MO-6615_27296_CA_MRP_20170215_GWSamplingReport

J.T. Ryerson & Son, Inc.
Free Product Recovery and Groundwater
Monitoring Report
December 2016
Former Integris Metals Facility
527 Atando Avenue
Charlotte, North Carolina
Delivering sustainable solutions in a more competitive world
ERM

Site Information
Site Identification
Date of Report: February 13, 2017
Facility I.D. None Incident Number 27296 Site Risk/Priority Risk Intermediate
Site Name: Former Inteeris Metals
Site Street Address: 527 Atando Avenue
City/Town: Charlotte Zip Code: 28206
County: Mecklenburg
Description of Geographical Data Point (e.g., diesel fill port): Fuel Oil #2 UST
Location Method (GPS, topographical map, other): Site reconnaissance and website
Latitude: 35.25785 Longitude:-80.816810 (Source Area Location)
Information about Contacts Associated With the Leaking UST System
UST Owner:
Joseph T. Ryerson & Son, Inc.
Address:
227 W. Monroe Street, Chicago, IL
Tel:
[phone]
UST Operator:
Joseph T. Ryerson & Son, Inc
Address:
227 W. Monroe Street, Chicago, IL
Tel:
[phone]
Property Owner:
Advantage Machinery Services
Address:
1407 Highway 601 South, Yadkinville, NC 27055
Tel:
[phone]
Property Occupant: Sunbelt -Turret Steel
Address:
527 Atando Avenue, Charlotte, NC 28206
Tel:
[phone]
Consultant/Contractor: ERM NC, Inc.
Address:
15720 Brixham Hill Avenue, Suite 120, Charlotte, NC 28277
Tel:
[phone]
Information about Release
Date Discovered: November 13, 2002
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Dispenser/Piping/UST): UST
Sizes and contents of UST system(s) from which the release occurred: 12,000 gallon Fuel Oil UST
Certification
I, Rick Tarravechia a Professional Engineer icensed Geolo i (circle one) for ERM NC, Inc.,
do certify that the information contained in this report is correct and accurate to the best of my
knowledge. (Affix Seal and Signature)
CA
01.
SEAL = ?
ERM NC, Inc. is licensed to practice geology and engineering in North Carolina. The certification
number of the company or corporation is C-470.
ERM NC, Inc. 1 GW Sampling Report - Atando Ave. 2-2017.docx

1.0 FREE PRODUCT RECOVERY ACTIVITIES
On December 27 and 28, 2016, ERM performed a surfactant injection and recovery event at the
Site. The injection event took place on December 27 using existing monitor well MW-1. An oil -
water interface probe was initially used to measure the free product thickness, which was 0.005
feet. Approximately 200 gallons of a 5% solution of surfactant (PetroSolvTM) were gravity fed
into MW-1 over a 4-hour period.
On December 28, a via vacuum truck was used to extract approximately 200 gallons of
groundwater and emulsified petroleum from MW-1. A copy of the materials manifest is
included in Appendix C.
2.0 GROUNDWATER MONITORING ACTIVITIES
2.1 GROUNDWATER ELEVATION MEASUREMENTS
Water level measurements were obtained in the site monitor wells prior to well purging and
sampling on December 29, 2016 using a decontaminated electronic water level meter. Using top
of casing elevations and the depth to water measurements, site groundwater elevations and
hydraulic gradients in the saprolite aquifer were calculated. Monitor well construction
information is presented in Table B-7. No free product was measured in monitor well MW-1;
therefore, it was included in the sampling network.
2.2 GROUNDWATER SAMPLE COLLECTION
The monitor wells were purged and sampled using low flow techniques with a peristaltic
pump and new polyethylene tubing dedicated to each well. Flow rates during purging
averaged 100 milliliters per minute. General groundwater quality parameters (pH,
temperature, conductivity, dissolved oxygen, and turbidity) were measured in the field
during purging using a flow -through sampling cell. Sampling was performed once the
parameters had stabilized. Low -flow samples were collected directly from the polyethylene
tubing. Field sampling sheets are included in Appendix A.
The samples were immediately placed on ice inside insulated shipping containers, and then
delivered under the appropriate chain -of- custody protocol to Shealy Environmental Services,
Inc. (Shealy) in West Columbia, South Columbia for analyses. The samples were analyzed for
volatile organic compounds (VOCs) by EPA Method 8260B for the EPA 602 plus xylenes list,
for semi -volatile organic compounds (SVOCs) by EPA Method 625, and volatile petroleum
hydrocarbons (VPH) and extractable hydrocarbons (EPH) by the Massachusetts Department
of Environmental Protection (MADEP) Methods. A copy of the laboratory report is in
Appendix B.
ERM NC, Inc. 2 GW Sampling Report - Atando Ave. 2-2017.docx

3.0 GROUNDWATER MONITORING RESULTS
3.1 GROUNDWATER ELEVATIONS AND FLOW
The depth to groundwater in the saprolite zone varies across the monitoring area from 14.18
feet below ground surface (bgs) in monitor well MW-4 to 19.69 feet bgs in monitor well MW-2.
Groundwater in the saprolite aquifer flows to the south toward an intermittent stream that is
located approximately 250 feet west of the source area, on the west side of the railroad tracks.
Groundwater flows under an average hydraulic gradient of 0.013 as shown in Figure 3.
Groundwater elevation data are summarized in Table B-7.
3.2 GROUNDWATER RESULTS
Laboratory analysis of groundwater samples detected target compounds in four of the six wells
sampled at the site. The highest concentrations of VOCs and SVOCs were in MW-1 and MW-2,
which is located downgradient from UST-1. The current and historical groundwater results are
summarized in Table B-4. Figure 4 illustrates analytical results from the December 2016 event. The
historical comparison of analytical results between samples collected from MW-1 in June 2016 and
December 2016 indicate that semivolatile hydrocarbons were reduced by one or more orders of
magnitude. This reduction appears to be the result of the surfactant injection/extraction event
discusse in Section 1.0. Benzene, fluorene, naphthalene, and VPH/EPH exceeded 2L groundwater
standards in several wells. However, gross contaminant levels were not exceeds in any site wells.
4.0 CONCLUSIONS
In order to remove free product and reduce the contaminant mass in MW-1, approximately 200
gallons of a 5% solution of surfactant (PetroSolvTM) were gravity fed into MW-1 on December
27. A via vacuum truck was then used to extract approximately 200 gallons of groundwater
and emulsified petroleum on the following day.
Groundwater samples collected from MW-1 showed a notable decrease in SVOC concentrations
from the June 2016 event. Benzene, fluorene, naphthalene, and VPH/EPH still exceeded 2L
groundwater standards in several wells acros the site. However, gross contaminant levels were
not exceeded in any site wells. Based on this single event, it appears that free product has been
removed from the source area, and SVOC concentrations have been significantly reduced in
monitor well MW-1. Continued free product gauging will be conducted to confirm the absence of
product over time. However, based on the preliminary results, it appears that the site will be
eligible for closure via Notice of Residual Petroleum.
ERM NC, Inc. 3 GW Sampling Report - Atando Ave. 2-2017.docx

Figures

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FIGURE 1
ERM NC, Inc. Site Location Map
ERM 527 7 Ata is Metals
Atando Avenue
Charlotte, North Carolina
DATE: 2/8/2017 SCALE: AS SHOWN DRAWN: AFreeman
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Shallow Well
Deep Well
UST op
Site
Building'
Paved
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Basemap Mecklenburg County.
...� Mecklenburg County: 2015Aerial, Site Features, Property lines
—mot
FIGURE 2
ERM NC, Inc. Site Plan
ERM Integris Metals
527 Atando Avenue
scAl_E: AS SHOWN oRAwM: AFreeman DATE:7211112.�l7 Charlotte, North Carolina
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Explanation
Shallow Well
Deep Well
Groundwater Elevation Contours
— —
(dashed in areas of less certainty)
--0—
Approximate direction of groundwater flow
UST
Q
Site
Building
Paved
M-
1
0
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Feet
Basemap Mecklenburg County.
Mecklenburg County: 2015Aerial, Site Features, Property lines

L
w
d
Atando Av J
r QG t,
I
0
f Not Sample Due to Standing Water
Around Wellhead
SVOCs - EPA Method 625 (Ng/1)
Not Sample Due to Standing Water
Around Wellhead
MADEP VPH/EPH (Ng/I)
Not Sample Due to Standing Water
Around Wellhead
Explanation f-
Y
00MW-1 12/29/2016 M W-2 12/29/2016
VOCs - EPA Method 602 (Ng4) / 8260B VOCs - EPA Method 602 (Ng4) / 8260B
Benzene 70 Benzene 60
y
T7Fthylbenzene 48 Ethylbenzene 10
Toluene 2.3 Xylenes (total) 3.7
Xylenes (total) 14 SVOCs - EPA Method 625 (Ng4)
SVOCs - EPA Method 625 (Ng/1) Naphthalene 54
Naphthalene 200 Phenanthrene 10
Phenanthrene 61 MADEP VPH/EPH (Ng/I)
MADEP VPH/EPH (Ng/I) C5-C8 Aliphatics VPH 86
C9-Cl2 Aliphatics - VPH 4,000 C9-C12 Aliphatics - VPH 260
C9-Cl8 Aliphatics - EPH 2,800 C9-C18 Aliphatics - EPH 260
C9-Cl0 Aromatics - VPH 1,900 C9-C10 Aromatics - VPH 220
UST-1 C11-C22 Aromatics - EPH 2,200 C11-C22 Aromatics - EPH 540
IF
0 W-�� .rl{ MW-2 UST-2
MW- MW-3
VOCS - — meuruu ouc Ipgnj i —
MW-4 12/29/2016 MW-4 Benzene Z
VOCs - EPA Method 602 (Ng/1) / 82608 O O DW-� DW-1 12/29/2016 Xylenes (total)Not Detected VOCs - EPA Method 602 (Ng4) / 8260B SVOCs - EPA Method 625 (Ng/1)
SVOCs - EPA Method 625 (Ng/1) Not Detected Naphthalene 7
Not Detected SVOCs - EPA Method 625 (Ng4) MADEP VPH/EPH (Vg/1)
MADEP VPH/EPH (Ng/I) Not Detected Not Detected
Not Detected MADEP VPH/EPH (Ng4) 0 25
Not Detected 50
Shallow Well-
__ 4
O Deep Well - - - -
'.
UST
Site
Building
Paved
Feet
Basemap Mecklenburg County.
Mecklenburg County: 2015Aerial, Site Features, Property lines
- FIGURE 4
ERM NC, Inc. Recent Groundwater
Concentrations Map
ERM Integris Metals
527 Atando Avenue
SCALE: AS SHOWN DRAWN: AFreeman DATE: 2/8/2017
Charlotte, North Carolina
115DCLTDCAI �DahlCharlotleWro�eds10345276 Ryerson Inc 2016 Free Produal Removal.hPV2yreraonGISIM%DQ017-01 1Fig4_CommW

Tables

TABLE B-1 SITE HISTORY - UST SYSTEM AND OTHER RELEASE INFORMATION
Facility I.D.: Not established
Date: February 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Release
Description of
Associated
UST ID
Current/
Capacity
Construction
Associated Piping
with UST
Number
Last Contents *
(gallons)
Details
and Pumps
Date Installed
Status of UST
System?
1
Fuel Oil #2
6,000
Steel
No dispensers. ""
1966 or as
Removed
Yes
2
Fuel Oil #2
6,000
Steel
No dispensers. "
early as 1949
Closed in Place
Yes
Incident
Material
Date of
Number
Released
Release
Description of Release
27296
Fuel Oil
11/13/2002
The release was discovered as part of due diligence for a property transaction in 2002. The amount of
product released from the UST is not known.
TABLE B-2 SITE HISTORY - OWNER/OPERATOR AND OTHER RESPONSIBLE PARTY INFORMATION
(most recent first) Facility I.D.: Not established
Date: February 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
UST ID Number
I Name of Owner or Operator
jDates of Ownership/Operation
Owner or Operator?
1 and 2
lJoseph T. Ryerson & Son, Inc.
Present
Owner
Address
Telephone Number
227 W. Monroe Street, Chicago, IL
Date of Release 11/13/2002
[phone]
ERM Page 1 of 1

TABLE B-4-1 SUMMARY OF GROUND WATER SAMPLING RESULTS - VOCs and SVOCs
Facility I.D.: 0 Facility I.D.: Not established
Date: Feb-17 Incident Number and Name: Incident Nun # 27296 / 527 Atando Avenue, Charlotte, NC
Analytical Method
VOCs - EPA Method 602 (pg/1) / 8260B
SVOCs - EPA Method 625 (pg/1)
m
m
o_
X
d
f6
O
f6
O
ly
Cu
Sample ID
Source
Date
m
w
X
¢
Z
o
z
d
NC Ground Water
Standard (21L)
1
600
600
500
2,000
3
NE
300
6
200
5,000
85,500
2,000
410
Gross Contamination
Level
84,500
260,000
170
NE
990
6,000
1/3/2003
Not Sampled Due to Free Product
MW-1
MW
6/14/2016
66
90
ND
ND
460
ND
ND
570
2,100
2,100
12/29/2016
70
48
2.3
14
ND
ND
ND
f
200
61
1/3/2003
55
15
2.0
98
ND
ND
ND
18
92
39
MW-2
MW
6/14/2016
61
19
ND
8
ND
ND
11
4.2
41
3.8
12/29/2016
60
10
ND
3.7
ND
ND
ND
ND
54
10
1/22/2003
1.6
ND
ND
ND
ND
11
ND
ND
ND
ND
MW-3
MW
6/14/2016
1.6
ND
2.1
2.1
ND
1.6
ND
ND
3.5
ND
12/29/2016
9.7
ND
ND
3.8
ND
ND
ND
ND
7.5
ND
1/22/2003
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
MW-4
MW
6/14/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1/22/2003
3.6
ND
1.8
ND
ND
ND
ND
ND
ND
ND
MW-5
MW
6/14/2016
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12/29/2016
Not Sample Due to Standing Water Around Wellhead
1/22/2003
ND
ND
ND
ND
ND
ND
ND
ND
ND
DW-1
MW
6/14/2016
NDFND
ND
ND
ND
I
ND
ND
ND
ND
ND
ND
12/29/2016
NDND
ND
ND
ND
ND
ND
ND
ND
ND
Only detected compounds are included in table.
pg/L = micrograms per liter
ND = Not detected
NE - Not Established
NA = Not Applicable NA = Not Applicable
Results shown in bold exceed the applicable Ground Water Standard (T15A 2L)
ERM Page 1 of 1

TABLE B-4-2 SUMMARY OF GROUND WATER SAMPLING RESULTS - MADEP
Facility I.D.: 0 Facility I.D.: Not established
Date: Feb-17 Incident Number and Name: Incident Nur # 27296 / 527 Atando Avenue, Charlotte, NC
Analytical Method
MADEP VPH/EPH (pg/1)
U
U
=
N
U
w
U
•N
=
Q
W
Eo
O
W
U
U
N
00 f6
N
00
f6
O
CO•U
U Q
U=
U Q
U=
U=
� Q
Sample ID
Source
Date
U Q
U>
U Q
U>
U w
U Q
NC Groundwater Standard (2L)
40
NA
7700
NA
200
NA
10,000
NA
Gross Contamination Level
1/3/2003
Not Sampled Due to Free Product
MW-1
MW
6/14/2016
1,700 13,000 1,400,000
8,200 600,000 180,000
12/29/2016
ND 4,000 2,800
1,900 2,200 ND
1/3/2003
ND
ND
1,100
770
1,600
ND
MW-2
MW
6/14/2016
ND
210
120
250
510
ND
12/29/2016
86
260
260
220
540
ND
1/22/2003
ND
ND
ND
ND
ND
ND
MW-3
MW
6/14/2016
ND
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
1/22/2003
ND
ND
ND
ND
ND
ND
MW-4
MW
6/14/2016
ND
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
1/22/2003
3,500
ND
ND
ND
ND
ND
MW-5
MW
6/14/2016
2,400
1 ND
ND
ND
ND
ND
12/29/2016
Not Sam le Due to Standin Water Around Wellhead
1/22/2003
ND
ND
ND
ND
ND
ND
DW-1
MW
6/14/2016
150
ND
ND
ND
ND
ND
12/29/2016
ND
ND
ND
ND
ND
ND
Only detected compounds are included in table.
pg/L = micrograms per liter
ND = Not detected
NE - Not Established
NA = Not Applicable NA = Not Applicable
Results shown in bold exceed the applicable Ground Water Standard (T15A 2L)
ERM Page 1 of 1

TABLE B-7 WELL CONSTRUCTION INFORMATION
Date: Feb-17 Incident Number and Name: Not established
Facility ID#: # 27296 / 527 Atando Avenue, Charlotte, NC
Top of
Depth to
Product
Ground
Date Water
Well Casing
Screened
Casing
Water
Thicknes
Water
Monitor
Level
Depth
Interval
Bottom of Well
Elevation
(feet
s
Elevation
Well ID
Date Installed
Measured
(feet BGS)
(feet BGS)
(feet BGS)
(feet*)
BTOC)
(feet)
' (feet)
Comments
MW-1
1/22/03
12/29/16
19
19-34
34
104.50
17.82
ND
86.68
MW-2
1/22/03
12/29/16
19
19-34
34
104.50
19.69
1 ND
84.81
MW-3
1/22/03
12/29/16
17
17-32
32
99.72
14.97
ND
84.75
MW-4
1/22/03
12/29/16
17
17-32
32
99.90
14.18
ND
85.72
1/22/03
12/29/16
17
17-32
32
101.79
Wellhead submerged in
MW-5
water.
DW-1
1/22/03
12/29/16
81
81-86
88
100.00
1 13.62
ND
86.38
Reference point for elevation measurements: 100 feet
If free product is present, ground water elevation should be calculated by: [top of casing elevation - depth to water] + [ free product thickness x 0.8581]
Feet BGS = Below Ground Surface Feet BTOC = Below Top of Casing
ERM Page 1 of 1

TABLE B-8 FREE PRODUCT RECOVERY RESULTS
Date: February 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Free Product Recovery Method: Bailer/Passive Skimmer/Sock/AFVR Facility ID#: NA
Method of Measurement: Bailer / Interface probe
Well ID
Product Type
Date of
Recovery
Casing
Diameter
(inches)
Product
Thickness
Before
Recovery (ft.)
Product
Thickness After
Recovery (ft.)
Amount of
Product
Recovered
(gallons)
Depth to Water
from Top of
Casing (ft.)
Comments
MW-1
Fuel Oil
1/3/03
2 0.05 0.00 <0.25 21.32
Bailer
1/22/03
2 0.02 0.00 <0.25 16.23
Bailer
3/10/03
2 0.04 0.00 <0.25 14.07
Bailer
3/25/03
2 0.00 0.00 <0.25 12.99
Bailer
4/4/03
2 0.03 0.00 <0.25 12.68
Bailer
5/30/03
2 0.01 0.00 <0.25 11.01
Bailer
6/27/03
2 0.02 0.00 <0.25 11.24
Bailer
7/17/03
2 0.01 0.00 <0.25 11.71
Bailer
8/26/03
2 0.01 0.00 <0.25 11.15
Bailer
9/2/03
2 0.01 0.00 <0.25 12.18
Bailer
11/14/03
2 0.01 0.00 <0.25 15.23
Bailer
11/24/03
2 0.01 0.00 <0.25 15.10
Bailer
12/19/03
2 0.04 0.00 <0.25 14.74
Bailer
1/29/04
2 0.05 0.00 <0.25 15.05
Bailer
3/9/04
2 0.00 0.00 <0.25 13.19
AFVR
4/8/04
2 0.04 0.00 <0.25 13.07
Bailer
5/10 to 5/19/04
Source Removal: UST and 416 tons of contaminated soil removed to depth of 17
feet.
5/24/04
2 0.08 0.00 0.20 13.22
Bailer
6/23/04
2 0.07 0.00 <0.25 15.00
Bailer
7/28/04
2 0.05 0.00 <0.25 15.75
Bailer
8/27/04
2 0.12 0.00 0.25 15.52
Bailer
10/5/04
2 0.05 0.00 <0.25 14.14
Bailer
11/1/04
2 0.10 0.00 0.25 14.67
Bailer
12/2/04
2 0.03 0.00 <0.25 14.53
Bailer
11/17/13
2 0.55 0.00 <0.25 17.89
Bailer
2/5/14
2 0.67 0.00 <0.25 15.34
Passive Skmr
2/17/14
2 <0.01 0.00 <0.25 14.55
Passive Skmr
2/27/14
2 <0.01 0.00 <0.25 14.01
Passive Skmr
3/27/14
2 <0.01 0.00 <0.25 13.60
Passive Skmr
8/6/14
2 <0.01 0.00 <0.25 14.45
Passive Skmr
4/10/15
2 <0.01 0.00 <0.25 14.01
Passive Skmr
5/27/15
2 0.01 0.00 <0.25 14.76
Passive Skmr
7/28/15
2 0.08 0.00 <0.25 17.72
Passive Skmr
1/28/16
2 0.19 0.00 0.00 12.92
Passive Skmr
2/18/16
2 0.13 0.00 0.00 13.22
Passive Skmr
3/25/16
2 <0.01 0.00 0.00 13.01
Sock
3/31/16
2 <0.01 0.00 0.00 12.91
Sock
4/14/16
2 <0.01 0.00 0.00 13.40
Sock
5/5/16
2 <0.01 0.00 0.00 13.66
Sock
6/14/16
2 0.02 0.00 0.00 13.92
Sock
12/27/16
2 0.015 0.00 0.00 16.62
Sock
12/27-12/28/16
Surfactant injection/extraction event
12/29/16
2 <0.01 1 0 1 0.00 1 17.80
AFVR

TABLE B-8 cont. FREE PRODUCT RECOVERY RESULTS
Date: February 2017 Incident Number and Name: # 27296 / 527 Atando Avenue, Charlotte, NC
Free Product Recovery Method: Bailer/Passive Skimmer/Sock/AFVR Facility ID#: 0
Method of Measurement: Bailer / Interface probe
Well ID
Product Type
Date of
Recovery
Casing
Diameter
(inches)
Product
Thickness
Before
Recovery (ft.)
Product
Thickness After
Recovery (ft.)
Amount of
Product
Recovered
(gallons)
Depth to Water
from Top of
Casing (ft.)
Comments
RW-1
Fuel Oil
11/24/03
4
0.05
0
0.25
15.20
Bailer
12/19/03
4
0.15
0
0.25
15.32
Bailer
1/29/04
4
0.42
0
0.25
15.56
Bailer
3/9/04
4
0.05
0
2.00
13.32
AFVR
4/8/04
4
0.15
0
0.25
13.29
Bailer
5/10 to 5/19/04
Source Removal:
UST and 416
tons of contaminated
soil removed
to depth of 17
feet.
5/24/04
4
0.17
0
0.30
13.43
Bailer
6/23/04
4
0.23
0
0.30
15.38
Bailer
7/28/04
4
0.27
0
0.30
15.46
Bailer
8/27/04
4
0.29
0
0.30
15.75
Bailer
10/5/04
4
0.15
0
0.30
13.87
Bailer
11/1/04
4
0.17
0
0.30
14.91
Bailer
12/2/04
4
0.03
0
<0.25
14.74
Bailer
2/27/14
4
<0.01
0
0.00
14.00
---
5/27/15
4
0.01
0
0.00
14.68
---
7/28/15
4
0.01
0
0.00
17.31
---
1/28/15
4
<0.01
0
0.00
13.41
---
2/28/16
4
<0.01
0
0.00
13.49
---
3/31/16
4
<0.01
0
0.00
13.23
---
4/14/16
4
<0.01
0
0.00
13.27
---
5/5/16
4
<0.01
0
0.00
13.66
---
6/14/16
4
<0.01
0
0.00
13.90
---
5/5/16
4
<0.01
0
0.00
13.66
---
12/29/16
4
<0.01
0
0.00
13.62
---
Total Gallons Recovered to Date: Approximately 6.25 gallons

Appendix A
Field Sampling Sheets

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: Ryerson - Atando
Sample Type: Circle one - (Monitor Well,
DPT, Surface Water, Potable WSW; other)
Job #:
Sample ID: 14 fv- )
Date: 12/ J 1 /16
Sampling Personnel:
Corey League
Weather Conditions: Sunny, Partly Cloudy,
Cloudy,
Rain; Other
Time:
Well Type: Flush S rfac Completion, Stick Up Completion
Well Tag Present:
Yes,
Well Locked: e , No
Lock Present: Y 9,
No
Well ID info. on Tag:
Yes, o
Well Bolted: Yes, N
Well Cap:
e , No
Well Cap Condition:
od, eplace, Other;
Well Pad Condition: Good,
Cracked, Replace, Other:
Well Location: Grass,
Asphalt, CoWete,
Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
51 101 151
20
feet -other:
Depth to Water D.T.W :
Well Diameter:
2� 4, 6, 8
Inches -other:
Field Parameters measured
with: Y ;%
(
Casing Type:
PJSk Steel
other:
Purge Rate:
mUmin
Sampling Device:
Pe&i,Staltic, Monsoon, Grundfos, Bailer, Other:
Tubing Type: Polyethylene, Teflon, Other:
Measuring Point:
O
other:/ 4/'OA
14, r
Pump Intake (ft below M.P.):
Color: 4,9,p
Odor:
Y(�es No
Time:
min
Volume
P u r ed
DTW:
feet
Temp
('C)
pH
std units
SpC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria`
.�
((jam)
(see note
below)'
+/_
3%
+/-
0.1 unit
+/-
3%
+/-
10%
+/_
10 mV
+/_
10%4
77
� ,r t7
/i! l/�
C� ����
� i�
�t�t
(f ��
'Cr./.r
'-
',
IF. tj
OF
r( ;hLp ti
Official Sampling Date &Time:
Samples Collected: Analysis Requested: Preservative:
3 - VOAs VOC by 8260 HCL
SVOC by 625
EPH
VPH
Notes:
(1) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2) -Stabilization crdeda based on three most recent consecutive measurements.
(3) -Total dtatVdol'/n In well to be less than 0.1 m (0.32 fl). Purging rate to be lowered as necessary to keep drawdown below 0.1 m (0.32 fl}.
(4) +/-10% when turbidity Is over 10 NTUs.
Hold
Time (days): Lab:
14 Shealy
Shealy
Shealy
Shealy

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name: Ryerson - Atando
Sample Type: Circle one - (Monitor Well,
DPT, Surface Water,
Potable WSW; other)
Job #:
Sample ID: OA1111e.
Date: 12/) i% /16
Sampling Personnel:
Corey League
Weather Conditions: Sunny, Partly Cloudy,
Cloudy, Rain; Other
Time: / - 4'
Well Type: Flush urfa
Completion, Stick Up Completion
Well Tag Present:
Y s, No
Well Locked: f9i Nq
Lock Present: ke , No
Well ID info. on Tag:
e , No
Well Bolted: Yes,
Well Cap:
, No
Well Cap Condition:
q6qd, Replace, Other;
Well Pad Condition: Good,
Cracked, Replace, Other:
Well Location: Grass,
Asphalt, C
c ete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
5, 10, 15,
o' feet -other:
Depth to Water D.T.W : t�)
G
Well Diameter:
41 6, 8
Inches -other:
Field Parameters measured with: y5 f ,
u
Casing Type:
feVC, Steel
other:
Purge Rate: iU
mUmin
Sampling Device:
P i'taltic, Monsoon, Grundfos, Bailer, Other:
Tubing Type: Po l et ylene,
Teflon, Other:
Measuring Point:
luc
other:
Pump Intake (ft be ow M.P.):
Color:
Odor: No
r�
Time:
min
=ue
DTW:
feet
Temp
(eC)
pH
std units
SPC
uS/cm
DO
mg/L
ORP
mV
Turb
NTU
Comments:
Stabalization
L
(gaH@M)
(see noteCriteria`
below)'
3%
0.1 unit
3%
10%
10 mV
10%4
f r �
���
y�
zz�
S
t7-
�,
r ti ti
I �. f
K y
i
'�'
s. �r
Id
(ylfr77
C�
Official Sampling Date &Time: / a%l`/%( %1!
Samples Collected: Analysis Requested: Preservative:
3 - VOAs VOC by 8260 HCL
SVOC by 625
EPH �
VPH
Notes:
(1) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) -Total drawdown in yell to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep dravrdown below 0.1 m (0.32 fl).
(4) +/-10 % when turbidity is over 10 NTUs.
Hold Time (days� Lab:
14 Shealy
Shealy
Shealy
Shealy

WATER MATRIX SAMPLING
FIELD DATA FORM
Site Name: Ryerson - Atando
Sample Type: Circle one - (Monitor Well,
DPT, Surface Water, Potable WSW; other)
Job #:
Sample ID: i,,,
Date: 12/ /16
Sampling Personnel:
Corey League
Weather Conditions: Sunny, Partly Cloudy,
lougy,
Rain; Other
Time: lo) 7
Well Type: Flush urface
ompletion, Stick Up Completion
Well Tag Present:
No
Well Locked: No
Lock Present: Yes,
No
Well ID info. on Tag:
e , No
Well Bolted: e , No
Well Cap:
Yes, No
Well Cap Condition:
,, Replace, Other;
Well Pad Condition: Good,
Cr. ke Replace, Other:
Well Location: Grass,
sph t, Concrete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
5aL`
Screen Length:
51 10, 15
20
feet -other:
Dept to Water D.T.W : Itl
i c
Well Diameter:
2, 4, 61 8
Inches -other:
Field Parameters measured
with: YS f 4
y
Casing Type:
E2, Steel
other:
Purge Rate: { y
mUnnin
Sampling Device:
PO t tic, Monsoon, Grundfos, Bailer, Other:
Tubing Type: PoIV thylene, Teflon, Other:
Measuring Point:
LY.e-P
other:
Pump Intake (ft be ow M.P.): "' /'
Color:
Odor:
Yes, o
Time:
min
Volume
Purged
DTW:
feet
Temp
(eC)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria`
L
(gauns)
(see note
below)'
+/- k
3%
+/-
0.1 unit
+/-
3%
+/-
10%
+/-
10 mV
+/-
10%4
C)i�Ell
l
fi
�e•c.y
l 1
lit6-q
e.5,z
©tO
1.
'
q.c,
(F2q
ii�'
�6I
'� �
)(14�,
U r °I J,
3 `
4 Ajt
Official Sampling Date &Time: q11 GL,!�
Samples Collected: Analysis Requested: Preservative:
3 - VOAs VOC by 8260 HCL
SVOC by 625
EPH
VPH
Notes:
(1) - Do not measure depth to bottom ofwell until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2) - Stablllzation cdteda based on three most recent consecutive measurements.
(3) -Total drawdovm in yell to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep dravrdo�m below 0.1 m (0.32 ft).
(4) +1-10 % when turbidity is over 10 NTUs.
Hold
Time (days Lab:
14 Shealy
Shealy
Shealy
Shealy

WATER MATRIX SAMPLING
FIELD DATA FORM E
RM
Site Name: Ryerson - Atando
Sample Type: Circle one - (Monitor Well,
DPT, Surface Water,
Potable WSW; other)
Job #:
Sample ID: t. ' got
Date: 12/ /16
Sampling Personnel:
Corey League
Weather Conditions: Sunny,
Pa, Clo))dy,
Cloudy, Rain;
Other
Time:
Well Type: Flush u ace Completion, Stick Up Completion
Well Tag Present:
No
Well Locked: Yes,
Lock Present: Yes, N
Well ID info. on Tag:
Yjs, No
Well Bolted: s, No
Well Cap:
tej, No
Well Cap Condition:
ad, Replace, Other;
Well Pad Condition: Good,
Cr ck d, Replace, Other:
Well Location: Grass,
p alt, Concrete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
51 101 15
20
feet -other:
Dept to Water D.T.W : (+1
t • / ;
Well Diameter:
41 61 8
Inches -other:
Field Parameters measured
with:
Casing Type:
I&C, Steel
other:
Purge Rate: )�jU
mUmin
Sampling Device:
P'ri" altic, Monsoon, Grundfos, Bailer, Other:
Tubing Type: Polyethylene, Teflon, Other:
Measuring Point:
6
other:
Pump Intake (ft below M.P.): '7 . `
Color:
Odor:
Yes, No)
Time:
min
Volume
Pur ed
DTW:
feet
Temp
CC)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria2
(ems)
F
(see note
below)'
0.1 unit
3%
10 m/V
10%4
:��
+3%
73(
%✓j
y y10%
�l•i
4�t1
�.(,
t ,Ji
i�.�'�r
�.
3i
3
,t
iv
11 .31
q
�s4
).o
,r
�(d.
3 4
1 IC9 1
Official Sampling Date &Time:
Samples Collected: Analysis Requested: Preservative:
Notes:
(1) - Do not measure depth to bottom of well until after purging and sampling to reduce resuspending fines that may be restlng on the well bottom.
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) -Total drawdown in well to be less than 0.1 m (0.32 ft). Purging rate to be lowered as necessary to keep drawdown below 0.1 m (0.32 ft).
(4)+/-10% when turbidity is over 10 NTUs.
Hold

WATER MATRIX SAMPLING
FIELD DATA FORM ERM
Site Name; Ryerson - Atando
Sample Type: Circle one - (Monitor Well, DPT, Surface Water, Potable WSW; other)
Job #:
Sample ID:
Date: 12/,/16
Sampling Personnel: Corey League
Weather Conditions: Sunny, Partly Cloudy, Cloudy, Rain; Other
Time:
Well Type: Flush Surface Completion, Stick Up Completion
Well Tag Present:
Yes, No
Well Locked: Yes, No Lock Present: Yes, No
Well ID info. on Tag:
Yes, No
Well Bolted: Yes, No Well Cap: Yes, No
Well Cap Condition:
Good, Replace, Other;
Well Pad Condition: Good, Cracked, Replace, Other:
Well Location: Grass,
Asphalt, Concrete, Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
51 101 15, 20
feet -other:
Depth to Water D.T.W : t+l
Well Diameter:
2, 41 61 8
Inches -other:
Field Parameters measured with:
Casing Type:
PVC, Steel
other:
Purge Rate: mumin
Sampling Device:
Peristaltic, Monsoon, Grundfos, Bailer, Other:
Tubing Type: Polyethylene, Teflon, Other:
Measuring Point:
TOC
other:
Pump Intake (ft below M.P.):
Color:
Odor:
Yes, No
Time:
min
Volume
Purged
DTW:
feet
Temp
CC)
pH
std units
SPC
uS/cm
DO
m /L
ORP
mV
Turb
NTU
Comments:
Stabalization
CriterW
(gallons)
(see note+/-
below)'
3%
0.1 unit
3%
10%
10 mV
10%4
64
l)'
r�
pfj/Cp .
Official Sampling Date &Time: �✓� �- �ffM1� ��'�
Samples Collected: Analysis Requested: Preservative:
3 - VOAs VOC by 8260 HCL
SVOC by 625
EPH
VPH
Notes:
(1) - Do not measure depth to bottom Orwell until after purging and sampling to reduce resuspending fines that maybe resting on the well bottom.
(2) -Stabilization criteria based on three most recent consecutive measurements.
(3) -Total dratvdown In well to be less Than 0.1 m (0.32 ft). Purging rate l0 6e lowered as necessary to keep drawdotm below 0.1 m (0.32 ft).
(4) +/-10%when turbidity Is over 10 NTUs.
Hold
Time (days): Lab:
14 Shealy
Shealy
Shealy
Shealy

WATER MATRIX SAMPLING
FIELD DATA FORM .ER
Site Name: Ryerson - Atando
Sample Type: Circle one - (Monitor Well, DPT, Surface Water, Potable WSW; other)
Job #:
Sample ID: lv'
Date: 12/ /16
Sampling Personnel: Corey League
Weather Conditions: Sunny, PTIly Ooudy, Cloudy,
Rain;
Other
Time:
Well Type: Flush S ac ompletion, Stick Up Completion
Well Tag Present:
Yes, g)
Well Locked: No Lock Present:
Ns,
No
Well ID info. on Tag:
04F
Well Bolted: e , No Well Cap: Y)zls, No
Well Cap Condition:
Replace, Other;
Well Pad Condition: Good, Cr 6 ed, Replace, Other:
Well Location: Grass, A4p It, Concrete,
Woods, Other;
Additional Comments:
Total Depth of Well (T.D.):
Screen Length:
5, 101 15,
20
feet -other:
Depth to Water D.T.W : t11
Well Diameter:
; 41 6, 8
Inches -other:
Field Parameters measured with: 11, oj�
Casing Type:
Pam, Steel
other:
Purge Rate: ry(1 mumin
Sampling Device:
Pe6taltic,
Monsoon,
Grundfos, Bailer, Other:
Tubing Type: Polyethylene, Teflon, Other:
Measuring Point:
YDC
other:
Pump Intake (ft below M.P.):
Color: y
Odor:
Yes, ,
Time:
min
Volume
Purged
DTW:
feet
Temp
CC)
pH
std units
SPC
uS/cm
DO
mg/L
ORP
mV
Turb
NTU
Comments:
Stabalization
Criteria`
/
�(gyuoAs)
(see note
below)'
+/-
3%
+/-
0.1 unit
+/-
3%
+/-
10%
+/-
10 mV
+/-
10%4
6t,
/to
A,
.G,
(60'
r174
fu
J.0
f3•
��lv
G.�f`�
1611
or
-1 b V,y
It
o
Official Sampling Date &Time:
Samples Collected: Analysis Requested: Preservative:
3 - VOAs VOC by 8260 HCL
SVOC by 625
EPH
PH V
Notes:
(1) - Do not measure depth to bottom Orwell until after purging and sampling to reduce resuspending fines that may be resting on the well bottom.
(2)-Stabilizatlon criteria based on three most recent consecutive measurements.
(3) -Total drawdown in yell to be less than 0.1 m (0,32 ft). Purging rate to be lowered as necessary to keep drawdmvn below 0.1 m (0.32 ft).
(4) +/-10% when turbidity is over 10 NTUs.
Hold
Time (days): Lab:
14 Shealy
Shealy
Shealy
Shealy

Appendix B
Laboratory Analytical Report

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
ERM NC, Inc.
Ballantyne One
15720 Brixham Hill Avenue, Suite 120
Charlotte, NC 28277
Attention: Michael Pressley
Project Name: Ryerson
Lot Number:RL31002
Date Completed:01/09/2017
Kelly M. Nance
Project Manager
LABORATORY
* ACCREDITATION
BUREAU ..,­
ACCREUIT.EDk mcims
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
ERM NC, Inc.
Lot Number: RL31002
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
GC/MS Semivolatiles
Samples -001, -002 and -004 were diluted 20x, 5x and 5x, respectively, due to matrix interference. The reporting limits have been raised
accordingly.
Samples -001 and -003 had the surrogate recovered outside of the acceptance limits due to objective evidence of matrix interference.
MA EPH
Sample -001 was diluted 5x due to high concentrations of target compounds. As a result, the associated surrogates were recovered outside of the
acceptance limits. No corrective action was required, as dilutions of 5x and
greater may impact surrogate recoveries.
MA VPH
Samples -001 and -002 had the surrogate recovered outside of the acceptance limits due to objective evidence of matrix interference.
Shealy Environmental Services, Inc. Page: 2 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
ERM NC, Inc.
Lot Number: RL31002
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
MW-1
Aqueous
12/29/20161545
12/30/2016
002
MW-2
Aqueous
12/29/20161440
12/30/2016
003
MW-3
Aqueous
12/29/20161035
12/30/2016
004
MW-4
Aqueous
12/29/20161130
12/30/2016
005
DW-1
Aqueous
12/29/20161225
12/30/2016
(5 samples)
Shealy Environmental Services, Inc. Page: 3 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
ERM NC, Inc.
Lot Number: RL31002
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
MW-1
Aqueous
Benzene
8260B
70
ug/L
5
001
MW-1
Aqueous
Ethylbenzene
8260B
48
ug/L
5
001
MW-1
Aqueous
Toluene
8260B
2.3
ug/L
5
001
MW-1
Aqueous
Xylenes (total)
8260B
14
ug/L
5
001
MW-1
Aqueous
Naphthalene
625
200
ug/L
7
001
MW-1
Aqueous
Phenanthrene
625
61
ug/L
7
001
MW-1
Aqueous
C9 - C18 Aliphatics
MADEP-EPH-
2800
ug/L
8
001
MW-1
Aqueous
C11 - C22 Aromatics
MADEP-EPH-
2200
ug/L
9
001
MW-1
Aqueous
C9 - C12 Aliphatics
MADEP-VPH-
4000
ug/L
10
001
MW-1
Aqueous
C9 - C10 Aromatics
MADEP-VPH-
1900
ug/L
11
002
MW-2
Aqueous
Benzene
8260B
60
ug/L
12
002
MW-2
Aqueous
Ethylbenzene
8260B
10
ug/L
12
002
MW-2
Aqueous
Xylenes (total)
8260B
3.7
ug/L
12
002
MW-2
Aqueous
Naphthalene
625
54
ug/L
14
002
MW-2
Aqueous
Phenanthrene
625
10
ug/L
14
002
MW-2
Aqueous
C11 - C22 Aromatics
MADEP-EPH-
540
ug/L
16
002
MW-2
Aqueous
C5 - C8 Aliphatics
MADEP-VPH-
86
ug/L
17
002
MW-2
Aqueous
C9 - C12 Aliphatics
MADEP-VPH-
260
ug/L
17
002
MW-2
Aqueous
C9 - C10 Aromatics
MADEP-VPH-
220
ug/L
18
003
MW-3
Aqueous
Benzene
8260B
9.7
ug/L
19
003
MW-3
Aqueous
Xylenes (total)
8260B
3.8
ug/L
19
003
MW-3
Aqueous
Naphthalene
625
7.5
ug/L
21
(22 detections)
Shealy Environmental Services, Inc. Page: 4 of 76
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Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-001
Description: MW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1545
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/03/20171713 JM1 30692
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
70
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
48
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
2.3
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
14
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 94 70-130
Bromofluorobenzene 110 70-130
Toluene-d8 100 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-001
Description: MW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1545
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 20 01/09/2017 1602 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9
625
ND
32
ug/L
1
Acenaphthylene
208-96-8
625
ND
32
ug/L
1
Anthracene
120-12-7
625
ND
32
ug/L
1
Benzidine
92-87-5
625
ND
160
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
32
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
32
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
32
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
32
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
32
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
32
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
32
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
32
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
32
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
32
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
32
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
32
ug/L
1
2-Chlorophenol
95-57-8
625
ND
32
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
32
ug/L
1
Chrysene
218-01-9
625
ND
32
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
32
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
32
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
32
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
32
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
160
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
32
ug/L
1
Diethylphthalate
84-66-2
625
ND
32
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
32
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
32
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
32
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
160
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
160
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
64
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
64
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
32
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
32
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
32
ug/L
1
Fluoranthene
206-44-0
625
ND
32
ug/L
1
Fluorene
86-73-7
625
ND
32
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
32
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
32
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
160
ug/L
1
Hexachloroethane
67-72-1
625
ND
32
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
32
ug/L
1
Isophorone
78-59-1
625
ND
32
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-001
Description: MW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1545
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 20 01/09/2017 1602 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Naphthalene
91-20-3
625
200
32
ug/L
1
Nitrobenzene
98-95-3
625
ND
32
ug/L
1
2-Nitrophenol
88-75-5
625
ND
64
ug/L
1
4-Nitrophenol
100-02-7
625
ND
160
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
32
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
32
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
32
ug/L
1
Pentachlorophenol
87-86-5
625
ND
160
ug/L
1
Phenanthrene
85-01-8
625
61
32
ug/L
1
Phenol
108-95-2
625
ND
32
ug/L
1
Pyrene
129-00-0
625
ND
32
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
32
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
32
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
70
37-129
2-Fluorophenol
41
24-127
Nitrobenzene-d5
63
38-127
Phenol-d5
67
28-128
Terphenyl-d14
68
10-148
2,4,6-Tribromophenol
N 173
41-144
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-001
Description: MW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1545
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 5 01/06/2017 1945 MEM 01/04/2017 1444 30959
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C18 Aliphatics MADEP-EPH-0 2800 500 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-0 ND 500 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) N 12 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-001
Description: MW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1545
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 5 01/06/2017 2114 MEM 01/04/2017 1444 30962
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C11 - C22 Aromatics MADEP-EPH-0 2200 500 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) N 4.4 40-140
2-Fluorobiphenyl (fractionation 1) 78 40-140
2-Bromonaphthalene (fractionation 2) 68 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-001
Description: MW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1545
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 VPH MADEP-VPH-04-1.1 20 01/04/20171743 JM1 30861
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 1500 ug/L 2
C9 - C12 Aliphatics MADEP-VPH- 4000 1500 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
N 152 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-001
Description: MW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1545
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 VPH MADEP-VPH-04-1.1 20 01/04/20171743 JM1 30862
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH- 1900 500 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
125 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-002
Description: MW-2 Matrix: Aqueous
Date Sampled:12/29/2016 1440
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/03/20171737 JM1 30692
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
60
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
10
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
3.7
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 76 70-130
Bromofluorobenzene 109 70-130
Toluene-d8 98 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-002
Description: MW-2 Matrix: Aqueous
Date Sampled:12/29/2016 1440
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 5 01/09/2017 1626 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9
625
ND
8.0
ug/L
1
Acenaphthylene
208-96-8
625
ND
8.0
ug/L
1
Anthracene
120-12-7
625
ND
8.0
ug/L
1
Benzidine
92-87-5
625
ND
40
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
8.0
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
8.0
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
8.0
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
8.0
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
8.0
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
8.0
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
8.0
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
8.0
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
8.0
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
8.0
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
8.0
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
8.0
ug/L
1
2-Chlorophenol
95-57-8
625
ND
8.0
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
8.0
ug/L
1
Chrysene
218-01-9
625
ND
8.0
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
8.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
8.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
8.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
8.0
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
40
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
8.0
ug/L
1
Diethylphthalate
84-66-2
625
ND
8.0
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
8.0
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
8.0
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
8.0
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
40
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
40
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
16
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
16
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
8.0
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
8.0
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
8.0
ug/L
1
Fluoranthene
206-44-0
625
ND
8.0
ug/L
1
Fluorene
86-73-7
625
ND
8.0
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
8.0
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
8.0
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
40
ug/L
1
Hexachloroethane
67-72-1
625
ND
8.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
8.0
ug/L
1
Isophorone
78-59-1
625
ND
8.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-002
Description: MW-2 Matrix: Aqueous
Date Sampled:12/29/2016 1440
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 5 01/09/2017 1626 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Naphthalene
91-20-3
625
54
8.0
ug/L
1
Nitrobenzene
98-95-3
625
ND
8.0
ug/L
1
2-Nitrophenol
88-75-5
625
ND
16
ug/L
1
4-Nitrophenol
100-02-7
625
ND
40
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
8.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
8.0
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
8.0
ug/L
1
Pentachlorophenol
87-86-5
625
ND
40
ug/L
1
Phenanthrene
85-01-8
625
10
8.0
ug/L
1
Phenol
108-95-2
625
ND
8.0
ug/L
1
Pyrene
129-00-0
625
ND
8.0
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
8.0
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
8.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
77
37-129
2-Fluorophenol
29
24-127
Nitrobenzene-d5
65
38-127
Phenol-d5
32
28-128
Terphenyl-d14
81
10-148
2,4,6-Tribromophenol
96
41-144
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-002
Description: MW-2 Matrix: Aqueous
Date Sampled:12/29/2016 1440
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 01/06/2017 2014 MEM 01/04/2017 1444 30959
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C18 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
41 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-002
Description: MW-2 Matrix: Aqueous
Date Sampled:12/29/2016 1440
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 01/06/2017 2143 MEM 01/04/2017 1444 30962
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C11 - C22 Aromatics MADEP-EPH-0 540 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) 58 40-140
2-Fluorobiphenyl (fractionation 1) 61 40-140
2-Bromonaphthalene (fractionation 2) 47 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-002
Description: MW-2 Matrix: Aqueous
Date Sampled:12/29/2016 1440
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171852 JM1 30715
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH- 86 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- 260 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
N 131 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-002
Description: MW-2 Matrix: Aqueous
Date Sampled:12/29/2016 1440
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171852 JM1 30716
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH- 220 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
N 144 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-003
Description: MW-3 Matrix: Aqueous
Date Sampled:12/29/2016 1035
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/03/20171539 JM1 30692
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
9.7
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
3.8
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 110 70-130
Bromofluorobenzene 100 70-130
Toluene-d8 98 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 19 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-003
Description: MW-3 Matrix: Aqueous
Date Sampled:12/29/2016 1035
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 01/09/2017 1426 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9
625
ND
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
1.6
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
ug/L
1
Fluorene
86-73-7
625
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
ug/L
1
Isophorone
78-59-1
625
ND
1.6
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-003
Description: MW-3 Matrix: Aqueous
Date Sampled:12/29/2016 1035
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 01/09/2017 1426 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Naphthalene
91-20-3
625
7.5
1.6
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
ND
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
72
37-129
2-Fluorophenol
N 13
24-127
Nitrobenzene-d5
41
38-127
Phenol-d5
N 15
28-128
Terphenyl-d14
68
10-148
2,4,6-Tribromophenol
72
41-144
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 21 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-003
Description: MW-3 Matrix: Aqueous
Date Sampled:12/29/2016 1035
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 01/06/2017 2044 MEM 01/04/2017 1444 30959
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C18 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-0 ND 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
47 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 22 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-003
Description: MW-3 Matrix: Aqueous
Date Sampled:12/29/2016 1035
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 01/06/2017 2213 MEM 01/04/2017 1444 30962
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C11 - C22 Aromatics MADEP-EPH-0 ND 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) 65 40-140
2-Fluorobiphenyl (fractionation 1) 77 40-140
2-Bromonaphthalene (fractionation 2) 42 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 23 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-003
Description: MW-3 Matrix: Aqueous
Date Sampled:12/29/2016 1035
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171921 JM1 30715
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
130 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 24 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-003
Description: MW-3 Matrix: Aqueous
Date Sampled:12/29/2016 1035
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171921 JM1 30716
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
117 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 25 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-004
Description: MW-4 Matrix: Aqueous
Date Sampled:12/29/2016 1130
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/03/20171603 JM1 30692
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
ND
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 113 70-130
Bromofluorobenzene 101 70-130
Toluene-d8 100 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 26 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-004
Description: MW-4 Matrix: Aqueous
Date Sampled:12/29/2016 1130
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 5 01/09/2017 1650 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9
625
ND
8.0
ug/L
1
Acenaphthylene
208-96-8
625
ND
8.0
ug/L
1
Anthracene
120-12-7
625
ND
8.0
ug/L
1
Benzidine
92-87-5
625
ND
40
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
8.0
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
8.0
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
8.0
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
8.0
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
8.0
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
8.0
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
8.0
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
8.0
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
8.0
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
8.0
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
8.0
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
8.0
ug/L
1
2-Chlorophenol
95-57-8
625
ND
8.0
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
8.0
ug/L
1
Chrysene
218-01-9
625
ND
8.0
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
8.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
8.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
8.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
8.0
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
40
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
8.0
ug/L
1
Diethylphthalate
84-66-2
625
ND
8.0
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
8.0
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
8.0
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
8.0
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
40
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
40
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
16
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
16
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
8.0
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
8.0
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
8.0
ug/L
1
Fluoranthene
206-44-0
625
ND
8.0
ug/L
1
Fluorene
86-73-7
625
ND
8.0
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
8.0
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
8.0
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
40
ug/L
1
Hexachloroethane
67-72-1
625
ND
8.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
8.0
ug/L
1
Isophorone
78-59-1
625
ND
8.0
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 27 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-004
Description: MW-4 Matrix: Aqueous
Date Sampled:12/29/2016 1130
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 5 01/09/2017 1650 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Naphthalene
91-20-3
625
ND
8.0
ug/L
1
Nitrobenzene
98-95-3
625
ND
8.0
ug/L
1
2-Nitrophenol
88-75-5
625
ND
16
ug/L
1
4-Nitrophenol
100-02-7
625
ND
40
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
8.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
8.0
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
8.0
ug/L
1
Pentachlorophenol
87-86-5
625
ND
40
ug/L
1
Phenanthrene
85-01-8
625
ND
8.0
ug/L
1
Phenol
108-95-2
625
ND
8.0
ug/L
1
Pyrene
129-00-0
625
ND
8.0
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
8.0
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
8.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
86
37-129
2-Fluorophenol
24
24-127
Nitrobenzene-d5
68
38-127
Phenol-d5
45
28-128
Terphenyl-d14
89
10-148
2,4,6-Tribromophenol
74
41-144
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 28 of 76
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MADEP EPH (aliphatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: RL31002-004
Description: MW-4 Matrix: Aqueous
Date Sampled:12/29/2016 1130
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 1 01/09/2017 1111 MEM 01/06/2017 1154 30982
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C19 - C36 Aliphatics - Unfractionated MADEP-EPH-0 ND 140 ug/L 2
C9 - C18 Aliphatics - Unfractionated MADEP-EPH-0 ND 140 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) - Unfractionated 47 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 29 of 76
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MADEP EPH (aromatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: RL31002-004
Description: MW-4 Matrix: Aqueous
Date Sampled:12/29/2016 1130
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 1 01/09/2017 1111 MEM 01/06/2017 1154 30983
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C11 - C22 Aromatics - Unfractionated MADEP-EPH-0 ND 140 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) - Unfractionated 62 40-140
2-Fluorobiphenyl (fractionation 1) 73 40-140
2-Bromonaphthalene (fractionation 2) 70 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 30 of 76
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MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-004
Description: MW-4 Matrix: Aqueous
Date Sampled:12/29/2016 1130
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171949 JM1 30715
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
118 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 31 of 76
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MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-004
Description: MW-4 Matrix: Aqueous
Date Sampled:12/29/2016 1130
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171949 JM1 30716
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
112 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 32 of 76
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Volatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-005
Description: DW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1225
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 01/03/20171627 JM1 30692
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
ND
1.0
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
1.0
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1.0
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260B
ND
1.0
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260B
ND
1.0
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260B
ND
1.0
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
1.0
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
1.0
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1.0
ug/L
1
Toluene
108-88-3
8260B
ND
1.0
ug/L
1
Xylenes (total)
1330-20-7
8260B
ND
1.0
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 112 70-130
Bromofluorobenzene 100 70-130
Toluene-d8 91 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 33 of 76
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Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-005
Description: DW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1225
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 01/09/2017 1514 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Acenaphthene
83-32-9
625
ND
1.6
ug/L
1
Acenaphthylene
208-96-8
625
ND
1.6
ug/L
1
Anthracene
120-12-7
625
ND
1.6
ug/L
1
Benzidine
92-87-5
625
ND
8.0
ug/L
1
Benzo(a)anthracene
56-55-3
625
ND
1.6
ug/L
1
Benzo(a)pyrene
50-32-8
625
ND
1.6
ug/L
1
Benzo(b)fluoranthene
205-99-2
625
ND
1.6
ug/L
1
Benzo(g,h,i)perylene
191-24-2
625
ND
1.6
ug/L
1
Benzo(k)fluoranthene
207-08-9
625
ND
1.6
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
625
ND
1.6
ug/L
1
Butyl benzyl phthalate
85-68-7
625
ND
1.6
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
625
ND
1.6
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
625
ND
1.6
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
625
ND
1.6
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
625
ND
1.6
ug/L
1
2-Chloronaphthalene
91-58-7
625
ND
1.6
ug/L
1
2-Chlorophenol
95-57-8
625
ND
1.6
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
625
ND
1.6
ug/L
1
Chrysene
218-01-9
625
ND
1.6
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
625
ND
1.6
ug/L
1
1,2-Dichlorobenzene
95-50-1
625
ND
1.6
ug/L
1
1,3-Dichlorobenzene
541-73-1
625
ND
1.6
ug/L
1
1,4-Dichlorobenzene
106-46-7
625
ND
1.6
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
625
ND
8.0
ug/L
1
2,4-Dichlorophenol
120-83-2
625
ND
1.6
ug/L
1
Diethylphthalate
84-66-2
625
ND
1.6
ug/L
1
Dimethyl phthalate
131-11-3
625
ND
1.6
ug/L
1
2,4-Dimethylphenol
105-67-9
625
ND
1.6
ug/L
1
Di-n-butyl phthalate
84-74-2
625
ND
1.6
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
625
ND
8.0
ug/L
1
2,4-Dinitrophenol
51-28-5
625
ND
8.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
625
ND
3.2
ug/L
1
2,6-Dinitrotoluene
606-20-2
625
ND
3.2
ug/L
1
Di-n-octylphthalate
117-84-0
625
ND
1.6
ug/L
1
1,2-Diphenylhydrazine(as azobenzene)
103-33-3
625
ND
1.6
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
625
ND
1.6
ug/L
1
Fluoranthene
206-44-0
625
ND
1.6
ug/L
1
Fluorene
86-73-7
625
ND
1.6
ug/L
1
Hexachlorobenzene
118-74-1
625
ND
1.6
ug/L
1
Hexachlorobutadiene
87-68-3
625
ND
1.6
ug/L
1
Hexachlorocyclopentadiene
77-47-4
625
ND
8.0
ug/L
1
Hexachloroethane
67-72-1
625
ND
1.6
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
625
ND
1.6
ug/L
1
Isophorone
78-59-1
625
ND
1.6
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Semivolatile Organic Compounds by GC/MS
Client: ERM NC, Inc. Laboratory ID: RL31002-005
Description: DW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1225
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625 625 1 01/09/2017 1514 RBH 01/04/2017 1457 30767
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Naphthalene
91-20-3
625
ND
1.6
ug/L
1
Nitrobenzene
98-95-3
625
ND
1.6
ug/L
1
2-Nitrophenol
88-75-5
625
ND
3.2
ug/L
1
4-Nitrophenol
100-02-7
625
ND
8.0
ug/L
1
N-Nitrosodimethylamine
62-75-9
625
ND
1.6
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
625
ND
1.6
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
625
ND
1.6
ug/L
1
Pentachlorophenol
87-86-5
625
ND
8.0
ug/L
1
Phenanthrene
85-01-8
625
ND
1.6
ug/L
1
Phenol
108-95-2
625
ND
1.6
ug/L
1
Pyrene
129-00-0
625
ND
1.6
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
625
ND
1.6
ug/L
1
2,4,6-Trichlorophenol
88-06-2
625
ND
1.6
ug/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2-Fluorobiphenyl
68
37-129
2-Fluorophenol
55
24-127
Nitrobenzene-d5
61
38-127
Phenol-d5
60
28-128
Terphenyl-d14
77
10-148
2,4,6-Tribromophenol
58
41-144
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 35 of 76
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MADEP EPH (aliphatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: RL31002-005
Description: DW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1225
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 01/05/2017 1943 MEM 01/04/2017 1444 30789
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C19 - C36 Aliphatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
C9 - C18 Aliphatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) - Unfractionated 41 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 36 of 76
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MADEP EPH (aromatics) - Unfractionated
Client: ERM NC, Inc. Laboratory ID: RL31002-005
Description: DW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1225
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 01/05/2017 1943 MEM 01/04/2017 1444 30790
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C11 - C22 Aromatics - Unfractionated MADEP-EPH-0 ND 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) - Unfractionated 57 40-140
2-Fluorobiphenyl (fractionation 1) 75 40-140
2-Bromonaphthalene (fractionation 2) 73 40-140
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 37 of 76
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MADEP VPH (aliphatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-005
Description: DW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1225
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171824 JM1 30715
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
C9 - C12 Aliphatics MADEP-VPH-0 ND 75 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
122 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 38 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aromatics)
Client: ERM NC, Inc. Laboratory ID: RL31002-005
Description: DW-1 Matrix: Aqueous
Date Sampled:12/29/2016 1225
Date Received:12/30/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/03/20171824 JM1 30716
CAS Analytical
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 25 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
116 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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QC Summary
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Volatile Organic Compounds by GC/MS - MB
Sample ID: SQ30692-001 Matrix: Aqueous
Batch:30692 Prep Method: 5030E
Analytical Method: 8260B
Parameter
Result
Q Dil
PQL
Units
Analysis Date
Benzene
ND
1
1.0
ug/L
01/03/2017 1020
Chlorobenzene
ND
1
1.0
ug/L
01/03/2017 1020
1,2-Dibromoethane (EDB)
ND
1
1.0
ug/L
01/03/2017 1020
1,4-Dichlorobenzene
ND
1
1.0
ug/L
01/03/2017 1020
1,2-Dichlorobenzene
ND
1
1.0
ug/L
01/03/2017 1020
1,3-Dichlorobenzene
ND
1
1.0
ug/L
01/03/2017 1020
Diisopropyl ether (IPE)
ND
1
1.0
ug/L
01/03/2017 1020
Ethylbenzene
ND
1
1.0
ug/L
01/03/2017 1020
Methyl tertiary butyl ether (MTBE)
ND
1
1.0
ug/L
01/03/2017 1020
Toluene
ND
1
1.0
ug/L
01/03/2017 1020
Xylenes (total)
ND
1
1.0
ug/L
01/03/2017 1020
Acceptance
Surrogate
0
Q /o Rec
Limit
Bromofluorobenzene 96 70-130
1,2-Dichloroethane-d4 94 70-130
Toluene-d8 96 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Volatile Organic Compounds by GC/MS - LCS
Sample ID: SQ30692-002
Matrix: Aqueous
Batch:30692
Prep Method:
5030E
Analytical Method: 8260B
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Benzene
50
49
1
97
70-130
01/03/2017 0920
Chlorobenzene
50
53
1
106
70-130
01/03/2017 0920
1,2-Dibromoethane (EDB)
50
51
1
102
70-130
01/03/2017 0920
1,4-Dichlorobenzene
50
50
1
101
70-130
01/03/2017 0920
1,2-Dichlorobenzene
50
51
1
103
70-130
01/03/2017 0920
1,3-Dichlorobenzene
50
52
1
104
70-130
01/03/2017 0920
Diisopropyl ether (IPE)
50
48
1
95
70-130
01/03/2017 0920
Ethylbenzene
50
53
1
105
70-130
01/03/2017 0920
Methyl tertiary butyl ether (MTBE)
50
44
1
88
70-130
01/03/2017 0920
Toluene
50
52
1
103
70-130
01/03/2017 0920
Xylenes(total)
100
110
1
108
70-130
01/03/2017 0920
Surrogate Q /o Rec Acceptance
0
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 91 70-130
Toluene-d8 96 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Semivolatile Organic Compounds by GC/MS - MB
Sample ID: SQ30767-001 Matrix: Aqueous
Batch:30767 Prep Method: 625
Analytical Method: 625 Prep Date: 01/04/2017 1457
Parameter
Result
Q Dil
PQL
Units
Analysis Date
1,2,4-Trichlorobenzene
ND
1
1.6
ug/L
01/09/2017 1002
1,2-Dichlorobenzene
ND
1
1.6
ug/L
01/09/2017 1002
1,2-Diphenylhydrazine(as azobenzene)
ND
1
1.6
ug/L
01/09/2017 1002
1,3-Dichlorobenzene
ND
1
1.6
ug/L
01/09/2017 1002
1,4-Dichlorobenzene
ND
1
1.6
ug/L
01/09/2017 1002
2,4,6-Trichlorophenol
ND
1
1.6
ug/L
01/09/2017 1002
2,4-Dichlorophenol
ND
1
1.6
ug/L
01/09/2017 1002
2,4-Dimethylphenol
ND
1
1.6
ug/L
01/09/2017 1002
2,4-Dinitrophenol
ND
1
8.0
ug/L
01/09/2017 1002
2,4-Dinitrotoluene
ND
1
3.2
ug/L
01/09/2017 1002
2,6-Dinitrotoluene
ND
1
3.2
ug/L
01/09/2017 1002
2-Chloronaphthalene
ND
1
1.6
ug/L
01/09/2017 1002
2-Chlorophenol
ND
1
1.6
ug/L
01/09/2017 1002
2-Nitrophenol
ND
1
3.2
ug/L
01/09/2017 1002
3,3'-Dichlorobenzidine
ND
1
8.0
ug/L
01/09/2017 1002
4,6-Dinitro-2-methyl phenol
ND
1
8.0
ug/L
01/09/2017 1002
4-Bromophenyl phenyl ether
ND
1
1.6
ug/L
01/09/2017 1002
4-Chloro-3-methyl phenol
ND
1
1.6
ug/L
01/09/2017 1002
4-Chlorophenyl phenyl ether
ND
1
1.6
ug/L
01/09/2017 1002
4-Nitrophenol
ND
1
8.0
ug/L
01/09/2017 1002
Acenaphthene
ND
1
1.6
ug/L
01/09/2017 1002
Acenaphthylene
ND
1
1.6
ug/L
01/09/2017 1002
Anthracene
ND
1
1.6
ug/L
01/09/2017 1002
Benzidine
ND
1
8.0
ug/L
01/09/2017 1002
Benzo(a)anth race ne
ND
1
1.6
ug/L
01/09/2017 1002
Benzo(a)pyrene
ND
1
1.6
ug/L
01/09/2017 1002
Benzo(b)fluoranthene
ND
1
1.6
ug/L
01/09/2017 1002
Benzo(g,h,i)perylene
ND
1
1.6
ug/L
01/09/2017 1002
Benzo(k)fluoranthene
ND
1
1.6
ug/L
01/09/2017 1002
bis (2-Chloro-1-methylethyl) ether
ND
1
1.6
ug/L
01/09/2017 1002
bis(2-Chloroethoxy)methane
ND
1
1.6
ug/L
01/09/2017 1002
bis(2-Chloroethyl)ether
ND
1
1.6
ug/L
01/09/2017 1002
bis(2-Ethylhexyl)phthalate
ND
1
1.6
ug/L
01/09/2017 1002
Butyl benzyl phthalate
ND
1
1.6
ug/L
01/09/2017 1002
Chrysene
ND
1
1.6
ug/L
01/09/2017 1002
Di-n-butyl phthalate
ND
1
1.6
ug/L
01/09/2017 1002
Di-n-octylphthalate
ND
1
1.6
ug/L
01/09/2017 1002
Dibenzo(a,h)anthracene
ND
1
1.6
ug/L
01/09/2017 1002
Diethylphthalate
ND
1
1.6
ug/L
01/09/2017 1002
Dimethyl phthalate
ND
1
1.6
ug/L
01/09/2017 1002
Fluoranthene
ND
1
1.6
ug/L
01/09/2017 1002
Fluorene
ND
1
1.6
ug/L
01/09/2017 1002
Hexachlorobenzene
ND
1
1.6
ug/L
01/09/2017 1002
Hexachlorobutadiene
ND
1
1.6
ug/L
01/09/2017 1002
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Semivolatile Organic Compounds by GC/MS - MB
Sample ID: SQ30767-001 Matrix: Aqueous
Batch:30767 Prep Method: 625
Analytical Method: 625 Prep Date: 01/04/2017 1457
Parameter
Result
Q Dil
PQL
Units
Analysis Date
Hexachlorocyclopentadiene
ND
1
8.0
ug/L
01/09/20171002
Hexachloroethane
ND
1
1.6
ug/L
01/09/20171002
Indeno(1,2,3-c,d)pyrene
ND
1
1.6
ug/L
01/09/20171002
Isophorone
ND
1
1.6
ug/L
01/09/20171002
N-Nitrosodi-n-propylamine
ND
1
1.6
ug/L
01/09/20171002
N-Nitrosodimethylamine
ND
1
1.6
ug/L
01/09/20171002
N-Nitrosodiphenylamine (Diphenylamine) ND
1
1.6
ug/L
01/09/2017 1002
Naphthalene
ND
1
1.6
ug/L
01/09/20171002
Nitrobenzene
ND
1
1.6
ug/L
01/09/20171002
Pentachlorophenol
ND
1
8.0
ug/L
01/09/20171002
Phenanthrene
ND
1
1.6
ug/L
01/09/20171002
Phenol
ND
1
1.6
ug/L
01/09/20171002
Pyrene
ND
1
1.6
ug/L
01/09/20171002
Acceptance
Surrogate
0
Q /o Rec
Limit
2,4,6-Tribromophenol
76
41-144
2-Fluorobiphenyl
83
37-129
2-Fluorophenol
42
24-127
Nitrobenzene-d5
69
38-127
Phenol-d5
48
28-128
Terphenyl-d 14
97
10-148
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: SQ30767-002
Matrix: Aqueous
Batch:30767
Prep Method:
625
Analytical Method: 625
Prep Date: 01/04/2017 1457
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
1,2,4-Trichlorobenzene
20
9.7
1
48
44-142
01/09/2017 1026
1,2-Dichlorobenzene
20
9.3
1
47
32-129
01/09/2017 1026
1,2-Diphenylhydrazine(as azobenzene)
20
15
1
76
30-130
01/09/2017 1026
1,3-Dichlorobenzene
20
8.5
1
43
0-172
01/09/2017 1026
1,4-Dichlorobenzene
20
8.4
1
42
20-124
01/09/2017 1026
2,4,6-Trichlorophenol
20
16
1
78
37-144
01/09/2017 1026
2,4-Dichlorophenol
20
13
1
63
39-135
01/09/2017 1026
2,4-Dimethylphenol
20
8.1
1
41
32-119
01/09/2017 1026
2,4-Dinitrophenol
40
22
1
56
0-191
01/09/2017 1026
2,4-Dinitrotoluene
20
21
1
107
39-139
01/09/2017 1026
2,6-Dinitrotoluene
20
18
1
91
50-158
01/09/2017 1026
2-Chloronaphthalene
20
14
1
70
60-118
01/09/2017 1026
2-Chlorophenol
20
12
1
62
23-134
01/09/2017 1026
2-Nitrophenol
20
12
1
61
29-182
01/09/2017 1026
3,3'-Dichlorobenzidine
20
12
1
59
0-262
01/09/2017 1026
4,6-Dinitro-2-methyl phenol
20
14
1
68
0-181
01/09/2017 1026
4-Bromophenyl phenyl ether
20
17
1
85
53-127
01/09/2017 1026
4-Chloro-3-methyl phenol
20
18
1
88
22-147
01/09/2017 1026
4-Chlorophenyl phenyl ether
20
16
1
80
25-158
01/09/2017 1026
4-Nitrophenol
40
34
1
84
0-132
01/09/2017 1026
Acenaphthene
20
15
1
76
47-145
01/09/2017 1026
Acenaphthylene
20
16
1
82
33-145
01/09/2017 1026
Anthracene
20
18
1
89
27-133
01/09/2017 1026
Benzidine
100
24
1
24
1-150
01/09/2017 1026
Benzo(a)anth race ne
20
17
1
84
33-143
01/09/2017 1026
Benzo(a)pyrene
20
16
1
78
17-163
01/09/2017 1026
Benzo(b)fluoranthene
20
17
1
83
24-159
01/09/2017 1026
Benzo(g,h,i)perylene
20
14
1
71
0-219
01/09/2017 1026
Benzo(k)fluoranthene
20
16
1
80
11-162
01/09/2017 1026
bis (2-Chloro-1-methylethyl) ether
20
13
1
64
36-166
01/09/2017 1026
bis(2-Chloroethoxy)methane
20
12
1
62
33-184
01/09/2017 1026
bis(2-Chloroethyl)ether
20
14
1
72
12-158
01/09/2017 1026
bis(2-Ethylhexyl)phthalate
20
17
1
86
8-158
01/09/2017 1026
Butyl benzyl phthalate
20
21
1
104
0-152
01/09/2017 1026
Chrysene
20
18
1
90
17-168
01/09/2017 1026
Di-n-butyl phthalate
20
20
1
100
1-118
01/09/2017 1026
Di-n-octylphthalate
20
15
1
77
4-146
01/09/2017 1026
Dibenzo(a,h)anthracene
20
12
1
60
0-227
01/09/2017 1026
Diethylphthalate
20
20
1
99
0-114
01/09/2017 1026
Dimethyl phthalate
20
19
1
93
0-112
01/09/2017 1026
Fluoranthene
20
14
1
72
26-137
01/09/2017 1026
Fluorene
20
17
1
83
59-121
01/09/2017 1026
Hexachlorobenzene
20
18
1
91
0-152
01/09/2017 1026
Hexachlorobutadiene
20
10
1
52
24-116
01/09/2017 1026
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: SQ30767-002
Matrix: Aqueous
Batch:30767
Prep Method:
625
Analytical Method: 625
Prep Date: 01/04/2017 1457
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Hexachlorocyclopentadiene
100
22
1
22
1-150
01/09/20171026
Hexachloroethane
20
9.3
1
46
40-113
01/09/20171026
Indeno(1,2,3-c,d)pyrene
20
12
1
60
0-171
01/09/20171026
Isophorone
20
13
1
65
21-196
01/09/20171026
N-Nitrosodi-n-propylamine
20
18
1
91
0-230
01/09/20171026
N-Nitrosodimethylamine
20
16
1
78
1-150
01/09/20171026
N-Nitrosodiphenylamine (Diphenylamine) 20
17
1
87
1-150
01/09/2017 1026
Naphthalene
20
12
1
59
21-133
01/09/20171026
Nitrobenzene
20
11
1
56
35-180
01/09/20171026
Pentachlorophenol
40
26
1
66
14-176
01/09/20171026
Phenanthrene
20
17
1
86
54-120
01/09/20171026
Phenol
20
11
1
54
5-112
01/09/20171026
Pyrene
20
15
1
73
52-115
01/09/20171026
Acceptance
Surrogate
0
Q /o Rec
Limit
2,4,6-Tribromophenol
97
41-144
2-Fluorobiphenyl
76
37-129
2-Fluorophenol
33
24-127
Nitrobenzene-d5
58
38-127
Phenol-d5
58
28-128
Terphenyl-d 14
72
10-148
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aliphatics) - Unfractionated - MB
Sample ID: SQ30789-001 Matrix: Aqueous
Batch:30789 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/04/2017 1444
Parameter Result Q Dil PQL Units Analysis Date
C19 - C36 Aliphatics - Unfractionated ND 1 100 ug/L 01/05/2017 1613
C9 - C18 Aliphatics - Unfractionated ND 1 100 ug/L 01/05/2017 1613
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 61 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aliphatics) - Unfractionated - LCS
Sample ID: SQ30789-002
Matrix: Aqueous
Batch:30789
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/04/2017 1444
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
730
1 81
40-140 01/05/2017 1643
C9 - C18 Aliphatics - Unfractionated
650
400
1 62
40-140 01/05/2017 1643
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 68 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aliphatics) - Unfractionated - LCSD
Sample ID: SQ30789-003
Matrix: Aqueous
Batch:30789
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/04/2017 1444
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
730
1 82 0.43 40-140
25 01/05/2017 1713
C9 - C18 Aliphatics - Unfractionated
650
400
1 62 0.14 40-140
25 01/05/2017 1713
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 65 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aromatics) - Unfractionated - MB
Sample ID: SQ30790-001 Matrix: Aqueous
Batch:30790 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/04/2017 1444
Parameter Result Q Dil PQL Units Analysis Date
C11 - C22 Aromatics - Unfractionated ND 1 100 ug/L 01/05/2017 1613
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2)
74
40-140
2-Fluorobiphenyl (fractionation 1)
73
40-140
o - Terphenyl (aromatic) - Unfractionated
63
40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aromatics) - Unfractionated - LCS
Sample ID: SQ30790-002
Matrix: Aqueous
Batch:30790
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/04/2017 1444
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics - Unfractionated
1400
880
1 63 40-140 01/05/2017 1643
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)
70
40-140
2-Fluorobiphenyl (fractionation 1)
81
40-140
o - Terphenyl (aromatic) - Unfractionated
63
40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aromatics) - Unfractionated - LCSD
Sample ID: SQ30790-003 Matrix: Aqueous
Batch:30790 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/04/2017 1444
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics - Unfractionated 1400 890 1 63 0.69 40-140 25 01/05/2017 1713
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2)
68
40-140
2-Fluorobiphenyl (fractionation 1)
77
40-140
o - Terphenyl (aromatic) - Unfractionated
62
40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aliphatics) - MB
Sample ID: SQ30959-001 Matrix: Aqueous
Batch:30959 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/04/2017 1444
Parameter Result Q Dil PQL Units Analysis Date
C19 - C36 Aliphatics ND 1 100 ug/L 01/06/2017 1646
C9 - C18 Aliphatics ND 1 100 ug/L 01/06/2017 1646
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 50 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 53 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aliphatics) - LCS
Sample ID: SQ30959-002
Matrix: Aqueous
Batch:30959
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/04/2017 1444
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit Analysis Date
C19 - C36 Aliphatics
400
280
1 69
40-140 01/06/2017 1716
C9 - C18 Aliphatics
300
130
1 43
40-140 01/06/2017 1716
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 60 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 54 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aliphatics) - LCSD
Sample ID: SQ30959-003
Matrix: Aqueous
Batch:30959
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/04/2017 1444
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C19 - C36 Aliphatics
400
280
1 69 0.24 40-140
25 01/06/2017 1746
C9 - C18 Aliphatics
300
130
1 43 0.76 40-140
25 01/06/2017 1746
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 58 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aromatics) - MB
Sample ID: SQ30962-001 Matrix: Aqueous
Batch:30962 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/04/2017 1444
Parameter Result Q Dil PQL Units Analysis Date
C11 - C22 Aromatics ND 1 100 ug/L 01/06/2017 1816
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 67 40-140
2-Fluorobiphenyl (fractionation 1) 71 40-140
o - Terphenyl (aromatic) 65 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 56 of 76
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MADEP EPH (aromatics) - LCS
Sample ID: SQ30962-002
Matrix: Aqueous
Batch:30962
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/04/2017 1444
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
850
660
1 78 40-140 01/06/2017 1845
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2) 65 40-140
2-Fluorobiphenyl (fractionation 1) 84 40-140
o - Terphenyl (aromatic) 71 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aromatics) - LCSD
Sample ID: SQ30962-003 Matrix: Aqueous
Batch:30962 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/04/2017 1444
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 850 600 1 70 9.6 40-140 25 01/06/2017 1915
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 61 40-140
2-Fluorobiphenyl (fractionation 1) 73 40-140
o - Terphenyl (aromatic) 64 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aliphatics) - Unfractionated - MB
Sample ID: SQ30982-001 Matrix: Aqueous
Batch:30982 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/06/2017 1154
Parameter Result Q Dil PQL Units Analysis Date
C19 - C36 Aliphatics - Unfractionated ND 1 100 ug/L 01/09/2017 0942
C9 - C18 Aliphatics - Unfractionated ND 1 100 ug/L 01/09/2017 0942
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 58 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aliphatics) - Unfractionated - LCS
Sample ID: SQ30982-002
Matrix: Aqueous
Batch:30982
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/06/2017 1154
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil % Rec
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
680
1 76
40-140 01/09/2017 1011
C9 - C18 Aliphatics - Unfractionated
650
390
1 60
40-140 01/09/2017 1011
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 66 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aliphatics) - Unfractionated - LCSD
Sample ID: SQ30982-003
Matrix: Aqueous
Batch:30982
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/06/2017 1154
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C19 - C36 Aliphatics - Unfractionated
900
700
1 77 2.3 40-140
25 01/09/2017 1041
C9 - C18 Aliphatics - Unfractionated
650
390
1 60 0.19 40-140
25 01/09/2017 1041
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 66 40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP EPH (aromatics) - Unfractionated - MB
Sample ID: SQ30983-001 Matrix: Aqueous
Batch:30983 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/06/2017 1154
Parameter Result Q Dil PQL Units Analysis Date
C11 - C22 Aromatics - Unfractionated ND 1 100 ug/L 01/09/2017 0942
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2)
70
40-140
2-Fluorobiphenyl (fractionation 1)
68
40-140
o - Terphenyl (aromatic) - Unfractionated
59
40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 62 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics) - Unfractionated - LCS
Sample ID: SQ30983-002
Matrix: Aqueous
Batch:30983
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/06/2017 1154
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics - Unfractionated
1400
840
1 60 40-140 01/09/2017 1011
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2)
69
40-140
2-Fluorobiphenyl (fractionation 1)
81
40-140
o - Terphenyl (aromatic) - Unfractionated
61
40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 63 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics) - Unfractionated - LCSD
Sample ID: SQ30983-003 Matrix: Aqueous
Batch:30983 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/06/2017 1154
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics - Unfractionated 1400 850 1 61 1.5 40-140 25 01/09/2017 1041
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2)
66
40-140
2-Fluorobiphenyl (fractionation 1)
79
40-140
o - Terphenyl (aromatic) - Unfractionated
61
40-140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 64 of 76
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MADEP VPH (aliphatics) - MB
Sample ID: SQ30715-001 Matrix: Aqueous
Batch:30715 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil PQL Units Analysis Date
C5 - C8 Aliphatics ND 1 75 ug/L 01/03/2017 1601
C9 - C12 Aliphatics ND 1 75 ug/L 01/03/2017 1601
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 117 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 65 of 76
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MADEP VPH (aliphatics) - LCS
Sample ID: SQ30715-002 Matrix: Aqueous
Batch:30715 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec Limit Analysis Date
C5 - C8 Aliphatics
150
160 1
103 70-130 01/03/2017 1504
C9 - C12 Aliphatics
150
150 1
99 70-130 01/03/2017 1504
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 101 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP VPH (aliphatics) - LCSD
Sample ID: SQ30715-003 Matrix: Aqueous
Batch:30715 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C5 - C8 Aliphatics
150
160
1 107 3.2 70-130
25 01/03/2017 1532
C9 - C12 Aliphatics
150
150
1 100 1.4 70-130
25 01/03/2017 1532
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 99 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP VPH (aromatics) - MB
Sample ID: SQ30716-001 Matrix: Aqueous
Batch:30716 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil PQL Units Analysis Date
C9 - C10 Aromatics ND 1 25 ug/L 01/03/2017 1601
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 110 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 68 of 76
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MADEP VPH (aromatics) - LCS
Sample ID: SQ30716-002 Matrix: Aqueous
Batch:30716 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 24 1 96 70-130 01/03/2017 1504
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 97 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP VPH (aromatics) - LCSD
Sample ID: SQ30716-003 Matrix: Aqueous
Batch:30716 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 25 25 1 100 3.7 70-130 25 01/03/2017 1532
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 95 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 70 of 76
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MADEP VPH (aliphatics) - MB
Sample ID: SQ30861-001 Matrix: Aqueous
Batch:30861 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil PQL Units Analysis Date
C5 - C8 Aliphatics ND 1 75 ug/L 01/04/2017 1715
C9 - C12 Aliphatics ND 1 75 ug/L 01/04/2017 1715
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 113 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 71 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aliphatics) - LCS
Sample ID: SQ30861-002 Matrix: Aqueous
Batch:30861 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q Dil
% Rec Limit Analysis Date
C5 - C8 Aliphatics
150
150 1
103 70-130 01/04/2017 1617
C9 - C12 Aliphatics
150
140 1
94 70-130 01/04/2017 1617
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 95 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP VPH (aliphatics) - LCSD
Sample ID: SQ30861-003 Matrix: Aqueous
Batch:30861 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C5 - C8 Aliphatics
150
150
1 99 3.3 70-130
25 01/04/2017 1646
C9 - C12 Aliphatics
150
130
1 89 6.3 70-130
25 01/04/2017 1646
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 92 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
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MADEP VPH (aromatics) - MB
Sample ID: SQ30862-001 Matrix: Aqueous
Batch:30862 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil PQL Units Analysis Date
C9 - C10 Aromatics ND 1 25 ug/L 01/04/2017 1715
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 108 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 74 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aromatics) - LCS
Sample ID: SQ30862-002 Matrix: Aqueous
Batch:30862 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 23 1 93 70-130 01/04/2017 1617
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 91 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 75 of 76
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MADEP VPH (aromatics) - LCSD
Sample ID: SQ30862-003 Matrix: Aqueous
Batch:30862 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 25 22 1 88 5.7 70-130 25 01/04/2017 1646
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 88 70-130
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. Page: 76 of 76
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
%Feed}'1=mirO11111CJ0lE.lS�r•:iR:Iswc�`�� O€'
�7vw nua,t hfu orxr: FiFflnIgC-07 Flfccrtvc Pots, I lif29 61d
f..xpir} I)noc: i [l2"ZI
aruple Receipt Cheeklist (SRC)
Client- �L COUICT Inspected by1da1c; i J 0 i, I o1>4: — Cs j oO 'k L.
Kleam-ofreoeipt: ;F';T ❑ Client u UPS u FcdEx
❑ Other
Yes ❑ No 3. Were custody seals present on tlto CMler?
Yes 0 -No - A-U" 2, If custody seals were Iin_5ml, were they Intact and uitl]rx)t; cr i?
pH wip ILA: 1 ._ CI strip ID;
Coal erJD/Orighial Canperaturcupon reGciptrDcrived (Corrected) lump-crahtne upon remipt:
Nfethod: TcrnpcTature 81ank ❑ Against Bottles rR Gaut ID. IR Cain CorTcetim Tactcir: �• � "C
ulbUd Of GCaiaut: % et Ice ❑ DIUe I= ❑Lary loe ❑ NLAw
Y'cs ❑
No
rl
)ftemperalura of any cooler exxxx3cd 6.41C, wsss lrmjcct lrfanagerNulifir�J2
PM x as Notifted hone / cmajI r Ntw_lo-face (Circle one).
Yea ❑
No f)
rio n
NA
4. I$ d1Q ppnlinMiBl. C011ricr'K povkl sli att;QOW to this form?
5. Were prQlm lolly procedures, (mlint ishad�'reeeive(1I fvllowe&
Yes
Ycs
Ni: ri
WQrQ sample IDs t]sted on the COO?
Yes
No r.r
7. WQrr satnJ)le I175 listed on all sample Conteincm'r
'y
:du ❑
i
S, Wtis collcxdon date a three iistad on the COC?Yes
Z
NO ❑
9. Wws so1b, bon date & tittil�_ h5fed on all sample Cuntainer!:?
No ❑
10. Did all cmnWincr label information (ID, date, titrre) a de wily the COC?
Nu 0
11, WcFc tests to 1re Wfo=od listed ott 11iC COC?
Y`cs
No C.
12. Did all sanipl es and vc in the proper c[1nlainars for each IeRC nrrd+or in good condition
unbrokcn, lids on etc,)?
ycs 16
No ri
13. Was adnquo-i tc sarn ie vo1u4m0 4)vailablc?
Yczs Ef
N, 0
14. W.cre all samples roceived witbia;� the I]Dldjng timie ur 48 hours, whiohcvu Gonw.; f-yg ?
No
YER I_I
1$_ Were any Hamnle- cnrrtairim lriissinjr'exce> q (circle one) samples Not listed on COC?
Yes ❑
No 07
i ❑
16. Were bubbk!. pmserpt -;�`povsiz :' ('/4"or 63ntn in diametel-) in any VOA vials?
Vrs
No ❑
NA ❑
17. Were a.11 PRO,1mcta1se'trutxiient w108reoei11letl al a pH of <2?
yCS r
No ❑
NA
18. Wac all cyanide midror sulfide samples rccciv d at a pI-I>12?
YCS ❑
No L: N
19. Were all arp'li m1t1r, NH3(TXI /cynnidc.'-phcuolr'BNA { 0,5mZrL} saniptc�, free rf rmidual
cJtlorine'�
Yes D
Na _A
21. Were Colloction tempel.ajurt�j dr_wunlciued crn the COC for NC sampics?
Yes u
No ❑ NA
21, Were cliini remarksr'regrieo; (i,c, rc-Tlested dilutions, MSr'MS17 ::t;sigiauons, etc..,)
c4rrol't]v transcribed frartl the COC inln the aonunent section in UMS?
Yes
I�ro El
22_ Woe the quote iifuIT) tr usrxl taker~ flmr r the, C�ntainet lalacl?
Sam Frewrvation (Must be calnplelcd for tiny saniple(s) inkx=ctly Ipre_Sert%vJ cx with lyeziapam)
Barry;,)
wore rcceived incorrectly preserved aind were adjusted siuu rduigly in
sampierecci}ping with
f)1� Oi. KNO;. HCl ldaOH) tiSin Sid#
SamJ tc(s�
_
were reccivcd with bubbles >6 mm in diameter,
Samplm(s)
- w rc received u.7th TRC>0.5 inpA, (IC421 is NO) and were
k4justed acwr(hngly in sal ie
recciving. with Frt jail I thiosulfare (Nas 20_,with SJ}C*ly ID. -
SC Dfinking ee-T Project Saniple(S) pH verified to be <2 by Dare:
Sam € s
were NO2 reteivixl rrt a PA of c.: 2 aaid Yyre ad'uaed auDDircling.ly usi SR#
Sarnple la'aels Lppl icd lyy:
Verified by- Date- a a A ti I&
C'nmmerlls'
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Appendix C
Waste Disposal Manifest

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De'signafed FaG{fry
Designate:l Facility
Designated F4cllity
Gesignaied Facility
Designated racility
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t��gt`t�i�tarrt ri3Clttcta �C2t' RGGyG(e
td_o.
Type
QTY
Nil/Vol
Profile Number
—�-- _ _
' }{
NA1993, Dies'ei fuel, 3, ill
ERG# 12$
-- �
NA1993, Fuei oil (tdo:1,2,4,5 or 6), 3, III
ERG# 128
}{
UNi?_03, Gasoline, 3, Il �
ERG# 128
X
NA1270, Petroleum 0ii, 3, III
ERG# 128
.. - t}311V2Y&al VUa$tE t.airips, i3att8i6e3, gal)a6tS, and taCtrl3niG8 foY Recycle
_
HM
Nts.
Type
Est. Mft.
c3Uitt
Shtpp6Eg P�arne and DescYption {it' applicable}
common tdame
i3iscYepancy
j{
RGt, UN2809, Marcuty contained in rnanufactured articles, $, III ERG# 172
Mercury Containing Articles
----------._
._.......--------
----4
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----
RQ, UN2809, Mercury,
-- --
8, ill ERCa# 172
hfiercury
Rt�, UN3432, Pofychioririated b;phenyls, solid, 9, I(' ERG# 17i
T$CA Exempt PCetamp Ballasts
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){
UN280iJ, Eattertas, rust, nonspiilable, $, ii( ERG# 154
sealed Lead Acid Batteries
i
UN2794, Batteries, wet, tilled with acid,. 8, Ilt ERG# 164
Lead Acid Batteries
�
UN2795, Batteries, rust: tiliad_wifh alkali, 8, 11I ERG# 154
NiGad. Batteries
�(�
UN3a90, Lithium batteries, S, ii � ERG# 138
__Wet
Lithium Batteries
;�
UN3028, Batteries, diy, eontainin j potassitirn hydroxido selid, 8,111 ERG# 154
__
Alkaline Batteries
}(
UN3028, Batteries, dry, containing potassium hydrdxide solid, 8, 111 ERG±t 154
NiCad Batteries
Universal Waste Lamps {Not DOT -Regulated per 49 CFR 173.164{e)
Fiuorescent iampe.4� or �
_ _
—�
__
_
Universal Waste Lamps (Not DOT -Regulated par 49 CFR 173.164(e)
FWorescent lamps 4` or>
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.164(e)
CirculartU-tube lamps
Universal Waste Lamps {Not DOT -Regulated per 49 CFR 173.164(e)
compact tamps
Universal Waste Lamps {Not DOT -Regulated per 49 CFR 173.164(e)
shattershield
Universal Waste Lamps (Not DOT -Regulated per 49 CFR 173.1 S4(e}
NiRrrtviu tamps
__
____
Universal Waste Lamps
(Plot DOT -Regulated
(tar 49 CFR 173.1 S4(e}
incandescent Lamps
Non -PCB Light Ballasts for Recycle (Not DOT -Regulated)
Non -PCB Light Ballasts
Electronic Equpmenftor Recycle {Not DOT -Regulated)
Electronics
3 Generator's Certification: This is fo cenity that the above -named
lnateriais era properly Gasified, desoritted; packaged; marked, and labeled, and ai8 in proper condition For transportation accortling to
the
I appiica6le regulations of the Department of Transportation. i Iurther
certify that none of the materials described above are a hazardous waste as defined fly EPA 4QCFR Part 26t or any applicable state law,
and
unless speciBcaily identified above the materials contain lass than 1,000
ppm total halogens and do not contain quantifiable levels (2ppm) of•PCBs as defined by EPA 40 CFft•Paris 279 and 78t.
Generator'slOiferor's Pr'intedlTyped Name
Signature
Month bay
Year
Transport 1 PrintedlType aino
' n re
Month Day
Year
r� 6r1
�
l
Trans rtar 2 PrintedtTyped Name
Sfgnat re �
Month Day
Year
Discrepancy indication /Additional Information:
Month Day
Yaar
Designated FaciUty CertEfilcation: I hereby acknotivledge receipt of the materials covered by this manifest except tar any discrepancy indicated abcva.
PrintedlTyped Name-----�------'------T-----^--
Signature --
— Month Uay
Yaar