17047 Soil Assessment Letter 20180726

Via Email

July 26, 2018

NC DEQ – Brownfields Section
1646 Mail Service Center
Raleigh, NC 27699-1646

Attn: Mr. Bill Schmithorst, PG

Subject: Soil Arsenic and Thallium - Proposed Warehouse Building
REEP-LRC Project 1
1900 Continental Boulevard
Charlotte, North Carolina
Brownfields Project No. 17047-13-60
H&H Job No. LRC-006

Dear Bill:

On behalf of the property owner, H&H is providing this response to DEQ’s inclusion of arsenic
and thallium as soil impacts in Exhibit 2 of the draft Brownfields Agreement. This response
includes a revised laboratory analytical report and soil data summary table for Brownfields
Assessment activities conducted in October 2016 at the REEP-LRC Project 1 site located at 1900
Continental Boulevard in Charlotte, North Carolina. The laboratory analytical report was revised
to include estimated concentrations detected between the method detection limit (MDL) and
laboratory reporting limit (RL) for metals analysis by EPA Method 6010. The purpose of the
revision is to determine if metals are present at the site at concentrations that pose a threat to human
health based on the North Carolina Department of Environmental Quality (DEQ) Risk Calculators
dated February 2018.

A summary of the revised soil concentrations from the October 2016 Brownfields Assessment
activities and soil concentrations detected during waste removal activities conducted in February
2018 is included in Table 1. The revised laboratory report along with chain of custody is included
in Appendix A. To evaluate if the metal concentrations detected in soil pose a risk to human health,
H&H utilized the highest metal concentrations detected in the soil samples collected at the site
Table 1 Summary of Soil Analytical Data
REEP-LRC Project 1
1900 Continental Boulevard
Charlotte, North CarolinaH&H Job No. LRC-006
Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7 SB-8 SB-9 SB-10 Base-2 Base-3 Ash-1 Depth (ft bgs)0-2 4-6 8-10 0-2 0-2 0-2 4-6 0-2 0-2 2-4 6 6 3 Sample Date 10/14/2016 10/14/2016 10/14/2016 10/13/2016 10/13/2016 10/13/2016 10/14/2016 10/14/2016 10/14/2016 10/14/2016 2/21/2018 2/21/2018 2/21/2018 Units
HSL Metals (6010D)
Range (mg/kg)Mean (mg/kg)RefAntimony<1.27 <6.08 <1.14 <1.18 2.34 J <1.23 <1.40 <1.30 1.67 J <1.20 0.63 B 0.67 B, J 0.53 B, J 93 <1.0-8.8 0.76 CArsenic4.13 7.42 J 3.78 2.94 4.88 5.22 3.94 5.00 4.95 4.98 1.8 J 1.5 J 13 3.0 1.0-18 4.8 ABeryllium0.608 J <1.22 1.40 1.07 J 1.18 J 1.25 1.59 1.09 J 1.51 0.815 J 1.7 2.8 0.35 470 BRL-2.0 0.11 ACadmium1.34 4.86 J 0.709 J 0.616 J 1.36 J 1.15 J 1.15 J 1.22 J 1.59 0.886 J 0.11 J 0.052 J 5.0 200 1.0-10 4.3 BChromium, Total 14.8 <5.47 6.64 7.84 18.6 16.3 3.33 41.9 17.8 10.7 3.4 B 76 B 35 B 6.5 7.0-300 65 ACopper5.78 <6.69 23.7 7.13 7.8 14.1 12.1 19.8 25.9 17.4 41 B 59 B 18 B 9,300 3.0-100 34 ALead50.8 4.13 J 28.2 23.9 74.8 44.1 39.8 43.9 156 34.2 16 22 31 800 BRL-50 16 AManganese1224483954104308814143652663093209001605,600 8.0-3,394 594 BMercury< 0.122 < 0.119 < 0.114 < 0.115 < 0.158 < 0.120 < 0.145 < 0.126 < 0.132 < 0.123 <0.025 <0.028 0.0079 J 9.7 0.03-0.52 0.121 ANickel9.47 <3.65 6.93 8.31 8.04 10.8 3.58 14.2 8.58 12.4 15 B 69 B 29 B 4,700 BRL-150 23 ASelenium<1.39 <6.69 <1.26 <1.30 <1.67 <1.35 <1.54 <1.43 <1.48 <1.32 5.3 4.3 0.79 J 1,200 <0.1-0.8 0.42 ASilver<0.507 <2.43 <0.458 <0.473 <0.607 <0.490 <0.559 <0.519 <.538 <0.479 0.049 J 0.050 J 0.095 J 1,200 BRL-5.0 NE DThallium<3.80 <3.65 <3.43 <3.55 <4.55 <3.68 <4.19 <3.89 <4.04 <3.59 0.046 J 0.16 J 0.071 J 2.3 <0.1-1.8 NE EZinc21.6 84.0 56.7 61.8 47.6 46.6 114 44.8 938 54.9 350 140 35,000 70,000 25-124 56 A
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (February 2018).
2) Range and Mean background values for North Carolina or Southeast soils taken from Elements in North American Soils by Dragun and Chekiri, 2005
Ref.A. North Carolina soils
B. Southeastern USA soils
C. Eastern USA soils
D. Soils of the conterminous USA
E. Major- and Trace-Element Concentrations in Soils from Two Continential-Scale Transects of the United States and Canada, U.S. Department of Interior, U.S. Geologic Survey. Open-File Report 2005-1253, Table 3. 2005.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Laboratory analytical methods are shown in parentheses.HSL = Hazardous Substance ListNE = not established; BRL = below reporting limit; ft bgs = feet below the ground surface B=analyte found in associated blank at grater than 1/2 reporting limitJ=estimated concentration detected below reporting limit but above method detection limit
mg/kg
Industrial/ Commercial
PSRGs(1)
Regional Background Metals in Soil2
S:\AAA-Master Projects\LRC Patriot (LRC)\LRC-006 New Building Waste Assessment\Brownfields\Soil Risk Calcs\Soil Data Table_Metals to MDL7/10/2018
Table 1 (Page 1 of 1)Hart & Hickman, PC
Hart & Hickman, PC
Appendix A
Revised Laboratory Report

ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: [phone]
TestAmerica Job ID: 490-114207-1
TestAmerica Sample Delivery Group: LRC-004
Client Project/Site: Continental Tire
Revision: 1
For:
Hart & Hickman, PC
2923 S Tryon Street
Suite 100
Charlotte, North Carolina 28203
Attn: Ralph McGee
Authorized for release by:
6/26/2018 5:05:22 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Hart & Hickman, PC
Project/Site: Continental Tire
TestAmerica Job ID: 490-114207-1
SDG: LRC-004
Page 2 of 108 TestAmerica Nashville6/26/2018 (Rev. 1)
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .89
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .95
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .100
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .101
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .102
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .107
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Sample Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID Client Sample ID ReceivedCollectedMatrix
490-114207-1 SB-4 (0-2)Soil 10/13/16 13:20 10/18/16 08:50
490-114207-2 SB-5 (0-2)Soil 10/13/16 14:10 10/18/16 08:50
490-114207-3 SB-6 (0-2)Soil 10/13/16 15:30 10/18/16 08:50
490-114207-4 SB-9 (0-2)Soil 10/14/16 15:30 10/18/16 08:50
490-114207-5 SB-8 (0-2)Soil 10/14/16 15:40 10/18/16 08:50
490-114207-6 SB-7 (4-6)Soil 10/14/16 15:50 10/18/16 08:50
490-114207-7 SB-1 (0-2)Soil 10/14/16 18:00 10/18/16 08:50
490-114207-8 SB-2 (4-6)Soil 10/14/16 18:27 10/18/16 08:50
490-114207-9 SB-3 (8-10)Soil 10/14/16 18:40 10/18/16 08:50
490-114207-10 SB-10 (2-4)Soil 10/14/16 19:15 10/18/16 08:50
490-114207-11 TMW-2 Water 10/17/16 14:20 10/18/16 08:50
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Job ID: 490-114207-1
Laboratory: TestAmerica Nashville
Narrative
Job Narrative
490-114207-1
REVISED REPORT: Revised to report the 6010D metals to the MDL at the client's request. This report replaces the one generated on
11/03/16 @ 1001.
Comments
No additional comments.
Receipt
The samples were received on 10/18/2016 8:50 AM; the samples arrived in good condition, properly preserved and, where required, on
ice. The temperatures of the 2 coolers at receipt time were 2.6º C and 3.3º C.
GC/MS VOA
Method 8260B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
analytical batch 490-380000.
Method 8260B: The laboratory control sample and/or the laboratory control sample duplicate (LCS/LCSD) for analytical batch 490-380848
recovered outside control limits for the following analyte(s): Chloroethane. Chloroethane has been identified as a poor performing analyte
when analyzed using this method; therefore, re-extraction/re-analysis was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270D: The continuing calibration verification (CCV) for analytical batch 490-381549 was outside the method criteria for
Bis[2-chloroisopropyl]ether. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be
acceptable; therefore, the data is reported. (CCVIS 490-381549/3)
Method 8270D: The following samples was diluted due to the nature of the sample matrix: SB-4 (0-2) (490-114207-1) and SB-9 (0-2)
(490-114207-4). Elevated reporting limits (RLs) are provided.
Method 8270D: Surrogate recovery for the following sample was outside control limits: SB-7 (4-6) (490-114207-6). Evidence of matrix
interference is present; therefore, re-extraction was not performed.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 6010D: The following samples was diluted to bring the concentration of target analytes within the calibration range: SB-4 (0-2)
(490-114207-1), SB-5 (0-2) (490-114207-2), SB-6 (0-2) (490-114207-3), SB-9 (0-2) (490-114207-4), SB-8 (0-2) (490-114207-5), SB-7 (4-6)
(490-114207-6), SB-1 (0-2) (490-114207-7), SB-2 (4-6) (490-114207-8), SB-3 (8-10) (490-114207-9) and SB-10 (2-4) (490-114207-10) at
5.0, 5.0, 5.0, 5.0, 5.0, 5.0, 5.0, 5.0, 5.0 and 5.0. Elevated reporting limits (RLs) are provided. Dilution prepared by mixing 2 mL of sample
with 8 mL of blank.
Method 6010D: The following sample was diluted to bring the concentration of target analytes within the calibration range: SB-2 (4-6)
(490-114207-8) at 5.0. Elevated reporting limits (RLs) are provided. Dilution prepared by mixing 2 mL of sample with 8 mL of blank.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
LCMS
Method 8330A: Surrogate 1,2-dinitrobenzene recovery for the following sample TMW-2 (490-114207-11) was outside the upper control
limit on the second column.129% (limit 75-118%). The surrogate was in control on the other column, indicating the sample extraction was
in control. This sample did not contain any target analytes; therefore, re-extraction and/or re-analysis was not performed. The surrogate
was reported from the in control column. Prep Batch # 347627, Analytical Batch # 348204/348206.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
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Case Narrative
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Job ID: 490-114207-1 (Continued)
Laboratory: TestAmerica Nashville (Continued)
Organic Prep
Method 3535: The following sample: TMW-2 (490-114207-11) was decanted prior to preparation due to wrong sample bottle size sent
from client. 3535/8330A
Method Prep/Air Dry: The following samples were air dried and sieved per the procedure; however, the samples contained material that
would not pass through the sieve: SB-4 (0-2) (490-114207-1), SB-5 (0-2) (490-114207-2), SB-6 (0-2) (490-114207-3), SB-9 (0-2)
(490-114207-4), SB-8 (0-2) (490-114207-5), SB-7 (4-6) (490-114207-6), SB-1 (0-2) (490-114207-7), SB-2 (4-6) (490-114207-8), SB-3
(8-10) (490-114207-9) and SB-10 (2-4) (490-114207-10). This material was removed and not extracted. The material appeared to be
rocks. Batch: preparation batch 280-348351, 280-348351 and 280-348351 Method: 8330A (Dry_Sample)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
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Definitions/Glossary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Qualifiers
GC/MS VOA
Qualifier Description
*LCS or LCSD is outside acceptance limits.
Qualifier
GC/MS Semi VOA
Qualifier Description
X Surrogate is outside control limits
Qualifier
HPLC/IC
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
X Surrogate is outside control limits
F2 MS/MSD RPD exceeds control limits
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Metals
Qualifier Description
F1 MS and/or MSD Recovery is outside acceptance limits.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-1Client Sample ID: SB-4 (0-2)
Matrix: SoilDate Collected: 10/13/16 13:20
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0772 0.0558 mg/Kg ☼10/13/16 12:20 10/21/16 01:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Benzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Bromobenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Bromochloromethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Bromodichloromethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Bromoform ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Bromomethane ND
0.0558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼2-Butanone (MEK)ND
0.00558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Carbon disulfide ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Carbon tetrachloride ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Chlorobenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Chlorodibromomethane ND
0.00558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Chloroethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Chloroform ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Chloromethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼2-Chlorotoluene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼4-Chlorotoluene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼cis-1,2-Dichloroethene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼cis-1,3-Dichloropropene ND
0.00558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2-Dibromo-3-Chloropropane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2-Dibromoethane (EDB)ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Dibromomethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2-Dichlorobenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,3-Dichlorobenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,4-Dichlorobenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Dichlorodifluoromethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,1-Dichloroethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2-Dichloroethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,1-Dichloroethene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2-Dichloroethene, Total ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2-Dichloropropane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,3-Dichloropropane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼2,2-Dichloropropane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,1-Dichloropropene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Diisopropyl ether ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Ethylbenzene ND
0.00558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Hexachlorobutadiene ND
0.0558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼2-Hexanone ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Isopropylbenzene ND
0.0112 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Methylene Chloride ND
0.0558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼4-Methyl-2-pentanone (MIBK)ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Methyl tert-butyl ether ND
0.00558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Naphthalene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼n-Butylbenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼N-Propylbenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼p-Isopropyltoluene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼sec-Butylbenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Styrene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-1Client Sample ID: SB-4 (0-2)
Matrix: SoilDate Collected: 10/13/16 13:20
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00223 mg/Kg ☼10/13/16 12:20 10/21/16 01:43 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,1,2,2-Tetrachloroethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Tetrachloroethene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Toluene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼trans-1,2-Dichloroethene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼trans-1,3-Dichloropropene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2,3-Trichlorobenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2,4-Trichlorobenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,1,1-Trichloroethane ND
0.00558 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,1,2-Trichloroethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Trichloroethene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Trichlorofluoromethane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2,3-Trichloropropane ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,2,4-Trimethylbenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼1,3,5-Trimethylbenzene ND
0.00223 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Vinyl chloride ND
0.00670 mg/Kg 10/13/16 12:20 10/21/16 01:43 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)98 70-130 10/13/16 12:20 10/21/16 01:43 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 10/13/16 12:20 10/21/16 01:43 170-130
1,2-Dichloroethane-d4 (Surr)106 10/13/16 12:20 10/21/16 01:43 170-130
Toluene-d8 (Surr)98 10/13/16 12:20 10/21/16 01:43 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.390 mg/Kg ☼10/20/16 10:37 10/27/16 02:46 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Acenaphthylene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Anthracene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Benzo[a]anthracene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Benzo[a]pyrene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Benzo[b]fluoranthene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Benzo[g,h,i]perylene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Benzo[k]fluoranthene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Bis(2-chloroethoxy)methane ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Bis(2-chloroethyl)ether ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼bis (2-chloroisopropyl) ether ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Bis(2-ethylhexyl) phthalate ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼4-Bromophenyl phenyl ether ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Butyl benzyl phthalate ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Carbazole ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼4-Chloroaniline ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼4-Chloro-3-methylphenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2-Chloronaphthalene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2-Chlorophenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼4-Chlorophenyl phenyl ether ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Chrysene ND
3.88 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Cresols ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Dibenz(a,h)anthracene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-1Client Sample ID: SB-4 (0-2)
Matrix: SoilDate Collected: 10/13/16 13:20
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 1.94 mg/Kg ☼10/20/16 10:37 10/27/16 02:46 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼1,3-Dichlorobenzene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼1,4-Dichlorobenzene ND
3.90 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼3,3'-Dichlorobenzidine ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2,4-Dichlorophenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Diethyl phthalate ND
3.90 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2,4-Dimethylphenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Dimethyl phthalate ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Di-n-butyl phthalate ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼4,6-Dinitro-2-methylphenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2,4-Dinitrophenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2,4-Dinitrotoluene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2,6-Dinitrotoluene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Di-n-octyl phthalate ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Fluoranthene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Fluorene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Hexachlorobenzene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Hexachlorobutadiene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Hexachlorocyclopentadiene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Hexachloroethane ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Indeno[1,2,3-cd]pyrene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Isophorone ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼1-Methylnaphthalene ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2-Methylnaphthalene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2-Methylphenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼3 & 4 Methylphenol ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Naphthalene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2-Nitroaniline ND
3.90 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼3-Nitroaniline ND
3.90 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼4-Nitroaniline ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Nitrobenzene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2-Nitrophenol ND
3.90 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼4-Nitrophenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼N-Nitrosodi-n-propylamine ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
3.90 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Pentachlorophenol ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Phenanthrene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Phenol ND
0.390 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼Pyrene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼1,2,4-Trichlorobenzene ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2,4,5-Trichlorophenol ND
1.94 mg/Kg 10/20/16 10:37 10/27/16 02:46 5☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)64 29-120 10/20/16 10:37 10/27/16 02:46 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)48 10/20/16 10:37 10/27/16 02:46 510-120
Nitrobenzene-d5 (Surr)55 10/20/16 10:37 10/27/16 02:46 527-120
Phenol-d5 (Surr)57 10/20/16 10:37 10/27/16 02:46 510-120
Terphenyl-d14 (Surr)82 10/20/16 10:37 10/27/16 02:46 513-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-1Client Sample ID: SB-4 (0-2)
Matrix: SoilDate Collected: 10/13/16 13:20
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)84 10-120 10/20/16 10:37 10/27/16 02:46 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.84 mg/Kg 10/27/16 14:58 11/01/16 14:35 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.84 mg/Kg 10/27/16 14:58 11/01/16 14:35 12,6-diamino-4-nitrotoluene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 12-Amino-4,6-dinitrotoluene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 14-Amino-2,6-dinitrotoluene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 12,4-Dinitrotoluene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 12,6-Dinitrotoluene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 12,4,6-Trinitrotoluene ND
0.461 mg/Kg 10/27/16 14:58 11/01/16 14:35 1m-Nitrotoluene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 1o-Nitrotoluene ND
0.369 mg/Kg 10/27/16 14:58 11/01/16 14:35 1p-Nitrotoluene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 1NitrobenzeneND
4.70 mg/Kg 10/27/16 14:58 11/01/16 14:35 1NitroglycerinND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 11,3,5-Trinitrobenzene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 11,3-Dinitrobenzene ND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 1HMXND
0.240 mg/Kg 10/27/16 14:58 11/01/16 14:35 1RDXND
0.461 mg/Kg 10/27/16 14:58 11/01/16 14:35 1TetrylND
3.69 mg/Kg 10/27/16 14:58 11/01/16 14:35 1PETNND
0.230 mg/Kg 10/27/16 14:58 11/01/16 14:35 1Picric acid ND
1,2-Dinitrobenzene 109 83-122 10/27/16 14:58 11/01/16 14:35 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.18 11.8 1.18 mg/Kg ☼10/20/16 10:21 10/21/16 02:27 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.37 1.42 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Arsenic 2.94
1.18 0.237 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Beryllium 1.07 J
1.18 0.118 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Cadmium 0.616 J
1.18 1.07 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Chromium 7.84
2.37 1.30 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Copper 7.13
1.18 0.592 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Lead 23.9
3.55 1.18 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Manganese 410
2.37 0.710 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Nickel 8.31
2.37 1.30 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Selenium <1.30
1.18 0.473 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Silver <0.473
11.8 3.55 mg/Kg 10/20/16 10:21 10/24/16 15:30 5☼Thallium <3.55
11.8 5.92 mg/Kg 10/20/16 10:21 10/21/16 02:27 1☼Zinc 61.8
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.115 mg/Kg ☼10/20/16 11:45 10/21/16 07:26 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 84.5 0.1 %10/18/16 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-2Client Sample ID: SB-5 (0-2)
Matrix: SoilDate Collected: 10/13/16 14:10
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.285 0.0653 mg/Kg ☼10/13/16 13:10 10/21/16 02:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Benzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Bromobenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Bromochloromethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Bromodichloromethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Bromoform ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Bromomethane ND
0.0653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼2-Butanone (MEK)ND
0.00653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Carbon disulfide ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Carbon tetrachloride ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Chlorobenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Chlorodibromomethane ND
0.00653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Chloroethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Chloroform ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Chloromethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼2-Chlorotoluene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼4-Chlorotoluene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼cis-1,2-Dichloroethene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼cis-1,3-Dichloropropene ND
0.00653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2-Dibromo-3-Chloropropane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2-Dibromoethane (EDB)ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Dibromomethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2-Dichlorobenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,3-Dichlorobenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,4-Dichlorobenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Dichlorodifluoromethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,1-Dichloroethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2-Dichloroethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,1-Dichloroethene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2-Dichloroethene, Total ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2-Dichloropropane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,3-Dichloropropane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼2,2-Dichloropropane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,1-Dichloropropene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Diisopropyl ether ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Ethylbenzene ND
0.00653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Hexachlorobutadiene ND
0.0653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼2-Hexanone ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Isopropylbenzene ND
0.0131 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Methylene Chloride ND
0.0653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼4-Methyl-2-pentanone (MIBK)ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Methyl tert-butyl ether ND
0.00653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Naphthalene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼n-Butylbenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼N-Propylbenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼p-Isopropyltoluene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼sec-Butylbenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Styrene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-2Client Sample ID: SB-5 (0-2)
Matrix: SoilDate Collected: 10/13/16 14:10
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00261 mg/Kg ☼10/13/16 13:10 10/21/16 02:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,1,2,2-Tetrachloroethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Tetrachloroethene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Toluene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼trans-1,2-Dichloroethene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼trans-1,3-Dichloropropene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2,3-Trichlorobenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2,4-Trichlorobenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,1,1-Trichloroethane ND
0.00653 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,1,2-Trichloroethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Trichloroethene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Trichlorofluoromethane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2,3-Trichloropropane ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,2,4-Trimethylbenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼1,3,5-Trimethylbenzene ND
0.00261 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Vinyl chloride ND
0.00784 mg/Kg 10/13/16 13:10 10/21/16 02:10 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)99 70-130 10/13/16 13:10 10/21/16 02:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 10/13/16 13:10 10/21/16 02:10 170-130
1,2-Dichloroethane-d4 (Surr)108 10/13/16 13:10 10/21/16 02:10 170-130
Toluene-d8 (Surr)98 10/13/16 13:10 10/21/16 02:10 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.106 mg/Kg ☼10/20/16 10:37 10/27/16 03:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Acenaphthylene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Anthracene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Benzo[a]anthracene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Benzo[a]pyrene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Benzo[b]fluoranthene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Benzo[g,h,i]perylene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Benzo[k]fluoranthene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Bis(2-chloroethoxy)methane ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Bis(2-chloroethyl)ether ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼bis (2-chloroisopropyl) ether ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Bis(2-ethylhexyl) phthalate ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼4-Bromophenyl phenyl ether ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Butyl benzyl phthalate ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Carbazole ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼4-Chloroaniline ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼4-Chloro-3-methylphenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2-Chloronaphthalene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2-Chlorophenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼4-Chlorophenyl phenyl ether ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Chrysene ND
1.06 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Cresols ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Dibenz(a,h)anthracene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-2Client Sample ID: SB-5 (0-2)
Matrix: SoilDate Collected: 10/13/16 14:10
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.528 mg/Kg ☼10/20/16 10:37 10/27/16 03:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼1,3-Dichlorobenzene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼1,4-Dichlorobenzene ND
1.06 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼3,3'-Dichlorobenzidine ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2,4-Dichlorophenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Diethyl phthalate ND
1.06 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2,4-Dimethylphenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Dimethyl phthalate ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Di-n-butyl phthalate ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼4,6-Dinitro-2-methylphenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2,4-Dinitrophenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2,4-Dinitrotoluene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2,6-Dinitrotoluene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Di-n-octyl phthalate ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Fluoranthene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Fluorene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Hexachlorobenzene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Hexachlorobutadiene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Hexachlorocyclopentadiene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Hexachloroethane ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Indeno[1,2,3-cd]pyrene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Isophorone ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼1-Methylnaphthalene ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2-Methylnaphthalene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2-Methylphenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼3 & 4 Methylphenol ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Naphthalene 0.202
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2-Nitroaniline ND
1.06 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼3-Nitroaniline ND
1.06 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼4-Nitroaniline ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Nitrobenzene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2-Nitrophenol ND
1.06 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼4-Nitrophenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼N-Nitrosodi-n-propylamine ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
1.06 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Pentachlorophenol ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Phenanthrene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Phenol ND
0.106 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼Pyrene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼1,2,4-Trichlorobenzene ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2,4,5-Trichlorophenol ND
0.528 mg/Kg 10/20/16 10:37 10/27/16 03:04 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)50 29-120 10/20/16 10:37 10/27/16 03:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)43 10/20/16 10:37 10/27/16 03:04 110-120
Nitrobenzene-d5 (Surr)46 10/20/16 10:37 10/27/16 03:04 127-120
Phenol-d5 (Surr)46 10/20/16 10:37 10/27/16 03:04 110-120
Terphenyl-d14 (Surr)75 10/20/16 10:37 10/27/16 03:04 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-2Client Sample ID: SB-5 (0-2)
Matrix: SoilDate Collected: 10/13/16 14:10
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)69 10-120 10/20/16 10:37 10/27/16 03:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.98 mg/Kg 10/27/16 14:58 10/31/16 11:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.98 mg/Kg 10/27/16 14:58 10/31/16 11:37 12,6-diamino-4-nitrotoluene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 12-Amino-4,6-dinitrotoluene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 14-Amino-2,6-dinitrotoluene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 12,4-Dinitrotoluene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 12,6-Dinitrotoluene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 12,4,6-Trinitrotoluene ND
0.495 mg/Kg 10/27/16 14:58 10/31/16 11:37 1m-Nitrotoluene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 1o-Nitrotoluene ND
0.396 mg/Kg 10/27/16 14:58 10/31/16 11:37 1p-Nitrotoluene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 1NitrobenzeneND
5.05 mg/Kg 10/27/16 14:58 10/31/16 11:37 1NitroglycerinND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 11,3,5-Trinitrobenzene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 11,3-Dinitrobenzene ND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 1HMXND
0.257 mg/Kg 10/27/16 14:58 10/31/16 11:37 1RDXND
0.495 mg/Kg 10/27/16 14:58 10/31/16 11:37 1TetrylND
3.96 mg/Kg 10/27/16 14:58 10/31/16 11:37 1PETNND
0.248 mg/Kg 10/27/16 14:58 10/31/16 11:37 1Picric acid ND
1,2-Dinitrobenzene 92 83-122 10/27/16 14:58 10/31/16 11:37 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony 2.34 J 15.2 1.52 mg/Kg ☼10/20/16 10:21 10/21/16 02:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
3.03 1.82 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Arsenic 4.88
1.52 0.303 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Beryllium 1.18 J
1.52 0.152 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Cadmium 1.36 J
1.52 1.36 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Chromium 18.6
3.03 1.67 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Copper 7.80
1.52 0.758 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Lead 74.8
4.55 1.52 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Manganese 430
3.03 0.910 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Nickel 8.04
3.03 1.67 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Selenium <1.67
1.52 0.607 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Silver <0.607
15.2 4.55 mg/Kg 10/20/16 10:21 10/24/16 15:35 5☼Thallium <4.55
15.2 7.58 mg/Kg 10/20/16 10:21 10/21/16 02:32 1☼Zinc 47.6
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.158 mg/Kg ☼10/20/16 11:45 10/21/16 07:34 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 62.9 0.1 %10/18/16 15:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-3Client Sample ID: SB-6 (0-2)
Matrix: SoilDate Collected: 10/13/16 15:30
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.160 0.0497 mg/Kg ☼10/13/16 14:30 10/21/16 02:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Benzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Bromobenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Bromochloromethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Bromodichloromethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Bromoform ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Bromomethane ND
0.0497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼2-Butanone (MEK)ND
0.00497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Carbon disulfide ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Carbon tetrachloride ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Chlorobenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Chlorodibromomethane ND
0.00497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Chloroethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Chloroform ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Chloromethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼2-Chlorotoluene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼4-Chlorotoluene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼cis-1,2-Dichloroethene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼cis-1,3-Dichloropropene ND
0.00497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2-Dibromo-3-Chloropropane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2-Dibromoethane (EDB)ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Dibromomethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2-Dichlorobenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,3-Dichlorobenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,4-Dichlorobenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Dichlorodifluoromethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,1-Dichloroethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2-Dichloroethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,1-Dichloroethene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2-Dichloroethene, Total ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2-Dichloropropane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,3-Dichloropropane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼2,2-Dichloropropane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,1-Dichloropropene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Diisopropyl ether ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Ethylbenzene ND
0.00497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Hexachlorobutadiene ND
0.0497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼2-Hexanone ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Isopropylbenzene ND
0.00995 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Methylene Chloride ND
0.0497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼4-Methyl-2-pentanone (MIBK)ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Methyl tert-butyl ether ND
0.00497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Naphthalene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼n-Butylbenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼N-Propylbenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼p-Isopropyltoluene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼sec-Butylbenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Styrene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-3Client Sample ID: SB-6 (0-2)
Matrix: SoilDate Collected: 10/13/16 15:30
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00199 mg/Kg ☼10/13/16 14:30 10/21/16 02:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,1,2,2-Tetrachloroethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Tetrachloroethene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Toluene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼trans-1,2-Dichloroethene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼trans-1,3-Dichloropropene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2,3-Trichlorobenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2,4-Trichlorobenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,1,1-Trichloroethane ND
0.00497 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,1,2-Trichloroethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Trichloroethene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Trichlorofluoromethane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2,3-Trichloropropane ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,2,4-Trimethylbenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼1,3,5-Trimethylbenzene ND
0.00199 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Vinyl chloride ND
0.00597 mg/Kg 10/13/16 14:30 10/21/16 02:38 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)100 70-130 10/13/16 14:30 10/21/16 02:38 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)107 10/13/16 14:30 10/21/16 02:38 170-130
1,2-Dichloroethane-d4 (Surr)109 10/13/16 14:30 10/21/16 02:38 170-130
Toluene-d8 (Surr)99 10/13/16 14:30 10/21/16 02:38 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0797 mg/Kg ☼10/20/16 10:37 10/27/16 03:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Acenaphthylene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Anthracene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Benzo[a]anthracene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Benzo[a]pyrene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Benzo[b]fluoranthene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Benzo[g,h,i]perylene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Benzo[k]fluoranthene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Bis(2-chloroethoxy)methane ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Bis(2-chloroethyl)ether ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼bis (2-chloroisopropyl) ether ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Bis(2-ethylhexyl) phthalate ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼4-Bromophenyl phenyl ether ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Butyl benzyl phthalate ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Carbazole ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼4-Chloroaniline ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼4-Chloro-3-methylphenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2-Chloronaphthalene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2-Chlorophenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼4-Chlorophenyl phenyl ether ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Chrysene ND
0.793 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Cresols ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Dibenz(a,h)anthracene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-3Client Sample ID: SB-6 (0-2)
Matrix: SoilDate Collected: 10/13/16 15:30
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.396 mg/Kg ☼10/20/16 10:37 10/27/16 03:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼1,3-Dichlorobenzene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼1,4-Dichlorobenzene ND
0.797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼3,3'-Dichlorobenzidine ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2,4-Dichlorophenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Diethyl phthalate ND
0.797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2,4-Dimethylphenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Dimethyl phthalate ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Di-n-butyl phthalate ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼4,6-Dinitro-2-methylphenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2,4-Dinitrophenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2,4-Dinitrotoluene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2,6-Dinitrotoluene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Di-n-octyl phthalate ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Fluoranthene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Fluorene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Hexachlorobenzene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Hexachlorobutadiene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Hexachlorocyclopentadiene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Hexachloroethane ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Indeno[1,2,3-cd]pyrene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Isophorone ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼1-Methylnaphthalene ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2-Methylnaphthalene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2-Methylphenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼3 & 4 Methylphenol ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Naphthalene 0.132
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2-Nitroaniline ND
0.797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼3-Nitroaniline ND
0.797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼4-Nitroaniline ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Nitrobenzene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2-Nitrophenol ND
0.797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼4-Nitrophenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼N-Nitrosodi-n-propylamine ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Pentachlorophenol ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Phenanthrene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Phenol ND
0.0797 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼Pyrene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼1,2,4-Trichlorobenzene ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2,4,5-Trichlorophenol ND
0.396 mg/Kg 10/20/16 10:37 10/27/16 03:23 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)59 29-120 10/20/16 10:37 10/27/16 03:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)48 10/20/16 10:37 10/27/16 03:23 110-120
Nitrobenzene-d5 (Surr)54 10/20/16 10:37 10/27/16 03:23 127-120
Phenol-d5 (Surr)53 10/20/16 10:37 10/27/16 03:23 110-120
Terphenyl-d14 (Surr)78 10/20/16 10:37 10/27/16 03:23 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-3Client Sample ID: SB-6 (0-2)
Matrix: SoilDate Collected: 10/13/16 15:30
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)72 10-120 10/20/16 10:37 10/27/16 03:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.82 mg/Kg 10/27/16 14:58 10/31/16 12:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.82 mg/Kg 10/27/16 14:58 10/31/16 12:00 12,6-diamino-4-nitrotoluene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 12-Amino-4,6-dinitrotoluene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 14-Amino-2,6-dinitrotoluene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 12,4-Dinitrotoluene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 12,6-Dinitrotoluene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 12,4,6-Trinitrotoluene ND
0.455 mg/Kg 10/27/16 14:58 10/31/16 12:00 1m-Nitrotoluene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 1o-Nitrotoluene ND
0.364 mg/Kg 10/27/16 14:58 10/31/16 12:00 1p-Nitrotoluene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 1NitrobenzeneND
4.64 mg/Kg 10/27/16 14:58 10/31/16 12:00 1NitroglycerinND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 11,3,5-Trinitrobenzene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 11,3-Dinitrobenzene ND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 1HMXND
0.236 mg/Kg 10/27/16 14:58 10/31/16 12:00 1RDXND
0.455 mg/Kg 10/27/16 14:58 10/31/16 12:00 1TetrylND
3.64 mg/Kg 10/27/16 14:58 10/31/16 12:00 1PETNND
0.227 mg/Kg 10/27/16 14:58 10/31/16 12:00 1Picric acid ND
1,2-Dinitrobenzene 96 83-122 10/27/16 14:58 10/31/16 12:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.23 12.3 1.23 mg/Kg ☼10/20/16 10:21 10/21/16 02:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.45 1.47 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Arsenic 5.22
1.23 0.245 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Beryllium 1.25
1.23 0.123 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Cadmium 1.15 J
1.23 1.10 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Chromium 16.3
2.45 1.35 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Copper 14.1
1.23 0.613 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Lead 44.1
3.68 1.23 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Manganese 881
2.45 0.735 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Nickel 10.8
2.45 1.35 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Selenium <1.35
1.23 0.490 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Silver <0.490
12.3 3.68 mg/Kg 10/20/16 10:21 10/24/16 15:40 5☼Thallium <3.68
12.3 6.13 mg/Kg 10/20/16 10:21 10/21/16 02:37 1☼Zinc 46.6
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.120 mg/Kg ☼10/20/16 11:45 10/21/16 07:37 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 81.9 0.1 %10/18/16 15:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-4Client Sample ID: SB-9 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:30
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.264 0.0613 mg/Kg ☼10/14/16 14:30 10/21/16 03:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Benzene 0.451
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Bromobenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Bromochloromethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Bromodichloromethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Bromoform ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Bromomethane ND
0.0613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼2-Butanone (MEK)0.0767
0.00613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Carbon disulfide 0.00844
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Carbon tetrachloride ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Chlorobenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Chlorodibromomethane ND
0.00613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Chloroethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Chloroform ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Chloromethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼2-Chlorotoluene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼4-Chlorotoluene ND
0.157 mg/Kg 10/14/16 14:30 10/25/16 13:59 1☼cis-1,2-Dichloroethene 3.98
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼cis-1,3-Dichloropropene ND
0.00613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2-Dibromo-3-Chloropropane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2-Dibromoethane (EDB)ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Dibromomethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2-Dichlorobenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,3-Dichlorobenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,4-Dichlorobenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Dichlorodifluoromethane 0.0312
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,1-Dichloroethane 0.0107
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2-Dichloroethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,1-Dichloroethene ND
0.157 mg/Kg 10/14/16 14:30 10/25/16 13:59 1☼1,2-Dichloroethene, Total 3.98
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2-Dichloropropane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,3-Dichloropropane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼2,2-Dichloropropane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,1-Dichloropropene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Diisopropyl ether ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Ethylbenzene 0.327
0.00613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Hexachlorobutadiene ND
0.0613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼2-Hexanone ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Isopropylbenzene 0.0179
0.0123 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Methylene Chloride ND
0.0613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼4-Methyl-2-pentanone (MIBK)0.423
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Methyl tert-butyl ether ND
0.00613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Naphthalene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼n-Butylbenzene 0.00388
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼N-Propylbenzene 0.0107
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼p-Isopropyltoluene 0.00917
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼sec-Butylbenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Styrene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-4Client Sample ID: SB-9 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:30
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00245 mg/Kg ☼10/14/16 14:30 10/21/16 03:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,1,2,2-Tetrachloroethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Tetrachloroethene 0.0200
0.157 mg/Kg 10/14/16 14:30 10/25/16 13:59 1☼Toluene 6.81
0.157 mg/Kg 10/14/16 14:30 10/25/16 13:59 1☼trans-1,2-Dichloroethene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼trans-1,3-Dichloropropene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2,3-Trichlorobenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2,4-Trichlorobenzene ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,1,1-Trichloroethane 0.0182
0.00613 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,1,2-Trichloroethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Trichloroethene 0.278
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Trichlorofluoromethane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2,3-Trichloropropane ND
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,2,4-Trimethylbenzene 0.0273
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼1,3,5-Trimethylbenzene 0.0134
0.00245 mg/Kg 10/14/16 14:30 10/21/16 03:05 1☼Vinyl chloride ND
0.235 mg/Kg 10/14/16 14:30 10/25/16 13:59 1☼Xylenes, Total 35.4
4-Bromofluorobenzene (Surr)119 70-130 10/14/16 14:30 10/21/16 03:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene (Surr)110 10/14/16 14:30 10/25/16 13:59 170-130
Dibromofluoromethane (Surr)115 10/14/16 14:30 10/21/16 03:05 170-130
Dibromofluoromethane (Surr)101 10/14/16 14:30 10/25/16 13:59 170-130
1,2-Dichloroethane-d4 (Surr)118 10/14/16 14:30 10/21/16 03:05 170-130
1,2-Dichloroethane-d4 (Surr)107 10/14/16 14:30 10/25/16 13:59 170-130
Toluene-d8 (Surr)105 10/14/16 14:30 10/21/16 03:05 170-130
Toluene-d8 (Surr)103 10/14/16 14:30 10/25/16 13:59 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.450 mg/Kg ☼10/20/16 10:37 10/27/16 03:42 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Acenaphthylene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Anthracene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Benzo[a]anthracene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Benzo[a]pyrene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Benzo[b]fluoranthene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Benzo[g,h,i]perylene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Benzo[k]fluoranthene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Bis(2-chloroethoxy)methane ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Bis(2-chloroethyl)ether ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼bis (2-chloroisopropyl) ether ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Bis(2-ethylhexyl) phthalate ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼4-Bromophenyl phenyl ether ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Butyl benzyl phthalate ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Carbazole ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼4-Chloroaniline ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼4-Chloro-3-methylphenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2-Chloronaphthalene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2-Chlorophenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼4-Chlorophenyl phenyl ether ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-4Client Sample ID: SB-9 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:30
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
Chrysene ND 0.450 mg/Kg ☼10/20/16 10:37 10/27/16 03:42 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
4.47 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Cresols ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Dibenz(a,h)anthracene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Dibenzofuran ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼1,2-Dichlorobenzene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼1,3-Dichlorobenzene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼1,4-Dichlorobenzene ND
4.50 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼3,3'-Dichlorobenzidine ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2,4-Dichlorophenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Diethyl phthalate ND
4.50 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2,4-Dimethylphenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Dimethyl phthalate ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Di-n-butyl phthalate ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼4,6-Dinitro-2-methylphenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2,4-Dinitrophenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2,4-Dinitrotoluene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2,6-Dinitrotoluene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Di-n-octyl phthalate ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Fluoranthene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Fluorene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Hexachlorobenzene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Hexachlorobutadiene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Hexachlorocyclopentadiene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Hexachloroethane ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Indeno[1,2,3-cd]pyrene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Isophorone ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼1-Methylnaphthalene ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2-Methylnaphthalene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2-Methylphenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼3 & 4 Methylphenol ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Naphthalene 0.482
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2-Nitroaniline ND
4.50 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼3-Nitroaniline ND
4.50 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼4-Nitroaniline ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Nitrobenzene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2-Nitrophenol ND
4.50 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼4-Nitrophenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼N-Nitrosodi-n-propylamine ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
4.50 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Pentachlorophenol ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Phenanthrene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Phenol ND
0.450 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼Pyrene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼1,2,4-Trichlorobenzene ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2,4,5-Trichlorophenol ND
2.23 mg/Kg 10/20/16 10:37 10/27/16 03:42 5☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)65 29-120 10/20/16 10:37 10/27/16 03:42 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-4Client Sample ID: SB-9 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:30
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2-Fluorophenol (Surr)49 10-120 10/20/16 10:37 10/27/16 03:42 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)59 10/20/16 10:37 10/27/16 03:42 527-120
Phenol-d5 (Surr)59 10/20/16 10:37 10/27/16 03:42 510-120
Terphenyl-d14 (Surr)66 10/20/16 10:37 10/27/16 03:42 513-120
2,4,6-Tribromophenol (Surr)81 10/20/16 10:37 10/27/16 03:42 510-120
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.96 mg/Kg 10/27/16 14:58 10/31/16 12:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.96 mg/Kg 10/27/16 14:58 10/31/16 12:23 12,6-diamino-4-nitrotoluene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 12-Amino-4,6-dinitrotoluene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 14-Amino-2,6-dinitrotoluene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 12,4-Dinitrotoluene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 12,6-Dinitrotoluene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 12,4,6-Trinitrotoluene ND
0.490 mg/Kg 10/27/16 14:58 10/31/16 12:23 1m-Nitrotoluene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 1o-Nitrotoluene ND
0.392 mg/Kg 10/27/16 14:58 10/31/16 12:23 1p-Nitrotoluene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 1NitrobenzeneND
5.00 mg/Kg 10/27/16 14:58 10/31/16 12:23 1NitroglycerinND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 11,3,5-Trinitrobenzene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 11,3-Dinitrobenzene ND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 1HMXND
0.255 mg/Kg 10/27/16 14:58 10/31/16 12:23 1RDXND
0.490 mg/Kg 10/27/16 14:58 10/31/16 12:23 1TetrylND
3.92 mg/Kg 10/27/16 14:58 10/31/16 12:23 1PETNND
0.245 mg/Kg 10/27/16 14:58 10/31/16 12:23 1Picric acid ND
1,2-Dinitrobenzene 106 83-122 10/27/16 14:58 10/31/16 12:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony 1.67 J 13.5 1.35 mg/Kg ☼10/20/16 10:21 10/21/16 02:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.69 1.61 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Arsenic 4.95
1.35 0.269 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Beryllium 1.51
1.35 0.135 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Cadmium 1.59
1.35 1.21 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Chromium 17.8
2.69 1.48 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Copper 25.9
1.35 0.673 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Lead 156
4.04 1.35 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Manganese 266
2.69 0.807 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Nickel 8.58
2.69 1.48 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Selenium <1.48
1.35 0.538 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Silver <0.538
13.5 4.04 mg/Kg 10/20/16 10:21 10/24/16 15:46 5☼Thallium <4.04
13.5 6.73 mg/Kg 10/20/16 10:21 10/21/16 02:42 1☼Zinc 938
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.132 mg/Kg ☼10/20/16 11:45 10/21/16 07:40 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
General Chemistry
RL RL
Percent Solids 73.0 0.1 %10/18/16 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Page 23 of 108 6/26/2018 (Rev. 1)
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-5Client Sample ID: SB-8 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:40
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.225 0.0490 mg/Kg ☼10/14/16 14:40 10/21/16 03:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Benzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Bromobenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Bromochloromethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Bromodichloromethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Bromoform ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Bromomethane ND
0.0490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼2-Butanone (MEK)ND
0.00490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Carbon disulfide ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Carbon tetrachloride ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Chlorobenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Chlorodibromomethane ND
0.00490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Chloroethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Chloroform ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Chloromethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼2-Chlorotoluene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼4-Chlorotoluene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼cis-1,2-Dichloroethene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼cis-1,3-Dichloropropene ND
0.00490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2-Dibromo-3-Chloropropane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2-Dibromoethane (EDB)ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Dibromomethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2-Dichlorobenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,3-Dichlorobenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,4-Dichlorobenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Dichlorodifluoromethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,1-Dichloroethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2-Dichloroethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,1-Dichloroethene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2-Dichloroethene, Total ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2-Dichloropropane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,3-Dichloropropane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼2,2-Dichloropropane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,1-Dichloropropene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Diisopropyl ether ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Ethylbenzene ND
0.00490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Hexachlorobutadiene ND
0.0490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼2-Hexanone ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Isopropylbenzene ND
0.00980 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Methylene Chloride ND
0.0490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼4-Methyl-2-pentanone (MIBK)ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Methyl tert-butyl ether ND
0.00490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Naphthalene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼n-Butylbenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼N-Propylbenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼p-Isopropyltoluene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼sec-Butylbenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Styrene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-5Client Sample ID: SB-8 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:40
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00196 mg/Kg ☼10/14/16 14:40 10/21/16 03:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,1,2,2-Tetrachloroethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Tetrachloroethene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Toluene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼trans-1,2-Dichloroethene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼trans-1,3-Dichloropropene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2,3-Trichlorobenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2,4-Trichlorobenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,1,1-Trichloroethane ND
0.00490 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,1,2-Trichloroethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Trichloroethene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Trichlorofluoromethane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2,3-Trichloropropane ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,2,4-Trimethylbenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼1,3,5-Trimethylbenzene ND
0.00196 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Vinyl chloride ND
0.00588 mg/Kg 10/14/16 14:40 10/21/16 03:33 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)101 70-130 10/14/16 14:40 10/21/16 03:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)105 10/14/16 14:40 10/21/16 03:33 170-130
1,2-Dichloroethane-d4 (Surr)107 10/14/16 14:40 10/21/16 03:33 170-130
Toluene-d8 (Surr)99 10/14/16 14:40 10/21/16 03:33 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0862 mg/Kg ☼10/20/16 10:37 10/27/16 04:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Acenaphthylene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Anthracene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Benzo[a]anthracene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Benzo[a]pyrene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Benzo[b]fluoranthene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Benzo[g,h,i]perylene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Benzo[k]fluoranthene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Bis(2-chloroethoxy)methane ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Bis(2-chloroethyl)ether ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼bis (2-chloroisopropyl) ether ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Bis(2-ethylhexyl) phthalate ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼4-Bromophenyl phenyl ether ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Butyl benzyl phthalate ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Carbazole ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼4-Chloroaniline ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼4-Chloro-3-methylphenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2-Chloronaphthalene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2-Chlorophenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼4-Chlorophenyl phenyl ether ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Chrysene ND
0.857 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Cresols ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Dibenz(a,h)anthracene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-5Client Sample ID: SB-8 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:40
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.428 mg/Kg ☼10/20/16 10:37 10/27/16 04:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼1,3-Dichlorobenzene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼1,4-Dichlorobenzene ND
0.862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼3,3'-Dichlorobenzidine ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2,4-Dichlorophenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Diethyl phthalate ND
0.862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2,4-Dimethylphenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Dimethyl phthalate ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Di-n-butyl phthalate ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼4,6-Dinitro-2-methylphenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2,4-Dinitrophenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2,4-Dinitrotoluene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2,6-Dinitrotoluene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Di-n-octyl phthalate ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Fluoranthene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Fluorene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Hexachlorobenzene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Hexachlorobutadiene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Hexachlorocyclopentadiene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Hexachloroethane ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Indeno[1,2,3-cd]pyrene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Isophorone ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼1-Methylnaphthalene ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2-Methylnaphthalene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2-Methylphenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼3 & 4 Methylphenol ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Naphthalene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2-Nitroaniline ND
0.862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼3-Nitroaniline ND
0.862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼4-Nitroaniline ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Nitrobenzene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2-Nitrophenol ND
0.862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼4-Nitrophenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼N-Nitrosodi-n-propylamine ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Pentachlorophenol ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Phenanthrene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Phenol ND
0.0862 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼Pyrene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼1,2,4-Trichlorobenzene ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2,4,5-Trichlorophenol ND
0.428 mg/Kg 10/20/16 10:37 10/27/16 04:01 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)51 29-120 10/20/16 10:37 10/27/16 04:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)44 10/20/16 10:37 10/27/16 04:01 110-120
Nitrobenzene-d5 (Surr)47 10/20/16 10:37 10/27/16 04:01 127-120
Phenol-d5 (Surr)46 10/20/16 10:37 10/27/16 04:01 110-120
Terphenyl-d14 (Surr)56 10/20/16 10:37 10/27/16 04:01 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-5Client Sample ID: SB-8 (0-2)
Matrix: SoilDate Collected: 10/14/16 15:40
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)59 10-120 10/20/16 10:37 10/27/16 04:01 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.92 mg/Kg 10/27/16 14:58 10/31/16 12:46 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.92 mg/Kg 10/27/16 14:58 10/31/16 12:46 12,6-diamino-4-nitrotoluene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 12-Amino-4,6-dinitrotoluene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 14-Amino-2,6-dinitrotoluene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 12,4-Dinitrotoluene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 12,6-Dinitrotoluene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 12,4,6-Trinitrotoluene ND
0.481 mg/Kg 10/27/16 14:58 10/31/16 12:46 1m-Nitrotoluene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 1o-Nitrotoluene ND
0.385 mg/Kg 10/27/16 14:58 10/31/16 12:46 1p-Nitrotoluene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 1NitrobenzeneND
4.90 mg/Kg 10/27/16 14:58 10/31/16 12:46 1NitroglycerinND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 11,3,5-Trinitrobenzene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 11,3-Dinitrobenzene ND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 1HMXND
0.250 mg/Kg 10/27/16 14:58 10/31/16 12:46 1RDXND
0.481 mg/Kg 10/27/16 14:58 10/31/16 12:46 1TetrylND
3.85 mg/Kg 10/27/16 14:58 10/31/16 12:46 1PETNND
0.240 mg/Kg 10/27/16 14:58 10/31/16 12:46 1Picric acid ND
1,2-Dinitrobenzene 103 83-122 10/27/16 14:58 10/31/16 12:46 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.30 13.0 1.30 mg/Kg ☼10/20/16 10:21 10/21/16 02:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.59 1.56 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Arsenic 5.00
1.30 0.259 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Beryllium 1.09 J
1.30 0.130 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Cadmium 1.22 J
1.30 1.17 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Chromium 41.9
2.59 1.43 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Copper 19.8
1.30 0.648 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Lead 43.9
3.89 1.30 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Manganese 365
2.59 0.778 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Nickel 14.2
2.59 1.43 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Selenium <1.43
1.30 0.519 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Silver <0.519
13.0 3.89 mg/Kg 10/20/16 10:21 10/24/16 15:51 5☼Thallium <3.89
13.0 6.48 mg/Kg 10/20/16 10:21 10/21/16 02:58 1☼Zinc 44.8
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.126 mg/Kg ☼10/20/16 11:45 10/21/16 07:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 76.5 0.1 %10/18/16 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-6Client Sample ID: SB-7 (4-6)
Matrix: SoilDate Collected: 10/14/16 15:50
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.122 0.0959 mg/Kg ☼10/14/16 14:50 10/21/16 04:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Benzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Bromobenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Bromochloromethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Bromodichloromethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Bromoform ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Bromomethane ND
0.0959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼2-Butanone (MEK)ND
0.00959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Carbon disulfide ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Carbon tetrachloride ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Chlorobenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Chlorodibromomethane ND
0.00959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Chloroethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Chloroform ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Chloromethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼2-Chlorotoluene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼4-Chlorotoluene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼cis-1,2-Dichloroethene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼cis-1,3-Dichloropropene ND
0.00959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2-Dibromo-3-Chloropropane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2-Dibromoethane (EDB)ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Dibromomethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2-Dichlorobenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,3-Dichlorobenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,4-Dichlorobenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Dichlorodifluoromethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,1-Dichloroethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2-Dichloroethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,1-Dichloroethene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2-Dichloroethene, Total ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2-Dichloropropane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,3-Dichloropropane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼2,2-Dichloropropane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,1-Dichloropropene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Diisopropyl ether ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Ethylbenzene ND
0.00959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Hexachlorobutadiene ND
0.0959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼2-Hexanone ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Isopropylbenzene ND
0.0192 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Methylene Chloride ND
0.0959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼4-Methyl-2-pentanone (MIBK)ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Methyl tert-butyl ether ND
0.00959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Naphthalene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼n-Butylbenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼N-Propylbenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼p-Isopropyltoluene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼sec-Butylbenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Styrene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-6Client Sample ID: SB-7 (4-6)
Matrix: SoilDate Collected: 10/14/16 15:50
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00383 mg/Kg ☼10/14/16 14:50 10/21/16 04:00 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,1,2,2-Tetrachloroethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Tetrachloroethene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Toluene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼trans-1,2-Dichloroethene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼trans-1,3-Dichloropropene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2,3-Trichlorobenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2,4-Trichlorobenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,1,1-Trichloroethane ND
0.00959 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,1,2-Trichloroethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Trichloroethene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Trichlorofluoromethane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2,3-Trichloropropane ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,2,4-Trimethylbenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼1,3,5-Trimethylbenzene ND
0.00383 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Vinyl chloride ND
0.0115 mg/Kg 10/14/16 14:50 10/21/16 04:00 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)100 70-130 10/14/16 14:50 10/21/16 04:00 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)105 10/14/16 14:50 10/21/16 04:00 170-130
1,2-Dichloroethane-d4 (Surr)105 10/14/16 14:50 10/21/16 04:00 170-130
Toluene-d8 (Surr)99 10/14/16 14:50 10/21/16 04:00 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0937 mg/Kg ☼10/20/16 10:37 10/27/16 04:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Acenaphthylene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Anthracene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Benzo[a]anthracene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Benzo[a]pyrene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Benzo[b]fluoranthene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Benzo[g,h,i]perylene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Benzo[k]fluoranthene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Bis(2-chloroethoxy)methane ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Bis(2-chloroethyl)ether ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼bis (2-chloroisopropyl) ether ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Bis(2-ethylhexyl) phthalate ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼4-Bromophenyl phenyl ether ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Butyl benzyl phthalate ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Carbazole ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼4-Chloroaniline ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼4-Chloro-3-methylphenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2-Chloronaphthalene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2-Chlorophenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼4-Chlorophenyl phenyl ether ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Chrysene ND
0.932 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Cresols ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Dibenz(a,h)anthracene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-6Client Sample ID: SB-7 (4-6)
Matrix: SoilDate Collected: 10/14/16 15:50
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.466 mg/Kg ☼10/20/16 10:37 10/27/16 04:20 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼1,3-Dichlorobenzene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼1,4-Dichlorobenzene ND
0.937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼3,3'-Dichlorobenzidine ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2,4-Dichlorophenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Diethyl phthalate ND
0.937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2,4-Dimethylphenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Dimethyl phthalate ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Di-n-butyl phthalate ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼4,6-Dinitro-2-methylphenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2,4-Dinitrophenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2,4-Dinitrotoluene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2,6-Dinitrotoluene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Di-n-octyl phthalate ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Fluoranthene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Fluorene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Hexachlorobenzene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Hexachlorobutadiene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Hexachlorocyclopentadiene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Hexachloroethane ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Indeno[1,2,3-cd]pyrene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Isophorone ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼1-Methylnaphthalene ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2-Methylnaphthalene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2-Methylphenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼3 & 4 Methylphenol ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Naphthalene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2-Nitroaniline ND
0.937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼3-Nitroaniline ND
0.937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼4-Nitroaniline ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Nitrobenzene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2-Nitrophenol ND
0.937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼4-Nitrophenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼N-Nitrosodi-n-propylamine ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Pentachlorophenol ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Phenanthrene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Phenol ND
0.0937 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼Pyrene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼1,2,4-Trichlorobenzene ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2,4,5-Trichlorophenol ND
0.466 mg/Kg 10/20/16 10:37 10/27/16 04:20 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)26 X 29-120 10/20/16 10:37 10/27/16 04:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)24 10/20/16 10:37 10/27/16 04:20 110-120
Nitrobenzene-d5 (Surr)24 X 10/20/16 10:37 10/27/16 04:20 127-120
Phenol-d5 (Surr)24 10/20/16 10:37 10/27/16 04:20 110-120
Terphenyl-d14 (Surr)32 10/20/16 10:37 10/27/16 04:20 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-6Client Sample ID: SB-7 (4-6)
Matrix: SoilDate Collected: 10/14/16 15:50
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)31 10-120 10/20/16 10:37 10/27/16 04:20 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.87 mg/Kg 10/27/16 14:58 10/31/16 13:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.87 mg/Kg 10/27/16 14:58 10/31/16 13:09 12,6-diamino-4-nitrotoluene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 12-Amino-4,6-dinitrotoluene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 14-Amino-2,6-dinitrotoluene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 12,4-Dinitrotoluene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 12,6-Dinitrotoluene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 12,4,6-Trinitrotoluene ND
0.467 mg/Kg 10/27/16 14:58 10/31/16 13:09 1m-Nitrotoluene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 1o-Nitrotoluene ND
0.374 mg/Kg 10/27/16 14:58 10/31/16 13:09 1p-Nitrotoluene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 1NitrobenzeneND
4.77 mg/Kg 10/27/16 14:58 10/31/16 13:09 1NitroglycerinND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 11,3,5-Trinitrobenzene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 11,3-Dinitrobenzene ND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 1HMXND
0.243 mg/Kg 10/27/16 14:58 10/31/16 13:09 1RDXND
0.467 mg/Kg 10/27/16 14:58 10/31/16 13:09 1TetrylND
3.74 mg/Kg 10/27/16 14:58 10/31/16 13:09 1PETNND
0.234 mg/Kg 10/27/16 14:58 10/31/16 13:09 1Picric acid ND
1,2-Dinitrobenzene 105 83-122 10/27/16 14:58 10/31/16 13:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.40 14.0 1.40 mg/Kg ☼10/20/16 10:21 10/21/16 03:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.79 1.68 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Arsenic 3.94
1.40 0.279 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Beryllium 1.59
1.40 0.140 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Cadmium 1.15 J
1.40 1.26 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Chromium 3.33
2.79 1.54 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Copper 12.1
1.40 0.699 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Lead 39.8
4.19 1.40 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Manganese 414
2.79 0.838 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Nickel 3.58
2.79 1.54 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Selenium <1.54
1.40 0.559 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Silver <0.559
14.0 4.19 mg/Kg 10/20/16 10:21 10/24/16 15:56 5☼Thallium <4.19
14.0 6.99 mg/Kg 10/20/16 10:21 10/21/16 03:04 1☼Zinc 114
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.145 mg/Kg ☼10/20/16 11:45 10/21/16 07:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 69.4 0.1 %10/18/16 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-7Client Sample ID: SB-1 (0-2)
Matrix: SoilDate Collected: 10/14/16 18:00
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0574 mg/Kg ☼10/14/16 17:00 10/21/16 04:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Benzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Bromobenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Bromochloromethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Bromodichloromethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Bromoform ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Bromomethane ND
0.0574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼2-Butanone (MEK)ND
0.00574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Carbon disulfide ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Carbon tetrachloride ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Chlorobenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Chlorodibromomethane ND
0.00574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Chloroethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Chloroform ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Chloromethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼2-Chlorotoluene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼4-Chlorotoluene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼cis-1,2-Dichloroethene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼cis-1,3-Dichloropropene ND
0.00574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2-Dibromo-3-Chloropropane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2-Dibromoethane (EDB)ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Dibromomethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2-Dichlorobenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,3-Dichlorobenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,4-Dichlorobenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Dichlorodifluoromethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,1-Dichloroethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2-Dichloroethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,1-Dichloroethene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2-Dichloroethene, Total ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2-Dichloropropane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,3-Dichloropropane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼2,2-Dichloropropane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,1-Dichloropropene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Diisopropyl ether ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Ethylbenzene ND
0.00574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Hexachlorobutadiene ND
0.0574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼2-Hexanone ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Isopropylbenzene ND
0.0115 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Methylene Chloride ND
0.0574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼4-Methyl-2-pentanone (MIBK)ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Methyl tert-butyl ether ND
0.00574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Naphthalene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼n-Butylbenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼N-Propylbenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼p-Isopropyltoluene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼sec-Butylbenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Styrene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-7Client Sample ID: SB-1 (0-2)
Matrix: SoilDate Collected: 10/14/16 18:00
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00229 mg/Kg ☼10/14/16 17:00 10/21/16 04:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,1,2,2-Tetrachloroethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Tetrachloroethene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Toluene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼trans-1,2-Dichloroethene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼trans-1,3-Dichloropropene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2,3-Trichlorobenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2,4-Trichlorobenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,1,1-Trichloroethane ND
0.00574 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,1,2-Trichloroethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Trichloroethene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Trichlorofluoromethane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2,3-Trichloropropane ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,2,4-Trimethylbenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼1,3,5-Trimethylbenzene ND
0.00229 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Vinyl chloride ND
0.00688 mg/Kg 10/14/16 17:00 10/21/16 04:28 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)100 70-130 10/14/16 17:00 10/21/16 04:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 10/14/16 17:00 10/21/16 04:28 170-130
1,2-Dichloroethane-d4 (Surr)109 10/14/16 17:00 10/21/16 04:28 170-130
Toluene-d8 (Surr)97 10/14/16 17:00 10/21/16 04:28 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0838 mg/Kg ☼10/20/16 11:13 10/21/16 16:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Acenaphthylene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Anthracene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Benzo[a]anthracene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Benzo[a]pyrene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Benzo[b]fluoranthene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Benzo[g,h,i]perylene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Benzo[k]fluoranthene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Bis(2-chloroethoxy)methane ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Bis(2-chloroethyl)ether ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼bis (2-chloroisopropyl) ether ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Bis(2-ethylhexyl) phthalate ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼4-Bromophenyl phenyl ether ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Butyl benzyl phthalate ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Carbazole ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼4-Chloroaniline ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼4-Chloro-3-methylphenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2-Chloronaphthalene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2-Chlorophenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼4-Chlorophenyl phenyl ether ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Chrysene ND
0.833 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Cresols ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Dibenz(a,h)anthracene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-7Client Sample ID: SB-1 (0-2)
Matrix: SoilDate Collected: 10/14/16 18:00
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.417 mg/Kg ☼10/20/16 11:13 10/21/16 16:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼1,3-Dichlorobenzene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼1,4-Dichlorobenzene ND
0.838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼3,3'-Dichlorobenzidine ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2,4-Dichlorophenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Diethyl phthalate ND
0.838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2,4-Dimethylphenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Dimethyl phthalate ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Di-n-butyl phthalate ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼4,6-Dinitro-2-methylphenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2,4-Dinitrophenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2,4-Dinitrotoluene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2,6-Dinitrotoluene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Di-n-octyl phthalate ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Fluoranthene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Fluorene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Hexachlorobenzene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Hexachlorobutadiene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Hexachlorocyclopentadiene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Hexachloroethane ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Indeno[1,2,3-cd]pyrene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Isophorone ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼1-Methylnaphthalene ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2-Methylnaphthalene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2-Methylphenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼3 & 4 Methylphenol ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Naphthalene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2-Nitroaniline ND
0.838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼3-Nitroaniline ND
0.838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼4-Nitroaniline ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Nitrobenzene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2-Nitrophenol ND
0.838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼4-Nitrophenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼N-Nitrosodi-n-propylamine ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Pentachlorophenol ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Phenanthrene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Phenol ND
0.0838 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼Pyrene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼1,2,4-Trichlorobenzene ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2,4,5-Trichlorophenol ND
0.417 mg/Kg 10/20/16 11:13 10/21/16 16:13 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)55 29-120 10/20/16 11:13 10/21/16 16:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)46 10/20/16 11:13 10/21/16 16:13 110-120
Nitrobenzene-d5 (Surr)49 10/20/16 11:13 10/21/16 16:13 127-120
Phenol-d5 (Surr)54 10/20/16 11:13 10/21/16 16:13 110-120
Terphenyl-d14 (Surr)72 10/20/16 11:13 10/21/16 16:13 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-7Client Sample ID: SB-1 (0-2)
Matrix: SoilDate Collected: 10/14/16 18:00
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)68 10-120 10/20/16 11:13 10/21/16 16:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.90 mg/Kg 10/27/16 14:58 10/31/16 13:32 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.90 mg/Kg 10/27/16 14:58 10/31/16 13:32 12,6-diamino-4-nitrotoluene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 12-Amino-4,6-dinitrotoluene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 14-Amino-2,6-dinitrotoluene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 12,4-Dinitrotoluene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 12,6-Dinitrotoluene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 12,4,6-Trinitrotoluene ND
0.474 mg/Kg 10/27/16 14:58 10/31/16 13:32 1m-Nitrotoluene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 1o-Nitrotoluene ND
0.379 mg/Kg 10/27/16 14:58 10/31/16 13:32 1p-Nitrotoluene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 1NitrobenzeneND
4.83 mg/Kg 10/27/16 14:58 10/31/16 13:32 1NitroglycerinND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 11,3,5-Trinitrobenzene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 11,3-Dinitrobenzene ND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 1HMXND
0.246 mg/Kg 10/27/16 14:58 10/31/16 13:32 1RDXND
0.474 mg/Kg 10/27/16 14:58 10/31/16 13:32 1TetrylND
3.79 mg/Kg 10/27/16 14:58 10/31/16 13:32 1PETNND
0.237 mg/Kg 10/27/16 14:58 10/31/16 13:32 1Picric acid ND
1,2-Dinitrobenzene 105 83-122 10/27/16 14:58 10/31/16 13:32 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.27 12.7 1.27 mg/Kg ☼10/20/16 10:21 10/21/16 03:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.53 1.52 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Arsenic 4.13
1.27 0.253 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Beryllium 0.608 J
1.27 0.127 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Cadmium 1.34
1.27 1.14 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Chromium 14.8
2.53 1.39 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Copper 5.78
1.27 0.633 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Lead 50.8
3.80 1.27 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Manganese 122
2.53 0.760 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Nickel 9.47
2.53 1.39 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Selenium <1.39
1.27 0.507 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Silver <0.507
12.7 3.80 mg/Kg 10/20/16 10:21 10/24/16 16:01 5☼Thallium <3.80
12.7 6.33 mg/Kg 10/20/16 10:21 10/21/16 03:09 1☼Zinc 21.6
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.122 mg/Kg ☼10/20/16 11:45 10/21/16 07:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 78.6 0.1 %10/18/16 15:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-8Client Sample ID: SB-2 (4-6)
Matrix: SoilDate Collected: 10/14/16 18:27
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0547 mg/Kg ☼10/14/16 17:27 10/21/16 04:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Benzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Bromobenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Bromochloromethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Bromodichloromethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Bromoform ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Bromomethane ND
0.0547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼2-Butanone (MEK)ND
0.00547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Carbon disulfide ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Carbon tetrachloride ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Chlorobenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Chlorodibromomethane ND
0.00547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Chloroethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Chloroform ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Chloromethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼2-Chlorotoluene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼4-Chlorotoluene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼cis-1,2-Dichloroethene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼cis-1,3-Dichloropropene ND
0.00547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2-Dibromo-3-Chloropropane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2-Dibromoethane (EDB)ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Dibromomethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2-Dichlorobenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,3-Dichlorobenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,4-Dichlorobenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Dichlorodifluoromethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,1-Dichloroethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2-Dichloroethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,1-Dichloroethene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2-Dichloroethene, Total ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2-Dichloropropane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,3-Dichloropropane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼2,2-Dichloropropane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,1-Dichloropropene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Diisopropyl ether ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Ethylbenzene ND
0.00547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Hexachlorobutadiene ND
0.0547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼2-Hexanone ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Isopropylbenzene ND
0.0109 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Methylene Chloride ND
0.0547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼4-Methyl-2-pentanone (MIBK)ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Methyl tert-butyl ether ND
0.00547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Naphthalene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼n-Butylbenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼N-Propylbenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼p-Isopropyltoluene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼sec-Butylbenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Styrene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-8Client Sample ID: SB-2 (4-6)
Matrix: SoilDate Collected: 10/14/16 18:27
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00219 mg/Kg ☼10/14/16 17:27 10/21/16 04:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,1,2,2-Tetrachloroethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Tetrachloroethene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Toluene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼trans-1,2-Dichloroethene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼trans-1,3-Dichloropropene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2,3-Trichlorobenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2,4-Trichlorobenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,1,1-Trichloroethane ND
0.00547 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,1,2-Trichloroethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Trichloroethene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Trichlorofluoromethane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2,3-Trichloropropane ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,2,4-Trimethylbenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼1,3,5-Trimethylbenzene ND
0.00219 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Vinyl chloride ND
0.00656 mg/Kg 10/14/16 17:27 10/21/16 04:55 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)98 70-130 10/14/16 17:27 10/21/16 04:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)109 10/14/16 17:27 10/21/16 04:55 170-130
1,2-Dichloroethane-d4 (Surr)109 10/14/16 17:27 10/21/16 04:55 170-130
Toluene-d8 (Surr)98 10/14/16 17:27 10/21/16 04:55 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0818 mg/Kg ☼10/20/16 11:13 10/21/16 17:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Acenaphthylene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Anthracene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Benzo[a]anthracene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Benzo[a]pyrene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Benzo[b]fluoranthene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Benzo[g,h,i]perylene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Benzo[k]fluoranthene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Bis(2-chloroethoxy)methane ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Bis(2-chloroethyl)ether ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼bis (2-chloroisopropyl) ether ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Bis(2-ethylhexyl) phthalate ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼4-Bromophenyl phenyl ether ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Butyl benzyl phthalate ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Carbazole ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼4-Chloroaniline ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼4-Chloro-3-methylphenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2-Chloronaphthalene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2-Chlorophenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼4-Chlorophenyl phenyl ether ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Chrysene ND
0.813 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Cresols ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Dibenz(a,h)anthracene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-8Client Sample ID: SB-2 (4-6)
Matrix: SoilDate Collected: 10/14/16 18:27
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.406 mg/Kg ☼10/20/16 11:13 10/21/16 17:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼1,3-Dichlorobenzene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼1,4-Dichlorobenzene ND
0.818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼3,3'-Dichlorobenzidine ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2,4-Dichlorophenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Diethyl phthalate ND
0.818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2,4-Dimethylphenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Dimethyl phthalate ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Di-n-butyl phthalate ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼4,6-Dinitro-2-methylphenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2,4-Dinitrophenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2,4-Dinitrotoluene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2,6-Dinitrotoluene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Di-n-octyl phthalate ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Fluoranthene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Fluorene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Hexachlorobenzene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Hexachlorobutadiene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Hexachlorocyclopentadiene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Hexachloroethane ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Indeno[1,2,3-cd]pyrene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Isophorone ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼1-Methylnaphthalene ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2-Methylnaphthalene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2-Methylphenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼3 & 4 Methylphenol ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Naphthalene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2-Nitroaniline ND
0.818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼3-Nitroaniline ND
0.818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼4-Nitroaniline ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Nitrobenzene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2-Nitrophenol ND
0.818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼4-Nitrophenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼N-Nitrosodi-n-propylamine ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Pentachlorophenol ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Phenanthrene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Phenol ND
0.0818 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼Pyrene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼1,2,4-Trichlorobenzene ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2,4,5-Trichlorophenol ND
0.406 mg/Kg 10/20/16 11:13 10/21/16 17:09 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)60 29-120 10/20/16 11:13 10/21/16 17:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)55 10/20/16 11:13 10/21/16 17:09 110-120
Nitrobenzene-d5 (Surr)56 10/20/16 11:13 10/21/16 17:09 127-120
Phenol-d5 (Surr)60 10/20/16 11:13 10/21/16 17:09 110-120
Terphenyl-d14 (Surr)80 10/20/16 11:13 10/21/16 17:09 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-8Client Sample ID: SB-2 (4-6)
Matrix: SoilDate Collected: 10/14/16 18:27
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)73 10-120 10/20/16 11:13 10/21/16 17:09 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.95 mg/Kg 10/27/16 14:58 10/31/16 13:55 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.95 mg/Kg 10/27/16 14:58 10/31/16 13:55 12,6-diamino-4-nitrotoluene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 12-Amino-4,6-dinitrotoluene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 14-Amino-2,6-dinitrotoluene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 12,4-Dinitrotoluene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 12,6-Dinitrotoluene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 12,4,6-Trinitrotoluene ND
0.488 mg/Kg 10/27/16 14:58 10/31/16 13:55 1m-Nitrotoluene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 1o-Nitrotoluene ND
0.390 mg/Kg 10/27/16 14:58 10/31/16 13:55 1p-Nitrotoluene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 1NitrobenzeneND
4.98 mg/Kg 10/27/16 14:58 10/31/16 13:55 1NitroglycerinND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 11,3,5-Trinitrobenzene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 11,3-Dinitrobenzene ND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 1HMXND
0.254 mg/Kg 10/27/16 14:58 10/31/16 13:55 1RDXND
0.488 mg/Kg 10/27/16 14:58 10/31/16 13:55 1TetrylND
3.90 mg/Kg 10/27/16 14:58 10/31/16 13:55 1PETNND
0.244 mg/Kg 10/27/16 14:58 10/31/16 13:55 1Picric acid ND
1,2-Dinitrobenzene 103 83-122 10/27/16 14:58 10/31/16 13:55 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <6.08 60.8 6.08 mg/Kg ☼10/20/16 10:21 10/24/16 16:17 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
12.2 7.30 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Arsenic 7.42 J
6.08 1.22 mg/Kg 10/20/16 10:21 10/24/16 19:23 5☼Beryllium <1.22
6.08 0.608 mg/Kg 10/20/16 10:21 10/24/16 19:23 5☼Cadmium 4.86 J
6.08 5.47 mg/Kg 10/20/16 10:21 10/24/16 19:23 5☼Chromium <5.47
12.2 6.69 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Copper <6.69
6.08 3.04 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Lead 4.13 J
18.2 6.08 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Manganese 448
12.2 3.65 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Nickel <3.65
12.2 6.69 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Selenium <6.69
6.08 2.43 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Silver <2.43
12.2 3.65 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Thallium <3.65
60.8 30.4 mg/Kg 10/20/16 10:21 10/24/16 16:17 5☼Zinc 84.0
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.119 mg/Kg ☼10/20/16 11:45 10/21/16 07:56 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 81.4 0.1 %10/18/16 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-9Client Sample ID: SB-3 (8-10)
Matrix: SoilDate Collected: 10/14/16 18:40
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 0.0565 mg/Kg ☼10/14/16 17:40 10/21/16 05:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Benzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Bromobenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Bromochloromethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Bromodichloromethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Bromoform ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Bromomethane ND
0.0565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼2-Butanone (MEK)ND
0.00565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Carbon disulfide ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Carbon tetrachloride ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Chlorobenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Chlorodibromomethane ND
0.00565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Chloroethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Chloroform ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Chloromethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼2-Chlorotoluene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼4-Chlorotoluene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼cis-1,2-Dichloroethene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼cis-1,3-Dichloropropene ND
0.00565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2-Dibromo-3-Chloropropane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2-Dibromoethane (EDB)ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Dibromomethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2-Dichlorobenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,3-Dichlorobenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,4-Dichlorobenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Dichlorodifluoromethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,1-Dichloroethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2-Dichloroethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,1-Dichloroethene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2-Dichloroethene, Total ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2-Dichloropropane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,3-Dichloropropane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼2,2-Dichloropropane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,1-Dichloropropene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Diisopropyl ether ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Ethylbenzene ND
0.00565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Hexachlorobutadiene ND
0.0565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼2-Hexanone ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Isopropylbenzene ND
0.0113 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Methylene Chloride ND
0.0565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼4-Methyl-2-pentanone (MIBK)ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Methyl tert-butyl ether ND
0.00565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Naphthalene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼n-Butylbenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼N-Propylbenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼p-Isopropyltoluene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼sec-Butylbenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Styrene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-9Client Sample ID: SB-3 (8-10)
Matrix: SoilDate Collected: 10/14/16 18:40
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00226 mg/Kg ☼10/14/16 17:40 10/21/16 05:23 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,1,2,2-Tetrachloroethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Tetrachloroethene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Toluene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼trans-1,2-Dichloroethene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼trans-1,3-Dichloropropene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2,3-Trichlorobenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2,4-Trichlorobenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,1,1-Trichloroethane ND
0.00565 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,1,2-Trichloroethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Trichloroethene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Trichlorofluoromethane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2,3-Trichloropropane ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,2,4-Trimethylbenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼1,3,5-Trimethylbenzene ND
0.00226 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Vinyl chloride ND
0.00678 mg/Kg 10/14/16 17:40 10/21/16 05:23 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)99 70-130 10/14/16 17:40 10/21/16 05:23 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)108 10/14/16 17:40 10/21/16 05:23 170-130
1,2-Dichloroethane-d4 (Surr)110 10/14/16 17:40 10/21/16 05:23 170-130
Toluene-d8 (Surr)97 10/14/16 17:40 10/21/16 05:23 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0746 mg/Kg ☼10/20/16 11:13 10/21/16 17:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Acenaphthylene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Anthracene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Benzo[a]anthracene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Benzo[a]pyrene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Benzo[b]fluoranthene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Benzo[g,h,i]perylene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Benzo[k]fluoranthene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Bis(2-chloroethoxy)methane ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Bis(2-chloroethyl)ether ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼bis (2-chloroisopropyl) ether ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Bis(2-ethylhexyl) phthalate ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼4-Bromophenyl phenyl ether ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Butyl benzyl phthalate ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Carbazole ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼4-Chloroaniline ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼4-Chloro-3-methylphenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2-Chloronaphthalene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2-Chlorophenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼4-Chlorophenyl phenyl ether ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Chrysene ND
0.741 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Cresols ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Dibenz(a,h)anthracene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-9Client Sample ID: SB-3 (8-10)
Matrix: SoilDate Collected: 10/14/16 18:40
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.371 mg/Kg ☼10/20/16 11:13 10/21/16 17:28 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼1,3-Dichlorobenzene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼1,4-Dichlorobenzene ND
0.746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼3,3'-Dichlorobenzidine ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2,4-Dichlorophenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Diethyl phthalate ND
0.746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2,4-Dimethylphenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Dimethyl phthalate ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Di-n-butyl phthalate ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼4,6-Dinitro-2-methylphenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2,4-Dinitrophenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2,4-Dinitrotoluene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2,6-Dinitrotoluene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Di-n-octyl phthalate ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Fluoranthene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Fluorene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Hexachlorobenzene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Hexachlorobutadiene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Hexachlorocyclopentadiene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Hexachloroethane ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Indeno[1,2,3-cd]pyrene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Isophorone ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼1-Methylnaphthalene ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2-Methylnaphthalene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2-Methylphenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼3 & 4 Methylphenol ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Naphthalene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2-Nitroaniline ND
0.746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼3-Nitroaniline ND
0.746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼4-Nitroaniline ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Nitrobenzene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2-Nitrophenol ND
0.746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼4-Nitrophenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼N-Nitrosodi-n-propylamine ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Pentachlorophenol ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Phenanthrene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Phenol ND
0.0746 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼Pyrene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼1,2,4-Trichlorobenzene ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2,4,5-Trichlorophenol ND
0.371 mg/Kg 10/20/16 11:13 10/21/16 17:28 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)50 29-120 10/20/16 11:13 10/21/16 17:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)47 10/20/16 11:13 10/21/16 17:28 110-120
Nitrobenzene-d5 (Surr)47 10/20/16 11:13 10/21/16 17:28 127-120
Phenol-d5 (Surr)52 10/20/16 11:13 10/21/16 17:28 110-120
Terphenyl-d14 (Surr)66 10/20/16 11:13 10/21/16 17:28 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-9Client Sample ID: SB-3 (8-10)
Matrix: SoilDate Collected: 10/14/16 18:40
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)61 10-120 10/20/16 11:13 10/21/16 17:28 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.88 mg/Kg 10/27/16 14:58 10/31/16 14:41 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.88 mg/Kg 10/27/16 14:58 10/31/16 14:41 12,6-diamino-4-nitrotoluene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 12-Amino-4,6-dinitrotoluene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 14-Amino-2,6-dinitrotoluene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 12,4-Dinitrotoluene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 12,6-Dinitrotoluene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 12,4,6-Trinitrotoluene ND
0.469 mg/Kg 10/27/16 14:58 10/31/16 14:41 1m-Nitrotoluene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 1o-Nitrotoluene ND
0.376 mg/Kg 10/27/16 14:58 10/31/16 14:41 1p-Nitrotoluene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 1NitrobenzeneND
4.79 mg/Kg 10/27/16 14:58 10/31/16 14:41 1NitroglycerinND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 11,3,5-Trinitrobenzene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 11,3-Dinitrobenzene ND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 1HMXND
0.244 mg/Kg 10/27/16 14:58 10/31/16 14:41 1RDXND
0.469 mg/Kg 10/27/16 14:58 10/31/16 14:41 1TetrylND
3.76 mg/Kg 10/27/16 14:58 10/31/16 14:41 1PETNND
0.235 mg/Kg 10/27/16 14:58 10/31/16 14:41 1Picric acid ND
1,2-Dinitrobenzene 107 83-122 10/27/16 14:58 10/31/16 14:41 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.14 11.4 1.14 mg/Kg ☼10/20/16 10:21 10/21/16 03:19 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.29 1.37 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Arsenic 3.78
1.14 0.229 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Beryllium 1.40
1.14 0.114 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Cadmium 0.709 J
1.14 1.03 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Chromium 6.64
2.29 1.26 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Copper 23.7
1.14 0.572 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Lead 28.2
3.43 1.14 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Manganese 395
2.29 0.686 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Nickel 6.93
2.29 1.26 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Selenium <1.26
1.14 0.458 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Silver <0.458
11.4 3.43 mg/Kg 10/20/16 10:21 10/24/16 16:22 5☼Thallium <3.43
11.4 5.72 mg/Kg 10/20/16 10:21 10/21/16 03:19 1☼Zinc 56.7
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.114 mg/Kg ☼10/20/16 11:45 10/21/16 07:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 87.6 0.1 %10/18/16 15:09 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-10Client Sample ID: SB-10 (2-4)
Matrix: SoilDate Collected: 10/14/16 19:15
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone 0.0631 0.0438 mg/Kg ☼10/14/16 18:15 10/21/16 05:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Benzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Bromobenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Bromochloromethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Bromodichloromethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Bromoform ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Bromomethane ND
0.0438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼2-Butanone (MEK)ND
0.00438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Carbon disulfide ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Carbon tetrachloride ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Chlorobenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Chlorodibromomethane ND
0.00438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Chloroethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Chloroform ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Chloromethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼2-Chlorotoluene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼4-Chlorotoluene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼cis-1,2-Dichloroethene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼cis-1,3-Dichloropropene ND
0.00438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2-Dibromo-3-Chloropropane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2-Dibromoethane (EDB)ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Dibromomethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2-Dichlorobenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,3-Dichlorobenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,4-Dichlorobenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Dichlorodifluoromethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,1-Dichloroethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2-Dichloroethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,1-Dichloroethene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2-Dichloroethene, Total ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2-Dichloropropane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,3-Dichloropropane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼2,2-Dichloropropane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,1-Dichloropropene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Diisopropyl ether ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Ethylbenzene ND
0.00438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Hexachlorobutadiene ND
0.0438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼2-Hexanone ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Isopropylbenzene ND
0.00876 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Methylene Chloride ND
0.0438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼4-Methyl-2-pentanone (MIBK)ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Methyl tert-butyl ether ND
0.00438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Naphthalene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼n-Butylbenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼N-Propylbenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼p-Isopropyltoluene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼sec-Butylbenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Styrene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼tert-Butylbenzene ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-10Client Sample ID: SB-10 (2-4)
Matrix: SoilDate Collected: 10/14/16 19:15
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 0.00175 mg/Kg ☼10/14/16 18:15 10/21/16 05:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,1,2,2-Tetrachloroethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Tetrachloroethene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Toluene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼trans-1,2-Dichloroethene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼trans-1,3-Dichloropropene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2,3-Trichlorobenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2,4-Trichlorobenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,1,1-Trichloroethane ND
0.00438 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,1,2-Trichloroethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Trichloroethene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Trichlorofluoromethane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2,3-Trichloropropane ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,2,4-Trimethylbenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼1,3,5-Trimethylbenzene ND
0.00175 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Vinyl chloride ND
0.00526 mg/Kg 10/14/16 18:15 10/21/16 05:50 1☼Xylenes, Total ND
4-Bromofluorobenzene (Surr)100 70-130 10/14/16 18:15 10/21/16 05:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)110 10/14/16 18:15 10/21/16 05:50 170-130
1,2-Dichloroethane-d4 (Surr)111 10/14/16 18:15 10/21/16 05:50 170-130
Toluene-d8 (Surr)98 10/14/16 18:15 10/21/16 05:50 170-130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene ND 0.0805 mg/Kg ☼10/20/16 11:13 10/21/16 17:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Acenaphthylene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Anthracene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Benzo[a]anthracene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Benzo[a]pyrene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Benzo[b]fluoranthene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Benzo[g,h,i]perylene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Benzo[k]fluoranthene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Bis(2-chloroethoxy)methane ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Bis(2-chloroethyl)ether ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼bis (2-chloroisopropyl) ether ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Bis(2-ethylhexyl) phthalate ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼4-Bromophenyl phenyl ether ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Butyl benzyl phthalate ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Carbazole ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼4-Chloroaniline ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼4-Chloro-3-methylphenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2-Chloronaphthalene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2-Chlorophenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼4-Chlorophenyl phenyl ether ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Chrysene ND
0.800 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Cresols ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Dibenz(a,h)anthracene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Dibenzofuran ND
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-10Client Sample ID: SB-10 (2-4)
Matrix: SoilDate Collected: 10/14/16 19:15
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,2-Dichlorobenzene ND 0.400 mg/Kg ☼10/20/16 11:13 10/21/16 17:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼1,3-Dichlorobenzene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼1,4-Dichlorobenzene ND
0.805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼3,3'-Dichlorobenzidine ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2,4-Dichlorophenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Diethyl phthalate ND
0.805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2,4-Dimethylphenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Dimethyl phthalate ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Di-n-butyl phthalate ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼4,6-Dinitro-2-methylphenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2,4-Dinitrophenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2,4-Dinitrotoluene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2,6-Dinitrotoluene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Di-n-octyl phthalate ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Fluoranthene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Fluorene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Hexachlorobenzene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Hexachlorobutadiene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Hexachlorocyclopentadiene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Hexachloroethane ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Indeno[1,2,3-cd]pyrene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Isophorone ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼1-Methylnaphthalene ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2-Methylnaphthalene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2-Methylphenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼3 & 4 Methylphenol ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Naphthalene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2-Nitroaniline ND
0.805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼3-Nitroaniline ND
0.805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼4-Nitroaniline ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Nitrobenzene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2-Nitrophenol ND
0.805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼4-Nitrophenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼N-Nitrosodi-n-propylamine ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼n-Nitrosodiphenylamine(as
diphenylamine)
ND
0.805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Pentachlorophenol ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Phenanthrene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Phenol ND
0.0805 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼Pyrene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼1,2,4-Trichlorobenzene ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2,4,5-Trichlorophenol ND
0.400 mg/Kg 10/20/16 11:13 10/21/16 17:47 1☼2,4,6-Trichlorophenol ND
2-Fluorobiphenyl (Surr)54 29-120 10/20/16 11:13 10/21/16 17:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
2-Fluorophenol (Surr)50 10/20/16 11:13 10/21/16 17:47 110-120
Nitrobenzene-d5 (Surr)49 10/20/16 11:13 10/21/16 17:47 127-120
Phenol-d5 (Surr)54 10/20/16 11:13 10/21/16 17:47 110-120
Terphenyl-d14 (Surr)77 10/20/16 11:13 10/21/16 17:47 113-120
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-10Client Sample ID: SB-10 (2-4)
Matrix: SoilDate Collected: 10/14/16 19:15
Date Received: 10/18/16 08:50
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
2,4,6-Tribromophenol (Surr)68 10-120 10/20/16 11:13 10/21/16 17:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2,4-diamino-6-nitrotoluene ND 1.85 mg/Kg 10/27/16 14:58 10/31/16 15:04 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.85 mg/Kg 10/27/16 14:58 10/31/16 15:04 12,6-diamino-4-nitrotoluene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 12-Amino-4,6-dinitrotoluene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 14-Amino-2,6-dinitrotoluene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 12,4-Dinitrotoluene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 12,6-Dinitrotoluene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 12,4,6-Trinitrotoluene ND
0.463 mg/Kg 10/27/16 14:58 10/31/16 15:04 1m-Nitrotoluene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 1o-Nitrotoluene ND
0.370 mg/Kg 10/27/16 14:58 10/31/16 15:04 1p-Nitrotoluene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 1NitrobenzeneND
4.72 mg/Kg 10/27/16 14:58 10/31/16 15:04 1NitroglycerinND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 11,3,5-Trinitrobenzene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 11,3-Dinitrobenzene ND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 1HMXND
0.241 mg/Kg 10/27/16 14:58 10/31/16 15:04 1RDXND
0.463 mg/Kg 10/27/16 14:58 10/31/16 15:04 1TetrylND
3.70 mg/Kg 10/27/16 14:58 10/31/16 15:04 1PETNND
0.231 mg/Kg 10/27/16 14:58 10/31/16 15:04 1Picric acid ND
1,2-Dinitrobenzene 104 83-122 10/27/16 14:58 10/31/16 15:04 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Method: 6010D - Metals (ICP)
RL MDL
Antimony <1.20 12.0 1.20 mg/Kg ☼10/20/16 10:21 10/21/16 03:24 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
2.40 1.44 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Arsenic 4.98
1.20 0.240 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Beryllium 0.815 J
1.20 0.120 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Cadmium 0.886 J
1.20 1.08 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Chromium 10.7
2.40 1.32 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Copper 17.4
1.20 0.599 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Lead 34.2
3.59 1.20 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Manganese 309
2.40 0.719 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Nickel 12.4
2.40 1.32 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Selenium <1.32
1.20 0.479 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Silver <0.479
12.0 3.59 mg/Kg 10/20/16 10:21 10/24/16 16:27 5☼Thallium <3.59
12.0 5.99 mg/Kg 10/20/16 10:21 10/21/16 03:24 1☼Zinc 54.9
Method: 7471B - Mercury (CVAA)
RL MDL
Mercury ND 0.123 mg/Kg ☼10/20/16 13:47 10/21/16 08:45 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
General Chemistry
RL RL
Percent Solids 81.4 0.1 %10/18/16 14:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-11Client Sample ID: TMW-2
Matrix: WaterDate Collected: 10/17/16 14:20
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS)
RL MDL
Acetone ND 25.0 ug/L 10/23/16 03:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/23/16 03:05 1BenzeneND
1.00 ug/L 10/23/16 03:05 1BromobenzeneND
1.00 ug/L 10/23/16 03:05 1BromochloromethaneND
1.00 ug/L 10/23/16 03:05 1BromodichloromethaneND
1.00 ug/L 10/23/16 03:05 1BromoformND
1.00 ug/L 10/23/16 03:05 1BromomethaneND
50.0 ug/L 10/23/16 03:05 12-Butanone (MEK)ND
1.00 ug/L 10/23/16 03:05 1Carbon disulfide ND
1.00 ug/L 10/23/16 03:05 1Carbon tetrachloride ND
1.00 ug/L 10/23/16 03:05 1ChlorobenzeneND
1.00 ug/L 10/23/16 03:05 1ChlorodibromomethaneND
1.00 ug/L 10/23/16 03:05 1ChloroethaneND
1.00 ug/L 10/23/16 03:05 1ChloroformND
1.00 ug/L 10/23/16 03:05 1ChloromethaneND
1.00 ug/L 10/23/16 03:05 12-Chlorotoluene ND
1.00 ug/L 10/23/16 03:05 14-Chlorotoluene ND
1.00 ug/L 10/23/16 03:05 1cis-1,2-Dichloroethene ND
1.00 ug/L 10/23/16 03:05 1cis-1,3-Dichloropropene ND
10.0 ug/L 10/23/16 03:05 11,2-Dibromo-3-Chloropropane ND
1.00 ug/L 10/23/16 03:05 11,2-Dibromoethane (EDB)ND
1.00 ug/L 10/23/16 03:05 1DibromomethaneND
1.00 ug/L 10/23/16 03:05 11,2-Dichlorobenzene ND
1.00 ug/L 10/23/16 03:05 11,3-Dichlorobenzene ND
1.00 ug/L 10/23/16 03:05 11,4-Dichlorobenzene ND
1.00 ug/L 10/23/16 03:05 1DichlorodifluoromethaneND
1.00 ug/L 10/23/16 03:05 11,1-Dichloroethane 2.79
1.00 ug/L 10/23/16 03:05 11,2-Dichloroethane ND
1.00 ug/L 10/23/16 03:05 11,1-Dichloroethene ND
1.00 ug/L 10/23/16 03:05 11,2-Dichloroethene, Total ND
1.00 ug/L 10/23/16 03:05 11,2-Dichloropropane ND
1.00 ug/L 10/23/16 03:05 11,3-Dichloropropane ND
1.00 ug/L 10/23/16 03:05 12,2-Dichloropropane ND
1.00 ug/L 10/23/16 03:05 11,1-Dichloropropene ND
2.00 ug/L 10/23/16 03:05 1Diisopropyl ether ND
1.00 ug/L 10/23/16 03:05 1EthylbenzeneND
2.00 ug/L 10/23/16 03:05 1HexachlorobutadieneND
10.0 ug/L 10/23/16 03:05 12-Hexanone ND
1.00 ug/L 10/23/16 03:05 1IsopropylbenzeneND
5.00 ug/L 10/23/16 03:05 1Methylene Chloride ND
10.0 ug/L 10/23/16 03:05 14-Methyl-2-pentanone (MIBK)ND
1.00 ug/L 10/23/16 03:05 1Methyl tert-butyl ether ND
5.00 ug/L 10/23/16 03:05 1NaphthaleneND
1.00 ug/L 10/23/16 03:05 1n-Butylbenzene ND
1.00 ug/L 10/23/16 03:05 1N-Propylbenzene ND
1.00 ug/L 10/23/16 03:05 1p-Isopropyltoluene ND
1.00 ug/L 10/23/16 03:05 1sec-Butylbenzene ND
1.00 ug/L 10/23/16 03:05 1StyreneND
1.00 ug/L 10/23/16 03:05 1tert-Butylbenzene ND
TestAmerica Nashville
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Client Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Lab Sample ID: 490-114207-11Client Sample ID: TMW-2
Matrix: WaterDate Collected: 10/17/16 14:20
Date Received: 10/18/16 08:50
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
RL MDL
1,1,1,2-Tetrachloroethane ND 1.00 ug/L 10/23/16 03:05 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 ug/L 10/23/16 03:05 11,1,2,2-Tetrachloroethane ND
1.00 ug/L 10/23/16 03:05 1TetrachloroetheneND
1.00 ug/L 10/23/16 03:05 1TolueneND
1.00 ug/L 10/23/16 03:05 1trans-1,2-Dichloroethene ND
1.00 ug/L 10/23/16 03:05 1trans-1,3-Dichloropropene ND
1.00 ug/L 10/23/16 03:05 11,2,3-Trichlorobenzene ND
1.00 ug/L 10/23/16 03:05 11,2,4-Trichlorobenzene ND
1.00 ug/L 10/23/16 03:05 11,1,1-Trichloroethane ND
1.00 ug/L 10/23/16 03:05 11,1,2-Trichloroethane ND
1.00 ug/L 10/23/16 03:05 1TrichloroetheneND
1.00 ug/L 10/23/16 03:05 1TrichlorofluoromethaneND
1.00 ug/L 10/23/16 03:05 11,2,3-Trichloropropane ND
1.00 ug/L 10/23/16 03:05 11,2,4-Trimethylbenzene ND
1.00 ug/L 10/23/16 03:05 11,3,5-Trimethylbenzene ND
1.00 ug/L 10/23/16 03:05 1Vinyl chloride ND
3.00 ug/L 10/23/16 03:05 1Xylenes, Total ND
4-Bromofluorobenzene (Surr)105 70-130 10/23/16 03:05 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane (Surr)101 10/23/16 03:05 170-130
1,2-Dichloroethane-d4 (Surr)115 10/23/16 03:05 170-130
Toluene-d8 (Surr)102 10/23/16 03:05 170-130
Method: 8330A - Nitroaromatics and Nitramines
RL MDL
2-Amino-4,6-dinitrotoluene ND 0.225 ug/L 10/21/16 16:35 10/25/16 10:59 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.225 ug/L 10/21/16 16:35 10/25/16 12:56 14-Amino-2,6-dinitrotoluene ND
1.12 ug/L 10/21/16 16:35 10/25/16 10:59 12,4-diamino-6-nitrotoluene ND
1.12 ug/L 10/21/16 16:35 10/25/16 10:59 12,6-diamino-4-nitrotoluene ND
0.450 ug/L 10/21/16 16:35 10/25/16 10:59 11,3-Dinitrobenzene ND
0.450 ug/L 10/21/16 16:35 10/25/16 10:59 12,4-Dinitrotoluene ND
0.225 ug/L 10/21/16 16:35 10/25/16 10:59 12,6-Dinitrotoluene ND
0.450 ug/L 10/21/16 16:35 10/25/16 10:59 1HMXND
0.450 ug/L 10/21/16 16:35 10/25/16 10:59 1m-Nitrotoluene ND
0.450 ug/L 10/21/16 16:35 10/25/16 10:59 1NitrobenzeneND
3.37 ug/L 10/21/16 16:35 10/25/16 10:59 1NitroglycerinND
0.450 ug/L 10/21/16 16:35 10/25/16 10:59 1o-Nitrotoluene ND
2.25 ug/L 10/21/16 16:35 10/25/16 10:59 1PETNND
2.25 ug/L 10/21/16 16:35 10/25/16 12:56 1Picric acid ND
1.12 ug/L 10/21/16 16:35 10/25/16 10:59 1p-Nitrotoluene ND
0.225 ug/L 10/21/16 16:35 10/25/16 12:56 1RDXND
0.225 ug/L 10/21/16 16:35 10/25/16 10:59 1TetrylND
1.12 ug/L 10/21/16 16:35 10/25/16 10:59 11,3,5-Trinitrobenzene ND
0.450 ug/L 10/21/16 16:35 10/25/16 10:59 12,4,6-Trinitrotoluene ND
1,2-Dinitrobenzene 84 75-118 10/21/16 16:35 10/25/16 10:59 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-380000/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380000
RL MDL
Acetone ND 0.0500 mg/Kg 10/21/16 01:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 10/21/16 01:16 1Benzene
ND 0.00200 mg/Kg 10/21/16 01:16 1Bromobenzene
ND 0.00200 mg/Kg 10/21/16 01:16 1Bromochloromethane
ND 0.00200 mg/Kg 10/21/16 01:16 1Bromodichloromethane
ND 0.00200 mg/Kg 10/21/16 01:16 1Bromoform
ND 0.00200 mg/Kg 10/21/16 01:16 1Bromomethane
ND 0.0500 mg/Kg 10/21/16 01:16 12-Butanone (MEK)
ND 0.00500 mg/Kg 10/21/16 01:16 1Carbon disulfide
ND 0.00200 mg/Kg 10/21/16 01:16 1Carbon tetrachloride
ND 0.00200 mg/Kg 10/21/16 01:16 1Chlorobenzene
ND 0.00200 mg/Kg 10/21/16 01:16 1Chlorodibromomethane
ND 0.00500 mg/Kg 10/21/16 01:16 1Chloroethane
ND 0.00200 mg/Kg 10/21/16 01:16 1Chloroform
ND 0.00200 mg/Kg 10/21/16 01:16 1Chloromethane
ND 0.00200 mg/Kg 10/21/16 01:16 12-Chlorotoluene
ND 0.00200 mg/Kg 10/21/16 01:16 14-Chlorotoluene
ND 0.00200 mg/Kg 10/21/16 01:16 1cis-1,2-Dichloroethene
ND 0.00200 mg/Kg 10/21/16 01:16 1cis-1,3-Dichloropropene
ND 0.00500 mg/Kg 10/21/16 01:16 11,2-Dibromo-3-Chloropropane
ND 0.00200 mg/Kg 10/21/16 01:16 11,2-Dibromoethane (EDB)
ND 0.00200 mg/Kg 10/21/16 01:16 1Dibromomethane
ND 0.00200 mg/Kg 10/21/16 01:16 11,2-Dichlorobenzene
ND 0.00200 mg/Kg 10/21/16 01:16 11,3-Dichlorobenzene
ND 0.00200 mg/Kg 10/21/16 01:16 11,4-Dichlorobenzene
ND 0.00200 mg/Kg 10/21/16 01:16 1Dichlorodifluoromethane
ND 0.00200 mg/Kg 10/21/16 01:16 11,1-Dichloroethane
ND 0.00200 mg/Kg 10/21/16 01:16 11,2-Dichloroethane
ND 0.00200 mg/Kg 10/21/16 01:16 11,1-Dichloroethene
ND 0.00200 mg/Kg 10/21/16 01:16 11,2-Dichloroethene, Total
ND 0.00200 mg/Kg 10/21/16 01:16 11,2-Dichloropropane
ND 0.00200 mg/Kg 10/21/16 01:16 11,3-Dichloropropane
ND 0.00200 mg/Kg 10/21/16 01:16 12,2-Dichloropropane
ND 0.00200 mg/Kg 10/21/16 01:16 11,1-Dichloropropene
ND 0.00200 mg/Kg 10/21/16 01:16 1Diisopropyl ether
ND 0.00200 mg/Kg 10/21/16 01:16 1Ethylbenzene
ND 0.00500 mg/Kg 10/21/16 01:16 1Hexachlorobutadiene
ND 0.0500 mg/Kg 10/21/16 01:16 12-Hexanone
ND 0.00200 mg/Kg 10/21/16 01:16 1Isopropylbenzene
ND 0.0100 mg/Kg 10/21/16 01:16 1Methylene Chloride
ND 0.0500 mg/Kg 10/21/16 01:16 14-Methyl-2-pentanone (MIBK)
ND 0.00200 mg/Kg 10/21/16 01:16 1Methyl tert-butyl ether
ND 0.00500 mg/Kg 10/21/16 01:16 1Naphthalene
ND 0.00200 mg/Kg 10/21/16 01:16 1n-Butylbenzene
ND 0.00200 mg/Kg 10/21/16 01:16 1N-Propylbenzene
ND 0.00200 mg/Kg 10/21/16 01:16 1p-Isopropyltoluene
ND 0.00200 mg/Kg 10/21/16 01:16 1sec-Butylbenzene
ND 0.00200 mg/Kg 10/21/16 01:16 1Styrene
TestAmerica Nashville
Page 50 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-380000/7
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380000
RL MDL
tert-Butylbenzene ND 0.00200 mg/Kg 10/21/16 01:16 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.00200 mg/Kg 10/21/16 01:16 11,1,1,2-Tetrachloroethane
ND 0.00200 mg/Kg 10/21/16 01:16 11,1,2,2-Tetrachloroethane
ND 0.00200 mg/Kg 10/21/16 01:16 1Tetrachloroethene
ND 0.00200 mg/Kg 10/21/16 01:16 1Toluene
ND 0.00200 mg/Kg 10/21/16 01:16 1trans-1,2-Dichloroethene
ND 0.00200 mg/Kg 10/21/16 01:16 1trans-1,3-Dichloropropene
ND 0.00200 mg/Kg 10/21/16 01:16 11,2,3-Trichlorobenzene
ND 0.00200 mg/Kg 10/21/16 01:16 11,2,4-Trichlorobenzene
ND 0.00200 mg/Kg 10/21/16 01:16 11,1,1-Trichloroethane
ND 0.00500 mg/Kg 10/21/16 01:16 11,1,2-Trichloroethane
ND 0.00200 mg/Kg 10/21/16 01:16 1Trichloroethene
ND 0.00200 mg/Kg 10/21/16 01:16 1Trichlorofluoromethane
ND 0.00200 mg/Kg 10/21/16 01:16 11,2,3-Trichloropropane
ND 0.00200 mg/Kg 10/21/16 01:16 11,2,4-Trimethylbenzene
ND 0.00200 mg/Kg 10/21/16 01:16 11,3,5-Trimethylbenzene
ND 0.00200 mg/Kg 10/21/16 01:16 1Vinyl chloride
ND 0.00600 mg/Kg 10/21/16 01:16 1Xylenes, Total
4-Bromofluorobenzene (Surr)96 70-130 10/21/16 01:16 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
108 10/21/16 01:16 1Dibromofluoromethane (Surr)70-130
106 10/21/16 01:16 11,2-Dichloroethane-d4 (Surr)70-130
98 10/21/16 01:16 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380000/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380000
Acetone 0.250 0.2048 mg/Kg 82 45-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 0.0500 0.04804 mg/Kg 96 70-130
Bromobenzene 0.0500 0.03989 mg/Kg 80 67-130
Bromochloromethane 0.0500 0.05343 mg/Kg 107 70-133
Bromodichloromethane 0.0500 0.04779 mg/Kg 96 70-130
Bromoform 0.0500 0.04780 mg/Kg 96 59-137
Bromomethane 0.0500 0.03728 mg/Kg 75 32-150
2-Butanone (MEK)0.250 0.2233 mg/Kg 89 50-149
Carbon disulfide 0.0500 0.04455 mg/Kg 89 66-138
Carbon tetrachloride 0.0500 0.05358 mg/Kg 107 70-131
Chlorobenzene 0.0500 0.04814 mg/Kg 96 70-130
Chlorodibromomethane 0.0500 0.04636 mg/Kg 93 70-130
Chloroethane 0.0500 0.04369 mg/Kg 87 37-150
Chloroform 0.0500 0.04947 mg/Kg 99 70-130
Chloromethane 0.0500 0.03482 mg/Kg 70 53-150
2-Chlorotoluene 0.0500 0.04471 mg/Kg 89 70-132
4-Chlorotoluene 0.0500 0.04361 mg/Kg 87 67-135
cis-1,2-Dichloroethene 0.0500 0.05011 mg/Kg 100 70-132
TestAmerica Nashville
Page 51 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380000/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380000
cis-1,3-Dichloropropene 0.0500 0.04528 mg/Kg 91 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dibromo-3-Chloropropane 0.0500 0.04430 mg/Kg 89 47-144
1,2-Dibromoethane (EDB)0.0500 0.04695 mg/Kg 94 69-130
Dibromomethane 0.0500 0.05125 mg/Kg 103 70-130
1,2-Dichlorobenzene 0.0500 0.04873 mg/Kg 97 70-134
1,3-Dichlorobenzene 0.0500 0.04832 mg/Kg 97 69-137
1,4-Dichlorobenzene 0.0500 0.04699 mg/Kg 94 66-134
Dichlorodifluoromethane 0.0500 0.05453 mg/Kg 109 32-150
1,1-Dichloroethane 0.0500 0.04501 mg/Kg 90 70-130
1,2-Dichloroethane 0.0500 0.05006 mg/Kg 100 65-134
1,1-Dichloroethene 0.0500 0.04873 mg/Kg 97 70-131
1,2-Dichloroethene, Total 0.100 0.09676 mg/Kg 97 70-130
1,2-Dichloropropane 0.0500 0.04524 mg/Kg 90 70-130
1,3-Dichloropropane 0.0500 0.04389 mg/Kg 88 70-130
2,2-Dichloropropane 0.0500 0.05209 mg/Kg 104 57-150
1,1-Dichloropropene 0.0500 0.04783 mg/Kg 96 70-130
Diisopropyl ether 0.0500 0.04302 mg/Kg 86 68-134
Ethylbenzene 0.0500 0.04833 mg/Kg 97 70-130
Hexachlorobutadiene 0.0500 0.05308 mg/Kg 106 64-137
2-Hexanone 0.250 0.1967 mg/Kg 79 47-148
Isopropylbenzene 0.0500 0.05099 mg/Kg 102 70-130
Methylene Chloride 0.0500 0.04821 mg/Kg 96 69-130
4-Methyl-2-pentanone (MIBK)0.250 0.1990 mg/Kg 80 48-150
Methyl tert-butyl ether 0.0500 0.04921 mg/Kg 98 54-145
Naphthalene 0.0500 0.04679 mg/Kg 94 55-149
n-Butylbenzene 0.0500 0.04503 mg/Kg 90 57-150
N-Propylbenzene 0.0500 0.04419 mg/Kg 88 62-150
p-Isopropyltoluene 0.0500 0.04838 mg/Kg 97 66-147
sec-Butylbenzene 0.0500 0.04912 mg/Kg 98 68-147
Styrene 0.0500 0.04740 mg/Kg 95 70-131
tert-Butylbenzene 0.0500 0.05007 mg/Kg 100 70-138
1,1,1,2-Tetrachloroethane 0.0500 0.04767 mg/Kg 95 70-130
1,1,2,2-Tetrachloroethane 0.0500 0.03859 mg/Kg 77 61-134
Tetrachloroethene 0.0500 0.05118 mg/Kg 102 70-130
Toluene 0.0500 0.04766 mg/Kg 95 70-130
trans-1,2-Dichloroethene 0.0500 0.04665 mg/Kg 93 70-130
trans-1,3-Dichloropropene 0.0500 0.04564 mg/Kg 91 67-130
1,2,3-Trichlorobenzene 0.0500 0.04861 mg/Kg 97 57-146
1,2,4-Trichlorobenzene 0.0500 0.04773 mg/Kg 95 47-150
1,1,1-Trichloroethane 0.0500 0.05290 mg/Kg 106 70-130
1,1,2-Trichloroethane 0.0500 0.04505 mg/Kg 90 70-130
Trichloroethene 0.0500 0.05324 mg/Kg 106 70-130
Trichlorofluoromethane 0.0500 0.04907 mg/Kg 98 53-150
1,2,3-Trichloropropane 0.0500 0.04349 mg/Kg 87 60-139
1,2,4-Trimethylbenzene 0.0500 0.04990 mg/Kg 100 70-140
1,3,5-Trimethylbenzene 0.0500 0.04641 mg/Kg 93 69-141
Vinyl chloride 0.0500 0.04413 mg/Kg 88 63-150
Xylenes, Total 0.100 0.09892 mg/Kg 99 70-130
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380000/4
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380000
4-Bromofluorobenzene (Surr)70 -130
Surrogate
95
LCS LCS
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)70 -130
1021,2-Dichloroethane-d4 (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380000/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380000
Acetone 0.250 0.2232 mg/Kg 89 45-145 9 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 0.0500 0.04924 mg/Kg 98 70-130 2 37
Bromobenzene 0.0500 0.04173 mg/Kg 83 67-130 5 40
Bromochloromethane 0.0500 0.05380 mg/Kg 108 70-133 1 15
Bromodichloromethane 0.0500 0.04887 mg/Kg 98 70-130 2 20
Bromoform 0.0500 0.04955 mg/Kg 99 59-137 4 17
Bromomethane 0.0500 0.03857 mg/Kg 77 32-150 3 45
2-Butanone (MEK)0.250 0.2354 mg/Kg 94 50-149 5 39
Carbon disulfide 0.0500 0.04530 mg/Kg 91 66-138 2 41
Carbon tetrachloride 0.0500 0.05554 mg/Kg 111 70-131 4 41
Chlorobenzene 0.0500 0.04972 mg/Kg 99 70-130 3 40
Chlorodibromomethane 0.0500 0.04738 mg/Kg 95 70-130 2 14
Chloroethane 0.0500 0.04425 mg/Kg 88 37-150 1 50
Chloroform 0.0500 0.05069 mg/Kg 101 70-130 2 15
Chloromethane 0.0500 0.03593 mg/Kg 72 53-150 3 47
2-Chlorotoluene 0.0500 0.04602 mg/Kg 92 70-132 3 41
4-Chlorotoluene 0.0500 0.04489 mg/Kg 90 67-135 3 41
cis-1,2-Dichloroethene 0.0500 0.05001 mg/Kg 100 70-132 0 18
cis-1,3-Dichloropropene 0.0500 0.04557 mg/Kg 91 70-130 1 42
1,2-Dibromo-3-Chloropropane 0.0500 0.04769 mg/Kg 95 47-144 7 38
1,2-Dibromoethane (EDB)0.0500 0.04801 mg/Kg 96 69-130 2 17
Dibromomethane 0.0500 0.05306 mg/Kg 106 70-130 3 19
1,2-Dichlorobenzene 0.0500 0.04953 mg/Kg 99 70-134 2 40
1,3-Dichlorobenzene 0.0500 0.04959 mg/Kg 99 69-137 3 41
1,4-Dichlorobenzene 0.0500 0.04886 mg/Kg 98 66-134 4 41
Dichlorodifluoromethane 0.0500 0.05655 mg/Kg 113 32-150 4 50
1,1-Dichloroethane 0.0500 0.04619 mg/Kg 92 70-130 3 42
1,2-Dichloroethane 0.0500 0.05128 mg/Kg 103 65-134 2 16
1,1-Dichloroethene 0.0500 0.04941 mg/Kg 99 70-131 1 43
1,2-Dichloroethene, Total 0.100 0.09798 mg/Kg 98 70-130 1 41
1,2-Dichloropropane 0.0500 0.04638 mg/Kg 93 70-130 2 15
1,3-Dichloropropane 0.0500 0.04532 mg/Kg 91 70-130 3 15
2,2-Dichloropropane 0.0500 0.05294 mg/Kg 106 57-150 2 42
1,1-Dichloropropene 0.0500 0.04867 mg/Kg 97 70-130 2 41
Diisopropyl ether 0.0500 0.04384 mg/Kg 88 68-134 2 36
Ethylbenzene 0.0500 0.04971 mg/Kg 99 70-130 3 38
Hexachlorobutadiene 0.0500 0.05715 mg/Kg 114 64-137 7 44
2-Hexanone 0.250 0.2047 mg/Kg 82 47-148 4 38
TestAmerica Nashville
Page 53 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380000/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380000
Isopropylbenzene 0.0500 0.05285 mg/Kg 106 70-130 4 39
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Methylene Chloride 0.0500 0.04914 mg/Kg 98 69-130 2 19
4-Methyl-2-pentanone (MIBK)0.250 0.2073 mg/Kg 83 48-150 4 41
Methyl tert-butyl ether 0.0500 0.05034 mg/Kg 101 54-145 2 36
Naphthalene 0.0500 0.04912 mg/Kg 98 55-149 5 37
n-Butylbenzene 0.0500 0.04647 mg/Kg 93 57-150 3 39
N-Propylbenzene 0.0500 0.04569 mg/Kg 91 62-150 3 38
p-Isopropyltoluene 0.0500 0.05028 mg/Kg 101 66-147 4 38
sec-Butylbenzene 0.0500 0.05103 mg/Kg 102 68-147 4 38
Styrene 0.0500 0.04833 mg/Kg 97 70-131 2 40
tert-Butylbenzene 0.0500 0.05235 mg/Kg 105 70-138 4 38
1,1,1,2-Tetrachloroethane 0.0500 0.04908 mg/Kg 98 70-130 3 41
1,1,2,2-Tetrachloroethane 0.0500 0.04031 mg/Kg 81 61-134 4 16
Tetrachloroethene 0.0500 0.05277 mg/Kg 106 70-130 3 41
Toluene 0.0500 0.04875 mg/Kg 98 70-130 2 40
trans-1,2-Dichloroethene 0.0500 0.04797 mg/Kg 96 70-130 3 41
trans-1,3-Dichloropropene 0.0500 0.04618 mg/Kg 92 67-130 1 41
1,2,3-Trichlorobenzene 0.0500 0.05008 mg/Kg 100 57-146 3 42
1,2,4-Trichlorobenzene 0.0500 0.04888 mg/Kg 98 47-150 2 43
1,1,1-Trichloroethane 0.0500 0.05443 mg/Kg 109 70-130 3 41
1,1,2-Trichloroethane 0.0500 0.04687 mg/Kg 94 70-130 4 17
Trichloroethene 0.0500 0.05385 mg/Kg 108 70-130 1 41
Trichlorofluoromethane 0.0500 0.05050 mg/Kg 101 53-150 3 49
1,2,3-Trichloropropane 0.0500 0.04393 mg/Kg 88 60-139 1 16
1,2,4-Trimethylbenzene 0.0500 0.05153 mg/Kg 103 70-140 3 38
1,3,5-Trimethylbenzene 0.0500 0.04829 mg/Kg 97 69-141 4 38
Vinyl chloride 0.0500 0.04636 mg/Kg 93 63-150 5 46
Xylenes, Total 0.100 0.1013 mg/Kg 101 70-130 2 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
96
LCSD LCSD
Qualifier Limits%Recovery
106Dibromofluoromethane (Surr)70 -130
1001,2-Dichloroethane-d4 (Surr)70 -130
98Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-380458/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
RL MDL
Acetone ND 25.0 ug/L 10/23/16 01:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 10/23/16 01:44 1Benzene
ND 1.00 ug/L 10/23/16 01:44 1Bromobenzene
ND 1.00 ug/L 10/23/16 01:44 1Bromochloromethane
ND 1.00 ug/L 10/23/16 01:44 1Bromodichloromethane
ND 1.00 ug/L 10/23/16 01:44 1Bromoform
ND 1.00 ug/L 10/23/16 01:44 1Bromomethane
ND 50.0 ug/L 10/23/16 01:44 12-Butanone (MEK)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-380458/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
RL MDL
Carbon disulfide ND 1.00 ug/L 10/23/16 01:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 10/23/16 01:44 1Carbon tetrachloride
ND 1.00 ug/L 10/23/16 01:44 1Chlorobenzene
ND 1.00 ug/L 10/23/16 01:44 1Chlorodibromomethane
ND 1.00 ug/L 10/23/16 01:44 1Chloroethane
ND 1.00 ug/L 10/23/16 01:44 1Chloroform
ND 1.00 ug/L 10/23/16 01:44 1Chloromethane
ND 1.00 ug/L 10/23/16 01:44 12-Chlorotoluene
ND 1.00 ug/L 10/23/16 01:44 14-Chlorotoluene
ND 1.00 ug/L 10/23/16 01:44 1cis-1,2-Dichloroethene
ND 1.00 ug/L 10/23/16 01:44 1cis-1,3-Dichloropropene
ND 10.0 ug/L 10/23/16 01:44 11,2-Dibromo-3-Chloropropane
ND 1.00 ug/L 10/23/16 01:44 11,2-Dibromoethane (EDB)
ND 1.00 ug/L 10/23/16 01:44 1Dibromomethane
ND 1.00 ug/L 10/23/16 01:44 11,2-Dichlorobenzene
ND 1.00 ug/L 10/23/16 01:44 11,3-Dichlorobenzene
ND 1.00 ug/L 10/23/16 01:44 11,4-Dichlorobenzene
ND 1.00 ug/L 10/23/16 01:44 1Dichlorodifluoromethane
ND 1.00 ug/L 10/23/16 01:44 11,1-Dichloroethane
ND 1.00 ug/L 10/23/16 01:44 11,2-Dichloroethane
ND 1.00 ug/L 10/23/16 01:44 11,1-Dichloroethene
ND 1.00 ug/L 10/23/16 01:44 11,2-Dichloroethene, Total
ND 1.00 ug/L 10/23/16 01:44 11,2-Dichloropropane
ND 1.00 ug/L 10/23/16 01:44 11,3-Dichloropropane
ND 1.00 ug/L 10/23/16 01:44 12,2-Dichloropropane
ND 1.00 ug/L 10/23/16 01:44 11,1-Dichloropropene
ND 2.00 ug/L 10/23/16 01:44 1Diisopropyl ether
ND 1.00 ug/L 10/23/16 01:44 1Ethylbenzene
ND 2.00 ug/L 10/23/16 01:44 1Hexachlorobutadiene
ND 10.0 ug/L 10/23/16 01:44 12-Hexanone
ND 1.00 ug/L 10/23/16 01:44 1Isopropylbenzene
ND 5.00 ug/L 10/23/16 01:44 1Methylene Chloride
ND 10.0 ug/L 10/23/16 01:44 14-Methyl-2-pentanone (MIBK)
ND 1.00 ug/L 10/23/16 01:44 1Methyl tert-butyl ether
ND 5.00 ug/L 10/23/16 01:44 1Naphthalene
ND 1.00 ug/L 10/23/16 01:44 1n-Butylbenzene
ND 1.00 ug/L 10/23/16 01:44 1N-Propylbenzene
ND 1.00 ug/L 10/23/16 01:44 1p-Isopropyltoluene
ND 1.00 ug/L 10/23/16 01:44 1sec-Butylbenzene
ND 1.00 ug/L 10/23/16 01:44 1Styrene
ND 1.00 ug/L 10/23/16 01:44 1tert-Butylbenzene
ND 1.00 ug/L 10/23/16 01:44 11,1,1,2-Tetrachloroethane
ND 1.00 ug/L 10/23/16 01:44 11,1,2,2-Tetrachloroethane
ND 1.00 ug/L 10/23/16 01:44 1Tetrachloroethene
ND 1.00 ug/L 10/23/16 01:44 1Toluene
ND 1.00 ug/L 10/23/16 01:44 1trans-1,2-Dichloroethene
ND 1.00 ug/L 10/23/16 01:44 1trans-1,3-Dichloropropene
ND 1.00 ug/L 10/23/16 01:44 11,2,3-Trichlorobenzene
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-380458/8
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
RL MDL
1,2,4-Trichlorobenzene ND 1.00 ug/L 10/23/16 01:44 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 1.00 ug/L 10/23/16 01:44 11,1,1-Trichloroethane
ND 1.00 ug/L 10/23/16 01:44 11,1,2-Trichloroethane
ND 1.00 ug/L 10/23/16 01:44 1Trichloroethene
ND 1.00 ug/L 10/23/16 01:44 1Trichlorofluoromethane
ND 1.00 ug/L 10/23/16 01:44 11,2,3-Trichloropropane
ND 1.00 ug/L 10/23/16 01:44 11,2,4-Trimethylbenzene
ND 1.00 ug/L 10/23/16 01:44 11,3,5-Trimethylbenzene
ND 1.00 ug/L 10/23/16 01:44 1Vinyl chloride
ND 3.00 ug/L 10/23/16 01:44 1Xylenes, Total
4-Bromofluorobenzene (Surr)108 70-130 10/23/16 01:44 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
99 10/23/16 01:44 1Dibromofluoromethane (Surr)70-130
112 10/23/16 01:44 11,2-Dichloroethane-d4 (Surr)70-130
106 10/23/16 01:44 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380458/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
Acetone 100 115.4 ug/L 115 39-150
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 20.0 19.65 ug/L 98 70-130
Bromobenzene 20.0 19.64 ug/L 98 70-130
Bromochloromethane 20.0 18.88 ug/L 94 70-130
Bromodichloromethane 20.0 20.51 ug/L 103 70-130
Bromoform 20.0 17.11 ug/L 86 70-137
Bromomethane 20.0 26.92 ug/L 135 53-150
2-Butanone (MEK)100 93.64 ug/L 94 55-143
Carbon disulfide 20.0 20.47 ug/L 102 64-135
Carbon tetrachloride 20.0 21.24 ug/L 106 70-147
Chlorobenzene 20.0 19.30 ug/L 96 70-130
Chlorodibromomethane 20.0 18.33 ug/L 92 70-133
Chloroethane 20.0 21.26 ug/L 106 60-138
Chloroform 20.0 21.82 ug/L 109 70-130
Chloromethane 20.0 21.91 ug/L 110 33-150
2-Chlorotoluene 20.0 20.63 ug/L 103 70-130
4-Chlorotoluene 20.0 20.86 ug/L 104 70-130
cis-1,2-Dichloroethene 20.0 20.15 ug/L 101 70-130
cis-1,3-Dichloropropene 20.0 19.85 ug/L 99 70-133
1,2-Dibromo-3-Chloropropane 20.0 14.57 ug/L 73 45-138
1,2-Dibromoethane (EDB)20.0 19.21 ug/L 96 70-130
Dibromomethane 20.0 18.83 ug/L 94 70-130
1,2-Dichlorobenzene 20.0 20.52 ug/L 103 70-130
1,3-Dichlorobenzene 20.0 20.53 ug/L 103 70-130
1,4-Dichlorobenzene 20.0 19.90 ug/L 99 70-130
Dichlorodifluoromethane 20.0 23.88 ug/L 119 48-150
TestAmerica Nashville
Page 56 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380458/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
1,1-Dichloroethane 20.0 21.91 ug/L 110 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 20.0 22.17 ug/L 111 70-130
1,1-Dichloroethene 20.0 20.62 ug/L 103 70-132
1,2-Dichloroethene, Total 40.0 41.51 ug/L 104 70-130
1,2-Dichloropropane 20.0 18.97 ug/L 95 70-130
1,3-Dichloropropane 20.0 20.27 ug/L 101 70-130
2,2-Dichloropropane 20.0 18.74 ug/L 94 60-143
1,1-Dichloropropene 20.0 21.43 ug/L 107 70-130
Diisopropyl ether 20.0 19.28 ug/L 96 66-142
Ethylbenzene 20.0 20.21 ug/L 101 70-130
Hexachlorobutadiene 20.0 20.59 ug/L 103 70-138
2-Hexanone 100 93.39 ug/L 93 54-142
Isopropylbenzene 20.0 19.57 ug/L 98 70-131
Methylene Chloride 20.0 20.00 ug/L 100 70-130
4-Methyl-2-pentanone (MIBK)100 94.33 ug/L 94 60-137
Methyl tert-butyl ether 20.0 18.92 ug/L 95 70-130
Naphthalene 20.0 19.08 ug/L 95 54-150
n-Butylbenzene 20.0 20.65 ug/L 103 68-137
N-Propylbenzene 20.0 20.59 ug/L 103 70-134
p-Isopropyltoluene 20.0 20.61 ug/L 103 66-130
sec-Butylbenzene 20.0 20.44 ug/L 102 70-135
Styrene 20.0 19.27 ug/L 96 70-130
tert-Butylbenzene 20.0 20.61 ug/L 103 70-130
1,1,1,2-Tetrachloroethane 20.0 19.43 ug/L 97 70-130
1,1,2,2-Tetrachloroethane 20.0 19.13 ug/L 96 69-131
Tetrachloroethene 20.0 19.92 ug/L 100 70-130
Toluene 20.0 20.74 ug/L 104 70-130
trans-1,2-Dichloroethene 20.0 21.36 ug/L 107 70-130
trans-1,3-Dichloropropene 20.0 19.00 ug/L 95 63-142
1,2,3-Trichlorobenzene 20.0 20.75 ug/L 104 46-150
1,2,4-Trichlorobenzene 20.0 20.35 ug/L 102 58-147
1,1,1-Trichloroethane 20.0 21.40 ug/L 107 70-135
1,1,2-Trichloroethane 20.0 19.47 ug/L 97 70-130
Trichloroethene 20.0 20.05 ug/L 100 70-130
Trichlorofluoromethane 20.0 24.47 ug/L 122 59-150
1,2,3-Trichloropropane 20.0 18.73 ug/L 94 70-131
1,2,4-Trimethylbenzene 20.0 19.32 ug/L 97 70-130
1,3,5-Trimethylbenzene 20.0 20.35 ug/L 102 70-130
Vinyl chloride 20.0 22.23 ug/L 111 57-137
Xylenes, Total 40.0 40.28 ug/L 101 70-132
4-Bromofluorobenzene (Surr)70 -130
Surrogate
106
LCS LCS
Qualifier Limits%Recovery
101Dibromofluoromethane (Surr)70 -130
1131,2-Dichloroethane-d4 (Surr)70 -130
103Toluene-d8 (Surr)70 -130
TestAmerica Nashville
Page 57 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380458/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
Acetone 100 93.10 ug/L 93 39-150 21 23
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 20.0 19.79 ug/L 99 70-130 1 12
Bromobenzene 20.0 19.28 ug/L 96 70-130 2 16
Bromochloromethane 20.0 18.37 ug/L 92 70-130 3 16
Bromodichloromethane 20.0 19.35 ug/L 97 70-130 6 14
Bromoform 20.0 15.80 ug/L 79 70-137 8 14
Bromomethane 20.0 27.00 ug/L 135 53-150 0 19
2-Butanone (MEK)100 85.80 ug/L 86 55-143 9 19
Carbon disulfide 20.0 19.82 ug/L 99 64-135 3 16
Carbon tetrachloride 20.0 20.59 ug/L 103 70-147 3 16
Chlorobenzene 20.0 19.25 ug/L 96 70-130 0 12
Chlorodibromomethane 20.0 18.09 ug/L 90 70-133 1 13
Chloroethane 20.0 20.17 ug/L 101 60-138 5 15
Chloroform 20.0 20.32 ug/L 102 70-130 7 14
Chloromethane 20.0 20.65 ug/L 103 33-150 6 20
2-Chlorotoluene 20.0 20.40 ug/L 102 70-130 1 15
4-Chlorotoluene 20.0 20.91 ug/L 105 70-130 0 15
cis-1,2-Dichloroethene 20.0 20.55 ug/L 103 70-130 2 15
cis-1,3-Dichloropropene 20.0 18.90 ug/L 94 70-133 5 15
1,2-Dibromo-3-Chloropropane 20.0 13.95 ug/L 70 45-138 4 19
1,2-Dibromoethane (EDB)20.0 17.79 ug/L 89 70-130 8 13
Dibromomethane 20.0 19.35 ug/L 97 70-130 3 14
1,2-Dichlorobenzene 20.0 19.86 ug/L 99 70-130 3 12
1,3-Dichlorobenzene 20.0 20.18 ug/L 101 70-130 2 13
1,4-Dichlorobenzene 20.0 19.85 ug/L 99 70-130 0 12
Dichlorodifluoromethane 20.0 22.94 ug/L 115 48-150 4 16
1,1-Dichloroethane 20.0 20.42 ug/L 102 70-130 7 17
1,2-Dichloroethane 20.0 22.59 ug/L 113 70-130 2 13
1,1-Dichloroethene 20.0 19.63 ug/L 98 70-132 5 20
1,2-Dichloroethene, Total 40.0 42.09 ug/L 105 70-130 1 14
1,2-Dichloropropane 20.0 19.91 ug/L 100 70-130 5 15
1,3-Dichloropropane 20.0 18.95 ug/L 95 70-130 7 12
2,2-Dichloropropane 20.0 17.75 ug/L 89 60-143 5 20
1,1-Dichloropropene 20.0 20.03 ug/L 100 70-130 7 16
Diisopropyl ether 20.0 19.28 ug/L 96 66-142 0 14
Ethylbenzene 20.0 19.20 ug/L 96 70-130 5 12
Hexachlorobutadiene 20.0 20.75 ug/L 104 70-138 1 16
2-Hexanone 100 90.21 ug/L 90 54-142 3 17
Isopropylbenzene 20.0 18.64 ug/L 93 70-131 5 13
Methylene Chloride 20.0 19.55 ug/L 98 70-130 2 15
4-Methyl-2-pentanone (MIBK)100 91.32 ug/L 91 60-137 3 21
Methyl tert-butyl ether 20.0 18.42 ug/L 92 70-130 3 16
Naphthalene 20.0 18.59 ug/L 93 54-150 3 15
n-Butylbenzene 20.0 20.29 ug/L 101 68-137 2 14
N-Propylbenzene 20.0 20.67 ug/L 103 70-134 0 14
p-Isopropyltoluene 20.0 20.17 ug/L 101 66-130 2 13
sec-Butylbenzene 20.0 20.13 ug/L 101 70-135 2 14
Styrene 20.0 18.39 ug/L 92 70-130 5 12
TestAmerica Nashville
Page 58 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380458/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
tert-Butylbenzene 20.0 20.49 ug/L 102 70-130 1 14
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,1,2-Tetrachloroethane 20.0 18.29 ug/L 91 70-130 6 13
1,1,2,2-Tetrachloroethane 20.0 18.76 ug/L 94 69-131 2 15
Tetrachloroethene 20.0 19.62 ug/L 98 70-130 2 17
Toluene 20.0 19.79 ug/L 99 70-130 5 13
trans-1,2-Dichloroethene 20.0 21.54 ug/L 108 70-130 1 15
trans-1,3-Dichloropropene 20.0 18.32 ug/L 92 63-142 4 13
1,2,3-Trichlorobenzene 20.0 19.54 ug/L 98 46-150 6 16
1,2,4-Trichlorobenzene 20.0 19.54 ug/L 98 58-147 4 15
1,1,1-Trichloroethane 20.0 21.42 ug/L 107 70-135 0 15
1,1,2-Trichloroethane 20.0 19.06 ug/L 95 70-130 2 13
Trichloroethene 20.0 18.40 ug/L 92 70-130 9 14
Trichlorofluoromethane 20.0 23.16 ug/L 116 59-150 5 22
1,2,3-Trichloropropane 20.0 18.29 ug/L 91 70-131 2 14
1,2,4-Trimethylbenzene 20.0 18.88 ug/L 94 70-130 2 13
1,3,5-Trimethylbenzene 20.0 20.63 ug/L 103 70-130 1 14
Vinyl chloride 20.0 21.86 ug/L 109 57-137 2 15
Xylenes, Total 40.0 38.64 ug/L 97 70-132 4 11
4-Bromofluorobenzene (Surr)70 -130
Surrogate
106
LCSD LCSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1081,2-Dichloroethane-d4 (Surr)70 -130
104Toluene-d8 (Surr)70 -130
Client Sample ID: TMW-2Lab Sample ID: 490-114207-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
Acetone ND 100 144.3 ug/L 121 39-150
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Benzene ND 20.0 20.84 ug/L 102 55-147
Bromobenzene ND 20.0 19.85 ug/L 99 60-133
Bromochloromethane ND 20.0 21.00 ug/L 105 59-132
Bromodichloromethane ND 20.0 20.86 ug/L 104 70-140
Bromoform ND 20.0 17.61 ug/L 88 53-150
Bromomethane ND 20.0 25.24 ug/L 126 30-150
2-Butanone (MEK)ND 100 102.7 ug/L 99 50-143
Carbon disulfide ND 20.0 21.27 ug/L 106 35-150
Carbon tetrachloride ND 20.0 23.09 ug/L 115 56-150
Chlorobenzene ND 20.0 20.62 ug/L 103 70-130
Chlorodibromomethane ND 20.0 20.05 ug/L 100 66-140
Chloroethane ND 20.0 23.63 ug/L 118 58-141
Chloroform ND 20.0 21.32 ug/L 107 66-138
Chloromethane ND 20.0 23.19 ug/L 116 10-150
2-Chlorotoluene ND 20.0 21.03 ug/L 105 67-138
4-Chlorotoluene ND 20.0 21.62 ug/L 108 69-138
cis-1,2-Dichloroethene ND 20.0 21.34 ug/L 104 68-131
TestAmerica Nashville
Page 59 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TMW-2Lab Sample ID: 490-114207-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
cis-1,3-Dichloropropene ND 20.0 19.28 ug/L 96 70-133
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
1,2-Dibromo-3-Chloropropane ND 20.0 15.08 ug/L 75 38-138
1,2-Dibromoethane (EDB)ND 20.0 19.13 ug/L 96 65-137
Dibromomethane ND 20.0 19.89 ug/L 99 70-130
1,2-Dichlorobenzene ND 20.0 20.96 ug/L 105 70-130
1,3-Dichlorobenzene ND 20.0 20.53 ug/L 103 68-131
1,4-Dichlorobenzene ND 20.0 20.14 ug/L 101 70-130
Dichlorodifluoromethane ND 20.0 26.16 ug/L 131 10-150
1,1-Dichloroethane 2.79 20.0 24.44 ug/L 108 61-139
1,2-Dichloroethane ND 20.0 23.58 ug/L 118 64-136
1,1-Dichloroethene ND 20.0 21.00 ug/L 105 54-150
1,2-Dichloroethene, Total ND 40.0 42.35 ug/L 106 60-134
1,2-Dichloropropane ND 20.0 20.62 ug/L 103 67-130
1,3-Dichloropropane ND 20.0 20.82 ug/L 104 70-130
2,2-Dichloropropane ND 20.0 17.47 ug/L 87 50-146
1,1-Dichloropropene ND 20.0 22.52 ug/L 113 54-150
Diisopropyl ether ND 20.0 20.00 ug/L 100 56-142
Ethylbenzene ND 20.0 20.67 ug/L 103 65-139
Hexachlorobutadiene ND 20.0 20.95 ug/L 105 61-141
2-Hexanone ND 100 105.7 ug/L 106 44-150
Isopropylbenzene ND 20.0 20.31 ug/L 102 70-137
Methylene Chloride ND 20.0 20.66 ug/L 103 64-130
4-Methyl-2-pentanone (MIBK)ND 100 99.07 ug/L 99 50-140
Methyl tert-butyl ether ND 20.0 19.64 ug/L 98 55-141
Naphthalene ND 20.0 18.71 ug/L 94 32-150
n-Butylbenzene ND 20.0 21.39 ug/L 107 61-141
N-Propylbenzene ND 20.0 21.16 ug/L 106 53-150
p-Isopropyltoluene ND 20.0 20.98 ug/L 105 66-137
sec-Butylbenzene ND 20.0 20.58 ug/L 103 55-136
Styrene ND 20.0 19.48 ug/L 97 70-130
tert-Butylbenzene ND 20.0 21.82 ug/L 109 70-138
1,1,1,2-Tetrachloroethane ND 20.0 20.58 ug/L 103 70-131
1,1,2,2-Tetrachloroethane ND 20.0 19.21 ug/L 96 56-145
Tetrachloroethene ND 20.0 21.21 ug/L 106 57-138
Toluene ND 20.0 20.86 ug/L 102 64-136
trans-1,2-Dichloroethene ND 20.0 21.01 ug/L 105 59-143
trans-1,3-Dichloropropene ND 20.0 19.10 ug/L 95 63-142
1,2,3-Trichlorobenzene ND 20.0 19.33 ug/L 97 36-150
1,2,4-Trichlorobenzene ND 20.0 18.99 ug/L 95 47-147
1,1,1-Trichloroethane ND 20.0 22.72 ug/L 114 68-144
1,1,2-Trichloroethane ND 20.0 19.30 ug/L 97 70-130
Trichloroethene ND 20.0 20.43 ug/L 102 63-135
Trichlorofluoromethane ND 20.0 25.62 ug/L 128 44-150
1,2,3-Trichloropropane ND 20.0 18.83 ug/L 94 65-131
1,2,4-Trimethylbenzene ND 20.0 20.34 ug/L 102 64-136
1,3,5-Trimethylbenzene ND 20.0 20.15 ug/L 101 69-139
Vinyl chloride ND 20.0 23.06 ug/L 115 57-150
Xylenes, Total ND 40.0 41.06 ug/L 103 69-132
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TMW-2Lab Sample ID: 490-114207-11 MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
4-Bromofluorobenzene (Surr)70 -130
Surrogate
102
MS MS
Qualifier Limits%Recovery
105Dibromofluoromethane (Surr)70 -130
1181,2-Dichloroethane-d4 (Surr)70 -130
102Toluene-d8 (Surr)70 -130
Client Sample ID: TMW-2Lab Sample ID: 490-114207-11 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
Acetone ND 100 131.8 ug/L 109 39-150 9 28
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Benzene ND 20.0 19.23 ug/L 94 55-147 8 22
Bromobenzene ND 20.0 18.03 ug/L 90 60-133 10 18
Bromochloromethane ND 20.0 19.47 ug/L 97 59-132 8 21
Bromodichloromethane ND 20.0 19.97 ug/L 100 70-140 4 196
Bromoform ND 20.0 17.12 ug/L 86 53-150 3 20
Bromomethane ND 20.0 26.26 ug/L 131 30-150 4 44
2-Butanone (MEK)ND 100 99.91 ug/L 96 50-143 3 28
Carbon disulfide ND 20.0 19.33 ug/L 97 35-150 10 34
Carbon tetrachloride ND 20.0 20.81 ug/L 104 56-150 10 18
Chlorobenzene ND 20.0 19.04 ug/L 95 70-130 8 15
Chlorodibromomethane ND 20.0 18.63 ug/L 93 66-140 7 19
Chloroethane ND 20.0 21.42 ug/L 107 58-141 10 31
Chloroform ND 20.0 20.14 ug/L 101 66-138 6 21
Chloromethane ND 20.0 21.37 ug/L 107 10-150 8 43
2-Chlorotoluene ND 20.0 19.32 ug/L 97 67-138 8 17
4-Chlorotoluene ND 20.0 19.24 ug/L 96 69-138 12 15
cis-1,2-Dichloroethene ND 20.0 19.79 ug/L 96 68-131 8 21
cis-1,3-Dichloropropene ND 20.0 18.61 ug/L 93 70-133 4 19
1,2-Dibromo-3-Chloropropane ND 20.0 14.70 ug/L 73 38-138 3 26
1,2-Dibromoethane (EDB)ND 20.0 17.84 ug/L 89 65-137 7 21
Dibromomethane ND 20.0 18.39 ug/L 92 70-130 8 19
1,2-Dichlorobenzene ND 20.0 19.30 ug/L 96 70-130 8 15
1,3-Dichlorobenzene ND 20.0 19.60 ug/L 98 68-131 5 14
1,4-Dichlorobenzene ND 20.0 18.72 ug/L 94 70-130 7 14
Dichlorodifluoromethane ND 20.0 23.51 ug/L 118 10-150 11 50
1,1-Dichloroethane 2.79 20.0 22.09 ug/L 97 61-139 10 23
1,2-Dichloroethane ND 20.0 22.09 ug/L 110 64-136 7 22
1,1-Dichloroethene ND 20.0 19.02 ug/L 95 54-150 10 24
1,2-Dichloroethene, Total ND 40.0 39.88 ug/L 100 60-134 6 22
1,2-Dichloropropane ND 20.0 19.55 ug/L 98 67-130 5 19
1,3-Dichloropropane ND 20.0 19.18 ug/L 96 70-130 8 17
2,2-Dichloropropane ND 20.0 15.29 ug/L 76 50-146 13 20
1,1-Dichloropropene ND 20.0 20.17 ug/L 101 54-150 11 24
Diisopropyl ether ND 20.0 18.86 ug/L 94 56-142 6 22
Ethylbenzene ND 20.0 19.16 ug/L 96 65-139 8 18
Hexachlorobutadiene ND 20.0 19.59 ug/L 98 61-141 7 26
2-Hexanone ND 100 99.68 ug/L 100 44-150 6 21
TestAmerica Nashville
Page 61 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: TMW-2Lab Sample ID: 490-114207-11 MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 380458
Isopropylbenzene ND 20.0 19.59 ug/L 98 70-137 4 17
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Methylene Chloride ND 20.0 18.68 ug/L 93 64-130 10 22
4-Methyl-2-pentanone (MIBK)ND 100 98.95 ug/L 99 50-140 0 24
Methyl tert-butyl ether ND 20.0 18.94 ug/L 95 55-141 4 24
Naphthalene ND 20.0 18.62 ug/L 93 32-150 1 40
n-Butylbenzene ND 20.0 19.98 ug/L 100 61-141 7 17
N-Propylbenzene ND 20.0 19.35 ug/L 97 53-150 9 18
p-Isopropyltoluene ND 20.0 19.64 ug/L 98 66-137 7 16
sec-Butylbenzene ND 20.0 19.37 ug/L 97 55-136 6 50
Styrene ND 20.0 18.30 ug/L 92 70-130 6 16
tert-Butylbenzene ND 20.0 20.68 ug/L 103 70-138 5 17
1,1,1,2-Tetrachloroethane ND 20.0 18.57 ug/L 93 70-131 10 16
1,1,2,2-Tetrachloroethane ND 20.0 18.95 ug/L 95 56-145 1 19
Tetrachloroethene ND 20.0 19.53 ug/L 98 57-138 8 17
Toluene ND 20.0 19.80 ug/L 97 64-136 5 18
trans-1,2-Dichloroethene ND 20.0 20.09 ug/L 100 59-143 4 25
trans-1,3-Dichloropropene ND 20.0 18.79 ug/L 94 63-142 2 18
1,2,3-Trichlorobenzene ND 20.0 19.64 ug/L 98 36-150 2 43
1,2,4-Trichlorobenzene ND 20.0 18.70 ug/L 94 47-147 2 24
1,1,1-Trichloroethane ND 20.0 21.22 ug/L 106 68-144 7 17
1,1,2-Trichloroethane ND 20.0 19.71 ug/L 99 70-130 2 18
Trichloroethene ND 20.0 19.26 ug/L 96 63-135 6 17
Trichlorofluoromethane ND 20.0 23.44 ug/L 117 44-150 9 32
1,2,3-Trichloropropane ND 20.0 17.47 ug/L 87 65-131 8 19
1,2,4-Trimethylbenzene ND 20.0 18.82 ug/L 94 64-136 8 18
1,3,5-Trimethylbenzene ND 20.0 18.44 ug/L 92 69-139 9 17
Vinyl chloride ND 20.0 21.32 ug/L 107 57-150 8 37
Xylenes, Total ND 40.0 38.02 ug/L 95 69-132 8 17
4-Bromofluorobenzene (Surr)70 -130
Surrogate
101
MSD MSD
Qualifier Limits%Recovery
102Dibromofluoromethane (Surr)70 -130
1141,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Client Sample ID: Method BlankLab Sample ID: MB 490-380848/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380848
RL MDL
Acetone ND 2.50 mg/Kg 10/25/16 13:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.100 mg/Kg 10/25/16 13:32 1Benzene
ND 0.100 mg/Kg 10/25/16 13:32 1Bromobenzene
ND 0.100 mg/Kg 10/25/16 13:32 1Bromochloromethane
ND 0.100 mg/Kg 10/25/16 13:32 1Bromodichloromethane
ND 0.100 mg/Kg 10/25/16 13:32 1Bromoform
ND 0.100 mg/Kg 10/25/16 13:32 1Bromomethane
ND 2.50 mg/Kg 10/25/16 13:32 12-Butanone (MEK)
TestAmerica Nashville
Page 62 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-380848/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380848
RL MDL
Carbon disulfide ND 0.250 mg/Kg 10/25/16 13:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.100 mg/Kg 10/25/16 13:32 1Carbon tetrachloride
ND 0.100 mg/Kg 10/25/16 13:32 1Chlorobenzene
ND 0.100 mg/Kg 10/25/16 13:32 1Chlorodibromomethane
ND 0.250 mg/Kg 10/25/16 13:32 1Chloroethane
ND 0.100 mg/Kg 10/25/16 13:32 1Chloroform
ND 0.100 mg/Kg 10/25/16 13:32 1Chloromethane
ND 0.100 mg/Kg 10/25/16 13:32 12-Chlorotoluene
ND 0.100 mg/Kg 10/25/16 13:32 14-Chlorotoluene
ND 0.100 mg/Kg 10/25/16 13:32 1cis-1,2-Dichloroethene
ND 0.100 mg/Kg 10/25/16 13:32 1cis-1,3-Dichloropropene
ND 0.250 mg/Kg 10/25/16 13:32 11,2-Dibromo-3-Chloropropane
ND 0.100 mg/Kg 10/25/16 13:32 11,2-Dibromoethane (EDB)
ND 0.100 mg/Kg 10/25/16 13:32 1Dibromomethane
ND 0.100 mg/Kg 10/25/16 13:32 11,2-Dichlorobenzene
ND 0.100 mg/Kg 10/25/16 13:32 11,3-Dichlorobenzene
ND 0.100 mg/Kg 10/25/16 13:32 11,4-Dichlorobenzene
ND 0.100 mg/Kg 10/25/16 13:32 1Dichlorodifluoromethane
ND 0.100 mg/Kg 10/25/16 13:32 11,1-Dichloroethane
ND 0.100 mg/Kg 10/25/16 13:32 11,2-Dichloroethane
ND 0.100 mg/Kg 10/25/16 13:32 11,1-Dichloroethene
ND 0.100 mg/Kg 10/25/16 13:32 11,2-Dichloroethene, Total
ND 0.100 mg/Kg 10/25/16 13:32 11,2-Dichloropropane
ND 0.100 mg/Kg 10/25/16 13:32 11,3-Dichloropropane
ND 0.100 mg/Kg 10/25/16 13:32 12,2-Dichloropropane
ND 0.100 mg/Kg 10/25/16 13:32 11,1-Dichloropropene
ND 0.100 mg/Kg 10/25/16 13:32 1Diisopropyl ether
ND 0.100 mg/Kg 10/25/16 13:32 1Ethylbenzene
ND 0.250 mg/Kg 10/25/16 13:32 1Hexachlorobutadiene
ND 2.50 mg/Kg 10/25/16 13:32 12-Hexanone
ND 0.100 mg/Kg 10/25/16 13:32 1Isopropylbenzene
ND 0.500 mg/Kg 10/25/16 13:32 1Methylene Chloride
ND 2.50 mg/Kg 10/25/16 13:32 14-Methyl-2-pentanone (MIBK)
ND 0.100 mg/Kg 10/25/16 13:32 1Methyl tert-butyl ether
ND 0.250 mg/Kg 10/25/16 13:32 1Naphthalene
ND 0.100 mg/Kg 10/25/16 13:32 1n-Butylbenzene
ND 0.100 mg/Kg 10/25/16 13:32 1N-Propylbenzene
ND 0.100 mg/Kg 10/25/16 13:32 1p-Isopropyltoluene
ND 0.100 mg/Kg 10/25/16 13:32 1sec-Butylbenzene
ND 0.100 mg/Kg 10/25/16 13:32 1Styrene
ND 0.100 mg/Kg 10/25/16 13:32 1tert-Butylbenzene
ND 0.100 mg/Kg 10/25/16 13:32 11,1,1,2-Tetrachloroethane
ND 0.100 mg/Kg 10/25/16 13:32 11,1,2,2-Tetrachloroethane
ND 0.100 mg/Kg 10/25/16 13:32 1Tetrachloroethene
ND 0.100 mg/Kg 10/25/16 13:32 1Toluene
ND 0.100 mg/Kg 10/25/16 13:32 1trans-1,2-Dichloroethene
ND 0.100 mg/Kg 10/25/16 13:32 1trans-1,3-Dichloropropene
ND 0.100 mg/Kg 10/25/16 13:32 11,2,3-Trichlorobenzene
TestAmerica Nashville
Page 63 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-380848/8
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380848
RL MDL
1,2,4-Trichlorobenzene ND 0.100 mg/Kg 10/25/16 13:32 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.100 mg/Kg 10/25/16 13:32 11,1,1-Trichloroethane
ND 0.250 mg/Kg 10/25/16 13:32 11,1,2-Trichloroethane
ND 0.100 mg/Kg 10/25/16 13:32 1Trichloroethene
ND 0.100 mg/Kg 10/25/16 13:32 1Trichlorofluoromethane
ND 0.100 mg/Kg 10/25/16 13:32 11,2,3-Trichloropropane
ND 0.100 mg/Kg 10/25/16 13:32 11,2,4-Trimethylbenzene
ND 0.100 mg/Kg 10/25/16 13:32 11,3,5-Trimethylbenzene
ND 0.100 mg/Kg 10/25/16 13:32 1Vinyl chloride
ND 0.150 mg/Kg 10/25/16 13:32 1Xylenes, Total
4-Bromofluorobenzene (Surr)107 70-130 10/25/16 13:32 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
100 10/25/16 13:32 1Dibromofluoromethane (Surr)70-130
109 10/25/16 13:32 11,2-Dichloroethane-d4 (Surr)70-130
102 10/25/16 13:32 1Toluene-d8 (Surr)70-130
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380848/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380848
Acetone 12.5 10.22 mg/Kg 82 45-145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzene 2.50 2.517 mg/Kg 101 70-130
Bromobenzene 2.50 2.662 mg/Kg 106 67-130
Bromochloromethane 2.50 2.460 mg/Kg 98 70-133
Bromodichloromethane 2.50 2.522 mg/Kg 101 70-130
Bromoform 2.50 2.422 mg/Kg 97 59-137
Bromomethane 2.50 1.239 mg/Kg 50 32-150
2-Butanone (MEK)12.5 12.03 mg/Kg 96 50-149
Carbon disulfide 2.50 2.257 mg/Kg 90 66-138
Carbon tetrachloride 2.50 2.650 mg/Kg 106 70-131
Chlorobenzene 2.50 2.609 mg/Kg 104 70-130
Chlorodibromomethane 2.50 2.406 mg/Kg 96 70-130
Chloroethane 2.50 0.9099 *mg/Kg 36 37-150
Chloroform 2.50 2.575 mg/Kg 103 70-130
Chloromethane 2.50 2.069 mg/Kg 83 53-150
2-Chlorotoluene 2.50 2.844 mg/Kg 114 70-132
4-Chlorotoluene 2.50 2.867 mg/Kg 115 67-135
cis-1,2-Dichloroethene 2.50 2.621 mg/Kg 105 70-132
cis-1,3-Dichloropropene 2.50 2.584 mg/Kg 103 70-130
1,2-Dibromo-3-Chloropropane 2.50 2.471 mg/Kg 99 47-144
1,2-Dibromoethane (EDB)2.50 2.553 mg/Kg 102 69-130
Dibromomethane 2.50 2.696 mg/Kg 108 70-130
1,2-Dichlorobenzene 2.50 2.778 mg/Kg 111 70-134
1,3-Dichlorobenzene 2.50 2.789 mg/Kg 112 69-137
1,4-Dichlorobenzene 2.50 2.823 mg/Kg 113 66-134
Dichlorodifluoromethane 2.50 2.712 mg/Kg 108 32-150
TestAmerica Nashville
Page 64 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-380848/5
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380848
1,1-Dichloroethane 2.50 2.397 mg/Kg 96 70-130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
1,2-Dichloroethane 2.50 2.752 mg/Kg 110 65-134
1,1-Dichloroethene 2.50 2.302 mg/Kg 92 70-131
1,2-Dichloroethene, Total 5.00 5.074 mg/Kg 101 70-130
1,2-Dichloropropane 2.50 2.513 mg/Kg 101 70-130
1,3-Dichloropropane 2.50 2.536 mg/Kg 101 70-130
2,2-Dichloropropane 2.50 2.639 mg/Kg 106 57-150
1,1-Dichloropropene 2.50 2.612 mg/Kg 104 70-130
Diisopropyl ether 2.50 2.329 mg/Kg 93 68-134
Ethylbenzene 2.50 2.682 mg/Kg 107 70-130
Hexachlorobutadiene 2.50 2.810 mg/Kg 112 64-137
2-Hexanone 12.5 11.49 mg/Kg 92 47-148
Isopropylbenzene 2.50 2.768 mg/Kg 111 70-130
Methylene Chloride 2.50 2.488 mg/Kg 100 69-130
4-Methyl-2-pentanone (MIBK)12.5 11.65 mg/Kg 93 48-150
Methyl tert-butyl ether 2.50 2.392 mg/Kg 96 54-145
Naphthalene 2.50 2.748 mg/Kg 110 55-149
n-Butylbenzene 2.50 2.960 mg/Kg 118 57-150
N-Propylbenzene 2.50 2.855 mg/Kg 114 62-150
p-Isopropyltoluene 2.50 2.865 mg/Kg 115 66-147
sec-Butylbenzene 2.50 2.900 mg/Kg 116 68-147
Styrene 2.50 2.695 mg/Kg 108 70-131
tert-Butylbenzene 2.50 2.812 mg/Kg 112 70-138
1,1,1,2-Tetrachloroethane 2.50 2.488 mg/Kg 100 70-130
1,1,2,2-Tetrachloroethane 2.50 2.533 mg/Kg 101 61-134
Tetrachloroethene 2.50 2.555 mg/Kg 102 70-130
Toluene 2.50 2.571 mg/Kg 103 70-130
trans-1,2-Dichloroethene 2.50 2.453 mg/Kg 98 70-130
trans-1,3-Dichloropropene 2.50 2.641 mg/Kg 106 67-130
1,2,3-Trichlorobenzene 2.50 2.890 mg/Kg 116 57-146
1,2,4-Trichlorobenzene 2.50 3.069 mg/Kg 123 47-150
1,1,1-Trichloroethane 2.50 2.631 mg/Kg 105 70-130
1,1,2-Trichloroethane 2.50 2.456 mg/Kg 98 70-130
Trichloroethene 2.50 2.630 mg/Kg 105 70-130
Trichlorofluoromethane 2.50 1.816 mg/Kg 73 53-150
1,2,3-Trichloropropane 2.50 2.586 mg/Kg 103 60-139
1,2,4-Trimethylbenzene 2.50 2.971 mg/Kg 119 70-140
1,3,5-Trimethylbenzene 2.50 2.911 mg/Kg 116 69-141
Vinyl chloride 2.50 2.387 mg/Kg 95 63-150
Xylenes, Total 5.00 5.397 mg/Kg 108 70-130
4-Bromofluorobenzene (Surr)70 -130
Surrogate
110
LCS LCS
Qualifier Limits%Recovery
103Dibromofluoromethane (Surr)70 -130
1081,2-Dichloroethane-d4 (Surr)70 -130
100Toluene-d8 (Surr)70 -130
TestAmerica Nashville
Page 65 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380848/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380848
Acetone 12.5 10.69 mg/Kg 86 45-145 4 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Benzene 2.50 2.534 mg/Kg 101 70-130 1 37
Bromobenzene 2.50 2.720 mg/Kg 109 67-130 2 40
Bromochloromethane 2.50 2.439 mg/Kg 98 70-133 1 15
Bromodichloromethane 2.50 2.442 mg/Kg 98 70-130 3 20
Bromoform 2.50 2.284 mg/Kg 91 59-137 6 17
Bromomethane 2.50 1.286 mg/Kg 51 32-150 4 45
2-Butanone (MEK)12.5 11.78 mg/Kg 94 50-149 2 39
Carbon disulfide 2.50 2.322 mg/Kg 93 66-138 3 41
Carbon tetrachloride 2.50 2.608 mg/Kg 104 70-131 2 41
Chlorobenzene 2.50 2.574 mg/Kg 103 70-130 1 40
Chlorodibromomethane 2.50 2.311 mg/Kg 92 70-130 4 14
Chloroethane 2.50 0.9510 mg/Kg 38 37-150 4 50
Chloroform 2.50 2.562 mg/Kg 102 70-130 0 15
Chloromethane 2.50 2.142 mg/Kg 86 53-150 3 47
2-Chlorotoluene 2.50 2.881 mg/Kg 115 70-132 1 41
4-Chlorotoluene 2.50 2.864 mg/Kg 115 67-135 0 41
cis-1,2-Dichloroethene 2.50 2.635 mg/Kg 105 70-132 1 18
cis-1,3-Dichloropropene 2.50 2.561 mg/Kg 102 70-130 1 42
1,2-Dibromo-3-Chloropropane 2.50 2.550 mg/Kg 102 47-144 3 38
1,2-Dibromoethane (EDB)2.50 2.510 mg/Kg 100 69-130 2 17
Dibromomethane 2.50 2.588 mg/Kg 104 70-130 4 19
1,2-Dichlorobenzene 2.50 2.873 mg/Kg 115 70-134 3 40
1,3-Dichlorobenzene 2.50 2.752 mg/Kg 110 69-137 1 41
1,4-Dichlorobenzene 2.50 2.749 mg/Kg 110 66-134 3 41
Dichlorodifluoromethane 2.50 2.776 mg/Kg 111 32-150 2 50
1,1-Dichloroethane 2.50 2.370 mg/Kg 95 70-130 1 42
1,2-Dichloroethane 2.50 2.693 mg/Kg 108 65-134 2 16
1,1-Dichloroethene 2.50 2.383 mg/Kg 95 70-131 3 43
1,2-Dichloroethene, Total 5.00 5.205 mg/Kg 104 70-130 3 41
1,2-Dichloropropane 2.50 2.504 mg/Kg 100 70-130 0 15
1,3-Dichloropropane 2.50 2.514 mg/Kg 101 70-130 1 15
2,2-Dichloropropane 2.50 2.636 mg/Kg 105 57-150 0 42
1,1-Dichloropropene 2.50 2.630 mg/Kg 105 70-130 1 41
Diisopropyl ether 2.50 2.368 mg/Kg 95 68-134 2 36
Ethylbenzene 2.50 2.626 mg/Kg 105 70-130 2 38
Hexachlorobutadiene 2.50 2.904 mg/Kg 116 64-137 3 44
2-Hexanone 12.5 11.59 mg/Kg 93 47-148 1 38
Isopropylbenzene 2.50 2.669 mg/Kg 107 70-130 4 39
Methylene Chloride 2.50 2.542 mg/Kg 102 69-130 2 19
4-Methyl-2-pentanone (MIBK)12.5 11.65 mg/Kg 93 48-150 0 41
Methyl tert-butyl ether 2.50 2.501 mg/Kg 100 54-145 4 36
Naphthalene 2.50 2.950 mg/Kg 118 55-149 7 37
n-Butylbenzene 2.50 3.087 mg/Kg 123 57-150 4 39
N-Propylbenzene 2.50 2.909 mg/Kg 116 62-150 2 38
p-Isopropyltoluene 2.50 2.866 mg/Kg 115 66-147 0 38
sec-Butylbenzene 2.50 2.922 mg/Kg 117 68-147 1 38
Styrene 2.50 2.603 mg/Kg 104 70-131 3 40
TestAmerica Nashville
Page 66 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-380848/6
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380848
tert-Butylbenzene 2.50 2.813 mg/Kg 113 70-138 0 38
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
1,1,1,2-Tetrachloroethane 2.50 2.423 mg/Kg 97 70-130 3 41
1,1,2,2-Tetrachloroethane 2.50 2.623 mg/Kg 105 61-134 4 16
Tetrachloroethene 2.50 2.519 mg/Kg 101 70-130 1 41
Toluene 2.50 2.566 mg/Kg 103 70-130 0 40
trans-1,2-Dichloroethene 2.50 2.570 mg/Kg 103 70-130 5 41
trans-1,3-Dichloropropene 2.50 2.587 mg/Kg 103 67-130 2 41
1,2,3-Trichlorobenzene 2.50 3.020 mg/Kg 121 57-146 4 42
1,2,4-Trichlorobenzene 2.50 3.124 mg/Kg 125 47-150 2 43
1,1,1-Trichloroethane 2.50 2.620 mg/Kg 105 70-130 0 41
1,1,2-Trichloroethane 2.50 2.430 mg/Kg 97 70-130 1 17
Trichloroethene 2.50 2.622 mg/Kg 105 70-130 0 41
Trichlorofluoromethane 2.50 2.103 mg/Kg 84 53-150 15 49
1,2,3-Trichloropropane 2.50 2.605 mg/Kg 104 60-139 1 16
1,2,4-Trimethylbenzene 2.50 2.959 mg/Kg 118 70-140 0 38
1,3,5-Trimethylbenzene 2.50 2.897 mg/Kg 116 69-141 0 38
Vinyl chloride 2.50 2.417 mg/Kg 97 63-150 1 46
Xylenes, Total 5.00 5.263 mg/Kg 105 70-130 3 38
4-Bromofluorobenzene (Surr)70 -130
Surrogate
113
LCSD LCSD
Qualifier Limits%Recovery
100Dibromofluoromethane (Surr)70 -130
1051,2-Dichloroethane-d4 (Surr)70 -130
101Toluene-d8 (Surr)70 -130
Method: 8270D - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 490-379813/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
RL MDL
Acenaphthene ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Acenaphthylene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Anthracene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Benzo[a]anthracene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Benzo[a]pyrene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Benzo[b]fluoranthene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Benzo[g,h,i]perylene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Benzo[k]fluoranthene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Bis(2-chloroethoxy)methane
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Bis(2-chloroethyl)ether
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1bis (2-chloroisopropyl) ether
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Bis(2-ethylhexyl) phthalate
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 14-Bromophenyl phenyl ether
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Butyl benzyl phthalate
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Carbazole
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 14-Chloroaniline
TestAmerica Nashville
Page 67 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-379813/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
RL MDL
4-Chloro-3-methylphenol ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12-Chloronaphthalene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12-Chlorophenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 14-Chlorophenyl phenyl ether
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Chrysene
ND 0.666 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Cresols
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Dibenz(a,h)anthracene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Dibenzofuran
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 11,2-Dichlorobenzene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 11,3-Dichlorobenzene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 11,4-Dichlorobenzene
ND 0.670 mg/Kg 10/20/16 10:36 10/25/16 22:15 13,3'-Dichlorobenzidine
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12,4-Dichlorophenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Diethyl phthalate
ND 0.670 mg/Kg 10/20/16 10:36 10/25/16 22:15 12,4-Dimethylphenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Dimethyl phthalate
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Di-n-butyl phthalate
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 14,6-Dinitro-2-methylphenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12,4-Dinitrophenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12,4-Dinitrotoluene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12,6-Dinitrotoluene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Di-n-octyl phthalate
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Fluoranthene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Fluorene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Hexachlorobenzene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Hexachlorobutadiene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Hexachlorocyclopentadiene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Hexachloroethane
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Indeno[1,2,3-cd]pyrene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Isophorone
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 11-Methylnaphthalene
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 12-Methylnaphthalene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12-Methylphenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 13 & 4 Methylphenol
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Naphthalene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12-Nitroaniline
ND 0.670 mg/Kg 10/20/16 10:36 10/25/16 22:15 13-Nitroaniline
ND 0.670 mg/Kg 10/20/16 10:36 10/25/16 22:15 14-Nitroaniline
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Nitrobenzene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12-Nitrophenol
ND 0.670 mg/Kg 10/20/16 10:36 10/25/16 22:15 14-Nitrophenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1N-Nitrosodi-n-propylamine
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Pentachlorophenol
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Phenanthrene
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Phenol
ND 0.0670 mg/Kg 10/20/16 10:36 10/25/16 22:15 1Pyrene
TestAmerica Nashville
Page 68 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-379813/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
RL MDL
1,2,4-Trichlorobenzene ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12,4,5-Trichlorophenol
ND 0.333 mg/Kg 10/20/16 10:36 10/25/16 22:15 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)59 29-120 10/25/16 22:15 1
MB MB
Surrogate
10/20/16 10:36
Dil FacPreparedAnalyzedQualifierLimits%Recovery
43 10/20/16 10:36 10/25/16 22:15 12-Fluorophenol (Surr)10-120
55 10/20/16 10:36 10/25/16 22:15 1Nitrobenzene-d5 (Surr)27-120
48 10/20/16 10:36 10/25/16 22:15 1Phenol-d5 (Surr)10-120
68 10/20/16 10:36 10/25/16 22:15 1Terphenyl-d14 (Surr)13-120
38 10/20/16 10:36 10/25/16 22:15 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379813/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
Acenaphthene 1.67 0.9651 mg/Kg 58 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 0.9440 mg/Kg 57 38-120
Anthracene 1.67 0.9713 mg/Kg 58 46-124
Benzo[a]anthracene 1.67 0.9660 mg/Kg 58 45-120
Benzo[a]pyrene 1.67 0.9349 mg/Kg 56 45-120
Benzo[b]fluoranthene 1.67 0.9242 mg/Kg 55 42-120
Benzo[g,h,i]perylene 1.67 1.014 mg/Kg 61 38-120
Benzo[k]fluoranthene 1.67 0.9696 mg/Kg 58 42-120
Bis(2-chloroethoxy)methane 1.67 0.7751 mg/Kg 47 32-120
Bis(2-chloroethyl)ether 1.67 0.6835 mg/Kg 41 31-120
bis (2-chloroisopropyl) ether 1.67 0.5703 mg/Kg 34 32-120
Bis(2-ethylhexyl) phthalate 1.67 0.8679 mg/Kg 52 43-120
4-Bromophenyl phenyl ether 1.67 0.9589 mg/Kg 58 40-120
Butyl benzyl phthalate 1.67 0.8570 mg/Kg 51 43-133
Carbazole 1.67 0.9537 mg/Kg 57 44-120
4-Chloroaniline 1.67 0.9523 mg/Kg 57 35-120
4-Chloro-3-methylphenol 1.67 1.060 mg/Kg 64 38-120
2-Chloronaphthalene 1.67 0.8911 mg/Kg 53 34-120
2-Chlorophenol 1.67 0.7754 mg/Kg 47 32-120
4-Chlorophenyl phenyl ether 1.67 1.019 mg/Kg 61 42-120
Chrysene 1.67 0.9495 mg/Kg 57 43-120
Cresols 3.33 1.789 mg/Kg 54 36-129
Dibenz(a,h)anthracene 1.67 1.004 mg/Kg 60 32-128
Dibenzofuran 1.67 0.9431 mg/Kg 57 41-120
1,2-Dichlorobenzene 1.67 0.7159 mg/Kg 43 33-120
1,3-Dichlorobenzene 1.67 0.7227 mg/Kg 43 32-120
1,4-Dichlorobenzene 1.67 0.7075 mg/Kg 42 32-120
3,3'-Dichlorobenzidine 1.67 0.8800 mg/Kg 53 39-120
2,4-Dichlorophenol 1.67 0.9534 mg/Kg 57 32-120
Diethyl phthalate 1.67 0.9580 mg/Kg 57 41-122
2,4-Dimethylphenol 1.67 1.053 mg/Kg 63 32-120
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379813/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
Dimethyl phthalate 1.67 0.9554 mg/Kg 57 55-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Di-n-butyl phthalate 1.67 0.8806 mg/Kg 53 46-127
4,6-Dinitro-2-methylphenol 3.33 1.750 mg/Kg 52 27-134
2,4-Dinitrophenol 3.33 1.420 mg/Kg 43 10-142
2,4-Dinitrotoluene 1.67 0.9378 mg/Kg 56 43-120
2,6-Dinitrotoluene 1.67 0.9134 mg/Kg 55 43-120
Di-n-octyl phthalate 1.67 0.8865 mg/Kg 53 40-130
Fluoranthene 1.67 0.9773 mg/Kg 59 46-120
Fluorene 1.67 0.9740 mg/Kg 58 42-120
Hexachlorobenzene 1.67 0.9467 mg/Kg 57 44-120
Hexachlorobutadiene 1.67 0.8400 mg/Kg 50 31-120
Hexachlorocyclopentadiene 1.67 0.5439 mg/Kg 33 24-120
Hexachloroethane 1.67 0.7633 mg/Kg 46 33-120
Indeno[1,2,3-cd]pyrene 1.67 0.9752 mg/Kg 59 41-121
Isophorone 1.67 0.8560 mg/Kg 51 33-120
1-Methylnaphthalene 1.67 0.9121 mg/Kg 55 32-120
2-Methylnaphthalene 1.67 0.8945 mg/Kg 54 28-120
2-Methylphenol 1.67 0.8991 mg/Kg 54 36-120
3 & 4 Methylphenol 1.67 0.8900 mg/Kg 53 37-120
Naphthalene 1.67 0.8236 mg/Kg 49 32-120
2-Nitroaniline 1.67 0.9744 mg/Kg 58 40-120
3-Nitroaniline 1.67 0.8830 mg/Kg 53 42-120
4-Nitroaniline 1.67 0.7399 mg/Kg 44 43-120
Nitrobenzene 1.67 0.8343 mg/Kg 50 26-120
2-Nitrophenol 1.67 0.8631 mg/Kg 52 29-120
4-Nitrophenol 3.33 1.761 mg/Kg 53 32-136
N-Nitrosodi-n-propylamine 1.67 0.8454 mg/Kg 51 35-120
Pentachlorophenol 3.33 1.839 mg/Kg 55 44-134
Phenanthrene 1.67 0.9547 mg/Kg 57 45-120
Phenol 1.67 0.8375 mg/Kg 50 30-120
Pyrene 1.67 0.9288 mg/Kg 56 43-120
1,2,4-Trichlorobenzene 1.67 0.8081 mg/Kg 48 29-120
2,4,5-Trichlorophenol 1.67 1.055 mg/Kg 63 39-120
2,4,6-Trichlorophenol 1.67 0.9768 mg/Kg 59 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
54
LCS LCS
Qualifier Limits%Recovery
412-Fluorophenol (Surr)10 -120
49Nitrobenzene-d5 (Surr)27 -120
50Phenol-d5 (Surr)10 -120
57Terphenyl-d14 (Surr)13 -120
562,4,6-Tribromophenol (Surr)10 -120
TestAmerica Nashville
Page 70 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-114146-A-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
Acenaphthene ND 2.02 1.383 mg/Kg 68 19-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene ND 2.02 1.346 mg/Kg 67 25-120☼
Anthracene ND 2.02 1.727 mg/Kg 85 28-125☼
Benzo[a]anthracene ND 2.02 1.745 mg/Kg 86 23-120☼
Benzo[a]pyrene ND 2.02 1.682 mg/Kg 83 15-128☼
Benzo[b]fluoranthene ND 2.02 1.693 mg/Kg 84 12-133☼
Benzo[g,h,i]perylene ND 2.02 1.793 mg/Kg 89 22-120☼
Benzo[k]fluoranthene ND 2.02 1.757 mg/Kg 87 28-120☼
Bis(2-chloroethoxy)methane ND 2.02 1.029 mg/Kg 51 24-120☼
Bis(2-chloroethyl)ether ND 2.02 1.039 mg/Kg 51 22-120☼
bis (2-chloroisopropyl) ether ND 2.02 0.8175 mg/Kg 40 20-120☼
Bis(2-ethylhexyl) phthalate ND 2.02 1.613 mg/Kg 80 26-120☼
4-Bromophenyl phenyl ether ND 2.02 1.615 mg/Kg 80 31-120☼
Butyl benzyl phthalate ND 2.02 1.508 mg/Kg 75 24-133☼
Carbazole ND 2.02 1.702 mg/Kg 84 25-123☼
4-Chloroaniline ND 2.02 1.279 mg/Kg 63 26-120☼
4-Chloro-3-methylphenol ND 2.02 1.551 mg/Kg 77 21-120☼
2-Chloronaphthalene ND 2.02 1.271 mg/Kg 63 24-120☼
2-Chlorophenol ND 2.02 1.114 mg/Kg 55 25-120☼
4-Chlorophenyl phenyl ether ND 2.02 1.575 mg/Kg 78 26-120☼
Chrysene ND 2.02 1.744 mg/Kg 86 20-120☼
Cresols ND 4.04 2.491 mg/Kg 62 10-200☼
Dibenz(a,h)anthracene ND 2.02 1.823 mg/Kg 90 12-128☼
Dibenzofuran ND 2.02 1.427 mg/Kg 71 21-120☼
1,2-Dichlorobenzene ND 2.02 1.101 mg/Kg 54 10-120☼
1,3-Dichlorobenzene ND 2.02 1.090 mg/Kg 54 10-120☼
1,4-Dichlorobenzene ND 2.02 1.085 mg/Kg 54 10-120☼
3,3'-Dichlorobenzidine ND 2.02 1.440 mg/Kg 71 10-120☼
2,4-Dichlorophenol ND 2.02 1.355 mg/Kg 67 17-120☼
Diethyl phthalate ND 2.02 1.675 mg/Kg 83 29-122☼
2,4-Dimethylphenol ND 2.02 1.335 mg/Kg 66 17-120☼
Dimethyl phthalate ND 2.02 1.522 mg/Kg 75 30-120☼
Di-n-butyl phthalate ND 2.02 1.633 mg/Kg 81 29-126☼
4,6-Dinitro-2-methylphenol ND 4.04 2.999 mg/Kg 74 10-134☼
2,4-Dinitrophenol ND 4.04 2.436 mg/Kg 60 10-150☼
2,4-Dinitrotoluene ND 2.02 1.644 mg/Kg 81 24-121☼
2,6-Dinitrotoluene ND 2.02 1.476 mg/Kg 73 24-120☼
Di-n-octyl phthalate ND 2.02 1.652 mg/Kg 82 27-130☼
Fluoranthene ND 2.02 1.750 mg/Kg 87 10-143☼
Fluorene ND 2.02 1.557 mg/Kg 77 20-120☼
Hexachlorobenzene ND 2.02 1.656 mg/Kg 82 25-120☼
Hexachlorobutadiene ND 2.02 1.225 mg/Kg 61 10-120☼
Hexachlorocyclopentadiene ND 2.02 0.7783 mg/Kg 39 10-120☼
Hexachloroethane ND 2.02 1.035 mg/Kg 51 10-120☼
Indeno[1,2,3-cd]pyrene ND 2.02 1.738 mg/Kg 86 22-121☼
Isophorone ND 2.02 1.164 mg/Kg 58 24-120☼
1-Methylnaphthalene ND 2.02 1.254 mg/Kg 62 10-120☼
2-Methylnaphthalene ND 2.02 1.214 mg/Kg 60 13-120☼
TestAmerica Nashville
Page 71 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-114146-A-1-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
2-Methylphenol ND 2.02 1.250 mg/Kg 62 23-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
3 & 4 Methylphenol ND 2.02 1.241 mg/Kg 61 19-120☼
Naphthalene ND 2.02 1.141 mg/Kg 56 10-120☼
2-Nitroaniline ND 2.02 1.501 mg/Kg 74 31-120☼
3-Nitroaniline ND 2.02 1.559 mg/Kg 77 31-120☼
4-Nitroaniline ND 2.02 1.438 mg/Kg 71 28-120☼
Nitrobenzene ND 2.02 1.140 mg/Kg 56 19-120☼
2-Nitrophenol ND 2.02 1.155 mg/Kg 57 23-120☼
4-Nitrophenol ND 4.04 3.273 mg/Kg 81 16-139☼
N-Nitrosodi-n-propylamine ND 2.02 1.103 mg/Kg 55 24-120☼
Pentachlorophenol ND 4.04 3.711 mg/Kg 92 19-145☼
Phenanthrene ND 2.02 1.723 mg/Kg 85 21-122☼
Phenol ND 2.02 1.185 mg/Kg 59 15-120☼
Pyrene ND 2.02 1.672 mg/Kg 83 20-123☼
1,2,4-Trichlorobenzene ND 2.02 1.170 mg/Kg 58 14-120☼
2,4,5-Trichlorophenol ND 2.02 1.703 mg/Kg 84 27-120☼
2,4,6-Trichlorophenol ND 2.02 1.468 mg/Kg 73 24-122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
57
MS MS
Qualifier Limits%Recovery
482-Fluorophenol (Surr)10 -120
52Nitrobenzene-d5 (Surr)27 -120
55Phenol-d5 (Surr)10 -120
81Terphenyl-d14 (Surr)13 -120
812,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114146-A-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
Acenaphthene ND 2.02 1.390 mg/Kg 69 19-120 1 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene ND 2.02 1.317 mg/Kg 65 25-120 2 50☼
Anthracene ND 2.02 1.494 mg/Kg 74 28-125 14 49☼
Benzo[a]anthracene ND 2.02 1.596 mg/Kg 79 23-120 9 50☼
Benzo[a]pyrene ND 2.02 1.501 mg/Kg 75 15-128 11 50☼
Benzo[b]fluoranthene ND 2.02 1.503 mg/Kg 75 12-133 12 50☼
Benzo[g,h,i]perylene ND 2.02 1.604 mg/Kg 80 22-120 11 50☼
Benzo[k]fluoranthene ND 2.02 1.559 mg/Kg 77 28-120 12 45☼
Bis(2-chloroethoxy)methane ND 2.02 0.9860 mg/Kg 49 24-120 4 50☼
Bis(2-chloroethyl)ether ND 2.02 0.8934 mg/Kg 44 22-120 15 50☼
bis (2-chloroisopropyl) ether ND 2.02 0.7443 mg/Kg 37 20-120 9 50☼
Bis(2-ethylhexyl) phthalate ND 2.02 1.435 mg/Kg 71 26-120 12 50☼
4-Bromophenyl phenyl ether ND 2.02 1.488 mg/Kg 74 31-120 8 37☼
Butyl benzyl phthalate ND 2.02 1.350 mg/Kg 67 24-133 11 50☼
Carbazole ND 2.02 1.505 mg/Kg 75 25-123 12 46☼
4-Chloroaniline ND 2.02 1.258 mg/Kg 62 26-120 2 50☼
4-Chloro-3-methylphenol ND 2.02 1.458 mg/Kg 72 21-120 6 49☼
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114146-A-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
2-Chloronaphthalene ND 2.02 1.225 mg/Kg 61 24-120 4 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
2-Chlorophenol ND 2.02 1.022 mg/Kg 51 25-120 9 50☼
4-Chlorophenyl phenyl ether ND 2.02 1.468 mg/Kg 73 26-120 7 50☼
Chrysene ND 2.02 1.500 mg/Kg 74 20-120 15 49☼
Cresols ND 4.03 2.317 mg/Kg 57 10-200 7 50☼
Dibenz(a,h)anthracene ND 2.02 1.627 mg/Kg 81 12-128 11 50☼
Dibenzofuran ND 2.02 1.366 mg/Kg 68 21-120 4 50☼
1,2-Dichlorobenzene ND 2.02 1.003 mg/Kg 50 10-120 9 50☼
1,3-Dichlorobenzene ND 2.02 0.9910 mg/Kg 49 10-120 9 50☼
1,4-Dichlorobenzene ND 2.02 0.9967 mg/Kg 49 10-120 8 50☼
3,3'-Dichlorobenzidine ND 2.02 1.316 mg/Kg 65 10-120 9 50☼
2,4-Dichlorophenol ND 2.02 1.298 mg/Kg 64 17-120 4 50☼
Diethyl phthalate ND 2.02 1.495 mg/Kg 74 29-122 11 45☼
2,4-Dimethylphenol ND 2.02 1.334 mg/Kg 66 17-120 0 50☼
Dimethyl phthalate ND 2.02 1.433 mg/Kg 71 30-120 6 46☼
Di-n-butyl phthalate ND 2.02 1.428 mg/Kg 71 29-126 13 49☼
4,6-Dinitro-2-methylphenol ND 4.03 2.737 mg/Kg 68 10-134 9 50☼
2,4-Dinitrophenol ND 4.03 2.427 mg/Kg 60 10-150 0 50☼
2,4-Dinitrotoluene ND 2.02 1.481 mg/Kg 74 24-121 10 50☼
2,6-Dinitrotoluene ND 2.02 1.386 mg/Kg 69 24-120 6 50☼
Di-n-octyl phthalate ND 2.02 1.445 mg/Kg 72 27-130 13 50☼
Fluoranthene ND 2.02 1.556 mg/Kg 77 10-143 12 50☼
Fluorene ND 2.02 1.482 mg/Kg 74 20-120 5 50☼
Hexachlorobenzene ND 2.02 1.509 mg/Kg 75 25-120 9 50☼
Hexachlorobutadiene ND 2.02 1.179 mg/Kg 59 10-120 4 50☼
Hexachlorocyclopentadiene ND 2.02 0.7662 mg/Kg 38 10-120 2 50☼
Hexachloroethane ND 2.02 0.9766 mg/Kg 48 10-120 6 50☼
Indeno[1,2,3-cd]pyrene ND 2.02 1.575 mg/Kg 78 22-121 10 50☼
Isophorone ND 2.02 1.115 mg/Kg 55 24-120 4 50☼
1-Methylnaphthalene ND 2.02 1.228 mg/Kg 61 10-120 2 50☼
2-Methylnaphthalene ND 2.02 1.200 mg/Kg 60 13-120 1 50☼
2-Methylphenol ND 2.02 1.145 mg/Kg 57 23-120 9 50☼
3 & 4 Methylphenol ND 2.02 1.172 mg/Kg 58 19-120 6 50☼
Naphthalene ND 2.02 1.119 mg/Kg 56 10-120 2 50☼
2-Nitroaniline ND 2.02 1.421 mg/Kg 71 31-120 5 50☼
3-Nitroaniline ND 2.02 1.415 mg/Kg 70 31-120 10 49☼
4-Nitroaniline ND 2.02 1.316 mg/Kg 65 28-120 9 49☼
Nitrobenzene ND 2.02 1.092 mg/Kg 54 19-120 4 50☼
2-Nitrophenol ND 2.02 1.083 mg/Kg 54 23-120 6 50☼
4-Nitrophenol ND 4.03 2.881 mg/Kg 71 16-139 13 45☼
N-Nitrosodi-n-propylamine ND 2.02 1.003 mg/Kg 50 24-120 10 50☼
Pentachlorophenol ND 4.03 3.183 mg/Kg 79 19-145 15 50☼
Phenanthrene ND 2.02 1.537 mg/Kg 76 21-122 11 50☼
Phenol ND 2.02 1.051 mg/Kg 52 15-120 12 50☼
Pyrene ND 2.02 1.512 mg/Kg 75 20-123 10 50☼
1,2,4-Trichlorobenzene ND 2.02 1.116 mg/Kg 55 14-120 5 50☼
2,4,5-Trichlorophenol ND 2.02 1.619 mg/Kg 80 27-120 5 50☼
2,4,6-Trichlorophenol ND 2.02 1.416 mg/Kg 70 24-122 4 50☼
TestAmerica Nashville
Page 73 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114146-A-1-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380971 Prep Batch: 379813
2-Fluorobiphenyl (Surr)29 -120
Surrogate
59
MSD MSD
Qualifier Limits%Recovery
432-Fluorophenol (Surr)10 -120
51Nitrobenzene-d5 (Surr)27 -120
49Phenol-d5 (Surr)10 -120
72Terphenyl-d14 (Surr)13 -120
742,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: Method BlankLab Sample ID: MB 490-379832/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
RL MDL
Acenaphthene ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Acenaphthylene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Anthracene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Benzo[a]anthracene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Benzo[a]pyrene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Benzo[b]fluoranthene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Benzo[g,h,i]perylene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Benzo[k]fluoranthene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Bis(2-chloroethoxy)methane
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Bis(2-chloroethyl)ether
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1bis (2-chloroisopropyl) ether
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Bis(2-ethylhexyl) phthalate
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 14-Bromophenyl phenyl ether
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Butyl benzyl phthalate
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Carbazole
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 14-Chloroaniline
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 14-Chloro-3-methylphenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12-Chloronaphthalene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12-Chlorophenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 14-Chlorophenyl phenyl ether
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Chrysene
ND 0.666 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Cresols
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Dibenz(a,h)anthracene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Dibenzofuran
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 11,2-Dichlorobenzene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 11,3-Dichlorobenzene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 11,4-Dichlorobenzene
ND 0.670 mg/Kg 10/20/16 11:13 10/21/16 15:35 13,3'-Dichlorobenzidine
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12,4-Dichlorophenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Diethyl phthalate
ND 0.670 mg/Kg 10/20/16 11:13 10/21/16 15:35 12,4-Dimethylphenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Dimethyl phthalate
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Di-n-butyl phthalate
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 14,6-Dinitro-2-methylphenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12,4-Dinitrophenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12,4-Dinitrotoluene
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-379832/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
RL MDL
2,6-Dinitrotoluene ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Di-n-octyl phthalate
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Fluoranthene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Fluorene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Hexachlorobenzene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Hexachlorobutadiene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Hexachlorocyclopentadiene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Hexachloroethane
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Indeno[1,2,3-cd]pyrene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Isophorone
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 11-Methylnaphthalene
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 12-Methylnaphthalene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12-Methylphenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 13 & 4 Methylphenol
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Naphthalene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12-Nitroaniline
ND 0.670 mg/Kg 10/20/16 11:13 10/21/16 15:35 13-Nitroaniline
ND 0.670 mg/Kg 10/20/16 11:13 10/21/16 15:35 14-Nitroaniline
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Nitrobenzene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12-Nitrophenol
ND 0.670 mg/Kg 10/20/16 11:13 10/21/16 15:35 14-Nitrophenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1N-Nitrosodi-n-propylamine
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1n-Nitrosodiphenylamine(as
diphenylamine)
ND 0.670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Pentachlorophenol
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Phenanthrene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Phenol
ND 0.0670 mg/Kg 10/20/16 11:13 10/21/16 15:35 1Pyrene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 11,2,4-Trichlorobenzene
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12,4,5-Trichlorophenol
ND 0.333 mg/Kg 10/20/16 11:13 10/21/16 15:35 12,4,6-Trichlorophenol
2-Fluorobiphenyl (Surr)46 29-120 10/21/16 15:35 1
MB MB
Surrogate
10/20/16 11:13
Dil FacPreparedAnalyzedQualifierLimits%Recovery
41 10/20/16 11:13 10/21/16 15:35 12-Fluorophenol (Surr)10-120
45 10/20/16 11:13 10/21/16 15:35 1Nitrobenzene-d5 (Surr)27-120
47 10/20/16 11:13 10/21/16 15:35 1Phenol-d5 (Surr)10-120
68 10/20/16 11:13 10/21/16 15:35 1Terphenyl-d14 (Surr)13-120
49 10/20/16 11:13 10/21/16 15:35 12,4,6-Tribromophenol (Surr)10-120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379832/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
Acenaphthene 1.67 1.337 mg/Kg 80 36-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 1.67 1.347 mg/Kg 81 38-120
Anthracene 1.67 1.427 mg/Kg 86 46-124
TestAmerica Nashville
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379832/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
Benzo[a]anthracene 1.67 1.457 mg/Kg 87 45-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Benzo[a]pyrene 1.67 1.401 mg/Kg 84 45-120
Benzo[b]fluoranthene 1.67 1.361 mg/Kg 82 42-120
Benzo[g,h,i]perylene 1.67 1.497 mg/Kg 90 38-120
Benzo[k]fluoranthene 1.67 1.541 mg/Kg 92 42-120
Bis(2-chloroethoxy)methane 1.67 1.144 mg/Kg 69 32-120
Bis(2-chloroethyl)ether 1.67 1.039 mg/Kg 62 31-120
bis (2-chloroisopropyl) ether 1.67 0.9528 mg/Kg 57 32-120
Bis(2-ethylhexyl) phthalate 1.67 1.413 mg/Kg 85 43-120
4-Bromophenyl phenyl ether 1.67 1.410 mg/Kg 85 40-120
Butyl benzyl phthalate 1.67 1.371 mg/Kg 82 43-133
Carbazole 1.67 1.410 mg/Kg 85 44-120
4-Chloroaniline 1.67 1.336 mg/Kg 80 35-120
4-Chloro-3-methylphenol 1.67 1.467 mg/Kg 88 38-120
2-Chloronaphthalene 1.67 1.283 mg/Kg 77 34-120
2-Chlorophenol 1.67 1.137 mg/Kg 68 32-120
4-Chlorophenyl phenyl ether 1.67 1.378 mg/Kg 83 42-120
Chrysene 1.67 1.391 mg/Kg 83 43-120
Cresols 3.33 2.676 mg/Kg 80 36-129
Dibenz(a,h)anthracene 1.67 1.534 mg/Kg 92 32-128
Dibenzofuran 1.67 1.356 mg/Kg 81 41-120
1,2-Dichlorobenzene 1.67 1.108 mg/Kg 66 33-120
1,3-Dichlorobenzene 1.67 1.046 mg/Kg 63 32-120
1,4-Dichlorobenzene 1.67 1.054 mg/Kg 63 32-120
3,3'-Dichlorobenzidine 1.67 1.131 mg/Kg 68 39-120
2,4-Dichlorophenol 1.67 1.350 mg/Kg 81 32-120
Diethyl phthalate 1.67 1.400 mg/Kg 84 41-122
2,4-Dimethylphenol 1.67 1.381 mg/Kg 83 32-120
Dimethyl phthalate 1.67 1.352 mg/Kg 81 55-120
Di-n-butyl phthalate 1.67 1.399 mg/Kg 84 46-127
4,6-Dinitro-2-methylphenol 3.33 1.424 mg/Kg 43 27-134
2,4-Dinitrophenol 3.33 1.057 mg/Kg 32 10-142
2,4-Dinitrotoluene 1.67 1.391 mg/Kg 83 43-120
2,6-Dinitrotoluene 1.67 1.309 mg/Kg 79 43-120
Di-n-octyl phthalate 1.67 1.453 mg/Kg 87 40-130
Fluoranthene 1.67 1.424 mg/Kg 85 46-120
Fluorene 1.67 1.375 mg/Kg 82 42-120
Hexachlorobenzene 1.67 1.473 mg/Kg 88 44-120
Hexachlorobutadiene 1.67 1.154 mg/Kg 69 31-120
Hexachlorocyclopentadiene 1.67 0.6902 mg/Kg 41 24-120
Hexachloroethane 1.67 1.055 mg/Kg 63 33-120
Indeno[1,2,3-cd]pyrene 1.67 1.462 mg/Kg 88 41-121
Isophorone 1.67 1.263 mg/Kg 76 33-120
1-Methylnaphthalene 1.67 1.292 mg/Kg 78 32-120
2-Methylnaphthalene 1.67 1.249 mg/Kg 75 28-120
2-Methylphenol 1.67 1.320 mg/Kg 79 36-120
3 & 4 Methylphenol 1.67 1.356 mg/Kg 81 37-120
Naphthalene 1.67 1.161 mg/Kg 70 32-120
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Page 76 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379832/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
2-Nitroaniline 1.67 1.373 mg/Kg 82 40-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
3-Nitroaniline 1.67 1.296 mg/Kg 78 42-120
4-Nitroaniline 1.67 1.172 mg/Kg 70 43-120
Nitrobenzene 1.67 1.122 mg/Kg 67 26-120
2-Nitrophenol 1.67 1.211 mg/Kg 73 29-120
4-Nitrophenol 3.33 2.913 mg/Kg 87 32-136
N-Nitrosodi-n-propylamine 1.67 1.264 mg/Kg 76 35-120
Pentachlorophenol 3.33 2.976 mg/Kg 89 44-134
Phenanthrene 1.67 1.436 mg/Kg 86 45-120
Phenol 1.67 1.242 mg/Kg 75 30-120
Pyrene 1.67 1.473 mg/Kg 88 43-120
1,2,4-Trichlorobenzene 1.67 1.150 mg/Kg 69 29-120
2,4,5-Trichlorophenol 1.67 1.579 mg/Kg 95 39-120
2,4,6-Trichlorophenol 1.67 1.369 mg/Kg 82 39-120
2-Fluorobiphenyl (Surr)29 -120
Surrogate
59
LCS LCS
Qualifier Limits%Recovery
482-Fluorophenol (Surr)10 -120
61Nitrobenzene-d5 (Surr)27 -120
59Phenol-d5 (Surr)10 -120
71Terphenyl-d14 (Surr)13 -120
722,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: SB-1 (0-2)Lab Sample ID: 490-114207-7 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
Acenaphthene ND 2.07 1.312 mg/Kg 63 19-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Acenaphthylene ND 2.07 1.319 mg/Kg 64 25-120☼
Anthracene ND 2.07 1.427 mg/Kg 69 28-125☼
Benzo[a]anthracene ND 2.07 1.457 mg/Kg 70 23-120☼
Benzo[a]pyrene ND 2.07 1.411 mg/Kg 68 15-128☼
Benzo[b]fluoranthene ND 2.07 1.437 mg/Kg 69 12-133☼
Benzo[g,h,i]perylene ND 2.07 1.534 mg/Kg 74 22-120☼
Benzo[k]fluoranthene ND 2.07 1.443 mg/Kg 70 28-120☼
Bis(2-chloroethoxy)methane ND 2.07 1.084 mg/Kg 52 24-120☼
Bis(2-chloroethyl)ether ND 2.07 1.099 mg/Kg 53 22-120☼
bis (2-chloroisopropyl) ether ND 2.07 0.9787 mg/Kg 47 20-120☼
Bis(2-ethylhexyl) phthalate ND 2.07 1.380 mg/Kg 67 26-120☼
4-Bromophenyl phenyl ether ND 2.07 1.434 mg/Kg 69 31-120☼
Butyl benzyl phthalate ND 2.07 1.381 mg/Kg 67 24-133☼
Carbazole ND 2.07 1.381 mg/Kg 67 25-123☼
4-Chloroaniline ND 2.07 1.241 mg/Kg 60 26-120☼
4-Chloro-3-methylphenol ND 2.07 1.392 mg/Kg 67 21-120☼
2-Chloronaphthalene ND 2.07 1.251 mg/Kg 60 24-120☼
2-Chlorophenol ND 2.07 1.181 mg/Kg 57 25-120☼
4-Chlorophenyl phenyl ether ND 2.07 1.345 mg/Kg 65 26-120☼
TestAmerica Nashville
Page 77 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SB-1 (0-2)Lab Sample ID: 490-114207-7 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
Chrysene ND 2.07 1.465 mg/Kg 71 20-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Cresols ND 4.14 2.628 mg/Kg 64 10-200☼
Dibenz(a,h)anthracene ND 2.07 1.541 mg/Kg 74 12-128☼
Dibenzofuran ND 2.07 1.290 mg/Kg 62 21-120☼
1,2-Dichlorobenzene ND 2.07 1.194 mg/Kg 58 10-120☼
1,3-Dichlorobenzene ND 2.07 1.185 mg/Kg 57 10-120☼
1,4-Dichlorobenzene ND 2.07 1.151 mg/Kg 56 10-120☼
3,3'-Dichlorobenzidine ND 2.07 1.089 mg/Kg 53 10-120☼
2,4-Dichlorophenol ND 2.07 1.289 mg/Kg 62 17-120☼
Diethyl phthalate ND 2.07 1.367 mg/Kg 66 29-122☼
2,4-Dimethylphenol ND 2.07 1.367 mg/Kg 66 17-120☼
Dimethyl phthalate ND 2.07 1.321 mg/Kg 64 30-120☼
Di-n-butyl phthalate ND 2.07 1.396 mg/Kg 67 29-126☼
4,6-Dinitro-2-methylphenol ND 4.14 1.547 mg/Kg 37 10-134☼
2,4-Dinitrophenol ND 4.14 1.227 mg/Kg 30 10-150☼
2,4-Dinitrotoluene ND 2.07 1.317 mg/Kg 64 24-121☼
2,6-Dinitrotoluene ND 2.07 1.298 mg/Kg 63 24-120☼
Di-n-octyl phthalate ND 2.07 1.407 mg/Kg 68 27-130☼
Fluoranthene ND 2.07 1.437 mg/Kg 69 10-143☼
Fluorene ND 2.07 1.343 mg/Kg 65 20-120☼
Hexachlorobenzene ND 2.07 1.463 mg/Kg 71 25-120☼
Hexachlorobutadiene ND 2.07 1.214 mg/Kg 59 10-120☼
Hexachlorocyclopentadiene ND 2.07 0.6598 mg/Kg 32 10-120☼
Hexachloroethane ND 2.07 1.198 mg/Kg 58 10-120☼
Indeno[1,2,3-cd]pyrene ND 2.07 1.502 mg/Kg 73 22-121☼
Isophorone ND 2.07 1.148 mg/Kg 55 24-120☼
1-Methylnaphthalene ND 2.07 1.237 mg/Kg 60 10-120☼
2-Methylnaphthalene ND 2.07 1.250 mg/Kg 60 13-120☼
2-Methylphenol ND 2.07 1.343 mg/Kg 65 23-120☼
3 & 4 Methylphenol ND 2.07 1.285 mg/Kg 62 19-120☼
Naphthalene ND 2.07 1.185 mg/Kg 57 10-120☼
2-Nitroaniline ND 2.07 1.361 mg/Kg 66 31-120☼
3-Nitroaniline ND 2.07 1.339 mg/Kg 65 31-120☼
4-Nitroaniline ND 2.07 1.185 mg/Kg 57 28-120☼
Nitrobenzene ND 2.07 1.142 mg/Kg 55 19-120☼
2-Nitrophenol ND 2.07 1.191 mg/Kg 58 23-120☼
4-Nitrophenol ND 4.14 2.771 mg/Kg 67 16-139☼
N-Nitrosodi-n-propylamine ND 2.07 1.179 mg/Kg 57 24-120☼
Pentachlorophenol ND 4.14 3.211 mg/Kg 78 19-145☼
Phenanthrene ND 2.07 1.456 mg/Kg 70 21-122☼
Phenol ND 2.07 1.274 mg/Kg 62 15-120☼
Pyrene ND 2.07 1.494 mg/Kg 72 20-123☼
1,2,4-Trichlorobenzene ND 2.07 1.173 mg/Kg 57 14-120☼
2,4,5-Trichlorophenol ND 2.07 1.556 mg/Kg 75 27-120☼
2,4,6-Trichlorophenol ND 2.07 1.355 mg/Kg 66 24-122☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
55
MS MS
Qualifier Limits%Recovery
TestAmerica Nashville
Page 78 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SB-1 (0-2)Lab Sample ID: 490-114207-7 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
2-Fluorophenol (Surr)10 -120
Surrogate
48
MS MS
Qualifier Limits%Recovery
58Nitrobenzene-d5 (Surr)27 -120
55Phenol-d5 (Surr)10 -120
68Terphenyl-d14 (Surr)13 -120
692,4,6-Tribromophenol (Surr)10 -120
Client Sample ID: SB-1 (0-2)Lab Sample ID: 490-114207-7 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
Acenaphthene ND 2.08 1.060 mg/Kg 51 19-120 21 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Acenaphthylene ND 2.08 1.018 mg/Kg 49 25-120 26 50☼
Anthracene ND 2.08 1.060 mg/Kg 51 28-125 30 49☼
Benzo[a]anthracene ND 2.08 1.102 mg/Kg 53 23-120 28 50☼
Benzo[a]pyrene ND 2.08 1.083 mg/Kg 52 15-128 26 50☼
Benzo[b]fluoranthene ND 2.08 1.160 mg/Kg 56 12-133 21 50☼
Benzo[g,h,i]perylene ND 2.08 1.160 mg/Kg 56 22-120 28 50☼
Benzo[k]fluoranthene ND 2.08 1.086 mg/Kg 52 28-120 28 45☼
Bis(2-chloroethoxy)methane ND 2.08 0.8319 mg/Kg 40 24-120 26 50☼
Bis(2-chloroethyl)ether ND 2.08 0.7452 mg/Kg 36 22-120 38 50☼
bis (2-chloroisopropyl) ether ND 2.08 0.6611 mg/Kg 32 20-120 39 50☼
Bis(2-ethylhexyl) phthalate ND 2.08 1.027 mg/Kg 49 26-120 29 50☼
4-Bromophenyl phenyl ether ND 2.08 1.079 mg/Kg 52 31-120 28 37☼
Butyl benzyl phthalate ND 2.08 1.026 mg/Kg 49 24-133 29 50☼
Carbazole ND 2.08 1.049 mg/Kg 50 25-123 27 46☼
4-Chloroaniline ND 2.08 0.9609 mg/Kg 46 26-120 25 50☼
4-Chloro-3-methylphenol ND 2.08 1.143 mg/Kg 55 21-120 20 49☼
2-Chloronaphthalene ND 2.08 0.9814 mg/Kg 47 24-120 24 50☼
2-Chlorophenol ND 2.08 0.8254 mg/Kg 40 25-120 35 50☼
4-Chlorophenyl phenyl ether ND 2.08 1.064 mg/Kg 51 26-120 23 50☼
Chrysene ND 2.08 1.081 mg/Kg 52 20-120 30 49☼
Cresols ND 4.16 1.943 mg/Kg 47 10-200 30 50☼
Dibenz(a,h)anthracene ND 2.08 1.147 mg/Kg 55 12-128 29 50☼
Dibenzofuran ND 2.08 1.054 mg/Kg 51 21-120 20 50☼
1,2-Dichlorobenzene ND 2.08 0.8020 mg/Kg 39 10-120 39 50☼
1,3-Dichlorobenzene ND 2.08 0.7819 mg/Kg 38 10-120 41 50☼
1,4-Dichlorobenzene ND 2.08 0.7816 mg/Kg 38 10-120 38 50☼
3,3'-Dichlorobenzidine ND 2.08 0.9326 mg/Kg 45 10-120 15 50☼
2,4-Dichlorophenol ND 2.08 1.001 mg/Kg 48 17-120 25 50☼
Diethyl phthalate ND 2.08 1.060 mg/Kg 51 29-122 25 45☼
2,4-Dimethylphenol ND 2.08 1.031 mg/Kg 50 17-120 28 50☼
Dimethyl phthalate ND 2.08 1.046 mg/Kg 50 30-120 23 46☼
Di-n-butyl phthalate ND 2.08 1.014 mg/Kg 49 29-126 32 49☼
4,6-Dinitro-2-methylphenol ND 4.16 0.9934 mg/Kg 24 10-134 44 50☼
2,4-Dinitrophenol ND 4.16 0.8196 mg/Kg 20 10-150 40 50☼
2,4-Dinitrotoluene ND 2.08 1.077 mg/Kg 52 24-121 20 50☼
2,6-Dinitrotoluene ND 2.08 1.008 mg/Kg 48 24-120 25 50☼
TestAmerica Nashville
Page 79 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: SB-1 (0-2)Lab Sample ID: 490-114207-7 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380030 Prep Batch: 379832
Di-n-octyl phthalate ND 2.08 1.084 mg/Kg 52 27-130 26 50☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Fluoranthene ND 2.08 1.079 mg/Kg 52 10-143 29 50☼
Fluorene ND 2.08 1.045 mg/Kg 50 20-120 25 50☼
Hexachlorobenzene ND 2.08 1.066 mg/Kg 51 25-120 31 50☼
Hexachlorobutadiene ND 2.08 0.8748 mg/Kg 42 10-120 32 50☼
Hexachlorocyclopentadiene ND 2.08 0.4335 mg/Kg 21 10-120 41 50☼
Hexachloroethane ND 2.08 0.7790 mg/Kg 37 10-120 42 50☼
Indeno[1,2,3-cd]pyrene ND 2.08 1.109 mg/Kg 53 22-121 30 50☼
Isophorone ND 2.08 0.9010 mg/Kg 43 24-120 24 50☼
1-Methylnaphthalene ND 2.08 0.9728 mg/Kg 47 10-120 24 50☼
2-Methylnaphthalene ND 2.08 0.9498 mg/Kg 46 13-120 27 50☼
2-Methylphenol ND 2.08 0.9609 mg/Kg 46 23-120 33 50☼
3 & 4 Methylphenol ND 2.08 0.9816 mg/Kg 47 19-120 27 50☼
Naphthalene ND 2.08 0.8673 mg/Kg 42 10-120 31 50☼
2-Nitroaniline ND 2.08 1.036 mg/Kg 50 31-120 27 50☼
3-Nitroaniline ND 2.08 1.037 mg/Kg 50 31-120 25 49☼
4-Nitroaniline ND 2.08 0.9536 mg/Kg 46 28-120 22 49☼
Nitrobenzene ND 2.08 0.8231 mg/Kg 40 19-120 32 50☼
2-Nitrophenol ND 2.08 0.9007 mg/Kg 43 23-120 28 50☼
4-Nitrophenol ND 4.16 2.114 mg/Kg 51 16-139 27 45☼
N-Nitrosodi-n-propylamine ND 2.08 0.8555 mg/Kg 41 24-120 32 50☼
Pentachlorophenol ND 4.16 2.305 mg/Kg 55 19-145 33 50☼
Phenanthrene ND 2.08 1.064 mg/Kg 51 21-122 31 50☼
Phenol ND 2.08 0.8736 mg/Kg 42 15-120 37 50☼
Pyrene ND 2.08 1.121 mg/Kg 54 20-123 28 50☼
1,2,4-Trichlorobenzene ND 2.08 0.8433 mg/Kg 41 14-120 33 50☼
2,4,5-Trichlorophenol ND 2.08 1.201 mg/Kg 58 27-120 26 50☼
2,4,6-Trichlorophenol ND 2.08 1.085 mg/Kg 52 24-122 22 50☼
2-Fluorobiphenyl (Surr)29 -120
Surrogate
45
MSD MSD
Qualifier Limits%Recovery
352-Fluorophenol (Surr)10 -120
42Nitrobenzene-d5 (Surr)27 -120
40Phenol-d5 (Surr)10 -120
53Terphenyl-d14 (Surr)13 -120
532,4,6-Tribromophenol (Surr)10 -120
Method: 8330A - Nitroaromatics and Nitramines
Client Sample ID: Method BlankLab Sample ID: MB 280-347627/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 348204 Prep Batch: 347627
RL MDL
2,4-diamino-6-nitrotoluene ND 1.00 ug/L 10/21/16 16:35 10/25/16 09:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.200 ug/L 10/21/16 16:35 10/25/16 09:50 12-Amino-4,6-dinitrotoluene
ND 1.00 ug/L 10/21/16 16:35 10/25/16 09:50 12,6-diamino-4-nitrotoluene
ND 0.200 ug/L 10/21/16 16:35 10/25/16 09:50 14-Amino-2,6-dinitrotoluene
TestAmerica Nashville
Page 80 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8330A - Nitroaromatics and Nitramines (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-347627/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 348204 Prep Batch: 347627
RL MDL
2,4-Dinitrotoluene ND 0.400 ug/L 10/21/16 16:35 10/25/16 09:50 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.200 ug/L 10/21/16 16:35 10/25/16 09:50 12,6-Dinitrotoluene
ND 0.400 ug/L 10/21/16 16:35 10/25/16 09:50 1m-Nitrotoluene
ND 0.400 ug/L 10/21/16 16:35 10/25/16 09:50 1Nitrobenzene
ND 3.00 ug/L 10/21/16 16:35 10/25/16 09:50 1Nitroglycerin
ND 0.400 ug/L 10/21/16 16:35 10/25/16 09:50 1o-Nitrotoluene
ND 0.400 ug/L 10/21/16 16:35 10/25/16 09:50 11,3-Dinitrobenzene
ND 0.400 ug/L 10/21/16 16:35 10/25/16 09:50 1HMX
ND 1.00 ug/L 10/21/16 16:35 10/25/16 09:50 1p-Nitrotoluene
ND 0.200 ug/L 10/21/16 16:35 10/25/16 09:50 1RDX
ND 0.200 ug/L 10/21/16 16:35 10/25/16 09:50 1Tetryl
ND 1.00 ug/L 10/21/16 16:35 10/25/16 09:50 11,3,5-Trinitrobenzene
ND 2.00 ug/L 10/21/16 16:35 10/25/16 09:50 1PETN
ND 0.400 ug/L 10/21/16 16:35 10/25/16 09:50 12,4,6-Trinitrotoluene
ND 2.00 ug/L 10/21/16 16:35 10/25/16 09:50 1Picric acid
1,2-Dinitrobenzene 80 75-118 10/25/16 09:50 1
MB MB
Surrogate
10/21/16 16:35
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-347627/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 348204 Prep Batch: 347627
2-Amino-4,6-dinitrotoluene 2.00 1.390 ug/L 70 57-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Amino-2,6-dinitrotoluene 2.00 1.390 ug/L 70 67-127
2,4-Dinitrotoluene 2.00 1.492 ug/L 75 68-120
2,6-Dinitrotoluene 2.00 1.420 ug/L 71 67-120
m-Nitrotoluene 2.00 1.229 ug/L 61 57-124
Nitrobenzene 2.00 1.421 ug/L 71 59-120
Nitroglycerin 20.0 16.64 ug/L 83 72-120
o-Nitrotoluene 2.00 1.210 ug/L 61 49-124
1,3-Dinitrobenzene 2.00 1.678 ug/L 84 73-120
HMX 2.00 1.608 ug/L 80 79-120
p-Nitrotoluene 2.00 1.335 ug/L 67 25-141
RDX 2.00 1.812 ug/L 91 79-120
Tetryl 2.00 1.501 ug/L 75 10-120
1,3,5-Trinitrobenzene 2.00 1.700 ug/L 85 73-120
PETN 20.0 16.44 ug/L 82 73-126
2,4,6-Trinitrotoluene 2.00 1.689 ug/L 84 74-120
Picric acid 2.00 1.712 J ug/L 86 80-120
1,2-Dinitrobenzene 75 -118
Surrogate
82
LCS LCS
Qualifier Limits%Recovery
TestAmerica Nashville
Page 81 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8330A - Nitroaromatics and Nitramines (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-347627/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 348204 Prep Batch: 347627
2-Amino-4,6-dinitrotoluene 2.00 1.331 ug/L 67 57-120 4 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
4-Amino-2,6-dinitrotoluene 2.00 1.340 ug/L 67 67-127 4 20
2,4-Dinitrotoluene 2.00 1.474 ug/L 74 68-120 1 20
2,6-Dinitrotoluene 2.00 1.406 ug/L 70 67-120 1 20
m-Nitrotoluene 2.00 1.204 ug/L 60 57-124 2 20
Nitrobenzene 2.00 1.389 ug/L 69 59-120 2 20
Nitroglycerin 20.0 16.61 ug/L 83 72-120 0 20
o-Nitrotoluene 2.00 1.206 ug/L 60 49-124 0 31
1,3-Dinitrobenzene 2.00 1.663 ug/L 83 73-120 1 20
HMX 2.00 1.574 ug/L 79 79-120 2 20
p-Nitrotoluene 2.00 1.335 ug/L 67 25-141 0 30
RDX 2.00 1.799 ug/L 90 79-120 1 20
Tetryl 2.00 1.484 ug/L 74 10-120 1 50
1,3,5-Trinitrobenzene 2.00 1.670 ug/L 83 73-120 2 20
PETN 20.0 15.98 ug/L 80 73-126 3 20
2,4,6-Trinitrotoluene 2.00 1.677 ug/L 84 74-120 1 20
Picric acid 2.00 1.749 J ug/L 87 80-120 2 20
1,2-Dinitrobenzene 75 -118
Surrogate
80
LCSD LCSD
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 280-89654-A-3-A MS
Matrix: Water Prep Type: Total/NA
Analysis Batch: 348204 Prep Batch: 347627
2-Amino-4,6-dinitrotoluene ND F1 2.19 1.326 ug/L 61 57-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Amino-2,6-dinitrotoluene ND F1 2.19 1.281 F1 ug/L 59 67-127
2,4-Dinitrotoluene ND F1 2.19 1.491 ug/L 68 68-120
2,6-Dinitrotoluene ND F1 2.19 1.425 F1 ug/L 65 67-120
m-Nitrotoluene ND F1 2.19 1.203 F1 ug/L 55 57-124
Nitrobenzene ND 2.19 1.410 ug/L 64 59-120
Nitroglycerin ND 21.9 21.63 ug/L 99 72-120
o-Nitrotoluene ND 2.19 1.184 ug/L 54 49-124
1,3-Dinitrobenzene ND 2.19 1.719 ug/L 79 73-120
HMX ND F1 2.19 1.705 F1 ug/L 78 79-120
p-Nitrotoluene ND 2.19 1.390 ug/L 64 25-141
RDX 0.254 F1 2.19 1.944 F1 ug/L 77 79-120
Tetryl ND 2.19 1.613 ug/L 74 10-120
1,3,5-Trinitrobenzene ND 2.19 1.763 ug/L 81 73-120
PETN ND 21.9 17.18 ug/L 79 73-126
2,4,6-Trinitrotoluene ND 2.19 1.743 ug/L 80 74-120
Picric acid ND F1 2.19 ND F1 ug/L 77 80-120
1,2-Dinitrobenzene 75 -118
Surrogate
76
MS MS
Qualifier Limits%Recovery
TestAmerica Nashville
Page 82 of 108 6/26/2018 (Rev. 1)
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8330A - Nitroaromatics and Nitramines (Continued)
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-89654-C-3-A MSD
Matrix: Water Prep Type: Total/NA
Analysis Batch: 348204 Prep Batch: 347627
2-Amino-4,6-dinitrotoluene ND F1 2.15 1.205 F1 ug/L 56 57-120 10 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Amino-2,6-dinitrotoluene ND F1 2.15 1.165 F1 ug/L 54 67-127 9 20
2,4-Dinitrotoluene ND F1 2.15 1.385 F1 ug/L 64 68-120 7 20
2,6-Dinitrotoluene ND F1 2.15 1.362 F1 ug/L 63 67-120 5 20
m-Nitrotoluene ND F1 2.15 1.204 F1 ug/L 56 57-124 0 20
Nitrobenzene ND 2.15 1.321 ug/L 61 59-120 7 20
Nitroglycerin ND 21.5 20.81 ug/L 97 72-120 4 20
o-Nitrotoluene ND 2.15 1.086 ug/L 50 49-124 9 31
1,3-Dinitrobenzene ND 2.15 1.621 ug/L 75 73-120 6 20
HMX ND F1 2.15 1.592 F1 ug/L 74 79-120 7 20
p-Nitrotoluene ND 2.15 1.238 ug/L 57 25-141 12 30
RDX 0.254 F1 2.15 1.804 F1 ug/L 72 79-120 7 20
Tetryl ND 2.15 1.522 ug/L 71 10-120 6 50
1,3,5-Trinitrobenzene ND 2.15 1.671 ug/L 78 73-120 5 20
PETN ND 21.5 16.28 ug/L 76 73-126 5 20
2,4,6-Trinitrotoluene ND 2.15 1.639 ug/L 76 74-120 6 20
Picric acid ND F1 2.15 ND F1 ug/L 74 80-120 5 20
1,2-Dinitrobenzene X 75 -118
Surrogate
73
MSD MSD
Qualifier Limits%Recovery
Client Sample ID: Method BlankLab Sample ID: MB 280-348557/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 349225 Prep Batch: 348557
RL MDL
2,4-diamino-6-nitrotoluene ND 2.00 mg/Kg 10/27/16 14:58 11/01/16 14:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 12-Amino-4,6-dinitrotoluene
ND 2.00 mg/Kg 10/27/16 14:58 11/01/16 14:12 12,6-diamino-4-nitrotoluene
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 14-Amino-2,6-dinitrotoluene
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 12,4-Dinitrotoluene
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 12,6-Dinitrotoluene
ND 0.500 mg/Kg 10/27/16 14:58 11/01/16 14:12 1m-Nitrotoluene
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 1Nitrobenzene
ND 5.10 mg/Kg 10/27/16 14:58 11/01/16 14:12 1Nitroglycerin
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 1o-Nitrotoluene
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 11,3-Dinitrobenzene
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 1HMX
ND 0.400 mg/Kg 10/27/16 14:58 11/01/16 14:12 1p-Nitrotoluene
ND 0.260 mg/Kg 10/27/16 14:58 11/01/16 14:12 1RDX
ND 0.500 mg/Kg 10/27/16 14:58 11/01/16 14:12 1Tetryl
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 11,3,5-Trinitrobenzene
ND 4.00 mg/Kg 10/27/16 14:58 11/01/16 14:12 1PETN
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 12,4,6-Trinitrotoluene
ND 0.250 mg/Kg 10/27/16 14:58 11/01/16 14:12 1Picric acid
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8330A - Nitroaromatics and Nitramines (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-348557/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 349225 Prep Batch: 348557
1,2-Dinitrobenzene 109 83-122 11/01/16 14:12 1
MB MB
Surrogate
10/27/16 14:58
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-348557/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 349225 Prep Batch: 348557
2-Amino-4,6-dinitrotoluene 2.50 2.494 mg/Kg 100 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
4-Amino-2,6-dinitrotoluene 2.50 2.568 mg/Kg 103 80-120
2,4-Dinitrotoluene 2.50 2.521 mg/Kg 101 80-120
2,6-Dinitrotoluene 2.50 2.439 mg/Kg 98 80-120
m-Nitrotoluene 2.50 2.599 mg/Kg 104 80-120
Nitrobenzene 2.50 2.557 mg/Kg 102 80-120
Nitroglycerin 25.0 24.55 mg/Kg 98 80-120
o-Nitrotoluene 2.50 2.535 mg/Kg 101 80-120
1,3-Dinitrobenzene 2.50 2.665 mg/Kg 107 80-120
HMX 2.50 2.293 mg/Kg 92 80-120
p-Nitrotoluene 2.50 2.596 mg/Kg 104 80-120
RDX 2.50 2.444 mg/Kg 98 80-120
Tetryl 2.50 2.517 mg/Kg 101 80-120
1,3,5-Trinitrobenzene 2.50 2.518 mg/Kg 101 80-120
PETN 25.0 24.93 mg/Kg 100 80-120
2,4,6-Trinitrotoluene 2.50 2.645 mg/Kg 106 80-120
Picric acid 2.50 2.581 mg/Kg 103 80-120
1,2-Dinitrobenzene 83 -122
Surrogate
103
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Matrix SpikeLab Sample ID: 280-89897-B-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 349025 Prep Batch: 348557
2-Amino-4,6-dinitrotoluene ND 2.34 2.085 mg/Kg 89 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
4-Amino-2,6-dinitrotoluene ND 2.34 2.138 mg/Kg 92 80-120
2,4-Dinitrotoluene ND 2.34 2.279 mg/Kg 98 80-120
2,6-Dinitrotoluene ND 2.34 2.318 mg/Kg 99 80-120
m-Nitrotoluene ND 2.34 2.373 mg/Kg 102 80-120
Nitrobenzene ND 2.34 2.291 mg/Kg 98 80-120
Nitroglycerin ND 23.4 22.60 mg/Kg 97 80-120
o-Nitrotoluene ND 2.34 2.324 mg/Kg 99 80-120
1,3-Dinitrobenzene ND 2.34 2.389 mg/Kg 102 80-120
HMX ND 2.34 2.083 mg/Kg 89 80-120
p-Nitrotoluene ND 2.34 2.339 mg/Kg 100 80-120
RDX ND 2.34 2.159 mg/Kg 92 80-120
Tetryl ND 2.34 2.493 mg/Kg 107 80-120
1,3,5-Trinitrobenzene ND 2.34 2.353 mg/Kg 101 80-120
PETN ND 23.4 23.37 mg/Kg 100 80-120
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 8330A - Nitroaromatics and Nitramines (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 280-89897-B-1-E MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 349025 Prep Batch: 348557
2,4,6-Trinitrotoluene 1.25 F1 F2 2.34 3.870 mg/Kg 112 80-120
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Picric acid ND F1 2.34 1.210 F1 mg/Kg 52 80-120
1,2-Dinitrobenzene 83 -122
Surrogate
102
MS MS
Qualifier Limits%Recovery
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 280-89897-B-1-F MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 349025 Prep Batch: 348557
2-Amino-4,6-dinitrotoluene ND 2.27 2.077 mg/Kg 91 80-120 0 20
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
4-Amino-2,6-dinitrotoluene ND 2.27 2.114 mg/Kg 93 80-120 1 20
2,4-Dinitrotoluene ND 2.27 2.253 mg/Kg 99 80-120 1 20
2,6-Dinitrotoluene ND 2.27 2.226 mg/Kg 98 80-120 4 20
m-Nitrotoluene ND 2.27 2.345 mg/Kg 103 80-120 1 20
Nitrobenzene ND 2.27 2.253 mg/Kg 99 80-120 2 20
Nitroglycerin ND 22.7 22.08 mg/Kg 97 80-120 2 20
o-Nitrotoluene ND 2.27 2.247 mg/Kg 99 80-120 3 20
1,3-Dinitrobenzene ND 2.27 2.358 mg/Kg 104 80-120 1 20
HMX ND 2.27 2.054 mg/Kg 90 80-120 1 20
p-Nitrotoluene ND 2.27 2.311 mg/Kg 102 80-120 1 20
RDX ND 2.27 2.127 mg/Kg 94 80-120 1 20
Tetryl ND 2.27 2.372 mg/Kg 104 80-120 5 20
1,3,5-Trinitrobenzene ND 2.27 2.320 mg/Kg 102 80-120 1 20
PETN ND 22.7 22.68 mg/Kg 100 80-120 3 20
2,4,6-Trinitrotoluene 1.25 F1 F2 2.27 5.622 F1 F2 mg/Kg 193 80-120 37 20
Picric acid ND F1 2.27 1.095 F1 mg/Kg 48 80-120 10 20
1,2-Dinitrobenzene 83 -122
Surrogate
103
MSD MSD
Qualifier Limits%Recovery
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 490-379801/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380098 Prep Batch: 379801
RL MDL
Antimony <0.958 9.58 0.958 mg/Kg 10/20/16 10:21 10/21/16 00:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.15 1.151.92 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Arsenic
<0.192 0.1920.958 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Beryllium
<0.0958 0.09580.958 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Cadmium
<0.862 0.8620.958 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Chromium
<1.05 1.051.92 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Copper
<0.479 0.4790.958 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Lead
<0.958 0.9582.87 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Manganese
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 490-379801/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380098 Prep Batch: 379801
RL MDL
Nickel <0.575 1.92 0.575 mg/Kg 10/20/16 10:21 10/21/16 00:38 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
<1.05 1.051.92 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Selenium
<0.383 0.3830.958 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Silver
<0.575 0.5751.92 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Thallium
<4.79 4.799.58 mg/Kg 10/20/16 10:21 10/21/16 00:38 1Zinc
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379801/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380098 Prep Batch: 379801
Antimony 39.2 36.59 mg/Kg 93 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Arsenic 19.6 16.75 mg/Kg 85 80-120
Beryllium 19.6 19.27 mg/Kg 98 80-120
Cadmium 19.6 18.65 mg/Kg 95 80-120
Chromium 78.4 79.86 mg/Kg 102 80-120
Copper 98.0 95.39 mg/Kg 97 80-120
Lead 19.6 18.80 mg/Kg 96 80-120
Manganese 196 190.2 mg/Kg 97 80-120
Nickel 196 187.9 mg/Kg 96 80-120
Selenium 19.6 17.41 mg/Kg 89 80-120
Silver 19.6 16.98 mg/Kg 87 80-120
Thallium 118 104.1 mg/Kg 88 80-120
Zinc 196 182.1 mg/Kg 93 80-120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 490-379801/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380098 Prep Batch: 379801
Antimony 38.8 36.74 mg/Kg 95 80-120 0 20
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Arsenic 19.4 17.89 mg/Kg 92 80-120 7 20
Beryllium 19.4 19.44 mg/Kg 100 80-120 1 20
Cadmium 19.4 18.95 mg/Kg 98 80-120 2 20
Chromium 77.5 80.78 mg/Kg 104 80-120 1 20
Copper 96.9 95.87 mg/Kg 99 80-120 1 20
Lead 19.4 18.95 mg/Kg 98 80-120 1 20
Manganese 194 192.6 mg/Kg 99 80-120 1 20
Nickel 194 188.3 mg/Kg 97 80-120 0 20
Selenium 19.4 18.41 mg/Kg 95 80-120 6 20
Silver 19.4 17.21 mg/Kg 89 80-120 1 20
Thallium 116 103.3 mg/Kg 89 80-120 1 20
Zinc 194 184.7 mg/Kg 95 80-120 1 20
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Matrix SpikeLab Sample ID: 490-114010-F-3-B MS
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380098 Prep Batch: 379801
Antimony 1.51 J 48.6 45.13 mg/Kg 90 75-125☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic 5.86 24.3 26.76 mg/Kg 86 75-125☼
Beryllium 0.317 J 24.3 23.38 mg/Kg 95 75-125☼
Cadmium 1.61 24.3 23.84 mg/Kg 91 75-125☼
Chromium 54.7 97.2 161.1 mg/Kg 109 75-125☼
Copper 15.6 122 136.1 mg/Kg 99 75-125☼
Lead 69.6 F1 24.3 90.02 mg/Kg 84 75-125☼
Manganese 281 F1 243 499.9 mg/Kg 90 75-125☼
Nickel 7.44 243 228.7 mg/Kg 91 75-125☼
Selenium <1.34 24.3 18.86 mg/Kg 78 75-125☼
Silver <0.488 24.3 20.90 mg/Kg 86 75-125☼
Thallium <0.732 F1 146 107.8 F1 mg/Kg 74 75-125☼
Zinc 22.1 243 240.5 mg/Kg 90 75-125☼
Client Sample ID: Matrix Spike DuplicateLab Sample ID: 490-114010-F-3-C MSD
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380098 Prep Batch: 379801
Antimony 1.51 J 50.4 46.23 mg/Kg 89 75-125 2 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Arsenic 5.86 25.2 26.97 mg/Kg 84 75-125 1 20☼
Beryllium 0.317 J 25.2 24.25 mg/Kg 95 75-125 4 20☼
Cadmium 1.61 25.2 24.55 mg/Kg 91 75-125 3 20☼
Chromium 54.7 101 150.0 mg/Kg 95 75-125 7 20☼
Copper 15.6 126 140.0 mg/Kg 99 75-125 3 20☼
Lead 69.6 F1 25.2 78.14 F1 mg/Kg 34 75-125 14 20☼
Manganese 281 F1 252 408.7 F1 mg/Kg 51 75-125 20 20☼
Nickel 7.44 252 236.8 mg/Kg 91 75-125 3 20☼
Selenium <1.34 25.2 21.40 mg/Kg 85 75-125 13 20☼
Silver <0.488 25.2 21.63 mg/Kg 86 75-125 3 20☼
Thallium <0.732 F1 151 117.0 mg/Kg 77 75-125 8 20☼
Zinc 22.1 252 246.5 mg/Kg 89 75-125 2 20☼
Method: 7471B - Mercury (CVAA)
Client Sample ID: Method BlankLab Sample ID: MB 490-379858/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379858
RL MDL
Mercury ND 0.100 mg/Kg 10/20/16 11:45 10/21/16 07:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379858/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379858
Mercury 0.160 0.1411 mg/Kg 88 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
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QC Sample Results
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method: 7471B - Mercury (CVAA) (Continued)
Client Sample ID: SB-4 (0-2)Lab Sample ID: 490-114207-1 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379858
Mercury ND 0.189 0.1761 mg/Kg 93 80-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: SB-4 (0-2)Lab Sample ID: 490-114207-1 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379858
Mercury ND 0.194 0.1772 mg/Kg 91 80-120 1 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Client Sample ID: Method BlankLab Sample ID: MB 490-379915/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379915
RL MDL
Mercury ND 0.0960 mg/Kg 10/20/16 13:47 10/21/16 08:40 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 490-379915/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379915
Mercury 0.161 0.1628 mg/Kg 101 80-120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Client Sample ID: SB-10 (2-4)Lab Sample ID: 490-114207-10 MS
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379915
Mercury ND 0.198 0.1623 mg/Kg 82 80-120☼
Analyte
MS MS
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: SB-10 (2-4)Lab Sample ID: 490-114207-10 MSD
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 380139 Prep Batch: 379915
Mercury ND 0.197 0.1666 mg/Kg 85 80-120 3 20☼
Analyte
MSD MSD
DUnitResultQualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits LimitRPD
RPD
Method: Moisture - Percent Moisture
Client Sample ID: SB-5 (0-2)Lab Sample ID: 490-114207-2 DU
Matrix: Soil Prep Type: Total/NA
Analysis Batch: 379206
Percent Solids 62.9 58.8 %5 20
Analyte
DU DU
DUnitResultQualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
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QC Association Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
GC/MS VOA
Prep Batch: 379444
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035490-114207-4 SB-9 (0-2)Total/NA
Prep Batch: 379446
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 5035490-114207-1 SB-4 (0-2)Total/NA
Soil 5035490-114207-2 SB-5 (0-2)Total/NA
Soil 5035490-114207-3 SB-6 (0-2)Total/NA
Soil 5035490-114207-4 SB-9 (0-2)Total/NA
Soil 5035490-114207-5 SB-8 (0-2)Total/NA
Soil 5035490-114207-6 SB-7 (4-6)Total/NA
Soil 5035490-114207-7 SB-1 (0-2)Total/NA
Soil 5035490-114207-8 SB-2 (4-6)Total/NA
Soil 5035490-114207-9 SB-3 (8-10)Total/NA
Soil 5035490-114207-10 SB-10 (2-4)Total/NA
Analysis Batch: 380000
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 379446490-114207-1 SB-4 (0-2)Total/NA
Soil 8260B 379446490-114207-2 SB-5 (0-2)Total/NA
Soil 8260B 379446490-114207-3 SB-6 (0-2)Total/NA
Soil 8260B 379446490-114207-4 SB-9 (0-2)Total/NA
Soil 8260B 379446490-114207-5 SB-8 (0-2)Total/NA
Soil 8260B 379446490-114207-6 SB-7 (4-6)Total/NA
Soil 8260B 379446490-114207-7 SB-1 (0-2)Total/NA
Soil 8260B 379446490-114207-8 SB-2 (4-6)Total/NA
Soil 8260B 379446490-114207-9 SB-3 (8-10)Total/NA
Soil 8260B 379446490-114207-10 SB-10 (2-4)Total/NA
Solid 8260BMB 490-380000/7 Method Blank Total/NA
Solid 8260BLCS 490-380000/4 Lab Control Sample Total/NA
Solid 8260BLCSD 490-380000/5 Lab Control Sample Dup Total/NA
Analysis Batch: 380458
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260B490-114207-11 TMW-2 Total/NA
Water 8260BMB 490-380458/8 Method Blank Total/NA
Water 8260BLCS 490-380458/4 Lab Control Sample Total/NA
Water 8260BLCSD 490-380458/5 Lab Control Sample Dup Total/NA
Water 8260B490-114207-11 MS TMW-2 Total/NA
Water 8260B490-114207-11 MSD TMW-2 Total/NA
Analysis Batch: 380848
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8260B 379444490-114207-4 SB-9 (0-2)Total/NA
Solid 8260BMB 490-380848/8 Method Blank Total/NA
Solid 8260BLCS 490-380848/5 Lab Control Sample Total/NA
Solid 8260BLCSD 490-380848/6 Lab Control Sample Dup Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
GC/MS Semi VOA
Prep Batch: 379813
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3550C490-114207-1 SB-4 (0-2)Total/NA
Soil 3550C490-114207-2 SB-5 (0-2)Total/NA
Soil 3550C490-114207-3 SB-6 (0-2)Total/NA
Soil 3550C490-114207-4 SB-9 (0-2)Total/NA
Soil 3550C490-114207-5 SB-8 (0-2)Total/NA
Soil 3550C490-114207-6 SB-7 (4-6)Total/NA
Solid 3550CMB 490-379813/1-A Method Blank Total/NA
Solid 3550CLCS 490-379813/2-A Lab Control Sample Total/NA
Solid 3550C490-114146-A-1-B MS Matrix Spike Total/NA
Solid 3550C490-114146-A-1-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 379832
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3550C490-114207-7 SB-1 (0-2)Total/NA
Soil 3550C490-114207-8 SB-2 (4-6)Total/NA
Soil 3550C490-114207-9 SB-3 (8-10)Total/NA
Soil 3550C490-114207-10 SB-10 (2-4)Total/NA
Solid 3550CMB 490-379832/1-A Method Blank Total/NA
Solid 3550CLCS 490-379832/2-A Lab Control Sample Total/NA
Soil 3550C490-114207-7 MS SB-1 (0-2)Total/NA
Soil 3550C490-114207-7 MSD SB-1 (0-2)Total/NA
Analysis Batch: 380030
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270D 379832490-114207-7 SB-1 (0-2)Total/NA
Soil 8270D 379832490-114207-8 SB-2 (4-6)Total/NA
Soil 8270D 379832490-114207-9 SB-3 (8-10)Total/NA
Soil 8270D 379832490-114207-10 SB-10 (2-4)Total/NA
Solid 8270D 379832MB 490-379832/1-A Method Blank Total/NA
Solid 8270D 379832LCS 490-379832/2-A Lab Control Sample Total/NA
Soil 8270D 379832490-114207-7 MS SB-1 (0-2)Total/NA
Soil 8270D 379832490-114207-7 MSD SB-1 (0-2)Total/NA
Analysis Batch: 380971
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270D 379813MB 490-379813/1-A Method Blank Total/NA
Solid 8270D 379813LCS 490-379813/2-A Lab Control Sample Total/NA
Solid 8270D 379813490-114146-A-1-B MS Matrix Spike Total/NA
Solid 8270D 379813490-114146-A-1-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 381549
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8270D 379813490-114207-1 SB-4 (0-2)Total/NA
Soil 8270D 379813490-114207-2 SB-5 (0-2)Total/NA
Soil 8270D 379813490-114207-3 SB-6 (0-2)Total/NA
Soil 8270D 379813490-114207-4 SB-9 (0-2)Total/NA
Soil 8270D 379813490-114207-5 SB-8 (0-2)Total/NA
Soil 8270D 379813490-114207-6 SB-7 (4-6)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
HPLC/IC
Prep Batch: 347627
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3535490-114207-11 TMW-2 Total/NA
Water 3535MB 280-347627/1-A Method Blank Total/NA
Water 3535LCS 280-347627/2-A Lab Control Sample Total/NA
Water 3535LCSD 280-347627/3-A Lab Control Sample Dup Total/NA
Water 3535280-89654-A-3-A MS Matrix Spike Total/NA
Water 3535280-89654-C-3-A MSD Matrix Spike Duplicate Total/NA
Drying Batch: 348094
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Prep/Air Dry280-89897-B-1-E MS Matrix Spike Total/NA
Solid Prep/Air Dry280-89897-B-1-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 348204
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8330A 347627490-114207-11 TMW-2 Total/NA
Water 8330A 347627MB 280-347627/1-A Method Blank Total/NA
Water 8330A 347627LCS 280-347627/2-A Lab Control Sample Total/NA
Water 8330A 347627LCSD 280-347627/3-A Lab Control Sample Dup Total/NA
Water 8330A 347627280-89654-A-3-A MS Matrix Spike Total/NA
Water 8330A 347627280-89654-C-3-A MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 348206
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8330A 347627490-114207-11 TMW-2 Total/NA
Drying Batch: 348351
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Prep/Air Dry490-114207-1 SB-4 (0-2)Total/NA
Soil Prep/Air Dry490-114207-2 SB-5 (0-2)Total/NA
Soil Prep/Air Dry490-114207-3 SB-6 (0-2)Total/NA
Soil Prep/Air Dry490-114207-4 SB-9 (0-2)Total/NA
Soil Prep/Air Dry490-114207-5 SB-8 (0-2)Total/NA
Soil Prep/Air Dry490-114207-6 SB-7 (4-6)Total/NA
Soil Prep/Air Dry490-114207-7 SB-1 (0-2)Total/NA
Soil Prep/Air Dry490-114207-8 SB-2 (4-6)Total/NA
Soil Prep/Air Dry490-114207-9 SB-3 (8-10)Total/NA
Soil Prep/Air Dry490-114207-10 SB-10 (2-4)Total/NA
Prep Batch: 348557
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Sieve/Ultrasoni 348351490-114207-1 SB-4 (0-2)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-2 SB-5 (0-2)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-3 SB-6 (0-2)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-4 SB-9 (0-2)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-5 SB-8 (0-2)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-6 SB-7 (4-6)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-7 SB-1 (0-2)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-8 SB-2 (4-6)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-9 SB-3 (8-10)Total/NA
Soil Sieve/Ultrasoni 348351490-114207-10 SB-10 (2-4)Total/NA
Solid Sieve/UltrasoniMB 280-348557/1-A Method Blank Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
HPLC/IC (Continued)
Prep Batch: 348557 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Sieve/UltrasoniLCS 280-348557/2-A Lab Control Sample Total/NA
Solid Sieve/Ultrasoni 348094280-89897-B-1-E MS Matrix Spike Total/NA
Solid Sieve/Ultrasoni 348094280-89897-B-1-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 349025
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8330A 348557490-114207-2 SB-5 (0-2)Total/NA
Soil 8330A 348557490-114207-3 SB-6 (0-2)Total/NA
Soil 8330A 348557490-114207-4 SB-9 (0-2)Total/NA
Soil 8330A 348557490-114207-5 SB-8 (0-2)Total/NA
Soil 8330A 348557490-114207-6 SB-7 (4-6)Total/NA
Soil 8330A 348557490-114207-7 SB-1 (0-2)Total/NA
Soil 8330A 348557490-114207-8 SB-2 (4-6)Total/NA
Soil 8330A 348557490-114207-9 SB-3 (8-10)Total/NA
Soil 8330A 348557490-114207-10 SB-10 (2-4)Total/NA
Solid 8330A 348557280-89897-B-1-E MS Matrix Spike Total/NA
Solid 8330A 348557280-89897-B-1-F MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 349225
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 8330A 348557490-114207-1 SB-4 (0-2)Total/NA
Solid 8330A 348557MB 280-348557/1-A Method Blank Total/NA
Solid 8330A 348557LCS 280-348557/2-A Lab Control Sample Total/NA
Metals
Prep Batch: 379801
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 3051A490-114207-1 SB-4 (0-2)Total/NA
Soil 3051A490-114207-2 SB-5 (0-2)Total/NA
Soil 3051A490-114207-3 SB-6 (0-2)Total/NA
Soil 3051A490-114207-4 SB-9 (0-2)Total/NA
Soil 3051A490-114207-5 SB-8 (0-2)Total/NA
Soil 3051A490-114207-6 SB-7 (4-6)Total/NA
Soil 3051A490-114207-7 SB-1 (0-2)Total/NA
Soil 3051A490-114207-8 SB-2 (4-6)Total/NA
Soil 3051A490-114207-9 SB-3 (8-10)Total/NA
Soil 3051A490-114207-10 SB-10 (2-4)Total/NA
Solid 3051AMB 490-379801/1-A Method Blank Total/NA
Solid 3051ALCS 490-379801/2-A Lab Control Sample Total/NA
Solid 3051ALCSD 490-379801/3-A Lab Control Sample Dup Total/NA
Solid 3051A490-114010-F-3-B MS Matrix Spike Total/NA
Solid 3051A490-114010-F-3-C MSD Matrix Spike Duplicate Total/NA
Prep Batch: 379858
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B490-114207-1 SB-4 (0-2)Total/NA
Soil 7471B490-114207-2 SB-5 (0-2)Total/NA
Soil 7471B490-114207-3 SB-6 (0-2)Total/NA
Soil 7471B490-114207-4 SB-9 (0-2)Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Metals (Continued)
Prep Batch: 379858 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B490-114207-5 SB-8 (0-2)Total/NA
Soil 7471B490-114207-6 SB-7 (4-6)Total/NA
Soil 7471B490-114207-7 SB-1 (0-2)Total/NA
Soil 7471B490-114207-8 SB-2 (4-6)Total/NA
Soil 7471B490-114207-9 SB-3 (8-10)Total/NA
Solid 7471BMB 490-379858/1-A Method Blank Total/NA
Solid 7471BLCS 490-379858/2-A Lab Control Sample Total/NA
Soil 7471B490-114207-1 MS SB-4 (0-2)Total/NA
Soil 7471B490-114207-1 MSD SB-4 (0-2)Total/NA
Prep Batch: 379915
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B490-114207-10 SB-10 (2-4)Total/NA
Solid 7471BMB 490-379915/1-A Method Blank Total/NA
Solid 7471BLCS 490-379915/2-A Lab Control Sample Total/NA
Soil 7471B490-114207-10 MS SB-10 (2-4)Total/NA
Soil 7471B490-114207-10 MSD SB-10 (2-4)Total/NA
Analysis Batch: 380098
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 379801490-114207-1 SB-4 (0-2)Total/NA
Soil 6010D 379801490-114207-2 SB-5 (0-2)Total/NA
Soil 6010D 379801490-114207-3 SB-6 (0-2)Total/NA
Soil 6010D 379801490-114207-4 SB-9 (0-2)Total/NA
Soil 6010D 379801490-114207-5 SB-8 (0-2)Total/NA
Soil 6010D 379801490-114207-6 SB-7 (4-6)Total/NA
Soil 6010D 379801490-114207-7 SB-1 (0-2)Total/NA
Soil 6010D 379801490-114207-9 SB-3 (8-10)Total/NA
Soil 6010D 379801490-114207-10 SB-10 (2-4)Total/NA
Solid 6010D 379801MB 490-379801/1-A Method Blank Total/NA
Solid 6010D 379801LCS 490-379801/2-A Lab Control Sample Total/NA
Solid 6010D 379801LCSD 490-379801/3-A Lab Control Sample Dup Total/NA
Solid 6010D 379801490-114010-F-3-B MS Matrix Spike Total/NA
Solid 6010D 379801490-114010-F-3-C MSD Matrix Spike Duplicate Total/NA
Analysis Batch: 380139
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B 379858490-114207-1 SB-4 (0-2)Total/NA
Soil 7471B 379858490-114207-2 SB-5 (0-2)Total/NA
Soil 7471B 379858490-114207-3 SB-6 (0-2)Total/NA
Soil 7471B 379858490-114207-4 SB-9 (0-2)Total/NA
Soil 7471B 379858490-114207-5 SB-8 (0-2)Total/NA
Soil 7471B 379858490-114207-6 SB-7 (4-6)Total/NA
Soil 7471B 379858490-114207-7 SB-1 (0-2)Total/NA
Soil 7471B 379858490-114207-8 SB-2 (4-6)Total/NA
Soil 7471B 379858490-114207-9 SB-3 (8-10)Total/NA
Soil 7471B 379915490-114207-10 SB-10 (2-4)Total/NA
Solid 7471B 379858MB 490-379858/1-A Method Blank Total/NA
Solid 7471B 379915MB 490-379915/1-A Method Blank Total/NA
Solid 7471B 379858LCS 490-379858/2-A Lab Control Sample Total/NA
Solid 7471B 379915LCS 490-379915/2-A Lab Control Sample Total/NA
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QC Association Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Metals (Continued)
Analysis Batch: 380139 (Continued)
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 7471B 379858490-114207-1 MS SB-4 (0-2)Total/NA
Soil 7471B 379858490-114207-1 MSD SB-4 (0-2)Total/NA
Soil 7471B 379915490-114207-10 MS SB-10 (2-4)Total/NA
Soil 7471B 379915490-114207-10 MSD SB-10 (2-4)Total/NA
Analysis Batch: 380749
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 379801490-114207-1 SB-4 (0-2)Total/NA
Soil 6010D 379801490-114207-2 SB-5 (0-2)Total/NA
Soil 6010D 379801490-114207-3 SB-6 (0-2)Total/NA
Soil 6010D 379801490-114207-4 SB-9 (0-2)Total/NA
Soil 6010D 379801490-114207-5 SB-8 (0-2)Total/NA
Soil 6010D 379801490-114207-6 SB-7 (4-6)Total/NA
Soil 6010D 379801490-114207-7 SB-1 (0-2)Total/NA
Soil 6010D 379801490-114207-8 SB-2 (4-6)Total/NA
Soil 6010D 379801490-114207-9 SB-3 (8-10)Total/NA
Soil 6010D 379801490-114207-10 SB-10 (2-4)Total/NA
Analysis Batch: 380945
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil 6010D 379801490-114207-8 SB-2 (4-6)Total/NA
General Chemistry
Analysis Batch: 379206
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Soil Moisture490-114207-1 SB-4 (0-2)Total/NA
Soil Moisture490-114207-2 SB-5 (0-2)Total/NA
Soil Moisture490-114207-3 SB-6 (0-2)Total/NA
Soil Moisture490-114207-4 SB-9 (0-2)Total/NA
Soil Moisture490-114207-5 SB-8 (0-2)Total/NA
Soil Moisture490-114207-6 SB-7 (4-6)Total/NA
Soil Moisture490-114207-7 SB-1 (0-2)Total/NA
Soil Moisture490-114207-8 SB-2 (4-6)Total/NA
Soil Moisture490-114207-9 SB-3 (8-10)Total/NA
Soil Moisture490-114207-10 SB-10 (2-4)Total/NA
Solid Moisture490-114198-A-3 MS Matrix Spike Total/NA
Solid Moisture490-114198-A-3 MSD Matrix Spike Duplicate Total/NA
Soil Moisture490-114207-2 DU SB-5 (0-2)Total/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Client Sample ID: SB-4 (0-2)Lab Sample ID: 490-114207-1
Matrix: SoilDate Collected: 10/13/16 13:20
Date Received: 10/18/16 08:50
Prep 5035 JLP10/13/16 12:20 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.304 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 01:43 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379813 10/20/16 10:37 MNM TAL NSHTotal/NA 30.51 g 1.00 mL
Analysis 8270D 5 381549 10/27/16 02:46 T1C TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.17 g 20 mL
Analysis 8330A 1 349225 11/01/16 14:35 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.500 g 100 mL
Analysis 6010D 5 380749 10/24/16 15:30 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.500 g 100 mL
Analysis 6010D 1 380098 10/21/16 02:27 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.615 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:26 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 14:44 BAA TAL NSHTotal/NA
Client Sample ID: SB-5 (0-2)Lab Sample ID: 490-114207-2
Matrix: SoilDate Collected: 10/13/16 14:10
Date Received: 10/18/16 08:50
Prep 5035 JLP10/13/16 13:10 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.083 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 02:10 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379813 10/20/16 10:37 MNM TAL NSHTotal/NA 30.09 g 1.00 mL
Analysis 8270D 1 381549 10/27/16 03:04 T1C TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.02 g 20 mL
Analysis 8330A 1 349025 10/31/16 11:37 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.524 g 100 mL
Analysis 6010D 5 380749 10/24/16 15:35 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.524 g 100 mL
Analysis 6010D 1 380098 10/21/16 02:32 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.604 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:34 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 15:09 BAA TAL NSHTotal/NA
Client Sample ID: SB-6 (0-2)Lab Sample ID: 490-114207-3
Matrix: SoilDate Collected: 10/13/16 15:30
Date Received: 10/18/16 08:50
Prep 5035 JLP10/13/16 14:30 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.136 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 02:38 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379813 10/20/16 10:37 MNM TAL NSHTotal/NA 30.77 g 1.00 mL
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Client Sample ID: SB-6 (0-2)Lab Sample ID: 490-114207-3
Matrix: SoilDate Collected: 10/13/16 15:30
Date Received: 10/18/16 08:50
Analysis 8270D T1C10/27/16 03:231 TAL NSH381549
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.20 g 20 mL
Analysis 8330A 1 349025 10/31/16 12:00 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.498 g 100 mL
Analysis 6010D 5 380749 10/24/16 15:40 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.498 g 100 mL
Analysis 6010D 1 380098 10/21/16 02:37 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.611 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:37 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 15:09 BAA TAL NSHTotal/NA
Client Sample ID: SB-9 (0-2)Lab Sample ID: 490-114207-4
Matrix: SoilDate Collected: 10/14/16 15:30
Date Received: 10/18/16 08:50
Prep 5035 JLP10/14/16 14:30 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.589 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 03:05 EML TAL NSHTotal/NA 5 g 5 mL
Prep 5035 379444 10/14/16 14:30 JLP TAL NSHTotal/NA 5.725 g 5.0 mL
Analysis 8260B 1 380848 10/25/16 13:59 EML TAL NSHTotal/NA 0.1 mL 5 mL
Prep 3550C 379813 10/20/16 10:37 MNM TAL NSHTotal/NA 30.61 g 1.00 mL
Analysis 8270D 5 381549 10/27/16 03:42 T1C TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.04 g 20 mL
Analysis 8330A 1 349025 10/31/16 12:23 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.509 g 100 mL
Analysis 6010D 5 380749 10/24/16 15:46 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.509 g 100 mL
Analysis 6010D 1 380098 10/21/16 02:42 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.621 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:40 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 14:44 BAA TAL NSHTotal/NA
Client Sample ID: SB-8 (0-2)Lab Sample ID: 490-114207-5
Matrix: SoilDate Collected: 10/14/16 15:40
Date Received: 10/18/16 08:50
Prep 5035 JLP10/14/16 14:40 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 6.669 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 03:33 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379813 10/20/16 10:37 MNM TAL NSHTotal/NA 30.48 g 1.00 mL
Analysis 8270D 1 381549 10/27/16 04:01 T1C TAL NSHTotal/NA
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Client Sample ID: SB-8 (0-2)Lab Sample ID: 490-114207-5
Matrix: SoilDate Collected: 10/14/16 15:40
Date Received: 10/18/16 08:50
Drying Prep/Air Dry CDC10/26/16 15:24 TAL DEN348351
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.08 g 20 mL
Analysis 8330A 1 349025 10/31/16 12:46 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.504 g 100 mL
Analysis 6010D 5 380749 10/24/16 15:51 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.504 g 100 mL
Analysis 6010D 1 380098 10/21/16 02:58 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.624 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:42 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 14:44 BAA TAL NSHTotal/NA
Client Sample ID: SB-7 (4-6)Lab Sample ID: 490-114207-6
Matrix: SoilDate Collected: 10/14/16 15:50
Date Received: 10/18/16 08:50
Prep 5035 JLP10/14/16 14:50 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 3.76 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 04:00 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379813 10/20/16 10:37 MNM TAL NSHTotal/NA 30.92 g 1.00 mL
Analysis 8270D 1 381549 10/27/16 04:20 T1C TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.14 g 20 mL
Analysis 8330A 1 349025 10/31/16 13:09 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.516 g 100 mL
Analysis 6010D 5 380749 10/24/16 15:56 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.516 g 100 mL
Analysis 6010D 1 380098 10/21/16 03:04 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.598 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:45 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 14:44 BAA TAL NSHTotal/NA
Client Sample ID: SB-1 (0-2)Lab Sample ID: 490-114207-7
Matrix: SoilDate Collected: 10/14/16 18:00
Date Received: 10/18/16 08:50
Prep 5035 JLP10/14/16 17:00 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.541 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 04:28 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379832 10/20/16 11:13 MNM TAL NSHTotal/NA 30.49 g 1.00 mL
Analysis 8270D 1 380030 10/21/16 16:13 WDS TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.11 g 20 mL
Analysis 8330A 1 349025 10/31/16 13:32 ACF TAL DENTotal/NA
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Client Sample ID: SB-1 (0-2)Lab Sample ID: 490-114207-7
Matrix: SoilDate Collected: 10/14/16 18:00
Date Received: 10/18/16 08:50
Prep 3051A PG110/20/16 10:21 TAL NSH379801
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 0.502 g 100 mL
Analysis 6010D 5 380749 10/24/16 16:01 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.502 g 100 mL
Analysis 6010D 1 380098 10/21/16 03:09 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.624 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:53 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 15:09 BAA TAL NSHTotal/NA
Client Sample ID: SB-2 (4-6)Lab Sample ID: 490-114207-8
Matrix: SoilDate Collected: 10/14/16 18:27
Date Received: 10/18/16 08:50
Prep 5035 JLP10/14/16 17:27 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.616 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 04:55 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379832 10/20/16 11:13 MNM TAL NSHTotal/NA 30.18 g 1.00 mL
Analysis 8270D 1 380030 10/21/16 17:09 WDS TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.05 g 20 mL
Analysis 8330A 1 349025 10/31/16 13:55 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.505 g 100 mL
Analysis 6010D 5 380749 10/24/16 16:17 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.505 g 100 mL
Analysis 6010D 5 380945 10/24/16 19:23 RDF TAL NSHTotal/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.617 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:56 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 14:44 BAA TAL NSHTotal/NA
Client Sample ID: SB-3 (8-10)Lab Sample ID: 490-114207-9
Matrix: SoilDate Collected: 10/14/16 18:40
Date Received: 10/18/16 08:50
Prep 5035 JLP10/14/16 17:40 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.056 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 05:23 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379832 10/20/16 11:13 MNM TAL NSHTotal/NA 30.77 g 1.00 mL
Analysis 8270D 1 380030 10/21/16 17:28 WDS TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.13 g 20 mL
Analysis 8330A 1 349025 10/31/16 14:41 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.499 g 100 mL
Analysis 6010D 5 380749 10/24/16 16:22 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.499 g 100 mL
TestAmerica Nashville
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Lab Chronicle
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Client Sample ID: SB-3 (8-10)Lab Sample ID: 490-114207-9
Matrix: SoilDate Collected: 10/14/16 18:40
Date Received: 10/18/16 08:50
Analysis 6010D RDF10/21/16 03:191 TAL NSH380098
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Prep 7471B 379858 10/20/16 11:45 LCS TAL NSHTotal/NA 0.601 g 100 mL
Analysis 7471B 1 380139 10/21/16 07:59 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 15:09 BAA TAL NSHTotal/NA
Client Sample ID: SB-10 (2-4)Lab Sample ID: 490-114207-10
Matrix: SoilDate Collected: 10/14/16 19:15
Date Received: 10/18/16 08:50
Prep 5035 JLP10/14/16 18:15 TAL NSH379446
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 7.015 g 5.0 mL
Analysis 8260B 1 380000 10/21/16 05:50 EML TAL NSHTotal/NA 5 g 5 mL
Prep 3550C 379832 10/20/16 11:13 MNM TAL NSHTotal/NA 30.68 g 1.00 mL
Analysis 8270D 1 380030 10/21/16 17:47 WDS TAL NSHTotal/NA
Drying Prep/Air Dry 348351 10/26/16 15:24 CDC TAL DENTotal/NA 1.0 g 1.0 g
Prep Sieve/Ultrasoni 348557 10/27/16 14:58 BMS TAL DENTotal/NA 2.16 g 20 mL
Analysis 8330A 1 349025 10/31/16 15:04 ACF TAL DENTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.513 g 100 mL
Analysis 6010D 5 380749 10/24/16 16:27 RDF TAL NSHTotal/NA
Prep 3051A 379801 10/20/16 10:21 PG1 TAL NSHTotal/NA 0.513 g 100 mL
Analysis 6010D 1 380098 10/21/16 03:24 RDF TAL NSHTotal/NA
Prep 7471B 379915 10/20/16 13:47 LCS TAL NSHTotal/NA 0.599 g 100 mL
Analysis 7471B 1 380139 10/21/16 08:45 LCS TAL NSHTotal/NA
Analysis Moisture 1 379206 10/18/16 14:44 BAA TAL NSHTotal/NA
Client Sample ID: TMW-2 Lab Sample ID: 490-114207-11
Matrix: WaterDate Collected: 10/17/16 14:20
Date Received: 10/18/16 08:50
Analysis 8260B EML10/23/16 03:051 TAL NSH380458
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 3535 347627 10/21/16 16:35 DLW TAL DENTotal/NA 444.8 mL 5 mL
Analysis 8330A 1 348206 10/25/16 12:56 ACF TAL DENTotal/NA
Prep 3535 347627 10/21/16 16:35 DLW TAL DENTotal/NA 444.8 mL 5 mL
Analysis 8330A 1 348204 10/25/16 10:59 ACF TAL DENTotal/NA
Laboratory References:
TAL DEN = TestAmerica Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Method Summary
TestAmerica Job ID: 490-114207-1Client: Hart & Hickman, PC
SDG: LRC-004Project/Site: Continental Tire
Method Method Description LaboratoryProtocol
SW8468260BVolatile Organic Compounds (GC/MS)TAL NSH
SW8468270DSemivolatile Organic Compounds (GC/MS)TAL NSH
SW8468330ANitroaromatics and Nitramines TAL DEN
SW8466010DMetals (ICP)TAL NSH
SW8467471BMercury (CVAA)TAL NSH
EPAMoisturePercent Moisture TAL NSH
SW8463051APreparation, Metals, Microwave Assisted TAL NSH
SW8463535Solid-Phase Extraction (SPE)TAL DEN
SW8463550CUltrasonic Extraction TAL NSH
SW8465030BPurge and Trap TAL NSH
SW8465035Closed System Purge and Trap TAL NSH
SW8467471BPreparation, Mercury TAL NSH
NonePrep/Air Dry Preparation, Air drying TAL DEN
SW846Sieve/Ultrasoni Sieve and Ultrasonic Water Bath Extraction (Explosives)TAL DEN
Protocol References:
EPA = US Environmental Protection Agency
None = None
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL DEN = TestAmerica Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL [phone]
TestAmerica Nashville
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Accreditation/Certification Summary
Client: Hart & Hickman, PC TestAmerica Job ID: 490-114207-1
Project/Site: Continental Tire SDG: LRC-004
Laboratory: TestAmerica Nashville
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program EPA Region Identification Number Expiration Date
North Carolina (WW/SW)3874State Program 12-31-18
Analysis Method Prep Method Matrix Analyte
The following analytes are included in this report, but accreditation/certification is not offered by the governing authority:
Moisture Soil Percent Solids
Laboratory: TestAmerica Denver
All accreditations/certifications held by this laboratory are listed. Not all accreditations/certifications are applicable to this report.
Authority Program EPA Region Identification Number Expiration Date
A2LA 2907.01DoD ELAP 10-31-19
A2LA ISO/IEC 17025 2907.01 10-31-19
Alabama State Program 4 40730 09-30-12 *
Alaska (UST)State Program 10 UST-30 01-08-19
Arizona State Program 9 AZ0713 12-20-18
California State Program 9 2513 01-18-19
Connecticut State Program 1 PH-0686 09-30-18
Florida NELAP 4 E87667 06-30-18
Georgia State Program 4 N/A 01-08-19 *
Illinois NELAP 5 200017 04-30-18 *
Iowa State Program 7 370 12-01-18
Kansas NELAP 7 E-10166 05-31-18 *
Louisiana NELAP 6 02096 06-30-18
Maine State Program 1 CO0002 03-03-19
Minnesota NELAP 5 8-999-405 12-31-18
Nevada State Program 9 CO0026 07-31-18
New Hampshire NELAP 1 205310 04-28-19
New Jersey NELAP 2 CO004 06-30-18
New York NELAP 2 11964 04-01-19
North Carolina (WW/SW)State Program 4 358 12-31-18
North Dakota State Program 8 R-034 01-08-19
Oklahoma State Program 6 8614 08-31-18
Oregon NELAP 10 4025 01-08-19
Pennsylvania NELAP 3 68-00664 07-31-18
South Carolina State Program 4 72002001 01-08-19
Texas NELAP 6 T104704183-17-14 09-30-18
USDA Federal 03-26-21
Utah NELAP 8 CO00026 07-31-18
Virginia NELAP 3 460232 06-14-19
Washington State Program 10 C583 08-03-18
West Virginia DEP State Program 3 354 12-31-18
Wisconsin State Program 5 999615430 08-31-18
Wyoming (UST)A2LA 8 2907.01 10-31-19
TestAmerica Nashville
* Accreditation/Certification renewal pending - accreditation/certification considered valid.
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-114207-1
SDG Number: LRC-004
Login Number: 114207
Question Answer Comment
Creator: McBride, Mike
List Source: TestAmerica Nashville
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
TrueSample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
TrueResidual Chlorine Checked.
TestAmerica Nashville
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Login Sample Receipt Checklist
Client: Hart & Hickman, PC Job Number: 490-114207-1
SDG Number: LRC-004
Login Number: 114207
Question Answer Comment
Creator: Muniz, Ashley T
List Source: TestAmerica Denver
List Creation: 10/20/16 04:08 PMList Number: 2
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
N/AIs the Field Sampler's name present on COC?Received project as a subcontract.
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
TestAmerica Nashville
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Hart & Hickman, PC
Appendix B
Risk Calculator Output