MO-6615_27296_CA_LSA_20030311_Phase2

ERM NC, PC
March 11, 2003
Reference: Phase II Limited Site Assessment Report
Integris Metals Facility
527 Atando Avenue
Mecklenburg County
Incident #: Pending
Mr. Steve Bograd
NCDENR - Division of Waste Management
UST Section
919 North Main Street
Mooresville, NC 28115
Dear Mr.Bograd:
7300 Carmel ExecutivePark
Suite 200
Charlotte, NC 28226
[phone]
[phone] (fax)
VIA FEDEX
RECEIVFn
ERMo
MAR 1 2 2003
NCDEPi �: c,an�rcun�Wcn,
AND NATURAL RESOURCES
MOORESVW,REQ$(*K OFFICF
On behalf of Integris Metals Inc., ERM is submitting a Phase II Limited
Site Assessment Report for the above referenced site. Please contact me
if you have any questions concerning the report.
Sincerely,
1.��-
Rick Tarravechia, P.G.
Project Manager
RT
enclosures: Phase II LSA Report
cc: R. Giles - Integris
A. Nash - Integris

A. Site Identification
DATE OF REPORT:
Facility I.D.:
Site Name:
Site Location:
Nearest City/Town:
Limited Site Assessment Report
March 11, 2003
NA UST Incident Number (if known): NA
Inc.
527 Atando Avenue
Charlotte
County: Mecklenburg
UST Owner: Integris Metals (formerly Rio Algom, Vincent Metal Goods, and Edgecomb Steel) _
Address: 455 85 Avenue NW, Minneapolis, MN 55433 Phone: [phone]
UST Operator:
Vincent Metal Goods
Address:
527 Atando Avenue
Phone:
704-372-9900
Charlotte, NC 28206
Property Owner:
Integris Metals
Address:
527 Atando Avenue
Phone:
_
704-372-9900
Charlotte, NC 28206
Property Occupant:
Integris Metals
Address:
527 Atando Avenue
Phone:
704-372-9900
Charlotte, NC 28206
Consultant/Contractor:
ERM NC, PC
Address:
7300 Carmel Executive Park, Ste. 200, Charlotte, NC 28226
Phone:
704-541-8345
Release Information:
Date Discovered: November 13, 2002
Latitude: 350 18' 40" N Longitude:
Estimated Quantity of Release: Unknown
Source of Release (e.g., Piping/UST): Two fuel oil USTs
Sizes and contents of UST system(s) from which the release occurred):
800 42' 44" W
Tank
Installation
Closure
Size in
Tank
Number
Dates
Date
Gallons
Construction
Contents
1
1966 or earlier
(possibly as
Out of service
since 1981
Est. 6,000
Steel
Fuel oil
2
Est. 6,000
Steel
Fuel oil
early as 1949
Complete and include in report items B through J in the order listed.
I, Rick Tarravechia a Professional Engineer(
nginee icensed G�ined
(circle one) for ERM NC, PC
(firm or company of employment), do certify that the informs ' n this report is correct and accurate to the
best of my knowledge. e. ,� 'I"Go"Ove �
.� 0_�
Rick Tarravechia, P.G.
(Please Affix Seal and
SEAL
1076
ERM NC, PC Page 2 of 8 Integris ISA Report.doc - 3/10/03

B. Risk Characterization
Submit the following questionnaire in its entirety. Answer all questions completely. Attach additional pages as needed to fully
explain answers. Base answers/explanations on information known, or required to be obtained, during the Limited Site
Assessment.
NOTE: Source area means point of release from a UST system.
Limited Site Assessment Risk Classification and Land Use Form
Part I — Groundwater/Surface WaterNaoor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non -drinking purposes? NO
2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release? NO
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water, filling
swimming pools) located within 250 feet of the source area of the release? NO
4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there is no other
source of water supply other than the groundwater)? NO
5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined space or pose
any other serious threat to public health, public safety or the environment? NO
If yes, describe.
6. Are there any other factors that would cause the release to pose an imminent danger to public health, public safety, or the
environment? NO
If yes, describe.
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? YES
If YES, does the maximum groundwater contaminant concentration exceed the surface water quality standards and criteria
found in 15A NCAC 2B .0200 by a factor of 10? YES
8. Is the source area of the release located within a approved or planned wellhead protection area as defined in 42 USC
300h-7(e)? NO
If yes, describe.
Is the release located in the Coastal Plain physiographic region as designated on a map entitled "Geology of North
Carolina" published by the Department in 1985? NO
If YES, is the source area of the release located in an area in which there is recharge to an unconfined or semi -confined
deeper aquifer that is being used or may be used as a source of drinking water? NOT APPLICABLE
If YES, describe.
9. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels (see Table 9
NCDENR, 4/2001) established by the Department? NO
ERM NC, PC Page 3 of 8 Integris LSA Report.doc - 3/10/03

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO
Describe.
Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or
other place of public assembly? NO
Describe.
Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g.,
manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an
inactive commercial or industrial enterprise, or is the land undeveloped? YES
Describe.
The facility receives raw metal products, then levels (straightens), cuts, slits, and re -packages the metal to customer
specifications. The final product is then distributed to fabricators and other end users.
Do children visit the property? NO
Explain.
Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)? NO
Explain.
There are no fences present along the subject property boundaries.
2. Do pavement, buildings, or other structures cap the contaminated soil?
YES
3. Describe.
Affected soils at the subject property are located beneath the concrete floor of the facility building (Both
former USTs and underground piping are inside the building). (see Table B-3)
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will remain capped in
the foreseeable future?
Affected soils at the subject property are located beneath the concrete floor of the facility building (Both
former USTs and underground piping are inside the building). (see Table B-3)
4. What is the zoning status of the property?
I-2: Industrial
Is the use of the property likely to change in the next 20 years? NO
Explain.
The site is located in an older, commercial/industrial section of the city of Charlotte.
or similar commercial use.
ERM NC, PC Page 4 of 8 Integris LSA Report.doc - 3/10/03

Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property containing source
area of the release):
1. What is the distance from the source area of the release to the nearest primary or secondary residence (permanent or
temporary)?
The nearest residence is approximately 300 feet west of the source of the release.
2. What is the distance from the source area of the release to the nearest school, daycare center, hospital, playground, park,
recreation area, church, nursing home or other place of public assembly?
With the exception of the residential houses west of the railroad tracks, the area surrounding the subject
property is highly industrial. No day cares, hospitals, playgrounds, nursing homes, etc. are located within
1,500 feet of the release. However, the office of a church pastor is located within a multi -tenant office park
approximately 550 feet northwest of the on -site source area.
3. What is the zoning status of properties in the surrounding area?
SEE FIGURE 2 — All properties within a 1,500-foot radius of the source of the release are zoned for either
Business, Industrial or Residential development.
4. Briefly characterize the use and activities of the land in the surrounding area.
Surrounding properties include a diaper cleaning service, two trucking services, a restaurant, a railroad, and
beyond the railroad a single family residential neighborhood.
C. Receptor Information
1. Water Supply Wells (Complete and attach Table B-5 and attach map showing well locations)
No water suDDly wells are within 1.500 feet of the site. SEE TABLE 5 AND FIGURE 2.
2. Public Water Supplies
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water supply.(indicate on map)
Describe.
Public water lines are present along all streets in the area.
3. Surface Water
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the source area of the release. This
information must be shown on the USGS topographic map.
A small intermittent creek is located approximately 250 feet west of the source of the release. This
intermittent creek runs parallel to the railroad (southeast), then veers to the southwest. During ERM's
January 2003 site visit, the intermittent creek was dry. During early March 2003, the intermittent creek
contained water. - SEE FIGURE 2.
4. Wellhead Protection Areas
Identify all planned or approved wellhead protection areas (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map. Wellhead protection areas are
defined in 42 USC 300h-7(e).
No wellhead
areas are present within 1,500 feet.
ERM NC, PC Page 5 of 9 Integris LSA Report.doc - 3/10/03

5. Describe Deep Aquifers in the Coastal Plain Physiographic Region (rfer tome 19 of the guidelines
NOTE: This requirement only pertains to releases in the Coastal Plain physiographic region as designated on a map entitled
"Geology of North Carolina" published by the Department in 1985.
6. Describe Subsurface Structures (refer to page 4-14 of the guidelines):
Subsurface structures located on or adjacent to the site include water, storm sewer, sanitary sewer, and
natural gas lines. There are no basements at or adjacent to the site. Based on the generally non-volatile
character of the affected soils (see Table 3), the potential for accumulation of hazardous vapors appears to
be minimal.
7. Property Owners and Occupants
Attach Table B-6, listing the names and addresses of property owners and occupants within or contiguous to the area
containing contamination and all property owners and occupants within or contiguous to the area where the contamination is
expected to migrate.
Discuss other relevant aspects of the site and nearby areas, including receptors. Provide data from available sources
and/or site investigations concerning the following: Land use information, including the uses and activities (involving
possible human exposure to contamination) that occur at the site and adjacent properties;
Escobar Truck Equipment Corporation, which appears to be an automotive garage, is located north of the facility on the
opposite side of Atando Avenue relative to the subject property. Dy-Dee Services, a commercial diaper laundering
service, is located adjacent and north of the subject site (on the same side of Atando Avenue as the subject facility).
Superior Mechanical Systems and Simpson Pallets Wood Products, Inc., a manufacturer of wood pallets, are located to
the east. Moss Trucking is located south of the facility, and the railroad tracks are located to the southwest and west. The
nearest residence is aooroximately 300 feet to the west.
Indicate on the site map other possible routes of exposure to contamination such as sewers, utility lines, conduits,
basements, septic tanks, drainfields, etc. —
NONE. Underground utilities are routed along the property boundaries or beneath the interior of the property
(services) and do not appear to intersect any areas of affected soil.
Distance to nearest body of surface water (e.g., ditch, pond, stream, river, etc.). —
NOTE: See the instructions for a water supply well survey on page 4-12:
SEE FIGURE 2. An intermittent stream located approximately 250 feet west of the subject property (on the
opposite side of the railroad tracks) is the nearest surface water body. During ERM's January 2003 site visit,
the intermittent creek was dry. During early March 2003, the intermittent creek contained water.
D. Site Geology and Hydrogeology
Describe the soil and geology encountered at the site. Discuss the effects of soil and geological characteristics on the
migration and attenuation of contaminants. Include information obtained during assessment activities (e.g., lithologic
descriptions made during drilling, probe surveys, tank closure, etc). If a Phase II investigation is required include a discussion
of groundwater flow direction and hydraulic gradient (vertical and horizontal).
The Charlotte area, including the subject site, is located within the Piedmont physiographic province of North
Carolina. The subject property is located within the Charlotte Belt, which is characterized by metamorphic rocks and
igneous rocks of varying age. According to the Geologic Map of Charlotte (1988), the subject property is underlain
predominantly by metamorphosed quartz diorites and tonalites. These metamorphosed igneous rocks are typically
medium to coarse grained and foliated. These rocks are of late Proterozoic age (900 to 570 millions years old).
Saprolite, a layer of weathered and variably decomposed bedrock, commonly mantles bedrock in this region.
Saprolite has the appearance of compact clayey to sandy soil, with original bedrock textures and features preserved.
Soils at the site are typically comprised of brown to red silty clay, based on field observations noted during the soil
sampling operations. Partially weathered bedrock was not encountered during drilling operations at the site.
PP RM NC, PC Page 6 of 8 Integris LSA Report.doc - 3/10/03

Groundwater occurs at depths ranging from 12 to 18 feet below grade, and flows to the south under a hydraulic
gradient of 0.07, as measured between wells MW-1 (located at the UST source area) and downgradient well MW-4.
E. Sampling Results
Phase I Investigation
NOTE: Responsible parties for all releases must perform a Phase 1 investigation.
A Phase I investigation includes the installation of one monitoring well in the source area of a release. Soil samples are to be
collected every five feet in the unsaturated zone and should be analyzed in accordance with the methods specified in Table 5
(NCDENR, 4/2001 - Analytical Methods for Petroleum Contaminated Soil). If the water table is encountered at 25 feet or
greater from the land surface, samples for laboratory analysis should be collected every 10 feet in the unsaturated zone.
Describe all soil sampling performed during the installation of the source well(s) (use maps and tables whenever possible) and
include:
location of soil samples; SEE FIGURES 3 and 4.
type of soil samples (from excavation, borehole, geoprobe, etc.); Geoprobe and hollow stem auger (SEE TABLE B-3).
Complete and attach Table B-3.
If multiple source areas have been identified, use individual tables for each source well installation.
2. Describe any groundwater sampling from the source area monitoring well(s). Use maps and tables whenever possible and
include:
location of groundwater samples/monitoring wells/water supply wells; SEE FIGURE 4.
Complete and attach Table B-4. (SEE TABLE B-4).
If multiple source areas have been identified, use individual tables for each source well.
Note: If free product is present, do not sample the monitoring well. Report the estimated thickness, type, and quantity of free
product present. 0.05 feet (one half inch) of free product (apparently weathered fuel oil) was originally
detected in well AM-1. Free product removal activities are on -going. SEE TABLE S.
3. Monitoring well construction information
© Complete and attach Table B-7. (SEE TABLE B-7).
F. Conclusions and Recommendations
Discuss the risk criteria that apply to the release and identify any other site -specific factors related to the release that may pose
a risk to human health and the environment. Also, discuss any site -specific conditions or possible actions that could result in
lowering the level of risk posed by the release.
The two on -site USTs located inside the building are the source of this release. The two USTs have not been in
use at the site since 1981. Although the tank contents have been evacuated, they have not been closed in
accordance with DENR procedures. In -place closure of the USTs (tanks foamed, lines capped, etc.) is planned
pending DENR approval of the Phase II LSA and subsequent free product recovery activities at the site. The in -
place closure has been selected because UST removal activities ( cutting concrete, excavation, dust, noise, etc.)
inside the building would be excessively disruptive to the continued operation of the facility.
The results of the sensitive receptor survey at the site indicate that there are no water supply wells within 1,500
feet of the site. A small, intermittent stream is located approximately 250 feet west of the UST source area, on the
opposite side of the railroad tracks from the subject property. ERM's on -site observations indicate that this
intermittent stream was dry during January 2003 but contained water during March 2003.
Less than one-half inch of free product is present in one on -site monitor well. Free product gauging and recovery
is on -going at the site. No other factors that may pose a risk to human health or the environment were identified
at the site. In addition, land use at the site and in the surrounding area support an industrial/commercial land use
designation for the site. In soils, industrial/commercial maximum soil contaminant concentrations (MSCCs) are
not exceeded in the source area petroleum -affected soils. Based on the lack of receptors, the soil concentrations
being below the industrial/commercial MSCCs, and because the affected soils are capped below the concrete floor
of the building, no removal of the affected soils has been performed and none is plannedat this time. In
groundwater, risk -based corrective action standards (GCLs) for the petroleum hydrocarbons detected at the site are
ERM NC, PC Page 7 of 8 Integris LSA Report.doc - 3/10/03/

not exceeded. Because less than a half inch of free product is present, the site currently meets the criteria for
classification as an Intermediate Risk site.
G. Free Product Investigation/Recovery (if applicable): Free product recovery is ongoing on a monthly basis. Reports
will be submitted to the Department on a quarterly basis. Free product removal activities to date are indicated in Table B-
8. The first Free Product Recovery Report will be submitted to the Department during July 2003.
If free product is still present or is discovered during the limited site assessment, continue or begin free product recovery
immediately in accordance with 15A NCAC 2N. 0705 and submit an up-to-date Free Product Recovery Report (Report 134).
H. Site History:
Update site history information provided in the 20-Day Report as necessary.
Using the format in Table B-1, list all UST systems currently or previously located at the site including UST system
number, product, capacity, date installed, date removed or closed, and whether a release was discovered. UST system
numbers should correspond to the site map information requested below. (SEE TABLE B-1)
Using the format in Table B-2, list the names, addresses, telephone numbers, and dates of ownership/operation of all
previous UST owners and operators of the UST system(s). (SEE TABLE B-2).
I. Figures (Please attach the following figures)
71/2 minute USGS topographic quadrangle map copy showing an area within a 1,500-foot radius of the source area of the
release and depicting the site location, all water supply wells, public water supplies, surface water intakes, surface water
bodies, designated well head protection areas, and areas of recharge to deeper aquifers in the Coastal Plan that are or may
be used as a source for drinking water. SEE FIGURE 1.
71/2 minute USGS topographic quadrangle map copy showing an area within a 1,500-foot radius of the source area of the
release and depicting the site location as well as all schools, daycare centers, hospitals, playgrounds, parks, recreation
areas, churches, nursing homes, or other places of public assembly. Also identify the zoning status of the area within the
1,500-foot radius. SEE FIGURE 2.
Site map with UST systems location(s) including piping and pump islands, site boundaries, buildings, named roads,
subsurface utilities, basements, adjacent properties, scale, and north arrow. SEE FIGURE 3.
© Site map showing the results of all soil sampling conducted. Indicate sample identifications, sample locations,
sampling depths, and analytical results. SEE FIGURES 3 & 4; AND TABLE B-3.
Site map showing the results of all groundwater sampling conducted. Indicate sample identifications, sample locations,
monitoring well identifications, and analytical results. SEE FIGURE 4 AND TABLE 4.
Site map showing the elevation of groundwater in the monitoring wells and the direction of groundwater flow. NOTE:
This requirement applies to the Phase H investigation only. SEE FIGURE 5.
NOTE: If possible, use a single base map to prepare site maps using a map scale of l inch = 40 feet (or a smaller scale for large
sites, if necessary). Maps andfrgures should include conventional symbols, notations, labeling, legends, scales, and north arrows
and should conform to generally accepted practices ofmap presentation such as those enumerated in the USGS Geological Survey
pamphlet, "Topographic Maps."
J. Other Information (Please attach the following information)
© Boring logs and lithologic descriptions; SEE APPENDIX A.
© Well construction records (Table B-7); SEE APPENDIX A.
Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature) made during groundwater sampling);
NOT APPLICABLE.
Standard procedures used for sampling, field equipment decontamination, field screening, etc.; SEE APPENDIX B.
Disposal manifests; SEE APPENDIX C.
© All laboratory reports and chain -of -custody documents. Laboratory analytical data sheets for initial soil
sampling presented in Initial Abatement Measures Report prepared by ERM and submitted to DENR
on December 2, 2002. LSA laboratory analytical data sheets are presented herein (SEE APPENDIX D).
ERM NC, PC Page 8 of 8 Integris LSA Repon.doe - 3/10/03

Figures

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Tables

TABLE B-1 SITE HISTORY
UST System Information Facility I.D.: NA
Date: 03/10/03 Incident Number and Name: Integris Metals - Pending
'
UST ID Number
Product -
-
Capacity (gallons)
Date Installed
Oa. ermanenty
Closed; or Still In Use'
-: Was Release -.
Associated with UST
Sys(am? (Yes/No) :
1
Fuel oil
est. 6,000
1966 or earlier
(possibly as early
as 1949)
Out of Service since
approximately 1981
Yes
2
Fuel oil
est. 6,000
1966 or earlier
(possibly as early
as 1949)
Out of Service since
approximately 1981
Yes
- Still in use means not permanently closed. FRP = Fiberglass reinforced plastic
TABLE B-2 SITE HISTORY
UST Owner/Operator Information (most recent first) Facility I.D.: NA
Date: March 10, 2003 Incident Number and Name: Integris Metals - Pending
UST ID Number
IName of Owner or Operator
jDates of Ownership/Operation
Owner or Operator?
1 and 2
IIntegris Metals
12001-present (never operated USTs)
owner
Address - -
-
Telephone Number
527 Atando Avenue
Charlotte, NC 28206
704-372-9900
UST ID Number:
Name of Owner or Operator
I Dates of Ownership/Operatiori -
Owner or Operator)
1 and 2
Rio Algom, Ltd.
1995.2001 (never operated USTs)
owner
Address - i.-
:: - - - - : :- -
Telephone Number
527 Atando Avenue
Charlotte, NC 28206
704-372-9900
UST ID Number •-
Name of Owner or Operator
jDates of Ownership/Operation
Owner:or Operator?
1 and 2
lVincent Metal Goods
1976-1995 (operated UST until 1981)
owner/operator
Address -
Telephone Number.
527 Atando Avenue
Charlotte, NC 28206
704.372-9900
UST ID Number ' -
Name of Owner or Operator
I Dates of Ownership/Operation
Owner or Operator?
1 and 2
1 Edgecomb Steel
1949 - 1974
owner/operator
Address
- -
Telephone Number
527 Atando Avenue
Charlotte, NC 28206
unknown
Integris Tables.xls:8-1&B-2 History Page 1 of 1

TABLE B,3
Date: 03/10/03
SUMMARY OF SOIL SAMPLING RESULTS
Incident Number and Name: Integris Metals - Pending
Facility I.D.: NA
Analytical Method.-' - `s -�.`
U
O>
EPA 8015 (mglkg)
VOCs - 8260 (mg/kg)
-
o
o
d
m
d
m
d
d
N
N
N
�
N
N
N
C a
(p 9
m 77
C
L
N
C
d
C
a
C
G
p
1r
y
C
C
d
C
a
d
L
N r
N
N
O
y
m
0
it Z
c
a
N
W
o
L
o
Depth
32 E
.=
H S
c
S.
v
coS
m
Co
n
o
H
n
o
E
c
Sample ID
Date .
(ft. BGL)
?
°
t
FO
w
m
C
N
.p.
O
6
N
z
d
N
M
UST Closure
Samples
VMG-1
10/19/02
1.5
NO
NO
NO
--
--
--
--
--
--
--
--
--
--
-
--
--
--
VMG-2
10/19/02
13
56
94
2,400
NO
NO
0.95
3.40
NO
NO
2.20
2.10
NO
0.90
1.50
9.50
1.60
7.40
3.40
VMG-3
10/19/02
14
64
140
2,500
NO
NO
0.78
NO
NO
NO
2.60
1.20
NO
0.65
0.57
6.50
1.40
0.41
NO
VMG-4
10/19/02
4
32
160
15,000
--
--
-
--
-
--
--
--
--
-
-
--
--
-
--
VMG-5
10/19/02
15.5
89
110
1,700
--
--
--
--
--
--
--
--
--
-
-
--
--
--
-
VMG-6
10/19/02
16
NO
NO
NO
-
--
--
--
--
-
--
--
-
--
--
--
--
--
-
VMG-7
10/19/02
4
NO
NO
NO
-
--
--
--
--
-
--
--
--
--
--
--
-
--
-
VMG-8
10/19/02
4
NO
NO
NO
-
--
--
--
--
--
--
--
--
--
--
--
--
--
-
VMG-9
10/19/02
14
NO
NO
NO
-
--
--
--
--
-
--
--
--
--
--
--
-
--
-
VMG-10
10/19/02
4
NO
NO
NO
--
--
--
--
--
-
--
--
--
--
-
-
--
--
-
VMG-11
10/19/02
16
23
100
8,100
-
--
--
--
--
-
--
--
--
--
--
--
--
-
--
VMG-12
10/19/02
16
62
120
2,100
NO
NO
0.99
0.85
NO
NO
4.20
2.70
0.43
1.40
2.70
11.0
3.90
19.0
4.50
VMG-13
10/19/02
6
45
480
12,000
NO
NO
NO
NO
NO
NO
10.0
4.20
NO
3.20
5.70
32.0
7.80
16.0
9.60
VMG-14
10/19/02
4
NO
NO
NO
--
--
--
--
--
-
--
--
--
--
--
--
--
-
--
VMG-15
10/19/02
4
50
290
5,200
--
--
--
--
--
-
--
--
--
--
--
--
--
-
--
LSA Samples
MW-1 @ 5
1/2/03
5
--
--
0.0056
NO
NO
0.0073
NO
NO
NO
NO
NO
NO
NO
NO
NO
0.015
0.0057
MW-1 @ 10
1/2/03
10
--
--
NO
NO
0.310
0.210
NO
NO
1.2
0.54
NO
0.230
0.560
11.0
0.540
1.6
0.55
MW-1 @ 15
1/2/03
15
--
--
NO
NO
0.49
0.55
NO
NO
1.1
0.71
NO
0.38
0.64
6.0
0.79
1.2
0.72
MW-1 @ 20
1/2/03
20
--
--
NO
NO
0.22
NO
NO
NO
0.88
0.50
NO
0.23
0.45
3.1
0.46
NO
NO
MW-2 @ 5
1/3/03
5
--
--
NO
NO
2.3
3.0
NO
NO
5.4
4.0
NO
3.3
3.5
26.0
7.0
20.0
11.0
MW-2 @ 10
1/3/03
10
--
--
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
0.63
NO
0.43
NO
MW-2 @ 15
1/3/03
15
--
--
0.0057
NO
0.018
0.019
NO
NO
NO
NO
NO
0.0061
NO
0.089
0.011
0.074
0.027
Soil -Groundwater MSCC 10 10
0.0056
7
0.24
5
0.92
0.37
4
3
3
2
NE
0.58
2
8
7
Residential MSCC,
22
3,200
1,560
32K
156
156
156
156
156
1,564
NE
63
156
782
120,440
782
Industrial/Commercial MSCC --
200
82K
40K
200K
4,088
4,088
4,088
4,088
4,088
40,880
NE
1,63 i
4.088
20,440
Soil P--••'•- Pr^' -2

TABLE B-3
Date: 03/10/03
SUMMARY OF SOIL SAMPLING RESULTS
Incident Number and Name: Integris Metals - Pending
Facility I.D.: NA
Analytical Method
VPH/EPH (mg/kg)
8270 (mg/kg)
2
io
m
c
@
c
t
a
E
d
o
yU
c
m
a�
Depth
U
U
U
U
U o
a
Sample ID
-Date
(ft.,BGL)
U
0
U
U
U
o¢
LL
N i
a
MW-1 @ 5
1/2/03
5
ND
NO
ND
NO
ND
ND
ND
ND
NO
MW-1 @ 10
112/03
10
ND
ND
2,200
190
61
760
1.2
17.0
4.0
MWA @ 15
1/2/03
15
ND
ND
420
83
39
94
1.0
12.0
2.4
MWA @ 20
1/2/03
20
ND
17
330
60
41
150
ND
2.7
0.71
MW-2 @ 5
1/3/03
5
NO
ND
2,200
460
210
1,600
5.0
78.0
15.0
MW-2 @ 10
113/03
10
ND
ND
ND
NO
ND
ND
ND
ND
ND
MW-2 @ 15
1/3/03
15
ND
NO
ND
NO
ND
ND
ND
ND
ND
Soil -Groundwater MSCC
72
3,255
Immobile
34
44
3
60
Residential MSCC
939
9,386
93,860
469
620
63
469
Industrial/Commerdial MSCC --
24,528
245,280
>100%
12,264
16,400
1,635
12,264
Only detected compounds are shown in table.
BGL = Below ground level NO = Not detected
Results shown in bold exceed NE = Not established
soil -groundwater MSCC. NA = Not Applicable
Integris Tables.xls:B-3 Soil Results Page 2 of 2

TABLE B-4 SUMMARY OF GROUND WATER SAMPLING RESULTS
Date: 03/10/03 Incident Number and NnmP-IntPr,rk Metal. - P.ndinc FacR !D'HA
EPA Method 602 (ugA)
MADEP VPHfEPH (ug/Q
EPA 625
E
x
E
<
C0
n
AS
Monitor-
Lu
2
0
:Well:
12
(Z
Z
2:
(3
.2
u-
Z
Q-
MW-1
1/3/03
Not Sampled
- Free
product
(fuel oil)
present in
well
MW-2
1/3/03
168
55
NO
15
98
NO
NO
NO
NO
1,100
NO
770
1,600
12
NO
18
92
39
MVV-3
1122103
3.6
1.6
2.0
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
11
NO
NO
NO
MW4
1122103
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
MVV-5
1/22103
5.4
3.6
1.8
NO
NO
NO
NO
3,500
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
OW-1
1/22103
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NG T. Md
1
1 1,000
1 29
1 530
1 200
1 70
PIN
Ell
4,200
142,0001
2
IP
0::-
80
1�
3
1=78=0 =1
210
lGross Contamination Level
5,000
1257,500
1 29,000
187,500
1200,000
1 70,000
E
NE
I NE
I NE
E -41
2,120
1 3,000
1 950
�1
1 15,500
1 410
jSdHdceWatef.StandArd:::
71.4
1 11
1 29,0001
88.5
1 11.6
1 19,000
1 2,000
25,000
NE
1 118 1 32
1 2,700
1 5.9
114,—
1,134
210
"-"indicates not analyzed.
NO = Not detected
MTBE = Methyl tart butyl ether
IPE = Isopropyl Ether
Results shown in bold exceed T15A 2L standards.
Only detected compounds are included in table.
NE = Not Established
NA = Not Applicable
Intends Tables.xis-8-4 GW Data P-- I -f 1

Z
0
a
0
LL
Z_
J
J
W
}
J
a
IL
N
K
W
F
Q
m
`o

TABLE B-7
Date: 10-Mar-03
WELL CONSTRUCTION INFORMATION
Incident Number and Name: Inte ris Metals - Pending Facility ID#: NA
Monitor
Well ID
Date
Installed
Date Water
Level
Measured
Well Casing
Depth
(feet BGS)
Screened
Interval
(feet BGS)
Bottom of
Well
(feet BGS)
Top of Casing
Elevation
(feet*)
Depth to
Water from
Top of Casing
(ft.)
Free Product
7hidrness (ft.)
Ground Water
Elevation' (ft.)
Comments
MW-1
1/2/03
1122/03
19
19-34
34
104.50
16.24
0.02
88.28
MW-2
1/3/03
1/22/03
19
19-34
34
104.50
18.03
0.00
86.47
MW-3
122/03
122/03
17
17-32
32
99.72
13.60
0.00
86.12
MW-4
121/03
122103
17
17-32
32
99.90
15.85
0.00
84.05
MW-5
122/03
122103
17
17-32
32
101.79
11.95
0.00
89.84
DW-1
121/03
1/22103
81
81-86
88
100.00
12.14
0.00
87.86
Reference point for elevation measurements: DW-1 TOC Assumed elevation: 100.00 ft. (DW-1 top -of -casing)
If free product is present, ground water elevation should be calculated by: (top of casing elevation - depth to water) + I free product thickness x 0.8581)
ft. BGS = feet below ground surface
Intagris Tables.xls:B-7 Well Const Page 1 of 1

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5 .
NUmbeHMap
ID
f;:, Properly Address { '?
6wner/OdcummiiMailin
Address-,- `
e
08505412
527 ATANDO AVE." INTEGRIS METALS
45585th Avenue NW
CHARLOTTE, NC 28206
Minneapolis, MN 55433
08505413
611 ATANDO AVE..
DYDEE WASH, INC.
611 ATANDO AVE.
CHARLOTTE, NC 28206
CHARLOTTE, NC 28206
08505411
503 ATANDO AVE."
MOSS TRUCKING CO., INC.
P.O. BOX 790376
CHARLOTTE, NC 28206
CHARLOTTE, NC 28206
NORFOLK SOUTHERN RAILROAD
THREE COMMERCIAL PLACE
08505502
RAILROAD
CORPORATION
NORFOLK VA 23510
CHARLOTTE, NC
ESCOBAR TRUCK EQUIPMENT 4
08507331
618ATANDOAVE.
CORPORATION
P.O.B. 790403
CHARLOTTE, NC 28206
MAURICIO & ADAN ESCOBAR
CHARLOTTE NC
SUPERIOR MECHANICAL SYSTEMS
08507332
600ATANDOAVE.
LEONARD& RUBY BURCH
P.O.B. 560711
CHARLOTTE, NC 28206
MANAGER: PAM BURRIS
ICHARLOTTE, NC 28256-0711
SIMPSON PALLETS WOOD PRODUCTS01
H
524 ATANDO AVE.
MELVIN L. & BARBARA SIMPSON
P.O.B. 790006
CHARLOTTE, NC 28206 1
CHARLOTTE, NO
ADJACENT PROPERTY MAP
TABLE
Environmental',
INTEORIS METALS
Resources
527 ATANDO AVENUE
D—�
FIRM
Management
CHARLOTTE, NORTH CAROLINA
D
Integds Tables Tax Map.xls:6.6 Owners Page 1 of 1

TABLE B-7
Date: 10-Mar-03
WELL CONSTRUCTION INFORMATION
Incident Number and Name: Inte ris Metals - Pending Facility ID#: NA
Monitor
Well ID
Date
Installed
Date Water
level
Measured
Well Casing
Depth
(feet BGS)
Screened
Interval
(feet BGS)
Bottom of
Well
(feet BGS)
Top of Casing
Elevation
(feet')
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness (ft.)
Ground Wate
Elevation* (ft.)
Comments
MW-1
1/2/03
1122/03
19
19-34
34
104.50
16.24
0.02
88.28
0.02 feet of free product
measured in well MW-1
MW-2
113/03
1/22/03
19
19-34
34
104.50
18.03
0.00
86.47
MW-3
1/22103
1/22/03
17
17-32
32
99.72
13.60
0.00
86.12
MW-4
1/21/03
1/22/03
17
17.32
32
99.90
15.85
0.00
84.05
MW-5
1/22103
1/22/03
17
17-32
32
101.79
11.95
0.00
89.84
DW-1
1/21/03
1/22/03
81
81.86
88
100.00
12.14
0.00
87.86
Reference point for elevation measurements: DW-1 TOC Assumed elevation: 100.00 ft. (DW-1 topof-casing)
If free product is present, ground water elevation should be calculated by: [top of casing elevation - depth to water] + [ free product thickness x 0.8581]
ft. BGS = feet below ground surface
Integris Tables.xls:B-7 Well Const Page 1 of 1

TABLE B-8 FREE PRODUCT RECOVERY RESULTS
Date: 10-Mar-03 Incident Number and Name: Integris Metals - Pending
Free Product Recovery Method: NA Facility ID#: NA
Method of Measurement: Bailer
Well 10
Product Type
Date of
Recovery
Casing
Diameter
(inches)
Product
Thickness
Before
Recovery (ft.)
Product
Thickness After
Recovery (ft.)
Amount of
Product
Recovered
(gallons)
Depth to Water
from Top of
Casing (ft.)
MW-1
Fuel Oil
01/032003
2
0.05
0.00
<0.25
21.32
MW-1
Fuel Oil
0122/2003
2
0.02
0.00
<0.25
16.23
MW-1
Fuel Oil
03/10/2003
2
0.04
0.00
<0.25
14.07
Total Gallons Recovered: Approximately 0.3 gallons
Total Gallons Recovered to Date: Approximately 0.3 gallons
Integris Tables.xis:8-8 FP Rec Page 1 of 1

Appendix A
Lthologic Logs and Monitor Well
Construction Diagrams

a,
8" DIAMETER BOLT
DOWN WELL COVER
2' X 2' CONCRETE PAD WATER TIGHT, LOCKABLE
WELL CAP
a n 6
NEAT CEMENT GROUT
TOP OF BENTONITE (FT,) 13
BOTTOM OF BENTONITE (FT.) 15
2 "DIA. SCH. 40 PVC RISER
PIPE, LENGTH
TOP OF SCREEN (FT.) 19
DEPTH TO
GROUND WATER (FT.) 21_32
SCHEDULE 40 PVC THREADED
FLUSH JOINT 0.01" MILL SLOTTED —
WELL SCREEN
WASHED SAND PACK —
BOTTOM OF SCREEN (FT.) 34
TOTAL DEPTH OF BORING (FT.) 34 PVC END CAP
BOREHOLE DIA. (IN.) 4.25
ERM-Southeast, Inc.
DRILLING LOG
MW-1
BPBp
g IN or
Date: 01/02/03 Project No. 49660 Project: Integns Metals
Owner: lntegris Metals Location: 527 Atando Ave., Charlotte, NC
Drilling CompanyGeologic Exploration Driller: Johnny Burr
Logged By: Thomas Hedrick Drilling Methoddfollow-Stem Auger
Surface Expression: Flush Mount Top of Casing Elevation: N/A
Total Depth:34 Hole Diameter: 4.25-inch Sampling Method:Ditect push; continuous macro
Comments: None. cores
TLV
Lithology
Blow
Depth
Description/Soil Classification
(ppm)
Unit
Count
(feet)
(Color, Texture, Structures)
— NA
Soil
NA
0-4
Six inches concrete; Brown to green silty CLAY,
feldspar present, no odor, plastic, slightly moist.
— 30
Soil
NA
4-8
Red to brown silty CLAY, no odor or staining, plastic,
dry.
— 32
Soil
NA
8 - 12
Tan silty CLAY, gas odor, no staining, plastic, dry,
crumbly.
— 25
Soil
NA
12 - 16
At 13 feet soil drastically changed to a gray, green,
white, and orange clayey SILT, strong odor, stained,
dry, slightly plastic, very crumbly.
— 40
Soil
NA
16 - 20
At 16 fat soil changed; Tan to brown silty CLAY, mild
vo or, no staining, plastic, dry, vains throughout.
— NA
Soil
NA
20 - 24
Dark brown to black silty CLAY, strong odor, no
staining, slightly moist, plastic.
— 32
Soil
NA
24 - 28
At 25 feet soil change; gray, green and white silty clay
with quartz sand parent, strong odor, staining, slightly
moist, slightly plastic.
NA=Not Applicable; ND=Not Detected
INTEGRIS METALS MW-1 Environmental
527 ATANW AVENUE DRILLING LOG AND MONITOR WELL to Resources
CHARLOTTE, NORTH CAROLINA CONSTRUCTION DIAGRAM ERM Management

t_
8" DIAMETER BOLT
DOWN WELL COVER
2' X 2' CONCRETE PAD WATER TIGHT, LOCKABLE
WELL CAP
NEAT CEMENT GROUT
TOP OF BENTONITE (FT.) 13
BOTTOM OF BENTONITE (FT.) 15
2'"DIA. SCH. 40 PVC RISER
PIPE, LENGTH
TOP OF SCREEN (FT.) 19
DEPTH TO
GROUND WATER (FT.) 1895 gy
SCHEDULE 40 .PVC THREADED
FLUSH JOINT 0.01" MILL SLOTTED
WELL SCREEN
WASHED SAND PACK
BOTTOM OF SCREEN (FT.) 34
TOTAL DEPTH OF BORING (FT.) 34 �/ PVC END CAP
BOREHOLE DIA. (IN.) 4.25
ERM-Southeast, Inc.
FDPJLLING LOG
Pegen "of Mw-2
Date: 01/03/03 Project No. 49660 Project: Integris Metals
Owner: Integris Metals Location: 527 Aland. Ave.. Charlotte, NC
Drilling CompanyGeologic Exploration Driller: Johnny Burt
Logged By: Thomas Hedrick Drilling Method:Hollow-Stem Auger
Surface Expression: Flush Mount Top of Casing Elevation: N/A
Total Depth:34 Hole Diameter: 4.25-inch Sampling Method: Direct push; continuous macro
Comments: None. cmes
TLV
Lithology
Blow
Depth
Description/Soil Classification
(ppen)
Unit
Count
(feet)
(Color, Texture, Structures)
— NA
Soil
NA
0-2
Teat inches concrete; tan silty CLAY, no odor or
staining, plastic, dry.
— NA
Soil
NA
2-3
Gray to green silty CLAY, gas odor, no staining, dry,
Plastic.
— NA
Soil
NA
3-4
Tan silty CLAY, no odor or staining, plastic, dry.
— 10
Soil
NA
4-8
Dark brown to red silty CLAY, at 5 feet mild odor,
plastic, no staining, slightly moist
— 12
Soil
NA
8 - 12
Same as above but is a lighter color and loses the red.
— 10
Soil
NA
12 - 16
At 13 feet soil change; Light can, orange to brown silty
CLAY, very plastic, no odor, no staining, dry.
— NA
Soil
NA
16 - 20
At 16 feet soil changed; soft grayish brown CLAY,
very plastic, slightly moist, no staining, gas odor,
quartz present.
— NA
Soil
NA
20 - 24
Same as above but there is an additional red color.
— NA
Soil
NA
24 - 28
Same as above; mica present, very moist.
— 40
Soil
NA
28 - 32
Same as above.
NA=Not Applicable; NO = Not Detected
INTEGRLS METALS Mw-2 Environmental
527 ATANDO AVENUE DMLING LOG AND MONITOR WELL to Resources
CHARLOTTE, NORTH CAROLINA CONSTRUCTION DIAGRAM LRM Management

sobumWaILM: z/14/os 1-1
8" DIAMETER BOLT
DOWN WELL COVER
2' X 2' CONCRETE PAD WATER TIGHT, LOCKABLE
WELL CAP
NEAT CEMENT GROUT
TOP OF BENTONITE (FT.) - 13 — —
ICI BOTTOM OF BENTONITE (FT.) 15 —
-22DIA. SCH. 40 PVC RISER
'. PIPE, LENGTH
TOP OF SCREEN (FT.) 17
DEPTH TO
GROUND WATER (FT.) 1365 _
SCHEDULE 40 PVC THREADED
FLUSH JOINT 0.01" MILL SLOTTED —
WELL SCREEN
WASHED SAND PACK —
BOTTOM OF SCREEN (FT.) 32
TOTAL DEPTH OF BORING (FT.) 33 �/ PVC END CAP
BOREHOLE DIA. (IN.) 8.25
ERM-Southeast, Inc.
DRILLING LOG
Boring No. MW-3
Page 1 of I
Date: 01/22/03 Project No. 49660 Project: Integris Metals
Owner: Integris Metals - Location: 527 Atando Ave., Charlotte, NC
Drilling CompanyGeologic Exploration Driller: Mark GeMs
Logged By: Thomas Hedrick Drilling MethodAir/Hollow-Stem Auger
Surface Expression: Flush Mount Top of Casing Elevation: N/A
Total Depth.32 Hole Diameter: 5.25-inch Sampling Method:None.
Comments: None.
TLV
Lithotogy
Blow
Depth
Description/Soil Classification
(ppm)
Unit
Count
(feet)
(Color, Texture, Structures)
— NA
Soil
NA
0-5
Brown to red CLAY, no odor or staining,
very plastic, moist.
— NA
Soil
NA
5 - 10
Brown to red silty CLAY, mica and feldspar present
(feldspar white clay), no odor or staining, moist, plastic.
— NA
Soil
NA
10 - 15
Same as above.
— NA
Soil
NA
15 - 20
Same as above.
— NA
Soil
- NA
20 - 25
Same as above.
— NA
Soil
NA
25 - 30
Same as above.
NA=Not Applicable; ND=Not Detected
INTEGRIS METALS MWW3 Environmental
527 ATANW AVENUE DRILLING LOG AND MONITOR WELL to Resources
CHARLOTTE, NORTH CAROU NA CONSTRUCTION DIAGRAM ERM Management

yooUMw4.Uwc [/14/W 1-1
2' X 2' CONCRETE PAD
NEAT CEMENT GROUT
TOP OF BENTONITE (FT.) 13
BOTTOM OF BENTONITE (FT.) 15
_'DIA. SCH. 40 PVC RISER
PIPE, LENGTH
TOP OF SCREEN (FT.) 17
8" DIAMETER BOLT
DOWN WELL COVER
WATER TIGHT, LOCKABLE
WELL CAP
" n o
DEPTH TO
GROUND WATER (FT.) 1585
SCHEDULE 40 PVC THREADED —
FLUSH JOINT 0.01" MILL SLOTTED
WELL SCREEN
WASHED SAND PACK
BOTTOM OF SCREEN (FT.) 32
TOTAL DEPTH OF BORING (FT.) 32
BOREHOLE DIA. (IN.) 8.25
PVC END CAP
ERM-Southeast, Inc.
DRILLING LOG
N MW -4
r. l" of
Date: 01n1/03 Project No. 49660 Project: Integm Metals
Owner•. Integris Metals London: 527 Atando Ave.. Charlotte NC
Drilling ConpanySGwlogic Exploration Driller. Jason Mantak
Logged By: Thomas Hedrick Drilling Method:Air Rotary
Surface Expression: Flush Mount Top of Cuing Elevation: N/A
Total DeptA:32 Hole Dlameter:8.25-inch Sampling Method: None.
Comments: None.
TLV
I Litho1o0
Blow
Depth
DeschiptiaNSuB Clu,dicalio,
(pp.)
Unit
Count
(feet)
(Color, Texture, Structures)
— NA
Soil
NA
0.5
Bmwa to red CLAY, no odor or staining,
very plastic, moist.
— NA
Soil
NA
5.10
Brown to tan silty CLAY, dry,
no odor or staining, plastic.
— NA
Soil
NA
10- 15
Same as above.
— NA
Soil
NA
15 - 20
Same as above with rock fragments 20- 30 too, schist.
— NA
Soil
NA
20- 25
Same as above, no rock fragments.
— NA
Sail
NA
25 - 30
Same as above. _
NA —Not Applicable; ND=Nat Detected
INTEGRIS METALS MW-4 Environmental
527 ATANW AVENUE DRILLING LOG AND MONITOR WELL No Resources
CHARLOTTE, NORTH CAROLINA CONSTRUCTION DIAGRAM ERM Management

HppUMWJ.UW4 L/14/DS lal
2' X 2' CONCRETE PAD
NEAT CEMENT GROUT
TOP OF BENTONITE (FT.) 13
BOTTOM OF BENTONITE (FT.) 15
2 "DIA. SCH. 40 PVC RISER
PIPE, LENGTH
TOP OF SCREEN (FT.) 17
8" DIAMETER BOLT
DOWN WELL COVER
WATER TIGHT, LOCKABLE
r-- WELL CAP
4 e V
DEPTH TO
GROUND WATER (FT.) 1195 1
SCHEDULE 40 PVC THREADED -
FLUSH JOINT 0.01" MILL SLOTTED
WELL SCREEN
WASHED SAND PACK
BOTTOM OF SCREEN (FT.) 32
TOTAL DEPTH OF BORING (FT.) 33
BOREHOLE DIA. (IN.) 8.25
PVC END CAP
ERM-Southeast, Inc.
r DRILLING LOG
n N W-5
Pag of 1
Date: 01/22/03 project No.
49660
project: Integrls Metals
Owner: Integris Metals
Location: 527 Alando Ave. Charlotte NC
Drilling Companys0cologic Exploration
Driller: Mark Gettys
Logged By: Thomas Hedrick
Drilling Method: in`Hollow-Stem Auger
Surface Expression: Flush Mount
Top of Casing Elevation: N/A
Total Depth:32 Hole Diameter: 8.25-inch
Sampling Method: None.
Comments• None.
TLV
Lithology
Blow
Depth
Description/Soil Classification
(ppm)
Unit
-Count
(feet)
(Color, Texture, Structures)
— NA
Soil
NA
0-5
Brown to red CLAY, no odor or staining,
very plastic, moist.
— NA
Soil
NA
S. 10
Brown to red silty CLAY, mica present,
no odor or staining, dry, plastic.
—NA
Soil
NA
10-15
Same as above but moist.
— NA
Soil
NA
15 - 20
Same as above.
—NA
Soil
NA
20-25
Some as above.
—NA
Soil
I NA
1 25-30
Same as above.
NA=Not Applicable; ND=Not Detected
INTEGRIS METALS Mw-5 gj Environmental
527 ATANDO AVENUE DRMLING LOG AND MONITOR WELL Resources
CHARLOTrrE, NORTH CAROLINA CONSTRUCTION DIAGRAM ERM Management

2" WATER TIGHT LOCKABLE 8" DIAMETER BOLT
WELL CAP /-DOWN WELL COVER
2' X 2' CONCRETE
PAD
NEAT CEMENT GROUT
UPPER WELL —
GORE DIA. (IN.) 8.25
6" PVC SURFACE -
CASING TO (FT.) 80
DEPTH TO
GROUNDWATER (Ff.)12.14
SCHEDULE 40
PVC RISER
DIAMETER (IN.) 2
LOWER WELL BORE
DIAMETER (IN.) 8.25
TOP OF BENTONITE (FT.) 77
BOTTOM OF
BENTONITE (FT.) 79
WASHED SAND
PACK
TOP OF SCREEN (FT.) 81 —
SCHEDULE 40 PVC THREADED
FLUSH JOINT .010" MILL —
SLOTTED WELL SCREEN
BOTTOM OF SCREEN (FT.) 86
PVC END CAP
BORING (FT.) OF (FT) 88
ERM-Southeast, Inc. DRILLING LOG Pa en¢ N of DI - I
Date: 01/21/03 ProjectNo. 49660 Project: Integris Metals
Owner: Integris Metals Location: 527 Atando Ave., Charlotte NC
Drilling Companyf3eologic Exploration Driller: Jason Mantak
Lagged By: Thomas Hedrick Drilling Method:Air Rotary
Surface Expression: Flush Mount Top of Casing Elevation: N/A
Total Depth:86 Hole Diameter: 8.25-inch Sampling Method:None.
Comments: None.
TLV
Lithology
Blow
Depth
Descriptiou/Soil Classification
(ppm)
Unit
Count
(feet)
(Color, Texture, Structures)
— NA
Soil
NA
0-5
Brown to red CLAY, no odor or staining,
very plastic, moist.
— NA
Soil
NA
5 - 10
Brown to tan silty CLAY, dry,
no odor or staining, plastic.
— NA
Soil
_ NA
10 - 15
Same as above.
— NA
Soil
NA
15 - 20
Same as above with rock fragments 20 - 30 cm, schist.
— NA
Soil
NA
20 - 25
Same as above, no rock fragments.
— NA
Soil
NA
25 - 30
Same as above.
— NA
Soil
NA
30 - 35
Same as above, rock fragments 5 - 10 can.
— NA
Soil
NA
35 - 40
Gray to green soil, homblend, quartz, schist to gniess.
— NA
Soil
NA
40 - 85
Same as above.
NA=Not Applicable; ND=Not Detected
INTEGRIS METALS DW-1 NJ Environmental
527 ATANDO AVENUE DRILLING LOG AND MONITOR WELL Resources
CHARLOTTE, NORTH CAROLINA CONSTRUCTION DIAGRAM ERM Management

WELL CONSTRUCTION RECORD
North Carolina - Department of Environmental and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRACTOR (INDIVIDUAL) NAME (print) JOHNNY BURR CERTIFICATION # 3098
WELL CONTRACTOR COMPANYNAvlE GEOLOGIC EXPI.ORATIoN INC. PHONE # [phone]
STATE WELL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT#
(if applicable) (if applicable)
1. WELL USE (Check Applicable Box): Residential ❑ MunicipaVPublic ❑ Industrial ❑ Agricultural ❑
Monitoring ® Recovery ❑ Heat Pump Water Injection ❑ Other[] If Other, list Use
2. WELL LOCATION:
Neatest Town: CHARLOTTE County MECKLENBURG
527 ATANDO AVE.
(Street Name, Numbers, Community, Subdivision, Lot No., Zip Code)
3.OWNER: wTEGRISMETALS.wC
Address 527 ATANDO AVE.
(Street or Route No.)
CHARLOTTE NC
Cm or Toxin State Zin Code
Area Cade -Phone Number
4. DATE DRILLED 1-2-03
5. TOTAL DEPTH: 35.o FEET
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
7. STATIC WATER LEVEL Below Top of Casing: 21.0 FT.
(Use "+- if Above Top of Casing)
8. TOP OF CASING IS 0.o FT. Above Land Surface*
*Top of casing terminated at/or below laud surface requires a
variance in accordance, with 15A NCAC 2C .0118.
9. YIELD (gpm): NSA METHOD OF TEST N/A
10. WATER ZONES (depth): N/A
11. DISINFECTION: Type N/A Amount
12. CASING: Wall Thickness
Depth Diameter or Weight/Ft. Material
From 0.0 To 19.0 Ft 2INCH SCH 40 PVC
From To Ft.
From To Ft.
13. Grout: Depth Material Method
From _ _ 0.0 To 13.0 FL Portland Beotoma, Slmry
From
To
Ft.
14. SCREEN:
Depth
From 19.0
To 35.0
F
From
To
Fi
15. SAND/GRAVEL PACK:
Depth
From I5.0
To 35.0
Ft
From
To
Ft
Diameter Slot Size Material
2.0 in. .010 in PVC
N. N
Size Material
2040 FINE SBJCA SAND
Topographic/Land setting
❑ Ridge ❑ Slope ❑ Valley ® Flat
(check appropriate box)
Latitude/longitude of well location
(degrees/mmutes/secaods)
Latitude/longitude source: ❑ GPS ❑ Topographic map
(check box)
PEETH DRILLING LOG
From To Formation Description
0.0 4.0 TAN CLAY WITH COBBLES
4.0 8.0 RED CLAY
8.0 21.0 TAN/RED CLAY
21.0 35.0 GREEN CLAY WITH COBBLES
LOCATION SKETCH
Show direction and distance in miles from at least
two State Roads or County Roads, inculed the road
numbers and common road names.
16. REMARKS: MW-1 BENTONITE SEAL FROM 13.0 TO 15.0 FEET
I DO NEARBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STANDARD/SS,, AND THAT
.
HAST A COPY OOFFyrTHIS RECORD HAS BEEN PROMDED TO THE WELL O`
da,4 B (.4A1/ k
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC
27699-1636 Phone No. [phone], within 30 days. GW-1 REV. 072001

WELL CONSTRUCTION RECORD
North Carolina - Department of Environmental and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME (print) jGHNNY BURR CERTIFICATION # 3098
WELL CONTRACTOR COMPANY NAME GEOLOGIC EXPLORATION, INC. PHONE # [phone]
STATE WELL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT#
(if applicable) (if applicable)
1. WELL USE (Check Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring ® Recovery ❑ Heat Pump Water Injection ❑ Other[] If Other, list Use
2. WELL LOCATION: Topo&mPhic/L it setting
Nearest Town: CHARLOTTE County MECKLENBURG ❑ Ridge LJ Slope ❑ Valley ® Flat
527 ATANDO AVE. (check appropriate box)
(Strat N®, Numbers, Community, Subdivision, Lot No., Zip Cade) Latitude/longitude of well location
3. OWNER: mTEGRis METALs, INC.
Address 527 ATANDO AVE.
(Street or Rare No.)
CHARLOTTE NC
ON Or Town Statc Tn Cade
Arco Code -Phone Number
4. DATE DRILLED 1-3-03
5. TOTAL DEPTH: 35A FEET
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
7. STATIC WATER LEVEL Below Top of Casing: 21.0 FT.
(Use-+ ifAbow Top ofCasimg)
S. TOP OF CASING IS o.o FT. Above Land Surface*
'Top ofming teminated atIm below Imd surface regimes a
waiame in aaordavice with 15A NCAC 2C .0118.
9. YIELD (gpm): N/A METHOD OF TEST WA
10. WATER ZONES (depth): N/A
11. DISINFECTION: Type
N/A
Amount
12. CASING:
Wall Thickness
Depth
Diameter or Weight/Ft Material
From 0.0
To 19.0
Ft
2INCH SCH 40 PVC
From
To
FL
From
To
Ft
13. Grout:
Depth
Material Method
Fmm 0.0
To 13.0
FL
Portland Bentnmite Slurry
From
To
FL
14. SCREEN:
Depth
Diameter Slot Size Material
From 19.o
To 35.0
Ft.
2.0 in. .010 in PVC
From
To
Ft
in. in
15. SAND/GRAVEL PACK:
Depth
Size Material
From 15.0
To 35.0
Ft
2040 FINE SILICA SAND
From
To
Ft.
(degrees/minutes/seconds)
Latitudellongitude source: ❑ GPS ❑ Topographic map
(chat box)
DEPTH DRILLING LOG
From To Formation Description
0.0 5.0 TAN CLAY WITH COBBLES
5.0
8.0
8.0
21.0
21.0
35.0
RED CLAY
TAN/RED CLAY
TAN CLAY
LOCATION SKETCH
Show direction and distance in miles from at least
two State Roads or County Roads, inculed the road
numbers and common road names.
16. REMARKS: MW-2 BENTONrrE SEAL FROM 13.0 TO 15.0 FEET r
I DO NEARBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH I SA NCAC 2C, WELL
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC
27699-1636 Phone No. [phone], within 30 days. GW-1 REV. 072001

WELL CONSTRUCTION RECORD
North Carolina - Department of Environmental and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME(print) MARKGETTYS CERTIFICATION# 2345
WELL CONTRACTOR COMPANY NAME Geologic Exploration, Inc. PHONE # [phone]
STATE WELL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT#
(if applicable) (ifapplicable)
1. WELL USE (Check Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring ® Recovery ❑ Heat Pump Water Injection ❑ Other❑ If Other, list Use
2. WELL LOCATION:
Nearest Town: CHARLOTTE County MECKLENBURG
527 ATANDO AVENUE
(Street Name, Numbers, Conn aunty, Subdivision, Lot No., Zip Code)
3.OWNER: INTEGRiswTAL5 Roc.
Address 527 ATANDO AVENUE
(Sow or Route No.)
CHARLOTTE NC
CiwrnTnwn State Zin Code
Area Cade -Phone Number
4. DATE DRILLED olrz2/o3
5. TOTAL DEPTH: 32.o FEET
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
7. STATIC WATER LEVEL Below Top of Casing: 15.0' FT.
(Use "+^ if Above Top of Casing)
8. TOP OF CASING IS o.o FT. Above Land Surface*
•Top Ofmtingterminated ayor below land surface requires a
vmiaace in accordance with 15ANCAC 2C.oI18.
9. YIELD (gpm): N/A METHOD OF TEST N/A
10. WATER ZONES (depth): N/A
11. DISINFECTION: Type
N/A
Amount
12. CASING:
Wall Thickness
Depth
Diameter or Weight/Ft.
Material
From 0.0
To 17.0
Ft
2INCH SCH 40
PVC
From
To
Ft
From
To
Ft.
13. Grout:
Depth
Material
Method
From 0.0
To Do
Ft
Pordandnentonite
Slimy
From
To
Ft
14. SCREEN:
Depth
Diameter Slot She
Material
From 17.0
To 32.0
Ft.
2.0 in. .010 in
PVC
From
To
Ft
in. ht
15. SAND/GRAVEL PACK:
Depth
Size Material
From 15.0
To 32.0
Ft.
20-40 FINE SILICA SAND
From
To
Ft.
Topographic(Land setting
❑ Ridge ❑ Slope ❑ Valley ® Flat
(check appropriate box)
Latitude/longitude of well location
(degrees/minutes/seoonds)
Latitude/longitude source: ❑ GPS ❑ Topographic map
(cheek box)
DEPTH DRILLING LOG
From To Formation Description
0.0 32.0 TAN SANDY SILTY CLAY
LOCATION SKETCH
Show direction and distance in miles from at least
two State Roads or County Roads, inculed the road
numbers and common road nsmec.
16. REMARKS: MW-3 BENTONITE SEAL FROM 13.0 TO 15.0 FEET
I DO HEARBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
UM
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC
27699-1636 Phone No. (919) 733-322I, within 30 days. GW-I REV. 072001

WELL CONSTRUCTION RECORD
North Carolina - Department of Environmental and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME (print) JASONMANTAK CERTIFICATION# 2580
WELL CONTRACTOR COMPANY NAME Ecologic Explorwoo, Inc. PHONE # [phone]
STATE WELL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT#
(ifapplimble) (ifapplicable)
1. WELL USE (Check Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring ® Recovery ❑ Heat Pump Water Injection ❑ Other[] If Other, list Use
2. WELL LOCATION:
Nearest Town: CHARLOTTE County MECKLENBURG
527 ATANDO AVENUE
(Street Name, Numbers, Community, Subdivision, Lot No., Zip Cade)
3. OWNER: DnEGRJS METALS, INC.
Address 527ATANDOAVENUE
(Street or Route No.)
CHARLOTTE NC
Ciwor`f w state Lo Code
1 )
Area Cade -Phone Number
4. DATE DRILLED olr2lro3
5. TOTAL DEPTH: 32.0 FEET
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
7.STATIC WATER LEVEL Below Top o£Casing: ls.n FT.
(Use-+ if Above Top of Casing)
8. TOP OF CASING IS o.o FT. Above Land Surface*
-Top of cadngterminzted atlor below land surface requires a
variance in accordance with 15A NCAC 2C.0118.
9. YIELD (gpm): NIA METHOD OF TEST N/A
10. WATER ZONES (depth): NIA
11. DISINFECTION: Type
N/A
Amount
12. CASING:
Wall Thickness
Depth
Diameter or WeightlFt.
Material
From 0.0
To 17.0
Fr
2INCH SCH 40
PVC
From
To
Ft
From
To
Ft.
13. Grout:
Depth
Material
Method
From 0.0
To 11.0
Ft.
Portland Bentwite
Slurry
From
To
Ft
14. SCREEN:
Depth
Diameter Slot Size
Material
From 17.0
To 32.0
Ft.
2.0 in. .010 in
PVC
From
To
Ft.
in. in
15. SAND/GRAVEL PACK:
Depth
Size Material
From 15.0
To 32.0
Ft
2040 FINE SILICA SAND
From
To
Ft
TopographiefLand setting
❑ Ridge ❑ Slope ❑ Valley ® Flat
(check appropriate box)
LatitudeAca gitude of well location
(degrees/minutes/secmds)
Latitudellongitude source: ❑ GPS ❑ Topographic map
(checkbox)
DEPTH DRILLING LOG
From To Formation Description
0.0
1.0
1.0
20.0
20.0
32.0
ASPHALT/GRAVEL
YELLOW CLAY
YELLOW CLAY WITH
WEATHERED ROCK
LOCATION SKETCH
Show direction and distance in miles from at least
two State Roads or County Roads, inculed the road
ntanbers and common road names. �tv
\eQ i Sx
16. REMARKS: MW4 13ENTOMITE SEAL FROM 11.0 TO 15.0 FEET
I DO HEARBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCWN STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC
27699-1636 Phone No. [phone], within 30 days. - GW-1 REV. 07/2001

WELL CONSTRUCTION RECORD
North Carolina - Department of Environmental and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME (print) MARKGETTYS CERTIFICATION# 2345
WELL CONTRACTOR COMPANY NAME Geolope Exploration, lac. PHONE # [phone]
STATE WELL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT#
(if applicable) (ifapplicable)
1. WELL USE (Check Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring ® Recovery ❑ Heat Pump Water Injection ❑ Other[] If Other, list Use
2. WELL LOCATION:
Nearest Town: CHARL077E County MECKLENBURG
527 ATANDO AVENUE
(Shut Nmne, Ntanbers, Community, Subdivision, Lot No., Zip Code)
3. OWNER: wrEGRIS METALS, INC.
Address 527 ATANDO AVENUE
(Strut or Route No.)
CHARLOTTE NC
CiN orTmvn Stare Zin Co&
Area Cade - Phone Number
4. DATE DRILLED o1/2yo3 -
5. TOTAL DEPTH: 32.0 FEET
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
7.STATIC WATER LEVEL Below Top o£Casing: 15.0 FT.
(Use .+.. ifAbove Top of Casing)
8. TOP OF CASING IS o.o FT. Above Land Surface -
*Top of casing to r ivated at/or below land s rf= requires a
variance in accordance with 15A NCAC 2C .0118.
9. YIELD (gpm): N/A METHOD OF TEST N/A
10. WATER ZONES (depth): N/A
11. DISINFECTION: Type N/A Amount
12. CASING: Wall Thickness
Depth Diameter or Weight/Ft. Material
From 0.0 To 17.0 Ft 2INCH SCH 40 PVC
From To Ft..
From To Ft
13. Grout: Depth Material Method
From 0.0 To 13.0 FL Portland Bmronite slurry
Form To Ft.
14. SCREEN: Depth Diameter Slot Size Material
From 17.0 To 32.0 Ft. 2.0 in. .010 in PVC
From To Ft. in. in
15. SAND/GRAVEL PACK:
Depth Size Material
From 15.0 To 32.0 FL 2040 FINE SILICA SAND
Front -To Ft.
Topographic(Land setting
❑ Ridge ❑ slope ❑ valley ® Flat
(check appropriate box)
LatitudeAongimde of well location
(degees/mtnutes/secouds)
Latitude/longitude source: ❑ GPS ❑ Topographic map
(cheek box)
DEPTH DRILLING LOG
From To Formation Description
0.0 32.0 ORANGE SANDY CLAY
LOCATION SKETCH
Show direction and distance in miles from at least
two State Roads or County Roads, inculed the road
numbers and common road names.
16. REMARKS: MW-5 BENTONITE SEAL FROM 13.0 TO 15.0 FEET
1 DO HEARBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL
CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
10CIL A4"
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC
27699-1636 Phone No. [phone], within 30 days. GW-1 REV. 07/2001

WELL CONSTRUCTION RECORD
North Carolina - Department of Environmental and Natural Resources - Division of Water Quality - Groundwater Section
WELL CONTRACTOR (INDIVIDUAL) NAME (print) JASON MANTAK CERTIFICATION # 2580
WELL CONTRACTOR COMPANY NAME Geologic Exploration, Inc. PHONE # [phone]
STATE WELL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT#
(if applicable) (ifapplimble)
1. WELL USE (Check Applicable Box): Residential ❑ Municipal/Public ❑ Industrial ❑ Agricultural ❑
Monitoring ® Recovery ❑ Heat Pump Water Injection ❑ Other❑ If Other, list Use
2. WELL LOCATION:
Nearest Town: CHARLOTTE County MECKLENBURG
527 ATANDO AVENUE
(Street Namc, Numbers, Community, Subdivision, Lot No., Zip Code)
3. OWNER: INTEGRIs METALS, INc
Address 527 ATANDO AVENUE
(Street or Route No.)
CHARLOTTE NC
Ciwor Town State Zin Code
( )
Arta Code - Phone Number
4. DATE DRILLED 0120/03-0121103
5. TOTAL DEPTH: 86.o FEET
6. DOES WELL REPLACE EXISTING WELL? YES ❑ NO
7. STATIC WATER LEVEL Below Top of Casing: la.n Fr.
(Use"+ if Above Top of Casing)
8. TOP OF CASING IS on FT. Above Land Surface*
OTop of casing terminated Wor below land surface requires a
vmiance in acwrdaoce with 15A NCAC 2C .0118.
9. YIELD (gpm): N/A NIETHOD OF TEST N/A
10. WATER ZONES (depth): N/A
11. DISINFECTION: Type
N/A Amount
12. CASING:
Wall Thickness
Depth
Diameter or Weigbt/Ft.
Material
From 0.0
To 81.0
Ft 2INCH SCH 40
PVC
From 0.0
To 78.0
Ft. 6518 INCH .188
GZV.
From
To
FL
13. Grout:
Depth
Material
Method
From 0.0
To 75.0
Ft. Portland Bentonite
Slurry
Fmm 0.0
To 78.0
Ft. Po land Bentonite
Sluny
14. SCREEN:
Depth
Diameter Slot Sim
Material
From 81.0
To 86.0
Ft. 2.0 m. .010 in
PVC
From
To
FL in. in
15. SAND/GRAVEL PACK:
Depth
Size Material
From 79.0
To 86.0
Ft. 2040 FINE SILICA SAND
From
To
Ft.
Topographic(Land setting
❑ Ridge ❑ Slope ❑ Valley ® Flat
(check appropriate box)
LatitudcAongitude of well location
(degreestminuleshemnds)
Latitude/longitude source: ❑ GPS ❑ Topographic map
(check bar)
DEPTH DRILLING LOG
From To Formation Description
0.0 1.0 Asphalt(Gravel
LO 23.0 Red/Brown Clay
23.0 3 LO Brown Clay with Weathered Rock
31.0 52.0 Brown Weathered Rock
52.0 70.0 Grey Weathered Rock
70.0 86.0 Grey Fractured Rock
LOCATION SKETCH
Show direction and distance in miles from at least
two State Roads or County Roads, inculed the road
numbers and common road names. X
16. REMARKS: DW-I BENTONITE SEAL FROM 75.0 TO 79.0 FEET
I DO NEARBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH ISA NCAC 2C, WELL
CONSTRUCTJON STANDARDS, AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER
Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC
27699-1636 Phone No. [phone], within 30 days. .. GW-1 REV. 072001

Appendix B
Standard Operating Procedures

SOIL SAMPLING AND ANALYSIS
Geoprobe Drilling/Sampling
The uppermost 4 to 8 feet of each boring were advanced using a 3.5-
inch stainless steel hand auger as a precaution against damaging
underground structures. Geoprobe soil samples were collected using
a 1.5-inch macro -core sampling tube lined with a plastic sleeve.
Continuous samples were collected in 4-foot intervals. New plastic
liners were used for each sample interval. Drilling and sampling
equipment were decontaminated using steam cleaning equipment
between borings.
Hollow Stem Auger Drilling/Sampling
Soil and saprolite aquifer monitor well borings at the site were
advanced using hollow stem auger drilling equipment or using a
hand auger. The sampling equipment was cleaned prior to, and
between each use by scrubbing with phosphate -free detergent,
rinsing in tap water, and rinsing again with distilled water.
Hollow stem auger soil samples were collected using a 2-inch
outside diameter stainless steel split spoon sampler. A 140 pound
hammer was used to drive the sampler through the sampling
interval and the blow count for each 6-inch interval was recorded.
Standard penetration testing and soil sampling were conducted in
accordance with ASTM D 1586 methods and procedures. Soil
samples were collected at 5-foot intervals above the water table.
Field Logging and Laboratory Analysis
Soil samples were visually inspected and the physical characteristics
logged upon retrieval of the sample from the soil boring.
All of the soil samples were retained for laboratory analysis by the
applicable methods specified in NCDENR soil and ground water
assessment guidelines (1/2/1998). Laboratory analyses were
conducted by Specialized Assays Environmental of Nashville,
Tennessee. Specialized Assays Environmental is a North Carolina
approved laboratory. Sample collection, handling, and preservation
were conducted in accordance with accepted protocol, including
chain -of -custody documentation.
Exxon Mobi1\4-3524\LSA 2000\StdProcedures.doc

Type III Monitor Well
The upper portion of the Type III well boring was advanced using
air hammer drilling equipment. A 6-inch diameter galvanized steel
casing was installed within a 10-inch nominal diameter boring and
tremie grouted in place. The casing grout was allowed to cure for a
period of approximately 24 hours prior to continuing the well
boring.
The lower portion of the well boring was advanced using mud
rotary drilling methods. Upon reaching the total depth of the well,
2-inch schedule 40 PVC well construction materials were placed in
the boring and grouted in place. The bentonite slurry is displaced
from the borehole during installation of the monitor well materials.
The surface completion of the Type III well was as for the Type II
monitor wells.
The location and elevation of the each top of well casing was
surveyed using a survey theodolite.
Monitor Well Development/PurgingMethods
Following installation, the monitor wells were developed by
removing a minimum of five well bore volumes of water by
pumping or bailing. For wells characterized by a slow recharge
rate, the well was pumped/bailed dry prior to sampling.
C il-IPIIl5'/YI$d&%'►AVIVA.)► it IIli'6Yh9
Following well development/purging, ground water samples were
collected from the site monitor wells using disposable plastic
bailers. The bailers were lowered into each well using new nylon
rope. Ground water elevation data were obtained an electronic depth
to water meter.
Ground Water samples were analyzed by the appropriate methods
specified in NCDENR soil and ground water assessment guidelines
(March 1993 and January 1998). Laboratory analyses were conducted
by Specialized Assays Environmental of Nashville, Tennessee.
Sample collection, handling, and preservation were conducted in
accordance with accepted protocol, including chain -of -custody
documentation.
Emmn Mobil\4-3524\LSA 2000\StdProcedures.doc

Appendix C
Disposal Manifests

HAZ-MAT
TRANSPORTATION AND DISPOSAL
P. O. BOX 37392 w CHARLOTTE, N,C. 2a237
f704 332-5600
FAX [phone]
NON -HAZARDOUS SPECIAL WASTE
NAME V it i�
ORIGINATING ADDRESS
MAILING C ADDRESS�t �
CITY l� 1 r STATE 1 (— ZIP
DES. OF WASTE:
WORK CONTRACTED By
Bill To (If different from Irdoe arum at left)
NAMI
ADDF
CRY
PHOt
CONI
1. WATER, OIL & COOLANT PUMPED FROM TANKS OR DRUMS
7- OFF SPEC LIGHT OIL, WATER & GAS PUMPED FROM TANKS OR DRUMS
3. 55 GALLON DRUMS REMOVED - SOLID
4. 55 GALLON DRUMS REMOVED - LIQUID
S.
s.
7.
8.
9. SERVICE CHARGE
10. TRANSPORTATION
13706
Manifest No.
P.O. No.
Job No. Qic -3,2 "'�
GENERATORS CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been prepedy
described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, If the waste is a treatment residue of a previously restricted
hazardous waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has been treated in accordance with the requirements of 40 CFR Part 268 and is no longer
a hazmtou�s waste as defined py 40 CFR Part 261. 1
Generator Authorized Agent Mach Signature 1/1 Shipment Data
HAZ- MAT TRANSPORTER II
TRANSPORTATION AND DISPOSAL e. Name
P. O. BOX 37392 • CHARLOTTE, N.C. 28237 f. Address
a Driver Name //Thle - �c+/✓ ford � i (r £
b. Phone No.7��32 j� Oy c. Truck No.—S
Hazardous Waste Transporter Permits
EPA
Site Name: Hez-Mat Transportation & Disposal. Inc.
Physical Address: 210 Dalton Avenue
Charlotte. N.C. 28237
e. Discrepancy Indication Space
This Is to anOy, OW all nor -hazardous material removed from above location has been received and will be disoos¢d of
am blended [ribs beneficial reusable fuel for use In large industrial burners. (2 Wade waters are to be treated with polyn
GiantMta the CMUD sanitation sewer system under permit IUP/5012. (1) Sludges from treatment systems are
(4) Our trail ent system operates on a first in, first out basis and product should be processed within seven days.
g. Driver Name / Title—
h. Phone No.
j. Transporter II Permit Nos.
a. Phone No.
b. Maiing Address:
proper
I. Truck
ORIGINAL. FIRALLS.D. - YELLOW-DIS OVER - PINK-18TLS.D. - SOLD -GENERATOR r'

HAZ-MAT 1.3419
TRANSPORTATION AND DISPOSAL ManBest No.
P. O. BOX 37392 • CHARLOTTE, N.C. 28237
(704 332-5600 P.O. No.
FAX (7�4) 375-7183 �j
NON -HAZARDOUS SPECIAL WASTE Job No. C/� 3a[ 2�
GENERATOR LOCATION�+
WORK CONTRACTED BY
NAME ".���Jy! y'—l^
— ca /s`�i
BIII To (If different from information at
left)
r
ORIGINATING ADDRESS 1 iA&L'1:.� "_47y-C_
'—
NAME C� 'r/�/,.
MAILING ADDRESS
�,���
ADDRESS D—CTIMl
V
Kam^',(
CITY - —STATE ZIP
`3 .l
CITY r 1`o �
sTT AATT'ErLP
PHONE NO.
,l.=pU
t'
PHONE NO.1,,,,�
CONTACTNAME -
tL,�
CONTACT NAME9=R=t=
DES. OF WASTE: r(1� 6!%RTt/' C *- rJ�CJ.e.�:3'&SC
N o.
jiil
ype
j
)[� )
n—Its' Quantity
Y. WATER, OIL & COOLANT PUMPED FROM TANKS OR DRUMS
2 OFF SPEC LIGHT OIL, WATER & GAS PUMPED FROM TANKS OR DRUMS
S. 55 GALLON DRUMS REMOVED - SOLID
4. 55 GALLON DRUMS REMOVED - LIQUID
8.
9. SERVICECHARGE
10. TRANSPORTATION
GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been property
described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, If the waste is a treatment residue of a previously restricted
hazardous waste subject to the Land Disposal Restrictions, 1 certfy and warrant that the waste has been treated in rdance with the requirements of 40 CFR Part 268 and is no longer
a hazardous waste as define by 40 CFR Part 2e61.
ou^1
1 I `ir � r� �t_Ae�YRe 4Y x � s!l� r O 1
Generator Aumodze0 Ag— enl�ame- J � . Signature Shipment Date
HAZ-MAT
TRANSPORTATION AND DISPOSAL -
P. O BOX 37392 • CHARLOTTE, N.C. 28237
& Driver Name / Title
L -'g�
b. Phone N - c. Truck No.
Hazardous Waste Transporter Permits
TRANSPORTER II
e. Name
g. Driver Name /
h. Phone No. I. Truck No.
1. Transporter II Permit Nos.
Site Name: Haz-Mat Transportation-& Disposal. Inc. a.'Phohe No. 704-332-5600,
Physical Address: 210 Dalton Avenue b. Maiing Address: P.O. Box 37392
Charlotte, N.C. 28237 -:>` Charlotte. N.C. 28237
e. Discrepancy Indication Space
This Is to mNty that all non -hazardous material removed from above location has been received and will be disposed of in acardance with applicable local, state and federal regulations In N8 following manner. (1) Petroleum produols'
8e blended Imo a beneficial reusable fuel for use in large Industrial burners. (2Waste waters am to be treated with polymers, oN adjusters, and a fldsulanL then flows through a dissohed air Rotation system for pmllretmem separdlon;
than Into Me CMUD sanitation sewer system under permit IUPi5012. 11) Sludges from treatment systems are Muted to E.P.A. approved fzcittles for proper disposal. Marital and Carillons of disposal are on file.
(4) Our keatmenl system operates on a firifin, first out basis and product should be processed within seven days.
SIGNATURE OF FACILITY AGEINrT DATE �$y
ORIGINAL -FINAL T.S.D. • YELLO ISPOSER • PINK-18TL8.0. • GOLD -GENERATOR

Appendix D
Limited Site Assessment
Laboratory Analytical Data
Sheets

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Lab Report
rin
PRISM
u eowm ms
w s.nw � n D.menw sawom
1/16/03
Page 2 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanavechia
Customer Sample
ID: MW-1 @ 5
7300 Carmel Exec. Park Ste. 200
Prism Sampfe ID:
AC68589
Charlotte, NO 28226
Login Group:
5149K7
Sample Collection Date7Tlme:
1/2/03
11:00
Lab Submittal Dalerrime:
1/6/03
08:00
The following analytical results have been obtained
for the
indicated sample which was submitted
to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEITIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
1,1-DICHLOROETHENE
Not detected
ug/kg
5.0
8260815035
IN/0301:54
KC
CIS-1,2-0ICHLOROETHENE
Not detected
ugAg
5.0
8260815035
10030154
KC
TRANS-I,2-0ICHLOROETHENE
Not tlelectetl
u91kg
5.0
8260816035
100301:u
KC
1.2-DICHLOROPROPANE
Not detected
ug/kg
5.0
8260815035
1M10301:54
KC
1,3-DICHLOROPROPANE
Not detected
ug/kg
5.0
8260B15035
1/9/0301:54
KC
2,2-0ICHLOROPROPANE
Not detected
ug/kg
5.0
8260BIW35
V9/0301:54
KC
1,1-0I0HLOROPROPENE
Not detected
ug/kg
5.0
0MW5035
V9/0301:54
KC
ETHYLBENZENE
Not detected
ug/kg
5.0
0280B/5035
1/910301:54
KC
HEXACHLOROOUTADIENE
Not detected
ug/k9
5.0
826OW5035
11910301:54
KC
ISOPROPYLBENZENE
Not detected
ugAg
5.0
8260B15035
11910301:54
KC
P-ISOPROPYLTOLUENE
Not detected
ug/kg
SO
8260815035
119/0301:54
KC
_ METHYLENE CHLORIDE
Not detected
ug/kg
100,0
8260815035
1N10301:5,1
KC
NAPHTHALENE
45
ug/kg
5.0
8260815035
1I9I0301:54
KC
N-PROPYWENZENE
Notdetected
ug/kg
5.0
82608IW35
IV0301:51
KC
STYRENE
Not detected
ug/kg
5.0
826DBIW35
1/9/0301:54
KC
1,1,12-TETRACHLOROETHANE
Not detected
ug/kg
5.0
82WW6036
IM0301:54
KC
1.12.2-TETRACHLOROETHANE
Not detected
ug/kg
5.0
82KWW35
1MI0301:St
KC
TETRACHLOROETHENE
NO detected
ug/kg
5.0
0260&5035
11910301:54
KC
TOLUENE
Notdetectetl
ug/kg
5.0
0280B/5035
119,0301:m
KC
1,2,3TRICHLOROBENZENE
Not detected
u9/xg
5c
6280915035
11910301:St
KC
1.2,4-TRICHLOROSENZENE
Not detected
ug/kg
5.0
026OW5035
11910301:54
KC
1,1.1-TRICHLOROETHANE
Not detected
ug/kg
5.0
0260815035
11910301:54
KC
1.1,2-TRICHLOROETHANE
Notdetected
ug/kg
5.0
8260W5035
11910301:54
KC
TRICHLOROETHENE
Not detected
ug/kg
5.0
8260B15035
1I910301:54
KC
TRICHLOROFWOROMETHANE
Not detected
ugBg
So
8260B15035
11910301:u
KC
1,2,3-TRICHLOROPROPANE
Not detected
uglk9
5.0
82BOB15035
119/0301:54
KC
1,2,4TRIMETHYLBENZENE
15
ug/kg
tic
82600/5035
11910301 St
KC
13,5-TRIMETHYLBENZENE
57
ug/kg
5.0
82BOBIS035
119/0301:51
KC
VINYL CHLORIDE
Notdetectetl
ug/kg
10.0
8260BIW35
1/910301:54
KC
TOTAL XYLENES
7.3
ug/kg
5.0
8260B15035
11910301:54
KC
2-BUTANONE(MEK)
Not detcoxcl
agAg
500
82MB15035
V9/0301:51
KC
NO Certification No. 402 - SC Ceffica ian No. 99012 - NO Drinking
Water Cart. No. 37735 - FL Certification No. E87519
449 Sprivgbrook Road A P.O.
Box 240543 A Charlotte, NC
28224-0543
Phone: 704 / 529-6364 ATM Free Numb,. 1.800
/ 529-6364 A Fox: 704 / 525-0409
Lab Report
,(f{J\ PRISM
uaoAnronlas,mc
_d
r,x s.,w.MeMuml n arw�ul savme
1/16103
Page 3 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
NII @ 5
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68589
Charlotte, NO 28226
'Login Group:
51491<7
Sample Collection Dale/Time:
112/03 11:00
-
Lab Submittal Date(Tme:
1/6103 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory.
TEST
TEST
REPORTING
METHOD
OATErhME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
2-CHLOROETHYL VINYL ETHER
Not detected
ug/kg
10J1
8260W5035
1/9I0301:54
KO
4-METHYL-2-PENTANONE(MIBK)
Not detected
ug/kg
50.0
826OW5035
1/9I0301:54
KC
ACETONE
120
ug/kg
100.0
8260&5035
1/910301:54
KC
CARBON DISULFIDE
Notdetected!
ag/kg
100,0
0250B15035
119I030154
KC
VINYLACETATE
NWdetected
ug/kg
50.0
82608/5035
11910301:54
KC
CIS-1,9-DICHLOROPROPENE
Not detected
ugAg
5.0
8260015035
1/910301:54
KC
TRANS-1.SDICHLOROPROPENE
Not detected
ugAg
5.0
U60BIN35
11910301:64
KC
241EXANONE
Not detected
ug/kg
50.0
8260B15035
IM0301:54
KC
IPE
Not detected
ug/kg
5.0
8260B15035
1/910301:54
KC
MTBE
Notdetected
ug/kg
5.0
8260WS035
11910301:54
KC
SURRDIBROMOFLUOROMETHANE
97
%
72-137
8260815035
VW0301:54
KC
SURRITOLUENE-00
95
%
73-128
8260W5035
119N301:54
KC
SURR:BROMOFLUOROBENZENE
103
%
69-131
826OW5035
11W0301:54
KC
C5C8 Aliphdice
NO detected!
mglkg
7
MADEPVPH
11&032129
JMV
C9-012 AIIphatics
Not delecoxi
mg/kg
6
MADEPVPH
11610321:29
JMV
C9-010 Art.w.
Not detected
mg/kg
2
MADEPVPH
11610321:29
JMV
Surrogate%Recovery-PID
III
%
(70-130)
MADEPVPH
11610321:29
JMV
Surrogate%Rewvery-FID
98
%
(70-130)
MADEPVPH
1MI032129
JMV
Dilution Factor
1
mglkg
MADEPVPH
1/6/032129
JMV
Dry Weight Received
17,08A
mglkg
MADEPVPH
1/6/032129
JMV
EXTRACTION FOR EPH Completed
MADEPVPH
1/6/0316:00
JMK
C9Ci8 ALIPHATICS Not detected mg/kg
40 MADEP-EPH
IM0318:52
GRR
C19C36 ALIPHATICS Notdetected mg/kg
2D MADEP-EPH
illI0318:52
GRR
C11-C22 AROMATICS Not detected mg/kg
20 MADEP-EPH
1910318:52
GRR
SURROGATE RECOVERY - ALIPHATIC 90 %
(40-140) MADEP-EPH
19/0318:52
GRR
SURROGATE RECOVERY - AROMATIC 103 %
(40.140) MADEP-EPH
1/l10318S2
GRR
SURR:2-FLUOROBIPHENYL 92 %
(40-140) MADEP-EPH
IU10310:52
GRR
SURR:2-RROMONAPH7HALENE 95 %
(40.140) MADEP-EPH
1RI0310:S2
GRR
DILUTION FACTOR 1 II
MAOEP-EPH
IU10310:52
GRR
NO Certification No. 402 - SC Certification No. 99012 - NO Drinking Water Cen, No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 A Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Nurober: 1-800
/ 529-6364 A Fax: 704 / 525-0409

Lab Report
PRISM
uea.'se,Ia,.
=
rue s.,„<. n„µixm n E�mlwMooul sauw,.
1/16/03
Page 4 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-1 @ 5
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
ACS8589
Charlotte, INC 28226
Login Group:
5149K7
Sample Collection Date/Time:
I Z03 11:00
Lab Submittal Date/Time:
116/03 0800
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory.
TEST
TEST
REPORTING
METHOD
DATERIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
DRYWEIGHT
8.2g
mg/kg
MADEP-EPH
Inns 1852
GRR
CALCULATIONS BASED ON DRY WT.
62
%DRY WT.
001
SM 2540G
1181031"o
CWC
PREP. METHOD 3550
completed
SW846-3550B
IR10308:00
JOE
ACENAPHTHENE
Not detected
ug/kg
400
SW8488270C
V9/0317:32
WAD
ACENAPHTHYLENE
Not detected
ugBg
400
SW8468270C
11910317:32
WAD
ANTHRACENE
Not detected
ug/kg
400
SW846412700
11910317:32
WAD
BENZO(A)ANTHRACENE
Not detected
ug/kg
400
SW8468270C
11910317:32
WAD
BENZO(B)FLUORANTHENE
Not detected
ugft
"oO
SWB468270C
1191031732
WAD
BENZO(K)FLUORANTHENE
Not detected
ug/kg
40D
SW8168270C
1/910317:32
WAD
BENZOIA)PYRENE
Not detected
Ug/kg
600
SW846-8270C
11910317:32
WAD
BENZO(GHI)PERYLENE
Not detected
ug/kg
400
SW846.9270G
15 317:32
WAD
BIS(2-CHLOROETHOXY)METHANE
Notdeteded
ug/kg
400
SW846-8270C
1191031732
WAD
BIS(2-0HLOROETHYL)ETHER
Not detected
ug/kg
400
SW84G8270C
M0317:32
WAD
BIS(2-0HLOROISOPROPYL)ETHER
Net detected
ugBg
400
SWS468270C
V910317:32
WAD
BIS(2-ETHYLHEXYL)PHTHAL4TE
Not detected
ug/kg
400
SWUS4270C
V9103 17:32
WAD
4-BROMOPHENYL PHENYL ETHER
Not detected
ug/kg
400
SW8468270C
1/91031732
WAD
BUTYL BENZYL PHTHAIATE
Not detected
ug/kg
400
SW8468270C
1/010317:32
WAD
4-CHLOR03 ETHYLPHENOL
Not detected
ug/kg
400
SW846A270C
1/9/0317:32
WAD
2-CHLORONAPHTHALENE
Not detected
ugN
400
SW846A270C
1003 17 32
WAD
2-CHLOROPHENOL
Not detected
ugBg
<00
SWB468270C
11910317:32
WAD
4OHLOROPHENYL PHENYL ETHER
Not detected
ug/kg
40D
SW846-8270C
119/0317:32
WAD
CHRYSENE
Not detected
ug/kg
40D
SW846-8270C
11910317:32
WAD
DtBENZO(A,H)4NTHRACENE
Not detected
ug/kg
400
SW846-8270C
119N317:32
WAD
DIBENZOFURAN
Not detected
ug/kg
400
SW84EB2700
IMM317:32
WAD
DI-N-BUTYLPHTHAIATE
Not detected
ug/kg
400
SWa46-6270C
IMM317:32
WAD
1,2-0IGHLOROSENZENE
Not detected
ugBg
400
SW846-8270C
1MI0317:32
WAD
1,3-0ICHLOROBENZENE
Notdetected
ug/kg
400
SWUM270C
119/0317:32
WAD
1,4-OICHLOROBENZENE
Net detected
ug/kg
400
SW846-837DC
11910317S2
WAD
2,4-0ICHLOROPHENOL
Not detected
ug/kg
400
SW846A27oC
11910317:32
WAD
DIETHYL PHTHALATE
Not detected
ug/kg
400
SW0464270C
1MI0317:32
WAD
NO Certification No. 402 - SC Certification No. 99012
- NO Drinking
Water Celt. No. 37735 - FL Certification No. E87519
449 SMingbmok Road ♦ P.O.
Box 240543 ♦
Charlotte, NC
28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 /
529-6364 ♦ Fax: 704 / 525-0409
Lab Report
'=\PRISM
Put s.My Merytivel a Ertmw .sauEare
1/16/03
Page 5 of 42
ERM Southeast, Inc.
Customer Project
ID: VMG
Attn: Mr. Rick Tarravechia
Customer
Sample
ID: MW-1 @5
7300 Carmel Exec. Park Ste, 200
Prism Sample
ID: AC68589
Chadotte, NC 28226
Login Group:
5149K7
Sample Collection Date/Tme:
1/2/03
1100
Lab Submittal Date/Time:
1/6103
0800
The following analytical results have been obtained
for the
indicated sample
Which was submitted
to this laboratory:
TEST
TEST
REPORTING
METHOD
OATERIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED ANALYST
2A-0IMETHYLPHENOL
Not detected
ug/kg
400
SWB4 8270C
11910317:32
WAD
DIMETHYL PHTHALATE
Not detected
ug/kg
400
SW846-8270C
1/910317:32
WAD
2,4-DINITROPHENOL
Not detected
UI
20M
SW846A270C
1/9I0317:32
WAD
2,4-DINITROTOLUENE
Not detected
ug/kg
400
SW846A270C
11910317:32
WAD
2,6-DINITROTOLUENE
Not detected
ug/kg
400
SWS468270C
11910317:32
WAD
DI-N-OCT PHTHALATE
Not detected
ug/kg
400
SW84682700
11910317:32
WAD
FLUORANTHENE
Not delecetl
ug/kg
400
SW846-8270C
1/910317:32
WAD
FLUORENE
Not detected
ug/kg
400
SWW-8270C
1/910317:32
WAD
HEXACHLOROSENZENE
Not detected
ug/kg
400
SW8464270C
V910317:32
WAD
HEXACHLOROBUTADIENE
Not detected
ugAg
400
SW846A270C
11910317:32
WAD
HEXACHLOROCYCLOPENTADIENE
Not detected
ug/kg
400
SW6468270C
11910317:32
WAD
HEXACHLOROETHANE
Not detected
u9/kg
400
SW546-8270C
11910317:32
WAD
INOENO(1,2,3-0D)PYRENE.
Not detected
ug/kg
400
SW846A270C
1/910317:32
WAD
ISOPHORONE
Net detected
ugMg
400
SW846U=
11910317:32
WAD
2-METHYL4,6-DINITROPHENOL
Not detected
III
2D00
SWS4 8270C
V9N31732
WAD
2-METHYL NAPHTHALENE
Not detected
ugBg
40o
SW84S8270C
1191031732
WAD
2-METHYL-PHENOL
Not detected
ug/kg
400
SW8468270C
1191031732
WAD
4-METHYL-PHENOL
Notdetected
ug/kg
400
SW846A270C
11910317.32
WAD
NAPHTHALENE
Not detected
ug/kg
400
SWM"2700
1,910317SZ
WAD
NITROBENZENE
Not detected
ugNg
400
SW846-8270C
15I0317:02
WAD
2-NITROPHENOL
Not detected
ugMg
400
SW846-8270C
1/9N317:32
WAD
4NITROPHENOL
Not detected
ug/kg
200D
SW846A270C
11910317:32
WAD
N-NITROSODIPHENYIAMINE
Not detected
ug/kg
400
SW846A270C
V9I0317:32
WAD
N-NITROSODI-N-PROPYLAMINE
Not detected
ug/kg
400
SW84682700
119/031732
WAD
PENTAOHLOROPHENOL
Not detected
ug/kg
2000
SW846-8270C
1/9/031732
WAD
PHENANTHRENE
Not detected
ug/kg
400
SW846-8270C
1R10317S2
WAD
PHENOL
Not detected
ug/kg
400
SW8468270C
IKA317:32
WAD
PYRENE
Not detected
ug/kg
400
SW846-0270C
1/910317:32
WAD
1,2,4TRICHLOROBENZENE
Not detected
ug/kg
4M
SW846A270C
1l9/11317:32
WAD
2,4,5-TRICHLOROPHENOL
Not detected!
ug/kg
400
SW8468270C
11910317:32
WAD
2,4,&TRIOHLOROPHENOL
Not detected
ug/kg
400
SW8468270C
11910317:32
WAD
NC Certficaton No. 402 - SC Certification
No. 99012 - NC Drinking
Water Gen. No. 37735 - FL Certification ND E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦ Charlotte, NC
28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800
/ 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
� PRISM
�5= 1A80PAlnPIES, INC
Ik
FW Sn JvayaW a EMba.9d.
1116103
Page 6 of 42
ERM Southeast, Inc.
Customer Project ID: VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID: MW-1 ® 5
7300 Cannel Exec. Park Ste, 200
Priam Sample ID: AC68589
Charlotte, NC 28226
Lopin Group: 51491<7
Sample Collection Date/Time: 1/2/03 11:00
Lab Submittal Date/Time: 1/6/03 0800
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST
REPORTING METHOD DATE?IME
PARAMETER RESULT
UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
Analysis Note for 8260: Acetone was detected in
this sample. Acetone method blank Concentration was <l0
ppb. Laboratory ccoonnttaa/mJination is not suspected.
e �-� l
Angela D. Overcash, V.P. Laboratory Services
NC Cedi0cal No. 402 - SC Certification No. 99012 - NC Drinking Water Cod. No. 37735 - FL Certification No. E87519
449 Springbmok Road A P.O. Box 240543 A Charlotte, NC 28226-0543
Phone: 704 / 529-6364 A TOU Fee Number. 1-800 / 529-6364 A Fax: 704 / 525-0409
Lab Report
_
�[ PRISM
ORAIORIR,INC.
�My
FUA yrrla MaNlk¢I x Em1mmn„1¢I $M,qm¢
1/16/03
Page 7 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarrevechia
Customer Sample ID:
MI 10
- 7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
ACS8590
Charlotte, NC 28226
Lopin Group:
5149K7
Sample Collection DateRime:
1/2103 11:15
Lab Submittal Date/Time:
1/6103 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT UNITS
LIMIT
REFERENCE
STARTED
ANALYST
TICS BY SEMIVOLATILE GCIMS
625I8270
1113V031802
WAD
625/8270 Tentatively Identified Compounds (10-largest
TICa):
<Ideatificaticn Claee>
<Closest spectral
Fib
<Est. Cost-
.................................
Unknown aliphatic
..............."`...
hydrocarbon (Leconte)
............
5700 ug/kg
Unknown aliphatic
hydrocarbon (Tetradecane)
4400 ug/kg
UNcnown aliphatic
hydrocarbon (Heptadecane)
12000 ug/kg
UIDorown aliphatic
hydrocarbon (Hexadecane,
tetramethyl)
2700 ug/kg
Unknown aliphatic
hydrocarbon (Nonadecane)
5100 ug/kg
- Unknown aliphatic
hydrocarbon (Ricosane)
3300 ug/kg
Unknown aromatic hydrocarbon
(Unknown)
4600 ug/kg
Unknown aromatic hydrocarbon
(Unknown)
2900 ug/kg
Unknown
(Unknown)
4600 ug/kg
_ Unknown
(Unknown)
4Son ug/kg
BENZENE
Not detected ug/kg
160
8260B15035
118/0321:05
NO
BROMOBENZENE
Not detected ug/kg
160
8260B15035
11810321:05
KC
BROMOCHLOROMETHANE
Not detected uglkg
160
82603IW35
11810321:06
KC
BROMODICHLOROMEDIANE
Not detected! uglkg
160
82600,5035
1Runs 21:06
KC
BROMOFORM
Not detected ug/kg
160
8260WS035
1/8/0321:06
KC
BROMOMETHANE
Not detected ugBg
320
62608/5035
1/&0321:05
KC
N-BIIIYLBENZENE
12N ug/kg
160
826OW5035
1/&0321:06
KC
SEC-BUTYLBENZENE
540 ug/kg
160
3260W5035
11&0321:05
KC
TERT-BUTYLBENZENE
Not detected ug/kg
.160
8260B15035
100321:06
KC
CARBON TETRACHLORIDE
Not detected ug/kg
160
826013I5035
100321:06
NO
CHLOROSENZENE
Not detected ug/kg
160
826OB15035
100321:06
KC
CHLORODISROMOMETHANE
Not detected ug/kg
160
8260D15035
11810321:06
NO
CHLOROETHANE
Not detected ugft
320
8260BI5035
11810321:06
KC
CHLOROFORM
Notdatected ugAg
160
8260B15035
1/8/0321:06
NO
CHLOROMETHANE
Not detected ug/kg
320
826OB/5035
1/810321:05
KC
24tHLOROTOLUENE
NAmtected uglkg
160
82605IN35
100321:as
KC
4CHLOROTOLUENE
Not detected! ugA,9
160
8260SI5035
1IV0321:06
KC
1,2-DIBROM0-3-CHLOROPROPANE Not detected uglkg
320
8260B15035
11810321:06
KC
1,2-DIBROMOETHANE
Not detected uglkg
ISO
6260W5035
11&0321:BE
KC
DIBROMOMETHANE
Not deteded uglkg
160
8260NS035
1/&0321:06
KC
1,2.DICHLOROBENZENE
Not detected ugAg
160
32608/5035
100321:06
KC
NC CeNBcafion No. 402 -
SC Cedfication No. 99012 - NO Drinking Water Ced. No. 37735 - FL Cergfcation No.
E87519
449
Springbrook Road A P.O. Box 240543 A Charlotte, NC
28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800
/ 529-6364 A Fax: 704 / 525-0409

Lab Report
PRISM
I Ak 1ABORATOMES. INC.
FA ServveN Mral 6 EnWrtnmenlel Wul-o
1116/03
Page 8 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanavechia
Customer Sample ID:
MW-1 @ 10
7300 Cannel Exec. Park Ste, 200
Prism Sample ID:
ACS8590
Charlotte, NC 28226
Login Group:
51491<7
Sample Collection Date/Time:
1/2/03 11:15
Lab Submittal DatelTime:
1/6/03 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING METHOD
DATEFnME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1.3 ICHLOROBENZENE
Not detected
ug/kg
ISO
8260B15035
1/BI0321:06
KC
1,4-0ICHLOROBENZENE
Not detected
ug/kg
160
8260815035
11810321:06
KC
DICHLORODIFLUOROMETHANE
Not detected
ug/kg
160
02MB/5035
11810321:06
KC
1,1-DICHLOROETHANE
Not detected
ugBg
160
026OWS035
1/810321:06
KC
1,2-DICHLOROETHANE
Nottletected
UgAg
160
8260WS035
1I810321:06
KC
1,1-DICHLOROETHENE
Notdeteted
ug/kg
160
82600/$035
118/0321:06
KC
CIS-1,2-0ICHLOROETHENE
Not detected
UgBg
160
82600I5035
1/8/0321:06
KC
TRANS-I,2-0ICHLOROETHENE
Not detected
ug/kg
160
8260BM35
1/810321:06
KC
1.2-0ICHLOROPROPANE
Not detected
Ug0k9
160
8260BIK35
1/&0321:06
KC
1,3-DICHLOROPR0PANE
Not detected
ugBg
160
8260815035
1/W0321:06
KC
2,2-01CHLOROPRGFANE
Not detected
UgBg
160
826013I5035
l/&0321:06
KC
1,1.DIOHLOROPROPENE
NO detected
ugBg
160
8260815035
100321:05
KC
ETHYLBENZENE
310 _
ug/kg
160
8260B15035
l/W0321:06
KC
HEXACHLOROBUTADIENE
Not detected
ug/kg
160
0260W5035
100321:as
KC
ISOPROPYLBENZENE
230
ug/kg
160
826OB15035
11&032106
KC
P-ISOPROPYLTOLUENE
MO
ugBg
160
0 OW5035
11810321:06
KC
METHYLENE CHLORIDE
Not detected
ugBg
32M
0260815035
10032106
KC
NAPHTHALENE
11000
ugf
160
8260915035
11810321:06
KC
N-PROPYLBENZENE
540 -
ug/kg
160
82608/6035
11810321:06
KC
STYRENE
NotdateCwd
ug/kg
160
8260B/5035
1181032196
KC
1.1,1,2-TE7TRACHLOROETHANE
Noltleteded
ug/kg
160
8260B15035
11=321:06
KC
1,12,2-TETRACHLOROETHANE
Not detectetl
UgAog
160
8260BW35
1/8A0321:06
KC
TETRACHLOROETHENE
Not detected!
ug/kg
160
8260B15035
1/W0321:06
KC
TOLUENE -
Not detected
ugBg
160
82BOB15035
11810321:06
KC
I.2a TRICHLOROBENZENE
Not detected
ug/kg
160
8260W5035
1/810321:06
KC
1,2,4-TRICHLOROBENZENE
Not detected
ug/kg
160
8260W5035
1l&0321:CIE
KC
1,1,1-TRICHLOROETHANE
Not detected
ug/kg
150
8260W5035
100321:as
KC
1,1,2-TRICHLOROETHANE
Not detected
ug/kg
150
8260BI5035
10032106
KC
TRICHLOROETHENE
Not detected
ug/kg
ISO
6260W5035
1IEI0321:05
KC
TRIOHLOROFLUOROMETHANE
Not detected
ugBg
160
0260W5035
1/&032106
KC
1,2,3-TRICHLOROPROPANE
Not detected
ugBg
160
8260315035
100321:06
KC
INC Certficadon No. 402 - SC
Certification No. 99012
- NC Drinking
Water Cart._
No. 37735 - FL
Certification No.
E87519
449 Springbrook Road ♦ P.O.
Box 240543
• Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number 1-800 / 529-6364 ♦
Fax: 704 / 525-0409
Lab Report
till PRISM
FAT S—xe AnaMlml x EWaInnaual Soutom
1116/03
Page 9 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarmvechia
Customer Sample ID:
MWA @ 10
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68590
Charlotte, INC 26226
Login Group:
51491<7
Sample Collection Date/Time:
1/2/03
11:15
Lab Submittal Daterrime:
1/6/03 -
08:00
The following analytical results have been
obtained for the indicated sample which was submitted
to this laboratory:
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE IME
STARTED
ANALYST
12,4-TRIMETHYLBENZENE
1600
ug*g
160
8260BM35
1/810321:06
KC
1,3,5-TRIMETHYLBENZENE
650
ug/kg
150
8260B15035
1/W0321:0s
KC
/
VINYLCHLORIDE
Not detected
Ug/kg
320
8260BIW35
1/810321:06
KC
TOTALCYLENES
210 -
ug/kg
160
8260WW35
1/810321:06
KC
2-BUTANONE IMEKI
Not detected
ug/kg
16W
8260WW35
1/810321:06
KC
2-CHLOROETHYL VINYL ETHER
Not detected
ug/kg
320
826OW5035
11=321:06
KC
4-METHYL-2-PENTANONE(MIBK)
Not detected
ugBg
1600
8260W5035
1IN0321:46
KC
ACETONE
NWdeacted
ug/kg
3200
8260B15035
11W032106
KC
CARBON DISULFIDE
Not detected
ug/kg
32W
8760815035
1IW0321:06
KC
VINYLACETATE
Not detected
ug/kg
16N
8260W5035
1IW032106
KC
CIS-I.3 ICHLOROPROPENE
Not detected
ug/kg
160
8260B15035
1I810321:06
KC
TRANS4,&DICHLOROPROPENE
Not detected
ug/kg
160
82602,5035
1/8N321:06
KC
2-HEXA14ONE
Not detected
ug/kg
16W
826OW5035
1IW0321:06
KC
IRE
Not detected
ugBg
160
8260B/5035
100321:06
KC
MTSE
Not detected
ug/kg
160
826OB15035
11810321:05
KC
m BURR AIBROMOFLUOROMETHANE
147'
%
72-137
8260W5035
I19I0321 U6
KC
SURR:TOLUENE-08
140-
%
73.128
826OW5035
11810321:06
KC -
BURR:BROMOFLUOROBENZENE
141'
%
69­131
82BOW5035
11810321:Oe
KO
C5-CBAllphatlos
Not detected
mgkkg
7
MADER VPH
IH31032342
JMV
C9-C12Atph,d.
Not detected
mglkg
6
MADER VPH
1/1&0323:42
JMV
C9C10Arcuou.
61
mgBg
2
MADEP VPH
IIINW23:42
JMV
Surrogate %Recovery -PTO
01
%
(70-130)
MADEP VPH
1/1310323:42
JMV
Sinogete%Recovery-FID
74
%
(70-130)
MADEP VPH
1/131W 2342
JMV
Dilution Fedor
1
mgBg
MAI EP VPH
111310323A2
JMV
Dry Weight Recelod!
13.38a
mg/kg
MADER VPH
1/13/032342
JMV
EXTRACTION FOR EPH Completed MADEP-EPH 180316:00
JMK
C&C18 ALIPHATIC$ 2200 mgBg 40 MADEP-EPH 1RI0320:35
ORR
ClaC36 ALIPHATICS 190 mg/kg 20 MADEP-EPH 19/0320:35
ORR
C1 IZ22 AROMATIC$ 760 mgixg 20 MADEP-EPH 1R10320:35
ORR
NC CerDFca0on No. 402 - SC CerINicatlon No. 99012 - NC Drinking Water Con. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28226-0543
Phone: 704 / 529-6364 ♦ Toll P. Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
; PRISM
d ueoR4malERdc.
Fx15—ke MwlNcW a Emitmmxttl SaMbns
1/16/03
Page 10 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mc Rick Tarravechia
Customer Sample ID:
MW-t @ 10
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68590
Charlotte, NC 28226
Login Group:
5149K7
Sample Collection.Daterrime:
12/03 11:15
Lab Submittal Date/Time:
1/6103 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATMME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
SURROGATE RECOVERY -ALIPHATIC
'MI
%
(40-140)
MADEP-EPH
19/032035
GRR
SURROGATE RECOVERY -AROMATIC
'MI
%
(40-140)
MADEP-EPH
lUI0320:35
GRR
SURR:2-FLUOROBIPHENYL
'MI
%
(40-140)
MADEP-EPH
1M0320:35
GRR
SURR:2-BROMONAFHTHALENE
-MI
%
H4 140)
MADEP£PH
1Z0320:35
GRR
DILUTION FACTOR
1
mglkg
MADEP.EPH
199320:35
GRR
DRY WEIGHT
7A9
mg/kg
MA➢EP-EPH
1910320:35
GRR
CALCULATIONS BASED ON DRY WT.
74
%DRY WT.
0.01
SM2540G
11810310:20
CWC
PREP. METHOD 3550
Completed
SW0463550B
19/0308:00
JDP
ACENAPHTHENE
Not detected
ug/kg
450
SW846A2700
1191W 23:14
WAD
ACENAPHTHYLENE
Not detected
UgAg
450
SW846-8270C
119/032314
WAD
ANTHRACENE
Not detected
ug/kg
450
SW84&8270C
11910323:14
WAD
BENZO(A)ANTHRACENE
Not detected
ug/kg
450
SW546.0270C
IN10323:14
WAD
BENZO(B)FLUORANTHENE
Notdetectetl
ug/kg
450
SWUM270C
199323:14
WAD
BENZO(K)FLUORANTHENE
Not detected
ug/kg
450
SWM427K
11W0323:14
WAD
BENZO(A)PYRENE
Not detected
UgAg
450
SW846-82700
11W0323:14
WAD
BENZO(GHI)PERYLENE
Not detected
ugAg
450
SW8468270C
11910323:14
WAD
BIS(2-CHLOROETHOW)METHANE
Not detected
UgAg
450
SW846A27QC
11910323:14
WAD
BIS(2-CHLOROETHYL)ETHER
Not detected
ug/kg
450
SWW4 82700
11910323:14
WAD
BIS(2-CHLOROISOPROPYL)E7HER
Nottleteded
UgAg
450
SW8468270C
1191032314
WAD
8IS(2-ETHYLHE"1-)PHTHA1-ATE
Not detected
ugAg
450
SW846-8270C
1MI0323:14
WAD
4-BROMOPHENYL PHENYL ETHER
Not detected!
UgAg
450
SW846-8270C
1/910323/4
WAD
BUTYL BENZYL PHTHALATE
Not detected
UgAg
450
SW84682700
199323:14
WAD
0.CHLORG-3-METHYLPHENOL .
Not detected
ug/kg
450
SWMM270C
19N323:14
WAD
2CHLORONAPHTHALENE
Not detected
ug/kg
450
SWM427X
1/9N323:14
WAD
2CHLOROPHENOL
Not detected
ugAg
460
SWM427W
1199323:14
WAD
4CHLOROPHENYL PHENYL ETHER
Not tletected
ug/kg
450
SWW-827W
VMS 23:14
WAD
CHRYSENE
Notdetected
UgAg
450
SW846-8270C
1/910323:14
WAD
DIBENZO(A.H)ANTHRACENE
Not detected
ug/kg
450
SW846A270C
11910323:14
WAD
DIBENZOFURAN
Nottleteded
ugkg
450
SW846-8270C
119/0323:14
WAD
DIN-BUTYLPHTHAL4TE
Not detected
ugAg
450
SW846-8270C
1910323:14
WAD
NC Confession No. 402 - SC Certification No. 99012
- NC Drinking Water Cert.
No. 37735 - FL Certification No. E87519
449 Springbro0k Road ♦ P.O.
Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
PRISM
_ L/.eOflleOltlEe.pG
Fitl Smite NWyYul6 Emlron„wlelSdWdn
1/16/03
Page 11 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-1 @ 10
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC68590
Charlotte, NC 28226
Lapin Group:
5149K7
.
Sample Collection Date/Time:
1/2/03 11:15
.
Lab Submittal DateRme:
1/6/03 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATE?IME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,2-DICHLOROBENZENE
Not detected
ugAg
450
SW016-8270C
1M0323:14
WAD
1,3-0ICHLOROBENZENE
Not detected
ug/kg
450
SWS468270C
1910323:14
WAD,
1,4DICHLOROBENZENE
Not detected
UgAg
450
SWW4270C
11910323:14
WAD
E,4-DICHLOROPHENOL
Not detected
ug/kg
450
SWBW3270C
IM0323:14
WAD
DIETHYL PHTHALATE
Not detected
ugAg
450
SW8458270C
1&0323:14
WAD
2,4-DIMETHYLPHENOL
Net detected
ug/kg
450
SWM4270C
IM0323:14
WAD
DIMETHYLPHTHAIATE
Not detected
UgAg
450
SWW4210C
119/0323:14
WAD
2,4-DINITROPHENOL
Not detected
ug/kg
2250
SW846-8270C
119/0323:14
WAD
2,4-DINITROTOLUENE
Not detected
ug/kg
450
SW0a68270C
1910323:14
WAD
2,&DINITROTOLUENE
Not detected
ug/kg
460
SW8468270C
1199323:14
WAD,
OIN-0CTYLPHTHALATE
Nottletected
UgAg
450
SW8464270C
119/0323:14
WAD
FLUORANTHENE
Notdeteded
UgAg
450
SWM4270C
1910323:14
WAD
FLUORENE
12W
ug/kg
450
SW846-6270C
1910323:14
WAD
HEXACHLOROBENZENE
Noldelected
ug/kg
450
SW8463270C
19/0323:14
WAD
HEXACHLOROBUTADIENE
Notdolected
ugAg
450
SW6468270C
1I9/0323:14
WAD
HEXACHLOROCYCLOPENTADIENE
Not detected
ug/kg
450
SW8463270C
1/910323:14
WAD
HEXACHLOROETHANE
Nottletected
ug/kg
450
SW846.8270C
1MI0323:14
WAD
INDENO(1,2,3CD)PYRENE
Not detected
ug/kg
450
SW8468270C
1IW0323:14
WAD
ISOPHORONE
Not detected
ug/kg
450
SW846-8270C
11W0323:14
WAD
2-METHYLAB-DINITROPHENOL
Not detected
ug/kg
2250
SW8468270C
1/910323:14
WAD
2-METHYL NAPHTHALENE
170p0
ugAg
450
SW(46.8270C
19I0323:14
WAD
2-METHYL-PHENOL
Not detected
ug/kg
450
SW846-8270C
IM10323:14
WAD
4-ME7HYL-PHENOL
Not detected
ug/kg
4$0
SW84682700
1910323:14
WAD
NAPHTHALENE
3500
ugAg
450
SW84&82700
1910323:14
WAD
NITROBENZENE
Not detected
ug/kg
450
SW846-82700
1199323:14
WAD
2-NITROPHENOL
Not detected
UgAg
450
SW846-8270C
1910323:14
WAD
4-NITROPHENOL
Not detected
Ug)kg
2250
SW846-8270C
19I0323:14
WAD
N-NITROSODIPHENYLAMINE
Not detected
ugAg
450
SW84&0270C
ISM 23:14
WAD
N-NITROSODIN-PROPYLAMINE
Not detected
ugAg
40)
SW84&0270C
1191032314
WAD
PENTACHLOROPHENOL
Not detected
ugAg
2250
SW546-0270C
1910323:14
WAD
PHENANTHRENE
4000,
ugAg
450
SWW-6270C
11910323:14
WAD
NC Cedfication No. 402 - SC Certification No. 99012
- NC Drinking
Water Cert. No. 37735 - FL Certification No.
E87519
449 Springbro0k Road ♦ P.O. Box 240543
♦ Charlotte, NC
28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number. 1-800 / 529-6364 ♦ Pax: 704 / 525-0409

Lab Report
PRISM
sur smte rm.pvw a anwmrvnemel sdeuxta
1/16103
Page 12 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-1 ®10
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC68590
Charlotte, NC 28226
Login Group:
5149K7
Sample Collection DateFrime:
112103
11:15
Lab Submittal Daterrme:
1/6/03
08:00
The following analytical results have been
obtained for the indicated sample which was submitted
to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEmME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
PHENOL
Not detected
uglkg
450
SWUO-8270C
1/910323:14
WAD
PYRENE
Not detected
ug/kg
450
SW84648270C
119M 23:14
WAD
1,2,4-TRICHLOROBENZENE
NO detected
uglkg
450
SW846-8270C
11910321:14
WAD
2A,STRICHLOROPHENOL
NO detected
ug/kg
450
SW848A270C
1I910323:14
WAD
2A,6-TRICHLOROPHENOL
Not detected
ug/kg
450
SW846A270C
IM10323:14
WAD
Sample Comments:
Analysis note for EPH:' - The surrogate recovery was outside the control limit due to matrix interference.
Analysis note for 8260; - - The surrogate recoveries were above the control limits. The analysis was repeated
at a 1:500 dilution, but the surrogates were diluted out. Matrix interference is suspected.
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certificston No. 99012 - NC Drinking Water Ced. No. 37735 - FL Certification No. E87519
449 Springlarook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 5296364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ F. 704 / 525-0409
Lab Report
ueoa4mmas, ixc.
�\ PRISM
LWI $qwy r.reMlmi 6 Emilcnme„pl etlWons
1116/03
Page 13 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanavechia
Customer Sample ID:
MW-1 @ 15
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68591
Charlotte, NC 28226
Lopin Group:
5149K7
Sample Collection Dale/Time:
1/2/03 11:30
Lab Submittal Date/Time:
1/6/03 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEITIME
PARAMETER
RESULT UNITS
LIMIT
REFERENCE
STARTED
ANALYST
TICS BY SEMIVOIATILE GCIMS -
625M270
111=317:47.
WAD
625/8270 Tentatively Identified Compounds (10-largest TICS):
<Identification Class,
<Closeet Spectral
Fib
'Est. COnc—
.«e--e-.-'----------------------
Unknown aliphatic
<-...............
hydrocarbon (Nonans)
-----
_.--------__
2000 ug/kg
Unknown aliphatic
hydrocarbon (Unknown)
4400 ug/kg
Umknown aliphatic
hydrocarbon (Unknown)
2100 ug/kg
Unknown aliphatic
hydrocarbon (Decane, 2-methyl)
2100 ug/kg
Unknown aliphatic
hydrocarbon Moderate)
2000 ug/kg
UNcnown aliphatic
hydrocarbon (Heptadecane)
5000 u9/kg
Unknown aliphatic
hydrocarbon (Nonadecane)
1900 ug/kg
-
UNcnown ATOMILiC hydrocarbon
(unknown)
38DO ug/kg
Unknown
(Unknown)
1800 u9/kg
Unknown aliphatic
hydrocarbon (Decane)
48DO ug/kg
BENZENE
Nctdetechd ug/kg
160
826OB15035
118A0303:14
KC
BROMOBENZENE
Not detected ug/kg
160
8260BI5035
100303:14
KC
BROMOCHLOROMETHANE
Not detected ug/kg
160
8260BI5035
VW0303:14
KC
BROMODICHLOROMETHANE
Not coated ug/kg
160
826OWW35
118/0303:14
KC
BROMOFORM
Not detected ugBg
-160
826OW5035
100303:14
KC
BROMOMETHANE
Not detected ug/kg
320
8260WS035
100303:14
KC
N-BMWENZENE
1100 ug/kg
160
8260515035
100303:14
KC
SEC-BUTYLBENZENE
710 ug/kg
160
8260W5035
1/610303:14
KC
TERT-BUTYLBENZENE
Not detected Vg/kg
160
826OW5035
1I8I0303:14
KC
CARBON TETRACHLORIDE
Not detected ugBg
160
826ON5035
1181030314
KC
CHLOROBENZENE
Not detected ug/kg
- 160 _
825OB15035
1181030314
KC
CHLORODIBROMOMETHANE
NOdetected ugAg
160
8260815035
11810303.14
KC
CHLOROETHANE
Nadeteded uglkg
320
826OB/5035
11&0303:14
KC
CHLOROFORM
Not detected uglkg
160
0260B/5035
11&0303:14
KC
CHLOROMETHANE
Not detected ugBg
320
82608/5035
1l&0303:14
KC
2LCHLOROTOLUENE
Not detected ug/kg
160
826OB15035
1IBUG 03:14
KC
4CHLOROTOLUENE
Notdeteded ug/kg
160
8250BIN35
100303:14l
KC
1,2-0IBROMO-3-0HLOROPROPANE Not detected ug/kg
320
826OB15035
1/&0303:14
KC
1R-0IBROMOETHANE
Not detected ug/kg
160
82601y5035
11910303A4
KC'
DIBROMOMETHANE
Not detected ugBg
160
826OB15035
1l&0303:14
KC
1,2-OICHLOROBENZENE
Nadetected ugBg
160
8260815035
VadG 03:14
KC
NC Certification No. 402 -
SC Cerlifcabon No. 99012 - NC Drinking
Water Cad.
No. 37735 - FL Certification No.
E87519
449
Springbrook Road ♦ P.O. Box 240543 ♦
Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 /
529-6364 ♦
Fax: 704 / 525-0409

Lab Report
PRISM
ueo6Aroelra, Ixa
AA
1. e.. Malylktl d Emim. StlWmf
1116/03
Page 14 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanavechie
Customer Sample ID:
MW-1 @ 15
7300 Carmel Exec. Park Ste, 200
Prism Sample ID:
AC68591
Charlotte, NC 28226
Lopin Group:
51491<7
Sample Collection DateTme:
1/2/03 11:30
Lab Submittal Date/Time:
116/03 0800
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
OATEMME
STARTED
ANALYST
1.bDICHLOROBENZENE
Not detected
ug/kg
160
82608I5035
IWO W:14
KC
1,4-0ICHLOROBENZENE
Not detected
ug/kg
160
82WWW35
100303:14
KC
DICHLORODIFLUOROMETHANE
Not detected
ug/kg
160
8260B15035
vsrotl0a14
KC
1,1-DICHLOROETHANE
Not detected
uglkg
160
6260W505
1I810303:14
KC
1,2-0ICHLOROE7HANE
Not detected
uglkg
160
8260W5035
1181030314
KC
1,1-0ICHLOROETHENE
Not detected
uglkg
160
82WBI5035
1I910303:14
KC
CISS12-DICHLOROETHENE
Not detected
ug/kg
ISO
626081503E
11810303:14
KC
TRANS4,2-DICHLOROETHENE
Not detected
ug/kg
160
B260WSOM
11810303:14
KC
1,243ICHLOROPROPANE
Not detected
ug/kg
160
5260WS035
1I11I0303:14
KC
1,3-DICHLOROPROPANE
Not detected
Upg
160
8260815035
1I810303:14
KC
2,2-DICHLOROPROPANE
Not detected
ughy
160
8260B/5035
1181030314
KC
t,1-DICHLOROPROPENE
Not detected
ug/kg
ISO
62601515035
1/810303:14
KC
ETHYLBENZENE
490
ug/kg
160
82BOB15035
1/810303:14
KC
HEXACHLOROBUTADIENE
Not detected
ug/kg
160
8260W5035
V810303:14
KC
ISOPROPYWENZENE
300
UgAg
160
8260W5035
1181030314
NO
P-tSOPROPYLTOLUENE
640
Ug/kg
160
8260B15035
1181030314
KC
METHYLENE CHLORIDE
Not detected
ug/kg
32M
8260B/5035
1/80303:14
KC
NAPHTHALENE
6"'
ug/kg
160
8260B15035
11810303:14
KC
N-PROPYLBENZENE
790 -
ugAg
160
8260W5035
1I8I0303:14
KC
STYRENE
Not detected
Ug/kg
160
82608/5035
1/80303:14
KC
1,1,1,2-TETRACHLOROETHANE
Not detected
LOAD
160
8260B/5035
V8/0303:14
KC
1,1,2,2-TETRACHLOROETHANE
Not detected
ug/kg
160
82601V5035
1/8/0303:14
KC
TETRACHLOROETHENE
Not detected
ug/kg
160
8260BSO35
11=303:14
KC
TOLUENE
Not detected
ug/kg
160
8260915035
1181030314
KC
1,2.lTRICHLOROBENZENE
Not detected
LOAD
160
826031503E
1181030314
KC
1,2,4-TRICHLOROBENZENE
Not detected
ug/kg
160
8260B15035
1181030114
KC
1,1,1-TRICHLOROE1HANE
Not detected
ug/kg
160
82609/5035
11810303:14
KC
1,1,2-TRICHLOROETHANE
Not detected
ug/kg
160
02608/5035
118/0303:14
KC
TRICHLOROETHENE
Not detected
ug/kg
160
8260W5035
11810303:14
KC
TRICHUCROFWOROMETHANE
Not detected
ug/kg
160
8280W5035
1181030314
KC
1,2,3-TRICHLOROPROPANE
Not detected
oglkg
160
8260B15035
11810303:14
KC
NC Certification No. 402 - SC
Certification No. 99012
- NC Drinking
Water Cart. No. 37735 - FL
Certification No.
E87519
449 Spdngbrook Road A P.O.
Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800
/ 529-6364 A
Fax: 704 / 525-0409
Lab Report
uaavAroelas,ma
=\PRISM
Re Service "'woxe d emhorrtantal
SMNtp
1/16/03
Page 15
of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample
ID: MW-1 @ 15
7300 Carmel Exec. Park Ste. 200
Prism Sample
ID: AC68591
Charlotte, NC 28226
Login Group: 5149K7
Sample
Collection Dateriime:
1/2/03
11:30
Lab
Submittal Date/Time:
1/6/03
08:00
The fallowing analytical results have
been obtained
for the indicated sample which was submitted
to this
laboratory:
TEST
TEST
REPORTING
METHOD
OATEITIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,2,4-TRIMETHYLBENZENE
12W
ug/kg
160
8260815035
1/810303:14
KC
1,3.5-TRIMETHYLBENZENE
720
ug/kg
160
8260815035
118O3 D3:14
KC
VINYL CHLORIDE
Not detected
ug/kg
320
82WB15035
1/8I0303.14
KC
TOTALXYLENES
5"
uglkg
160
8260B15035
1/810303;14
KC
2-BUTANONE(MEN)
Not detected
Uglkg
1600
8260B15035
1/810303:14
KC
2-CHLOROETHYL VINYL ETHER
Not detected
Ug/kg
320
8280B15035
1IN0303:14
KC
4-METHYL-2-PENTANONE(MIBK)
Not deeded!
Uglkg
1600
82605/5035
IIN0303:14
KC
ACETONE
Not deteclei
uglkg
3200
0260W5035
100303:14
KC
CARBON DISULFIDE
Not detected
ug/kg
3200
826OW5035
1I8/0303:14
KC
VINYL ACETATE
Not detected
ug/kg
1600
8260815035
11=303:14
KC
CIS-1.1DICHLOROPROPENE
Net deeded
uglkg
160
8260815035
1/8/0303:14
KC
TRANS-I,3-DICHLOROPROPENE
Not detected
ug/kg
160
82608/5035
11810303:14
KC
2-HEXANONE
Not detected
uglkg
1600
8260B15035
IIN0303:14
KC
IPE
Not deleded
uglkg
160
826013I5035
11W030:14
KC
MTBE
NedeteRed
uglkg
160
8260W5035
180303:14
KC
SURROIBROMOFLUOROMETHANE
159'
%
72-137
8260B15035
1I610303:14
KC
SURR:TOLUENE.D8
160-
%
73-128
8260W5035
11&0303:14
KC
SURR:BROMOFLUOROBENZENE
183-
%
6P131
8260915035
11810303:14
KC
CS Mtphados
Not detected
mglkg
35
MADEPVPH
1111103 De02
JMV
C9 12MIdatioe
Not detected
mg/kg
30
MADEPVPH
111110 ":02
JMV
C9C10Amma6ce
39
mg/kg
10
MADEPVPH
1I11I0304:02
JMV
Sumgale% Recovery-PID
DO
%
(70-130)
MADEPVPH
V11/0304:02
JMV
Surrogate%Recovery-PD
DO
%
(70-130)
MADEPVPH
1111/0304:02
JMV
Dilution Fedor
5
ngft
MADEPVPH
111110304:02
JMV
Dry Welpht Reoelved
14.71g
mglkg
MADEPVPH
1/1110304:02
JMV
EXTRACTION FOR EPH Completed MADEP-EPH 1I61031600
JMK
C9 18 ALIPHATICS 420 mg/kg 40 MADEP-EPH 1M0322:18
GRR
C19-C36 ALIPHATIOS 83 mglkg 20 MADEP-EPH IU10322:18
GRR
C11-C22AROMATICS 64 mg/kg 20 MADEP-EPH 1rrIW22:18
GRR
NC Certification No. 402 - SC Certification No, 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box U0543 A Charlotte, NC 28226-0543
Phone: 704 / 529-6364 A Toll Free Number. 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
PR ,,ISM
LABORATORICS, INC
RN a4nke NaMbl a EnN,m.I tke.x
1/16103
Page 16 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW4 @ 15
7300 Cannel Exec, Park Ste, 200
Prism Sample ID:
AC68591
Charlotte, INC 28226
Lopin Group:
51491<7
Sample Collection Date/Time:
1/2/03 11:30
Lab Submittal Date/Time:
1/6/03 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATE71ME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
SURROGATE RECOVERY - ALIPHATIC
'MI
%
140-140)
MADEP-EPH
IR10322:18
GRR
SURROGATE RECOVERY - AROMATIC
'MI
%
(40.140)
MADEP-EPH
IRRIG22:18
GRR
SURR2-FLUOROBIPHENYL
64
%
(40-140)
MADEP-EPH
1910322AU
GRR
SURR:2-BROMONAPHTHALENE
51
%
(40-140)
MADEP-EPH
1RI0322:18
GRR
DILUTION FACTOR
1
mgfkg
MADEP-EPH
1910322:18
GRR
DRY WEIGHT
7.8g
mg/kg
MADEP-EPH
IMIN MAN
GRR
CALCULATIONS BASED ON DRY WT.
78
%DRY WT.
0.01
SM 2540G
1/9/0310:20
CWC
PREP. METHOD 3550
Completed
SWM-35508
1910308:00
JDP
ACENAPHTHENE
Not detected
ug/kg
430
SW84B-8270C
1110103
WAD
ACENAPHTHYLENE
Not detected
ug/kg
430
SWS46A270C
1110/03
WAD
ANTHRACENE
Not detected
uglkg
430
SW046.8270C
1110103
WAD
BENZO(A)ANTHRACENE
Not detedetl
ugBg
430
SW846A270C
1I1=3
WAD
BENZO(B)FLUORANTHENE
Not detected!
ug/kg
430
SW8464t270C
111WO
WAD
BENZO(K)FLUORANTHENE
Not detected
ugBg
430
SW846A270C
1110103
WAD
BENZO(A)PYRENE
Not detected
uglkg
430
SW845d270C
1IIW03
WAD
BENZO(GHI)PERYLENE
Notdetected
ug/kg
430
SW846-8270C
1110103
WAD
SIS(Z-CHLOROETHOXY)METHANE
Not detected
ugBg
430
SWE4 8270C
1I10I03
WAD
13IS(2-0HLOROETHYL)ETHER
Not detected
ugBg
430
SWW-8270C
1110103
WAD
BISI2-0HLOROISOPROPYOETHER
Not detected
ug/kg
430
SWM-8270C
1110'03
WAD
3ISI2-5THYLHEXYL)PHTHALATE
Not detected
ug/kg
d30
SW8464270C
1/10103
WAD
bBROMOPHENYL PHENYL ETHER
Not detedetl
ug/kg
430
SW846.8270C
111=3
WAD
BUTYL BENZYL PHTHAIATE
Not detected
uglkg
430
SW846-8270C
1I1M
WAD
4 HLORO-o-METHYLPHENOL
Not detedetl
ugBg
430
SWIPI A270C
1/10813
WAD
2-0HLORONAPHTHALENE
Not detected
uglkg
430
SW848-8270C
1I1Nm
WAD
2-0HLOROPHENOL
Notdetected
ug/kg
430
SWM"270C
111010
WAD
4CHLOROPHENYL PHENYL ETHER
Not detected
ug/kg
430
SWUM270C
1110103
WAD
CHRYSENE
Not detected
ugBg
430
SWMM270C
1I1w03
WAD
DISENZO(AH)ANTHRACENE
Not detected
ugBg
430
SW846A270C
111WO
WAD
DISENZOFURAN
Not detedetl
uglkg
430
SW846-8270C
111WM
WAD
DI-N-BUTYLPHTHALATE
Nat detected
uglkg
430
SW845A270C
1110103
WAD
NO Certification No. 402 - SC Cedifoa6on No. 99012
- NO Drinking
Water Can. No. 37735 - FL Certification No, E87519
449 Springbrcok Road A P.O.
Box 240543 A
Charlotte, NC
29224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800
/ 529-6364 A Fax: 704 / 525-0409
Lab Report
`\ PRISM
ueoRMRIr5,INc.
Fud Se
EnNranirenW eoM1nbne
1/16/03
Page 17 of 42
ERM Southeast, Inc.
Customer Project
ID: VMG
Attn: Mr. Rick Tarravechia
Customer Sample
ID: MW-1 @ 15
7300 Cannel Exec. Park Ste. 200
Prism Sample
ID: AC68591
Charlotte, NC 26226
Low Group:
51491<7
Sample Collection Date/Time:
1/2/03
11:30
Lab Submittal Date/Time:
116/03
0800
The following analytical results have been obtained for the
indicated sample
which was submitted
to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEITIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,2-DICHLOROSENZENE
Not detected
ug/kg
430
SW846-9270C
1/10/03
WAD
1$DICHLOROBENZENE
Not detected
ug/kg
430
SW846A2700
1110/03
WAD
1.4DICHLOROBENZENE
Not detedetl
ugBg
430
SWS46-8270C
1110103
WAD
2,4-DICHLOROPHENOL
Not detected
ugBg
430
SW846-82700
1110103
WAD
DIETHYL PHTHALATE
Not detected
ugBg
430
SWS45-8270C
1I10/03
WAD
A4AIMETHYLPHENOL
Notdetected
uglkg
430
SW84641270C
1/10103
WAD
DIMETHYL PHTHALATE
Not detedetl
ug/kg
430
SWed6-8270C
1110103
WAD
2,4DINITROPHENOL
Not detected
uglkg
2150
SWe96-8270C
1/101W
WAD
2.4DINITROTOLUENE
Not detected
uglkg
430
SW846-8270C
1/10/03
WAD
2,6-0INITROTOLUENE
Not detected
ugBg
430
SW8464270C
111W03
WAD
DI-N-0CTYLPHTHALATE
Not detected
ug/kg
430
SW846-8370C
1110103
WAD
FLUORANTHENE
Not detected
ug/kg
430
SW846-8270C
1110/03
WAD
FLUORENE
low
ugBg
430
SW846-8270C
1110103
WAD
HEXACHLOROBENZENE
Not detected
ug/kg
430
SWS48b270C
1/10A03
WAD
HEXACHLOROBUTADIENE
Not tletected
ugBg
430
SWa48-6270C
1110103
WAD
HEXACHLOROCYCLOPENTADIENE
Not tletecetl
ugBg
4 O
SW645-E270C
11101M
WAD
HEXACHLOROETHANE
Not detected
ug/kg
430
SW8 270C
1/10103
WAD
INDENO(1,2,3-00)PYRENE
Not detected
ugBg
430
SW846-9270C
1110A3
WAD
ISOPHORONE
Not detected
ug/kg
430
SW846-8270C
111NO3
WAD
2-METHYL4,6-DINITR0PHENOL
Not detedetl
ugBg
2150
SW646-8270C
1110103
WAD
2-METHYL NAPHTHALENE
12000
ugBg
430
SW646A270C
1110103
WAD
2-METHYL-PHENOL
Not detected
ug/kg
430
SW846.8270C
1I10103
WAD
4-METHYL-PHENOL
Not detected
ugBg
430
SW846-8270C
1110/03
WAD
NAPHTHALENE
38W
ugBg
430
SW048-5270C
1110103
WAD
NITROBENZENE
Not detected
ugBg
430
SWW-8270C
1110I03
WAD
2-NITROPHENOL
Not tletected
ugBg
430
SW84fi-8270C
111W03
WAD
d-NITROPHENOL
Not detected
uglkg
2150
SW846-8270C
1H0103
WAD
N-NITROSODIPHENYLAMINE
Not detected
uglkg
430
SW846-8270C
1110103
WAD
N-NITROSODI-N-PROPYIAMINE
Not detected
ug/kg
430
SWMB-8270C
1/10/03
WAD
PENTACHLOROPHENOL
Not detected
ug/kg
2150
SW646-8270C
1/10103
WAD
PHENANTHRENE
24M
ugft
430
SW846-8270C
1110103
WAD
NO Certification No. 402 - SC Certification No. 99012
- NO Drinking
Water Cart. No. 37735 - FL Certification No.
E87519
449 Springbrook Road A P.O.
Box 240543 A Charlotte, NC
282240543
Phone: 704 / 529-6364 A Toll Free Number: 1-900
/ 529-6364 A Fax: 704 / 525-0409

Lab Report
1/16/03
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, INC 28226
\PRISM
FNI Sewn MuMkeld 5-a—ett edu4am
Page 18 of 42
Customer Project ID:
VMG
Customer Sample ID:
MINA ®15
Prism Sample ID:
AC68591
Lopin Group:
5149K7
Sample Collection Date[Time:
V2/03 11:30
Lab Submittal Date/Time:
1/6103 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DAMITIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
PHENOL
Not detected
uglkg
430
SW846-020C
11IO/W
WAD
PYRENE
Not detected
ug/kg
430
SW046.82700
111W03
WAD
1,2+TRICHLOROSENZENE
Not deteced
uP%g
430
SW846-82702
1I10103
WAD
2,4.STRICHLOROPHENOL
Not detected
ug/kg
430
SWUS-S270C
1110103
WAD
2.4,6-TRICHLOROPHENOL
Not detected
ug/kg
430
SWS4M270C
1I10103
WAD
Sample Comments:
Analysis note for EPH: `- Surrogate recovery was outside the control limits due to matrix interference.
Analysis note for 8260: - The surrogate recoveries Were above the control limits. The analysis was repeated
at a 1:500 dilution, but the surrogates were diluted out. Matrix Interference is suspected.
Analysis note for VPH: `- Surrogates were diluted out.
Angela D. Overman, V.P. Laboratory Services
NC Certification No. 402 - SC Certificabon No. 99012 - NC Drinking Water Can. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-900 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report\
PRISM
uao6ATaeas. uw.
FW SeM[e.4ary4-al a Emhwmentll $dNlm¢
1/16103
Page 19 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanavechia
Customer Sample ID:
MW-1 @ 20
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68592
Charlotte, NC 28226
Login Group:
5149K7
Sample Collection DateTme:
1/2/03 11.45
Lab Submittal Date[Time:
1/6/03 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATEMME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
TICa BY SEMIVOtATILE GUMS 62518270 119/031618 WAD
625/8270 Tentatively Identified Compounds (10-largest TICs):
<Identification Classy <Closest Spectral Fib 'Set. Cone—
-----------------••---- ---------------------- ------------
Unknown aliphatic hydrocarbon (Undecane) 2700 ug/kg
Unknown aliphatic hydrocarbon (Tetradecane) 5900 ug/kq
Unknown aliphatic hydrocarbon (Pentadecane) 5300 ug/kg
Unknown aliphatic hydrocarbon (aeptadecane) 6300 ug/kg
Unknown aliphatic hydrocarbon (Pentadecane, tat ethyl) 4600 ug/kg
Urtk:mrn aliphatic hydrocarbon (Nonadecane) 3200 ug/kg
Unknown aliphatic hydrocarbon (Bicoeane) 2300 ug/kg
Unknown aromatic hydrocarbon (Naphthalene, dimethyl) 3200 ug/kg
Unknown aromatic hydrocarbon (Naphthalene, trimethyl) 2800 ug/kg
Uh]kaotn aromatic hydrocarbon (Naphthalene, trimethyl) 2400 ug/kq
BENZENE Not detected uglkg 160 8260B15W5 111010312:03 INC
BROMOSENZENE Not detected uglkg 160 02608/5035 fIVO 12:0S KC
BROMOCHLOROMETHANE Not detected uglkg 160 8260B15035 111010312:03 KC
BROMOOICHLOROMETHANE Not detected ug/kg 160 82600N35 1HW031203 KC
BROMOFORM Not detected uglkg 160 8260B15035 111W0312S3 KC
SROMOMETHANE Not detested uglkg 320 82608/5035 1I1010312:03 KC
N-BUTYMENZENE 880 uglkg 160 82608/5035 1110/0312:03 KC
SEC-BUTYLBENZENE -500 ug/kg 160 8260W5035 111010312:03 KC
TERT-BUTYLBENZENE Not detected uglkg 160 8260W5035 111W0312:03 KC
CARBON TETRACHLORIDE Not detected uglkg 1B0 0260W5035 111W0312:03 KC
CHLOROBENZENE NO deteced uglkg 150 8260W5035 111010312:03 KC
CHLOROOSROMOMETHANE Not detained uglkg 160 0260SIS035 V1W0312.03 KC
CHLOROETHANE Not deeced uglkg 320 526OW5035 111W0312S3 KC
CHLOROFORM Not detected uglkg 160 0260B15035 111010312:03 KC
CHLOROMETHANE Not detected ug/kg 320 0260B15035 1110I0312o03 KC
2-CHLOROTOLUENE Not detected uglkg 100 8260a15035 1I1W0312:03 INC
4-CHLOROTOLUENE NO deeded ug/kg 160 0260B15035 1I101031203 KC
1,2-0IBROMO.3-CHLOROPROPANE Not detected ug/kg 320 8260B15035 1/1010312:03 KC
1.2-0IBROMOETHANE Not detected ug/kg 160 82BOWS035 IIIW0312:03 KC
DIBROMOMETHANE Not detected Uglkg 160 02e01315035 MW0312:03 KC
1,2.DICHLOROBENZENE Not detected ugBg 160 8260B15035 1I1W0312:03 KC
NC CerMca50n No. 402 - SC Certglcabon No. 99012 - NC Drinking Water Can, No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll I. Number 1400 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report }� \ PRISM
_..-,ueoBeroBl6s, Ixc.
Full3erv'm M¢x0¢tl 8 EmlrtnmenYl StluConS
1/16/03 Page 20 of 42
ERM Southeast, Inc. Customer Project ID: VMG
Attn: Mr. Rick Tanavechia Customer Sample ID: MW-1@20
7300 Cannel Exec. Park Ste. 200 Prism Sample ID: AC68592
Charlotte, NC 28226 Low Group: 5149K7
Sample Collection Date/Time: 1/2/03 11:45
Lab Submittal Date/Time: 1/6/03 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD DATErIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE STARTED
ANALYST
1,8-0ICHLOROBENZENE
Not detected
Ug/kg
160
826OB150M 1110103 12:03
KC
1,4AIOHLOROBENZENE
Not detected
ug/kg
160
826OW5035 1I1N0312:03
KC
DICHLORODIFLUOROMETHANE
Not detected
Ug/kg
16U
82KW5035 1I1010312:03
KC
1.1-DICHLOROETHANE
Not detected
ug*g
180
826OB15035 1/101M 12:03
KC
1,2-DICHLOROETHANE
Notdeteded
ug/kg
180
8260515035 111010312:03
KC
L1-DICHLOROETHENE
Notdetected
ug/kg
160
8260815035 1110/0312:03
KC
CIS-1.2-DiCHLOROETHENE
Not detected
ug/kg
160
8260BIW35 111010312:03
KC
TRANS-I,2-0ICHLOROETHENE
Not detected
ug/kg
160
8260615035 IM0103 12:03
KC
1,2-DICHLOROPROPANE
Not detected
ug/kg
160
8260BIWW Motto 12:03
KC
1,3-DICHLOROPROPANE
Not detected
ug/kg
160
826OW5035 111010312:03
KC
2,2-0ICHLOROPROPANE
NO detected
ug4cg
160
8260W5035 1I1010312d3
KC
1,1-0ICHLOROPROPENE
Not detected
ug/kg
160
82608/5035 1I101W 12:03
KC
ETHYLBENZENE
2Z0
ug/kg
160
826OWS035 111010312:03
KC
HERACHLOROBUTAOIENE
Notdeteded
ug/kg
150
8260B5035 11101W 12:03
KC
ISOPROPYLBENZENE
230
ug/kg
160
826OW5035 111010312:03
KC
P-ISOPROPYLTOLUENE
450
ug/kg
160
8260WW35 1110/0312:03
KC
METHYLENE CHLORIDE
NO detected
ug/kg
3200
8260BM35 V1010312:03
KC
NAPHTHALENE
3100
ug/kg
160
8260B/5035 1I1010312:03
KC
NPROPYLBENZENE
460
ugft
160
8260B15035 111W031203
KC
STYRENE
Not detected
ug/kg
160
8260W5035 1I10I031203
KC
1,1,1.2-TETRACHLOROETHANE
NO detected
Og)kg
160
8260W5035 1/1010312'.03
KC
1, 1,2,2-TETRACHLOROETHANE
Notdetected
ug/kg
160
8260SIM35 111010312:03
KC
TETRACHLOROETHENE
Nat detected
ug/kg
160
OMOBI5035 111010312:03
KC
TOLUENE
Not detected
ug/kg
160
8260815035 1I10I0312:03
KC
1,2,3-TRICHLOROBENZENE
Not detected
ug/kg
160
8260815035 111010312:03
KC
1.2,4-TRICHLOROBENZENE
Not detected
ug/kg
160
826OB15035 1110I0312:03
KC
Ltd-TRICHLOROETHANE
Not detected
Uglkg
160
8260SM35 MODS 12:03
KC
1,1,2-TRICHLOROETHANE
Not detected
Uglkg
160
8260815035 111010312:03
KC
TRICHLOROETHENE
Not deteced
ugAg
160
8260615035 111010312:03
KC
TRICHLOROFLUOROMETHANE
Not detected
ug/kg
160
6260615035 1/1010312:03
KC
1,2.YTRIOHLOROPROPANE
Not detected
ug/kg
1B0
8260815035 Malta 12:03
KO
NC CergfceJon No. 402 - SC Cengicaeod
No. 99012
- NC Drinking Water Con, No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦ Charlotte, NC
282240543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800
/ 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
�\
PRISM
wuroslss, lxc
FUII aeMrolreMiuld 6,rbdvnenlel$o'iin¢
1116103
Page 21
of 42
ERM Southeast, Inc.
Customer Project ID: VMG
Attn: Mr. Rick Tarravechia
Customer Sample
ID: MW-1 @ 20
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68592
Charlotte, NC 28226
Lopin Group:
5149K7
Sample Collection Daterrime:
112/03
11:45
Lab Submittal Date/Time:
116/03
08:00
The following analytical results have been obtained
for the
indicated sample which was submitted
to this
laboratory.
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1.2.4TRIMETHYLBENZENE
Not detected
ug/kg
160
8260SIM35
1/1010312:03
KC
1,3,5-TRIMETHYLBENZENE
Not detected
ug/kg
160
8260W5035
1/10/0312:03
KC
VINYL CHLORIDE
Not detected
ug/kg
320
8260WS035
111=312:03
KC
TOTAL%YLENES
Not detected
ug/kg
160
8260W5035
Made 12:03
KC
2-BUTANONE(MEK)
NO detected
Ug/kg
law
8260815035
1110M 12:03
KC
2-CHLOROETHYL VINYL ETHER
Not detected
UgAg -
320
8MB15035
1/10I0312:03
KC
FMETHYL-2PENTANONE(MIBK)
Not detected
ug/kg
16W
8263815035
11100312:03
KC
ACETONE
Notdetected
ug/kg
3200
826OB15035
111010312:03
KC
CARBON DISULFIDE
Not detttled
ug/kg
3200
8260B15035
111010312:03
KO
VINYLACETATE
Notcutected
ug/kg
1500
8260BI5036
111010312:03
KO
CIS-1,3-DICHLOROPROPENE
Not detected
ug/kg
160
6260015035
111010312:03
KC
TRANS-I,3-0ICHLOROPROPENE
Not detected
ugBg
160
8260815035
III W0312,03
KC
2-HE%ANONE
Not detected
ug/kg
1600
8260B15035
Ill ON31203
KC
IPE
Not detected
uglk9
160
8260B15035
1I10/0312:03
KC
MITRE
Not detected!
ug/kg
160
826OB15035
111W0312:03
KC
SURROIBROMOFLUOROMETHANE
14P
%
72-137
8260815035
111W0312:03
KC
SURR:TOLUENE-D8
13r
%
73-128
8260815035
1110/0312:03
KC
SURR:BROMOFLUOROBENZENE
133-
%
69-031
82606/5035
111010 12:03
KC
CS-C8 Aliphatice
Not detected
mglkg
14
MADEP VPH
Ill1IN 04:54
JMV
C9-C12 AIlph.t.
17
mg/kg
12
MADEP VPH
1/111030454
JMV
C9-Cl0 Ammadm
41
mg/kg
4
MADEP VPH
111110304:54
JMV
Smmgate%Recovery-PID
86
%
(70.130)
MADEP VPH
1/1110304:54
JMV
Surmgete% Recovery - FIG
08
%
(70.130)
MADEP VPH
1111103 o4:54
JMV
DilutJon Factor
2
mg/kg
MADEP VPH
111110304:56
JMV
Cry Weight Received
12,60a
mglkg
MADEP VPH
1/1110304:54
JMV
EXTRACTION FOR EPH Completed MADEP-EPH 1/610316:00
JMK
C9 18ALIPHATICS - 330 mpg 40 MADEP-EPH 118103
GRR
C19-035 ALIPHATICS 60 mgAg 20 MADEP£PH 118103
GRR
C11C22 AROMATICS 150 mg/kg 20 MADEP-EPH 118103
GRR
NC Certification No. 402 - SC CeNficaBon No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-63M ♦ Tall Free Number 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
PRISM
p\
Fu18eMv PneN4al4 ErtArtnmmbl9dNwu
1116/03
Page 22 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
II @ 20
7300 Camlel Exec. Park Ste. 200
Prism Sample ID:
AC68592
Charlotte, NC 28226
Loon Group:
5149K7
_
Sample Collection Date[Time:
1/2/03 1145
Lab Submittal Date/rime:
1/6103 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory.
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
SURROGATE RECOVERY -ALIPHATIC
'MI
%
(40-140)
MADEP-EPH
1003
GRR
SURROGATE RECOVERY - AROMATIC
'MI
%
(40-140)
MADEP-EPH
118N3
GRR
SURR:2-FLUOROBIPHENYL
125
% -
(40.140)
MADEP-EPH
118103
GRR
SURR:2-BROMONAPHTHAIENE
107
%
(40.140)
MADEP-EPH
V8103
GRR
DILUTION FACTOR
1
mpg
MADEP-EPH
1/8103
GRR
ORYWEIGHT
7.6It
mglkg
MADEP-EPH
11BN3
GRR
CALCULATIONS BASED ON DRY WT,
76
%DRY WT.
0.01
SM210G
11810310:20
CWC
PREP, METHOD 3550
Comeleted
SW846-35508
1910308:00
JDP
ACENAPHTHENE
Not detected
ug/kg
N0
SW846-827W
1910318:18
WAD
ACENAPHTHYLENE
Not tletedetl
ug/kg
440
SW846-8270C
119/0318:18
WAD
ANTHRACENE
Not detected
ug/kg
440
SW846-8270C
11910318:18
WAD
BENZO(A)ANTHRACENE
Net detected
ug/kg
440
SWU642700
IM10318:10
WAD
BENZO(B)FLUORANTHENE
Not detected
ug/kg
"o
SW846-8270C
1NW3 IS 18
WAD
BENZO(K)FLUORANTHENE
Not detected
ug/kg
440
SW846d270G
V91031818
WAD
SENZO(AIPYRENE
Not detected
ug/kg
4W
SWM"270C
11W03 Isla
WAD
BENZO(GHI)PERYLENE
Not detected
Ug/kg
440
SWS4 8270C
11910318:18
WAD
BIS(2-CHLOROETHOXY)METHANE
Not detected
ug/kg
44o
SW84G82703
11W031818
WAD
BIS(2-CHLOROETHYL)ETHER
Not detected
ug/kg
440
SW846-8270C
11910318:18
WAD
BIS(2-CHLOR0ISOPROPYL)ETHER
Not detected
Uglkg
440
SWW4270C
1MI0318:18
WAD
BIS(2-ETHYL1EXYL)PHTHALATE
Not detected
ug/kg
440
SW846.8270C
119/031818
WAD
4-BROMOPHENYL PHENYL ETHER
Notddected
ug/kg
MO
SW846-8270C
1MI0318:18
WAD
BUTYL BENZYL PHTHALATE
Not detected
ug/kg
Mc
SW848-8270C
11910318:18
WAD
4-CHLOR08METHYLPHENOL
Not detected
ug/kg
440
SW846-82700
119I0318:10
WAD
2LHLORONAPHTHALENE
Not detected
Uglkg
"0
SW846-8270C
11910318:18
WAD
2-CHLOROPHENOL
Not detected
ug/kg
440
SW846A270C
1NN318:18
WAD
4CHLOROPHENYL PHENYL ETHER
Not tletedetl
ug/kg
440
SW846-B270C
119103 IS 10
WAD
CHRYSENE
Not detected
ug/kg
440
SW846-8270C
1Nr0318:18
WAD
DIBENZO(A,H)ANTHRACENE
Not detected
ug/kg
"It
SW840A270C
IM10310:18
WAD
DIBENZOFURAN
Not detected
ug&g
MO
SW846-8270C
119103 late
WAD
DIN-BUTYLPHTHALATE
Not detected
Ug)kg
"o
SW846A270C
1)9)0316:18
WAD
NO Certification No. 402 - SC Certification No. 99012
- NO Drinking Water Cert.
No. 37735 - FL CertRicetion No. E87519
449 Spdngbmok Road ♦ P.O.
Box 240543 ♦ Charlene, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number 1-800 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
PRISM
uaoBATewlS.lxc.
FWI aertY Melyllml6 Emiro-m�melSduene
1/16/03
Page 23 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MWIA@20
7300 Carmel Exec. Park Ste, 200
Prism Sample ID:
AC68592
Charlotte, NC 28226
Looin Group:
5149K7
Sample Collection Date/Time:
112/03
11:45
Lab Submittal Date[Time:
116/03
08:00
The following analytical results have been
obtained for the indicated sample which was submitted
to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEMME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1.2-DICHLOROSENZENE
Not detected
ug/kg
440
SW846-8270C
1/9/0318:10
WAD
1,3-0ICHLOROBENZENE
Not detected
ug/kg
440
SW846A2700
'119)0318:18
WAD
1,4DICHLOROBENZENE
Not detected
ug/kg
"0
SW846-8270C
1I8/0318:18
WAD
2,4.DICHLOROPHENOL
NotdoWded
ug/kg
440
SW84"270C
1191031818
WAD
DIETHYL PHTHALATE
Notdeleded
ug/kg
"It
SWMM270C
1/91031818
WAD
2.0.DIMETHYLPHENOL
Not detected
ug/kg
440
SW046-0270C
1I9103 IS 18
WAD
DIMETHYLPHTHALATE
Not detected
ug/kg
440
SW046-8270C
119/0310:10
WAD
2,0.DINITROPHENOL
Not detected
upit
2200
SW0M270C
AMOS late
WAD
2A-DINITROTOLUENE
Notdeteded
ug/kg
440
SW846-0270C
119/0318:10
WAD
2,6-DINITROTOLUENE
Not detected
ug/kg
440
SW845-8270C
1/91031818
WAD
OIN-0CTYLPHT 1ALATE
Not detected
ug/kg
4W
SWB4 8270C
1/910318:18
WAD
FLUORANTHENE
Not detected
ug/kg
"It
SW846-8270C
M0318:18
WAD
FLUORENE
Not detected
ug/kg
440
SW846-8270C
119/0318:18
WAD
HEXACHLOROBENZENE
Not detected
ug/k9
"0
SW646.8270C
1NN318:18
WAD
HEXACHLOROBUTADIENE
Not detected
upg
440
SW846-8270C
IM/0318:16
WAD
HEXACHLOROCYCLOPENTADIENE
Notdeteded
upg
"0
SW846A270C
119N318:18
WAD
HEXACHLOROETHANE
Not detected
ug/kg
6W
SW846-8270C
1191031818
WAD
INDENO(1,2,3-0D)PYRENE
Not tletedetl
ugBg
440
SW846.8270C
1/9103 IS18
WAD
ISOPHORONE
Not detected
ug/kg
440
SW846-8270C
11910310:18
WAD
2METHYL4,6-0INITR0PHENOL
Not detected
uipg
2200
SW846-0270C
VW0318:18
WAD
2-METHYLNAPHTHAI_ENE
27N
upg
440
SW04041270C
1191031818
WAD
2-METHYL-PHENOL
Not detected
ug/kg
44o
SW04641270C
11910318:10
WAD
0.METHYL-PHENOL
Not detected
upg
bdo
SW848-0270C
11910310:18
WAD
NAPHTHALENE
1000
ug/kg
"It
SWS4 8270C
11WO318:13
WAD
NITROBENZENE
Not detected
ug/kg
440
SW846-82700
1*10318:10
WAD
2NITROPHENOL
Not detected
ug/kg
44o
SW84041210C
119I03 is 18
WAD
4NITROPHENOL
Not detected
ug/kg
2200
SWWA270C
IM10310:10
WAD
N-NITROSODIPHENYIAMINE
Not detected
Ug/kg
440
SWW4270C
IM10310:10
WAD
NNITROSODI-N-PROPYLAMINE
Not detected
Ug/kg
440
SWW4270C
11910310:10
WAD
PENTACHLOROPHENOL
Not detected
ugAg
2200
SWSWA270C
1/910310:18
WAD
PHENANTHRENE
710
ugfcg
440
SW846-8270C
1NI0310:18
WAD
NC Certification No. 402 - SC Certifcahon
No. 99012
- NC Drinking
Water Cert. No. 37735 - FL Certification No.
E87519
449 Springbmok Road ♦ P.O. Box 240543
♦ Charlotte, NC
28224-0543
Phone: 704 / 529-6364 A Toll Fro , Number: 1-800 / 529-6364 ♦ Fact 704 / 525-0409

Lab Report
1116103
ERM Southeast, Inc.
Alm: Mr. Rick Tamevechta
7300 Carmel Exec. Park Ste, 200
Charlotte, NC 28226
PRISM
s, ueoanroelrs,lxc
FWI ServWV McMkelnEmi,wrtanalsduCons
Page 24 of 42
Customer Project ID:
VMG
Customer Sample ID:
MWA@20
Prism Sample ID:
AC68592
Looin Group:
5149K7
Sample Collection Date/Time;
1/2103 11:45
Lab Submittal Date/Time:
1/6/03 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEhTIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
PHENOL
Not detected
ug/kg
"a
SW846-8270C
11910318:18
WAD
PYRENE
Not detected
ug/kg
440
SW84641270C
119103 ISIS
WAD
1,2,4-TRIOHLOROBENZENE
Not detected
ug/kg
4W
SW8468270C
bs/0310:18
WAD
2A.5-TRICHLOROPHENOL
Not detected
ug/kg
440
SW84E827DC
119103 18 18
WAD
2,46-TRICHLOROPHENOL
Not detected
ug/kg
440
SW846d270C
1191031818
WAD
Sample Comments:
Analysis note for SICK Surrogate recovery was outside the Control limits due to matrix interference.
Analysis note for 8260:- The surrogate recovery was outside of the control limits. The analysis was
repeated at a 1:500 dilution, but the surrogates were diluted out. Matrix interference is suspected.
Angela D. Overeash, V.P. Laboratory Services
INC Certification No. 402 - SC Certification No. 99012 - NO Drinking Water Can. No. 37735 - FL Certification No. E87519
449 Spongbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
'
j��;L uaoaeromEs,wo.
FWI eeMce/.reMl®In EnNrtnmeMal SOMcns
1116103
Page 25 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-2@5
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC68593
Charlotte, NC 28226
Looin Group:
5149K7
Sample Collection Date/Time:
1/3/03 12:15
Lab Submittal Date/Time:
1/6/03 08:00
The following analytical results have been obtained
for the indicated sample which was submitted to this laboratory:
TEST TEST
REPORTING METHOD DATEIrIME
PARAMETER RESULT
UNITS LIMIT REFERENCE STARTED ANALYST
TIC. BY SEMNOIATILE GC/MS 62UK70 1113r0317:00 WAD
625/6270 Tentatively Identified Compounds (10-largest TIC6):
,Identification Class, Cloeeet Spectral Fib cEat. Cann —
Unknown aliphatic hydrocarbon (Pentadecane) 61000 ug/kg
Unknown aliphatic hydrocarbon (Hexadecane) 54000 ug/kg
Unknown aliphatic hydrocarbon (Heptadecane) 62000 ug/kq
unionown aliphatic hydrocarbon (Pentadecane,tetramethyl) 33000 ug/kg
Unknown aliphatic hydrocarbon (Nonadecane) 46000 ug/kg
Unknown aliphatic hydrocarbon (Eic.... a) 32000 ug/kg
ouldnown aromatic hydrocarbon (Naphthalene, dimethyl) 60000 ug/kg
Unknown a ma[ic hydrocarbon (Unknown) 33000 ug/kg
Unknown accost hydrocarbon (Naphthalene, trimethyl) 30000 ug/kg
Unknown aromatic hydrocarbon (Naphthalene, trimethyl) 28000 ug/kg
BENZENE - Not detected ug/kg 1500 8260W5035 Vales 03:52 KC
BROMOSENZENE Not detected ug/kg 1500 8260W5035 115I0303:52 KC
BROMOCHLOROMETHANE NMdetected ugdcg 1500 8260W5035 11810303:52 KC
BROMODICHLOROMETHANE Notdetected ugAg 1500 8260815035 11810303B2 KC
BROMOFORM Not detected ug/kg Iwo 8260W5035 118/0303:52 KC
BROMOMETHANE Not retested ug/kg 30M 8260B/5035 1I8I0303:52 KC
N-BUTYLBENZENE 54W ug/kg 1500 8260B15035 11810303:52 KC
SEC-BUTYLBENZENE 4000 ug/kg 1500 8260W5035 bales 03:52 KC
TERT-BUTYLBENZENE Nottletected ug/kg 1500 82609/5035 1/810303S2 KC
CARBON TETRACHLORIDE Not detected ug/kg less 82600S035 1/8M303:52 KC
CHLOROBENZENE Not detected ug/kg 1500 8260W5035 11810303S2 KC
CHLORODIBROMOMETHANE Not detested ug/kg 1600 8260815035 Idly, 03:52 KC
CHLOROETHANE Not detected ug/kg 3" 82509/5035 11810303:52 KC
CHLOROFORM Not detectetl ug/kg 1500 8260915035 1I8I0303:52 KC
CHLOROMETHANE Notdetected ug/kg 3000 8260815035 1181030352 KC
2-CHLOROTOLUENE Not detected ug/kg 1500 8260015035 1I810303:52 KC
4-CHLOROTOLUENE Not detected ug/kg 1500 0260015035 1/810303:52 KC
1,2-DiBROMOaCHLOROPROPANE Not detected ug/kg 3000 8260815035 118/0303A2 KC
1,2-DIBROMOETHANE Notdetected ug/kg 1500 0260915035 1/81030352 NO
DIBROMOMETHANE Not detected ug/kg 1500 82603/5035 1I8/0303:52 KC
1,2-DICHLOROBENZENE Not detected Ug1kg 1500 8260915035 1181030362 NO
NC Cafficalmn No. 402 - SC Cedification No. 99D12 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Fee Number. 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
f�\ PRISM
d� ueaaAroe¢s.wc.
fW ServY.a.4uM4aa EnNmrvneMe.POxffiK
1/16/03
Page 26 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
. Attn: Mr. Rick Tamavechia
Customer Sample ID:
MW-2 rig 5
7300 Carmel Exec. Park Ste, 200
Prism Sample ID:
AC68593
Charlotte, INC 28226
Lopin Group:
51491<7
Sample Collection DateMme:
1/3/03
12:15
Lab Submittal Date/rime:
1/6/03
08:00
The following analytical results have been
obtained for the indicated sample which was submitted
to this laboratory
TEST
TEST
REPORTING
METHOD
DATETIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,3-0ICHLOROBENZENE
Not detected
Ug/kg
15M
026013I5035
11W0303:52
KC
1,4DICHLOROBENZENE
Not detected
ug/kg
1500
02608/5035
1I8I0303:52
KC
DICHLOROOIFLUOROMETHANE
Not detected
UgAg
1500
8280B15035
11610303:52
KC
11-0ICHLOROETHANE
Net detected
Ug/kg
ISoo
U60WW35
1I8I030352
KC
1,2-DICHLOROETHANE
Not detected
Ug/kg
1500
026OWS035
1181030352
KC
1,1-DICHLOROE7HENE
Not detected
ug/kg
150D
02mB15035
1181030352
KC
CIS-1,2-DICHLOROE7HENE
Not detected
ug/kg
1Sm
8260W5035
11810303:52
KC
TRANS-I,2-DICHLOROETHENE
Not detected
ug/kg
15M
826OW5035
11810303:52
KC
1,2-DICHLOROPROPANE
Not detected
Ug/kg
150)
8260B/5035
1/810303:52
KC
1,3-DICHLOROPROPANE
Not detected
ug/kg
ISM
02608/5035
1161030352
KC
2,2-DICHLOROPROPANE
Not detected
ug/kg
ism
8260WS035
118I0303:52
KC
IJ-DICHLOROPROPENE
Not dielectetl
ug/kg
1500
8260W5035
11810303:52
KC
ETHYLBENZENE
23M
Ug/kg
1500
826OW5035
1/OI0303:52
KO
HEXACHLOROBUTADIENE
Not detected
Ug/kg
15W
826081503E
1I810303:52
KC
tSOPROPYLBENZENE
33M
ug/kg
1500
826OWS035
11810303:52
KC
PASOPROPYLTOLUENE
35W
ug/kg
1500
826OW5035
VIV0303:52
KC
METHYLENE CHLORIDE
Not detected
ug/kg
30000
e260B/5035
11810303:52
KC
NAPHTHALENE
25000
ug/kg
1500
8260W5035
1/8/0303:52
KC
N-PROPYLBENZENE
700D
ug/kg
Ism
82608I5035
400303:52
KC
STYRENE
Not detected
ug/kg
1500
82609/5035
1I8/0303:52
KC
1,1,1,2-TETRACHLOROETHANE
Not detected
UgAg
1500
8260W5035
IISM303:52
KC
IA2,2-TETRACHLOROE7HANE
Not detected
ug/kg
15M
826OW5035
11810303:52
KC
TETRkCHLOROETHENE
Not detected
ug/kg
ism
8260W5035
11810303:52
KC
TOLUENE
Not detected
ug/kg
15M
826081503E
11810303:52
KC
1,2,1TRICHLOROBENZENE
Net detected
ug/kg
1500
8260W5035
11=303:62
KC
1,2,4TRICHLOROBENZENE
Not detected
Ug/kg
1500
826OW5035
TWO 03:52
KC
1,1,1.TRICHLOROETHANE
Not detected
ug/kg
1500
825OW5035
11810303:52
KC
IA2-TRICHLOROETHANE
Net detected
ug/kg
1500
02508/5035
1/010303:52
KC
TRICHLOROETHENE
Notdeleoted
ug/kg
1500
8260W5035
11910303:62
KC
TRICHLOROFLUOROMETHANE
Net detected
UgAg
1500
0260BIS035
1IM303:52
KC
1,23TRICHLOROPROPANE
Not detected
ug/kg
ism
026OB15035
11W0303:52
NO
NC Cediecation No. 402 - SC
Codification No. 99012
- NO Drinking Water Cart. No. 37735 - FL
Certification No.
E87519
449 Springbrook Road ♦ P.O.
Box 240543 A Charlene, NC 28224-0543
Phone: 704 / 529-6364 ♦ TOB Free Number:
1-80D / 529-6364 ♦
Fax: 704 / 525-0409
Lab Report
PRISM
_ ueoaAroxlFs,rac.
FLII sour a seN,o�maow saMio,�
1/16/03
Page 27 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanevechia
Customer Sample ID:
M1W4 5
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68593
Chadotte, INC 28226
Lopin Group:
5149K7
Sample Collection Date/Time:
1/3103 12:15
Lab Submittal Date/Time:
1/6/03 08:00
The following analytical results have been
obtained for the indicated sample which was submitted W this laboratory:
TEST
TEST
-
REPORTING
METHOD
DATEMME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,2.4TRIMETHYLBENZENE
20000
Wft
1500
8260BIW35 -
1/SI0303:52
KC
1,3,5-TRIME7HY1-BENZENE
11000
Ughog
1500
8260B15035
11=303:52
KC
VINYL CHLORIDE
Not detected
ug/kg
3000
8260B15035
V810303:52
KC
TOTALXYLENES-
Soon
ug/kg
15M
8260B15035
1810303:52
KC
2-8UTANONE(MEK)
Not dialectic
UgAg
15000
8260W5035
1I0/0303:52
KC
2-CHLOROETHYL VINYL ETHER
Not detected
ug/kg
3000
8260B/5035
1I8m303:52
KC
LMETHYL-2-PENTANONE(MIBK)
Not detected
ug/kg
15000
8260B15035
11=303:52
KC
ACETONE
Not detected
UgAg
30000
8260B/5035
ISV030352
KC
CARBON DISULFIDE
Not detected
ugiRg
30000
0260W5035
1I910303:52
KC
VINYLACETATE
Not detected
ug/kg
15000
02BOW5035
IIN0303:52
KC
CIS-1,3-DICKLOROPROPENE
Not detected
ug/kg
1500
82603I5035
1I8I0303S2
KC
TRANS-I,3-DICHLOROPROPENE
Net detected
ug/kg
1500
0250815035
11810303:52
NO
2496XANONE
Not detected!
ug/kg
15000
8260BI5035
1I810303:52
KC
IPE
Net detected
ugft
ISO
B2601315035
11810303:52
KC
WEE
Not detected
ug/kg
1500
82608I5035
1/BI0303:52
KC
SURR:DIBROMOFLUOROMETHANE
DO
%
72-137
8NOW5035
118I0303ZI!
KC
SURR:TOLUENE-D8
DO
%
73-128
8260BIW35
V8I0303:52
KC
SURR:BROMOFLUOROSENZENE
DO
%
69-131
8260BM35
11WO303:52
KC
C5-CS Nipmaos
Net detected
mgAg-
140
MADEPVPH
111410312:55
JMV
C9-012 AllphaOes
Net detected!
mglkg
120
MADEPVPH
11141W 12:55
JMV
C8-010 Aromatics
210
mpg
40
MADEPVPH
111410312:55
JMV
SvHgate%Recovery-PID
DO
%
(70-130)
MADEPVPH
111410312:55
JMV
Surrogate%Recovery -FID
DO
%
(70-130)
MADEPVPH
1114/0312:55
JMV
Dilution Factor
20
mg/kg
MADEPVPH
111410312:55
JMV
Dry Weight Received
IB.49B
mglkg
MADEPVPH
1114/0312ES
JMV
EXTRACTIONFOREPH Completed MADEP-EPH 1IN0316:00
JMK
09-018ALIPHATICS 22W mg/kg 40 MADEP-EPH 1IN0301:42
GRR
019-036ALIPHATICS 460 mglkg 20 MADEP-EPH 1I8I0301:42
GRR
Ctt-C22AROMATICS 16M mg/kg 20 MADEP-EPH 11810301:42
GRR
NO Certifcaton No. 402 - SC Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Tat Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
koftism
FWI SeMce.Ye! lIEnnvvtpnW SdWme
1116/03
Page 28 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tam vechia
Customer Sample ID:
MW-2 @ 5
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68593
Charlotte, NC 28226
Login Group:
5149K7
Sample Collection Date/Time:
113/03 12:15
Lab Submittal Date/Time:
116/03 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory'.
TEST
TEST
REPORTING
METHOD
DATETIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
SURROGATE RECOVERY -ALIPHATIC
-MI
%
(40-140)
MADEP£PH
11810301:42
GRR
SURROGATE RECOVERY - AROMATIC
'MI
%
(40.140)
MADEP-EPH
11&0301:42
GRR
SURR:2-FLUOROBIPHENYL
-MI
%
(40-140)
MADEP-EPH
118I030164
GRR
SURR:2-BROMONAPHTHALENE
-MI
%
- (40-140)
MADEP-EPH
11&0301:42
GRR
DILUTION FACTOR
1
mg/kg
MADEP-EPH
Vans 01:42
GRR
DRY WEIGHT
8.59
mg/kg
MADEP-EPH
1I60301:42
GRR
CALCULATIONS BASED ON DRY WT.
85
%DRY WT.
0.01
SM2UOG
1181031020
CWC
PREP, METHOD 35W
Completed
SWa1635508
1R10308:00
JDP
ACENAPHTHENE
Not detected
uglkg
3900
SW846 70C
111WWITA0
WAD
ACENAPHTHYLENE
Not detected
uglkg
3900
SVAW6-8270C
11IY031700
WAD
ANTHRACENE
Not tleteded
upiq
3900
SW846-8270C
1I13I0317:00
WAD
BENZO(A)ANTHRACENE
Notdetected
UgBg
3900
SWM(E8270C
111310317g0
WAD
BENZO(B)FLUORANTHENE
Not detestd
U9B9
3900
SW8463270C
1113I0317:00
WAD
BENZOUQFLUORANTHENE
Not detected
uglkg
3900
SW846-8270C
IIIW 317:00
WAD
BENZO(A)"RENE
Not detected
ugBg
3900
SW846-8270C
1I1W0317:00
WAD
BENZOtGHUPERYLENE
Net tleteded
ug/kg
3900
SWS488270C
1I1 W0317:00
WAD
BIS(2-CHLOROETHOXY)METHANE
Not detected
uglkg
3900
SWW-8270C
1HW0317.00
WAD
8I8(2-CHLOROETHYL)ETHER
Notdetected
Uglkg
3900
SW846-8270C
111310317:00
WAD
B15(2-CHLOROISOPROPYL)ETHER
Not detected
uglkg
390D
SW846-8270C
lh310317:W
WAD
BIS(2£THYLHEXYL)PHTHALATE
Not tleteded
ugAkg
3000
SW846-8270C
111W0317:00
WAD
4-BROMOPHENYL PHENYL ETHER
Not detected!
uglkg
39M
SW8463270C
1NW0317gO
WAD
BUTYL BENZYL PHTHALATE
Not tleteded
ug/kg
3900
SW848-8270C
111310317:00
WAD
4-CHLORO-3-METHYLPHENOL
Not tleteded
UgBg
3900
SWM-8270C
111W0317:00
WAD
2-CHLORONAPHTHALENE
Not tleteded
VgAg
39N
SW846d270C
l/IW03 ITO
WAD
2CHLOROPHENOL
Not detected
UgBg
3900
SW846-8270C
VIM 17A0
WAD
4-CHLOROPHENYL PHENYL ETHER
Not detect"
ug/kg
3900
SW6463270C
Ill 10317:00
WAD
CHRYSENE
Not detected
ug/kg
3900
SW846-8270C
1I13:N 17:00
WAD
OIBENZO(A,HANTHRACENE
Not tleteded
.UgBg
3900
SWMZ-8270C
1I13I0317:00
WAD
DIBENZOFURAN
Not tleteded
UgBg
39M
SWa468270C
VIWC317:00
WAD
DI-N-BUTYLPHTHALATE
Not detected
UgNg
3900
SW846-8270C
111W0317:00
WAD
NC Certification No. 402 - SC CeNfcaeon No. 99012
- NO Drinking
Water Can. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦
Charlotte, NC
28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-900 /
529-6364 ♦ F. 704 / 525-0409
Lab Report
PRISM
�- ueoeAroelsgtxc
Fov semreAreNnea n se.Im�meoW slow,..
1A 6/03
Page 29 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Alm Mr. Rick Tanavechia
Customer Sample ID:
MW-2 @ 5
7300 Carmel Exec. Park Ste, 200
Prism Sample ID:
AC68593
Charlotte, NC 28226
Login Group:
51491<7
Sample Collection Date/Time:
1/3103 12:15
Lab Submittal Dale/Time:
1/6103 0800
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATETIME
'PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,2-DICHLOROBENZENE
Not detected
uglkg
3900
SW048-8270C
IIIW0317:00
WAD
1,3-DICHLOR09ENZENE
Not detected
UgBg
3900
SW8463270C
111&'0317:00
WAD
1,4-DICHLOROBENZENE
Not detected
UgBg
3900
SWUM270C
l/l W0317:00
WAD
2,4-DICHLOROPHENOL
Notcetected
Ug/kg
3900
SW846-8270C
111W0317:00
WAD
DIETHYL PHTHALATE
Neltletected
ugBg
3900
SW846-8270C
111W0317:00
WAD
2,4-DIMETHYLPHENOL
Not detected
UgBg
3900
SWU64270C
111W0317:00
WAD
DIMETHYL PHTHALATE
Noldeteded
ug/kg
3900
SWUS4270C
111W0317:00
WAD
2,4-DINITROPHENOL
Not detected
uglkg
19500
SW846-6270C
VISI0317:00
WAD
2,4-DINITROTOLUENE
Not detected
UgAg
3900
SW846-8270C
111W0317:00
WAD
2,6-DINITROTOLUENE
Not detected
Ug/kg
3900
SW846-8270C
111W031700
WAD
DI-N-OCTYLPHTHAIATE
Not tleteded
uglkg
3900
SW846-8270C
1I1W0317:00
WAD
FLUORANTHENE
Not tleteded
Uglkg
3900
SW846-8270C
1H&W 17:00
WAD
FLUORENE
Saw
ug/kg '
3900
SWB6-8270C
111&031700
WAD
HEXACHLOROBENZENE
Not tleteded
UgBg
3900
SW846-6270C
111W031700
WAD
HEXACHLOROBUTADIENE
Nottletected
ugtkg
3900
SW8,t"270C
111WW 1700
WAD
HEXACHLOROOYCLOPENTADIENE
Not deleoted
UgBg
3900
SWUS4270C
111W0317:00
WAD
HEXACHLOROETHANE
Not detected
UgBg
3900
SW8463270C
111W0317:00
WAD
INDENO(1,2,3-CD)PYRENE
Not tleteded
uglkg
3900
SW84S45270C
111&0317:00
WAD
ISOPHORONE
Not detected
ug/kg
39W
SWS4 lx?70C
111SIO 17:00
WAD
2-METHYL4,6-DINITROPHENOL
Not detected
UgBg
19500
SWW-8270C
111W0317:00
WAD
2-METHYL NAPHTHALENE
76M
ug/kg
39M
SW066-8270C
111W0317:00
WAD
2-METHYL-PHENOL
Not detected'
ugIkg
3900
SW846-8270C
I/l W0317aO
WAD
4-METHYL-PHENOL
Net tleteded
UgBg
3900
SW846-8270C
WW03 P:00
WAD
NAPHTHALENE
7100
UgBg
3800
SW846.8270C
1I1W0317gO
WAD
NITROBENZENE
Not detected
UgBg
3900
SWINiM270C
1I1&0317:00
WAD
2-NITROPHENOL
Nottletected
uglkg
3900
SW846-8270C
111W0317:0
WAD
4-NITROPHENOL
Not detected
Uglkg
195M
SW846-8270C
1/l S/%17:00
WAD
N-NITROSODIPHENYIAMINE
Not detected
UgBg
3900
SW846-8270C
VIVO Ill=
WAD
N-NITROSODI-N-PROPYLAMINE
Not tleteded
UgBg
3900
SW846-8270C
1/1310317:00
WAD
PENTACHLOROPHENOL
Not detected
uglkg
19500
SW846-8270C
Ill W0317:00
WAD
PHENANTHRENE
15000
uglkg
3900
SW846-8270C
1I1W031700
WAD
NO Certfication No. 402 - SC Ccr i8cabon
No. 99012
- NO Dunking
Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook
Road ♦ P.O.
Box 240543
♦ Charlotte. NC
2822,1-0543
Phone: 704 / 529-63M ♦ Toll Free Number:
1-800 / 529-6364 ♦ F.: 704 / 525-0409

Lab Report
PRISM
ueowroeice, INC
FW Sr 16 EnWrnmenW Stluhm
1/16/03
Page 30 of 42
ERM Southeast, Inc.
Customer Project ID: VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID: MW-2 a 5
7300 Carmel Exec. Park Ste. 200
Prism Sample ID: AC68593
Charlotte, NC 28226
Logtn Group: 5149K7
Sample Collection Date/Time: 1/3/03 12:15
Lab Submittal Date77ime: 1/6/03 08:00
The following analytical results have been obtained
for the indicated sample which was submitted to this laboratory:
TEST TEST
REPORTING METHOD DATITIME
PARAMETER RESULT
UNITS LIMIT REFERENCE STARTED ANALYST
PHENOL Not detected
ug/kg 3900 SW046A270C 111310317:00 WAD
PYRENE Not detected
ug/kg 3900 SW846-8270C 1113103 Wad WAD
1,2,4-TRICHLOROBENZENE NMdetected
ug/kg 3900 SW846-827OC 1113N31TAO WAD
2,4.5-TmCHLOROPHENOL Not detected
ug/kg 3900 SW846-0270C 1113103 17:00 WAD
2,4,6-TRICHLOROPHENOL Not detected
ugfK9 3900 SW846-8270C 1/1310317:00 WAD
Sample Comments:
Analysis note for EPH:'- Surrogate recovery was outside the control limits due to matrix interference.
Analysis note for 8260: '- The surrogates were
diluted out at a 1:500 dilution.
Analysis note for VPH: The surrogates were diluted out at a 1:20 dilution.
Angela D. Overcash, V.P. Laboratory Services
NO Certification No. 402 - SC Certifmation No. 99012 - NO Dunking Water Cert. No. 37735 - FL Certification No. E87519
449 Spdngbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28214-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: [phone]
Lab Report
1/16103
ERM Southeast, Inc.
Attn: Mr. Rick Tanavechia
7300 Carmel Exec. Park Ste. 200
ChadoBe, NC 28226
The following analytical results have
PRISM
uaow,roniEs.mc
Put Emho,menel SaM1,Nne
Page 31 of 42
Customer Project ID: VMG
Customer Sample ID: MW-2 @ 10
Prism Sample ID: AC68594
Login Group: 5149K7
Sample Collection Date/Time: 1/3/03 12:25
Lab Submittal DatefTime: 1/6/03 08:00
been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATETIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
TIC48YSEMIVOLATILEGGMS
62518270
t/910312:05
WAD
625/8270 Tentatively Identified
Compounds
(30-largest
TICS):
<Identification Class>
<Closest
Spectral Fit>
<Est. Onto—
.. — .......................
No TIC'S were detected.
==.=. ......................
............
BENZENE
Not detected
ug/kg
290
8260N5035
1I8103 o4:30
KC
BROMOBENZENE
Not detected
ug/kg.
290
B260W5035
100303:30
NO
BROMOCHLOROMETHANE
Not detected
ug/kg
29D
U60BI5035
11810304:30
KC
BROMODICHLOROMETHANE
Not detected
ug/kg
290
82600I5035
VIV0304:30
KC
BROMOFORM
Not detected
ug/kg
290
8250B/5035
11810304:30
KC
BROMOMETHANE
Not detected
ug/kg
580
U606/5035
11&0304:30
KC
N-6UTYWENZENE
Not detected
ug/kg
290
8260815035
1AV0304:30
KC
SEO-BUTYLBENZENE
Not detected
ug/kg
290
8260615035
118,0304:30
KC
TERT-BUTYLBENZENE
Not detected
ug/kg
290
8260B15035
11810304:30
KC
CARBON TETRACHLORIDE -
Not detected
ugAg
290
8260D/5035
11&0304:30
KC
CHLOROBENZENE
Not detected
ugAg
290
8260BIW35
11&03(W30
KC
CHLORODIBROMOMETHANE
Not detected
ug/kg
290
8260B/W35
1189304:30
KC
CHLOROETHANE
Not detected
ug/kg
580
8260B15035
100304:30
KC
CHLOROFORM
Not detected
ug/kg
290
8260B15035
11810304SO
KC
CHLOROMETHANE
Not detected
ug/kg
580
8260B/5035
118103 O,1SO
KC
2-0HLOROTOLUENE
Not detected
ug/kg
290
8260W5035
1I8ID304:30
KC
4-CHLOROTOLUENE
Not detected
ugAg
290
8260B15035
1/&0304:30
KC
1,2-0IBROMO-3-CHLOROPROPANE
Not detected
ug/kg
580
8260B15035
1/8/0304:30
KC
1,2.DIBROMOETHANE
Not detected
ug/kg
290
B260W5035
118/03 DC30
KC
DIBROMOMETHANE
Not detected
Uglkg
290
8260015035
11810304:30
KC
1.2.DICHLOROBENZENE
Not detected
ugBg
290
826OB15035
11810304:30
KC
1,3-DICHLOROBENZENE
Not detected
ug/kg
290
62SOB15035
11810304:30
KC
1.4-0ICHLOROBENZENE
Not detected
ug/kg
290
8260B15035
1/810y 04:30
KC
DICHLORODIFLUOROMETHANE
Not detected
ug/kg
290
826OB15035
1/803 oa30
KC
1,1-DICHLOROETHANE
Not detected
ug/kg
290
8260B15035
118/0304:30
KC
1,2-DICHLOROETHANE
Not detected
ug/kg
290
8260WS035
1/81030430
KC
NC Ceft icatlan No. 402 - SC Cedlficabon
No. 99012
- NO Onnong
Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦ Charlotte, NC 28224-0543
Phone: [phone] ♦ Toll Free Number: 1-800 / 529-6364 A
Fax: 704 / 525-0409

Lab Report
PRISM
f "_ ueoxxroelea, mc.
FPutl Servo MxMMky a EnvhmmaMSl SOWloiu
1/16/03
Page 32 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarrevechla
Customer Sample ID:
MW-2 ®10
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC68594
Charlotte, NC 28226
Loan Group:
5149K7
Sample Collection Date/Time:
1/3103 12:25
Lab Submittal Date7Tene:
1/6/03 0800
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATERIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
11-DICHLOROETHENE
Not detected
ugft
290
826OW5035
1I810304:30
KC
CIS-1,2-DICHLOROETHENE
Not detected
ugMg
290
826OB15035
1/8103":so
KC
TRANS-I,2-DICHLOROETHENE
Notdeteced
ugft
290
8260B/5035
V810304:30
KC
1,2-DICHLOROPROPANE
Not detected
ug/kg
290
8260WS035
11810304:30
KC
1,SDICHLOROPROPANE
Not detected
u1
290
8260BIK35
118/0304:30
KC
2,2-0ICHLOROPROPANE
Not detected
upg
290
82601115035
118/0304:30
KC
1,1-DICHLOROPROPENE
Not detected
ugAg
290
826OB15035
1I8/0304:30
KC
ETHYLBENZENE
Not detected
ug/kg
290
826OB15035
1I8/0 NSO
KC
HEMCHLOR08UTADIENE
Not detected
ugft
290
025OW5035
1181030430
KC
ISOPROPYLBENZENE
Noldeteded
ug/kg
290
8260915035
11810304:30
KC
PASOPROPYLTOLUENE
Notdeteced
uglkg
2W
826OWS035
11810306:30
KC
METHYLENE CHLORI OE
Notdetacted
uglkg
5800
82608IW35
11W030,120
KC
NAPHTHALENE
630
Li
290
82608IW35
118103 N:30
KC
N-PROPYLBENZENE
Notdetacted
ug)kg
290
826OBW35
1/8I0304:30
KC
STYRENE
Not detected
ug/kg
290
8260B15035
11810304:30
KC
1, 1, 1.2-TETRACHLOROETHANE
Not detected
ug/kg
290
8260B15035
11810304SO
KC
1, 1,22-TETRACHLOROETHANE
Not detected
ug/kg
290
8260BIS035
1/W03a4:3o
KC
TETRACHLOROETHENE
Not deluded
ugAg
290
OMB15035
1/81030430
KC
TOLUENE
Not deteded
ug/kg
290
3260815035
11810'104:30
KC
1,2,3-TRICHLOROBENZENE
Not detected
ugAg
290
enOW5035
11810304:30
KC
1,2.0.TRICHLOROBENZENE
Not detected
ug/kg
290
826OW5035
1I8I0304:30
KC
1,1,1-TRICHLOROETRANE
Not detected
ug/kg
290
82609I5035
1ISM304:30
KC
1,1,2-TRICHLOROETHARE
Not detected
uglkg
290
82608/5035
11810306:30
KC
TRICHLOROETHENE
Not deteded
ugNg
290
82608/5035
100304:30
KC
TRICHLOROFLUOROMETHANE
Not detected
uglkg
290
8260815035
100304:30
KC
1,2,3-TRICHLOROPROPANE
Not deduced
ug/kg
290
826OB15035
1/6IO304:30
KC
1,2,4TRIMETHYLBENZENE
430
ug/kg
290
826OB15035
1I8I0304:30
KC
1,3,5-TRIMETHYLBENZENE
Not deeded
ug/kg
290
62BOW5035
110I03(Mal)
KC
VINYL CHLORIDE
Not detected
ug/kg
580
02SOBI5035
1I810304:30
KC
TOTALXYLENES
Not detected
ugNg
290
02WBI5035
118,0304:30
KC
2-BUTANONE(MEK)
Not detected
aglkg
2900
826OW5035
1AW?04:30
KC
NC Codification No. 402 - SC Certification
No. 99012
- NC Drinking
Water Cart. No. 37735 - FL
Certification No.
E87519
449 Springbrook Road 4 P.O.
Box 240543
♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364
♦ Toll Free Number. 1-800 / 529-6364 ♦
F. 704 / 525-0409
Lab Report
PRISM
ueaxAroBlas.mc.
Fw � M.ySa a ama_w sdwoia
1/16/03
Page 33 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanavechia
Customer Sample ID:
MW-2 @ 10
7300 Cannel Exec. Park Ste. 200
Prism Samole ID:
AC68594
Charlotte, NC 28M
Lupin Group:
51491<7
Sample Collection Date/Time:
113/03 1225
Lab Submittal Date7Time:
116/03 0800
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DA=IME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
2-0HLOROETHYL VINYL ETHER
Notdeaced
ug/kg
sea
8260315035
11810304:30
KC
4-METHYL-2-PENTMONE took)
Not detected
uglkg
2900
826OD15035
11810304:30
KC
ACETONE
Not detected
ug/kg
5800
826OW5035
1,810304:30
KC
CARBON DISULFIDE
Not deter4ed
ugft
5800
8260H/5035
118I0304:30
KC
VINYLACETATE
Not detected
ugft
2900
826OW5035
V810304:30
KC
CISI,3-DICHLOROPROPENE
Not detected
ug/kg
290
8MR15035
11=304:30
KC
TRANS-I,3-DICHLOROPROPENE
Not detected
ug/kg
290
826OW5035
118103 G4:30
KC
2-HEXANONE
Not detected
ug/kg
2900
82501315035
11810304:30
KC
IPE
Not detected
ug/kg
290
826OD15035
1/8,0304:30
KC
MTBE
Not detected
uglkg
290
82600IM35
11W03(NiSo
KC
SURRDIBROMOFLUOROMETHANE
105
%
72-137
8260B15035
1/810304:30
KC
SURR:TOWENE-D8
119
%
73-128
826OB15035
118I0304:30
KC
SURR:BROMOFLUOROBENZENE
121
%
69.131
826OB1035
1I810304:30
KC
CS-08 AIIp1Ha60.1
Not detected!
mg/kg
7
MADEPVPH
1113,0322:51
JMV
0& 12AIIVhtuds
Not detected
mg/kg
6
MADEPVPH
1I1310322:51
JMV
09C10 Af0matlas -
Not detected
mglkg
2
MADEPVPH
111310322:51
JMV
Sumogate%Recovery -PID
80
%
(70-130)
MADEPVPH
11131WM51
JMV
Surrogate%Recovery - FIG
83
%
(70-130)
MADEPVPH
1113I0322:51
JMV
Dilution Factor
1
mg/kg
MADEPVPH
111310322:51
JMV
cry Weight Received
16,119
mglkg
MADEPVPH
111V0322:51
JMV
EXTRACTION FOR EPH Completed
MADEPVPH
11610316:00
JMK
C9-C18 ALIPHATICS Not detected mg/kg
40 MADEP-EPH
11810303:24
GRR
CIfrC36 ALIPHATIC$ Not detected mg/kg
20 MADEP-EPH
11WOS 03:24
GRR
C11L22 AROMATICS Not detected mg/kg
20 MADEP-EPH
1I81030324
GRR
SURROGATE RECOVERY -ALIPHATIC 89 %
(40-140) MADEP-EPH
11810303:24
GRR
SURROGATE RECOVERY -AROMATIC 105 %
(4 140) MADEP-EPH
11810303:24
GRR
SURR:2-FLUOROBIPHENYL 89 %
(40-140) MAOEP-EPH
1I81030324
GRR
SURR:2-BROMONAPHTHALENE 92 %
(40-140) MADEP-EPH
100303:24
GRR
DILUTION FACTOR 1 mg/kg
MADEP-EPH
VEM 03:24
GRR
NC Cedification No. 402 - SC Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 4 Toll Free Number: 1-800
/ 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
PRISM
ueo64Tomes,Wc.
��_
'
- FW SnNx MuMkN d EMrmmeNel $Mutisu
. 1116103
Page 34 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tanavechia
Customer Sample ID:
MW-2 10
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC68594
Charlotte, INC 28226
Lapin Group:
5149K7
Sample Collection DalaTime:
1/3103 12:25
Lab Submittal Date[Time:
1/6103 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory.
TEST TEST REPORTING METHOD DATENIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
ORYWEIGHT 8.5It mg/kg MADEP-EPH 11B1030324 GRR
CALCUTATIONS BASED ON DRY WT.
85
%DRY WT.
0.01
SM 2540G
lIV6310:20
cwc
PREP. METHOD 3550
Completed
SW846J5500
117103"po
JDP
ACENAPHTHENE
Not detected
waft
400
SW846A270C
119I0312:05
WAD
ACENAPHTHYLENE
Notdetected
ugBg
400
SW846A270G
19I0312:05
WAD
ANTHRACENE
Not detected
ugkg
400
SWS4 8270C
100312:05
WAD
BENZO(A)AN ARACENE
Not detected
ug/kg
400
SW846A2700
1NI0312:05
WAD
BENZOIB)FLUORANTHENE
Notdetected
ug/kg
400
SW646A270C
119N312:05
WAD
BENZO(K)FLUORANTHENE
Notdetected
UgAg
400
SW846-6270C
1MM312:05
WAD
BENZO(A)PYRENE
Notdetected
ugAg
400
SW046A270C
IMM31205
WAD
BENZO(GHUPERYLENE
Notdetected
Uglkg
400
SWB46A270C
1I9/0312:05
WAD
BIS(2LHLOROETHOXY)METHANE
Notdetected
UgAg
400
SW846-8Z70C
V9/0S 12:05
WAD
BIS(2LHLOR0ETHYL)ETHER
Not detected
ug/kg
400
SWUM270C
11W0312:05
WAD
BIS(2-CHLOROISOPROPYL)ETHER
Notdetected
ug/kg
400
SWS4 8270C
M)0312:05
WAD
BIS(2-ETHYLHEXYL)PH7HALATE
Notdetected
ug/kg
400
SW048.8270C
100312:05
WAD
4-BROMOPHENYL PHENYL ETHER
Notdetected
ug/kg
400
SWB4 8270C
1191031205
WAD
BUTYL BENZYL PHTHALATE
Notdetected
ug/kg
t00
SW846-8270C
11910312:05
WAD
4CHLOROdMETHYLPHENOL
Notdetected
ug/kg
400
SWB4 8270C
11910312:05
WAD
2-CHLORONAPHTHALENE
Notdetected
ug/kg
400
SWB468270C
IM10312:05
WAD
2L11LOROPHENOL
Not detected
ug/kg
400
SW0468270C
119/0312:05
WAD
4-CHLOROPHENYL PHENYL ETHER
Notdetected
ug/kg
400
SWI4 8270C
IG/0312:05
WAD
CHRYSENE
Not dotected
ug/kg
400
SW& 270C
1191012:05
WAD
DIBENZO(A,H)ANTHRACENE
Notdetected
ug/kg
400
SW846-8270C
11910312:05
WAD
DIBENZOFURAN
Not detected
ug/kg
40
SWB46-8270C
119/031205
WAD
DINAUTYLPH7HALATE
Not detected
ug/kg
400
SW048-8270C
1191012:05
WAD
1,2.DICHLOROBENZENE
Not detected
Uglkg
400
SWB4 8270C
1MM312:05
WAD
1,3DICHLOROBENZENE
Notdetected
UgAg
400
SW848-82700
11910312:05
WAD
1,4-DICHLOROSENZENE
Net detected
UgAg
400
SWW-6270C
11910312:05
WAD
2,4DIGHLOROPHENOL
Not detMed
ug/kg
400
SWIPI"270C
11W0312:05
WAD
DIETHYL PHTHALATE
Notdetected
UgAg
400
SW& 270C
1191012:05
WAD
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking Water Cent.
No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number. 1-800 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
PRISM
ueoRxToalEs,txc.
FW eervlm Melyli'el d Emimrvnmel ealWma
1/16/03
Page 35 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-2 @ 10
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
ACS8594
Charlotte, INC 28226
Login Group:
5149K7
Sample Collection Date/Time:
113103 12:25
Lab Submittal Date/Time:
1/6/03 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEITIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
2,4DIMETHYLPHENOL
Not detected
ug41g
400
SWB46A270C
1/9/0312:05
WAD
DIMETHYL PHTHALATE
Not detected
ug/kg
400
SW846A270C
1/9/0312:05
WAD
2,4-DINITROPHENOL
Notdetected
ug/kg
2000
SW846-8270C
1MI0312:05
WAD
2,4DINITROTOLUENE
Notdetected
ug/kg
400
SW846-82700
11910312:05
WAD
2,6-DINITROTOLUENE
Not detodod
ug/kg
400
SW046A270C
11910012:05
WAD
DI-N-OCTYLPHTHALATE
Notdetected
ug/kg
400
SW046.0270C
119/0312:05
WAD
FLUORANTHENE
Notdetected
ug/kg
400
SWW-8270C
1191031205
WAD
FLUORENE
Notdetected
ug/kg
400
SW8468270C
11910312:05
WAD
HEXACHLOROBENZENE
Notdetected
Uglkg
400
SWB46-8270C
1191031205
WAD
HEXACHLOROBUTAOIENE
Notdetected
ug/kg
400
SW846A270C
1I9I0312:05
WAD
HEMCHLOROCYCLOPENTADIENE
Notdetected
ug/kg
400
SWB46A270C
100212:05
WAD
HEXACHLOROETHANE
Notdetected
ug/kg
400
SWMA270C
119/0312:05
WAD
INDENO(1.2,3 D)PYRENE
Notdetected
ug/kg
400
SW& 270C
IM0312:05
WAD
ISOPHORONE
Not detecetl
ug/kg
400
SWB46A270C
IM10312:05
WAD
2-METHYL4,6-DINITROPHENOL
Not Bete Aol
ug/kg
2000
SW846A270C
1/9/0312o5
WAD
2-METHYL NAPHTHALENE
Not detected
ug/kg
400
SWB46A270C
IM10312:05
WAD
2-METHYL-PHENOL
Notdetected
UgAg
400
SWMA2700
1I9I03 12:05
WAD
44ETHYL-PHENOL
Not detected
ug/kg
400
SW845-82700
1/9I0312.05
WAD
NAPHTHALENE
Notdetected
ug/kg
400
SW846A270C
11910312:05
WAD
NITROBENZENE
Not detected
ug/kg
400
SW846A270C
11910312O5
WAD
2-NITROPHENOL
Notdetected
ug&g
400
SWW-8270C
1/9/0312:05
WAD
4-NITROPHENOL
Notdetected
Ug/kg
2000
SW846A270C
1/91W 12:06
WAD
N-NITROSODIPHENYLAMINE
Notdetected
ug4tg
400
SW846A270C
1/9/031295
WAD
NNITROSODI-N-PROPYIAMINE
Not detected
ug/kg
400
SWS4 8270C
1/9*312:05
WAD
PENTACHLOROPHENOL
Not detected
UgAg
2000
SWUM270C
1510312:05
WAD
PHENANTHRENE
Notdetected
UgAg
4D0
SWU64270C
IM0312:05
WAD
PHENOL
Notdetected
ug1k9
400
SW846427X
1/9/0312:05
WAD
PYRENE
Not detected
ug*g
400
SW846d270C
M0312:05
WAD
1.2,4TRIOHLOROBENZENE
Notdetected
ug/kg
400
SW846A270C
11910312:05
WAD
2.4,5-TRICHLOROPHENOL
Notdetected
ug/kg
400
SW846A270C
11910312:05
WAD
2,4,6TRICHLOROPHENOL
Notdetected
ug/kg
400
SWa46-0270C
11WO312:05
WAD
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking
Water Cart. No. 37735 - FL Certification No.
E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
1/16/03
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NO 28226
A\PRISM
Full&x I.,uMtsl a sonmmmmMl SdAmns
Page 36 of 42
Customer Project ID:
VMG
Customer Sample ID:
MW-2@10
Prism Sample ID:
ACS8594
Login Grand:
5149K7
Sample Collection Date/Tme:
1/3/03 12:25
Lab Submittal Date/rime:
1/6/03 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory.
TEST TEST REPORTING METHOD DATE71ME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
Angela D. Overcesh, V.P. Laboratory Services
NC Certification No. 402 - SC Certifi..t.r No. 99012 - NC Drinking Water Ced. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charisma, NC 28224-0543
Phone: [phone]CA ♦ Toll Ford Number. 1-800 / 529-6364 A Fart 704 / 525-0409
Lab Report
PRISM
ONNttIPIEa,INF
Full So. ao.10.1. EnA.aoel So..
1116/03
Page 37
of 42
ERM Southeast, Inc.
Customer
Project
ID: VMG
Attn: Mr. Rick Tarravechia
Customer Sample
ID: MW-2@15
7300 Cannel Exec. Park Ste. 200
Prism Sample
ID: AC66595
Login Group: 5149K7
Charlade. NC 28226
Sample Collection Date7Time:
1/3/03
1240
Lab Submittal Dale/rime:
1/6103
08:00
The following analytical results have
been obtained for the Indicated
sample
which was submitted
to this
laboratory:
TEST
TEST
REPORTING
METHOD
DATETIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
TICS BY SEMIVOLATILE GCIMS
6298270
1191032008
WAD
625/6270 Tentatively Identified
Compounds (10-largest
TICe):
cIdentification Clas S>
dl0eest Spectral sib
cE.t. Conc.>
---------- ---------------___—..--______--
No TIC'. were detected.
------------
BENZENE
5.7
UgAg
5.0
82601315035
11910302:37
KC
BROMOBENZENE
Not detected
upkg
SA
8260BIN35
1191030237
KC
BROMOCHLOROMETHANE
Not detected
UgAg
5.o
8260BM35
1191030237
KC
BROMODICHLOROMETHANE
Not detected
Ug/kg
5.0
8260BM35
1/91030237
KC
BROMOFORM
Not detected
Ug/k9
50
82WBI5035
1/210302:37
KC
BROMOMETHANE
Not detected
ug/kg
10.0
82WO15035
1/910302:37
KC
N-BUTYLBENZENE
Not detected
ug/kg
50
8260B/5035
119/0302:37
KC
SEC-BUTYWENZENE
Notdetetted
uglkg
Se
8260BIB035
19/0302:37
INC
TERT-BUTYLBENZENE
Not detested
UgAg
$.a
8260BM35
1910302:37
KC
CARBON TETRACHLORIDE
Not Interest
UgAg
5.0
e260B15035
1M10302S7
KC
CHLOROBENZENE
Not detected
UgAg
5.0
8260B/5035
19I0302:37
KC
CHLOROOIBROMOMETHANE
Not detetted
ug/kg
5.o
826oB/5035
191W 02:37
KC
OHLOROETHANE
Not detected
Ug/kg
10.0
8260BM35
1910302:37
KC
CHLOROFORM
Not detected
UgAg
5.0
6260B/5035
1910302:37
KC
CHLOROMETHANE
Not detected
ugft
too
826OB15035
1Islas 02:37
KC
2-CHLOROTOLUENE
Not detected
UgMg
5.0
8260B/5035
IM10302:37
KC
4CHLOROTOLUENE
Not detected
Ug/kg
5.0
8260B15035
1I9N302:37
KC
1.2-DIBROMO-3-CHLOROPROPANE
Not detected
UgAg
10,0
8260B15035
1/910:,02:37
KC
1.2-DIBROMOETHANE
Not detered
uglkg
5.0
826OB15035
11910302:37
KC
DIBROMOMETHANE
Not detected
UgAg
5.0
8260B15035
IN10302:37
KC
1,2-DICHLOROBENZENE
Not detected
uglkg
So
826OB15035
191W 02:37
KC
1,3-DICHLOROBENZENE
Not detected
UgAg
5.0
8260W50M
IN10302:37
KC
1.4DICHLOROBENZENE
Not detested
uglkg
5.0
8260B15035
IN10302:37
KC
DICHLORODIFLUCROMETHANE
Notdetetted
ug/k9
5.0
8260B15035
1910302:37
KC
1,1-DIOHLOROETHANE
Not detected
ug/k9
5.0
8260W5035
1/910302:37
KC
1,2-DICHLOROETHANE
Not detetted
UgAg
So
8260B15035
1/91030237
KC
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Gen. No. 37735 - FL Cenifcation No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-900 / 529-6364 1 Fax: 704 / 525-0409

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Lab Report
AL y
PRISM
L.R OP IOPIEa, INe.
FNI So. M9 . A Emimnmanrel Sdulbne
1/16/03
Page 40 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Atthn Mr. Rick Tarravechia
Customer Sample ID:
1,1111IF-2@15
7300 Cannel Exec. Park Ste. 200
- Prism Sample ID:
AC68595
' Charlotte, NC 28226
Loon Group:
5149K7
Sample Collection Date/Time:
113/03
12:40
Lab Submittal Date/Time:
1/6/03
08:0D
The following analytical results have been
obtained for the indicated sample which was submitted
to this laboratory:
TEST TEST REPORTING METHOD DATEFTIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
DRYWEIGHT 7.5g mglkg MADEP-EPH 1/810305:07 GRR
CALCULATIONS BASED ON DRY WT.
75
%DRY WT.
0.01
SM 2540G
118N31010
cWC
PREP. METHOD 35M
Completed
SW646-35508
1UN300:00
JDP
ACENAPHTHENE
Not detected
Ug/kg
450
SW8468270C
11910320:08
WAD
ACENAPHTHYLENE
Not detected
Uglk9
450
SW846-8270C
11910320:08
WAD
ANTHRACENE
Net detected!
ugAg
450
SW846A270C
1/E0320:08
WAD
BENZO(A)AWTHRACENE
Not detected
ug/kg
450
SW846A270C
11910320:08
WAD
BENZO(B)FLUORANTHENE
Not detected
ug/kg
450
SWW-8270C
INN320:08
WAD
BENZO(K)FLUORANTHENE
Not detected
ug/kg
450
SWB4682700
IM10320CS
WAD
BENZO(A)PYRENE
Not detected
ug/kg
450
SW846827X
IM10320M
WAD
BENZO(GHI)PERYLENE
Not detected
ug/kg
450
SW848-82711C
1191032008
WAD
SIS(2-CHLOROETHOYY)METHANE
Not detected
ug/kg
450
SW8468270C
1/91)320:08
WAD
BIS(2-CHLOROETHYL)ETHER
Net detected
Ug/kg
450
Sw848A270C
1/9N320:08
WAD
BIS(2CHLOROISOPROPYL)ETHER
Not detected
ug/kg
450
SW846A270C
1/91032008
WAD
BIS(2-ETHY1-HEXYL)PHTHALATE
Not detected
ug/kg
460
SW846A270C
1/910320:08
WAD
4-BROMOPHENYL PHENYL ETHER
Not detected
ugkg
450
SW8468270C
11910320:08
WAD
BUYL BENZYL PHTHAIATE
Not detected
Uglk9
450
SW8468270G
IR1032008
WAD
4-0HLORO-3-METHYLPHENOL
Not detected
Ug/kg
450
SW8468270C
1191032008
WAD
2-CHLORONAPHTHALENE
Not detected
Ug/kg
450
SWW-8270C
119/0,. 20:08
WAD
2-CHLOROPHENOL
NMdetecled
ug/xg
450
SWM-8270C
11910320:OB
WAD
4-CHLOROPHENYL PHENYL ETHER
Not detected
UPI;;
450
SW846-8270C
119/0320:08
WAD
CHRYSENE
Not detected
ug/kg
450
SW846-82700
1/910320:08
WAD
DIBENZO(A,H)AHTHRACENE
Not detected
ug/kg
450
SW846-027DC
1W0320:08
WAD
DISENZOFURAN
Not detected
ug/kg
450
SWB45-8270C
IM10320:08
WAD
DbN-DUTYLPHTHAIATE
Not detected
Ug/kg
450
SWUM270C
1/9/0320:08
WAD
1,2-DICHLOROBENZENE
Not detected
uglkg
450
SW846A270C
1/9/0320:08
WAD
1,3-DICHLOROBENZENE
Net detected
Ug/kg
450
SW846A270C
119/0320:08
WAD
1,4DICHLOROBENZENE
Net detected
UgAg
450
SW846A270C
11910320:08
WAD
2,4-DGHLOROPHENOL
Notdetected
UgAg
450
SW846.8270C
1/91032008
WAD
DIETHYL PHTHALATE
Notdetected
ug/kg
450
SW646A270C
11910320:08
WAD
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking Water Can.
No. 37735 - FL Certification No. E87519
449 Springbmok Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number:
1-800 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
PRISM
ueowmBras.INc.
FNI $eMce AmNllml It EmirnmeMel 6cMons
1116/03
Page 41 of 42
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-2 @ 15
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC68595
Charlotte, NC 28226
Lapin Group:
5149K7
Sample Collection Date/Time:
1/3/03 12:40
Lab Submittal Date/Time:
116103 08:00
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATETIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
2,4-DIME1-HYLPHENOL
Not detected
Ug/kg
450
SW846A270C
11910320:08
WAD
DIMETHYL PHTHALATE
Not detected
ug/kg
450
SW846-8270C
119/032008
WAD
2,4DINITROPHENOL
Not detected
ug/kg
2250
SWMB-8270C
119/0320:N
WAD
2,4-DINITROTOLUENE
Not detected
ug/kg
450
SW845-82700
119/0320:08
WAD
2,6-0INITROTOLUENE
Not detected
ug/kg
450
SW8468270C
119/0320:08
WAD
DI-N-OCTYtPHTHAIATE
Not detected
Upg
450
sW846A2703
11910320:08
WAD
FLUORANTHENE
Not detected
ug/xg
450
SW046A2mC
1191M 2008
WAD
FLUORENE
Not detected
Ug/kg
450
SW846A270C
11910320:08
WAD
HEXACHLOROBENZENE
Not detected
ugkg
450
SW845.8270C
1191032008
WAD
HEXACHLOROBUTADIENE
Not detected
UgAg
450
SWW-8270C
1N10320:08
WAD
HEXACHLOROCYCLOPENTADIENE
Not detected
ug/xg
450
SW846-8270C
1N10320:08
WAD
HEXACHLOROETHANE
Net detected
ugkg
450
SWW-8270C
IN/0320:03
WAD
INDENO(1.2,3-CD)PYRENE
Notdetected
ug/kg
450
SW846A270C
1MI0320:08
WAD
ISOPHORONE
Not detected
ug/kg
450
SWW-8270C
IM10320:08
WAD
2-METHYL4,6-DINITROPHENOL
Not detected
Ug/kg
2250
SW846A270C
I910320:08
WAD
2-MITWL NAPHTHALENE
Notdetected
Ug/kg
450
SW8WA270C
Taos 20:00
WAD
2-METHYL-PHENOL
Not detected
Ug/kg
450
SWB46A2700
1191W20:08
WAD
"ETHYL -PHENOL
Net detected
ug/kg
450
SW846-6270C
119N320:08
WAD
NAPHTHALENE
Not detected
ug/kg
450
SW846A270C
1/91032008
WAD
NITROBENZENE
Not detected
uglkg
450
Si
1/910320:08
WAD
2-NITROPHENOL
Not detected
uglkg
450
SWM6-8270C
119/0320:08
WAD
4NITROPHENOL
Not detected
ug/kg
2250
SW846.8270C
1191032008
WAD
NWTROSODIPHENYL4MINE
Not detected
ug/kg
450
SW846A27oC
119N[I 20:08
WAD
N-NITROSODI-N-PROPYLAMINE
Not detected
Ug/kg
450
SW84682703
1I910320:08
WAD
PENTACHLOROPHENOL
Not detected
Ug/kg
U50
SW84662703
1/91032008
WAD
PHENANTHRENE
Not detected
ug/kg
450
SW846-8270C
1/91032008
WAD
PHENOL
Not detected
ug/kg
450
SWW-8270C
1191032008
WAD
PYRENE
Not detected
ug/kg
450
SW846-8270C
1191032008
WAD
1,2,4-TRICHLOROBENZENE
Not detected
ugAg
450
SWUS-8270C
1191W20:08
WAD
2,4,5-TRICHLOROPHENOL
Net detected
ug/kg
450
SW8464270C
119/0320:08
WAD
2,4,6-TRICHLOROPMENOL
Not detected
Ug/kg
450
SW84682700
IKY0320:08
WAD
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking
Water Gen. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543
♦ Charlotte, NC
28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. Laboratory Name Prism Laboratories, Inc.
Project Name VMG NC Certification # (Lab) 402
Site Location Charlotte, NC Sample Matnx Soil
Sample Information and Analytical Results
Method for Ranges: MADEP VPH
VPH Surrogate Standards
Aliphatic: 2,5-Dibromotoluene
Aromatic: 2,5-Dibromotoluene
Sample Identification
AC68589
Collection Option (for soil)"
1
Date Collected
1/2/03
Date Received
1/6/03
Date Extracted
1/6/03
Date Analyzed
1/6/03
% Dry Solids
82 %
Dilution Factor
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample
Results
CS - C8 Aliphatics"
mg/kg
2.0
7.0
<7.0
-7.0
C9 - CI Aliphatics"
mg/kg
1.3
6.0
<6.0
<6.0
C9-CIO Aromatics"
mg/kg
0.4
2.0
<2.0
<2.0
Sample Surrogate Acceptance Range
70-130%
70.130%
Aliphatic Surrogate % Recovery - FID
94%
98%
Aromatic Surrogate%Recovery -PID
116%
111%
-
' Option 1 = Established fill line on vial Option 2 = Sampling Device (indicate brand, e.g. EnCorew) Option 3 = Field weight of soil
Unadjusted value. Should exclude the concentration of any sunagate(5), internal standards, and/or concentrations of other ranges that elute within the specified range.
MDL = Method Detection Limit RL= Reporting Limit Blank = Laboratory Method Blank or Trip Blank whichever is higher (indicate, type)
VPH rev. ll/UU
Were all performancefacceptance standards for required QA/QC procedures achieved?
Were any significant modifications to the VPH method made?
Page 1 of 3 No trip blank was submitted.
Yes No- Details Attached
No Yes - Details Attached
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VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. - Laboratory Name Prism Laboratories, Inc.
Project Name VMG NC Certification # (Lab) 402
Site Location Charlotte, NC Sample Matrix Soil
Sample Information and Analytical Results
Method for Ranges: MADEP VPH
VPH Surrogate Standards
Aliphatic: 2,5-Dibromotoluene
Aromatic: 2,5-Dibromotoluene
Sample Identification
AC68591
AC68592
Collection Option (for soil)*
1
i
Date Collected
1/2/03
112/03
Date Received
1/6/03
1/6/03
Date Extracted
1110103
1/10103
Date Analyzed
1/11/03
1111/03
% Dry Solids
78%
76%
Dilution Factor
5
2
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample
Results
Sample
Results
C5-C8 Aliphatics•'
mg/kg
2.0
7.0
<7.0
<35
<14
C9 - C12 Aliphatics••
mglkg
1.3
6.0
<6.0
<30
17
C9 - C10 Aromatics-
mg/kg
0.4
2.0
<2.0
39
41
Sample Surrogate Acceptance Range
70-130%
70-130%
70-130%
Aliphatic Surrogate % Recovery - FID
95%
"DO
88%
Aromatic Surrogate % Recovery - PID
119%
`DO
86%
' Option 1 = Established fill line on vial Option 2 = Sampling Device (indicate brand, e.g. EnCorew) Option 3 = Field weight of soil
" Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, and/or concentrations of other ranges that elute within the specified range.
MDL= Method Detection Limit RL=Reporting Limit Blank= Laboratory Method Blank or Trip Blank whichever is higher (indicate type)
VPH rev. 11/00
Were all performance/acceptance standards for required QA/QC procedures achieved? Yes No -Details Attached
Were any significant modifications to the VPH method made? No Yes • Details Attached
Page 3 of 3 • The surrogates were diluted out No rap blank was submitted.
VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. Laboratory Name Prism Laboratories, Inc.
Project Name VMG NC Certification # (Lab) 402
Site Location Charlotte, NC Sample Matrix Soil
Sample Information and Analytical Results -
Method for Ranges: MADEP VPH
VPH Surrogate Standards
Aliphatic: 2,5-Dibromotoluene
Aromatic: 2,5-Dibromotoluene
Sample Identification
AC68590
AC68593
AC68594
AC68595
Collection Option (for soil)*
1
1
1
1
Date Collected
12/03
113/03
1/3/03
113/03
Date Received
1/6/03
1/6103
1/6103
1/6103
Date Extracted
1/13/03
1113103
1113/03
1113/03
Date Analyzed
1/13/03
1114103
1/13/03
1/13/03
%Dry Solids
74%
85%
85%
75%
Dilution Factor
1
20
1
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample
Results
Sample
Results
Sample
Results
Sample
Results
C5-C8 Aliphatics••
mg/kg
2.0
7.0
<7.0
<7.0
<140
<7.0
<7.0
C9 - C12 Aliphatics•`
mg/kg
1.3
6.0
<6.0
<6.0
<120
<6.0
<6.0
C9 - C10 Aromatics-
mg/kg
0.4
2.0
<2.0g74%
210.0
<2.0
<2.0
Sample Surrogate Acceptance Range
70-130%
70-130%
70-130 %
70-130%
Aliphatic Surrogate %Recovery -FID
92 %
`DO
83%
76%
Aromatic Surrogate%Recovery-PID
-
94%
`DO
88%
77%
' Option 1 = Established fill line on vial Option 2 = Sampling Device (indicate brand, e.g. EnCorew) Option 3 = Field weight of soil
" Unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, and/or concentrations of other ranges that elute wahin the specified range.
MDL = Method Detection Limit RL = Reporting Limit Blank= Laboratory Method Blank or Trip Blank whichever is higher (indicate type)
VPH rev. 11/00
Were all pertormance/acceptance standards for required ILUQC procedures achieved? Yes No - Details Attached
Were any significant modifications to the VPH method made] Q No Yes - Details Attached
Page 2 of 3 `The surrogates were diluted out No trip blank was submitted.

EPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. Laboratory Name Prism Laboratories, Inc.
Project Name VMG NC Certification # (Lab) 402
Site Location Charlotte, NC Sample Matrix Soil
Sample Information and Analytical Results
Method for Ranges: MADEP EPH
EPH Surrogate Standards
Aliphatic: 1-Chloro-octadecane
Aromatic: o-Terphenyl
EPH Fractionation Surrogates
#1: 2-Bromonaphthalene
#2: 2-Fluorobiphenyl
Sample Identification
AC68593
I AC68594
AC68595
Date Collected
1l3/03
113/03
1/3/03
Date Received
1/6/03
116/03
1/6103
Date Extracted
116/03
116103
1/6103
Date Analyzed
118/03
118/03
1/8103
% Dry Solids
85%
85%
75%
Dilution Factor
1
1
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample Results
C9-C18 Aliphatics'
mg/kg
10
40
<40
2200
<40
<40
C19-C36 Aliphatics'
mg/kg
5.7
20
<20
460
<20
<20
C11-C22 Aromatics'
mg/kg
16
20
<20
1600
<20
<20
Sample Surrogate Acceptance Range
40-140%
40-140%
40-140%
40-140%
Aliphatic Surrogate % Recovery
88%
-MI(HIGH)
89%
86%
Aromatic surrogate % Recovery
109%
`MI(HIGH)
105%
121%
Fractionation Surrogate Acceptance Range
40-140%
40-140%
40-140%
40-140%
Fractionation Surrogate #1 % Recovery
72%
-MI(HIGH)
92%
90%
Fractionation Surrogate #2 % Recovery 1 90% 'MI(HIGH) 89% 107%
'Unadjusted value. Should exclude the concentration of any sunogale(s), internal standards, and/or concentrations of other ranges that elute Within the specified range.
MDL= Method Detection Umil RL=Reporting Limit Blank= Laboratory Method Blank
EPH rev. 11/00
Were all performance/acceptance standards for required DA/DC procedures achieved?
Was blank correction applied as a significant modification of the method 7
Were any significant modifications to the EPH method made?
Page 2 of 2 ' surrogate recovery outside of the control limit due to matrix Interference.
Yes No - Details Attached
Yes No
No Yes - Details Attached
EPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. Laboratory Name Prism Laboratories, Inc.
Project Name VMG NC Certification#(Lab) 402
Site Location Charlotte, NC Sample Matrix Soil
Sample Information and Analytical Results
Method for Ranges: MADEP EPH
EPH Surrogate Standards
Aliphatic: 1-Chloro-octadecane
Aromatic: c-Terphenyl
EPH Fractionation Surrogates
#1: 2-Bromonaphthalene
#2: 2-Fluorobiphenyl
Sample Identification
AC68589
AC68590
AC68591
AC68592
Date Collected
112/03
1/2103
1/2/03
1/2/03
Date Received
1/6103
1/6/03
1/6103
1/6103
Date Extracted
116133
1/6/03
1/6103
116/03
Date Analyzed
117103
117/03
V!7/03
118103
%Dry Solids
82%
74%
78%
76%
Dilution Factor
1
1
1
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample Results
C9-C18AIiphall.
mg/kg
10
40
<40
<40
2200
420
330
C19 - C36 Aliphatics'
mg/kg
5.7
20
<20
1 <20
190
- 83
60
C11-C22Aromatics-
mg/kg
16
20
<201VMJ111(7H4110GH)
60
94
150
Sample Surrogate Acceptance Range
40-140%140%
40-140%
40.140%
Aliphatic Surrogate % Recovery
88%HIGH)
-MI(HIGH)
'MI(HIGH)
Aromatic Surrogate % Recovery
109%(HIGH)
-MI(HIGH)
'MI(HIGH)
Fractionation Surrogate Acceptance Range
40.140%140%
40-140%
40-140%
Fractionation Surrogate #1 % Recovery-
72%(HIGH)
51 %
107%
Fractionation Surrogate #2 %Recovery 90%(HIGH) 64% 125%
' Unadjusted value. Should exclude the concentration of any sum gate(s), internal standards, and/or concentrations of other ranges that elute within the specified range.
MDL= Method Detection Limit RL=Reporting Limit Blank= Laboratory Method Blank
EPH rev. 11/00
Were all performance/acceptance standards for required DA/DC procedures achieved?
Was blank correction applied as a significant modification of the method 7
Were any significant modifications to the EPH method made?
Page 1 of 2 ' Surrogate recovery outside of the control limit due to matrix interference.
Yes No- Details Attached
Yes CiOD
No Yes -Details Attached

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Lab Report
� PRISM
IABORATOPIE; INC.
'
FUA evMcf AraMY'el6 Emirovnmlvl edullons
1/16103
Page 2 of 4
ERM Southeast, Inc.
Customer Project ID:
VMG
Attn: Mr. Rick Tarmvechia
Customer Sample ON
MW-2
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC68598
Charlotte, NC 28226
Login Group:
51501<1
Sample Collection Date/Time:
1/3103 16:00
Lab Submittal Date/Time:
1/6103 08:00
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
OATE/TIME
STARTED
ANALYST
4-BROMOPHENYL PHENYL ETHER
Not detected
ug/L
10
EPA625
11S/0319:29
LAC
BUTYL BENZYL PHTHALATE
Notdetected
ug/L
10
EPA625
1/9/0319:29
LAC
4-CHLORO3-METHYLPIHENOL
Notdetected
ug/L
10
EPA625
119I0319:29
111
2-CHLORONAPHTHALENE
Net detected
ug1L
10
EPA625
11910319:29
IAC
2-CHLOROPHENOL
Not detected
ug/L
10
EPA625
IM10319:29
IAC
4-0HLOROPHENYL PHENYL ETHER
Not detected
ug/L
10
EPA625
IN10319:29
IAC
CHRYSENE
Not detected
Ug/L
10
EPA625
1I9/031929
IAC
DIBENZO(A.H}ANTHRACENE
Not detected
ug/L
10
EPA625
1191031929
IAC
DI-N-BUTYLPHTHALATE
Not detected
ug/L
10
EPA625
1MI031929
IAC
1,2-DICHLOROBENZENE
Nal detected
Ug/L
10
EPA625
1MI0319:29
IAC
1,3-DICHLOROBENZENE
Notdetected
uglL
10
EPA625
1I9/031a29
LAC
1,4-DICHLOROBENZENE
Not detected
ug/L
10
EPA625
1/9/031929
IAC
3.3'-0ICHLOROBENZIDINE
Not detected
ug/L
50
EPA 625
1MIC319:29
LAC
2,4-DICHLOROPHENOL
Not detected
ug11-
10
EPA625
1/910319:29
LAC
DIETHYL PHTHALATE
Notde1e01ed
ug/L
10
EPA625
1A9/0319:29
IAC
2+13IMETHYLPHENOL
Not detected
ug/L
10
EPA 625
1MI0319:29
LAC
DIMETHYL PHTHALATE
Not detected
ug/L
10
EPA625
1I9I031929
LAC
2,4-OINITROPHENOL
Not detected
ug/L
50
EPA625
1M10319:29
LAC
2p-0INfTROTOLUENE
Not detected
ug/L
10
EPA625
19(0319:29
LAC
2,6-0INQROTOLUENE
Not detected
uglL
10
EPA625
100319'.29
LAC
01-N-OCTYLPHTHAIATE
Not detected
ug/L
10
EPA625
IaoG 19:29
LAC
FLUORANTHENE
Not detected
ug/L
10
EPA625
IM1031a29
LAC
FLUORENE
16
ug/L
10
EPA625
IM0319:29
IAC
HExACHLOROBENZENE
Not detected
ug/L
10
EPA625
1M1031a29
IAC
HEXACHLOROBIITADIENE
Not detected
ug/L
10
EPA625
1I9/0319:29
IAO
HEXACHLOROETHANE
Not detected
ug/L
10
EPA625
1W031923
IAC
INDENO(1,2,3-CD)PYRENE
Not detected
Ug1L
10
EPA625
119/031a29
IAC
ISOPHORONE
Not detected
ug/L
10
EPA625
IM1031929
LAG
2-METHYL4,6-DINITROPHENOL
Not detected
ug/L
50
EPA625
11910319:29
LAC
NAPHTHALENE
92
ug/L
10
EPA625
11910319:29
LAC
NITROBENZENE
NCtdetectad
ug/L
10
EPA625
1MI0319:29
LAC
NC Certification No. 402 - SC Certification
No. 99012
- NO Drinking
Water Cert.
No. 37735 - FL
Certificatlon No.
E87519
449 Springbrook
Road ♦ P.O.
Box 240543 ♦
Charlotte, NC 28224-0543
Phone: 704 / 529-6364
♦ Toll Free Number
1-900 /
529-6364 ♦
Fax: 704 / 525-0409
Lab Report
wk
PRISM
ueoR.F.I[s, IRc.
Funs nArerrcml A F,,t—mel Wa cos
1/16/03
Page 3 of
ERM Southeast, Inc.
Customer
Project ID: VMG
Attn: Mr. Rick Tarrdvechia
Customer
Sample ID: MW-2
7300 Carmel Exec. Park Ste. 200
Prism Sample ID: AC68598
Charlotte, NC 28226
Lopin Group:
5150KI
Sample Collection DateTme:
113103
1600
Lab Submittal Date/Time:
1/6/03
08:00
The following analytical results have been obtained
for the
indicated sample which was submitted
to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEIRME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
2-NITROPHENOL
Not detected
Ug/L
10
EPA625
1191031a29
IAC
4-NITROPHENOL
Not detected
ug/L
50
EPA625
1I910319:29
LAC
N-NITROSODI-N-PROPYIAMINE
Not detected
ug/L
10
EPA625
1MM31929
IAC
PENTACHLOROPHENOL
Not detected
ug/L
50
EPA625
1191031929
IAC
PHENAI,HRENE
39
ug/L
10
EPA 525
11910319:29
LAC
PHENOL
Notdetected
ug/L
10
EPA625
11910319:29
LAC
PYRENE
Not detected
ug/L
10
EPA625
11910319:29
LAC
1.2,4-TRICHLOROBENZENE
Not detected
ug/L
10
EPA625
11910319:29
LAC
2A,6-TRICHLOROPHENOL
Notdetected
ug/L
10
EPA625
11910319:29
LAC
CS BAIPM1atip
Not detected
ug/L
150
MADEP VPH
IM0323:50
JMV
CS-C12 AIiphatim
Not detected
ug/L
100
MADEP VPH
VD0323:50
JMV
C9-010 Aromatics
770
ug/L
30
MAGER VPH
IR10323:50
JMV
Surrogate%Recovery -PIO
85
% -
170430)
MADER VPH
tO/0323:50
JMV
Surrogate% Recovery-FID
74
%
(70-130)
NADER VPH
1910323:50
JMV
OIINIon Factor
1
ug/L
MADEP VPH
19/0323:%
JMV
EXTRACTION FOR EPH
Completed
MADEP-EPH
V13/0308:0o
SM
Ca-C18 ALIPHATICS
1100
ug/L
250
MADEP-EPH
111410310:08
GRR
C19L36 ALIPHATICS
Not detected
ug/L
250
MADEP-EPH
111410310:08
- GRR
C11-C22 AROMATICS
1600
uglL
180
MADEP-EPH
V1410310:08
GRR
SURROGATE RECOVERY - ALIPHATIC
88
%
(40-140)
MADEP-EPH
1/IV0310:08
GRR
SURROGATE RECOVERY -AROMATIC
•MI
%
(40-140)
MADEP-EPH
1114/0310:08
GRR
SURR:2-FLUOROSIPHENYL
11M
%
(4a140)
MADEP-EPH
VIV0310:08
GRR
SURR:2-SROMONAPHTHALENE
91
%
(40-140)
MADEP-EPH
VIV0310:08
GRR
DILUTION FACTOR
1
ug/L
MADEP-EPH
1/1V0310:08
GRR
NO CertMcabon No. 402 - SC Certification No. 99012 - NO Drinking Water Ceri. No. 37735 - FL Certification No. E87619
449 Springbrook Road A P.O. Box 210543 A Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number. 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. Laboratory Name Prism Laboratories, Inc.
Project Name VMG NC Certification If (Lab) 402
Site Location Charlotte, NC Sample Matrix Water
Sample Information and Analytical Results
Method for Ranges: MADEP VPH
VPH Surrogate Standards
Allphatic: 2,5-Dibromotoluene
Aromatic: 2,5-Dibromotoluene
Sample Identification
AC68598
Collection Option (for soil)`
NA
Date Collected
113/03
Date Received
116103
Date Extracted
NA
Date Analyzed
lr7103
%Dry Solids
NA
Dilution Factor
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample Results
C6-CB Aliphatics"
ug/L
47
150
<150
<150
C9-C12 Aliphatics"
ug/L
28
100
<100
<100
C9-Cie Aromatics"
ug/L
10
30
<30
770
Sample Surrogate Acceptance Range
70-130%
70-130%
Aliphatic Surrogate % Recovery - FID
115%
74%
Aromatic Surrogate%Recovery -PID
87%
85%
Option 1 = Established fill line on vial Option 2 = Sampling Device (indicate brand, e.g. EnCorerN) Option 3 = Field weight of soil
" unadjusted value. Should exclude the concentration of any surrogate(s), internal standards, andfor concentrations of other ranges that elute within the specified range.
MDL= Method Detection Limit RL=Repading Limit Blank= Laboratory Method Blank or Trip Blank whichever is higher (indicate type)
VPH rev. 11/00
Were all performance/acceptance standards for required DA/OC procedures achieved?
Were any significant modifications to the VPH method made?
No VPH Trip Blank was submitted.
Page i of 1 VPH
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No Yes -Details Attached

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EPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. Laboratory Name Prism Laboratories, Inc
Project Name VMG NC Certification # (Lab) 402
Site Location Charlotte, NC Sample Matrix Water
Sample Information and Analytical Results
Method for Ranges: MADEP EPH
EPH Surrogate Standards
Aliphatic: 1-Chloro-octaderane
Aromatic: o-Terphenyl
EPH Fractionation Surrogates
#1: 2-Bromonaphthalene
#2: 2-Fluorobiphenyl
Sample Identification
AC68598
Date Collected
1/3/03
Date Received
116/03
Date Extracted
1/13/03
Date Analyzed
1/14/03
%Dry Solids
NA
Dilution Factor
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample Results
C9-C18 Aliphatics'
ug/L
130
250
<250
1100
C19 - C36 Aliphatics`
ug/L
120
250
<250
Q50
C11 - C22 Aromatics'
ug/L
78
180
<180
1600
Sample Surrogate Acceptance Range
40-140%
40-140%
Aliphatic Surrogate % Recovery
50%
88%
Aromatic Surrogate %Recovery
133%
`MI(high)
Fractionation Surrogate Acceptance Range
40-140%
40-140%
Fractionation Surrogate #1 % Recovery
126%
91%
Fractionation Surrogate #2 % Recovery
I
1
1 127%
104%
' Unadjusted value. Should exclude the concentration of any sumogate(s), internal standards, andlor concentrations of other ranges that elute within the specified range.
MDL = Method Detection Limit RL= Reporting Limit Blank= Laboratory Method Blank
EPH rev. 11/00
Were all performance/acceptance standards for required Q IDC procedures achieved?
Was blank correction applied as a significant modification of the method ?
Were any significant modifications to the EPH method made?
Page 1 of 1 EPH
' Surrogate recovery outside control limits due to matrix interference. -
OED No - Details Attached
Yes No
No Yes - Details Attached

Lab Report
2/6/03
ERM Southeast, Inc.
Attn: Mr. Rick Tarrevechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
ueoeAToelse, INC.
Fur ae,Na McMIM a E—mental SW.Mmv
Page i of 16
ustomer Project ID:
Integris Metals
Customer Sample tD:
MW43
Prism Sample ID:
AC70820
Login Group:
5594K4
Sample Callection Date/Time:
1122/03
17:00
Lab Submittal Date/Time:
1124103
08:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEmME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
BENZENE
1.6
ug/L
1.0
EPA602
11291031037
KTE
ETHYLBENZENE
Not detected
ug&
1.0
EPA 602
11291031837
KTE
IPE
Not detected
ug/L
So
EPA 602
V2910318:37
KTE
WRE
Not detected
ug/L
5.0
EPA 602
112910318:37
KTE
TOLUENE
2.0
ug/L
1.0
EPA 602
1129031IX
KTE
xYLENES
Not detected
ug/L
3.0
EPA 602
11291031837
KTE
PREP. METHOD 625
Completed
-
EPA 625
112910311do
SM
ACENAPHTHENE
Not detected
ug1L
10
EPA625
ZIV0303:43
LAC
ACENAPHTHYLENE
Not detected
ug/L
10
EPA625
V1103 MAD
LAC
ANTHRACENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
BENZO(A)AWHRACENE
Not detected
ugA-
10
EPA625
2111030343
IAC
BENZO(B)FLUORANTHENE
Not detected
ug/L
10
EPA625
21V0303:43
LAC
BENZO(K)FLUORANTHENE
Not detected
ug/L
10
EPA625
V110303:43
LAc
BENZO(A)PYRENE -
Not detected
ug1L
10
EPA625
2111030343
LAC
BENZO(GHHPERYLENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
BIS(2-0HLOROETHOxY)METHANE
Not detected
ug/L
10
EPA625
V110303:43
IAC
BIS(2-0HLOROETHYL)ETHER
Notdetected
ug1L
10
EPA625
V110303:43
LAC
BIS(2- 11LOROISOPROPYL(ETHER
Not detected
ugA
10
EPA625
V110303.43
LAC
BIS(2-ETHYLHE%YL(PHTHALATE
11
ugA
10
EPA625
21110303:43
LAC
443ROMOPHENYL PHENYL ETHER
Not detected
ug/L
10
EPA625
21110303:43
LAC
BUTYL BENZYL PHTHALATE
Not detected
ug/L
10
EPA625
V110303:43
LAC
0-CHLORO-3-METHYLPHENOL
Not detected
ug/L
10
EPA625
V110303:43
LAC
2CHLORONAPHTHALENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
2-CHLOROPHENOL
Not detected
ug/L
10
EPA625
V110303:43
tAC
4-CHLOROPHENYL PHENYL ETHER
Not detected
ug/L
10
EPA625
V110303:43
LAC
CHRYSENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
DIBENZO(A,HIANTHRACENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
DI-N-BUTYLPHTHAIATE
Not detected
ug/L
10
EPA625
D110303:43
LAC
1,2-DICHLOROBENZENE
Not detected
ug/L
10
EPA625
V110303:43
LAD
NO Certification No. 402 - SC Certificaton
No. 99012
- NC Drinking
Water Can.
No. 37735 - FL
Certification No. E87519
449 Spdngbmok Road ♦ P.O.
Box 240543
♦ Charlotte, NC 28226-0543
Phone: 704 / 529-63M ♦ Toll Free Number: 1-800 / 529-6364 ♦ F. 704 / 525-0409
Lab Report
PRISM
4'F ueo6Aronres,INc.
Full aeMw aruM'ml a EmYmnmenhl $dWore
2/6I03
Page 2 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-3
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC70820
Charlotte, NC 28226
Login Group:
55941<4
Sample Collection Date/Time:
1/22/03 17:00
Lab Submittal DatefTime:
1124/03 08:15
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEITIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,3-0ICHLOROBENZENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
1,4-DICHLOROBENZENE
Not detected
ugl-
10
EPA625
V110303,43
LAC
3,3'-DICHLOROBENZIOINE
Not detected
ug/L
50
EPA 625
V110303M3
LAC
2,4-DICHLOROPHENOL
Not detected
ug/L
10
EPA625
V110303:43
LAC
DIETHYL PHTHALATE
Not detected
ug/L
10
EPA625
W110303:43
LAC
2.4-0IMETHYLPHENOL
Not detected
ug/L
10
EPA625
21110303:43
LAC
DIMETHYL PHTHALATE
Not detected
ug/L
10
EPA625
V110303:43
IAC
2,4DINITROPHENOL
Not detected
ug/L
50
EPA625 -
VI/0303:43
LAC
2,4-0INITROTOLUENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
2,6-DINITROTOLUENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
DI-N-OCTYLPHTHALATE
Not detected
ug/L
10
EPA625
V110303:43
LAG
FLUORANTHENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
FLUORENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
HEYACHLOROBENZENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
HE%ACHLOROBUTAOIENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
HEXACHLOROETHANE
Not detected
ug/L
10
EPA625 -
VIA)303:43
LAO
INDENON,2,3-CO)PYRENE
Not detected
ug/L
10
EPA625
V110303:43
LAC
ISOPHORONE
Net detected
ug/L
10
EPA 625
D110303:43
tAC
2-METHYL4,6-0INITROPHENOL
Not detected
ug/L
50
EPA625
D110303:43
LAC
NAPHTHALENE
Not detected
ug/L
10
EPA 625
V1103 03 43
LAC
NITROBENZENE
Not detected
uglL
10
EPA625
V1I0303:43
LAC
2-NITROPHENOL
Not detected
ug/L
10
EPA625
V110303:43
LAC
4-NITROPHENOL
Not detected
ug1L
50
EPA 625
V110303:43
LAC
N-NRROSOOI-R-PROPYLAMINE
Not detected
uglL
10
EPA625
V110303:43
LAC
PENTACHLOROPHENOL
Not detected
ug/L
50
EPA625
2111030343
LAC
PHENANTHRENE
Noldetected
ug/L
10
EPA625
V110303:43
LAC
PHENOL
Notdetected
ug/L
10
EPA625
VV0303:43
IAC
PYRENE
Notdetected
ug/L
10
EPA625
V1103 03 43
LAC
12,LTRICHLOROSENZENE
Notdetected
uql
10
EPA625
D11030343
LAC
2,4,6-TRICHLOROPHENOL
Not detected
UgA-
10
EPA625
V110303:43
LAC
NC Certification No. 402 - SC
Certificabion No. 99012
- NC Drinking
Water Cert.
No. 37735 - FL
Certification No.
E87519
449 Springbrock Road ♦ P.O.
Box 240543
a Chariot, NC 28224-0543
Phone: 704 / 529-63M ♦ Toll Free Number: 1-800 / 529-6364 •
Fax: 704 / 525-0409

Lab Report
PRISM
f- ueoaxroalFs,INe.
FW $erv4a.Wlytlnl6 EmlrnmeMtl Stlubv
2/6103
Page 3 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Terravechia
Customer Sample ID:
MWJ
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC70820
Charlotte, NC 28226
Lopin Group:
5594K4
Sample Collection Date?ime:
1/22/03 17:00
Lab Submittal DalerTime:
1/24103 08:15
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATE?IME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
C5 Il Aflpbaem
Not detucled
ug/L
150
MADEP VPH
V310318:00
JMV
C9-012A4phatice
Not deleeted
ug/L
100
MADEP VPH
M/03 is:00
JMV
C9-Cto Aromatics
Not delecled
ug/L
30
MAGER VPH
VW0318:00
JMV
Senopate%Recovery-PID
94
%
(70-130)
MADEP VPH
D3103 16 00
JMV
Suvo9ale%Recovery-FID
90
%
(70-130)
MADEP VPH
VW031500
JMV
Dilution Factor
1
ug/L
MADEP VPH
V3/0318:00
JMV
EMRACTION FOR EPH
CCmpleted
MADEP-EPH
1130)0311:00
am
C9-C18 AUPHATICS
Notdeleoled
ug/L
250
MADEP-EPH
=03III
GRR
C19-C36 ALIPHATICS
Not detected
ug/L
250
MADEP.EPH
2/10310:34
GRR
C11-C22AROMATICS
Net detected
ug/L
180
MADEP-EPH
VW0310:34
GRR
SURROGATE RECOVERY -ALIPHATIC
86
%
(40-140)
MADEP-EPH
VW0310:34
GRR
SURROGATE RECOVERY - AROMATIC
131
%
(40-140)
MADEP-EPH
2/10310:34
GRR
SURR12-FLUOROBIPHENYL
123
%
(40.140)
MADEP-EPH
VW0310:34
GRR
SURR:2-2ROMONAPiiTHALENE
118
%
(40-140)
MADEP-EPH
WY0310:34
GRR
DILUTION FACTOR
1
ug/L
MADEP-EPH
2J10310:34
GRR
NO CertMcatlon No. 402 - SC Certification No. 99012 - NO Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 A Charlotte, NC 28226-0543
Phony 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 A Fax: [phone]
Lab Report
PRISM
,F- L4eoluroalEs,lxc.
FUAaervY McMIu16 EmlMnmenlel9dulme
2/6/03
Page 4 of 16
ERM Southeast, Inc.
Customer Project ID:
Integra Metals
Attn: Mr. Rick Tarravechis
Customer Sample ID:
Ml
7300 Carmel Exec, Park Ste. 200
Prism Sample ID:
AC70820
Charlotte, NC 28226
Lopin Group:
55941<4
Sample Collection Dale/Time:
1122/03 17:00
Lab Submittal Date/Time:
1124/03 08:15
The fallowing analytical results have been obtained
for the indicated sample which was submitted to this laboratory:
TEST TEST
REPORTING METHOD DATEaIME
PARAMETER RESULT
UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
Sample for EPH preserved upon receipt.
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Cemication No. E87519
449 Springbrook Road A P.O. Box 240543 A Charlooe, NC 28221-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
2/6/03
ERM Southeast, Inc.
Attn: Mr. Rick Tamavechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
f.kPRISM
ueo64roxlas lnc
Full $eriee4reblkN a BM,mmanYl SMubnf
Page 5 of 16
Customer Project ID:
Integris Metals
Customer Sample ID:
MW4
Prism Sample ID:
AC70821
Loom Group:
5594K4
Sample Collection DaleMme:
1122/03
1330
Lab Submittal Date/Time:
1124/03
08:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATEmME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
BENZENE
Not detected
UgIL
1.0
EPA 602
112910319: 11
KTE
ETIIYLBENZENE
Not detectetl
UgIL
1.0
EPA 602
112910319: 11
KTE
IPE
Not detected
ug/L
5.0
EPA 602
112910319: 11
KTE
MTBE
Not detected
ugl
5.0
EPA 602
1/2910319: 11
KTE
TOLUENE
Net detected
UgIL
1.0
EPA 602
112910319: 11
KTE
XYLENES
Not detected
ug/L
3.0
EPA 602
1129/0319: 11
KTE
PREP. METHOD 625
Completed
EPA 625
V29/0307:00
SM
ACENAPHTHENE
Not detected
ugA-
10
EPA 625
V11030432
LAC
ACENAPHTHYLENE
Not detected
ugr-
10
EPA625
V110304:32
LAC
ANTHRACENE
Not detected
Ugr-
10
EPA 625
V110304:32
LAC
EIRWO(A)AJTHRACENE
Not detected
ug/L
10
EPA625
V110304:32
LAC
BENZO(B)FLUORANTHENE
Not detected
ug/L
10
EPA625
V110304:32
LAC
BENZO(K)FLUORAHTHENE
Notdetected
ug/L
10
EPA625
VV0304:32
LAC
BENZO(A)PYRENE
Not detected
ug/L
10
EPA625
V1103 M:32
LAC
BENZO(GHI)PERYLENE
Not detected
ug/L
10
EPA625
V1103 M:32
LAC
3IS(2-CHLOROET)1OXY)METHANE
Notdateced
ug/L
10
EPA625
21110304:32
LAC
BIS(2-CHLOROETHYL)ETHER
Not detected
ugf-
10
EPA625
2I110304:32
LAC
BIS(2-CHLOROISOPROPYL)ETHER
Not detected
ug/L
10
EPA625
211103 M:32
LAC
Bls(2-ETHYLHEXYL)PHTHALATE
Not detected
ug/L
10
EPA625
2I110304:32
LAC
4-BROMOPHENYL PHENYL ETHER
Not detected
uglL
10
EPA625
2/l/0304:32
LAC
BUTYL BENZYL PHTHALATE-
Not detected
ug/L
10
EPA625
V110304:32
LAC
4-CHLORO3-METHYLPHENOL
Not detected
uglL
10
EPA625
V11030432
LAC
2L111UORONAPHTHALENE
Net detected
ug/L
10
EPA625
V110304:32
LAC
2-CHLOROPHENOL
Net detected
ug/L
10
EPA625
V110304:32
LAC
4L11LOROPHENYL PHENYL ETHER
Not deected
ug/L
10
EPA 625
V1103 M:32
LAC
CHRYSENE
Not detected
ug/L
10
EPA625
V110304:32
LAC
DIBENZO(A,H}ANTHRACENE
Not detected
ug/L
10
EPA625
Z11I0304:32
LAC
DI-N-BUTYLPHTHALATE
Not detected
ug/L
10
EPA625
V110304:32
LAC
1,2-DICHLOROSENZENE
Notdetected
ug/L
10
EPA 525
V110304:32
LAC
1.3-DICHLOROSENZENE
Not detected
ug/L
10
EPA625
2J1103 M:32
LAC
NC Certification No. 402 - SC CerUication No. 99012
- NC
Drinking Water Can.
Na 37735 - FL
Cenficatton No.
E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦ Charlotte. NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number:
1-800 / 529-6364 ♦
Fax: 704 / 525-0409
Lab Report
,' j\ PRISM
1 Luda4rom0% INC.
-.
FNI SeINx Metfical6 EnNrnmenYlStluCo�
216/03
Page 6 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tanavechia
- Customer Sample ID:
MW4
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC70821
Charlotte, NC 28226
Login Group:
5594K4
Sample Collection DatelTime:
1122/03 13:30
Lab Submittal Dale/Time:
1124/03 08:15
The fallowing analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DAT ITIME
PARAMETER
RESULT
UNITS LIMIT
REFERENCE
STARTED
ANALYST
1p-DICHLOROBENZENE
Not detected
ug/L
10
EPA625
211103 M:32
LAC
3,3'-DICHLOROBENZIOINE
Not detected
Ug1L
50
EPA 525
W110304:32
LAC
2,0.DICHLOROPHENOL
Not detected
ug/L
10
EPA625
VIAL 04:32
LAC
DIETHYL PHTHALATE
Not detected
ug/L
10
EPA625
VVIO 04:32
LAC
2A-DIMETHYLPHENOL
Not detected
ug/L
10
EPA625
2/110304:32
LAC
DIMETHYL PHTHALATE
Not detected
ug/L
10
EPA625
2/110304:32
LAC
2,4-DINITROPHENOL
Not detected
uglL
So
EPA625
2/1I0304:32
LAC
2,4DINITROTOLUENE
Not detected
ugA-
10
EPA625
2/1I0304:32
LAC
2,6-DINITROTOLUENE
Not detected
ug/L
10
EPA625
V110304:32
LAC
DIN-0CTYLPHTHALATE
Nottleteced
ug/L
10
EPA625
211/0304:32
LAC
FLUORANTHENE
Not detected
ug/L
10
EPA625
V110304:32
LAC
FLUORENE
Not detected
ug/L
10
EPA625
VV0304s2
LAC
HEXACHLOROBENZENE
Not detected
ug/L
10
EPA625
V110304:32
LAC
HEXACHLOROBUTADIENE
Not detected
ugf-
10
EPA 625
21110304:32
LAC
HEXACHLOROETHANE
Not detected
ug/L
10
EPA625
2A 10304:32
LAC
INDENO(1,2,3-CD)PYRENE
Not detected
ug/L
10
EPA625
21110304:32
LAC
ISOPHORONE
Not detected
ug/L
10
EPA625
211103 M:32
LAC
2-METHY446-DINITROPHENOL
Net detected
uglL
50
EPA 525
2I11030432
LAC
NAPHTHALENE
Not detected
ug/L
10
EPA625
VIAO 04:32
LAC
NITROBENZENE
Not detected
ug/L
10
EPA625
2J110304:32
LAC
2-NITROPHENOL
Not detected
ug/L
10
EPA625
V110304:32
LAC
4-NITROPHENOL
Not detected
ug4-
50
EPA625
ZJ1/0304S2
LAC
N-NITROSODI-N-PROPYIAMINE
Not detected
ug/L
10
EPA625
4I1I0304:32
LAC
PENTACHLOROPHENOL
Not detectetl
ugf-
50
EPA625
V110304:32
LAC
PHENANTHRENE
Not detected
ugf-
10
EPA625
Z110304:32
LAC
PHENOL
Not detected
ug/L
10
EPA625
tYlKa 04:32
LAC
PYRENE
Not detected
ug/L
10
EPA 625
VI(0304:32
LAC
1,2,STRICHLOROBENZENE
Not detected
ug/L
10
EPA625
2/1/030432
LAC
2.4.6-TRICHLOROPHENOL
Not detected
ug/L
10
EPA625
V110304:32
LAC
25-08 Aliphatics
Notti.xot l
ug/L
150
MADEPVPH
W310316:15
JMV
NC Certification No. 402 - SC Certification No. 99012
- NC
Drinking Water Cert.
No. 37735 - FL
Certification No.
E87519
449 Springbrock Road ♦ P.O.
Box 240543 ♦ Charlotte, NC 2822 0543
Phone: 704 / 529-6364
♦ Toll Free Number:
1-800 / 529-6364 ♦
Fax: 704 / 525-0409

Lab Report
PRISM
ueoa4loelas, INc
FA Serviro MYylbi a Emi,ommenW eGNlwu
2/6/03
Page 7 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Atm- Mr. Rick Tarravechia
Customer Sample ID:.
MWA
7300 Camtel Exec. Park Ste. 200
Prism Sample ID:
AC70821
Loath Group:
5594K4
Charlotte, NO 28226
Sample Collection Date/Time:
1/22/03 13:30
Lab Submittal Date/Time:
1124/03 08:15
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory.
TEST
TEST
REPORTING
METHOD
DATEmME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
C9-C12 A Iphatice
Noldetected
ug(L
100
MADEPVPH
2/3/0316:15
JMV
C9-C10Aarmdca
Not detected
ug/L
30
MADEPVPH
V3N316:15
JMV
SumNI%Recovery-IND
125
%
(70-130)
MADEPVPH
M10316:15
JMV
Sumpeta%Recovery -FIO
117
%
(70-130)
MADEPVPH
M0316:15
JMV
DIIWon Factor
1
ugA-
MADEPVPH
W10316:15
JMV
EXTRACTION FOR EPH
Completed
MADEPVPH
113010311:00
SM
29-016 ALIPHATICS
Not detected
Ug/L
250
MADEPVPH
VW0311:25
GRR
C19-036 ALIPHATICS
Not detected
MI
250
MADEPVPH
V310311:25
GRR
C11-C22 AROMATICS
Not detected
ug/L
160
MADEP-EPH
VV0311:25
GRR
SURROGATE RECOVERY - ALIPHATIC
103
%
(40-140)
MADEP-EPH
V310311:25
GRR
SURROGATE RECOVERY - AROMATIC
125
%
(40.140)
MADEP-EPH
VW031125
GRR
SURR:2-FLUOROBIPHENYL
122
%
(40-140)
MADEP-EPH
D310311:25
GRR
SURR:2-BROMONAPHTHALENE
122
%
(40-140)
MADEP-EPH
V310311:25
GRR
DILUTION FACTOR
t
ug/L
MADEP-EPH
2/W0311:25
GRR
NO Certification No 402 - SC Certification No. 99012 - NO Drinking Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NO 28224-0543
Phone: 704 / 529-63M A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409
Lab Report
!\ PRISM
ueoBAroeres, Ixc.
Fee sem•.4„eyaw a Hmmnmmmal saeeo,n
2/6/03
Page 8 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MP/4
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
ACT0821
Charlotte, NC 28226
Lonin Group:
5594K4
Sample Collection DateRme:
1/22/03 13:30
Lab Submittal Date/Time:
1124103 08:15
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATENIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NO Certification No. 402 - SC CeNfwlion No. 99012 - NO Drinking Water Cert. No. 37735 - FL Codification No. E87519
449 Springbmok Road A P.O. Box 240543 A Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Tall Free Number: 1-800 / 529-6364 ♦ F.: 70 t / 525-0409

Lab Report
<\ PRISM
,� uao6AroBlax,lnc
Ful Servlm AmlylheltEmbonmeMeladuti:rn
2/6103
Page 9 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-5
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC70822
Charlotte, INC 28226
Loqin Group:
55941<4
Sample Collection Date/Time:
1/22/03 18:00
- Lab Submittal Dalerrime:
1/24103 0815
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
-TEST
TEST
REPORTING
METHOD
DATERIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
BENZENE
3.6
ug/L
1.0
EPA602
112910319:46
KTE
ETHYLBENZENE
Not detected
ug/L
1.0
EPA 602
112910319:46
KTE
IPE
Not detected
ug/L
5.0
EPA602
1I29/0319:46
KTE
MTBE
Not tletectetl
uglL
5.0
EPA602
112910319:46
KTE
TOLUENE
is
ugA-
1.0
EPA602
1/2910319:46
KTE
XYLENES
Not detected
uglL
3.0
EPA602
V2910319A6
KTE
PREP. METHOD 625
Completed
EPA625
11291031100
BM
ACENAPHTHENE
Not detected
ug/L
10
EPA 625
V11030520
LAO
ACENAPHTHYLENE
Not detected
ug&
10
EPA625
Z1/0305:20
LAC
ANTHRACENE
Not detected
add-
10
EPA625
V110305:20
LAC
BENZO(A)ANTHRACENE
Not detected
ug/L
10
EPA625
V11030520
LAC
BENZO(B)FLUORANTHENE
Not detected
ugA-
10
EPA625
V110305:20
LAC
BENZO(K)FLUORANTHENE
Not detected
UgIL
10
EPA625
21110305:20
LAC
BENZO(A)PYRENE
Not detected
UgIL
10-
EPA625
Z110305:20
LAC
BENZO(GHI)PERYLENE
Not detected
UgIL
10
EPA625
211I0305.20
LAC
BIS(2-CHLOROETHOXY)METHANE
Not detected
ug/L
10
EPA625
V110305:20
IAC
BIS(2-CHLOROETHYL)ETHER
Not detected
UgIL
10
EPA625
W110305'.20
LAC
SIS(DCHLOROtSOPROPYL)ETHER
Not detected
ug/L
10
EPA625
V110305:20
IAC
BIS(2-ETHYLHEx L)PHTHALATE
Not detected
ug/L
10
EPA625
V110305:20
IAC
4-BROMOPHENYL PHENYL ETHER
Not detected
ug/L
10
EPA625
V110305:20
LAC
BUTYL BENZYL PHTHALATE
Not detected
ug/L
10
EPA625
D110305:20
LAC
4-CHLOR03METHYLPHENOL
Notdetected
ug/L
10
EPA625
D11030520
LAC
2-CHLORONAPHTHALENE
Notdetectdt
UgIL
10
EPA625
2111030520
LAC
2-CHLOROPHENOL -
Notdetected
ug/L
10
EPA625
21110305:20
LAC
4CHLOROPHENYL PHENYL ETHER
Not detected
ug/L
10
EPA625
21110305:20
IAc
OHRYSENE
Not detected
UgIL
10
EPA625
V110305:20
LAC
DIBENZOIA.HIANTHRACENE
Not detected
UgIL
10
EPA625
Z1/0305:20
LAC
DI-N-BUTYLPHTHALATE
Not detected
ug/L
10
EPA 625
Z1/0305:20
LAC
1,2-0ICHLOROBENZENE
Not detected
ug/L
10
EPA625
21110305:20
t c
1.3-0ICHLOROBENZENE
Not detected
UgIL
10
EPA625
2/1/030520
LAC
NO Certifiwdon No. 402 - SC Certification
No. 99012
- NO Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Spongbrook Road ♦ P.O.
Box 240543
♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number:
1-800 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
a` PRISM
£.:. , uaoxAlaaFa,lxc.
Fu115¢Mv MCFAkal6 Emlmrmenlel $dWan¢
2/6/03
Page 10 of 16
ERM Southeast, Inc. -
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tarrevechia
Customer Sample ID:
MW-5
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC70822
Login Group:
5594K4
Charlotte, NC 28226
Sample Collection Dale/Time:
1122/03 18:00
Lab Submittal Date/Time:
1/24/03 08:15
The following analytical results have been obtained for the Indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATERIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1,4-0ICHLOROBENZENE
Not detected
ug/L
10
EPA625
21110305:20
LAC
3.£-DICHLOROBENZIDINE
Not detected
ug/L
50
EPA 625
2111030520
LAC
2,4-DICHLOROPHENOL
Not detected
Dg&
10
EPA625
Z11D305a0
LAC
DIETHYL PHTHALATE
Not detected
ug/L
10
EPA 625
V110305:20
LAC
2.4-DIMETHYLPHENOL
Not detected
ug/L
10
EPA625
21110305:20
LAC
DIMETHYL PHTHALATE
Not detected
ug/L
10
EPA625
V110305:20
LAG
2,4-DINITROPHENOL
Not detected
ug/L
50
EPA625
V110305:20
IAC
2,4-DINITROTOLUENE
Not detected
ug/L
10
EPA625
V110305:20
LAC
26-0INITROTOLUENE
Not detected
ugl
10
EPA625
V1103 05 20
IAC
DI-N-0C7Y1-PHTHALATE
Not detected
ugl
10
EPA625
V110305:20
LAC
FLUORANTHENE
Not detected
ug/L
10
EPA625
VV030520
LAC
FLUORENE
Notdetected
UgIL
10
EPA625
2/11030520
LAC
HEXACHLOROBENZENE
Notdetected
UgIL
10
EPA625
V1103 05 20
LAC
HEXACHLOROBUTAOIENE -
Notdetected
ug/L
10
EPA625
V110305:20
IAC
HEXACHLOROETHANE
Not detected
ug/L
10
EPA625
W110305:20
LAO
INOEN0(1,2,3-CO)PYRENE
Not detected
ug/L
10
EPA625
V110305:20
LAC
ISOPHORONE
Not detected
ug/L
10
EPA625
21110305:20
IAC
2-METHYU.6-DINITROPHENOL
Not detected!
ug/L
50
EPA 625
VI10305:20
LAC
NAPHTHALENE
Not tletected
uglL
10
EPA 625
V110305:20
LAC
NITROBENZENE
Not detected
ug/L
10
EPA 625
21110305:20
LAC
2-NITROPHENOL
Not detected
UgIL
10
EPA625
2111030520
LAC
4-NITROPHENOL
Not detected
UgIL
50
EPA625
2/110305:20
LAC
N-NITROSODI-N-PROPYLAMINE
Notdetected
UgIL
10
EPA625
Z110305:20
IAC
PENTACHLOROPHENOL
Not detected
ug/L
5D
EPA625
V110305:20
LAC
PHENANTHRENE
Not detected
ug/L -
10
EPA625
VIAo 05:20
IAO
PHENOL
Not detected
ugk
10
EPA625
V110305:20
LAC
PYRENE
Not detected
ug/L
10 -
EPA625
Z1103 05 20
LAC
1.2,4-TRICHLOROBENZENE
Not detected
ug/L
10
EPA625
21110305,20
LAC
2,4,6-TRICHLOROPHENOL
Not detected
ug/L
10
EPA625
211I030520
IAC
C5-C8 Allphatka 3500 ug/L 150 MADEP VPH VV0313:17 JMV
NO Cenlfication No. 402 - SC Certiflnation No. 99012 - NC Drinking Water Con. No. 37735 - FL Cenfication No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
, ` \ PRISM
LABONJ DRiEe, INC.
F,d same Ane�I a E,rnmmmmmi swuvo
. 2/6103
Page 11 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MW-5
7300 Carmel Exec. Park Ste, 200
Prism Sample ID:
AC70822
Login Group:
55941<4
Chadotte, NC 28226
Sample Collection Date/Time:
1/22103 1800
Lab Submittal Dale/Time:
1/24103 08:15
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
OATEITME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
C& 12 Aliphallm
Notdetected
ug/L
100
MADEP VPH
V410313:17
JMV
09-C10 Aromatic
Not detected
ug/L
30
MADEP VPH
VV031317
JMV
Surrogate%Recovery-PID
124
%
(70-130)
MADEP VPH
V410313:17
JMV
Sumgale%Recovery-FID
122
%
(70-130)
MADEP VPH
2410313:17
JMV
'DIINIon Factor
1
ug/L
MADEP VPH
VV0313:17
JMV
EXTRACTION FOR EPH
Completed
MADEP-EPH
113010311:0o
SM
C9-C18 ALIPHATICS
Not detected
ug/L
250
MADEP-EPH
VN0312:17
GRR
C19-C36 ALIPHATICS
Not detected
uglL
250
MADEP-EPH
VN0312:17
GRR
C11-C22 AROMATICS
Not deto Aad
ug/L
180
MADEP-EPH
V310312:17
GRR
SURROGATE RECOVERY - ALIPHATIC
97
%
(40-140)
MADEP-EPH
V310312:17
GRR
SURROGATE RECOVERY -AROMATIC
I
%
(40-14C)
MADEP-EPH
VV0312:17
GRR
SURR:2-FLUCROBIPHENYL
127
%
(40-140)
MADEP-EPH
VW0312:17
GRR
SURR:2-BROMONAPHTHALENE
123
%
(40.140)
MADEP-EPH
VTO312:17
GRR
DILUTION FACTOR
1
ug/L
MADEP-EPH
W310312:17
GRR
NO Certification No. 402 - SC Certification No. 99012 - INC Drinking Water Can. No. 37735 - FL Certification No. E87519
449 Spdngbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-81)0 / 529-6364 ♦ Fax: 704 / 525-0409
Lab Report
!.4\ PRISM
ueoaAmelFs, mc.
FWI SeMce MflfYal a Emi,mmmbl eoFNMs
2/6/03
Page 12 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tarravechia
Customer Sample ID:
MI
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC70822
Login Group:
5594K4
Charlotte, NC 28226
Sample Collection Date/Time:
1/22/03 18:00
Lab Submittal Daterrime:
1/24103 08:15
The following analytical results have been obtained
for the indicated sample which was submitted to this laboratory,
TEST TEST
REPORTING METHOD DATEFTIME
PARAMETER RESULT
UNITS LIMIT REFERENCE STARTED ANALYST
Sample C0mments:
Sample for EPH pprrees/eerved upon receipt.
Angela D. Overcash, V.P. Laboratory Services
NC Codification No. 402 - SC Certification No. 99012 - NC Drinking Water Con. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, INC 2822A-0543
Phone: 704 / 5296364 ♦ Toll Free Number: 1-800 / 5296364 ♦ Fax: 704 / 525-0409

Lab Report
2/6/03
ERM Southeast, Inc.
Attn: Mr. Rick Tarmvechia
7300 Cannel Exec. Park Ste. 200
Charlotte, NC 28226
;\PRISM
ueo6eroelEs, Ixc.
FUX aerviwx,W/4u16 Emmm�menbl5dutim¢
Page 13 of 16
Customer Project ID:
Integrls Metals
Customer Sample ID:
DW-1
Prism Sample ID:
AC70823
Login Group:
55941<4
Sample Collection Date/Time:
1/22103 14:15
Lab Submittal Date/Time:
1/24/03 08:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATEMNE
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
BENZENE
Not detected
U91
10
EPA 602
1I2910320:20
KTE
ETHYLBENZENE
Not detected
Ug1L
10
EPA$02
1@9/032020
KTE
IPE
Not detected
ug/L
5.0
EPA602
V29I0320:20
KTE
MTBE
Not detected
Ug/L
5o
EPA602
1129I032D:20
KTE
TOLUENE
Notdeteded
UgIL
1.0
EPA602
112910320:20
KTE
XYLENES
Not detected
ugfL
3.0
EPA 602
11291032020
KTE
PREP. METHOD 625
Completed
EPA625
1/2910311:00
SM
ACENAPHTHENE
Not detected
UgIL
10
EPA625
V1I0306:07
LAC
ACENAPHTHYLENE
Not detected
UgIL
10
EPA625
V11030c07
LAG
ANTHRACENE
Not detected
UgIL
10
EPA625
2111030607
LAC
BENZO(A)ANTHRACENE
Not detected
ug/L
10
EPA625
21110306:07
LAC
BENZO(B)FLUORANTHENE
Not detected
Ug1L
10
EPA625
V1I0306:07
LAC
BENZO(OFLUORANTHENE
Not detected
ug/L
10
EPA625
W110306:07
LAC
BENZO(A)PYRENE
Not detected
UgIL
10
EPA625
V110306:07
LAC
BENZO(GHI)PERYLENE
Not detected
Ug/L
10
EPA625
V110306:07
LAC
BIS(2-CHLOROETHOXY)METHANE
Not detected
ug/L
10
EPA625
211103 Oem
LAC
BIS(211LOROETHYL)ETHER
Not detected
ug/L
10
EPA625
211103 M:07
LAC
BIS(2- 11LOROISOPROPYQ[FTHER
Not detected
ug/L
10
EPA625
V110306:07
LAC
BIS(2-ETHYLHExYL)PHTHA1,ATE
Not detected
ug/L
10
EPA625
21110306:07
LAC
d-OROMOPHENYL PHENYL ETHER
Notdeteded
ug/L
10
EPA625
Y1 10306:07
LAC
BUTYL BENZYL PHTHALATE
Notdeteded
UgIL
10
EPA625
W110306:07
LAC
4-CHLORO-3-METHYLPHENOL
Notdeteded
ug/L
10
EPA625
W110306:07
LAC
2CHLORONAPHTHALENE
Not detected
ug/L
10
EPA625
21110306:07
LAC
2-CHLOROPHENOL
Not detected
ug/L
10
EPA625
211103 M 07
LAC
4-CHLOROPHENYL PHENYL ETHER
Notdeteded
ug/L
10
EPA625
211I0306:07
LAC
CHRYSENE
Notdeteded
ug/L
10
EPA625
VV0306:07
LAC
OIBENZO(A,HIANTHRACENE
Not detected
ug/L
10
EPA625
VV0306:07
LAC
01-N-BUT(LPHTHALATE
Nat doodled
UgIL
10
EPA625
W1103 M07
LAC
1,2-DICHLOROBENZENE
Not detected
ug/L
10
EPA625
D1103 OS07
lAC
1,3-DICHLOROBENZENE
Not detected
UgIL
10
EPA625
W110306:07
LAC
NC Certifcabon No. 402 - SC Certification No. 99012
- NC Drinking
Water Cart.
No. 37735 - FL
Cadlf ca on No. E87519
449 Springbrook Road A P.O. Box 240543
A Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Fred Number: 1-800 / 529-6364 A Fax: 704 / 525-0409
Lab Report
€
PRISM
4BORATORIELINe.
k
FUA $ervim Nat,To16 Emi,cnrenNl SdNwm
2/6103
Page 14 of 16
ERM Southeast, Inc.
Customer Project ID:
Integrls Metals
..Attn: Mr. Rick Tarravechia
Customer Sample ID:
DW-1
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC70823
Lapin Group:
5594K4
Charlotte, NC 28226
Sample Collection Date/Time:
1/22103 1415
Lab Submittal Date7Time:
1/24103 08:15
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST
TEST
REPORTING
METHOD
DATE/TIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
1.4-DICHLOROBENZENE
Not detected
ug/L
10
EPA625
W110306:07
LAC
3,3'-DICHLOROBENZIDINE
Not detected
ug/L
So
EPA625
V110306:07
LAC
2,4-DICHLOROPHENOL
Not detected
ug/L
10
EPA625
V110306:07
LAC
DIETHYL PHTHALATE
Not detected
ug/L
10
EPA625
211103 Do 07
LAC
2,4-DIMETHYLPHENOL
Not detected
ug/L
10
EPA625
21110306:07
LAC
DIMETHYL PHTHALATE
Not detected
UgIL
10
EPA 625
V1103 M 07
IAG
2,4-DINITROPHENOL
Not tletectetl
ug/L
50
EPA625
V11030607
LAD
2p-DINITROTOLUENE
Not detected
uglL
10
EPA625
V110306:07
LAC
2,6-DINITROTOLUENE
Not detected
uglL
10
EPA625
2111D306:07
LAC
DI-N-OCTYLPHTHALATE
Not detected
ug/L
10
EPA625
2/110 M07
LAC
FLUORANTHENE
Not detected
ug/L
10
EPA625
21110306:07
LAC
FLUORENE
Not detected
ug/L
10
EPA625
V1103%D7
LAC
HEXACHLOROBENZENE
Not detected
UgIL
10
EPA625
V110306o7
LAC
HEXACHLOROBUTADIENE
Nat detected
UgIL
10
EPA625
V110306:07
LAO
HEXACHLOROETHANE
Notdeteded
ug/L
10
EPA625
VV0306:07
LAC
INDENO(1.2.3-CD)PYRENE
Not detected
ug/L
10
EPA625
2N10306:07
LAC
ISOPHORONE
Notdeteded
ug1L
10
EPA625
21110306:07
LAC
2-METHYL4,6-DINITROPHENOL
Not detected
uglL
50
EPA625
W1103 06 07
LAC
NAPHTHALENE
Not detected
uglL
10
EPA625
VV0306:07
LAC
NITROBENZENE
Not detected
UgIL
10
EPA625
V110306:07
LAC
2-NITROPHENOL
Not detected
UgIL
10
EPA625
21110306:07
LAC
4-NITROPHENOL
Not detected
ug/L
50
EPA625
V110306:07
LAC
N-NITROSODI-N-PROPYLAMINE
Not detected
ug/L
10
EPA625
V11030S 07
LAC
PENTACHLOROPHENOL
Not detected
ugf-
50
EPA625
V11030 07
LAD
PHENANTI-RENE
Not detected
UgIL
10
EPA625
211103 US OT
lAC
PHENOL
Not detected
ug/L
10
EPA625
21110306:07
LAC
PYRENE
Notdeteded
ug/L
10
EPA625
V110306:07
LAC
1,2.4-TRICHLOROSENZENE
Not detected
ug/L
10
EPA625
V110306:07
LAC
24,6-TRICHLOROPHENOL
Notdeteded
Ug/L
10
EPA625
V1103 06 07
LAG
CS SAIIph0ce Not detected Ug/L 150 MADEPVPH =10317:08 JM\
NC Certification No. 402 - SC Cenifcabon No. 99012 - NC Drinking Water Coo. No. 37735 - FL Certification No. E87519
449 Springbmok Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
PRISM
ueosxroales, Ixc.
'
FJ sa.w AreMxd a eimm�aoul soiwore
2/6103
Page 15 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tarravechia
Customer Sample ID:
DW-1
7300 Carmel Exec. Park Ste. 200
Prism Sample ID:
AC70823
Login Group:
55941<4
Charlotte, NC 28226
Sample Collection Daterrime:
1122103 14:15
Lab Submittal Date/Time:
1124/03 08:15
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
TEST
REPORTING
METHOD
DATERIME
PARAMETER
RESULT
UNITS
LIMIT
REFERENCE
STARTED
ANALYST
C9C13 Aliphatice
Notdetected
uglL
100
MADEP VPH
2 0317:08
JMV
Cg-C10Aromalica
Not detected
ug/L
30
MADEP VPH
2/3/0317:08
JMV
SUmpate% Recovery -ED
119
%
(70-130)
MADEP VPH
V310317:08
JMV
Surrogate% ReCAvery -FID
120
%
(70-130)
MADEP VPH
=0317:08
JMV
Dilution Factor
1
ug4-
MADEP VPH
23/0317:08
JMV
EXTRACTION FOR EPH
Completed
MADEP£PH
113010311:00
SM
C9-C18 ALIPHATICS
Not detected
uglL
250
MADEP£PH
23I0313:08
GRR
C19-C36 ALIPHATICS
Not deeded
ug/L
250
MADEP-EPH
V310313:08
GRR
CI 1C22 AROMATICS
Not detected
ug/L
180
MADEP-EPH
2W0313:08
GRR
SURROGATE RECOVERY - ALIPHATIC
94
%
(40-140)
MADEP-EPH
2W031308
GRR
SURROGATE RECOVERY - AROMATIC
132
%
(40.140)
MADEP-EPH
VW0313:08
GRR
SURR:2-FWOROBIPHENYL
121
%
(40-140)
MADEP-EPH
VW0313:08
GRR
SURR:2-BROMONAPHTHALENE
116
to
(40-140)
MADEP-EPH
VW0313:08
GAR
DILUTION FACTOR
1
ug/l
MADEP-EPH
V310313:08
GRR
NC Certification No. 402 - SC Cedifcation No. 99012 - NC Drinking Water Carl. N0. 37735 - FL Certification No. E87519
449 Springbiock Road A P.O. Box 240543 A Charlotte, NC 28224-0543
Phone: 704 / 529.6364 A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409
Lab Report
PRISM
ueonxromrs, INC.
Full $e,Nce MwMIgI a Enrrtmn.l SdMw
2/6/03
Page 16 of 16
ERM Southeast, Inc.
Customer Project ID:
Integris Metals
Attn: Mr. Rick Tamavechia
Customer Sample ID:
DW-1
7300 Cannel Exec. Park Ste. 200
Prism Sample ID:
AC70823
Charlotte, INC 28226
lapin GrouD:
5594K4
Sample Collection Date/Time:
1/22/03 14:15
Lab Submittal Dale/Time:
1/24/03 08:15
The following analytical results have been
obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DAT WE
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
Sample Comments:
L�
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cen. No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28221-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

VPH (Aliphatics/Aromatics) Laboratory Reporting Form
Client Name ERM Southeast, Inc. Laboratory Name Prism Laboratories, Inc.
Project Name Integra Metals NC Certification # (Lab) 402
Site Location Atando Ave., Charlotte, NC Sample Matrix Water
Sample Information and Analytical Results
Method for Ranges: MADEP VPH
VPH Surrogate Standards
Aliphatic: 2,5-0ibromotoluene
Aromatic: 2,6-0ibromotoluene
Sample Identification
AC70820
AC70821
AC70822
AC70823
Collection Option (for soil)`
NA
NA
NA
NA
Date Collected
1IM03
1/22/03
1/22/03
1/22/03
Date Received
1/24/03
1/24/03
1/24/03
1124/03
Date Extracted
NA
NA
NA
NA
Date Analyzed
2/3/03
2/3/03
2/4/03
213/03
% Dry Solids
NA
NA
NA
NA
Dilution Factor
1
1
1
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample Results
C6 -CB Aliphatics"'
ug/L
47
150
<150
<150
1150
1 3500
1 <150
C9-C12 Aliphatics"
ug/L
28
100
Q00
<100
<100
<100
<100
C9 -C10 Aromatics—
ug/L
10
30
<30
<30
<30
<30
<30
Sample Surrogate Acceptance Range
70-130%
70-130%
70-130%
70-130%
70-130%
Aliphatic Surrogate%Recovery -FID
108%
90%
117%
122%
120%
Aromatic Surrogate%Recovery -PID
112%
94%
125%
124%
119%
Option 1 = Established fill line on vial OPtion 2 = Sampling Device (indicate brand, e.g. EnGOMTM) Option 3 = Field weight of soil
"Unadjusted value. Should exclude the concentration of any sunogate(s), internal standards, antllor concentrations of other ranges Mat elute within the speufied range.
MDL= Method Detection Limit RL=Reponing Limit Blank= Laboratory Method Blank or Trip Blank whichever is higher (indicate type)
VPH rev. 11/00
Were all performance/acceptance standards for required QA/QC procedures achieved?
Were any significant modifications to the VPH method made?
No VPH Trip Blank was submitted.
Page 1 of 1 VPH
EPH (Aliphatics/Aromatics) Laboratory Reporting Fore
Client Name ERM Southeast, Inc. Laboratory Name
Project Name Integris Metals NC Certification # (Lab)
Site Location Atando Ave., Charlotte, NC Sample Matrix
Yes No- Details Attached
No Yes- Details Attached
Prism Laboratories, Inc
402
Water
Sample Information and Analytical Results
Method for Ranges: MADEP EPH
EPH Surrogate Standards
Aliphatic: 1-Chloro-octadecane
Aromatic: o-Terphenyl
EPH Fractionation Surrogates
#1: 2-Bromonaphthalene
#2: 2-Fluorobiphenyl
Sample Identification
AC70820
AC70821
I AC70822
I AC70823
Date Collected
1122/03
1/22103
1/22103
1122103
Date Received
1124103
1/24103
124/03
1124/03
Date Extracted
1130103
1/30103
1/30/03
1/30/03
Date Analyzed
2/3/03
213/03
2/3/03
213103
% Dry Solids
NA
NA
NA
NA
Dilution Factor
1
1
1
1
Hydrocarbon Ranges
Units of Measure
MDL
RL
Blank
Sample Results
C9-CIS Aliphatics'
ug/L
130
250
250
<250
<250
<250
<250
C19-C36 Aliphatics'
ug/L
120
250
<250
1 <250
<250
<250
<250
C11 - C22 Aromatics"
ug/L
78
180
<180
<180
<180
<180
<180
Sample Surrogate Acceptance Range
40-140%
40-140%
40-140%
40-140%
40-140%
Aliphatic Surrogate % Recovery
49%
86%
103%
97%
94%
Aromatic Surrogate % Recovery
138%
131%
125%
134%
132%
Fractionation Surrogate Acceptance Range
40-140%
40-140%
40-140%
40-140%
40-140%
Fractionation Surrogate #1 % Recovery
134%
118%
122%
123%
116%
Fractionation Surrogate #2 % Recovery
1
130%
123%
122%
127%
121%
Unadjusted value. Should exclude the concentration of any sumogme(s), internal standards, and/or concentrations of other ranges that elute within the specified range.
MDL = Method Detection Limit RL = Reporting Limit Blank = Laboratory Method Blank
EPH rev. 11100
Were all performance/acceptance standards for required QA/QC procedures achieved?
Was blank correction applied as a significant modification of the method ?
Were any significant modifications to the EPH method made?
Page 1 of 1 EPH
as No- Details Attached
Yes No
No Yes -Details Attached