION METHOD (ug/1) (ug/1) (ug/1) (ug/1) C5 - C8 ALIPHATICS C5 - C8 ALIPHATICS VPH <50.0 <98.0 420 42,000 C9 - C12 ALIPHATICS VPH <50.0 C9 - C18 ALIPHATICS <148 4,200 4,200,000 C9 - C18 ALIPHATICS EPH <98.0 C19 - C36 ALIPHATICS C19 - C36 ALIPHATICS EPH <98.0 <98.0 42,000 42,000,000 C9 - C10 AROMATICS VPH <50.0 C9 - C22 AROMATICS <148 210 210,000 C11 - C22 AROMATICS EPH <98.0 SAMPLES ANALYZED BY THE MASSACHUSETTS DEPARTMENT OF ENVIRONEMNTAL PROTECTION (MADEP) METHOD VPH -VOLATILE PETROLEUM HYDROCARBONS. EPH - EXTRACTABLE PETROLEUM HYDROCARBONS. APPENDIX A NOTICE OF REGULATORY REQUIREMENTS NOVEMBER 9, 2018 ROY COOPER Governor MICHAEL S. REGAN Secrerary MICHAEL SCOTT Director Adam Duerr Exeter 4100 Meadow Oak, LLC 6285 Barfield Road, Suite 224 Atlanta, GA 30328 Dear Mr. Duerr: NORTH CAROLINA Environmental Quality November 09, 2018 Re: Notice of Regulatory Requirements 15A NCAC 2L .0405 Risk -based Assessment and Corrective Action for Petroleum Underground Storage Tanks Exeter Meadow Oak 4101 Meadow Oak Drive, Charlotte Mecklenburg County Incident number: 40849 Risk Classification: Unknown The UST Closure Report received by the UST Section, Division of Waste Management, Mooresville Regional Office on October 24, 2018 has been reviewed. The report indicates that soil contamination exceeds the lower of the residential or soil -to -groundwater maximum soil contaminant concentration (MSCCs) established in Title 15A NCAC 2L .0411. Therefore, the UST Section hereby confirms that you must comply with assessment and reporting requirements of Title 15A NCAC 2L .0405, within the timeframes specified in the attached rule. The requirements of Title 15A NCAC 2L .0405 include the preparation and submittal of a Limited Site Assessment (LSA) Report, in accordance with the rule and the most recent version of the Guidelines forAssessment and Corrective Action for UST Releases, within 120 days of discovery of the release. Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer, certified by the State of North Carolina, is required to prepare and certify all reports submitted to the Department of Environmental Quality in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b). NORTH C+4RpL'Yn� Q�5 uf EmlmmYeHsl 9� r North Carolina Department of Environmental Quality I Division of Waste Management Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville. North Carolina 28115 704.663.1699 Please note that before you sell, transfer, or request a "No Further Action" determination for a property that has not been remediated to below "unrestricted use" standards, you must file a Notice of Residual Petroleum ("Notice") with the Register of Deeds in the county where the property is located (NCGS 14313-279.9 and 14313-279.11). Failure to comply with the State's rules in the manner and time specified may result in the assessment of civil penalties and/or the use of other enforcement mechanisms. If you have any questions regarding trust fund eligibility or reimbursement from the Commercial or Noncommercial Leaking Petroleum Underground Storage Tank Cleanup Funds, please contact the UST Section Trust Fund Branch at (919) 707-8171. If you have any questions regarding the actions that must be taken or the rules mentioned in this letter, please contact me by email at Trudy.Beverly@ncdenr.gov or telephone at (704) 235-2182. Sincerely, a �Je{�cl Trudy Beverly, L.G. Hydrogeologist Mooresville Regional Office UST Section, Division of Waste Management, NCDEQ cc: Shawna Caldwell, Mecklenburg County Health Department Joseph Nestor, Matt McDuffie, Michelle Forness, & Brandon Fulton, ECS Southeast, LLP (via email) NORTH C.4R0.'+1A�E Q� un of En- r,nn H-, 9Nor North Carolina Department of Environmental Quality I Division of Waste Management Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville. North Carolina 28115 704.663.1699 APPENDIX 6 WATER SUPPLY WELL QUESTIONNAIRES AND TRACKING INFORMATION ECS SOUTHEAST, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F NC Registered Geologists Firm C-406 -406 SC Registered Engineering Firm 3239 January 9, 2018 Lakepointe Corporate Center Associates, LLC c/o Childress Klein Properties, Inc. 301 S College Street Charlotte NC 28202 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14304123 Cascade Pointe Boulevard Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ.) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (jnestoreecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecsiimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP fit, ?(, -7q f-b- ' Joseph P. Nestor, P.G., P.E. Matthew H. M`Duffie, P.G. Senior Environmental Project Manager Principal Geologist 0nestor ecslirnited.com mmcduffie@ecslimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed 01 /08/2019 Identity Parcel ID IGIS ID 14304123 114304123 Property Characteristics Legal desc TR-1 M33-709 Land Area 2.111 AC Fire District CITY OF CHARLOTTE Special District Account Type NC CORP Municipality CHARLOTTE Property Use INDUSTRIAL Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer No FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone IN:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone IN:VIEW COMMUNITY FLOODPLAIN TO VERIFY Ownership Owner Name Mailing Address C/O CHILDRESS KLEIN PROPERTIES INC 301 S COLLEGE ST CHARLOTTE NC 28202 LAKEPOINTE CORPORATE CENTER ASSOCIATES LLC 301 S COLLEGE ST CHARLOTTE NC 28202 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 17703-255 09/01/2004 17703-249 09/01/2004 17703-241 09/01/2004 17703-235 09/01/2004 $8,470,000.00 17703-229 09/01/2004 09944-094 09/28/1998 $0.00 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.02 Post Construction District Jurisdiction Charlotte District Central Catawba Situs Addresses Tied to Parcel CASCADE POINTE BV CHARLOTTE Stream Watershed Districts Stream Watershed Name SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 0.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds. plats, tax maps, Polaris 3C Map — Mecklenburg County, Nord] Carolina Date Printed: 1 /8/2019 6:48:00 PM 14307104 14304106 14304124 14304123 2211 . 222 I 7 1 2 � 353/1 / 340 14304125 GII 14326112 1 14303133 f S 1 3400 F /14303106 10 Alp �...� d� 4 4320109 IL 1 6110 01 _ 1 430310 - -- s 6111 1 •4 ���� ~~~ \I 1 03 14303105 4 14326114 *� 14327302 23 3 •14303198 } a 1 2 320 0 0 J9.0t75.035 0.07,E Miles � W E 113�61i15 i LI,. 190�z391 —� r �-YrtcrY+vnt'R��-- �ti s 1 This map or report is prepared for the inventory r,' real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, surreys, plani metric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for venfication. Mecklenburg County and its mapp;ng contractors assume no legal responsibility for the information contained herein- Request for Water Supply Well Information A release of petroleum product or other .regulated material has occurred within 1500 feet of the property receiving this survey_ This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L _0405_ IncidentNambei 40849 Incident Name Exeter Meadow Oaks ('The above inftarnaation is to be completed by Responsl e . - or Tileir representative) Please Provide the Follo-%x-iug Information (to the best of your knowledge) Name and telephone number of person completing the survey Address of property receiving survey _ Cit Y Gontnty What is the source of drinking water for this property? Public Water .l Water Supply Well I Stream Intake 7 Other lease explain below Is there a water supply well on this ,property? Yes 1 No If "No" disregard remaining questions and returni survey Dame and address of owner(s) of property with water supply well Hole many water supply wells are on this property? INhat .is the well(s) used for? (check all that apply) Thinking . Irrigation . Swimming Pool Water Livestock , Other (specify) . I'Vel.l not used How mails residences are connected to the well (list addresses)? How deep is the well(s)? Date well was installed' What is the casing depth of the well(s)? JA711at is the screen inter -,-al of the well(,,)? Additional water supply well information, (This hart to be completed by Responsible Party or their representative) Please return completed survey to by January30, usltlg ogle of the follojti-ing ECS Southeast, LLP; 2019 methods: Fax to C61; •L1_1:1.1:1 �.'YTaIl tll �. Fcti 5r�utneasl, I.,I»1 ,. L1[lu: i Nestor; 1812 r.e„1*,i- Pc,rit 17rive guile n; Citar•intte, NC 111217 3. Telephone 704-280-7422 4. E-mail to jnestor@ecsIimited.com It t (--m have aIn giiestions. please coliiact r ie l'OilSi�17",dicated abo5: e or t.tle '-NC DENR. Di'.'1�IO11 a.f ET�'aste .�rallagetlie¢:t. UST Section Trl.idy lltvcrly Regional Office a. 704-235-21112 ECrwSex ECS SOUTHEAST, L L P "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F NC Registered Geologists Firm C-406 -406 SC Registered Engineering Firm 3239 January 9, 2018 Lakepointe Corporate Center Associates, LLC c/o Childress Klein Properties, Inc. 301 S College Street Charlotte NC 28202 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14304124 Cascade Pointe Boulevard Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ.) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (inestor@ecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com January 9, 2019 If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP r � q,x�f-ojz " Joseph P. Nestor, P.G., P.E. Matthew H. M`Duffie, P.G. Senior Environmental Project Manager Principal Geologist lnestor@ecsiimited.com mmcduffie@ecsiimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 !6- POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed Identity Parcel ID GIS ID 14304124 114304124 Property Characteristics Legal desc COS M33-709 Land Area 0.599 AC Fire District CITY OF CHARLOTTE Special District Account Type INDIVIDUAL Municipality CHARLOTTE Property Use INDUSTRIAL COMMON AREA Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer No FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUT:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN TO VERIFY Situs Addresses Tied to Parcel CASCADE POINTE BV CHARLOTTE 01 /08/2019 Ownership Owner Name Mailing Address C/O CHILDRESS KLEIN 301 SOUTH COLLEGE ST PROPERTIES UNIT 2800 CHARLOTTE NC 28202 LAKEPOINTE CORPORATE 301 SOUTH COLLEGE ST CENTER PROPERTY UNIT 2800 OWNERS ASSOCIATION CHARLOTTE NC 28202 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 31469-71 12/30/2016 17703-255 09/01/2004 17703-249 09/01/2004 17703-241 09/01/2004 17703-235 09/01/2004 $8,470,000.00 17703-229 09/01/2004 09944-094 09/28/1998 $0.00 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.02 Post Construction District Jurisdiction Charlotte District Central Catawba Stream Watershed Districts Stream Watershed Name I SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 0.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G Map — Mecklenburg County, North Carolina Date Printed: 1/8/2019 6:48:00 PM 14307104 2221 14304106 14304124 4123 221, 222 . ... . ... 3408 Ilk, 25 143041 14326112 t 14303133 3400/ /14303106 -ere 01 f4,30310 14303105 14326114 1432-73W 14303198- 2320 4123 qlM p� 0 N •. . 1111111,111, E kO �0.0f75.035 0.071 Miles .1 91 A It AII This map or report is prepared forthe inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, surveys, planimetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification. Mecklenburg County and its mapping contractors assume no legal responsibility for the information contained herein. ly3C)y lay Cc, 5e"1 de- PC, %V1 Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405. Incident Number; 40849 Incident NaMeL Exeter Meadow Oaks (The above inforivatian Is to a completed ley Responsi a ,ofleir represeit a I` >? Please Provide the Following Information {to the best of -our knowledge) Name and telephone number of person completing the survey Address ofproperty receiving sun�ey _ City Count What is the source of drinking water for this property? Public Water 1 Water Supply Well / Stream Intake f Other lease explain below' Is there a water supply- well on this property? Yes / No If "No" disregard remaining questions and return sur�we. Name and address of owner(s) of property with water supply well Hole maIly water su2ply wells are on this property? What is the well(s) used for? (check all that apply) Drinking . Irrigation Swimming Pool Water Livestock Other (specify) Well not used Hoxx many residences are connected to the well (list addresses)? How deep is the well(s)? Date -well -ovas installed" iArhat is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information: is Dart to be completed by Responsible Party or their representati--e) ase return completed surAre r to by January 30, using one of the following ECS Southeast, LLP; 2019 t11' F!, ar• to :O ECT Southeast, LLP; Attn: j Nestor: 181Z Cei,ter Park Drive S,aite D; Charlotte. NC 28ZI7 _ , Telephone 704-280-7422 4. E-mail to jnestor@ecslimited.com It y'Clll have ally CiLle5tI0I15- l3 ease col:;aCt t e consultant indicated abme or the V(=' DE\R DES i�1o11 of Wa;te 1�1,wagenler.t. 1 ST Section Trudy Beverly Regional Office a 704-235-2182 ECS SOUTHEAST, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F-1078 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 January 9, 2018 City of Charlotte Property Management 600 East 4th Street Charlotte NC 28202 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14311110 2801 Horseshoe Lane Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ, ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ.) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (inestar(Tecslimited.cam). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP Joseph P. Nestor, P.G., P.E. Matthew H. M`Duffie, P.G. Senior Environmental Project Manager Principal Geologist inestor@ecslimited.com mmcduffie@ecslimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 1 2 Ri- POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed: 01 /08/2019 Identity Parcel ID GIS ID 14311110 114311110 Property Characteristics Legal desc NA Land Area 9.67 AC Fire District CITY OF CHARLOTTE Special District Account Type EXEMPT Municipality CHARLOTTE Property Use INDUSTRIAL Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer I Yes FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUTMIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN TO VERIFY Situs Addresses Tied to Parcel 2801 HORSESHOE LN CHARLOTTE Ownership Owner Name Mailing Address CITY OF CHARLOTTE 600 E 4TH ST CHARLOTTE NC 28202 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 16223-893 10/02/2003 $580,000.00 08/23/1994 $0.00 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.03 Post Construction District Jurisdiction Charlotte District Central Catawba Stream Watershed Districts Stream Watershed Name I SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 10.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G Map — Mecklenburg County, North Carolina Date Printed: 1/8/2019 3:35:29 PM 14309107 �44y e I ` 143 0,7.104 N. I{I $N i 143267,12'' • `t — ��ear< Lace s � Ilk g `� 14326109 14� a� 432 304 ; p , 14326114 R 14327302 43263 `�� 14326116' sNo {1„b12�ip 0.05 Miles 14327 do 1432 6117 his map or report is prepared tortNe i ventory of re propertywt in MeCAlOnUL ecorded deeds, p a s, tax maps, surveys, planimetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification. Mecklenburg County and its mapping contractors assume no legal reWonsibility for the information contained heroin. 1143i1110 Q66l Hoa�,�l�oe L-, e Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405- Incident Number: 40849 Incident Name Exeter Meadow Oaks (Tile above information is t0 be completed by Responsi e Fany or their represell a 1Vt Please Provide the Following Information (to the best of your knowledge) Name and telephone number of person completing the survey Address of property receiving surrey c1ty County What is the source of drinking water for this property? Public Water / -Water Supply Well / Stream Intake Other (please : lease explain below IS there a water supply well on this property? Yes / No If "No" disregard remaining questions and return stuvey Name and address of owner(s) of property with water supply well How many water supply wells are on this property? What is the well(s) used for? (check all that apply) .Drinking . Irrigation . Swimming Pool Water Livestock , Other (specifi.) Well not used Hoti+ many residences are connected to the well (list addresses)? How deep is the well(s)? Late well was installed^ What is the casing depth of the well(s)? 1A711at is the screen inter,,al of the well(s)? Additional water supply well information: (Tills part to be completed by Responsible Party or their representative) Please returIl completed .Survey to by January 30, using one of the following 111eChOdS: ECS Southeast, LLP; 2019 Fax to :1:. io ECS Southeast, 1111; Attu: j Nestor; 11312 (:enter Park Drive Suite 1); Charlotte, NC 28L,17 3 Telephone 704-280-7422 -1 E-mail to jnestor@ecshmited.coni If ycm have ally questioIs. please collt;lct the coIlsultant indicated abo-., e or the NC' DE R. DIA-IS1011 of %Waste Mai-agenient_ UST Section I' tidy Deveily Regional Office 1 701 '!35-2t1.i2 ECS SOUTHEAST, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F-1078 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 January 9, 2018 Naman Cascade, LLC c/o Naman Hotels PO Box 4540 Florence SC 29502 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14304122 2227 Cascade Pointe Boulevard Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (ir,estor2ecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP Joseph P. Nestor, P.G., P.E. Matthew H. McDuffie, P.G. Senior Environmental Project Manager Principal Geologist jnestor@ecslimited.com mmcduffie@ecslimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed Identity Parcel ID GIS ID 14304122 114304122 Property Characteristics Legal desc TR-2 M33-709 Land Area 4.183 AC Fire District CITY OF CHARLOTTE Special District Account Type NON -NC CORP Municipality CHARLOTTE Property Use INDUSTRIAL Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer I No FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone IN:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone IN:VIEW COMMUNITY FLOODPLAIN TO VERIFY Situs Addresses Tied to Parcel 2227 CASCADE POINTE BV CHARLOTTE 01 /08/2019 Ownership Owner Name Mailing Address NAMAN CASCADE LLC PO BOX 4540 FLORENCE SC 29502 C/O NAMAN HOTELS PO BOX 4540 FLORENCE SC 29502 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 30309-703 09/29/2015 $1,800,000.00 11709-156 11/09/2000 $1,400,000.00 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.02 Post Construction District Jurisdiction Charlotte District Central Catawba Stream Watershed Districts Stream Watershed Name I SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 10.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G Map — Mecklenburg County, Noi-th Carolina y" I 14326112 Date Printed: 1/8/2019 6:48:00 PM 4 14307104 g �' 2221 14304124 14304123 3408' 14304125 i f� 14303133 I 3400 143031 r • 326109 I . 1 6110 • 4 01 1!430310 11'0— i 303_ 14303105 1► �. � 14326114 `� q .� 14327 2300 •�14303198 N °j 320 3 0 �`-�M1 0,10 j0 t75.035 0.071 Miles d' 739s y 'Y 7'3 -=•Yoritltloni'R�!_— I,I S This map or report' is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, surveys, planimetric maps, and other public recordsand data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification. Mecklenburg County and its mapping contractors assume no legal responsibility for the information contained herein. tti30 y/a,)- a a�� Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code A .0405. Incident Number: 40849 Incident Name (The above information is to be completed by Response Exeter Meadow Oaks e earty or tricar represeli a ve. Please Provide the Following Information (to the best of your knowledge) Name and telephone number of person completing the survey Address of property receiving survey City Colulty What is the source of drinking water for this property? Public Water % «rater Supply Well J Stream Intake / Other Iease explain below Is there a water supply well on this property? Yes P �No If "No" disregard remaining questions and return sure, ey Name and address of owner(s) of property with water supply well Hole maIly water supply wells are on this property? What is the well(s) used for? (check all that apply) Drinking . Irrigation Swimming Pool Water Livestock , Other (specify) - Well not used Hole many residences are connected to the well (list addresses)? Hoye deep is the well(s)? Date well was installed' What is the casing depth of the x-,'ell(s)? What is the screen inter. -al of the w ell(s)? Additional water supply well information: (This part to be completed by Responsible Party or their representative) Please return completed Sur;-ey to by J.anuaryN, uslilg one of the following methods:ECS Southeast, LLP; J 2019 1. Faxto — V1,411 to i. LY tfietist, LI.S , Hive J Nr%urr If31"l Center Park Drive 5uhr Q; fharls�ite, N{: 'Lt3L 17 3. Telephone -280-7422 ;170 4. E-mail to tor @ ecsliinited.coin It you have aIiv clues,loIls. please contact t le considtom 111d1cated above or the -N DENR. Dr,-'iion of Xaste \I3llagelilei7t_ UST SCCtloll Trudy Beverly Regional Office a 7()e}-2.�$-LYf32 ECS SOUTHEAST, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F-1078 NC Registered Geologists Firm 0-406 SC Registered Engineering Firm 3239 January 9, 2018 BIFIN, LTD c/o Biesse America, Inc. 4110 Meadow Oak Drive Charlotte NC 28208 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14326109 Oak Lake Boulevard Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (inestor@ecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP Joseph P. Nestor, P.G., P.E. Matthew H. M`Duffie, P.G. Senior Environmental Project Manager Principal Geologist inestor ecslimited.corn mmcduffie@ecslimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 ®I" POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed: 01/08/2019 Identity i Ownership Parcel ID GIS ID Owner Name 14326109 114326109 INC %BIESSE AMERICA Property Characteristics Legal desc M57-390 Land Area 10.023 AC Fire District CITY OF CHARLOTTE Special District Account Type NC CORP Municipality CHARLOTTE Property Use INDUSTRIAL Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer I Yes FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUT:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN TO VERIFY LTD BIFIN Mailing Address 4110 MEADOW OAK DR CHARLOTTE NC 28208 4110 MEADOW OAK DR CHARLOTTE NC 28208 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 23277-346 01/15/2008 10078-236 11/30/1998 $862,000.00 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.03 Post Construction District Jurisdiction Charlotte District Central Catawba Stream Watershed Districts Stream Watershed Name I SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 0.00 sq ft Situs Addresses Tied to Parcel OAK LAKE BV CHARLOTTE This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G .Map — Mecklenburg County, North Carolina Date Printed: 1/8/2019 3:35:29 PM 14309107 _ 1 1430110 g .t 1432s11r' S 1 ti = 1 i " J��y (�•a�99 14326109 � � �� 14� i 432$301 Q 14326114 ��1g9 IN A r 730Z 43Z63 14326116 �,� y0 lk �. 1431 2+372 4 6115 PV ^y3` LIP 0,0rA0 , 0.05 Miles ti 14326117 This map or report is prepared for the Inventory of real property w l InMecklenburg Munty and Is compiled om reoor a dee s, patslax maps, %irveys, planimetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for veriflcation. Mecklenburg Count and Its mapp[nq contractors assume no legal responsibilityforthe information contained herein. 1y3C�L61U� co, U Lake NJ Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey- This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405. Incident Number: 40849 Incident Name Exeter Meadow Oaks (The above information is to be completed by Responsitne Yam or meir represen a eye Please Provide the Following Information (to the best of your knowledge) Frame and telephone number of person completing the survey Address of property receivvig survey Cit county What is the source of drinking water for this property? Public Water 1 Water Supply Well 1 Stream Intake 1 Other lease explain below Is there a water supply well on this property? Yes 1 No If "No" disregard remaining questions and return curve Name and address of owner(s) of property with water supply well Hole many water supply wells are on this property? What is the well(s) used for? (check all that apply) .Drinking . Irrigation . Swimming Pool Water Livestock , Other (Specify) . Well not used Hole many residences are connected to the well (list addresses)? Hole deep is the well(s)? Date well was installed^ What is the casing depth of the w e.11(s)? What is the screen interval of the well(S)7 Additional water supply well information: (This part to be completed by Responsible Party or their representative) Please return completed sun ey to by lanuary.10, using one of the following methods.-ECS Southeast, LLP; 2019 ?. Fax to all to ECS Southeast. LLP; Aan: I Nestor; 1812 Center ]?ark. Drive Suite U; Chariour, NC 28.217 3. Telephone 704-280-7422 4. E-1na11 to jnestor@ecslimited.com It vc)u have any quesuoas5 please contact the consultaIlt 111d1Cated above or the SIC DF—NR. Dii-B1Qn of lVa ste ��Ial.agenlent, L ST Section f'rt�dy Beverly Regional Office' a 7i7q-?3a 2.11i'271 EiECS SOUTHEAST, LLP "Setting the Standard for Service" mi. Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F NC Registered Geologists Firm C-406-406 SC Registered Engineering Firm 3239 January 9, 2018 BIFIN, LTD c/o Biesse America, Inc. 4110 Meadow Oak Drive Charlotte NC 28208 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14326110 Oak Lake Boulevard Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ.) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (inestor@ecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.eeslimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP ?.(n P. 71,E fit, X -7q e-DJJ.,' Joseph P. Nestor, P.G., P.E. Matthew H. M`Duffie, P.G. Senior Environmental Project Manager Principal Geologist 0nestor ecslimited.com mmcduffie@ecslimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed Identity Parcel ID I GIS ID 14326110 114326110 Property Characteristics Legal desc M57-390 Land Area 2.916 AC Fire District CITY OF CHARLOTTE Special District Account Type NC CORP Municipality CHARLOTTE Property Use INDUSTRIAL Zoning Contact appropriate Planning Department or see Map. Post Construction District Water Quality Buffer Jurisdiction Charlotte Parcel Inside Water Quality Buffer I No District Central Catawba 01/08/2019 Ownership Owner Name Mailing Address % BIESSE AMERICA INC BIFIN LTD PO BOX 19849 CHARLOTTE NC 28219 Deed Reference(s) and Sale Price Deed Sale Date I Sale Price 07712-794 03/23/1994 1 $182,000.00 FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUT:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN TO VERIFY Situs Addresses Tied to Parcel OAK LAKE BV CHARLOTTE Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.03 Stream Watershed Districts Stream Watershed Name SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 1 0.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G Map - Meddenburg County, North Carolina Date Printed: 1/8/2019 3:35:29 PIVI 14309107 1 430u JOL p-11 2"' 014,31111-10 4b %J ILA 119 14326109 i0o —pOWITJ 14326114 '90 < 7302 4326 143261111116 0.05 Miles 1 6117 This map or report is prepared for the lhvenbry of real property within Macklen5—u—rg7-aunty an scampi a ram moord dee s p 914 tax maps, surveys, planimetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification Mecklenburg County and its mapping contractors assume no legal responsibility for the Information contained herein_ rLi-'2)a(��v O o, V_ Lc, vice Q) Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L _0405- Inr..identNurnber: 40849 Incident Name (The above information is to be completed by Respons} Exeter Meadow Oaks e. Party or t1leir represen a ive Please Provide the Following Information (to the best of -our knowledge) Name and telephone number of person completing the survey Address of property receiving survey CitV County What is the source of drinking water for this property? Public Water /Water Supply Well / Stream Intake / Other lease explain below Is there a water supply well on this property? Yes / No If "No" disregard remaining questions and return stuvey Name and address of owner(s) of property with ~Dater supply well How many water supply wells are on this property? -%Vhat is the wells): used for? (check all that apply) Drinking - Irrigation . Swimming Pool Water Livestock , Other (specify) . 'Well not used Hou.- many residences are connected to the well (list addresses)? Hov., deep is the well(s)? Date well was installed? R'hat is the casing depth of the we11(s)? Whit is the screen interval of the well(s)? Additional water supply well information: (This part to be completed by Responsible Party or their representative) Please return coipleted sur, e Y' to - b-y January 30, using one of the following ECS Southeast, LLP; 2019 rnetlwcls: -- :. Fax to . ir-iall to ,. , -CS Snut.heast, LLP; Attn: I iVesfpr: 1812 Center Park l'}rit r Stu[r D; f;harlo[lc, NC f$2l7 3. Telephone 704-280-7422 4, E-inatl to jnestor@ecslimited.com It you have any questions_ please coi:tact t ie consultant indicated above or the NC* DENR Division of -Waste "tiai'agenler.t_ L tiT Section l'rucEyBe�erly ReLnonal Office ?t� 7f]•{-235.2I82 ECS SOUTHEAST, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F-1078 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 January 9, 2018 Spratt Legacy Partners, LLC PO Box 43586 Charlotte NC 28215 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14326114 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ.) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (jnestoreecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP Joseph P. Nestor, P.G., P.E. Matthew H. McDuffie, P.G. Senior Environmental Project Manager Principal Geologist jnestor@ecslimited.com mmcduffie@ecslimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed Identity Parcel ID IGIS ID 14326114 114326114 Property Characteristics Legal desc NA Land Area 2.134 AC Fire District CITY OF CHARLOTTE Special District Account Type INDIVIDUAL Municipality CHARLOTTE Property Use COMMERCIAL Zoning Contact appropriate Planning Department or see Map. 01/08/2019 Ownership Owner Name Mailing Address SPRATT LEGACY PO BOX 43586 PARTNERS LLC CHARLOTTE NC 28215 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 28581-428 08/01/2013 28581-423 08/01/2013 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.03 Water Quality Buffer Post Construction District Parcel Inside Water Quality Buffer I No Jurisdiction Charlotte FEMA and Community Floodplain District I Central Catawba FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUT:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN TO VERIFY Situs Addresses Tied to Parcel MEADOW OAK DR CHARLOTTE Stream Watershed Districts Stream Watershed Name I SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 10.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G Map — Mecklenburg County, North Carolina 14309107 H Date Printed: 1/8/2019 3:35:29 PM I. - - 1. ■ !. 143261.12' '! 4311110� r I IP 00 a 1 U �T 14326109 1 I a"' by 1432�301A 14326114 f �r 1 432630 14326116 1 0 '� 1m ', 0.05 Miles w % r �' 1 by �!y�ryt� 14326117 / Z "< 12r ThIs map or report Is prepared for the lnvenlory ❑ real property within Mecklenburg ounty and iscampiled From recorded deeds, p ats� tax maps, surveys, planimetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification- Mecklenburg County and As mapping contractors assume no legal rosponsibillty for the information contained herein. 1LA 3,;�6 119 4A &L,j C)C1V bQ ,vim Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405- Inc.identNumber: 40849 Incident Name Exeter Meadow Oaks (Tile above information is to be completed by Responsible Fam or mear represen a ive Please Provide the Following Information (to the best of sour knowledge) Name and telephone number of person completing the survey Address of property receiving survey city County What is the source of drinking water for this property? Public X ater / Water Supply Well d Stream Intake 7 Other lease explain below Is there a water supply well on this property'. Yes I _\ o If "No" disregard remaining questions and return survey Name and address of owner(s) of property with water supply well How many water su ly wells are on this property? What is the well(s) used for? (check all that apply) Drinking . Irrigation - Swimmine Pool Water Livestock . Other (Specify) I'Ve.11 not used How many residences are connected to the well (list addresses)? How deep is the. well(s)? Date well was installed? What is the casing depth of the Well(S)7 What is the screen interval of the W el1(s)? Additional water supply well informatioll: (This part to be completed by Responsible Part-,- or their representative) Please return completed surve v to by January 30, using one of the following ECs Southeast, LLP; 2019 111et110C1S: 1. Fax t(1 � - !�,Iail to ] I. --.CS Southeast, LLl'; Attn: J Nestor; 1t3I:. ceiaer I7 atic Drive sti,tt D; C11nrlcatta, H{: 28217 3. Telephone 704-280-7422 4. E-mail to jnestor@ecslimited.com If � ou have anv questions- please con —.act t 7e consultant Indicated above or the -NC DE'R- Divisic-In of Waste _teat ageillet:t. L ST Section 1 rudy f3e�erEy Regional Office a 704-23S.22E32 ECS SOUTHEAST, LLP "Setting the Standard for Service" i:.. Geotechnical • Construction Materials • Environmental • Facilities January 9, 2018 BIFIN, LTD c/o Biesse America, Inc. 4110 Meadow Oak Drive Charlotte NC 28208 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14326111 4110 Meadow Oak Drive Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: NC Registered Engineering Firm F-1078 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ.) ESC requeststhat you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (inestor , ecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP Joseph P. Nestor, P.G., P.E. Senior Environmental Project Manager inestor@ecslimited.con) 704-200-3436 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 Matthew H. McDuffie, P.G. Principal Geologist mmcduffieC4)ecsli_m ted.co_m 704-525-5152 POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed: 01/08/2019 Identity Parcel ID GIS ID 14326111 114326111 Property Characteristics Legal desc TR 1 H M25-407 Land Area 3.2 AC Fire District CITY OF CHARLOTTE Special District Account Type NC CORP Municipality CHARLOTTE Property Use INDUSTRIAL Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer No Post Construction District Ownership Owner Name Mailing Address C/O BIESSE AMERICA INC PO BOX 19849 CHARLOTTE NC 28219 BIFIN LTD PO BOX 19849 CHARLOTTE NC 28219 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 07333-539 06/09/1993 1$204,000.00 FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUT:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN I TO VERIFY Situs Addresses Tied to Parcel 4110 MEADOW OAK DR CHARLOTTE Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 39.03 Jurisdiction Charlotte District Central Catawba Stream Watershed Districts Stream Watershed Name I SUGAR Built -Upon Area Restriction Allowed Built -Upon Area 0.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G Map — Mecklenburg County, North Carolina Date Printed: 1/8/2019 3:35:29 PM 14309107 1434, 2 ,N 4�1 12' 1430110 4V 1p 14326109 j Lis i0o 14326114 7302 14326116 N - 0.05 Miles 14327 V 1432 6117 s map or report is prepared-forthe Inventoryof real property within Mecklenburg aunty and Iscamp lled from rmccorded dee s p ats, WK maps, surveys, planimetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary Information sources should be consulted for verification. Mecklenburg County and its ma In contractors assume no legal responsibility for the information contained herein. Iy3a(,Ii� Ll I I Mec dot.j Optk Diz,W— Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405. Incident Number: 40849 Incident Name Exeter Meadow Oaks (The above information is to be completed by Respazisi e P.-my ci err represen a ive Please Provide the Following Information (to the best of your knowledge) Name and telephone number of person completing the survey Address of property receiving survey City County What is the source of drinking seater for this property? Public Water ater Supply Wen / Stream Intake I Other lease explain below) Is there a xvater supply well on this property? Yes I No If -No" disregard remaining questions and return surrey Name and address of owiler(s) of property with water supply well Hour malty water supply wells are on this property? What is the well(s) used for? (check all that apply) Drinking . Irrigation . Swimming Pool Water Livestock Other (specify) - AVell not used Hour many residences are connected to the well (list addresses)? How deep is the w ell(s)? Date well was installed`` What is the easing depth of the well(s)? What is the screen interval of the well(s)? Additional water supply well information (This part to be completed by Responsible Party or their representat've) Please return completed survey to bS- January 30, using one of the following CS Southeast, LLP; 2019 methods: E 1 Fax to i.OL`,lla;lt!tS }.'-1 .:+Tall to ECS Snuthe:15I. UP; Aum J Nestar; 1812 Center Park Dhve Suite D; Charlotte, NC 28217 3. Telephone 1 704-280-7422 4. E-mail to I jnestor@ecslimited.com Tf you has: e aIiv iities llons- p eise cot::ac[ t le Lf]tI5111t lllC lIldicated abo.•e of the _NC DENR. Divisinn of'Va&te .tiJlnzigelllect. UST Section Trmly Beverly, Regional Office a 7Ur4-2:i,-'21i,92 f to. ECS SOUTHEAST, L L R "Setting the Standard for Service" u. Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F NC Registered Geologists Firm C-406-406 SC Registered Engineering Firm 3239 January 9, 2018 Cole of Charlotte NC, LLC c/o Ryan PO Box 4900, Dept 604 Scottsdale, AZ 85261 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14327301 2400 Yorkmont Road Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ.) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (jnestor@ecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.eeslimited.com If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP Joseph P. Nestor, P.G., P.E. Matthew H. M`Duffie, P.G. Senior Environmental Project Manager Principal Geologist inestor@ecshmited.com mmcduffie@ecslimiteci.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 E3c Property Characteristics Legal desc M22-503 Land Area 7.27 AC Fire District CITY OF CHARLOTTE Special District Account Type NON -NC CORP Municipality CHARLOTTE Property Use OFFICE Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer No FEMA and Community Floodplain FEMA Panel# 3710452200J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUT:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN TO VERIFY POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed: 01/08/2019 Identity Ownership Parcel ID IGIS ID Owner Name 14327301 114327301 COLE OF CHARLOTTE NC LLC C/O RYAN Mailing Address PO BOX 4900 DEPT 604 SCOTTSDALE AZ 85261 PO BOX 4900 DEPT 604 SCOTTSDALE AZ 85261 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 27931-887 12/21/2012 $19,694,000.00 27276-738 04/17/2012 $0.00 27276-717 04/17/2012 $15,050,000.00 17604-540 08/10/2004 1$0.00 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 38.05 Post Construction District Jurisdiction Charlotte District Central Catawba Stream Watershed Districts Stream Watershed Name 71 SUGAR Situs Addresses Tied to Parcel Built -Upon Area Restriction 2400 YORKMONT RD CHARLOTTE [Allow�edBlt-Upon Area 0.00 sq ft 2400 YORKMONT RD CHARLOTTE This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds. plats, tax maps, Polaris 3G Map — Mecklenburg County, North Carolina 14309107 1 , 14311110 14�zs.1�r' i Date Printed: 1/8/2019 3:35:29 PM Ip ■ 47 14326109 # 14 � 1 h� 1 26 1 a� ti a2 ao1 o+ - 14326114 CpA V-99 1 Y7302 43263 14326116 I 2 P �.O'OIAm ti 0.05 Miles 143 3 , f it MT I 14326111 '� IMIS map or report is prepared for the Irventory at real property wlihin Mecklenburg aunty and iscompHed rrommreCOrdeddeeds, PINS, taX maps, surveys, plan lmetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for v4ariflcation. Mecklenburg County and its mapping contractors assume no legal responsibility forthe information contained herein. -75 a40d YOO Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey- This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405. Incident Number: 40849 Incident wine Exeter Meadow Oaks (The above information is to e coipleted by Response a arty or eir represen a ive Please Provide the Following Information (to the best of your knowledge) Name and telephone number of person completing the survey Address of property receiving survey _ City County What is the source of drinking water for this property? Public MY'ater / Water Supply Well / Stream Intake l Other lease explain below Is there a water supply well on this property? Yes I No If "No" disregard remaining questions and return survey Name and address of owner(s)of property- with water supply well Hole many water su2,elN, wells are on this property? What is the well(s) used for? (check all that apply) Drinking . Irrigation . Swimming Pool Water Livestock , Other (specifV) Well not used Hour mangy,• residences are connected to the well (list addresses)? How deep is the well(s)? Date well was installed'' What is the casing depth of the rr e11(s)? Whit is the screen,interval of the well(s)? Additional water supply well information: (This part to be completed by Responsible Part- or their representative) Please return completed surve 4 to ECS Southeast, LLP; by]anuary 30, usirig one of the following 2019 methods.- 1.Fax to ,(:.o,:=t1*1t.1:<<. �. Mail to ECS Southeast, LLP; Attn: j Nestor; 1812 Center Park Drive Suite D; Charlotte, NC 28217 _ Telephone 704-280-7422 4. E-mall to jnestor@ecslimited.com If y`ou have and" questions_ please cont.lct the consultant indicated above or the ti]C DFNR- Division of %'Waste `Management, 'UST Section 'Trudy Beverly Realoi]31 Office 3 704-235-2102 G ECS SOUTHEAST, LLP "Setting the Standard for Service" Geotechnical • Construction Materials • Environmental • Facilities NC Registered Engineering Firm F-1078 NC Registered Geologists Firm C-406 SC Registered Engineering Firm 3239 January 9, 2018 Cole of Charlotte NC, LLC c/o Ryan PO Box 4900, Dept 604 Scottsdale, AZ 85261 Forwarded via Certified Mail Re: Request for Water Supply Information Tax Parcel 14327302 2300 Yorkmont Road Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:6535-L Dear Sir/Madame: ECS Southeast, LLP (ECS) is performing an environmental investigation in regards to a release of fuel oil which occurred from an underground storage tank (UST) located at the former North Carolina Correctional Facility (Prison Camp #704) located at 4101 Meadow Oak Drive in Charlotte, Mecklenburg County, North Carolina. ECS understands that the UST was owned and operated by the North Carolina State Highway & Public Works Commission. You were identified thorough the Mecklenburg County Geographic Information System as the owner of a tax parcel located near the former North Carolina Correctional Facility. The specific tax parcel for which you were identified as owner is referenced above. The North Carolina Department of Environmental Quality (NCDEQ) has requested that steps be taken to determine if water supply wells are in use near the former North Carolina Correctional Facility. As is the policy of NCDEQ ECS is forwarding a questionnaire to you to make inquiry as to whether a water supply well(s) is (are) present on the property which you own and, if so, to request information regarding well construction details. The template for the questionnaire was provided by NCDEQ. ECS requests that you also provide a telephone number and/or an email address on the questionnaire in the event we need to follow up with you. (This information will only be used for the purpose of investigating this release incident and will not be shared with others with the exception of the NCDEQ) ESC requests that you review, complete, and return the questionnaire to ECS by January 30, 2018. A self-addressed stamp envelop is enclosed for your convenience. If it is more convenient for you, please scan and email the document back to ECS (iinestor@ecslimited.com). ECS Capitol Services, PLLC • ECS Florida, LLC • ECS Mid -Atlantic, LLC • ECS Midwest, LLC • ECS Southeast, LLP • ECS Texas, LLP www.ecslimited.com January 9, 2019 If you have questions or comments regarding this request, feel free to contact Joseph Nestor of ECS at 704-280-7422. You may also contact Trudy Beverly of the NCDEQ at 704-235-2182. Thanks you for your prompt attention to this matter. ECS SOUTHEAST, LLP fit, X -7qeo//,' Joseph P. Nestor, P.G., P.E. Matthew H. M`Duffie, P.G. Senior Environmental Project Manager Principal Geologist inestor@ecslimited.com mmcduffie@ecslimited.com 704-200-3436 704-525-5152 Attachment: Request for Water Supply Information ECS Project No. 49-6535-L Page 12 POLARIS 3G PARCEL OWNERSHIP AND GIS SUMMARY Date Printed: Identity Parcel ID I GIS ID 14327302 114327302 Property Characteristics Legal desc M22-503 Land Area 7.79 AC Fire District CITY OF CHARLOTTE Special District Account Type NON -NC CORP Municipality CHARLOTTE Property Use OFFICE Zoning Contact appropriate Planning Department or see Map. Water Quality Buffer Parcel Inside Water Quality Buffer INo FEMA and Community Floodplain FEMA Panel# 3710452300J FEMA Panel Date 03/02/2009 FEMA Flood Zone OUT:VIEW FEMA FLOODPLAIN TO VERIFY Community Flood Zone OUT:VIEW COMMUNITY FLOODPLAIN TO VERIFY 01 /08/2019 IOwnership Owner Name F Mailing Address COLE OF CHARLOTTE NC PO BOX 4900 DEPT 604 LLC SCOTTSDALE AZ 85261 C/O RYAN PO BOX 4900 DEPT 604 SCOTTSDALE AZ 85261 Deed Reference(s) and Sale Price Deed Sale Date Sale Price 27931-882 12/21/2012 $22,477,000.00 27276-734 04/17/2012 $0.00 27276-711 04/17/2012 $20,350,000.00 17604-523 08/10/2004 $0.00 Site Location ETJ Area Charlotte Charlotte Historic District No Charlotte 6/30/2011 Annexation Area No Census Tract # 38.05 Post Construction District Jurisdiction Charlotte District Central Catawba Stream Watershed Districts Stream Watershed Name I SUGAR Situs Addresses Tied to Parcel Built -Upon Area Restriction 2300 YORKMONT RD CHARLOTTE Allowed Built -Upon Area 10.00 sq ft This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, Polaris 3G Map — Mecklenburg County, North Carolina 14309107 1452¢712 14311110 r 14326109 f��3ppp�3] 14326114 Date Printed: 1/8/2019 3:35:29 PM ONE 13'� Oc r 14301 g 44327302 W432630 14326116 .0,4121$ 0.05 Miles 143 0 ` `, 14326117 ,f -�° .`14�272u; This map or report is prepared for the inventory of real property within Meck en urg ❑unty an scampTaMr-amrecorded deeds, plats. tax maps, surveys, pianimetric maps, and other public records and data. Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification- Mecklenburg County and its mapping contractors assume no legal responsibility for the information contained herein. ee* a-�v&� 'ouVWU,,�-�-P,oC� Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405. Incident Number: 40849 Incident Name Exeter Meadow Oaks (The above information is to be completed by Responsible ar,), Of U2elr represenra ive Please Provide the Follom ing Information (to the best of wour knowledge) Name and telephone number of person completing the. survey Address of property receiving survey Ci County What is the source of drinking water for this property? Public '%'*'a ter / «'ater Supply Well/ Stream Intake/ Other lease explain below J'Surve Is there a -►rater supply well on this property? Yes f No If `No" disregard remaining questions and return Name and address of owner(s) of property with -water supply well Hove many -water supply -wells are on this property? What is the well(s) used for? (check all that apply) Drinking - Irrigation . Swimming Pool Water Livestock. Other (specif- . NVel.l not used How many residences are connected to the well (list addresses)? How deep is the well(s)? Date well -vas installed? What is the casing depth of the well(s)? What is the screen interval of the well(s)? Additional watersupply well information: (This part to be completed by Responsible Party or their representative) Please return completed server to by lru,u,siy 30, using one of the following ECS Southeast, LLP; 2019 methods: I-Faxto o '. all fo ECS SGllieas{, LI,P; Attii: j NeLSai; 1$.12 Criiter I'ork [)Five Suite [J; L'h,trlcltli, NC .3k}217 3_ Telephone 704-280-7422 4. E-mail to jnestoraecslimited.com If you have any hues ons. please coo—acr t i� consultant indicated above of the NIL DE\R Division o.f Xaste .' IanateIllent_'LtiT Section Trudy 13two-fly Re?101ial �ttll'e a 7U1 23i 21ii2 Postal CERTIFIED MAIL,,, RECEIPT (Domestic Only; ED m ❑- Postage S y9-b535-L Certified Fee �� �' I F-)1 G� "'i q Return Receipt Fee (Endorsement Required) Postmark Here Restricted Delivery Fee (Endorsement Required) i arL,'1 S . I 3D-4 W' Total Postage & Fees $ L� 1 3 a�3Do`�, M Sent To 'l�'-CharJe NG.1-�_G_�- c� �C Street, Apt. No.; �^ or PO Box No. PQ WX___ ____----- Cify, (,r_7-� +_ L 7 �, p boy--------------- Slate, ZlP+4 ate Ate- 8 a6l :rr rr. (Domestic Mall C r9 M r-=[ Postage�- Er t110119 7" I�1 Certified Fee ED cJ E:J Postmark Return Receipt Fee (Endorsement Required) Here d Restricted Delivery Fee FCAIXe I. 114311110 d (Endorsement Required) EF' M Total Postage & Fees rq $ r-qd C-eet --o-c-hG<<S�3et[�iy �� L_ _5-1-1CkOQ�e ar C� arPOBoxNo.-oVd__&�+iJ__=_!Sh-5�� ------------------- - - City, Slate, Z1P+4 (Domestic Mall C For delivery informi m ra Postage $ 49-6535 -L E' d Certified Fee J t` f, I� 0/ 19 Return Receipt Fee Postmark Here (Endorsement Required) parcels;I Restricted Delivery Fee p (Endorsement Required) L! 30 1 a3 J—u 304I 2'4 d Total Postage & Fees ,q $ ` Sent To C3 4pke o;n e r c k�_Ccn4�x__L sso_c�a1�5. C] Street, Ap. No.; l r+ or PO Box NO. --- - --------- --- ---- City, State, ZIP+4 PS Form N a- :11 August 2006 See Reverse for Jnstructions (Domestic Mail Only; No Insuran .■ For delivery information visit our wet a Q' Postage $ H9-6535-L Certified Fee 1 p t� Return Receipt Fee (Endorsement Requ6red} Postmark Here ���'� `�•' p Restricted Delivery Fee (Endorsement Required} I LI 3a01 Cr C3 Total Postage & Fees $ 1 g 3 i, 10 u3ab i I 1 .� Sent To 1 F I IJ , L-SO �/O G i es se. Arnefy ca, I n c' O r� +------------------------------------- -- Sirset, Apt. 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No.; Cti OBoxNo- Po bXState, ZfP+4 }e }1G a$al j PS Form :,, August 2D06 See Reverse for Instructions ■ Complete items 1, 2, and 3. ■ Print your name and address on the reverse so that we can return the card to you. • Attach this card to the back of the mailpiece, or on the front if space permits. i. Article Addressed to: (�IFIN) LTD CA> i3iesfeArnericcl, inc. Hilo meadow Day, Orve �harlo��e, ►vca$ao8 A. Signature X ❑ Agent ❑ Addressee B. Received by (Printed Name) C. Date of Delivery kw?x; k(PnSeQ 9 D. Is deliver�`address different from item iT ❑ Yes If YES, enter delivery address below: © No 3. Service Type press® ❑ PrioRegistered ❑ Adult Signature 0 Registered MaiITM' erect Ma ❑ Adult Signature Restricted Delivery ❑ Registered Mail Restricte )i Certified Maim Delivery 9590 9402 1421 5329 9544 89 0 Certified Mail Restricted Delivery '� Return Recelpt for 0 Collect on Delivery Merchandise P. Artinla Kh imhpr (fransfar frnm sarvica fahall ❑ Collect on Delivery Restficted Delivery ❑ Signature Confirmationr^" ❑ Signature Confirmation 71113 1090 0000 9143 1854 ed Mail ed Mail Restricted Delivery Restricted Delivery $500i _ PS Form 3811, July 2015 PSN 7530-02-000-9053 Domestic Return Receipt ■ Complete items 1, 2, and 3. ■ Print your name and address on the reverse so that we can return the card to you. ■ Attach this card to the back of the mailpiece, or on the front if space permits. 1. Article Addressed to: Cik� a CL,Gr1of4G Pr,oper+y manage meO} (� 00 Ea53 L4 i h siree+ �harlo fie, QC 2$aQa A. Sign tu— /� -. ��/f ❑ Agent X " �-" L �-e © Addresses B. R ived by (Printed Name) C. Date of Delivery JAJ I R D. lilkelivery address different from item ? 0 If YES, enter delivery address below: ❑ No >I 3. Service Type PriorityMall Express® I I I I �II I I� III I I II Il 0}4I Adult Signature 0 Registered MaiIT"" li I fkl ❑ Adult Signature Restricted Delivery ❑ Registered Mali Restricted !I 9590 9402 1421 5329 9544 85 �CertifiedMail® ❑ Certified Mail Restricted Delivery Delivery Retum Receipt for ❑ Collect on Delivery tl Collect on Delivery Restricted Delivery — ' Merchandise Q Signature ConfrnnationTm U Signature Confirmation 6r+irlo Ni imhnr !Transfer from SP,rViCA label} [] 1 ]r [ 0000 ti 3 Q sured Mail Mail Restricted Delivery sure Restricted Delivery 5d ve00} PS Form 3811, July 2015 PSN 7530-02-000-9053 Domestic Return Receipt i Complete items 1, 2, and 3. • Print your name and address on the reverse so that we can return the card to you. ■ Attach this card to the back of the mailpiece, or on the front if space permits. t. Article Addressed to: SQrCtf� L-'Tc_ PCfjnefS, LAG PC) Box 1-1S58(" GhGrlo!-fie, ,S G �8a15 I I I1Ili III ill I II I III IIII I II II1I IIIII ��) 9590 9402 1421 5329 9544 96 2, Article. Namhar rrrarrefar from — -, 1<.+.�n 7D1r3 logo 0000 9143 18611 PS Form 3811, July 2015 PSN 7530-02-000-9053 COMPLETE ■ Complete items 1, 2, and 3. ■ Print your name and address on the reverse so that we can return the card to you. ■ Attach this card to the back of the mailpiece, or on the front if space permits. 1. Article Addressed to: N G tmGn CGScnd e, L L G c/o ?'tGmm H'0rels 90 Box H5N0 Flove►xe, SC �95Da ll 1111111 IN 1il l 11I II# I I### I IIII I III I II III Ill 9590 9402 1421 5329 9544 72 2. Article Number (Transfer from servrce faaelr 7013 logo 0000 9143 1847 PS Form 3811, July 2015 PSN 7530-02-000-9053 A. C. Date Agent D. Is delivery address different from item 1? © Yes If YES, enter delivery address below: ❑ No 3Service Type CIPriority Mal Express® E Aduit Signature ❑ Registered MalITM ❑ Adu;t Signature Restricted Delivery fl Registered Mail Restricted 91 Certified Maile Delivery ❑ Certified Mail Restricted Delivery Return Receipt for ❑ Collect on Delivery Merchandise n r�llect on Delivery Restricted Delivery ❑ Signature ConfirmatfonT .ured Mail ❑ Signature Confirmation ured Mail Restricted Delivery Restricted Delivery ,-.er $500) Domestic Return Receipt A. Agent X ❑ Addressee B. Aeceiy,red by fdrifed NafnV V. uate aT venvery D. Is delivery address different from item 1? ❑ Yes If YES, enter delivery address below: 0 No 3. Service Type ❑ Priority Mail Express® p Adult Signature ❑ Registered Mal"" C7 Adult Signature ResMcted Delivery ❑ Registered Mail Restriotei 1CCert;fied Mail® ❑ Certified Mail Restricted Delivery Delivery -Return Receipt for -Merchandise ❑ Collect on Delivery ❑ Collect an Delivery Restricted Delivery M Signature ConfinnationTM red Mail ❑ Signature Confirmation red Mail Restricted Dellvery Restricted Delivery r $500) Domestic Return Receipt USPS.com® - USPS Tracking® Results Page 1 of 2 ALERT: EXTREME COLD HAS CAUSED USPS SERVICE DISRUPTIONS ACROSS THE... USPS Tracking FAQs > (https://www.usps.com/fags/uspstracking-faqs.htm) Track Another Package + Tracking Number: 70131090000091431823 Remove X Your item was returned to the sender at 3:20 pm on January 22, 2019 in CHARLOTTE, NC 28217 because the forwarding order for this address is no longer valid. 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Sign Up (https://reg.usps.com/entreg/RegistrationAction_input? *NOTE: Black and white (grayscale) images show the outside, front of letter -sized envelopes and mailpieces mated equipment. https:Htools.usps.com/golTrackConfirmAction?tRef=fullpage&tLc=2&text28777=&tLabe... 1/31/2019 b@Yl 1y30 y/a'�)_ a c45«Ae P01V%4e- Blv� Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405. Incident Number: 140849 Incident Name Exeter Meadow Oaks (The above iriforn-iatioi3 is to a completed by Respsi e ar y or eir represe—i a is-e Please Provide tlm.e Following Information (to the best of your knowledne) ItiYame and telephone number of person coma leting the sui" ,ey r Address of Rope y. feceiviiig survey �� t ✓(� city [OU& Coluitjr 'hat is the source of drinking. water for this property Public Watex l V4rater Supply Well I Stream Intake / Other lease explain below Is there a water supply well on this property? Yes 1 iINO If "No" disregard remaining questions and return survev Name and address of owner(s) of property with water .supply well Hots many water supply -wells are on this rta emir? 1AThat is the well(s) used for^ (check all that apply) Drinking . Irrigation swimming Pool Water Livestock , Other (specify) ,%Fell not used How man), residences .are connected to the well (list addresses)? Hour deep is the w ell(s)? Date well was installed' What is the casing depth of the well(s)7 What is the screen 1nterr,-a1 of the Well(S)7 Additional water supply well information: (This part to be completed by Responsible Party or their representative) Please return completed SLiri ei' t0 lj` January 30, LISitlr oneo the follotj'IIICT , ECS Southeast, LLP; 2019 methods: 1 Fax to 11l f.l;i;• .'%fail to i?(:S Soutl%ca t, UP; At In: I Nestor; litl'L Center Park prise Suite I); Charlotte, NC18217 . Telephone 704-280-7422 . E-mail to jnestor a ecslimited.com If you have any ques%ons, please contact C le Consultant indicated above or the NC_' DE1R. Dnr'sion of tVa;te linagenient- UST Section FTrudy Beverly Regional Office a� 704-235-2182 I 2(J� a-�-��, Iy3a��ll L(I fU Mec doLj Oc k D21w— Request for Water Supply Well Information A release of petroleum product or other regulated material has occurred within 1500 feet of the property receiving this survey. This survey is being conducted as part of the investigation of the release as required by the State of North Carolina in Title 15A North Carolina Administrative Code 2L .0405. Incident Number- Incident Name Exeter Meadtrw0alcs (The above information is to be completed by Response a Farry or t eir represeu a ive. Please Provide the Following Information (to the best of rout.• knowledge) Name and telephone number of person completing the survey �P/nIT IVA Address of property receiving survey city County What is the source of drinking water for this prop `ty? Public Wate • 1 -%eater Supply Well i Stream Intake I Other lease explain below Is there a water suppl}� well on this property' Y1?Lio If "No" disregard remaining questions and return survey Name and address of owner(s) of property with watersupply well How inane water supply wells are on this property? What is the well(s) used for? (check all that apply) Drinking . Irrigation swituming Pool Water Livestock , Other (specify-) . -%yell not used Hour many residences are connected to the well (list addresses)? Hour deep is the. well(s)? Date well was. installed? What is the casing depth of the well(s)? What is the screed inten.-al of the w ell(s)? Additional water supply well information: (This part to be completed by Responsible Part-,- or their fe.preselltati': e) Please returIl colllpleted sun.-e V to t y January M, using one of the follo-wing methods- ECS Southeast, LLP; 2019 Facto i..or,..t','.11i:t vTail to ECS Southeast, LLP; Attn:1 N.estar; 1812 Cejiler Park Drive Suite G; CharInue, NC 28217 3. Telephone 704-280-7422 4. E-mail to jnestor@ecslimited.com If you have an, quesuons. plea -Se co€::act tile Consultant indict tired above or the -NC DENR. Division of -%Vaste _tilanageine-..t, T_ ST Section Trtitly Deverl.v Regional Office a y04-23 v 21R"? jz, d h� 3PtiJ 143 �t �o� C)Q v Request for Water Supply ell Information A release of petroleum product or other regulated mat al has occurred within 1500 feet of the property receiving this survey_ This survey is being conduct as part of the investigation of the release as required by the State of North Carolina in Title 1,5KNorth Carolina Administrative Code 2L .0405_ Incident Number: 40849 IncidentNav4j Exeter Meadow Oaks (The above information is to b a completed by Responsa a FaNy or ffieLr represenra ive- Please Provide the Foilo-wing Infor.mat:ion (to the best of your knowledge) Name and telephone number of er n com letin thesurvey � �' ` "� � O� Address of property receiving survey p g y � r City +-�o joylqrl Comity What is the source of drinking water for this property? Public Water/ Water Supply Well I Stream In ke / Other lease explain below - �- �7a- � t� Alt : c Is there. a water supply well on this propert_y? ye): Na If `-No" disregard remaining questions and return survey Name and address of owner(s) of property with water supply well Hour many water supply wells are on this property? what is the well(s) used for? (check all that apply) Drinking _ Irrigation . Swimming Pool Water Livestock , Other (specify) . 117el.l not used How many residences are connected to the well (list addresses)? How deep is the. well(s)? Date well was installed:' What is the casing depth of the tvell(s)? What is the screen interval of the w ell(s)? Additional water supply well information (This part to be completed by Responsible Party or their representative) Please return completed Surve v' to ECS Southeast, LLP; by January 30, using one of the following 2019 methods: 1. Fax to �. 011�a_l.l;ll;i'• �`:1:: _ 11;'i 'i': to , FXS Southeast, UP: Aum ] Ne%lor; [If 12 Center Park Dnve Suite D; Charlotte. NC 28217 3 Telephone 704-280-7422 4. E-mail to jnestor@ecsiimited.com If yott has•-e any s.UeSTioUS- p eaS,e contact t 12 consultant indic;ited above or the _NC DE1R. Division of _tilanazeinet:t_ t 5T Section i'rudyt3cvcriy Regional Office a 7i11.2 ,=?'i8 �t Legac� Par oers, u,c, ioX 1-135$(o p cz 1 fio4+e, Nc a$';k15 -�L CHARLOTTE NC 282 17JAN'19 P.M 4 L 1812 Center Park Drive, Suite D, Charlotte, NC 28217 A+- n:,)oe ►Jes+ov +5+" -9 A SWITNEV Bowan 02 W $ DD1.21° 0000308461 JAN 10 2019 MAILED FROM ZIPCODE28217 APPENDIX C BORING LOG PROJECT: Meadow Oak Industrial MONITORING WELL NOI MW-1 CLIENT: Exeter 4100 Meadow Oak, LLC PROJECT NO. 6535-L LOCATION: ELEVATION: Former Heating Oil UST Basin DRILLER: DATE DRILLED: LOGGED BY: GEX 1/15/2019 Randy Cavalier DRILL RIG: DEPTH TO WATER: 28.39 Elevation/ o a� a — 0 WELL Depth (Ft) m E E co z E o n �n �- C ° w - SOIL DESCRIPTION CONSTRUCTION � Co U 7.6 MH Fill Brown SILT, Fill ; MH/CH Dark Brown/Red Clayey SILT 7.5 354 00 00 R 1,086 Red/Brown SILT i 15 9.1 Brown w/ Black Mottled SILT MW1-15 MH 8.6 22. 8.1 Dark Brown SILT MW1-25 s s Water 30 Water 37. Bottom of Boring 45 52. Figure Paae 1 of 1 APPENDIX D LABORATORY DATA SHEETS AND CHAIN OF CUSTODY RECORDS aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 24, 2019 Joe Nestor ECS Southeast 1812 Center Park Drive Suite D Charlotte, NC 28217 RE: Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Dear Joe Nestor: Enclosed are the analytical results for sample(s) received by the laboratory on January 17, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, p Taylor Ezell taylor.ezell@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: MEADOW OAK INDUSTRIAL PHASE I 92414388 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92414388001 MW1-15 MADEP EPH SEM 7 PASI-C MADEP VPH LMB 6 PASI-C EPA 8270D BPJ 74 PASI-C EPA 8260E DLK 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92414388002 MW1-25 MADEP EPH SEM 7 PASI-C MADEP VPH LMB 6 PASI-C EPA 8270D BPJ 74 PASI-C EPA 8260E DLK 70 PASI-C ASTM D2974-87 KDF 1 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-15 Lab ID: 92414388001 Collected: 01/15/19 09:45 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Aliphatic (C09-C18) 481 mg/kg 144 10 01/17/19 21:05 01/24/19 07:16 N2 Aliphatic (C19-C36) ND mg/kg 144 10 01/17/19 21:05 01/24/19 07:16 N2 Aromatic (C11-C22) 282 mg/kg 28.8 2 01/17/19 21:05 01/24/19 07:16 N2 Surrogates Nonatriacontane (S) 0 % 40-140 10 01/17/19 21:05 01/24/19 07:16 7194-86-7 S4 o-Terphenyl (S) 242 % 40-140 2 01/17/19 21:05 01/24/19 07:16 84-15-1 S5 2-Fluorobiphenyl (S) 113 % 40-140 2 01/17/19 21:05 01/24/19 07:16 321-60-8 2-Bromonaphthalene (S) 490 % 40-140 2 01/17/19 21:05 01/24/19 07:16 580-13-2 S5 VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Aliphatic (C05-CO8) ND mg/kg 3.5 1 01/18/19 16:42 01/18/19 22:54 N2 Aliphatic (C09-C12) 49.3 mg/kg 3.5 1 01/18/19 16:42 01/18/19 22:54 N2 Aliphatic(C09-C12)Adjusted 24.2 mg/kg 3.5 1 01/18/19 16:42 01/18/19 22:54 N2 Aromatic (C09-C10) 25.1 mg/kg 3.5 1 01/18/19 16:42 01/18/19 22:54 N2 Surrogates 4-Bromofluorobenzene (FID) (S) 104 % 70-130 1 01/18/19 16:42 01/18/19 22:54 460-00-4 4-Bromofluorobenzene (PID) (S) 93 % 70-130 1 01/18/19 16:42 01/18/19 22:54 460-00-4 8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546 Acenaphthene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 83-32-9 Acenaphthylene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 208-96-8 Aniline ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 62-53-3 Anthracene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 120-12-7 Benzo(a)anthracene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 56-55-3 Benzo(a)pyrene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 50-32-8 Benzo(b)fluoranthene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 205-99-2 Benzo(g,h,i)perylene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 191-24-2 Benzo(k)fluoranthene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 207-08-9 Benzoic Acid ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 65-85-0 Benzyl alcohol ND ug/kg 9520 10 01/17/19 19:46 01/22/19 16:35 100-51-6 4-Bromophenylphenyl ether ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 101-55-3 Butylbenzylphthalate ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 9520 10 01/17/19 19:46 01/22/19 16:35 59-50-7 4-Chloroaniline ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 111-44-4 2-Chloronaphthalene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 91-58-7 2-Chlorophenol ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 7005-72-3 Chrysene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 218-01-9 Dibenz(a,h)anthracene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 53-70-3 Dibenzofuran ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 132-64-9 1,2-Dichlorobenzene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 95-50-1 1,3-Dichlorobenzene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 541-73-1 1,4-Dichlorobenzene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 91-94-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-15 Lab ID: 92414388001 Collected: 01/15/19 09:45 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546 2,4-Dichlorophenol ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 120-83-2 Diethylphthalate ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 84-66-2 2,4-Dimethylphenol ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 105-67-9 Dimethylphthalate ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 131-11-3 Di-n-butylphthalate ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 9520 10 01/17/19 19:46 01/22/19 16:35 534-52-1 L2 2,4-Dinitrophenol ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 51-28-5 L2 2,4-Dinitrotoluene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 121-14-2 2,6-Dinitrotoluene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 606-20-2 Di-n-octylphthalate ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 117-81-7 Fluoranthene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 206-44-0 Fluorene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 87-68-3 Hexachlorobenzene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 118-74-1 Hexachlorocyclopentadiene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 77-47-4 Hexachloroethane ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 193-39-5 Isophorone ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 78-59-1 1-Methylnaphthalene 12300 ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 90-12-0 2-Methylnaphthalene 9460 ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 15831-10-4 Naphthalene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 91-20-3 2-Nitroaniline ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 88-74-4 3-Nitroaniline ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 99-09-2 4-Nitroaniline ND ug/kg 9520 10 01/17/19 19:46 01/22/19 16:35 100-01-6 Nitrobenzene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 98-95-3 2-Nitrophenol ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 88-75-5 4-Nitrophenol ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 100-02-7 N-Nitrosodimethylamine ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 621-64-7 N-Nitrosodiphenylamine ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 108-60-1 L1 Pentachlorophenol ND ug/kg 23800 10 01/17/19 19:46 01/22/19 16:35 87-86-5 Phenanthrene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 85-01-8 Phenol ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 108-95-2 Pyrene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 129-00-0 1,2,4-Trichlorobenzene ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 120-82-1 2,4,5-Trichlorophenol ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 95-95-4 2,4,6-Trichlorophenol ND ug/kg 4760 10 01/17/19 19:46 01/22/19 16:35 88-06-2 Surrogates Nitrobenzene-d5 (S) 0 % 23-110 10 01/17/19 19:46 01/22/19 16:35 4165-60-0 D3,S4 2-Fluorobiphenyl (S) 0 % 30-110 10 01/17/19 19:46 01/22/19 16:35 321-60-8 S4 Terphenyl-d14 (S) 0 % 28-110 10 01/17/19 19:46 01/22/19 16:35 1718-51-0 S4 Phenol-d6 (S) 0 % 22-110 10 01/17/19 19:46 01/22/19 16:35 13127-88-3 S4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-15 Lab ID: 92414388001 Collected: 01/15/19 09:45 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV Microwave Surrogates 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Analytical Method: EPA 8270D Preparation Method: EPA 3546 0 % 13-110 10 01/17/1919:46 01/22/1916:35 367-12-4 S4 0 % 27-110 10 01/17/1919:46 01/22/1916:35 118-79-6 S4 8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A Acetone ND ug/kg 122 1 01/18/19 11:37 01/18/19 16:20 67-64-1 Benzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 71-43-2 Bromobenzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 108-86-1 Bromochloromethane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 74-97-5 Bromodichloromethane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 75-27-4 Bromoform ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 75-25-2 Bromomethane ND ug/kg 12.2 1 01/18/19 11:37 01/18/19 16:20 74-83-9 2-Butanone (MEK) ND ug/kg 122 1 01/18/19 11:37 01/18/19 16:20 78-93-3 n-Butylbenzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 104-51-8 sec-Butylbenzene 12.7 ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 135-98-8 tert-Butyl benzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 98-06-6 Carbon tetrachloride ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 56-23-5 Chlorobenzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 108-90-7 Chloroethane ND ug/kg 12.2 1 01/18/19 11:37 01/18/19 16:20 75-00-3 Chloroform ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 67-66-3 Chloromethane ND ug/kg 12.2 1 01/18/19 11:37 01/18/19 16:20 74-87-3 2-Chlorotoluene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 95-49-8 4-Chlorotoluene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 96-12-8 Dibromochloromethane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 106-93-4 Dibromomethane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 74-95-3 1,2-Dichlorobenzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 95-50-1 1,3-Dichlorobenzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 541-73-1 1,4-Dichlorobenzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 106-46-7 Dichlorodifluoromethane ND ug/kg 12.2 1 01/18/19 11:37 01/18/19 16:20 75-71-8 1,1-Dichloroethane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 75-34-3 1,2-Dichloroethane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 107-06-2 1,1-Dichloroethene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 75-35-4 cis-1,2-Dichloroethene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 156-59-2 trans-1,2-Dichloroethene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 156-60-5 1,2-Dichloropropane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 78-87-5 1,3-Dichloropropane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 142-28-9 2,2-Dichloropropane ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 594-20-7 1,1-Dichloropropene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 563-58-6 cis-1,3-Dichloropropene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 10061-02-6 Diisopropyl ether ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 108-20-3 Ethylbenzene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 6.1 1 01/18/19 11:37 01/18/19 16:20 87-68-3 2-Hexanone ND ug/kg 60.8 1 01/18/19 11:37 01/18/19 16:20 591-78-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-15 Lab ID: 92414388001 Collected: 01/15/19 09:45 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260/5035A Volatile Organics Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260E Preparation Method: EPA 5035A 6.5 ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 98-82-8 27.7 ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 99-87-6 32.1 ug/kg 24.3 1 01/18/1911:37 01/18/1916:20 75-09-2 ND ug/kg 60.8 1 01/18/1911:37 01/18/1916:20 108-10-1 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 1634-04-4 112 ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 91-20-3 7.4 ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 103-65-1 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 100-42-5 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 630-20-6 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 79-34-5 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 127-18-4 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 108-88-3 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 87-61-6 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 120-82-1 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 71-55-6 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 79-00-5 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 79-01-6 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 75-69-4 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 96-18-4 83.1 ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 95-63-6 29.6 ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 108-67-8 ND ug/kg 60.8 1 01/18/1911:37 01/18/1916:20 108-05-4 ND ug/kg 12.2 1 01/18/1911:37 01/18/1916:20 75-01-4 ND ug/kg 12.2 1 01/18/1911:37 01/18/1916:20 1330-20-7 ND ug/kg 12.2 1 01/18/1911:37 01/18/1916:20 179601-23-1 ND ug/kg 6.1 1 01/18/1911:37 01/18/1916:20 95-47-6 109 % 70-130 1 01/18/1911:37 01/18/1916:20 2037-26-5 118 % 70-130 1 01/18/1911:37 01/18/1916:20 460-00-4 74 % 70-132 1 01/18/1911:37 01/18/1916:20 17060-07-0 Analytical Method: ASTM D2974-87 30.0 % 0.10 1 REPORT OF LABORATORY ANALYSIS 01/17/19 17:54 C9 L2 This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-25 Lab ID: 92414388002 Collected: 01/15/19 10:00 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Aliphatic (C09-C18) ND mg/kg 13.6 1 01/17/19 21:05 01/22/19 16:25 N2 Aliphatic (C19-C36) ND mg/kg 13.6 1 01/17/19 21:05 01/22/19 16:25 N2 Aromatic (C11-C22) ND mg/kg 13.6 1 01/17/19 21:05 01/22/19 16:25 N2 Surrogates Nonatriacontane (S) 61 % 40-140 1 01/17/19 21:05 01/22/19 16:25 7194-86-7 o-Terphenyl (S) 63 % 40-140 1 01/17/19 21:05 01/22/19 16:25 84-15-1 2-Fluorobiphenyl (S) 13 % 40-140 1 01/17/19 21:05 01/22/19 16:25 321-60-8 SO 2-Bromonaphthalene (S) 13 % 40-140 1 01/17/19 21:05 01/22/19 16:25 580-13-2 SO VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Aliphatic (C05-CO8) 8.2 mg/kg 3.4 1 01/18/19 16:42 01/18/19 23:24 N2 Aliphatic (C09-C12) 18.2 mg/kg 3.4 1 01/18/19 16:42 01/18/19 23:24 N2 Aliphatic(C09-C12)Adjusted 10.5 mg/kg 3.4 1 01/18/19 16:42 01/18/19 23:24 N2 Aromatic (C09-C10) 7.6 mg/kg 3.4 1 01/18/19 16:42 01/18/19 23:24 N2 Surrogates 4-Bromofluorobenzene (FID) (S) 128 % 70-130 1 01/18/19 16:42 01/18/19 23:24 460-00-4 4-Bromofluorobenzene (PID) (S) 127 % 70-130 1 01/18/19 16:42 01/18/19 23:24 460-00-4 8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546 Acenaphthene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 83-32-9 Acenaphthylene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 208-96-8 Aniline ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 62-53-3 Anthracene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 120-12-7 Benzo(a)anthracene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 56-55-3 Benzo(a)pyrene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 50-32-8 Benzo(b)fluoranthene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 205-99-2 Benzo(g,h,i)perylene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 191-24-2 Benzo(k)fluoranthene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 207-08-9 Benzoic Acid ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 65-85-0 Benzyl alcohol ND ug/kg 9230 10 01/17/19 19:46 01/22/19 17:03 100-51-6 4-Bromophenylphenyl ether ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 101-55-3 Butylbenzylphthalate ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 85-68-7 4-ChIoro-3-methyl phenol ND ug/kg 9230 10 01/17/19 19:46 01/22/19 17:03 59-50-7 4-Chloroaniline ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 111-44-4 2-Chloronaphthalene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 91-58-7 2-Chlorophenol ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 7005-72-3 Chrysene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 218-01-9 Dibenz(a,h)anthracene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 53-70-3 Dibenzofuran ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 132-64-9 1,2-Dichlorobenzene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 95-50-1 1,3-Dichlorobenzene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 541-73-1 1,4-Dichlorobenzene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 106-46-7 3,3'-Dichlorobenzidine ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 91-94-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-25 Lab ID: 92414388002 Collected: 01/15/19 10:00 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546 2,4-Dichlorophenol ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 120-83-2 Diethylphthalate ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 84-66-2 2,4-Dimethylphenol ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 105-67-9 Dimethylphthalate ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 131-11-3 Di-n-butylphthalate ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 9230 10 01/17/19 19:46 01/22/19 17:03 534-52-1 L2 2,4-Dinitrophenol ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 51-28-5 L2 2,4-Dinitrotoluene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 121-14-2 2,6-Dinitrotoluene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 606-20-2 Di-n-octylphthalate ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 117-81-7 Fluoranthene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 206-44-0 Fluorene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 87-68-3 Hexachlorobenzene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 118-74-1 Hexachlorocyclopentadiene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 77-47-4 Hexachloroethane ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 193-39-5 Isophorone ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 78-59-1 1-Methylnaphthalene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 90-12-0 2-Methylnaphthalene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 15831-10-4 Naphthalene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 91-20-3 2-Nitroaniline ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 88-74-4 3-Nitroaniline ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 99-09-2 4-Nitroaniline ND ug/kg 9230 10 01/17/19 19:46 01/22/19 17:03 100-01-6 Nitrobenzene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 98-95-3 2-Nitrophenol ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 88-75-5 4-Nitrophenol ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 100-02-7 N-Nitrosodimethylamine ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 621-64-7 N-Nitrosodiphenylamine ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 108-60-1 L1 Pentachlorophenol ND ug/kg 23100 10 01/17/19 19:46 01/22/19 17:03 87-86-5 Phenanthrene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 85-01-8 Phenol ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 108-95-2 Pyrene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 129-00-0 1,2,4-Trichlorobenzene ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 120-82-1 2,4,5-Trichlorophenol ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 95-95-4 2,4,6-Trichlorophenol ND ug/kg 4620 10 01/17/19 19:46 01/22/19 17:03 88-06-2 Surrogates Nitrobenzene-d5 (S) 0 % 23-110 10 01/17/19 19:46 01/22/19 17:03 4165-60-0 D3,S4 2-Fluorobiphenyl (S) 0 % 30-110 10 01/17/19 19:46 01/22/19 17:03 321-60-8 S4 Terphenyl-d14 (S) 0 % 28-110 10 01/17/19 19:46 01/22/19 17:03 1718-51-0 S4 Phenol-d6 (S) 0 % 22-110 10 01/17/19 19:46 01/22/19 17:03 13127-88-3 S4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-25 Lab ID: 92414388002 Collected: 01/15/19 10:00 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV Microwave Surrogates 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) Analytical Method: EPA 8270D Preparation Method: EPA 3546 0 % 13-110 10 01/17/1919:46 01/22/1917:03 367-12-4 S4 0 % 27-110 10 01/17/1919:46 01/22/1917:03 118-79-6 S4 8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A Acetone ND ug/kg 106 1 01/18/19 11:37 01/18/19 16:40 67-64-1 Benzene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 71-43-2 Bromobenzene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 108-86-1 Bromochloromethane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 74-97-5 Bromodichloromethane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 75-27-4 Bromoform ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 75-25-2 Bromomethane ND ug/kg 10.6 1 01/18/19 11:37 01/18/19 16:40 74-83-9 2-Butanone (MEK) ND ug/kg 106 1 01/18/19 11:37 01/18/19 16:40 78-93-3 n-Butylbenzene 8.5 ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 104-51-8 sec-Butylbenzene 6.7 ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 135-98-8 tert-Butyl benzene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 98-06-6 Carbon tetrachloride ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 56-23-5 Chlorobenzene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 108-90-7 Chloroethane ND ug/kg 10.6 1 01/18/19 11:37 01/18/19 16:40 75-00-3 Chloroform ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 67-66-3 Chloromethane ND ug/kg 10.6 1 01/18/19 11:37 01/18/19 16:40 74-87-3 2-Chlorotoluene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 95-49-8 4-Chlorotoluene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 96-12-8 Dibromochloromethane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 106-93-4 Dibromomethane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 74-95-3 1,2-Dichlorobenzene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 95-50-1 1,3-Dichlorobenzene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 541-73-1 1,4-Dichlorobenzene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 106-46-7 Dichlorodifluoromethane ND ug/kg 10.6 1 01/18/19 11:37 01/18/19 16:40 75-71-8 1,1-Dichloroethane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 75-34-3 1,2-Dichloroethane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 107-06-2 1,1-Dichloroethene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 75-35-4 cis-1,2-Dichloroethene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 156-59-2 trans-1,2-Dichloroethene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 156-60-5 1,2-Dichloropropane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 78-87-5 1,3-Dichloropropane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 142-28-9 2,2-Dichloropropane ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 594-20-7 1,1-Dichloropropene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 563-58-6 cis-1,3-Dichloropropene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 10061-02-6 Diisopropyl ether ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 108-20-3 Ethylbenzene 5.9 ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 100-41-4 Hexachloro-1,3-butadiene ND ug/kg 5.3 1 01/18/19 11:37 01/18/19 16:40 87-68-3 2-Hexanone ND ug/kg 52.9 1 01/18/19 11:37 01/18/19 16:40 591-78-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Sample: MW1-25 Lab ID: 92414388002 Collected: 01/15/19 10:00 Received: 01/17/19 11:05 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260/5035A Volatile Organics Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260E Preparation Method: EPA 5035A 5.5 ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 98-82-8 14.7 ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 99-87-6 ND ug/kg 21.2 1 01/18/1911:37 01/18/1916:40 75-09-2 ND ug/kg 52.9 1 01/18/1911:37 01/18/1916:40 108-10-1 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 1634-04-4 35.9 ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 91-20-3 8.5 ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 103-65-1 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 100-42-5 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 630-20-6 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 79-34-5 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 127-18-4 L2 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 108-88-3 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 87-61-6 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 120-82-1 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 71-55-6 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 79-00-5 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 79-01-6 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 75-69-4 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 96-18-4 53.5 ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 95-63-6 13.3 ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 108-67-8 ND ug/kg 52.9 1 01/18/1911:37 01/18/1916:40 108-05-4 ND ug/kg 10.6 1 01/18/1911:37 01/18/1916:40 75-01-4 ND ug/kg 10.6 1 01/18/1911:37 01/18/1916:40 1330-20-7 ND ug/kg 10.6 1 01/18/1911:37 01/18/1916:40 179601-23-1 ND ug/kg 5.3 1 01/18/1911:37 01/18/1916:40 95-47-6 106 % 70-130 1 01/18/1911:37 01/18/1916:40 2037-26-5 100 % 70-130 1 01/18/1911:37 01/18/1916:40 460-00-4 70 % 70-132 1 01/18/1911:37 01/18/1916:40 17060-07-0 Analytical Method: ASTM D2974-87 27.3 % 0.10 1 REPORT OF LABORATORY ANALYSIS 01/17/19 17:54 This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 30 Pace Analytical Services, LLC ceAnalX cal ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 QC Batch: 453342 Analysis Method: MADEP VPH QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil Associated Lab Samples: 92414388001, 92414388002 METHOD BLANK: 2477396 Associated Lab Samples: 92414388001, 92414388002 Parameter Units Aliphatic (C05-008) mg/kg Aliphatic (C09-C12) mg/kg Aromatic (C09-C10) mg/kg 4-Bromofluorobenzene (FID) (S) % 4-Bromofluorobenzene (PID) (S) % Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 01/18/1915:03 N2 ND 2.5 01/18/1915:03 N2 ND 2.5 01/18/1915:03 N2 78 70-130 01/18/1915:03 86 70-130 01/18/1915:03 LABORATORY CONTROL SAMPLE & LCSD: 2477397 2477398 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C05-CO8) mg/kg 15.1 12.4 11.7 82 78 70-130 6 25 N2 Aliphatic (C09-C12) mg/kg 15.1 14.1 13.3 93 88 30-130 6 25 N2 Aromatic (C09-C10) mg/kg 5 5.2 4.9 104 98 70-130 6 25 N2 4-Bromofluorobenzene (FID) (S) % 86 79 70-130 4-Bromofluorobenzene (PID) (S) % 96 88 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 QC Batch: 453256 Analysis Method: EPA 8260B QC Batch Method: EPA 5035A Analysis Description: 8260 MSV 5035A Volatile Organics Associated Lab Samples: 92414388001, 92414388002 METHOD BLANK: 2476808 Associated Lab Samples: 92414388001, 92414388002 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.3 01/18/19 14:59 1,1,1-Trichloroethane ug/kg ND 5.3 01/18/19 14:59 1,1,2,2-Tetrachloroethane ug/kg ND 5.3 01/18/19 14:59 1,1,2-Trichloroethane ug/kg ND 5.3 01/18/19 14:59 1,1-Dichloroethane ug/kg ND 5.3 01/18/19 14:59 1,1-Dichloroethene ug/kg ND 5.3 01/18/19 14:59 1,1-Dichloropropene ug/kg ND 5.3 01/18/19 14:59 1,2,3-Trichlorobenzene ug/kg ND 5.3 01/18/19 14:59 1,2,3-Trichloropropane ug/kg ND 5.3 01/18/19 14:59 1,2,4-Trichlorobenzene ug/kg ND 5.3 01/18/19 14:59 1,2,4-Trimethylbenzene ug/kg ND 5.3 01/18/19 14:59 1,2-Dibromo-3-chloropropane ug/kg ND 5.3 01/18/19 14:59 1,2-Dibromoethane (EDB) ug/kg ND 5.3 01/18/19 14:59 1,2-Dichlorobenzene ug/kg ND 5.3 01/18/19 14:59 1,2-Dichloroethane ug/kg ND 5.3 01/18/19 14:59 1,2-Dichloropropane ug/kg ND 5.3 01/18/19 14:59 1,3,5-Trimethylbenzene ug/kg ND 5.3 01/18/19 14:59 1,3-Dichlorobenzene ug/kg ND 5.3 01/18/19 14:59 1,3-Dichloropropane ug/kg ND 5.3 01/18/19 14:59 1,4-Dichlorobenzene ug/kg ND 5.3 01/18/19 14:59 2,2-Dichloropropane ug/kg ND 5.3 01/18/19 14:59 2-Butanone (MEK) ug/kg ND 106 01/18/19 14:59 2-Chlorotoluene ug/kg ND 5.3 01/18/19 14:59 2-Hexanone ug/kg ND 53.0 01/18/19 14:59 4-Chlorotoluene ug/kg ND 5.3 01/18/19 14:59 4-Methyl-2-pentanone (MIBK) ug/kg ND 53.0 01/18/19 14:59 Acetone ug/kg ND 106 01/18/19 14:59 Benzene ug/kg ND 5.3 01/18/19 14:59 Bromobenzene ug/kg ND 5.3 01/18/19 14:59 Bromochloromethane ug/kg ND 5.3 01/18/19 14:59 Bromodichloromethane ug/kg ND 5.3 01/18/19 14:59 Bromoform ug/kg ND 5.3 01/18/19 14:59 Bromomethane ug/kg ND 10.6 01/18/19 14:59 Carbon tetrachloride ug/kg ND 5.3 01/18/19 14:59 Chlorobenzene ug/kg ND 5.3 01/18/19 14:59 Chloroethane ug/kg ND 10.6 01/18/19 14:59 Chloroform ug/kg ND 5.3 01/18/19 14:59 Chloromethane ug/kg ND 10.6 01/18/19 14:59 cis-1,2-Dichloroethene ug/kg ND 5.3 01/18/19 14:59 cis-1,3-Dichloropropene ug/kg ND 5.3 01/18/19 14:59 Dibromochloromethane ug/kg ND 5.3 01/18/19 14:59 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 METHOD BLANK: 2476808 Associated Lab Samples: 92414388001, 92414388002 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed Dibromomethane ug/kg ND 5.3 01/18/19 14:59 Dichlorodifluoromethane ug/kg ND 10.6 01/18/19 14:59 Diisopropyl ether ug/kg ND 5.3 01/18/19 14:59 Ethylbenzene ug/kg ND 5.3 01/18/19 14:59 Hexachloro-1,3-butadiene ug/kg ND 5.3 01/18/19 14:59 Isopropylbenzene (Cumene) ug/kg ND 5.3 01/18/19 14:59 m&p-Xylene ug/kg ND 10.6 01/18/19 14:59 Methyl-tert-butyl ether ug/kg ND 5.3 01/18/19 14:59 Methylene Chloride ug/kg ND 21.2 01/18/19 14:59 n-Butylbenzene ug/kg ND 5.3 01/18/19 14:59 n-Propylbenzene ug/kg ND 5.3 01/18/19 14:59 Naphthalene ug/kg ND 5.3 01/18/19 14:59 o-Xylene ug/kg ND 5.3 01/18/19 14:59 p-Isopropyltoluene ug/kg ND 5.3 01/18/19 14:59 sec-Butylbenzene ug/kg ND 5.3 01/18/19 14:59 Styrene ug/kg ND 5.3 01/18/19 14:59 tert-Butyl benzene ug/kg ND 5.3 01/18/19 14:59 Tetrachloroethene ug/kg ND 5.3 01/18/19 14:59 Toluene ug/kg ND 5.3 01/18/19 14:59 trans-1,2-Dichloroethene ug/kg ND 5.3 01/18/19 14:59 trans- 1,3-Dichloropropene ug/kg ND 5.3 01/18/19 14:59 Trichloroethene ug/kg ND 5.3 01/18/19 14:59 Trichlorofluoromethane ug/kg ND 5.3 01/18/19 14:59 Vinyl acetate ug/kg ND 53.0 01/18/19 14:59 Vinyl chloride ug/kg ND 10.6 01/18/19 14:59 Xylene (Total) ug/kg ND 10.6 01/18/19 14:59 1,2-Dichloroethane-d4 (S) % 92 70-132 01/18/19 14:59 4-Bromofluorobenzene (S) % 99 70-130 01/18/19 14:59 Toluene-d8 (S) % 103 70-130 01/18/19 14:59 Qualifiers LABORATORY CONTROL SAMPLE: 2476809 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg 52 52.0 100 70-130 1,1,1-Trichloroethane ug/kg 52 49.4 95 70-130 1,1,2,2-Tetrachloroethane ug/kg 52 47.9 92 55-130 1,1,2-Trichloroethane ug/kg 52 52.4 101 70-130 1,1-Dichloroethane ug/kg 52 46.2 89 68-130 1,1-Dichloroethene ug/kg 52 49.2 95 70-130 1,1-Dichloropropene ug/kg 52 49.3 95 70-130 1,2,3-Trichlorobenzene ug/kg 52 53.7 103 70-130 1,2,3-Trichloropropane ug/kg 52 48.4 93 70-130 1,2,4-Trichlorobenzene ug/kg 52 53.1 102 70-130 1,2,4-Trimethylbenzene ug/kg 52 51.1 98 69-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 LABORATORY CONTROL SAMPLE: Parameter 2476809 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2-Dibromo-3-chloropropane ug/kg 52 57.2 110 57-141 1,2-Dibromoethane (EDB) ug/kg 52 50.9 98 70-130 1,2-Dichlorobenzene ug/kg 52 51.1 98 70-130 1,2-Dichloroethane ug/kg 52 48.7 94 70-130 1,2-Dichloropropane ug/kg 52 50.4 97 70-130 1,3,5-Trimethylbenzene ug/kg 52 51.3 99 70-130 1,3-Dichlorobenzene ug/kg 52 50.8 98 70-130 1,3-Dichloropropane ug/kg 52 52.6 101 70-130 1,4-Dichlorobenzene ug/kg 52 49.8 96 70-130 2,2-Dichloropropane ug/kg 52 49.8 96 70-130 2-Butanone (MEK) ug/kg 104 106 102 60-130 2-Chlorotoluene ug/kg 52 51.6 99 70-130 2-Hexanone ug/kg 104 107 103 70-132 4-Chlorotoluene ug/kg 52 50.9 98 70-130 4-Methyl-2-pentanone (MIBK) ug/kg 104 101 97 69-130 Acetone ug/kg 104 86.7J 83 49-148 Benzene ug/kg 52 51.9 100 70-130 Bromobenzene ug/kg 52 52.7 101 70-130 Bromochloromethane ug/kg 52 48.9 94 70-130 Bromodichloromethane ug/kg 52 49.0 94 70-130 Bromoform ug/kg 52 48.8 94 68-136 Bromomethane ug/kg 52 53.5 103 60-140 Carbon tetrachloride ug/kg 52 48.6 94 70-130 Chlorobenzene ug/kg 52 49.8 96 70-130 Chloroethane ug/kg 52 49.1 94 51-147 Chloroform ug/kg 52 46.5 89 70-130 Chloromethane ug/kg 52 54.1 104 48-130 cis-1,2-Dichloroethene ug/kg 52 50.0 96 70-130 cis-1,3-Dichloropropene ug/kg 52 54.0 104 70-130 Dibromochloromethane ug/kg 52 52.7 101 70-130 Dibromomethane ug/kg 52 52.2 100 70-130 Dichlorodifluoromethane ug/kg 52 49.7 96 49-130 Diisopropyl ether ug/kg 52 50.3 97 66-130 Ethylbenzene ug/kg 52 50.4 97 70-130 Hexachloro-1,3-butadiene ug/kg 52 51.5 99 70-130 Isopropylbenzene (Cumene) ug/kg 52 51.1 98 70-130 m&p-Xylene ug/kg 104 100 96 70-130 Methyl-tert-butyl ether ug/kg 52 50.2 97 70-130 Methylene Chloride ug/kg 52 46.3 89 50-137 n-Butylbenzene ug/kg 52 51.3 99 70-130 n-Propylbenzene ug/kg 52 52.2 100 70-130 Naphthalene ug/kg 52 54.9 106 70-131 o-Xylene ug/kg 52 52.4 101 70-130 p-Isopropyltoluene ug/kg 52 51.2 99 70-130 sec-Butylbenzene ug/kg 52 52.7 101 70-130 Styrene ug/kg 52 51.4 99 70-130 tert-Butyl benzene ug/kg 52 52.7 101 69-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 LABORATORY CONTROL SAMPLE: Parameter 2476809 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Tetrachloroethene ug/kg 52 28.1 54 56-130 L2 Toluene ug/kg 52 47.8 92 70-130 trans-1,2-Dichloroethene ug/kg 52 49.4 95 70-130 trans- 1,3-Dichloropropene ug/kg 52 52.3 101 70-130 Trichloroethene ug/kg 52 53.6 103 70-141 Trichlorofluoromethane ug/kg 52 49.5 95 67-130 Vinyl acetate ug/kg 104 81.0 78 10-136 Vinyl chloride ug/kg 52 55.2 106 67-130 Xylene (Total) ug/kg 156 152 98 70-130 1,2-Dichloroethane-d4 (S) % 90 70-132 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 96 70-130 MATRIX SPIKE SAMPLE: Parameter 2477060 Units 92414475001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg ND 24.7 21.1 85 52-133 1,1,1-Trichloroethane ug/kg ND 24.7 20.3 82 49-137 1,1,2,2-Tetrachloroethane ug/kg ND 24.7 ND 0 39-150 M1 1,1,2-Trichloroethane ug/kg ND 24.7 19.6 80 48-140 1,1-Dichloroethane ug/kg ND 24.7 20.3 82 46-135 1,1-Dichloroethene ug/kg ND 24.7 23.2 94 38-149 1,1-Dichloropropene ug/kg ND 24.7 18.3 74 41-140 1,2,3-Trichlorobenzene ug/kg ND 24.7 11.7 47 10-158 1,2,3-Trichloropropane ug/kg ND 24.7 21.8 89 33-157 1,2,4-Trichlorobenzene ug/kg ND 24.7 11.7 47 10-155 1,2,4-Trimethylbenzene ug/kg ND 24.7 16.8 68 24-154 1,2-Dibromo-3-chloropropane ug/kg ND 24.7 17.7 72 33-158 1,2-Dibromoethane (EDB) ug/kg ND 24.7 21.4 87 40-136 1,2-Dichlorobenzene ug/kg ND 24.7 18.4 75 27-146 1,2-Dichloroethane ug/kg ND 24.7 21.1 86 49-140 1,2-Dichloropropane ug/kg ND 24.7 21.8 89 44-143 1,3,5-Trimethylbenzene ug/kg ND 24.7 17.1 69 40-144 1,3-Dichlorobenzene ug/kg ND 24.7 17.9 73 33-140 1,3-Dichloropropane ug/kg ND 24.7 22.6 92 47-147 1,4-Dichlorobenzene ug/kg ND 24.7 17.6 72 35-139 2,2-Dichloropropane ug/kg ND 24.7 20.9 85 41-140 2-Butanone (MEK) ug/kg ND 49.4 42.1J 85 10-181 2-Chlorotoluene ug/kg ND 24.7 18.9 77 38-147 2-Hexanone ug/kg ND 49.4 45.2J 92 18-169 4-Chlorotoluene ug/kg ND 24.7 19.1 78 36-145 4-Methyl-2-pentanone (MIBK) ug/kg ND 49.4 42.3J 86 16-175 Acetone ug/kg ND 49.4 50J 82 10-200 Benzene ug/kg ND 24.7 22.3 90 46-136 Bromobenzene ug/kg ND 24.7 20.8 84 38-149 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 30 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 MATRIX SPIKE SAMPLE: 2477060 92414475001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Bromochloromethane ug/kg ND 24.7 20.9 85 44-142 Bromodichloromethane ug/kg ND 24.7 20.3 82 41-140 Bromoform ug/kg ND 24.7 17.8 72 34-145 Bromomethane ug/kg ND 24.7 21.2 86 14-162 Carbon tetrachloride ug/kg ND 24.7 20.3 82 44-141 Chlorobenzene ug/kg ND 24.7 21.1 86 39-141 Chloroethane ug/kg ND 24.7 22.2 90 10-182 Chloroform ug/kg ND 24.7 21.1 85 45-140 Chloromethane ug/kg ND 24.7 24.0 98 19-149 cis-1,2-Dichloroethene ug/kg ND 24.7 21.3 86 38-150 cis-1,3-Dichloropropene ug/kg ND 24.7 21.5 87 30-144 Dibromochloromethane ug/kg ND 24.7 20.8 84 36-145 Dibromomethane ug/kg ND 24.7 22.9 93 41-145 Dichlorodifluoromethane ug/kg ND 24.7 22.4 91 16-146 Diisopropyl ether ug/kg ND 24.7 20.8 84 41-143 Ethylbenzene ug/kg ND 24.7 20.2 82 35-144 Hexachloro-1,3-butadiene ug/kg ND 24.7 7.7 31 10-160 Isopropylbenzene (Cumene) ug/kg ND 24.7 18.1 74 30-152 m&p-Xylene ug/kg ND 49.4 39.6 80 33-145 Methyl-tert-butyl ether ug/kg ND 24.7 20.1 82 49-140 Methylene Chloride ug/kg ND 24.7 37.6 133 10-174 n-Butylbenzene ug/kg ND 24.7 12.1 49 10-160 n-Propylbenzene ug/kg ND 24.7 17.8 72 24-159 Naphthalene ug/kg ND 24.7 15.3 62 10-171 o-Xylene ug/kg ND 24.7 20.8 84 31-150 p-Isopropyltoluene ug/kg ND 24.7 14.1 57 21-154 sec-Butylbenzene ug/kg ND 24.7 14.9 61 19-159 Styrene ug/kg ND 24.7 19.9 81 15-152 tert-Butyl benzene ug/kg ND 24.7 16.8 68 31-141 Tetrachloroethene ug/kg ND 24.7 10.9 44 19-141 Toluene ug/kg ND 24.7 20.7 84 31-146 trans-1,2-Dichloroethene ug/kg ND 24.7 21.2 86 28-157 trans- 1,3-Dichloropropene ug/kg ND 24.7 21.8 88 25-146 Trichloroethene ug/kg ND 24.7 33.7 137 34-149 Trichlorofluoromethane ug/kg ND 24.7 20.6 84 10-167 Vinyl acetate ug/kg ND 49.4 15.9J 32 10-200 Vinyl chloride ug/kg ND 24.7 23.1 94 36-155 Xylene (Total) ug/kg ND 73.9 60.4 82 29-148 1,2-Dichloroethane-d4 (S) % 89 70-132 4-Bromofluorobenzene (S) % 102 70-130 Toluene-d8 (S) % 103 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 SAMPLE DUPLICATE: 2477059 Parameter Units 92414311017 Result Dup Result 1,1,1,2-Tetrachloroethane ug/kg ND ND 1,1,1-Trichloroethane ug/kg ND ND 1,1,2,2-Tetrachloroethane ug/kg ND ND 1,1,2-Trichloroethane ug/kg ND ND 1,1-Dichloroethane ug/kg ND ND 1,1-Dichloroethene ug/kg ND ND 1,1-Dichloropropene ug/kg ND ND 1,2,3-Trichlorobenzene ug/kg ND ND 1,2,3-Trichloropropane ug/kg ND ND 1,2,4-Trichlorobenzene ug/kg ND ND 1,2,4-Trimethylbenzene ug/kg ND ND 1,2-Dibromo-3-chloropropane ug/kg ND ND 1,2-Dibromoethane (EDB) ug/kg ND ND 1,2-Dichlorobenzene ug/kg ND ND 1,2-Dichloroethane ug/kg ND ND 1,2-Dichloropropane ug/kg ND ND 1,3,5-Trimethylbenzene ug/kg ND ND 1,3-Dichlorobenzene ug/kg ND ND 1,3-Dichloropropane ug/kg ND ND 1,4-Dichlorobenzene ug/kg ND ND 2,2-Dichloropropane ug/kg ND ND 2-Butanone (MEK) ug/kg ND ND 2-Chlorotoluene ug/kg ND ND 2-Hexanone ug/kg ND ND 4-Chlorotoluene ug/kg ND ND 4-Methyl-2-pentanone (MIBK) ug/kg ND ND Acetone ug/kg ND ND Benzene ug/kg ND ND Bromobenzene ug/kg ND ND Bromochloromethane ug/kg ND ND Bromodichloromethane ug/kg ND ND Bromoform ug/kg ND ND Bromomethane ug/kg ND ND Carbon tetrachloride ug/kg ND ND Chlorobenzene ug/kg ND ND Chloroethane ug/kg ND ND Chloroform ug/kg ND ND Chloromethane ug/kg ND ND cis-1,2-Dichloroethene ug/kg ND ND cis-1,3-Dichloropropene ug/kg ND ND Dibromochloromethane ug/kg ND ND Dibromomethane ug/kg ND ND Dichlorodifluoromethane ug/kg ND ND Diisopropyl ether ug/kg ND ND Ethylbenzene ug/kg ND ND Hexachloro-1,3-butadiene ug/kg ND ND Isopropylbenzene (Cumene) ug/kg ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 SAMPLE DUPLICATE: 2477059 Parameter Units 92414311017 Result Dup Result m&p-Xylene ug/kg ND ND Methyl-tert-butyl ether ug/kg ND ND Methylene Chloride ug/kg ND ND n-Butylbenzene ug/kg ND ND n-Propylbenzene ug/kg ND ND Naphthalene ug/kg ND ND o-Xylene ug/kg ND ND p-Isopropyltoluene ug/kg ND ND sec-Butylbenzene ug/kg ND ND Styrene ug/kg ND ND tert-Butyl benzene ug/kg ND ND Tetrachloroethene ug/kg ND ND Toluene ug/kg ND ND trans-1,2-Dichloroethene ug/kg ND ND trans- 1,3-Dichloropropene ug/kg ND ND Trichloroethene ug/kg ND ND Trichlorofluoromethane ug/kg ND ND Vinyl acetate ug/kg ND ND Vinyl chloride ug/kg ND ND Xylene (Total) ug/kg ND ND 1,2-Dichloroethane-d4 (S) % 76 77 4-Bromofluorobenzene (S) % 100 101 Toluene-d8 (S) % 104 102 RPD Qualifiers 1 0 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 QC Batch: 453143 Analysis Method: EPA 8270D QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave Associated Lab Samples: 92414388001, 92414388002 METHOD BLANK: 2476348 Associated Lab Samples: 92414388001, 92414388002 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/kg ND 326 01/18/19 21:45 1,2-Dichlorobenzene ug/kg ND 326 01/18/19 21:45 1,3-Dichlorobenzene ug/kg ND 326 01/18/19 21:45 1,4-Dichlorobenzene ug/kg ND 326 01/18/19 21:45 1-Methylnaphthalene ug/kg ND 326 01/18/19 21:45 2,2'-Oxybis(1-chloropropane) ug/kg ND 326 01/18/19 21:45 2,4,5-Trichlorophenol ug/kg ND 326 01/18/19 21:45 2,4,6-Trichlorophenol ug/kg ND 326 01/18/19 21:45 2,4-Dichlorophenol ug/kg ND 326 01/18/19 21:45 2,4-Dimethylphenol ug/kg ND 326 01/18/19 21:45 2,4-Dinitrophenol ug/kg ND 1630 01/18/19 21:45 2,4-Dinitrotoluene ug/kg ND 326 01/18/19 21:45 2,6-Dinitrotoluene ug/kg ND 326 01/18/19 21:45 2-Chloronaphthalene ug/kg ND 326 01/18/19 21:45 2-Chlorophenol ug/kg ND 326 01/18/19 21:45 2-Methylnaphthalene ug/kg ND 326 01/18/19 21:45 2-Methylphenol(o-Cresol) ug/kg ND 326 01/18/19 21:45 2-Nitroaniline ug/kg ND 1630 01/18/19 21:45 2-Nitrophenol ug/kg ND 326 01/18/19 21:45 3&4-Methyl phenol (m&p Cresol) ug/kg ND 326 01/18/19 21:45 3,3'-Dichlorobenzidine ug/kg ND 1630 01/18/19 21:45 3-Nitroaniline ug/kg ND 1630 01/18/19 21:45 4,6-Dinitro-2-methyl phenol ug/kg ND 651 01/18/19 21:45 4-Bromophenylphenyl ether ug/kg ND 326 01/18/19 21:45 4-ChIoro-3-methyl phenol ug/kg ND 651 01/18/19 21:45 4-Chloroaniline ug/kg ND 1630 01/18/19 21:45 4-Chlorophenylphenyl ether ug/kg ND 326 01/18/19 21:45 4-Nitroaniline ug/kg ND 651 01/18/19 21:45 4-Nitrophenol ug/kg ND 1630 01/18/19 21:45 Acenaphthene ug/kg ND 326 01/18/19 21:45 Acenaphthylene ug/kg ND 326 01/18/19 21:45 Aniline ug/kg ND 326 01/18/19 21:45 Anthracene ug/kg ND 326 01/18/19 21:45 Benzo(a)anthracene ug/kg ND 326 01/18/19 21:45 Benzo(a)pyrene ug/kg ND 326 01/18/19 21:45 Benzo(b)fluoranthene ug/kg ND 326 01/18/19 21:45 Benzo(g,h,i)perylene ug/kg ND 326 01/18/19 21:45 Benzo(k)fluoranthene ug/kg ND 326 01/18/19 21:45 Benzoic Acid ug/kg ND 1630 01/18/19 21:45 Benzyl alcohol ug/kg ND 651 01/18/19 21:45 bis(2-Chloroethoxy)methane ug/kg ND 326 01/18/19 21:45 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 METHOD BLANK: 2476348 Associated Lab Samples: 92414388001, 92414388002 Parameter Units Matrix: Blank Result Solid Reporting Limit Analyzed bis(2-Chloroethyl) ether ug/kg ND 326 01/18/19 21:45 bis(2-Ethylhexyl)phthalate ug/kg ND 326 01/18/19 21:45 Butylbenzylphthalate ug/kg ND 326 01/18/19 21:45 Chrysene ug/kg ND 326 01/18/19 21:45 Di-n-butylphthalate ug/kg ND 326 01/18/19 21:45 Di-n-octylphthalate ug/kg ND 326 01/18/19 21:45 Dibenz(a,h)anthracene ug/kg ND 326 01/18/19 21:45 Dibenzofuran ug/kg ND 326 01/18/19 21:45 Diethylphthalate ug/kg ND 326 01/18/19 21:45 Dimethylphthalate ug/kg ND 326 01/18/19 21:45 Fluoranthene ug/kg ND 326 01/18/19 21:45 Fluorene ug/kg ND 326 01/18/19 21:45 Hexachloro-1,3-butadiene ug/kg ND 326 01/18/19 21:45 Hexachlorobenzene ug/kg ND 326 01/18/19 21:45 Hexachlorocyclopentadiene ug/kg ND 326 01/18/19 21:45 Hexachloroethane ug/kg ND 326 01/18/19 21:45 Indeno(1,2,3-cd)pyrene ug/kg ND 326 01/18/19 21:45 Isophorone ug/kg ND 326 01/18/19 21:45 N-Nitroso-di-n-propylamine ug/kg ND 326 01/18/19 21:45 N-Nitrosodimethylamine ug/kg ND 326 01/18/19 21:45 N-Nitrosodiphenylamine ug/kg ND 326 01/18/19 21:45 Naphthalene ug/kg ND 326 01/18/19 21:45 Nitrobenzene ug/kg ND 326 01/18/19 21:45 Pentachlorophenol ug/kg ND 1630 01/18/19 21:45 Phenanthrene ug/kg ND 326 01/18/19 21:45 Phenol ug/kg ND 326 01/18/19 21:45 Pyrene ug/kg ND 326 01/18/19 21:45 2,4,6-Tribromophenol (S) % 64 27-110 01/18/19 21:45 2-Fluorobiphenyl (S) % 70 30-110 01/18/19 21:45 2-Fluorophenol (S) % 76 13-110 01/18/19 21:45 Nitrobenzene-d5 (S) % 56 23-110 01/18/19 21:45 Phenol-d6 (S) % 80 22-110 01/18/19 21:45 Terphenyl-d14 (S) % 83 28-110 01/18/19 21:45 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2476349 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg 1680 1150 69 52-130 1,2-Dichlorobenzene ug/kg 1680 1320 79 51-130 1,3-Dichlorobenzene ug/kg 1680 1310 78 50-130 1,4-Dichlorobenzene ug/kg 1680 1320 79 49-130 1-Methylnaphthalene ug/kg 1680 1520 90 55-130 2,2'-Oxybis(1-chloropropane) ug/kg 1680 2440 146 30-130 L1 2,4,5-Trichlorophenol ug/kg 1680 1300 78 55-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 LABORATORY CONTROL SAMPLE: Parameter 2476349 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4,6-TrichIorophenol ug/kg 1680 1270 76 57-130 2,4-DichIorophenol ug/kg 1680 1360 81 56-130 2,4-Dimethylphenol ug/kg 1680 1170 70 51-130 2,4-Dinitrophenol ug/kg 8390 1720 20 27-133 L2 2,4-Dinitrotoluene ug/kg 1680 1200 72 61-130 2,6-Dinitrotoluene ug/kg 1680 1260 75 60-130 2-Chloronaphthalene ug/kg 1680 1590 95 52-130 2-Chlorophenol ug/kg 1680 1560 93 54-130 2-Methylnaphthalene ug/kg 1680 1510 90 54-130 2-Methylphenol(o-Cresol) ug/kg 1680 1400 84 51-130 2-Nitroaniline ug/kg 3360 2350 70 51-130 2-Nitrophenol ug/kg 1680 971 58 49-130 3&4-Methyl phenol (m&p Cresol) ug/kg 1680 1380 82 11-163 3,3'-Dichlorobenzidine ug/kg 3360 2430 73 10-132 3-Nitroaniline ug/kg 3360 3260 97 55-130 4,6-Dinitro-2-methyl phenol ug/kg 3360 1050 31 47-142 L2 4-Bromophenylphenyl ether ug/kg 1680 1300 77 59-130 4-Chloro-3-methylphenol ug/kg 3360 2520 75 55-130 4-Chloroaniline ug/kg 3360 2870 86 54-130 4-Chlorophenylphenyl ether ug/kg 1680 1350 81 58-130 4-Nitroaniline ug/kg 3360 3300 98 54-130 4-Nitrophenol ug/kg 8390 5310 63 48-130 Acenaphthene ug/kg 1680 1480 88 60-130 Acenaphthylene ug/kg 1680 1600 95 60-130 Aniline ug/kg 1680 1360 81 43-130 Anthracene ug/kg 1680 1650 98 63-130 Benzo(a)anthracene ug/kg 1680 1610 96 59-130 Benzo(a)pyrene ug/kg 1680 1690 101 57-130 Benzo(b)fluoranthene ug/kg 1680 1820 109 54-130 Benzo(g,h,i)perylene ug/kg 1680 1500 90 59-130 Benzo(k)fluoranthene ug/kg 1680 1690 101 54-130 Benzoic Acid ug/kg 8390 4420 53 19-130 Benzyl alcohol ug/kg 3360 2900 87 50-130 bis(2-Chloroethoxy)methane ug/kg 1680 1300 77 54-130 bis(2-Chloroethyl) ether ug/kg 1680 1290 77 48-130 bis(2-Ethylhexyl)phthalate ug/kg 1680 1520 90 45-134 Butylbenzylphthalate ug/kg 1680 1640 98 46-138 Chrysene ug/kg 1680 1610 96 58-130 Di-n-butylphthalate ug/kg 1680 1470 87 60-130 Di-n-octylphthalate ug/kg 1680 1700 102 53-130 Dibenz(a,h)anthracene ug/kg 1680 1500 89 59-130 Dibenzofuran ug/kg 1680 1480 88 60-130 Diethylphthalate ug/kg 1680 1290 77 60-130 Dimethylphthalate ug/kg 1680 1300 77 60-130 Fluoranthene ug/kg 1680 1710 102 65-130 Fluorene ug/kg 1680 1540 92 63-130 Hexachloro-1,3-butadiene ug/kg 1680 947 56 46-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 LABORATORY CONTROL SAMPLE: Parameter 2476349 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Hexachlorobenzene ug/kg 1680 1360 81 58-130 Hexachlorocyclopentadiene ug/kg 1680 622 37 23-130 Hexachloroethane ug/kg 1680 1070 64 47-130 Indeno(1,2,3-cd)pyrene ug/kg 1680 1510 90 60-130 Isophorone ug/kg 1680 984 59 49-130 N-Nitroso-di-n-propylamine ug/kg 1680 1200 71 47-130 N-Nitrosodimethylamine ug/kg 1680 1380 82 45-130 N-Nitrosodiphenylamine ug/kg 1680 1570 93 59-130 Naphthalene ug/kg 1680 1500 89 55-130 Nitrobenzene ug/kg 1680 1040 62 49-130 Pentachlorophenol ug/kg 3360 2180 65 10-132 Phenanthrene ug/kg 1680 1600 95 62-130 Phenol ug/kg 1680 1370 81 46-130 Pyrene ug/kg 1680 1730 103 53-130 2,4,6-Tribromophenol (S) % 83 27-110 2-Fluorobiphenyl (S) % 74 30-110 2-Fluorophenol(S) % 87 13-110 Nitrobenzene-d5(S) % 61 23-110 Phenol-d6 (S) % 85 22-110 Terphenyl-d14 (S) % 86 28-110 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 QC Batch: 452951 Analysis Method: MADEP EPH QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil Associated Lab Samples: 92414388001, 92414388002 METHOD BLANK: 2475356 Matrix: Solid Associated Lab Samples: 92414388001, 92414388002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aliphatic (C09-C18) mg/kg ND 10.0 01/18/19 06:55 N2 Aliphatic (C19-C36) mg/kg ND 10.0 01/18/19 06:55 N2 Aromatic (C11-C22) mg/kg ND 10.0 01/18/19 06:55 N2 2-Bromonaphthalene (S) % 66 40-140 01/18/19 06:55 2-Fluorobiphenyl (S) % 64 40-140 01/18/19 06:55 Nonatriacontane (S) % 61 40-140 01/18/19 06:55 o-Terphenyl (S) % 53 40-140 01/18/19 06:55 LABORATORY CONTROL SAMPLE & LCSD: Parameter 2475357 Units Spike Conc. 2475358 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Max Limits RPD RPD Qualifiers Aliphatic (C09-C18) mg/kg 10 ND ND 61 58 40-140 50 N2 Aliphatic (C19-C36) mg/kg 13.3 ND ND 63 63 40-140 50 N2 Aromatic (C11-C22) mg/kg 28.2 14.9 14.5 53 52 40-140 2 50 N2 2-Bromonaphthalene (S) % 63 61 40-140 2-Fluorobiphenyl (S) % 63 62 40-140 Nonatriacontane (S) % 68 71 40-140 o-Terphenyl(S) % 57 61 40-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 30 Pace Analytical Services, LLC ceAnalX cal ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 QC Batch: 453132 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92414388001, 92414388002 SAMPLE DUPLICATE: 2476314 92414388001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 30.0 31.1 4 SAMPLE DUPLICATE: 2476315 92414423001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 57.5 58.1 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 30 Pace Analytical Services, LLC ceAnalX cal ® 9800 Kiney Ave. Suite 100 Huntersville, NC 28078078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. SO Surrogate recovery outside laboratory control limits. S4 Surrogate recovery not evaluated against control limits due to sample dilution. S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis). REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /24/2019 01:26 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 30 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: MEADOW OAK INDUSTRIAL PHASE I Pace Project No.: 92414388 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92414388001 MW1-15 MADEP EPH 452951 MADEP EPH 453209 92414388002 MW1-25 MADEP EPH 452951 MADEP EPH 453209 92414388001 MW1-15 MADEP VPH 453342 MADEP VPH 453348 92414388002 MW1-25 MADEP VPH 453342 MADEP VPH 453348 92414388001 MW1-15 EPA 3546 453143 EPA 8270D 453324 92414388002 MW1-25 EPA 3546 453143 EPA 8270D 453324 92414388001 MW1-15 EPA 5035A 453256 EPA 8260B 453292 92414388002 MW1-25 EPA 5035A 453256 EPA 8260B 453292 92414388001 MW1-15 ASTM D2974-87 453132 92414388002 MW1-25 ASTM D2974-87 453132 Date: 01/24/2019 01:26 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 30 Document Name:_ Oacutitent Revised: Fearuary +, IssuingAutnancY; aceAnalyfica! Document No.: pace Carolinas gsia[1 Office I F-CAR-CS•033-Rev.06 Laboratory receiving samples: Raleigh❑ Mechanicsville❑ Asheville ❑ Eden❑ Greenwood ❑ Huntersvilte ll,I OTir }� SampleCondiliClient Name: IW92414388 Upon Re(eipt Project #: Courier: [2Ee-d-Ex_ _ ❑UPS ❑USPS ❑Client 0 Commercial ❑Pace ❑Other: 92414388 Custody Seal Present? ❑Yes ❑No. Seals Intact? ❑Yes ONO cate(Inttlals Person Examining Contents"- { Biological Tissue Frozen?. Packing Mate;fah: ❑Bubble Wrap ❑Bubble Bags []None. ❑ Other []yes []NO ❑N/A Thermometer: Type of Ice: ❑'Net []Blue ❑Non: I�dt bun ID: 92`F046 CoolerTemprQ: { Correctlon Factor: Add/SubtractN Q,0 _ Temp Should be above freezing to 6'C j [Samples out of temp criteria. Samples on Ice, cooling process Coolertemp Corrected ('C): hasten USDA Regulated Soil (❑ N/A, water sample) lesorl&ate from a forel n source (Intec ationally, B Did samales origlaate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did sAmp Nawai[ and Fuerto Rico)? []Yes No ❑Yes ONo Chain of Custody Present? ❑Yes I]No El N/A 1. Samples Arrived within Hold Time? ]yes, []No ❑N/A 2. Short Hold Time Analysis (c71hr.)? []yes ❑No ❑NIA 3. Rush Turn Around Time Requested? []yes []NO ❑NIA 4• SuffsdentVolume? '❑Yes ❑Na ❑NIA S. Correct Containers Used? -Pace Containers Used? ❑Yes ❑Yes ❑No ❑No ❑NIA ❑N/A 6. Containers Intact? ❑Yes []No I]N/A 7. Dissolved analysis. Samples Field Filtered? Dyes ONO ❑NIA I Sample Labels Match COC? Dyes []No ❑NIA 9, -includesDate/Tlme/lD/Analysis Matrix; c L Heads ace in VOA Vials (>5-6mm)? Trip Blank Present? []Yes ❑Yes ❑No ❑Na ON/A []N/A 10, 11, Trip BlankCuslody Seals Present? Oyes ❑No EIN/A COMMEWSISAMPLE DISCREPANCY Lot ID of S CLIENT NO-RFICATtONIRESOLLITSON Person contacted: Date/Time: Field Data Required? ❑Yes ONO Project Manager SCURF Review: Date: Date: Project Manager SRF Review: Page 28 of 30 V V..Y�44G4,� 4\o41�c. :onalition-Upon-Recel� Document No.: f-CAR-05-033-Rev.05 Page i of 2 _ issuing Authority: f arnlima5 Ouafity Office *Check mark top half of box if pH and/or dechforination is verifled and within the acceptance range for preservation samples, Exceptfans: VOA, Collform, TOC, Oil and Grease, oROIBO15 (water) DOC, LLHS **Bottom half of box 1s to list number of bottle Prole 1W4# : 92414388 pM Due Date: 01/24/19 CLIENT: 92—ECS z M U z u 1 J N ama Y V U. Z 7 u 1 J N m z 'O m ? 7 u 6 J lw ry Z Q a rzxu d `yr V N V x O Q. N V s m Z G J O Z Oil ar � z 6., d U A. x x O u d J E y 7 M l7 s E v Q V e « N u T .rd+ Z N 2 e a u J �Ou71 l7 N v s a �. s Q a._�+ la ¢ V x g a = m J l9 a y 7 a 4 E (n V i7 a .� a J O [a A a zQUW p N o J l7 ] t+ a i J D > a 55 O^. o 7 J D l7 01 ? j o a N 46 p �! a 7 .y .i a z H d H J E 6. a n Jrr G �dy a. F V O .... d J- E O a Ln m ? y a E a G E �p� la a S y a m 0 L O Va > z N .? e E a G N 1. NMI 1 3 4 5 6 7 8 4 1Q 1 2. pH Adjustment Log. for Preserved Samples Sample IA Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot # adlusted added Note: Whenever there Is a discrepancy affecting North Caroltna compliance samples, a capy of this form will he sent to the North Carolina DEHNR Certiricatlon Offlce (I.e. Out of hold, Incorrect preservative, out of temp, incorrect containers. Page 29 of 30 `cea,raryrrcar CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company: ECS Charlotte Report To, Joe Nestor Attention' Address: 1812 Center Park Drive Copy To: Company Name: Charlotte, NC 28217 Address. Requiatory Agency Emall', jnestor ecslimited. com Purchase Order # Pace Ouote Phone. NONE Fax Project Name: Meadow Oak Industrial Phase t Pace Project Manager: j 9 taylocexell pacela6s.cam, State! Loeadan Requested Due Date: Project #: Pace Profile #: NC R uested Analysis Filtered YIN ti Z MATRix CODE D COLLECTED z Preservatives } ❑�w�3 war�r ow - O o WaSm WT °u m wnsi�wotcr ww Produd P SAMPLE ID So-119o1id SL - � .-r z on OL O START END y F m One Character per box. W.P. wPrt Q fA-Z, 0-91, -) A.1 A other Oa a } ,n H m in o U Sample Ids must be unique ,ter, �z x J p p o Cc oa - / /iq w 1— a a x x o N o a o O] o x 0 >7 o 3� y DATE TIME DATE TIME w � x z z M � Cc 1 (A 74 V t�rs,f 'Yi f1 V, V V 2 - ? 5 L- +�i J r tl ✓ (yi 3 4 5 6 7 8 4 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY AFFILIATION DATE TIME CEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS 17 IN ho , SAMPLER NAME AND SIGNATURE 0 PRINT Name of SAMPLER: m z m} m $ @ m ? SIGNATURE of SAMPLER: DATE Signed: H IX IL) co `c} aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 January 25, 2019 Joe Nestor ECS Southeast 1812 Center Park Drive Suite D Charlotte, NC 28217 RE: Project: GROUNDWATER Pace Project No.: 92414635 Dear Joe Nestor: Enclosed are the analytical results for sample(s) received by the laboratory on January 18, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, p Taylor Ezell taylor.ezell@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: GROUNDWATER Pace Project No.: 92414635 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: GROUNDWATER 92414635 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92414635001 MW-1 MADEP EPH SEM 7 PASI-C MADEP VPH LMB 6 PASI-C EPA 625.1 PKS 58 PASI-C SM 6200B GAW 16 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 24 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GROUNDWATER Pace Project No.: 92414635 Sample: MW-1 Lab ID: 92414635001 Collected: 01/18/19 15:15 Received: 01/18/19 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH Aliphatic (C09-C18) ND ug/L 98.0 1 01/24/19 11:45 01/25/19 08:07 N2 Aliphatic (C19-C36) ND ug/L 98.0 1 01/24/19 11:45 01/25/19 08:07 N2 Aromatic (C11-C22) ND ug/L 98.0 1 01/24/19 11:45 01/25/19 08:07 N2 Surrogates Nonatriacontane (S) 73 % 40-140 1 01/24/19 11:45 01/25/19 08:07 7194-86-7 o-Terphenyl (S) 79 % 40-140 1 01/24/19 11:45 01/25/19 08:07 84-15-1 2-Fluorobiphenyl (S) 84 % 40-140 1 01/24/19 11:45 01/25/19 08:07 321-60-8 2-Bromonaphthalene (S) 74 % 40-140 1 01/24/19 11:45 01/25/19 08:07 580-13-2 VPH NC Water Analytical Method: MADEP VPH Aliphatic (C05-CO8) ND ug/L 50.0 1 01/24/19 18:00 N2 Aliphatic (C09-C12) ND ug/L 50.0 1 01/24/19 18:00 N2 Aliphatic(C09-C12)Adjusted ND ug/L 50.0 1 01/24/19 18:00 N2 Aromatic (C09-C10) ND ug/L 50.0 1 01/24/19 18:00 N2 Surrogates 4-Bromofluorobenzene (FID) (S) 80 % 70-130 1 01/24/19 18:00 460-00-4 4-Bromofluorobenzene (PID) (S) 79 % 70-130 1 01/24/19 18:00 460-00-4 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Acenaphthene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 83-32-9 Acenaphthylene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 208-96-8 Anthracene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 120-12-7 Benzo(a)anthracene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 56-55-3 Benzo(a)pyrene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 50-32-8 Benzo(b)fluoranthene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 205-99-2 Benzo(g,h,i)perylene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 191-24-2 Benzo(k)fluoranthene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 207-08-9 4-Bromophenylphenyl ether ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 101-55-3 Butylbenzylphthalate ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 85-68-7 4-ChIoro-3-methyl phenol ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 59-50-7 bis(2-Chloroethoxy)methane ND ug/L 9.8 1 01/21/19 12:12 01/22/19 22:23 111-91-1 bis(2-Chloroethyl) ether ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 111-44-4 2-Chloronaphthalene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 91-58-7 2-Chlorophenol ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 95-57-8 4-Chlorophenylphenyl ether ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 7005-72-3 Chrysene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 218-01-9 Dibenz(a,h)anthracene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 53-70-3 3,3'-Dichlorobenzidine ND ug/L 24.5 1 01/21/19 12:12 01/22/19 22:23 91-94-1 2,4-Dichlorophenol ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 120-83-2 Diethylphthalate ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 84-66-2 2,4-Dimethylphenol ND ug/L 9.8 1 01/21/19 12:12 01/22/19 22:23 105-67-9 Dimethylphthalate ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 131-11-3 Di-n-butylphthalate ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/L 19.6 1 01/21/19 12:12 01/22/19 22:23 534-52-1 2,4-Dinitrophenol ND ug/L 49.0 1 01/21/19 12:12 01/22/19 22:23 51-28-5 2,4-Dinitrotoluene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 121-14-2 2,6-Dinitrotoluene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 606-20-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 24 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: GROUNDWATER Pace Project No.: 92414635 Sample: MW-1 Parameters ANALYTICAL RESULTS Lab ID: 92414635001 Collected: 01/18/19 15:15 Received: 01/18/19 16:20 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual 625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Di-n-octylphthalate ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 117-81-7 Fluoranthene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 206-44-0 Fluorene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 86-73-7 Hexachloro-1,3-butadiene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 87-68-3 Hexachlorobenzene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 118-74-1 Hexachlorocyclopentadiene ND ug/L 9.8 1 01/21/19 12:12 01/22/19 22:23 77-47-4 Hexachloroethane ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 193-39-5 Isophorone ND ug/L 9.8 1 01/21/19 12:12 01/22/19 22:23 78-59-1 Naphthalene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 91-20-3 Nitrobenzene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 98-95-3 2-Nitrophenol ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 88-75-5 4-Nitrophenol ND ug/L 49.0 1 01/21/19 12:12 01/22/19 22:23 100-02-7 N-Nitrosodimethylamine ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 62-75-9 N-Nitroso-di-n-propylamine ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 621-64-7 N-Nitrosodiphenylamine ND ug/L 9.8 1 01/21/19 12:12 01/22/19 22:23 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 108-60-1 Pentachlorophenol ND ug/L 9.8 1 01/21/19 12:12 01/22/19 22:23 87-86-5 Phenanthrene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 85-01-8 Phenol ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 108-95-2 Pyrene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 129-00-0 1,2,4-Trichlorobenzene ND ug/L 4.9 1 01/21/19 12:12 01/22/19 22:23 120-82-1 2,4,6-TrichIorophenol ND ug/L 9.8 1 01/21/19 12:12 01/22/19 22:23 88-06-2 Surrogates Nitrobenzene-d5 (S) 83 % 10-120 1 01/21/19 12:12 01/22/19 22:23 4165-60-0 2-Fluorobiphenyl (S) 76 % 15-120 1 01/21/19 12:12 01/22/19 22:23 321-60-8 Terphenyl-d14 (S) 61 % 11-131 1 01/21/19 12:12 01/22/19 22:23 1718-51-0 Phenol-d6 (S) 27 % 10-120 1 01/21/19 12:12 01/22/19 22:23 13127-88-3 2-Fluorophenol (S) 38 % 10-120 1 01/21/19 12:12 01/22/19 22:23 367-12-4 2,4,6-Tribromophenol (S) 74 % 10-137 1 01/21/19 12:12 01/22/19 22:23 118-79-6 602 Volatiles by Method 6200 Analytical Method: SM 6200B Benzene ND ug/L 1.0 1 01/23/19 10:50 71-43-2 Chlorobenzene ND ug/L 1.0 1 01/23/19 10:50 108-90-7 1,2-Dichlorobenzene ND ug/L 1.0 1 01/23/19 10:50 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 01/23/19 10:50 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 01/23/19 10:50 106-46-7 Diisopropyl ether ND ug/L 1.0 1 01/23/19 10:50 108-20-3 Ethylbenzene ND ug/L 1.0 1 01/23/19 10:50 100-41-4 Isopropylbenzene (Cumene) ND ug/L 1.0 1 01/23/19 10:50 98-82-8 Methyl-tert-butyl ether ND ug/L 1.0 1 01/23/19 10:50 1634-04-4 Naphthalene ND ug/L 2.0 1 01/23/19 10:50 91-20-3 Toluene ND ug/L 1.0 1 01/23/19 10:50 108-88-3 m&p-Xylene ND ug/L 2.0 1 01/23/19 10:50 179601-23-1 o-Xylene ND ug/L 1.0 1 01/23/19 10:50 95-47-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: GROUNDWATER Pace Project No.: 92414635 Sample: MW-1 Lab ID: 92414635001 Collected: 01/18/19 15:15 Received: 01/18/19 16:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 602 Volatiles by Method 6200 Analytical Method: SM 6200B Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 01/23/19 10:50 460-00-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 1 01/23/19 10:50 17060-07-0 Toluene-d8(S) 97 % 70-130 1 01/23/19 10:50 2037-26-5 Date: 01/25/2019 11:40 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 QC Batch: 454352 Analysis Method: MADEP VPH QC Batch Method: MADEP VPH Analysis Description: VPH NC Water Associated Lab Samples: 92414635001 METHOD BLANK: 2481535 Associated Lab Samples: 92414635001 Parameter Units Aliphatic (C05-008) ug/L Aliphatic (C09-C12) ug/L Aromatic (C09-C10) ug/L 4-Bromofluorobenzene (FID) (S) % 4-Bromofluorobenzene (PID) (S) % Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 50.0 01/24/1917:00 N2 ND 50.0 01/24/1917:00 N2 ND 50.0 01/24/1917:00 N2 80 70-130 01/24/1917:00 80 70-130 01/24/1917:00 LABORATORY CONTROL SAMPLE & LCSD: 2481536 2481537 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C05-CO8) ug/L 300 345 328 115 109 70-130 5 25 N2 Aliphatic (C09-C12) ug/L 300 307 290 102 97 30-130 6 25 N2 Aromatic (C09-C10) ug/L 100 95.3 92.0 95 92 70-130 4 25 N2 4-Bromofluorobenzene (FID) (S) % 78 83 70-130 4-Bromofluorobenzene (PID) (S) % 77 83 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 QC Batch: 453769 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 602 by 6200B Associated Lab Samples: 92414635001 METHOD BLANK: 2479176 Associated Lab Samples: 92414635001 Parameter Units 1,2-Dichlorobenzene ug/L 1,3-Dichlorobenzene ug/L 1,4-Dichlorobenzene ug/L Benzene ug/L Chlorobenzene ug/L Diisopropyl ether ug/L Ethylbenzene ug/L Isopropylbenzene (Cumene) ug/L m&p-Xylene ug/L Methyl-tert-butyl ether ug/L Naphthalene ug/L o-Xylene ug/L Toluene ug/L 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Matrix: Water Blank Result Reporting Limit Analyzed ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 2.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 2.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 ND 1.0 01/23/19 09:29 98 70-130 01/23/19 09:29 94 70-130 01/23/19 09:29 100 70-130 01/23/19 09:29 LABORATORY CONTROL SAMPLE: Parameter 2479177 Units Spike Conc. LCS Result 1,2-Dichlorobenzene ug/L 50 51.1 1,3-Dichlorobenzene ug/L 50 50.2 1,4-Dichlorobenzene ug/L 50 49.9 Benzene ug/L 50 50.5 Chlorobenzene ug/L 50 49.6 Diisopropyl ether ug/L 50 51.6 Ethylbenzene ug/L 50 50.2 Isopropylbenzene (Cumene) ug/L 50 51.9 m&p-Xylene ug/L 100 101 Methyl-tert-butyl ether ug/L 50 52.7 Naphthalene ug/L 50 53.5 o-Xylene ug/L 50 51.1 Toluene ug/L 50 49.0 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % LCS % Rec Qualifiers % Rec Limits 102 60-140 100 60-140 100 60-140 101 60-140 99 60-140 103 60-140 100 60-140 104 60-140 101 60-140 105 60-140 107 60-140 102 60-140 98 60-140 102 70-130 97 70-130 95 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2479178 2479179 MS MSD 92414635001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,2-Dichlorobenzene ug/L ND 20 20 22.6 21.5 113 108 60-140 5 1,3-Dichlorobenzene ug/L ND 20 20 23.0 21.8 115 109 60-140 5 1,4-Dichlorobenzene ug/L ND 20 20 22.6 22.2 113 111 60-140 2 Benzene ug/L ND 20 20 22.3 21.8 112 109 60-140 2 Chlorobenzene ug/L ND 20 20 21.6 22.4 108 112 60-140 4 Diisopropyl ether ug/L ND 20 20 22.1 21.9 110 110 60-140 1 Ethylbenzene ug/L ND 20 20 22.0 22.7 110 113 60-140 3 Isopropylbenzene (Cumene) ug/L ND 20 20 22.6 23.6 113 118 60-140 4 m&p-Xylene ug/L ND 40 40 44.8 46.4 112 116 60-140 3 Methyl-tert-butyl ether ug/L ND 20 20 22.0 21.5 110 108 60-140 2 Naphthalene ug/L ND 20 20 22.4 21.6 112 108 60-140 4 o-Xylene ug/L ND 20 20 21.7 22.7 108 114 60-140 5 Toluene ug/L ND 20 20 21.9 21.6 109 108 60-140 1 1,2-Dichloroethane-d4 (S) % 96 98 70-130 4-Bromofluorobenzene (S) % 96 102 70-130 Toluene-d8(S) % 99 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 24 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 QC Batch: 453488 Analysis Method: EPA 625.1 QC Batch Method: EPA 625.1 Analysis Description: 625 MSS Associated Lab Samples: 92414635001 METHOD BLANK: 2477938 Associated Lab Samples: 92414635001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,2,4-Trichlorobenzene ug/L ND 5.0 01/22/19 11:42 2,2'-Oxybis(1-chloropropane) ug/L ND 5.0 01/22/19 11:42 2,4,6-Trichlorophenol ug/L ND 10.0 01/22/19 11:42 2,4-Dichlorophenol ug/L ND 5.0 01/22/19 11:42 2,4-Dimethylphenol ug/L ND 10.0 01/22/19 11:42 2,4-Dinitrophenol ug/L ND 50.0 01/22/19 11:42 2,4-Dinitrotoluene ug/L ND 5.0 01/22/19 11:42 2,6-Dinitrotoluene ug/L ND 5.0 01/22/19 11:42 2-Chloronaphthalene ug/L ND 5.0 01/22/19 11:42 2-Chlorophenol ug/L ND 5.0 01/22/19 11:42 2-Nitrophenol ug/L ND 5.0 01/22/19 11:42 3,3'-Dichlorobenzidine ug/L ND 25.0 01/22/19 11:42 4,6-Dinitro-2-methyl phenol ug/L ND 20.0 01/22/19 11:42 4-Bromophenylphenyl ether ug/L ND 5.0 01/22/19 11:42 4-Chloro-3-methylphenol ug/L ND 5.0 01/22/19 11:42 4-Chlorophenylphenyl ether ug/L ND 5.0 01/22/19 11:42 4-Nitrophenol ug/L ND 50.0 01/22/19 11:42 Acenaphthene ug/L ND 5.0 01/22/19 11:42 Acenaphthylene ug/L ND 5.0 01/22/19 11:42 Anthracene ug/L ND 5.0 01/22/19 11:42 Benzo(a)anthracene ug/L ND 5.0 01/22/19 11:42 Benzo(a)pyrene ug/L ND 5.0 01/22/19 11:42 Benzo(b)fluoranthene ug/L ND 5.0 01/22/19 11:42 Benzo(g,h,i)perylene ug/L ND 5.0 01/22/19 11:42 Benzo(k)fluoranthene ug/L ND 5.0 01/22/19 11:42 bis(2-Chloroethoxy)methane ug/L ND 10.0 01/22/19 11:42 bis(2-Chloroethyl) ether ug/L ND 5.0 01/22/19 11:42 bis(2-Ethylhexyl)phthalate ug/L ND 5.0 01/22/19 11:42 Butylbenzylphthalate ug/L ND 5.0 01/22/19 11:42 Chrysene ug/L ND 5.0 01/22/19 11:42 Di-n-butylphthalate ug/L ND 5.0 01/22/19 11:42 Di-n-octylphthalate ug/L ND 5.0 01/22/19 11:42 Dibenz(a,h)anthracene ug/L ND 5.0 01/22/19 11:42 Diethylphthalate ug/L ND 5.0 01/22/19 11:42 Dimethylphthalate ug/L ND 5.0 01/22/19 11:42 Fluoranthene ug/L ND 5.0 01/22/19 11:42 Fluorene ug/L ND 5.0 01/22/19 11:42 Hexachloro-1,3-butadiene ug/L ND 5.0 01/22/19 11:42 Hexachlorobenzene ug/L ND 5.0 01/22/19 11:42 Hexachlorocyclopentadiene ug/L ND 10.0 01/22/19 11:42 Hexachloroethane ug/L ND 5.0 01/22/19 11:42 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 24 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 METHOD BLANK: 2477938 Associated Lab Samples: 92414635001 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed Indeno(1,2,3-cd)pyrene ug/L ND 5.0 01/22/19 11:42 Isophorone ug/L ND 10.0 01/22/19 11:42 N-Nitroso-di-n-propylamine ug/L ND 5.0 01/22/19 11:42 N-Nitrosodimethylamine ug/L ND 5.0 01/22/19 11:42 N-Nitrosodiphenylamine ug/L ND 10.0 01/22/19 11:42 Naphthalene ug/L ND 5.0 01/22/19 11:42 Nitrobenzene ug/L ND 5.0 01/22/19 11:42 Pentachlorophenol ug/L ND 10.0 01/22/19 11:42 Phenanthrene ug/L ND 5.0 01/22/19 11:42 Phenol ug/L ND 5.0 01/22/19 11:42 Pyrene ug/L ND 5.0 01/22/19 11:42 2,4,6-Tribromophenol (S) % 72 10-137 01/22/19 11:42 2-Fluorobiphenyl (S) % 87 15-120 01/22/19 11:42 2-Fluorophenol (S) % 42 10-120 01/22/19 11:42 Nitrobenzene-d5 (S) % 77 10-120 01/22/19 11:42 Phenol-d6 (S) % 27 10-120 01/22/19 11:42 Terphenyl-d14 (S) % 76 11-131 01/22/19 11:42 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2477939 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ug/L 50 32.8 66 44-142 2,2'-Oxybis(1-chloropropane) ug/L 50 43.0 86 36-166 2,4,6-Trichlorophenol ug/L 50 36.4 73 37-144 2,4-Dichlorophenol ug/L 50 34.6 69 39-135 2,4-Dimethylphenol ug/L 50 34.6 69 32-120 2,4-Dinitrophenol ug/L 250 168 67 1-191 2,4-Dinitrotoluene ug/L 50 45.6 91 39-139 2,6-Dinitrotoluene ug/L 50 46.6 93 50-158 2-Chloronaphthalene ug/L 50 40.2 80 60-120 2-Chlorophenol ug/L 50 30.9 62 23-134 2-Nitrophenol ug/L 50 35.8 72 29-181 3,3'-Dichlorobenzidine ug/L 100 83.0 83 1-262 4,6-Dinitro-2-methyl phenol ug/L 100 88.3 88 1-181 4-Bromophenylphenyl ether ug/L 50 43.3 87 53-127 4-ChIoro-3-methyl phenol ug/L 100 74.0 74 22-147 4-Chlorophenylphenyl ether ug/L 50 42.4 85 25-158 4-Nitrophenol ug/L 250 104 42 1-132 Acenaphthene ug/L 50 46.1 92 47-145 Acenaphthylene ug/L 50 49.1 98 33-145 Anthracene ug/L 50 51.7 103 27-133 Benzo(a)anthracene ug/L 50 50.4 101 33-143 Benzo(a)pyrene ug/L 50 48.6 97 17-163 Benzo(b)fluoranthene ug/L 50 47.8 96 24-159 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 24 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 LABORATORY CONTROL SAMPLE: 2477939 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(g,h,i)perylene ug/L 50 43.4 87 1-219 Benzo(k)fluoranthene ug/L 50 47.2 94 11-162 bis(2-Chloroethoxy)methane ug/L 50 39.7 79 33-184 bis(2-Chloroethyl) ether ug/L 50 37.7 75 12-158 bis(2-Ethylhexyl)phthalate ug/L 50 55.2 110 8-158 Butylbenzylphthalate ug/L 50 56.1 112 1-152 Chrysene ug/L 50 47.7 95 17-168 Di-n-butylphthalate ug/L 50 53.5 107 1-120 Di-n-octylphthalate ug/L 50 56.9 114 4-146 Dibenz(a,h)anthracene ug/L 50 46.6 93 1-227 Diethylphthalate ug/L 50 47.8 96 1-120 Dimethylphthalate ug/L 50 45.3 91 1-120 Fluoranthene ug/L 50 50.3 101 26-137 Fluorene ug/L 50 46.8 94 59-121 Hexachloro-1,3-butadiene ug/L 50 30.5 61 24-120 Hexachlorobenzene ug/L 50 44.4 89 1-152 Hexachlorocyclopentadiene ug/L 50 34.2 68 25-150 Hexachloroethane ug/L 50 31.6 63 40-120 Indeno(1,2,3-cd)pyrene ug/L 50 47.1 94 1-171 Isophorone ug/L 50 37.4 75 21-196 N-Nitroso-di-n-propylamine ug/L 50 41.4 83 1-230 N-Nitrosodimethylamine ug/L 50 29.5 59 25-150 N-Nitrosodiphenylamine ug/L 50 49.5 99 25-150 Naphthalene ug/L 50 40.2 80 21-133 Nitrobenzene ug/L 50 41.0 82 35-180 Pentachlorophenol ug/L 100 66.4 66 14-176 Phenanthrene ug/L 50 52.0 104 54-120 Phenol ug/L 50 17.0 34 5-120 Pyrene ug/L 50 45.9 92 52-120 2,4,6-Tribromophenol (S) % 88 10-137 2-Fluorobiphenyl (S) % 83 15-120 2-Fluorophenol (S) % 39 10-120 Nitrobenzene-d5 (S) % 87 10-120 Phenol-d6 (S) % 28 10-120 Terphenyl-d14 (S) % 74 11-131 MATRIX SPIKE SAMPLE: 2477941 92413985038 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/L ND 47.6 28.2 59 44-142 2,2'-Oxybis(1-chloropropane) ug/L ND 47.6 46.4 97 36-166 2,4,6-Trichlorophenol ug/L ND 47.6 32.4 68 37-144 2,4-Dichlorophenol ug/L ND 47.6 30.1 63 39-135 2,4-Dimethylphenol ug/L 29.6 47.6 60.1 64 32-120 2,4-Dinitrophenol ug/L ND 238 157 66 1-191 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 24 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 MATRIX SPIKE SAMPLE: 2477941 92413985038 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2,4-Dinitrotoluene ug/L ND 47.6 38.8 81 39-139 2,6-Dinitrotoluene ug/L ND 47.6 40.4 85 50-158 2-Chloronaphthalene ug/L ND 47.6 32.1 67 60-120 2-Chlorophenol ug/L ND 47.6 26.0 55 23-134 2-Nitrophenol ug/L ND 47.6 27.7 58 29-182 3,3'-Dichlorobenzidine ug/L ND 95.2 ND 0 1-262 M1 4,6-Dinitro-2-methyl phenol ug/L ND 95.2 80.2 84 1-181 4-Bromophenylphenyl ether ug/L ND 47.6 38.2 80 53-127 4-Chloro-3-methylphenol ug/L ND 95.2 71.4 75 22-147 4-Chlorophenylphenyl ether ug/L ND 47.6 36.3 76 25-158 4-Nitrophenol ug/L ND 238 106 45 1-132 Acenaphthene ug/L ND 47.6 38.4 81 47-145 Acenaphthylene ug/L ND 47.6 38.9 82 33-145 Anthracene ug/L ND 47.6 44.9 94 27-133 Benzo(a)anthracene ug/L ND 47.6 43.5 91 33-143 Benzo(a)pyrene ug/L ND 47.6 43.2 91 17-163 Benzo(b)fluoranthene ug/L ND 47.6 45.6 96 24-159 Benzo(g,h,i)perylene ug/L ND 47.6 47.7 100 1-219 Benzo(k)fluoranthene ug/L ND 47.6 45.5 95 11-162 bis(2-Chloroethoxy)methane ug/L ND 47.6 30.8 65 33-184 bis(2-Chloroethyl) ether ug/L ND 47.6 29.8 63 12-158 bis(2-Ethylhexyl)phthalate ug/L ND 47.6 48.3 102 8-158 Butylbenzylphthalate ug/L ND 47.6 47.9 101 1-152 Chrysene ug/L ND 47.6 41.5 87 17-168 Di-n-butylphthalate ug/L ND 47.6 45.9 96 1-120 Di-n-octylphthalate ug/L ND 47.6 52.5 110 4-146 Dibenz(a,h)anthracene ug/L ND 47.6 48.7 102 1-227 Diethylphthalate ug/L ND 47.6 38.9 82 1-120 Dimethylphthalate ug/L ND 47.6 36.5 77 1-120 Fluoranthene ug/L ND 47.6 43.6 92 26-137 Fluorene ug/L 1.01 47.6 39.5 81 59-121 Hexachloro-1,3-butadiene ug/L ND 47.6 27.3 57 24-120 Hexachlorobenzene ug/L ND 47.6 37.3 78 1-152 Hexachlorocyclopentadiene ug/L ND 47.6 25.2 53 25-150 Hexachloroethane ug/L ND 47.6 28.7 60 40-120 Indeno(1,2,3-cd)pyrene ug/L ND 47.6 48.4 102 1-171 Isophorone ug/L ND 47.6 30.0 63 21-196 N-Nitroso-di-n-propylamine ug/L ND 47.6 33.2 70 1-230 N-Nitrosodimethylamine ug/L ND 47.6 24.4 51 25-150 N-Nitrosodiphenylamine ug/L ND 47.6 42.4 89 25-150 Naphthalene ug/L 223 47.6 220 -6 21-133 M1 Nitrobenzene ug/L ND 47.6 30.2 63 35-180 Pentachlorophenol ug/L ND 95.2 71.1 75 14-176 Phenanthrene ug/L ND 47.6 46.2 97 54-120 Phenol ug/L ND 47.6 16.4 34 5-120 Pyrene ug/L ND 47.6 44.1 93 52-120 2,4,6-Tribromophenol (S) % 90 10-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 MATRIX SPIKE SAMPLE: 2477941 92413985038 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Fluorobiphenyl (S) % 70 15-120 2-Fluorophenol(S) % 36 10-120 Nitrobenzene-d5 (S) % 74 10-120 Phenol-d6 (S) % 29 10-120 Terphenyl-d14 (S) % 50 11-131 SAMPLE DUPLICATE: 2477940 Parameter Units 92414358008 Result Dup Result 1,2,4-Trichlorobenzene ug/L ND ND 2,2'-Oxybis(1-chloropropane) ug/L ND ND 2,4,6-Trichlorophenol ug/L ND ND 2,4-Dichlorophenol ug/L ND ND 2,4-Dimethylphenol ug/L ND ND 2,4-Dinitrophenol ug/L ND ND 2,4-Dinitrotoluene ug/L ND ND 2,6-Dinitrotoluene ug/L ND ND 2-Chloronaphthalene ug/L ND ND 2-Chlorophenol ug/L ND ND 2-Nitrophenol ug/L ND ND 3,3'-Dichlorobenzidine ug/L ND ND 4,6-Dinitro-2-methyl phenol ug/L ND ND 4-Bromophenylphenyl ether ug/L ND ND 4-Chloro-3-methylphenol ug/L ND ND 4-Chlorophenylphenyl ether ug/L ND ND 4-Nitrophenol ug/L ND ND Acenaphthene ug/L ND ND Acenaphthylene ug/L ND ND Anthracene ug/L ND ND Benzo(a)anthracene ug/L ND ND Benzo(a)pyrene ug/L ND ND Benzo(b)fluoranthene ug/L ND ND Benzo(g,h,i)perylene ug/L ND ND Benzo(k)fluoranthene ug/L ND ND bis(2-Chloroethoxy)methane ug/L ND ND bis(2-Chloroethyl) ether ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Butylbenzylphthalate ug/L ND ND Chrysene ug/L ND ND Di-n-butylphthalate ug/L ND ND Di-n-octylphthalate ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Diethylphthalate ug/L ND ND Dimethylphthalate ug/L ND ND Fluoranthene ug/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 SAMPLE DUPLICATE: 2477940 Parameter Units 92414358008 Result Dup Result Fluorene ug/L ND ND Hexachloro-1,3-butadiene ug/L ND ND Hexachlorobenzene ug/L ND ND Hexachlorocyclopentadiene ug/L ND ND Hexachloroethane ug/L ND ND Indeno(1,2,3-cd)pyrene ug/L ND ND Isophorone ug/L ND ND N-Nitroso-di-n-propylamine ug/L ND ND N-Nitrosodimethylamine ug/L ND ND N-Nitrosodiphenylamine ug/L ND ND Naphthalene ug/L ND ND Nitrobenzene ug/L ND ND Pentachlorophenol ug/L ND ND Phenanthrene ug/L ND ND Phenol ug/L ND ND Pyrene ug/L ND ND 2,4,6-Tribromophenol (S) % 73 50 2-Fluorobiphenyl (S) % 87 74 2-Fluorophenol(S) % 41 32 Nitrobenzene-d5 (S) % 94 79 Phenol-d6 (S) % 30 25 Terphenyl-d14 (S) % 38 30 RPD Qualifiers 36 14 22 15 15 21 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: GROUNDWATER Pace Project No.: 92414635 QC Batch: 454240 Analysis Method: MADEP EPH QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water Associated Lab Samples: 92414635001 METHOD BLANK: 2480995 Matrix: Water Associated Lab Samples: 92414635001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aliphatic (C09-C18) ug/L ND 100 01/25/19 06:45 N2 Aliphatic (C19-C36) ug/L ND 100 01/25/19 06:45 N2 Aromatic (C11-C22) ug/L ND 100 01/25/19 06:45 N2 2-Bromonaphthalene (S) % 85 40-140 01/25/19 06:45 2-Fluorobiphenyl (S) % 87 40-140 01/25/19 06:45 Nonatriacontane (S) % 90 40-140 01/25/19 06:45 o-Terphenyl (S) % 86 40-140 01/25/19 06:45 LABORATORY CONTROL SAMPLE & LCSD: 2480996 2480997 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C09-C18) ug/L 300 188 232 63 77 40-140 21 50 N2 Aliphatic (C19-C36) ug/L 400 294 322 73 80 40-140 9 50 N2 Aromatic (C11-C22) ug/L 850 568 658 67 77 40-140 15 50 N2 2-Bromonaphthalene (S) % 64 84 40-140 2-Fluorobiphenyl (S) % 87 91 40-140 Nonatriacontane (S) % 77 84 40-140 o-Terphenyl(S) % 75 84 40-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: GROUNDWATER Pace Project No.: 92414635 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /25/2019 11:40 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 24 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: GROUNDWATER 92414635 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92414635001 MW-1 MADEP EPH 454240 MADEP EPH 454459 92414635001 MW-1 MADEP VPH 454352 92414635001 MW-1 EPA 625.1 453488 EPA 625.1 453681 92414635001 MW-1 SM 6200B 453769 Date: 01/25/2019 11:40 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 24 t.aborataryreceiving samples: Raleigh[] Mechanicsville❑ Asheville Q Eden[] Greenwood ❑ NantersviNe ❑ 4635 Sample Condition Client Name: Project IWO# • 9241 Upon Reteipt Cvurler_,.._., ❑USPSCllent Cl CbmCitmrnerdal ❑Pace QOther 92414635 Custody Seat Present? QYes allo. Seals intact? Dyes MNo paw/tnitlsis Person Examining Conteets: ) Biological Tissue Frozen? . Parking Material: QBuhble Wrap [j8ubf;[e Bags ❑iVone . ❑ Other []Yes ❑No ❑NfA Therrnometec 92T046 Type of Ice: Mwet ❑Blue ❑Nose ❑14 Gun ID: Cooleriemp ('Q: M Correction Factor: Add/Subtract CC) �= Tempshould be above freezingto 6'C 1 ❑Samples Out of temp criterlar, Samples on Ice cooling process CoolerTemp Corrected ('C): h ib*n USDA Regulated Soil {0. N/A, water sample) Did samples od4 hate In a quarantine zone within the United Stater CA, NY, or 5G (check maps)? old. samples Originate from a Foreign Source (int� atienaily, Yes No Sndud°n3 Hawaii and Puerto Rico)? Q Chain of Custody Present? ❑YeS ONO ❑NIA L Samples Arrived within hold Time? ❑Yes ❑No ❑NIA• Shormold Time Analysls (<72 hr.)? ❑Yes QNo ONJA R• RushTurnArouncl Time Requested? ❑Yes - ONO ❑NIA 4. SuffidentVolume? ❑Yes ❑No ❑NIA S. Correct Containers Used? ©Yes ONO ©NJA 6• -Pace containers Used? ❑Yes ❑No ❑NJA Containers Intact? ❑Yes ©No ❑NIA 7• Dissolved aml sis:Samples Field Filtered? ❑Yes ONO ONJA 8, Sample Lab elsMatch COC? No ❑NJA 9. -Includes Date/TlmeJJDfAnalysis Matrix:. Beads ace in VOA Vials(>5-6mm)? ❑Yes ON. ❑NJA 10. Trin Atank pt.- rPnO ❑YeS ❑No ❑NJA 11. COMMENISISAMPLE DISCREPANCY Lot 0ofSplit containers: CLIENT ND'rIFICATION/RESOWTION Person contacted: Date/Time: Fleid Data Requsted? ❑Yes QNo t Date: Project Manager SCURF Review: X Date: � Project Manager SRF Review: Page 19 of 24 ��aceAnaical Document No.: IssuingAuthanty: r F-CAR-CS-033-Rev.06 Pace Caralinas Quality Office *Check mark top half of box if pH and/or dechlorination is Project 1 WD# : 92414635 verified and within the acceptance range for preservation PM: PTE: Due hate: 01/25/19 samples, CLIENT: 92—ECS Exceptta iv VOA, Collform, TOC, Oil and Grease, 011018015 (water) DOC, LLHg "Bottom half of box is to list number of bottle w 2 v d a. 3 u v fJ J E a m z u. i7 a 7 U t � J' E Leal i m z yN 1' W d a v 16 J E a m 05 i, u d � yj S i a V V y -dr c o N v E 4 r4 _ V y .-d-. r" O z E N iL m � y el alp '+ v ,, ¢ 'u _ a.. £ 6 canm A.- i .a. T O tv E a z a t2 0 E v 7 $ m a e 7 �E d �' l7 ¢ N V'CL Y a U T iE1 d rr +.7 ¢ x tll a c Z ¢ lE N L7' a _ v 'i O C N S G q. 'i t7 a ra T v d ^ 2 Q ...� E [V m L7 ¢ z x '1 a E E N .� q m U a 4 2 T a ?, E Y ari t9 o a _ ..' m O z Q ? 6 q m C9 } Q Q 6 S a 7 E E Y as '� > _ 4 y m .QN. VI m y Y a x i0 L) -� a .� y C7ri > ^ Z, o. kn H 2 u -- 16 J g a ~ w7 m O N N N x J, E 4 per, m a a N a c E A E 7 l? a m ip } c J E a 3 in > z N i a Q E o N (7 A 1 ELM I Ld IN z 3 4 5 6 7 a 9 14 pH Adjustment Log. for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time�adjuslad n Amaunt of Preservative Lot k added Bate: Whenever there rs a discrepancy affecting North Carallna compliance Cut of hold, incorrect preservative, out of temp, incorrect contalners. a copy of this farm will be sent to the North Carolina DEHNR Certification Office (Le. Page 20 of 24 cerjrrrar CHAIN -OF -CUSTODY 1 Analytical Request Document - The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section S Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company: ECS Charlotte Report To: Joe Nestor Attention Address: 1812 Center Park Drive Copy To: 1 _ t A r, . j>-�/ Company Name: Charlotte, NC 28217 cSw� a�.,r-Z-r� �:,_,�, �M,-L'�1., �,- �-� Address: Regulatory Agency Email: jneslor ecslirn1ed.com Purchase OrderM Pace Quote, Phone- NONE JFax Project Name: Groundwater Pace Project Manager: taylacezell pacelahs, com. State 1 Location Requested Due Dale: Project #: Pace Profile M NC Requested An lysiS Filtered Y!N d Z MATRIX CODE ` V° COLLECTED Z Preservatives } ❑ranking Wow o U Uattl Wa Wr am � W Waste w'I" W W a Q Z Nmuct P SAMPLE ID S.WS.hd y o d od o� _ START AND r— One Character per box. W,P. wp 11 m (A-Z,0-911,-j air AR ethe, OT ❑ Q a w b uj o U U Samplc I.I. must lac unique Tlasue Ty X w Ja p v o R + w m U LL m 0. p ra — T t� rn N L ` L C Q U Z cJ O = l\L 1 Y DATE TIME DATE TIME # _ _ = z z O > ran wcc 2 3 4 5 fi 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE U o PRINT Name of SAMPLER; '-2 h ..tJ.-ti'l L� �✓ a w i rt d z o � � a z - z SIGNATURE of SAMPLER: DATE Signed: -Y Laboratory receiving samples: Ratelgh❑ Mechanicsville[]Asheville ❑ Eden[]Greenwood ❑ Fiuntersville 0635 Client Name: IWO# : 9241 Project � 1 �1� �l l lttil I II1 .aFg_d_Cx._ uUPS ❑U5P5 ❑ C rritnerdal ❑Pace Qother: - 92414635 Custody Seal Present? Des NO Seals Intact? []Yes QNo �J �s-.1�--r pats/lnitleis Person Examining Cantents: Blologlcal Tissue Frozen?, Packingi.Natedal: ❑Bubble Wrap ❑Bub le Bags []None ❑ Other ❑Yes []No []N/A Thermometer; 9 Tp4& Type of Ice. Mwet ❑slue ❑Nare e]IR Gun ID: Cooler Temp (IQ: ii , ` Correction factor: Add/Subtract ( 0 �_ Tempihould.be abovefreezingto VC QSarnples out of temp uiterM Samples an ice.cnoling process CoolerTernp Corrected ('Cl: ftas6egun , USDA Regulated Soil ([i N/A, water sample] Did samples originate in a quarantine one within the United States: CA, NY, or Sr- (check rnaps)? Old samples originate from foreign;ource(Int�lonallY, Inds nHavaaii and PueRo Rlco)? Dies [ J of Custody Present? d Short Hold Time Analysis (<72 hr RushTurn Around Time Request Stiff tdentVolume7 CorrectContainers Used? -Pace Containers Used? Containers Intact? Dissolved analysis: samples Field Sample Labels Match COC? ies D atell ce in VOA Trip 8lankCustady Seals Present COMMENTSISAMPLE DISCREPANCY ]Yes ]No QNIA 1 ?Yes DNo ❑NJA �. Yes QN , DNJA 3: Yes ENO E]N1A 4. DYes ❑N4 ❑NJA 5• []Yes ©No ©N/A & T:,__ r7m . r-1es1A 1 7 ©Yes []No []N/A 9, s hAatrlx;. ? []Yes []No ❑NJA 10. ©Yes []No❑NJA 11. Lot 0 of split contalners: CLIENT NO71FICATiONIRESCILLITION Person contacted: pate/Time: Field Data Required? ❑Yes QNo Date: Project Manager SCURF Review: }/ Date: 'L — Project Manager SRF Revlew: Page 22 of 24 l aeeAnafytical Dg:ument No.,. Issuing Authority: r F•CAR-CS•O33,Rev.06 Pace Carollnas Quality 0ffice *Check mark top half of box if pH and/or dechlorination is Project 1 40# 92414635 verified and within the acceptance range for preservation PM: PTE: Due Date: O1/25/19 samples, CLIENT: 92—ECS Excepticns: VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, ltHg **Bottom half of box is to Iist number of bottle Z 6i Z o. e <} a J E O i es Z 77, Z Q. c U i -$ E m 2 6i a e U A a J E 7 a m Q � d a 7 G Y rr 9 i or tr V x O V ma E Lh a m 2V z U n �l E Z a m .Uyyi S A a E `�`� N d W = O m U m a .J E U. a m o £ }r LL e ? :: .7 l�7 d N V' a u x s L7 d a! Q� c 41 -c E L." l7 ¢ Sv O y x E Q. ; l� d V A. 7 = W E Q J E rev M [3 Q 7 2 ¢ o tK d o m l7 ¢ 2 2 < O > J E Y 0y5 a z p Z d O j E q a�i 7 z $ a a i i o o ? > J J E E 7 a Pal A >- a 2 N vpi, :- Y 6. > Y ¢ 7- .$ \ j ar > Y t7 } ¢ U e. E H d. ¢ d E rq i= N w a N ?. u N a E G a m Z G 5 a .r7Q E o ¢ ' 10 E t�7 H 7 a W rrs L m l7 'N I - I NN�l 3 b 5 6 7 a 4 10 11 PH Adjustment Log. for Preserved Samples Sample ID Type of Pfeservative pH upon receipt Date preservation adjusted Time preservation Arn=t of Preservative Lot q adlusled I added Note: Whenevar there is a discrepancy affecting North Carolina compliance Out of hold, Incorrect preservative, out of temp, incorrect containers. a copy of this farm will he sent to the North Carolina DEHNR CertIFIGUon Office (Le. Page 23 of 24 ' JcenruV, r CHAIN -OF -CUSTODY 1 Analytical Requi Document .... „ The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section a Section C Required Client Information: Required Project Information: Invoice Information: Page : 1 Of 1 Company: ECS Charlotte Report TO ,Joe Nestor Attention--�C•�;1�_ Address: 1512 Center Park Drive Copy Ta: - ,_ x, � �;. � / Company Name: Charlotte, NC 28217 Address: Regulatory Agency Email; jrieslor ecslimited.Com Purchase Order #: Pace Quote. Phone: NONE IFax Project Names Groundwater Pace Project Manager, taylor.ezeB@pacelabs.com. State 1 Location Requested Due Date: Project#: Pace Profile #: NC Re (tested An is Filtered YIN v Z MATRIX LOP£ o CQLtECiED S Preservatives > Pllnking water Pw VWIV, wT 3 r} U ~ w waste water ww N.durt P SAMPLE ID 8°,V5°°d SL m } Oil oi_ START EN❑ F F m .Q One Character per box. W.V. Wa w a = A # (A-Z, 0.91. •) A;r AIR Other OT 00 a w ¢ t; m m M H }+ L) 9 Sample Ids must be unique Tls•.ua Ts 0 x O w ` in �O o n +' O o �r / 1J t v 1/ L( of l b tL = M 2 1 r N DATE TIME DATE TIME N >< __= z z 2 o w ca 2 3 4 5 s 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATION DATE 11ME ACCEPTED 9Y I AFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE U c '10 PRINT Name of SAMPLER: w m m} v o y 1O y c SIGNATURE of SAMPLER: DATE igned: I l 1— K U rn Data File:\\v92wintarget\chem\92mss6.i\012219.b\01221913.D Report Date: 29-Jan-2019 08:48 TENTATIVELY IDENTIFIED COMPOUNDS Client Name: Lab Smp Id: 92414388001 Operator : BPJ Sample Location: Sample Matrix: SOIL Analysis Type: SV Inj Date: 22-JAN-2019 16:35 Number TICS found: 10 Client SDG: 92MSS6-012219 Sample Date: Sample Point: Date Received: Level: LOW CONCENTRATION UNITS: (ug/L or ug/KG) ug/Kg CAS NUMBER I I I COMPOUND NAME 1. 629-50-5 ITridecane 2. 629-59-4 ITetradecane 3. 573-98-8 (Naphthalene, 1,2-dimethyl- 1 4. 629-62-9 IPentadecane 5. 544-76-3 IHexadecane 6. (Unknown 7. 629-78-7 IHeptadecane 8. 1730-37-6 19H-Fluorene, 1-methyl- 1 9. 629-92-5 INonadecane 10. 112-95-8 IEicosane 1 I I_ Page 1 I RT I I EST. CONC. I I Q I 8.5081 434001 NJ-1 9.0801 115001 NJ-1 9.4591 61101 NJ_ 1 9.6141 77901 NJ-1 10.1181 172001 NJ-1 10.4531 159001 _J_ 1 10.5931 440001 NJ-1 10.8201 290001 NJ_ 1 11.4701 265001 NJ-1 11.8801 I 240001 I NJ-1 1 Data File: \\v92wintarget\ohem\92mss6.i\012219.b\01221913.D Page 2 Date : 22-JAN-2019 16:35 Client ID; Instrument; 92mss6.i Sample Info; 92414388001X10, 16776 Volume Injeoted {uL}; 1.0 Operator; BPJ Column phase; RXi-5Sil NS Column diameter; 0.18 \\v92wintarget\ohem\92mss6.i\012219.b\01221913.D 0.9- o m 0 . I I c I 0.7- 0.6 n < { -U .. v y� I m m 0.4- I � m �C M o0 4 O F] i I N {} 0.3- � ° --I I -c {} I c N G a� i 4 0.2- c� m I 37 i ' I $ 0. .�1. . . .�2. .�3. . . .�4. .�5. . . .�6. . . .�7. Nin APPENDIX E NCDEQ WELL CONSTRUCTION PERMIT WELL CONSTRUCTION RECORD 1 Environmental Quality April 19, 2018 Adam Duerr (via email) Exeter Property Group 6285 Barfield Road Suite 225 Atlanta, GA 30328 ROY COOPER Governor MICHAEL S. REGAN Secretary LINDA CULPEPPER Interim Director RE: Monitoring Well Construction Permit Permit #WM0300961 4101 Meadow Oak Drive, Charlotte Mecklenburg County Dear Mr. Duerr, In accordance with your completed application received on April 19, 2018, we are forwarding herewith Monitoring Well Construction Permit Numbered WM0300961 and issued for the construction of three temporary direct push monitoring well points located near the subject site in Charlotte, Mecklenburg County. This Permit will be effective for one year from the date of issuance and shall be subject to the conditions and limitations as specified therein. Should you have any questions, please contact Edward Watson at (704) 663-1699 ext. 2198, or by email at edward.watson@ncdenr.gov. Sincerely, DocuSigned by: A*,� H P F161 FB69AWMA3... Andrew H. Pitner, P.G., Assistant Regional Supervisor Mooresville Regional Office Water Quality Regional Operations Section Division of Water Resources, NCDEQ CC: WQROS, Central Office (via Laserfiche) Chris Orrell, GIT, ECS Southeast, LLP (via email) State of North Carolina I Environmental Quality I Water Resources I Water Quality Regional Operations Mooresville Regional Office 1 610 East Center Avenue, Suite 3011 Mooresville, North Carolina 28115 704 663 1699 NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws, Rules and Regulations. PERMISSION IS HEREBY GRANTED TO Exeter Property Group (ECS Southeast, LLP, as Agent) FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of three direct push temporary well point owned by Exeter Property Group and located at 4101 Meadow Oak Drive, Charlotte, Mecklenburg County. This Permit is issued in accordance with the application received on April 19, 2018, in conformity with specifications and supporting data, all of which are filed with the Department of Environmental Quality and are considered integral parts of this Permit. This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well construction. If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding. This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions, limitations, or exceptions as follows: 1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as part of an investigation for contamination from an underground storage tank or dry cleaner incident. 2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency. 3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application. 4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o). 5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources' Information Processing Unit within 30 days of the well completion. 6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a well abandonment record (GW-30) shall be submitted to the Division of Water Resources' Information Processing Unit within 30 days of the well abandonment. 7. Adequate permits must be obtained from Mecklenburg County Groundwater and Wastewater Services. Permit issued the 19t1i day of April, 2018 FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DocuSigned by: F161 FB69A2D84A3... Andrew H. Pitner, P.G., Assistant Regional Supervisor Division of Water Resources By Authority of the Environmental Management Commission Permit No. # WM0300961 WELL CONSTRUCTION RECORD This form can be used for single or multiple wells For Internal Use ONLY: 1. Well Contractor Information: JOHNNY BURR Well Contractor Name A - 3098 NC Well Contractor Certification Number GEOLOGIC EXPLORATION, INC Company Name 2. Well Construction Permit #: List all applicable well construction permits (i.e. County, State, Variance, etc) 3. Well Use (check well use): Water Supply Well: ❑Agricultural ❑Geothermal (Heating/Cooling Supply) ❑ hmdustrial/Commercial ❑ Irrigation Non -Water Supply Well: El Aquifer Recharge El Aquifer Storage and Recovery ❑Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling ❑Municipal/Public El Residential Water Supply (single) ❑Residential Water Supply (shared) El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑Subsidence Control ❑Tracer ❑Other (explain under #21 F 4. Date Well(s) Completed: 01/15/19 Well ID# MW-1 5a. Well Location: MEADOW OAKS Facility/Owner Name Facility ID# (if applicable) 4101 MEADOW OAK DRIVE CHARLOTTE 28208 Physical Address, City, and Zip MECKLENBURG County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 350 11' 35.11" N 800 55' 16.39" W 6. Is (are) the well(s): ❑] Permanent or ❑Temporary 7. Is this a repair to an existing well: ❑Yes or ONo If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: 1 For multiple injection or non -water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: 40.0 (ft.) For multiple wells list all depths if different (example- 3@200' and 2@100') 10. Static water level below top of casing: 25.0 (ft.) If water level is above casing, use "+" 11. Borehole diameter: 8.0 (in.) 12. Well construction method: AUGER (i.e. auger, rotary, cable, direct push, etc.) 14. WATER ZONES FROM TO DESCRIPTION rt. rt. ft. ft. 15. OUTER CASING for multi -cased wells OR LINER if a licable FROM TO DIAMETER THICKNESS MATERIAL ft. ft. in. 16. INNER CASING OR TUBING eother at closed -loop) FROM TO DIAMETER THICKNESS MATERIAL 0.0 ff 25.0 ft. 2.0 "' SCH 40 PVC rt rt in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL 25.0 ft' 40.0 ft- 2.0 in. .010 SCH 40 PVC ft. ft, in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT 0.0 It' 18 0 ft' PORTLANDBENTONITE SLURRY ft. ft. rt. rt. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD 22.0 ft• 40.0 ft. 20-40 FINE SILICA SAND rt. rt. 20. DRILLING LOG attach additional sheets if necessary) FROM TO DESCRIPTION color, hardness, soil/rock type, grain size, etc.) 0.0 ft• 12.0 ft TAN/BROWN ROCKY CLAY 12.0 ft. 34.0 ft• RED/ORANGE CLAY 34.0 ft• 40.0 ft• RED SILTY CLAY rt. ft. rt. et. ft. fit. rt. er. 21. REMARKS BENTONITE SEAL FROM 18.0 TO 22.0 FEET 22. Certification: Signature of Certified Well Contractor 01/17/19 Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Quality, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Iniection Wells: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Quality, Underground Injection Control Program, FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636 13a. Yield (gpm) Method of test: 24c. For Water Supply & Iniection Wells: In addition to sending the form to the address(es) above, also submit one copy of this form within 30 days of 13b. Disinfection type: Amount: completion of well construction to the county health department of the county where constructed. Form GW-1 North Carolina Department of Environment and Natural Resources - Division of Water Quality Revised Jan. 2013 Beverly, Trudy From: Joseph Patrick Nestor <JNestor@ecslimited.com> Sent: Tuesday, February 5, 2019 4:18 PM To: Beverly, Trudy Cc: Adam Duerr; Matthew H. McDuffie, P.G.; Brandon Fulton, LSS, PSC, PWS Subject: [External] NCDEQ Incident No. 40849 - ECS Project No. 49-6535-L (Meadow Oaks Industrial) - 4101 Meadow Oak Drive - Charlotte Attachments:[9faf678e-9b31-4570-a0d5-55bff32e7ee2]00-0-0000030621_40849_CA_LSA_20190205 _Phase I LSA Meadow Oaks.pdf • External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to nc. ov Trudy: Attached to this email is the Phase I Limited Site Assessment Report (Phase I LSA Report) for the referenced site. Also included with the report is a request for No Further Action and a Notice of Residual Petroleum (NORP) which has been executed by the property owner. The NORP includes restrictions for the use of groundwater and residential land use. The hard copy and a CD with the report is being forwarded to you by Federal Express for delivery tomorrow. We will follow up with you tomorrow to discuss this matter and answer questions you may have. Thank you for your attention to this important matter. JOSEPH PATRICK NESTOR I Environmental Senior Project Manager T 704.525.5152 1 C 704.280.7422 1812 Center Park Drive, Suite D I Charlotte I NC 1 28217 ECS SOUTHEAST, LLP www.ecslimited.com Linkedln I Facebook I Twitter Confidential/proprietary message/attachments. Delete message/attachments if not intended recipient. ------------------------------------------------------- This message has been analyzed by Deep Discovery Email Inspector. 1