MO-8920_40424_CA_IAR_20141114_Initial Abatement Action Report

November 14, 2014 Geological Resources, Inc.
Mr. Ron Taraban
NCDENR, UST Section
Mooresville Regional Office
610 East Center Ave
Mooresville, NC 28115
Re: Initial Abatement Action Report
The Rock Worship Center
1113 Fordham Road
Charlotte, Mecklenburg County, NC
Incident Number: Pending
GRI Project No: 3605
Dear Mr. Taraban,
Please find enclosed the referenced report for the above mentioned site. If you have any questions, please do not
hesitate to contact Johanna Teschner, P.G. at 704-698-1227.
Sincerely,
Geological Resources, Inc.
J ckieDonnelly /�'
Administrative Assistant
Enclosure
Cc: Pastor Frank Jacobs
file
3502 Mayes Road • Monroe, North Carolina 28110
Phone [phone] [phone] • Fax [phone]

INITIAL ABATEMENT ACTION REPORT
THE ROCK WORSHIP CENTER
1113 FORDHAM ROAD
CHARLOTTE, MECKLENBURG COUNTY
NORTH CAROLINA
INCIDENT NUMBER: PENDING
GRI PROJECT NUMBER: 3605
Prepared for:
Pastor Frank Jacobs
1113 Fordham Road
Charlotte, North Carolina 28208
Prepared by:
Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
November 14, 2014
Mic addSenglau , P.G.
Staff Geologist
Johanna M. Teschner, P. G.
Project Manager

1. Site Identification:
Date of Report: November 12, 2014
Facility ID Number: N/A Incident Number: Pending
Site Name: The Rock Worship Center
Site Address: 1113 Fordham Road
City: Charlotte State: NC Zip Code: 28208 County: Mecklenburg
Description of Geographical Data Point: Calculated from topographic map.
Latitude: 35.21749850 N Longitude: 80.8756155' W
2. Contacts Associated with Leaking UST System:
UST Owner: Rock Worship Center
1134 West Boulevard
UST Operator:
Property Owner:
Primary Consultant:
Charlotte, North Carolina 28208
Rock Worship Center
1134 West Boulevard
Charlotte, North Carolina 28208
Rock Worship Center.
1134 West Boulevard
Charlotte, North Carolina 28208
Geological Resources, Inc.
3502 Hayes Road
Monroe, North Carolina 28110
[phone]
Laboratory: Accutest Laboratories - Southeast
4405 Vineland Road, Suite C-15
Orlando, Florida 32811
[phone]
North Carolina Certification No. 573
3. Release Information
Date Discovered: Petroleum odor and soil staining were observed during the UST closure
on November 4, 2014.
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release: Unknown
UST Size/Contents: One 550-gallon heating oil UST was removed from the site on
November 4, 2014.

4. Certification:
I, Johanna M. Teschner, a
information contained in this
Geological'Resources, Inc. is
certification numbers of the c
EXECUTIVE; SUMMARY
for Geological Resources, Inc., do certify that the
;curate to the best of my knowledge.
eology and engineering in North Carolina. The
and C-2727,respectively.
The site is an active religious facility located at 1113 Fordham Road, in Charlotte, Mecklenburg County,
North Carolina. Land use in the immediate vicinity of the site is residential. Public water is available to
the site and surrounding properties. One 550-gallon heating oil UST was removed on November 4, 2014.
A closure soil sample was collected from immediately beneath the UST. Concentrations of TPH-GRO
and TPH-DRO that exceeded the RALs were reported in the closure sample. Based on field observations,
limited over -excavation was conducted. Upon completion of excavation activities, one soil sample was
collected from the base of the excavation and four soil samples from the sidewalls of the excavation.
Concentrations of one or more BTEX constituents, naphthalene, MTBE, n-butylbenzene,
ispropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene, 1,2,4-trimethylbenzene, acenapthene, 2-
methylnapthalene, C5-C8 aliphatics, C9-C18 aliphatics, C9-C10 aromatics, and Cl 1-C22 aromatics that
exceeded the soil to water MSCCs were reported in all five excavation samples. The concentrations of
C9-C18 aliphatics, C9-C10 aromatics, and Cl 1-C22 aromatics in CS-1-10', CS-2-10', CS-3-10'and CS-
4-10' exceeded the Residential Soil Cleanup Levels.
ii

TABLE OF CONTENTS
A. SITE HISTORY AND CHARACTERIZATION.............................................................................1
B. SITE CHECK......................................................................................................................................I
C. UST CLOSURE...................................................................................................................................I
D. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT...........................................3
E. GROUNDWATER AND SURFACE WATER INVESTIGATION..............................................3
F. INITIAL RESPONSE AND ABATEMENT ACTION....................................................................3
G. EXCAVATION OF CONTAMINATED SOIL................................................................................3
H. SUMMARY AND CONCLUSIONS.................................................................................................4
I. LIMITATIONS...................................................................................................................................5
FIGURES
Figure 1:
Site Location Map
Figure 2:
Site Map with Soil Sample Locations
Figure 3:
Soil Quality Map
TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Summary of Soil Sample Analytical Results
APPENDICES
Appendix A: UST-61 Form
Appendix B: Laboratory Analytical Report — Soil Samples
iii

A. SITE HISTORY AND CHARACTERIZATION
1. UST Owner and Operator Information:
In accordance with the Initial Abatement Action (IAA) Report guidelines, the UST owner and operator
information has been summarized in Table 1.
2. UST System Information:
In accordance with the IAA Report guidelines, the UST system information has been summarized in
Table 2.
3. Non -UST Information:
Not applicable.
4. Comprehensive Description of the Release:
On November 4, 2014, the 550-gallon heating oil UST was removed. Based on field observations, a
release was suspected at the site. A 24-Hour Release and UST Leak Reporting Form (UST-61 Form) was
submitted to NCDENR on November 11, 2014. A copy of the UST-61 Form is included as Appendix A.
5. Description of the Site Characteristics:
The Rock Worship Center is an active religious facility located at 1113 Fordham Road, in Charlotte,
Mecklenburg County, North Carolina (Figure 1). The adjoining properties are residential. Public water
is available to the site and surrounding properties.
6. Summary of Initial Abatement Actions, Assessment Activities, and Corrective Actions:
The UST was a non-commercial, non -regulated heating oil tank. The 550-gallon heating oil UST was
removed from the site on November 4, 2014. Based on field observations, limited excavation activities
were conducted. Excavation was limited due to the presence of the church building and sidewalks.
B. SITE CHECK
A site check was not part of the initial abatement activities.
C. UST CLOSURE
1. Preparation for Closure:
A Charlotte Fire Department UST removal permit was obtained. Prior to closure, Charlotte Fire Inspector
Kevin Miller was notified. A copy of the permit application was provided in the 20-Day report submitted
on November 13, 2014.
2. Closure Procedure:
On November 4, 2014, one 550-gallon UST was purged of approximately 50 gallons of fluids and
subsequently removed. The UST was in poor condition with some small holes observed. The dimensions
1

of the UST were 48 inches in diameter by 6 feet in length. The UST was transported off -site and properly
disposed of. Information and manifests pertaining to the removed fluids, disposal of the UST and
contaminated soil were included in the 20-Day report
One closure soil sample (UST-1 (7')) was collected from beneath the UST and submitted for laboratory
analyses of total petroleum hydrocarbons -gasoline range organics and diesel range organics (TPH-
GRO/DRO). A sample was also collected from the stockpiled soil for analysis for TPH-DRO/GRO.
Concentrations of TPH-GRO and TPH-DRO reported in the closure sample exceeded the regulatory
action levels (RALs). Concentrations of TPH-GRO and TPH-DRO above the RAL were also reported in
the sample collected from the stockpiled soil.
3. Residual Material:
Approximately 50 gallons of fluids were pumped from the UST prior to removal.
4. Release Information:
A UST-61 Form was submitted to NCDENR on November 11, 2014. A copy of the UST-61 form is
presented in Appendix A.
5. Soil Excavation Activities:
Based on field observations, limited soil excavation activities were conducted (Figure 2). A total of
18.82 tons of contaminated soil was transported to Environmental Soils, Inc., a permitted disposal facility
in Lattimore, Cleveland County, North Carolina,
6. Site Investigation:
Upon completion of excavation activities, GRI collected one confirmation soil sample (CS-5-10') from
the base of the excavation and four soil samples (CS-1-10', CS-2-10', CS-3-10' and CS-4-10') from the
sidewalls of the excavation. The confirmation soil samples were analyzed for volatile organic compounds
(VOCs) using EPA Method 8260B, semi-VOCs using EPA Method 8270, and MADEP Methods EPH
and VPH.
The dimensions of the excavation and soil sample locations are included on the Site Map presented as
Figure 2. No ground water or bedrock was encountered during excavation activities at the site. A
summary of soil sample analytical results is presented as Table 3. A copy of the laboratory analytical
report has been included as Appendix B.
2

D. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT
No free product was observed beneath the UST during closure activities.
E. GROUNDWATER AND SURFACE WATER INVESTIGATION
Ground water and surface water investigation was not conducted as part of the initial abatement actions.
F. INITIAL RESPONSE AND ABATEMENT ACTION
Initial Response Actions:
The 550-gallon heating oil UST was removed from the site on November 4, 2014. Based on field
observations, over -excavation activities were continued on the UST basin. Excavation was limited due to
the proximity of the church building and sidewalks. The excavation was baekfilled to grade with clean
fill material. A 20-Day Report was previously submitted on November 12, 2014.
• Source Control Actions: The UST system was removed on November 4, 2014.
• Contaminant Migration Control Measures: The release was to the sub -surface; therefore no
contaminant migration control measures were necessary.
• Measures Taken to Mitigate Fire/Safety Hazards: There are not any immediate fire or safety
hazards present as a result of the release.
• Measures Taken to Identify and Mitigate Pollution Hazards: The release was to the sub -surface;
therefore, no migration control measures were necessary.
2. Initial Abatement Actions:
• Contaminated Soil Storage/Treatment and/or Disposal: A total of 18.82 tons of contaminated soil
was transported to Environmental Soil, Inc., a permitted disposal facility in Cleveland County, North
Carolina.
G. EXCAVATION OF CONTAMINATED SOIL
1. Extent of Soil Contamination:
Based on the observations from GRI staff, excavation activities were conducted. A total of 18.82 tons
of contaminated soil was removed. The final UST basin over -excavation dimensions were
approximately 9 feet long by 10 feet wide and 10 feet deep. No free product or ground water was
encountered in the excavation. Contaminated soil was transported to a permitted disposal facility.
2. Excavation Process:
The excavation activities were conducted using a track hoe.
3

3. Sampling Description:
All soil samples were collected directly from the bucket of the excavator by GRI personnel. Samples
were collected with clean, disposable nitrile gloves, immediately placed in laboratory -supplied
glassware and placed on ice.
4. Sampling Results:
Concentrations of one or more of BTEX constituents, naphthalene, MTBE, n-butylbenzene,
ispropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene, 1,2,4-trimethylbenzene, acenapthene, 2-
methy1napthalene, C5-C8 aliphatics, C9-C18 aliphatics, C9-C10 aromatics, and Cll-C22 aromatics
that exceeded the Soil to Water Maximum Soil Contaminant Concentrations (MSCCs) specified in
T15A NCAC 2L.0202 were reported in CS-1-10', CS-2-10', CS-3-10', CS-4-10' and CS-5-10'. The
concentrations of C9-C18 aliphatics, C9-C10 aromatics, and Cll-C22 aromatics in CS-1-10', CS-2-
10', CS-3-10'and CS-4-10' exceeded the Residential Soil Cleanup Levels. A summary of soil sample
analytical results is presented as Table 3. A copy of the laboratory analytical report is included in
Appendix B.
5. Soil Disposal:
According to the disposal manifests, a total of 18.82 tons of overburden and contaminated soil were
loaded and transported to Environmental Soils, Inc.
H. SUMMARY AND CONCLUSIONS
• On November 4, 2014, one 550-gallon, non -regulated heating oil UST was removed.
• The site is located in a residential area. Public water is available to the site and surrounding
properties.
• Based on field observations, over excavation was conducted. A total of 18.82 tons of contaminated
soil was transported to a permitted disposal facility.
• Neither ground water nor free product was encountered in the excavation.
• Concentrations of one or more of BTEX constituents, naphthalene, MTBE, n-butylbenzene,
ispropylbenzene, n-propylbenzene, 1,3,5-trimethylbenzene, 1,2,4-trimethylbenzene, acenapthene, 2-
methylnapthalene, C5-C8 aliphatics, and C9-C10 aromatics that exceeded the MSCC specified in
T15A NCAC 2L.0202 were reported in the excavation samples. The concentrations of C9-C18
aliphatics, C9-C10 aromatics, and Cl 1-C22 aromatics in CS-1-10', CS-2-10', CS-3-10'and CS-4-10'
exceeded the Residential Soil Cleanup Levels.
4

I. LIMITATIONS
This report has been prepared for the exclusive use of the Pastor Frank Jacobs for the specific application
to the referenced site in Mecklenburg County, North Carolina. The assessment was conducted based on
the scope of work and level of effort specified by the NCDENR and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
geology and hydrogeology practices in the State of North Carolina, available information and our
professional judgment. No other warranty is expressed or implied.
The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
5

FIGURES

LEGEND
------------ UNDERGROUND STORAGE
TANK
—-—EXCA✓AT/ONAREA
f SOIL SAMPLE LOCATION
2—
f
I
/
/ I
/
I
/
I /
CS-5-10'
i UST-1-7'
I f /
I CS 3`10'
I I
I
/
i
/ 556
Area
(Approx. 9' W x 10' L
X 10' Deep)
V Heating 0// UST
Sta.ts —
Rock Worship Center
Church Building
sae
0 1.5 3 6 Sar MAP
>713 FarMAP
Rood
( IN FEET) Charlotte, Mecklenburg County, NC
Geo%gica/ Resources, Inc. 1 Inch = 3 ft Dote.* 11111114 1 Drown by. ECH I Figure: 2

LEGEND
-- UNDERGROUND STORAGE
TANK
—-
—EXCAVA710N AREA
f
SOIL SAMPLE LOCARON
4.780
GASOLINE —RANGE 7PH
33,70D
DIESEL —RANGE TPH
0.732
BENZENE
15.0
TOLUENE
17.2
ETHYLBENZENE
91.3
XYLENES
35.8
NAPHTHALENE
BSA
2—METHYLNAPHTHALEN£
C0VaW RAApJS /N mg/kg
<D.=88 LESS
7NAN we Lk7NO2 DEI 77av L7M7Y srmvw
IN 7NE L480RA MRY REPa9T
'J' E 17MA7ED VALUE
Rock Worship Center
Church Building
I \
—2-10'
/ 0.826
// 15.3 `
16.8
21.0
G$-1-1D' 30A
0.5'D /
1.0
17.
81.3 `
35.8
d 69.4 j
m£ ,
CS-5-10' / UST-1-7'
m.000ea
iioo 7> / soeh"oi
% 0.0743 j
0.0754 J
/ 1.78
/ I 3.23 Excouation Area
2 6 (Approx. 9' W x 10' L
� zo.s X 10' Deep)
\ J /
550—Gallon
V Heating Oil UST
Stairs
0 1.5 3 6 SOIL QUALITY MAP (11104114)
I? 1113 Fordhom Rood
( IN FEET) Charlotte, Mecklenburg County, NC
Geo%gica/ Resources, Inc. 1 inch = 3 ft Date: 11114114 1 Drawn by. ECH I Figure: 3

TABLES

H
0
�
0
z
q
p
m
R.
o
v
t�
v
F
q
0
d
O
�
p
�
q
o
�
R
�
N
O
~
W
h
N
�
�
N
A
N
U
z
0
U
a
.,y
O
a
o
U
3
p
m
�
o
0
�
z
�
�
z
F

r.
8
tsw�^
�)§§/
)ƒ
\�§
§\
�t
t)\]§
)
)2/
�
»
%
q)
/
4ƒ
\
)-
e)
)A
z
u
«d
;
£]
\
t£
(d
u3
®
;!
3
§$
/
au
]
!mot$
�-
�f!!
/
\S)
°

TABLE 3
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
THE ROCK WORSHIP CENTER (INCIDENT NO. PENDING)
Date: 11/12/14
Facility ID #: NA
Analytical Method
5030/
3550/
EPA Methods 8260B and 8270
MADEP Methods VPH and EPH
80p1y5B
8015B
F
w
C4
ai
A
F
v
m
Ci
p
a
e
T
'yS'
aN0
"
p
4
T
O
�
w
P
Pa
F
P' `�
tl
o
s
o
q
v
i,
tl
CJ
U
U
U
U
7
H
(�
q
'�'
U U
U
U
U
LJ
[,�
e•i
N
U
U
Q
RAL
10
10
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Soil -to -Water MSCCs
NA
NA
0.0056
4.3
4.9
4.6
0.16
0.091
4.3
1.7
1.7
8.3
8.5
8.2
3.6
68
540
540
NE
31
31
Residential Soil Cleanup Levels
NA
NA
18
1,200
1,560
3,129
313
350
626
1,564
626
782
782
940
63
939
1,500
1,500
31,000
469
469
SP-1
11/04/14
Stockpile
---
3,680
21,700
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
UST-1-7'
11/04/14
Base Sample
7
4,780
33,700
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
NR
CS-1-10'
11/04/14
10
NR
NR
0.732
15.0
17.2
91.3
35.8
<0.069
12.4
10.1
17.4
20.4
50.1
5.25 J
69.4
204
<25.0
5,270
1,240
2,830
3,300
CS-2-10'
11/04/14
10
NR
NR
0.626
15.3
18.8
99.9
21.0
<0.077
16.0
10.4
19.9
23.7
91.2
<1.10
30.1
267
<27.0
14,000
3,740
3,590
6,020
CS-3-10'
11/04/14
Side Wall
10
NR
NR
0.0754 J
1.78
3.23
18.8
12.6
<0.057
3.38
2.59
4.52
6.18
20.4
1.64 J
20.5
58.6
<20.0
7,790
4"
847
905
CS-4-10'
11/04/14
10
NR
NR
1.03
12.0
13.3
76.6
72.8
<0.074
13.2
11.6
17.1
20.0
82.0
10.6J
167
219
<26.0
17,500
3,920
3,060
72,400
CS-5-10'
11/04/14
10
NR
NR
1 <0.000881
0.0075
1 0.0069
1 0.0412
0.0143
<0.00088
0.0115
0.0041 J
0.0124
0.0176
0.0647
0.342J
5.55
<20.0
<20.0
615
163
357
338
Notes:
• Results reported in mg/kg (milligrams per kilogram).
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MSCCs: Maximum Soil Contaminant Concentrations.
• <: Less than the reporting limit specified in the laboratory report.
• J: Estimated value.
• NR: Analyses not requested.
• Concentrations in bold face type exceed the RALs and/or the soil -to -water MSCCs. Concentrations in italics exceeded the Residential Soil Cleanup Levels.
• For other detectable contaminant concentrations below the MSCCs, please refer to the applicable laboratory reports.
Page 1 of 1

APPENDICES

APPENDIX A
UST-61 Form

f l4haJ 1"NtiffI I ����r'
.�up�1' Nil a
�Nf O
ulI"
qm iidlua►tne !,l llw d �tl� CMuI.I.�l Jq,nlhlJ, hllI,I I d�l<fa!iV,Cdillll I,I lilll h. r4d: Idll�,1 I H�da411�11 ,dlra,I�dF(d J�1 d,nalr IIa
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
an underground storage tank (US'f) system. This form Is required to be submitted within 24 hours of discovery of a known or
In NC suspected release
(D'yVM USE t�NLY) �i 4:'I
Suspected Contamination? (YIN) Y
Facility ID Number
]nettlant# j "� il
IRlsk`,(H f,L;U) l { (,
Confirmed GW Contamination? (YIN)
Date Leak Discovered
.
Received On Received By :
Rpportad;by (circle oqe) Phone Pa>F or Report ,.';, •
Confirmed Soil Contamination ?(Y/N) °^"
Samples Taken?(Y/N) _
Comm/Non-Commerclal?
Rag/Non-regulated? Wm —
Region .'. Ij ,' .
Free Product? (Y/N) N If Yes, State Greatest
%..
Thickness
INCIDENT DESCRIPTION
Incident Name: Gzr y
i�„A,,j,,Y^��.9.•lt
Address: �1 -5 vkw(Nt max ` iklad
Couiriv.
�p�
City/Town: "ko*cc
C
cc��
Zlp Code:z�,Qv
Regional Office (circle one)! Asheville, Mooresville, Fayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (dodmaldeBrew): -3-5, `I'4q9'96 Longitude (decimal degrees); gc),IV95(p 155
Obtained by:
Q GPS
Briefly describe suspected or confirmed release: (Including but not limited to: nature or release, date of release, amount
ofrelease, amount of free product present and recoveE efforts, initial responses conducted, impacts to receptors)
19 Topographic map
cX1
Q GIS Address matching
iJn
❑ Other
❑ Unknown
Derc beJocatiOn:\Ni25't
rt�Y '�Thcn `•
�ordNamPd 4
� .
HOW RELEASE WAS DISCOVERED (Release code)
(Check one)
❑ Release Detection Equipment or Methods ® Visual/Odor ❑ Groundwater Contamination
�. During UST Closure/Removal ❑ Water in Tank ❑ Surface Water Contamination
❑ Property Transfer ❑ Water Supply Well Contamination ❑ Other(specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check one to indicate primary (Check one to indicate primary (Check one) (Check one to indicate primary product type
source) cause) raleased)
Tank ❑ spill `.Petroleum ❑ Gasoline/ Diesel ❑ DieselNeg. Oil
Kerosene Blend
❑ Piping ❑ Overfill ❑ Non -Petroleum Heating Oil ❑ Vegetable Oil 100%
❑ Dispenser Corrosion Q Both ❑ Other Petroleum ❑ E10—E20
❑ Submersible Turbine Pump ❑ Physical or Mechanical Products Q E21 — E84
❑
Damage Location Metals
❑ Delivery Problem Install Problem (Check one) ❑ Other Inorganics ❑ E85 — Egg
❑
❑ Other Organics ❑ Ethanol 100%
❑ Other Other Facility
❑ ❑
E01 — E09
❑ Unknown Cl unknown
Unknown ❑Residence
Definitions presented on reverse Definitions presented on reverse C11 Other
Ownership
1. Municipal 2. Military 3. Unknown 4, Private 5. Federal 6. County 7. State
Operation Tyne
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
.00
UST Form 61 (07J08) ragw 1 "'

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? t. Yes 2. No <iVnknowiti
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users (James, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
USTOwner/Company
ww 1_
Point of Contact
Address
113`� Wei Sot��e�laVc�
IVa�- %ifiwiy_ JaC0bs
City State
UtCaNI� NG
Zip Code Telephone Number
ZS(L08 1 1-04-sss14
UST SYSTEM OPERATOR
UST Operator/Company
Address
City
State
Zip Code
Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner
Address
S,NM F- Pis N60\o E-
City
State
Zip Code
Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
5e.o-' ak\ aC�lc-1 "
Person Reporting Incidon (jyltrgi
pany
To Number' W-2245— Ib
Title
Address�pZ, Qj ((��,i(uG, 28110
Date fi
11 It'I
o..an 9 of 9
UST Fort 61 (02108)
Depmitions of Sources
Tank means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vans, vapor recovery, or fill
lines are excluded)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Deliveryproblem: identifies releases that occurred during product delivery, to the tank. (Typical causes associated with this source we spills and overfills.)
Other: serves as the option to use when the release soumo is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the sourco has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may room, from the fill pipe at the tank or when the nuzzle fails to shut offat the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g, puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, ar other component bas a release due to corrosion (e,g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other. use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown.: use when the cause has not been determined

APPENDIX13
Laboratory Analytical Report — Soil Samples

e Hardcopy 2.0
Automated Report
Southeast
■ ,�.ccuTEST
L A H OR AT OR E E 5
Technical Report for
GRI (Geological Resources Inc.)
The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Accutest Job Number: FA19708
Sampling Date: 11/04/14
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; nml@geol
carriekennedy@geologicalresourcesinc. corn;
ATTN: Johanna Teschner
Total number of pages in report: 88
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
urcesmc. corn;
gicalresourcesinc. corn
Norm Farmer
Technical Director
Client Service contact: Muna Mohammed 407-425-6700
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
hq://www.accutest.com
■■ 1 of 88
ACCUTEST
FA19708

Sections:
Table of Contents
-1-
Section1: Sample Summary...................................................................................................
3
Section2: Summary of Hits....................................................................................................
4
Section3: Sample Results........................................................................................................
9
3.1: FA19708-1: SP-1..........................................................................................................
10
3.2: FA19708-2: UST-1-7.....................................................................................................
12
3.3: FA19708-3: CS-1-10.....................................................................................................
14
3.4: FA19708-4: CS-2-10.....................................................................................................
20
3.5: FA19708-5: CS-3-10.....................................................................................................
26
3.6: FA19708-6: CS-4-10.....................................................................................................
32
3.7: FA19708-7: CS-5-10.....................................................................................................
38
Section4: Misc. Forms............................................................................................................
44
4.1: Chain of Custody...........................................................................................................
45
Section 5: GUMS Volatiles - QC Data Summaries..............................................................
48
5.1: Method Blank Summary................................................................................................
49
5.2: Blank Spike Summary...................................................................................................
53
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
57
Section 6: GUMS Semi-volatiles - QC Data Summaries.....................................................
61
6.1: Method Blank Summary................................................................................................
62
6.2: Blank Spike Summary...................................................................................................
68
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
70
Section7: GC Volatiles - QC Data Summaries.....................................................................
72
7.1: Method Blank Summary................................................................................................
73
7.2: Blank Spike Summary...................................................................................................
76
7.3: Blank Spike/Blank Spike Duplicate Summary..............................................................
77
7A Matrix Spike/Matrix Spike Duplicate Summary...........................................................
79
7.5: Duplicate Summary.......................................................................................................
80
Section 8: GC Semi-volatiles - QC Data Summaries............................................................
82
8.1: Method Blank Summary................................................................................................
83
8.2: Blank Spike Summary...................................................................................................
85
8.3: Blank Spike/Blank Spike Duplicate Summary..............................................................
86
8A Matrix Spike/Matrix Spike Duplicate Summary...........................................................
87
8.5: Duplicate Summary.......................................................................................................
88
0
0
0
0
0
■ 2 of 88
w ACCUTEST
FA19708

Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No: FA19708
The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample I D
FA19708-1 11/04/14 09:42 CNB 11/05/14 SO Soil SP-1
FA19708-2 11/04/14 10:02 CNB 11/05/14 SO Soil UST-1-7'
FA19708-3 11/04/14 11:23 CNB 11/05/14 SO Soil CS-1-10'
FA19708-4 11/04/14 11:36 CNB 11/05/14 SO Soil CS-2-10'
FA19708-5 11/04/14 11:43 CNB 11/05/14 SO Soil CS-3-10'
FA19708-6 11/04/14 11:50 CNB 11/05/14 SO Soil CS-4-10'
FA19708-7 11/04/14 11:59 CNB 11/05/14 SO Soil CS-5-10'
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
■ 3 of 88
ACCUTEST
FA19708

Summary of Hits
Job Number:
FA19708
Account:
GRI (Geological Resources Inc.)
Proj ect:
The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Collected:
11/04/ 14
.ab Sample I D Client Sample I D Result/
malyte Qual RL MDL Units Method
FA19708-1 SP-1
TPH-GRO (C6-C10) 3680 430 210 mg/kg SW846 8015C
TPH (C10-C28) 21700 B 2200 1300 mg/kg SW846 8015C
FA19708-2 UST-1-7'
TPH-GRO (C6-C10) 4780 880 440 mg/kg SW846 8015C
TPH (C10-C28) 33700 B 2000 1200 mg/kg SW846 8015C
FA19708-3 CS-1-10'
Page 1 of 5
Benzene
732
350
69
ug/kg
SW846 8260B
n-Butylbenzene
12400
3500
690
ug/kg
SW846 8260B
Cyclohexane
1810
350
73
ug/kg
SW846 8260B
Ethylbenzene
17200
3500
690
ug/kg
SW846 8260B
Isopropylbenzene
10100
350
69
ug/kg
SW846 8260B
Methylcyclohexane
9890
350
69
ug/kg
SW846 8260B
Methylene chloride
286 J
690
280
ug/kg
SW846 8260B
Naphthalene
35800
3500
1400
ug/kg
SW846 8260B
n-Propylbenzene
17400
3500
690
ug/kg
SW846 8260B
1,2,4-Trimethylbenzene
80100
3500
690
ug/kg
SW846 8260B
1,3,5-Trimethylbenzene
20400
3500
690
ug/kg
SW846 8260B
Toluene
15000
3500
690
ug/kg
SW846 8260B
Xylene (total)
91300
10000
1800
ug/kg
SW846 8260B
Acenaphthene a
5250 J
8000
1000
ug/kg
SW846 8270D
Acenaphthylene a
1510 J
8000
800
ug/kg
SW846 8270D
Anthracene a
940 J
8000
800
ug/kg
SW846 8270D
Dibenzofuran a
2200 J
8000
800
ug/kg
SW846 8270D
Fluorene a
11200
8000
800
ug/kg
SW846 8270D
2-Methylnaphthalene a
69400
8000
800
ug/kg
SW846 8270D
Naphthalene a
15000
8000
800
ug/kg
SW846 8270D
Phenanthrenea
17400
8000
800
ug/kg
SW846 8270D
Pyrene a
4430 J
8000
800
ug/kg
SW846 8270D
Benzene
1000
710
710
ug/kg
MADEP VPH REV 1.1
Ethylbenzene
36300
1400
710
ug/kg
MADEP VPH REV 1.1
Naphthalene
95800
3500
2100
ug/kg
MADEP VPH REV 1.1
Toluene
21500
1400
710
ug/kg
MADEP VPH REV 1.1
m,p-Xylene
77200
2800
1400
ug/kg
MADEP VPH REV 1.1
o-Xylene
63100
1400
710
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics (Unadj.)
226000
71000
25000
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)
2830000
1400000
490000
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics
204000
71000
25000
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics
2830000
1400000
490000
ug/kg
MADEP VPH REV 1.1
Acenaphthene
15300
12000
6000
ug/kg
MADEP EPH REV 1.1
■ 4 of 88
■ ACCUTEST
FA19708

Summary of Hits Page 2 of 5
Job Number:
FA19708
Account:
GRI (Geological Resources Inc.)
Proj ect:
The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Collected:
11/04/ 14
Lab Sample I D Client Sample I D Result/
Analyte Qual RL MDL Units Method
Acenaphthylene
8540 J
12000
6000
ug/kg
MADEP EPH REV 1.1
Fluorene
8750 J
12000
6000
ug/kg
MADEP EPH REV 1.1
2-Methylnaphthalene
62500
12000
6000
ug/kg
MADEP EPH REV 1.1
Naphthalene
10400 J
12000
6000
ug/kg
MADEP EPH REV 1.1
Phenanthrene
11400 J
12000
6000
ug/kg
MADEP EPH REV 1.1
CI I-C22 Aromatics (Unadj.)
3420000
600000
450000
ug/kg
MADEP EPH REV 1.1
CI I-C22 Aromatics
3300000
600000
450000
ug/kg
MADEP EPH REV 1.1
C9-C18 Aliphatics
5270000
600000
300000
ug/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
1240000
600000
300000
ug/kg
MADEP EPH REV 1.1
FA19708-4 CS-2-10'
Benzene
626
380
77
ug/kg
SW846 8260B
n-Butylbenzene
16000
3800
770
ug/kg
SW846 8260B
Cyclohexane
2150
380
81
ug/kg
SW846 8260B
Ethylbenzene
18800
3800
770
ug/kg
SW846 8260B
Isopropylbenzene
10400
380
77
ug/kg
SW846 8260B
Methylcyclohexane
13100
380
77
ug/kg
SW846 8260B
Naphthalene
21000
3800
1500
ug/kg
SW846 8260B
n-Propylbenzene
19900
3800
770
ug/kg
SW846 8260B
1,2,4-Trimethylbenzene
91200
3800
770
ug/kg
SW846 8260B
1,3,5-Trimethylbenzene
23700
3800
770
ug/kg
SW846 8260B
Toluene
15300
3800
770
ug/kg
SW846 8260B
Xylene (total)
99900
12000
2000
ug/kg
SW846 8260B
Fluorene a
3710 J
8400
840
ug/kg
SW846 8270D
2-Methylnaphthalene a
30100
8400
840
ug/kg
SW846 8270D
Naphthalene a
9350
8400
840
ug/kg
SW846 8270D
Phenanthrene a
4480 J
8400
840
ug/kg
SW846 8270D
Pyrene a
2120 J
8400
840
ug/kg
SW846 8270D
Benzene
895
780
780
ug/kg
MADEP VPH REV 1.1
Ethylbenzene
43600
1600
780
ug/kg
MADEP VPH REV 1.1
Naphthalene
97000
3900
2300
ug/kg
MADEP VPH REV 1.1
Toluene
22400
1600
780
ug/kg
MADEP VPH REV 1.1
m,p-Xylene
84900
3100
1600
ug/kg
MADEP VPH REV 1.1
o-Xylene
71300
1600
780
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics (Unadj.)
290000
78000
27000
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)
3590000
1600000
550000
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics
267000
78000
27000
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics
3590000
1600000
550000
ug/kg
MADEP VPH REV 1.1
2-Methylnaphthalene
119000
50000
25000
ug/kg
MADEP EPH REV 1.1
C11-C22 Aromatics (Unadj.)
6140000
2500000
1900000
ug/kg
MADEP EPH REV 1.1
CI I-C22 Aromatics
6020000
2500000
1900000
ug/kg
MADEP EPH REV 1.1
C9-C18 Aliphatics
14000000
2500000
1200000
ug/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
3740000
2500000
1200000
ug/kg
MADEP EPH REV 1.1
■ 5 of 88
■ ACCUTEST
FA19708

Summary of Hits Page 3 of 5
Job Number:
FA19708
Account:
GRI (Geological Resources Inc.)
Proj ect:
The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Collected:
11/04/ 14
Lab Sample I D Client Sample I D Result/
Analyte Qual RL MDL Units Method
FA19708-5 CS-3-10'
Benzene
n-Butylbenzene
Cyclohexane
Ethylbenzene
Isopropylbenzene
Methylcyclohexane
Naphthalene
n-Propylbenzene
1, 2, 4-Trimethylbenzene
1, 3, 5-Trimethylbenzene
Toluene
Xylene (total)
Acenaphthene a
Anthracene a
Dibenzofuran a
Fluoranthenea
Fluorene a
2-Methylnaphthalene a
Naphthalene a
Phenanthrene a
Pyrene a
Ethylbenzene
Naphthalene
Toluene
m,p-Xylene
o-Xylene
C5- C8 Aliphatics (Unadj.)
C9- C10 Aromatics (Unadj.)
C5- C8 Aliphatics
C9- C10 Aromatics
Acenaphthene
Acenaphthylene
Fluorene
2-Methylnaphthalene
Naphthalene
CI I-C22 Aromatics (Unadj.)
CI I-C22 Aromatics
C9-C18 Aliphatics
C 19-C36 Aliphatics
FA19708-6 CS-4-10'
Benzene
75.4 J
3380
359
3230
2590
2240
12600
4520
20400
6180
1780
18800
1640 J
263 J
566 J
201 J
2430
20500
4740
4330
1220 J
7470
32600
2300
13600
13700
60900
847000
280
280
280
280
280
280
2800
280
2800
280
280
850
2000
2000
2000
2000
2000
2000
2000
2000
2000
1200
2900
1200
2300
1200
58000
580000
57
57
60
57
57
57
1100
57
570
57
57
150
250
200
200
200
200
200
200
200
200
580
1700
580
1200
580
20000
200000
58600
58000
20000
847000
580000
200000
4130 J
4500
2300
2720 J
4500
2300
2950 J
4500
2300
18000
4500
2300
2400 J
4500
2300
935000
230000
170000
905000
230000
170000
1790000
230000
110000
488000
230000
110000
1030 370 74
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8260B
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
SW846 8270D
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP VPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg
MADEP EPH REV 1.1
ug/kg SW846 8260B
■ 6 of 88
■ ACC UTEST
FA19708

Summary of Hits Page 4 of 5
Job Number:
FA19708
Account:
GRI (Geological Resources Inc.)
Proj ect:
The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Collected:
11/04/ 14
Lab Sample I D Client Sample I D Result/
Analyte Qual RL MDL Units Method
n-Butylbenzene
13200
370
74
ug/kg
SW846 8260B
Cyclohexane
2230
370
79
ug/kg
SW846 8260B
Ethylbenzene
13300
3600
720
ug/kg
SW846 8260B
Isopropylbenzene
11600
370
74
ug/kg
SW846 8260B
Methylcyclohexane
9520
370
74
ug/kg
SW846 8260B
Naphthalene
72800
3600
1400
ug/kg
SW846 8260B
n-Propylbenzene
17100
3600
720
ug/kg
SW846 8260B
1,2,4-Trimethylbenzene
82000
3600
720
ug/kg
SW846 8260B
1,3,5-Trimethylbenzene
20000
3600
720
ug/kg
SW846 8260B
Toluene
12000
370
74
ug/kg
SW846 8260B
Xylene (total)
76600
11000
1900
ug/kg
SW846 8260B
Acenaphthene a
10600 J
17000
2100
ug/kg
SW846 8270D
Anthracene a
2380 J
17000
1700
ug/kg
SW846 8270D
Dibenzofuran a
4740 J
17000
1700
ug/kg
SW846 8270D
Fluorene a
17300
17000
1700
ug/kg
SW846 8270D
2-Methylnaphthalene a
167000
17000
1700
ug/kg
SW846 8270D
Naphthalene a
37900
17000
1700
ug/kg
SW846 8270D
Phenanthrene a
39700
17000
1700
ug/kg
SW846 8270D
Pyrene a
6270 J
17000
1700
ug/kg
SW846 8270D
Benzene
1430
760
760
ug/kg
MADEP VPH REV 1.1
Ethylbenzene
30800
1500
760
ug/kg
MADEP VPH REV 1.1
Naphthalene
158000
3800
2300
ug/kg
MADEP VPH REV 1.1
Toluene
15400
1500
760
ug/kg
MADEP VPH REV 1.1
m,p-Xylene
65000
3000
1500
ug/kg
MADEP VPH REV 1.1
o-Xylene
56300
1500
760
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics (Unadj.)
236000
76000
26000
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)
3060000
1500000
530000
ug/kg
MADEP VPH REV 1.1
C5- C8 Aliphatics
219000
76000
26000
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics
3060000
1500000
530000
ug/kg
MADEP VPH REV 1.1
Acenaphthene
62500 J
63000
31000
ug/kg
MADEP EPH REV 1.1
Fluorene
32500 J
63000
31000
ug/kg
MADEP EPH REV 1.1
2-Methylnaphthalene
307000
63000
31000
ug/kg
MADEP EPH REV 1.1
Naphthalene
53000 J
63000
31000
ug/kg
MADEP EPH REV 1.1
Phenanthrene
43000 J
63000
31000
ug/kg
MADEP EPH REV 1.1
CI I-C22 Aromatics (Unadj.)
12900000
3100000
2400000
ug/kg
MADEP EPH REV 1.1
CI I-C22 Aromatics
12400000
3100000
2400000
ug/kg
MADEP EPH REV 1.1
C9-C 18 Aliphatics
17500000
3100000
1600000
ug/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
3920000
3100000
1600000
ug/kg
MADEP EPH REV 1.1
FA19708-7 CS-5-10'
Acetone
85.6
44
13
ug/kg
SW846
8260B
n-Butylbenzene
11.5
4.4
0.88
ug/kg
SW846
8260B
Ethylbenzene
6.9
4.4
0.88
ug/kg
SW846
8260B
Isopropylbenzene
4.1 J
4.4
0.88
ug/kg
SW846
8260B
■■ 7 of 88
ACCUTEST
FA19708

Summary of Hits Page 5 of 5
Job Number:
FA19708
Account:
GRI (Geological Resources Inc.)
Proj ect:
The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Collected:
11/04/ 14
Lab Sample I D Client Sample I D Result/
Analyte Qual RL MDL Units Method
Methylcyclohexane
1.3 J
4.4
0.88
ug/kg
SW846 8260B
Naphthalene
14.3
4.4
1.8
ug/kg
SW846 8260B
n-Propylbenzene
12.4
4.4
0.88
ug/kg
SW846 8260B
1,2,4-Trimethylbenzene
64.7
4.4
0.88
ug/kg
SW846 8260B
1,3,5-Trimethylbenzene
17.6
4.4
0.88
ug/kg
SW846 8260B
Toluene
7.5
4.4
0.88
ug/kg
SW846 8260B
Xylene (total)
41.2
13
2.3
ug/kg
SW846 8260B
Acenaphthene a
342 J
970
120
ug/kg
SW846 8270D
Acenaphthylene a
117 J
970
97
ug/kg
SW846 8270D
Dibenzofuran a
140 J
970
97
ug/kg
SW846 8270D
Fluorene a
623 J
970
97
ug/kg
SW846 8270D
2-Methylnaphthalene a
5550
970
97
ug/kg
SW846 8270D
Naphthalene a
1500
970
97
ug/kg
SW846 8270D
Phenanthrene a
957 J
970
97
ug/kg
SW846 8270D
Pyrene a
373 J
970
97
ug/kg
SW846 8270D
Ethylbenzene
599 J
1200
580
ug/kg
MADEP VPH REV 1.1
Naphthalene
9960
2900
1700
ug/kg
MADEP VPH REV 1.1
m,p-Xylene
1510 J
2300
1200
ug/kg
MADEP VPH REV 1.1
o-Xylene
3320
1200
580
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics (Unadj.)
357000
120000
41000
ug/kg
MADEP VPH REV 1.1
C9- C10 Aromatics
357000
120000
41000
ug/kg
MADEP VPH REV 1.1
Acenaphthene
1440
1200
600
ug/kg
MADEP EPH REV 1.1
Fluorene
903 J
1200
600
ug/kg
MADEP EPH REV 1.1
2-Methylnaphthalene
5580
1200
600
ug/kg
MADEP EPH REV 1.1
Naphthalene
744 J
1200
600
ug/kg
MADEP EPH REV 1.1
Phenanthrene
601 J
1200
600
ug/kg
MADEP EPH REV 1.1
CI I-C22 Aromatics (Unadj.)
348000
60000
45000
ug/kg
MADEP EPH REV 1.1
C11-C22 Aromatics
338000
60000
45000
ug/kg
MADEP EPH REV 1.1
C9-C18 Aliphatics
615000
60000
30000
ug/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
163000
60000
30000
ug/kg
MADEP EPH REV 1.1
(a) Dilution required due to matrix interference.
■ 8 of 88
ACCUTEST
FA19708

Section 3
Southeast
■ ,�.ccuTEST
L A H OR AT OR E E 5
Sample Results
Report of Analysis
■■ 9 of 88
E ACCUTEST
FA19708 1PBDRATOR15

Accutest Laboratories
Report of Analysis
Client Sample I D: SP-1
Lab Sample I D: FA19708-1 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8015C Percent Solids. 72.5
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 j
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD130694.D 10 11/06/14 JG n/a n/a GCD5353
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 5.21 g 5.0 m1 20.0 ul
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
Result
RL M DL Units Q
3680
430 210 mg/kg
Run#1
Run#2 Limits
139%
56-149%
101%
66-132%
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N =
Indicates presumptive evidence of a compound
■■ 10 of 88
M ACCUTEST
FA19708 1PBDRATOR15

Accutest Laboratories
Report of Analysis
Client Sample I D: SP-1
Lab Sample I D: FA19708-1 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8015C SW846 3550C Percent Solids. 72.5
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 j
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 JJ005946.1) 250 11/10/14 SJL 11/06/14 OP53810 GJJ239
Run #2
Initial Weight Final Volume
Run#1 19.7g 1.0M1
Run #2
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
(a) Outside control limits due to dilution.
Result
RL MDL Units Q
21700
2200 1300 mg/kg B
Run#1
Run#2 Limits
0% a
56-122%
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N =
Indicates presumptive evidence of a compound
■■ 11 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Client Sample I D: UST-1-7
Lab Sample I D: FA19708-2 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8015C Percent Solids: 75.5
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 N
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 CD130701.D 10 11/06/14 JG n/a n/a GCD5353
Run #2
Initial Weight Final Volume Methanol Aliquot
Run#1 4.64g 5.0ml 10.0u1
Run #2
CAS No.
Compound
TPH-GRO (C6-C 10)
CAS No.
Surrogate Recoveries
460-00-4
4-Bromofluorobenzene
98-08-8
aaa-Trifluorotoluene
Result
RL M DL Units Q
4780
880 440 mg/kg
Run#1
Run#2 Limits
124%
56-149%
94%
66-132%
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N =
Indicates presumptive evidence of a compound
■ 12 of 88
■ ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Client Sample I D: UST-1-7
Lab Sample I D: FA19708-2 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8015C SW846 3550C Percent Solids: 75.5
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 N
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 JJ005950.1) 250 11/10/14 SJL 11/06/14 OP53810 GJJ239
Run #2
Initial Weight Final Volume
Run #1 20.3 g 1.0 M1
Run #2
CAS No. Compound
TPH (C10-C28)
CAS No. Surrogate Recoveries
84-15-1 o-Terphenyl
(a) Outside control limits due to dilution.
Result
RL MDL Units Q
33700
2000 1200 mg/kg B
Run#1
Run#2 Limits
0% a
56-122%
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N =
Indicates presumptive evidence of a compound
■ 13 of 88
■ ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-1-10'
Lab Sample I D: FA19708-3 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8260B Percent Solids: 81.8
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 Y16999.13
1
11/05/14
AD
n/a
n/a
VY747
Run #2 Y17000.13
1
11/05/14
AD
n/a
n/a
VY747
Initial Weight Methanol Aliquot
Run #1 5.25 g 100 ul
Run #2 5.25 g 10.0 ul
VOA Special List
CAS No. Compound Result RL M DL Units Q
67-64-1
Acetone
ND
3500
1000
ug/kg
71-43-2
Benzene
732
350
69
ug/kg
75-27-4
Bromodichloromethane
ND
350
69
ug/kg
75-25-2
Bromoform
ND
350
75
ug/kg
104-51-8
n-Butylbenzene
12400 a
3500
690
ug/kg
108-90-7
Chlorobenzene
ND
350
69
ug/kg
75-00-3
Chloroethane
ND
350
160
ug/kg
67-66-3
Chloroform
ND
350
78
ug/kg
75-15-0
Carbon disulfide
ND
350
69
ug/kg
56-23-5
Carbon tetrachloride
ND
350
96
ug/kg
110-82-7
Cyclohexane
1810
350
73
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
350
69
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
350
69
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
350
150
ug/kg
106-93-4
1,2-Dibromoethane
ND
350
120
ug/kg
107-06-2
1,2-Dichloroethane
ND
350
69
ug/kg
78-87-5
1,2-Dichloropropane
ND
350
69
ug/kg
124-48-1
Dibromochloromethane
ND
350
69
ug/kg
75-71-8
Dichlorodifluoromethane
ND
350
87
ug/kg
156-59-2
cis-1,2-Dichloroethylene
ND
350
69
ug/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
350
69
ug/kg
541-73-1
m-Dichlorobenzene
ND
350
69
ug/kg
95-50-1
o-Dichlorobenzene
ND
350
69
ug/kg
106-46-7
p-Dichlorobenzene
ND
350
78
ug/kg
156-60-5
trans-1,2-Dichloroethylene
ND
350
93
ug/kg
10061-02-6
trans- 1, 3-Dichloropropene
ND
350
69
ug/kg
100-41-4
Ethlbenzene
17200 a
3500
690
ug/kg
591-78-6
2-Hexanone
ND
1700
340
ug/kg
98-82-8
Isopropylbenzene
10100
350
69
ug/kg
108-10-1
4-Methyl-2-pentanone
ND
1700
350
ug/kg
79-20-9
Methyl acetate
ND
1700
350
ug/kg
74-83-9
Methyl bromide
ND
350
130
ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 14 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Aient Sample I D: CS-1-10'
.ab Sample I D: FA19708-3 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: SW846 8260B Percent Solids: 81.8
'roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
VOA Special List
CAS No.
Compound
Result
RL
M DL
Units Q
74-87-3
Methyl chloride
ND
350
140
ug/kg
108-87-2
Methylcyclohexane
9890
350
69
ug/kg
75-09-2
Methylene chloride
286
690
280
ug/kg J
78-93-3
Methyl ethyl ketone
ND
1700
520
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
350
69
ug/kg
91-20-3
Naphthalene
35800 a
3500
1400
ug/kg
103-65-1
n-Propylbenzene
17400 a
3500
690
ug/kg
100-42-5
Styrene
ND
350
69
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
350
69
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
350
98
ug/kg
79-00-5
1, 1, 2-Trichloroethane
ND
350
110
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
350
80
ug/kg
95-63-6
1,2,4-Trimethylbenzene
80100 a
3500
690
ug/kg
108-67-8
1,3,5-Trimethylbenzene
20400 a
3500
690
ug/kg
127-18-4
Tetrachloroethylene
ND
350
87
ug/kg
108-88-3
Toluene
15000 a
3500
690
ug/kg
79-01-6
Trichloroethylene
ND
350
71
ug/kg
75-69-4
Trichlorofluoromethane
ND
350
69
ug/kg
75-01-4
Vinyl chloride
ND
350
71
ug/kg
1330-20-7
Xylene (total)
91300 a
10000
1800
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
105%
75-124%
2037-26-5
Toluene-D8
98%
98%
75-126%
460-00-4
4-Bromofluorobenzene
114%
106%
71-133%
17060-07-0
1,2-Dichloroethane-D4
99%
99%
72-135%
(a) Result is from Run# 2
Page 2 of 2 w
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 15 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-1-10'
Lab Sample I D: FA19708-3 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids: 81.8
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a U047759.13 40 11/10/14 NJ 11/05/14 OP53802 SU2190
Run #2
Initial Weight Final Volume
Run#1 30.4g 1.0M1
Run #2
ABN Special List
CAS No. Compound Result RL M DL Units Q
65-85-0
Benzoic Acid
ND
40000
8000
ug/kg
95-57-8
2-Chlorophenol
ND
8000
800
ug/kg
59-50-7
4-Chloro-3-methyl phenol
ND
8000
800
ug/kg
120-83-2
2,4-Dichlorophenol
ND
8000
830
ug/kg
105-67-9
2,4-Dimethylphenol
ND
8000
890
ug/kg
51-28-5
2,4-Dinitrophenol
ND
40000
8000
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
16000
3200
ug/kg
95-48-7
2-Methylphenol
ND
8000
800
ug/kg
3&4-Methylphenol
ND
8000
1600
ug/kg
88-75-5
2-Nitrophenol
ND
8000
800
ug/kg
100-02-7
4-Nitrophenol
ND
40000
6400
ug/kg
87-86-5
Pentachlorophenol
ND
40000
6400
ug/kg
108-95-2
Phenol
ND
8000
800
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
8000
800
ug/kg
83-32-9
Acenaphthene
5250
8000
1000
ug/kg
208-96-8
Acenaphthylene
1510
8000
800
ug/kg
120-12-7
Anthracene
940
8000
800
ug/kg
56-55-3
Benzo(a)anthracene
ND
8000
800
ug/kg
50-32-8
Benzo(a)pyrene
ND
8000
800
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
8000
800
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
8000
800
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
8000
880
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
8000
800
ug/kg
85-68-7
Butyl benzyl phthalate
ND
8000
1600
ug/kg
91-58-7
2-Chloronaphthalene
ND
8000
960
ug/kg
106-47-8
4-Chloroaniline
ND
8000
800
ug/kg
218-01-9
Chrysene
ND
8000
800
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
8000
800
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
8000
800
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
8000
840
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
8000
1200
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
8000
910
ug/kg
J
J
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 16 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Client Sample I D: CS-1-10'
Lab Sample I D: FA19708-3 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids: 81.8
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
ABN Special List
CAS No. Compound Result RL M DL Units Q
606-20-2
2,6-Dinitrotoluene
ND
8000
880
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
8000
800
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
8000
800
ug/kg
132-64-9
Dibenzofuran
2200
8000
800
ug/kg J
84-74-2
Di-n-butyl phthalate
ND
16000
1600
ug/kg
117-84-0
Di-n-octyl phthalate
ND
8000
1600
ug/kg
84-66-2
Diethyl phthalate
ND
16000
1600
ug/kg
131-11-3
Dimethyl phthalate
ND
8000
1600
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
16000
1600
ug/kg
206-44-0
Fluoranthene
ND
8000
800
ug/kg
86-73-7
Fluorene
11200
8000
800
ug/kg
118-74-1
Hexachlorobenzene
ND
8000
800
ug/kg
87-68-3
Hexachlorobutadiene
ND
8000
800
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
8000
800
ug/kg
67-72-1
Hexachloroethane
ND
8000
800
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
8000
800
ug/kg
78-59-1
Isophorone
ND
8000
800
ug/kg
91-57-6
2-Methylnaphthalene
69400
8000
800
ug/kg
91-20-3
Naphthalene
15000
8000
800
ug/kg
98-95-3
Nitrobenzene
ND
8000
800
ug/kg
621-64-7
N-Nitroso-di-n-propylamine
ND
8000
800
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
8000
800
ug/kg
85-01-8
Phenanthrene
17400
8000
800
ug/kg
129-00-0
Pyrene
4430
8000
800
ug/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
0% b
40-102%
4165-62-2
Phenol-d5
0% b
41-100%
118-79-6
2,4,6-Tribromophenol
0% b
42-108%
4165-60-0
Nitrobenzene-d5
0% b
40-105%
321-60-8
2-Fluorobiphenyl
0% b
43-107%
1718-51-0
Terphenyl-d14
0% b
45-119%
(a) Dilution required due to matrix interference.
(b) Outside control limits due to dilution.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 17 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of 1 w
Client Sample I D: CS-1-10'
Lab Sample I D: FA19708-3 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: MADEP VPH REV 1.1 Percent Solids: 81.8
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 UV066525.13
1
11/05/14
AH
n/a
n/a
GUV3537
Run #2 UV066539.13
10
11/06/14
AH
n/a
n/a
GUV3538
Initial Weight Final Volume Methanol Aliquot
Run #1 5.25 g 5.1 ml 10.0 ul
Run #2 5.25 g 5.1 ml 5.0 ul
MADEPVPH List
CAS No.
Compound
Result
RL
M DL
Units Q
71-43-2
Benzene
1000
710
710
ug/kg
100-41-4
Ethylbenzene
36300
1400
710
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
1400
710
ug/kg
91-20-3
Naphthalene
95800
3500
2100
ug/kg
108-88-3
Toluene
21500
1400
710
ug/kg
m,p-Xylene
77200
2800
1400
ug/kg
95-47-6
o-Xylene
63100
1400
710
ug/kg
C5- C8 Aliphatics (Unadj.)
226000
71000
25000
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
71000
25000
ug/kg
C9- C10 Aromatics (Unadj.)
2830000 a
1400000
490000
ug/kg
C5- C8 Aliphatics
204000
71000
25000
ug/kg
C9- C 12 Aliphatics
ND
71000
25000
ug/kg
C9- C 10 Aromatics
2830000 a
1400000
490000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
557% c
0% b
70-130%
460-00-4
BFB
372% c
0% b
70-130%
(a) Result is
from Run# 2
(b) Outside
control limits due to dilution.
(c) Outside
control limits due to matrix interference.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 18 of 88
■ ACCUTEST
FA19708 1PBDRATOR15

Accutest Laboratories
Report of Analysis
,Iient Sample I D: CS-1-10'
.ab Sample I D: FA19708-3 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 81.8
'roj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 w
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN010949.13 50 11/13/14 NAF 11/06/14 OP53815 GNN481
Run #2
Initial Weight Final Volume
un # 1 20.3 g 2.0 ml
un #2
MAEPH List
CAS No.
Compound
Result
RL
M DL
Units Q
83-32-9
Acenaphthene
15300
12000
6000
ug/kg
208-96-8
Acenaphthylene
8540
12000
6000
ug/kg J
120-12-7
Anthracene
ND
12000
6000
ug/kg
56-55-3
Benzo(a)anthracene
ND
12000
6000
ug/kg
50-32-8
Benzo(a)pyrene
ND
12000
6000
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
12000
6000
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
12000
6000
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
12000
6000
ug/kg
218-01-9
Chrysene
ND
12000
6000
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
12000
6000
ug/kg
206-44-0
Fluoranthene
ND
12000
6000
ug/kg
86-73-7
Fluorene
8750
12000
6000
ug/kg J
193-39-5
Indeno(1,2,3-cd)pyrene
ND
12000
6000
ug/kg
91-57-6
2-Methylnaphthalene
62500
12000
6000
ug/kg
91-20-3
Naphthalene
10400
12000
6000
ug/kg J
85-01-8
Phenanthrene
11400
12000
6000
ug/kg J
129-00-0
Pyrene
ND
12000
6000
ug/kg
C11-C22 Aromatics (Unadj.)
3420000
600000
450000
ug/kg
C11-C22 Aromatics
3300000
600000
450000
ug/kg
C9-C18 Aliphatics
5270000
600000
300000
ug/kg
C19-C36 Aliphatics
1240000
600000
300000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
0% a
40-140%
580-13-2
2-Bromonaphthalene
0% a
40-140%
84-15-1
o-Terphenyl
0% a
40-140%
321-60-8
2-Fluorobiphenyl
0% a
40-140%
(a) Outside control limits due to dilution.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 19 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-2-10'
Lab Sample I D: FA19708-4 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8260B Percent Solids: 80.3
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 Y17002.13
1
11/05/14
AD
n/a
n/a
VY747
Run #2 Y17003.13
1
11/05/14
AD
n/a
n/a
VY747
Initial Weight Methanol Aliquot
Run #1 4.82 g 100 ul
Run #2 4.82 g 10.0 ul
VOA Special List
CAS No. Compound Result RL M DL Units Q
67-64-1
Acetone
ND
3800
1200
ug/kg
71-43-2
Benzene
626
380
77
ug/kg
75-27-4
Bromodichloromethane
ND
380
77
ug/kg
75-25-2
Bromoform
ND
380
83
ug/kg
104-51-8
n-Butylbenzene
16000 a
3800
770
ug/kg
108-90-7
Chlorobenzene
ND
380
77
ug/kg
75-00-3
Chloroethane
ND
380
170
ug/kg
67-66-3
Chloroform
ND
380
87
ug/kg
75-15-0
Carbon disulfide
ND
380
77
ug/kg
56-23-5
Carbon tetrachloride
ND
380
110
ug/kg
110-82-7
Cyclohexane
2150
380
81
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
380
77
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
380
77
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
380
160
ug/kg
106-93-4
1,2-Dibromoethane
ND
380
140
ug/kg
107-06-2
1,2-Dichloroethane
ND
380
77
ug/kg
78-87-5
1,2-Dichloropropane
ND
380
77
ug/kg
124-48-1
Dibromochloromethane
ND
380
77
ug/kg
75-71-8
Dichlorodifluoromethane
ND
380
97
ug/kg
156-59-2
cis-1,2-Dichloroethylene
ND
380
77
ug/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
380
77
ug/kg
541-73-1
m-Dichlorobenzene
ND
380
77
ug/kg
95-50-1
o-Dichlorobenzene
ND
380
77
ug/kg
106-46-7
p-Dichlorobenzene
ND
380
86
ug/kg
156-60-5
trans-1,2-Dichloroethylene
ND
380
100
ug/kg
10061-02-6
trans- 1, 3-Dichloropropene
ND
380
77
ug/kg
100-41-4
Ethlbenzene
18800 a
3800
770
ug/kg
591-78-6
2-Hexanone
ND
1900
380
ug/kg
98-82-8
Isopropylbenzene
10400
380
77
ug/kg
108-10-1
4-Methyl-2-pentanone
ND
1900
380
ug/kg
79-20-9
Methyl acetate
ND
1900
380
ug/kg
74-83-9
Methyl bromide
ND
380
140
ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 20 of 88
■ ACCUTEST
FA19708 1ABDRATOR16

Accutest Laboratories
Report of Analysis
Aient Sample I D: CS-2-10'
.ab Sample I D: FA19708-4 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: SW846 8260B Percent Solids: 80.3
'roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
VOA Special List
CAS No.
Compound
Result
RL
M DL
Units Q
74-87-3
Methyl chloride
ND
380
150
ug/kg
108-87-2
Methylcyclohexane
13100
380
77
ug/kg
75-09-2
Methylene chloride
ND
770
310
ug/kg
78-93-3
Methyl ethyl ketone
ND
1900
580
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
380
77
ug/kg
91-20-3
Naphthalene
21000 a
3800
1500
ug/kg
103-65-1
n-Propylbenzene
19900 a
3800
770
ug/kg
100-42-5
Styrene
ND
380
77
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
380
77
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
380
110
ug/kg
79-00-5
1, 1, 2-Trichloroethane
ND
380
120
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
380
88
ug/kg
95-63-6
1,2,4-Trimethylbenzene
91200 a
3800
770
ug/kg
108-67-8
1,3,5-Trimethylbenzene
23700 a
3800
770
ug/kg
127-18-4
Tetrachloroethylene
ND
380
97
ug/kg
108-88-3
Toluene
15300 a
3800
770
ug/kg
79-01-6
Trichloroethylene
ND
380
78
ug/kg
75-69-4
Trichlorofluoromethane
ND
380
77
ug/kg
75-01-4
Vinyl chloride
ND
380
78
ug/kg
1330-20-7
Xylene (total)
99900 a
12000
2000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
106%
104%
75-124%
2037-26-5
Toluene-D8
98%
100%
75-126%
460-00-4
4-Bromofluorobenzene
113%
110%
71-133%
17060-07-0
1,2-Dichloroethane-D4
99%
96%
72-135%
(a) Result is from Run# 2
Page 2 of 2 a
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 21 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-2-10'
Lab Sample I D: FA19708-4 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids: 80.3
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a U047760.13 40 11/10/14 NJ 11/05/14 OP53802 SU2190
Run #2
Initial Weight Final Volume
Run #1 29.8 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL M DL Units Q
65-85-0
Benzoic Acid
ND
42000
8400
ug/kg
95-57-8
2-Chlorophenol
ND
8400
840
ug/kg
59-50-7
4-Chloro-3-methyl phenol
ND
8400
840
ug/kg
120-83-2
2,4-Dichlorophenol
ND
8400
860
ug/kg
105-67-9
2,4-Dimethylphenol
ND
8400
920
ug/kg
51-28-5
2,4-Dinitrophenol
ND
42000
8400
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
17000
3300
ug/kg
95-48-7
2-Methylphenol
ND
8400
840
ug/kg
3&4-Methylphenol
ND
8400
1700
ug/kg
88-75-5
2-Nitrophenol
ND
8400
840
ug/kg
100-02-7
4-Nitrophenol
ND
42000
6700
ug/kg
87-86-5
Pentachlorophenol
ND
42000
6700
ug/kg
108-95-2
Phenol
ND
8400
840
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
8400
840
ug/kg
83-32-9
Acenaphthene
ND
8400
1100
ug/kg
208-96-8
Acenaphthylene
ND
8400
840
ug/kg
120-12-7
Anthracene
ND
8400
840
ug/kg
56-55-3
Benzo(a)anthracene
ND
8400
840
ug/kg
50-32-8
Benzo(a)pyrene
ND
8400
840
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
8400
840
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
8400
840
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
8400
910
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
8400
840
ug/kg
85-68-7
Butyl benzyl phthalate
ND
8400
1700
ug/kg
91-58-7
2-Chloronaphthalene
ND
8400
990
ug/kg
106-47-8
4-Chloroaniline
ND
8400
840
ug/kg
218-01-9
Chrysene
ND
8400
840
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
8400
840
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
8400
840
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
8400
870
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
8400
1200
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
8400
950
ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 22 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Client Sample I D: CS-2-10'
Lab Sample I D: FA19708-4 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids: 80.3
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
ABN Special List
CAS No. Compound Result RL M DL Units Q
606-20-2
2,6-Dinitrotoluene
ND
8400
910
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
8400
840
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
8400
840
ug/kg
132-64-9
Dibenzofuran
ND
8400
840
ug/kg
84-74-2
Di-n-butyl phthalate
ND
17000
1700
ug/kg
117-84-0
Di-n-octyl phthalate
ND
8400
1700
ug/kg
84-66-2
Diethyl phthalate
ND
17000
1700
ug/kg
131-11-3
Dimethyl phthalate
ND
8400
1700
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
17000
1700
ug/kg
206-44-0
Fluoranthene
ND
8400
840
ug/kg
86-73-7
Fluorene
3710
8400
840
ug/kg J
118-74-1
Hexachlorobenzene
ND
8400
840
ug/kg
87-68-3
Hexachlorobutadiene
ND
8400
840
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
8400
840
ug/kg
67-72-1
Hexachloroethane
ND
8400
840
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
8400
840
ug/kg
78-59-1
Isophorone
ND
8400
840
ug/kg
91-57-6
2-Methylnaphthalene
30100
8400
840
ug/kg
91-20-3
Naphthalene
9350
8400
840
ug/kg
98-95-3
Nitrobenzene
ND
8400
840
ug/kg
621-64-7
N-Nitroso-di-n-propylamine
ND
8400
840
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
8400
840
ug/kg
85-01-8
Phenanthrene
4480
8400
840
ug/kg J
129-00-0
Pyrene
2120
8400
840
ug/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
0% b
40-102%
4165-62-2
Phenol-d5
0% b
41-100%
118-79-6
2,4,6-Tribromophenol
0% b
42-108%
4165-60-0
Nitrobenzene-d5
0% b
40-105%
321-60-8
2-Fluorobiphenyl
0% b
43-107%
1718-51-0
Terphenyl-d14
0% b
45-119%
(a) Dilution required due to matrix interference.
(b) Outside control limits due to dilution.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■V 23 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of 1 P
Client Sample I D: CS-2-10'
Lab Sample I D: FA19708-4 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: MADEP VPH REV 1.1 Percent Solids: 80.3
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 UV066526.D
1
11/05/14
AH
n/a
n/a
GUV3537
Run #2 UV066540.13
10
11/06/14
AH
n/a
n/a
GUV3538
Initial Weight Final Volume Methanol Aliquot
Run # 1 4.82 g 5.1 ml 10.0 ul
Run #2 4.82 g 5.1 ml 5.0 ul
MADEPVPH List
CAS No.
Compound
Result
RL
M DL
Units Q
71-43-2
Benzene
895
780
780
ug/kg
100-41-4
Ethylbenzene
43600
1600
780
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
1600
780
ug/kg
91-20-3
Naphthalene
97000
3900
2300
ug/kg
108-88-3
Toluene
22400
1600
780
ug/kg
m,p-Xylene
84900
3100
1600
ug/kg
95-47-6
o-Xylene
71300
1600
780
ug/kg
C5- C8 Aliphatics (Unadj.)
290000
78000
27000
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
78000
27000
ug/kg
C9- C10 Aromatics (Unadj.)
3590000 a
1600000
550000
ug/kg
C5- C8 Aliphatics
267000
78000
27000
ug/kg
C9- C 12 Aliphatics
ND
78000
27000
ug/kg
C9- C 10 Aromatics
3590000 a
1600000
550000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
422% c
0% b
70-130%
460-00-4
BFB
253% c
0% b
70-130%
(a) Result is
from Run# 2
(b) Outside
control limits due to dilution.
(c) Outside
control limits due to matrix interference.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 24 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
'Iient Sample I D: CS-2-10'
.ab Sample I D: FA19708-4 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 80.3
'roj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 P
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
:un #1 NN010957.13 200 11/13/14 NAF 11/06/14 OP53815 GNN481
:un #2
Initial Weight Final Volume
:un # 1 20.1 g 2.0 ml
:un #2
MAEPH List
CAS No.
Compound
Result
RL
M DL Units Q
83-32-9
Acenaphthene
ND
50000
25000 ug/kg
208-96-8
Acenaphthylene
ND
50000
25000 ug/kg
120-12-7
Anthracene
ND
50000
25000 ug/kg
56-55-3
Benzo(a)anthracene
ND
50000
25000 ug/kg
50-32-8
Benzo(a)pyrene
ND
50000
25000 ug/kg
205-99-2
Benzo(b)fluoranthene
ND
50000
25000 ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
50000
25000 ug/kg
207-08-9
Benzo(k)fluoranthene
ND
50000
25000 ug/kg
218-01-9
Chrysene
ND
50000
25000 ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
50000
25000 ug/kg
206-44-0
Fluoranthene
ND
50000
25000 ug/kg
86-73-7
Fluorene
ND
50000
25000 ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
50000
25000 ug/kg
91-57-6
2-Methylnaphthalene
119000
50000
25000 ug/kg
91-20-3
Naphthalene
ND
50000
25000 ug/kg
85-01-8
Phenanthrene
ND
50000
25000 ug/kg
129-00-0
Pyrene
ND
50000
25000 ug/kg
C11-C22 Aromatics (Unadj.)
6140000
2500000
1900000 ug/kg
C11-C22 Aromatics
6020000
2500000
1900000 ug/kg
C9-C18 Aliphatics
14000000
2500000
1200000 ug/kg
C19-C36 Aliphatics
3740000
2500000
1200000 ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
0% a
40-140%
580-13-2
2-Bromonaphthalene
0% a
40-140%
84-15-1
o-Terphenyl
0% a
40-140%
321-60-8
2-Fluorobiphenyl
0% a
40-140%
(a) Outside control limits due to dilution.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 25 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-3-10'
Lab Sample ID: FA19708-5 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8260B Percent Solids. 85.8
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 Y17004.13
1
11/05/14
AD
n/a
n/a
VY747
Run #2 Y17005.13
1
11/05/14
AD
n/a
n/a
VY747
Initial Weight Methanol Aliquot
Run #1 6.02 g 100 ul
Run #2 6.02 g 10.0 ul
VOA Special List
CAS No. Compound Result RL M DL Units Q
67-64-1
Acetone
ND
2800
850
ug/kg
71-43-2
Benzene
75.4
280
57
ug/kg J
75-27-4
Bromodichloromethane
ND
280
57
ug/kg
75-25-2
Bromoform
ND
280
61
ug/kg
104-51-8
n-Butylbenzene
3380
280
57
ug/kg
108-90-7
Chlorobenzene
ND
280
57
ug/kg
75-00-3
Chloroethane
ND
280
130
ug/kg
67-66-3
Chloroform
ND
280
64
ug/kg
75-15-0
Carbon disulfide
ND
280
57
ug/kg
56-23-5
Carbon tetrachloride
ND
280
79
ug/kg
110-82-7
Cyclohexane
359
280
60
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
280
57
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
280
57
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
280
120
ug/kg
106-93-4
1,2-Dibromoethane
ND
280
100
ug/kg
107-06-2
1,2-Dichloroethane
ND
280
57
ug/kg
78-87-5
1,2-Dichloropropane
ND
280
57
ug/kg
124-48-1
Dibromochloromethane
ND
280
57
ug/kg
75-71-8
Dichlorodifluoromethane
ND
280
71
ug/kg
156-59-2
cis-1,2-Dichloroethylene
ND
280
57
ug/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
280
57
ug/kg
541-73-1
m-Dichlorobenzene
ND
280
57
ug/kg
95-50-1
o-Dichlorobenzene
ND
280
57
ug/kg
106-46-7
p-Dichlorobenzene
ND
280
63
ug/kg
156-60-5
trans-1,2-Dichloroethylene
ND
280
76
ug/kg
10061-02-6
trans- 1, 3-Dichloropropene
ND
280
57
ug/kg
100-41-4
Ethlbenzene
3230
280
57
ug/kg
591-78-6
2-Hexanone
ND
1400
280
ug/kg
98-82-8
Isopropylbenzene
2590
280
57
ug/kg
108-10-1
4-Methyl-2-pentanone
ND
1400
280
ug/kg
79-20-9
Methyl acetate
ND
1400
280
ug/kg
74-83-9
Methyl bromide
ND
280
110
ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 26 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Aient Sample I D: CS-3-10'
.abSample ID: FA19708-5 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: SW846 8260B Percent Solids. 85.8
'roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
VOA Special List
CAS No. Compound
74-87-3
Methyl chloride
108-87-2
Methylcyclohexane
75-09-2
Methylene chloride
78-93-3
Methyl ethyl ketone
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
71-55-6
1, 1, 1 -Trichloroethane
79-34-5
1,1,2,2-Tetrachloroethane
79-00-5
1, 1, 2-Trichloroethane
120-82-1
1,2,4-Trichlorobenzene
95-63-6
1,2,4-Trimethylbenzene
108-67-8
1,3,5-Trimethylbenzene
127-18-4
Tetrachloroethylene
108-88-3
Toluene
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
75-01-4
Vinyl chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
Result
RL
M DL
Units Q
ND
280
110
ug/kg
2240
280
57
ug/kg
ND
570
230
ug/kg
ND
1400
420
ug/kg
ND
280
57
ug/kg
12600a
2800
1100
ug/kg
4520
280
57
ug/kg
ND
280
57
ug/kg
ND
280
57
ug/kg
ND
280
80
ug/kg
ND
280
91
ug/kg
ND
280
65
ug/kg
20400a
2800
570
ug/kg
6180
280
57
ug/kg
ND
280
71
ug/kg
1780
280
57
ug/kg
ND
280
58
ug/kg
ND
280
57
ug/kg
ND
280
58
ug/kg
18800
850
150
ug/kg
Run#1 Run#2 Limits
1868-53-7
Dibromofluoromethane
105%
104%
75-124%
2037-26-5
Toluene-D8
98%
97%
75-126%
460-00-4
4-Bromofluorobenzene
112%
107%
71-133%
17060-07-0
1,2-Dichloroethane-D4
97%
97%
72-135%
(a) Result is from Run# 2
Page 2 of 2 P
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 27 of 88
■ ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-3-10'
Lab Sample ID: FA19708-5 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids. 85.8
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a T015326.1) 10 11/07/14 NJ 11/05/14 OP53802 ST717
Run #2
Initial Weight Final Volume
Run #1 29.8 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL M DL Units Q
65-85-0
Benzoic Acid
ND
9800
2000
ug/kg
95-57-8
2-Chlorophenol
ND
2000
200
ug/kg
59-50-7
4-Chloro-3-methyl phenol
ND
2000
200
ug/kg
120-83-2
2,4-Dichlorophenol
ND
2000
200
ug/kg
105-67-9
2,4-Dimethylphenol
ND
2000
220
ug/kg
51-28-5
2,4-Dinitrophenol
ND
9800
2000
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
3900
780
ug/kg
95-48-7
2-Methylphenol
ND
2000
200
ug/kg
3&4-Methylphenol
ND
2000
390
ug/kg
88-75-5
2-Nitrophenol
ND
2000
200
ug/kg
100-02-7
4-Nitrophenol
ND
9800
1600
ug/kg
87-86-5
Pentachlorophenol
ND
9800
1600
ug/kg
108-95-2
Phenol
ND
2000
200
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
2000
200
ug/kg
83-32-9
Acenaphthene
1640
2000
250
ug/kg
208-96-8
Acenaphthylene
ND
2000
200
ug/kg
120-12-7
Anthracene
263
2000
200
ug/kg
56-55-3
Benzo(a)anthracene
ND
2000
200
ug/kg
50-32-8
Benzo(a)pyrene
ND
2000
200
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
2000
200
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
2000
200
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
2000
210
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
2000
200
ug/kg
85-68-7
Butyl benzyl phthalate
ND
2000
390
ug/kg
91-58-7
2-Chloronaphthalene
ND
2000
230
ug/kg
106-47-8
4-Chloroaniline
ND
2000
200
ug/kg
218-01-9
Chrysene
ND
2000
200
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
2000
200
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
2000
200
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
2000
200
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
2000
290
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
2000
220
ug/kg
J
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 28 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
3Iient Sample I D: CS-3-10'
-ab Sample I D: FA19708-5 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids. 85.8
project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
ABN Special List
CAS No.
Compound
Result
RL
M DL
Units Q
606-20-2
2, 6-Dinitrotoluene
ND
2000
210
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
2000
200
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
2000
200
ug/kg
132-64-9
Dibenzofuran
566
2000
200
ug/kg J
84-74-2
Di-n-butyl phthalate
ND
3900
390
ug/kg
117-84-0
Di-n-octyl phthalate
ND
2000
390
ug/kg
84-66-2
Diethyl phthalate
ND
3900
390
ug/kg
131-11-3
Dimethyl phthalate
ND
2000
390
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
3900
390
ug/kg
206-44-0
Fluoranthene
201
2000
200
ug/kg J
86-73-7
Fluorene
2430
2000
200
ug/kg
118-74-1
Hexachlorobenzene
ND
2000
200
ug/kg
87-68-3
Hexachlorobutadiene
ND
2000
200
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
2000
200
ug/kg
67-72-1
Hexachloroethane
ND
2000
200
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
2000
200
ug/kg
78-59-1
Isophorone
ND
2000
200
ug/kg
91-57-6
2-Methylnaphthalene
20500
2000
200
ug/kg
91-20-3
Naphthalene
4740
2000
200
ug/kg
98-95-3
Nitrobenzene
ND
2000
200
ug/kg
621-64-7
N-Nitroso-di-n-propylamine
ND
2000
200
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
2000
200
ug/kg
85-01-8
Phenanthrene
4330
2000
200
ug/kg
129-00-0
Pyrene
1220
2000
200
ug/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
72%
40-102%
4165-62-2
Phenol-d5
84%
41-100%
118-79-6
2,4,6-Tribromophenol
69%
42-108%
4165-60-0
Nitrobenzene-d5
85%
40-105%
321-60-8
2-Fluorobiphenyl
79%
43-107%
1718-51-0
Terphenyl-d14
84%
45-119%
(a) Dilution required due to matrix interference.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 29 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of 1 P
Client Sample I D: CS-3-10'
Lab Sample ID: FA19708-5 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: MADEP VPH REV 1.1 Percent Solids. 85.8
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 UV066527.13
1
11/05/14
AH
n/a
n/a
GUV3537
Run #2 UV066542.13
10
11/06/14
AH
n/a
n/a
GUV3538
Initial Weight Final Volume Methanol Aliquot
Run #1 6.02 g 5.1 ml 10.0 ul
Run #2 6.02 g 5.1 ml 10.0 ul
MADEPVPH List
CAS No.
Compound
Result
RL
M DL
Units Q
71-43-2
Benzene
ND
580
580
ug/kg
100-41-4
Ethylbenzene
7470
1200
580
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
1200
580
ug/kg
91-20-3
Naphthalene
32600
2900
1700
ug/kg
108-88-3
Toluene
2300
1200
580
ug/kg
m,p-Xylene
13600
2300
1200
ug/kg
95-47-6
o-Xylene
13700
1200
580
ug/kg
C5- C8 Aliphatics (Unadj.)
60900
58000
20000
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
58000
20000
ug/kg
C9- C10 Aromatics (Unadj.)
847000 a
580000
200000
ug/kg
C5- C8 Aliphatics
58600
58000
20000
ug/kg
C9- C12 Aliphatics
ND
58000
20000
ug/kg
C9- C10 Aromatics
847000 a
580000
200000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
246% c
0% b
70-130%
460-00-4
BFB
219% c
0% b
70-130%
(a) Result is
from Run# 2
(b) Outside
control limits due to dilution.
(c) Outside
control limits due to matrix interference.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 30 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
,Iient Sample I D: CS-3-10'
.abSample ID: FA19708-5 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: MADEP EPH REV 1.1 SW846 3546 Percent Solids. 85.8
'roj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 P
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN010952.13 20 11/13/14 NAF 11/06/14 OP53815 GNN481
Run #2
Initial Weight Final Volume
un #1 20.5 g 2.0 m1
un #2
MAEPH List
CAS No.
Compound
Result
RL
M DL
Units Q
83-32-9
Acenaphthene
4130
4500
2300
ug/kg J
208-96-8
Acenaphthylene
2720
4500
2300
ug/kg J
120-12-7
Anthracene
ND
4500
2300
ug/kg
56-55-3
Benzo(a)anthracene
ND
4500
2300
ug/kg
50-32-8
Benzo(a)pyrene
ND
4500
2300
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
4500
2300
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
4500
2300
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
4500
2300
ug/kg
218-01-9
Chrysene
ND
4500
2300
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
4500
2300
ug/kg
206-44-0
Fluoranthene
ND
4500
2300
ug/kg
86-73-7
Fluorene
2950
4500
2300
ug/kg J
193-39-5
Indeno(1,2,3-cd)pyrene
ND
4500
2300
ug/kg
91-57-6
2-Methylnaphthalene
18000
4500
2300
ug/kg
91-20-3
Naphthalene
2400
4500
2300
ug/kg J
85-01-8
Phenanthrene
ND
4500
2300
ug/kg
129-00-0
Pyrene
ND
4500
2300
ug/kg
C11-C22 Aromatics (Unadj.)
935000
230000
170000
ug/kg
C11-C22 Aromatics
905000
230000
170000
ug/kg
C9-C18 Aliphatics
1790000
230000
110000
ug/kg
C19-C36 Aliphatics
488000
230000
110000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
0% a
40-140%
580-13-2
2-Bromonaphthalene
0% a
40-140%
84-15-1
o-Terphenyl
0% a
40-140%
321-60-8
2-Fluorobiphenyl
0% a
40-140%
(a) Outside control limits due to dilution.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 31 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-4-10'
Lab Sample ID: FA19708-6 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8260B Percent Solids. 79.0
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 Y17007.13
1
11/05/14
AD
n/a
n/a
VY747
Run #2 F0067011.13
1
11/06/14
AD
n/a
n/a
VF2291
Initial Weight Methanol Aliquot
Run#1 5.18g 100ul
Run #2 5.35 g 10.0 ul
VOA Special List
CAS No. Compound Result RL M DL Units Q
67-64-1
Acetone
ND
3700
1100
ug/kg
71-43-2
Benzene
1030
370
74
ug/kg
75-27-4
Bromodichloromethane
ND
370
74
ug/kg
75-25-2
Bromoform
ND
370
80
ug/kg
104-51-8
n-Butylbenzene
13200
370
74
ug/kg
108-90-7
Chlorobenzene
ND
370
74
ug/kg
75-00-3
Chloroethane
ND
370
170
ug/kg
67-66-3
Chloroform
ND
370
84
ug/kg
75-15-0
Carbon disulfide
ND
370
74
ug/kg
56-23-5
Carbon tetrachloride
ND
370
100
ug/kg
110-82-7
Cyclohexane
2230
370
79
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
370
74
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
370
74
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
370
160
ug/kg
106-93-4
1,2-Dibromoethane
ND
370
130
ug/kg
107-06-2
1,2-Dichloroethane
ND
370
74
ug/kg
78-87-5
1,2-Dichloropropane
ND
370
74
ug/kg
124-48-1
Dibromochloromethane
ND
370
74
ug/kg
75-71-8
Dichlorodifluoromethane
ND
370
94
ug/kg
156-59-2
cis-1,2-Dichloroethylene
ND
370
74
ug/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
370
74
ug/kg
541-73-1
m-Dichlorobenzene
ND
370
74
ug/kg
95-50-1
o-Dichlorobenzene
ND
370
74
ug/kg
106-46-7
p-Dichlorobenzene
ND
370
83
ug/kg
156-60-5
trans-1,2-Dichloroethylene
ND
370
100
ug/kg
10061-02-6
trans- 1, 3-Dichloropropene
ND
370
74
ug/kg
100-41-4
Ethlbenzene
13300 a
3600
720
ug/kg
591-78-6
2-Hexanone
ND
1900
360
ug/kg
98-82-8
Isopropylbenzene
11600
370
74
ug/kg
108-10-1
4-Methyl-2-pentanone
ND
1900
370
ug/kg
79-20-9
Methyl acetate
ND
1900
370
ug/kg
74-83-9
Methyl bromide
ND
370
140
ug/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 32 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Aient Sample I D: CS-4-10'
.abSample ID: FA19708-6 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: SW846 8260B Percent Solids. 79.0
'roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
VOA Special List
CAS No.
Compound
Result
RL
M DL
Units Q
74-87-3
Methyl chloride
ND
370
150
ug/kg
108-87-2
Methylcyclohexane
9520
370
74
ug/kg
75-09-2
Methylene chloride
ND
740
300
ug/kg
78-93-3
Methyl ethyl ketone
ND
1900
560
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
370
74
ug/kg
91-20-3
Naphthalene
72800 a
3600
1400
ug/kg
103-65-1
n-Propylbenzene
17100 a
3600
720
ug/kg
100-42-5
Styrene
ND
370
74
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
370
74
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
370
100
ug/kg
79-00-5
1, 1, 2-Trichloroethane
ND
370
120
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
370
86
ug/kg
95-63-6
1,2,4-Trimethylbenzene
82000 a
3600
720
ug/kg
108-67-8
1,3,5-Trimethylbenzene
20000 a
3600
720
ug/kg
127-18-4
Tetrachloroethylene
ND
370
94
ug/kg
108-88-3
Toluene
12000
370
74
ug/kg
79-01-6
Trichloroethylene
ND
370
76
ug/kg
75-69-4
Trichlorofluoromethane
ND
370
74
ug/kg
75-01-4
Vinyl chloride
ND
370
76
ug/kg
1330-20-7
Xylene (total)
76600 a
11000
1900
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
105%
101%
75-124%
2037-26-5
Toluene-D8
97%
92%
75-126%
460-00-4
4-Bromofluorobenzene
115%
104%
71-133%
17060-07-0
1,2-Dichloroethane-D4
98%
100%
72-135%
(a) Result is from Run# 2
Page 2 of 2
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 33 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-4-10'
Lab Sample ID: FA19708-6 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids. 79.0
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a U047761.13 80 11/10/14 NJ 11/05/14 OP53802 SU2190
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL M DL Units Q
65-85-0
Benzoic Acid
ND
84000
17000
ug/kg
95-57-8
2-Chlorophenol
ND
17000
1700
ug/kg
59-50-7
4-Chloro-3-methyl phenol
ND
17000
1700
ug/kg
120-83-2
2,4-Dichlorophenol
ND
17000
1700
ug/kg
105-67-9
2,4-Dimethylphenol
ND
17000
1900
ug/kg
51-28-5
2,4-Dinitrophenol
ND
84000
17000
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
34000
6800
ug/kg
95-48-7
2-Methylphenol
ND
17000
1700
ug/kg
3&4-Methylphenol
ND
17000
3400
ug/kg
88-75-5
2-Nitrophenol
ND
17000
1700
ug/kg
100-02-7
4-Nitrophenol
ND
84000
14000
ug/kg
87-86-5
Pentachlorophenol
ND
84000
14000
ug/kg
108-95-2
Phenol
ND
17000
1700
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
17000
1700
ug/kg
83-32-9
Acenaphthene
10600
17000
2100
ug/kg
208-96-8
Acenaphthylene
ND
17000
1700
ug/kg
120-12-7
Anthracene
2380
17000
1700
ug/kg
56-55-3
Benzo(a)anthracene
ND
17000
1700
ug/kg
50-32-8
Benzo(a)pyrene
ND
17000
1700
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
17000
1700
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
17000
1700
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
17000
1800
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
17000
1700
ug/kg
85-68-7
Butyl benzyl phthalate
ND
17000
3400
ug/kg
91-58-7
2-Chloronaphthalene
ND
17000
2000
ug/kg
106-47-8
4-Chloroaniline
ND
17000
1700
ug/kg
218-01-9
Chrysene
ND
17000
1700
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
17000
1700
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
17000
1700
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
17000
1800
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
17000
2500
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
17000
1900
ug/kg
J
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 34 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
Client Sample I D: CS-4-10'
Lab Sample ID: FA19708-6 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids. 79.0
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
ABN Special List
CAS No. Compound Result RL M DL Units Q
606-20-2
2,6-Dinitrotoluene
ND
17000
1800
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
17000
1700
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
17000
1700
ug/kg
132-64-9
Dibenzofuran
4740
17000
1700
ug/kg J
84-74-2
Di-n-butyl phthalate
ND
34000
3400
ug/kg
117-84-0
Di-n-octyl phthalate
ND
17000
3400
ug/kg
84-66-2
Diethyl phthalate
ND
34000
3400
ug/kg
131-11-3
Dimethyl phthalate
ND
17000
3400
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
34000
3400
ug/kg
206-44-0
Fluoranthene
ND
17000
1700
ug/kg
86-73-7
Fluorene
17300
17000
1700
ug/kg
118-74-1
Hexachlorobenzene
ND
17000
1700
ug/kg
87-68-3
Hexachlorobutadiene
ND
17000
1700
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
17000
1700
ug/kg
67-72-1
Hexachloroethane
ND
17000
1700
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
17000
1700
ug/kg
78-59-1
Isophorone
ND
17000
1700
ug/kg
91-57-6
2-Methylnaphthalene
167000
17000
1700
ug/kg
91-20-3
Naphthalene
37900
17000
1700
ug/kg
98-95-3
Nitrobenzene
ND
17000
1700
ug/kg
621-64-7
N-Nitroso-di-n-propylamine
ND
17000
1700
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
17000
1700
ug/kg
85-01-8
Phenanthrene
39700
17000
1700
ug/kg
129-00-0
Pyrene
6270
17000
1700
ug/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
0% b
40-102%
4165-62-2
Phenol-d5
0% b
41-100%
118-79-6
2,4,6-Tribromophenol
0% b
42-108%
4165-60-0
Nitrobenzene-d5
0% b
40-105%
321-60-8
2-Fluorobiphenyl
0% b
43-107%
1718-51-0
Terphenyl-d14
0% b
45-119%
(a) Dilution required due to matrix interference.
(b) Outside control limits due to dilution.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■■ 35 of 88
0 ACCUTEST
FA19708 1PBDRATOR15

Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample I D: CS-4-10'
Lab Sample ID: FA19708-6 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: MADEP VPH REV 1.1 Percent Solids. 79.0
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 UV066528.13
1
11/05/14
AH
n/a
n/a
GUV3537
Run #2 UV066543.13
10
11/06/14
AH
n/a
n/a
GUV3538
Initial Weight Final Volume Methanol Aliquot
Run # 1 5.18 g 5.1 ml 10.0 ul
Run #2 5.18 g 5.1 ml 5.0 ul
MADEPVPH List
CAS No.
Compound
Result
RL
M DL
Units Q
71-43-2
Benzene
1430
760
760
ug/kg
100-41-4
Ethylbenzene
30800
1500
760
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
1500
760
ug/kg
91-20-3
Naphthalene
158000
3800
2300
ug/kg
108-88-3
Toluene
15400
1500
760
ug/kg
m,p-Xylene
65000
3000
1500
ug/kg
95-47-6
o-Xylene
56300
1500
760
ug/kg
C5- C8 Aliphatics (Unadj.)
236000
76000
26000
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
76000
26000
ug/kg
C9- C10 Aromatics (Unadj.)
3060000 a
1500000
530000
ug/kg
C5- C8 Aliphatics
219000
76000
26000
ug/kg
C9- C 12 Aliphatics
ND
76000
26000
ug/kg
C9- C 10 Aromatics
3060000 a
1500000
530000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
424% c
0% b
70-130%
460-00-4
BFB
256% c
0% b
70-130%
(a) Result is
from Run# 2
(b) Outside
control limits due to dilution.
(c) Outside
control limits due to matrix interference.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 36 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
,Iient Sample I D: CS-4-10'
.abSample ID: FA19708-6 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: MADEP EPH REV 1.1 SW846 3546 Percent Solids. 79.0
'roj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN010958.13 250 11/13/14 NAF 11/06/14 OP53815 GNN481
Run #2
Initial Weight Final Volume
un # 1 20.1 g 2.0 ml
un #2
MAEPH List
CAS No.
Compound
Result
RL
M DL Units Q
83-32-9
Acenaphthene
62500
63000
31000 ug/kg J
208-96-8
Acenaphthylene
ND
63000
31000 ug/kg
120-12-7
Anthracene
ND
63000
31000 ug/kg
56-55-3
Benzo(a)anthracene
ND
63000
31000 ug/kg
50-32-8
Benzo(a)pyrene
ND
63000
31000 ug/kg
205-99-2
Benzo(b)fluoranthene
ND
63000
31000 ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
63000
31000 ug/kg
207-08-9
Benzo(k)fluoranthene
ND
63000
31000 ug/kg
218-01-9
Chrysene
ND
63000
31000 ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
63000
31000 ug/kg
206-44-0
Fluoranthene
ND
63000
31000 ug/kg
86-73-7
Fluorene
32500
63000
31000 ug/kg J
193-39-5
Indeno(1,2,3-cd)pyrene
ND
63000
31000 ug/kg
91-57-6
2-Methylnaphthalene
307000
63000
31000 ug/kg
91-20-3
Naphthalene
53000
63000
31000 ug/kg J
85-01-8
Phenanthrene
43000
63000
31000 ug/kg J
129-00-0
Pyrene
ND
63000
31000 ug/kg
C11-C22 Aromatics (Unadj.)
12900000
3100000
2400000 ug/kg
C11-C22 Aromatics
12400000
3100000
2400000 ug/kg
C9-C18 Aliphatics
17500000
3100000
1600000 ug/kg
C19-C36 Aliphatics
3920000
3100000
1600000 ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
0% a
40-140%
580-13-2
2-Bromonaphthalene
0% a
40-140%
84-15-1
o-Terphenyl
0% a
40-140%
321-60-8
2-Fluorobiphenyl
0% a
40-140%
(a) Outside control limits due to dilution.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 37 of 88
M ACCUTEST
FA19708 1PBDRATOR15

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-5-10'
Lab Sample ID: FA19708-7 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8260B Percent Solids. 85.3
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 F0067014.D
1
11/06/14
AD
n/a
n/a
VF2291
Run #2 a Y17008.13
1
11/05/14
AD
n/a
n/a
VY747
Initial Weight
Run # 1 6.64 g
Run #2 6.89 g
VOA Special List
CAS No. Compound Result RL M DL Units Q
67-64-1
Acetone
85.6
44
13
ug/kg
71-43-2
Benzene
ND
4.4
0.88
ug/kg
75-27-4
Bromodichloromethane
ND
4.4
0.88
ug/kg
75-25-2
Bromoform
ND
4.4
0.95
ug/kg
104-51-8
n-Butylbenzene
11.5
4.4
0.88
ug/kg
108-90-7
Chlorobenzene
ND
4.4
0.88
ug/kg
75-00-3
Chloroethane
ND
4.4
2.0
ug/kg
67-66-3
Chloroform
ND
4.4
1.0
ug/kg
75-15-0
Carbon disulfide b
ND
4.4
0.88
ug/kg
56-23-5
Carbon tetrachloride
ND
4.4
1.2
ug/kg
110-82-7
Cyclohexane
ND
4.4
0.94
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
4.4
0.88
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
4.4
0.88
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
4.4
1.9
ug/kg
106-93-4
1,2-Dibromoethane
ND
4.4
1.6
ug/kg
107-06-2
1,2-Dichloroethane
ND
4.4
0.88
ug/kg
78-87-5
1,2-Dichloropropane
ND
4.4
0.88
ug/kg
124-48-1
Dibromochloromethane
ND
4.4
0.88
ug/kg
75-71-8
Dichlorodifluoromethane
ND
4.4
1.1
ug/kg
156-59-2
cis-1,2-Dichloroethylene
ND
4.4
0.88
ug/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
4.4
0.88
ug/kg
541-73-1
m-Dichlorobenzene
ND
4.4
0.88
ug/kg
95-50-1
o-Dichlorobenzene
ND
4.4
0.88
ug/kg
106-46-7
p-Dichlorobenzene
ND
4.4
0.99
ug/kg
156-60-5
trans-1,2-Dichloroethylene
ND
4.4
1.2
ug/kg
10061-02-6
trans- 1, 3-Dichloropropene
ND
4.4
0.88
ug/kg
100-41-4
Ethlbenzene
6.9
4.4
0.88
ug/kg
591-78-6
2-Hexanone
ND
22
4.3
ug/kg
98-82-8
Isopropylbenzene
4.1
4.4
0.88
ug/kg
108-10-1
4-Methyl-2-pentanone
ND
22
4.4
ug/kg
79-20-9
Methyl acetate
ND
22
4.4
ug/kg
74-83-9
Methyl bromide
ND
4.4
1.7
ug/kg
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 38 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
,Iient Sample I D: CS-5-10'
.abSample ID: FA19708-7 Date Sampled: 11/04/14
4atrix: SO - Soil Date Received: 11/05/14
Mthod: SW846 8260B Percent Solids. 85.3
'roject: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
VOA Special List
CAS No. Compound
74-87-3
Methyl chloride
108-87-2
Methylcyclohexane
75-09-2
Methylene chloride
78-93-3
Methyl ethyl ketone
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
71-55-6
1, 1, 1 -Trichloroethane
79-34-5
1,1,2,2-Tetrachloroethane
79-00-5
1, 1, 2-Trichloroethane
120-82-1
1,2,4-Trichlorobenzene
95-63-6
1,2,4-Trimethylbenzene
108-67-8
1,3,5-Trimethylbenzene
127-18-4
Tetrachloroethylene
108-88-3
Toluene
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
75-01-4
Vinyl chloride
1330-20-7
Xylene (total)
CAS No. Surrogate Recoveries
Result
RL
M DL
Units Q
ND
4.4
1.8
ug/kg
1.3
4.4
0.88
ug/kg J
ND
8.8
3.5
ug/kg
ND
22
6.6
ug/kg
ND
4.4
0.88
ug/kg
14.3
4.4
1.8
ug/kg
12.4
4.4
0.88
ug/kg
ND
4.4
0.88
ug/kg
ND
4.4
0.88
ug/kg
ND
4.4
1.2
ug/kg
ND
4.4
1.4
ug/kg
ND
4.4
1.0
ug/kg
64.7
4.4
0.88
ug/kg
17.6
4.4
0.88
ug/kg
ND
4.4
1.1
ug/kg
7.5
4.4
0.88
ug/kg
ND
4.4
0.90
ug/kg
ND
4.4
0.88
ug/kg
ND
4.4
0.90
ug/kg
41.2
13
2.3
ug/kg
Run#1 Run#2 Limits
1868-53-7
Dibromofluoromethane
94%
109%
75-124%
2037-26-5
Toluene-D8
92%
93%
75-126%
460-00-4
4-Bromofluorobenzene
116%
110%
71-133%
17060-07-0
1,2-Dichloroethane-D4
105%
106%
72-135%
(a) Confirmation run for internal standard areas.
(b) Associated BS recovery outside control limits.
Page 2 of 2 P
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 39 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of
Client Sample I D: CS-5-10'
Lab Sample ID: FA19708-7 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids. 85.3
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a T015328.1) 5 11/07/14 NJ 11/05/14 OP53802 ST717
Run #2
Initial Weight Final Volume
Run #1 30.2 g 1.0 ml
Run #2
ABN Special List
CAS No. Compound Result RL M DL Units Q
65-85-0
Benzoic Acid
ND
4900
970
ug/kg
95-57-8
2-Chlorophenol
ND
970
97
ug/kg
59-50-7
4-Chloro-3-methyl phenol
ND
970
97
ug/kg
120-83-2
2,4-Dichlorophenol
ND
970
100
ug/kg
105-67-9
2,4-Dimethylphenol
ND
970
110
ug/kg
51-28-5
2,4-Dinitrophenol
ND
4900
970
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
1900
390
ug/kg
95-48-7
2-Methylphenol
ND
970
97
ug/kg
3&4-Methylphenol
ND
970
190
ug/kg
88-75-5
2-Nitrophenol
ND
970
97
ug/kg
100-02-7
4-Nitrophenol
ND
4900
780
ug/kg
87-86-5
Pentachlorophenol
ND
4900
780
ug/kg
108-95-2
Phenol
ND
970
97
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
970
97
ug/kg
83-32-9
Acenaphthene
342
970
120
ug/kg
208-96-8
Acenaphthylene
117
970
97
ug/kg
120-12-7
Anthracene
ND
970
97
ug/kg
56-55-3
Benzo(a)anthracene
ND
970
97
ug/kg
50-32-8
Benzo(a)pyrene
ND
970
97
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
970
97
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
970
97
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
970
110
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
970
97
ug/kg
85-68-7
Butyl benzyl phthalate
ND
970
190
ug/kg
91-58-7
2-Chloronaphthalene
ND
970
120
ug/kg
106-47-8
4-Chloroaniline
ND
970
97
ug/kg
218-01-9
Chrysene
ND
970
97
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
970
97
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
970
97
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
970
100
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
970
140
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
970
110
ug/kg
J
J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■r 40 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
3Iient Sample I D: CS-5-10'
-ab Sample I D: FA19708-7 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: SW846 8270D SW846 3550C Percent Solids. 85.3
project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
ABN Special List
CAS No.
Compound
Result
RL
M DL
Units Q
606-20-2
2, 6-Dinitrotoluene
ND
970
110
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
970
97
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
970
97
ug/kg
132-64-9
Dibenzofuran
140
970
97
ug/kg J
84-74-2
Di-n-butyl phthalate
ND
1900
190
ug/kg
117-84-0
Di-n-octyl phthalate
ND
970
190
ug/kg
84-66-2
Diethyl phthalate
ND
1900
190
ug/kg
131-11-3
Dimethyl phthalate
ND
970
190
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
1900
190
ug/kg
206-44-0
Fluoranthene
ND
970
97
ug/kg
86-73-7
Fluorene
623
970
97
ug/kg J
118-74-1
Hexachlorobenzene
ND
970
97
ug/kg
87-68-3
Hexachlorobutadiene
ND
970
97
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
970
97
ug/kg
67-72-1
Hexachloroethane
ND
970
97
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
970
97
ug/kg
78-59-1
Isophorone
ND
970
97
ug/kg
91-57-6
2-Methylnaphthalene
5550
970
97
ug/kg
91-20-3
Naphthalene
1500
970
97
ug/kg
98-95-3
Nitrobenzene
ND
970
97
ug/kg
621-64-7
N-Nitroso-di-n-propylamine
ND
970
97
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
970
97
ug/kg
85-01-8
Phenanthrene
957
970
97
ug/kg J
129-00-0
Pyrene
373
970
97
ug/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
79%
40-102%
4165-62-2
Phenol-d5
92%
41-100%
118-79-6
2,4,6-Tribromophenol
77%
42-108%
4165-60-0
Nitrobenzene-d5
97%
40-105%
321-60-8
2-Fluorobiphenyl
81%
43-107%
1718-51-0
Terphenyl-d14
88%
45-119%
(a) Dilution required due to matrix interference.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
■V 41 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis Page 1 of 1 P
Client Sample I D: CS-5-10'
Lab Sample ID: FA19708-7 Date Sampled: 11/04/14
Matrix: SO - Soil Date Received: 11/05/14
Method: MADEP VPH REV 1.1 Percent Solids. 85.3
Project: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
Run #1 UV066529.13
1
11/05/14
AH
n/a
n/a
GUV3537
Run #2 UV066546.13
10
11/06/14
AH
n/a
n/a
GUV3538
Initial Weight Final Volume Methanol Aliquot
Run #1 6.07 g 5.1 ml 10.0 ul
Run #2 6.07 g 5.1 ml 50.0 ul
MADEPVPH List
CAS No.
Compound
Result
RL
M DL
Units Q
71-43-2
Benzene
ND
580
580
ug/kg
100-41-4
Ethylbenzene
599
1200
580
ug/kg J
1634-04-4
Methyl Tert Butyl Ether
ND
1200
580
ug/kg
91-20-3
Naphthalene
9960
2900
1700
ug/kg
108-88-3
Toluene
ND
1200
580
ug/kg
m,p-Xylene
1510
2300
1200
ug/kg J
95-47-6
o-Xylene
3320
1200
580
ug/kg
C5- C8 Aliphatics (Unadj.)
ND
58000
20000
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
58000
20000
ug/kg
C9- C10 Aromatics (Unadj.)
357000 a
120000
41000
ug/kg
C5- C8 Aliphatics
ND
58000
20000
ug/kg
C9- C12 Aliphatics
ND
58000
20000
ug/kg
C9- C 10 Aromatics
357000 a
120000
41000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
184% c
0% b
70-130%
460-00-4
BFB
198% c
0% b
70-130%
(a) Result is
from Run# 2
(b) Outside
control limits due to dilution.
(c) Outside
control limits due to matrix interference.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■r 42 of 88
ACCUTEST
FA19708

Accutest Laboratories
Report of Analysis
,Iient Sample I D: CS-5-10'
.abSample ID: FA19708-7 Date Sampled: 11/04/14
mtrix: SO - Soil Date Received: 11/05/14
Mthod: MADEP EPH REV 1.1 SW846 3546 Percent Solids. 85.3
'roj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Page 1 of 1 P
File I D DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN010954.13 5 11/13/14 NAF 11/06/14 OP53815 GNN481
Run #2
Initial Weight Final Volume
un#1 19.7g 2.0m1
un #2
MAEPH List
CAS No.
Compound
Result
RL
M DL
Units Q
83-32-9
Acenaphthene
1440
1200
600
ug/kg
208-96-8
Acenaphthylene
ND
1200
600
ug/kg
120-12-7
Anthracene
ND
1200
600
ug/kg
56-55-3
Benzo(a)anthracene
ND
1200
600
ug/kg
50-32-8
Benzo(a)pyrene
ND
1200
600
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
1200
600
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
1200
600
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
1200
600
ug/kg
218-01-9
Chrysene
ND
1200
600
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
1200
600
ug/kg
206-44-0
Fluoranthene
ND
1200
600
ug/kg
86-73-7
Fluorene
903
1200
600
ug/kg J
193-39-5
Indeno(1,2,3-cd)pyrene
ND
1200
600
ug/kg
91-57-6
2-Methylnaphthalene
5580
1200
600
ug/kg
91-20-3
Naphthalene
744
1200
600
ug/kg J
85-01-8
Phenanthrene
601
1200
600
ug/kg J
129-00-0
Pyrene
ND
1200
600
ug/kg
C11-C22 Aromatics (Unadj.)
348000
60000
45000
ug/kg
C11-C22 Aromatics
338000
60000
45000
ug/kg
C9-C18 Aliphatics
615000
60000
30000
ug/kg
C19-C36 Aliphatics
163000
60000
30000
ug/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
80%
40-140%
580-13-2
2-Bromonaphthalene
181% a
40-140%
84-15-1
o-Terphenyl
113%
40-140%
321-60-8
2-Fluorobiphenyl
128%
40-140%
(a) Outside control limits due to matrix interference.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
■■ 43 of 88
■ ACCUTEST
FA19708

Section 4
Southeast
E ACCUTEST
L A B O RAT D R I ES
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
■■ 44 of 88
E ACCUTEBT
FA19708 `A.... .1-

Accutest Laboratories Southeast
Chain of Custody Fjo a �.ACCUTEST 440SVinelardRoad,SuitcC-15 prlando, ^ 32811Accute PAGE OOFT
LABORATORIES TEL. 407-425-G700 • FAX: [phone] CCuteSt UOte
www.accutest.com
Client/Re orti IMormahon :::�+"".e_+-„ :.:..:,- _.. Pro eM. IMonnation .,ww' :� Anal vat Information .,,.a„�; :":�" Matdx Codes
Company Name tP7EcLo xcgL (LZSvu,Cdc'u; _,�,at.v
Prolact Name:
1-0Ly I�..dGK. rA}zLyNtit� Ce:.rse
M
(�
O
t o
�.n
M
b�.1
W
d y
O
r*
Dw. onnlang water
Gw - Ground Water
WW - Water
SW - Surface Water
so•SW
SIO sludge
a-o7
LIO-Other Liquid
AIR -Air
SOI-- Other Sdid
WP - wipe
I LAB USE ONLY
/ ./
Address JSOL /dqr LS r^�.iri
SIree1 Irr3 rwz(-N(-ir}N nORp
r,
G •.�6u ? stale P'L zi &tic
city C �t.Dl'f Slate N
Y1Yk S_
Project COn[act� RA �� E-mail
M.T.Q4
ProledF
Phone#
0tt f?4 r— /a/O
Fax#
Sample(s) Namets) (Printed)
C uF'r; f�µcri ggiu 4+v
Client Purchase Order x
c test
sample
Field ID / Point of Collection
on
0.ram.ED
MATRIX
roraL<
eF
g
s
-
fi _ 1 rani trh�
I
q�
'
-n
Kt
I
'
E4'.T A' 1-4-71
1
1007-
oif,
So
3
S—{-lo" ia-
v4s
I
�
1
1131,
`/.
's - `I -W me
Nsn
}C
S
"lv1 1/L
TURNAROUND TIME Business Days)
Data
Deliverable
Information
M"++a
Comments
/
Remarks
Approved By: / Rush Code
❑ 1 D Days Standard Approved
7 Day RUSH ._ _
❑ 5Day RUSH —_-. _
❑ 3Day EMERGENCY
❑ 2 Day EMERGENCY
❑ 1 Day EMERGENCY _--_--_,.-
❑ OTHER
Emergency or Rush T/A Data Available VIA Email or Lablink
COMMERCIAL 'A" ( RESULTS ONLY)
'"
❑ COMMERCIAL "B"(RESULTS PLUS OC)
�REDTi(EPA LEVEL 3) ACCUT73T
��jj����QQ _
El FULT1 (EPAtL 28—C 7 Q U-7 EN C : T ( DR
DEDD-S CC 1 NC "82 J13 (J
QL
Sam
le Criatody must be
documented below each time samples change possession. indudin courier clelhrem
Received By: `'� -r Relin uishe b Dat Tinme: Recei B
2 '149�Z `�� "":t Zfi J 9 9 Y—(J-S'1 W 3V 4
Relln U h by Sampler:
1
Date Time:
11 t tiro
Relinquished bye
5
Date Time:
Received By:
6
Relinquished by:
7
Date Time:
1
Received By:
S
Lab Use Only: Custody Seal in Place: Y N Temp Blank Provided: Y N Preserved where Applicable: Y N Total # of Coolers: Cooler Temperature (a) Celsius: ,
FA19708: Chain of Custody
Page 1 of 3
■ 45 of 88
ACCUTEST
FA19708

ACCUTEST LABORATORIES SAMPLE RECEIPT CONFIRMATION
ACCUTEST'SJOB NUMBER: _ a CLIENT:_ 0,PST PROJECT: I ke GC.
GC U)u�S\�:
DATE/TIME RFCF.IVED:_IL-O 5 -1 y Knn '36 (MM/DDP1'Y 24:00) NUMBER OF COOLERS RECEIVED:
METHOD OF DELIVERY: FEDEX UPS ACCUTEST COURIER DELIVERY OTHER:
AIRBILL NUMBERS:- LqQ K 3 of r7i q
COOLER INFORMATION TEMPERATURE INFORMATION
?
CUSTODY SEAL NOT PRESENT OR NOT INTACT 1R THERM ID I CORR. FACTOR -F G'
CHAIN OF CUSTODY NOT RECEIVED (COC) OBSERVED TEMPS: 2. 6
ANALYSIS REQUESTED 1S UNCLEAR OR MISSING CORRECTED TEMPS: J D
SAMPLE DATES OR TIMES UNCLEAR OR MISSING SAMPLE INFORMATION
TEMPERATURE CRITERIA NOT MET INCORRECT NUMBER OF CONTAINERS USED
SAMPLE RECEIVED IMPROPERLY PRESERVED
TRIP BLANK INFORMATION
INSUFFICIENT VOLUME FOR ANALYSIS
TRIP BLANK. PROVIDED . DATES/TIMES ON COC DO NOT MATCH SAMPLE LABEL
TRIP BLANK NOT PROVIDED ID'S ON COC DO NOT MATCH LABEL
TRIP BLANK NOT ON COC VOC VIALS HAVE HEADSPACE (MACRO BUBBLES)
TRIP BLANK INTACT BOTTLES RECEIVED BUT ANALYSIS NOT REQUESTED
TRIP BLANK NOT INTACT NO BOTTLES RECEIVED FOR ANALYSIS REQUESTED
RECEIVED WATER TRIP BLANK UNCLEAR FILTERING OR COMPOSITING INSTRUCTIONS
RECEIVED SOIL TRIP BLANK SAMPLE CONTAINER(S) RECEIVED BROKEN
5035 FIELD KITS NOT RECEIVED WITHIN 48 HOURS
MISC. INFORMATION
BULK VOA SOIL JARS NOT RECEIVED WITHIN 48 HOURS
NUMBER OF ENCORES? 25-GRAM 5-GRAM % SOLIDS JAR NOT RECEIVED
NUMBER OF 5035 FIELD KITS ? 7— RESIDUAL CHLORINE PRESENT LOT# 14-860
NUMBER OF LAB FILTERED METALS ? (APPLICABLE TO EPA 600 SERIES OR NORTII CAROLINA ORGANICS)
pH PAPER LOT#s WD)E RANGE, A636122 NARROW RANGE— HC421754 OTHER (specify) 405-230010
SUMMARY OF COMMENTS:
TECHNICIAN SIGNATURE/DATE EVIEWER SIGNATURE/DATE I- S- i q
NF 10/14 receipt confirmation 102914.x1s
FA19708: Chain of Custody
Page 2 of 3
■ 46 of 88
E ACCUTEST
FA19708

4
Fan#asuorua
j
W
w
a�
ogm
Uj
CD
cc
01)
In OO
co G M
..I�
a
�-- u.w i7
cry
..IT
W Z C2
€
uY
at
c.a c W
_
00
--
'
z
a
i
FA19708: Chain of Custody
Page 3 of 3
L
a
■ 47 of 88
Xs, CCUTEST
FA19708

Section 5
Southeast
■ ,�.ccuTEST
L A H OR AT OR E E 5
GUMS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
■ 48 of 88
ACCUTEST
FA19708

Method Blank Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY747-MB
Y16986.D
1
11/05/14
AD
n/a
n/a
VY747
The QC reported here applies to the fol I owing samples:
FA19708-3, FA19708-4, FA19708-5, FA19708-6
CAS No. Compound
Result RL
Method: SW846 8260B
M DL Units Q
67-64-1
Acetone
ND
50
15
ug/kg
71-43-2
Benzene
ND
5.0
1.0
ug/kg
75-27-4
Bromodichloromethane
ND
5.0
1.0
ug/kg
75-25-2
Bromoform
ND
5.0
1.1
ug/kg
104-51-8
n-Butylbenzene
ND
5.0
1.0
ug/kg
108-90-7
Chlorobenzene
ND
5.0
1.0
ug/kg
75-00-3
Chloroethane
ND
5.0
2.3
ug/kg
67-66-3
Chloroform
ND
5.0
1.1
ug/kg
75-15-0
Carbon disulfide
ND
5.0
1.0
ug/kg
56-23-5
Carbon tetrachloride
ND
5.0
1.4
ug/kg
110-82-7
Cyclohexane
ND
5.0
1.1
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
5.0
1.0
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
5.0
1.0
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
5.0
2.1
ug/kg
106-93-4
1,2-Dibromoethane
ND
5.0
1.8
ug/kg
107-06-2
1,2-Dichloroethane
ND
5.0
1.0
ug/kg
78-87-5
1,2-Dichloropropane
ND
5.0
1.0
ug/kg
124-48-1
Dibromochloromethane
ND
5.0
1.0
ug/kg
75-71-8
Dichlorodifluoromethane
ND
5.0
1.3
ug/kg
156-59-2
cis- 1, 2-Dichloroethylene
ND
5.0
1.0
ug/kg
10061-01-5 cis- 1, 3 -Dichloropropene
ND
5.0
1.0
ug/kg
541-73-1
m-Dichlorobenzene
ND
5.0
1.0
ug/kg
95-50-1
o-Dichlorobenzene
ND
5.0
1.0
ug/kg
106-46-7
p-Dichlorobenzene
ND
5.0
1.1
ug/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
5.0
1.3
ug/kg
10061-02-6 trans- 1, 3 -Dichloropropene
ND
5.0
1.0
ug/kg
100-41-4
Ethylbenzene
ND
5.0
1.0
ug/kg
591-78-6
2-Hexanone
ND
25
4.9
ug/kg
98-82-8
Isopropylbenzene
ND
5.0
1.0
ug/kg
108-10-1
4-Methyl-2-pentanone
ND
25
5.0
ug/kg
79-20-9
Methyl acetate
ND
25
5.0
ug/kg
74-83-9
Methyl bromide
ND
5.0
1.9
ug/kg
74-87-3
Methyl chloride
ND
5.0
2.0
ug/kg
108-87-2
Methylcyclohexane
ND
5.0
1.0
ug/kg
75-09-2
Methylene chloride
ND
10
4.0
ug/kg
78-93-3
Methyl ethyl ketone
ND
25
7.5
ug/kg
■ 49 of 88
ACCUTEST
FA19708

Method Blank Summary Page 2 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY747-MB
Y16986.D
1
11/05/14
AD
n/a
n/a
VY747
The QC reported here applies to the fol lowing samples: Method: SW846 8260B
FA19708-3, FA19708-4, FA19708-5, FA19708-6
CAS No.
Compound
Result
RL
M DL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
5.0
1.0
ug/kg
91-20-3
Naphthalene
ND
5.0
2.0
ug/kg
103-65-1
n-Propylbenzene
ND
5.0
1.0
ug/kg
100-42-5
Styrene
ND
5.0
1.0
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
5.0
1.0
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
5.0
1.4
ug/kg
79-00-5
1,1,2-Trichloroethane
ND
5.0
1.6
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
1.2
ug/kg
95-63-6
1,2,4-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-67-8
1,3,5-Trimethylbenzene
ND
5.0
1.0
ug/kg
127-18-4
Tetrachloroethylene
ND
5.0
1.3
ug/kg
108-88-3
Toluene
ND
5.0
1.0
ug/kg
79-01-6
Trichloroethylene
ND
5.0
1.0
ug/kg
75-69-4
Trichlorofluoromethane
ND
5.0
1.0
ug/kg
75-01-4
Vinyl chloride
ND
5.0
1.0
ug/kg
1330-20-7
Xylene (total)
ND
15
2.7
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
108%
75-124%
2037-26-5
Toluene-D8
104%
75-126%
460-00-4
4-Bromofluorobenzene
109%
71-133%
17060-07-0
1,2-Dichloroethane-D4
102%
72-135%
■■ 50 of 88
M ACCUTEST
FA19708 1PBDRATOR15

Method Blank Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
dF2291-MB
F0067009.D 1
11/06/14
AD
n/a
n/a
VF2291
The QC reported here applies to the following samples: Method: SW846 8260B
FA19708-6, FA19708-7
CAS No. Compound Result RL MDL Units Q
67-64-1
Acetone
ND
50
15
ug/kg
71-43-2
Benzene
ND
5.0
1.0
ug/kg
75-27-4
Bromodichloromethane
ND
5.0
1.0
ug/kg
75-25-2
Bromoform
ND
5.0
1.1
ug/kg
104-51-8
n-Butylbenzene
ND
5.0
1.0
ug/kg
108-90-7
Chlorobenzene
ND
5.0
1.0
ug/kg
75-00-3
Chloroethane
ND
5.0
2.3
ug/kg
67-66-3
Chloroform
ND
5.0
1.1
ug/kg
75-15-0
Carbon disulfide
ND
5.0
1.0
ug/kg
56-23-5
Carbon tetrachloride
ND
5.0
1.4
ug/kg
110-82-7
Cyclohexane
ND
5.0
1.1
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
5.0
1.0
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
5.0
1.0
ug/kg
96-12-8
1,2-Dibromo-3-chloropropane
ND
5.0
2.1
ug/kg
106-93-4
1,2-Dibromoethane
ND
5.0
1.8
ug/kg
107-06-2
1,2-Dichloroethane
ND
5.0
1.0
ug/kg
78-87-5
1,2-Dichloropropane
ND
5.0
1.0
ug/kg
124-48-1
Dibromochloromethane
ND
5.0
1.0
ug/kg
75-71-8
Dichlorodifluoromethane
ND
5.0
1.3
ug/kg
156-59-2
cis- 1, 2-Dichloroethylene
ND
5.0
1.0
ug/kg
10061-01-5 cis- 1, 3 -Dichloropropene
ND
5.0
1.0
ug/kg
541-73-1
m-Dichlorobenzene
ND
5.0
1.0
ug/kg
95-50-1
o-Dichlorobenzene
ND
5.0
1.0
ug/kg
106-46-7
p-Dichlorobenzene
ND
5.0
1.1
ug/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
5.0
1.3
ug/kg
10061-02-6 trans- 1, 3 -Dichloropropene
ND
5.0
1.0
ug/kg
100-41-4
Ethylbenzene
ND
5.0
1.0
ug/kg
591-78-6
2-Hexanone
ND
25
4.9
ug/kg
98-82-8
Isopropylbenzene
ND
5.0
1.0
ug/kg
108-10-1
4-Methyl-2-pentanone
ND
25
5.0
ug/kg
79-20-9
Methyl acetate
ND
25
5.0
ug/kg
74-83-9
Methyl bromide
ND
5.0
1.9
ug/kg
74-87-3
Methyl chloride
ND
5.0
2.0
ug/kg
108-87-2
Methylcyclohexane
ND
5.0
1.0
ug/kg
75-09-2
Methylene chloride
ND
10
4.0
ug/kg
78-93-3
Methyl ethyl ketone
ND
25
7.5
ug/kg
■■ 51 of 88
M ACCUTEST
FA19708 1PBDRATOR15

Method Blank Summary Page 2 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VF2291-MB
F0067009.D 1
11/06/14
AD
n/a
n/a
VF2291
The QC reported here applies to the fol lowing samples: Method: SW846 8260B
FA19708-6, FA19708-7
CAS No.
Compound
Result
RL
M DL
Units Q
1634-04-4
Methyl Tert Butyl Ether
ND
5.0
1.0
ug/kg
91-20-3
Naphthalene
ND
5.0
2.0
ug/kg
103-65-1
n-Propylbenzene
ND
5.0
1.0
ug/kg
100-42-5
Styrene
ND
5.0
1.0
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
5.0
1.0
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
5.0
1.4
ug/kg
79-00-5
1,1,2-Trichloroethane
ND
5.0
1.6
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
1.2
ug/kg
95-63-6
1,2,4-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-67-8
1,3,5-Trimethylbenzene
ND
5.0
1.0
ug/kg
127-18-4
Tetrachloroethylene
ND
5.0
1.3
ug/kg
108-88-3
Toluene
ND
5.0
1.0
ug/kg
79-01-6
Trichloroethylene
ND
5.0
1.0
ug/kg
75-69-4
Trichlorofluoromethane
ND
5.0
1.0
ug/kg
75-01-4
Vinyl chloride
ND
5.0
1.0
ug/kg
1330-20-7
Xylene (total)
ND
15
2.7
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
91%
75-124%
2037-26-5
Toluene-D8
95%
75-126%
460-00-4
4-Bromofluorobenzene
113%
71-133%
17060-07-0
1,2-Dichloroethane-D4
90%
72-135%
■ 52 of 88
ACCUTEST
FA19708

Blank Spike Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY747-BS
Y16985.1)
1
11/05/14
AD
n/a
n/a
VY747
The QC reported here applies to the following samples: Method: SW846 8260B
FA19708-3, FA19708-4, FA19708-5, FA19708-6
Spike BSP BSP
CAS No. Compound ug/kg ug/kg % Limits
67-64-1
Acetone
250
237
95
61-152
71-43-2
Benzene
50
51.4
103
76-126
75-27-4
Bromodichloromethane
50
50.7
101
74-130
75-25-2
Bromoform
50
50.5
101
76-127
104-51-8
n-Butylbenzene
50
50.0
100
71-128
108-90-7
Chlorobenzene
50
55.3
ill
81-129
75-00-3
Chloroethane
50
54.9
110
68-133
67-66-3
Chloroform
50
50.3
101
72-123
75-15-0
Carbon disulfide
50
57.4
115
72-122
56-23-5
Carbon tetrachloride
50
52.6
105
78-133
110-82-7
Cyclohexane
50
49.5
99
73-126
75-34-3
1, 1 -Dichloroethane
50
50.0
100
73-125
75-35-4
1, 1 -Dichloroethylene
50
48.8
98
81-136
96-12-8
1,2-Dibromo-3-chloropropane
50
44.4
89
70-137
106-93-4
1,2-Dibromoethane
50
52.4
105
77-126
107-06-2
1,2-Dichloroethane
50
47.0
94
74-128
78-87-5
1,2-Dichloropropane
50
49.8
100
74-125
124-48-1
Dibromochloromethane
50
52.1
104
76-127
75-71-8
Dichlorodifluoromethane
50
61.7
123
68-168
156-59-2
cis- 1, 2-Dichloroethylene
50
51.7
103
74-126
10061-01-5 cis- 1, 3 -Dichloropropene
50
50.5
101
80-123
541-73-1
m-Dichlorobenzene
50
57.1
114
81-129
95-50-1
o-Dichlorobenzene
50
56.6
113
80-129
106-46-7
p-Dichlorobenzene
50
51.7
103
76-130
156-60-5
trans- 1, 2-Dichloroethylene
50
49.5
99
70-127
10061-02-6 trans- 1, 3 -Dichloropropene
50
53.4
107
75-131
100-41-4
Ethylbenzene
50
51.7
103
77-123
591-78-6
2-Hexanone
250
221
88
72-133
98-82-8
Isopropylbenzene
50
57.0
114
80-136
108-10-1
4-Methyl-2-pentanone
250
220
88
76-132
79-20-9
Methyl acetate
250
269
108
67-137
74-83-9
Methyl bromide
50
54.4
109
65-139
74-87-3
Methyl chloride
50
55.5
ill
71-144
108-87-2
Methylcyclohexane
50
52.1
104
75-128
75-09-2
Methylene chloride
50
51.9
104
74-137
78-93-3
Methyl ethyl ketone
250
222
89
75-137
* = Outside of Control Limits.
■ 53 of 88
ACC UTEST
FA19708

Blank Spike Summary Page 2 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VY747-BS
Y16985.1)
1
11/05/14
AD
n/a
n/a
VY747
The QC reported here applies to the fol lowing samples:
FA19708-3, FA19708-4, FA19708-5, FA19708-6
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
1634-04-4
Methyl Tert Butyl Ether
50
47.7
95
77-120
91-20-3
Naphthalene
50
43.7
87
79-129
103-65-1
n-Propylbenzene
50
54.1
108
80-135
100-42-5
Styrene
50
53.3
107
78-125
71-55-6
1,1,1-Trichloroethane
50
50.6
101
70-129
79-34-5
1,1,2,2-Tetrachloroethane
50
46.8
94
71-126
79-00-5
1,1,2-Trichloroethane
50
48.5
97
74-124
120-82-1
1,2,4-Trichlorobenzene
50
53.5
107
78-130
95-63-6
1,2,4-Trimethylbenzene
50
51.1
102
74-123
108-67-8
1,3,5-Trimethylbenzene
50
50.3
101
73-122
127-18-4
Tetrachloroethylene
50
58.7
117
79-130
108-88-3
Toluene
50
51.1
102
76-124
79-01-6
Trichloroethylene
50
52.1
104
75-128
75-69-4
Trichlorofluoromethane
50
57.3
115
73-145
75-01-4
Vinyl chloride
50
53.0
106
76-141
1330-20-7
Xylene (total)
150
163
109
80-129
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
105%
75-124%
2037-26-5
Toluene-D8
104%
75-126%
460-00-4
4-Bromofluorobenzene
106%
71-133%
17060-07-0
1,2-Dichloroethane-D4
90%
72-135%
* = Outside of Control Limits.
Method: SW846 8260B
■ 54 of 88
ACC UTEST
FA19708

Blank Spike Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VF2291-BS
F0067008.D 1
11/06/14
AD
n/a
n/a
VF2291
The QC reported here applies to the following samples: Method: SW846 8260B
FA19708-6, FA19708-7
CAS No. Compound
Spike BSP BSP
ug/kg ug/kg % Limits
67-64-1
Acetone
250
333
133
61-152
71-43-2
Benzene
50
56.4
113
76-126
75-27-4
Bromodichloromethane
50
58.1
116
74-130
75-25-2
Bromoform
50
48.2
96
76-127
104-51-8
n-Butylbenzene
50
56.7
113
71-128
108-90-7
Chlorobenzene
50
59.9
120
81-129
75-00-3
Chloroethane
50
63.9
128
68-133
67-66-3
Chloroform
50
55.6
ill
72-123
75-15-0
Carbon disulfide
50
70.6
141*
72-122
56-23-5
Carbon tetrachloride
50
54.4
109
78-133
110-82-7
Cyclohexane
50
51.3
103
73-126
75-34-3
1, 1 -Dichloroethane
50
55.7
ill
73-125
75-35-4
1, 1 -Dichloroethylene
50
55.7
ill
81-136
96-12-8
1,2-Dibromo-3-chloropropane
50
60.5
121
70-137
106-93-4
1,2-Dibromoethane
50
57.7
115
77-126
107-06-2
1,2-Dichloroethane
50
56.7
113
74-128
78-87-5
1,2-Dichloropropane
50
56.6
113
74-125
124-48-1
Dibromochloromethane
50
59.8
120
76-127
75-71-8
Dichlorodifluoromethane
50
50.1
100
68-168
156-59-2
cis- 1, 2-Dichloroethylene
50
55.9
112
74-126
10061-01-5 cis- 1, 3 -Dichloropropene
50
56.9
114
80-123
541-73-1
m-Dichlorobenzene
50
59.4
119
81-129
95-50-1
o-Dichlorobenzene
50
62.9
126
80-129
106-46-7
p-Dichlorobenzene
50
57.0
114
76-130
156-60-5
trans- 1, 2-Dichloroethylene
50
55.4
ill
70-127
10061-02-6 trans- 1, 3 -Dichloropropene
50
58.7
117
75-131
100-41-4
Ethylbenzene
50
56.9
114
77-123
591-78-6
2-Hexanone
250
285
114
72-133
98-82-8
Isopropylbenzene
50
60.7
121
80-136
108-10-1
4-Methyl-2-pentanone
250
296
118
76-132
79-20-9
Methyl acetate
250
339
136
67-137
74-83-9
Methyl bromide
50
56.8
114
65-139
74-87-3
Methyl chloride
50
50.6
101
71-144
108-87-2
Methylcyclohexane
50
53.7
107
75-128
75-09-2
Methylene chloride
50
57.5
115
74-137
78-93-3
Methyl ethyl ketone
250
281
112
75-137
* = Outside of Control Limits.
■ 55 of 88
ACC UTEST
FA19708

Blank Spike Summary Page 2 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
VF2291-BS
F0067008.D 1
11/06/14
AD
n/a
n/a
VF2291
The QC reported here applies to the fol lowing samples:
FA19708-6, FA19708-7
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
1634-04-4
Methyl Tert Butyl Ether
50
54.3
109
77-120
91-20-3
Naphthalene
50
60.4
121
79-129
103-65-1
n-Propylbenzene
50
62.9
126
80-135
100-42-5
Styrene
50
56.1
112
78-125
71-55-6
1,1,1-Trichloroethane
50
55.3
ill
70-129
79-34-5
1,1,2,2-Tetrachloroethane
50
58.8
118
71-126
79-00-5
1,1,2-Trichloroethane
50
55.3
ill
74-124
120-82-1
1,2,4-Trichlorobenzene
50
60.3
121
78-130
95-63-6
1,2,4-Trimethylbenzene
50
58.2
116
74-123
108-67-8
1,3,5-Trimethylbenzene
50
57.7
115
73-122
127-18-4
Tetrachloroethylene
50
57.1
114
79-130
108-88-3
Toluene
50
55.4
ill
76-124
79-01-6
Trichloroethylene
50
56.7
113
75-128
75-69-4
Trichlorofluoromethane
50
56.5
113
73-145
75-01-4
Vinyl chloride
50
51.3
103
76-141
1330-20-7
Xylene (total)
150
179
119
80-129
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
92%
75-124%
2037-26-5
Toluene-D8
93%
75-126%
460-00-4
4-Bromofluorobenzene
111%
71-133%
17060-07-0
1,2-Dichloroethane-D4
88%
72-135%
* = Outside of Control Limits.
Method: SW846 8260B
■ 56 of 88
ACC UTEST
FA19708

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA19680-3MS
Y16993.1)
1
11/05/14
AD
n/a
n/a
VY747
FA19680-3MSD
Y16994.1)
1
11/05/14
AD
n/a
n/a
VY747
FA19680-3
Y16992.1)
1
11/05/14
AD
n/a
n/a
VY747
The QC reported here applies to the fol I owing samples: Method: SW846 8260B
FA19708-3, FA19708-4, FA19708-5, FA19708-6
FA19680-3
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
67-64-1
Acetone
29.2 J
392
351
82
365
358
90
2
61-152/27
71-43-2
Benzene
ND
78.3
74.2
95
73
67.4
92
10
76-126/26
75-27-4
Bromodichloromethane
ND
78.3
72.8
93
73
68.2
93
7
74-130/25
75-25-2
Bromoform
ND
78.3
73.5
94
73
69.8
96
5
76-127/26
104-51-8
n-Butylbenzene
ND
78.3
73.2
93
73
64.2
88
13
71-128/35
108-90-7
Chlorobenzene
ND
78.3
78.9
101
73
70.9
97
11
81-129/29
75-00-3
Chloroethane
ND
78.3
82.6
105
73
57.6
79
36*
68-133/29
67-66-3
Chloroform
ND
78.3
73.2
93
73
66.6
91
9
72-123/26
75-15-0
Carbon disulfide
1.4 J
78.3
71.7
90
73
74.1
100
3
72-122/29
56-23-5
Carbon tetrachloride
ND
78.3
72.9
93
73
64.7
89
12
78-133/29
110-82-7
Cyclohexane
ND
78.3
68.6
88
73
60.5
83
13
73-126/32
75-34-3
1, 1 -Dichloroethane
ND
78.3
72.2
92
73
65.3
89
10
73-125/27
75-35-4
1, 1 -Dichloroethylene
ND
78.3
65.5
84
73
62.2
85
5
81-136/28
96-12-8
1,2-Dibromo-3-chloropropane
ND
78.3
64.8
83
73
63.8
87
2
70-137/29
106-93-4
1,2-Dibromoethane
ND
78.3
74.0
94
73
68.0
93
8
77-126/26
107-06-2
1,2-Dichloroethane
ND
78.3
69.9
89
73
65.4
90
7
74-128/23
78-87-5
1,2-Dichloropropane
ND
78.3
73.7
94
73
67.5
92
9
74-125/25
124-48-1
Dibromochloromethane
ND
78.3
74.0
94
73
68.4
94
8
76-127/27
75-71-8
Dichlorodifluoromethane
ND
78.3
80.4
103
73
74.4
102
8
68-168/29
156-59-2
cis- 1, 2-Dichloroethylene
ND
78.3
73.1
93
73
68.3
94
7
74-126/26
10061-01-5 cis-1,3-Dichloropropene
ND
78.3
73.6
94
73
68.5
94
7
80-123/26
541-73-1
m-Dichlorobenzene
ND
78.3
82.2
105
73
73.2
100
12
81-129/33
95-50-1
o-Dichlorobenzene
ND
78.3
80.3
103
73
74.6
102
7
80-129/32
106-46-7
p-Dichlorobenzene
ND
78.3
74.9
96
73
67.7
93
10
76-130/32
156-60-5
trans- 1, 2-Dichloroethylene
ND
78.3
71.0
91
73
65.8
90
8
70-127/27
10061-02-6 trans-1,3-Dichloropropene
ND
78.3
77.3
99
73
69.4
95
11
75-131/28
100-41-4
Ethylbenzene
ND
78.3
72.9
93
73
65.0
89
11
77-123/31
591-78-6
2-Hexanone
ND
392
331
85
365
323
88
2
72-133/26
98-82-8
Isopropylbenzene
ND
78.3
80.2
102
73
71.2
98
12
80-136/32
108-10-1
4-Methyl-2-pentanone
ND
392
338
86
365
328
90
3
76-132/26
79-20-9
Methyl acetate
ND
392
403
103
365
396
108
2
67-137/30
74-83-9
Methyl bromide
ND
78.3
80.7
103
73
69.6
95
15
65-139/31
74-87-3
Methyl chloride
ND
78.3
80.1
102
73
71.9
98
11
71-144/27
108-87-2
Methylcyclohexane
ND
78.3
67.3
86
73
60.1
82
11
75-128/31
75-09-2
Methylene chloride
ND
78.3
81.7
104
73
75.6
104
8
74-137/28
78-93-3
Methyl ethyl ketone
ND
392
333
85
365
330
90
1
75-137/25
* = Outside of Control Limits.
■■ 57 of 88
ACCUTEST
FA19708

Matrix Spike/Matrix Spike Duplicate Summary Page 2of2
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
ample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcr
A19680-3MS
Y16993.1)
1
11/05/14
AD
n/a
n/a
VY747
A19680-3MSD
Y16994.1)
1
11/05/14
AD
n/a
n/a
VY747
A19680-3
Y16992.1)
1
11/05/14
AD
n/a
n/a
VY747
The QC reported here applies to the fol lowing samples:
FA19708-3, FA19708-4, FA19708-5, FA19708-6
Method: SW846 8260B
FA19680-3
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
1634-04-4
Methyl Tert Butyl Ether
ND
78.3
70.7
90
73
68.2
93
4
77-120/24
91-20-3
Naphthalene
ND
78.3
70.0
89
73
67.9
93
3
79-129/33
103-65-1
n-Propylbenzene
ND
78.3
76.8
98
73
68.1
93
12
80-135/33
100-42-5
Styrene
ND
78.3
77.8
99
73
69.4
95
11
78-125/30
71-55-6
1, 1, 1-Trichloroethane
ND
78.3
74.2
95
73
64.4
88
14
70-129/27
79-34-5
1,1,2,2-Tetrachloroethane
ND
78.3
70.5
90
73
67.3
92
5
71-126/30
79-00-5
1,1,2-Trichloroethane
ND
78.3
72.2
92
73
66.0
90
9
74-124/28
120-82-1
1,2,4-Trichlorobenzene
ND
78.3
82.6
105
73
76.0
104
8
78-130/34
95-63-6
1,2,4-Trimethylbenzene
ND
78.3
74.2
95
73
66.2
91
11
74-123/34
108-67-8
1,3,5-Trimethylbenzene
ND
78.3
72.1
92
73
64.5
88
11
73-122/33
127-18-4
Tetrachloroethylene
ND
78.3
74.6
95
73
65.5
90
13
79-130/31
108-88-3
Toluene
ND
78.3
72.5
93
73
64.8
89
11
76-124/30
79-01-6
Trichloroethylene
ND
78.3
72.4
92
73
66.6
91
8
75-128/27
75-69-4
Trichlorofluoromethane
ND
78.3
77.9
99
73
70.6
97
10
73-145/31
75-01-4
Vinyl chloride
ND
78.3
77.4
99
73
69.7
95
10
76-141/27
1330-20-7
Xylene (total)
ND
235
231
98
219
206
94
11
80-129/30
CAS No.
Su r r ogate Recover i es
MS
MSD
FA19680-3
Limits
1868-53-7
Dibromofluoromethane
104%
107%
108%
75-124%
2037-26-5
Toluene-138
102%
101%
100%
75-126%
460-00-4
4-Bromofluorobenzene
104%
104%
109%
71-133%
17060-07-0
1,2-Dichloroethane-D4
92%
94%
112%
72-135%
* = Outside of Control Limits.
■ 58 of 88
ACCUTEST
FA19708

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA19708-6MS
F0067012.D
1
11/06/14
AD
n/a
n/a
VF2291
FA19708-6MSD
F0067013.D
1
11/06/14
AD
n/a
n/a
VF2291
FA19708-6
F0067011.D
1
11/06/14
AD
n/a
n/a
VF2291
The QC reported here applies to the fol I owing samples:
FA19708-6, FA19708-7
CAS No. Compound
FA19708-6 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
67-64-1
Acetone
ND
181000
231000
128
181000
210000
116
10
61-152/27
71-43-2
Benzene
739
J 36200
37400
101
36200
38400
104
3
76-126/26
75-27-4
Bromodichloromethane
ND
36200
38100
105
36200
39700
110
4
74-130/25
75-25-2
Bromoform
ND
36200
34300
95
36200
36600
101
6
76-127/26
104-51-8
n-Butylbenzene
13100
36200
51800
107
36200
57600
123
11
71-128/35
108-90-7
Chlorobenzene
ND
36200
39500
109
36200
40500
112
3
81-129/29
75-00-3
Chloroethane
ND
36200
25700
71
36200
32200
89
22
68-133/29
67-66-3
Chloroform
ND
36200
37800
104
36200
40100
111
6
72-123/26
75-15-0
Carbon disulfide
ND
36200
44100
122
36200
46100
127*
4
72-122/29
56-23-5
Carbon tetrachloride
ND
36200
35100
97
36200
38500
106
9
78-133/29
110-82-7
Cyclohexane
1930
J 36200
38500
101
36200
40600
107
5
73-126/32
75-34-3
1, 1 -Dichloroethane
ND
36200
39300
109
36200
39200
108
0
73-125/27
75-35-4
1, 1 -Dichloroethylene
ND
36200
35800
99
36200
37300
103
4
81-136/28
96-12-8
1,2-Dibromo-3-chloropropane
ND
36200
43600
120
36200
49800
137
13
70-137/29
106-93-4
1,2-Dibromoethane
ND
36200
40800
113
36200
42700
118
5
77-126/26
107-06-2
1,2-Dichloroethane
ND
36200
39400
109
36200
39800
110
1
74-128/23
78-87-5
1,2-Dichloropropane
ND
36200
38300
106
36200
38900
107
2
74-125/25
124-48-1
Dibromochloromethane
ND
36200
38400
106
36200
41600
115
8
76-127/27
75-71-8
Dichlorodifluoromethane
ND
36200
36000
99
36200
37000
102
3
68-168/29
156-59-2
cis- 1, 2-Dichloroethylene
ND
36200
39900
110
36200
42200
117
6
74-126/26
10061-01-5 cis-1,3-Dichloropropene
ND
36200
36200
100
36200
41300
114
13
80-123/26
541-73-1
m-Dichlorobenzene
ND
36200
39200
108
36200
43500
120
10
81-129/33
95-50-1
o-Dichlorobenzene
ND
36200
40600
112
36200
44400
123
9
80-129/32
106-46-7
p-Dichlorobenzene
ND
36200
37800
104
36200
41000
113
8
76-130/32
156-60-5
trans- 1, 2-Dichloroethylene
ND
36200
38600
107
36200
39400
109
2
70-127/27
10061-02-6 trans-1,3-Dichloropropene
ND
36200
39000
108
36200
41700
115
7
75-131/28
100-41-4
Ethylbenzene
13300
36200
50500
103
36200
55900
118
10
77-123/31
591-78-6
2-Hexanone
ND
181000
228000
126
181000
236000
130
3
72-133/26
98-82-8
Isopropylbenzene
9850
36200
55700
127
36200
59100
136
6
80-136/32
108-10-1
4-Methyl-2-pentanone
ND
181000
241000
133*
181000
245000
135*
2
76-132/26
79-20-9
Methyl acetate
ND
181000
238000
131
181000
237000
131
0
67-137/30
74-83-9
Methyl bromide
ND
36200
30100
83
36200
33700
93
11
65-139/31
74-87-3
Methyl chloride
ND
36200
36700
101
36200
37600
104
2
71-144/27
108-87-2
Methylcyclohexane
7440
36200
44900
103
36200
45300
105
1
75-128/31
75-09-2
Methylene chloride
ND
36200
36800
102
36200
37900
105
3
74-137/28
78-93-3
Methyl ethyl ketone
ND
181000
209000
115
181000
204000
113
2
75-137/25
* = Outside of Control Limits.
■ 59 of 88
ACC UTEST
FA19708

Matrix Spike/Matrix Spike Duplicate Summary Page 2of2
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
ample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcr
A19708-6MS
F0067012.D
1
11/06/14
AD
n/a
n/a
VF2291
A19708-6MSD
F0067013.D
1
11/06/14
AD
n/a
n/a
VF2291
A19708-6
F0067011.D
1
11/06/14
AD
n/a
n/a
VF2291
The QC reported here applies to the fol lowing samples:
FA19708-6, FA19708-7
CAS No. Compound
1634-04-4
Methyl Tert Butyl Ether
91-20-3
Naphthalene
103-65-1
n-Propylbenzene
100-42-5
Styrene
71-55-6
1, 1, 1-Trichloroethane
79-34-5
1,1,2,2-Tetrachloroethane
79-00-5
1,1,2-Trichloroethane
120-82-1
1,2,4-Trichlorobenzene
95-63-6
1,2,4-Trimethylbenzene
108-67-8
1,3,5-Trimethylbenzene
127-18-4
Tetrachloroethylene
108-88-3
Toluene
79-01-6
Trichloroethylene
75-69-4
Trichlorofluoromethane
75-01-4
Vinyl chloride
1330-20-7
Xylene (total)
FA19708-6
Spike
MS
MS
ug/kg Q
ug/kg
ug/kg
%
ND
36200
39400
109
72800
36200
108000
97
17100
36200
56900
110
ND
36200
41100
113
ND
36200
38800
107
ND
36200
41500
115
ND
36200
63600
176*
ND
36200
38800
107
82000
36200
118000
99
20000
36200
56700
101
ND
36200
36900
102
8340
36200
44000
98
ND
36200
38700
107
ND
36200
34000
94
ND
36200
34200
94
76600
109000
198000
112
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
36200 40200 111 2
36200 122000 136* a 12
36200 63800 129 11
36200 44300 122 7
36200 40400 112 4
36200 45100 125 8
36200 67100 185* 5
36200 41600 115 7
36200 132000 138*a 11
36200 65000 124* 14
36200 41000 113 11
36200 50400 116 14
36200 39600 109 2
36200 35200 97 3
36200 35300 97 3
109000 213000 126 7
CAS No.
Su r r ogate Recover i es
MS
MSD
FA19708-6
Limits
1868-53-7
Dibromofluoromethane
92%
96%
101%
75-124%
2037-26-5
Toluene-D8
92%
98%
92%
75-126%
460-00-4
4-Bromofluorobenzene
105%
114%
104%
71-133%
17060-07-0
1,2-Dichloroethane-D4
89%
88%
100%
72-135%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
77-120/24
79-129/33
80-135/33
78-125/30
70-129/27
71-126/30
74-124/28
78-130/34
74-123/34
73-122/33
79-130/31
76-124/30
75-128/27
73-145/31
76-141/27
80-129/30
■ 60 of 88
ACC UTEST
FA19708

Section 6
Southeast
■,N.ccuTEST
L A H OR AT OR E E 5
GUMS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
0
■■ 61 of 88
ACCUTEST
FA19708

Method Blank Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53802-MB
T015285.1)
1
11/06/14
NJ
11/05/14
OP53802
ST716
The QC reported here applies to the fol I owing samples:
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No. Compound
Result RL
Method: SW846 8270D
M DL Units Q
65-85-0
Benzoic Acid
ND
830
170
ug/kg
95-57-8
2-Chlorophenol
ND
170
17
ug/kg
59-50-7
4-Chloro-3-methyl phenol
ND
170
17
ug/kg
120-83-2
2,4-Dichlorophenol
ND
170
17
ug/kg
105-67-9
2,4-Dimethylphenol
ND
170
18
ug/kg
51-28-5
2,4-Dinitrophenol
ND
830
170
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
330
67
ug/kg
95-48-7
2-Methylphenol
ND
170
17
ug/kg
3&4-Methylphenol
ND
170
33
ug/kg
88-75-5
2-Nitrophenol
ND
170
17
ug/kg
100-02-7
4-Nitrophenol
ND
830
130
ug/kg
87-86-5
Pentachlorophenol
ND
830
130
ug/kg
108-95-2
Phenol
ND
170
17
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
170
17
ug/kg
83-32-9
Acenaphthene
ND
170
21
ug/kg
208-96-8
Acenaphthylene
ND
170
17
ug/kg
120-12-7
Anthracene
ND
170
17
ug/kg
56-55-3
Benzo(a)anthracene
ND
170
17
ug/kg
50-32-8
Benzo(a)pyrene
ND
170
17
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
170
17
ug/kg
191-24-2
Benzo(g, h, i)perylene
ND
170
17
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
170
18
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
170
17
ug/kg
85-68-7
Butyl benzyl phthalate
ND
170
33
ug/kg
91-58-7
2-Chloronaphthalene
ND
170
20
ug/kg
106-47-8
4-Chloroaniline
ND
170
17
ug/kg
218-01-9
Chrysene
ND
170
17
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
170
17
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
170
17
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
170
17
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
170
25
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
170
19
ug/kg
606-20-2
2, 6-Dinitrotoluene
ND
170
18
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
170
17
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
170
17
ug/kg
132-64-9
Dibenzofuran
ND
170
17
ug/kg
■ 62 of 88
ACCUTEST
FA19708

Method Blank Summary Page 2 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
;ample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Bat&
)P53802-MB
T015285.1)
1
11/06/14
NJ
11/05/14
OP53802
ST716
The QC reported here applies to the following samples: Method: SW846 8270D
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No.
Compound
Result
RL
M DL
Units
Q
84-74-2
Di-n-butyl phthalate
ND
330
33
ug/kg
117-84-0
Di-n-octyl phthalate
ND
170
33
ug/kg
84-66-2
Diethyl phthalate
ND
330
33
ug/kg
131-11-3
Dimethyl phthalate
ND
170
33
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
330
33
ug/kg
206-44-0
Fluoranthene
ND
170
17
ug/kg
86-73-7
Fluorene
ND
170
17
ug/kg
118-74-1
Hexachlorobenzene
ND
170
17
ug/kg
87-68-3
Hexachlorobutadiene
ND
170
17
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
170
17
ug/kg
67-72-1
Hexachloroethane
ND
170
17
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
170
17
ug/kg
78-59-1
Isophorone
ND
170
17
ug/kg
91-57-6
2-Methylnaphthalene
ND
170
17
ug/kg
91-20-3
Naphthalene
ND
170
17
ug/kg
98-95-3
Nitrobenzene
ND
170
17
ug/kg
621-64-7
N-Nitroso-di-n-propylamine
ND
170
17
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
170
17
ug/kg
85-01-8
Phenanthrene
ND
170
17
ug/kg
129-00-0
Pyrene
ND
170
17
ug/kg
CAS No.
Surrogate Recoveries
Limits
367-12-4
2-Fluorophenol
70%
40-102%
4165-62-2
Phenol-d5
80%
41-100%
118-79-6
2,4,6-Tribromophenol
79%
42-108%
4165-60-0
Nitrobenzene-d5
72%
40-105%
321-60-8
2-Fluorobiphenyl
76%
43-107%
1718-51-0
Terphenyl-d14
93%
45-119%
CAS No.
Tentatively Identified Compounds
R.T.
Est.
Conc.
Units Q
79-00-5
Ethane, 1,1,2-trichloro-
3.30
180
ug/kg JN
system artifact/aldol-condensation
3.69
270
ug/kg J
■ 63 of 88
ACCUTEST
FA19708

Method Blank Summary Page 3 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53802-MB
T015285.1)
1
11/06/14
NJ
11/05/14
OP53802
ST716
The QC reported here applies to the fol lowing samples: Method:
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No. Tentatively Identified Compounds
R.T. Est. Conc.
Units
Q
system artifact/aldol-condensation
3.90 5700
ug/kg
J
79-34-5 Ethane, 1,1,2,2-tetrachloro-
4.43 420
ug/kg
JN
Total TIC, Semi -Volatile
600
ug/kg
J
■ 64 of 88
ACCUTEST
FA19708

Method Blank Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53802-MB
T015322.1)
1
11/07/14
NJ
11/05/14
OP53802
ST717
The QC reported here applies to the fol I owing samples:
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No. Compound
Result RL
Method: SW846 8270D
M DL Units Q
65-85-0
Benzoic Acid
ND
830
170
ug/kg
95-57-8
2-Chlorophenol
ND
170
17
ug/kg
59-50-7
4-Chloro-3-methyl phenol
ND
170
17
ug/kg
120-83-2
2,4-Dichlorophenol
ND
170
17
ug/kg
105-67-9
2,4-Dimethylphenol
ND
170
18
ug/kg
51-28-5
2,4-Dinitrophenol
ND
830
170
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
330
67
ug/kg
95-48-7
2-Methylphenol
ND
170
17
ug/kg
3&4-Methylphenol
ND
170
33
ug/kg
88-75-5
2-Nitrophenol
ND
170
17
ug/kg
100-02-7
4-Nitrophenol
ND
830
130
ug/kg
87-86-5
Pentachlorophenol
ND
830
130
ug/kg
108-95-2
Phenol
ND
170
17
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
170
17
ug/kg
83-32-9
Acenaphthene
ND
170
21
ug/kg
208-96-8
Acenaphthylene
ND
170
17
ug/kg
120-12-7
Anthracene
ND
170
17
ug/kg
56-55-3
Benzo(a)anthracene
ND
170
17
ug/kg
50-32-8
Benzo(a)pyrene
ND
170
17
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
170
17
ug/kg
191-24-2
Benzo(g, h, i)perylene
ND
170
17
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
170
18
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
170
17
ug/kg
85-68-7
Butyl benzyl phthalate
ND
170
33
ug/kg
91-58-7
2-Chloronaphthalene
ND
170
20
ug/kg
106-47-8
4-Chloroaniline
ND
170
17
ug/kg
218-01-9
Chrysene
ND
170
17
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
170
17
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
170
17
ug/kg
108-60-1
bis(2-Chloroisopropyl)ether
ND
170
17
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
170
25
ug/kg
121-14-2
2,4-Dinitrotoluene
ND
170
19
ug/kg
606-20-2
2, 6-Dinitrotoluene
ND
170
18
ug/kg
91-94-1
3,3'-Dichlorobenzidine
ND
170
17
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
170
17
ug/kg
132-64-9
Dibenzofuran
ND
170
17
ug/kg
■ 65 of 88
ACCUTEST
FA19708

Method Blank Summary Page 2 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
;ample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Bat&
)P53802-MB
T015322.1)
1
11/07/14
NJ
11/05/14
OP53802
ST717
The QC reported here applies to the following samples: Method: SW846 8270D
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No.
Compound
Result
RL
M DL
Units
Q
84-74-2
Di-n-butyl phthalate
ND
330
33
ug/kg
117-84-0
Di-n-octyl phthalate
ND
170
33
ug/kg
84-66-2
Diethyl phthalate
ND
330
33
ug/kg
131-11-3
Dimethyl phthalate
ND
170
33
ug/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
330
33
ug/kg
206-44-0
Fluoranthene
ND
170
17
ug/kg
86-73-7
Fluorene
ND
170
17
ug/kg
118-74-1
Hexachlorobenzene
ND
170
17
ug/kg
87-68-3
Hexachlorobutadiene
ND
170
17
ug/kg
77-47-4
Hexachlorocyclopentadiene
ND
170
17
ug/kg
67-72-1
Hexachloroethane
ND
170
17
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
170
17
ug/kg
78-59-1
Isophorone
ND
170
17
ug/kg
91-57-6
2-Methylnaphthalene
ND
170
17
ug/kg
91-20-3
Naphthalene
ND
170
17
ug/kg
98-95-3
Nitrobenzene
ND
170
17
ug/kg
621-64-7
N-Nitroso-di-n-propylamine
ND
170
17
ug/kg
86-30-6
N-Nitrosodiphenylamine
ND
170
17
ug/kg
85-01-8
Phenanthrene
ND
170
17
ug/kg
129-00-0
Pyrene
ND
170
17
ug/kg
CAS No.
Surrogate Recoveries
Limits
367-12-4
2-Fluorophenol
71%
40-102%
4165-62-2
Phenol-d5
82%
41-100%
118-79-6
2,4,6-Tribromophenol
75%
42-108%
4165-60-0
Nitrobenzene-d5
70%
40-105%
321-60-8
2-Fluorobiphenyl
73%
43-107%
1718-51-0
Terphenyl-d14
87%
45-119%
CAS No.
Tentatively Identified Compounds
R.T.
Est.
Conc.
Units Q
79-00-5
Ethane, 1,1,2-trichloro-
3.28
190
ug/kg JN
system artifact/aldol-condensation
3.67
320
ug/kg J
■ 66 of 88
ACCUTEST
FA19708

Method Blank Summary Page 3 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53802-MB
T015322.1)
1
11/07/14
NJ
11/05/14
OP53802
ST717
The QC reported here applies to the fol lowing samples: Method:
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No. Tentatively Identified Compounds
R.T. Est. Conc.
Units
Q
system artifact/aldol-condensation
3.88 6700
ug/kg
J
79-34-5 Ethane, 1,1,2,2-tetrachloro-
4.40 450
ug/kg
JN
Total TIC, Semi -Volatile
640
ug/kg
J
■■ 67 of 88
ACCUTEST
FA19708

Blank Spike Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53802-BS
T015284.D
1
11/06/14
NJ
11/05/14
OP53802
ST716
The QC reported here applies to the following samples: Method: SW846 8270D
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No. Compound
Spike BSP BSP
ug/kg ug/kg % Limits
65-85-0
Benzoic Acid
3330
2580
77
36-118
95-57-8
2-Chlorophenol
1670
1340
80
48-104
59-50-7
4-Chloro-3-methyl phenol
1670
1340
80
52-108
120-83-2
2,4-Dichlorophenol
1670
1310
79
51-105
105-67-9
2,4-Dimethylphenol
1670
1330
80
43-96
51-28-5
2,4-Dinitrophenol
3330
3130
94
40-119
534-52-1
4,6-Dinitro-o-cresol
3330
3190
96
64-121
95-48-7
2-Methylphenol
1670
1360
82
46-107
3&4-Methylphenol
3330
2650
80
44-111
88-75-5
2-Nitrophenol
1670
1330
80
49-104
100-02-7
4-Nitrophenol
3330
3010
90
56-116
87-86-5
Pentachlorophenol
3330
3180
95
61-114
108-95-2
Phenol
1670
1330
80
45-110
88-06-2
2,4,6-Trichlorophenol
1670
1480
89
56-109
83-32-9
Acenaphthene
1670
1380
83
56-109
208-96-8
Acenaphthylene
1670
1380
83
56-106
120-12-7
Anthracene
1670
1390
83
61-110
56-55-3
Benzo(a)anthracene
1670
1430
86
66-111
50-32-8
Benzo(a)pyrene
1670
1370
82
59-104
205-99-2
Benzo(b)fluoranthene
1670
1430
86
67-113
191-24-2
Benzo(g, h, i)perylene
1670
1380
83
67-113
207-08-9
Benzo(k)fluoranthene
1670
1470
88
67-114
101-55-3
4-Bromophenyl phenyl ether
1670
1190
71
62-110
85-68-7
Butyl benzyl phthalate
1670
1530
92
65-113
91-58-7
2-Chloronaphthalene
1670
1310
79
53-106
106-47-8
4-Chloroaniline
1670
1140
68
30-115
218-01-9
Chrysene
1670
1440
86
65-112
111-91-1
bis(2-Chloroethoxy)methane
1670
1200
72
48-105
111-44-4
bis(2-Chloroethyl)ether
1670
1190
71
46-103
108-60-1
bis(2-Chloroisopropyl)ether
1670
1250
75
40-110
7005-72-3
4-Chlorophenyl phenyl ether
1670
1290
77
58-106
121-14-2
2,4-Dinitrotoluene
1670
1340
80
59-109
606-20-2
2,6-Dinitrotoluene
1670
1350
81
61-107
91-94-1
3,3'-Dichlorobenzidine
1670
1270
76
36-114
53-70-3
Dibenzo(a,h)anthracene
1670
1440
86
68-115
132-64-9
Dibenzofuran
1670
1390
83
57-108
* = Outside of Control Limits.
■ 68 of 88
ACC UTEST
FA19708

Blank Spike Summary Page 2 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
;ample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Bat&
)P53802-BS
T015284.D
1
11/06/14
NJ
11/05/14
OP53802
ST716
The QC reported here applies to the fol lowing samples:
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
84-74-2
Di-n-butyl phthalate
1670
1440
86
63-108
117-84-0
Di-n-octyl phthalate
1670
1550
93
64-119
84-66-2
Diethyl phthalate
1670
1350
81
61-109
131-11-3
Dimethyl phthalate
1670
1360
82
59-108
117-81-7
bis(2-Ethylhexyl)phthalate
1670
1520
91
64-115
206-44-0
Fluoranthene
1670
1370
82
60-108
86-73-7
Fluorene
1670
1380
83
58-109
118-74-1
Hexachlorobenzene
1670
1250
75
59-111
87-68-3
Hexachlorobutadiene
1670
1210
73
41-108
77-47-4
Hexachlorocyclopentadiene
1670
1240
74
49-110
67-72-1
Hexachloroethane
1670
1190
71
40-105
193-39-5
Indeno(1,2,3-cd)pyrene
1670
1280
77
66-116
78-59-1
Isophorone
1670
1180
71
42-89
91-57-6
2-Methylnaphthalene
1670
1290
77
47-106
91-20-3
Naphthalene
1670
1160
70
44-104
98-95-3
Nitrobenzene
1670
1160
70
43-108
621-64-7
N-Nitroso-di-n-propylamine
1670
1310
79
48-108
86-30-6
N-Nitrosodiphenylamine
1670
1500
90
62-110
85-01-8
Phenanthrene
1670
1430
86
63-111
129-00-0
Pyrene
1670
1480
89
65-115
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
75%
40-102%
4165-62-2
Phenol-d5
83%
41-100%
118-79-6
2,4,6-Tribromophenol
88%
42-108%
4165-60-0
Nitrobenzene-d5
73%
40-105%
321-60-8
2-Fluorobiphenyl
82%
43-107%
1718-51-0
Terphenyl-d14
97%
45-119%
* = Outside of Control Limits.
Method: SW846 8270D
■ 69 of 88
ACC UTEST
FA19708

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53802-MS
T015293.1)
1
11/07/14
NJ
11/05/14
OP53802
ST716
OP53802-MSD
T015294.1)
1
11/07/14
NJ
11/05/14
OP53802
ST716
FA19700-2
T015292.1)
1
11/07/14
NJ
11/05/14
OP53802
ST716
The QC reported here applies to the folIowing samples:
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No. Compound
FA19700-2 Spike MS
ug/kg Q ug/kg ug/kg
Method: SW846 8270D
MS Spike MSD MSD Limits
% ug/kg ug/kg % RPD Rec/RPD
65-85-0
Benzoic Acid
ND
4660
3330
71
4710
3360
71
1
36-118/41
95-57-8
2-Chlorophenol
ND
2330
1740
75
2350
1710
73
2
48-104/26
59-50-7
4-Chloro-3-methyl phenol
ND
2330
1730
74
2350
1750
74
1
52-108/21
120-83-2
2,4-Dichlorophenol
ND
2330
1640
70
2350
1640
70
0
51-105/27
105-67-9
2,4-Dimethylphenol
ND
2330
1750
75
2350
1760
75
1
43-96/23
51-28-5
2,4-Dinitrophenol
ND
4660
3650
78
4710
3690
78
1
40-119/32
534-52-1
4,6-Dinitro-o-cresol
ND
4660
3840
82
4710
3780
80
2
64-121/29
95-48-7
2-Methylphenol
ND
2330
1790
77
2350
1780
76
1
46-107/24
3&4-Methylphenol
ND
4660
3510
75
4710
3520
75
0
44-111/24
88-75-5
2-Nitrophenol
ND
2330
1720
74
2350
1660
71
4
49-104/27
100-02-7
4-Nitrophenol
ND
4660
3940
85
4710
4000
85
2
56-116/23
87-86-5
Pentachlorophenol
ND
4660
4040
87
4710
3970
84
2
61-114/23
108-95-2
Phenol
ND
2330
1760
76
2350
1760
75
0
45-110/24
88-06-2
2,4,6-Trichlorophenol
ND
2330
1890
81
2350
1870
79
1
56-109/25
83-32-9
Acenaphthene
ND
2330
1780
76
2350
1770
75
1
56-109/23
208-96-8
Acenaphthylene
ND
2330
1760
76
2350
1760
75
0
56-106/23
120-12-7
Anthracene
ND
2330
1790
77
2350
1740
74
3
61-110/21
56-55-3
Benzo(a)anthracene
ND
2330
1840
79
2350
1790
76
3
66-111/23
50-32-8
Benzo(a)pyrene
ND
2330
1750
75
2350
1690
72
3
59-104/23
205-99-2
Benzo(b)fluoranthene
ND
2330
1820
78
2350
1770
75
3
67-113/24
191-24-2
Benzo(g,h,i)perylene
ND
2330
1810
78
2350
1770
75
2
67-113/21
207-08-9
Benzo(k)fluoranthene
ND
2330
1900
82
2350
1860
79
2
67-114/22
101-55-3
4-Bromophenyl phenyl ether
ND
2330
1520
65
2350
1490
63
2
62-110/21
85-68-7
Butyl benzyl phthalate
ND
2330
2110
91
2350
2070
88
2
65-113/20
91-58-7
2-Chloronaphthalene
ND
2330
1700
73
2350
1680
71
1
53-106/23
106-47-8
4-Chloroaniline
ND
2330
1070
46
2350
1250
53
16
30-115/30
218-01-9
Chrysene
ND
2330
1840
79
2350
1800
77
2
65-112/25
111-91-1
bis(2-Chloroethoxy)methane
ND
2330
1550
67
2350
1560
66
1
48-105/24
111-44-4
bis(2-Chloroethyl)ether
ND
2330
1560
67
2350
1550
66
1
46-103/27
108-60-1
bis(2-Chloroisopropyl)ether
ND
2330
1630
70
2350
1670
71
2
40-110/25
7005-72-3
4-Chlorophenyl phenyl ether
ND
2330
1610
69
2350
1640
70
2
58-106/21
121-14-2
2,4-Dinitrotoluene
ND
2330
1700
73
2350
1710
73
1
59-109/20
606-20-2
2,6-Dinitrotoluene
ND
2330
1770
76
2350
1770
75
0
61-107/22
91-94-1
3,3'-Dichlorobenzidine
ND
2330
1030
44
2350
1250
53
19
36-114/28
53-70-3
Dibenzo(a,h)anthracene
ND
2330
1840
79
2350
1790
76
3
68-115/23
132-64-9
Dibenzofuran
ND
2330
1790
77
2350
1810
77
1
57-108/22
* = Outside of Control Limits.
■■ 70 of 88
M ACCUTEST
FA19708 1PBDRATOR15

Matrix Spike/Matrix Spike Duplicate Summary Page 2of2
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
)P53802-MS
T015293.1)
1
11/07/14
NJ
11/05/14
OP53802
ST716
)P53802-MSD
T015294.1)
1
11/07/14
NJ
11/05/14
OP53802
ST716
;A19700-2
T015292.1)
1
11/07/14
NJ
11/05/14
OP53802
ST716
The QC reported here applies to the following samples: Method: SW846 8270D
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
FA19700-2
Spike
MS
MS
Spike
MSD
MSD
Limits
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg
%
ug/kg
ug/kg
%
RPD
Rec/RPD
84-74-2
Di-n-butyl phthalate
ND
2330
1910
82
2350
1870
79
2
63-108/19
117-84-0
Di-n-octyl phthalate
ND
2330
2200
94
2350
2140
91
3
64-119/21
84-66-2
Diethyl phthalate
ND
2330
1750
75
2350
1760
75
1
61-109/20
131-11-3
Dimethyl phthalate
ND
2330
1740
75
2350
1750
74
1
59-108/20
117-81-7
bis(2-Ethylhexyl)phthalate
ND
2330
2110
91
2350
2050
87
3
64-115/23
206-44-0
Fluoranthene
ND
2330
1680
72
2350
1650
70
2
60-108/25
86-73-7
Fluorene
ND
2330
1770
76
2350
1760
75
1
58-109/21
118-74-1
Hexachlorobenzene
ND
2330
1550
67
2350
1520
65
2
59-111/21
87-68-3
Hexachlorobutadiene
ND
2330
1480
64
2350
1480
63
0
41-108/27
77-47-4
Hexachlorocyclopentadiene
ND
2330
1520
65
2350
1480
63
3
49-110/31
67-72-1
Hexachloroethane
ND
2330
1510
65
2350
1530
65
1
40-105/32
193-39-5
Indeno(1,2,3-cd)pyrene
ND
2330
1680
72
2350
1630
69
3
66-116/22
78-59-1
Isophorone
ND
2330
1520
65
2350
1530
65
1
42-89/22
91-57-6
2-Methylnaphthalene
ND
2330
1630
70
2350
1640
70
1
47-106/27
91-20-3
Naphthalene
ND
2330
1480
64
2350
1480
63
0
44-104/27
98-95-3
Nitrobenzene
ND
2330
1520
65
2350
1530
65
1
43-108/25
621-64-7
N-Nitroso-di-n-propylamine
ND
2330
1760
76
2350
1770
75
1
48-108/27
86-30-6
N-Nitrosodiphenylamine
ND
2330
1980
85
2350
1910
81
4
62-110/21
85-01-8
Phenanthrene
ND
2330
1860
80
2350
1810
77
3
63-111/22
129-00-0
Pyrene
ND
2330
1980
85
2350
1920
82
3
65-115/25
CAS No.
Su r r ogate Recover i es
MS
MSD
FA19700-2
Limits
367-12-4
2-Fluorophenol
71%
70%
69%
40-102%
4165-62-2
Phenol-d5
79%
78%
78%
41-100%
118-79-6
2,4,6-Tribromophenol
78%
77%
76%
42-108%
4165-60-0
Nitrobenzene-d5
69%
69%
72%
40-105%
321-60-8
2-Fluorobiphenyl
76%
74%
73%
43-107%
1718-51-0
Terphenyl-dl4
91%
89%
94%
45-119%
* = Outside of Control Limits.
■■ 71 of 88
N ACCUTEST
FA19708 1PBDRATOR15

Southeast
■ ,�.ccuTEST
L A H OR AT OR E E 5
GC Volatiles
QC Data Summaries
Section 7
a
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
■ 72 of 88
ACCUTEST
FA19708

Method Blank Summary Page 1 of 1
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUV3537-MB
UV066514.D
1
11/05/14
AH
n/a
n/a
GUV3537
The QC reported here applies to the folIowing samples: Method: MADEP VPH REV 1.1
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No.
Compound
Result
RL
MDL
Units Q
71-43-2
Benzene
ND
51
51
ug/kg
100-41-4
Ethylbenzene
ND
100
51
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
100
51
ug/kg
91-20-3
Naphthalene
ND
260
150
ug/kg
108-88-3
Toluene
ND
100
51
ug/kg
m,p-Xylene
ND
200
100
ug/kg
95-47-6
o-Xylene
ND
100
51
ug/kg
C5- C8 Aliphatics (Unadj.)
ND
5100
1800
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
5100
1800
ug/kg
CAS No.
Surrogate Recoveries
Limits
460-00-4
BFB
96%
70-130%
460-00-4
BFB
99%
70-130%
■■ 73 of 88
M ACCUTEST
FA19708 1PBDRATOR15

Method Blank Stimmary Page 1 of 1
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUV3538-MB
UV066537.D
1
11/06/14
AH
n/a
n/a
GUV3538
The QC reported here applies to the folIowing samples: Method: MADEP VPH REV 1.1
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
iv
CAS No. Compound Result RL M DL Units
P Q
C9- C10 Aromatics (Unadj.) ND 5100 1800 ug/kg
CAS No. Su r r ogat e Recover i es Limits
460-00-4 BFB 97% 70-130%
460-00-4 BFB 99% 70-130%
■ 74 of 88
ACCUTEST
FA19708

Method Blank Summary Page I of I
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GCD5353-MB
CD130690.D
1
11/06/14
JG
n/a
n/a
GCD5353
The QC reported here applies to the following samples: Method: SW846 8015C
FA19708-1, FA19708-2
V
w
CAS No. Compound
P
Result
RL M DL Units Q
TPH-GRO (C6-C10)
ND
5.0 2.5 mg/kg
CAS No. Sur r ogat e Recover i es
Limits
460-00-4 4-Bromofluorobenzene
82%
56-149%
98-08-8 aaa-Trifluorotoluene
81%
66-132%
■■ 75 of 88
ACCUTEST
FA19708

Blank SpikeSUmmary Page I of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GCD5353-BS
CD130689.D
1
11/06/14
JG
n/a
n/a
GCD5353
The QC reported here applies to the following samples: Method: SW846 8015C
FA19708-1, FA19708-2
Spike
BSP BSP
CAS No. Compound
mg/kg
mg/kg % Limits
TPH-GRO (C6-C10)
20
19.6 98 74-128
CAS No. Sur r ogat e Recover i es
BSP
Limits
460-00-4 4-Bromofluorobenzene
104%
56-149%
98-08-8 aaa-Trifluorotoluene
104%
66-132%
* = Outside of Control Limits.
■ 76 of 88
■ ACCUTEST
FA19708 "°°""'°""°

Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUV3537-BS
UV066511.13
1
11/05/14
AH
n/a
n/a
GUV3537
GUV3537-BSD
UV066512.13
1
11/05/14
AH
n/a
n/a
GUV3537
The QC reported here applies to the folIowing samples: Method: MADEP VPH REV 1.1
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
Spike
BSP
BSP
BSD
BSD
CAS No.
Compound
ug/kg
ug/kg
%
ug/kg
%
71-43-2
Benzene
4160
4130
99
4160
100
100-41-4
Ethylbenzene
4160
4190
101
4210
101
1634-04-4
Methyl Tert Butyl Ether
4160
4310
104
4430
106
91-20-3
Naphthalene
4160
3970
95
4010
96
108-88-3
Toluene
4160
4160
100
4190
101
m,p-Xylene
8320
8570
103
8610
103
95-47-6
o-Xylene
4160
4180
100
4210
101
C5- C8 Aliphatics (Unadj.)
12500
13500
108
13900
111
C9- C12 Aliphatics (Unadj.)
8320
8090
97
7990
96
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
460-00-4
BFB
87%
96%
70-130%
460-00-4
BFB
89%
98%
70-130%
* = Outside of Control Limits.
Limits
RPD
Rec/RPD
1
70-130/25
0
70-130/25
3
70-130/25
1
70-130/25
1
70-130/25
0
70-130/25
1
70-130/25
3
70-130/25
1
70-130/25
■■ 77 of 88
ACCUTEST
FA19708

Blank Spike/Blank Spike Duplicate Summary Page I of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUV3538-BS
UV066534.1)
1
11/06/14
AH
n/a
n/a
GUV3538
GUV3538-BSD
UV066535.1)
1
11/06/14
AH
n/a
n/a
GUV3538
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
V
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
N
Spike BSP BSP BSD BSD Limits
CAS No. Compound ug/kg ug/kg % ug/kg % RPD RedRPD
C9- C10 Aromatics (Unadj.) 4160 3920 94 4170 100 6 70-130/25
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
460-00-4
BFB
97%
93%
70-130%
460-00-4
BFB
100%
96%
70-130%
* = Outside of Control Limits.
■ 78 of 88
■ ACCUTEST
FA19708

Matrix Spike/Matrix Spike Duplicate Summary Page I of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA19708-2MS
CD130702.D
10
11/06/14
JG
n/a
n/a
GCD5353
FA19708-2MSD
CD130703.D
10
11/06/14
JG
n/a
n/a
GCD5353
FA19708-2
CD130701.D
10
11/06/14
JG
n/a
n/a
GCD5353
The QC reported here applies to the following samples: Method: SW846 8015C
V
FA19708-1, FA19708-2 P.
FA19708-2 Spike MS MS Spike MSD MSD Limits
CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg mg/kg % RPD RecIRPD
TPH-GRO (C6-C10) 4780 3500 7630 81 3500 7360 74 4 74-128/17
CAS No.
Sur r ogat e Recover i es
MS
MSD
FA19708-2
Limits
460-00-4
4-Bromofluorobenzene
140%
133%
124%
56-149%
98-08-8
aaa-Trifluorotoluene
107%
110%
94%
66-132%
* = Outside of Control Limits.
■■ 79 of 88
ACCUTEST
FA19708

Duplicate Summary Page 1 of l
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA19680-lDUP
UV066515.13
1
11/05/14
AH
n/a
n/a
GUV3537
FA19680-1 a
UV066516.13
1
11/05/14
AH
n/a
n/a
GUV3537
FA19680-1
UV066521.13
1
11/05/14
AH
n/a
n/a
GUV3537
The QC reported here applies to the folIowing samples: Method: MADEP VPH REV 1.1
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
FA 19680-1
D U P
CAS No.
Compound
ug/kg Q
ug/kg Q
RPD
Limits
71-43-2
Benzene
ND b
ND
nc
50
100-41-4
Ethylbenzene
ND b
ND
nc
50
1634-04-4
Methyl Tert Butyl Ether
ND b
ND
nc
50
91-20-3
Naphthalene
ND b
ND
nc
50
108-88-3
Toluene
ND b
ND
nc
50
m,p-Xylene
ND b
ND
nc
50
95-47-6
o-Xylene
ND b
ND
nc
50
C5- C8 Aliphatics (Unadj.)
ND b
ND
nc
50
C9- C12 Aliphatics (Unadj.)
ND b
ND
nc
50
C5- C8 Aliphatics
ND b
ND
nc
50
C9- C12 Aliphatics
ND b
ND
nc
50
CAS No.
Surrogate Recoveries
DUP
FA19680-1
FA19680-1 Limits
460-00-4 BFB 149%* d 141%* ° 130% 70-130%
460-00-4 BFB 147%* d 144%* ° 135%* c 70-130%
(a) Confirmation run.
(b) Result is from Run #2.
(c) Outside control limits; however, sample is ND.
(d) Outside control limits.
* = Outside of Control Limits.
■ 80 of 88
ACCUTEST
FA19708

Duplicate Summary Page 1 of l
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Prcj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA19708-4DUP
UV066541.D
10
11/06/14
AH
n/a
n/a
GUV3538
FA19708-4
UV06654O.D
10
11/06/14
AH
n/a
n/a
GUV3538
The QC reported here applies to the folIowing samples: Method: MADEP VPH REV 1.1
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7 v,
iv
FA 19708-4 DU P
CAS No. Compound ug/kg Q ug/kg Q RPD Limits
C9- C10 Aromatics (Unadj.) 3590000 3150000 13 50
C9- C10 Aromatics 3590000 3150000 13 50
CAS No. SurrogateRecover ies DUP FA19708-4 Limits
460-00-4 BFB 0%* a 0%* a 70-130%
460-00-4 BFB 0%* a 0%* a 70-130%
(a) Outside control limits due to dilution.
* = Outside of Control Limits.
■■ 81 of 88
M ACCUTEST
FA19708 1PBDRATOR15

Section 8
Southeast
■ ,�.ccuTEST
L A H OR AT OR E E 5
GC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
a
■ 82 of 88
ACCUTEST
FA19708

Method Blank Summary Page I of I
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53815-MB
NN010906.13
1
11/11/14
NAF
11/06/14
OP53815
GNN479
The QC reported here applies to the following samples: Method: MADEPEPHREVIA
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No.
Compound
Result
RL
MDL
Units Q
83-32-9
Acenaphthene
ND
200
100
ug/kg
208-96-8
Acenaphthylene
ND
200
100
ug/kg
120-12-7
Anthracene
ND
200
100
ug/kg
56-55-3
Benzo(a)anthracene
ND
200
100
ug/kg
50-32-8
Benzo(a)pyrene
ND
200
100
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
200
100
ug/kg
191-24-2
Benzo(g, h, i)perylene
ND
200
100
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
200
100
ug/kg
218-01-9
Chrysene
ND
200
100
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
200
100
ug/kg
206-44-0
Fluoranthene
ND
200
100
ug/kg
86-73-7
Fluorene
ND
200
100
ug/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
200
100
ug/kg
91-57-6
2-Methylnaphthalene
ND
200
100
ug/kg
91-20-3
Naphthalene
ND
200
100
ug/kg
85-01-8
Phenanthrene
ND
200
100
ug/kg
129-00-0
Pyrene
ND
200
100
ug/kg
CII-C22 Aromatics (Unadj.)
ND
10000
7500
ug/kg
C11-C22 Aromatics
ND
10000
7500
ug/kg
C9-C18 Aliphatics
ND
10000
5000
ug/kg
C19-C36 Aliphatics
ND
10000
5000
ug/kg
CAS No. Surrogate Recoveries Limits
3386-33-2
1-Chlorooctadecane
84%
40-140%
580-13-2
2-Bromonaphthalene
86%
40-140%
84-15-1
o-Terphenyl
73%
40-140%
321-60-8
2-Fluorobiphenyl
83%
40-140%
■ 83 of 88
ACCUTEST
FA19708

Method Blank Summary Page 1 of 1
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53810-MB
JJ005944.D
1
11/10/14
SJL
11/06/14
OP53810
GJJ239
The QC reported here applies to the following samples: Method: SW846 8015C
FA19708-1, FA19708-2
PO
CAS No. Compound Result RL M DL Units Q iv
TPH (C 10-C28) 5.57 6.3 3.8 mg/kg J
CAS No. Sur r ogate Recover i es Limits
84-15-1 o-Terphenyl 90% 56-122%
■ 84 of 88
ACCUTEST
FA19708

Blank SpikeSUmmary Page I of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53810-BS
JJ005945.D
1
11/10/14
SJL
11/06/14
OP53810
GJJ239
The QC reported here applies to the following samples: Method: SW846 8015C
FA19708-1, FA19708-2
w
Spike BSP BSP iv
CAS No. Compound mg/kg mg/kg % Limits
TPH (C10-C28) 50 40.4 81 62-116
CAS No. Sur r ogat e Recover i es BSP Limits
84-15-1 o-Terphenyl 86% 56-122%
* = Outside of Control Limits.
■ 85 of 88
■ ACCUTEST
FA19708 "°°""'°""°

Blank Spike/Blank Spike Duplicate Summary Page I of l
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
;ample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcr
)P53815-BS
NN010904.13
1
11/11/14
NAF
11/06/14
OP53815
GNN479
)P53815-BSD
NN010905.13
1
11/11/14
NAF
11/06/14
OP53815
GNN479
The QC reported here applies to the folIowing samples: Method: MADEPEPHREVIA
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
Spike
BSP
BSP
BSD
BSD
Limits
CAS No.
Compound
ug/kg
ug/kg
%
ug/kg
%
RPD
Rec/RPD
83-32-9
Acenaphthene
5000
3920
78
3540
71
10
40-140/30
208-96-8
Acenaphthylene
5000
3810
76
3530
71
8
40-140/30
120-12-7
Anthracene
5000
4640
93
4250
85
9
40-140/30
56-55-3
Benzo(a)anthracene
5000
5270
105
4840
97
9
40-140/30
50-32-8
Benzo(a)pyrene
5000
5400
108
4980
100
8
40-140/30
205-99-2
Benzo(b)fluoranthene
5000
5350
107
4890
98
9
40-140/30
191-24-2
Benzo(g, h, i)perylene
5000
5560
ill
5160
103
7
40-140/30
207-08-9
Benzo(k)fluoranthene
5000
5380
108
4970
99
8
40-140/30
218-01-9
Chrysene
5000
5210
104
4790
96
8
40-140/30
53-70-3
Dibenzo(a,h)anthracene
5000
5640
113
5210
104
8
40-140/30
206-44-0
Fluoranthene
5000
4830
97
4420
88
9
40-140/30
86-73-7
Fluorene
5000
4180
84
3800
76
10
40-140/30
193-39-5
Indeno(1,2,3-cd)pyrene
5000
5580
112
5140
103
8
40-140/30
91-57-6
2-Methylnaphthalene
5000
3590
72
3410
68
5
40-140/30
91-20-3
Naphthalene
5000
3200
64
3000
60
6
40-140/30
85-01-8
Phenanthrene
5000
4550
91
4160
83
9
40-140/30
129-00-0
Pyrene
5000
4860
97
4450
89
9
40-140/30
CII-C22 Aromatics (Unadj.)
85000
87900
103
84000
99
5
40-140/30
C9-C18 Aliphatics
30000
22000
73
27800
93
23
40-140/30
C19-C36 Aliphatics
40000
34500
86
35100
88
2
40-140/30
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
3386-33-2
1-Chlorooctadecane
105%
106%
40-140%
580-13-2
2-Bromonaphthalene
101%
91%
40-140%
84-15-1
o-Terphenyl
93%
86%
40-140%
321-60-8
2-Fluorobiphenyl
98%
88%
40-140%
Sample
Compound
Col #1
Col #2
Breakthrough
Limit
OP53815-BS 2-Methylnaphthalene
3590
ND
0.0%
5.0
OP53815-BS Naphthalene
3200
ND
0.0%
5.0
OP53815-BSD 2-Methylnaphthalene
3410
ND
0.0%
5.0
OP53815-BSD Naphthalene
3000
ND
0.0%
5.0
* = Outside of Control Limits.
F0
w
L
■ 86 of 88
ACC UTEST
FA19708

Matrix Spike/Matrix Spike Duplicate Summary Page I of
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP53810-MS
JJ005947.D
250
11/10/14
SJL
11/06/14
OP53810
GJJ239
OP53810-MSD
JJ005948.D
250
11/10/14
SJL
11/06/14
OP53810
GJJ239
FA19708-1
JJ005946.1)
250
11/10/14
SJL
11/06/14
OP53810
GJJ239
The QC reported here applies to the following samples: Method: SW846 8015C
FA19708-1, FA19708-2
w
FA19708-1 Spike MS MS Spike MSD MSD Limits P,
CAS No. Compound mg/kg Q mg/kg mg/kg % mg/kg mg/kg % RPD RecIRPD
TPH (C10-C28) 21700 B 70 29900 11712* a70.7 28800 10038* 4 62-116/35
CAS No. Sur r ogat e Recover i es MS MSD FA19708-1 Limits
84-15-1 o-Terphenyl 0%* b 0%* b 0%* b 56-122%
(a) Outside control limits due to high level in sample relative to spike amount.
(b) Outside control limits due to dilution.
* = Outside of Control Limits.
■ 87 of 88
■ ACCUTEST
FA19708 "°°""'°""°

Duplicate Summary Page I of l
Job Number: FA19708
Account: GRINCC GRI (Geological Resources Inc.)
Proj ect: The Rock Worship Center; 1113 Fordham Rd, Charlotte, NC
Sample
File I D
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
)P53815-DUP
NN010950.13
40
11/13/14
NAF
11/06/14
OP53815
GNN481
,A19708-3
NN010949.13
50
11/13/14
NAF
11/06/14
OP53815
GNN481
The QC reported here applies to the fol I owing samples: Method: MADEPEPHREVIA
FA19708-3, FA19708-4, FA19708-5, FA19708-6, FA19708-7
CAS No. Compound
FA19708-3 DUP
ug/kg Q ug/kg Q RPD Limits
83-32-9
Acenaphthene
15300
6390 J
82*
30 a
208-96-8
Acenaphthylene
8540 J
ND
200*
30 a
120-12-7
Anthracene
ND
ND
nc
30 a
56-55-3
Benzo(a)anthracene
ND
ND
nc
30 a
50-32-8
Benzo(a)pyrene
ND
ND
nc
30 a
205-99-2
Benzo(b)fluoranthene
ND
ND
nc
30 a
191-24-2
Benzo(g, h, i)perylene
ND
ND
nc
30 a
207-08-9
Benzo(k)fluoranthene
ND
ND
nc
30 a
218-01-9
Chrysene
ND
ND
nc
30 a
53-70-3
Dibenzo(a,h)anthracene
ND
ND
nc
30 a
206-44-0
Fluoranthene
ND
ND
nc
30 a
86-73-7
Fluorene
8750 J
ND
200*
30 a
193-39-5
Indeno(1,2,3-cd)pyrene
ND
ND
nc
30 a
91-57-6
2-Methylnaphthalene
62500
27400
78*
30 a
91-20-3
Naphthalene
10400 J
ND
200*
30 a
85-01-8
Phenanthrene
11400 J
ND
200*
30 a
129-00-0
Pyrene
ND
ND
nc
30 a
CII-C22 Aromatics (Unadj.)
3420000
1440000
81*
30 a
C11-C22 Aromatics
3300000
1400000
81*
30 a
C9-C18 Aliphatics
5270000
3330000
45*
30 a
C19-C36 Aliphatics
1240000
798000
43*
30 a
CAS No.
Surrogate Recoveries
DUP
FA19708-3
Limits
3386-33-2
1-Chlorooctadecane
0%* b
0%* b
40-140%
580-13-2
2-Bromonaphthalene
0%* b
0%* b
40-140%
84-15-1
o-Terphenyl
0%* b
0%* b
40-140%
321-60-8
2-Fluorobiphenyl
0%* b
0%* b
40-140%
(a) Advisory control limits.
(b) Outside control limits due to dilution.
* = Outside of Control Limits.
F0
it
■ 88 of 88
ACCUTEST
FA19708