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Home My WebLink AboutMO-8920_40424_CA_LAB_20141121_Revised Lab Reporte-Hardeopp 2.0 Technical Report for GRI (Geological Resources Inc.) The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Accutest Job Number: FA19708 Sampling Date: 11/04/14 Report to: GRI jmt@geologicalresourcesinc.com nml@geologicalresourcesinc.com; carriekennedyggE ologicalresourcesinc.com; yr@geo ATTN: Johanna Teschner Total number of pages in report: 90 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Norm Farmer Technical Director Client Service contact: Mona Mohammed 407-425-6700 Certifications: FL (E83510), LA (03051). KS (13-10327), IA (366). tL (200063), NC (573). NJ (FL002), SC (96038001) DoD FLAP (L-A-E L2229), CA (2937), TX (T104704404). PA (68-03573). VA (460177). AK, All, GA, KY, MA, NV, OK, UT, WA This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories. Test results relate only to samples analyzed. In ffim O ACOU-rEST LAUURATURIEb- November 21, 2014 Ms. Johanna Teschner Geological Resources Inc 2301 F. Crown Point EX Dr Charlotte, NC 28207 RE: Accutest job FA19708 Reissue Dear Mr. Teschner, The final report forjob number FA19708 has been edited to reflect requested corrections. These edits have been incorporated into the revised report. 1-methylnaphthalene has been reported. Accutest apologies for any inconvenience this may have caused. Please feel free to contact us if we can be of further assistance. Sincerely, Accutest Laboratories, SE Florida ♦ 4405 Vineland Road ♦ Suite C-15 • Orlando, FL 32811 ♦ tel: 407 425-6700 ♦ fax: 407 425-0707 ♦ htpp:/,-%acc-,tcmm Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • lei: 407-425-6700 - fax: 407-425-0707 • hOp://www.accutest-com Mr 1 of 90 M® 2 of 90 Accutest 1 i�+raorica is the sole nothooty formthoming cdils or modificaGmrs to thss ACCLJTEST. ACCLJTBt3T° do vnn u. Unnulhorizcd rmalifcmion al ibi rr,+ort is strictly pmh;bited. W970e Fal9roa Sections: Table of Contents 0 -1- © Accutest Laboratories Section1: Sample Summary.................................................................................................. 4 Section2: Summary of Hits.................................................................................................... 5 ® Section 3: Sample Results........................................................................................................ 10 Sample Summary 3.1: FA197O8-1: SP-1.......................................................................................................... 3.2: FA197O8-2: UST-1-7..................................................................................................... 11 13 GRI (Geological Resources Inc.) Job No: FA19708 3.3: FA197O8-3: CS-1-10..................................................................................................... 3.4: FA197O8-4: CS-2-10..................................................................................................... 15 21 © The Rack Worship Center; 1113 Fordham Rd, Charlotte, NC 3.5: FA197O8-5: CS-3-10..................................................................................................... 3.0: FA197O8-6: CS-4-10..................................................................................................... 27 33 Sample Number Collected Date Time By Matrix Received Code Type Client Sample ID 1.7: FA197O8-7: CS-5-10'.................................................................................................... Section4: disc. Forms............................................................................................................ 39 45 FA19708-1 11/04/14 09:42 CNB 11/05/14 SO Soil SP-1 4.1: Chain of Custody........................................................................................................... 46 Section 5: CCIMS Volatiles - QC Data Summaries.............................................................. 50 FAT970$-2 11/09/19 10:02 CNB I1/05/19 SO Soil UST-I-T S.1.: Method Blank Summary................................................................................................ 51 5.2: Blank Spike Summary ................................................................................................... 55 FA19708-3 "' I1/04/14 11:23 CNB 11/05/14 SO Soil CS-1-10' 5.3: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 59 Section 6: CC/M8 Sent i-volafiles - QC Data Summaries..................................................... 63 FA19708.4 11/04/14 11:36 CNB 11/05/14 SO Soil CS-2-10' € 6.1: Method Blank Summary ................................................................................................ 64 6.2: Blank Spike Summary ................................................................................................... 70 FA1970$-5 11/09/19 11:93 CNB 1]/05/14 SO Sail CS 3-10' , 6.3: Matrix Spike/Matrix Spike Duplicate Summary72 Section 7: CC Volatiles - QC Data Summaries..................................................................... 74 7.1: Method Blank Summary 75 FA19708-6 11/04/14 11:50 CNB 11/05/14 SO Soil CS4.10' 7.2: Blank Spike Summary ................................................................................................... 78 7.3: Blank Spike/Blank Spike Duplicate Summary .............................................................. 79 FA19708.7 11/04/14 11:59 CNB 11/05/14 SO Soil CS-5-10' '< 7.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 81 7.5: Duplicate Summary ....................................................................................................... 82 Section 8: CC :Semi-volatiles - QC Data Summaries............................................................ 84 8.1. Method Blank Summary ................................................................................................ 85 8.2: Blank Spike Summary ................................................................................................... 87 8.3: Blank Spike/Blank Spike Duplicate Summary .............................................................. 88 8.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 89 8.5: Duplicate Summary ....................................................................................................... 90 Soil samples reported on a dry weight basis unless otherwise indicated on result page. 1� ME 3 of 90 ME 4 of 90 M ACC UTEST. a ACCUTEST. FA19708 '""'"" -'" FAI9109 Summary of Hits Job Number: FA19708 Account: GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Collected: 11/04/14 Page 1 of 5 © Summary of Hits Page 2 of 5 Job Number: FA19708 Account: GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Collected: 11/04/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA19708-1 SP-1 TPH-GRO(C6-CIO) 3680 430 210 mg/kg SW846 8015C TPH (CIO-C28) 21700 B 2200 1300 mg/kg SW846 8015C FA19708-2 UST-1-7' TPH-GRO (C6-CIO) 4780 880 440 mg/kg SW846 8015C TPH (CIO-C28) 33700 B 2000 1200 mg/kg SW846 8015C FA19708-3 CS-1-10' Benzene n-Buylbenzene Cyclohexane Ethylbenzene Isopropylbenzene Methylcyclohexane Methylene chloride Naphthalene n-Propylbenzene 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Toluene Xylene (total) Acenaphthene a Acenaphthylene a Anthracene a Dibenzofuran a Fluorene a 1-Methybiaphthalene a 2-Methylnaphthalene a Naphthalene a Phenanthrene a Pyrene a Benzene Ethylbenzene Naphthalene Toluene m,p-Xylene o-Xylene C5- C8 Aliphatics (Unadj.) C9- CIO Aromatics (Unadj.) C5- C8 ABphatics C9- CIO Aromatics Lab Sample ID Client Sample 1D Result/ Analyte Qual RL MDL Units Method Acenaphthene 15300 12000 6000 ug/kg MADEP EPH REV 1.1 Acenaphthylene 85401 12000 6000 ug/kg MADEP EPH REV 1.1 Fluorene 8750 J 12000 6000 ug/kg MADEP EPH REV 1.1 2-Methylnaphthalene 62500 12000 6000 ug/kg MADEP EPH REV 1.1 Naphthalene 10400 J 12000 6000 ug/kg MADEP EPH REV 1.1 Phenanthrene 11400 J 12000 6000 ug/kg MADEP EPH REV 1.1 Cll-C22 Aromatics (Unadj.) 3420000 600000 450000 ug/kg MADEP EPH REV 1.1 Cll-C22 Aromatics 3300000 600000 450000 ug/kg MADEP EPH REV 1.1 C9-C18 ABphatics 6270000 600000 300000 ug/kg MADEP EPH REV 1.1 C19-C36 Aliphatics 1240000 1 600000 300000 ug/kg MADEP EPH REV 1.1 FA19708-4 CS-2-10' 350 69 ug/kg SW846 8260B 3500 690 ug/kg SW846 8260B Benzene 350 73 ug/kg SW846 8260B n-Buylbenzene 3500 690 ug/kg SW846 8260B Cyclohexane 350 69 ug/kg SW846 8260B Ethylbenzene 350 69 ug/kg SW846 8260B Isopropylbenzene 690 280 ug/kg SW846 8260B Methylcyclohexane 3500 1400 ug/kg SW846 8260B Naphthalene 3500 690 ug/kg SW846 8260B n-Propylbenzene 3500 690 ug/kg SW846 8260B 1,2,4-Trimethylbenzene 3500 690 ug/kg SW846 8260B 1,3,5-Trimethylbenzene 3500 690 ug/kg SW846 8260B Toluene 10000 1800 ug/kg SW846 8260B Xylene (total) 8000 1000 ug/kg SW846 8270D Fluorene a 8000 800 ug/kg SW846 8270D I-Methylnaphthalene a 8000 800 ug/kg SW846 8270D 2-Methylnaphthalene a 8000 800 ug/kg SW846 8270D Naphthalene a 8000 800 ug/kg SW846 8270D Phenanthrene a 8000 800 ug/kg SW846 8270D Pyrene a 8000 800 ug/kg SW846 8270D Benzene 8000 800 ug/kg SW846 8270D Ethylbenzene 8000 800 ug/kg SW846 8270D Naphthalene 8000 800 ug/kg SW846 8270D Toluene 710 710 ug/kg MADEP VPH REV 1.1 m,p-Xylene 1400 710 ug/kg MADEP VPH REV 1.1 o-Xylene 3500 2100 ug/kg MADEP VPH REV 1.1 C5- C8 Aliphatics (Unadj.) 1400 710 ug/kg MADEP VPH REV 1.1 C9- CIO Aromatics (Unadj.) 2800 1400 ug/kg MADEP VPH REV 1.1 C5- C8 ABphatics 1400 710 ug/kg MADEP VPH REV 1.1 C9- CIO Aromatics 71000 25000 ug/kg MADEP VPH REV 1.1 2-Methyhiaphthalene 1400000 490000 ug/kg MADEP VPH REV 1.1 Cll-C22 Aromatics (Unadj.) 71000 25000 ug/kg MADEP VPH REV 1.1 Cll-C22 Aromatics 1400000 490000 ug/kg MADEP VPH REV 1.1 C9-C18 ABphatics me 5 of 90 8 ACC UTEST FA19708 380 77 ug/kg SW846 8260B 3800 770 ug/kg SW846 8260B 380 81 ug/kg SW846 8260B 3800 770 ug/kg SW846 8260B 380 77 ug/kg SW846 8260B 380 77 ug/kg SW846 8260B 3800 1500 ug/kg SW846 8260B 3800 770 ug/kg SW846 8260B 3800 770 ug/kg SW846 8260B 3800 770 ug/kg SW846 8260B 3800 770 ug/kg SW846 8260B 12000 2000 ug/kg SW846 8260B 8400 840 ug/kg SW846 8270D 8400 840 ug/kg SW846 8270D 8400 840 ug/kg SW846 8270D 8400 840 ug/kg SW846 8270D 8400 840 ug/kg SW846 8270D 8400 840 ug/kg SW846 8270D 780 780 ug/kg MADEP VPH REV I.1 1600 780 ug/kg MADEP VPH REV 1.1 3900 2300 ug/kg MADEP VPH REV 1.1 1600 780 ug/kg MADEP VPH REV 1.1 3100 1600 ug/kg MADEP VPH REV 1.1 1600 780 ug/kg MADEP VPH REV 1.1 78000 27000 ug/kg MADEP VPH REV 1.1 1600000 550000 ug/kg MADEP VPH REV 1.1 78000 27000 ug/kg MADEP VPH REV 1.1 1600000 550000 ug/kg MADEP VPH REV 1.1 50000 25000 ug/kg MADEP EPH REV 1.1 2500000 1900000 ug/kg MADEP EPH REV 1.1 2500000 1900000 ug/kg MADEP EPH REV 1.1 2500000 1200000 ug/kg MADEP EPH REV 1.1 so 6 of 90 w ACCtJTEBT. FA19708 Summary of Hits Page 3 of 5 Summary of Hits Page 4 of 5 Job Number: FA19708 © Account: GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Collected: I1/04/14 Job Number: FA19708 Account: GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Collected: 11/04/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method C19-06 Aliphatics FA19708-5 CS-3-10' Benzene n-Butylbenzene Cyclohexane Ethylbenzene Isopropylbenzene Methylcyclohexane Naphthalene n-Propylbenzene 1, 2, 4 -Trime thylb enzene 1, 3, 5-Trimethylbenzene Toluene Xylene (total) Acenaphthene a Anthracene a Dibenzofuran8 Fluoranthene a Fluorene a 1-Methylnaphthalene a 2-Methylnaphthalene a Naphthalene a Phenanthrene a Pyrene a Ethylbenzene Naphthalene Toluene m,p-Xylene o-Xylene C5- C8 Allphatics (Unadj.) C9- C10 Aromatics (Unadj.) C5- C8 Aliphatics C9- C10 Aromatics Acenaphthene Acenaphthylene Flumene 2-Methylnaphthalene Naphthalene C11-C22 Aromatics (Unadj.) CII-C22 Aromatics C9-C18 Aliphatics C19-06 Aliphatics 37400M 2500000 1200000 ug/kg MADEP EPH REV 1.1 280 280 280 280 280 280 2800 280 2800 280 280 850 2000 2000 2000 2000 2000 2000 2000 2000 2000 2000 1200 2900 1200 2300 1200 58000 580000 58000 580000 4500 4500 4500 4500 4500 230000 230000 230000 230000 57 57 1100 57 570 57 57 150 250 200 200 200 200 200 200 200 200 200 580 1700 580 1200 580 20000 200000 20000 200000 2300 2300 2300 2300 2300 170000 170000 110000 110000 ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8260B SW846 8270D SW846 8270D SW846 8270D SW846 8270D SW846 8270D SW846 8270D SW846 8270D SW846 8270D SW846 8270D SW846 8270D MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP VPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 MADEP EPH REV 1.1 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA19708-6 CS-4.10' Benzene n-Butylbenzene Cyclohexane Ethylbenzene Isopropylbenzene Methylcyclohexane Naphthalene n-Propylbenzene 1,2,4-Trimethylbenzene 1, 3, 5-Trimethyl b enzene Toluene Xylene (total) Acenaphthenea Anthracene a Dibenzofuran a Fluorene a 1-Methylnaphthalene a 2-Methylnaphthalene a Naphthalene a Phenanthrene a Pyrene a Benzene Ethylbenzene Naphthalene Toluene m,p-Xylene o-Xylene C5- C8 Aliphatics (Unadj.) C9- C10 Aromatics (Unadj.) C5- C8 Aliphatics C9- C10 Aromatics Acenaphthene Fluorene 2-Melhylnaphlhalene Naphthalene Phenanthrene Cll-C22 Aromatics (Unadj.) C11-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics 370 74 ug/kg SW846 8260B 370 74 ug/kg SW846 8260B 370 79 ug/kg SW846 8260B 3600 720 ug/kg SW846 8260B 370 74 ug/kg SW846 8260B 370 74 ug/kg SW846 8260B 3600 1400 ug/kg SW846 8260B 3600 720 ug/kg SW846 8260B 3600 720 ug/kg SW846 8260B 3600 720 ug/kg SW846 8260B 370 74 ug/kg SW846 8260B 11000 1900 ug/kg SW846 8260B 17000 2100 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 17000 1700 ug/kg SW846 8270D 760 760 ug/kg MADEP VPH REV 1.1 1500 760 ug/kg MADEP VPH REV 1.1 3800 2300 ug/kg MADEP VPH REV 1.1 1500 760 ug/kg MADEP VPH REV 1.1 3000 1500 ug/kg MADEP VPH REV 1.1 1500 760 ug/kg MADEP VPH REV 1.1 76000 26000 ug/kg MADEP VPH REV 1.1 1500000 530000 ug/kg MADEP VPH REV 1.1 76000 26000 ug/kg MADEP VPH REV 1.1 1500000 530000 ug/kg MADEP VPH REV 1.1 63000 31000 ug/kg MADEP EPH REV 1.1 63000 31000 ug/kg MADEP EPH REV 1.1 63000 31000 ug/kg MADEP EPH REV 1.1 63000 31000 ug/kg MADEP EPH REV 1.1 63000 31000 ug/kg MADEP EPH REV 1.1 3100000 2400000 ug/kg MADEP EPH REV 1.1 3100000 2400000 ug/kg MADEP EPH REV 1.1 3100000 1600000 ug/kg MADEP EPH REV 1.1 3100000 1600000 ug/kg MADEP EPH REV 1.1 ED 7 of 90 NM 8 of 90 w ACGUTEST. w ACCUTE6T, FAi9708 """"""""° FA19708 Summary of Hits Jab Number: FA19708 Account: GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Collected: 11/04/14 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method FA19708-7 CS-5-10' Acetone n-Butylbenzene Ethylbenzene Isopropylbenzene Methylcyclohexane Naphthalene n-Propylbenzene 1, 2, 4-Trimethylbenzene 1, 3, 5-Trimethylbenzene Toluene Xylene (total) Acenaphthene a Acenaphthylene a Dibenzofuran a Fluorenea 1-Methylnaphthalene a 2-Methylnaphthalene a Naphthalene a Phenanthrene a Pyrene a Ethylbenzene Naphthalene m,p-Xylene o-Xylene C9- CIO Aromatics (Unadj.) C9- CIO Aromatics Acenaphthene Fluorene 2-Methylnaphthalene Naphthalene Phenanthrene CI1-C22 Aromatics (Unadj.) CII-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics (a) Dilution required due to matrix interference. Page 5 of 5 44 13 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 4.4 1.8 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 4.4 0.88 ug/kg SW846 8260B 13 2.3 ug/kg SW846 8260B 970 120 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 970 97 ug/kg SW846 8270D 1200 580 ug/kg MADEP VPH REV 1.1 2900 1700 ug/kg MADEP VPH REV 1.1 2300 1200 ug/kg MADEP VPH REV 1.1 1200 580 ug/kg MADEP VPH REV 1.1 120000 41000 ug/kg MADEP VPH REV 1.1 120000 41000 ug/kg MADEP VPH REV 1.1 1200 600 ug/kg MADEP EPH REV 1.1 1200 600 ug/kg MADEP EPH REV 1.1 1200 600 ug/kg MADEP EPH REV 1.1 1200 600 ug/kg MADEP EPH REV 1.1 1200 600 ug/kg MADEP EPH REV 1.1 60000 45000 ug/kg MADEP EPH REV 1.1 60000 45000 ug/kg MADEP EPH REV 1.1 60000 30000 ug/kg MADEP EPH REV 1.1 60000 30000 ug/kg MADEP EPH REV 1.1 /® 9 of 90 E AGCUTEST. FA19708 Sample Results Report of Analysis Section 3 C41 M® 10 of 90 a ACCLJTEST. Accutest Laboratories Report of Analysis Page 1 of 1 at Sample ID: SP-1 Sample ID: FA19708-1 Date Sampled: 11/04/14 rix: SO - Soil Date Received: 11/05/14 hod: SW846 8015C Percent Solids: 72.5 cut: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 CD130694.D 10 11/06/14 JG n/a n/a GCD5353 #2 Initial Weight Final Volumt Run #1 5.21 g 5.0 ml Run #2 CAS No. Compound TPH-GRO (C6-C10) CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene 98-08-8 aaa-Trilluorololuene Methanol Aliquot 20.0 ul Result RL MDL Units Q 3680 430 210 mg/kg Run# 1 Run# 2 Limits 139% 56-149% 101% 66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyle found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound me 11 of 90 ACCUTEST. FA19708 Accutesl Laboratories Report of Analysis Page 1 of I it Sample ID: SP-1 Sample ID: FA19708-1 Date Sampled: 11/04/14 six: SO - Soil Date Received: 11/05/14 rod: SW846 8015C SW846 3550C Percent Solids: 72.5 Oct: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 JJ005946.D 250 11/10/14 SJL 11/06/14 OP53810 GJJ239 #2 Initial Weight Final Volume Ron #1 19.7 g 1.0 ml Run #2 CAS No. Compound TPH (C10-C28) CAS No. Surrogate Recoveries 84-15-1 o-Terphenyl (a) Outside control limits due to dilution. Result RL MDL Units Q 21700 2200 1300 mg/kg B Run# 1 Run# 2 Limits 0% a 56-122% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MR 12 of 90 M ACCUTEST. Accutest Laboratories Report of Analysis Page 1 of 1 N it Sample ID: UST-1-7' 11/04/14 Sample ID: FA19708-2 Date Sampled: six: SO - Soil Date Received: 11/05/14 tod: SW846 8015C Percent Solids: 75.5 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 C13130701.1) 10 11/06/14 JG n/a n/a GCD5353 #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.64 g 5.0 ml 10.0 ul Run #2 CAS No. Compound TPH-GRO (C6-CI0) CAS No. Surrogate Recoveries 460-00-4 4-Bromofluorobenzene 98-08-8 aaa-Trifluorotoluene Result RL MDL Units Q 4780 880 440 mg/kg Run# 1 Run# 2 Limits t124%__ 56-149% 94% 66-132% ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyse found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound so 13 of 90 E ACCUTEST. Accutest Laboratories Report of Analysis Page 1 of 1 N at Sample ID: UST-1-7' 11/04/14 Sample ID: FA19708-2 Date Sampled: rix: SO - Soil Date Received: 11/05/14 hod: SW846 8015C SW846 3550C Percent Solids: 75.5 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 JJ005950.D 250 11/10/14 SJL I1/06/14 OP53810 GJJ239 #2 Initial Weight Final Volume Run #1 20.3 g 1.0 ml Run #2 CAS No. Compound Result RL MDL Units Q TPH (CIO-C28) 33700- 2000 1200 mg/kg B CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 84-15-1 o-Terphenyl 0% a , 56-122% (a) Outside control limits due to dilution. NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound on 14 of 90 ACCUTEST. FAWN �•""'••""�", Accutest Laboratories Report of Analysis Page 1 of 2 w at Sample ID: CS-1-10' Sample ID: FA19708-3 Date Sampled: 11/04/14 rix: SO - Soil Date Received: 11/05/14 hod: SW846 8260B Percent Solids: 81.8 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 Y16999.1) 1 11/05/14 AD n/a n/a VY747 #2 Y17000.1) I 11/05/14 AD n/a n/a VY747 Initial Weight Methanol Aliquot :an #1 5.25 g 100 ul ;un #2 5.25 g 10.0 ul VOA Special List CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 3500 1000 ug/kg 71-43-2 Benzene 732 350 69 ug/kg 75-27-4 Bromodichloromethane ND 350 69 ug/kg 75-25-2 Bromoform ND 350 75 ug/kg 104-51-8 n-Butylbenzene 12400 a '.3500 690 ug/kg 108-90-7 Chlorobenzene ND 350 69 ug/kg 75-00-3 Chloroethane ND 350 160 ug/kg 67-66-3 Chloroform ND 350 78 ug/kg 75-15-0 Carbon disulfide ND 350 69 ug/kg 56-23-5 Carbon tetrachloride ND 350 96 ug/kg 110-82-7 Cyclohexane 1810 350 73 ug/kg 75-34-3 1,1-Dichloroethane ND 350 69 ug/kg 75-35-4 1,1-Dichloroethylene ND 350 69 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 350 150 ug/kg 106-93-4 1,2-Dibromoethane ND 350 120 ug/kg 107-06-2 1,2-Dichloroethane ND 350 69 ug/kg 78-87-5 1,2-Dichloropropane ND 350 69 ug/kg 124-48-1 Dibromochloromethane ND 350 69 ug/kg 75-71-8 Dichlorodifluoromethane ND 350 87 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 350 69 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 350 69 ug/kg 541-73-1 m-Dichlorobenzene ND 350 69 ug/kg 95-50-1 o-Dichlorobenzene ND 350 69 ug/kg 106-46-7 p-Dichlorobenzene ND 350 78 ug/kg 156-60-5 trans- 1, 2- Dichloroethylene NO 350 93 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 350 69 ug/kg 100-41-4 Ethylbenzene 17200 a s3500 690 ug/kg 591-78-6 2-Hexanone ND 1700 340 ug/kg 98-82-8 Isopropylbenzene 10100 350 69 ug/kg 108-10-1 4-Methyl-2-pentanone ND 1700 350 ug/kg 79-20-9 Methyl acetate NO 1700 350 ug/kg 74-83-9 Methyl bromide ND 350 130 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound fM 15 of 90 w ACC[JTEST. FA19708 Accutest Laboratories Report of Analysis :lien Sample ID: CS-1-10' ab Sample ID: FA19708-3 Date Sampled: 11/04/14 4atrix: SO - Soil Date Received: 11/05/14 4thod: SW846 8260B Percent Solids: 81.8 roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC VOA Special List CAS No. Compound 74-87-3 Methyl chloride 108-87-2 Methylcyclohexane 75-09-2 Methylene chloride 78-93-3 Methyl ethyl ketone 1634-04-4 Methyl Tert Butyl Ether 91-20-3 Naphthalene 103-65-1 n-Propylbenzene 100-42-5 Styrene 71-55-6 1, 1, 1-Trichloroethane 79-34-5 1, 1, 2,2-Tetrachloroethane 79-00-5 1, 1, 2-Trichloroethane 120-82-1 1, 2A -Trichlorobenzene 95-63-6 1,2,4-Trimethylbenzene 108-67-8 1,3,5-Trimethylbenzene 127-18-4 Tetrachloroethylene 108-88-3 Toluene 79-01-6 Trichloroethylene 75-69-4 Trichlorofluoromethane 75-01-4 Vinyl chloride 1330-20-7 Xylene (total) CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 2037-26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 (a) Result is from Run# 2 Result RL MDL Units Q ND350 140 ug/kg 9890 350 69 ug/kg 296 690 280 ug/kg J ND 1700 520 ug/kg ND 350 69 ug/kg 358008 3500 1400 ug/kg 17400 a 3500 690 ug/kg ND 350 69 ug/kg ND 350 69 ug/kg ND 350 98 ug/kg ND 350 110 ug/kg ND 350 80 ug/kg 80100 3500 690 ug/kg 204009, 3500 690 ug/kg ND 350 87 ug/kg 15000a : 3500 690 ug/kg ND 350 71 ug/kg ND 350 69 ug/kg ND 350 71 ug/kg 91300a 10000 1800 ug/kg Run# I Run# 2 Limits 103%105%' 75-124% 98% < 98% ° 75-126% 114% 106% 71-133% 99% 99% 72-135% Page 2 of 2 L ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound so 16 of 90 w ACCUTEST. FAt9108 Acculest Laboratories Report of Analysis Page 1 of 2 W it Sample ID: CS-1-10' Sample ID: FA19708-3 Date Sampled: 11/04/14 -ix: SO - Soil Date Received: 11/05/14 rod: SW846 8270D SW846 3550C Percent Solids: 81.8 act: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1a U047759.1) 40 11/10/14 NI 11/05/14 OP53802 SU2190 #2 Initial Weight Final Volume '.un #1 30.4 g 1.0 ml An #2 ABN Special List CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 40000 8000 ug/kg 95-57-8 2-Chlorophenol ND 8000 800 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 8000 800 ug/kg 120-83-2 2,4-Dichlorophenol ND 8000 830 ug/kg 105-67-9 2,4-Dimethylphenol ND 8000 890 ug/kg 51-28-5 2,4-Dinitrophenol ND 40000 8000 ug/kg 534-52-1 4,6-DWtro-o-cresol ND 16000 3200 ug/kg 95-48-7 2-Methylphenol ND 8000 800 ug/kg 3&4-Methylphenol ND 8000 1600 ug/kg 58-75-5 2-Nitrophenol ND 8000 800 ug/kg 100-02-7 4-Nitrophenol ND 40000 6400 ug/kg 87-86-5 Pentachlorophenol ND 40000 6400 ug/kg 108-95-2 Phenol ND 8000 800 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 8000 800 ug/kg 83-32-9 Acenaphthene 5250 8000 1000 ug/kg J 208-96-8 Acenaphthylene 1610 8000 800 ug/kg J 120-12-7 Anthracene 946 8000 800 ug/kg I 56-55-3 Benzo(a)anthracene ND 8000 800 ug/kg 50-32-8 Benzo(a)pyrene ND 18000 800 ug/kg 205-99-2 Benzo(b)fluoranthene ND 8000 800 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 8000 800 ug/kg 207-08-9 Benzo(k)fluoranthene ND 8000 880 ug/kg 101-55-3 4-Bromophenylphenyl ether NO, 8000 800 ug/kg 85-68-7 Butyl benzyl phthalate ND 8000 1600 ug/kg 91-58-7 2-Chloronaphthalene ND 8000 960 ug/kg 106-47-8 4-Chloroaniline ND 8000 800 ug/kg 218-01-9 Chrysene ND 8000 800 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 8000 800 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 8000 800 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 8000 840 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 8000 1200 ug/kg 121-14-2 2,4-Dinitrotoluene ND 8000 910 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound s® 17 of 90 w ACCUTEST. FA19108 I..... . Accutest Laboratories Report of Analysis 'Bent Sample ID: CS-1-10' ab Sample ID: FA19708-3 Date Sampled: 11/04/14 latrix: SO - Soil Date Received: 11/05/14 lethod: SW846 8270D SW846 3550C Percent Solids: 81.8 roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ABN Special List CAS No. Compound Result RL MDL Units Q 606-20-2 2,6-Dinitrotoluene ND :8000 880 ug/kg 91-94-1 3,T-Dichlorobenzidine ND 8000 800 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 8000 800 ug/kg 132-64-9 Dibenzofuran 2200 8000 800 ug/kg J 84-74-2 Di-n-butyl phthalate ND 16000 1600 ug/kg 117-84-0 Di-n-octyl phthalate ND 8000 1600 ug/kg 84-66-2 Diethyl phthalate ND 16000 1600 ug/kg 131-11-3 Dimethyl phthalate ND 8000 1600 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 16000 1600 ug/kg 206-44-0 Fluoranthene NDI 8000 800 ug/kg 86-73-7 Fluorene 112008000 800 ug/kg 118-74-I Hexachlorobenzene ND 8000 800 ug/kg 87-68-3 Hexachlorobutadiene ND., >' 8000 800 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 8000 800 ug/kg 67-72-1 Hexachloroethane NO 8000 800 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 8000 800 ug/kg 78-59-1 Isophorone ND 8000 800 ug/kg 90-12-0 I-Methylnaphthalene 97400 8000 800 ug/kg 91-57-6 2-Methylnaphthalene 69400' 8000 800 ug/kg 91-20-3 Naphthalene 1500D 8000 800 ug/kg 95-95-3 Nitrobenzene ND :8000 800 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 8000 800 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 8000 800 ug/kg 85-01-8 Phenanthrene 17400 8000 800 ug/kg 129-00-0 Pyrene 4430 8000 800 ug/kg I CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 0% b 40-102% 4165-62-2 Phenol-d5 0%b 41-100% 118-79-6 2,4,6-Tribromophenol 0%b 42-108% 4165-60-0 Nitrobenzene-d5 096 b 40-105% 321-60-8 2-Fluorobiphenyl 0% b 43-107% 1718-51-0 Terphenyl-dl4 0% b 45-119% (a) Dilution required due to matrix interference. (b) Outside control limits due to dilution. Page 2 of 27W,, u NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound s® 18 of 90 ACCUTEST. FAi9708 Accutest Laboratories Report of Analysis Page 1 of 1 W Client Sample ID: CS-1-10' Lab Sample ID: FA19708-3 Date Sampled: I1/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: MADEP VPH REV 1.1 Percent Solids: 81.8 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UV066525.D 1 11/05/14 Ali n/a n/a GUV3537 Run#2 UV066539.D 10 11/06/14 AH n/a n/a GUV3538 Initial Weight Final Volume Methanol Aliquot on #1 5.25 g 5.1 ml 10.0 ul .on #2 5.25 g 5.1 ml 5.0 ul Accutest Laboratories Report of Analysis Page I of 1 W Client Sample ID: CS-1-10' Lab Sample ID: FA19708-3 Date Sampled: 11/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 81.8 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN010949.1) 50 11/13/14 NAF I1/06/14 OP53815 GNN481 Run #2 Initial Weight Final Volume an #1 20.3 g 2.0 ml on #2 MADEP VPH List MAEPH List CAS No. Compound Result RL MDL Units Q CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 1000 710 710 ug/kg 83-32-9 Acenaphthene 15300 12000 6000 ug/kg 100-41-4 Ethylbenzene 36300 1400 710 ug/kg 208-96-8 Acenaphthylene 8540 :. 12000 6000 ug/kg J 1634-04-4 Methyl Tert Butyl Ether ND 1400 710 ug/kg 120-12-7 Anthracene ND 12000 6000 ug/kg 91-20-3 Naphthalene 95800 3500 2100 ug/kg 56-55-3 Benzo(a)anthracene ND 12000 6000 ug/kg 108-88-3 Toluene 21500 1400 710 ug/kg 50-32-8 Benzo(a)pyrene NA 12000 6000 ug/kg m,p-Xylene 77200 2800 1400 ug/kg 205-99-2 Benzo(b)fluoranthene ND 12000 6000 ug/kg 95-47-6 o-Xylene 63100 1400 710 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 12000 6000 ug/kg C5- C8 Aliphatics (Unadj.) 226000 71000 25000 ug/kg 207-08-9 Benzo(k)fluoranthene ND 12000 6000 ug/kg C9- C12 Aliphatics (Unadj.) ND 71000 25000 ug/kg 218-01-9 Chrysene ND 12000 6000 ug/kg C9- CIO Aromatics (Unadj.) 2830000 a 1400000 490000 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 12000 6000 ug/kg C5- C8 Aliphatics 204000 71000 25000 ug/kg 206-44-0 Fluoranthene NO 12000 6000 ug/kg C9- C12 Aliphatics ND 71000 25000 ug/kg 86-73-7 Fluorene 8750 12000 6000 ug/kg J C9- CIO Aromatics 28300004 ;1400000 490000 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 12000 6000 ug/kg 91-57-6 2-Methylnaphthalene 62500 i 12000 6000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 91-20-3 Naphthalene 10400 : 12000 6000 ug/kg J 85-01-8 Phenanthrene 11400 z 12000 6000 ug/kg J 460-00-4 BFB 557% c 0% b 70-130% 129-00-0 Pyrene ND 12000 6000 ug/kg 460-00-4 BFB 37296c 0%b 70-130% Cll-C22 Aromatics (Unadj.) 3420000 1600000 450000 ug/kg Cll-C22 Aromatics 3300000 600000 450000 ug/kg (a) Result is from Run# 2 C9-C18 Aliphatics 5270000 600000 300000 ug/kg (b) Outside control limits due to dilution. CI9-06 Aliphatics 1240000 600000 300000 ug/kg (c) Outside control limits due to matrix interference. CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 I-Chlorooctadecane 0%A 40-140% 580-13-2 2-Bromonaphthalene 0%4 40-140% 84-15-I o-Terphenyl 0% a 40-140% 321-60-8 2-Fluorobiphenyl 0% a 40-140% (a) Outside control limits due to dilution. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■�q 19 of 90 ACCUTEBT. FAMUS ,•,'•,..• ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■d 20 of 90 M ACCUTEST, FAWN Accutest Laboratories Report of Analysis Page 1 of 2 A Client Sample ID: CS-2-10' 11/04/14 Lab Sample ID: FA19708-4 Date Sampled: Matrix: SO - Soil Date Received: 11/05/14 Method: SW846 8260B Percent Solids: 80.3 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 Y17002.1) 1 11/05/14 AD n/a n/a VY747 Run #2 Y17003.1) 1 11/05/14 AD n/a n/a VY797 Initial Weight Methanol Aliquot Run #I 4.82 g 100 ul Run #2 4.82 g 10.0 ul I VOA Special List CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone NA 3800 1200 ug/kg 71-43-2 Benzene 626 1 380 77 ug/kg 75-27-4 Bromodichloromethane NO: 380 77 ug/kg 75-25-2 Bromoform ND 380 83 ug/kg 104-51-8 n-Butylbenzene 160009 <3800 770 ug/kg 108-90-7 Chlorobenzene Np 380 77 ug/kg 75-00-3 Chloroethane ND 380 170 ug/kg 67-66-3 Chloroform ND 380 87 ug/kg 75-15-0 Carbon disulfide ND 380 77 ug/kg 56-23-5 Carbon tetrachloride ND 380 110 ug/kg I10-82-7 Cyclohexane 2150 i380 81 ug/kg 75-34-3 1,1-Dichloroethane ND,,:::380 77 ug/kg 75-35-4 I,1-Dichloroethylene NO 380 77 ug/kg 96-12-8 1. 2 -Dibromo- 3 -chloropropane NO 380 160 ug/kg 106-93-4 1,2-Dibromoethane NO 380 140 ug/kg 107-06-2 1,2-Dichloroethane NO 380 77 ug/kg 78-87-5 1,2-Dichloropropane IND i 380 77 ug/kg 124-48-1 Dibromochloromethane NO 380 77 ug/kg 75-71-8 Dichlorodifluoromethane ND 380 97 ug/kg 156-59-2 cis-1,2-Dichloroethylene NO 380 77 ug/kg 10061-01-5 cis-1,3-Dichloropropene NO 380 77 ug/kg 541-73-1 m-Dichlorobenzene NO 380 77 ug/kg 95-50-1 o-Dichlorobenzene ND .......... ....... 380 77 ug/kg 106-46-7 p-Dichlorobenzene ND 380 86 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 380 100 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 380 77 ug/kg 100-41-4 Ethylbenzene 19800 a 3800 770 ug/kg 591-78-6 2-Hexanone NO 1900 380 ug/kg 98-82-8 Isopropylbenzene 104Q0 380 77 ug/kg 108-10-1 4-Methyl-2-pentanone ND 1900 380 ug/kg 79-20-9 Methyl acetate NO 1900 380 ug/kg 74-83-9 Methyl bromide NO 380 140 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound s® 21 of 90 W ACCUTEST. FAI9708 Accutest Laboratories Report of Analysis Tent Sample ID: CS-2-10' ab Sample ID: FA19708-4 Date Sampled: 11/04/14 4atrix: SO - Soil Date Received: 11/05/14 4thod: SW846 8260B Percent Solids: 80.3 roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC VOA Special List CAS No. Compound 74-87-3 Methyl chloride 108-87-2 Methylcyclohexane 75-09-2 Methylene chloride 78-93-3 Methyl ethyl ketone 1634-04-4 Methyl Tert Butyl Ether 91-20-3 Naphthalene 103-65-1 n-Propylbenzene 100-42-5 Styrene 71-55-6 1, 1, 1 -Trichloroethane 79-34-5 1, 1, 2,2-Tetrachloroethane 79-00-5 1, 1, 2-Trichloroethane 120-82-1 1,2,4-Trichlorobenzene 95-63-6 1,2,4-Trimethylbenzene 108-67-8 1,3,5-Trimethylbenzene 127-18-4 Tetrachloroethylene 108-88-3 Toluene 79-01-6 Trichloroethylene 75-69-4 Trichlorofluoromethane 75-01-4 Vinyl chloride 1330-20-7 Xylene (total) CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 2037-26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 (a) Result is from Run# 2 Result RL MDL Units Q NO 380 150 ug/kg 13100 380 77 ug/kg NO 770 310 ug/kg NO r 1900 580 ug/kg NO 380 77 ug/kg 210004 3800 1500 ug/kg 199004_ :3800 770 ug/kg NO dd 380 77 ug/kg NO 380 77 ug/kg NO, 380 110 ug/kg NO ? 380 120 ug/kg ND t 380 88 ug/kg 91200' 3800 770 ug/kg 23700 3800 770 ug/kg Na,--"'. 380 97 ug/kg 15300' 3800 770 ug/kg ND 380 78 ug/kg NIX 380 77 ug/kg NO, 380 78 ug/kg 99906a 12000 2000 ug/kg Run# 1 Run# 2 Limits 106% 104%, 75-124% 98% 160%I 75-126% 113% 110% ; 71-133% 99% 96%: 72-135% Page 2 of 2 L ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound s■ 22 of 90 a ACCUTE6T. FAI9708 Accutest Laboratories Report of Analysis Page 1 of 2 A Client Sample ID: CS-2-10' Lab Sample ID: FA19708-4 Date Sampled: 11/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: SW846 8270D SW846 3550C Percent Solids: 80.3 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 8 U047760.1) 40 11/10/14 NJ 11/05/14 OP53802 SU2190 Run #2 Initial Weight Final Volume ,on #1 29.8 g 1.0 ml .un #2 ABN Special List CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid NO 42000 8400 ug/kg 95-57-8 2-Chlorophenol NO 8400 840 ug/kg 59-50-7 4-Chloro-3-methyl phenol NO 8400 840 ug/kg 120-83-2 2,4-Dichlorophenol NO 8400 860 ug/kg 105-67-9 2,4-Dimethylphenol NO 8400 920 ug/kg 51-28-5 2,4-Dinitrophenol ND 42000 8400 ug/kg 534-52-1 4,6-Dinitro-o-cresol NO 17000 3300 ug/kg 95-48-7 2-Methylphenol ND 8400 840 ug/kg 3&4-Methylphenol NO 8400 1700 ug/kg 88-75-5 2-Nitrophenol NO 8400 840 ug/kg 100-02-7 4-Nitrophenol NO 42000 6700 ug/kg 87-86-5 Pentachlorophenol ND 42000 6700 ug/kg 108-95-2 Phenol NO 8400 840 ug/kg 88-06-2 2,4,6-Trichlorophenol NO 8400 840 ug/kg 83-32-9 Acenaphthene NO 8400 1100 ug/kg 208-96-8 Acenaphthylene ND 8400 840 ug/kg 120-12-7 Anthracene ND:,,8400 840 ug/kg 56-55-3 Benzo(a)anthracene NO 8400 840 ug/kg 50-32-8 Benzo(a)pyrene NO 8400 840 ug/kg 205-99-2 Benzo(b)fluoranthene NO 8400 840 ug/kg 191-24-2 Benzo(g,h,t)perylene NO 8400 840 ug/kg 207-08-9 Benzo(k)fluoranthene NO 8400 910 ug/kg 101-55-3 4-Bromophenyl phenyl ether NO 8400 840 ug/kg 85-68-7 Butyl benzyl phthalate NO 8400 1700 ug/kg 91-58-7 2-Chloronaphthalene ND 8400 990 ug/kg 106-47-8 4-Chloroaniline NO 8400 840 ug/kg 218-01-9 Chrysene NO 8400 840 ug/kg I11-91-1 bis(2-Chloroethoxy)methane NO 8400 840 ug/kg 111-44-4 bis(2-Chloroethyl)ether NO 8400 840 ug/kg 108-60-1 bis(2-Chlorolsopropyl)ether NO 8400 870 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether NO 8400 1200 ug/kg 121-14-2 2,4-Dinitrotoluene NO 8400 950 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ■p 23 of 90 M AGCIJTEST. FAI9708 Accutest Laboratories Report of Analysis 'lient Sample ID: CS-2-10' ab Sample ID: FA19708-4 Date Sampled: 11/04/14 4atrix: SO - Soil Date Received: I1/05/14 fethod: SW846 8270D SW846 3550C Percent Solids: 80.3 roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ABN Special List CAS No. Compound Result RL MDL Units Q 606-20-2 2,6-Dinitrotoluene NO, 8400 910 ug/kg 91-94-1 3,3'-Dichlorobenzidine NO 8400 840 ug/kg 53-70-3 Dibenzo(a,h)anthracene NO 8400 840 ug/kg 132-64-9 Dibenzofuran NO 8400 840 ug/kg 84-74-2 Di-n-butyl phthalate ND 17000 1700 ug/kg 117-84-0 Di-n-octyl phthalate NO 8400 1700 ug/kg 84-66-2 Diethyl phthalate NO 17000 1700 ug/kg 131-11-3 Dimethyl phthalate NO 8400 1700 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate NO 17000 1700 ug/kg 206-44-0 Fluoranthene NO 8400 840 ug/kg 86-73-7 Fluorene 3710 8400 840 ug/kg J 118-74-1 Hexachlorobenzene NO 8400 840 ug/kg 87-68-3 Hexachlorobutadiene ND 8400 840 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 8400 840 ug/kg 67-72-1 Hexachloroethane NO 8400 840 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 8400 840 ug/kg 78-59-1 Isophorone ND 8400 840 ug/kg 90-12-0 1-Methylnaphthalene 20100 3 8400 840 ug/kg 91-57-6 2-Methylnaphthalene 30100 8400 840 ug/kg 91-20-3 Naphthalene 0350 " 8400 840 ug/kg 98-95-3 Nitrobenzene ND 8400 840 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 8400 840 ug/kg 86-30-6 N-Nitrosodiphenylamine NO 8900 840 ug/kg 85-01-8 Phenambrene 4480 8400 840 ug/kg J 129-00-0 Pyrene 2120 8400 840 ug/kg J CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 0% 6 40-102% 4165-62-2 Phenol-d5 0% b 41-100% 118-79-6 2,4,6-Tribromophenol 0%b 42-108% 4165-60-0 Nitrobenzene-d5 0% b 40-105% 321-60-8 2-Fluorobiphenyl 0% b 43-107% 1718-51-0 Terphenyl-dl4 0966 ' 45-119% (a) Dilution required due to matrix interference. (h) Outside control limits due to dilution. Page 2 of 2 r1 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MR 24 of 90 M ACCUTEST, FAI9709 Accutest Laboratories Report of Analysis Page I of 1 A Client Sample ID: CS-2-10' Lab Sample ID: FA19708-4 Date Sampled: 11/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: MADEP VPH REV 1.1 Percent Solids: 80.3 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 UV066526.1) 1 11/05/14 Ali n/a n/a GUV3537 Run #2 UV066540.1) 10 11/06/14 AH n/a n/a GUV3538 Initial Weight Final Volume Methanol Aliquot Run #1 4.82 g 5.1 nil 10.0 ul Run #2 4.82 g 5.1 nil 5.0 111 MADEP VPH List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 895 780 780 ug/kg 100-41-4 Ethylbenzene 43660 1600 780 ug/kg 1634-04-4 Methyl Ter( Butyl Ether ND 1600 780 ug/kg 91-20-3 Naphthalene 97000 3900 2300 ug/kg 108-88-3 Toluene 22400 :I600 780 ug/kg m,p-Xylene 84000 3100 1600 ug/kg 95-47-6 o-Xylene 71300 1600 780 ug/kg C5- C8 ABphatics (Unadj.) 290000 78000 27000 ug/kg C9- C12 Aliphatics (Unadj.) ND 78000 27000 ug/kg C9- CIO Aromatics (Unadj.) 3590000 a 1600000 550000 ug/kg C5- C8 ABphatics 267000 78000 27000 ug/kg C9- C12 ABphatics ND 78000 27000 ug/kg C9- CIO Aromatics 35900000 1600000 550000 ug/kg CAS No. Surrogate Recoveries Run# I Run# 2 Limits 460-00-4 BFB 422%c 0%b 70-130% 460-00-4 BFB 253%c 096b 70-130% (a) Result is from Run# 2 (b) Outside control limits due to dilution. (c) Outside control limits due to matrix interference ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ma 25 of 90 W ACCIJTE^E.T. FA19708 Accutest Laboratories Report of Analysis Page 1 of 1 it Sample ID: CS-2-10' Sample ID: FA19708-4 Date Sampled: I1/04/14 rix: SO - Soil Date Received: I1/05/14 iod: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 80.3 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 NN010957.D 200 11/13/14 NAF I1/06/14 OP53815 GNN981 #2 Run #1 Run #2 Initial Weight Final Volume 20.1 g 2.0 nil MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene ND 50000 25000 ug/kg 208-96-8 Acenaphihylene ND 50000 25000 ug/kg 120-12-7 Anthracene ND 50000 25000 ug/kg 56-55-3 Benzo(a)anthracene ND 50000 25000 ug/kg 50-32-8 Benzo(a)pyrene ND, 50000 25000 ug/kg 205-99-2 Benzo(b)fluoranthene ND 50000 25000 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 50000 25000 ug/kg 207-08-9 Benzo(k)fluoranthene NlY1.1 50000 25000 ug/kg 218-01-9 Chrysene NO 50000 25000 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 50000 25000 ug/kg 206-44-0 Fluoranthene ND 50000 25000 ug/kg 86-73-7 Fluorene ND 50000 25000 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND; 50000 25000 ug/kg 91-57-6 2-Me(hylnaphthalene 119000; 50000 25000 ug/kg 91-20-3 Naphthalene ND 50000 25000 ug/kg 85-01-8 Phenanthrene ND 50000 25000 ug/kg 129-00-0 Pyrene ND 50000 25000 ug/kg ClI-C22 Aromatics (Unadj.) 6140000 2500000 1900000 ug/kg Cll-C22 Aromatics 6020000,1_2500000 1900000 ug/kg C9-C18 ABphatics 14000006 12500000 1200000 ug/kg C19-C36 Aliphatics 3740000 j2500000 1200000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane O a 40-140% 580-13-2 2-Bromonaphthalene 0%a 40-140% 84-15-1 o-Terphenyl 0% a 40-140% 321-60-8 2-Fluorobiphenyl 0% a 40-140% (a) Outside control limits due to dilution NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyse found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound Mw 26 of 90 rAt9708 •.••"•••"••", Accutest Laboratories Report of Analysis Page 1 of 2 it Sample ID: CS-3-10' Sample ID: FA19708-5 Date Sampled: I1/04/14 rix: SO - Soil Date Received: 11/05/14 rod: SW846 8260B Percent Solids: 85.8 act: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 Y17004.1) 1 11/05/14 AD n/a n/a VY747 #2 Y17005.1) I 11/05/14 AD n/a n/a VY747 Initial Weight Methanol Aliquot on #1 6.02 g 100 ul :un #2 6.02 g 10.0 ul VOA Special List CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone NA 2800 850 ug/kg 71-43-2 Benzene 75,4 280 57 ug/kg J 75-27-4 Bromodichloromethane ND 280 57 ug/kg 75-25-2 Bromoform ND .280 61 ug/kg 104-51-8 n-Butylbenzene 3380 280 57 ug/kg 108-90-7 Chlorobenzene ND 280 57 ug/kg 75-00-3 Chloroethane ND 280 130 ug/kg 67-66-3 Chloroform ND 280 64 ug/kg 75-15-0 Carbon disulfide ND 280 57 ug/kg 56-23-5 Carbon tetrachloride ND 280 79 ug/kg 110-82-7 Cyclohexane 369 280 60 ug/kg 75-34-3 I,I-Dichloroethane ND 280 57 ug/kg 75-35-4 1,1-Dichloroethylene ND @ 280 57 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 280 120 ug/kg 106-93-4 1,2-Dibromoethane ND 280 100 ug/kg 107-06-2 1,2-Dichloroethane ND 280 57 ug/kg 78-87-5 1,2-Dichloropropane ND 280 57 ug/kg 124-48-1 Dibromochloromethane ND 280 57 ug/kg 75-71-8 Dichlorodifluoromethane ND 280 71 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 280 57 ug/kg 10061-01-5 cis-1,3-Dichloropropee ND 280 57 ug/kg 541-73-I m-Dichlorobenzene NI) 280 57 ug/kg 95-50-1 o-Dichlorobenzene ND 280 57 ug/kg 106-46-7 p-Dichlorobenzene ND 280 63 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 280 76 ug/kg 10061-02-6 trans-1,3-Dichloropropee ND 280 57 ug/kg 100-41-4 Ethylbenzene 3230 280 57 ug/kg 591-78-6 2-Hexanone ND 1400 280 ug/kg 98-82-8 Isopropylbenzene 2690 280 57 ug/kg 108-10-1 4-Methyl-2-pentanone Np 1400 280 ug/kg 79-20-9 Methyl acetate ND 1400 280 ug/kg 74-83-9 Methyl bromide ND 280 110 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound on 27 of 90 M ACCUTEST. FA19708 Accutest Laboratories Report of Analysis 'Iient Sample ID: CS-3-10' ab Sample ID: FA19708-5 Date Sampled: 11/04/14 fatrix: SO - Soil Date Received: 11/05/14 mthod: SW846 8260B Percent Solids: 85.8 roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC VOA Special List CAS No. Compound Result RL MDL Units Q 74-87-3 Methyl chloride ND 280 110 ug/kg 108-87-2 Methylcyclohexane 2240 s 280 57 ug/kg 75-09-2 Methylene chloride ND 570 230 ug/kg 78-93-3 Methyl ethyl ketone ND 1400 420 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 280 57 ug/kg 91-20-3 Naphthalene 126004 i 2800 1100 ug/kg 103-65-1 n-Propylbenzene 4520 280 57 ug/kg 100-42-5 Styrene ND 280 57 ug/kg 71-55-6 I, I,I-Trichloroethane ND 280 57 ug/kg 79-34-5 1, 1, 2,2-Tetrachloroethane ND 280 80 ug/kg 79-00-5 1,1,2-Trichloroethane ND 280 91 ug/kg 120-82-1 1,2,4-Trichlorobenzene 10 280 65 ug/kg 95-63-6 1,2,4-Trimethylbenzene 20404 2800 570 ug/kg 108-67-8 1. 3,5 -Trimethylbenzene 6180 280 57 ug/kg 127-18-4 Tetrachloroethylene ND 280 71 ug/kg 108-88-3 Toluene 1780 280 57 ug/kg 79-01-6 Trichloroethylene ND 280 58 ug/kg 75-69-4 Trichlorofluoromethane ND 280 57 ug/kg 75-01-4 Vinyl chloride ND 280 58 ug/kg 1330-20-7 Xylene (total) 18800 1 850 150 ug/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 105% 104% 75-124% 2037-26-5 Toluene-D8 98% 97% 75-126% 460-00-4 4-Bromofluorobenzene 112% ', 107% 71-133% 17060-07-0 1,2-Dichloroethane-D4 97% 97% 72-135% (a) Result is from Run# 2 Page 2 of 2 L ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound on 28 of 90 w ACCUTEST. FA19709 •••: •-,"�•, Accutest Laboratories Report of Analysis Page 1 of 2 Client Sample ID: CS-3-10' Lab Sample ID: FA19708-5 Date Sampled: I I/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: SW846 8270D SW846 3550C Percent Solids: 85.8 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1a T015326.D 10 11/07/14 NJ 11/05/14 OP53802 ST717 6Run #2 Run #1 Run #2 Initial Weight Final Volume 29.8 g 1.0 ml ABN Special List CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 9800 2000 ug/kg 95-57-8 2-Chlorophenol ND 2000 200 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 2000 200 ug/kg 120-83-2 2,4-Dichlorophenol NO 2000 200 ug/kg 105-67-9 2,4-Dimethylphenol ND 2000 220 ug/kg 51-28-5 2,4-Dinitrophenol NO, 9800 2000 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 3900 780 ug/kg 95-48-7 2-Methylphenol ND 2000 200 ug/kg 3&4-Methylphenol ND 2000 390 ug/kg 88-75-5 2-Nitrophenol ND 2000 200 ug/kg 100-02-7 4-Nitrophenol NDI 9800 1600 ug/kg 87-86-5 Pentachlorophenol ND 9800 1600 ug/kg 108-95-2 Phenol ND 2000 200 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 2000 200 ug/kg 83-32-9 Acenaphthene 1640 2000 250 ug/kg J 208-96-8 Acenaphthylene ND 2000 200 ug/kg 120-12-7 Anthracene 2601 2000 200 ug/kg J 56-55-3 Benzo(a)anthracene ND 2000 200 ug/kg 50-32-8 Benzo(a)pyrene ND 2000 200 ug/kg 205-99-2 Benzo(b)fluoranthene ND 2000 200 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 2000 200 ug/kg 207-08-9 Benzo(k)fluoranthene ND 2000 210 ug/kg 101-55-3 4-Bromophenyl phenyl ether NIT:2000 200 ug/kg 85-68-7 Butyl benzyl phthalate ND 2000 390 ug/kg 91-58-7 2-Chloronaphthalene ND 2000 230 ug/kg 106-47-8 4-Chloroaniline NO 2000 200 ug/kg 218-01-9 Chrysene ND 2000 200 ug/kg 111-91-1 bis(2-Chloroethoxy)methane :ND 2000 200 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 2000 200 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 2000 200 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 2000 290 ug/kg 121-14-2 2,4-Dinitrotoluene ND 2000 220 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound me 29 of 90 w AGGUTEST. FA19708 Accutest Laboratories Report of Analysis 3ient Sample ID: CS-3-10' .ab Sample ID: FA19708-5 Date Sampled: 11/04/14 4atrix: SO - Soil Date Received: 11/05/14 4thod: SW846 8270D SW846 3550C Percent Solids: 85.8 roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ABN Special List CAS No. Compound Result 606-20-2 2,6-Dinitrotoluene ND 91-94-1 3,3'-Dicblorobenzidine ND 53-70-3 Dibenzo(a,h)anthracene NO 132-64-9 Dibenzofuran 566 84-74-2 Di-n-butyl phthalate ND 117-84-0 Di-n-octyl phthalate NO 84-66-2 Diethyl phthalate ND 131-11-3 Dimethyl phthalate ND '•. 117-81-7 bis(2-Ethylhexyl)phthalate ND 206-44-0 Fluoranthene 201 86-73-7 Fluorene 2430 118-74-1 Hexachlorobenzene ND 87-68-3 Hexachlorobutadtene ND 77-47-4 Hexachlorocyclopentadiene ND 67-72-1 Hexachloroethane ND 193-39-5 Indeno(1,2,3-cd)pyrene ND 78-59-1 Isophorone ND 90-12-0 1-Methylnaphthalene 14900' 91-57-6 2-Methylnaphthalene 20500' 91-20-3 Naphthalene 4740 98-95-3 Nitrobenzene ND 621-64-7 N-Nitroso-di-n-propylamine ND 86-30-6 N-Nitrosodiphenylamine ND 1. 85-01-8 Phenanthrene 4330 129-00-0 Pyrene 1220 > CAS No. Surrogate Recoveries Run# 1 367-12-4 2-Fluorophenol 72% 4165-62-2 Phenol-d5 84% 118-79-6 2,4,6-Tribromophenol 69% 4165-60-0 Nitrobenzene-d5 85% 321-60-8 2-Fluorobiphenyl 79% 1718-51-0 Terphenyl-d14 84% (a) Dilution required due to matrix interference RL MDL Units Q 2000 210 ug/kg 2000 200 ug/kg 2000 200 ug/kg 2000 200 ug/kg 1 3900 390 ug/kg 2000 390 ug/kg 3900 390 ug/kg 2000 390 ug/kg 3900 390 ug/kg 2000 200 ug/kg J 2000 200 ug/kg 2000 200 ug/kg =2000 200 ug/kg 2000 200 ug/kg 2000 200 ug/kg r2000 200 ug/kg .2000 200 ug/kg 2000 200 ug/kg -2000 200 ug/kg 2000 200 ug/kg 2000 200 ug/kg 2000 200 ug/kg 2000 200 ug/kg 2000 200 ug/kg 2000 200 ug/kg J Run# 2 Limits 40-102% 41-100% 42-108 % 40-105% 43-107% 45-119% Page 2 of 2 w r ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound E. 30 of 90 w AGGUTEST, FA19708 Accutest Laboratories Report of Analysis Page 1 of 1 at Sample ID: CS-3-10' Sample ID: FA19708-5 Date Sampled: 11/04/14 rix: SO - Soil Date Received: 11/05/14 and: MADEP VPH REV 1.1 Percent Solids: 85.8 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 UV066527.1) 1 11/05/14 AH n/a n/a GUV3537 #2 UV066542.1) 10 11/06/14 AH n/a n/a GUV3538 Initial Weight Final Volume Methanol Aliquot :un #1 6.02 g 5.1 nil 10.0 ul ,on #2 6.02 g 5.1 nil 10.0 ul Acculest Laboratories Report of Analysis Page 1 of 1 it Sample ID: CS-3-10' Sample ID: FA19708-5 Date Sampled: 11/04/14 -ix: SO - Soil Date Received: 11/05/14 1od: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 85.8 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 NN010952.D 20 11/13/14 NAF 11/06/14 OP53815 GNN481 #2 Initial Weight Final Volume on #I 20.5 g 2.0 nil on #2 MADEP VPH List MAEPH List CAS No. Compound Result RL MDL Units Q CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene NO 580 580 ug/kg 83-32-9 Acenaphthene 4130 4500 2300 ug/kg J 100-41-4 Ethylbenzene 7410 1200 580 ug/kg 208-96-8 Acenaphthylene 2720 ' 4500 2300 ug/kg J 1634-04-4 Methyl Ter( Butyl Ether ND 1200 580 ug/kg 120-12-7 Anthracene ND 4500 2300 ug/kg 91-20-3 Naphthalene 32600 2900 1700 ug/kg 56-55-3 Benzo(a)anthracene ND :4500 2300 ug/kg 108-88-3 Toluene 2300 1200 580 ug/kg 50-32-8 Benzo(a)pyrene ND 4500 2300 ug/kg m,p-Xylene 13000 2300 1200 ug/kg 205-99-2 Benzo(b)fluoranthene ND 4500 2300 ug/kg 95-47-6 o-Xylene 13100 1200 580 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 4500 2300 ug/kg C5- C8 Aliphatirs (Unadj.) 166M 58000 20000 ug/kg 207-08-9 Benzo(k)fluoranthene ND 9500 2300 ug/kg C9- C12 Aliphatics (Unadj.) ND 58000 20000 ug/kg 218-01-9 Chrysene ND 4500 2300 ug/kg C9- C10 Aromatics (Unadj.) 847004 1580000 200000 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND :4500 2300 ug/kg C5- C8 Aliphatics 58600 58000 20000 ug/kg 206-44-0 Fluoranthene ND r4500 2300 ug/kg C9- C12 Aliphatics ND 58000 20000 ug/kg 86-73-7 Fluorene 2950 4500 2300 ug/kg J C9- C10 Aromatics 9470M ° ;580000 200000 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 4500 2300 ug/kg 9157-6 2-Methylnaphthalene 18000 9500 2300 ug/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 91-20-3 Naphthalene 2400 4500 2300 ug/kg j 85-01-8 Phenanthrene ND 4500 2300 ug/kg 460-00-4 BFB 246% a 0% b 70-130% 129-00-0 Pyrene ND 4500 2300 ug/kg 460-00-4 BFB 219%c 0%b 70-130% C11-C22Aromatics (Unadj.) 935000 230000 170000 ug/kg C11-C22 Aromatics 90$000 230000 170000 ug/kg (a) Result is from Run# 2 C9-C18 A6phatics 17916,610, 230000 110000 ug/kg (b) Outside control limits due to dilution. C19-C36 Aliphadcs 488000* _ J 230000 110000 ug/kg (c) Outside control limits due to matrix interference. CAS No. Surrogate Recoveries Run# I Run# 2 Limits 3386-33-2 I-Chlorooctadecane .................... 0%s..;<._ 40-140% 580-13-2 2-Bromonaphthalene 0%° 40-140% 84-15-1 o-Terphenyl 0% A 40-140% 321-60-8 2-Fluorobiphenyl 0% ° 40-140% (a) Outside control limits due to dilution. ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound ME 31 of 90 w ACCLITEST. FA19708 NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound on 32 of 90 ACCUTEST. FAI9708 Acculest Laboratories Report of Analysis Page 1 of 2 oW Client Sample ID: CS-4-10' Lab Sample ID: FA19708-6 Date Sampled: 11/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: SW846 8260B Percent Solids: 79.0 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 Y17007.D 1 11/05/14 AD n/a n/a VY747 Run #2 F0067011.D 1 11/06/14 AD n/a n/a VF2291 Initial Weight Methanol Aliquot Run #1 5.18 g 100 ul Run #2 5 35 g 10.0 ul VOA Special List CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 3700 1100 ug/kg 71-43-2 Benzene 1030 370 74 ug/kg 75-27-4 Bromodichloromethane ND 370 74 ug/kg 75-25-2 Bromoform ND 370 80 ug/kg 104-51-8 n-Butylbenzene 13200 370 74 ug/kg 108-90-7 Chlorobenzene ND 370 74 ug/kg 75-00-3 Chloroethane ND 370 170 ug/kg 67-66-3 Chloroform ND-370 84 ug/kg 75-15-0 Carbon disulfide ND 370 74 ug/kg 56-23-5 Carbon tetrachloride NA ::,370 100 ug/kg 110-82-7 Cyclohexane 2230 370 79 ug/kg 75-34-3 1,1-Dichloroethane ND 370 74 ug/kg 75-35-4 1,1-Dichloroethylene ND 370 74 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 370 160 ug/kg 106-93-4 1,2-Dibromoethane ND 370 130 ug/kg 107-06-2 1,2-Dichloroethane ND 370 74 ug/kg 78-87-5 1,2-Dichloropropane ND 370 74 ug/kg 124-48-1 Dibromoflhoromethane ND 370 74 ug/kg 75-71-8 Dichlorodifluoromethane ND 370 94 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 370 74 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 370 74 ug/kg 541-73-1 m-Dichlorobenzene ND 370 74 ug/kg 9550-1 o-Dichlorobenzene ND 370 74 ug/kg 106-46-7 p-Dichlorobenzene ND 370 83 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 370 100 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 370 74 ug/kg 100-41-4 Ethylbenzene 113300 a 3600 720 ug/kg 591-78-6 2-Hexanone ND 1900 360 ug/kg 98-82-8 Isopropylbenzene 11600 370 74 ug/kg 108-10-1 4-Methyl-2-pentanone ND 1900 370 ug/kg 79-20-9 Methyl acetate ND 1900 370 ug/kg 74-83-9 Methyl bromide ND 370 140 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 00 33 of 90 w ACCUTEST. FA79r08 Accutest Laboratories Report of Analysis 'lien Sample ID: CS-4-10' ,ab Sample ID: FA19708-6 Date Sampled: 11/04/14 4atrix: SO - Soil Date Received: 11/05/14 4ethod: SW846 8260B Percent Solids: 79.0 'reject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC VOA Special List CAS No. Compound 74-87-3 Methyl chloride 108-87-2 Methylcyclohexane 75-09-2 Methylene chloride 78-93-3 Methyl ethyl ketone 1634-04-4 Methyl Tert Butyl Ether 91-20-3 Naphthalene 103-65-1 n-Propylbenzene 100-42-5 Styrene 71-55-6 1, 1, 1 -Trichloroethane 79-34-5 1,1,2,2-Tetrachloroethane 79-00-5 1, 1, 2-Trichl oroethane 120-82-1 1,2,4-Trichlorobenzene 95-63-6 1,2,4-Trimethylbenzene 108-67-8 1,3,5-Trimethylbenzene 127-18-4 Tetrachloroethylene 108-88-3 Toluene 79-01-6 Trichloroethylene 75-69-4 Trichlorofluoromethane 75-01-4 Vinyl chloride 1330-20-7 Xylene (total) CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 2037-26-5 Toluene-138 460-00-4 4-Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 (a) Result is from Run# 2 Result RL MDL Units Q ND " 370 150 ug/kg 9520 370 74 ug/kg ND 740 300 ug/kg ND > 1900 560 ug/kg ND : 370 74 ug/kg 728000 3600 1400 ug/kg 17100a ' 3600 720 ug/kg NO 370 74 ug/kg ND 370 74 ug/kg NO 370 100 ug/kg ND ! 370 120 ug/kg ND 370 86 ug/kg 82000 3600 720 ug/kg 200004 3600 720 ug/kg NO, - '370 94 ug/kg 12000 ' 370 74 ug/kg ND 1370 76 ug/kg ND 370 74 ug/kg ND 370 76 ug/kg 76600a ;11000 1900 ug/kg Run# 1 Run# 2 Limits 105% 101%75-124% 97% 92% ,' 75-126% 115% 104%- 71-133% 98% 100%' 72-135% Page 2 of 2 ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound V13 MM 34 of 90 w ACCUTEST° FA19708 •.••.,••••,••", Accutest Laboratories Report of Analysis Page 1 of 2 m Client Sample ID: CS-4-10' Lab Sample ID: FA19708-6 Date Sampled: 11/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: SW846 8270D SW846 3550C Percent Solids: 79.0 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID OF Analyzed By Prep Date Prep Batch Analytical Batch Run #1a U047761.1) 80 11/10/14 NJ 11/05/14 OP53802 SU2190 Run #2 Initial Weight Final Volume An #1 30.0 g 1.0 ml .on #2 ABN Special List CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid NI), 84000 17000 ug/kg 95-57-8 2-Chlorophenol ND17000 1700 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 17000 1700 ug/kg 120-83-2 2,4-Dichlorophenol ND 17000 1700 ug/kg 105-67-9 2,4-Dimelhylphenol ND 17000 1900 ug/kg 51-28-5 2,4-Dinitrophenol ND 84000 17000 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 34000 6800 ug/kg 95-48-7 2-Methylphenol ND 17000 1700 ug/kg 3&4-Methylphenol ND 17000 3400 ug/kg 88-75-5 2-Nitrophenol ND 17000 1700 ug/kg 100-02-7 4-Nitrophenol ND 84000 14000 ug/kg 87-86-5 Pentachlorophenol ND 84000 14000 ug/kg 108-95-2 Phenol ND 17000 1700 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 17000 1700 ug/kg 83-32-9 Acenaphthene 10600 17000 2100 ug/kg J 208-96-8 Acenaphthylene ND 17000 1700 ug/kg 120-12-7 Anthracene 2380 17000 1700 ug/kg J 56-55-3 Benzo(a)anthracene ND ` 17000 1700 ug/kg 50-32-8 Benzo(a)pyrene ND 17000 1700 ug/kg 205-99-2 Benzo(b)fluoranthene NO 17000 1700 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 17000 1700 ug/kg 207-08-9 Benzo(k)fluoranthene ND 17000 1800 ug/kg 101-55-3 4-Bromophenyl phenyl ether ND 9 17000 1700 ug/kg 85-68-7 Butyl benzyl phthalate IND 17000 3400 ug/kg 91-58-7 2-Chloronaphthalene ND 17000 2000 ug/kg 106-47-8 4-Chloroaniline ND 17000 1700 ug/kg 218-01-9 Chrysene ND 17000 1700 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 17000 1700 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 17000 1700 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 17000 1800 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether NO 17000 2500 ug/kg 121-14-2 2,4-Dinitrotoluene ND 17000 1900 ug/kg ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound N® 35 of 90 0 AGGUTEST. MUM Acculest Laboratories Report of Analysis ;lien Sample ID: CS-4-10' ,ab Sample ID: FA19708-6 Date Sampled: 11/04/14 4atrix: SO - Soil Date Received: 11/05/14 4ethod: SW846 8270D SW846 3550C Percent Solids: 79.0 'roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ABN Special List CAS No. Compound Result RL MDL Units Q 606-20-2 2,6-Dinitrotoluene ND 117000 1800 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 17000 1700 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 17000 1700 ug/kg 132-64-9 Dibenzofuran 4740 17000 1700 ug/kg J 84-74-2 Di-n-butyl phthalate ND 34000 3400 ug/kg 117-84-0 Di-n-octyl phthalate ND 17000 3400 ug/kg 84-66-2 Diethyl phthalate ND 34000 3400 ug/kg 131-I1-3 Dimethyl phthalate ND 17000 3400 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 34000 3400 ug/kg 206-44-0 Fluoranthene ND 17000 1700 ug/kg 86-73-7 Fluorene 17300 17000 1700 ug/kg 118-74-1 Hexachlorobenzene ND 17000 1700 ug/kg 87-68-3 Hexachlorobutadiene ND 17000 1700 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 17000 1700 ug/kg 67-72-1 Hexachloroethane ND 17000 1700 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 17000 1700 ug/kg 7859-1 Isophorone ND 17000 1700 ug/kg 90-12-0 1-Methylnaphthalene 112600< 17000 1700 ug/kg 91-57-6 2-Methylnaphthalene 1670001 17000 1700 ug/kg 91-20-3 Naphthalene 37000 17000 1700 ug/kg 98-95-3 Nitrobenzene ND 17000 1700 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 17000 1700 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 17000 1700 ug/kg 85-01-8 Phenanthrene 39700 > '17000 1700 ug/kg 129-00-0 Pyrene 6270 '; '17000 1700 ug/kg J CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 096 b 40-102% 4165-62-2 Phenol-d5 0%b 41-100% 118-79-6 2,4,6-Tribromophenol 0%b 42-108% 4165-60-0 Nitrobenzene-d5 0% b 40-105% 321-60-8 2-Fluorobiphenyl 0% b 43-107% 1718-51-0 Terphenyl-dl4 0% b 45-119% (a) Dilution required due to matrix interference. (b) Outside control limits due to dilution. Page 2 of 2 L NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M® 36 of 90 0 A= JTEBT, FAWN "°"" Accutest Laboratories Report of Analysis Page I of I rn it Sample ID: CS-4-10' Sample ID: FA19708-6 Date Sampled: 11/04/14 rix: SO - Soil Date Received: 11/05/14 iod: MADEP VPH REV 1.1 Percent Solids: 79.0 cot: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 UV066528.1) 1 11/05/14 All n/a n/a GUV3537 #2 UV066543.D 10 I1/06/14 AH n/a n/a GUV3538 Initial Weight Final Volume Methanol Aliquot ,on #1 5.18 g 5.1 ml 10.0 ul ,on #2 5.18 g 5.1 m] 5.0 ul MADEP VPH List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene 1430 760 760 ug/kg 100-41-4 Ethylbenzene 30800 1500 760 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1500 760 ug/kg 91-20-3 Naphthalene 1580M 3800 2300 ug/kg 108-88-3 Toluene 16400 1500 760 ug/kg m,p-Xylene 65000 3000 1500 ug/kg 95-47-6 o-Xylene 56300 1500 760 ug/kg C5- C8 Aliphades (Unadj.) MOO,,76000 26000 ug/kg C9- C12 Aliphatics (Unadj.) ND 76000 26000 ug/kg C9- C10 Aromatics (Unadj.) 3660000 a ; 1500000 530000 ug/kg C5- C8 Aliphatics 219000 76000 26000 ug/kg C9- C12 Aliphatics ND 76000 26000 ug/kg C9- C10 Aromatics 30600600 '1500000 530000 u9/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 424%c 0%b 70-130% 460-00-4 BFB 25Mc O%b 70-130% (a) Result is from Run# 2 (b) Outside control limits due to dilution. (c) Outside control limits due to matrix interference ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound No 37 of 90 a ACCUTEST. FA19708 ••,,••.••.•.•, Accutesl Laboratories Report of Analysis Page I of 1 Client Sample ID: CS-4-10' Lab Sample ID: FA19708-6 Date Sampled: 11/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: MADEP EPH REV I.1 SW846 3546 Percent Solids: 79.0 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN010958.1) 250 11/13/14 NAF 11/06/14 OP53815 GNN481 Run #2 Initial Weight Final Volume .on #1 20.1 g 2.0 ml :on #2 MAEPH List CAS No. Compound 83-32-9 Acemphthene 208-96-8 Acenaphthylene 120-12-7 Anthracene 56-55-3 Benzo(a)anthracene 50-32-8 Benzo(a)pyrene 205-99-2 Benzo(b)fluoranthene 191-24-2 Benzo(g h,i)perylene 207-08-9 Benzo(k)fluoranthene 218-01-9 Chrysene 53-70-3 Dibenzo(a,h)anthracene 206-44-0 Fluoranthene 86-73-7 Fluorene 193-39-5 Indeno(1,2,3-cd)pyrene 91-57-6 2-Methylnaphthalene 91-20-3 Naphthalene 85-01-8 Phenanthrene 129-00-0 Pyrene Cll-C22 Aromatics (Unadj.) C11-C22 Aromatics C9-CI8 Aliphatics C19-C36 Aliphatirs CAS No. Surrogate Recoveries 3386-33-2 1-Chloro o ctadecane 580-13-2 2-Bromonaphthalene 84-15-1 o-Terphenyl 321-60-8 2-Fluorobiphenyl (a) Outside control limits due to dilution Result RL MDL Units Q 62500 63000 31000 ug/kg J ND 63000 31000 ug/kg ND 63000 31000 ug/kg ND 63000 31000 ug/kg ND 63000 31000 ug/kg ND t63000 31000 ug/kg NO 63000 31000 ug/kg ND 63000 31000 ug/kg ND 63000 31000 ug/kg ND r 63000 31000 ug/kg ND 63000 31000 ug/kg 32500 63000 31000 ug/kg I ND 63000 31000 ug/kg 307000 63000 31000 ug/kg 5300063000 31000 ug/kg J 43000 63000 31000 ug/kg J ND 63000 31000 ug/kg 12900NO 3100000 2400000 ug/kg 12400000 3100000 2400000 ug/kg 17500000 !,3100000 1600000 ug/kg 392M $3100000 1600000 ug/kg Run# 1 Run# 2 Limits 0%a_i 40-140% 0%a 40-140% 0%a ` 40-140% 0%a 40-140% NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MM 38 of 90 N ACCUTEST, FA19709 Accutest Laboratories Report of Analysis Page 1 of 2 at Sample ID: CS-5-10' Sample ID: FA19708-7 Date Sampled: I1/04/14 rix: SO - Soil Date Received: 11/05/14 rod: SW846 8260B Percent Solids: 85.3 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1 F0067014.D 1 11/06/14 AD n/a n/a VF2291 #2 a Y17008.1) 1 11/05/14 AD n/a n/a VY747 Initial Weight :an #1 6.64 g ,on 02 6.89 g VOA Special List CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone $5.6 44 13 ug/kg 71-43-2 Benzene ND 4.4 0.88 ug/kg 75-27-4 Bromodichloromethane ND 4.4 0.88 ug/kg 75-25-2 Bromoform ND 4.4 0.95 ug/kg 104-51-8 n-Butylbenzene 11.5 4.4 0.88 ug/kg 108-90-7 Chlorobenzene ND 4.4 0.88 ug/kg 75-00-3 Chloroethane ND 4.4 2.0 ug/kg 67-66-3 Chloroform ND 4.4 1.0 ug/kg 75-15-0 Carbon disulfide b ND 4.4 0.88 ug/kg 56-23-5 Carbon tetrachloride ND 4.4 1.2 ug/kg 110-82-7 Cyclohexane ND 4.4 0.94 ug/kg 75-34-3 1,1-Dichloroethane NO 4.4 0.88 ug/kg 75-35-4 1,1-Dichloroethylene ND 4.4 0.88 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 4.4 1.9 ug/kg 106-93-4 1,2-Dibromoethane ND 4.4 1.6 ug/kg 107-06-2 1,2-Dichloroethane ND 4.4 0.88 ug/kg 78-87-5 1,2-Dichloropropane ND 4.4 0.88 ug/kg 124-48-1 Dibromochoromethane ND 4.4 0.88 ug/kg 75-71-8 Dichlorodifluoromethane ND 4.4 1.1 ug/kg 156-59-2 cis-1,2-Dichloroethylene NA _`.4.4 0.88 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 4.4 0.88 ug/kg 541-73-1 m-Dichlorobenzene ND 4.4 0.88 ug/kg 95-50-1 o-Dichlorobenzene ND 4.4 0.88 ug/kg 106-46-7 p-Dichlorobenzene ND 4.4 0.99 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 4.4 1.2 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 4.4 0.88 ug/kg 100-41-4 Ethylbenzene 69 4.4 0.88 ug/kg 591-78-6 2-Hexanone ND 22 4.3 ug/kg 98-82-8 Isopropylberzene 4.1 4.4 0.88 ug/kg j 108-10-1 4-Methyl-2-pentanone ND 22 4.4 ug/kg 79-20-9 Methyl acetate ND 22 4.4 ug/kg 74-83-9 Methyl bromide NO 4.4 1.7 ug/kg ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound so 39 of 90 �ACCUTEST. FA19708 Accutest Laboratories Report of Analysis 'lient Sample ID: CS-5-10' ab Sample ID: FA19708-7 Date Sampled: 11/04/14 latrix: SO - Soil Date Received: 11/05/14 lethod: SW846 8260B Percent Solids: 85.3 roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC VOA Special List CAS No. Compound Result RL MDL Units Q 74-87-3 Methyl chloride ND 4.4 1.8 ug/kg 108-87-2 Methylcyclohexane 1.3 4.4 0.88 ug/kg j 75-09-2 Methylene chloride ND 8.8 3.5 ug/kg 78-93-3 Methyl ethyl ketone ND 22 6.6 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 4.4 0.88 ug/kg 91-20-3 Naphthalene 14.314.4 1.8 ug/kg 103-65-1 n-Propylbenzene 12.9 4.4 0.88 ug/kg 100-42-5 Styrene ND 4.4 0.88 ug/kg 71-55-6 1,1,1-Trichloroethane ND 4.4 0.88 ug/kg 79-34-5 1, 1, 2,2-Tetrachloroethane ND 4.4 1.2 ug/kg 79-00-5 1, 1, 2-Trichloroeth ane NO, 4.4 1.4 ug/kg 120-82-1 1,2,4-Trichlornbenzene ND 4.4 1.0 ug/kg 95-63-6 1,2,4-Trimethylbenzene 64.7 4.4 0.88 ug/kg 108-67-8 1,3,5-Trimethylbenzene 17.6 4.4 0.88 ug/kg 127-18-4 Tetrachloroethylene ND 4.4 1.1 ug/kg 108-88-3 Toluene 7.5 4.4 0.88 ug/kg 79-01-6 Trichloroethylene ND 4.4 0.90 ug/kg 75-69-4 Trichlorofluoromethane ND 4.4 0.88 ug/kg 75-01-4 Vinyl chloride ND 4.4 0.90 ug/kg 1330-20-7 Xylene (total) 41.2 13 2.3 ug/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 1868-53-7 Dibromofluoromethane 94% 10996 75-124% 2037-26-5 Toluene-D8 929/6 93% 75-126% 460-00-4 4-Bmmofluorobenzene 116% : 110% 71-133% 17060-07-0 1,2-Dichloroethane-D4 105% 106% 72-135% (a) Confirmation run for internal standard areas. (b) Associated BS recovery outside control limits Page 2 of 2 y ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound U ffi® 40 of 90 a ACCUTE8T, FAt9709 Accutest Laboratories Report of Analysis Page 1 of 2 it Sample ID: CS-5-10' Sample ID: FA19708-7 Date Sampled: 11/04/14 •ix: SO - Soil Date Received: 11/05/14 iod: SW846 8270D SW846 3550C Percent Solids: 85.3 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #1a T015328.1) 5 11/07/14 NJ 11/05/14 OP53802 ST717 #2 Run #1 Run #2 Initial Weight Final Volume 30.2 g 1.0 ml ABN Special List CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 4900 970 ug/kg 95-57-8 2-Chlorophenol ND 970 97 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 970 97 ug/kg 120-83-2 2,4-Dichlorophenol ND 970 100 ug/kg 105-67-9 2,4-Dimethylphenol NO 970 110 ug/kg 51-28-5 2,4-Dinitrophenol ND 4900 970 ug/kg 534-52-1 4,6-Dinitro-o-cresol NID 1900 390 ug/kg 95-48-7 2-Methylphenol ND 970 97 ug/kg 3&4-Methylphenol ND 970 190 ug/kg 88-75-5 2-Nitrophenol ND 970 97 ug/kg 100-02-7 4-Nitrophenol ND 4900 780 ug/kg 87-86-5 Pentachlorophenol ND 4900 780 ug/kg 108-95-2 Phenol ND 970 97 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 970 97 ug/kg 83-32-9 Acenaphthene 342 970 120 ug/kg J 208-96-8 Acenaphthylene 117 970 97 ug/kg J 120-12-7 Anthracene ND 970 97 ug/kg 56-55-3 Benzo(a)anlhracene I ND 970 97 ug/kg 50-32-8 Benzo(a)pyrene ND 970 97 ug/kg 205-99-2 Benzo(b)fluoranthene NU 970 97 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 970 97 ug/kg 207-08-9 Benzo(k)fluoranthene ND 970 110 ug/kg 101-55-3 4-Bromophenyl phenyl ether ND 970 97 ug/kg 85-68-7 Butyl benzyl phthalate ND 970 190 ug/kg 91-58-7 2-Chloronaphthalene ND 970 120 ug/kg 106-47-8 4-Chloroan line ND 970 97 ug/kg 218-01-9 Chrysene ND 970 97 ug/kg 111-91-1 bis(2-Cbloroethoxy)methane ND 970 97 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 970 97 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 970 100 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 970 140 ug/kg 121-14-2 2,4-Dinitrotoluene ND 970 110 ug/kg ND = Not detected MDL = Method Detection Limit j = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound m® 41 of 90 ACCUTEST. FAI9708 Accutest Laboratories Report of Analysis :lient Sample ID: CS-5-10' .ab Sample ID: FA19708-7 Date Sampled: 11/04/14 4atrix: SO - Soil Date Received: 11/05/14 4thod: SW846 8270D SW846 3550C Percent Solids: 85.3 reject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ABN Special List CAS No. Compound Result RL MDL Units Q 606-20-2 2,6-Dinitrotoluene ND_,_ < 970 110 ug/kg 91-94-1 3,T-Dichloroben7idine ND 970 97 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 970 97 ug/kg 132-64-9 Dibenzofuran 140 970 97 ug/kg J 84-74-2 Di-n-butyl phthalate ND 1900 190 ug/kg 117-84-0 Di-n-octyl phthalate ND 970 190 ug/kg 84-66-2 Diethyl phthalate ND 1900 190 ug/kg 131-11-3 Dimethyl phthalate ND 970 190 ug/kg 117-81-7 bis(2-Ethythexyl)phthalate ND 1900 190 ug/kg 206-44-0 Fluoranthene ND 970 97 ug/kg 86-73-7 Flumene 623 970 97 ug/kg J 118-74-1 Hexachlorobenzene ND 970 97 ug/kg 87-68-3 Hexachlorobutadiene ND 970 97 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 970 97 ug/kg 67-72-1 Hexachloroethane ND 970 97 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 970 97 ug/kg 78-59-1 Isophorone ND 970 97 ug/kg 90-12-0 1-Methylnaphthalene 3900 ;970 97 ug/kg 91-57-6 2-Methylnaphthalene 5550 970 97 ug/kg 91-20-3 Naphthalene 1500 970 97 ug/kg 98-95-3 Nitrobenzene ND 970 97 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 970 97 ug/kg 86-30-6 N-Nitrosodiphenylamtne ND 970 97 ug/kg 85-01-8 Phenanthrene 957 970 97 ug/kg J 129-00-0 Pyrene 373 970 97 ug/kg J CAS No. Surrogate Recoveries Run# I Run# 2 Limits 367-12-4 2-Fluorophenol 79% 40-102% 4165-62-2 Phenol-d5 92% 41-100% 118-79-6 2,4,6-Tribromophenol 77% 42-108% 4165-60-0 Nitrobenzene-d5 97% 40-105% 321-60-8 2-Fluorobiphenyl 81% 43-107% 1718-51-0 Terphenyl-d14 88% 45-119% (a) Dilution required due to matrix interference. Page 2 of 2 y ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound r so 42 of 90 w ACCUTEST. FA19700 Acculest Laboratories Report of Analysis Page I of 1 nt Sample ID: CS-5-10' Sample ID: FA19708-7 Date Sampled: 11/04/14 rix: SO - Soil Date Received: 11/05/14 hod: MADEP VPH REV 1.1 Percent Solids: 85.3 ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch #I UV066529.1) 1 I1/05/14 AH n/a n/a GUV3537 #2 UV066546.1) 10 11/06/14 AH n/a n/a GUV3538 Initial Weight Final Volume Methanol Aliquot :un 01 6.07 g - 5.1 ml 10.0 at :un #2 6.07 g 5.1 ml 50.0 ul MADEP VPH List CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 580 580 ug/kg 100-41-4 Ethylbenzene 599 1200 580 ug/kg J 1634-04-4 Methyl Tert Butyl Ether ND 1200 580 ug/kg 91-20-3 Naphthalene 9960 2900 1700 ug/kg 108-88-3 Toluene NO 1200 580 ug/kg m,p-Xylene 1610 2300 1200 ug/kg J 95-47-6 o-Xylene 3920 1200 580 ug/kg C5- C8 ABphatics (Unadj.) ND 58000 20000 ug/kg C9- C12 Aliphatics (Unadj.) NO 58000 20000 ug/kg C9- C10 Aromatics (Unadj.) 3570010 a ! 120000 41000 ug/kg C5- C8 Atiphatics ND 58000 20000 ug/kg C9- C12 Aliphatics ND 58000 20000 ug/kg C9- C10 Aromatics 3570000 120000 41000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 BFB 184%e 0%b 70-130% 460-00-4 BFB 198%c '0%b 70-130% (a) Result is from Run# 2 (b) Outside control limits due to dilution. (c) Outside control limits due to matrix interference. NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound M® 43 of 90 M.4CCUTEST. FAM08 Accutest Laboratories Report of Analysis Page I of I Client Sample ID: CS-5-10' Lab Sample ID: FA19708-7 Date Sampled: 11/04/14 Matrix: SO - Soil Date Received: 11/05/14 Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 85.3 Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 NN010954.D 5 11/13/14 NAF I1/06/14 OP53815 GNN481 Run #2 Initial Weight Final Volume un#1 19.7g 2.0ml (in #2 MAEPH List CAS No. Compound Result RL MDL Units Q 83-32-9 Acenaphthene 1440 1200 600 ug/kg 208-96-8 Acenaphthylene ND 1200 600 ug/kg 120-12-7 Anthracene ND 1200 600 ug/kg 56-55-3 Benzo(a)anthracene ND 1200 600 ug/kg 50-32-8 Benzo(a)pyrene ND 1200 600 ug/kg 205-99-2 Benzo(b)fluoranthene ND 1200 600 ug/kg 191-24-2 Benzo(g,h,i)perylene NO 1200 600 ug/kg 207-08-9 Benzo(k)fluoranthene ND 1200 600 ug/kg 218-01-9 Chrysene ND 1200 600 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 1200 600 ug/kg 206-99-0 Fluoranthene ND _ 1200 600 ug/kg 86-73-7 Flumene 903 ' 1200 600 ug/kg J 193-39-5 Indeno(1,2,3-cd)pyrene 101 1200 600 ug/kg 91-57-6 2-Methylnaphthalene 5580 ', 1200 600 ug/kg 91-20-3 Naphthalene 744 1200 600 ug/kg J 85-01-8 Phenanthrene 601 1200 600 ug/kg J 129-00-0 Pyrene ND 1200 600 ug/kg Cl l-C22 Aromatics (Unadj.) 348000: ,1,60000 45000 ug/kg Cll-C22 Aromatics 338006 _60000 45000 ug/kg C9-C18 Atiphatics 615000 60000 30000 ug/kg C19-C36 Aliphatics 1630001 60000 30000 ug/kg CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 80% 40-140% 580-13-2 2-Bromonaphthalene 181%a' 40-140% 84-15-1 o-Terphenyl 113% 40-140% 321-60-8 2-Fluorobiphenyl 128% , 40-140% (a) Outside control limits due to matrix interference NO = Not detected MDL = Method Detection Limit J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound MM 44 of 90 M ACCU-rEET. FAIG70e Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Section 4 o® 45 of 90 W ACCUTEST. W9709 ""'•" """" ONE ONE .• © ■■®■■i■[l,'l■1�■■■�1■■i�■tom■■■■■■■■■� ■ FA19708: Chain of Custody Page 1 of 4 J Ei 46 of 90 N ACCUTEST. FAi9709 :•'•"••"�:" ACCUTEEST LABORATORIES SAMPLE RECEIPT CONFIRMATION ACCUTESTSJOB NUMBER:1- 7AQ__/CLIENT: PROJECT: DATE/TIME RECRIVEU: I-O S'!'I Q 30(MM/DDNY 2a:00) NUMBER OF COOLERS RECEIVED: 1 METHOD OFDELIVERY: FEBEX UPS AC EST COURIER DELIVERY OTHER:__ AIRBILL NUMBERS: Ao53 1Z2) Sylo COOLER INFORMATION TEMPERATURE INFORMATION CUSTODYSEAL NOTPRESENTORNOTINTACT I CORR. FACTOR 4O.y_ CHAIN OF CUSTODY NOT RECEIVED (COC) PIRTHIRMID OBSERVED TEMPS: 2.6 ANALYSIS REQUESTED IS UNCLEAR OR MISSING CORRECTED TEMPS: 34 SAMPLE DATES OR TIMES UNCLEAR OR MISSING SAMPLE INFORMATION TEMPERATURE CRITERIA NOT MET IINCORRECr NUMBER OF CONTAINERS USED TRIP BLANK INFORMATION TRIP BLANK PROVIDED. TRIP BLANK NOT PROVIDED TRIP BLANK NOT 016 COC TRIP BLANK INTACT TRIP BLANK NOT INTACT RECEIVED WATER TRIP BLANK RECEIVED SOIL TRIP BLANK MISC. INFORMATION NUMBEROF ENCORES? PS-GRpM_ 5-GRAM NUMBEROF5035FMLDIOTS7 NUMBER OF LAB FILTERED METALS 7 pII PAPER LOT#s WIDE RANGFL_ A036122 SUMMARY OF COMMENTS: SAMPLE RECEIVED IMPROPERLY PRESERVED INSUFFICIENT VOLUME FOR ANALYSIS DATESITIMES ON CDC DO NOT MATCH SAMPLE LABEL ID'S ON COC DO NOT MATCH LABEL VOC VIALS HAVE HEADSPACE (MACRO BUBBLES) BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED NO BOTTLES RECEIVED FOR ANALYSIS REQUESTED UNCLEAR FILTERING OR COMPOS1TING INSTRUCTIONS SAMPLE CONTAINER(S) RECEIVED BROKEN 5035 FIELD KITS NOT RECEIVED WITHIN 4E HOURS BULK VOA SOIL JARS NOT RECEIVED WITHIN 48 HOURS SOLIDS JAR NOT RECEIVED RESIDUAL CHLORINE PRESENT LOT#_ 14-860 (APP-11LETO EPA 600 MRIE50RNORTII CAROLINA ORGA.41L5) NARROW RANGE_ HC421754 OTHER(spmify) 405-230010 TECHNICIAN SIGNATURE/DATE. LOS-IY /D _ EVIEWERSIGNATUREATE l-S -Iq NF 10/14 receipt confi0na0on 702914.EIS PA19708: Chain of Custody Page 2 of 4 ME 47 of 90 N ACC UTEST, FA19709 W.a N� 9 Z ¢ NJ 3 LL cc N I m 'e o ® RUN FA19708: Chain of Custody Page 3 of 4 No 48 of 90 ACCUTEST. FA19700 Job Change Order: FA19708_11/21/2014 Requested Dale: 112112014 Received Date: 11/62014 Account Name: GRI (Geological Resources Inc.) Due Date: 11/10/2014 Project The Rock Worship Center. 1113 Fordham Rd, Deliverable: COMMB CSR MMO TAT (Days): 7 Sample#: Change: Per client request report l-methylnaphthalene. FAI9708 3. 4, 5, 6, 7 Above Changes Per: Johanna Teschner Date: 11/212014 f•A19708: Chain of Custody Page 4 of 4 To CI'ent The Charge Order is confirmation of the redsio previously discussed vdlh the Aocul-t Client Service Page 1 of 1 0 GUMS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Section 5 H of 50 of 90 a�ACCU-r9Es9N� GCUTEST. FA19708 """" °° FA19708 Method Blank Summary Page 1 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC 'ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch rY747-MB Y16986.D 1 11/05/14 AD n/a n/a VY747 The QC reported here applies to the following samples: Method: SW846 8260B FA19708-3, FA19708-4, FA19708-5, FA19708-6 CAS No. Compound Result RL MDL Units Q 67-64-1 Acetone ND 50 15 ug/kg 71-43-2 Benzene ND 5.0 1.0 ug/kg 75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg 75-25-2 Bromoform NO 5.0 1.1 ug/kg 104-51-8 o-Butylbenzene ND 5.0 1.0 ug/kg 108-90-7 Chlorobenzene ND > 5.0 1.0 ug/kg 75-00-3 Chloroethane ND 5.0 2.3 ug/kg 67-66-3 Chloroform ND 5.0 1.1 ug/kg 75-15-0 Carbon disulfide ND 5.0 1.0 ug/kg 56-23-5 Carbon tetrachloride ND 5.0 1.4 ug/kg 110-82-7 Cyclohexane ND 5.0 1.1 ug/kg 75-34-3 1,1-Dichloroethane ND 5.0 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 2.1 ug/kg 106-93-4 1,2-Dibromoethane ND 5.0 1.8 ug/kg 107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg 124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 5.0 1.3 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropee ND 5.0 1.0 ug/kg 541-73-1 m-Dichlorobenzene ND 5.0 1.0 ug/kg 95-50-1 o-Dichlorobenzene ND 5.0 1.0 ug/kg 106-46-7 p-Dichlorobenzene ND 5.0 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.3 ug/kg 10061-02-6 trans-1,3-Dichloropropee ND 5.0 1.0 ug/kg 100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg 591-78-6 2-Hexanone ND 25 4.9 ug/kg 98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg 108-10-1 4-Methyl-2-pentanone ND 25 5.0 ug/kg 79-20-9 Methyl acetate DW 25 5.0 ug/kg 74-83-9 Methyl bromide ND 5.0 1.9 ug/kg 74-87-3 Methyl chloride ND 5.0 2.0 ug/kg 108-87-2 Methylcyclohexane ND 5.0 1.0 ug/kg 75-09-2 Methylene chloride ND 10 4.0 ug/kg 78-93-3 Methyl ethyl ketone ND 25 7.5 ug/kg F ffin 51 of 90 M ACCUTE8T. FA19708 Method Blank Summary Page 2 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC 'ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl /Y747-MB Y16986.1) 1 11/05/14 AD n/a n/a VY747 The QC reported here applies to the following samples: Method: SW846 8260B FA19708-3, FA19708-4, FA19708-5, FA19708-6 CAS No. Compound Result RL MDL Units Q 1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg 100-42-5 Styrene ND 5.0 1.0 ug/kg 71-55-6 1, 1, 1 -Trichloroethane ND 5.0 1.0 ug/kg 79-34-5 1, 1, 2,2-Tetrachloroethane ND 5.0 1.4 ug/kg 79-00-5 1, 1, 2-Trichloroethane ND 5.0 1.6 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.2 ug/kg 95-63-6 1, 2,4 -Tri methylbenzene ND 5.0 1.0 ug/kg 108-67-8 1, 3,5 -Trimethylbenzene IND 5.0 1.0 ug/kg 127-I8-4 Tetrachloroethylene ND 5.0 1.3 ug/kg 108-88-3 Toluene ND 5.0 1.0 ug/kg 79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg 75-69-4 Trichurofluoromethane ND 5.0 1.0 ug/kg 75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg 1330-20-7 Xylene (total) ND 15 2.7 ug/kg CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 108% 75-124% 2037-26-5 Toluene-D8 104% 75-126% 460-00-4 4-Bromofluorobenzene 109% 71-133% 17060-07-0 1,2-Dichloroethane-D4 102% 72-135% Ful M® 52 of 90 E ACCUTEST, FA19r99 •••: •••"�• Method Blank Summary Page 1 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl rF2291-MB F0067009.1) 1 11/06/14 AD n/a n/a VF2291 The QC reported here applies to the following samples: FA19708-6, FA19708-7 CAS No. Compound 67-64-1 Acetone 71-43-2 Benzene 75-27-4 Bromodichloromethane 75-25-2 Bromoform 104-51-8 n-Butylbenzene 108-90-7 Chlorobenzene 75-00-3 Chloroelhane 67-66-3 Chloroform 75-15-0 Carbon disulfide 56-23-5 Carbon tetrachloride 110-82-7 Cyclohexane 75-34-3 1,1-Dichloroethane 75-35-4 1,1-Dichloroethylene 96-12-8 1, 2-Dibromo-3-chloropropane 106-93-4 1, 2-Dibromoethane 107-06-2 1,2-Dichloroethane 78-87-5 1,2-Dichloropropane 124-48-1 Dibromochloromethane 75-71-8 Dichlorodifluoromethane 156-59-2 cis-1,2-Dichloroethylene 10061-01-5 cis-1,3-Dichloropropene 541-73-1 m-Dichlorobenzene 95-50-1 o-Dichlorobenzene 106-46-7 p-Dichlorobenzene 156-60-5 trans- 1, 2-Dichloroethylene 10061-02-6 trans -1,3-Dichloropropene 100-41-4 Ethylbenzene 591-78-6 2-Hexanone 98-82-8 Isopropylbenzene 108-10-1 4-Methyl-2-pentanone 79-20-9 Methyl acetate 74-83-9 Methyl bromide 74-87-3 Methyl chloride 108-87-2 Methylcyclohexane 75-09-2 Methylene chloride 78-93-3 Methyl ethyl ketone Result RL MDL Method: SW846 8260B Units Q ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg No 53 of 90 � ACC UTEST. FAI9708 Method Blank Summary Page 2 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl T2291-MB F0067009.D 1 11/06/14 AD n/a n/a VF2291 The QC reported here applies to the following samples: Method: SW846 8260B FA19708-6, FA19708-7 CAS No. Compound Result RL MDL Units Q 1634-04-4 Methyl Tert Butyl Ether ND::-5.0 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 2.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg 100-42-5 Styrene ND 5.0 1.0 ug/kg 71-55-6 1, 1, 1 -Trichloroethane ND 5.0 1.0 ug/kg 79-34-5 1, 1, 2,2-Tetrachloroethane ND_ 5.0 1.4 ug/kg 79-00-5 1, 1, 2-Trichloroethane NJ> 5.0 1.6 ug/kg 120-82-1 1, 2,4 -Trichlorobenzene __ 140 45.0 1.2 ug/kg 95-63-6 1,2,4-Trimethylbenzene PO 5.0 1.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 15.0 1.3 ug/kg 108-88-3 Toluene ND 5.0 1.0 ug/kg 79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 5.0 1.0 ug/kg 75-01-4 Vinyl chloride ND 5.0 1.0 ug/kg 1330-20-7 Xylene (total) 'ND 15 2.7 ug/kg CAS No. Surrogate Recoveries Limits 1868-53-7 Dibromofluoromethane 91% 75-124% 2037-26-5 Toluene-D8 95% _ 75-126% 460-00-4 4-Bromofluorobenzene 113% 71-133% 17060-07-0 1,2-Dichloroethane-D4 966 72-135% me 54 of 90 w ACCUTEST. FAi9708 Blank Spike Summary Page 1 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC !ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl lY747-BS Y16985.1) 1 11/05/14 AD n/a n/a VY747 The QC reported here applies to the following samples: FAI9708-3, FA19708-4, FA19708-5, FA19708-6 Spike BSP BSP CAS No. Compound ug/kg ug/kg % 67-64-1 Acetone 250 237 95 71-43-2 Benzene 50 51.4 103'. 75-27-4 Bromodichloromethane 50 50.7 101 75-25-2 Bromoform 50 50.5 101 104-51-8 n-Butylbenzene 50 50.0 1001 108-90-7 Chlorobenzene 50 55.3 I111 75-00-3 Chloroethane 50 54.9 110' 67-66-3 Chloroform 50 50.3 101 75-15-0 Carbon disulfide 50 57.4 115 56-23-5 Carbon tetrachloride 50 52.6 105 110-82-7 Cyclohexane 50 49.5 99 75-34-3 1,1-Dichioroethane 50 50.0 100 75-35-4 1,1-Dichloroethylene 50 48.8 98 :. 96-12-8 1,2-Dibromo-3-chloropropane 50 44.4 99 106-93-4 1,2-Dibromoethane 50 52.4 105' 107-06-2 1,2-Dichloroethane 50 47.0 94 78-87-5 1,2-Dichloropropane 50 49.8 100 ! 124-48-1 Dibromochloromethane 50 52.1 104' 75-71-8 Dichlorodifluoromethane 50 61.7 1231: 156-59-2 cis-1,2-Dichloroethylene 50 51.7 103 10061-01-5 cis-1,3-Dichloropropee 50 50.5 101 541-73-1 m-Dichlorobenzene 50 57.1 114 95-50-1 o-Dichlorobenzene 50 56.6 11V 106-46-7 p-Dichlorobenzene 50 51.7 103 156-60-5 trans-1,2-Dichloroethylene 50 49.5 99 10061-02-6 trans- 1,3-Dichloropropee 50 53.4 107 100-41-4 Ettylbenzene 50 51.7 103 591-78-6 2-Hexanone 250 221 88" 98-82-8 Isopropylbenzene 50 57.0 114i1 108-10-1 4-Methyl-2-pentanone 250 220 88 79-20-9 Methyl acetate 250 269 108i 74-83-9 Methyl bromide 50 54.4 109 74-87-3 Methyl chloride 50 55.5 Ill i 108-87-2 Methylcyclohexane 50 52.1 104 75-09-2 Methylene chloride 50 51.9 104 78-93-3 Methyl ethyl ketone 250 222 89; . = Outside of Control Limits. Limits 61-152 76-126 74-130 76-127 71-128 81-129 68-133 72-123 72-122 78-133 73-126 73-125 81-136 70-137 77-126 74-128 74-125 76-127 68-168 74-126 80-123 81-129 80-129 76-130 70-127 75-131 77-123 72-133 80-136 76-132 67-137 65-139 71-144 75-128 74-137 75-137 Method: SW846 8260B ffin 55 of 90 E ACCUTEST. FA19708 Blank Spike Summary Page 2 of 2 Job Number: FA19708 Account: GRiNCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl FY747-BS Y16985.D 1 11/05/14 AD n/a n/a VY747 The QC reported here applies to the following samples: Method: SW846 8260B FA19708-3, FA19708-4, FA19708-5, FA19708-6 CAS No. Compound 1634-04-4 Methyl Tert Butyl Ether 91-20-3 Naphthalene 103-65-1 n-Propylbenzene 100-42-5 Styrene 71-55-6 1, 1, 1 -Trichloroethane 79-34-5 1, 1, 2,2 -Tetrachloroethane 79-00-5 1, 1, 2-Trichloroethane 120-82-1 1, 2,4 -Trichlorobenzene 95-63-6 1, 2 A-Trimethylbenzene 108-67-8 1,3,5-Trimethylbenzene 127-18-4 Tetrachloroethylene 108-88-3 Toluene 79-01-6 Trichloroethylene 75-69-4 Trichlorofluoromethane 75-01-4 Vinyl chloride 1330-20-7 Xylene (total) CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 2037-26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 = Outside of Control Limits. Spike BSP BSP ug/kg ug/kg % Limits 50 47.7 -:95 77-120 50 43.7 87 79-129 50 54.1 108 80-135 50 53.3 101 78-125 50 50.6 101 70-129 50 46.8 94 71-126 50 48.5 97 74-124 50 53.5 107 < 78-130 50 51.1 102 74-123 50 50.3 101 € 73-122 50 58.7 117 4 79-130 50 51.1 102 '4 76-124 50 52.1 104 75-128 50 57.3 115 73-145 50 53.0 106 : 76-141 150 163 109 80-129 BSP Limits 105% 'r 75-124% 104% 75-126% 106% 71-133% 90%_ 72-135% Mn 56 of 90 w ACCUTEST. FA19708 Blank Spike Summary Page 1 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch T2291-BS F0067008.D 1 11/06/14 AD n/a n/a VF2291 The QC reported here applies to the following samples: FA19708-6, FA19708-7 Spike BSP BSP CAS No. Compound ug/kg ug/kg % 67-64-1 Acetone 250 333 133 71-43-2 Benzene 50 56.4 113 75-27-4 Bromodichloromethane 50 58.1 116 75-25-2 Bromoform 50 48.2 96, 104-51-8 n-Butylbenzene 50 56.7 113 108-90-7 Chlorobenzene 50 59.9 120 75-00-3 Chloroethane 50 63.9 128 67-66-3 Chloroform 50 55.6 Ill 75-15-0 Carbon disulfide 50 70.6 1411 56-23-5 Carbon tetrachloride 50 54.4 109 110-82-7 Cyclohexane 50 51.3 103 75-34-3 1,1-Dichloroethane 50 55.7 111 75-35-4 1,1-Dichloroethylene 50 55.7 111 96-12-8 1,2-Dibromo-3-chloropropane 50 60.5 121 106-93-4 1,2-Dibromoethane 50 57.7 115 107-06-2 1,2-Dichloroethane 50 56.7 113` 78-87-5 1,2-Dichloropropane 50 56.6 113 124-48-1 Dibromochloromethane 50 59.8 120' 75-71-8 Dichlorodifluoromethane 50 50.1 100 156-59-2 cis-1,2-Dichloroethylene 50 55.9 I'm 10061-01-5 cis-1,3-Dichloropropene 50 56.9 114 541-73-1 m-Dichlorobenzene 50 59.4 119 95-50-1 o-Dichlorobenzene 50 62.9 126 106-46-7 p-Dichlorobenzene 50 57.0 114 156-60-5 trans-1,2-Dichloroethylene 50 55.4 °Ill 10061-02-6 trans-1,3-Dichloropropene 50 58.7 117 100-41-4 Euhylbenzene 50 56.9 114 591-78-6 2-Hexanone 250 285 114'' 98-82-8 Isopropylbenzene 50 60.7 121 108-10-1 4-Methyl-2-pentanone 250 296 118 79-20-9 Methyl acetate 250 339 136 74-83-9 Methyl bromide 50 56.8 114r 74-87-3 Methyl chloride 50 50.6 101' 108-87-2 Methylcyclohexane 50 53.7 107 75-09-2 Methylene chloride 50 57.5 115 78-93-3 Methyl ethyl ketone 250 281 112, Outside of Control Limits. Limits 61-152 76-126 74-130 76-127 71-128 81-129 68-133 72-123 72-122 78-133 73-126 73-125 81-136 70-137 77-126 74-128 74-125 76-127 68-168 74-126 80-123 81-129 80-129 76-130 70-127 75-131 77-123 72-133 80-136 76-132 67-137 65-139 71-144 75-128 74-137 75-137 Method: SW846 8260B s® 57 of 90 ACCUTEST. FA19708 Blank Spike Summary Page 2 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl tF2291-BS F0067008.1) 1 11/06/14 AD n/a n/a VF2291 The QC reported here applies to the following samples: Method: SW846 8260B FAI9708-6, FA19708-7 CAS No. Compound 1634-04-4 Methyl Tert Butyl Ether 91-20-3 Naphthalene 103-65-1 n-Propylbenzene 100-42-5 Styrene 71-55-6 1. 1. 1 -Trichloroethane 79-34-5 1, 1, 2,2-Tetrachloroethane 79-00-5 1. 1, 2-Trich uro ethane 120-82-1 1,2,4-Trichlorobenzene 95-63-6 1,2,4-Trimethylbenzene 108-67-8 1,3,5-Trimethylbenzene 127-18-4 Tetrachloroethylene 108-88-3 Toluene 79-01-6 Trichloroethylene 75-69-4 Trichlorofluoromethane 75-01-4 Vinyl chloride 1330-20-7 Xylene (total) CAS No. Surrogate Recoveries 1868-53-7 Dibromofluoromethane 2037-26-5 Toluene-D8 460-00-4 4-Bromofluorobenzene 17060-07-0 1,2-Dichloroethane-D4 = Outside of Control Limits. Spike BSP BSP ug/kg ug/kg % Limits 50 54.3 109 77-120 50 60.4 121 79-129 50 62.9 126 80-135 50 56.1 112 < 78-125 50 55.3 111_ 70-129 50 58.8 118 71-126 50 55.3 111__` 74-124 50 60.3 121 78-130 50 58.2 116 r' 74-123 50 57.7 115 73-122 50 57.1 114 79-130 50 55.4 111 76-124 50 56.7 113 75-128 50 56.5 113 73-145 50 51.3 103 76-141 150 179 119 80-129 BSP Limits 92% _ 75-124% W6 75-126% 111% $1 71-133% ,88%_ ;;; 72-135% Em 58 of 90 U ACCUTEST. FAI9708 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ;ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch A19680-3MS Y16993.D I 11/05/14 AD n/a n/a VY747 A19680-3MSD Y16994.D 1 11/05/14 AD n/a n/a VY747 'A19680-3 Y16992.1) 1 11/05/14 AD n/a n/a VY747 The QC reported here applies to the following samples: FA19708-3, FA19708-4, FA19708-5, FA19708-6 FA19680-3 Spike MS CAS No. Compound ug/kg Q ug/kg ug/kg 67-64-1 Acetone 29.2 J 392 351 71-43-2 Benzene ND 78.3 74.2 75-27-4 Bromodichloromethane NO 78.3 72.8 75-25-2 Bromoform ND 78.3 73.5 104-51-8 n-Butylbenzene ND 78.3 73.2 108-90-7 Chlorobenzene ND 78.3 78.9 75-00-3 Chloroethane NO 78.3 82.6 67-66-3 Chloroform ND 78.3 73.2 75-15-0 Carbon disulfide 1.4 J 78.3 71.7 56-23-5 Carbon tetrachloride ND 78.3 72.9 110-82-7 Cyclohexane ND 78.3 68.6 75-34-3 1,1-Dichloroethane ND 78.3 72.2 75-35-4 1,1-Dichloroethylene NO 78.3 65.5 96-12-8 1,2-Dibromo-3-chloropropane ND 78.3 64.8 106-93-4 1,2-Dibromoethane ND 78.3 74.0 107-06-2 1,2-Dichloroethane ND 78.3 69.9 78-87-5 1,2-Dichloropropane NO 78.3 73.7 124-48-1 Dibromochloromethane ND 78.3 74.0 75-71-8 Dichlorodifluoromethane ND 78.3 80.4 156-59-2 cis- 1, 2-Dichloroethylene NO 78.3 73.1 10061-01-5 cis- 1, 3-Dichloropropene ND 78.3 73.6 541-73-1 m-Dichlorobenzene ND 78.3 82.2 95-50-1 o-Dichlorobenzene ND 78.3 80.3 106-46-7 p-Dichlorobenzene ND 78.3 74.9 156-60-5 trans -1,2-Dichloroethylene ND 78.3 71.0 10061-02-6 trans-1,3-Dichloropropene NO 78.3 77.3 100-41-4 Ethylbenzene NO 78.3 72.9 591-78-6 2-Hexanone NO 392 331 98-82-8 Isopropylbenzene ND 78.3 80.2 108-10-1 4-Methyl-2-pentanone ND 392 338 79-20-9 Methyl acetate NO 392 403 74-83-9 Methyl bromide ND 78.3 80.7 74-87-3 Methyl chloride NO 78.3 80.1 108-87-2 Methylcyclohexane NO 78.3 67.3 75-09-2 Methylene chloride NO 78.3 81.7 78-93-3 Methyl ethyl ketone ND 392 333 = Outside of Control Limits. Method: SW846 8260B MS Spike MSD MSD Limits % ug/kg ug/kg % RPD Rec/RPD 358 90 2 61-152/27 67.4 92 10 76-126/26 68.2 93 7 74-130/25 69.8 96 5 76-127/26 64.2 88 :' 13 71-128/35 70.9 97 11 81-129/29 57.6 79 " 36* 68-133/29 66.6 91 9 72-123/26 74.1 1003 - 72-122/29 64.7 89 12 78-133/29 60.5 83 131,73-126/32 65.3 89 10 73-125/27 62.2 95 s 5 81-136/28 63.8 87 2 70-137/29 68.0 93 8 77-126/26 65.4 90 7 74-128/23 67.5 92 ;' 9 74-125/25 68.4 94 8 76-127/27 74.4 162 8 > 68-168/29 68.3 94 7 74-126/26 68.5 94 7 80-123/26 73.2 10012 81-129/33 74.6 102' 7 80-129/32 67.7 93 ; 10 76-130/32 65.8 00_;_.. 8 70-127/27 69.4 95 11 75-131/28 65.0 89 11 77-123/31 323 88 272-133/26 71.2 98 12 80-136/32 328 90 " 3 _ 76-132/26 396 108' 2 -: 67-137/30 69.6 95 1$ 65-139/31 71.9 98 11 71-144/27 60.1 82 ` 41 75-128/31 75.6 104 8 74-137/28 330 90 1 75-137/25 on 59 of 90 0 ACClJTEBT• Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ;ample File ID OF Analyzed By Prep Date Prep Batch Analytical Batch iA19680-3MS Y16993.D 1 11/05/14 AD n/a n/a VY747 iA19680-3MSD Y16994.1) 1 11/05/14 AD n/a n/a VY747 ,A19680-3 Y16992.1) 1 I1/05/14 AD n/a n/a VY747 The QC reported here applies to the following samples: Method: SW846 8260B FA19708-3, FA19708-4, FA19708-5, FA19708-6 FA19680-3 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD 1634-04-4 Methyl Tert Butyl Ether ND 78.3 70.7 90 73 68.2 93 4 77-120/24 91-20-3 Naphthalene ND 78.3 70.0 89 73 67.9 93 3; 79-129/33 103-65-1 n-Propylbenzene ND 78.3 76.8 98 73 68.1 93 12 80-135/33 100-42-5 Styrene ND 78.3 77.8 99 73 69.4 95 11 78-125/30 71-55-6 1, 1, 1 -Trichloroethane ND 78.3 74.2 95 73 64.4 88 14 70-129/27 79-34-5 1, 1, 2,2-Tetrachloroethane ND 78.3 70.5 90 73 67.3 92 5: 71-126/30 79-00-5 1, 1, 2 -Trichloroethane NO 78.3 72.2 92 73 66.0 90 9 74-124/28 120-82-1 1, 2A -Trichlorobenzene ND 78.3 82.6 105 73 76.0 104 8 78-130/34 95-63-6 1,2A-Trimethylbenzene ND 78.3 74.2 95 73 66.2 91 111 74-123/34 108-67-8 1,3,5-Trimethylbenzene ND 78.3 72.1 92 73 64.5 88 11 73-122/33 127-18-4 Tetrachloroethylene NO 78.3 74.6 95 73 65.5 90 13 79-130/31 108-88-3 Toluene ND 78.3 72.5 93 73 64.8 89 11 76-124/30 79-01-6 Trichloroethylene NO 78.3 72.4 92 73 66.6 91 8' 75-128/27 75-69-4 Trichlorofluoromethane ND 78.3 77.9 99 73 70.6 97 10 73-145/31 75-01-4 Vinyl chloride ND 78.3 77.4 99 73 69.7 95 10 76-141/27 1330-20-7 Xylene (total) ND 235 231 98 219 206 94 11 80-129/30 CAS No. Surrogate Recoveries MS MSD FA19680-3 Limits 1868-53-7 Dibromofluoromethane 104% : 107% 108%' 75-124% 2037-26-5 Toluene-D8 102% 101% 100%s' 75-126% 460-00-4 4-Bromofluorobenzene 104% 104% 109%I' 71-133% 17060-07-0 1,2-Dichloroethane-D4 92% 94% 112%: 72-135% * = Outside of Control Limits. Mn 60 of 90 U ACCIJTEST. FA19708 Matrix Spike/Matrix Spike Duplicate Summary Page I of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ;ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch A19708-6MS F0067012.D 1 11/06/14 AD n/a n/a VF2291 ?A19708-61VISD F0067013.D 1 11/06/14 AD n/a n/a VF2291 ;A19708-6 F0067011.D 1 11/06/14 AD n/a n/a VF2291 The QC reported here applies to the following samples: Method: SW846 8260B FA19708-6, FA19708-7 FA19708-6 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD 67-64-1 Acetone NO 181000 231000 128 181000 210000 116 10 " 61-152/27 71-43-2 Benzene 739 J 36200 37400 101 36200 38400 104> 3 76-126/26 75-27-4 Bromodichloromethane ND 36200 38100 105 36200 39700 110 4 74-130/25 75-25-2 Bromoform NO 36200 34300 95 36200 36600 101' 6 76-127/26 104-51-8 n-Butylbenzene 13100 36200 51800 107 36200 57600 123 11 71-128/35 108-90-7 Chlorobenzene NO 36200 39500 109 36200 40500 112i 3 81-129/29 75-00-3 Chloroethane NO 36200 25700 71 36200 32200 89 22 68-133/29 67-66-3 Chloroform NO 36200 37800 104 36200 40100 111 6 72-123/26 75-15-0 Carbon disulfide ND 36200 44100 122 < 36200 46100 127' 4 72-122/29 56-23-5 Carbon tetrachloride ND 36200 35100 97 36200 38500 106i 9 78-133/29 110-82-7 Cyclohexane 1930 J 36200 38500 101 36200 40600 107 5 73-126/32 75-34-3 1,1-Dichloroethane NO 36200 39300 109 i 36200 39200 108< 0 73-125/27 75-35-4 1,1-Dichloroethylene NO 36200 35800 991, 36200 37300 103 4 81-136/28 96-12-8 1,2-Dibromo-3-chloropropane NO 36200 43600 120 36200 49800 137 13 70-137/29 106-93-4 1,2-Dibromoethane NO 36200 40800 113 36200 42700 118 5 77-126/26 107-06-2 1,2-Dichloroethane NO 36200 39400 109 36200 39800 410` 1 74-128/23 78-87-5 1,2-Dichloropropane NO 36200 38300 106 36200 38900 107' 21, 74-125/25 124-48-1 Dibromocbloromethane NO 36200 38400 100 % 36200 41600 1116! 8 76-127/27 75-71-8 Dichlorodifluoromethane NO 36200 36000 99 36200 37000 102i 3 68-168/29 156-59-2 cis-1,2-Dichloroethylene NO 36200 39900 110 = 36200 42200 117 6 74-126/26 10061-01-5 cis- 1, 3 -Dichloropropene ND 36200 36200 100 36200 41300 114i 13 80-123/26 541-73-1 m-Dichlorobenzene NO 36200 39200 168 36200 43500 120' 10 81-129/33 95-50-1 o-Dichlorobenzene ND 36200 40600 112 36200 44400 123.9 80-129/32 106-46-7 p-Dichlorobenzene ND 36200 37800 104 36200 41000 113j 8 76-130/32 156-60-5 trans-1,2-Dichloroethylene ND 36200 38600 107 36200 39400 109 2 70-127/27 10061-02-6 trans-1,3-Dichloropropene ND 36200 39000 108 36200 41700 115 71, 75-131/28 100-41-4 Ethlbenzene 13300 36200 50500 103 36200 55900 118 10 77-123/31 591-78-6 2-Hexanone NO 181000 228000 126 181000 236000 130' 3 72-133/26 98-82-8 Isopropylbenzene 9850 36200 55700 127 36200 59100 1*1 6 80-136/32 108-10-1 4-Methyl-2-pentanone NO 181000 241000 133' 181000 245000 M!' 2 76-132/26 79-20-9 Methyl acetate NO 181000 238000 131 181000 237000 131° 0 67-137/30 74-83-9 Methyl bromide NO 36200 30100 83 36200 33700 93 ' 11 65-139/31 74-87-3 Methyl chloride ND 36200 36700 101 ' 36200 37600 104' 2 71-144/27 108-87-2 Methylcyclohexane 7440 36200 44900 103 36200 45300 105 1 75-128/31 75-09-2 Methylene chloride ND 36200 36800 162 < 36200 37900 105' 3 74-137/28 78-93-3 Methyl ethyl ketone NO 181000 209000 115 1:' 181000 204000 111 2 75-137/25 Outside of Control Limits MR 61 of 90 M ACCUTEST. FAI9788 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ;ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch A19708-6MS F0067012.1) 1 I1/06/14 AD n/a n/a VF2291 A19708-6MSD F0067013.1) 1 I1/06/14 AD n/a n/a VF2291 A19708-6 F0067011.1) 1 I1/06/14 AD n/a n/a VF2291 The QC reported here applies to the following samples: Method: SW846 8260B FA19708-6, FA19708-7 FA19708-6 Spike MS MS Spike MSD MSD Limits CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % RPD Rec/RPD 1634-04-4 Methyl Tert Butyl Ether ND 36200 39400 109 36200 40200 111 2 77-120/24 91-20-3 Naphthalene 72800 36200 108000 97 36200 122000 136+ a 12 79-129/33 103-65-1 n-Propylbenzene 17100 36200 56900 110 36200 63800 129 11 80-135/33 100-42-5 Styrene ND 36200 41100 113 ! 36200 44300 122 7 78-125/30 71-55-6 1. 1, 1 -Trichloroethane NO 36200 38800 107 36200 40400 112 4'• 70-129/27 79-34-5 1, 1, 2,2-Tetrachloroethane NO 36200 41500 115 36200 45100 125 8' 71-126/30 79-00-5 1,1,2-Trichloroethane ND 36200 63600 176' 36200 67100 185* 5i 74-124/28 120-82-1 1,2,4-Tichlorobenzene NO 36200 38800 107 < 36200 41600 115 7u 78-130/34 95-63-6 1,2,4-Trimethylbenzene 82000 36200 118000 99 36200 132000 I38' 9 11 74-123/34 108-67-8 1,3,5-Trimethylbenzene 20000 36200 56700 11011 36200 65000 124" 14 73-122/33 127-18-4 Tetrachloroethylene NO 36200 36900 102 ! 36200 41000 113 11 79-130/31 108-88-3 Toluene 8340 36200 44000 198 36200 50400 116 14 76-124/30 79-01-6 Trichloroethylene NO 36200 38700 107` 36200 39600 109 2i 75-128/27 75-69-4 Trichlorofluoromethane NO 36200 34000 94 36200 35200 97 3 73-145/31 75-01-4 Vinyl chloride NO 36200 34200 94 36200 35300 97 3` 76-141/27 1330-20-7 Xylene(total) 76600 109000 198000 :112 109000 213000 126 7 80-129/30 CAS No. Surrogate Recoveries MS MSD FA19708-6 Limits 1868-53-7 Dibromofluoromethane 92% 96% 101% 75-124% 2037-26-5 Toluene-D8 92% 98% + 92% i 75-126% 460-00-4 4-Bromofluorobenzene 105% 114% 104%'. 71-133% 17060-07-0 1,2-Dichloroethane-D4 89% 89% '; 10096 72-135% (a) Outside control limits due to high level in sample relative to spike amount = Outside of Control Limits. ME 62 of 90 N ACCUTEST° FAWN GUMS Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Section 6 Method Blank Summary Page 1 of 3 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC lample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P53802-MB T015285.1) 1 11/06/14 NJ 11/05/14 OP53802 ST716 The QC reported here applies to the following samples: Method: SW846 8270D aFA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 MO 63 of 90 M ^CCUTE8T. FAI9708 " •.•• CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 830 170 ug/kg 95-57-8 2-Chlorophenol ND :170 17 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 170 17 ug/kg 120-83-2 2,4-Dichlorophenol ND 170 17 ug/kg 105-67-9 2,4-Dimethylphenol ND 170 18 ug/kg 51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg 95-48-7 2-Methylphenol ND 170 17 ug/kg 3&4-Methylphenol ND 170 33 ug/kg 88-75-5 2-Nitrophenol ND 170 17 ug/kg 100-02-7 4-Nitrophenol ND 830 130 ug/kg 87-86-5 Penlachlorophenol ND 930 130 ug/kg 108-95-2 Phenol ND : 170 17 ug/kg 88-06-2 2,4,6-Trichlorophenol W '170 17 ug/kg 83-32-9 Acenaphthene ND 170 21 ug/kg 208-96-8 Acenaphthylene ND 170 17 ug/kg 120-12-7 Anthracene ND :170 17 ug/kg 56-55-3 Benzo(a)anthracene ND 170 17 ug/kg 50-32-8 Benzo(a)pyrene ND 170 17 ug/kg 205-99-2 Benzo(b)fluoranthene ND 170 17 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg 207-08-9 Benzo(k)fluoranthene ND 170 18 ug/kg 101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg 85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg 91-58-7 2-Chloronaphthalene NO 170 20 ug/kg 106-47-8 4-Chloroaniline ND 170 17 ug/kg 218-01-9 Chrysene ND 170 17 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 170 17 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 9170 17 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 170 25 ug/kg 121-14-2 2,4-Dinitrotoluene to 170 19 ug/kg 606-20-2 2,6-Dinitrotoluene 10 170 18 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 170 17 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 170 17 ug/kg 132-64-9 Dibenzofuran ND 170 17 ug/kg F MM 64 of 90 E ACCUTEBT. FA19706 Method Blank Summary Page 2 of 3 Job Number: FA19708 Account: GRWCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP53802-MB T015285.1) 1 11/06/14 NJ 11/05/14 OP53802 ST716 The QC reported here applies to the following samples: Method: SW846 8270D FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Compound Result RL MDL Units Q 84-74-2 Di-n-butyl phthalate ND 330 33 ug/kg 117-84-0 Di-n-octyl phthalate ND 170 33 ug/kg 84-66-2 Diethyl phthalate ND 330 33 ug/kg 131-11-3 Dimethyl phthalate ND 170 33 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalale ND 330 33 ug/kg 206-44-0 Fluoranthene ND 170 17 ug/kg 86-73-7 Fluorene ND 170 17 ug/kg 118-74-1 Hexachlorobenzene ND 170 17 ug/kg 87-68-3 Hexachlorobutadiene ND 170 17 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 170 17 ug/kg 67-72-1 Hexachloroethane ND 170 17 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 170 17 ug/kg 78-59-1 Isophorone ND 170 17 ug/kg 90-12-0 1-Methylnaphthalene ND 170 17 ug/kg 91-57-6 2-Methylnaphthalene ND 170 17 ug/kg 91-20-3 Naphthalene ND 170 17 ug/kg 98-95-3 Nitrobenzene ND 170 17 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 170 17 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 170 17 ug/kg 85-01-8 Phenanthrene ND 170 17 ug/kg 129-00-0 Pyrene ND 170 17 ug/kg CAS No. Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 70% 40-102% 4165-62-2 Phenol-d5 80% 41-100% 118-79-6 2,4,6-Tribromophenol 79% 42-108% 4165-60-0 Nitrobenzene-d5 72% 40-105% 321-60-8 2-Fluorobiphenyl 76% 43-107% 1718-51-0 Terphenyl-d14 9A 45-119% CAS No. Tentatively Identified Compounds R.T. Est. Cone. Units Q 79-00-5 Ethane, 1,1,2-trichloro- 3.30 180 ug/kg JN ■ Im Mr 65 of 90 ACCUTEST. FA19708 Method Blank Summary Page 3 of 3 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP53802-MB T015285.1) 1 11/06/14 NJ 11/05/14 OP53802 ST716 The QC reported here applies to the following samples: Method: FAI9708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Tentatively Identified Compounds R.T. Est. Cone. Units Q system artifact/aldol-condensation 3.69 270 ug/kg J system artifact/aldol-condensation 3.90 5700 ,ug/kg J 79-34-5 Ethane, 1,1,2,2-tetrachloro- 4.43 420 ug/kg JN Total TIC. Semi -Volatile 600 ug/kg I Im s■ 66 of 90 E ACCUTE6T. FA19708 ••�•,••"�•" Method Blank Summary Page I of 3 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl IP53802-MB T015322.1) 1 11/07/14 NJ 11/05/14 OP53802 ST717 The QC reported here applies to the following samples: Method: SW846 8270D FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Compound Result RL MDL Units Q 65-85-0 Benzoic Acid ND 830 170 ug/kg 95-57-8 2-Chlorophenol ND 170 17 ug/kg 59-50-7 4-Chloro-3-methyl phenol ND 170 17 ug/kg 120-83-2 2,4-Dichlorophenol ND 170 17 ug/kg 105-67-9 2,4-Dimethylphenol ND 170 18 ug/kg 51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg 95-48-7 2-Methylphenol ND 170 17 ug/kg 3&4-Methylphenol ND 170 33 ug/kg 88-75-5 2-Nitrophenol ND 170 17 ug/kg 100-02-7 4-Nitrophenol ND 830 130 ug/kg 87-86-5 Pentachlorophenol ND 830 130 ug/kg 108-95-2 Phenol ND 170 17 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 170 17 ug/kg 83-32-9 Acenaphthene ND 170 21 ug/kg 208-96-8 Acenaphthylene ND 170 17 ug/kg 120-12-7 Anthracene ND 170 17 ug/kg 56-55-3 Benzo(a)anthracene ND 170 17 ug/kg 50-32-8 Benzo(a)pyrene ND 170 17 ug/kg 205-99-2 Benzo(b)fluoranthene ND 170 17 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg 207-08-9 Benzo(k)fluoranthene ND 170 18 ug/kg 101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg 85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg 91-58-7 2-Chloronaphthalene ND 170 20 ug/kg 106-47-8 4-Chloroanibne ND 170 17 ug/kg 218-01-9 Chrysene NDe 170 17 ug/kg 111-91-1 bis(2-Chloroethoxy)methane NO 170 17 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 170 17 ug/kg 108-60-1 bis(2-Chloroisopropyl)ether ND 170 17 ug/kg 7005-72-3 4-Chlorophenyl phenyl ether ND 170 25 ug/kg 121-14-2 2,4-Dinitrotoluene ND 170 19 ug/kg 606-20-2 2,6-Dinitrotoluene ND 170 18 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 170 17 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 170 17 ug/kg 132-64-9 Dibenzofuran ND 170 17 ug/kg MO 67 of 90 ACGUTEST, FA19708 Method Blank Summary Page 2 of 3 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC 'ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl )P53802-MB T015322.1) 1 11/07/14 NJ 11/05/14 OP53802 ST717 The QC reported here applies to the following samples: Method: SW846 8270D FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Compound Result RL MDL Units Q 84-74-2 Di-n-butyl phthalate ND 330 33 ug/kg 117-84-0 Di-n-octyl phthalate ND 170 33 ug/kg 84-66-2 Diethyl phthalate ND 330 33 ug/kg 131-11-3 Dimethyl phthalate ND 170 33 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg 206-44-0 Fluoranthene ND 170 17 ug/kg 86-73-7 Fluorene ND 170 17 ug/kg 118-74-1 Hexachlorobenzene ND 170 17 ug/kg 87-68-3 Hexachlorobutadiene ND 170 17 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 170 17 ug/kg 67-72-1 Hexachloroethane 10 170 17 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 170 17 ug/kg 78-59-1 Isophorone ND 170 17 ug/kg 90-12-0 I-Methylnaphthalene ND 170 17 ug/kg 91-57-6 2-Methylnaphthalene ND 170 17 ug/kg 91-20-3 Naphthalene ND 170 17 ug/kg 98-95-3 Nitrobenzene ND 170 17 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 170 17 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 170 17 ug/kg 85-01-8 Phenanthrene ND 170 17 ug/kg 129-00-0 Pyrene ND 170 17 ug/kg CAS No. Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 7196 40-102% 4165-62-2 Phenol-d5 $2% 41-100% 118-79-6 2,4,6-Tribromophenol 75% 42-108% 4165-60-0 Nitrobenzene-d5 70% 40-105% 321-60-8 2-Fluorobiphenyl 73% > 43-107% 1718-51-0 Terphenyl-d14 87% 45-119% CAS No. Tentatively Identified Compounds R.T. Est. Cone. Units Q 79-00-5 Ethane, 1,1,2-trichloro- 3.28 190 ug/kg JN F so 68 of 90 E ACGUTEST. FAIS708 Method Blank Summary Page 3 of 3 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Date] P53802-MB T015322.1) 1 11/07/14 NJ 11/05/14 OP53802 ST717 The QC reported here applies to the following samples: Method: FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Tentatively Identified Compounds R.T. Est. Conc. Units Q system artifact/aldol-condensation 3.67 320 ug/kg J system artifact/aldol-condensation 3.88 6700 ug/kg J 79-34-5 Ethane, 1,1,2,2-tetrachloro- 4.40 450 ug/kg JN Total TIC, Semi-Volatlle 640 ug/kg J M9 69 of 90 E ACCUTEST. FA19708 Blank Spike Summary Page 1 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl ,P53802-BS T015284.1) 1 11/06/14 NJ 11/05/14 OP53802 ST716 The QC reported here applies to the following samples: FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 Spike BSP BSP CAS No. Compound ug/kg ug/kg % Limits 65-85-0 Benzoic Acid 3330 2580 77 36-I18 95-57-8 2-Chlorophenol 1670 1340 80 48-104 59-50-7 4-Chloro-3-methyl phenol 1670 1340 80 52-108 120-83-2 2,4-Diehlorophenol 1670 1310 791. 51-105 105-67-9 2,4-Dimethylphenol 1670 1330 80 43-96 51-28-5 2,4-Dinitrophenol 3330 3130 94 40-119 534-52-1 4,6-Dinitro-o-cresol 3330 3190 98 64-121 95-48-7 2-Methylphenol 1670 1360 82 46-107 3&4-Methylphenol 3330 2650 80 44-111 88-75-5 2-Nitrophenol 1670 1330 80 49-104 100-02-7 4-Nitrophenol 3330 3010 90_ 56-116 87-86-5 Pentachlorophenol 3330 3180 95 61-114 108-95-2 Phenol 1670 1330 801 45-110 88-06-2 2,4,6-Trichlorophenol 1670 1480 :01, 56-109 83-32-9 Acenaphthene 1670 1380 83 56-109 208-96-8 Acenaphthylene 1670 1380 83 56-106 120-12-7 Anthracene 1670 1390 83 61-110 56-55-3 Benzo(a)anthracene 1670 1430 86 66-I11 50-32-8 Benzo(a)pyrene 1670 1370 82 59-104 205-99-2 Benzo(b)fluoranthene 1670 1430 86 67-113 191-24-2 Benzo(g,h,i)perylene 1670 1380 83 67-113 207-08-9 Benzo(k)fluoranthene 1670 1470 88 67-114 101-55-3 4-Bromophenyl phenyl ether 1670 1190 71 62-110 85-68-7 Butyl benzyl phthalate 1670 1530 92 65-113 91-58-7 2-Chloronaphthalene 1670 1310 79 53-106 106-47-8 4-Chloroaniline 1670 1140 68 30-115 218-01-9 Chrysene 1670 1440 86 65-112 111-91-1 bis(2-Chloroethoxy)methane 1670 1200 72 48-105 111-44-4 bis(2-Chloroethyl)ether 1670 1190 71 46-103 108-60-1 bis(2-Chloroisopropyl)ether 1670 1250 75 40-110 7005-72-3 4-Chlorophenyl phenyl ether 1670 1290 77 59-106 121-14-2 2,4-Dinitrotoluene 1670 1340 80 59-109 606-20-2 2,6-Dinitrotoluene 1670 1350 81 61-107 91-94-1 3,3'-Dichlorobenztdine 1670 1270 76 36-114 53-70-3 Dibenzo(a,h)anthracene 1670 1440 86 68-115 132-64-9 Dibenzofuran 1670 1390 83" `` 57-108 = Outside of Control Limits. Method: SW846 8270D ME 70 of 90 EA,( --CUTEST FA19708 '""""- """' Blank Spike Summary Page 2 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batcl IP53802-BS T015284.D 1 11/06/14 NJ 11/05/14 OP53802 ST716 The QC reported here applies to the following samples: FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 Spike BSP BSP CAS No. Compound ug/kg ug/kg % 84-74-2 Di-n-butyl phthalate 1670 1440 86 117-84-0 Di-n-octyl phthalate 1670 1550 93 84-66-2 Diethyl phthalate 1670 1350 81 131-11-3 Dimethyl phthalate 1670 1360 82 117-81-7 bis(2-Ethylhexyl)phthalate 1670 1520 91 206-44-0 Fluoranthene 1670 1370 82 86-73-7 Fluorene 1670 1380 83 1 118-74-1 Hexachlorobenzene 1670 1250 75 87-68-3 Hexachlorobuladiene 1670 1210 73 , 77-47-4 Hexachlorocyclopentadiene 1670 1240 74 67-72-1 Hexachloroethane 1670 1190 71 193-39-5 Indeno(1,2,3-cd)pyrene 1670 1280 77 1 78-59-1 Isophorone 1670 1180 71 90-12-0 1-Methylnaphthalene 1670 1270 76 91-57-6 2-Methylnaphthalene 1670 1290 77 91-20-3 Naphthalene 1670 1160 70 98-95-3 Nitrobenzene 1670 1160 70 621-64-7 N-Nitroso-di-n-propylamine 1670 1310 79 86-30-6 N-Nitrosodiphenylamine 1670 1500 90 85-01-8 Phenanthrene 1670 1430 86 129-00-0 Pyrene 1670 1480 89 CAS No. Surrogate Recoveries BSP Limits 367-12-4 2-Fluorophenol 15% 40-102% 4165-62-2 Phenol-d5 83% 41-100% 118-79-6 2,4,6-Tribromophenol 88% 42-108% 4165-60-0 Nitrobenzene-8 73% 40-105% 321-60-8 2-Fluorobiphenyl 82% 43-107% 1718-51-0 Terphenyl-d14 97% 45-119% = Outside of Control Limits. Limits 63-108 64-119 61-109 59-108 64-115 60-108 58-109 59-111 41-108 49-110 40-105 66-I16 42-89 49-106 47-106 44-104 43-108 48-108 62-110 63-111 65-115 Method: SW846 8270D so 71 of 90 W ACCUTEST. FA19708 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch IP53802-MS T015293.D 1 11/07/14 NJ 11/05/14 OP53802 ST716 IP53802-MSD T015294.D 1 11/07/14 NJ 11/05/14 OP53802 ST716 Al9700-2 T015292.1) 1 11/07/14 NJ 11/05/14 OP53802 ST716 The QC reported here applies to the following samples: Method: SW846 8270D FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Compound 65-85-0 Benzoic Acid 95-57-8 2-Chlorophenol 59-50-7 4-Chloro-3-methyl phenol 120-83-2 2,4-Dichlorophenol 105-67-9 2,4-Dimethylphenol 51-28-5 2,4-Dinitrophenol 534-52-1 4,6-Dinitro-o-cresol 95-48-7 2-Methylphenol 3&4-Methylphenol 88-75-5 2-Nitrophenol 100-02-7 4-Nitrophenol 87-86-5 Pentachlorophenol 108-95-2 Phenol 88-06-2 2,4,6-Trichlorophenol 83-32-9 Acenaphthene 208-96-8 Acenaphthylene 120-12-7 Anthracene 56-55-3 Benzo(a)anthracene 50-32-8 Benzo(a)pyrene 205-99-2 Benzo(b)fluoranthene 191-24-2 Benzo(g h,i)perylene 207-08-9 Benzo(k)fluoranthene 101-55-3 4-Bromophenyl phenyl ether 85-68-7 Butyl benzyl phthalate 91-58-7 2-Chloronaphthalene 106-47-8 4-Chloroaniline 218-01-9 Chrysene 111-91-1 bis(2-Chloroethoxy)methane 111-44-4 bis(2-Chloroethyl)ether 108-60-1 bis(2-Chloroisopropyl)ether 7005-72-3 4-Chlorophenol phenyl ether 121-14-2 2,4-Dinitrotoluene 606-20-2 2,6-Dinitrotoluene 91-94-1 3,3'-Dichlorobenzidine 53-70-3 Dibenzo(a,h)anthracene 132-64-9 Dibenzofuran Outside of Control Limits. FA19700.2 Spike MS MS ug/kg Q ug/kg ug/kg % ND 4660 3330 .71: NO 2330 1740 75 ND 2330 1730 74< NO 2330 1640 70 NO 2330 1750 75 NO 4660 3650 78 NO 4660 3840 82 NO 2330 1790 77 < NO 4660 3510 75 ND 2330 1720 74 ND 4660 3940 85 ND 4660 4040 87 NO 2330 1760 76 r ND 2330 1890 81 ND 2330 1780 76 NO 2330 1760 76 ND 2330 1790 77'' ND 2330 1840 79 ND 2330 1750 75J` ND 2330 1820 78 ND 2330 1810 78 ND 2330 1900 82 ND 2330 1520 65 NO 2330 2110 91 ND 2330 1700 73 NO 2330 1070 46 ND 2330 1840 79 ND 2330 1550 67 ND 2330 1560 67 NO 2330 1630 70' ND 2330 1610 69, ND 2330 1700 73 ND 2330 1770 76 ND 2330 1030 44 ND 2330 1840 79 ND 2330 1790 77 Spike MSD MSD ug/kg ug/kg % 4710 3360 71 2350 1710 73 2350 1750 74 2350 1640 70 2350 1760 75 4710 3690 78 4710 3780 80 2350 1780 76 4710 3520 75 2350 1660 71 4710 4000 85 4710 3970 89 2350 1760 75 2350 1870 79 2350 1770 15 2350 1760 15 2350 1740 74 2350 1790 76 2350 1690 72 2350 1770 75 2350 1770 75 2350 1860 79 2350 1490 63 2350 2070 88 2350 1680 71 2350 1250 53 2350 1800 77 2350 1560 66 2350 1550 66 2350 1670 71 2350 1640 70 2350 1710 73 2350 1770 76 2350 1250 53 2350 1790 76 2350 1810 77_ Limits RPD Rec/RPD 1 36-118/41 2 48-104/26 L 52-108/21 0 51-105/27 1 43-96/23 1 40-119/32 2 64-121/29 146-107/24 0'r < 44-111/24 4 49-104/27 2i 56-116/23 2< 61-114/23 0` 45-110/24 11 56-109/25 1 56-109/23 0` 56-106/23 9: 61-110/21 3s 66-111/23 3! 59-104/23 3<i 67-113/24 23 67-113/21 2' 67-114/22 2 62-110/21 2 65-113/20 1' 53-106/23 16 30-115/30 2 65-112/25 1 48-105/24 17 46-103/27 2 40-110/25 2 58-106/21 1 59-109/20 0 61-107/22 19 36-114/28 3 68-115/23 1 57-108/22 an 72 of 90 ACCUTEST. FA19708 Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch IP53802-MS T015293.1) I 11/07/14 NJ 11/05/14 OP53802 ST716 IP53802-MSD T015294.1) I 11/07/14 NJ 11/05/14 OP53802 ST716 A19700-2 T015292.1) 1 11/07/14 NJ 11/05/14 OP53802 ST716 The QC reported here applies to the following samples: Method: SW846 8270D FAI9708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 FA19700-2 Spike MS MS Spike MSD MSD CAS No. Compound ug/kg Q ug/kg ug/kg % ug/kg ug/kg % 84-74-2 Di-n-butyl phthalate ND 2330 1910 82 2350 1870 79 117-84-0 Di-n-octyl phthalate ND 2330 2200 94 2350 2140 91 84-66-2 Diethyl phthalate ND 2330 1750 75 2350 1760 75 131-11-3 Dimethyl phthalate ND 2330 1740 75 2350 1750 74 117-81-7 bis(2-Ethylhexyl)phthalale ND 2330 2110 91 2350 2050 87 206-44-0 Fluoranthene ND 2330 1680 72 2350 1650 70 " 86-73-7 Fluorene ND 2330 1770 76 2350 1760 75 i 118-74-1 Hexachlorobenzene ND 2330 1550 67 2350 1520 65 87-68-3 Hexachlorobutadiene ND 2330 1480 64 2350 1480 63 77-47-4 Hexachlorocyclopentadiene ND 2330 1520 65 2350 1480 63 67-72-1 Hexachloroethane ND 2330 1510 65 2350 1530 65 - 193-39-5 Indeno(1,2,3-cd)pyrene NO 2330 1680 72 2350 1630 69 ' 78-59-1 Isophorone ND 2330 1520 65 2350 1530 65 90-12-0 1-Methylnaphthalene ND 2330 1610 69 2350 1600 68 91-57-6 2-Methylnaphthalene ND 2330 1630 70 2350 1640 70 91-20-3 Naphthalene ND 2330 1480 64 2350 1480 63 '- 98-95-3 Nitrobenzene NO 2330 1520 65 2350 1530 65 621-64-7 N-Nitroso-di-n-propylamine ND 2330 1760 76 2350 1770 75 86-30-6 N-Nitrosodiphenylamine ND 2330 1980 85 2350 1910 81 85-01-8 Phenanthrene ND 2330 1860 80 2350 1810 77 129-00-0 Pyrene ND 2330 1980 85 2350 1920 82._ CAS No. Surrogate Recoveries MS MSD FA19700-2 Limits 367-12-4 2-Fluorophenol 71% 70% 69% 40-102% 4165-62-2 Phenol-d5 79% 78% 78% 41-100% 118-79-6 2,4,6-Tribromophenol 78% 77% 76% 42-108% 4165-60-0 Nitrobenzene-d5 69% 69% 72% 40-105% 321-60-8 2-Fluorobiphenyl 76% 74% 73% 43-107% 1718-51-0 Terphenyl-d14 91% 89% 94% 45-119% = Outside of Control Limits. Limits RPD Rec/RPD 2 63-108/19 3 .- 64-119/21 1 ''. 61-109/20 1 59-108/20 3 64-115/23 2 60-108/25 1 58-109/21 2 ': 59-111/21 0 41-108/27 3 49-110/31 1 40-105/32 3 66-116/22 1 42-89/22 1 49-106/26 1 47-106/27 0 44-104/27 1 43-108/25 1 48-108/27 4 62-110/21 3 63-111/22 3 65-115/25 me 73 of 90 8 ACCUTEST. FAt9708 GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Section 7 so 74 of 90 E ACCUTEST. FAI9708 Method Blank Summary Page 1 of I Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUV3537-MB UV066514.1) 1 11/05/14 AH n/a n/a GUV3537 The QC reported here applies to the following samples: Method: MADEP VPH REV 1. FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Compound Result RL MDL Units Q 71-43-2 Benzene ND 51 51 ug/kg 100-41-4 Ethylbenzene ND 100 51 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 100 51 ug/kg 91-20-3 Naphthalene ND 260 150 ug/kg 108-88-3 Toluene ND 100 51 ug/kg m,p-Xylene ND 200 100 ug/kg 95-47-6 o-Xylene ND 100 51 ug/kg C5- C8 Aliphadcs (Unadj.) ND 5100 1800 ug/kg C9- C12 Aliphatics (Unadj.) Nb 5100 1800 ug/kg CAS No. Surrogate Recoveries Limits 460-00-4 BFB 96% 70-130% 460-00-4 BFB 99% 70-130% Method Blank Summary Page I of I Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUV3538-MB UV066537.D 1 11/06/14 AH n/a n/a GUV3538 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 � FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 i N © CAS No. Compound Result RL MDL Units Q C9- CIO Aromatics (Unadj.) ND 5100 1800 ug/kg CAS No. Surrogate Recoveries Limits 460-00-4 BFB 97% 70-130% 460-00-4 BFB 99% 70-130% MM 75 of 90 W ACCUTEST, FAI9708 Mn 76 of 90 ACCUTEST, FA19708 Method Blank Summary Page 1 of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GCD5353-MB CD130690.1) I 11/06/14 JG n/a n/a GCD5353 The QC reported here applies to the following samples: Method: SW846 8015C FAI9708-1, FA19708-2 CAS No. Compound Result RL MDL Units Q TPH-GRO (C6-C10) ND 5.0 2.5 mg/kg CAS No. Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 82% 56-149% 98-08-8 aaa-Trifluorotoluene 91% 66-132% Blank Spike Summary Page 1 of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GCD5353-BS CD130689.D 1 11/06/14 JG n/a n/a GCD5353 The QC reported here applies to the following samples: FA19708-1, FA19708-2 w © Spike BSP BSP CAS No. Compound mg/kg mg/kg % Limits TPH-GRO (C6-C10) 20 19.6 98 74-128 CAS No. Surrogate Recoveries BSP Limits 460-00-4 4-13romofluorobenzene 104% 56-149% 98-08-8 aaa-Trifluorotoluene 104% 66-132% = Outside of Control Limits. M® 77 of 90 E ACCU-FE=E3 . FA19708 ".•• Method: SW846 8015C N M ME 78 of 90 M AC0U-rEST. FA19708 ...I. .1- Blank Spike/Blank Spike Duplicate Summary Page I of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUV3537-BS UV066511.1) 1 11/05/14 AH n/a n/a GUV3537 GUV3537-BSD UV066512.1) 1 11/05/14 AH n/a n/a GUV3537 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD 71-43-2 Benzene 4160 4130 99 4160 100 1 70-130/25 100-41-4 Ethylbenzene 4160 4190 101 4210 101 0 70-130/25 1634-04-4 Methyl Ted Butyl Ether 4160 4310 104 4430 106 3 70-130/25 91-20-3 Naphthalene 4160 3970 95 4010 961 70-130/25 108-88-3 Toluene 4160 4160 100 4190 101 1 70-130/25 m,p-Xylene 8320 8570 103 8610 103 U 70-130/25 95-47-6 o-Xylene 4160 4180 100 4210 101 1 70-130/25 C5- C8 Aliphatics(Unadj.) 12500 13500 108 13900 111 3 70-130/25 C9- C12 Aliphatics (Unadj.) 8320 8090 97 7990 96 1 70-130/25 CAS No. Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 87% 96% 70-130% 460-00-4 BFB 89% 98% 70-130% = Outside of Control Limits. Blank Spike/Blank Spike Duplicate Summary Page 1 of I Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GUV3538-BS UV066534.D 1 11/06/14 AH n/a n/a GUV3538 GUV3538-BSD UV066535.D 1 11/06/14 All n/a n/a GUV3538 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 v FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 © Spike BSP BSP BSD BSD Limits CAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD C9- C10 Aromatics (Unadj.) 4160 3920 94 4170 100 6 70-130/25 MR 79 of 90 M ACCUTEST. FA19708 CAS No. Surrogate Recoveries BSP BSD Limits 460-00-4 BFB 97% 93% 70-130% 460-00-4 BFB 100% ` 96% 70-130% = Outside of Control Limits. �I is N MA 80 of 90 E ACCUTEST. FA19708 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC unple File ID DF Analyzed By Prep Date Prep Batch Analytical Batc k19708-2MS CD130702.D 10 11/06/14 JG n/a n/a GCD5353 %19708-2MSD CD130703.D 10 11/06/14 JG n/a n/a GCD5353 U9708-2 CD130701.1) 10 11/06/14 JG n/a n/a GCD5353 The QC reported here applies to the following samples: Method: SW846 8015C FA19708-1, FA19708-2 a FA19708-2 Spike MS MS Spike MSD MSD Limits CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg mg/kg % RPD Rec/RPD TPH-GRO (C6-CIO) 4780 3500 7630 81 3500 7360 74 4 74-128/17 CAS No. Surrogate Recoveries MS MSD FA19708-2 Limits 460-00-4 4-Bromofluorobenzene 140% 133% 124% 56-149% 98-08-8 aaa-Tritluorotoluene 107% 110% 94% 66-132% = Outside of Control Limits. s® 81 of 90 E ACCUTEBT. FA19708 Duplicate Summary Page 1 of I Jab Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch FA19680-1DUP UV066515.1) 1 11/05/14 AH n/a n/a GUV3537 FA19680-1 a UV066516.1) 1 11/05/14 AH n/a n/a GUV3537 FA19680-1 UV066521.1) 1 11/05/14 AH n/a n/a GUV3537 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 FA19680-1 DUP CAS No. Compound ug/kg Q ug/kg Q RPD Limits 71-43-2 Benzene ND b ND nc 4 50 100-41-4 Ethylbenzene ND 6 ND uc '' 50 1634-04-4 Methyl Tert Butyl Ether ND 6 ND nc ' < 50 91-20-3 Naphthalene ND 6 ND tte 50 108-88-3 Toluene ND 6 ND nc 50 m,p-Xylene ND 6 ND Be ,' 50 95-47-6 o-Xylene ND 6 ND nc ', 50 C5- C8 Aliphatics (Unadj J ND 6 ND nc 50 C9- C12 Aliphatics (Unadj.) ND 6 ND uc 50 C5- C8 Aliphatics ND 6 ND nc 50 C9- C12 Aliphatics ND 6 ND nc 50 CAS No. Surrogate Recoveries DUP FA19680-1 FA19680-1 Limits 460-00-4 BFB 149%s'd 141%* c 130% 70-130% 460-00-4 BFB 14796* a 144%* c 135%* c 70-130% (a) Confirmation ran. (b) Result is from Ran #2. (c) Outside control limits; however, sample is ND. (d) Outside control limits. = Outside of Control Limits. me 82 of 90 U ACCUTEST. W9708 Duplicate Summary Page I of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch A197084DUP UV066541.1) 10 11/06/14 AH n/a n/a GUV3538 A19708-4 UV066540.D 10 11/06/14 AH n/a n/a GUV3538 The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1 FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 FA19708-4 DUP CAS No. Compound ug/kg Q ug/kg Q RPD Limits C9- CIO Aromatics(Unadj.) 3590000 3150000 13 50 C9- CIO Aromatics 3590000 3150000 13- 50 CAS No. Surrogate Recoveries 460-00-4 BFB 460-00-4 BFB (a) Outside control limits due to dilution. = Outside of Control Limits. DUP FA19708.4 Limits 0%* a 0%* a 70-130% 0%* a 0%* a 70-130% on 83 of 90 E ACCUTEET. FAI9708 GC Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Section 8 M® 84 of 90 a ACCUTEET, FAI9708 Method Blank Summary Page I of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP53815-MB NN010906.1) 1 11/11/14 NAF 11/06/14 OP53815 GNN479 The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1 FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 CAS No. Compound 83-32-9 Acenaphthene 208-96-8 Acenaphthylene 120-12-7 Anthracene 56-55-3 Benzo(a)anthracene 50-32-8 Benzo(a)pyrene 205-99-2 Benzo(b)fluoranthene 191-24-2 Benzo(g,h,i)perylene 207-08-9 Benzo(k)fluoranthene 218-01-9 Chrysene 53-70-3 Dibenzo(a,h)anthracene 206-44-0 Fluoranthene 86-73-7 Fluorene 193-39-5 Indeno(1,2,3-cd)pyrene 91-57-6 2-Methylnaphthalene 91-20-3 Naphthalene 85-01-8 Phenanthrene 129-00-0 Pyrene Cll-C22 Aromatics (Unadj.) Cll-C22 Aromatics C9-C18 Aliphatics C19-C36 Aliphatics CAS No. Surrogate Recoveries 3386-33-2 1-Chloroocladecane 580-13-2 2-Bromonaphthalene 84-15-1 o-Terphenyl 321-60-8 2-Fluorobiphenyl Result RL MDL Units Q ND 200 100 ug/kg NO _ _ 200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg NO -200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg ND ;200 100 ug/kg ND 200 100 ug/kg ND 200 100 ug/kg ND < 200 100 ug/kg ND 200 100 ug/kg ND 10000 7500 ug/kg ND 10000 7500 ug/kg ND 10000 5000 ug/kg ND 10000 5000 ug/kg Limits 84% 40-140% 86%, .. 40-140% 73% 40-140% 83%- 40-140% Method Blank Summary Page I of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP53810-MB JJ005944.D 1 11/10/14 SJL 11/06/14 OP53810 GJJ239 The QC reported here applies to the following samples: Method: SW846 8015C FA19708-1, FA19708-2 PD CAS No. Compound Result RL MDL Units Q ro TPH (C10-C28) 5.57 6.3 3.8 mg/kg J CAS No. Surrogate Recoveries Limits 84-15-1 o-Terphenyl 90% 56-122% M® 85 of 90 M® 86 of 90 M ACCUTEST EA,( --CUTEST FAt9708 """"""'" FAt9706 Blank Spike Summary Page 1 of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Bat&: P53810-BS JJ005945.D 1 11/10/14 SJL 11/06/14 OP53810 GJJ239 The QC reported here applies to the following samples: Method: SW846 8015C FA19708-1, FA19708-2 Spike BSP BSP 00 CAS No. Compound mg/kg mgfkg % Limits -' TPH (Cl0-C28) 50 40.4 81 62-116 CAS No. Surrogate Recoveries BSP Limits 84-15-1 o-Terphenyl 86% 56-122% = Outside of Control Limits. /n 87 of 90 ACCUTEST. FA19708 Blank Spike/Blank Spike Duplicate Summary Page I of I Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Bate P53815-BS 1111010904.1) 1 11/11/14 NAF 11/06/14 OP53815 GNN479 P53815-BSD NN010905.1) 1 11/11/14 NAF 11/06/14 OP53815 GNN479 The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1 FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 Spike BSP BSP BSD BSD Limits CAS No. Compound ug/kg ug/kg % ug/kg % RPD Rec/RPD 83-32-9 Acenaphthene 5000 3920 78 3540 71 10 40-140/30 208-96-8 Acenaphthylene 5000 3810 76 3530 71 8 40-140/30 120-12-7 Anthracene 5000 4640 93 4250 85 9 ' 40-140/30 5655-3 Benzo(a)anthracene 5000 5270 105 4840 97 9 40-140/30 50-32-8 Benzo(a)pyrene 5000 5400 108 4980 100 $ 40-140/30 205-99-2 Benzo(b)fluoranthene 5000 5350 107 4890 98 9 40-140/30 191-24-2 Benzo(g,h,i)perylene 5000 5560 111 5160 103 7 40-140/30 207-08-9 Benzo(k)fluoranthene 5000 5380 10$ `; 4970 99 8 40-140/30 218-01-9 Chrysene 5000 5210 10,4 'I 4790 96 $ 40-140/30 53-70-3 Dibenzo(a,h)anthracene 5000 5640 113 " 5210 104 8 40-140/30 206-44-0 Fluoranthene 5000 4830 97 4420 88 '9 < 40-140/30 86-73-7 Fluorene 5000 4180 84 3800 76 10 40-140/30 193-39-5 Indeno(1,2,3-cd)pyrene 5000 5580 1121 5140 103 8 40-140/30 91-57-6 2-Methylnaphthalene 5000 3590 72 3410 68 5 40-140/30 91-20-3 Naphthalene 5000 3200 64 3000 60 8 40-140/30 85-01-8 Phenanthrene 5000 4550 91 4160 83 9 40-140/30 129-00-0 Pyrene 5000 4860 97 4450 89 9 40-140/30 C11-C22 Aromatics (Unadj.) 85000 87900 103 84000 99 5 `' 40-140/30 C9-CI8 Aliphatics 30000 22000 13 27800 93 23 40-140/30 C19-06 Aliphatics 40000 34500 86 35100 88 2 40-140/30 CAS No. Surrogate Recoveries BSP BSD Limits 3386-33-2 1-Chlorooctadecane 105% 106% 40-140% 580-13-2 2-Bromonaphthalene 101% 01% 40-140% 84-15-1 o-Terphenyl 93% 90% ; 40-140% 321-60-8 2-Fluorobiphenyl 98% $8% 40-140% Sample Compound Col#1 Col#2 Breakthrough Limit OP53815-BS 2-Methylnaphthalene 3590 ND 0.0% 5.0 OP53815-BS Naphthalene 3200 ND 0.0% 5.0 OP53815-BSD 2-Methylnaphthalene 3410 NO 0.0% 5.0 OP53815-BSD Naphthalene 3000 NO 0.0% 5.0 = Outside of Control Limits. MR 88 of 90 ACCUTEST. FA19708 Matrix Spike/Matrix Spike Duplicate Summary Page I of I Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch )P53810-MS JJ005947.D 250 11/10/14 SJL 11/06/14 OP53810 GJJ239 )P53810-MSD JJ005948.D 250 11/10/14 SJL 11/06/14 OP53810 GJJ239 A19708-1 JJ005946.D 250 11/10/14 SJL 11/06/14 OP53810 GJJ239 The QC reported here applies to the following samples: Method: SW846 8015C FA19708-1, FA19708-2 eo FA19708-1 Spike MS MS Spike MSD MSD Limits a CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg mg/kg % RPD Rec/RPD TPH (C10-C28) 21700 B 70 29900 11712* a/0.7 28800 ',10038* 41 62-116/35 CAS No. Surrogate Recoveries MS MSD FA19708-1 Limits 84-15-1 o-Terphenyl 0%* b 0%* b 0%* b 56-122% (a) Outside control limits due to high level in sample relative to spike amount. (b) Outside control limits due to dilution. = Outside of Control Limits. /® 89 of 90 E ACCUTEST, FA19708 Duplicate Summary Page 1 of 1 Job Number: FA19708 Account: GRINCC GRI (Geological Resources Inc.) Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC ample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch )P53815-DUP NN010950.1) 40 11/13/14 NAF 11/06/14 OP53815 GNN481 A19708-3 NN010949.1) 50 11/13/14 NAF 11/06/14 OP53815 GNN481 The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1 FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 FA19708-3 DUP CAS No. Compound ug/kg Q ug/kg Q RPD Limits 83-32-9 Acenaphthene 15300 6390 J 82*: 30 a 208-96-8 Acenaphthylene 8540 J NO 200* 30 a 120-12-7 Anthracene ND NO nc 4 30 a 56-55-3 Benzo(a)anthracene NO NO Ile z 30 a 50-32-8 Benzo(a)pyrene NO NO Ile 30 a 205-99-2 Benzo(b)fluoranthene ND ND Be 30 a 191-24-2 Benzo(g,h,i)perylene ND ND nc 30 a 207-08-9 Benzo(k)fluoranthene ND NO nc 301 218-01-9 Chrysene NO ND Inc 30 a 53-70-3 Dibenzo(a,h)anthracene ND ND ne 30 a 206-44-0 Fluoranthene NO ND nc 30 a 86-73-7 Fluorene 8750 J ND 200* 30 a 193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc t 30 a 91-57-6 2-Methylnaphthalene 62500 27400 78* " 30 a 91-20-3 Naphthalene 10400 J ND 200* 30 a 85-01-8 Phenanthrene 11400 J ND 200* 30 a 129-00-0 Pyrene NO ND nc ; 301 CI1-C22 Aromatics (Unadj.) 3420000 1440000 81*' - ' 30 a CIl-C22 Aromatics 3300000 1400000 81*' 30 a C9-C18 Aliphatics 5270000 3330000 45*' 30 a C19-C36 Aliphatics 1240000 798000 43*1,' 30 a CAS No. Surrogate Recoveries DUP FA19708-3 Limits 3386-33-2 I-Chlorooctadecane 0%* b 0%* b 40-140% 580-13-2 2-Bromonaphthalene 0%* b 0%* b 40-140% 84-15-1 o-Terphenyl 0%* b' 0%*:6 40-140% 321-60-8 2-Fluorobiphenyl 0%* b, 0%*:b 40-140% (a) Advisory control limits. (b) Outside control limits due to dilution. = Outside of Control Limits. so 90 of 90 E ACCUTEST. FA19708