MO-6615_27296_CA_MRP_20180202_SamplingLetter2-2018FINAL

ERM NC, Inc.
15720 Brixham Hill Avenue,
Suite 120
Charlotte, NC 28277
February2, 2018 Tele: 704-541-8345
Fax:[phone]
Mr. Brett Morris
NCDEQ - Mooresville Regional Office
Division of Waste Management -UST Section
610 East Center Avenue, Suite 301 ERM
Mooresville, North Carolina 28115
Tele: 704-663-1699 via FedEx
Subject: MW-4 Results and Free Product Gauging
Former Integris Metals Facility
527 Atando Avenue
Charlotte, North Carolina
Dear Mr. Morris:
On behalf of J.T. Ryerson & Son, Inc. (Ryerson), ERM NC, Inc. (ERM) would like to
provide the results of recent activities at the above referenced facility. A
groundwater sampling event conducted in September 2017 detected several semi -
volatile organic compounds (SVOCs) in monitor wells MW-4 above their respective
gross contaminant levels (GCLs). SVOCs have not been detected in MW-4 during
historical (January 2003, June 2016 and December 2016) sampling events. ERM re -
sampled MW-4 for SVOCs on January 8, 2018. The laboratory did not detect SVOCs
in the January sample. Based on the lack of SVOC detections in the January 2018
sample and on the historic data which shows no detections, it appears that the
September 2017 data was anomalous and not representative of groundwater
conditions at this location. A copy of the laboratory report is attached.
Monitor well MW-1 has historically contained measureable free
product. ERM has employed various free product recovery
methods since it was discovered in 2003, including vacuum
recovery, active bailing, passive bailing, absorbent socks, and
surfactant injection/recovery. During the September 2017
sampling event, an absorbent sock had been present in the well
for at least 6 months. No measureable product was observed at
that time. The absorbent sock was removed from the well on
September 5, 2017. Four months later, on January 8, 2018, ERM
gauged MW-1 with an oil -water interface probe and free
product was not detected. A bailer was also used to visually
confirm the absence of product. The picture to the right

Former Integris Metals - Atando Ave
February 2, 2018
Page 2
indicates that a sheen of product is present, but it is not measurable using the
interface probe and is less than 1/8-inch thick. Additionally, the December 2016 and
September 2017 analytical results from MW-1 indicated that dissolved hydrocarbon
concentrations are below GCLs in this well. No measurable product has been
gauged in MW-1 since the December 2016 surfactant injection/recovery activity.
Additionally, 4-inch diameter free product recovery well RW-1, located three feet
from MW-1, has not detected free product over the last twelve gauging events. The
last detection of free product in RW-1 occurred in 2004, when 0.03 feet was
measured. Historical groundwater sampling data and free product gauging data is
attached herein.
Based on the results of the data from the December 2016 and September 2017
sampling events, and the follow-up activities in January 2018, ERM proposes that
closure be granted for this incident.
If you have any questions, please contact us at 704-541-8345.
Sincerely,
Michael Pressley, P.G
Project Manager
enclosures
cc: Mr. Mark Silver - Ryerson
Rick Tarravechia, P.G., RSM
Partner in Charge

TABLE B-4-1 SUMMARY OF GROUND WATER SAMPLING RESULTS - VOCs and SVOCs
Date: January 2018 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Analytical Method
VOCs - EPA Method 602 (pg/1) / 8260B
SVOCs - EPA Method 625 (Ng/1)
C
N
c
N
N
N
O
C
_
Co
O
U
N
N
C
U
M
47
c
O
r-
Q
f0
N
t
C
W
O
N
C
E
T
Q
Co
O
Co
o
O
w
O
�
N
°
-
L
m
O
C
(0
o
7
Y
O
C
w
m
m
n
T
X
L
L
ll.l
N
(6
m
L
D_
T
ro
C
)
(0
C
N
a�
c
a
�-
U
r>
N
O
C
m
C
_N
N
L
L
N
c
d
L
C
Co
N
C
�`
O
O
C
NL.
C
N
N
C
N
C
N
C
N
N
.C.
L
O
O
N
O.
C
Sample ID
Source
Date
N
Co
L
w
O
H
>+
X
C
Q
U
¢
N
Co
N
Co
N
Co
Co
m
U
C
z
a
NC Ground Water Standard (21L)
1
600
600
500
2,000
80
0.05
0.05
0.05
200
0.5
5
3
NE
300
300
6
6
200
Gross Contamination Level
5,000
84,500
260,000
85,500
2,000
2,120
4.7
0.81
0.75
200
0.5
5
170
NE
300
990
6,000
6,000
410
1 /3/2003
Not Sampled Due to Free Product
MW-1
MW
6/14/2016
66
90
ND
ND
460
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
570
ND
2,100
2,100
12/29/2016
70
48
2.3
14
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
ND
ND
200
61
9/5/2017
47
28
ND
6.7
21
19
ND
ND
ND
ND
ND
VD
ND
ND
ND
36
ND
240
98
1/3/2003
55
15
2.0
98
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
18
ND
92
39
MW-2
MW
6/14/2016
61
19
ND
8
ND
ND
ND
ND
ND
ND
ND
VD
ND
11
ND
4.2
ND
41
3.8
12/29/2016
60
10
ND
3.7
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
ND
ND
54
10
9/5/2017
59
14
ND
5.6
ND
1.8
ND
ND
ND
ND
N
VD
ND
ND
ND
7.5
ND
84
8.4
1/22/2003
1.6
ND
ND
ND
ND
ND
ND
ND
ND
ND
N
VD
11
ND
ND
ND
ND
ND
ND
MW-3
MW
6/14/2016
1.6
ND
2.1
2.1
ND
ND
ND
ND
ND
ND
N
VD
1.6
ND
ND
ND
ND
3.5
ND
12/29/2016
9.7
ND
ND
3.8
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
ND
ND
7.5
ND
9/5/2017
3.2
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
ND
ND
4.6
ND
1/22/2003
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
ND
ND
ND
ND
6/14/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
ND
ND
ND
ND
MW-4
MW
12/29/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
VD
ND
ND
ND
ND
ND
ND
ND
9/5/2017
ND
ND
ND
ND
ND
ND
2.3
3.3
6.2
1.7
2.0
3.2
1.7
ND
4.3
ND
1.7
ND
ND
1/8/2018
ND
ND
I ND
I ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
I ND
ND
ND
ND
1/22/2003
3.6
ND
1.8
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-5
MW
6/14/2016
ND
ND
1 ND
1 ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12/29/2016
Not Sample Due to Standing Water Around Wellhead
9/5/2017
1 1.2
1 ND
I ND
I ND
I ND
I ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1/22/2003
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
DW-1
MW
6/14/2016
1 ND
ND
ND
ND
ND
PSkmr
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND:ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
NDND
9/5/2017
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Only detected compounds are included in table. NA = Not Applicable NA = Not NA = Not Applicable
Ng/L = micrograms per liter Results shown in bold exceed the applicable Ground Water Standard (T15A 2L)
ND = Not detected
NE - Not Established
ERM Page 1 of 1

TABLE B-8 FREE PRODUCT RECOVERY RESULTS
Date: January 2018 ncident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Free Product ecovery Method: Bailer/Passive Skimmer/SocW7VFF- Facility ID#: Not established
Method of Measurement: Bailer/I Interface pro e
Well ID
Product Type
Date of
Recovery
Casing
Diameter
(inches)
Product
Thickness
Before
Recovery (ft.)
Product
Thickness After
Recovery (ft.)
Amount of
Product
Recovered
(gallons)
Depth to Water
from Top of
Casing (ft.)
Comments
MW-1
Fuel Oil
1/3/03
2
0.05
0.00
<0.25
21.32
Bailer
1/22/03
2
0.02
0.00
<0.25
16.23
Bailer
3/10/03
2
0.04
0.00
<0.25
14.07
Bailer
3/25/03
2
0.00
0.00
<0.25
12.99
Bailer
4/4/03
2
0.03
0.00
<0.25
12.68
Bailer
5/30/03
2
0.01
0.00
<0.25
11.01
Bailer
6/27/03
2
0.02
0.00
<0.25
11.24
Bailer
7/17/03
2
0.01
0.00
<0.25
11.71
Bailer
8/26/03
2
0.01
0.00
<0.25
11.15
Bailer
9/2/03
2
0.01
0.00
<0.25
12.18
Bailer
11/14/03
2
0.01
0.00
<0.25
15.23
Bailer
11/24/03
2
0.01
0.00
<0.25
15.10
Bailer
12/19/03
2
0.04
0.00
<0.25
14.74
Bailer
1/29/04
2
0.05
0.00
<0.25
15.05
Bailer
3/9/04
2
0.00
0.00
<0.25
13.19
AFVR
4/8/04
2
0.04
0.00
<0.25
13.07
Bailer
5/10 to 5/19/04
Source Removal: UST and 416 tons of contaminated soil removed to depth of 17 feet.
5/24/04
2
0.08
0.00
0.20
13.22
Bailer
6/23/04
2
0.07
0.00
<0.25
15.00
Bailer
7/28/04
2
0.05
0.00
<0.25
15.75
Bailer
8/27/04
2
0.12
0.00
0.25
15.52
Bailer
10/5/04
2
0.05
0.00
<0.25
14.14
Bailer
11/1/04
2
0.10
0.00
0.25
14.67
Bailer
12/2/04
2
0.03
0.00
<0.25
14.53
Bailer
11/17/13
2
0.55
0.00
<0.25
17.89
Bailer
2/5/14
2
0.67
0.00
<0.25
15.34
P.Skmr
2/17/14
2
<0.01
0.00
<0.25
14.55
P.Skmr
2/27/14
2
<0.01
0.00
<0.25
14.01
P.Skmr
3/27/14
2
<0.01
0.00
<0.25
13.60
P.Skmr
8/6/14
2
<0.01
0.00
<0.25
14.45
P.Skmr
4/10/15
2
<0.01
0.00
<0.25
14.01
P.Skmr
5/27/15
2
0.01
0.00
<0.25
14.76
P.Skmr
7/28/15
2
0.08
0.00
<0.25
17.72
P.Skmr
1/28/16
2
0.19
0.00
0.00
12.92
P.Skmr
2/18/16
2
0.13
0.00
0.00
13.22
P.Skmr
3/25/16
2
<0.01
0.00
0.00
13.01
Sock
3/31/16
2
<0.01
0.00
0.00
12.91
Sock
4/14/16
2
<0.01
0.00
0.00
13.40
Sock
5/5/16
2
<0.01
0.00
0.00
13.66
Sock
6/14/16
2
0.02
0.00
0.00
13.92
Sock
12/27/16
2
0.015
0.00
0.00
16.62
Sock
12/27-12/28/16
Surfactant injection/extraction event
12/29/16
2
<0.01
0
0.00
17.80
Bailer
9/5/17
2
<0.01
0
0.00
15.94
Sock
1/8/18
2
<0.01
0
0.00
17.71
Bailer

TABLE B-8 cont. FREE PRODUCT RECOVERY RESULTS
Date: September 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte
Free Product Recovery Method: Bailer/Passive Skimmer/Sock/AFVR Facility ID : Not established
Method of Measurement: Bailer Interface pro e
Well ID
Product Type
Date of
Recovery
Casing
Diameter
(inches)
Product
Thickness
Before
Recovery (ft.)
Product
Thickness After
Recovery (ft.)
Amount of
Product
Recovered
(gallons)
Depth to Water
from Top of
Casing (ft.)
Comments
RW-1
Fuel Oil
11/24/03
4
0.05
0
0.25
15.20
Bailer
12/19/03
4
0.15
0
0.25
15.32
Bailer
1/29/04
4
0.42
0
0.25
15.56
Bailer
3/9/04
4
0.05
0
2.00
13.32
AFVR
4/8/04
4
0.15
0
0.25
13.29
Bailer
5/10 to 5/19/04
Source Removal:
UST and 416
tons of contaminated
soil removed
to depth of
17 feet.
5/24/04
4
0.17
0
0.30
13.43
Bailer
6/23/04
4
0.23
0
0.30
15.38
Bailer
7/28/04
4
0.27
0
0.30
15.46
Bailer
8/27/04
4
0.29
0
0.30
15.75
Bailer
10/5/04
4
0.15
0
0.30
13.87
Bailer
11/1/04
4
0.17
0
0.30
14.91
Bailer
12/2/04
4
0.03
0
<0.25
14.74
Bailer
2/27/14
4
<0.01
0
0.00
14.00
---
5/27/15
4
0.01
0
0.00
14.68
---
7/28/15
4
0.01
0
0.00
17.31
---
1/28/15
4
<0.01
0
0.00
13.41
---
2/28/16
4
<0.01
0
0.00
13.49
---
3/31/16
4
<0.01
0
0.00
13.23
---
4/14/16
4
<0.01
0
0.00
13.27
---
5/5/16
4
<0.01
0
0.00
13.66
---
6/14/16
4
<0.01
0
0.00
13.90
---
5/5/16
4
<0.01
0
0.00
13.66
---
12/29/16
4
<0.01
0
0.00
13.62
---
9/5/17
4
<0.01
0
0.00
15.82
---
1/8/18
4
<0.01
0
0.00
17.52
Total Gallons Recovered to Date: Approximately 6.25 gallons

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM NC, Inc.
Ballantyne One
15720 Brixham Hill Avenue, Suite 120
Charlotte, NC 28277
Attention: Michael Pressley
Project Name: Atando Avenue
Project Number: 0345276
Lot Number:TA10099
Date Completed:01/15/2018
01/22/2018 1:13 PM
Approved and released by:
Project Manager: Kelly M. Nance
pCCRF�4
AM
ACCREDITED
qB
11900 ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 16

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
ERM NC, Inc.
Lot Number: TA10099
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 16

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM NC, Inc.
Lot Number: TA10099
Sample Number Sample ID Matrix Date Sampled Date Received
001 MW-4 Aqueous 01/08/20181430 01/10/2018
(1 sample)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 16

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
ERM NC, Inc.
Lot Number: TA10099
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 16

Semivolatile Organic Compounds by GC/MS
Client:ERM NC, Inc. Laboratory ID:TA10099-001
Description: MW-4 Matrix: Aqueous
Date Sampled:01/08/2018 1430
Date Received:01/10/2018
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 625 625
1 01/14/2018 1754 CMP2
01/11/2018 1714 61673
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9
625
ND
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
1.6
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
ug/L
1
Fluorene
86-73-7
625
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
ug/L
1
Isophorone
78-59-1
625
ND
1.6
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 16

Semivolatile Organic Compounds by GC/MS
Client:ERM NC, Inc. Laboratory ID:TA10099-001
Description: MW-4 Matrix: Aqueous
Date Sampled:01/08/2018 1430
Date Received:01/10/2018
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 01/14/2018 1754 CMP2 01/11/2018 1714 61673
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Naphthalene
91-20-3
625
ND
1.6
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
ND
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
71 37-129
2-Fluorophenol
58 24-127
Nitrobenzene-d5
69 38-127
Phenol-d5
52 28-128
Terphenyl-d14
100 10-148
2,4,6-Tribromophenol
87 41-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 16

QC Summary
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 16

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: TQ61673-001 Matrix: Aqueous
Batch: 61673 Prep Method: 625
Analytical Method: 625 Prep Date: 01/11/2018 1714
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Acenaphthene
ND
1
1.6
ug/L
01/14/2018 0941
Acenaphthylene
ND
1
1.6
ug/L
01/14/2018 0941
Anthracene
ND
1
1.6
ug/L
01/14/2018 0941
Benzidine
ND
1
8.0
ug/L
01/14/2018 0941
Benzo(a)anthracene
ND
1
1.6
ug/L
01/14/2018 0941
Benzo(a)pyrene
ND
1
1.6
ug/L
01/14/2018 0941
Benzo(b)fluoranthene
ND
1
1.6
ug/L
01/14/2018 0941
Benzo(g,h,i)perylene
ND
1
1.6
ug/L
01/14/2018 0941
Benzo(k)fluoranthene
ND
1
1.6
ug/L
01/14/2018 0941
4-Bromophenyl phenyl ether
ND
1
1.6
ug/L
01/14/2018 0941
Butyl benzyl phthalate
ND
1
1.6
ug/L
01/14/2018 0941
bis (2-Chloro-1-methylethyl) ether
ND
1
1.6
ug/L
01/14/2018 0941
4-Chloro-3-methyl phenol
ND
1
1.6
ug/L
01/14/2018 0941
bis(2-Chloroethoxy)methane
ND
1
1.6
ug/L
01/14/2018 0941
bis(2-Chloroethyl)ether
ND
1
1.6
ug/L
01/14/2018 0941
2-Chloronaphthalene
ND
1
1.6
ug/L
01/14/2018 0941
2-Chlorophenol
ND
1
1.6
ug/L
01/14/2018 0941
4-Chlorophenyl phenyl ether
ND
1
1.6
ug/L
01/14/2018 0941
Chrysene
ND
1
1.6
ug/L
01/14/2018 0941
Dibenzo(a,h)anthracene
ND
1
1.6
ug/L
01/14/2018 0941
1,2-Dichlorobenzene
ND
1
1.6
ug/L
01/14/2018 0941
1,3-Dichlorobenzene
ND
1
1.6
ug/L
01/14/2018 0941
1,4-Dichlorobenzene
ND
1
1.6
ug/L
01/14/2018 0941
3,3'-Dichlorobenzidine
ND
1
8.0
ug/L
01/14/2018 0941
2,4-Dichlorophenol
ND
1
1.6
ug/L
01/14/2018 0941
Diethylphthalate
ND
1
1.6
ug/L
01/14/2018 0941
Dimethyl phthalate
ND
1
1.6
ug/L
01/14/2018 0941
2,4-Dimethylphenol
ND
1
1.6
ug/L
01/14/2018 0941
Di-n-butyl phthalate
ND
1
1.6
ug/L
01/14/2018 0941
4,6-Dinitro-2-methyl phenol
ND
1
8.0
ug/L
01/14/2018 0941
2,4-Dinitrophenol
ND
1
8.0
ug/L
01/14/2018 0941
2,4-Dinitrotoluene
ND
1
3.2
ug/L
01/14/2018 0941
2,6-Dinitrotoluene
ND
1
3.2
ug/L
01/14/2018 0941
Di-n-octylphthalate
ND
1
1.6
ug/L
01/14/2018 0941
1,2-Diphenylhydrazine(as azobenzene)
ND
1
1.6
ug/L
01/14/2018 0941
bis(2-Ethylhexyl)phthalate
ND
1
1.6
ug/L
01/14/2018 0941
Fluoranthene
ND
1
1.6
ug/L
01/14/2018 0941
Fluorene
ND
1
1.6
ug/L
01/14/2018 0941
Hexachlorobenzene
ND
1
1.6
ug/L
01/14/2018 0941
Hexachlorobutadiene
ND
1
1.6
ug/L
01/14/2018 0941
Hexachlorocyclopentadiene
ND
1
8.0
ug/L
01/14/2018 0941
Hexachloroethane
ND
1
1.6
ug/L
01/14/2018 0941
Indeno(1,2,3-c,d)pyrene
ND
1
1.6
ug/L
01/14/2018 0941
Isophorone
ND
1
1.6
ug/L
01/14/2018 0941
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 16

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: TQ61673-001 Matrix: Aqueous
Batch: 61673 Prep Method: 625
Analytical Method: 625 Prep Date: 01/11/2018 1714
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Naphthalene
ND
1
1.6
ug/L
01/14/2018 0941
Nitrobenzene
ND
1
1.6
ug/L
01/14/2018 0941
2-Nitrophenol
ND
1
3.2
ug/L
01/14/2018 0941
4-Nitrophenol
ND
1
8.0
ug/L
01/14/2018 0941
N-Nitrosodimethylamine
ND
1
1.6
ug/L
01/14/2018 0941
N-Nitrosodi-n-propylamine
ND
1
1.6
ug/L
01/14/2018 0941
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
1.6
ug/L
01/14/2018 0941
Pentachlorophenol
ND
1
8.0
ug/L
01/14/2018 0941
Phenanthrene
ND
1
1.6
ug/L
01/14/2018 0941
Phenol
ND
1
1.6
ug/L
01/14/2018 0941
Pyrene
ND
1
1.6
ug/L
01/14/2018 0941
1,2,4-Trichlorobenzene
ND
1
1.6
ug/L
01/14/2018 0941
2,4,6-Trichlorophenol
ND
1
1.6
ug/L
01/14/2018 0941
Acceptance
Surrogate
0
Q /o Rec
Limit
2-Fluorobiphenyl
74
37-129
2-Fluorophenol
57
24-127
Nitrobenzene-d5
75
38-127
Phenol-d5
61
28-128
Terphenyl-d 14
109
10-148
2,4,6-Tribromophenol
82
41-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 16

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: TQ61673-002
Matrix: Aqueous
Batch: 61673
Prep Method: 625
Analytical Method: 625
Prep Date: 01/11/2018 1714
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
20
19
1
94
47-145
01/14/2018 1006
Acenaphthylene
20
19
1
95
33-145
01/14/2018 1006
Anthracene
20
21
1
105
27-133
01/14/2018 1006
Benzidine
100
85
1
85
1-150
01/14/2018 1006
Benzo(a)anthracene
20
20
1
102
33-143
01/14/2018 1006
Benzo(a)pyrene
20
18
1
89
17-163
01/14/2018 1006
Benzo(b)fluoranthene
20
20
1
99
24-159
01/14/2018 1006
Benzo(g,h,i)perylene
20
23
1
117
0-219
01/14/2018 1006
Benzo(k)fluoranthene
20
20
1
100
11-162
01/14/2018 1006
4-Bromophenyl phenyl ether
20
19
1
95
53-127
01/14/2018 1006
Butyl benzyl phthalate
20
24
1
122
0-152
01/14/2018 1006
bis (2-Chloro-1-methylethyl) ether
20
16
1
78
36-166
01/14/2018 1006
4-Chloro-3-methyl phenol
20
19
1
94
22-147
01/14/2018 1006
bis(2-Chloroethoxy)methane
20
19
1
94
33-184
01/14/2018 1006
bis(2-Chloroethyl)ether
20
16
1
82
12-158
01/14/2018 1006
2-Chloronaphthalene
20
18
1
88
60-118
01/14/2018 1006
2-Chlorophenol
20
17
1
86
23-134
01/14/2018 1006
4-Chlorophenyl phenyl ether
20
19
1
95
25-158
01/14/2018 1006
Chrysene
20
21
1
106
17-168
01/14/2018 1006
Dibenzo(a,h)anthracene
20
24
1
120
0-227
01/14/2018 1006
1,2-Dichlorobenzene
20
16
1
79
32-129
01/14/2018 1006
1,3-Dichlorobenzene
20
16
1
80
0-172
01/14/2018 1006
1,4-Dichlorobenzene
20
16
1
80
20-124
01/14/2018 1006
3,3'-Dichlorobenzidine
20
16
1
81
0-262
01/14/2018 1006
2,4-Dichlorophenol
20
19
1
93
39-135
01/14/2018 1006
Diethylphthalate
20
22
1
108
0-114
01/14/2018 1006
Dimethyl phthalate
20
21
1
104
0-112
01/14/2018 1006
2,4-Dimethylphenol
20
17
1
84
32-119
01/14/2018 1006
Di-n-butyl phthalate
20
22
1
111
1-118
01/14/2018 1006
4,6-Dinitro-2-methyl phenol
20
19
1
93
0-181
01/14/2018 1006
2,4-Dinitrophenol
40
32
1
79
0-191
01/14/2018 1006
2,4-Dinitrotoluene
20
23
1
113
39-139
01/14/2018 1006
2,6-Dinitrotoluene
20
20
1
101
50-158
01/14/2018 1006
Di-n-octylphthalate
20
20
1
98
4-146
01/14/2018 1006
1,2-Diphenylhydrazine(as azobenzene)
20
17
1
87
30-130
01/14/2018 1006
bis(2-Ethylhexyl)phthalate
20
22
1
112
8-158
01/14/2018 1006
Fluoranthene
20
21
1
107
26-137
01/14/2018 1006
Fluorene
20
19
1
96
59-121
01/14/2018 1006
Hexachlorobenzene
20
19
1
94
0-152
01/14/2018 1006
Hexachlorobutadiene
20
16
1
82
24-116
01/14/2018 1006
Hexachlorocyclopentadiene
100
56
1
56
1-150
01/14/2018 1006
Hexachloroethane
20
16
1
78
40-113
01/14/2018 1006
Indeno(1,2,3-c,d)pyrene
20
24
1
118
0-171
01/14/2018 1006
Isophorone
20
19
1
95
21-196
01/14/2018 1006
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 16

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: TQ61673-002
Matrix: Aqueous
Batch: 61673
Prep Method: 625
Analytical Method: 625
Prep Date: 01/11/2018 1714
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Naphthalene
20
18
1
90
21-133
01/14/20181006
Nitrobenzene
20
18
1
88
35-180
01/14/20181006
2-Nitrophenol
20
19
1
97
29-182
01/14/20181006
4-Nitrophenol
40
36
1
91
0-132
01/14/20181006
N-Nitrosodimethylamine
20
17
1
86
1-150
01/14/20181006
N-Nitrosodi-n-propylamine
20
17
1
87
0-230
01/14/20181006
N-Nitrosodiphenylamine (Diphenylamine) 20
17
1
84
1-150
01/14/2018 1006
Pentachlorophenol
40
39
1
97
14-176
01/14/20181006
Phenanthrene
20
20
1
100
54-120
01/14/20181006
Phenol
20
16
1
82
5-112
01/14/20181006
Pyrene
20
22
1
108
52-115
01/14/20181006
1,2,4-Trichlorobenzene
20
17
1
85
44-142
01/14/20181006
2,4,6-Trichlorophenol
20
18
1
92
37-144
01/14/20181006
Acceptance
Surrogate
0
Q /o Rec
Limit
2-Fluorobiphenyl
93
37-129
2-Fluorophenol
78
24-127
Nitrobenzene-d5
91
38-127
Phenol-d5
81
28-128
Terphenyl-d 14
108
10-148
2,4,6-Tribromophenol
110
41-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 16

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: TA10099-001 MS
Matrix: Aqueous
Batch: 61673
Prep Method: 625
Analytical Method: 625
Prep Date: 01/11/2018 1714
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
ND
20
15
1
76
47-145
01/14/2018 1819
Acenaphthylene
ND
20
15
1
76
33-145
01/14/2018 1819
Anthracene
ND
20
20
1
100
27-133
01/14/2018 1819
Benzidine
ND
100
23
1
23
1-150
01/14/2018 1819
Benzo(a)anthracene
ND
20
21
1
105
33-143
01/14/2018 1819
Benzo(a)pyrene
ND
20
19
1
93
17-163
01/14/2018 1819
Benzo(b)fluoranthene
ND
20
25
1
123
24-159
01/14/2018 1819
Benzo(g,h,i)perylene
ND
20
12
1
61
0-219
01/14/2018 1819
Benzo(k)fluoranthene
ND
20
24
1
120
11-162
01/14/2018 1819
4-Bromophenyl phenyl ether
ND
20
17
1
87
53-127
01/14/2018 1819
Butyl benzyl phthalate
ND
20
24
1
120
0-152
01/14/2018 1819
bis (2-Chloro-1-methylethyl) ether
ND
20
11
1
55
36-166
01/14/2018 1819
4-Chloro-3-methyl phenol
ND
20
15
1
76
22-147
01/14/2018 1819
bis(2-Chloroethoxy)methane
ND
20
14
1
70
33-184
01/14/2018 1819
bis(2-Chloroethyl)ether
ND
20
11
1
57
12-158
01/14/2018 1819
2-Chloronaphthalene
ND
20
14
1
71
60-118
01/14/2018 1819
2-Chlorophenol
ND
20
13
1
64
23-134
01/14/2018 1819
4-Chlorophenyl phenyl ether
ND
20
16
1
81
25-158
01/14/2018 1819
Chrysene
ND
20
22
1
111
17-168
01/14/2018 1819
Dibenzo(a,h)anthracene
ND
20
14
1
72
0-227
01/14/2018 1819
1,2-Dichlorobenzene
ND
20
13
1
64
32-129
01/14/2018 1819
1,3-Dichlorobenzene
ND
20
13
1
65
0-172
01/14/2018 1819
1,4-Dichlorobenzene
ND
20
13
1
63
20-124
01/14/2018 1819
3,3'-Dichlorobenzidine
ND
20
11
1
54
0-262
01/14/2018 1819
2,4-Dichlorophenol
ND
20
15
1
73
39-135
01/14/2018 1819
Diethylphthalate
ND
20
21
1
103
0-114
01/14/2018 1819
Dimethyl phthalate
ND
20
18
1
91
0-112
01/14/2018 1819
2,4-Dimethylphenol
ND
20
13
1
65
32-119
01/14/2018 1819
Di-n-butyl phthalate
ND
20
23
1
114
1-118
01/14/2018 1819
4,6-Dinitro-2-methyl phenol
ND
20
18
1
90
0-181
01/14/2018 1819
2,4-Dinitrophenol
ND
40
32
1
79
0-191
01/14/2018 1819
2,4-Dinitrotoluene
ND
20
21
1
105
39-139
01/14/2018 1819
2,6-Dinitrotoluene
ND
20
18
1
88
50-158
01/14/2018 1819
Di-n-octylphthalate
ND
20
24
1
122
4-146
01/14/2018 1819
1,2-Diphenylhydrazine(as azobenzene)
ND
20
15
1
74
30-130
01/14/2018 1819
bis(2-Ethylhexyl)phthalate
ND
20
22
1
109
8-158
01/14/2018 1819
Fluoranthene
ND
20
22
1
111
26-137
01/14/2018 1819
Fluorene
ND
20
16
1
82
59-121
01/14/2018 1819
Hexachlorobenzene
ND
20
18
1
90
0-152
01/14/2018 1819
Hexachlorobutadiene
ND
20
14
1
68
24-116
01/14/2018 1819
Hexachlorocyclopentadiene
ND
100
30
1
30
1-150
01/14/2018 1819
Hexachloroethane
ND
20
12
1
59
40-113
01/14/2018 1819
Indeno(1,2,3-c,d)pyrene
ND
20
14
1
71
0-171
01/14/2018 1819
Isophorone
ND
20
14
1
72
21-196
01/14/2018 1819
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 16

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: TA10099-001 MS
Matrix: Aqueous
Batch: 61673
Prep Method: 625
Analytical Method: 625
Prep Date: 01/11/2018 1714
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Naphthalene
ND
20
15
1
73
21-133
01/14/20181819
Nitrobenzene
ND
20
13
1
67
35-180
01/14/20181819
2-Nitrophenol
ND
20
16
1
78
29-182
01/14/20181819
4-Nitrophenol
ND
40
32
1
80
0-132
01/14/20181819
N-Nitrosodimethylamine
ND
20
12
1
61
1-150
01/14/20181819
N-Nitrosodi-n-propylamine
ND
20
13
1
63
0-230
01/14/20181819
N-Nitrosodiphenylamine (Diphenylamine)
ND
20
16
1
82
1-150
01/14/2018 1819
Pentachlorophenol
ND
40
41
1
104
14-176
01/14/20181819
Phenanthrene
ND
20
19
1
96
54-120
01/14/20181819
Phenol
ND
20
11
1
56
5-112
01/14/20181819
Pyrene
ND
20
21
1
107
52-115
01/14/20181819
1,2,4-Trichlorobenzene
ND
20
14
1
69
44-142
01/14/20181819
2,4,6-Trichlorophenol
ND
20
16
1
79
37-144
01/14/20181819
Acceptance
Surrogate
0
Q /o Rec
Limit
2-Fluorobiphenyl
74
37-129
2-Fluorophenol
59
24-127
Nitrobenzene-d5
69
38-127
Phenol-d5
54
28-128
Terphenyl-d 14
104
10-148
2,4,6-Tribromophenol
113
41-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 13 of 16

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 14 of 16

SHEALY ENVIRONMENTAL SERVICES, INC.
CD
t
L
z
-E
w
e
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 15 of 16

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy Fiiviwolw�lnJSrr:iGea,]ov. Page I arL
l.'oc,L11arr Ncnlh_r iiF ] $C--�} C] F:Ffca-m'r 1�. +�CE�'2718
m�xi� Receipt hecl�!>i�� �l��
Client: ~ Yl' Cooler lnspeffrW hyldate, Ci 6-IA2 / I 10 • i ` + hat a1= Y't4,o6-I e,
me am of receipt;
Client Lj UPS redrx I c3R,
3fe�J,
_
WCre cuctndy seals 'esentol.'ak L;uolm-7
EIYCSJ
4 l N0 2TNA12.1frustod
'Seal; wewc present, 1.-e= Lhcv intact and nr&T rkm'7
.)H Strip
Tf)_
Chlorine Ship ID:
"ouler ID 1 f}righi a I ternpeiatuer pppn rcco:pt ; Derived (Correoted) telrtpt rEu lure upon receipt,
oc
'let}tod.
I
m .A irr1L RLIttlos 11t QUn ID: TR Oun Gmfectiom Factar: :'C
4iethod of coo lajlt -
ZWcflcc El lee Padm 17 EIb , f ] N om
[� Yes
� No
4 NA
I 1t LVnrperxture ofanv�golcr exceeded6,0`C,��as l'rn .iecr. MAnager odfh--d?
_
PM wai NnLlJtcd by: phone i erna.iI } faces -to -face (circle one},
IJ Yes
] No
KA
4, Is dic commelvial courier's pacb;ing Slip atMd ter [bis farm?
es
Q No
5, Wcre proper ctletrdy Erocedures (Nhii tashedfrecoivod) followed?
es
No
6, Were sanllrl� JDs listed on tl_e COC?
Yes
i . No
1 Were sample IDs lisred (rn all sam le eorttaiocr.'
Yes
No
8. W&-i collection date &time Iiser;d on file C °
Yes
No
9. 'r ub uullccdan date & time listed q+] all Nmn le contaitlers ?
Ycs
© Mo
10. Did all Cootainer lnbcl infmTn4ion (ID, date, tiom,-) Who with the coc
Yes
0 No
l 1 , Wom rests to be performed listed {rn $c t " '
Yes
❑ No
1 -- Did €rJT-gwuples arrive in the proper containers for c.36 test iACVor in good COT14i[ion
11
1unbrr}kun. Us on, erc.)9
cs _; No 11. Was adequasumph: volume avaiJablt~-?
es Ar4 14, Were all sampics received within; the. hDldipgthnc or43 liirurs, whichever ODri]t S first?
_. Yes 1 D 15, Were Amy sanl les oontal.rrt�r� mi ssiloglexcess (f ircle ona ) samplus Not listed l7t'S ?
�� Yes _ 17Jlr I iG. Far VOA and RSK-175 sa]nglcs, iyurc bubble:, pm%ent: °,pea -sire' (b},'or 6mm in diameter)
In an}'411116 VD-+1 vial.;7
7 Yes _] T1c, • INA I?, W ere all DMinctals+'nutric_0 tir,mplcs reoe v424 UL a pH of C: 2?
J Yes _ ZVo NA J$. Ya'ere all cyaTli4'r sam ias roc'Uiacd �E a ll i :} 12 and 51.11nde-5ninplo rcacived at a rH � 97
Yeg El No �Ai 9. wcruall bppli able J�lils?T r'cyanldr`p}lcnol+b25 t<: il..Smg}L}samp as renarrT siduaJ
Yes Na L HA 2l), Werk clicnti%errrarks+`rcquosts(Le- r gM5LUd dilurians, kf ,+1gSDdesignaLuns,;:tc,,.}
oomectly trarvL�cribed froth, tllti COC into the antttiMftt secti011 ill .LINTS?
Yes No 21- Dk ,TK. quote number Lise-d taken from the i.:untainwr label's
Sample 1'rovi-vadorr (14'Eusl hr, rmnpleted f�r 4:14 samplc(s) ir3cwTatly preserved or wilh hcadspaae,)
SaLuFla(s} wurc received incorrectly poeservvd and were adjurtad moording.1
i r mmplc receMng With (FLS114,1•iNO3, HC1, NaOH) us iTt¢ SR 4
wt:re received with bubbles >6 tom in diameter.
ample,(iL) were I+eoelvml with FRC : 41-5 rag's (if 42.1 is no_) and wove
diustcd accordingly in samplerecei%�g with sodiwn il,ir)xulfalc � S2 w1 with 5hcaiyI'D: _
C D--irtlLinlg Water Project Sample(s) pH Yt�rifiod Lu be <2. by Date,
am 1a(s)_ q*CN MOC T%::ceivexi AT a pH of-.2 alld WO= auijUSA accordingly asinp SR4
bart!cxlc labels applied by: i' l L .} fate; / - f 4� - 1 '.
Commuits:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 16 of 16