MO-6615_27296_CA_IAR_20021202

ERM NC, PC
December 2, 2002
Mr. Allen Schiff
NCDENR - Division of Waste Management
UST Section
919 N. Main Street
Mooresville NC 28115
Re: Initial Abatement Report
(20-Day Report)
Integris Metals facility
527 Atando Avenue
Charlotte, North Carolina
Dear Allen:
RECEIVED
DEC 0 32002
NC DEPT OF ENVIRONMENT
AND NATURAL RESOURCES
MOORESVILLE REGIONAL OFFICE
On behalf of Integris Metals, ERM is submitting one copy of the Initial.
Abatement Report (20-Day Report) prepared for the underground storage
tank (UST) release incident at the above referenced facility. A 24-hour
notification was submitted to you regarding this incident on November
13, 2002. Integris Metals is currently preparing to conduct a Phase I LSA.
Please do not hesitate to call' me at 704-541-8345 if you have any questions.
Sincerely,
Rick Tarravechia, P.G.
Project Manager
cc: Ms. Aimee Nash, Integris Metals
7300 Carmel Executive Park
Suite 200
Charlotte, NC 28226
[phone]
[phone] (Fax)
9

Integris Metals, Inc.
Initial Abatement Measures Report
Integris Metals
527AtandoAvenue RECEIVED
Charlotte, North Carolina ,
[DEC .0 3 2002
NC DEFT OF ENVIRONMENT
AND NATURAL RESOURCES.
MOORESVILLE REGIONAL OFFICE
December 2, 2002

A. Site Identification
DATE OF REPORT:
Facility I.D.:
Site Name:
Site Location:
Nearest City/Town:
UST Owner:
Address:
UST Operator:
Address:
Property Owner:
Address:
Property Occupant:
Address:
Consultant/Contractor:
Address:
Release Information:
Initial Abatement Measures Report
December 2. 2002
0-003949 UST Incident Number (if known): Unknown
Integris Metals
527 Atando Avenue
Charlotte County: Mecklenburg
Integrisetals (formerly Rio Algom, Vincent Metal Goods, and Edgecomb Steel)
455 85 MAvenue NW Phone: [phone]
Minneapolis, MN 55433
Vincent Metal Goods
527 Atando Avenue Phone: [phone]
Charlotte, NC 28206
Integris Metals
527 Atando Avenue Phone: [phone]
Charlotte, NC 28206
Integris Metals
527 Atando Avenue Phone: [phone]
Charlotte, NC 28206
ERM NC, PC
7300 Carmel Executive Park, Ste. 200, Charlotte, NC 28226 Phone: [phone]
Date Discovered: November 13, 2002
Latitude: 350 18' 40" N Longitude:
Estimated Quantity of Release: Unknown
Source of Release (e.g., Piping/UST): Two fuel oil USTs
contents of UST system(s) from which the release occurred):
800 42' 44" W
Tank
Installation
Closure
Size in
Tank
Number
Dates
Date
Gallons
Construction
Contents
1
1966 or earlier
(possibly as
Out of service
since 1981
Est. 6,000
Steel
Fuel oil
2
Est. 6,000
Steel
Fuel oil
early as 1949
Complete and include in report items B through J in the order listed.
I, Richard J. Tarravechia a Professional Engineer ' sed Geolo ' ircle one) for ERM NC. PC
(firm or company of employment), do cgjftfgrrthWQe information contained in this report is correct and accurate to the
best of my knowledge. ,.•`�a�� CAR01�A.,.
Richard J. Tarravechia, P.G.
(Please Affix Seal and Signature)
SEAL
1076 Q
J, TAR;.•`•
ERM NC, PC Page 2 of 4 Integris 20-Day Repomdoc— 12/2/02

B. Initial Abatement Activities
Discuss the following items:
temoval of regulated substance from UST;
700 gallons of residual product and one 55 gallon drum of sludge were removed from the two fuel oil USTs
on September 19, 2002.
Source control actions;
Removal of residual product from the two fuel oil USTs.
Contaminant migration control measures (sorbents, berms, etc.);
None required.
© Measures taken to mitigate fire/safety hazards;
None required.
Contaminated soil storage, treatment, and/or disposal;
Status of free product investigation and associated removal (if applicable).
FN—otapplicable.
C. Site History:
Using the format in Table B-1, list all UST systems currently or previously located at the site including
UST system number, product, capacity, date installed, date removed or closed, and whether a release was
discovered. UST system numbers should correspond to the site map information requested below. — See Table B-1
© Using the format in Table B-2, list the names, addresses, telephone numbers, and dates of
ownership/operation of all previous UST owners and operators of the UST system(s). — See Table B-2
D. Source Investigation
Use maps and tables whenever possible and provide the rationale for sampling performed.
To the extent information is available, describe soil sampling performed to confirm the presence and source of the
release including:
location of soil samples; SEE FIGURE 4 AND TABLE B-3
type of soil samples (from excavation, borehole, geoprobe, etc.);
date of sampling;
soil sample collection procedures (split spoon, grab, hand auger, etc.);
depth of soil samples below land surface;
© soil sample identification;
soil sample analyses; and
soil sample analytical results (list any contaminant above MDL).
Describe any groundwater sampling performed to confirm the presence and source of the release including:
location of groundwater samples/monitoring wells/water supply wells;
date of sampling; NO GROUND WATER SAMPLING HAS BEEN CONDUCTED.
groundwater sample collection procedures (bailer, pump, etc.);
groundwater sample identification;
groundwater sample analyses; and
groundwater sample analytical results (list any contaminant above MDL).
E. Figures
7'h minute USGS topographic quadrangle map (copy) with site location identified and showing an area
within 1,500-foot radius of source of release. SEE FIGURES 1 AND 3.
Site map with UST system location(s) including piping and pump islands, site boundaries, buildings,
named roads, subsurface utilities, basements, adjacent properties, and any on -site water supply wells,
ditched or adjoining surface waters. SEE FIGURE 2.
ERM NC, PC Page 3 of 4 Integris 20-Day Repon.doe — 12/2/02

Site map showing the results of all soil sampling conducted to date. Indicate sample identifications, sample
locations, sampling; depths, and analytical results. SEE FIGURE 4.
Site map showing the results of all groundwater sampling conducted to date. Indicate sample
identifications, sample locations/monitoring well identifications, and analytical results. NOT APPLICABLE
NOTE. If possible, use a single base map to prepare site plans using a map scale of I inch = 40 feet (or a smaller
scale for large sites, if'necessary). Maps and figures should include conventional symbols, notations, labeling,
legends, scales, and north arrows and should conform to generally accepted practices ofmap presentation such as
those enumerated in the USGS Geological Survey pamphlet, "Topographic Maps. "
F. Tables
Use format in Table B-3 to summarize soil sampling results. SEE TABLE B-3.
© Use format in Table B4 to summarize groundwater sampling results. NOT APPLICABLE
G. Appendices
Boring logs and lithologic descriptions; SEE APPENDIX A
© Well construction records (Table B-7); NOT APPLICABLE
Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature, etc.) made during
groundwater sampling; NOT APPLICABLE
Standard procedures used for sampling, field equipment decontamination, field screening, etc.; SEE APPENDIX B
Disposal manifests; SEE APPENDIX C
Laboratory reports and chain -of -custody documents and SEE APPENDIX D
Site -specific Health and Safety Plan (if not provided in an UST tank closure report).
ERM NC, PC Page 4 of Integris 20-Day Report.doc— 122/02

Figures

.a. � . ���.� 1 ! •G?� � trs' �� i
i6i
i
9 L9vttla Aoe I �I.� It l'i���'• 1� ���'f�l e� �t� t b I�'�� \`\� �f,`
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!(i) re` ./ .✓-•tom .s {I 11t ,-+`� .. ,In J/i/•_(.
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�.'�'"'!. `IN i�i� �..•�`i� •�`��r'� '� Ir�9 17 f�� i1R\ .�'fi/ L,` �"s�� �h` L•t
r'Y ••'- • l i 18 i1/ i •..._. - 4\nn � � 4 ^ ' `I\ ' ! a' \„r ;z ' I
!�'_i'.*• .�.'L' i. 1 4�• ✓mil' �yI nd7-
).June. n
t,l •T� � a ii. A•-s';/ \ ! ..-�^�'J' $ug ,. IF y.�` - u�jekl f ��II.
Source: Daniel N.C. 7:5 Minute Topographic I
Quadrangle, 1972: Contour Interval = 10 feet SCALE: 1 INCH = 2,000 FEET
RGURE
Environmental SITE LOCATION MAP
Resources. VINCENT METAL GOODS
ERM Manaeement' CHARLOTTE, NORTH CAROLINA 1

PROPERTY BOUNDARY
I I r
1 I
I I
IINTEGRIS METALS
I I Ld
I I z
Z
ui
I ,
a
0
I O ; UST-1 Z
F
I a
0
I
rc
x Ox I-tK: UST-2 ._
0 I I
a
i
L N
x
u
0
0
0
JSCALE IN FEET
0 25 50 100
FIGURE
= Environmental STYE PLAN
ma PnWRM METALS
ManResources 527 ATANDO AVENUE 2ERM $ CHARLOTTE, NORTH CAROU NA
m

O 00-F
-
nnep ,
O
n&49;
o
tI O
0� Do ° � �' •o'
d O�
Q�,,l� O
n� �a0 Oho
N e \
O ` /
\ q " 1% O�• Q 0 " SCALE IN FEET
MAP SOURCE: MECKLENBURG COUNTY ENGINEERING AND BUILDING STANDARDS DEPT. PIANIMETRIC MAPS O 400
3
Environmental SENSITIVE RECEPTOR AND ZONING MAP FIGURE
_ DnWRIS METALS
Resources
ann Management 527 ATANW AVENUE 3
n ERM S CHARLOTTE" NORTH CAROLINA
m

FILL PORT Vi VMG-6
IN VMG-9
II �/
II % VMG-7
VMG-5
II / �VMC-8
I.
VMG-4 1 ,:''153;- ®VMG-2
II ®VMG-3
I I
II
II
II
III
vmC-10 .II
fUl
II
I I
II
I I
II
II®°L'c-1s
II
II
II
II
II ®VMG-13
I I
VMG-1 VMG-12
II
®II
VMG-1s II
®O FILL PORT
vMG-1
EL GEND
® GEOPROBE SOIL BORING
OLD FURNACE
OFFICES
SCALE IN FEET
15 30
Environmental SOIL SAMPLE LOCATION MAP
Resources IIV'EGRIS MATS 4
s ERM Management �ArNORTH � UNA
T

Tables

TABLE B-1 SITE HISTORY
UST System Information Facility I.D.: 0-003949
Date: December 2, 2002 Incident Number and Name: Integris Metals - Pending
UST ID Number
-
Product
Capacity (gallons)
Date Installed
..
Date Pennanentty JASWasia�el�ase
Closed, or Still in USe'
sociad UST
"System? (Yes/No)
1
Fuel oil
est. 6,000
1966 or earlier
(possibly as early
as 1949)
Out of Service since
approximately 1981
Yes
2
Fuel oil
est. 6,000
1966 or earlier
(possibly as early
as 1949)
Out of Service since
approximately 1981
Yes
- Still in use means not permanently closed. FRP = Fiberglass reinforced plastic
TABLE B-2 SITE HISTORY
UST Owner/Operator Information (most recent first) Facility I.D.: 0-003949
Date: December 2, 2002 Incident Number and Name: Integris Metals - Pending
UST ID Number
I Name of Owner or Operator
Dates of Ownership/Operation
Owner or Operator?
1 and 2
Intgris Metals
12001-present (never operated USTs)
owner
Address ""
Telephone Number
527 Atando Avenue
Charlotte, NC 28206
704-372-9900
UST ID Number
Name of Owner or Operator
jDates of Ownership/Operation .
Owner or Operator? -
1 and 2
Rio Algom, Ltd.
1995-2001 (never operated USTs)
owner
Address --
" .:-
Telephone Number
527 Atando Avenue
Charlotte, NC 28206
704-372-9900
UST ID Number
IName of Owner or Operator
Dates of Ownership/Operation '-
Owner or Operator? "
1 and 2
IVincent Metal Goods
1976.1995 (operated UST until 1981)
owner/operator
Address -
-
Telephone Number
527 Atando Avenue
Chadotte, NC 28206
704-372-9900
UST ID Number - -
Name of Owner or Operator
Dates of Ownership/Operation
Owner or Operator?
1 and 2
Edgecomb Steel
1949 - 1974
owner/operator
Address
Telephone Number
527 Atando Avenue
Charlotte. NC 28206
unknown
Integris Tables.xls:B-1&B-2 History Page 1 of 1

TABLE B-3 SUMMARY OF SOIL SAMPLING RESULTS
Date: 12/01/02 Incident Number and Name: Integris Metals - Pending Facility I.D.: NA
Analytical Method
r j
O
EPA 8015 (mg/kg)
VOCs - 8260 (mg/kg)
%
M
c
C
C
N
N
N
O
N
N
C
N
d
0_ L
1N1
L
T
a
N t
C
N
O
N
T
J
2
CL
.L..
L
Depth
9 E
N=
N
N=
C
J
T
_
W
RI
O
2
J
QI
�]
O
d
2
O
.L..
L
O
O N
b 2'
Sample ID
Date
(ft. BGL)
ii n
r
m
F
N
In
d
H
cCi
a
0
w
X
y
n
z
VMG-1
10/19/02
NO
NO
VMG-2
10/19/02
13
56
94
2,400
ND
ND
0.95
3.40
NO
NO
2.20
2.10
NO
0.90
1.50
9.50
1.60
7.40
3.40
VMG-3
10/19/02
14
64
140
2,500
ND
NO
0.78
NO
NO
NO
2.60
1.20
NO
0.65
0.57
6.50
1.40
0.41
NO
VMG-4
10/19/02
160
15,000
VMG-5
10/19/02
110
1,700
VMG-6
10/19/02
ND
ND
VMG-7
10/19/02
NO
ND
VMG-8
10/19/02
NO
ND
VMG-9
10/19/02
NO
NO
VMG-10
10/19/02
NO
NO
VMG-11
10/19/02
100
8,100
VMG-12
10/19/02
16
62
120
2,100
NO
ND
0.99
0.85
ND
NO
4.20
2.70
0.43
1.40
2.70
11.0
3.90
19.0
4.50
VMG-13
10/19/02
6
45
480
12,000
NO
NO
NO
ND
ND
ND
10.0
4.20
NO
3.20
5.70
32.0
7.80
16.0
9.60
VMG-14
10/19/02
NO
NO-
VMG-15
10/19/02
1 290
5,200
Soil -Groundwater MSCC -- 10 10
0.0056
7
0.24
5
0.92
0.37F1,
3
3
2
NE
0.58
2
8
7
Residential MSCC -
22
3,200
1,560
32K
156
156
166
156
1,564
NE
63
156
782
782
Industrial/Commercial MSCC
200
82K
40K
200K
4,088
4,0888
4,088
4,088
40,880
NE
1,635
4,088
20,440
20,440
Analytical Method
VPH/EPH (mg/kg)
8270 (mg/kg)
N
N
L
N
L
L
p
E
Q
to
N N
Depth
N
c7
Q
U
O
o
E
Sample ID
Date
(ft. BGQ
U
U
U
U
U
o
U Q
Soil -Groundwater MSCC
72
3,255
mmobil
34
Residential MSCC _
939
9,386
193,860
469
Industrial/Commercial MSCC
24,528
245,280
>100%
12,264
Only detected compounds are shown in table
mg/kg=Milligrams/kilogram --= Not analyzed
BGL = Below ground level NO = Not detected
Results shown in bold exceed NE = Not established
soil -groundwater MSCC NA=Not Applicable
Integris Tables.xls:B-3 Soil Results Page 2 of 2

Appendix A
Boring Logs

SOIL BORING LOGS
INTEGRIS METALS
CHARLOTTE, NORTH CAROLINA
Boring I.D.
Interval
(feet)
VOCs
(ppm)
Sample Description
VMG-1
0-0.75
Gravel
0.754
0
Reddish brown silty CLAY. No odor.
VMG-2
—
—
Intersected top of UST 15.5 ft. from manhole. Re -locate boring to 18 ft. from manhole.
04
2
Reddish brown silty CLAY. No odor.
4-8
32
Reddish brown silty CLAY. Slight odor.
8-12
56
Reddish brown silty CLAY. Mottled and gray 11.5-13 ft. Moderate odor.
13
56
Refusal on concrete.
VMG-3
0-4
0
Reddish brown silty CLAY. Slight odor.
4-8
13
Reddish brown silty CLAY. Slight odor.
8-12
45
Reddish brown silty CLAY. Slight odor.
12-14
64
Reddish brown silty CLAY, Strong odor. Green staining.
14-16
58
Reddish brown silty CLAY, Strong odor. Green staining.
VMG-4
-
—
Intersected UST 18 feet from manhole at depth of 4.5 ft. Re -located boring.
0-4
32
Reddish brown silty CLAY. Slight Odor
4-8
0
Reddish brown silty CLAY.
8-11
0
Reddish brown silty CLAY.
VMG-5
0-4
0
Reddish brown silty CLAY.
4-8
0
Reddish brown silty CLAY.
8-12
2
Reddish brown silty CLAY.
12-14
68
Reddish brown silty CLAY. Odor.
14-15.5
89
Same as above. Refusal at 15.5 feet BGL.
VMG-6
0-4
0
Yellowish brown silty CLAY. No odor.
4-8
0
Yellowish brown silty CLAY. No odor.
8-12
0
Yellowish brown silty CLAY. No odor.
12-16
0
Yellowish brown silty CLAY. No odor.
VMG-7
0-4
0
Hard reddish brown CLAY. No staining or odor.
4-6
0
Hard reddish brown CLAY. No staining or odor.
6-8
0
Hard reddish brown CLAY. No staining or odor.
VMG-8
0-2
0
Reddish brown silty CLAY. Fill soil. No odor.
2-4
0
Reddish brown silty CLAY. Fill soil. No odor.
4-6
0
Reddish brown silty CLAY. Fill soil. No odor.
6-8
0
Reddish brown silty CLAY. Fill soil. No odor.
VMG-9
0-4
0
Orange brown silty CLAY. No odor.
4-8
0
Orange brown silty CLAY. No odor.
8-12
0
Orange brown silty CLAY. No odor.
12-16
8
Orange brown silty CLAY. No odor.
VMG-10
0-4
0
Reddish brown silty CLAY. No odor.
4-8
0
Reddish brown silty CLAY. No odor.
8-12
0
Same as above. Intermixed gravel at 11 feet.
VMG-11
0-4
0
Reddish brown silty CLAY. No odor.
4-8
0
Reddish brown silty CLAY. No odor. -
8-12
0.5
Reddish brown silty CLAY. No odor.
12-14
6
Reddish brown silty CLAY. No odor.
14-16
23
Reddish brown silty CLAY. No odor.
Boring Logs.XLS:Geoprobe Log Page 1 of 2 12/02/2002

Boring I.D.
Interval
(feet)
VOcs
(ppm)
Sample Description
VMG-12
0-4
0.5
Reddish brown silty CLAY. No odor.
4-8
1.5
Reddish brown silty CLAY. No odor.
8-12
1.5
Green SILT. No odor.
12-16
62
Green silt, odorous.
VMGA 3
0-2
13
Reddish brown silty CLAY. Slight odor.
2-4
35
Reddish brown silty CLAY. Odor.
4-6
45
Reddish brown silty CLAY. Odor.
6-8
38
Reddish brown silty CLAY. Odor.
8-10
12
Reddish brown silty CLAY. Slight odor.
10-12
0
Reddish brown silty CLAY. No odor.
12-16
13
Reddish brown silty CLAY. No odor.
VMG-14
0-2
0
Reddish brown silty CLAY, no odor.
2-4
0
Soil grades to yellow -brown clayey SILT, no odor.
4-7
0
Yellow -brown -green hard SILT.
7-8
0
Hard red brown CLAY.
VMG-15
0-2
0
Brown yellow clayey SILT. No odor.
2-4
50
Brown yellow clayey SILT. No odor.
4-6
28
Red brown CLAY. No odor.
6-8
28
Red brown CLAY. No odor.
8-10
50
Red brown CLAY. No odor.
10-12
34
Red brown CLAY. No odor.
Drilling Method:
Geoprobe macro -core
Logged by:
R.10Tarravechia
Date:
/191 002
Boring Logs.XLS:Geoprobe Log Page 2 of 2 12/02/2002

Appendix B
Standard Procedures

SOIL SAMPLING AND ANALYSIS
Geoprobe Drilling/Sampling
Geoprobe soil samples were collected using a 1.5-inch macro -core
sampling tube lined with a plastic sleeve. Continuous samples were
collected in 4-foot intervals. New plastic liners were used for each
sample interval. Drilling and sampling equipment were
decontaminated using steam -cleaning equipment between borings.
Field Logging and Laboratory Analysis
Soil samples were visually inspected and the physical characteristics
logged upon retrieval of the sample from the soil boring. Soil
samples were screened in the field using an organic vapor meter
(Bacharach TLV, HNu photo -ionization detector, or comparable
equipment), and using the headspace screening method. This
equipment was calibrated prior to use.
Laboratory analyses were conducted by a North Carolina approved
laboratory. Sample collection, handling, and preservation were
conducted in accordance with accepted protocol, including chain -of -
custody documentation.
Wj erryVnitche11\procedur. doc

Appendix C
Disposal Manifests

Appendix D
Laboratory Reports and Chain of
Custody Documents

Appendix C
Disposal Manifests

HAZ-MAT
TRANSPORTATION AND DISPOSAL
P. O. BOX 37392 • CHARLOTTE, N.C. 28237
(704 332-5600
FAX [phone]
NON -HAZARDOUS SPECIAL WASTE
GENERATOR LOCATION ,(
NAME 11�YeClI/YY
ORIGINATING ADDRESST,Q.�✓r
MAILING ADDRESS
CITY - STATE ZIP
PHONE NO.
CONTACT NAME
Manifest No. 1.3419
P.O. No.
Job No. 61A- 3-;7- 2?
WORK CONTRACTED BY
Bill To (If different from information at left) 004:
Gr //
NAME
ADDRESS^ /J l_`W�
CITY �^.\tt,'1D.�1 � (� SpTTAT�TE�r1N('• ZIP
PHONE NO.
CONTACTNAME�-
DES. OF WASTE: (el%R.X/G LURTC% lj*'(JCL.✓:�SG /' I/ I u
PniM anmy
-" DESCRIPTION
QUANTITY
LINE TO
AL
1. WATER, OIL & COOLANT PUMPED FROM TANKS OR DRUMS
2. OFF SPEC LIGHT OIL, WATER & GAS PUMPED FROM TANKS OR DRUMS
3. 55 GALLON DRUMS REMOVED - SOLID
4. 55 GALLON DRUMS REMOVED - LIQUID
5.
6. C G
��
7.
a- io d
9. SERVICE CHARGE
10. TRANSPORTATION
GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been properly
described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if the waste is a treatment residue of a previously restricted
hazardous waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has been treated in ordance with the requirements of 40 CFR Part 268 and is no longer
a hazardous waste as define by 40 CFR Part 261. IN
r�Ic61 k ;1,�;►�tl�� Ian 4 --1 > z
Generator Authorized Agent -Name J Signature Shipment Date
HAZ- MAT TRANSPORTER II
TRANSPORTATION AND DISPOSAL e. Name
P. O BOX 37392 • CHARLOTTE, N.C. 28237 1. Address
a. Driver Namp. //,TNe ] •�- g. Driver Name / Title
b. Phone No/'� '�'� ZU c. Truck No. �/ �� h. Phone No. I. Truck No.
Hazardous Waste Transporter Permits J. Transporter II Permit Nos.
EPA NCR 000003186
EPA D04 461370
river ignature Shiprem Date Driver Signature Shlrnerd Date
SecaiionnniAILISXEIQF[MIiI4I1TK1?;OEfi(1'1��0 r5..
Site Name: Haz-Mat Transportation & Disposal. Inc. a. Phone No. 704-332.5600
Physical Address: 210 Dalton Avenue b. Melling Address: P.O. Box 37392
Charlotte, N.C. 28237 Charlotte. N.C. 28237
e. Discrepancy Indication Space
This Is moodily that all non -hazardous material removed from above location has been received and will be
are blended Into a beneficial reusable fuel for use in large industrial burners. (2) Wade waters are to be treate
than into the CMUD sanitation sewer system under permit IUP15012. ) Sludges from treatment
(4) Our treatment system operates an a firs] in, first out basis and product should be processed within seven
proper
are on
SIGNATURE OF FACILITY AGENT DATE M NrH DAY YIEARVO
ORIGINAL - FINAL Y.S.O. • YELLO IIISPOSER • PINK-1STTS.0. • GOLD -GENERATOR

HAZ-MAT
TRANSPORTATION AND DISPOSAL
13706
Manifest No.
P. 6. BOX 37392 • CHARLOTTE, N.C. 28237 P0. No.
VO4 332-5600
FAX [phone]
NON -HAZARDOUS SPECIAL WASTE Job No.
GENENAME��V(nu—nl 1 f I�'I ���5 WORKCONTRACTEDfrom
DBV .
(��__,,,,�� JJ�� /�,� Bill To (N different from inforMmation at left)A � Pic -
ORIGINATING ADDRESS — r7'ILr'1G+1� � NAME e RI ' / Nc i
MAILING
ADDRESS j,�
CITY �'`� IQ 1 l C� /� 9� STATE ZIP
PHONE NO.
ADDRESS
CITY
PHONE NO.
LO
CONTACT NAME k
- / - CONTACTNAME T\I VI I I CY" (AV L --Tlz—
DES.OFWASTE:—�L.�f�, 1N1 TG✓ )"/ i/ I D Quantity
DESCRIPTION
QUANTITY
LINET
3TAL
1. WATER, OIL & COOLANT PUMPED FROM TANKS OR DRUMS
2. OFF SPEC LIGHT OIL, WATER & GAS PUMPED FROM TANKS OR DRUMS
a. 55 GALLON DRUMS REMOVED - SOLID
4. 55 GALLON DRUMS REMOVED - UOUID
5.
6.
7.
6. G2J
9. SERVICE CHARGE 7-a
10. TRANSPORTATION
GENERATOR'S CERTIFICATION: I hereby certify that the above named material is not a hazardous waste as defined by 40 CFR Part 261 or any applicable state law, has been property
described, classified and packaged, and is in proper condition for transportation according to applicable regulations; AND, if the waste is a treatment residue of a previously restricted
hazardous waste subject to the Land Disposal Restrictions, I certify and warrant that the waste has been treated in accordance with the requirements of 40 CFR Part 268 and is no longer
a hazardous waste as defined by 40 CFR Part 261. 1 t
Generator Authorized gent Naute Signature unionism Date
HAZ-MAT
TRANSPORTATION AND DISPOSAL
P. O. BOX 37392 - CHARLOTIE, N.C. 28237
a. Driver Name/ 7Tale JG 'e-
b.Phone No./il % ---7-7Z _-,E400 c.Truck No.
Hazardous Waste Transporter Permits
EPA NCR 000003186
EPA NCD04M370 /1 /f
Site Name: Haz-Mat Transportation & Disposal Inc.
Physical Address: 210 Dalton Avenue
Charlotte. N.C. 28237
e. Discrepancy Indication Space
This is to certify mat all non -hazardous material
am blended Into a beneficial reusable fuel for us
than into the CMUD sanitation mar systei
(4) Our treatment system operates on a first In,
am
e. Name
g.Driver Name
h. Phone No. I. Truck No.
j. Transporter II Permit Nos.
a. Phone No.
b. Maiing Address:
proper
1-1•I- �
on
Isunamne ur rauuhTaurnh �M�y- „� _J DATE (MONTH i (DAY 1�( YEAR Cr2 /
ORIGINAL - FINAL T.S.D. • YELLOW --DIS R • PINK -iST18.0. • GOLD -GENERATOR

Appendix D
Laboratory Reports and Chain of
Custody Documents

1.
Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, INC 28226
I PRISM
1 LABORATORIES, INC
Full Service Analytical & Environmental Solutions
Customer Project ID:
VMG
Customer Sample ID:
VMG-1
Prism Sample ID:
AC61489
Loqin Group:
A0024K15
Sample Collection DatefTime:
10/19/02
Lab Submittal Date/Time:
10/21/02
Page 1 of 23
07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
Less than
mg/kg
10
8015MOD/3550
10/23/02 19:18
EHT
TPH-GASOLINE RANGE / PREP. 5030
Less than
mg/kg
1.0
8015MOD/5030
10/21/02 20:16
JMV
CALCULATIONS BASED ON DRY WT.
85
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
Nov 1 4 2002
INC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 2 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-2
Prism Sample ID:
AC61490
Loqin Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATEFFIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
TPH - DIESEL RANGE
2400
mg/kg
500
8015MOD/3550
10/24/02 03:47
EHT
TPH-GASOLINE RANGE / PREP. 5030
94
mg/kg
10
8015MOD/5030
10/22/02 10:50
JMV
BENZENE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
BROMOBENZENE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
BROMOCHLOROMETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
BROMODICHLOROMETHANE
Not detected
ug/kg
320
826OB15035
10/22/02 00:38
KC
BROMOFORM
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
BROMOMETHANE
Not detected
ug/kg
640
8260B/5035
10/22/02 00:38
KC
N-BUTYLBENZENE
2200
ug/kg
320
8260B/5035
10/22/02 00:38
KC
SEC-BUTYLBENZENE
2100
ug/kg
320
8260B/5035
10/22/02 00:38
KC
TERT-BUTYLBENZENE
Not detected
ug/kg
320
826013/5035
10/22/02 00:38
KC
CARBON TETRACHLORIDE
Not detected
ug/kg
320
8260B15035
10/22/02 00:38
KC
CHLOROBENZENE
Not detected
ug/kg
320
82BOB15035
10122/0200:38
KC
CHLORODIBROMOMETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
CHLOROETHANE
Not detected
ug/kg
640
8260B15035
10/22/02 00:38
KC
CHLOROFORM
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
CHLOROMETHANE
Not detected
ug/kg
640
8260B/5035
10/22/02 00:38
KC
2-CHLOROTOLUENE
Not detected
ug/kg
320
826OB15035
1012210200:38
KC
4-CHLOROTOLUENE
Not detected
ug/kg
320
82608/5035
10/22/02 00:38
KC
1,2-DIBROMO-3-CHLOROPROPANE
Not detected
ug/kg
640
82608/5035
10/22/02 00:38
KC
1,2-DIBROMOETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
DIBROMOMETHANE
Not detected
ug/kg
320
826OB/5035
10/22/02 00:38
KC
1,2-DICHLOROBENZENE
Not detected
ug/kg
320
8260B15035
10122/0200:38
KC
1,3-DICHLOROBENZENE
Not detected
ug/kg
320
82608/5035
10/2210200:38
KC
1,4-DICHLOROBENZENE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
DICHLORODIFLUOROMETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
1,1-DICHLOROETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
1,2-DICHLOROETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
1,1-DICHLOROETHENE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
CIS-1,2-DICHLOROETHENE
Not detected
ug/kg
320
8260B15035
10/22/02 00:38
KC
TRANS-I,2-DICHLOROETHENE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking Water Cert.
No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O.
Box 240543 A Charlotte, NC
28224-0543
Phone: 704 / 529-6364 A Toll Free Number:
1-800
/ 529-6364 A
Fax: 704 / 525-0409

r
Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
AIL PRISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 3 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-2
Prism Sample ID:
AC61490
Login Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
1,2-DICHLOROPROPANE
Not detected
ug/kg
320
8260B/5035
10/22/02
00:38
KC
1,3-DICHLOROPROPANE
Not detected
ug/kg
320
82608/5035
10/22/02
00:38
KC
2,2-DICHLOROPROPANE
Not detected
ug/kg
320
8260B/5035
10/22/02
00:38
KC
1,1-DICHLOROPROPENE
Not detected
ug/kg
320
826OB/5035
10/22/02
00:38
KC
ETHYLBENZENE
950
ug/kg
320
826OB15035
10/22/02
00:38
KC
HEXACHLOROBUTADIENE
Not detected
ug/kg
320
8260B/5035
10/22/02
00:38
KC
ISOPROPYLBENZENE
900
ug/kg
320
826013/5035
10/22/02
00:38
KC
P-ISOPROPYLTOLUENE
1500
ug/kg
320
8260B/5035
10/22/02
00:38
KC
METHYLENE CHLORIDE
Not detected
ug/kg
6400
8260B15035
10/22/02
00:38
KC
NAPHTHALENE
9500
ug/kg
320
826OB/5035
10/22/02
00:38
KC
N-PROPYLBENZENE
1600
ug/kg
320
82606/5035
10/22/02
00:38
KC
STYRENE -
Not detected
ug/kg
320
826013/5035
10/22/02
00:38
KC
1,1,1,2-TETRACHLOROETHANE
Not detected
ug/kg
320
82608/5035
10/2210200:38
KC
1,1,2,2-TETRACHLOROETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02
00:38
KC
TETRACHLOROETHENE
Not detected
ug/kg
320
826013/5035
10/22/02
00:38
KC
TOLUENE
Not detected
ug/kg
320
826013/5035
10/22/02
00:38
KC
1,2,3-TRICHLOROBENZENE
Not detected
ug/kg
320
8260B/5035
10/22/02
00:38
KC
1,2,4-TRICHLOROBENZENE
Not detected
ug/kg
320
8260B15035
10/22/02
00:38
KC
1,1,1-TRICHLOROETHANE
Not detected
ug/kg
320
826013/5035
10/2210200:38
KC
1,1,2-TRICHLOROETHANE
Not detected
ug/kg
320
826013/5035
10/22/02
00:38
KC
TRICHLOROETHENE
Not detected
ug/kg
320
826OB15035
10/22/02
00:38
KC
TRICHLOROFLUOROMETHANE
Not detected
ug/kg
320
8260B/5035
10/22/02
00:38
KC
1,2,3-TRICHLOROPROPANE
Not detected
ug/kg
320
8260B15035
10/22/02
00:38
KC
1,2,4-TRIMETHYLBENZENE
7400
ug/kg
320
" 826OB15035
10/22/02
00:38
KC
1,3,5-TRIMETHYLBENZENE
3400
ug/kg
320
82608/5035
10/2210200:38
KC
VINYL CHLORIDE
Not detected
ug/kg
640
826013/5035
10/22/02
00:38
KC
TOTAL XYLENES
3400
ug/kg
320
82606/5035
10/22/02
00:38
KC
2-BUTANONE (MEK)
Not detected
ug/kg
3200
82608/5035
10/22/02
00:38
KC
2-CHLOROETHYL VINYL ETHER
Not detected
ug/kg
640
826013/5035
10/22/02
00:38
KC
4-METHYL-2-PENTANONE (MIBK)
Not detected
ug/kg
3200
826OB/5035
10/22/02
00:38
KC
ACETONE
Not detected
ug/kg
6400
826OB15035
10/22/02
00:38
KC
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking Water Cert.
No. 37735 - FL
Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543
♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364
♦ Toll Free Number: 1-800
/ 529-6364 ♦ Fax: 704 / 525-0409

Lab Report PRISM
f!
LABORATORIES, INC
Full Service Analylical & Environmental Solutions
10/25/02 Page 4 of 23
ERM Southeast, Inc. Customer Project ID: VMG
Attn: Mr. Rick Tarravechia Customer Sample ID: VMG-2
7300 Carmel Exec. Park Ste. 200 Prism Sample ID: AC61490
Charlotte, INC 28226 Login Group: A0024K15
Sample Collection Date/Time: 10/19/02
Lab Submittal Date/Time: 10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATErrIME
STARTED
ANALYST
CARBON DISULFIDE
Not detected
ug/kg
6400
8260B/5035
10/22/02 00:38
KC
VINYL ACETATE
Not detected
ug/kg
3200
82608/5035
10/22/02 00:38
KC
CIS-1,3-DICHLOROPROPENE
Not detected
ug/kg
320
826OB/5035
10/22/02 00:38
KC
TRANS-I,3-DICHLOROPROPENE
Not detected
ug/kg
320
8260B15035
10/22/02 00:38
KC
2-HEXANONE
Not detected
ug/kg
3200
826OB15035
10/22/02 00:38
KC
IPE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
MTBE
Not detected
ug/kg
320
8260B/5035
10/22/02 00:38
KC
SURR:DIBROMOFLUOROMETHANE
111
%
72-137
8260B15035
10/22/02 00:38
KC
SURR:TOLUENE-D8
102
%
73-128
8260B/5035
10/22/02 00:38
KC
SURR:BROMOFLUOROBENZENE
123
%
69-131
8260B/5035
1012210200:38
KC
CALCULATIONS BASED ON DRY WT.
77
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
GVF
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
1 PR.ISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 5 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG3
Prism Sample ID:
AC61491
Loqin Group:
AO024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
TPH - DIESEL RANGE
2500
mg/kg
500
8015MOD/3550
10/24/02 09:22
EHT
TPH-GASOLINE RANGE / PREP. 5030
140
mg/kg
10
8015MOD/5030
10/22/02 12:01
JMV
BENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
BROMOBENZENE
Not detected
ug/kg
340
82608/5035
10/22/02 01:17
KC
BROMOCHLOROMETHANE
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
BROMODICHLOROMETHANE
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
BROMOFORM
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
BROMOMETHANE
Not detected
ug/kg
680
8260B15035
10/22/02 01:17
KC
N-BUTYLBENZENE
2600
ug/kg
340
8260B15035
10/22/02 01:17
KC
SEC-BUTYLBENZENE
1200
ug/kg
340
826013/5035
10/22/02 01:17
KC
TERT-BUTYLBENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
CARBON TETRACHLORIDE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
CHLOROBENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
CHLORODIBROMOMETHANE
Not detected
ug/kg
340
82606/5035
10/22/02 01:17
KC
CHLOROETHANE
Not detected
ug/kg
680
826013/5035
10/22/02 01:17
KC
CHLOROFORM
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
CHLOROMETHANE
Not detected
ug/kg
680
82608/5035
10/22/02 01:17
KC
2-CHLOROTOLUENE
Not detected
ug/kg
340
8260B/5035
10122/0201:17
KC
4-CHLOROTOLUENE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
1,2-DIBROMO-3-CHLOROPROPANE
Not detected
ug/kg
680
826013/5035
10122/0201:17
KC
1,2-DIBROMOETHANE
Not detected
ug/kg
340
82608/5035
10/22/02 01:17
KC
DIBROMOMETHANE
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
1,2-DICHLOROBENZENE
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
1,3-DICHLOROBENZENE
Not detected
ug/kg
340
82608/5035
10/22/02 01:17
KC
1,4-DICHLOROBENZENE
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
DICHLORODIFLUOROMETHANE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
1,1-DICHLOROETHANE
Not detected
ug/kg
340
82606/5035
10/22/02 01:17
KC
1,2-DICHLOROETHANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
1,1-DICHLOROETHENE
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
CIS-1,2-DICHLOROETHENE
Not detected
ug/kg
340
82606/5035
10/22/02 01:17
KC
TRANS-I,2-DICHLOROETHENE
Not detected
ug/kg
340
82608/5035
10/22/02 01:17
KC
INC Certification No. 402 - SC Certification No. 99012 -
NC Drinking
Water Cert.
No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box
240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number:
1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
i' LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 6 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-3
Prism Sample ID:
AC61491
Login Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
1,2-DICHLOROPROPANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
1,3-DICHLOROPROPANE
Not detected
ug/kg
340
82606/5035
10/22/02 01:17
KC
2,2-DICHLOROPROPANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
1,1-DICHLOROPROPENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
ETHYLBENZENE
780
ug/kg
340
8260B15035
10/22/02 01:17
KC
HEXACHLOROBUTADIENE
Not detected
ug/kg
340
8260B15035
10/2210201:17
KC
ISOPROPYLBENZENE
650
ug/kg
340
8260B15035
10/22/02 01:17
KC
P-ISOPROPYLTOLUENE
570
ug/kg
340
8260B/5035
10/22/02 01:17
KC
METHYLENE CHLORIDE
Not detected
ug/kg
6800
826013/5035
10/22/02 01:17
KC
NAPHTHALENE
6500
ug/kg
340
8260B/5035
10/22/02 01:17
KC
N-PROPYLBENZENE
1400
ug/kg
340
826OB15035
10/22/02 01:17
KC
STYRENE
Not detected
ug/kg
340
82608/5035
10/22/02 01:17
KC
1,1,1,2-TETRACHLOROETHANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
1,1,2,2-TETRACHLOROETHANE
Not detected
ug/kg
340
82608/5035
10/22/02 01:17
KC
TETRACHLOROETHENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
TOLUENE
Not detected
ug/kg
340
826013/5035
10/22/02 01:17
KC
1,2,3-TRICHLOROBENZENE
Not detected
ug/kg
340
826OB15035
10/22/02 01:17
KC
1,2,4-TRICHLOROBENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
1,1,1-TRICHLOROETHANE
Not detected
ug/kg
340
8260B/5035
10/2210201:17
KC
1,1,2-TRICHLOROETHANE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:17
KC
TRICHLOROETHENE
Not detected
ug/kg
340
82608/5035
10/22/02 01:17
KC
TRICHLOROFLUOROMETHANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
1,2,3-TRICHLOROPROPANE
Not detected
ug/kg
340
82606/5035
10/22/0201A7
KC
1,2,4-TRIMETHYLBENZENE
410
ug/kg
340
8260B/5035
10/2210201:17
KC
1,3,5-TRIMETHYLBENZENE
Not detected
ug/kg
340
826OB15035
10/22/02 01:17
KC
VINYL CHLORIDE
Not detected
ug/kg
680
82608/5035
10/22/02 01:17
KC
TOTAL XYLENES
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
2-BUTANONE (MEK)
Not detected
ug/kg
3400
826013/5035
10/22/02 01:17
KC
2-CHLOROETHYL VINYL ETHER
Not detected
ug/kg
680
826013/5035
10/22/02 01:17
KC
4-METHYL-2-PENTANONE (MIRK)
Not detected
ug/kg
3400
82608/5035
10/22/02 01:17
KC
ACETONE
Not detected
ug/kg
6800
8260B/5035
10/22/02 01:17
KC
NC Certification No. 402 - SC Certification
No. 99012 -
INC Drinking Water Cert.
No. 37735 - FL
Certification No. E87519
449 Springbrook Road ♦ P.O. Box
240543 ♦ Charlotte, NC
28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number:
1-800 / 529-6364 ♦
Fax: 704 / 525-0409

Lab Report
PRISM
LABORATORIES, INC
Full Service Analytical 8 Environmental Solutions
10/25/02 Page 7 of 23
ERM Southeast, Inc. Customer Project ID: VMG
Attn: Mr, Rick Tarravechia Customer Sample ID: Vill
7300 Carmel Exec. Park Ste. 200 Prism Sample ID: AC61491
Charlotte, NC 28226 Login Group: A00241<15
Sample Collection Date/Time: 10/19/02
Lab Submittal Date/Time: 10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
CARBON DISULFIDE
Not detected
ug/kg
6800
8260B/5035
10/22/02 01:17
KC
VINYL ACETATE
Not detected
ug/kg
3400
8260B/5035
10/22/02 01:17
KC
CIS-1,3-DICHLOROPROPENE
Not detected
ug/kg
340
8260B/5035
10122/0201:17
KC
TRANS-I,3-DICHLOROPROPENE
Not detected
ug/kg
340
8260B/5035
10122/0201:17
KC
2-HEXANONE
Not detected
ug/kg
3400
8260B/5035
10/2210201:17
KC
IPE
Not detected
ug/kg
340
8260B15035
10122/0201:17
KC
MTBE
Not detected
ug/kg
340
8260B15035
10/22/02 01:17
KC
SURR:DIBROMOFLUOROMETHANE
93
%
72-137
8260B/5035
10/22/02 01:17
KC
SURR:TOLUENE-D8
95
%
73-128
8260B/5035
10/22/02 01:17
KC
SURR:BROMOFLUOROBENZENE
124
%
69-131
826OB15035
10/22/02 01:17
KC
CALCULATIONS BASED ON DRY WT.
73
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 8 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-4
Prism Sample ID:
AC61492
Loqin Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
15000
mg/kg
500
8015MOD/3550
10/24/02 12:24
EHT
TPH-GASOLINE RANGE / PREP. 5030
160
mg/kg
20
8015MOD/5030
10/21/02 22:09
JMV
CALCULATIONS BASED ON DRY WT.
87
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr, Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, INC 28226
PRISM
'x LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 9 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-5
Prism Sample ID:
AC61493
Loqin Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
1700
mg/kg
500
8015MOD13550
10/24/02 13:10
EHT
TPH-GASOLINE RANGE / PREP. 5030
110
mg/kg
5.0
8015MOD15030
10/21/02 22:46
JMV
CALCULATIONS BASED ON DRY WT.
89
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
INC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, INC 28226
.i' PRISM
LABORATORIES, INC
Full Service Analytical 8 Environmental Solutions
Page 10 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-6
Prism Sample ID:
AC61494
Loqin Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
Less than
mg/kg
10
8015MOD/3550
10/23/02 16:12
EHT
TPH-GASOLINE RANGE / PREP. 5030
Less than
mg/kg
1.0
8015MOD15030
10/21/02 23:24
JMV
CALCULATIONS BASED ON DRY WT.
72
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
INC Certification No. 402 - SC Certification No. 99012 - INC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
LABORATORIES, INC
Full service Analytical 8 Environmental Solutions
Page 11 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-7
Prism Sample ID:
AC61495
Login Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
Less than
mg/kg
10
8015MOD13550
10/23/02 21:38
EHT
TPH-GASOLINE RANGE / PREP. 5030
Less than
mg/kg
1.0
8015MOD/5030
10/22/02 01:17
JMV
CALCULATIONS BASED ON DRY WT.
86
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
INC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 12 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-8
Prism Sample ID:
AC61496
Loqin Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
Less than
mg/kg
10
8015MOD/3550
10/23/02 22:23
EHT
TPH-GASOLINE RANGE / PREP. 5030
Less than
mg/kg
1.0
8015MOD/5030
10/22/02 18:27
JMV
CALCULATIONS BASED ON DRY WT.
87
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
LABORATORIES, INC
Full Service Analytical & Environmental Solutions
Page 13 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-9
Prism Sample ID:
AC61497
Login Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
Less than
mg/kg
10
8015MOD13550
10/23/02 16:58
EHT
TPH-GASOLINE RANGE / PREP. 5030
Less than
mg/kg
1.0
8015MOD15030
10/22/02 02:32
JMV
CALCULATIONS BASED ON DRY WT.
75
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cart. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
LABORATORIES, INC
Full Service Analytical & Environmental Solutions
Page 14 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-10
Prism Sample ID:
AC61498
Loqin Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
Less than
mg/kg
10
8015MOD/3550
10/23/02 18:31
EHT
TPH-GASOLINE RANGE / PREP. 5030
Less than
mg/kg
1.0
8015MOD/5030
10/22/02 03:10
JMV
CALCULATIONS BASED ON DRY WT.
81
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
ftisM
-' LABORATORIES, INC
Full Service Analytical & Environmental Solutions
Page 15 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-11
Prism Sample ID:
AC61499
Loqin Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
8100
mg/kg
1000
8015MOD/3550
10/24/02 11:39
EHT
TPH-GASOLINE RANGE / PREP. 5030
100
mg/kg
10
8015MOD/5030
10/22/02 03:47
JMV
CALCULATIONS BASED ON DRY WT.
75 -
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road A P.O. Box 240543 A Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
N9' y LABORATORIES, INC
3
Full Service Analytical & Environmental Solutions
Page 16 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-12
Prism Sample ID:
AC61500
Loqin Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATEITIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
TPH - DIESEL RANGE
2100
nrl
500
8015MOD/3550
10/24/02 13:55
EHT
TPH-GASOLINE RANGE / PREP. 5030
120
mg/kg
10
8015MOD/5030
10/22/02
12:39
JMv
BENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02
01:56
KC
BROMOBENZENE
Not detected
ug/kg
340
826OB15035
10/22/02
01:56
KC
BROMOCHLOROMETHANE
Not detected
ug/kg
340
8260B/5035
10122/0201:56
KC
BROMODICHLOROMETHANE
Not detected
ug/kg
340
82608/5035
10/22/02
01:56
KC
BROMOFORM
Not detected
ug/kg
340
82608/5035
10/22/02
01:56
KC
BROMOMETHANE
Not detected
ug/kg
680
82608/5035
10/22/02
01:56
KC
N-BUTYLBENZENE
4200
ug/kg
340
8260B/5035
10/22/02
01:56
KC
SEC-BUTYLBENZENE
2700
ug/kg
340
826OB15035
10/22/02
01:56
KC
TERT-BUTYLBENZENE
430
ug/kg
340
82608/5035
10/22/02
01:56
KC
CARBON TETRACHLORIDE
Not detected
ug/kg
340
8260B/5035
10/2210201:56
KC
CHLOROBENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02
01:56
KC
CHLORODIBROMOMETHANE
Not detected
ug/kg
340
82608/5035
10/22/02
01:56
KC
CHLOROETHANE
Not detected
ug/kg
680
82608/5035
10/22/02
01:56
KC,
CHLOROFORM
Not detected
ug/kg
340
82608/5035
10/22/02
01:56
KC
CHLOROMETHANE
Not detected
ug/kg
680
8260B/5035
1012210201:56
KC
2-CHLOROTOLUENE
Not detected
ug/kg
340
8260B15035
10122/0201:56
KC
4=CHLOROTOLUENE
Not detected
ug/kg
340
826OB/5035
10/22/02
01:56
KC
1,2-DIBROMO-3-CHLOROPROPANE
Not detected
ug/kg
680
82606/5035
10/22/02
01:56
KC
1,2-DIBROMOETHANE
Not detected
ug/kg
340
82608/5035
10/22/02
01:56
KC
DIBROMOMETHANE
Not detected
ug/kg
340
8260B15035
10/22/02
01:56
KC
1,2-DICHLOROBENZENE
Not detected
ug/kg
340
826OB/5035
10/22/02
01:56
KC
1,3-DICHLOROBENZENE
Not detected
ug/kg
340
8260B15035
10/22/02
01:56
KC
1,4-DICHLOROBENZENE
Not detected
ug/kg
340
826013/5035
10/22/02
01:56
KC
DICHLORODIFLUOROMETHANE
Not detected
ug/kg
340
8260B/5035
10/22/02
01:56
KC
1,1-DICHLOROETHANE
Not detected
ug/kg
340
8260B/5035
10/22/02
01:56
KC
1,2-DICHLOROETHANE
Not detected
ug/kg
340
8260B15035
10122/0201:56
KC
1,1-DICHLOROETHENE
Not detected
ug/kg
340
82608/5035
10/22/02
01:56
KC
CIS-1,2-DICHLOROETHENE
Not detected
ug/kg
340
82608/5035
10/22/02
01:56
KC
TRANS-I,2-DICHLOROETHENE
Not detected
ug/kg
340
8260B15035
10/22/02
01:56
KC
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking Water Cert.
No. 37735 - FL Certification
No.
E87519
449 Springbrook
Road ♦ P.O. Box 240543 A Charlotte, NC
28224-0543
Phone: 704 / 529-6364
♦ Toll Free Number:
1-800
/ 529-6364 ♦
Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
ftism
LABORATORIES, INC.
'/Mgftlal
Full Service Analytical & Environmental Solutions
Page 18 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-12
Prism Sample ID:
AC61500
Loqin Group:
A0024Kl5
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
CARBON DISULFIDE
Not detected
ug/kg
6800
826013/5035
10/22/02 01:56
KC
VINYL ACETATE
Not detected
ug/kg
3400
8260B/5035
10/22/02 01:56
KC
CIS-1,3-DICHLOROPROPENE
Not detected
ug/kg
340
826OB15035
10/22/02 01:56
KC
TRANS-I,3-DICHLOROPROPENE
Not detected
ug/kg
340
826013/5035
10/22/02 01:56
KC
2-HEXANONE
Not detected
ug/kg
3400
826013/5035
10122/0201:56
KC
IPE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
MTBE
Not detected
ug/kg
340
82608/5035
10/22/02 01:56
KC
SURR:DIBROMOFLUOROMETHANE
101
%
72-137
8260B/5035
10122/0201:56
KC
SURR:TOLUENE-D8
104
%
73-128
82608/5035
10/22/02 01:56
KC
SURR:BROMOFLUOROBENZENE
167'
%
69-131
8260B/5035
10/22/02 01:56
KC
CALCULATIONS BASED ON DRY WT.
74
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments:
Analysis note for 8260:* - The surrogate recovery was outside of the control limits. The analysis was repeated
at a 1:500 dilution, but the surrogates were diluted out. Matrix interference is suspected.
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 17 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-12
Prism Sample ID:
AC61500
Loqin Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
1,2-DICHLOROPROPANE
Not detected
ug/kg
340.
82606/5035
10/22/02 01:56
KC
1,3-DICHLOROPROPANE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
2,2-DICHLOROPROPANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:56
KC
1,1-DICHLOROPROPENE
Not detected
ug/kg
340
8260B15035
10/22/02 01:56
KC
ETHYLBENZENE
990
ug/kg
340
8260B15035
10/22/02 01:56
KC
HEXACHLOROBUTADIENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
ISOPROPYLBENZENE
1400
ug/kg
340
8260B15035
10/22/02 01:56
KC
P-ISOPROPYLTOLUENE
2700
ug/kg
340
826OB/5035
10/22/02 01:56
KC
METHYLENE CHLORIDE
Not detected
ug/kg
6800
82BOB15035
10/22/02 01:56
KC
NAPHTHALENE
11000
ug/kg
340
8260B/5035
10/22/02 01:56
KC
N-PROPYLBENZENE
3900
ug/kg
340
8260B15035
10122/0201:56
KC
STYRENE
Not detected
ug/kg
340
8260B15035
10/22/02 01:56
KC
1,1,1,2-TETRACHLOROETHANE
Not detected
ug/kg
340
826OB/5035
10/22/02 01:56
KC
1,1,2,2-TETRACHLOROETHANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:56
KC
TETRACHLOROETHENE
Not detected
ug/kg
340
826OB15035
10/22/02 01:56
KC
TOLUENE
Not detected
ug/kg
340
826OB15035
10/22/02 01:56
KC
1,2,3-TRICHLOROBENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
1,2,4-TRICHLOROBENZENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
1,1,1-TRICHLOROETHANE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
1,1,2-TRICHLOROETHANE
Not detected
ug/kg
340
82608/5035
1012210201:56
KC
TRICHLOROETHENE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
TRICHLOROFLUOROMETHANE
Not detected
ug/kg
340
8260B/5035
10/22/02 01:56
KC
1,2,3-TRICHLOROPROPANE
Not detected
ug/kg
340
8260B15035
10/22/02 01:56
KC
1,2,4-TRIMETHYLBENZENE
19000
ug/kg
340
8260B/5035
10/22/02 01:56
KC
1,3,5-TRIMETHYLBENZENE
4500
ug/kg
340
8260B15035
10/22/02 01:56
KC
VINYL CHLORIDE
Not detected
ug/kg
680
8260B15035
10/22/02 01:56
KC
TOTAL XYLENES
850
ug/kg
340
826013/5035
10/22/02 01:56
KC
2-BUTANONE (MEK)
Not detected
ug/kg
3400
8260B/5035
10/22/02 01:56
KC
2-CHLOROETHYL VINYL ETHER
Not detected
ug/kg
680
82606/5035
10/22/02 01:56
KC
4-METHYL-2-PENTANONE (MIRK)
Not detected
ug/kg
3400
826013/5035
10/22/02 01:56
KC
ACETONE
Not detected
ug/kg
6800
8260B15035
10/22/02 01:56
KC
NC Certification No. 402 - SC Certification
No. 99012 -
NC Drinking Water Cert.
No. 37735 - FL
Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number:
1-800 / 529-6364 A
Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
,LL LABORATORIES, INC
Full Service Analytical & Environmental Solutions
Page 19 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-13
Prism Sample ID:
AC61501
Login Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER RESULT UNITS LIMIT REFERENCE STARTED ANALYST
TPH - DIESEL RANGE
12000
mg/kg
5000
8015MOD/3550
10/24/02
15:29
EHT
TPH-GASOLINE RANGE / PREP. 5030
480
mg/kg
40
8015MOD15030
10/22/02
05:03
JMv
BENZENE
Not detected
ug/kg
2900
8260B/5035
10/22/02
02:35
KC
BROMOBENZENE
Not detected
ug/kg
2900
82608/5035
10/22/02
02:35
KC
BROMOCHLOROMETHANE
Not detected
ug/kg
2900
8260B15035
10/22/02
02:35
KC
BROMODICHLOROMETHANE
Not detected
ug/kg
2900
8260B/5035
10/22/02
02:35
KC
BROMOFORM
Not detected
ug/kg
2900
8260B/5035
10/22/02
02:35
KC
BROMOMETHANE
Not detected
ug/kg
5800
826013/5035
10/22/02
02:35
KC
N-BUTYLBENZENE
10000
ug/kg
2900
826013/5035
10/22/02
02:35
KC
SEC-BUTYLBENZENE
4200
ug/kg
2900
82608/5035
10/22/02
02:35
KC
TERT-BUTYLBENZENE
Not detected
ug/kg
2900
8260B/5035
10/22/02
02:35
KC
CARBON TETRACHLORIDE
Not detected
ug/kg
2900
82606/5035
10/22/02
02:35
KC
CHLOROBENZENE
Not detected
ug/kg
2900
82608/5035
10/22/02
02:35
KC
CHLORODIBROMOMETHANE
Not detected
ug/kg
2900
82606/5035
10/2210202:35
KC
CHLOROETHANE
Not detected
ug/kg
5800
826013/5035
10/22/02
02:35
KC
CHLOROFORM
Not detected
ug/kg
2900
8260B/5035
10122/0202:35
KC
CHLOROMETHANE
Not detected
ug/kg
5800
82608/5035
10/22/02
02:35
KC
2-CHLOROTOLUENE
Not detected
ug/kg
2900
8260B/5035
10/2210202:35
KC
4-CHLOROTOLUENE
Not detected
ug/kg
2900
8260B/5035
1012210202:35
KC
1,2-DIBROMO-3-CHLOROPROPANE
Not detected
ug/kg
5800
82608/5035
10122/0202:35
KC
1,2-DIBROMOETHANE
Not detected
ug/kg
2900
8260B/5035
10/2210202:35
KC
DIBROMOMETHANE
Not detected
ug/kg
2900
826OB15035
10/22/02
02:35
KC
1,2-DICHLOROBENZENE
Not detected
ug/kg
2900
8260B/5035
10/22/02
02:35
KC
1,3-DICHLOROBENZENE
Not detected
ug/kg
2900
82606/5035
10/22/02
02:35
KC
1,4-DICHLOROBENZENE
Not detected
ug/kg
2900
826013/5035
10/22/02
02:35
KC
DICHLORODIFLUOROMETHANE
Not detected
ug/kg
2900
826013/5035
10/22/02
02:35
KC
1,1-DICHLOROETHANE
Not detected
ug/kg
2900
82608/5035
10/22/02
02:35
KC
1,2-DICHLOROETHANE
Not detected
ug/kg
2900
82608/5035
10/22/02
02:35
KC
1,1-DICHLOROETHENE
Not detected
ug/kg
2900
8260B15035
10/22/02
02:35
KC
CIS-1,2-DICHLOROETHENE
Not detected
ug/kg
2900
8260B/5035
10/22/02
02:35
KC
TRANS-I,2-DICHLOROETHENE
Not detected
ug/kg
2900
8260B/5035
10/22/02
02:35
KC
NC Certification No. 402 - SC Certification
No. 99012
- NC Drinking
Water Cert.
No. 37735 - FL Certification
No.
E87519
449 Springbrook
Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number:
1-800
/ 529-6364 A
Fax: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
°. PRISM
LABORATORIES, INC
Full Service Analytical & Environmental Solutions
Page 20 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-13
Prism Sample ID:
AC61501
Login Group:
A0024K15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
TEST TEST REPORTING METHOD DATE/TIME
PARAMETER - RESULT UNITS LIMIT REFERENCE STARTED ANALYST
1,2-DICHLOROPROPANE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
1,3-DICHLOROPROPANE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
2,2-DICHLOROPROPANE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
1,1-DICHLOROPROPENE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
ETHYLBENZENE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
HEXACHLOROBUTADIENE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
ISOPROPYLBENZENE
3200
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
P-ISOPROPYLTOLUENE
5700
ug/kg
2900
8260B15035
10/22/02 02:35
KC
METHYLENE CHLORIDE
Not detected
ug/kg
58000
8260B15035
10/22/02 02:35
KC
NAPHTHALENE
32000
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
N-PROPYLBENZENE
7800
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
STYRENE
Not detected
ug/kg
2900
82606/5035
10/22/02 02:35
KC
1, 1,1,2-TETRACHLOROETHANE
Not detected
ug/kg
2900
8260B15035
10/22/02 02:35
KC
1,1,2,2-TETRACHLOROETHANE
Not detected
ug/kg
2900
826013/5035
10/22/02 02:35
KC
TETRACHLOROETHENE
Not detected
ug/kg
2900
8260B/5035
10/2210202:35
KC
TOLUENE
Not detected
ug/kg
2900
82608/5035
10/22/02 02:35
KC
1,2,3-TRICHLOROBENZENE
Not detected
ug/kg
2900
826oB/5035
10/22/02 02:35
KC
1,2,4-TRICHLOROBENZENE
Not detected
ug/kg
2900
826oB/5035
10/22/02 02:35
KC
1,1,1-TRICHLOROETHANE
Not detected
ug/kg
2900
8260B/5035
10122/0202:35
KC
1,1,2-TRICHLOROETHANE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
TRICHLOROETHENE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
TRICHLOROFLUOROMETHANE
Not detected
ug/kg
2900
8260B15035
10/22/02 02:35
KC
1,2,3-TRICHLOROPROPANE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
1,2,4-TRIMETHYLBENZENE
16000
ug/kg
2900
8260B15035
1012210202:35
KC
1,3,5-TRIMETHYLBENZENE
9600
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
VINYL CHLORIDE
Not detected
ug/kg
5800
826OB15035
10/22/02 02:35
KC
TOTAL XYLENES
Not detected
ug/kg
2900
826OB15035
10/22/02 02:35
KC
2-BUTANONE(MEK)
Not detected
ug/kg
29000
826013/5035
10/22/02 02:35
KC
2-CHLOROETHYL VINYL ETHER
Not detected
ug/kg
5800
8260B15035
10/22/02 02:35
KC
4-METHYL-2-PENTANONE (MIBK)
Not detected
ug/kg
29000
8260B/5035
10/22/02 02:35
KC
ACETONE
Not detected
ug/kg
58000
8260B/5035
10/22/02 02:35
KC
NC Certification No. 402 - SC Certification No. 99012
- NC Drinking Water Cart. No.
37735 - FL
Certification No.
E87519
449 Springbrook Road ♦ P.O.
Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364
♦ Toll Free Number:
1-800 / 529-6364 A Fax:
704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
::- 7 LABORATORIES, INC.
Y .-
Full Service Analytical & Envimnmental Solutions
Page 21 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-13
Prism Sample ID:
AC61501
Loqin Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATEIrIME
STARTED
ANALYST
CARBON DISULFIDE
Not detected
ug/kg
58000
8260B/5035
10/22/02 02:35
KC
VINYL ACETATE
Not detected
ug/kg
29000
8260B/5035
10/22/02 02:35
KC
CIS-1,3-DICHLOROPROPENE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
TRANS-I,3-DICHLOROPROPENE
Not detected
ug/kg
2900
8260B/5035
10/22/02 02:35
KC
2-HEXANONE
Not detected
ug/kg
29000
826013/5035
10/22/02 02:35
KC
IPE
Not detected
ug/kg
2900
826013/5035
10/22/02 02:35
KC
MTBE
Not detected
ug/kg
2900
8260B15035
10/22/02 02:35
KC
SURR:DIBROMOFLUOROMETHANE
DO'
%
72-137
8260B15035
10/22/02 02:35
KC
SURR:TOLUENE-D8
DO'
%
73-128
8260B15035
10/22/02 02:35
KC
SURR:BROMOFLUOROBENZENE
DO'
%
69-131
8260B/5035
1012210202:35
KC
CALCULATIONS BASED ON DRY WT.
85
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments:
Analysis note for 8260: ' - The surrogates were diluted out at a 1:500 dilution.
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 ♦ Far: 704 / 525-0409

Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
PRISM
" LABORATORIES, INC
Full Service Analytical & Environmental Solutions
Page 22 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-14
Prism Sample ID:
AC61502
Login Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATE/TIME
STARTED
ANALYST
TPH - DIESEL RANGE
Less than
mg/kg
10
8015MOD/3550
10/23/02 17:45
EHT
TPH-GASOLINE RANGE / PREP. 5030
Less than
mg/kg
1.0
8015MOD/5030
10/22/02 05:40
JMV
CALCULATIONS BASED ON DRY WT.
91
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments:
Angela D. Overcash, V.P. Laboratory Services
C
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 ♦ Charlotte, NC 28224-0543
Phone: 704 / 529-6364 A Toll Free Number: 1-800 / 529-6364 A Fax: 704 / 525-0409

S
Lab Report
10/25/02
ERM Southeast, Inc.
Attn: Mr. Rick Tarravechia
7300 Carmel Exec. Park Ste. 200
Charlotte, NC 28226
AL PR.ISM
LABORATORIES, INC.
Full Service Analytical & Environmental Solutions
Page 23 of 23
Customer Project ID:
VMG
Customer Sample ID:
VMG-15
Prism Sample ID:
AC61503
Loqin Group:
A00241<15
Sample Collection Date/Time:
10/19/02
Lab Submittal Date/Time:
10/21/02 07:50
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory
TEST
PARAMETER
TEST
RESULT
UNITS
REPORTING
LIMIT
METHOD
REFERENCE
DATEITIME
STARTED
ANALYST
TPH - DIESEL RANGE
5200
mg/kg
1000
8015MOD/3550
10/24/02 10:53
EHT
TPH-GASOLINE RANGE / PREP. 5030
290
mg/kg
40
8015MOD/5030
10/22/02 13:16
JMV
CALCULATIONS BASED ON DRY WT.
93
% DRY WT.
0.01
SM 2540 G
10/23/02 11:00
CWC
PREP. METHOD 3550
Completed
SW846-3550
10/23/02 07:00
JDP
Sample Comments
Angela D. Overcash, V.P. Laboratory Services
NC Certification No. 402 - SC Certification No. 99012 - NC Drinking Water Cert. No. 37735 - FL Certification No. E87519
449 Springbrook Road ♦ P.O. Box 240543 A Charlotte, NC 28224-0543
Phone: 704 / 529-6364 ♦ Toll Free Number: 1-800 / 529-6364 ♦ Fax: 704 / 525-0409

. . APRISM
LAfORAT0111lf, INC.
- Full Bel a EnNronmental Solutions
N9 SpHnpbrook Raid • P.O. Box 2/0519 • Charlotte, NC 26224-05e3
Client Company_ Name: N • `
Report TO/Con tact Name:,2.4r-��' �k.( in Ue�- 6--
CHAIN OF CUSTODY RECORD
PAGE I OF Z QUOTE a TO ENSURE PROPER BILLING:
Project Name: 11"", (�
Short Hold Analysis: (Yes) (No) UST Project: (Yes) (No)
"Please ATTACH any project specific reporting
Provisions and/or OC Requirements
Invoice To: ku It '17Zr r.AVQ: 4 Lat
Samples INTACT upon snivel?
Received ON WET ICE? Temp
PROPER PRESERVATIVES Indicated?
Recalved WITHIN HOLDING TIMES?
CUSTODY SEALS INTACT?
VOLATILES reed W/OUT HEADSPACE?
PROPER CONTAINERS used?
YES NO N/A
HePO any nw:cola. -
B(- Purchase Order No./Billing Reference
-
TO 'BE FILLED IN. BY CLIENT/SAMPLING PERSONNEL
Phone: 7riA �4-r ..Sr 3�lF (Yes) (No): �q C4f 5-6 Requested Due Date O t Day ❑ 2 Days 3 Days ❑ n Days o 5 Days
Certification: NELAC_ USACE_ FL_ NC
Site Location Name: AA, Ci-. O 6-9 Days ❑ Standard ID days
SC _ OTHER N/A
Site Location Physical Address: Samples received after 15:00 w` Flbe processed next business day.
Water Clorinated: 'YES NO
Turnaround time Is based on business days, excluding weekends and holidays.
_ _
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
Sample Iced Upon Collection: YESZNO _
'
TIME
MATRIX
SAMPLE CONTAINER
�
ANALYSES REQUESTED
SUB
dRISM
OLIENT-.''
." DATE.
'COLLECTED
_
,COLLECTED
(SOIL,
PRESERVA-
O 0 1 D REMARKS
Al
�B
CENT.
�B
SAMPLE DESCRIPTION
MILITARY
WATER OR
-'TYPE
NO.
SIZE
TIVES
/�
"1
ti �M ��.
ID NO.
ID NO.
HOURS-
.SLUDGE)
SEE BELOW
A9
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Sampler's Signature Sampled By.(Print Name) Affiliation
-_ -
Upon relinquishing, this Chaln f Custody is your authorization for Prism to proceed with the analyses as requested above.
Any changes must be
submitted in writing to !gtfr Pro ecf'Mana er. There wIII be charges for any changes after analyses have been initialized.
Re q h IS at Received By: (Signature) Date
Military/Hours Additional Comments: its Arrival Time:
t
�R lm;uiahed Byf (Si dtule . Rmelved By: (Signature) Date
- y,,1� � y� f Site Departure Tim:
oTA�
I'. - ..
(t�r<
3 aG•( Field Tech Fee:
ReNnriulshetl By .(Signature) - Rmey Fo am lAbe as By: Date
Mileage:
Method of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED SHUT W CUSTODY R SEALS FOR NSPORTATION TO THE LABORATORY. Lop n G
up N0. '
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC NTIL RECEIVED ATTH BORATORY.
R ��d 4 t<
❑ Fed Ex O UPS . Ijl Hand4allwrod O Priam Field Service O Other
l5
NPOES:
I US'f:
GROUNDWATER:
ND
DRINKING WATER:
SOLID WASTE:
RCRA: I CERCLA:
LANDFILL:
OTHER:
O NC' O SO
O NC O SC
I O NC !] SC
I O NC ❑ SC
❑ NC ❑ SC
O NC O SO O NC O SC
O NC O SC
❑ NC. ❑ SC
-rnmiaiiul TYPP CnnFC. A - Amhar r. - Ciaa, n - rtace P - Potin- TI=Taflnn-I inorl Can Vr)A = VOIB}IIp nrnAniCe
AnRIVAIF I%Rr0 aad RnAnAl
FINAL REPORT COPY

PR•I5M
I LAaOaATOgl61NC.
Full Service Analytical6 ElMmnmental Solutions
440 Sprtngbreok Road • P.O. Box 240543 • Chedotte, NC 28224-050
Client Company Name:
Report To/Contact Name: pp
IC. IG11.W o./. irw
CHAIN OF CUSTODY RECORD.;
PAGE _(,_ OF 2 QUOTE 4 TO ENSURE PROPER BILLING: ,_ Samples INTACT Upon arrival?
Project Name:y /A Cr
Received ON WET ICE? Temp
Short Hold Analysis: (Yes) (No) UST Project: es (NO) PROPER PRESERVATIVES Indicated?
'Please ATTACH any project specific reporting Received WITHIN HOLDING TIMES7
provisions and/or OC Re�gyjtemen% CUSTODY SEALS INTACT?
Invoice To: (�Zyj (n. VOLATILES reed W/OUT HEADSPACE?
A __. PROPER CONTAINERS used?
Purchase Order NoJBilling Reference
-
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL/
Phone:` Fax (Yes) (No):
Requested Due Date O 1 Day O 2 DaysI Days 04 Days ❑ 5 Days
Certification: NELAC_ USACE_ FL_ NC
�/
Site Location Name, `
❑ 6r9 Days ❑ Standard 10 days
SC _ OTHER N/A
Site location Ph Srical Addreasi4-
y
Samples received after 15:00 will be processed next business day.
Water Clorinated: YES NO
-
Turnaround time is based on business days, excluding weekends and holitleys.
_ _
(SEE REVERSE SIDE FOR RUSH TURNAROUND FEES)
Sample Iced Upon Collection: YES —NO
'
TIME
MATRIX
SAMPLE CONTAINER
ANALYSES REOUESTED
sU8
PRISM
' :CLIENT'- - -
DATE .�
COLLECTED
(SOIL,
PRESERVA•
❑ p
LAB
LAB
*TYPE
NO.
SIZE
SAMPLE. DESCRIPTION'
COLILItCTED ''
MILITARY-
'HOURS
WATER OR
TIVES
7 b REMARKS
N
CERT.
ID NO.
•
. SLUDGE)
SEE BELOW
a�
ID NO.
C
' I
b149
{Z`
o
btu
bf5ol
p
15o 2
6 (w.Z,
,Sampler's Signature
Sampled By (Print Name) Affiliation
Upon relinquishing, this Chain of Custody Is your authorization for Prism to proceed with the analyses as requested above. Any changes must be
sub Itted'.in wilt h t e P 'm Project Mana er.There will be char es for an chan es after anal ses have been Initialized.
Rmived By: (Signature) Date Milltarynioum Additional Com7
ments: !Site Arrival Time:
Re quithed By. (Sig ur
Received By: (Signature) Data �[ 7a ID TyjT ! Site Departure Time:
Relinquished By: (Signature)
Field Tech Fee:
Reim or P stn "bomt es B. Det
Mileage:
Method of Shipman NOTE: ALL SAMPLE COOLERS SHOULD
6ETAPEO SHUT WITH DY S FOR TRANSPORTATION TO THE LABORATORY. a In G p He. -
- SAMPLES ARE NOT ACCEPTED AND VERIFIED
AGAINST CDC TIL RECEI ED ATTHE LABORATORY.
O Fed Ea .O UPS O Hand-delvare l O Prism Reid Ser*A
OOlher A O
S TER:
DRICKIN ATER: .L A: LANDFILL: OTHER:
•�
❑ NC ❑ SO OC ❑ SC . O NC 0 SC
SC NC ❑ SCSOLIDWASTE O NC O SO O NC ❑ SC ❑ NC ❑ SC ❑ NC ❑ SC r
1
0. I ❑ ❑
O ❑ O I ❑ O ❑ PINAI 01=101`10Tl-e)DV
'CONTAINER TYPE CODES: A = Amber C = Clear G = Glass P = Plastic: TL = Teflnn-Lined Can VOA = Volatile Omanirc Analvsis (7Rrn Hand RnanP)