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HomeMy WebLinkAbout3412_Forsyth_OldSalisburyRoad_CDLF_GW_FID1276026_20190122ENR USE ❑N! Y: ❑Pa er Report El Electronic Data - Email CD data loaded: Yes / No Doc/Event #: NC DENR Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: • Prepare one form for each individually monitored unit. • Please type or print legibly. • Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc ). • Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. • Attach a notification table of any methane gas values that attain or exceed explosive gas levels This includes any structures on or nearby the facility (NCAC 13B 1629 (4)(a)(i) Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): HDR Engineering, Inc. of the Carolinas Contact for questions about data formatting. Include data preparers name, telephone number and E-mail address: Name: Eric A. Wright Phone: 704-338-6719 E-mail: eric.wright@hdrinc.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address Facility Permit # (.0500 or. 1600) October 20-24, 2006) 3336 Old Salisbury Road November 26-27, 201 and [OldSalisbury Road landfill Winston-Salem, NC 27127 34 12 .0500 December 11, 2018 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring ❑X Detection Monitoring LX] Assessment Monitoring Corrective Action T e of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells �X Methane gas monitoring data Groundwater monitoring data from private water supply wells Corrective action data (specify) Leachate monitoring data ❑ Other(specify) X Surface water monitoring data Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Eric A. Wright Project Engineer 704-338-6719 Facility Representative Name Title 1 /18/2019 Signature f Date 440 South Church Street Suite 1000 Charlotte INC 28202 Facility Representative Address F-0116 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 (Area Code) Telephone Number Affix NC Licensed/ Professional `N%%%I111111 �2• " ` , � ,, S&L �� Seal This page intentionally left blank. F)I a I ^ Winston-Salem • Forsyth County City/County Utilities Water • Sewer • Solid Waste Disposal HDR Project No. 10043322 ■iA Assessment Monitoring Report Groundwater Sampling Event Second Semi -Annual 2018 Old Salisbury Road Landfill NCDEQ Permit NO. 34-12 Forsyth County, North Carolina January 2019 This page intentionally left blank. Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Contents Contents Contents......................................................................................................................................... i 1 General..................................................................................................................................1 1.1 Facility Background........................................................................................................1 1.2 Regulatory Authority.......................................................................................................1 1.3 Assessment Monitoring..................................................................................................1 1.4 Geologic Characteristics.................................................................................................3 1.4.1 Regional Geologic and Hydrogeologic Setting........................................................3 1.4.2 Site Specific Topography and Drainage..................................................................3 1.4.3 Site Specific Hydrogeology.....................................................................................3 2 Monitoring Network................................................................................................................4 3 Data Collection......................................................................................................................5 3.1 Water Level Measurements............................................................................................5 3.2 Groundwater Flow..........................................................................................................7 3.3 Sample Collection and Analysis.....................................................................................7 4 Analytical Results..................................................................................................................8 4.1 Groundwater...................................................................................................................8 4.2 Surface Water.................................................................................................................9 4.3 Landfill Gas...................................................................................................................13 5 Summary & Conclusions.....................................................................................................13 Tables Table 1 Existing groundwater monitoring well details ............... Table 2 Sampling parameters and schedule ............................ Table 3 Groundwater elevations ............................................... Table 4 Hydraulic gradient and flow velocity ............................. Table 5 Lab detections — November 2018................................ Figures Figure 1 Groundwater contours and sample locations .................. Figure 2 Historical groundwater elevations .................................... Figure 3 MW-2R groundwater detections ...................................... .................2 .................6 .................9 Winston-Salem City/County Utilities i Assessment Monitoring Report ��� Contents Appendices Appendix A — Summary of Groundwater Monitoring Results Appendix B — Laboratory Report Appendix C — Field Data Appendix D — Electronic Files Acronyms 2L 15A NCAC Subchapter 02L - Groundwater Classification and Standards pg/L micrograms per liter EPA United States Environmental Protection Agency MCL Maximum Contaminant Level MDL method detection limit NC DENR North Carolina Department of Environment and Natural Resources' NCDEQ North Carolina Department of Environmental Quality' ND not detected in sample NE standard not established NS not sampled NTU Nephelometric turbidity units PCB polychlorinated biphenyl PCE tetrachloroethene PRL practical reporting limit PVC polyvinyl chloride SWSL solid waste section limits SVOC semi -volatile organic compound VOC volatile organic compound USGS U.S. Geological Survey Prior to September 18, 2015, the NCDEQ was referred to as the NC DENR. Both naming conventions are used in this report, as appropriate. Winston-Salem City/County Utilities I Assessment Monitoring Report ��� General 1 General HDR Engineering, Inc. of the Carolinas (HDR), on behalf of the Winston-Salem City/County Utility Commission (the City), is submitting this Assessment Monitoring Report for the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North Carolina. 1.1 Facility Background OSR covers approximately 56 acres within a 140-acre tract north of Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The Forsyth/Davidson County line borders the site to the south (Figure 1). The facility was issued a permit to operate on July 3, 1996 and opened in August of the same year. 1.2 Regulatory Authority OSR is currently operating under North Carolina Department of Environmental and Natural Resources (NC DENR) facility permit number 34-12 dated April 6, 2015 (DIN 23258). Groundwater monitoring and reporting requirements are outlined in items 36 to 45 of the permit. NC Solid Waste Management (SWM) Rules 15A NCAC 13B .0544(b) and .0544(c) define the requirements for OSR's groundwater and surface water monitoring plans, respectively. The groundwater monitoring plan was approved by NC DENR on March 5, 2015 (DIN 23910). 1.3 Assessment Monitoring OSR is in assessment monitoring due to exceedances of Groundwater Quality Standards, as specified in 15 NCAC 02L .0202 (2L Standards) or Interim Maximum Allowable Concentrations (IMACs), for benzene and tetrachloroethene (PCE) detected in well MW-2R during 2011. On December 9, 2011, an Assessment Monitoring Plan for MW-2R was submitted in accordance with 15A NCAC 13B. This plan was approved with two exceptions on January 17, 2012. The first exception required the location of MW-15 to be in the same flow path as MW-2R; the second required all wells to be sampled for Appendix 11 constituents. In February 2014, the City requested, and NC DENR approved, the following modifications to the facility's Assessment Monitoring Plan. • Groundwater monitoring wells MW-1 R, MW-2R, MW-4R and MW-15 will be sampled semiannually for Appendix I and the previously detected Appendix II constituents; • All groundwater monitoring wells will be sampled during every other Fall event (odd years) for the entire Appendix II constituent list. • Additional Appendix II constituents detected will be added to the sampling program for subsequent semiannual events. In January 2016 (the Fall 2015 Report), HDR recommended changes to the semi-annual sampling schedule. North Carolina Department of Environmental Quality (NCDEQ) approved sampling for additional detected parameters. No parameters were removed from the sampling schedule. On May 29, 2018, NCDEQ added 1,4-dioxane to the sampling plan for all wells on a semi- annual basis. '�JC �731 M W, I LEGEND 8-7g EXISTING CONTOURS PROPERTY BOUNDARY PERMIT/PHASE BOUNDARY - - - - 735 - - - - GROUNDWATER CONTOURS EXISTING MONITORING WELL ABANDONED MONITORING WELL METHANE PROBE SURFACE WATER SAMPLE LOCATION APPROXIMATE GROUNDWATER MM-9 FLOW DIRECTION NOTES .Q-r--�726.70 1. SITE TOPOGRAPHIC INFORMATION FOR A MW-1 PORTION OF I & II AND ALL OF PHASES III -VI -10 I SW-2 & SURROUNDING AREA PROVIDED BY CARTOGRAPHIC AERIAL MAPPING, INC. FOR THE I BRADY SURVEYING COMPANY DATED JAN. 3, 2014. THE REMAINING SITE TOPOGRAPHIC INFORMATION PROVIDED BY CARTOGRAPHIC a.♦ 1 AERIAL MAPPING INC. FOR BRADY SURVEYING �Q COMPANY DATED JAN. 3 2011. I 2. PROPERTY SURVEY TAKEN FROM DATA 72927 SUPPLIED BY BRADY SURVEYING, INC. DATED / MW-11 MARCH 14, 1994. �\ 7 ) 3. GROUNDWATER ELEVATIONS ARE IN MEAN SEA LEVEL, MEASURED ON NOVEMBER 26, 2018, I1V � ---_1 SCALE IN FEET -r r�,> � ♦ 4M-I1 M �� \ R`S'♦♦♦ it ���� \� i 200 100 0 200 400 MW-S p ��0 ♦ ♦ A �\ ♦ MW 1 �_ � � ♦♦I�'♦♦ ♦♦ ♦MM 12 MM 7 „7 i� 60.08 � ♦ 7 '�}}} , ' ���, ♦ I 440 MWy u� ♦ MIME ' l 777 75;�* B_1 GL MW 3 r \ .r_A4W�-2f2 SW♦ `♦ iii ♦ 767 21 � �- �� MM 759.94 ♦ A ` \V ♦ AV �. \ El-4R .: \ \\ ♦ - \ \ - �A _ 0861.34� a V '-�-♦ ♦�=3 \ \ ` \♦ ♦ \ MW-1R \ I ♦� -ryt♦♦ '�"..: \\ ♦\1M mac- _- ° �,. MM-4SO -4 ♦\ MM-4 ♦♦ MM 0 ITY � 773.56 �� - - — MW-5R - - - FORSYTH COUNTY DAVIDSON COUNTY PROJECT TITLE OLD SALISBURY ROAD C & D LANDFILL SHEET TITLE GROUNDWATER CONTOURS AND SAMPLE LOCATIONS NOVEMBER 2018 PROJECT NUMBER 10043322 PROJECT MANAGER M. PLUMMER, P.E. DATE JANUARY 2019 REFERENCE SHEET LAYOUT 1 REFERENCE DOCUMENT OOD-03 EXHIBIT NUMBER FIGURE 1 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� General 1.4 Geologic Characteristics This section paraphrases the descriptions in the original July 2003 Ground Water Monitoring Plan and the 2003 Design Hydrogeologic Investigation Report. 1.4.1 Regional Geologic and Hydrogeologic Setting Per the 1985 Geologic Map of North Carolina, OSR is located in the Charlotte belt of the Piedmont Physiographic Province. This province is characterized by metamorphic and igneous plutonic rocks, which have been extensively weathered and eroded, forming an undulating topography. Subsurface conditions generally consist of topsoil underlain by residual soils, saprolite, partially weathered rock (PWR), and fractured rock. There is generally a gradual transition between material types with varying thickness. Bedrock is typically fractured granodiorite overlain by PWR, overlain by highly weathered bedrock (saprolite). Saprolite varies in thickness from a few feet to over 100 feet. Saprolite retains some of the original (relict) structural features of the parent rock. The near surface residual soils are formed by physical and chemical weathering of the saprolite and usually do not retain the relict structural features. Groundwater is present within fractures and joints in the bedrock and within the pore spaces of the overlying-saprolite and residual soils. Groundwater is primarily recharged by precipitation and commonly located within the saprolite layer. Groundwater moves laterally and downward toward streams and surface water bodies and generally follows the surface topography. 1.4.2 Site Specific Topography and Drainage Surface drainage at OSR is primarily controlled by a north -northwestern trending ridge within the property. This ridge directs runoff northeast, west and southwest into tributaries of South Fork Muddy Creek. The majority of surface runoff is directed to South Fork Muddy Creek to the north. A small area on the southeast portion of the site appears to drain south into Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow to the west where they converge with Muddy Creek and eventually with the Yadkin River. 1.4.3 Site Specific Hydrogeology As documented in the Design Hydrogeological Investigation Report submitted by HDR on December 2, 2003, the uppermost aquifer underlying the facility is comprised of three stratigraphic units. The stratigraphic downward progression of the three units is saprolite transitioning into PWR, then bedrock. Groundwater flows through the pore space of the saprolite and PWR, while groundwater flow through the bedrock is primarily through fractures. OSR was constructed within the unconsolidated micaceous silty sands and sandy silts produced by the in -situ weathering of the granodioritic parent rock. There is no evidence of discrete flow patterns resulting from relict quartz veins, dikes, healed fractures, or strong preferential alignment of minerals (i.e., foliation). In general, groundwater flows from areas of higher elevation to areas of lower elevation. As such, the water table generally mimics the topography. Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Monitoring Network 2 Monitoring Network The monitoring network consists of fourteen groundwater wells and four surface water sampling point. Sampling of site monitoring wells and surface water monitoring locations is conducted on a semiannual basis. Details of monitoring wells are provided in Table 1. Groundwater monitoring well MW-1 R is located hydraulically upgradient of the landfill and is considered as the background well for the site. Upstream surface water (SW-1) and downstream surface water (SW-2) samples are obtained from the adjacent stream to the east. Two surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity of MW-21R. SW-3 is located south of the entrance road near MW-2R; while SW-4 is located on the north side of the entrance road, downstream of SW-3. Table 1 Existing groundwater monitoring well details OSR LF WELL NC Sate Plane Installed Northing NC Sate Plane Easting Well Diameter (inches) Well Depth (below ground) Depth: Ground to Top of Screen Screened Interval 00 Screened Interval Geology Top Of Casing Elevation Ot MSL) Ground Elevation (lt MSL) MW-1R 12/27/1995 820,411 1,622,983 2 60.0 45 15 Granitic saprolite 836.42 833.40 MW-2R 12/29/1995 820,974 1,622,722 2 23.0 8 15 Granitic saprolite 785.22 781.81 MW-3R 7/7/1999 821,237 1,621,463 2 27.0 12 15 Granitic saprolite 776.60 772.90 MW-4R 12/28/1995 820,435 1,621,428 2 20.0 5 15 Granitic saprolite 767.96 765.70 MW-5R 12/29/1995 820,137 1,622,130 2 32.0 17 15 Granitic saprolite 784.36 782.30 MW-7 12/28/1995 820,886 1,621,424 2 48.0 33 15 Granitic saprolite 803.66 802.10 MW-8 7/7/1999 821,930 1,621,485 2 27.0 12 15 Granitic saprolite 762.50 759.80 MW-9 8/11/2004 822,311 1,621,986 2 60.0 45 15 Sand 790.28 788.04 MW-10 8/10/2004 822,626 1,622,699 2 21.0 6 15 Sand 738.21 735.70 MW-11 8/10/2004 822,307 1,622,838 2 20.0 5 15 Sand 732.59 730.35 MW-12 8/9/2004 821,844 1,622,955 2 16.0 6 10 Silt 739.07 736.41 MW-13 8/9/2004 821,500 1,622,915 2 20.0 5 15 Sand 751.23 749.19 MW-14 8/11/2004 822,420 1,622,260 2 60.0 45 15 Sand 783.88 781.44 MW-15 4/6/2012 821,083 1,622,884 2 48.2 33.2 15 Bedrock 802.85 800.58 The sampling plan for OSR is provided in Table 2. This plan requires full Appendix 11 sampling for all wells every two years and sampling for Appendix I any detected Appendix II constituents during the other events. 4 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Data Collection Table 2 Sampling parameters and schedule Method Parameter(s) Frequency Monitoring Surface Wells Water EPA 300.0 Sulfate 2x/year 2x/ ear All All All All EPA 6010 Trace Metals _ Mercury_ Pesticides: All EPA 7470 2x/ ear All All Fall of odd years 2019 All None Pesticides recently detected: EPA 8081 4,4'-DDD, 4,4'-DDT, Aldrin, alpha-BHC, MW-1 R, MW-2R, delta-BHC, Endosulfan 1, Endosulfan 11, 2x/year MW-4, MW-7, None Endrin, Endrin aldehyde, Heptachlor, MW-10 & MW-15 Heptachlor epoxide & Methox chlor EPA 8082 PCBs: All Fall of odd years 2019 All None Herbicides: All Fall of odd years 2019 All None Herbicides previously detected: MW-1 R, MW-2R, EPA 8151 2,4,5-TP (Silvex), 2,4-D 2x/year MW-4R & MW-15 None App I VOCs + Tetrah drofuran 2x/ ear All All Appendix 11 VOCs Fall of odd years 2019 All None EPA 8260 Apendix II VOCs recently detected: Dichlorodifluoromethane 2x/year All None 1,4-Dioxane 2x/ ear All All SVOCs: All Fall of odd years 2019 All None SVOCs recently detected: EPA 8270 Benzo(a)anthracene, Bis(2- MW-1 R, MW-2R, ethyl hexyl)phthalate, Chrysene 2x/year MW-4R , MW-3R SW-2 Dibenz(a,h)anth racene, & Indeno(1,2,3- & MW-15 cd)pyrene SM 2320B Alkalinity 2x/year All All SM 2540C Total Dissolved Solids 2x/year All All SM 4500 Chloride, Cyanide, Sulfide 2x/ ear All All Field Temperature, Specific conductance, 2x/year All All Dissolved Oxygen, Redox, Turbidity, pH Field Total well depth, static water level 2x/ ear All NA 3 Data Collection 3.1 Water Level Measurements On November 26, 2018, static groundwater level measurements were obtained from groundwater monitoring wells MW-1 R through MW-5R and MW-7 through MW-15. Groundwater depths were measured from the top of the PVC casing. Groundwater is measured to the nearest 0.01 foot prior to purging each well. Depth to water data is used to calculate static groundwater elevations. Groundwater elevations from this event are presented in Table 3. Historic groundwater elevations are depicted on Figure 2. 5 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Data Collection Table 3 Groundwater elevations Well ID Top of Ground Well Screen Depth to Groundwater Casing Elevation Depth Length Water Elevation Elevation (ft MSL) (ft) (ft) (ft) (ft MSL) (ft MSL) MW-1 R 836.42 833.40 60 15 35.08 801.34 MW-2R 785.22 781.81 23 15 7.47 777.75 MW-3R 776.6 772.9 27 15 16.52 760.08 MW-4R 767.96 765.7 20 15 8.02 759.94 MW-5R 784.36 782.3 32 15 10.80 773.56 MW-7 803.66 802.1 48 15 36.45 767.21 MW-8 762.50 759.8 27 15 14.77 747.73 MW-9 790.28 788.04 60 15 53.48 736.80 MW-10 738.21 735.70 21 15 11.51 726.70 MW-11 732.59 730.35 20 15 3.32 729.27 MW-12 739.07 736.41 16 10 4.47 734.60 MW-13 751.23 749.19 20 15 7.89 743.34 MW-14 783.88 781.44 60 15 51.94 731.94 MW-15 802.85 800.58 48.2 15 38.77 764.08 ID - identification ft - feet MSL - mean sea level _ 810 800 0 790 m 780 c 0 770 a� m 760 0 3 750 CO L 1' 740 �a 3 c 730 0 L C9 720 O`3 OR 05 66 61 pub & NO N� N l- N3 NIk Nb N6 K1 NQ) N,) �O � � � � � saw � saw saw say saw saw say saw � P", SeP SeP Sample Date Figure 2 Historical groundwater elevations +MW-1 R fMW-2R -l-- M W-5 R BMW-6R +MW-7 MW-15 --�<- MW-4R f MW-3R --@- M W-8 MW-13 M W-9 --A- MW-12 -W-- MW-14 MW-11 ►I VIM5 6 Winston-Salem City/County Utilities I Assessment Monitoring Report Data Collection 3.2 Groundwater Flow Hydraulic gradients were calculated between representative well pairs. The flow velocities have been calculated based on the values for historic hydraulic conductivity (0.466 ft./day) and effective porosity (25%), as presented in Table 2-9 of the December 2003 OSR Design Hydrogeologic Investigation Report for the landfill. Hydraulic gradients and flow velocities are presented in Table 4. The minimum and maximum values are based on the historic data collected from the site beginning in May 2003. HDR estimates a travel time of about four years between MW-2R and MW-15, based on the estimated flow rate of 49 ft./yr. and a distance of 195 feet. Table 4 Hydraulic gradient and flow velocity Hydraulic Based on Historic Gradient Record (ft./ft. ) Flow May Nov May Nov May Nov Velocity Minimum Maximum 2016 2016 2017 2017 2018 2018 (ft./yr.) MW-1 R to 0.024 0.038 0.02 0.02 0.027 0.027 0.027 0.03 MW-4R 19 18 19 18 26 MW-1 R to 0.027 0.040 0.037 0.04 0.03 0.04 0.03 0.02 MW-2R 18 27 25 27 26 27 26 18 MW-2R to 0.060 0.064 0.06 0.06 0.06 ��42 742 MW-13 41 43 7742 42 42 MW-13 to 0.013 0.015 0.01 0.01 0.01 0.01 0.01 0.01 MW-10 9 10 9 9 9 10 10 10 MW-2R to 0.072 0.07 0.06 0.06 0.06 0.07 MW-15 46 49 49 47 47 47 48 48 3.3 Sample Collection and Analysis Between November 26 and 27, 2018, groundwater samples were collected from fourteen wells and four surface water locations by Pace Analytical Laboratories, Inc. (Pace) of Huntersville, North Carolina (NC Cert. # 5342), on behalf of HDR. On December 11, 2018, MW-3R was resampled due to misplaced sample containers. Low -flow sampling techniques were used to purge groundwater from each well until stabilization of field parameters (pH, conductivity, redox, temperature, turbidity, and dissolved oxygen) occurred. Samples were collected from each of the groundwater wells using the dedicated QED TM MicroPurge® pumps that were installed in August 2004, except MW-15, which is sampled with a variable speed submersible pump. Field parameters were recorded and are presented in Appendix B. Groundwater samples were labeled with the project name, sample ID, date, and time the sample was collected. This same information was recorded on a chain -of -custody form. The Winston-Salem City/County Utilities I Assessment Monitoring Report L I Analytical Results samples were placed in a cooler chilled with ice, then transported under chain -of -custody procedures to Pace. 4 Analytical Results 4.1 Groundwater During this sampling event, twenty-seven detections exceeded the 2L Standard. These exceedances consisted of ten parameters at ten well locations. The constituents detected above 2L Standards or IMACs for this event are: • Benzene in MW-2R • Methylene chloride in MW-7 • Tetrachloroethene in MW-2R • 1,4-Dioxane (p-Dioxane) in MW-10 • Sulfate in MW-10 • Cobalt in MW-2R, MW-3R, MW-4R, and MW-10 • Iron in MW-2R, MW-3R, MW-4R, MW-10, MW-11, MW-12, MW-14 • Manganese in MW-2R, MW-3R, MW-4R, MW-10, MW-11, MW-12, MW-14, MW-15 • Vanadium in MW-5R • Total dissolved solids in MW-2R and MW-10 1,4-Dioxane was added to the sampling schedule for this event with a 2L Standard of 3 pg/L. Three wells had detections for 1,4-Dioxane(MW-2R, MW-4R, and MW-10). MW-10 exceeded the 2L Standard with a result of 8.5 pg/L. Detections during this sampling event are presented in Table 6. Field parameters are presented in Table 7. Historical detections are presented in Appendix A. A copy of the laboratory report is provided in Appendix B. The field data sheets are provided in Appendix C. A Microsoft Excel file containing the analytical data in NCDEQ electronic data deliverable format is include as part of Appendix D. In 2011, MW-2R analytical detections of benzene and PCE above groundwater standards triggered assessment monitoring. The trends of constituents that have detections in MW-2R are shown on Figure 3. Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Analytical Results 111111 11111 1111 111 ����_-�III♦����� 11 1 �� � 0.1 �• . . . OSR Construction Groundwater & Demolition Landfill Detections Permit 34-12 --i—Total Dissolved Solids Total as CaCO3 Sodium Manganese • Tetrahydrofuran • • . - Vinyl chloride . ..- . r��-0—Alkalinity, �I -1--,ilr\lA7l••� -1 . . . . . . CollectedDate . . . Figure 3 MW-2R groundwater detections 4.2 Surface Water Surface water analytical results were compared to 15A NCAC 02B (2B Standards). As the 2B Standards do not have water quality criteria for alkalinity and iron, the EPA Nationally Recommended Water Quality Criteria for Class C freshwater was applied. There were no 2B exceedances however all locations exceeded the Class C standards for alkalinity and iron. SW-1 alkalinity concentrations have had a downward trend since 2012. SW-2 alkalinity concentrations have had an upward trend since November 2014. SW-3 and SW-4 alkalinity concentrations are within historical values and do not show a trend. SW-1, SW-2, SW-3, and SW-4 iron concentrations are within historical values and do not show a trend. Based on comparison to historical data, the exceedances observed during the November 2018 sampling event are consistent with historical values. Detections during this sampling event are presented in Table 6. Field parameters are presented in Table 7. Historical detections are presented in Appendix A. A copy of the laboratory report is provided in Appendix B. The field data sheets are provided in Appendix C. A Microsoft Excel file containing the analytical data in NCDEQ electronic data deliverable format is included as part of Appendix D. 9 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Analytical Results This page intentionally left blank. 10 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Analytical Results Table 5 Lab detections - November 2018 � -A 300.0 /L 250000 250000 pg/L Sulfate 95900 1300 104000 8090 12700 1060W357000 o 91700 5650 49900 4140 20000 16000 27500 SM 0:"0'-q /L 20000 NE pg/L Alkalinity, Total as CaCO3 84100 573000 192000 291000 35600 78500 24200 33500 652000 161000 117000 52800 67100 89900 27400 62600 181000 _ 145000 now-ROMT1 p /L �S _ 230000 250000 pg/L Chloride 8920 34500 2660 25200 15100 6580 3110 5330 88500 1 11800 14400 5120 3840 128000 18300 12800 1 12000 24800 SM 00 /L ML 5 70 pg/L Cyanide 4.1 5 4.3 4 4.2 4.1 SM 00 /L NE NE pg/L Sulfide 53.8 /L 139000 237000 154000 144000 236000 NE 500000 pg/L Total Dissolved Solids 164000 off 213000 496000 156000 171000 68000 301000 111000 395000 106000 241000 off I .. .1: p /L NE 6 pg/L 1,1-Dichloroethane 1.3 26000 NE pg/L 4-Methyl-2-pentanone (MIBK) 0.65 1.19 1 pg/L Benzene EO.5 0.37 0.55 NE 70 pg/L cis-1,2-Dichloroethene 0.38 0.86 NE 1000 pg/L Dichlorodifluoromethane 0.99 2.4 670 500 pg/L m&p-Xylene 1.1 11000 3 pg/L Methylene Chloride 0.59 NE 500 pg/L o-Xylene 0.53 0.7 0.7 pg/L Tetrachloroethene 1:: 110000 NE pg/L Tetrahydrofuran 45.4 50.5 169 11 600 pg/L Toluene 0.26 2.5 3 pg/L Trichloroethene 0.9 NE 2000 pg/L Trichlorofluoromethane 1.2 1.3 1 0.86 0.21 NE 88 pg/L Vinyl acetate 2 Ad -TY.•1' •• pg/L NE 3 pg/L 1,4-Dioxane (p-Dioxane) 2.1 2.48.5 'A 601 1D p /L 21000 700 pg/L Barium 284 258 275 222 59.8 161 36 215 83.1 95.8 132 124 246 24.4 47 78.8 122 124 6.5 4 pg/L Beryllium 0.62 0.88 0.69 0.83 11 10 pg/L Chromium 3.3 4.2 5.6 5.5 NE 1 pg/L Cobalt NE 1000 pg/L Copper 2.6 4.1 1000 300 pg/L Iron 250 1 1 Off-We1 71.8 1840 4140 2500 3890 42.4 NE 15 pg/L Lead 2.6 NE 50 pg/L Manganese 16.7 : • 1 10.7 11 9.8 • 115®�®i � 1 44 4 25 100 pg/L Nickel 16.1 5 11.1 3.3 6.3 NE NE pg/L Sodium 16500 64400 2770 42600 15700 151000 1 13600 1 17600 10900 18600 26100 11800 11900 1 16900 20000 14600 17700 8300 NE 0.3 pg/L Vanadium NE 1000 pg/L Zinc 5.1 5.2 6 5.3 5.8 7.1 6.9 pg/L 0.012 1 pg/L Mercury 0.57 Note - To distinguish non detections (ND) from not sampled (NS), refer to complete laboratory analysis. This table represents both ND and NS as blanks 678 6 11 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Analytical Results Table 6 - Field parameters - November 2018 mg/L IEEq= 0.4 0.5 1 3.6 -39.6 -27.7 3.4 3.3 4.2 6.2 7.2 6.2 -59.7 44.2 -21.1 -5.9 3.2 15.3 15.7 10.9 Oxygen, Dissolved my 0.4 1.6 1.5 0.8 5.5 2.5 4.9 6.7 3.5 163.8 5.7 7.5 -40.1 8.4 -135.3 2.8 -43.2 -69.5 6.8 4.1 48 7.1 198.2 0.55 30.8 0.8 145 1.1 158.8 9.4 -175.7 7.1 -55.8 6.6 REDOX NTU Turbidity Std. Units 5.4 6.3 6.5 6.3 6.2 5.6 5.7 5.7 6.5 5.9 5.9 5.5 5.7 6.1 6 6.6 6.5 6.7 pH feet 35.08 7.47 16.52 8.02 10.8 36.45 14.77 53.48 11.51 3.32 4.47 7.89 51.94 38.77 Static Water Level Total Well Depth mhos/cm 60 21 27 20 30 48 27 60 21 20 15.7 20 60 48 218.7 1145 426 671 170.1 238.2 54.1 152.3 1866 346.4 426 124.8 178 699 1 125.1 203.7 376 374.7 Specific Conductance de C 13.5 14 15.1 14.7 13.8 7.3 14.6 14.5 13 13.4 14.8 14.2 13.6 15.5 11 11.1 11 11.7 Temperature 12 Winston-Salem City/County Utilities i Assessment Monitoring Report ��� Summary & Conclusions 4.3 Landfill Gas Landfill gas is measured at MW-2R and wells in the vicinity of MM-1 during each groundwater sampling event. The results indicate the presence of carbon dioxide above ambient levels in MM-1. The City is responsible for quarterly sampling of all methane monitoring wells and the related reporting, which is not included in this document. Gas readings taken during this event are presented in Table 7. Table 7 - Gas Readings Date ID # CH4 (%) COZ (%) 02 (%) Balance (%) 26-Nov-18 MM-1 0.0% 4.4% 18.0% 77.6% 26-Nov-18 MW-1 R 0.0% 0.1 % 20.2% 79.7% 26-Nov-18 MW-2R 0.0% 0.6% 22.6% 76.8% 26-Nov-18 MW-13 0.0% 0.2% 19.9% 79.9% 26-Nov-18 MW-15 0.0% 0.2% 19.8% 80.0% Highlighted cells are outside of normal atmospheric ranges 5 Summary & Conclusions 1,4-Dioxane was added to the sampling schedule for this event with a 2L Standard of 3 pg/L. MW-10 exceeded the 2L Standard with a result of 8.5 pg/L. 1,4-Dioxane will continue to be monitored. Other detections from this event are generally consistent with previous events. No changes to the current plan are recommended at this time. 13 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Summary & Conclusions This page intentionally left blank. 14 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix A — Summary of Groundwater Monitoring Results Appendix A— Summary of Groundwater Monitoring Results 1 Appendix II Detections 2 Detections by Well Location 3 Detections by Date 4 Surface Water Detections Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix A — Summary of Groundwater Monitoring Results This page intentionally left blank. Al 50 pg/L 50 pg/L 70 pg/L 70 pg/L 70 pg/L 0.3 pg/L 0.3 pg/L 0.1 pg/L 0.1 pg/L 0.1 pg/L 0.1 pg/L 0.002 pg/L 0.002 pg/L 40 pg/L 40 pg/L 40 pg/L 42 pg/L 42 pg/L 42 pg/L 2 pg/L 2 pg/L 2 pg/L 2 pg/L 2 pg/L 0.008 pg/L 0.008 pg/L 0.004 pg/L 0.004 pg/L 0.004 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column .. Labels •• Row Labels 2,4,5-TP Silvex MW-2R 2,4-D MW-2R MW-15 Pentachlorophenol Equipment Blank 4,4'-DDD MW-15 SW-3 SW-4 Dieldrin MW-7 Endosulfan I MW-7 MW-10 Endosulfan II MW-4R SW-3 Endrin MW-2R SW-1 Endrin aldehyde MW-2R Heptachlor MW-10 Heptachlor epoxide MW-7 MW-10 W-S GW Revised.xlsb 1 of 7 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value V Column Labels 00 w Row Labels z NE pg/L NE pg/L NE pg/L NE pg/L 40 pg/L 40 pg/L 0.05 pg/L 0.05 pg/L 200 pg/L 200 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 1000 pg/L 1000 pg/L 5 pg/L 5 pg/L 0.005 pg/L 0.005 pg/L 100 pg/L 100 pg/L 100 pg/L 0.05 pg/L 0.05 pg/L 2,4-Dinitrotoluene MW-2R 1 5.9 2,6-Dinitrotoluene MW-2R 1 1 8.1 3&4-Meth (phenol m&p Cresol) SW-3 1 3.6 Benzo a anthracene MW-1 R Benzo ,h,i pe lene MW-3R I 1 1 _ bis 2-Eth (hex I phthalate 2.4 MW-1 R MW-2R 1.1 MW-5R 1 M W-9 MW-14 • But lbenz !phthalate MW-4R 1.7 Chrysene MW-1 R 1.5 Dibenz a,h anthracene MW-3R Di-n-octylphthalate MW-8 5.6 MW-12 5.6 Indeno(1,2,3-cd)pyrene MW-3R W-S GW Revised.xlsb 2 of 7 Al 6 pg/L 6 pg/L 6 pg/L 0.4 pg/L 0.4 pg/L 6 pg/L 6 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 40 pg/L 40 pg/L 40 pg/L 40 pg/L 40 pg/L NE pg/L NE pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard ColumnValue .. .•- •• . • Row Labels o 0 1,1-Dichloroethane MW-2R 0.39 0.54 0.48 0.48 0.53 0.49 1.1 0.83 1.3 1.2 1.2 MW-7 1.3 1 1.1 1.6 1.4 1.3 1.5 1.2 0.91 1.1 1.3 0.81 0.9 0.8 1.2 1,2-Dichloroethane MW-2R 1 0.24 _ 1,4-Dichlorobenzene 0.46 0.38 0.4 MW-2R 1 0.41 0.37 0.39 _ 1,4-Dioxane (p-Dioxane) MW-2R 2.1 MW-4R 2.4 MW-10 2-Hexanone MW-2R 0.5 MW-10 0.72 0.69 0.96 SW-2 1.8 SW-4 3.1 4-Meth I-2-pentanone MIBK 2.5 2.6 5.6 2.2 MW-1 0 0.65 1.7 1.1 2.8 Acetone 18.3 Equipment Blank MW-2R 10.3 20 MW-3R 21.4 MW-4R 11 MW-5R 18.4 MW-7 15.7 MW-8 15.8 MW-10 16.4 13.7 12.1 22.5 14.1 11.8 MW-11 21.1 MW-12 12.1 MW-13 17.3 MW-14 14.7 MW-15 13.2 SW-1 11.2 W-S GW Revised.xlsb 3 of 7 Al 6000 pg/L 6000 pg/L 6000 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 700 pg/L 700 pg/L 3000 pg/L 3000 pg/L 3000 pg/L 70 pg/L 70 pg/L 70 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Value Column .. Labels •• . CD • Row Labels SW-2 12.9 SW-3 16.2 SW-4 16 Benzene MW-2R MW-4R 0.38 0.42 0.28 0.27 MW-7 0.37 0.41 0.39 0.38 0.43 0.42 0.26 0.29 MW-10 0.55 0.55 0.57 0.52 0.83 0.46 0.44 SW-3 0.42 0.54 0.32 0.88 Carbon disulfide MW-10 1 2.1 2 5.2 Chloroethane MW-2R 2.1 M W-7 Chloroform M W-2 R _ MW-15 I 0.45 0.44 0.44 0.4 0.44 0.7 0.44 0.26 0.49 0.77 0.6 Chloromethane MW-2R 0.25 _ MW-7 0.13 MW-11 0.23 SW-2 0.12 cis- 1,2-Dichloroethene MW-1 R 0.85 0.71 0.76 0.62 0.38 0.2 MW-2R 0.38 0.55 0.66 0.6 0.51 0.47 0.26 0.5 0.38 0.41 0.3 MW-7 0.86 0.85 1.1 1.1 1.1 1.1 0.77 0.8 0.73 0.73 0.37 0.54 0.7 MW-10 0.23 0.27 0.23 0.2 0.33 0.35 MW-12 0.23 SW-2 0.33 SW-3 0.26 1.31 0.3 1.3 0.2 0.5 0.3 0.6 W-S GW Revised.xlsb 4 of 7 Al 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 600 pg/L 600 pg/L 600 pg/L 500 pg/L 500 pg/L 500 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 6 pg/L 6 pg/L W-S GW Revised.xlsb Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard Dichlorodifluoromethane MW-2R MW-7 MW-9 0.99 MW-12 MW-14 2.4 Ethylbenzene MW-1 R MW-10 m&p-X lene MW-7 1.1 MW-10 Methylene Chloride Equipment Blank MW-1 R MW-2R MW-3R MW-4R MW-5R MW-7 MW-8 MW-10 MW-11 MW-12 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4 Naphthalene MW-2R 1.2 1.7 1.2 3 3.6 3.9 0.41 0.53 1.7 1.6 1.4 0.68 1.3 1.1 1.2 2.4 1.7 1.1 0.62 1.5 0.88 3.6 2.3 0.38 0.55 1.2 2.2 2.1 0.26 1 0.76 0.23 3.6 2.1 0.41 11 0.73 1.8 0.84 1.5 1.1 0.68 1.2 1.1 1.1 1.8 2.3 1.3 2.3 2.3 2.9 1.1 2.8 1.2 1.4 2 2 1.6 2.4 2 1 1.2 2.1 1 2.9 0.28 1 0.3 1 0.861 1.31 1.6 5 of 7 Al NE NE NE NE NE NE NE NE NE NE NE NE Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard 500 pg/L _ o-Xylene 500 pg/L MW-2R 500 pg/L MW-7 500 pg/L MW-10 0.7 pg/L Tetrachloroethe 0.7 pg/L MW-2R 0.7 pg/L MW-7 0.7 pg/L MW-14 pg/L Tetrahydrofurar pg/L Equipment BIB pg/L MW-2R pg/L MW-4R pg/L MW-7 pg/L MW-10 pg/L MW-11 pg/L MW-12 pg/L MW-15 pg/L SW-2 pg/L SW-3 pg/L SW-4 600 pg/L Toluene 600 pg/L MW-2R 600 pg/L MW-10 600 pg/L SW-2 3 pg/L Trichloroethene 3 pg/L MW-1 R 3 pg/L MW-2R 3 pg/L MW-7 lumn .• Labels C• • • . W 0 0.33 0.31 0.54 0.5 0.6 0.59 0.65 0.62 0.68 0.46 0.63 0.47 0.27 0.4 0.36 0.3 0.53 0.78 1.1 0.97 1 2.1 0.43 0.85 0.65 ne 0:: 0• 0.48 0.61 ink 3.2 45.4 46 59.1 28 36.3 39.1 49.6 35.8 34.6 79.2 72.6 99.6 111 93 9.3 13.6 3.5 7 5.8 15.9 11.8 11.7 8.5 14 50.5 24.9 20.1 32 21.7 13.5 17.7 14.1 8.8 5.2 13.7 24 26 169 192 135 131 182 237 6.1 120 145 106 18.6 5 4.5 5.9 11.4 26.8 12.4 14.8 12 16.8 27.3 19.8 16.9 15.5 21.4 14.7 7.4 6.3 61.3 18.4 3.4 6.3 3.3 10.2 9.7 18.9 5.1 4.8 5.7 3.5 3.6 4.1 4.4 0.27 0.26 0.35 0.27 0.63 0.52 0.65 0.9 0.93 1.3 0.93 1 1.2 0.71 0.66 0.79 0.85 0.71 0.89 0.7 0.8 0.58 W-S GW Revised.xlsb 6 of 7 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard 2000 tag/L _ Trichlorofluor 2000 tag/L MW-2R 2000 tag/L MW-7 2000 tag/L MW-9 2000 tag/L MW-10 2000 tag/L MW-12 2000 tag/L MW-14 2000 tag/L MW-15 2000 tag/L SW-4 88 tag/L Vinyl acetate 88 tag/L MW-2R 0.03 tag/L Vinyl chloride 0.03 tag/L MW-2R 500 tag/L Xylenes (Tot; 500 tag/L MW-2R 500 tag/L MW-7 500 tag/L MW-10 Column Labels . M a amethane 1.5 0.71 1 1.5 2.4 3.7 12 1.2 1.2 1.6 1.6 0.91 1.5 0.92 1.4 0.79 1.2 0.62 0.47 1.3 1.3 1.4 1.2 1.4 1 1.3 1.1 0.98 0.96 0.47 0.69 0.2 0.33 1 0.89 1.4 0.52 1 2.8 1.4 0.82 0.22 0.32 0.86 0.79 0.8 0.87 0.75 0.58 1.1 0.54 0.59 0.57 0.34 0.21 0.42 0.22 0.71 2.1 4.4 5.1 4.8 4.4 3.9 5.3 7.6 0.32 0.27 0.25 2 �I) 1 1 1I Ewa 1.1 W-S GW Revised.xlsb 7 of 7 This page intentionally left blank. A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location MW-1 R NE pg/L Alkalinity, Total as CaCO3 71400 54900 84100 76100 68600 64300 10 pg/L Arsenic 700 pg/L Barium 284 263 260 272 241 228 0.05 pg/L Benzo(a)anthracene 3 pg/L bis(2- Ethyl hexyl)phthalate 700 pg/L Carbon disulfide 250000 pg/L Chloride 8920 9040 9290 8860 9630 9000 10 pg/L Chromium 4 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 0.85 0.71 0.76 0.62 0.38 0.2 70 pg/L Cyanide 600 pg/L Ethylbenzene 0.38 300 pg/L Iron 111 43.1 54.8 96.2 78.8 15 pg/L Lead 50.0 pg/L Manganese 16.7 17.6 11.8 12.5 7.3 7.2 1 pg/L Mercury 0.57 0.34 0.23 3 pg/L Methylene Chloride 2.3 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 16500 15500 15200 15800 14600 13300 250000 pg/L Sulfate 1380 1080 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 164000 166000 153000 165000 154000 138000 3 pg/L Trichloroethene 0.65 1000 pg/L Zinc 5.1 5 5.5 5.7 MW-2R 6 pg/L 1,1-Dichloroethane 0.39 0.54 0.53 0.48 0.48 350 pg/L 1,1-Dichloroethene 0.4 pg/L 1,2-Dichloroethane 0.24 6 pg/L 1,4-Dichlorobenzene 0.41 0.37 0.46 0.39 3 pg/L 1,4-Dioxane (p-Dioxane) 2.1 50 pg/L 2,4,5-TP (Silvex) 0.072 70 pg/L 2,4-D NE pg/L 2,4-Dinitrotoluene NE pg/L 2,6-Dinitrotoluene 4000 pg/L 2-Butanone (MEK) 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 10.3 0.002 pg/L Aldrin NE pg/L Alkalinity, Total as CaCO3 573000 663000 670000 587000 571000 482000 0.006 pg/L alpha-BHC 1 pg/L Antimony 10 pg/L Arsenic 700 pg/L Barium 258 289 323 323 272 324 1 pg/L Benzene 3 pg/L bis(2- Ethyl hexyl)phthalate 2 pg/L Cadmium 250000 pg/L Chloride 34500 42200 47600 50400 47600 47700 3000 pg/L Chloroethane 70 pg/L Chloroform 3 pg/L Chloromethane 10 pg/L Chromium 3.3 2.7 2.8 2.6 70 pg/L cis-1,2-Dichloroethene 0.38 0.55 0.66 0.6 0.51 0.47 1 pg/L Cobalt I . 1000 pg/L Copper 2.6 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 1 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 70 pg/L Cyanide 4.1 5 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron . 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese is 8.88 is 1 pg/L Mercury NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 1.1 6 pg/L Naphthalene 100 pg/L Nickel 16.1 16.8 20.3 17 NS pg/L Nitrogen, Ammonia 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 64400 73200 77600 72400 250000 pg/L Sulfate 95900 105000 122000 110000 0.7 pg/L Tetrachloroethene 0.88 NE pg/L Tetrahydrofuran 45.4 46 59.1 28 36.3 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids .:: : 1 f l • .a 3 pg/L Trichloroethene 0.9 0.93 1.3 0.93 1 2000 pg/L Trichlorofluoromethane 1.5 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 2 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 192000 115000 78900 10 pg/L Arsenic 5.7 9 700 pg/L Barium 275 234 278 200 pg/L Benzo(g,h,i)perylene 3 pg/L bis(2- Ethyl hexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 2660 2180 2650 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 5 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 15 pg/L Lead 4.9 3.4 50 pg/L Manganese •� �� 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 2770 2680 2380 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND W-S GW Revised.xlsb 5.1 18.51 1 17.9 70200 61500 121000 115000 39.1 49.6 1.2 0.71 0.71 21.4 114000 133000 87800 5.5 3.9 3.3 309 297 278 25201 20501 1 2470 IN E 300 86400 77200 5 2240 2450 5.5 2310 2 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 250000 pg/L Sulfate 1300 691 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 213000 177000 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 2.4 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 291000 101000 10 pg/L Arsenic 700 pg/L Barium 222 270 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 25200 12500 3 pg/L Chloromethane 10 pg/L Chromium 6.4 1 pg/L Cobalt 1 - 1000 pg/L Copper 5 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron •' 1 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 5 4.1 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 42600 17800 250000 pg/L Sulfate 104000 50300 NE pg/L Sulfide 105 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 0.029 500000 pg/L Total Dissolved Solids 496000 250000 0.3 pg/L Vanadium 1 1000 pg/L Zinc 5.2 19.9 MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 35600 33600 10 pg/L Arsenic 700 pg/L Barium 59.8 52.5 3 pg/L bis(2- Ethyl hexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 15100 15200 3 pg/L Chloromethane 10 pg/L Chromium 5.5 5.3 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 88.2 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb `I[*WII1] 11 461000 315000 198 343 1.7 49200 35800 3.2 7.5 5.8 65500 42100 179000 125000 9.3 1530 133000 168000 454000 255 0.38 58400 214 8 71000 193000 13.6 5.8 8.6 8.4 18.4 33500 32300 32700 53.2 57.1 55.9 1800 188000 99000 210 13800 3.2 M 2.8 4.2 2.9 3.2 14500 48700 3.5 241000 �'' 17.8 30800 55.9 16200 15100 16400 15300 111111MI 4.6 5.8 5.1 4.4 37.9 68.4 87.8 4.2 3 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 14600 12800 13500 13900 14200 13100 250000 pg/L Sulfate 8090 8220 7830 7740 8450 7620 500000 pg/L Total Dissolved Solids 156000 164000 144000 156000 145000 154000 0.3 pg/L Vanadium 1000 pg/L Zinc 7.3 MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1, 1, 1 -Trichloroethane _ 6 pg/L 1,1-Dichloroethane 1.3 1.1 1.6 1.4 1.3 1.5 1.2 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone 15.7 NE pg/L Alkalinity, Total as CaCO3 78500 75900 80400 85000 80100 71700 10 pg/L Arsenic 700 pg/L Barium 161 158 152 163 140 129 1 pg/L Benzene 0.37 0.41 0.39 0.38 0.43 0.42 0.26 4 pg/L Beryllium 0.62 2.1 0.58 0.019 pg/L beta-BHC 700 pg/L Carbon disulfide 250000 pg/L Chloride 6580 6490 7390 5290 4820 4430 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 0.86 0.85 1.1 1.1 1.1 1.1 0.77 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.62 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.15 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 35 25 25.2 15 pg/L Lead 500 pg/L m&p-Xylene 1.1 1.7 1.6 1.4 1.2 2.2 1.8 50 pg/L Manganese 44 43.8 43 35.6 28.8 1 pg/L Mercury 3 pg/L Methylene Chloride 1.7 500 pg/L o-Xylene 0.59 0.65 0.62 0.68 0.46 0.63 0.47 20 pg/L Silver NE pg/L Sodium 17700 16600 15300 17800 16200 16400 250000 pg/L Sulfate 12700 14200 13400 6720 3800 2930 0.7 pg/L Tetrachloroethene 0.48 NE pg/L Tetrahydrofuran 50.5 24.9 20.1 32 21.7 13.5 500000 pg/L Total Dissolved Solids 171000 181000 175000 175000 153000 137000 3 pg/L Trichloroethene 0.58 2000 pg/L Trichlorofluoromethane 1.2 1.2 1.6 1.6 0.91 1.5 0.92 500 pg/L Xylenes (Total) 1000 pg/L Zinc 6 9 5 8.9 5.7 5.2 MW-8 6000 pg/L Acetone 15.8 NE pg/L Alkalinity, Total as CaCO3 24200 27000 28200 20800 25800 24800 10 pg/L Arsenic 700 pg/L Barium 36 41.2 46.5 42.9 44 38.3 250000 pg/L Chloride 3110 3660 3860 3060 2670 1960 10 pg/L Chromium 2.6 4.9 4.1 70 pg/L Cyanide 9.9 4.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 4 of 50 A2 Facility Permit ICY,9 K Old Salisbury Road Landfill (C&D) Historical detections b well location 100 pg/L Di-n-octylphthalate 300 pg/L Iron 42.4 39.3 15 pg/L Lead 50 pg/L Manganese 4 4.4 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 8300 8810 250000 pg/L Sulfate 1060 2980 500000 pg/L Total Dissolved Solids 68000 75000 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 31800 33500 10 pg/L Arsenic 700 pg/L Barium 215 193 3 pg/L bis(2- Ethyl hexyl)phthalate 250000 pg/L Chloride 5330 4830 10 pg/L Chromium 4.2 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.99 1.2 1. 300 pg/L Iron 250 35.3 15 pg/L Lead 50 pg/L Manganese 10.7 4.2 20 pg/L Silver NE pg/L Sodium 15700 14300 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 139000 133000 2000 pg/L Trichlorofluoromethane 1.3 1.3 1. 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) 8.5 40 pg/L 2-Hexanone 0.72 NE pg/L 4-Methyl-2-pentanone (MIBK 0.65 1.7 6000 pg/L Acetone 16.4 13. NE pg/L Alkalinity, Total as CaCO3 652000 506000 10 pg/L Arsenic 700 pg/L Barium 83.1 94.7 1 pg/L Benzene 0.55 0.55 0.5 4 pg/L Beryllium 700 pg/L Carbon disulfide 2. 250000 pg/L Chloride 88500 158000 10 pg/L Chromium 5.6 4.1 70 pg/L cis- 1,2-Dichloroethene 0.23 0.2 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 4.3 4.8 40 pg/L Endosulfan I 600 pg/L Ethylbenzene 0.4 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron I I of 15 pg/L Lead 2.6 3.9 500 pg/L m&p-Xylene 0.68 1. 50 pg/L Manganese 00 of 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 11.1 8.5 500 pg/L o-Xylene 0.53 0.78 1. yw III -pop, 37.6 3.6 3 2.7 9860 9240 9700 4740 2700 4090 82000 67000 67000 5.3 27900 25400 23300 196 207 195 4430 4610 4360 7.2 7 1.2 1.5 0.88 166 149 10.6 4.6 8.5 14900 15400 15700 960 3440 136000 141000 135000 4 1.2 1.4 1 2.8 5.1 1.1 2.5 7 12.1 22.5 14.1 520000 446000 626000 2.6 106 221 148 7 0.52 0.83 1 2 5.2 163000 : M 202000 4.6 4.2 6.4 7 0.23 0.2 0.33 5.4 1 0.53 0.55 2.6 3;=4.1 2.1 7.6 6.9 10.7 1 0.97 1 2.1 2.9 1.1 8280 1630 87000 21200 197 6850 128 6.3 14200 103000 1.3 29000 5.2 292 3.2 9640 9.1 16.4 4.1 0.12 2.8 4.7 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 5 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 151000 157000 138000 123000 250000 pg/L Sulfate 64100 w1amillus 1 1 NE pg/L Sulfide 240 127 NE pg/L Tetrahydrofuran 169 192 135 131 182 0.2 pg/L Thallium 0.043 2000 pg/L Tin 600 pg/L Toluene 0.26 0.35 0.27 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-11 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 1 161000 95.8 11800 4 . I I II O 130000 82.8 12500 4.4 1.1 15 pg/L Lead 50 pg/L Manganese FF 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 13600 12000 250000 pg/L Sulfate 20700 15300 NE pg/L Sulfide 53.8 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 237000 232000 0.3 pg/L Vanadium 1000 pg/L Zinc MW-12 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 117000 65800 10 pg/L Arsenic 700 pg/L Barium 132 82.8 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 0.88 250000 pg/L Chloride 14400 11100 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 0.23 70 pg/L Cyanide 4.8 1000 pg/L Dichlorodifluoromethane 100 pg/L Di-n-octylphthalate 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 175 50 pg/L Manganese 3 pg/L Methylene Chloride Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 5.4 21.1 130000 135000 89.8 102 130001 13500 0.23 12300 11700 16200 14100 4.5 2180001 226000 :0122 555000 10300 15800 6.1 3.1 311000 5.11 1 34 107000 104000 93.1 103 14500 14500 4.1 1.4 12000 11200 17100 15200 189000 236000 12.1 73800 64500 72900 55900 84.2 113 144 190 104001 19700 23300 26000 125 274 E, 6 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 3.3 20 pg/L Silver NE pg/L Sodium 17600 13400 250000 pg/L Sulfate 91700 64300 NE pg/L Tetrahydrofuran 5.9 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 301000 218000 2000 pg/L Trichlorofluoromethane 1 0.89 1.1 1000 pg/L Zinc MW-13 350 pg/L 1,1-Dichloroethene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 52800 47200 10 pg/L Arsenic 700 pg/L Barium 124 114 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 0.69 0.63 250000 pg/L Chloride 5120 4790 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 71.8 108 15 pg/L Lead 50 pg/L Manganese 9.8 7.4 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 10900 9540 250000 pg/L Sulfate 5650 4510 NE pg/L Sulfide NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 111000 107000 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 67100 61800 10 pg/L Arsenic 700 pg/L Barium 246 212 4 pg/L Beryllium 0.83 0.59 3 pg/L bis(2- Ethyl hexyl)phthalate 250000 pg/L Chloride 3840 3930 3 pg/L Chloromethane 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 2.4 3 3.1 300 pg/L Iron 124 15 pg/L Lead 50 pg/L Manganese 17.4 1 pg/L Mercury 3 pg/L Methylene Chloride Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 4.41 6.21 1 5.5 13200 16200 19200 19200 62400 86100 129000 169000 11.4 26.8 12.4 0.021 219000 288000 286000 382000 0.52 1 2.8 1.4 17.3 44600 42400 42300 41000 116 120 91.6 210 0.52 2.2 4770 4310 4100 4590 3.8 8.5 NO 343 11000 ME �: 0 9740 1 10000 9380 1 9420 4960 5670 5390 7280 2.5 90000 1 89000 79000 1 145000 5.7 12.8 40.5 14.7 63500 55300 59700 50400 214 221 188 188 0.54 0.6 0.57 0.83 3620 3260 3410 3470 4.3 3.9 3.6 2.3 3.6 93.9 134 123 18.4 18.1 13.7 21.6 L. 7 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 6.3 2.6 20 pg/L Silver NE pg/L Sodium 18600 16900 17100 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 154000 152000 142000 2000 pg/L Trichlorofluoromethane 0.86 0.79 0.8 0.87 0.3 pg/L Vanadium 1000 pg/L Zinc 5.3 MW-15 350 pg/L 1,1-Dichloroethene 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 89900 112000 10 pg/L Arsenic 700 pg/L Barium 24.4 11.4 250000 pg/L Chloride 128000 89700 70 pg/L Chloroform 0.45 0.4, 10 pg/L Chromium 1000 pg/L Copper 3 70 pg/L Cyanide 4.2 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 26100 20500 250000 pg/L Sulfate 49900 54600 NE pg/L Sulfide NE pg/L Tetrahydrofuran 14.8 0.2 pg/L Thallium 0.27 110000 17.1 89800 0.44 19800 59600 500000 pg/L Total Dissolved Solids 395000 369000 370000 2000 pg/L Trichlorofluoromethane 0.21 0.42 0.22 0.71 0.3 pg/L Vanadium 1000 pg/L Zinc 5.8 6.6 1llllllE 7.1 SW-1 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 27400 49200 10 pg/L Arsenic 700 pg/L Barium 47 68.2 4 pg/L Beryllium 2 pg/L Cadmium 250000 pg/L Chloride 18300 29700 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 2 pg/L Endrin 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 16900 16200 663 1400 0.61 0.048 130000 118000 0.75 0.58 13.2 98100 101000 22.7 14 104000 98000 0.4 0.44 2.6 2.7 21600 20200 58300 58700 12 16.8 0.049 410000 371000 2.1 4.4 16.21 6.3 2.7 15400 85000 1.1 104000 11 94000 0.7 227 2.4 20100 63700 27.3 418000 5.1 5.9 43600 33200 57400 27700 3.6 47.5 86.8 65.9 69.5 35700 49200 26800 26000 8.6 4.4 4.7 F21 8 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 11800 15600 17000 23000 14200 13000 250000 pg/L Sulfate 4140 2060 2730 2530 3410 4320 500000 pg/L Total Dissolved Solids 106000 131000 123000 143000 116000 118000 0.3 pg/L Vanadium 1000 pg/L Zinc 5.2 10.1 7.2 SW-2 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone 12.9 NE pg/L Alkalinity, Total as CaCO3 62600 56000 57600 46200 58800 32300 10 pg/L Arsenic 3.7 700 pg/L Barium 78.8 74.2 65.4 77.5 108 73.1 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3 pg/L bis(2- Ethyl hexyl)phthalate 250000 pg/L Chloride 12800 13500 15200 13800 6190 9720 3 pg/L Chloromethane 0.12 10 pg/L Chromium 2.8 3.8 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 0.33 1 pg/L Cobalt 1000 pg/L Copper 4.1 70 pg/L Cyanide 4.2 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 15 pg/L Lead 2.7 50 pg/L Manganese • . .0 1 pg/L Mercury 3 pg/L Methylene Chloride 3.1 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 11900 11300 11600 11600 10200 8420 250000 pg/L Sulfate 20000 11100 9920 10900 6270 17100 NE pg/L Sulfide NE pg/L Tetrahydrofuran 61.3 600 pg/L Toluene 0.52 500000 pg/L Total Dissolved Solids 144000 135000 125000 129000 106000 113000 0.3 pg/L Vanadium 1000 pg/L Zinc SW-3 40 pg/L 3&4-Methylphenol(m&p Cresol) 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 16.2 NE pg/L Alkalinity, Total as CaCO3 181000 356000 477000 251000 520000 161000 700 pg/L Barium 122 223 217 173 270 114 1 pg/L Benzene 0.42 250000 pg/L Chloride 12000 22300 33800 18400 34000 10500 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 0.26 1 pg/L Cobalt Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 9 of 50 A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location 1000 pg/L Copper 70 pg/L Cyanide 4.6 6 42 pg/L Endosulfan II 300 pg/L Iron 19911 1 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 1 100 pg/L Nickel 3.9 5.5 3.6 6.8 NE pg/L Sodium 16900 27000 35500 24600 38400 14700 250000 pg/L Sulfate 16000 18500 33800 15200 18500 11400 NE pg/L Tetrahydrofuran 3.4 6.3 2000 pg/L Tin 2.8 500000 pg/L Total Dissolved Solids 241000 413000 RM11111JI 321000 231000 0.3 pg/L Vanadium 1000 pg/L Zinc 7.1 9.6 SW-4 350 pg/L 1,1-Dichloroethene 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 16 NE pg/L Alkalinity, Total as CaCO3 145000 211000 192000 187000 240000 148000 700 pg/L Barium 124 138 110 121 128 113 250000 pg/L Chloride 24800 29800 36800 27400 27900 20300 70 pg/L Chloroform 10 pg/L Chromium 4.7 1 pg/L Cobalt 70 pg/L Cyanide 4.1 5.6 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron 4 : 0 1520 1 .10 50 pg/L Manganese 2900 2930 3 pg/L Methylene Chloride 1.2 116goo900 100 pg/L Nickel 2.6 2.5 NE pg/L Sodium 20000 23400 25600 23400 26000 250000 pg/L Sulfate 27500 24400 26700 18200 28600 16600 NE pg/L Tetrahydrofuran 5.7 3.5 3.6 500000 pg/L Total Dissolved Solids 236000 327000 317000 289000 325000 229000 2000 pg/L Trichlorofluoromethane 0.32 0.3 pg/L Vanadium 1000 pg/L Zinc 6.9 8.3 7.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 10 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location MW-1 R NE pg/L Alkalinity, Total as CaCO3 29800 27500 48100 39600 37600 30000 28100 26300 27100 10 pg/L Arsenic 700 pg/L Barium 207 164 142 124 106 109 91.7 93.8 82.6 0.05 pg/L Benzo(a)anthracene 3 pg/L bis(2-Ethylhexyl)phthalate 2.4 700 pg/L Carbon disulfide 250000 pg/L Chloride 8510 7640 7090 5600 5880 5910 5320 5350 10 pg/L Chromium 5 pg/L Chrysene 1.5 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 4.4 600 pg/L Ethylbenzene 300 pg/L Iron 82.8 85.8 52.9 15 pg/L Lead 50.0 pg/L Manganese 2.8 2.9 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 13200 11600 10600 10800 9940 9080 9180 9440 7670 250000 pg/L Sulfate 1070 1700 1720 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 78000 133000 120000 91000 103000 84000 95000 93000 95000 3 pg/L Trichooroethene 1000 pg/L Zinc 5.6 MW-2R 6 pg/L 1, 1 -Dichloroethane 0.49 0.83 1.3 1.2 1.2 1.1 1.1 350 pg/L 1,1-Dichloroethene 36.6 0.4 pg/L 1,2-Dichloroethane 6 pg/L 1,4-Dichlorobenzene 0.38 0.4 3 pg/L 1,4-Dioxane (p-Dioxane) 50 pg/L 2,4,5-TP (Silvex) 0.14 0.23 70 pg/L 2,4-D 0.43 1.1 NE pg/L 2,4-Dinitrotoluene 5.9 NE pg/L 2,6-Dinitrotoluene 8.1 4000 pg/L 2-Butanone (MEK) 40 pg/L 2-Hexanone 0.48 0.1 pg/L 4,4'-DDT 1 6000 pg/L Acetone 20.3 0.002 pg/L Aldrin NE pg/L Alkalinity, Total as CaCO3 440000 358000 453000 344000 349000 363000 277000 196000 0.006 pg/L alpha-BHC 1 pg/L Antimony 10 pg/L Arsenic r324 700 pg/L Barium 279 287 339 311 324 335 366 1 pg/L Benzene 3 pg/L bis(2-Ethylhexyl)phthalate 1.1 2 pg/L Cadmium 250000 pg/L Chloride 48700 44200 49800 50500 56700 50000 64000 61500 3000 pg/L Chloroethane 2.1 70 pg/L Chloroform 0.16 3 pg/L Chloromethane 0.25 10 pg/L Chromium 3.4 70 pg/L cis-1,2-Dichloroethene 0.26 0.5 0.38 0.41 0.26 0.25 0.33 1 pg/L Cobalt 1 6.31 9.6 1000 pg/L Copper Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 11 of 50 A2 Facility Permit 70 pg/L Cyanide 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 6 pg/L Naphthalene 100 pg/L Nickel NS pg/L Nitrogen, Ammonia 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium Old Salisbury Road Landfill (C&D) Historical detections by well location 7.5 4.2 0.26 0.27 0.23 0.28 1 : 3080 • .1 2580 1650 766 877 1730 3190 3.3 90 •11 9"1 7950 8710 7880 8400 8280 0.83 1.3 2.3 0.86 1.3 1.6 1.9 18 17 25.9 20.6 27.1 20.7 21.8 22.3 0.33 0.31 0.54 0.54 0.63 1 16.5 5.2 61400 51400 58300 59700 46200 45700 43400 38400 115000 98400 117000 136000 128000 115000 79500 95000 1• 35.8 34.6 79.2 72.6 99.6 111 93.2 152 0.27 MM 0.66 0.79 0.85 0.71 0.89 0.68 0.77 0.82 1 1.5 2.4 3.7 12 12.1 16.9 20.9 0.98 1.6 5.8 8.7 16.8 155000 12.2 155000 21.1 175000 24.5 35.2 150000 102000 107000 177000 142000 8.9 271 214 221 205 201 216 173 228 1 2990 2990 2940 3260 3620 3860 3920 6.2 10.4 =18.1 9.1 6.5 11 11 3.8 2.7 2.7 2.3 2590 2770 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 12 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) 250000 pg/L Sulfate 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver Historical detections by well location 2200 3000 3740 4230 3400 5070 5420 6860 5.8 137000 .. 182000 191000 187000 193000 175000 172000 168000 8.7 10.5 1 144000 117000 286000 222000 224000 203000 174000 64300 143000 184 306 305 264 296 375 400 407 328 0.42 0.28 0.27 16900 22200 50500 29700 46.6 36500 33700 34500 33200 29200 4.3 49.4 5.9 11•• 0.12 292 126 89.5 158 145 .: 3.7 2.8 7.2 5.3 11.5 23800 23000 55400 39700 42600 42600 43600 40400 35300 70300 72700 143000 85200 113000 97600 73600 98700 61800 7 5.8 15.9 11.8 11.7 8.5 13.5 8.8 161000 304000 445000 496000 413000 435000 374000 345000 .• 111 5.9 7.5 7.2 13.6 32300 28600 24000 31700 34800 134000 32800 31900 31200 92.7 54 58.2 54.4 53.9 57.7 53.4 57.5 85.2 1 16200 15700 15500 13900 15200 16200 16100 16100 16400 4.8 4.8 5.6 5.2 113 5.1 221 123 126 102 209 1 .11 • 1 2.6 6.1 43.5 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 13 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 11300 13100 13700 1 250000 pg/L Sulfate 7430 8000 8180 500000 pg/L Total Dissolved Solids 104000 166000 163000 1E 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1,1,1-Trichloroethane 6 pg/L 1,1-Dichloroethane 0.91 1.1 1.3 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone 1600 13800 13000 14500 14200 13300 1060 8310 11200 8400 7910 7020 '000 154000 131000 157000 149000 139000 11.4 15.3 0.811 0.9 NE pg/L Alkalinity, Total as CaCO3 67300 64100 62400 51900 51600 10 pg/L Arsenic 700 pg/L Barium 140 122 111 90.8 98.8 1 pg/L Benzene 0.29 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon disulfide 250000 pg/L Chloride 6050 4340 4300 3600 5160 3000 pg/L Chloroethane 3 pg/L Chloromethane 0.13 10 pg/L Chromium 70 pg/L cis-1 2-Dichloroethene 0.8 0.73 0.73 0.37 0.54 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 1 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 76.5 15 pg/L Lead 500 pg/L m&p-Xylene 0.84 1.5 1.1 50 pg/L Manganese 33.6 27.1 22.9 1 pg/L Mercury 3 pg/L Methylene Chloride 2.1 2.9 500 pg/L o-Xylene 0.27 0.4 0.36 20 pg/L Silver NE pg/L Sodium 15700 16300 16600 1 250000 pg/L Sulfate 10100 1850 1360 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 17.7 14.1 8.8 500000 pg/L Total Dissolved Solids 78000 145000 138000 1� 3 pg/L Trichooroethene 2000 pg/L Trichlorofluoromethane 1.4 0.79 1.2 500 pg/L Xylenes (Total) 1000 pg/L Zinc 6.8 MW-8 6000 pg/L Acetone 15.51 19.4 13000 13.7 116000 0.47 0.841 1.21 1 63500I 51900I 50200 115 95.1 100 5340 3810 1.3 0.721 0.621 0.5 0.96 24.9 17.4 10.2 0.27 14300 13900 13700 2090 24.2 26 18.9 108000 111000 109000 0.25 0.29 1.2 0.79 NE pg/L Alkalinity, Total as CaCO3 23200 20000 22800 21300 19700 22800 19500 10 pg/L Arsenic 2.6 700 pg/L Barium 34.4 30 38 30.7 25.4 28.5 26.9 250000 pg/L Chloride 2040 1960 1350 1800 1510 2070 1860 10 pg/L Chromium 70 pg/L Cyanide 5.1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 20100 27.5 14 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Di-n-octylphthalate 5.6 300 pg/L Iron 48.6 54 136 61.5 60.8 57.8 15 pg/L Lead 50 pg/L Manganese 3.3 3.4 19.9 6.8 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 7940 6940 7810 6160 5580 6120 6980 6250 250000 pg/L Sulfate 1350 1860 2100 500000 pg/L Total Dissolved Solids 79000 61000 64000 50000 61000 51000 58000 52000 1000 pg/L Zinc 7.1 15.2 MW-9 NE pg/L Alkalinity, Total as CaCO3 18300 21700 23400 18900 18300 18400 17200 20100 10 pg/L Arsenic 3.5 700 pg/L Barium 186 182 193 168 170 174 142 142 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 4710 4290 3610 3610 3950 4300 3560 10 pg/L Chromium 70 pg/L Cyanide 4.7 1000 pg/L Dichlorodifluoromethane 0.76 0.28 0.28 300 pg/L Iron 55.9 15 pg/L Lead 50 pg/L Manganese 4 3.5 7.6 20 pg/L Silver NE pg/L Sodium 14500 14500 14600 12400 250000 pg/L Sulfate 1110 2030 2100 500000 pg/L Total Dissolved Solids 142000 134000 141000 107000 2000 pg/L Trichlorofluoromethane 1.1 0.98 0.96 0.47 1000 pg/L Zinc 5.3 MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone 0.69 0.96 NE pg/L 4-Methyl-2-pentanone (MIBK 2.6 5.6 2.2 6000 pg/L Acetone 11.8 NE pg/L Alkalinity, Total as CaCO3 48200 47300 42200 31400 10 pg/L Arsenic 700 pg/L Barium 241 660 262 132 1 pg/L Benzene 0.46 0.44 4 pg/L Beryllium 1.9 2.8 1.4 700 pg/L Carbon disulfide 250000 pg/L Chloride 47400 51800 2220 1820 10 pg/L Chromium 3.5 6.7 70 pg/L cis-1,2-Dichloroethene 0.35 1 pg/L Cobalt 1000 pg/L Copper 6.3 3.8 70 pg/L Cyanide 9.8 40 pg/L Endosulfan 1 0.17 600 pg/L Ethylbenzene 0.4 1 0.73 0.008 pg/L Heptachlor 0 0.004 pg/L Heptachlor epoxide 300 pg/L Iron . � 15 pg/L Lead 11.6 4.1 500 pg/L m&p-Xylene 1.2 1.1 50 pg/L Manganese ;8.5 10.9 1 pg/L Mercury 0.29 0.33 0.51 3 pg/L Methylene Chloride 100 pg/L Nickel 3.9 5.9 500 pg/L o-Xylene 0.43 0.85 0.65 136 :. 6.9 16.6 13500 12900 13100 12600 3200 124000 100000 118000 123000 0.69 0.36 0.49 26700 32100 25500 413000 112 115 101 96.5 1790 2040 1800 84.3 92.8 218 55.1 7.9 5.1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 15 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-11 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-12 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 100 pg/L Di-n-octylphthalate 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride Historical detections by well location 19800 14100 6860 5280 63600 8770 260 120 145 106 18.6 5 8.5 0.63 403000 279000 86000 63000 66000 46000 63000 49000 • 0.2 0.33 0.38 0.49 27.2 21.2 6.2 0.05 127000 132000 143000 175000 161000 189000 153000 120000 97.2 93.7 96.8 94.3 87.8 87 76.8 70.3 1.3 14900 14400 15000 12400 14000 14200 12900 10800 2.8 4.2 Me fit of Wllmfrdflf� ..... 2.9 3.6 1771 5.6 12000 9460 10000 8490 9070 8290 8770 7460 19100 15300 12800 10700 10400 11000 10400 9700 130 4.4 281000 239000 228000 207000 236000 228000 220000 161000 19200 • 92 37200 41000 40500 45500 39300 29600 40200 95.7 60.9 59.2 61.1 47.6 50.1 50.5 46.9 1.2 9000 8070 8240 6180 6230 5820 4900 8200 5.3 0.23 5.6 253 I=WT 6 9.7 • • 14.6 :.r 3 3.6 15.7 2 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 16 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 3.2 4.1 20 pg/L Silver NE pg/L Sodium 13700 11200 12800 11000 10500 11100 11000 11600 250000 pg/L Sulfate 70800 73600 32800 48000 27400 51800 24200 20500 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 234000 163000 135000 149000 126000 138000 127000 130000 2000 pg/L Trichlorofluoromethane 0.82 0.22 0.32 1000 pg/L Zinc 30.8 MW-13 350 pg/L 1,1-Dichloroethene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 37100 36900 36200 46400 43200 58700 43900 52200 10 pg/L Arsenic 2.6 700 pg/L Barium 71.5 89.3 130 77.1 106 176 279 144 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 0.68 0.66 1.2 250000 pg/L Chloride 3270 3760 5870 10 pg/L Chromium 2.9 3 1 pg/L Cobalt 1000 pg/L Copper 3.8 70 pg/L Cyanide 5 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 1120 6 15 pg/L Lead 2.9 5.4 50 pg/L Manganese 41.2 100 pg/L Nickel 20 pg/L Silver 38801 5700 232 34.1 48.8 1.5 2.4 3.5 1.4 3820 6150 5380 7.1 r�yt 8610 11300 3760 NE pg/L Sodium 12200 10700 10700 11200 11700 19100 14600 16700 250000 pg/L Sulfate 10100 9330 8660 8680 9360 7820 9770 9420 NE pg/L Sulfide 151 106 178 NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 110000 107000 119000 113000 114000 87000 144000 110000 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc 8.6 7.9 13.7 17.2 37.3 51 20 MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 51500 45200 42300 37400 32800 35600 28900 30100 10 pg/L Arsenic 700 pg/L Barium 183 179 193 163 140 254 160 122 4 pg/L Beryllium 0.63 0.54 0.6 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 3930 3510 3720 3630 4100 4290 4790 3 pg/L Chloromethane 10 pg/L Chromium 4.5 6.6 6 1000 pg/L Copper 4.8 9.5 5.8 70 pg/L Cyanide 5.3 6 1000 pg/L Dichlorodifluoromethane 2.1 300 pg/L Iron 142 15 pg/L Lead 50 pg/L Manganese . • 25.7 1 40.2 1 1 pg/L Mercury 3 pg/L Methylene Chloride Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 17 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 2.8 2.8 5.3 8.6 13.7 12.5 20 pg/L Silver NE pg/L Sodium 15800 14500 14400 12800 12300 13500 15000 14300 250000 pg/L Sulfate 1080 1790 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 135000 131000 119000 1 2000 pg/L Trichlorofluoromethane 0.54 0.59 0.57 0.3 pg/L Vanadium 1000 pg/L Zinc 6.3 13.3 MW-15 350 pg/L 1, 1 -Dichloroethene 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 103000 91500 54700 10 pg/L Arsenic 4.5 700 pg/L Barium 74 105 41.5 250000 pg/L Chloride 113000 98200 146000 70 pg/L Chloroform 0.44 0.26 10 pg/L Chromium 5.4 7.6 1000 pg/L Copper 7.1 8.8 70 pg/L Cyanide 300 pg/L Iron 233 15 pg/L Lead 6 6.8 50 pg/L Manganese 33 3 pg/L Methylene Chloride 100 pg/L Nickel 3.9 4.3 NE pg/L Sodium 21800 20300 24000 250000 pg/L Sulfate 70000 65400 43800 NE pg/L Sulfide NE pg/L Tetrahydrofuran 19.8 16.9 15.5 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 362000 360000 464000 3 2000 pg/L Trichlorofluoromethane 4.8 4.4 3.9 0.3 pg/L Vanadium : 1000 pg/L Zinc 35.4 49 5.3 SW-1 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 35100 44500 63700 10 pg/L Arsenic 5.9 700 pg/L Barium 65 72.2 276 4 pg/L Beryllium 1.1 2 pg/L Cadmium 0.7 250000 pg/L Chloride 21600 31500 19500 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 3.9 16.4 70 pg/L Cyanide 2 pg/L Endrin 300 pg/L Iron •' 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 8.7 20 pg/L Selenium 7 20 pg/L Silver Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 1230001 1020001 1270001 145000 11.71 1 27.41 23 3.1 0.062 3600 64300 78900 77600 75300 7.1 5.7 8.6 23.8 59.6 143 115 3400 124000 124000 143000 60600 0.49 0.77 0.63 0.49 1.4 6.7 7.2 10.5 IN 160 317 327 t200 25300 26700 21200 16300 a500 53200 41200 35600 25800 100 21.4 14.7 7.4 6.3 3000 410000 442000 298000 260000 5.3 7.6 4.3 8.1 7.3 17.1 .. .. 5.61 51.1 72700I 58000I 79700I 47200 71.1 58.9 63.3 70.4 181001 206001 197001 25300 0.08 18 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 12800 16000 12500 14500 13000 12400 15500 14300 250000 pg/L Sulfate 4460 3690 3130 2820 2190 2700 2090 500000 pg/L Total Dissolved Solids 113000 140000 122000 126000 125000 104000 131000 98000 0.3 pg/L Vanadium 1000 pg/L Zinc 7.5 69.8 SW-2 40 pg/L 2-Hexanone 1.8 NE pg/L 3,3'-Dichlorobenzidine 3.6 NE pg/L 3-Methylcholanthrene 2.9 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 43200 33200 2390 41300 48900 48600 44700 44200 10 pg/L Arsenic 6.2 700 pg/L Barium 70 171 59.7 50.1 51.7 46.5 53.4 0.05 pg/L Benzo(a)anthrace ne 17 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 1.8 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3.7 0.64 3 pg/L bis(2-Ethylhexyl)phthalate 1.1 250000 pg/L Chloride 12500 4050 28200 10700 11600 10800 10300 11300 3 pg/L Chloromethane 10 pg/L Chromium 3.2 5 pg/L Chrysene 1.1 70 pg/L cis-1,2-Dichloroethene ;81.6 1 pg/L Cobalt 1000 pg/L Copper 3.2 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 0 300 pg/L Iron .fly lifs 15 pg/L Lead 7.4 7 50 pg/L Manganese 291 1020 1010 219 152 153 106 157 1 pg/L Mercury 0.2 3 pg/L Methylene Chloride 100 pg/L Nickel 16.4 3.1 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 11300 8390 17600 9840 10300 9160 9990 9890 250000 pg/L Sulfate 11600 7280 5620 12700 5490 5090 4240 6180 NE pg/L Sulfide 142 NE pg/L Tetrahydrofuran 18.4 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 105000 125000 117000 120000 114000 91000 101000 101000 0.3 pg/L Vanadium 1000 pg/L Zinc 249 28 SW-3 40 pg/L 3&4-Methylphenol (m&p Cres 3.6 0.1 pg/L 4,4'-DDD 0.079 0.1 pg/L 4,4'-DDT 0.09 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 210000 118000 389000 259000 516000 293000 317000 221000 160000 700 pg/L Barium 152 105 206 181 348 185 315 179 123 1 pg/L Benzene 0.54 0.32 0.88 0.34 0.25 250000 pg/L Chloride 16300 27000 27000 16900 34800 20000 24300 22800 20900 10 pg/L Chromium 3.4 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 19 of 50 A2 Facility Permit 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-4 350 pg/L 1, 1 -Dichloroethene 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc Old Salisbury Road Landfill (C&D) Historical detections by well location 4.4 0.071 0.085 2.7 2.8 2.8 4.8 12 20900 18200 29900 29900 41100 25000 33800 21300 18500 27000 17000 16800 26300 62500 20100 36400 26400 19800 3.3 10.2 9.7 18.9 5.1 4.8 4.5 300000 233000 473000 319000 8 M 327000 432000 329000 237000 13.6 10.8 0.58 3.1 0.062 0.054 187000 242000 140000 158000 152000 147000 220000 158000 131000 115 187 82.8 126 101 106 151 136 105 19800 19000 24300 30800 31000 26900 28800 30900 23600 0.97 0.066 0.061 •0 4180 1640 2140 1060 0•0 1650 2430 2420 1290 3.6 20200 23800 17800 24400 20100 18200 29000 20000 17900 24900 23500 17600 23500 23000 13200 32300 23600 19500 4.1 4.4 267000 371000 222000 257000 270000 255000 349000 272000 234000 0.27 0.25 1.4 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 20 of 50 A2 Facility Permit MW-1 R NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.05 pg/L Benzo(a)anthracene 3 pg/L bis(2-Ethylhexyl)phthalate 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 600 pg/L Ethylbenzene 300 pg/L Iron 15 pg/L Lead 50.0 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichooroethene 1000 pg/L Zinc MW-2R 6 pg/L 1, 1 -Dichloroethane 350 pg/L 1,1-Dichloroethene 0.4 pg/L 1,2-Dichloroethane 6 pg/L 1,4-Dichlorobenzene 3 pg/L 1,4-Dioxane (p-Dioxane) 50 pg/L 2,4,5-TP (Silvex) 70 pg/L 2,4-D NE pg/L 2,4-Dinitrotoluene NE pg/L 2,6-Dinitrotoluene 4000 pg/L 2-Butanone (MEK) 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 0.002 pg/L Aldrin NE pg/L Alkalinity, Total as CaCO3 0.006 pg/L alpha-BHC 1 pg/L Antimony 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 250000 pg/L Chloride 3000 pg/L Chloroethane 70 pg/L Chloroform 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper Old Salisbury Road Landfill (C&D) Histor 1.2 38.7 3.7 219000 165000 351 62400 39900 0.26 0.46 cal detections by well location 84.7 85.4 85.3 92.8 74.3 85 90.3 1.4 0.96 1.4 2 0.88 0.64 0.49 0.51 0.29 0.48 0.62 0.43 1.1 273 223 103 80.7 88.5 98.8 102 0.36 3.4 5.4 0.49 1.2 1.6 0.5 0.79 0.26 105 Will Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 21 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 70 pg/L Cyanide 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron •'� 15 pg/L Lead 500 pg/L m&p-Xylene 0.6E 0.74 50 pg/L Manganese 1 pg/L Mercury NS pg/L Methane 1280 40 pg/L Methoxychlor 3 pg/L Methylene Chloride mm 6 pg/L Naphthalene 100 pg/L Nickel 20.9 NS pg/L Nitrogen, Ammonia 0.12 500 pg/L o-Xylene 1.2 0.84 20 pg/L Selenium 20 pg/L Silver 5 2.5 0.85 NE pg/L Sodium 31800 27200 250000 pg/L Sulfate 96300 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 197 274 226 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 498000 3 pg/L Trichloroethene 0.88 0.65 0.671 0.681 0.581 1.2 2000 pg/L Trichlorofluoromethane 20.1 31.6 36.11 21.91 22 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone 33.3 NE pg/L Alkalinity, Total as CaCO3 155000 10 pg/L Arsenic 700 pg/L Barium 237 301 302 200 pg/L Benzo(g,h,i)perylene 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver 0.6 NE pg/L Sodium Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND W-S GW Revised.xlsb 1 0.93 4 314 289 252 231 293 273 310 0.82 26.1 3.3 0.63 1I 0.29I 11.81.5 089 18.17 22 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 250000 pg/L Sulfate 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 180000 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 126 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 3 pg/L Chloromethane 0.15 10 pg/L Chromium 1.3 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver 0.88 NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 63.7 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 7.6 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver 0.57 Highlighted cells are at or above the current standard. Blank cells indicate either NS or N W-S GW Revised.xlsb 335 55.9 0.68 1.3 1.3 53 5.8 0.16 D. 334 58.3 263 5.4 1.2 0.58 4.8 2.4 2.6 172 287 200 0.4 <1]LlL1� 54.3 66.8 52.6 56.1 57.5 70.6 58 5 8.6 5.2 5.3 5.6 8.4 6.4 0.61 0.281 0.781 0.561 1 1 23 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1, 1, 1 -Trichloroethane _ 0.82 6 pg/L 1, 1 -Dichloroethane 1.9 3.8 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 47700 10 pg/L Arsenic 700 pg/L Barium 97.1 104 100 1 pg/L Benzene 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon disulfide 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 0.55 70 pg/L cis-1,2-Dichloroethene 0.67 0.71 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 1.4 50 pg/L Manganese 12.7 1 pg/L Mercury 3 pg/L Methylene Chloride 500 pg/L o-Xylene 0.39 20 pg/L Silver 0.84 0.23 NE pg/L Sodium 12000 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 124000 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.34 0.48 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone 3.8 NE pg/L Alkalinity, Total as CaCO3 19600 10 pg/L Arsenic 700 pg/L Barium 24.4 27.3 26.8 250000 pg/L Chloride 10 pg/L Chromium 0.96 0.62 70 pg/L Cyanide Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 3.4 99.3 104 86.9 99 95.7 101 89 12.5 <Il i.i�ml]Llil 0.881 0.421 0.96 1 7.3 1 0.66 8.8 27.2 25 32.8 24 26.6 30 1.4 0.78 0.97 0.42 24 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 151 7 5410 81000 45.4 0.1 17400 10 pg/L Arsenic 700 pg/L Barium 141 153 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver 0.43 NE pg/L Sodium 11900 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 128000 2000 pg/L Trichlorofluoromethane 0.42 0.26 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane(p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MIBK 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 21700 10 pg/L Arsenic 700 pg/L Barium 91.3 80.7 1 pg/L Benzene 4 pg/L Beryllium 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 0.63 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan 1 600 pg/L Ethylbenzene 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 6.8 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene Highlighted cells are at or above the current standard. Blank cells indicate either NS or N W-S GW Revised.xlsb 157 134 38.9 D. 0.27 0.16 0.15 128 173 124 7.6 0.47 0.321 0.181 0.36 0.1 0.13 1 124 1 0.22 0.16 1171 140 0.32 46.6 39.1 38.9 41.9 42 40.8 52 13 0.65 25 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 20 pg/L Selenium 20 pg/L Silver 0.1 NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 89000 2000 pg/L Trichlorofluoromethane 0.68 0.5 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-11 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 122000 700 pg/L Barium 57.5 56. 200 pg/L Benzo(g,h,i)perylene 250000 pg/L Chloride 8480 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron o f f 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver 1. NE pg/L Sodium 6480 250000 pg/L Sulfate 7590 NE pg/L Sulfide NE pg/L Tetrahydrofuran 12. 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 165000 0.3 pg/L Vanadium 1000 pg/L Zinc MW-12 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 40200 10 pg/L Arsenic 700 pg/L Barium 60.1 39. 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 8030 3 pg/L Chloromethane 0.2 10 pg/L Chromium 2. 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 100 pg/L Di-n-octylphthalate 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride 2 0.19 2 2 48.1 37.6 31.8 28.4 28.6 29.2 23.1 25 8.7 2 0.48 0.5 0.79 0.41 0.39 1 2.7 1 44.9 40.6 38 34.5 57.9 60.5 47.3 31 1 6 1.1 2.4 2 1.8 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 26 of 50 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 26 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 20 pg/L Silver 0.7 NE pg/L Sodium 9980 250000 pg/L Sulfate 15300 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 124000 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-13 350 pg/L 1,1-Dichloroethene _ 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 44500 10 pg/L Arsenic 700 pg/L Barium 139 164 176 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 2.3 250000 pg/L Chloride 10 pg/L Chromium 5.5 3.9 4 1 pg/L Cobalt 1000 pg/L Copper 6.1 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 6 15 pg/L Lead 6.4 4.3 50 pg/L Manganese 100 pg/L Nickel 20 pg/L Silver 0.72 NE pg/L Sodium 20200 250000 pg/L Sulfate 9460 NE pg/L Sulfide NE pg/L Tetrahydrofuran 18.6 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 159000 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc 31.6 MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 30400 10 pg/L Arsenic 700 pg/L Barium 143 125 129 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 0.24 10 pg/L Chromium 1.8 2.3 1000 pg/L Copper 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 0.21 0.39 19.8 0.371 0.15 1261 1171 79.21 88.71 64.6 Ism, Imix, II mix, CINOVAI 18.6 7.3 130 242 97.9 583 186 3 � 0.4 � 4.1 7.2 0.26 130 210 1.7 6.6 5.2 0.098 27 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 20 pg/L Silver 0.74 0.39 0.54 0.46 0.56 0.48 NE pg/L Sodium 12700 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 138000 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc 12 MW-15 350 pg/L 1, 1 -Dichloroethene 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc SW-1 6000 pg/L Acetone 22.7 2.2 NE pg/L Alkalinity, Total as CaCO3 19600 10 pg/L Arsenic 3.7 700 pg/L Barium 42.5 69.9 61.9 92.5 77.7 45.6 78.2 79.7 70.3 88 4 pg/L Beryllium 2 pg/L Cadmium 250000 pg/L Chloride 19100 10 pg/L Chromium 0.61 0.67 1.2 0.61 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 2 pg/L Endrin 300 pg/L Iron •� 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver 0.4 0.28 0.62 0.39 0.37 0.51 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 28 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 9390 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 140000 0.3 pg/L Vanadium 1000 pg/L Zinc SW-2 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone 4 NE pg/L Alkalinity, Total as CaCO3 26100 10 pg/L Arsenic 700 pg/L Barium 81 49.2 57.6 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 10900 3 pg/L Chloromethane 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 1 15 pg/L Lead 50 pg/L Manganese .1 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver 0.2 NE pg/L Sodium 8650 250000 pg/L Sulfate 38300 NE pg/L Sulfide NE pg/L Tetrahydrofuran 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 189000 0.3 pg/L Vanadium 1000 pg/L Zinc 13.5 SW-3 40 pg/L 3&4-Methylphenol(m&p Cres 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 1 pg/L Benzene 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 59.4 52.11 46.31 50.6 0.42 1 50.6 5.5 49.4 300 11 0.08 0.2 0.36 0.5 0.26 0.26 29 of 50 A2 Facility Permit 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-4 350 pg/L 1,1-Dichloroethene 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 30 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) MW-1 R NE pg/L Alkali 10 pg/L Arse 700 pg/L Bariu 0.05 pg/L Benz 3 pg/L bis(2- 700 pg/L Carb o 250000 pg/L Chlor 10 pg/L Chro 5 pg/L Chry 70 pg/L cis-1, 70 pg/L Cyani 600 pg/L Ethyl 300 pg/L Iron 15 pg/L Lead 50.0 pg/L Mang 1 pg/L Merc 3 pg/L Meth 20 pg/L Sele 20 pg/L Silve NE pg/L Sodi u 250000 pg/L Sulfa 600 pg/L Tolu e 500000 pg/L Total 3 pg/L Trichl 1000 pg/L Zinc MW-2 6 pg/L 1,1-D 350 pg/L 1,1-D 0.4 pg/L 1,2-D 6 pg/L 1,4-D 3 pg/L 1,4-D 50 pg/L 2,4,5 70 pg/L 2,4-D NE pg/L 2,4-D NE pg/L 2,6-D 4000 pg/L 2-But 40 pg/L 2-He 0.1 pg/L 4,4'- 6000 pg/L Acet o 0.002 pg/L Aldrin NE pg/L Alkali 0.006 pg/L alpha 1 pg/L Anti m 10 pg/L Arse 700 pg/L Bariu 1 pg/L Benz 3 pg/L bis(2- 2 pg/L Cad 250000 pg/L Chlor 3000 pg/L Chlor 70 pg/L Chlor 3 pg/L Chlor 10 pg/L Chro 70 pg/L cis-1, 1 pg/L Coba 1000 pg/L Copp Historical detections by well location nity, Total as CaCO3 nic 5.8 m 94 82 78 48 95 96.3 460 120 100 130 280 87 150 o(a)anthracene Ethyl hexyl)phthalate n disulfide ide mium 2 3.5 4.3 2.3 5 6.6 6.6 sene 2-Dichloroethene de benzene 10 anese ury ylene Chloride nium 5.5 r m to ne 21 Dissolved Solids oroethene R ichloroethane ichloroethene ichloroethane ichlorobenzene ioxane (p-Dioxane) TP (Silvex) initrotoluene initrotoluene anone (MEK) 2-Hex DDT ne nity, Total as CaCO3 -BHC ony nic m 90 52 62 43 52 55 60 56 140 100 160 280 61 ene Ethyl hexyl)phthalate mium 1.9 ide oethane oform omethane mium 2.2 2.1 3.9 2-Dichloroethene It er Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 31 of 50 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 31 of 50 A2 Facility Permit 70 pg/L Cyanide 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 6 pg/L Naphthalene 100 pg/L Nickel NS pg/L Nitrogen, Ammonia 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium Old Salisbury Road Landfill (C&D) Historical detections by well location 0.34 230 290 300 300 340 2.3 71 8.9 7.4 8.4 t70 200 220 13 370 400 3.7 2.3 14 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 32 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 250000 pg/L Sulfate 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 220 220 180 150 14C 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 5.1 700 pg/L Barium 58 57 54 53 8C 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 6.2 6.2 3.5 5.6 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 0.4 3 pg/L Methylene Chloride 20 pg/L Silver Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 9.2 W 97 94 86 61 2.6 5.5 5 IN 5.3 6 5.6 550 350 141 8.1 5 7 5 76 65 72 65 150 610 270 400 7.3 8.7 9.5 7.4 5.1 13 7.6 7.6 33 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1, 1, 1 -Trichloroethane 6 pg/L 1, 1 -Dichloroethane 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 76 74 60 53 6 1 pg/L Benzene 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon disulfide 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 4.4 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 0.24 3 pg/L Methylene Chloride 500 pg/L o-Xylene 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 29 29 26 25 3C 250000 pg/L Chloride 10 pg/L Chromium 2.4 70 pg/L Cyanide Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 28 25I 24I 41 86 530 2.2 2.4 3.2 M®MME 5.3 52 77 3.2 3.8 1 6 6.8 2.6 3 621 41 4.1 2.6 34 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 6.7 50 pg/L Manganese 1 pg/L Mercury 0.26 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 140 100 100 85 95 240 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 14 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MIBK 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 71 48 46 82 5E 1 pg/L Benzene 4 pg/L Beryllium 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan 1 600 pg/L Ethylbenzene 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 0.2 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. 98 6.8 W-S GW Revised.xlsb 35 of 50 A2 Facility Permit 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-11 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-12 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 100 pg/L Di-n-octylphthalate 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride Old Salisbury Road Landfill (C&D) Historical detections 6.2 by well to 24 26 27 24 28 47 3.9 3.3 66 55 77 50 77 74 4 2.1 cation Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 36 of 50 A2 Facility Permit 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-13 350 pg/L 1,1-Dichloroethene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride Old Salisbury Road Landfill (C&D) -listorical detections by well to 65 59 46 57 160 2 4.8 9.2 11 250 120 69 66 170 3.9 3.2 13 5.9 8 0.44 cation Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 37 of 50 A2 Facility Permit 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-15 350 pg/L 1, 1 -Dichloroethene 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc SW-1 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 2 pg/L Cadmium 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 2 pg/L Endrin 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver Old Salisbury Road Landfill (C&D) t0 O O Z co O Q Q � O O Z � O j O O Z O 7� Q O @ M O O Z • 1.1 23 750 20 •• 36 52 57 38 ation Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 38 of 50 A2 Facility Permit NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-2 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-3 40 pg/L 3&4-Methylphenol(m&p Ci 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 1 pg/L Benzene 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 44 Old Salisbury Road Landfill (C&D) Historical detections by well location 1 150 5WA 7.6 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 39 of 50 A2 Facility Permit 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-4 350 pg/L 1,1-Dichloroethene 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 40 of 50 A2 Facility Permit MW-1 R NE pg/L Alkalinity, T 10 pg/L Arsenic 700 pg/L Barium 0.05 pg/L Benzo(a)an 3 pg/L bis(2-Ethyl 700 pg/L Carbon dis 250000 pg/L Chloride 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dic 70 pg/L Cyanide 600 pg/L Ethylbenze 300 pg/L Iron 15 pg/L Lead 50.0 pg/L Manganes 1 pg/L Mercury 3 pg/L Methylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 600 pg/L Toluene 500000 pg/L Total Disso 3 pg/L Trichloroet 1000 pg/L Zinc MW-2R 6 pg/L 1,1-Dichlor 350 pg/L 1,1-Dichlor 0.4 pg/L 1,2-Dichlor 6 pg/L 1,4-Dichlor 3 pg/L 1,4-Dioxan 50 pg/L 2,4,5-TP (S 70 pg/L 2,4-D NE pg/L 2,4-Dinitrot NE pg/L 2,6-Dinitrot 4000 pg/L 2-Butanon 40 pg/L 2-Hexanon 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 0.002 pg/L Aldrin NE pg/L Alkalinity, T 0.006 pg/L alpha-BHC 1 pg/L Antimony 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 3 pg/L bis(2-Ethyl 2 pg/L Cadmium 250000 pg/L Chloride 3000 pg/L Chloroetha 70 pg/L Chloroform 3 pg/L Chlorometh 10 pg/L Chromium 70 pg/L cis-1,2-Dic 1 pg/L Cobalt 1000 pg/L Copper Old Salisbury Road Landfill (C&D) hexyl)phthalate ulfide hloroethene e hene e e hexyl)phthalate hloroethene Historical detections by well location otal as CaCO3 110 130 150 160 100 290 100 180 224 thracene 28 23 5.2 7.8 3 6 ne 12 6 0.2 Chloride Ived Solids oethane oethene oethane obenzene (p-Dioxane) ilvex) oluene oluene (MEK) e 86 otal as CaCO3 180 120 150 190 340 200 160 350 �1 ne ane 3 � 7.8 17 4 9 7 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 41 of 50 A2 Facility Permit 70 pg/L Cyanide 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 6 pg/L Naphthalene 100 pg/L Nickel NS pg/L Nitrogen, Ammonia 500 pg/L o-Xylene 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-3R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 3 pg/L bis(2- Ethyl hexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium Old Salisbury Road Landfill (C&D) Historical detections by well location 6.5 6.9 .: 14 8 0.4 5.9 6 300 52 620 ffS III :.1 :�� •� l 9 0.2 1 1 0.7 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 42 of 50 A2 Facility Permit 250000 pg/L Sulfate 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 3 pg/L bis(2- Ethyl hexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver Highlighted cells are at or above the current standard. Blank cells Old Salisbury Road Landfill (C&D) Historical detections by well location 7.5 570 :.�Mjn gang a 9.5 0.36 200 200 240 8.1 8.2 ndicate either NS or NE 0.21 6501 280 6 0.3 150 5 480 � 610 330 620 25 14 595 0.8 W-S GW Revised.xlsb 43 of 50 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 82 59 10 pg/L Chromium 2.8 15 pg/L Lead 5.8 1 pg/L Mercury MW-7 200 pg/L 1,1,1-Trichloroethane 6 pg/L 1,1-Dichloroethane 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 9.8 700 pg/L Barium 360 390 MM 1 pg/L Benzene 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon disulfide 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 2.5 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 8.7 12 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 500 pg/L o-Xylene 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. 1601 3601 2601 3001 590 9 Iu' �m NN EE '''' W-S GW Revised.xlsb 44 of 50 A2 Facility Permit 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 3 pg/L bis(2- Ethyl hexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MIBk 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 4 pg/L Beryllium 700 pg/L Carbon disulfide 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan I 600 pg/L Ethylbenzene 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 45 of 50 A2 Facility Permit 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-11 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-12 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 100 pg/L Di-n-octylphthalate 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 46 of 50 A2 Facility Permit 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-13 350 pg/L 1,1-Dichloroethene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2- Ethyl hexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 47 of 50 A2 Facility Permit 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-15 350 pg/L 1,1-Dichloroethene 70 pg/L 2,4-D 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc SW-1 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 2 pg/L Cadmium 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 2 pg/L Endrin 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 48 of 50 A2 Facility Permit NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-2 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine NE pg/L 3-Methylcholanthrene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 3 pg/L bis(2- Ethyl hexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyre ne 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-3 40 pg/L 3&4-Methylphenol(m&p Cr 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 1 pg/L Benzene 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 49 of 50 A2 Facility Permit 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc SW-4 350 pg/L 1,1-Dichloroethene 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 700 pg/L Barium 250000 pg/L Chloride 70 pg/L Chloroform 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb 50 of 50 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units rrrr pg/L NE pg/L 00000TotalDissolved NE pg/L Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance deg C Field Temperature EPA 300.0 Sulfate TotalEPA 8151 Alkalinity, - •3 . . • - SM 11 SM 1 Sulfide Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance deg C 357000 rI �- ..1r _- 1111■OF . �� �� �� . ��� . ��� 111 EFFA 11 :••11111♦- err 726000 -Ew,rr 1370000 r0I 1 1 ONO 11 1111■IIIIL.....IILnn... : 1 1 11 111......111'+'��•' : 111 111♦®"' --11111,11111,11111,11111,11111,11111,11111,11111.11111,----_- ---------------_- 1/18/2019 1 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 11 . 1 600 pg/L 1000 rr pg/L 0 100 pg/L 0.3 pg/L 1000 rrrr rr pg/L ■ rNE pg/L Concentration Column Label MW-1R MW-2R MW-3R MW-4R MW-5R MEMO=y MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field Temperature EPA 8260B Chloride o-Xylene--1111■1111■1111■1111■111�1111■1111■111�1111■1111■1111■1111■1111■111♦- .. - - . Vinyl acetate EPA 8260B Mod. EPA 6010D Cobalt88 ... Iron SodiumNE Vanadium EPA 7470A May-1 8 EPA 300.0 EPA 6010 Cobalt_ Iron Sodiumr� 1.7 -----------_- ------ 5.7 --------_- 0.88 -------------_- --------------_- -� 15.9 11.3 35 ----- -----------_- 22 2090 5030 28200 371 653 8920 7940 -�,�,©-----®-®-�-_� 584 24700 1620 336 170 115 . �� . '11111,•••. .�� '.11 I 111 .I .INI 1.1■ :.1I . 11111♦- 4.8 ®--®--------®�_- Job mom r�■ r �r ®: ■ - r� ®".r - 307000 �r .- r� �- .■r - 20.5 11 10.4 ----- 18 -----_- 4260 84300 3980 3300 27300 ®®i. 453 _- 10300 8100 357 17500 1580 95.5 507 _- �r ®" ■ :■r :r� - ..r� ®r rr err r�r rr .•rr r �� _- 1/18/2019 2 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 0.3 pg/L 1000 pg/L 1 pg/L 6 pg/L 6 pg/L 40 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L Row Labels Vanadium Zinc EPA 7470 pg/L Mercury EPA 8260 pg/L 1,1-Dichloroethane 1,4-Dichlorobenzene 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide SM 4500-S2D pg/L Sulfide Field feet Static Water Level Total Well Depth mg/I Oxygen, Dissolved 9 5 19.9 6.6 0.34 0.39 1.1 0.41 0.72 1.7 16.4 0.41 0.55 0.45 0.71 0.55 0.85 0.23 1.2 3 1.7 0.68 1.7 2.4 0.65 0.78 46 24.9 192 5.9 14.8 0.93 1.2 1.3 0.89 0.79 0.42 76100 663000 115000 101000 33600 75900 27000 31800 506000 130000 65800 47200 61800 112000 166000 � 177000 250000 164000 181000 75000 133000 MIOe 232000 218000 107000 152000 369000 9040 42200 2180 12500 15200 6490 3660 4830 158000 12500 11100 4790 3930 89700 5 4.8 4.4 4.8 4.2 105 240 71.02 15.65 38.14 16.68 21.98 74.1 31.8 106.92 23.28 7.57 9.22 16.97 104.4 78.28 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1.09 0.71 1.1 0.21 5.49 1.2 5.49 6.55 0.13 1.53 0.36 4.06 5.48 2.01 1/18/2019 3 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 1 . .111 ./L pg/L 1 •/L 11 • 1 • 111 • 0.03 ./L Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 6020B EPA 8260 Acetone Carbon disulfide Chloroform--------------�_- • - • • _ _ • • • • - Vinyl chloride Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature 300.0 ME M, mmnmm���� --- 1 1 -----------_- ---------®-----_- 2.5700 -----------_- ------®--®-----_- 1.5 -------------_- 1.4EPA -------------_- Mrs M... -----_- 1/18/2019 4 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 1111 . 1 . 1 .Chromium®-® 11 ./L 1 . NE pg/L 1.3 pg1L 1 . 1 . 1 . .111 ./L 1 ./L 1 . 0.03 ./L NE pg/L Concentration •-Sulfate Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 .n 11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank EPA 6010 Cobalt23.5 Iron Sodium11 Vanadium EPA 7470 EPA 8151 ■ . .. - . EPA 8260 Acetone Chloroform--------------�_- Chloride .. - - - Vinyl chloride 8270 Alkalinity, 011 Total 111 - 'lll �- 'e, llllllllllll --------------_- 10.2 --®�--�--_® 9.4 93 30101 787001 365 ----- 22.5-----_- 3270 29300 ®�� 1050 _- 106001 54401 1050 13800 1590 169 317 .11 . 11 11 - 11 ••11 :111 11 11 11 •:11 _� 4.9 --------- 3.6 _- 1 1 -------------_- --------------�_- ---------------_ 1 1 ---------®-----_- 2.6 -----------_- ------ 4.6 --------_- 1.8 -------------_- 1.4EPA . 1111 :•11. 111 11 - :111 : 11 •11 1111 1111 :11 �.11 . 11 1111 _- 1/18/2019 5 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 11111 . 250000 ./L NE pg/L 1111 . 700 . 1 ./L 11 •/L 1 • 11 . NE pg/L 1 . 1 •/L 111 • 0.4 •/L NE pg/L .111 •/L 11 •/L 1 • 600 •/L 11 • Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank , "tal Dissolved . . Chloride. Sulfide Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 - EPA 6010 ChromiumCobalt Iron • • Vanadium EPA 8260 1,2-Dichloroethane • - • _ Acetone Carbon disulfide • • - - ■ • • _ _ _ Ethylbenzene--1111■1111■1111■1111■1111■1111■1111■®1111■1111■1111■1111■1111■111♦- • - 111 918000 .'111 862000 " 111 - 111 111 .111 1430000 :111 •111 •1111 111 1111 _- 11 IIL.n... .. 11 . 11 1111■11�111�" 1' 1 11� . 1 11 111 1 = 11 11�111...�... : • : 11 111♦- OF NEF M., 1111 - 111 ----- 333000 11 ----_- -®1111■®1111■1111■1111■1111■1111■®IIIIm1111■1111■1111■1111■111♦- 20.6 3870 - - 59.9 302 ----- ----- 21.8 2400 -----_- 26700 ----_- -�1111■1111�' 9200 - 801 ---- 1111■1111■1111■1111■1111■1111®' 8390 1720 1111■1111■1111■1111■1111■111♦- ----_- ' 11 1111■ 11 1111■1111■1111■1111■1111■ 111 11 1111■1111■1111■1111■111♦- --1111■1111■1111■1111■1111■1111■1111■ 1 1 1111■1111■1111■1111■1111■111♦- --1111■111®"' 1111■1111■1111■1111■1111■®1111■1111■1111■1111■1111■111♦- 2.7 -----_- -�1111■1111■1111■1111■1111■1111■1111■11111.1111■1111■1111■1111■1111■111♦- --1111■1111■1111■1111■1111■1111■1111■®1111■1111■1111■1111■1111■111♦- -®1111■IIIIm1111■1111■1111■1111■1111■®®1111■1111■1111■1111■111♦- 2.1 -------------_- --1111■1111■1111■1111■1111■1111■1111■©1111■1111■1111■1111■1111■111♦- --1111■1111■1111■1111■1111■1111■1111■11111.®1111■1111■1111■1111■111♦- --1111■1111■1111■1111■1111■1111■1111■®1111■1111■1111■1111■1111■111♦- 1/18/2019 6 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 500 600 pg/L ■rrrr pg/L 0000• 300 ■ 100 NE pg/L ■ 2000 0.3 pg/L Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 -----_- MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank . • TotalNE Alkalinity, • Total Dissolved • • • Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature May-1 7 EPA 300.0 EPA 6010 Cobalt •n • Sodium Vanadium EPA 8260 ------ ------ -----_- r�■- r�■----- ".err r�■----_- 796000 - 552000 ----- 1150000 11r - :■r ----- 318000 71r ----_- �������ww�����■��� -- 11.5 ------------_- --®------------_ 89300 --®---- 714 1740 _® 18.2 ®- -----------®--®_- 6460 --- 51.9 134 359 ----------- r r r r r• ---------------_� 4.4 --------- 5 _- 1/18/2019 7 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 1 ./L 1 . 11 . 1 . pg/L 11111 . 1 . 1111 . 11 ./L 1 . 1 . Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-51R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Chloroform------- . . - - ------® o-Xylene--------------_- • . - - - Alkalinity, • TotalNE , Total• -• Solids. CyanideField feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 EPA 6010 Cobalt Iron ------�_- -------_- -------------�-_- .:.11 - '111 - 11 - 111 1:1111 -- .' 11 11 11MET 11 _- 111 - 111 - .111 - 111 . 111 111 -- ::111 :•111 1111 1111 _- --®-®--®-----®-_- ®:1 111 111 ®:' 1 - :111.1 ®" 1 555000 11 •111 ®'1 'II 11 16.5 1780 9.8 86400 100 ----- 39.5 2430 -----_- 32400 343 ® 781 _- ® 8570 5920 1320 12300 1670 148 259 _- --©------------_- 1/18/2019 8 of 34 A3 Facility Permit 34-12 Qualifier (Multiple items Old Salisbury Road Landfill (C&D) Historical detections by date 2L Units NE pg/L 0.3 pg/L 1000 pg/L 0.008 pg/L 0.004 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 700 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L Concentration Row Labels Column Labels 15700 184000 12000 19200 9380 16200 20200 Sodium Vanadium Zinc EPA 8081 pg/L Heptachlor Heptachlor epoxide EPA 8260 pg/L 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Carbon disulfide Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C NgIL Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide 14600 70200 2450 71000 14200 16200 9700 5.7 8.4 7.3 5.7 5.1 12.8 6.3 0.53 1.5 0.39 2.5 14.1 0.38 0.42 0.83 5.2 0.44 0.2 0.47 1.1 0.33 0.62 0.88 2.3 0.38 0.55 2.2 2.1 0.63 2.1 0.48 39.1 13.6 21.7 237 26.8 16.8 1.2 1.5 1 2.8 0.58 4.4 64300 571000 133000 454000 32700 80100 25800 23300 626000 107000 72900 42300 59700 101000 154000 ��� 168000 ��� 145000 153000 67000 135000 I811 189000 286000 79000 118000 371000 9630 47600 2050 58400 16400 4820 2670 4360 202000 14500 23300 4100 3410 98000 5.4 1/18/2019 9 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units rrrr 1 • 1000 pg/L rr pg/L r Concentration Row Labels Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 8260 Chloride feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature May-1 6 EPA 300.0 AntimonyEPA 6010 Cobalt Copper----------�--_- Iron • ------ 3.7Field --------_- r:� r�� :r� �r-��- :rr �r .•err �- �� _- 4.7 -------------_- 18 10.2 10.5 ----- 3.1 --------- ® -®-®------®�®-_- 4360 10900 77200 6800 1550 515 11800 19.1 530 29400 --�--_- 1820 312 90.8 11000 284 312 ®_- 116 _- 1/18/2019 10 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 21 Units NE • 1.3 pg/L 1 •/L 1 • 11 • 11 . 1 . 0.03 ./L pg/L 11111 . 1111 ./L 1 . Concentration •Sodium Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MEMO=9 MW-6R MW-7 MW-8 MW-9 11on MW-10 1 11 MW-11 11 MW-12 11 MW-13 � MW-14 '11 MW-15 Trip Blank Equipment Blank Vanadium EPA 7470 EPA 8081 EPA 8260 Chloroform--------------�_- ■ • • - - • - Chloride o-Xylene--------------_- • . - - - Vinyl chloride TotalNE Alkalinity, • , TotalDissolved . • SM 1 Chloride SM 1 CyanideField feet Static Water Level Field feet Static Water Level Total Well Depth Oxygen, Dissolved 11 . 11 � 11 MEIN 11 - .'11111111111111®' '1 4.2 4.2 ---- 20 -- 22.6 --_- 1.7 ------------_- --------------_- ------®--------_- 4.4 3.4 3.2 - 9.5 6 1.3 -------------_- 0.72 -------------_- '•11 111 :11 ••111 1:11 - 11:11 11 •111 1'111 •11 111 1'11 1'111 _- :111 769000 ::111 111 '111 - 111 111 1 111 111 .111 111 111 111 :111 _- ---------------_- 11 _- ---------------_- -®��---®-®®----_- --®1 ------------_- 1/18/2019 11 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 0000 rr ■ 100 r 2000 f.3 pg/L 6000 600 0 Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 EPA 6010 Cobalt on Vanadium EPA 7470 EPA 8081 EPA 8260 . . r ■ r�■ r■ r ■r �- rr �� .rr �r �:rr r �■ r:r rr�■ _- ---------®--®r 17.4 9.1 28.3 2.5 ---- 3.1 2.9 ----_- 3080 9010 68200 312 7100 407 ®-----®-®-� 32600 1890 -- -�®� 3690 587 34600 2020 523 790 62.1 466 69.3 t297 ---------- --------------_- 8.8 11.9 9.9 - 3.7 ---- 5.6 3.5 - 2.6 - 18.9 --------------_- 1.5 -------------_- --------------_- 1/18/2019 12 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L NE pg/L 200 pg/L 0.005 pg/L 100 pg/L 0.05 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L Row Labels 1.2 2 Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 pg/L 2,4-Dinitrotoluene 2,6-Dinitrotoluene Benzo(g,h,i)perylene Dibenz(a,h)anthracene Di-n-octylphthalate Indeno(1,2,3-cd)pyrene SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide Field feet Static Water Level Total Well Depth mg/I Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance 'C Field Temperature May-15 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Barium Beryllium Chromium Cobalt 1.3 2.3 0.27 0.43 7!7 35.8 7 17.7 120 0.27 0.66 1 1.4 1.1 0.82 0.54 4.8 5.9 8.1 1 5.6 5.6 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000 41000 37100 51500 103000 78000 .LIII 137000 161000 104000 78000 79000 142000 403000 281000 234000 110000 135000 362000 8510 48700 2990 16900 16200 6050 2040 4710 47400 14900 9000 3270 3930 113000 7.5 5.1 4.7 9.8 4.2 5.3 5 5.3 72.25 16.3 43.76 20.31 23.2 76.9 36.73 107.71 24.15 7.17 9.51 17.47 104.89 78.88 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 2.2 2 0.2 3.3 5.9 0.7 4.4 6.3 0.2 0.1 3.4 1.2 4.8 2.8 1 5.6 3 9.6 1 1 1.6 2.6 295 9.3 8.9 51.6 5.9 154.9 5.4 6.1 6.3 5.8 5.8 5.5 5.4 5.3 5.4 5.9 5.8 5.5 5.4 6.2 34.8 -35.2 -91.6 48.8 52.6 30.9 4 54.3 -77.7 -38.7 -23.3 5.2 49.6 34.8 163.2 1044 211.4 395.9 164.5 1966. 58.4 151.5 365.1 400.8 281.5 108.9 152.1 596.2 16 15.9 15.2 15.5 15.9 15.3 15.6 15.9 16.5 15.8 16.2 16.2 16.3 15.6 1700 98400 3000 72700 8000 1850 1860 2030 8770 15300 73600 9330 1790 65400 164 287 214 306 54 122 30 182 660 93.7 60.9 89.3 179 105 2.8 0.66 0.54 4.8 6.7 i i 2.9 7.6 1/18/2019 13 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units Concentration Column Label MW-1R MW-2R MW-3R MW-4R MW-5R NONE=w MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 Trip MW-12 MW-13 MW-14 MW-15 Blank Equipment Blank 11 ./L 1 . NE pg1L 1 . 1.3 pg/L 1 . 600 ./L 3 pg/L 1 . 0.03 ./L NE pg/L 11111 . 1111 . Iron Sodium Vanadium EPA 7470 EPA 8151 EPA 8260 Ethylbenzene--------------_- Methylene Chloride • • _ _ _ Vinyl chloride Alkalinity, Total as CaCO3•.11 , TotalDissolved . . • •-_- 365500 31400 5241 14001 6951 10600 9560 56000�®--�- - 11900 7980 315 736 1990 271 - 11 - . 11 11 11 11off1 11 off11 1 11 _- 5.1 -------------_- 11.4 8.8 - 4.3 ---- 4.9 3.2 - 3.4 - 24.7 _- -------------_- 1.7 ----®--®-----_- 1.2 -------------_- 0.7 -------------_- :111 1 111 111 :.11 - .� 11 1111 :•11 11 111 11 .•11 11 11 _- 111 632000 111 1111 ..111 - 111 . 111 •111 •111 •111 . 111 1 111 111 .1111 _- 1/18/2019 14 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 1111 . 1 ./L 11 •/L 1 • 100 . NE pg/L 1.3 pg/L 11 • 11 . 1 . Concentration Row Labels Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 EPA 6010 ChromiumCobalt Iron Sodium Vanadium EPA 7470 EPA 8260 • - Chloride o-Xylene-----------_- • . - - - 25 13.3 82 ----- 2.6 ----_- 2580 49700 529 1160 35700 758 2720 2620 -®-®-------®-®-_- 9880 9380 1040 130 2030 199 55.6 120 1 11 11111 _- 2.8 2.7 5.6 ----- 3.6 - 7.1 5.5 -_- 2.5 -----------_- 3.7 ----®--------_- 2 -------------_- 1/18/2019 15 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 250000 pg/L 1 pg/L 10 pg/L 700 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L 20 pg/L NE pg/L 1000 pg/L Row Labels 106 15.5 Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 23208 pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide SM 4500-S21) pg/L Sulfide Field feet Static Water Level Total Well Depth mg/I Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance °C Field Temperature May-14 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Antimony Arsenic Barium Chromium Cobalt Iron Manganese Nickel Selenium Sodium Zinc 79.2 15.9 8.8 0.85 2.4 1.2 0.96 0.57 3.9 37600 453000 177000 286000 24000 62400 22800 18300 42200 143000 405001 36200 42300 54700 120000 §ffLVA 191000 ILVZIIsl 163000 138000 64000 141000 86000 228000 135000 119000 119000 464000 7090 49800 2940 50500 15500 4300 1350 3610 2220 15000 8240 5870 3720 146000 4.4 4.2 10.4 4.3 5.1 260 130 151 69.7 17.18 21.87 18.4 22.36 36.9 37.58 104.74 24.68 5.4 10.76 18.48 103.8 79 60 21 271 20 30 48 27 60 21 20 15.58 20 60 50.85 1 0.5 6.3 0.5 5 0.5 2.3 8.3 0.5 0.5 0.5 3.8 1.25 1.7 3.53 5.2 10 3.6 1.2 9.1 2 98 9.9 5.2 152 7.8 20.1 5.6 6.1 6 5.9 6 5.6 5.7 5.5 5.1 5.9 5.9 5.6 5.6 6.2 194 38 13 158 198 184 224 252 198 -61 101 232 242 182 138 1150 363 971 184 186 59 161 106 440 203 120 159 647 14.8 13.2 13.2 13.7 12.9 13.7 13 12.4 15.31 15.41 15.4 13.8 11.9 16.7 136000 4230 85200 8060 10700 48000 8680 59500 8.9 124 324 205 264 54.4 90.8 30.7 168 1321 94.3 61.1 77.1 163 8.6 20.6 5.6 52.9 123 6.1 15.5 10.9 •84 14.61 232 34.1 142 40.2 292 34.7 16.5 11.5 10800 59700 39700 13600 14200 6160 12400 8490 11000 11200 12800 24200 11.4 17.2 11.7 1/18/2019 16 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 1 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 700 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L Row Labels EPA 7470 pg/L Mercury EPA 8260 pg/L 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C pg/L Total Dissolved Solids SM 4500-CI-E pg/L Chloride Field feet Static Water Level Total Well Depth mg/I Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance .0 Field Temperature November-13 EPA 300.0 pg/L Sulfate EPA 6010 pg/L Barium Cobalt Iron Manganese Nickel Sodium Vanadium Zinc 0.51 1 0.831 0.81 0.28 0.49 0.38 0.37 0.31 1.1 72.6 11.8 5.2 18.6 21.4 0.71 3.7 0.62 0.47 0.2 0.32 0.34 5.3 30000 344000 155000 222000 31900 51900 21300 18300 31400 175000 45500 46400 37400 96600 91000 � 187000 445000 167000 126000 50000 107000 63000 207000 149000 113000 124000 373000 5600 50500 3260 29700 13900 3600 1800 3610 1820 12400 6180 3880 3630 83400 70.78 14.24 37.86 14.47 20.22 74.12 26.82 52.72 11.34 8.55 9.77 17.91 103.61 76.95 60 21 27 20 30 37.05 27 60 21 20 15.58 20 60 50.85 5.3 4.8 6.3 6.2 8.6 3.8 8.4 8.7 8.3 7.5 8.4 6.8 8.1 5.4 3 11 6 17 10 6 8 51 4 22 15 147 118 50 5.6 5.8 6 5.7 5.7 5.3 5 5.2 5 6 5.9 5.6 5.5 6.3 411 243 146 374 389 363 389 436 436 27 315 367 437 406 137 1040 367 715 194 171 64 155 86 430 243 149 156 623 18.4 19.6 18.7 14.8 14.7 17.2 16 17.7 15 14.4 15 16.6 17.7 17.8 128000 3400 113000 8310 10400 27400 9360 53200 106 311 201 296 53.9 98.8 25.4 170 112 87.8 47.6 106 140 23.8 f 8 89.51 136 136 84.3 253 1 239 . 1 27.1 • • 5.3 19.4 6.8 6.9 7.9 48.8 1 14 9940 46200 42600 13800 13000 5580 13500 9070 10500 11700 12300 25300 12.2 17.1 1/18/2019 17 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 50 pg/L 70 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L Row Labels EPA 8151 pg/L 2,4,5-TP (Silvex) 2,4-D EPA 8260 pg/L 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B pg/L Alkalinity, Total as CaCO3 SM 2540C NgIL Total Dissolved Solids SM 4500-CI-E pg/L Chloride SM 4500-CN-E pg/L Cyanide Field feet Static Water Level Total Well Depth mg/I Oxygen, Dissolved NTU Turbidity Std. Units Field pH mV REDOX pmhos/cm Field Specific Conductance 'C Field Temperature 0.23 1.1 1 1.31 0.9 0.27 0.77 0.41 0.54 0.28 0.86 0.54 99.6 11.7 13.7 5 14.7 0.89 12 0.47 0.69 0.33 7.6 28100 349000 155000 224000 31700 51600 19700 18400 26700 161000 39300 43200 32800 64300 103000 ��� 193000 496000 154000 116000 61000 124000 66000 236000 126000 114000 123000 410000 5880 56700 3620 36500 15200 5160 1510 3950 1790 14000 6230 5700 4100 124000 7.1 5.9 6 5.2 71.87 16.65 45.08 18.63 22.73 76.44 36.08 106.03 24.77 9.1 10.56 18.83 104.66 79.28 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 8.7 0.9 0.7 7.5 5.6 0.5 10.2 9.2 2.2 0.5 6.5 1.3 6.5 2.8 1 3 1 12 3 2 5 11 4 8 9 123 250 21 5.6 5.6 5.9 5.8 5.9 5.5 5.4 5.2 5.2 5.9 5.8 5.4 5.4 6.2 228 68 8 207 239 200 357 363 327 -66 189 280 355 241 104 840 316 678 168 144 48 138 63 385 153 115 123 614 18.3 13.8 15.9 17.2 17.4 16.5 15.1 16.3 16.7 16.7 17.1 14.8 16.7 17 1/18/2019 18 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 1111 . 11 ./L 1 . 1 40 ./L .111 ./L 1 ./L 11 . 1 . NE pg/L 11111 . 1111 ./L 1 . Concentration Column Labels Trip Equipment MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Blank Blank May-1 3 EPA 300.0 EPA 6010 Cobalt Iron .. EPA 8260 2-Hexanone Acetone Chloroform--------------�_- Chloride • • • _ _ _ Alkalinity, Total as CaCO3 , Total Dissolved • .s Chloride CyanideField feet Static Water Level Total Well Depth Oxygen, Dissolved 111 1 1 • .11 11 -- 11 11 - 111 :11 �- 11 _- ������� 18.2 64.1 35.3 ------ 65.1 - 6.6 --_- 877 34100 867 30700 324 8610 5820 4140 _- 7880 9630 496 --_-_�_ 1890 ®_ 158 240 160 offm I off moon ------------ 14.6 9.9 8.6 _- -------------_- -------------_- 1.4 -------------_- 4.2 -------------_- ------------_- 1.5 -------------_- . 11 .11 :•11 _- 589000 111 111 111 - 1:111 111 11111.111 :111 :111 111 1 111� 111 _- OIL 1111 Emu 11 -----©--------_- 1/18/2019 19 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 0000 700 pg/L 1000 300 pg/L 0 100 r 1000 r 1 1 1 •/L 11 • r r0 pg/L Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 EPA 6010 Barium Cobalt ... Iron • EPA 8081 .. ■ ■ ■ Heptachlor epoxide EPA .1 Chloride • • . Xylenes (Total)EPA 8270 ■r .■r r■ - r --- r r rr �- .r _- r -- 15.2 35.5 -----------_- --------���_- 1730 25300 344 29000 1430 11300 4520 12300 _- -��----------®-_- 8400 11600 541 1740 301 251 317 ------------ -®-----®--��®®�_- 18.7 8 28.6 -------------- r r . _- ------ 0.12 --------_- ---------------_- 1.3 -------------_- 4.5 -------------_- -------------_- 1.8 -------------_- ------------_- 1/18/2019 20 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 00000TotalDissolved NE pg/L rr 100 NE pg/L 0.3 pg/L 1000 Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-51R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank - . - . •s SM 1 • Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 EPA 6010 . Sodium Vanadium 1.4 ----- -------_- 564000 r rrr II err •:rr� _- ---------------_- ------------�- r _- ---------- - 3190 41500 ®i' --�-® 26300 539 3760 1140 10000 - 8280 ® 9310 370 ----------®-_- --®i --- 1580 ® 91.5 170 327 7.2 - 23.4 -®----------�-®_- 1/18/2019 21 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 1 1 11 1 11. 1 1 . 0.019 0.002 111: 1 1 14 pg/L 40 ./L 11 . 1 . 0.05 ./L NE pg/L 11111 . 1111 . Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank EPA 8081 - ■ ■ ■ - -DDT . .. • - . - Dieldrin Heptachlor Heptachlor epoxide MethoxychlorEPA 8260 Chloride o-Xylene-------------_- • . - - - EPA 8270 • . lndeno(1,2,3-cd)pyrene----------- Alkalinity, •3 Total • TotalDissolved . • • •-_- ---- 0.13 --------_- 110- 0.18 -------------_- ---- 0.14 --1 0.1 --------_- - 0.069 0.081 --------_- 0.48-------------_- ------ 0.066 -------------_- 1.5 -------------_- 3.2 -------------_- 1.7 -------------_- -- 5.5 ------------_- 1.2 1.5 --_- 111 1111 11 11 1 11 11 _- 111 531000 .:111111•I11 - 1.111 111 111•111 K . 111 1111K 1111 111 .1111 _- 1/18/2019 22 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units NE pg/L 250000 r 0 pg/L 10 pg/L 300 pg/L NE pg/L r.3 pg/L 1000 NE pg/L 00000 250000 Concentration Row Labels SM 1 1 Cyanide SM 1 Sulfide Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 EPA 6010 Barium Chromium Cobalt Iron Manganese----------_- Sodium Vanadium Alkalinity, Total as CaCO3 .. • • • . • SM Chloride--- feet Static Water Level Total Well Depth Oxygen, Dissolved Column Labels MW-1R MW-2R MW-3R MW-4R MW-51R MW-6R MW-7 MW-8 w MW-9 -------_- MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank ------ ------- -------_- --- r r----------_- 14.7 --- 15 --- 368 257 3540 ®----------_- -- r r r ----------_- 13 ----®----------_- rr -- r •err ----------_- rME=Field ----------_- 1/18/2019 23 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 250000 1000 rr 0 . 100 NE pg/L r 1000 r pg/L 500 r NE pg/L ■rrrrTotalDissolved Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 300.0 EPA 6010 Copper . Sodium . EPA 8260 1,1-Dichloroethene6000 . Chloride3.5 . • . Total Alkalinity, • . . '. r--------� r--_- 11.8 --------��---_- -_ 2980 40300 -_-_-_-_®_-_ 424 23000 3030 6140 2050 7920 7310 1250 58.3 140 71 -©�------- ---_- ------------ 10.8 -®-----®----�®-_- -®-------------�® 2 -------------_- -®-------------_- -------------_ 3.2 1.8 •r�r err --- r� •.■r r� r� rr■ rr �r �-rr -_- ..:r�r :r�rr --- err r�r :err :•rrr rr� err •rr� :r�r -_- 1/18/2019 24 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 250000 pg/L NS pg/L NE pg/L 1 pg/L 0.7 pg/L NE pg/L NS pg/L NE pg/L 250000 pg/L Row Labels SM 4500-CI-E pg/L Chloride Field feet Static Water Level Total Well Depth mg/I Oxygen, Dissolved NTU Turbidity Std. Units Field pH my REDOX pmhos/cm Field Specific Conductance 'C Field Temperature June-11 EPA 350.1 pg/L Nitrogen, Ammonia EPA 6010 pg/L Sodium EPA 8260 pg/L Benzene Tetrachloroethene Tetrahydrofuran RSK 175 pg/L Methane SM 2320B pg/L Alkalinity, Total as CaCO3 SM 4500-CI-E pg/L Chloride Field feet Static Water Level Total Well Depth mg/I Oxygen, Dissolved NTU Turbidity Std. Units Field pH my REDOX 62400 8480 8030 36.52 16.58 44.06 9.04 11.1 77.6 17.03 52.19 12.24 7.38 9.19 17.83 52.08 21 27 48 27 60 21 20 15.58 20 60 1.7 3.1 4 5.8 6.8 4.5 0.6 2 6.9 6.2 1 4 3 4 1 2 37 54 223 154 5.9 6 5.8 5.6 5.6 5.6 6.3 6 5.9 5.8 95 71 207 206 205 223 -1481 216 239 218 762 306 158 48 141 58 289 155 127 139 12.7 13.8 12.3 15.2 14.9 14.2 13.5 13 13.3 14.3 0.12 27200 274 1280 165000 39900 8.31 21 4.2 3 5.8 88 1/18/2019 25 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 11 • 1 ./L 11 . 1 . 11 pg/L 1 • Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field Specific Conductance Field Temperature May-1 1 • 6010 • 8260 • • - - Chloroform-------------_- Chloride o-Xylene------------_- • • - - - feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units EPAField Field pH mv REDOX Field Specific Conductance Field Temperature 6010 Barium • 8260 Chloride ---------------_- ---------------_- ------®--------_- 1.3 -------------_- 4.1 -------------_- 1.4 ---------------_- -®�-®--------_- ---------------_- 4.2 -------------_- 1/18/2019 26 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units Concentration Row Labels Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 8260 Field feet Static Water Level Total Well Depth Oxygen, Dissolved NTU Turbidity Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 6010 EPA 8260 Field feet Static Water Level Total Well Depth Oxygen, Dissolved 1/18/2019 27 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units „ :wwwwwww�wwwwww� 350 . 700 . Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank NTU Turbidity Std. Units Field ' mv REDOX��®www®ww pmhos/cm��wwwwwww�wwwwww� d Specific Conductance��wwwwwww�wwwwww� Field TemperatureField feet Static Water Level TotalDepth��wwwwwww�wwwwww� g/l Oxygen, DissolvedNTU Turbidity Std. Units Field • mv - .• •��wwwwwww�wwwwww� Field Specific Conductance��wwwwwww�wwwwww� Field Temperature��wwwwwww�ww®www September-09 EPA 6010 "- • •EPA 8260 .. .. disulfide��wwww®ww®wwwwww� Methylene Chloride i •• . • feet Field Static = Water Level :.®®wwwwww®wwwwww� th 'Oxygen,Tur��wwwwwww�wwwwww� NTU ..®wwww®ww©®wwwww� Std. Units Field • mv REDOX pmhos/cm��wwwwwww�wwwwww� d Specific Conductance��wwwwwww�®wwwww� ©www©w©�iw©®®wwww� ww®www ��wwwwwww�wwwwww� ��wwwww®w®w®wwww� ��wwwwwww�wwwwwww ��wwwwwww�wwwwww� ��wwwwwww�wwwww�� ��wwwwwww�wwwwww� ��wwwwwww�wwwwww� �_�wwwwwww�wwwwww� ��wwwwwww�wwwwww� �_�wwwwwww�ww®www ��wwwwwww�wwwwww� ��wwwwwww�wwwww�� ��wwwwwww�wwwwww� ��wwwwwww�wwwwww� ��wwwww®www®www ��wwwwwww�www®www 10.7w_- ��wwwwwww�wwwwww� ��wwwwwww�wwwwww� ��wwwwwww�wwwwww� ��wwwwwww�wwwww�� ��wwwwwww�wwwwww� ��wwwwwww�wwwwww� ��wwwwwww�wwwwww� ®w®www®�wwwwww� ��wwwwwww�wwwwww� ��wwwwwww�wwwwww� ��w®wwwww®www®www 1/18/2019 28 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 700Carbondisulfide Concentration Column Label MW-1R MW-2R MW-3R MW-4R MW-5R NEON=9 MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field Temperature EPA 6010 EPA 8260 Field feet Static Water Level Total Well Depth Oxygen, Dissolved Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 6010 EPA 8260 Field feet Static Water Level Total Well Depth Oxygen, Dissolved Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature --®------------_- 40.2 -_- ------------- 26.2 -_- 1/18/2019 29 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 4001 . Concentration Column Labels Trip Equipment MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Blank Blank EPA 6010 EPA 7470 EPA 8260 Field feet Static Water Level Total Well Depth Oxygen, Dissolved Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature November-'7 Field feet Static Water Level Total Well Depth Oxygen, Dissolved Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature April-' . - ML ���M ML ■fit ---------------_� 1/18/2019 30 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 11 . 1 . 1 ./L 11 . Concentration Column Labels MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank feet Static Water Level Total Well Depth Oxygen, Dissolved Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature Cadmium Chromium feet Static Water Level Total Well Depth Oxygen, Dissolved Std. Units Field pH mv REDOX Field Specific Conductance Field Temperature EPA 6010---------------_- -- 24Field ---- -------_- 2 ------------_- ------------- 35 23Field -_- -_- 1/18/2019 31 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 11 • 1 •/L 1 • 1 . 11pg/L 10 pg/L 700 . 1 •/L 1 • 1 • 11pg/L 1 •/L 1 . 11 • 1 •Chromium®--®®- 11 . Concentration Column Labels MW-1R MW-2R MW-31R MW-4R MW-51R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank EPA 7470 EPA 8260 Chloromethane June-05 Chromium--1111■1111■®1111■1111■1111■1111■11111■1111■1111■1111■1111■1111■111♦- . Barium Chromium Chromium Selenium May---1111■1111■1111■1111■1111■1111■1111■1111®' i , Barium Chromium • November-03 • CadmiumIII�IIIIm1111m1111m1111�1111m1111■11111■1111■1111■1111■1111■1111■111♦- 5.4 _w _--L s_ ■--_ �_� IIIIm®1111■®®IIIIm1111m1111m1111m1111m1111m1111■111♦- ®-1111■1111■1111■1111■1111■1111■1111■11111■1111■1111■1111■1111■1111■111♦- --1111■1111■®1111■1111■1111■1111■11111■1111■1111■1111■1111■1111■111♦- ®III�IIIIm1111m1111■IIIIm' IIII�IIIIm®1111®' IIIIm1111m1111m" 1111■111♦- 14 --1111■1111■1111■1111■1111■1111■III�IIIIm1111m1111m1111m1111m1111■111♦- 14 13 1111■1111■1111■1111■1111■111♦- --1111■1111■1111■1 1111■1111■1 1111■1111■11111■111111■1111■1111■1111■111♦- --1111■1111■1111■1111■1111■1111■1111■11111■ 1111■1111■1111■1111■1111■111♦- --1111■ 1111■ 1111■1111■1111■1111■1111■ 11111■ 1111■1111■1111■1111■ 1111■111♦- --1111■®�©1111■1111■1111101111■11111■1111■1111■1111■1111■1111■111♦- ®III�IIII.,....IIIIm' 1111®' IIIIm111�1111■11111■1111■1111■1111■1111■1111■111♦- 14 ®® 26 28 -------_- 18 ®-- 41 --1111■1111■1111■1111■111®"' 1111■1111■11111■1111■1111■1111■1111■1111■111♦- 22 ----- 24 --------_- -� i-_---------_` ---- 2.7 ----------_- 17-------_- 11®IIIIm" IIIIm' IIIIm111�1111m1111■11111■1111■1111■1111■1111■1111■111♦- 1/18/2019 32 of 34 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date 2L Units 10 • 700 600 rr rr 700 700 10 •/L 1pg/L 700 pg/L Concentration Column Labels Trip Equipment MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Blank Blank • November-011 • Chromium-------_- . Chromium-------_- •mium 1---� Chromium • Arsenic Barium Chromium�� Chloride ©- 15 - 23 26 23 -------_- -- 21-----------_- �- 16 12 •� 900 19 95 35 36 140 16 17 1300 95 270 38 36 36 2700 94 150 -------_- -------_- ®: r 22 �� ®- :6 16 18 950 50 53 . -- 16 46 -------_- r 38 ®i 49 1300 2600 210 92 26 210 -------_- -------_- -- -- 31 1500 100 80 -©- 28 82 45 89 2600 4200 580 240 65 400 -------_- -------_- -------_- -------_- -------_� 14 24 40 860 60 40-®--------_- r 29 ��--------_- 62 --------_- -- 13 13 950 110 50 10 38 16 10 - - - 960 190 30 10 --------_- --------_- --------_- --------_- 1/18/2019 33 of 34 A3 6000 pg/L 10 pg/L 700 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 700 pg/L 2 pg/L 10 pg/L 15 pg/L 20 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 4000 pg/L 700 pg/L 2 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items Historical detections by date Concentration Column Labels Trip Equipment MW-1R MW-2R MW-31R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Blank Blank Acetone Arsenic 11 -------------_- Barium disufficle 1100 1400 2000 �� 1300Carbon --------_- Chromium Lead- 12 210 68 77 300 39 76 96 29 12 - 350 36 --------_- -------_- Mercury -- r -------_---_- Arsenic Barium Chromium Lead- r 49 34 19 860 850 25 130 32 43 820 170 69 33 20 1200 430 38 --------_- --------_- --------_- Barium Chromium Lead® 11 43 31 16 26 55 29 16 31 14 1800 410 53Mercury --------_- --------_- --------_- 1-----------_� Barium Cadmium 3 800 ®� ®i r� 750 --------_- Chromium Lead ©� -� 28 27 - 70 21 180 23Silver --------_- Barium®t Chromium Lead r -� 790 20 15 720 47 16 43 20Mercury 10 ��--------_- 970 21 Barium�®i Cadmium--- 1230 7Carbon 1000 -----------_- 1400 1930 --------_- disufficle Chromium 21 96 12 28 Lead 26 15 17 19 18 17 --------_- Mercury 1.8 �® 1.7 ®i . 1.4 1.4 --------_- 1/18/2019 34 of 34 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Surface water detections of concern within the last 6 years -Max of Result Row LabelsD- Column Labels 79- units SW-1 EPA 300.0 250000 pg/L Sulfate 4140 2060 2730 2530 3410 4320 4460 3690 3130 2820 2190 2700 2090 EPA 6010 150 pg/L Arsenic 3.6 5.9 21000 pg/L Barium 68.2 47.5 86.8 65.9 69.5 65 72.2 276 65.8 71.1 58.9 63.3 6.5 pg/L Beryllium 1.1 NE pg/L Cadmium 0.7 11 pg/L Chromium 13 NE pg/L Cobalt 9 14.6 NE pg/L Copper 8.6 3.9 16.4 1000 pg/L Iron 6560 4900 5040 5660 5520 9830 8870 155000 8210 22800 6900 25500 NE pg/L Lead 18.3 NE pg/L Manganese 926 461 804 1050 465 688 1160 1760 749 1530 855 1720 25 pg/L Nickel 8.7 NE pg/L Selenium 7 NE pg/L Sodium 15600 17000 23000 14200 13000 12800 16000 12500 14500 13000 12400 15500 NE pg/L Vanadium 4.3 37 NE pg/L Zinc 5.2 10.1 7.2 7.5 69.8 EPA 6010D 21000 pg/L Barium 47 1000 pg/L Iron 1840 NE pg/L Manganese 135 NE pg/L Sodium 11800 EPA 8081 0.002 pg/L Endrin 0.08 EPA 8260 2000 pg/L Acetone 11.2 11000 pg/L Methylene Chloride 2 Field Field pH 6 6.5 7.4 6.5 6.4 6.7 6.3 6.1 6.4 6.2 6.4 6.1 Field Specific Conductance 125.1 211.3 211 250.9 208.3 92.6 228.7 247 205 246 208 261 Field Temperature 11 22.8 8 21 17.2 9.4 20.4 10.8 21.2 13.7 22.4 14.7 Oxygen, Dissolved 6.2 4.34 6.6 4.7 3.25 5.5 4.5 0.5 5.5 3 5 8.7 REDOX 44.2 6.6 -121.9 -7.1 14.7 -78.3 11 7 284 -31 -13 -21 Static Water Level Total Well Depth 0 Turbidity 15.3 25.06 4.96 15.12 19.33 48.7 26.5 363.9 51 35 45 3 SM 2320B 20000 pg/L Alkalinity, Total as CaCO3 27400 49200 43600 33200 57400 27700 35100 44500 63700 45200 72700 58000 79700 SM 2540C NE pg/L Total Dissolved Solids 106000 131000 123000 143000 116000 118000 113000 140000 122000 126000 125000 104000 131000 SM 4500-CI-E 230000 pg/L Chloride 18300 29700 35700 49200 26800 26000 21600 31500 19500 23700 18100 20600 19700 SM 4500-CN-E 5 pg/L Cyanide 4.4 4.7 1 /18/2019 1 of 4 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple Items) Surface water detections of concern within the last 6 years -Max of Result Column Labels 79- SW-2 EPA 300.0 250000 pg/L Sulfate 20000 11100 9920 10900 6270 17100 11600 7280 5620 12700 5490 5090 4240 EPA 6010 150 pg/L Arsenic 3.7 17 6.2 21000 pg/L Barium 74.2 65.4 77.5 108 73.1 70 700 171 59.7 50.1 51.7 46.5 6.5 pg/L Beryllium 3.7 0.64 11 pg/L Chromium 2.8 3.8 40.3 3.2 NE pg/L Cobalt 5.9 4.4 NE pg/L Copper 81.6 3.2 1000 pg/L Iron 2540 1740 1790 29900 1510 2070 226000 75000 2130 3360 1400 1280 NE pg/L Lead 2.7 75 7.4 NE pg/L Manganese 397 196 304 1160 317 291 1020 1010 219 152 153 106 25 pg/L Nickel 16.4 3.1 NE pg/L Sodium 11300 11600 11600 10200 8420 11300 8390 17600 9840 10300 9160 9990 NE pg/L Vanadium 3.2 127 11.6 NE pg/L Zinc 249 28 EPA 6010D 21000 pg/L Barium 78.8 NE pg/L Copper 4.1 1000 pg/L Iron 4140 NE pg/L Manganese 615 NE pg/L Sodium 11900 EPA 7470 0.012 pg/L Mercury 0.2 EPA 8260 NE pg/L 2-Hexanone 1.8 2000 pg/L Acetone 12.9 NE pg/L Chloromethane 0.12 NE pg/L cis-1,2-Dichloroethene 0.33 11000 pg/L Methylene Chloride 3.1 110000 pg/L Tetrahydrofuran 61.3 18.4 11 pg/L Toluene 0.52 Field Field pH 6.6 6.5 6.8 7.1 6.8 6.5 6.6 6.5 6.3 6.8 6.7 7 6.7 Field Specific Conductance 203.7 179.4 783.6 181 172 208.7 88.6 185.9 324 183 134 144 135 Field Temperature 11.1 19 3.2 10.3 21 21.5 11.9 19.7 11.2 19.7 12.7 23 12.7 Oxygen, Dissolved 7.2 6.82 2.4 7.8 6.3 1.91 3.5 0.2 2.11 7.3 4 9.5 6.7 REDOX -21.1 -4.8 -68.9 -50.3 -15.2 -57 -84.6 -79.4 -36 252 -12 -10 -21 Static Water Level Total Well Depth 0 Turbidity 15.7 19.24 554.5 8.66 14.72 34.84 20.5 385.5 136.9 23 2 11 1 SM 2320B 20000 pg/L Alkalinity, Total as CaCO3 62600 56000 57600 46200 58800 32300 43200 33200 2390 41300 48900 48600 44700 SM 2540C NE pg/L Total Dissolved Solids 144000 135000 125000 129000 106000 113000 105000 125000 117000 120000 114000 91000 101000 1 /18/2019 2 of 4 A4 Facility Permit Qualifier SM 4500-CI-E 230000 pg/L Chloride SM 4500-CN-E 5 pg/L Cyanide SM 4500-S2D NE pg/L Sulfide SW-3 EPA 300.0 250000 pg/L Sulfate EPA 6010 21000 pg/L Barium 11 pg/L Chromium NE pg/L Cobalt NE pg/L Copper 1000 pg/L Iron NE pg/L Lead NE pg/L Manganese 25 pg/L Nickel NE pg/L Sodium NE pg/L Tin NE pg/L Vanadium NE pg/L Zinc EPA 6010D 21000 pg/L Barium 1000 pg/L Iron NE pg/L Manganese NE pg/L Sodium NE pg/L Zinc EPA 8081 NE pg/L 4,4'-DDD 0.05 pg/L Endosulfan II EPA 8260 2000 pg/L Acetone 1.19 pg/L Benzene NE pg/L cis-1,2-Dichloroethene 11000 pg/L Methylene Chloride 110000 pg/L Tetrahydrofuran EPA 8270 NE pg/L 3&4-Methylphenol(m&p Cresol) Field Field pH Field Specific Conductance Field Temperature Oxygen, Dissolved REDOX Static Water Level Total Well Depth Turbidity SM 2320B 20000 pg/L Alkalinity, Total as CaCO3 34-12 Old Salisbury Road Landfill (C&D) (Multiple Items) Surface water detections of concern within the last 6 years 12800 13500 15200 13800 6190 9720 12500 4050 28200 10700 11600 10800 10300 4.2 142 16000 18500 33800 15200 18500 11400 27000 17000 16800 26300 62500 20100 36400 223 217 173 270 114 152 105 206 181 348 185 315 3.4 5.3 7.2 3 6.8 3.4 14.8 14.4 25.3 13 4.4 13100 1720 8240 10500 3390 4160 4940 5270 8890 11700 9560 16500 2.7 6310 7340 4750 8350 2310 3860 1420 5080 4320 8930 3990 5200 3.9 5.5 3.6 6.8 2.8 2.8 4.8 12 27000 35500 24600 38400 14700 20900 18200 29900 29900 41100 25000 33800 2.8 2.5 5.6 9.7 9.8 9.6 13.6 10.8 122 2500 2130 16900 7.1 0.079 0.071 16.2 0.42 0.54 0.32 0.88 0.34 0.26 1 3.4 6.3 3.3 10.2 9.7 18.9 5.1 4.8 3.6 6.5 6.5 6.7 6.6 6.5 6.4 6.9 6.6 6.5 6.2 6.3 6.2 376 702 959 549 1006 274.8 364.2 885 649 899 575 700 11 21.5 7.9 21.2 15.6 8.2 17.5 12.5 18.9 15.1 22.4 10 6.2 1.34 3 4.3 2.81 3.2 6.9 4.5 2.9 2.5 1.9 2.1 -5.9 -33.2 -19 -49.6 -23.6 -90 -15.8 -45 127 -15 -53 -26 0 10.9 45.87 14.79 7.94 13.52 9.1 42.7 16.6 14 57 13 14 181000 356000 477000 251000 520000 161000 210000 118000 389000 259000 516000 293000 317000 1/18/2019 3 of 4 A4 Facility Permit Qualifier SM 2540C NE pg/L Total Dissolved Solids SM 4500-CI-E 230000 pg/L Chloride SM 4500-CN-E 5 pg/L Cyanide SW-4 EPA 300.0 250000 pg/L Sulfate EPA 6010 21000 pg/L Barium 11 pg/L Chromium NE pg/L Cobalt 1000 pg/L Iron NE pg/L Manganese 25 pg/L Nickel NE pg/L Sodium NE pg/L Vanadium NE pg/L Zinc EPA 6010D 21000 pg/L Barium 1000 pg/L Iron NE pg/L Manganese NE pg/L Sodium NE pg/L Zinc EPA 8081 NE pg/L 4,4'-DDD EPA 8260 NE pg/L 2-Hexanone 2000 pg/L Acetone 11000 pg/L Methylene Chloride 110000 pg/L Tetrahydrofuran NE pg/L Trichlorofluoromethane Field Field pH Field Specific Conductance Field Temperature Oxygen, Dissolved REDOX Static Water Level Total Well Depth Turbidity SM 2320B 20000 pg/L Alkalinity, Total as CaCO3 SM 2540C NE pg/L Total Dissolved Solids SM 4500-CI-E 230000 pg/L Chloride SM 4500-CN-E 5 pg/L Cyanide 34-12 Old Salisbury Road Landfill (C&D) (Multiple Items) Surface water detections of concern within the last 6 years 241000 413000 600000 321000 623000 231000 300000 233000 473000 319000 705000 327000 432000 12000 22300 33800 18400 34000 10500 16300 27000 27000 16900 34800 20000 24300 4.6 6 27500 24400 26700 18200 28600 16600 24900 23500 17600 23500 23000 13200 32300 138 110 121 128 113 115 187 82.8 126 101 106 151 4.7 5.9 10.4 3020 802 1480 1520 1520 2240 9220 638 2520 1790 4180 1640 3580 1020 2900 2930 1930 2550 5050 739 2250 1080 1650 2430 2.6 2.5 3.6 23400 25600 23400 26000 16900 20200 23800 17800 24400 20100 18200 29000 3.5 5.9 8.3 7.3 124 3890 1470 20000 6.9 0.11 3.1 16 1.2 5.7 3.5 3.6 4.1 4.4 0.32 0.27 0.25 6.7 7 7.1 7.3 7.2 7 6.5 6.7 6.8 6.8 6.9 6.8 374.7 530 509.1 461 549.9 247.9 603 344 478 369 367 523 11.7 22.3 8.1 20.4 17 9 18.2 10 19.3 12.8 23.3 12.4 7.5 7.12 7.5 6 6.33 7.6 3.5 8.18 7 4.3 5.8 6.7 -40.1 -42.6 -2.7 -38.5 -72.6 -87.1 -25.5 27 262 61 -31 83 0 8.4 9.89 3.5 7.13 6.16 3.2 18.6 28.3 33 4 15 92 145000 211000 192000 187000 240000 148000 187000 242000 140000 158000 152000 147000 220000 236000 327000 317000 289000 325000 229000 267000 371000 222000 257000 270000 255000 349000 24800 29800 36800 27400 27900 20300 19800 19000 24300 30800 31000 26900 28800 4.1 5.6 1 /18/2019 4 of 4 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix B — Laboratory Report Appendix Laboratory Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix B — Laboratory Report This page intentionally left blank. aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 December 14, 2018 Sean Quarry HDR Engineering 440 South Church Street Suite 1000 Charlotte, NC 28202 RE: Project: OSR Pace Project No.: 92408417 Dear Sean Quarry: Enclosed are the analytical results for sample(s) received by the laboratory between November 27, 2018 and December 11, 2018. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Some analyses have been subcontracted outside of the Pace Network. The subcontracted laboratory report has been attached. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR Pace Project No.: 92408417 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR 92408417 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92408417001 MW-8 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417002 MW-9 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417003 MW-14 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417004 MW-11 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR Pace Project No.: 92408417 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417005 MW-12 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417006 MW-13 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417007 SW-1 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417008 SW-3 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR Pace Project No.: 92408417 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CRV 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417009 SW-4 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417010 MW-10 EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417011 SW-2 EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270D PKS 8 PASI-C EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR Pace Project No.: 92408417 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417012 MW-4R EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270D PKS 11 PASI-C EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417013 MW-2R EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270D PKS 11 PASI-C EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417014 EQUIPMENT BLANK EPA 8081B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270D PKS 8 PASI-C EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR 92408417 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92408417015 TRIP BLANK EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C 92408417016 MW-1 R EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270D PKS 8 PASI-C EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417017 MW-15 EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8270D PKS 8 PASI-C EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417018 MW-3R EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417019 MW-7 EPA 8081 B SEM 14 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR 92408417 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417020 MW-5R EPA 601OD SH1 18 PASI-A EPA7470A JMW1 1 PASI-A EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 CEH 1 PASI-A SM 4500-S2D-2011 GC 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 NAL 1 PASI-A SM 4500-CN-E-2011 KDF1 1 PASI-A 92408417021 TRIP BLANK EPA 8260E CL 53 PASI-C EPA 8260B Mod. DLK 3 PASI-C 92408417022 MW-3R EPA 8270D PKS 8 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-8 Lab ID: 92408417001 Collected: 11/26/18 10:25 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:08 7440-38-2 Barium 36.0 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:08 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:08 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-50-8 Iron 42AJ ug/L 50.0 1 11/29/18 03:35 11/30/18 05:08 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7439-92-1 Manganese 4.OJ ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:08 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-22-4 Sodium 8300 ug/L 5000 1 11/29/18 03:35 11/30/18 05:08 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:08 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:08 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 10:54 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 21:48 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 21:48 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 21:48 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 21:48 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 21:48 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 21:48 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 21:48 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 21:48 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 21:48 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 21:48 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 21:48 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 21:48 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 21:48 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 21:48 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 21:48 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 21:48 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 21:48 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 21:48 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 21:48 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 21:48 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 21:48 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 21:48 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 21:48 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-8 Lab ID: 92408417001 Collected: 11/26/18 10:25 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 97 % 106 % 97 % Analytical Method: EPA 8260E Mod ND ug/L 100 % 105 % Analytical Method: SM 2320B-2011 24200 ug/L Analytical Method: SM 2540C-2011 68000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/27/18 21:48 107-06-2 1.0 1 11/27/18 21:48 75-35-4 1.0 1 11/27/18 21:48 156-59-2 1.0 1 11/27/18 21:48 156-60-5 1.0 1 11/27/18 21:48 78-87-5 1.0 1 11/27/18 21:48 10061-01-5 1.0 1 11/27/18 21:48 10061-02-6 1.0 1 11/27/18 21:48 100-41-4 5.0 1 11/27/18 21:48 591-78-6 5.0 1 11/27/18 21:48 74-88-4 1.0 1 11/27/18 21:48 75-09-2 5.0 1 11/27/18 21:48 108-10-1 1.0 1 11/27/18 21:48 100-42-5 1.0 1 11/27/18 21:48 630-20-6 1.0 1 11/27/18 21:48 79-34-5 1.0 1 11/27/18 21:48 127-18-4 10.0 1 11/27/18 21:48 109-99-9 1.0 1 11/27/18 21:48 108-88-3 1.0 1 11/27/18 21:48 71-55-6 1.0 1 11/27/18 21:48 79-00-5 1.0 1 11/27/18 21:48 79-01-6 1.0 1 11/27/18 21:48 75-69-4 1.0 1 11/27/18 21:48 96-18-4 2.0 1 11/27/18 21:48 108-05-4 1.0 1 11/27/18 21:48 75-01-4 2.0 1 11/27/18 21:48 179601-23-1 1.0 1 11/27/18 21:48 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 21:48 460-00-4 11/27/18 21:48 17060-07-0 11/27/18 21:48 2037-26-5 11/30/18 23:21 123-91-1 11/30/18 23:21 17060-07-0 11/30/18 23:21 2037-26-5 11 /28/18 18:37 11/28/18 15:17 11 /29/18 18:54 18496-25-8 Page 10 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-8 Lab ID: 92408417001 Collected: 11/26/18 10:25 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 1060 ug/L 1000 1 11/28/18 21:09 14808-79-8 Analytical Method: SM 4500-CI-E-2011 3110 ug/L 1000 1 12/02/1817:07 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:30 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-9 Lab ID: 92408417002 Collected: 11/26/18 11:20 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:21 7440-38-2 Barium 215 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:21 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:21 7440-43-9 Chromium 4.2J ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-50-8 Iron 250 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:21 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7439-92-1 Manganese 10.7 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:21 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-22-4 Sodium 15700 ug/L 5000 1 11/29/18 03:35 11/30/18 05:21 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:21 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:21 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 10:57 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 22:05 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 22:05 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 22:05 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 22:05 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 22:05 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 22:05 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 22:05 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 22:05 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 22:05 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 22:05 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 22:05 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 22:05 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 22:05 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 22:05 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 22:05 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 22:05 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 22:05 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 22:05 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:05 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:05 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 22:05 110-57-6 Dichlorodifluoromethane 0.991 ug/L 1.0 1 11/27/18 22:05 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 22:05 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-9 Lab ID: 92408417002 Collected: 11/26/18 11:20 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 1.3 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 94 % 105 % 95 % Analytical Method: EPA 8260E Mod ND ug/L 101 % 106 % Analytical Method: SM 2320B-2011 33500 ug/L Analytical Method: SM 2540C-2011 139000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/27/18 22:05 107-06-2 1.0 1 11/27/18 22:05 75-35-4 1.0 1 11/27/18 22:05 156-59-2 1.0 1 11/27/18 22:05 156-60-5 1.0 1 11/27/18 22:05 78-87-5 1.0 1 11/27/18 22:05 10061-01-5 1.0 1 11/27/18 22:05 10061-02-6 1.0 1 11/27/18 22:05 100-41-4 5.0 1 11/27/18 22:05 591-78-6 5.0 1 11/27/18 22:05 74-88-4 1.0 1 11/27/18 22:05 75-09-2 5.0 1 11/27/18 22:05 108-10-1 1.0 1 11/27/18 22:05 100-42-5 1.0 1 11/27/18 22:05 630-20-6 1.0 1 11/27/18 22:05 79-34-5 1.0 1 11/27/18 22:05 127-18-4 10.0 1 11/27/18 22:05 109-99-9 1.0 1 11/27/18 22:05 108-88-3 1.0 1 11/27/18 22:05 71-55-6 1.0 1 11/27/18 22:05 79-00-5 1.0 1 11/27/18 22:05 79-01-6 1.0 1 11/27/18 22:05 75-69-4 1.0 1 11/27/18 22:05 96-18-4 2.0 1 11/27/18 22:05 108-05-4 1.0 1 11/27/18 22:05 75-01-4 2.0 1 11/27/18 22:05 179601-23-1 1.0 1 11/27/18 22:05 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 22:05 460-00-4 11/27/18 22:05 17060-07-0 11/27/18 22:05 2037-26-5 11/30/18 23:40 123-91-1 11/30/18 23:40 17060-07-0 11/30/18 23:40 2037-26-5 11 /28/18 18:42 11/28/18 15:17 11 /29/18 18:56 18496-25-8 Page 13 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-9 Lab ID: 92408417002 Collected: 11/26/18 11:20 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 ND ug/L 1000 1 11/28/18 21:27 14808-79-8 Analytical Method: SM 4500-CI-E-2011 5330 ug/L 1000 1 12/02/1817:08 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:31 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-14 Lab ID: 92408417003 Collected: 11/26/18 12:05 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:37 7440-38-2 Barium 246 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-39-3 Beryllium 0.83J ug/L 1.0 1 11/29/18 03:35 11/30/18 05:37 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:37 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-50-8 Iron 653 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:37 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7439-92-1 Manganese 170 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7439-96-5 Nickel 6.3 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:37 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-22-4 Sodium 18600 ug/L 5000 1 11/29/18 03:35 11/30/18 05:37 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:37 7440-62-2 Zinc 5.3J ug/L 10.0 1 11/29/18 03:35 11/30/18 05:37 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 10:59 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 22:22 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 22:22 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 22:22 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 22:22 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 22:22 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 22:22 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 22:22 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 22:22 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 22:22 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 22:22 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 22:22 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 22:22 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 22:22 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 22:22 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 22:22 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 22:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 22:22 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 22:22 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:22 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:22 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 22:22 110-57-6 Dichlorodifluoromethane 2.4 ug/L 1.0 1 11/27/18 22:22 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 22:22 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-14 Lab ID: 92408417003 Collected: 11/26/18 12:05 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 0.86J ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 95 % 106 % 97 % Analytical Method: EPA 8260E Mod ND ug/L 102 % 106 % Analytical Method: SM 2320B-2011 67100 ug/L Analytical Method: SM 2540C-2011 154000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/27/18 22:22 107-06-2 1.0 1 11/27/18 22:22 75-35-4 1.0 1 11/27/18 22:22 156-59-2 1.0 1 11/27/18 22:22 156-60-5 1.0 1 11/27/18 22:22 78-87-5 1.0 1 11/27/18 22:22 10061-01-5 1.0 1 11/27/18 22:22 10061-02-6 1.0 1 11/27/18 22:22 100-41-4 5.0 1 11/27/18 22:22 591-78-6 5.0 1 11/27/18 22:22 74-88-4 1.0 1 11/27/18 22:22 75-09-2 5.0 1 11/27/18 22:22 108-10-1 1.0 1 11/27/18 22:22 100-42-5 1.0 1 11/27/18 22:22 630-20-6 1.0 1 11/27/18 22:22 79-34-5 1.0 1 11/27/18 22:22 127-18-4 10.0 1 11/27/18 22:22 109-99-9 1.0 1 11/27/18 22:22 108-88-3 1.0 1 11/27/18 22:22 71-55-6 1.0 1 11/27/18 22:22 79-00-5 1.0 1 11/27/18 22:22 79-01-6 1.0 1 11/27/18 22:22 75-69-4 1.0 1 11/27/18 22:22 96-18-4 2.0 1 11/27/18 22:22 108-05-4 1.0 1 11/27/18 22:22 75-01-4 2.0 1 11/27/18 22:22 179601-23-1 1.0 1 11/27/18 22:22 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 22:22 460-00-4 11/27/18 22:22 17060-07-0 11/27/18 22:22 2037-26-5 12/01/18 00:00 123-91-1 12/01 /18 00:00 17060-07-0 12/01 /18 00:00 2037-26-5 11 /28/18 18:58 11 /28/18 15:20 11 /29/18 18:57 18496-25-8 Page 16 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-14 Lab ID: 92408417003 Collected: 11/26/18 12:05 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 ND ug/L 1000 1 11/28/18 21:44 14808-79-8 Analytical Method: SM 4500-CI-E-2011 3840 ug/L 1000 1 12/02/1817:09 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:32 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-11 Lab ID: 92408417004 Collected: 11/26/18 10:36 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:40 7440-38-2 Barium 95.8 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:40 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:40 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-50-8 Iron 28200 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:40 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7439-92-1 Manganese 1620 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:40 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-22-4 Sodium 13600 ug/L 5000 1 11/29/18 03:35 11/30/18 05:40 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:40 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:40 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:01 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 22:39 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 22:39 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 22:39 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 22:39 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 22:39 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 22:39 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 22:39 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 22:39 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 22:39 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 22:39 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 22:39 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 22:39 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 22:39 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 22:39 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 22:39 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 22:39 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 22:39 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 22:39 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:39 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:39 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 22:39 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 22:39 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 22:39 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 18 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-11 Lab ID: 92408417004 Collected: 11/26/18 10:36 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 94 % 108 % 99 % Analytical Method: EPA 8260E Mod ND ug/L 101 % 105 % Analytical Method: SM 2320B-2011 161000 ug/L Analytical Method: SM 2540C-2011 237000 ug/L Analytical Method: SM 4500-S2D-2011 53.8J ug/L 1.0 1 11/27/18 22:39 107-06-2 1.0 1 11/27/18 22:39 75-35-4 1.0 1 11/27/18 22:39 156-59-2 1.0 1 11/27/18 22:39 156-60-5 1.0 1 11/27/18 22:39 78-87-5 1.0 1 11/27/18 22:39 10061-01-5 1.0 1 11/27/18 22:39 10061-02-6 1.0 1 11/27/18 22:39 100-41-4 5.0 1 11/27/18 22:39 591-78-6 5.0 1 11/27/18 22:39 74-88-4 1.0 1 11/27/18 22:39 75-09-2 5.0 1 11/27/18 22:39 108-10-1 1.0 1 11/27/18 22:39 100-42-5 1.0 1 11/27/18 22:39 630-20-6 1.0 1 11/27/18 22:39 79-34-5 1.0 1 11/27/18 22:39 127-18-4 10.0 1 11/27/18 22:39 109-99-9 1.0 1 11/27/18 22:39 108-88-3 1.0 1 11/27/18 22:39 71-55-6 1.0 1 11/27/18 22:39 79-00-5 1.0 1 11/27/18 22:39 79-01-6 1.0 1 11/27/18 22:39 75-69-4 1.0 1 11/27/18 22:39 96-18-4 2.0 1 11/27/18 22:39 108-05-4 1.0 1 11/27/18 22:39 75-01-4 2.0 1 11/27/18 22:39 179601-23-1 1.0 1 11/27/18 22:39 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 22:39 460-00-4 11/27/18 22:39 17060-07-0 11/27/18 22:39 2037-26-5 12/01/18 00:19 123-91-1 12/01 /18 00:19 17060-07-0 12/01 /18 00:19 2037-26-5 11 /28/18 19:29 11 /28/18 15:20 11 /29/18 18:57 18496-25-8 Page 19 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-11 Lab ID: 92408417004 Collected: 11/26/18 10:36 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 4500CNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 20700 ug/L 1000 1 11/28/18 22:36 14808-79-8 Analytical Method: SM 4500-CI-E-2011 11800 ug/L 1000 1 12/02/1817:11 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 4.OJ ug/L 8.0 1 11/28/18 12:45 11/29/18 09:33 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 20 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-12 Lab ID: 92408417005 Collected: 11/26/18 11:59 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:43 7440-38-2 Barium 132 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-39-3 Beryllium 0.88J ug/L 1.0 1 11/29/18 03:35 11/30/18 05:43 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:43 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-50-8 Iron 371 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:43 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7439-92-1 Manganese 336 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7439-96-5 Nickel 3.3J ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:43 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-22-4 Sodium 17600 ug/L 5000 1 11/29/18 03:35 11/30/18 05:43 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:43 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:43 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:04 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 22:56 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 22:56 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 22:56 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 22:56 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 22:56 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 22:56 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 22:56 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 22:56 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 22:56 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 22:56 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 22:56 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 22:56 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 22:56 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 22:56 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 22:56 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 22:56 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 22:56 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 22:56 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:56 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 22:56 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 22:56 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 22:56 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 22:56 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-12 Lab ID: 92408417005 Collected: 11/26/18 11:59 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 1.0J ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 98 % 107 % 96 % Analytical Method: EPA 8260E Mod ND ug/L 98 % 104 % Analytical Method: SM 2320B-2011 117000 ug/L Analytical Method: SM 2540C-2011 301000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/27/18 22:56 107-06-2 1.0 1 11/27/18 22:56 75-35-4 1.0 1 11/27/18 22:56 156-59-2 1.0 1 11/27/18 22:56 156-60-5 1.0 1 11/27/18 22:56 78-87-5 1.0 1 11/27/18 22:56 10061-01-5 1.0 1 11/27/18 22:56 10061-02-6 1.0 1 11/27/18 22:56 100-41-4 5.0 1 11/27/18 22:56 591-78-6 5.0 1 11/27/18 22:56 74-88-4 1.0 1 11/27/18 22:56 75-09-2 5.0 1 11/27/18 22:56 108-10-1 1.0 1 11/27/18 22:56 100-42-5 1.0 1 11/27/18 22:56 630-20-6 1.0 1 11/27/18 22:56 79-34-5 1.0 1 11/27/18 22:56 127-18-4 10.0 1 11/27/18 22:56 109-99-9 1.0 1 11/27/18 22:56 108-88-3 1.0 1 11/27/18 22:56 71-55-6 1.0 1 11/27/18 22:56 79-00-5 1.0 1 11/27/18 22:56 79-01-6 1.0 1 11/27/18 22:56 75-69-4 1.0 1 11/27/18 22:56 96-18-4 2.0 1 11/27/18 22:56 108-05-4 1.0 1 11/27/18 22:56 75-01-4 2.0 1 11/27/18 22:56 179601-23-1 1.0 1 11/27/18 22:56 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 22:56 460-00-4 11/27/18 22:56 17060-07-0 11/27/18 22:56 2037-26-5 12/01/18 00:38 123-91-1 12/01 /18 00:38 17060-07-0 12/01 /18 00:38 2037-26-5 11/28/18 19:41 11 /28/18 15:20 11 /29/18 18:57 18496-25-8 Page 22 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-12 Lab ID: 92408417005 Collected: 11/26/18 11:59 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 91700 ug/L 1000 1 11/29/18 00:20 14808-79-8 Analytical Method: SM 4500-CI-E-2011 14400 ug/L 1000 1 12/02/1817:12 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:34 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-13 Lab ID: 92408417006 Collected: 11/26/18 13:03 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:46 7440-38-2 Barium 124 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-39-3 Beryllium 0.69J ug/L 1.0 1 11/29/18 03:35 11/30/18 05:46 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:46 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-50-8 Iron 71.8 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:46 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7439-92-1 Manganese 9.8 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:46 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-22-4 Sodium 10900 ug/L 5000 1 11/29/18 03:35 11/30/18 05:46 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:46 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:46 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:06 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 23:13 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 23:13 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 23:13 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 23:13 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 23:13 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 23:13 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 23:13 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 23:13 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 23:13 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 23:13 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 23:13 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 23:13 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 23:13 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 23:13 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 23:13 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 23:13 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 23:13 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 23:13 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 23:13 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 23:13 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 23:13 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 23:13 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 23:13 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-13 Lab ID: 92408417006 Collected: 11/26/18 13:03 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 95 % 108 % 97 % Analytical Method: EPA 8260E Mod ND ug/L 97 % 104 % Analytical Method: SM 2320B-2011 52800 ug/L Analytical Method: SM 2540C-2011 111000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/27/18 23:13 107-06-2 1.0 1 11/27/18 23:13 75-35-4 1.0 1 11/27/18 23:13 156-59-2 1.0 1 11/27/18 23:13 156-60-5 1.0 1 11/27/18 23:13 78-87-5 1.0 1 11/27/18 23:13 10061-01-5 1.0 1 11/27/18 23:13 10061-02-6 1.0 1 11/27/18 23:13 100-41-4 5.0 1 11/27/18 23:13 591-78-6 5.0 1 11/27/18 23:13 74-88-4 1.0 1 11/27/18 23:13 75-09-2 5.0 1 11/27/18 23:13 108-10-1 1.0 1 11/27/18 23:13 100-42-5 1.0 1 11/27/18 23:13 630-20-6 1.0 1 11/27/18 23:13 79-34-5 1.0 1 11/27/18 23:13 127-18-4 10.0 1 11/27/18 23:13 109-99-9 1.0 1 11/27/18 23:13 108-88-3 1.0 1 11/27/18 23:13 71-55-6 1.0 1 11/27/18 23:13 79-00-5 1.0 1 11/27/18 23:13 79-01-6 1.0 1 11/27/18 23:13 75-69-4 1.0 1 11/27/18 23:13 96-18-4 2.0 1 11/27/18 23:13 108-05-4 1.0 1 11/27/18 23:13 75-01-4 2.0 1 11/27/18 23:13 179601-23-1 1.0 1 11/27/18 23:13 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 23:13 460-00-4 11/27/18 23:13 17060-07-0 11/27/18 23:13 2037-26-5 12/01/18 00:57 123-91-1 12/01 /18 00:57 17060-07-0 12/01 /18 00:57 2037-26-5 11 /28/18 19:50 11 /28/18 15:20 11 /29/18 18:58 18496-25-8 Page 25 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-13 Lab ID: 92408417006 Collected: 11/26/18 13:03 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 5650 ug/L 1000 1 11/29/18 00:37 14808-79-8 Analytical Method: SM 4500-CI-E-2011 5120 ug/L 1000 1 12/02/1817:13 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:34 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 26 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-1 Lab ID: 92408417007 Collected: 11/26/18 12:05 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:49 7440-38-2 Barium 47.0 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:49 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:49 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-50-8 Iron 1840 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:49 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7439-92-1 Manganese 135 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:49 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-22-4 Sodium 11800 ug/L 5000 1 11/29/18 03:35 11/30/18 05:49 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:49 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:49 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:09 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 23:30 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 23:30 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 23:30 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 23:30 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 23:30 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 23:30 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 23:30 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 23:30 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 23:30 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 23:30 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 23:30 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 23:30 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 23:30 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 23:30 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 23:30 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 23:30 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 23:30 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 23:30 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 23:30 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 23:30 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 23:30 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 23:30 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 23:30 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 27 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-1 Lab ID: 92408417007 Collected: 11/26/18 12:05 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 96 % 107 % 97 % Analytical Method: EPA 8260E Mod ND ug/L 103 % 105 % Analytical Method: SM 2320B-2011 27400 ug/L Analytical Method: SM 2540C-2011 106000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/27/18 23:30 107-06-2 1.0 1 11/27/18 23:30 75-35-4 1.0 1 11/27/18 23:30 156-59-2 1.0 1 11/27/18 23:30 156-60-5 1.0 1 11/27/18 23:30 78-87-5 1.0 1 11/27/18 23:30 10061-01-5 1.0 1 11/27/18 23:30 10061-02-6 1.0 1 11/27/18 23:30 100-41-4 5.0 1 11/27/18 23:30 591-78-6 5.0 1 11/27/18 23:30 74-88-4 1.0 1 11/27/18 23:30 75-09-2 5.0 1 11/27/18 23:30 108-10-1 1.0 1 11/27/18 23:30 100-42-5 1.0 1 11/27/18 23:30 630-20-6 1.0 1 11/27/18 23:30 79-34-5 1.0 1 11/27/18 23:30 127-18-4 10.0 1 11/27/18 23:30 109-99-9 1.0 1 11/27/18 23:30 108-88-3 1.0 1 11/27/18 23:30 71-55-6 1.0 1 11/27/18 23:30 79-00-5 1.0 1 11/27/18 23:30 79-01-6 1.0 1 11/27/18 23:30 75-69-4 1.0 1 11/27/18 23:30 96-18-4 2.0 1 11/27/18 23:30 108-05-4 1.0 1 11/27/18 23:30 75-01-4 2.0 1 11/27/18 23:30 179601-23-1 1.0 1 11/27/18 23:30 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 23:30 460-00-4 11/27/18 23:30 17060-07-0 11/27/18 23:30 2037-26-5 12/01/18 01:17 123-91-1 12/01 /18 01:17 17060-07-0 12/01 /18 01:17 2037-26-5 11 /28/18 19:58 11/28/18 15:21 11 /29/18 18:59 18496-25-8 Page 28 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-1 Lab ID: 92408417007 Collected: 11/26/18 12:05 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 4140 ug/L 1000 1 11/29/18 00:55 14808-79-8 Analytical Method: SM 4500-CI-E-2011 18300 ug/L 1000 1 12/02/1817:14 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:35 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-3 Lab ID: 92408417008 Collected: 11/26/18 15:45 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:52 7440-38-2 Barium 122 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:52 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:52 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-50-8 Iron 2500 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:52 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7439-92-1 Manganese 2130 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:52 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-22-4 Sodium 16900 ug/L 5000 1 11/29/18 03:35 11/30/18 05:52 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:52 7440-62-2 Zinc 7.1J ug/L 10.0 1 11/29/18 03:35 11/30/18 05:52 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:16 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 23:47 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 23:47 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 23:47 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 23:47 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 23:47 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 23:47 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 23:47 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 23:47 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 23:47 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 23:47 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 23:47 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 23:47 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 23:47 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 23:47 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 23:47 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 23:47 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 23:47 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 23:47 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 23:47 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 23:47 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 23:47 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 23:47 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 23:47 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-3 Lab ID: 92408417008 Collected: 11/26/18 15:45 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 97 % 110 % 94 % Analytical Method: EPA 8260E Mod ND ug/L 106 % 106 % Analytical Method: SM 2320B-2011 181000 ug/L Analytical Method: SM 2540C-2011 241000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/27/18 23:47 107-06-2 1.0 1 11/27/18 23:47 75-35-4 1.0 1 11/27/18 23:47 156-59-2 1.0 1 11/27/18 23:47 156-60-5 1.0 1 11/27/18 23:47 78-87-5 1.0 1 11/27/18 23:47 10061-01-5 1.0 1 11/27/18 23:47 10061-02-6 1.0 1 11/27/18 23:47 100-41-4 5.0 1 11/27/18 23:47 591-78-6 5.0 1 11/27/18 23:47 74-88-4 1.0 1 11/27/18 23:47 75-09-2 5.0 1 11/27/18 23:47 108-10-1 1.0 1 11/27/18 23:47 100-42-5 1.0 1 11/27/18 23:47 630-20-6 1.0 1 11/27/18 23:47 79-34-5 1.0 1 11/27/18 23:47 127-18-4 10.0 1 11/27/18 23:47 109-99-9 1.0 1 11/27/18 23:47 108-88-3 1.0 1 11/27/18 23:47 71-55-6 1.0 1 11/27/18 23:47 79-00-5 1.0 1 11/27/18 23:47 79-01-6 1.0 1 11/27/18 23:47 75-69-4 1.0 1 11/27/18 23:47 96-18-4 2.0 1 11/27/18 23:47 108-05-4 1.0 1 11/27/18 23:47 75-01-4 2.0 1 11/27/18 23:47 179601-23-1 1.0 1 11/27/18 23:47 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/27/18 23:47 460-00-4 11/27/18 23:47 17060-07-0 11/27/18 23:47 2037-26-5 12/01/18 01:36 123-91-1 12/01 /18 01:36 17060-07-0 12/01 /18 01:36 2037-26-5 11/28/18 20:03 11/28/18 15:21 11 /29/18 19:04 18496-25-8 Page 31 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-3 Lab ID: 92408417008 Collected: 11/26/18 15:45 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 16000 ug/L 1000 1 11/29/18 01:12 14808-79-8 Analytical Method: SM 4500-CI-E-2011 12000 ug/L 1000 1 12/02/1817:24 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:36 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 32 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-4 Lab ID: 92408417009 Collected: 11/26/18 14:45 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:55 7440-38-2 Barium 124 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:55 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:55 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-50-8 Iron 3890 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:55 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7439-92-1 Manganese 1470 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:55 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-22-4 Sodium 20000 ug/L 5000 1 11/29/18 03:35 11/30/18 05:55 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:55 7440-62-2 Zinc 6.9J ug/L 10.0 1 11/29/18 03:35 11/30/18 05:55 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:18 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 00:04 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 00:04 107-13-1 Benzene ND ug/L 1.0 1 11/28/18 00:04 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 00:04 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 00:04 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 00:04 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 00:04 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 00:04 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 00:04 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 00:04 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 00:04 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 00:04 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 00:04 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 00:04 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 00:04 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 00:04 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 00:04 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 00:04 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:04 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:04 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 00:04 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 00:04 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 00:04 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-4 Lab ID: 92408417009 Collected: 11/26/18 14:45 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 95 % 105 % 97 % Analytical Method: EPA 8260E Mod ND ug/L 102 % 106 % Analytical Method: SM 2320B-2011 145000 ug/L Analytical Method: SM 2540C-2011 236000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/28/18 00:04 107-06-2 1.0 1 11/28/18 00:04 75-35-4 1.0 1 11/28/18 00:04 156-59-2 1.0 1 11/28/18 00:04 156-60-5 1.0 1 11/28/18 00:04 78-87-5 1.0 1 11/28/18 00:04 10061-01-5 1.0 1 11/28/18 00:04 10061-02-6 1.0 1 11/28/18 00:04 100-41-4 5.0 1 11/28/18 00:04 591-78-6 5.0 1 11/28/18 00:04 74-88-4 1.0 1 11/28/18 00:04 75-09-2 5.0 1 11/28/18 00:04 108-10-1 1.0 1 11/28/18 00:04 100-42-5 1.0 1 11/28/18 00:04 630-20-6 1.0 1 11/28/18 00:04 79-34-5 1.0 1 11/28/18 00:04 127-18-4 10.0 1 11/28/18 00:04 109-99-9 1.0 1 11/28/18 00:04 108-88-3 1.0 1 11/28/18 00:04 71-55-6 1.0 1 11/28/18 00:04 79-00-5 1.0 1 11/28/18 00:04 79-01-6 1.0 1 11/28/18 00:04 75-69-4 1.0 1 11/28/18 00:04 96-18-4 2.0 1 11/28/18 00:04 108-05-4 1.0 1 11/28/18 00:04 75-01-4 2.0 1 11/28/18 00:04 179601-23-1 1.0 1 11/28/18 00:04 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/28/18 00:04 460-00-4 11/28/18 00:04 17060-07-0 11/28/18 00:04 2037-26-5 12/01/18 01:55 123-91-1 12/01 /18 01:55 17060-07-0 12/01 /18 01:55 2037-26-5 11/28/18 20:13 11/29/18 01:14 11 /29/18 19:04 18496-25-8 Page 34 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-4 Lab ID: 92408417009 Collected: 11/26/18 14:45 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 27500 ug/L 1000 1 11/29/18 01:29 14808-79-8 Analytical Method: SM 4500-CI-E-2011 24800 ug/L 1000 1 12/02/1817:27 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 4.1J ug/L 8.0 1 11/28/18 12:45 11/29/18 09:39 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-10 Lab ID: 92408417010 Collected: 11/26/18 13:30 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Date: 12/14/2018 09:55 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 309-00-2 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 319-84-6 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 319-86-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 72-54-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 50-29-3 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 959-98-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 33213-65-9 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 72-20-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 7421-93-4 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 76-44-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 13:47 1024-57-3 ND ug/L 0.15 1 11/28/18 09:56 11/30/18 13:47 72-43-5 94 % 10-130 1 11/28/18 09:56 11/30/18 13:47 877-09-8 185 % 10-130 1 11/28/18 09:56 11/30/18 13:47 2051-24-3 S5 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-36-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:58 7440-38-2 83.1 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-39-3 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:58 7440-41-7 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 05:58 7440-43-9 5.6 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-47-3 22.0 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-48-4 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-50-8 5030 ug/L 50.0 1 11/29/18 03:35 11/30/18 05:58 7439-89-6 2.6J ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7439-92-1 24700 ug/L 25.0 5 11/29/18 03:35 11/30/18 15:39 7439-96-5 11.1 ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-02-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:58 7782-49-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-22-4 151000 ug/L 25000 5 11/29/18 03:35 11/30/18 15:39 7440-23-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-31-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 05:58 7440-62-2 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 05:58 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:20 7439-97-6 Analytical Method: EPA 8260E ND ug/L 25.0 1 11/28/18 00:22 67-64-1 ND ug/L 10.0 1 11/28/18 00:22 107-13-1 0.55J ug/L 1.0 1 11/28/18 00:22 71-43-2 ND ug/L 1.0 1 11/28/18 00:22 74-97-5 ND ug/L 1.0 1 11/28/18 00:22 75-27-4 ND ug/L 1.0 1 11/28/18 00:22 75-25-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-10 Lab ID: 92408417010 Collected: 11/26/18 13:30 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Bromomethane ND ug/L 2.0 1 11/28/18 00:22 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 00:22 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 00:22 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 00:22 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 00:22 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 00:22 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 00:22 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 00:22 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 00:22 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 00:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 00:22 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 00:22 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:22 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:22 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 00:22 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 00:22 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 00:22 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/28/18 00:22 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/28/18 00:22 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 00:22 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 00:22 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/28/18 00:22 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 00:22 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 00:22 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/28/18 00:22 100-41-4 2-Hexanone ND ug/L 5.0 1 11/28/18 00:22 591-78-6 lodomethane ND ug/L 5.0 1 11/28/18 00:22 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/28/18 00:22 75-09-2 4-Methyl-2-pentanone (MIBK) 0.65J ug/L 5.0 1 11/28/18 00:22 108-10-1 Styrene ND ug/L 1.0 1 11/28/18 00:22 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 00:22 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 00:22 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/28/18 00:22 127-18-4 Tetrahydrofuran 169 ug/L 10.0 1 11/28/18 00:22 109-99-9 Toluene 0.26J ug/L 1.0 1 11/28/18 00:22 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 1 11/28/18 00:22 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/28/18 00:22 79-00-5 Trichloroethene ND ug/L 1.0 1 11/28/18 00:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/28/18 00:22 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/28/18 00:22 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/28/18 00:22 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/28/18 00:22 75-01-4 m&p-Xylene ND ug/L 2.0 1 11/28/18 00:22 179601-23-1 o-Xylene 0.53J ug/L 1.0 1 11/28/18 00:22 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 11/28/18 00:22 460-00-4 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 11/28/18 00:22 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 37 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-10 Lab ID: 92408417010 Collected: 11/26/18 13:30 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Surrogates Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E 96 % 70-130 1 11/28/18 00:22 2037-26-5 Analytical Method: EPA 8260E Mod. 8.5 ug/L 2.0 1 12/01/18 03:12 123-91-1 100 % 50-150 1 12/01/18 03:12 17060-07-0 106 % 50-150 1 12/01/18 03:12 2037-26-5 Analytical Method: SM 2320B-2011 652000 ug/L 5000 1 11/28/18 20:22 Analytical Method: SM 2540C-2011 1370000 ug/L 50000 1 11/29/18 01:14 Analytical Method: SM 4500-S2D-2011 ND ug/L 100 1 11/29/1819:04 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 357000 ug/L 7000 7 11/29/18 06:58 14808-79-8 Analytical Method: SM 4500-CI-E-2011 88500 ug/L 10000 10 12/02/1818:50 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 4.3J ug/L 8.0 1 11/28/18 12:45 11/29/18 09:40 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 38 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-2 Lab ID: 92408417011 Collected: 11/26/18 13:15 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:02 7440-38-2 Barium 78.8 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:02 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:02 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-48-4 Copper 4.1J ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-50-8 Iron 4140 ug/L 50.0 1 11/29/18 03:35 11/30/18 06:02 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7439-92-1 Manganese 615 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:02 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-22-4 Sodium 11900 ug/L 5000 1 11/29/18 03:35 11/30/18 06:02 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:02 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:02 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:23 7439-97-6 8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C Benzo(a)anthracene ND ug/L 10.0 1 11/27/18 16:06 11/28/18 15:23 56-55-3 Chrysene ND ug/L 10.0 1 11/27/18 16:06 11/28/18 15:23 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 11/27/18 16:06 11/28/18 15:23 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 1 11/27/18 16:06 11/28/18 15:23 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1 11/27/18 16:06 11/28/18 15:23 193-39-5 Surrogates Nitrobenzene-d5 (S) 79 % 13-130 1 11/27/18 16:06 11/28/18 15:23 4165-60-0 2-Fluorobiphenyl (S) 67 % 13-130 1 11/27/18 16:06 11/28/18 15:23 321-60-8 Terphenyl-d14 (S) 76 % 25-130 1 11/27/18 16:06 11/28/18 15:23 1718-51-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 00:39 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 00:39 107-13-1 Benzene ND ug/L 1.0 1 11/28/18 00:39 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 00:39 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 00:39 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 00:39 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 00:39 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 00:39 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 00:39 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 00:39 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 00:39 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 00:39 75-00-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 39 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-2 Lab ID: 92408417011 Collected: 11/26/18 13:15 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Chloroform ND ug/L 1.0 1 11/28/18 00:39 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 00:39 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 00:39 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 00:39 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 00:39 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 00:39 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:39 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:39 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 00:39 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 00:39 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 00:39 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/28/18 00:39 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/28/18 00:39 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 00:39 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 00:39 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/28/18 00:39 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 00:39 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 00:39 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/28/18 00:39 100-41-4 2-Hexanone ND ug/L 5.0 1 11/28/18 00:39 591-78-6 lodomethane ND ug/L 5.0 1 11/28/18 00:39 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/28/18 00:39 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/28/18 00:39 108-10-1 Styrene ND ug/L 1.0 1 11/28/18 00:39 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 00:39 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 00:39 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/28/18 00:39 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 11/28/18 00:39 109-99-9 Toluene ND ug/L 1.0 1 11/28/18 00:39 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 1 11/28/18 00:39 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/28/18 00:39 79-00-5 Trichloroethene ND ug/L 1.0 1 11/28/18 00:39 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/28/18 00:39 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/28/18 00:39 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/28/18 00:39 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/28/18 00:39 75-01-4 m&p-Xylene ND ug/L 2.0 1 11/28/18 00:39 179601-23-1 o-Xylene ND ug/L 1.0 1 11/28/18 00:39 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 11/28/18 00:39 460-00-4 1,2-Dichloroethane-d4 (S) 107 % 70-130 1 11/28/18 00:39 17060-07-0 Toluene-d8(S) 97 % 70-130 1 11/28/18 00:39 2037-26-5 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 12/03/18 12:46 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 50-150 1 12/03/18 12:46 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 40 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: SW-2 Lab ID: 92408417011 Collected: 11/26/18 13:15 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV SIM Surrogates Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E Mod. 106 % 50-150 1 12/03/1812:46 2037-26-5 Analytical Method: SM 2320B-2011 62600 ug/L 5000 1 11/28/18 20:32 Analytical Method: SM 254OC-2011 144000 ug/L 25000 1 11/29/18 01:14 Analytical Method: SM 4500-S2D-2011 ND ug/L 100 1 11/29/1819:07 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 20000 ug/L 1000 1 11/29/18 02:04 14808-79-8 Analytical Method: SM 4500-CI-E-2011 12800 ug/L 1000 1 12/02/1817:32 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 4.2J ug/L 8.0 1 11/28/18 12:45 11/29/18 09:41 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 41 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-411 Lab ID: 92408417012 Collected: 11/26/18 14:55 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8270 RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Date: 12/14/2018 09:55 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 309-00-2 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 319-84-6 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 319-86-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 72-54-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 50-29-3 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 959-98-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 33213-65-9 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 72-20-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 7421-93-4 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 76-44-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:00 1024-57-3 ND ug/L 0.15 1 11/28/18 09:56 11/30/18 14:00 72-43-5 80 % 10-130 1 11/28/18 09:56 11/30/18 14:00 877-09-8 242 % 10-130 1 11/28/18 09:56 11/30/18 14:00 2051-24-3 S5 Analytical Method: EPA 6010D Preparation Method: EPA 3010A ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-36-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:05 7440-38-2 222 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-39-3 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:05 7440-41-7 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:05 7440-43-9 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-47-3 35.0 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-48-4 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-50-8 475 ug/L 50.0 1 11/29/18 03:35 11/30/18 06:05 7439-89-6 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7439-92-1 584 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7439-96-5 5.01 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-02-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:05 7782-49-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-22-4 42600 ug/L 5000 1 11/29/18 03:35 11/30/18 06:05 7440-23-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-31-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:05 7440-62-2 5.2J ug/L 10.0 1 11/29/18 03:35 11/30/18 06:05 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:25 7439-97-6 Analytical Method: EPA 8270D Preparation Method: EPA 3510C ND ug/L 10.0 1 11/27/1816:06 11/28/1815:53 56-55-3 ND ug/L 10.0 1 11/27/1816:06 11/28/1815:53 218-01-9 ND ug/L 10.0 1 11/27/1816:06 11/28/1815:53 53-70-3 ND ug/L 6.0 1 11/27/1816:06 11/28/1815:53 117-81-7 ND ug/L 10.0 1 11/27/1816:06 11/28/1815:53 193-39-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 42 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-4R Lab ID: 92408417012 Collected: 11/26/18 14:55 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C Surrogates Nitrobenzene-d5 (S) 68 % 13-130 1 11/27/18 16:06 11/28/18 15:53 4165-60-0 2-Fluorobiphenyl (S) 59 % 13-130 1 11/27/18 16:06 11/28/18 15:53 321-60-8 Terphenyl-d14 (S) 67 % 25-130 1 11/27/18 16:06 11/28/18 15:53 1718-51-0 Phenol-d6 (S) 51 % 10-130 1 11/27/18 16:06 11/28/18 15:53 13127-88-3 2-Fluorophenol (S) 57 % 10-130 1 11/27/18 16:06 11/28/18 15:53 367-12-4 2,4,6-Tribromophenol (S) 77 % 10-137 1 11/27/18 16:06 11/28/18 15:53 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 00:56 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 00:56 107-13-1 Benzene ND ug/L 1.0 1 11/28/18 00:56 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 00:56 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 00:56 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 00:56 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 00:56 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 00:56 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 00:56 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 00:56 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 00:56 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 00:56 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 00:56 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 00:56 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 00:56 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 00:56 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 00:56 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 00:56 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:56 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 00:56 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 00:56 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 00:56 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 00:56 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/28/18 00:56 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/28/18 00:56 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 00:56 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 00:56 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/28/18 00:56 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 00:56 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 00:56 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/28/18 00:56 100-41-4 2-Hexanone ND ug/L 5.0 1 11/28/18 00:56 591-78-6 lodomethane ND ug/L 5.0 1 11/28/18 00:56 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/28/18 00:56 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/28/18 00:56 108-10-1 Styrene ND ug/L 1.0 1 11/28/18 00:56 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 00:56 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 00:56 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 43 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-4R Lab ID: 92408417012 Collected: 11/26/18 14:55 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Tetrachloroethene ND ug/L 1.0 1 11/28/18 00:56 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 11/28/18 00:56 109-99-9 Toluene ND ug/L 1.0 1 11/28/18 00:56 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 1 11/28/18 00:56 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/28/18 00:56 79-00-5 Trichloroethene ND ug/L 1.0 1 11/28/18 00:56 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/28/18 00:56 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/28/18 00:56 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/28/18 00:56 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/28/18 00:56 75-01-4 m&p-Xylene ND ug/L 2.0 1 11/28/18 00:56 179601-23-1 o-Xylene ND ug/L 1.0 1 11/28/18 00:56 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 11/28/18 00:56 460-00-4 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 11/28/18 00:56 17060-07-0 Toluene-d8(S) 96 % 70-130 1 11/28/18 00:56 2037-26-5 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) 2.4 ug/L 2.0 1 12/01/18 03:31 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 101 % 50-150 1 12/01/18 03:31 17060-07-0 Toluene-d8 (S) 105 % 50-150 1 12/01/18 03:31 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Alkalinity, Total as CaCO3 291000 ug/L 5000 1 11/29/18 16:13 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Total Dissolved Solids 496000 ug/L 25000 1 11/29/18 01:14 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Sulfide ND ug/L 100 1 11/29/1819:07 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Sulfate 104000 ug/L 2000 2 11/29/18 07:16 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Chloride 25200 ug/L 1000 1 12/02/1817:33 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Cyanide ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:41 57-12-5 Date: 12/14/2018 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 44 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-211 Lab ID: 92408417013 Collected: 11/26/18 14:52 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8270 RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Date: 12/14/2018 09:55 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 309-00-2 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 319-84-6 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 319-86-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 72-54-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 50-29-3 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 959-98-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 33213-65-9 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 72-20-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 7421-93-4 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 76-44-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:25 1024-57-3 ND ug/L 0.15 1 11/28/18 09:56 11/30/18 14:25 72-43-5 86 % 10-130 1 11/28/18 09:56 11/30/18 14:25 877-09-8 242 % 10-130 1 11/28/18 09:56 11/30/18 14:25 2051-24-3 S5 Analytical Method: EPA 6010D Preparation Method: EPA 3010A ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-36-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:14 7440-38-2 258 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-39-3 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:14 7440-41-7 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:14 7440-43-9 3.3J ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-47-3 15.9 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-48-4 2.6J ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-50-8 2090 ug/L 50.0 1 11/29/18 03:35 11/30/18 06:14 7439-89-6 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7439-92-1 8920 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7439-96-5 16.1 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-02-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:14 7782-49-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-22-4 64400 ug/L 5000 1 11/29/18 03:35 11/30/18 06:14 7440-23-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-31-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:14 7440-62-2 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:14 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:27 7439-97-6 Analytical Method: EPA 8270D Preparation Method: EPA 3510C ND ug/L 10.0 1 11/27/1816:06 11/28/1816:54 56-55-3 ND ug/L 10.0 1 11/27/1816:06 11/28/1816:54 218-01-9 ND ug/L 10.0 1 11/27/1816:06 11/28/1816:54 53-70-3 ND ug/L 6.0 1 11/27/1816:06 11/28/1816:54 117-81-7 ND ug/L 10.0 1 11/27/1816:06 11/28/1816:54 193-39-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 45 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-2R Lab ID: 92408417013 Collected: 11/26/18 14:52 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C Surrogates Nitrobenzene-d5 (S) 66 % 13-130 1 11/27/18 16:06 11/28/18 16:54 4165-60-0 2-Fluorobiphenyl (S) 57 % 13-130 1 11/27/18 16:06 11/28/18 16:54 321-60-8 Terphenyl-d14 (S) 66 % 25-130 1 11/27/18 16:06 11/28/18 16:54 1718-51-0 Phenol-d6 (S) 50 % 10-130 1 11/27/18 16:06 11/28/18 16:54 13127-88-3 2-Fluorophenol (S) 55 % 10-130 1 11/27/18 16:06 11/28/18 16:54 367-12-4 2,4,6-Tribromophenol (S) 77 % 10-137 1 11/27/18 16:06 11/28/18 16:54 118-79-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 01:13 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 01:13 107-13-1 Benzene 1.7 ug/L 1.0 1 11/28/18 01:13 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 01:13 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 01:13 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 01:13 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 01:13 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 01:13 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 01:13 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 01:13 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 01:13 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 01:13 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 01:13 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 01:13 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 01:13 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 01:13 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 01:13 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 01:13 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 01:13 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 01:13 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 01:13 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 01:13 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 01:13 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/28/18 01:13 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/28/18 01:13 75-35-4 cis-1,2-Dichloroethene 0.38J ug/L 1.0 1 11/28/18 01:13 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 01:13 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/28/18 01:13 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 01:13 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 01:13 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/28/18 01:13 100-41-4 2-Hexanone ND ug/L 5.0 1 11/28/18 01:13 591-78-6 lodomethane ND ug/L 5.0 1 11/28/18 01:13 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/28/18 01:13 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/28/18 01:13 108-10-1 Styrene ND ug/L 1.0 1 11/28/18 01:13 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 01:13 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 01:13 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-2R Lab ID: 92408417013 Collected: 11/26/18 14:52 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 450OS2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E 0.88J ug/L 1.0 1 11/28/18 01:13 127-18-4 45.4 ug/L 10.0 1 11/28/18 01:13 109-99-9 ND ug/L 1.0 1 11/28/18 01:13 108-88-3 ND ug/L 1.0 1 11/28/18 01:13 71-55-6 ND ug/L 1.0 1 11/28/18 01:13 79-00-5 0.901 ug/L 1.0 1 11/28/18 01:13 79-01-6 ND ug/L 1.0 1 11/28/18 01:13 75-69-4 ND ug/L 1.0 1 11/28/18 01:13 96-18-4 2.OJ ug/L 2.0 1 11/28/18 01:13 108-05-4 ND ug/L 1.0 1 11/28/18 01:13 75-01-4 ND ug/L 2.0 1 11/28/18 01:13 179601-23-1 ND ug/L 1.0 1 11/28/18 01:13 95-47-6 90 % 70-130 1 11/28/18 01:13 460-00-4 107 % 70-130 1 11/28/18 01:13 17060-07-0 97 % 70-130 1 11/28/18 01:13 2037-26-5 Analytical Method: EPA 8260E Mod. 2.1 ug/L 2.0 1 12/01/18 03:51 123-91-1 101 % 50-150 1 12/01/18 03:51 17060-07-0 105 % 50-150 1 12/01/18 03:51 2037-26-5 Analytical Method: SM 2320B-2011 573000 ug/L 5000 1 11/28/18 20:58 M1 Analytical Method: SM 2540C-2011 726000 ug/L 50000 1 11/29/18 01:14 Analytical Method: SM 4500-S2D-2011 ND ug/L 100 1 11/29/1819:07 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 95900 ug/L 1000 1 11/29/18 02:38 14808-79-8 Analytical Method: SM 4500-CI-E-2011 34500 ug/L 1000 1 12/02/1817:34 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 4.1J ug/L 8.0 1 11/28/18 12:45 11/29/18 09:42 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 47 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: EQUIPMENT BLANK Lab ID: 92408417014 Collected: 11/26/18 08:40 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8270 RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Date: 12/14/2018 09:55 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 309-00-2 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 319-84-6 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 319-86-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 72-54-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 50-29-3 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 959-98-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 33213-65-9 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 72-20-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 7421-93-4 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 76-44-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 14:51 1024-57-3 ND ug/L 0.15 1 11/28/18 09:56 11/30/18 14:51 72-43-5 71 % 10-130 1 11/28/18 09:56 11/30/18 14:51 877-09-8 69 % 10-130 1 11/28/18 09:56 11/30/18 14:51 2051-24-3 Analytical Method: EPA 6010D Preparation Method: EPA 3010A ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-36-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:18 7440-38-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-39-3 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:18 7440-41-7 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:18 7440-43-9 6.0 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-47-3 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-48-4 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-50-8 25.8J ug/L 50.0 1 11/29/18 03:35 11/30/18 06:18 7439-89-6 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7439-92-1 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7439-96-5 2.8J ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-02-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:18 7782-49-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-22-4 ND ug/L 5000 1 11/29/18 03:35 11/30/18 06:18 7440-23-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-31-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:18 7440-62-2 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:18 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:35 7439-97-6 Analytical Method: EPA 8270D Preparation Method: EPA 3510C ND ug/L 10.0 1 11/27/1816:06 11/28/1817:55 56-55-3 ND ug/L 10.0 1 11/27/1816:06 11/28/1817:55 218-01-9 ND ug/L 10.0 1 11/27/1816:06 11/28/1817:55 53-70-3 ND ug/L 6.0 1 11/27/1816:06 11/28/1817:55 117-81-7 ND ug/L 10.0 1 11/27/1816:06 11/28/1817:55 193-39-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 48 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: EQUIPMENT BLANK Lab ID: 92408417014 Collected: 11/26/18 08:40 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C Surrogates Nitrobenzene-d5 (S) 67 % 13-130 1 11/27/18 16:06 11/28/18 17:55 4165-60-0 2-Fluorobiphenyl (S) 60 % 13-130 1 11/27/18 16:06 11/28/18 17:55 321-60-8 Terphenyl-d14 (S) 70 % 25-130 1 11/27/18 16:06 11/28/18 17:55 1718-51-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 19:15 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 19:15 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 19:15 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 19:15 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 19:15 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 19:15 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 19:15 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 19:15 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 19:15 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 19:15 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 19:15 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 19:15 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 19:15 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 19:15 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 19:15 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 19:15 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 19:15 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 19:15 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 19:15 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 19:15 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 19:15 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 19:15 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 19:15 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/27/18 19:15 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/27/18 19:15 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/27/18 19:15 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/27/18 19:15 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/27/18 19:15 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/27/18 19:15 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/27/18 19:15 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/27/18 19:15 100-41-4 2-Hexanone ND ug/L 5.0 1 11/27/18 19:15 591-78-6 lodomethane ND ug/L 5.0 1 11/27/18 19:15 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/27/18 19:15 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/27/18 19:15 108-10-1 Styrene ND ug/L 1.0 1 11/27/18 19:15 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/27/18 19:15 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/27/18 19:15 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/27/18 19:15 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 11/27/18 19:15 109-99-9 Toluene ND ug/L 1.0 1 11/27/18 19:15 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: EQUIPMENT BLANK Lab ID: 92408417014 Collected: 11/26/18 08:40 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L 1.0 1 11/27/1819:15 71-55-6 ND ug/L 1.0 1 11/27/1819:15 79-00-5 ND ug/L 1.0 1 11/27/1819:15 79-01-6 ND ug/L 1.0 1 11/27/1819:15 75-69-4 ND ug/L 1.0 1 11/27/1819:15 96-18-4 ND ug/L 2.0 1 11/27/1819:15 108-05-4 ND ug/L 1.0 1 11/27/1819:15 75-01-4 ND ug/L 2.0 1 11/27/1819:15 179601-23-1 ND ug/L 1.0 1 11/27/1819:15 95-47-6 96 % 70-130 1 11/27/1819:15 460-00-4 103 % 70-130 1 11/27/1819:15 17060-07-0 98 % 70-130 1 11/27/1819:15 2037-26-5 Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1 11/30/1818:32 123-91-1 101 % 50-150 1 11/30/1818:32 17060-07-0 105 % 50-150 1 11/30/1818:32 2037-26-5 Analytical Method: SM 2320B-2011 ND ug/L 5000 1 11/28/18 21:33 Analytical Method: SM 2540C-2011 ND ug/L 25000 1 11/29/18 01:15 Analytical Method: SM 4500-S2D-2011 ND ug/L 100 1 11/29/1819:08 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 ND ug/L 1000 1 11/29/18 03:30 14808-79-8 Analytical Method: SM 4500-CI-E-2011 678J ug/L 1000 1 12/02/1817:39 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:45 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 50 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: TRIP BLANK Lab ID: 92408417015 Collected: 11/26/18 00:00 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 18:58 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 18:58 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 18:58 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 18:58 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 18:58 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 18:58 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 18:58 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 18:58 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 18:58 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 18:58 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 18:58 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 18:58 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 18:58 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 18:58 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 18:58 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 18:58 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 18:58 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 18:58 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 18:58 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 18:58 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 18:58 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 18:58 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 18:58 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/27/18 18:58 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/27/18 18:58 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/27/18 18:58 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/27/18 18:58 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/27/18 18:58 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/27/18 18:58 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/27/18 18:58 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/27/18 18:58 100-41-4 2-Hexanone ND ug/L 5.0 1 11/27/18 18:58 591-78-6 lodomethane ND ug/L 5.0 1 11/27/18 18:58 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/27/18 18:58 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/27/18 18:58 108-10-1 Styrene ND ug/L 1.0 1 11/27/18 18:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/27/18 18:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/27/18 18:58 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/27/18 18:58 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 11/27/18 18:58 109-99-9 Toluene ND ug/L 1.0 1 11/27/18 18:58 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 1 11/27/18 18:58 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/27/18 18:58 79-00-5 Trichloroethene ND ug/L 1.0 1 11/27/18 18:58 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/27/18 18:58 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/27/18 18:58 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/27/18 18:58 108-05-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: TRIP BLANK Lab ID: 92408417015 Collected: 11/26/18 00:00 Received: 11/27/18 08:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Vinyl chloride ND ug/L 1.0 1 11/27/18 18:58 75-01-4 m&p-Xylene ND ug/L 2.0 1 11/27/18 18:58 179601-23-1 o-Xylene ND ug/L 1.0 1 11/27/18 18:58 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/27/18 18:58 460-00-4 1,2-Dichloroethane-d4 (S) 104 % 70-130 1 11/27/18 18:58 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 11/27/18 18:58 2037-26-5 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 11/30/18 18:51 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 99 % 50-150 1 11/30/18 18:51 17060-07-0 Toluene-d8 (S) 104 % 50-150 1 11/30/18 18:51 2037-26-5 Date: 12/14/2018 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 52 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MWAR Lab ID: 92408417016 Collected: 11/27/18 09:37 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8270 RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Date: 12/14/2018 09:55 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 309-00-2 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 319-84-6 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 319-86-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 72-54-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 50-29-3 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 959-98-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 33213-65-9 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 72-20-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 7421-93-4 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 76-44-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:03 1024-57-3 ND ug/L 0.15 1 11/28/18 09:56 11/30/18 15:03 72-43-5 116 % 10-130 1 11/28/18 09:56 11/30/18 15:03 877-09-8 122 % 10-130 1 11/28/18 09:56 11/30/18 15:03 2051-24-3 Analytical Method: EPA 6010D Preparation Method: EPA 3010A ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-36-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:21 7440-38-2 284 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-39-3 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:21 7440-41-7 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:21 7440-43-9 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-47-3 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-48-4 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-50-8 ND ug/L 50.0 1 11/29/18 03:35 11/30/18 06:21 7439-89-6 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7439-92-1 16.7 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7439-96-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-02-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:21 7782-49-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-22-4 16500 ug/L 5000 1 11/29/18 03:35 11/30/18 06:21 7440-23-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-31-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:21 7440-62-2 5.1J ug/L 10.0 1 11/29/18 03:35 11/30/18 06:21 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A 0.57 ug/L 0.20 1 11/29/18 21:10 11/30/18 11:46 7439-97-6 Analytical Method: EPA 8270D Preparation Method: EPA 3510C ND ug/L 10.0 1 11/28/18 14:30 11/28/18 22:54 56-55-3 ND ug/L 10.0 1 11/28/18 14:30 11/28/18 22:54 218-01-9 ND ug/L 10.0 1 11/28/18 14:30 11/28/18 22:54 53-70-3 ND ug/L 6.0 1 11/28/18 14:30 11/28/18 22:54 117-81-7 ND ug/L 10.0 1 11/28/18 14:30 11/28/18 22:54 193-39-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 53 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MWAR Lab ID: 92408417016 Collected: 11/27/18 09:37 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C Surrogates Nitrobenzene-d5 (S) 72 % 13-130 1 11/28/18 14:30 11/28/18 22:54 4165-60-0 2-Fluorobiphenyl (S) 62 % 13-130 1 11/28/18 14:30 11/28/18 22:54 321-60-8 Terphenyl-d14 (S) 70 % 25-130 1 11/28/18 14:30 11/28/18 22:54 1718-51-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 01:30 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 01:30 107-13-1 Benzene ND ug/L 1.0 1 11/28/18 01:30 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 01:30 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 01:30 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 01:30 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 01:30 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 01:30 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 01:30 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 01:30 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 01:30 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 01:30 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 01:30 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 01:30 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 01:30 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 01:30 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 01:30 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 01:30 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 01:30 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 01:30 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 01:30 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 01:30 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 01:30 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/28/18 01:30 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/28/18 01:30 75-35-4 cis-1,2-Dichloroethene 0.85J ug/L 1.0 1 11/28/18 01:30 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 01:30 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/28/18 01:30 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 01:30 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 01:30 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/28/18 01:30 100-41-4 2-Hexanone ND ug/L 5.0 1 11/28/18 01:30 591-78-6 lodomethane ND ug/L 5.0 1 11/28/18 01:30 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/28/18 01:30 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/28/18 01:30 108-10-1 Styrene ND ug/L 1.0 1 11/28/18 01:30 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 01:30 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 01:30 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/28/18 01:30 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 11/28/18 01:30 109-99-9 Toluene ND ug/L 1.0 1 11/28/18 01:30 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MWAR Lab ID: 92408417016 Collected: 11/27/18 09:37 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L 1.0 1 11/28/18 01:30 71-55-6 ND ug/L 1.0 1 11/28/18 01:30 79-00-5 ND ug/L 1.0 1 11/28/18 01:30 79-01-6 ND ug/L 1.0 1 11/28/18 01:30 75-69-4 ND ug/L 1.0 1 11/28/18 01:30 96-18-4 ND ug/L 2.0 1 11/28/18 01:30 108-05-4 ND ug/L 1.0 1 11/28/18 01:30 75-01-4 ND ug/L 2.0 1 11/28/18 01:30 179601-23-1 ND ug/L 1.0 1 11/28/18 01:30 95-47-6 95 % 70-130 1 11/28/18 01:30 460-00-4 106 % 70-130 1 11/28/18 01:30 17060-07-0 99 % 70-130 1 11/28/18 01:30 2037-26-5 Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1 12/03/1813:44 123-91-1 104 % 50-150 1 12/03/1813:44 17060-07-0 111 % 50-150 1 12/03/1813:44 2037-26-5 Analytical Method: SM 2320B-2011 84100 ug/L 5000 1 11/28/18 21:37 Analytical Method: SM 2540C-2011 164000 ug/L 25000 1 11/29/18 01:15 Analytical Method: SM 4500-S2D-2011 ND ug/L 100 1 11/29/1819:11 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 ND ug/L 1000 1 11/29/18 04:23 14808-79-8 Analytical Method: SM 4500-CI-E-2011 8920 ug/L 1000 1 12/02/1817:41 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:49 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 55 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-15 Lab ID: 92408417017 Collected: 11/27/18 11:47 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8270 RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Date: 12/14/2018 09:55 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 309-00-2 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 319-84-6 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 319-86-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 72-54-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 50-29-3 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 959-98-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 33213-65-9 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 72-20-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 7421-93-4 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 76-44-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:16 1024-57-3 ND ug/L 0.15 1 11/28/18 09:56 11/30/18 15:16 72-43-5 97 % 10-130 1 11/28/18 09:56 11/30/18 15:16 877-09-8 115 % 10-130 1 11/28/18 09:56 11/30/18 15:16 2051-24-3 Analytical Method: EPA 6010D Preparation Method: EPA 3010A ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-36-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:24 7440-38-2 24.4 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-39-3 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:24 7440-41-7 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:24 7440-43-9 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-47-3 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-48-4 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-50-8 ND ug/L 50.0 1 11/29/18 03:35 11/30/18 06:24 7439-89-6 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7439-92-1 115 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7439-96-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-02-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:24 7782-49-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-22-4 26100 ug/L 5000 1 11/29/18 03:35 11/30/18 06:24 7440-23-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-31-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:24 7440-62-2 5.8J ug/L 10.0 1 11/29/18 03:35 11/30/18 06:24 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:49 7439-97-6 Analytical Method: EPA 8270D Preparation Method: EPA 3510C ND ug/L 10.0 1 11/28/18 14:30 11/28/18 23:23 56-55-3 ND ug/L 10.0 1 11/28/18 14:30 11/28/18 23:23 218-01-9 ND ug/L 10.0 1 11/28/18 14:30 11/28/18 23:23 53-70-3 ND ug/L 6.0 1 11/28/18 14:30 11/28/18 23:23 117-81-7 ND ug/L 10.0 1 11/28/18 14:30 11/28/18 23:23 193-39-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 56 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-15 Lab ID: 92408417017 Collected: 11/27/18 11:47 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C Surrogates Nitrobenzene-d5 (S) 73 % 13-130 1 11/28/18 14:30 11/28/18 23:23 4165-60-0 2-Fluorobiphenyl (S) 62 % 13-130 1 11/28/18 14:30 11/28/18 23:23 321-60-8 Terphenyl-d14 (S) 65 % 25-130 1 11/28/18 14:30 11/28/18 23:23 1718-51-0 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 01:47 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 01:47 107-13-1 Benzene ND ug/L 1.0 1 11/28/18 01:47 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 01:47 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 01:47 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 01:47 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 01:47 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 01:47 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 01:47 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 01:47 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 01:47 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 01:47 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 01:47 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 01:47 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 01:47 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 01:47 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 01:47 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 01:47 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 01:47 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 01:47 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 01:47 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 01:47 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 01:47 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/28/18 01:47 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/28/18 01:47 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 01:47 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 01:47 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/28/18 01:47 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 01:47 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 01:47 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/28/18 01:47 100-41-4 2-Hexanone ND ug/L 5.0 1 11/28/18 01:47 591-78-6 lodomethane ND ug/L 5.0 1 11/28/18 01:47 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/28/18 01:47 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/28/18 01:47 108-10-1 Styrene ND ug/L 1.0 1 11/28/18 01:47 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 01:47 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 01:47 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/28/18 01:47 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 11/28/18 01:47 109-99-9 Toluene ND ug/L 1.0 1 11/28/18 01:47 108-88-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 57 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-15 Lab ID: 92408417017 Collected: 11/27/18 11:47 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L 1.0 1 11/28/18 01:47 71-55-6 ND ug/L 1.0 1 11/28/18 01:47 79-00-5 ND ug/L 1.0 1 11/28/18 01:47 79-01-6 0.21J ug/L 1.0 1 11/28/18 01:47 75-69-4 ND ug/L 1.0 1 11/28/18 01:47 96-18-4 ND ug/L 2.0 1 11/28/18 01:47 108-05-4 ND ug/L 1.0 1 11/28/18 01:47 75-01-4 ND ug/L 2.0 1 11/28/18 01:47 179601-23-1 ND ug/L 1.0 1 11/28/18 01:47 95-47-6 96 % 70-130 1 11/28/18 01:47 460-00-4 107 % 70-130 1 11/28/18 01:47 17060-07-0 97 % 70-130 1 11/28/18 01:47 2037-26-5 Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1 12/03/1814:04 123-91-1 103 % 50-150 1 12/03/1814:04 17060-07-0 110 % 50-150 1 12/03/1814:04 2037-26-5 Analytical Method: SM 2320B-2011 89900 ug/L 5000 1 11/28/18 21:46 Analytical Method: SM 2540C-2011 395000 ug/L 25000 1 11/29/18 01:15 Analytical Method: SM 4500-S2D-2011 ND ug/L 100 1 11/29/1819:11 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 49900 ug/L 1000 1 11/29/18 04:40 14808-79-8 Analytical Method: SM 4500-CI-E-2011 128000 ug/L 5000 5 12/02/1818:52 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:50 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 58 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-311 Lab ID: 92408417018 Collected: 11/27/18 09:42 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:27 7440-38-2 Barium 275 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:27 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:27 7440-43-9 Chromium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-47-3 Cobalt 11.3 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-50-8 Iron 90800 ug/L 50.0 1 11/29/18 03:35 11/30/18 06:27 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7439-92-1 Manganese 7940 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:27 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-22-4 Sodium 2770J ug/L 5000 1 11/29/18 03:35 11/30/18 06:27 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-31-5 Vanadium ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:27 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:27 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:51 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 02:04 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 02:04 107-13-1 Benzene ND ug/L 1.0 1 11/28/18 02:04 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 02:04 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 02:04 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 02:04 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 02:04 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 02:04 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 02:04 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 02:04 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 02:04 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 02:04 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 02:04 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 02:04 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 02:04 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 02:04 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 02:04 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 02:04 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 02:04 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 02:04 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 02:04 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 02:04 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 02:04 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 59 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-3R Lab ID: 92408417018 Collected: 11/27/18 09:42 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 98 % 106 % 96 % Analytical Method: EPA 8260E Mod ND ug/L 98 % 105 % Analytical Method: SM 2320B-2011 192000 ug/L Analytical Method: SM 2540C-2011 213000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/28/18 02:04 107-06-2 1.0 1 11/28/18 02:04 75-35-4 1.0 1 11/28/18 02:04 156-59-2 1.0 1 11/28/18 02:04 156-60-5 1.0 1 11/28/18 02:04 78-87-5 1.0 1 11/28/18 02:04 10061-01-5 1.0 1 11/28/18 02:04 10061-02-6 1.0 1 11/28/18 02:04 100-41-4 5.0 1 11/28/18 02:04 591-78-6 5.0 1 11/28/18 02:04 74-88-4 1.0 1 11/28/18 02:04 75-09-2 5.0 1 11/28/18 02:04 108-10-1 1.0 1 11/28/18 02:04 100-42-5 1.0 1 11/28/18 02:04 630-20-6 1.0 1 11/28/18 02:04 79-34-5 1.0 1 11/28/18 02:04 127-18-4 10.0 1 11/28/18 02:04 109-99-9 1.0 1 11/28/18 02:04 108-88-3 1.0 1 11/28/18 02:04 71-55-6 1.0 1 11/28/18 02:04 79-00-5 1.0 1 11/28/18 02:04 79-01-6 1.0 1 11/28/18 02:04 75-69-4 1.0 1 11/28/18 02:04 96-18-4 2.0 1 11/28/18 02:04 108-05-4 1.0 1 11/28/18 02:04 75-01-4 2.0 1 11/28/18 02:04 179601-23-1 1.0 1 11/28/18 02:04 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/28/18 02:04 460-00-4 11/28/18 02:04 17060-07-0 11/28/18 02:04 2037-26-5 12/03/18 20:51 123-91-1 12/03/18 20:51 17060-07-0 12/03/18 20:51 2037-26-5 11/28/18 21:54 11/29/18 01:15 11 /29/18 19:11 18496-25-8 Page 60 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-3R Lab ID: 92408417018 Collected: 11/27/18 09:42 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 4500CNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 1300 ug/L 1000 1 11/29/18 04:57 14808-79-8 Analytical Method: SM 4500-CI-E-2011 2660 ug/L 1000 1 12/02/1817:43 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 5.OJ ug/L 8.0 1 11/28/18 12:45 11/29/18 09:51 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 61 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-7 Lab ID: 92408417019 Collected: 11/27/18 10:48 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8260 MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Date: 12/14/2018 09:55 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 309-00-2 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 319-84-6 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 319-86-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 72-54-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 50-29-3 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 959-98-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 33213-65-9 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 72-20-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 7421-93-4 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 76-44-8 ND ug/L 0.050 1 11/28/18 09:56 11/30/18 15:29 1024-57-3 ND ug/L 0.15 1 11/28/18 09:56 11/30/18 15:29 72-43-5 132 % 10-130 1 11/28/18 09:56 11/30/18 15:29 877-09-8 S5 98 % 10-130 1 11/28/18 09:56 11/30/18 15:29 2051-24-3 Analytical Method: EPA 6010D Preparation Method: EPA 3010A ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-36-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:30 7440-38-2 161 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-39-3 0.62J ug/L 1.0 1 11/29/18 03:35 11/30/18 06:30 7440-41-7 ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:30 7440-43-9 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-47-3 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-48-4 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-50-8 ND ug/L 50.0 1 11/29/18 03:35 11/30/18 06:30 7439-89-6 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7439-92-1 44.0 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7439-96-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-02-0 ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:30 7782-49-2 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-22-4 17700 ug/L 5000 1 11/29/18 03:35 11/30/18 06:30 7440-23-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-31-5 ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:30 7440-62-2 6.OJ ug/L 10.0 1 11/29/18 03:35 11/30/18 06:30 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:53 7439-97-6 Analytical Method: EPA 8260E ND ug/L 25.0 1 11/28/18 02:21 67-64-1 ND ug/L 10.0 1 11/28/18 02:21 107-13-1 0.37J ug/L 1.0 1 11/28/18 02:21 71-43-2 ND ug/L 1.0 1 11/28/18 02:21 74-97-5 ND ug/L 1.0 1 11/28/18 02:21 75-27-4 ND ug/L 1.0 1 11/28/18 02:21 75-25-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 62 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-7 Lab ID: 92408417019 Collected: 11/27/18 10:48 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Bromomethane ND ug/L 2.0 1 11/28/18 02:21 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 02:21 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 02:21 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 02:21 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 02:21 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 02:21 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 02:21 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 02:21 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 02:21 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 02:21 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 02:21 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 02:21 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 02:21 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 02:21 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 02:21 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 02:21 75-71-8 1,1-Dichloroethane 1.3 ug/L 1.0 1 11/28/18 02:21 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/28/18 02:21 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/28/18 02:21 75-35-4 cis-1,2-Dichloroethene 0.86J ug/L 1.0 1 11/28/18 02:21 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/28/18 02:21 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/28/18 02:21 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 02:21 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/28/18 02:21 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/28/18 02:21 100-41-4 2-Hexanone ND ug/L 5.0 1 11/28/18 02:21 591-78-6 lodomethane ND ug/L 5.0 1 11/28/18 02:21 74-88-4 Methylene Chloride 5.7 ug/L 1.0 1 11/28/18 02:21 75-09-2 C9 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/28/18 02:21 108-10-1 Styrene ND ug/L 1.0 1 11/28/18 02:21 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 02:21 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/28/18 02:21 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/28/18 02:21 127-18-4 Tetrahydrofuran 50.5 ug/L 10.0 1 11/28/18 02:21 109-99-9 Toluene ND ug/L 1.0 1 11/28/18 02:21 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 1 11/28/18 02:21 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/28/18 02:21 79-00-5 Trichloroethene ND ug/L 1.0 1 11/28/18 02:21 79-01-6 Trichlorofluoromethane 1.2 ug/L 1.0 1 11/28/18 02:21 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/28/18 02:21 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/28/18 02:21 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/28/18 02:21 75-01-4 m&p-Xylene 1.1J ug/L 2.0 1 11/28/18 02:21 179601-23-1 o-Xylene 0.59J ug/L 1.0 1 11/28/18 02:21 95-47-6 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 11/28/18 02:21 460-00-4 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 11/28/18 02:21 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 63 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-7 Lab ID: 92408417019 Collected: 11/27/18 10:48 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Surrogates Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E 96 % 70-130 1 11/28/18 02:21 2037-26-5 Analytical Method: EPA 8260E Mod. ND ug/L 2.0 1 12/03/1814:23 123-91-1 105 % 50-150 1 12/03/1814:23 17060-07-0 111 % 50-150 1 12/03/1814:23 2037-26-5 Analytical Method: SM 2320B-2011 78500 ug/L 5000 1 11/28/18 22:06 Analytical Method: SM 2540C-2011 171000 ug/L 25000 1 11/29/18 01:15 Analytical Method: SM 4500-S2D-2011 ND ug/L 100 1 11/29/1819:12 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 12700 ug/L 1000 1 11/29/18 05:15 14808-79-8 Analytical Method: SM 4500-CI-E-2011 6580 ug/L 1000 1 12/02/1817:44 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:52 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 64 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-511 Lab ID: 92408417020 Collected: 11/27/18 11:05 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Antimony ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-36-0 Arsenic ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:33 7440-38-2 Barium 59.8 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-39-3 Beryllium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:33 7440-41-7 Cadmium ND ug/L 1.0 1 11/29/18 03:35 11/30/18 06:33 7440-43-9 Chromium 5.5 ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-47-3 Cobalt ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-48-4 Copper ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-50-8 Iron ND ug/L 50.0 1 11/29/18 03:35 11/30/18 06:33 7439-89-6 Lead ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7439-92-1 Manganese ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7439-96-5 Nickel ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-02-0 Selenium ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:33 7782-49-2 Silver ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-22-4 Sodium 14600 ug/L 5000 1 11/29/18 03:35 11/30/18 06:33 7440-23-5 Tin ND ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-31-5 Vanadium 4.8J ug/L 5.0 1 11/29/18 03:35 11/30/18 06:33 7440-62-2 Zinc ND ug/L 10.0 1 11/29/18 03:35 11/30/18 06:33 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury ND ug/L 0.20 1 11/29/18 21:10 11/30/18 11:56 7439-97-6 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/28/18 02:38 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/28/18 02:38 107-13-1 Benzene ND ug/L 1.0 1 11/28/18 02:38 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/28/18 02:38 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/28/18 02:38 75-27-4 Bromoform ND ug/L 1.0 1 11/28/18 02:38 75-25-2 Bromomethane ND ug/L 2.0 1 11/28/18 02:38 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/28/18 02:38 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/28/18 02:38 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/28/18 02:38 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/28/18 02:38 108-90-7 Chloroethane ND ug/L 1.0 1 11/28/18 02:38 75-00-3 Chloroform ND ug/L 1.0 1 11/28/18 02:38 67-66-3 Chloromethane ND ug/L 1.0 1 11/28/18 02:38 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/28/18 02:38 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/28/18 02:38 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/28/18 02:38 106-93-4 Dibromomethane ND ug/L 1.0 1 11/28/18 02:38 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/28/18 02:38 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/28/18 02:38 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/28/18 02:38 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/28/18 02:38 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/28/18 02:38 75-34-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 65 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-5R Lab ID: 92408417020 Collected: 11/27/18 11:05 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260 MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 12/14/2018 09:55 AM Analytical Method: EPA 8260E ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 95 % 106 % 97 % Analytical Method: EPA 8260E Mod ND ug/L 105 % 111 % Analytical Method: SM 2320B-2011 35600 ug/L Analytical Method: SM 2540C-2011 156000 ug/L Analytical Method: SM 4500-S2D-2011 ND ug/L 1.0 1 11/28/18 02:38 107-06-2 1.0 1 11/28/18 02:38 75-35-4 1.0 1 11/28/18 02:38 156-59-2 1.0 1 11/28/18 02:38 156-60-5 1.0 1 11/28/18 02:38 78-87-5 1.0 1 11/28/18 02:38 10061-01-5 1.0 1 11/28/18 02:38 10061-02-6 1.0 1 11/28/18 02:38 100-41-4 5.0 1 11/28/18 02:38 591-78-6 5.0 1 11/28/18 02:38 74-88-4 1.0 1 11/28/18 02:38 75-09-2 5.0 1 11/28/18 02:38 108-10-1 1.0 1 11/28/18 02:38 100-42-5 1.0 1 11/28/18 02:38 630-20-6 1.0 1 11/28/18 02:38 79-34-5 1.0 1 11/28/18 02:38 127-18-4 10.0 1 11/28/18 02:38 109-99-9 1.0 1 11/28/18 02:38 108-88-3 1.0 1 11/28/18 02:38 71-55-6 1.0 1 11/28/18 02:38 79-00-5 1.0 1 11/28/18 02:38 79-01-6 1.0 1 11/28/18 02:38 75-69-4 1.0 1 11/28/18 02:38 96-18-4 2.0 1 11/28/18 02:38 108-05-4 1.0 1 11/28/18 02:38 75-01-4 2.0 1 11/28/18 02:38 179601-23-1 1.0 1 11/28/18 02:38 95-47-6 70-130 1 70-130 1 70-130 1 2.0 1 50-150 1 50-150 1 5000 1 25000 1 100 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 11/28/18 02:38 460-00-4 11/28/18 02:38 17060-07-0 11/28/18 02:38 2037-26-5 12/03/18 14:43 123-91-1 12/03/18 14:43 17060-07-0 12/03/18 14:43 2037-26-5 11/28/18 22:15 11/29/18 01:15 11 /29/18 19:16 18496-25-8 Page 66 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-5R Lab ID: 92408417020 Collected: 11/27/18 11:05 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 12/14/2018 09:55 AM Analytical Method: EPA 300.0 Rev 2.1 1993 8090 ug/L 1000 1 11/29/18 05:32 14808-79-8 Analytical Method: SM 4500-CI-E-2011 15100 ug/L 1000 1 12/02/1817:45 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 ND ug/L 8.0 1 11/28/18 12:45 11/29/18 09:53 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 67 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: TRIP BLANK Lab ID: 92408417021 Collected: 11/27/18 00:00 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Acetone ND ug/L 25.0 1 11/27/18 18:40 67-64-1 Acrylonitrile ND ug/L 10.0 1 11/27/18 18:40 107-13-1 Benzene ND ug/L 1.0 1 11/27/18 18:40 71-43-2 Bromochloromethane ND ug/L 1.0 1 11/27/18 18:40 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/27/18 18:40 75-27-4 Bromoform ND ug/L 1.0 1 11/27/18 18:40 75-25-2 Bromomethane ND ug/L 2.0 1 11/27/18 18:40 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/27/18 18:40 78-93-3 Carbon disulfide ND ug/L 2.0 1 11/27/18 18:40 75-15-0 Carbon tetrachloride ND ug/L 1.0 1 11/27/18 18:40 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/27/18 18:40 108-90-7 Chloroethane ND ug/L 1.0 1 11/27/18 18:40 75-00-3 Chloroform ND ug/L 1.0 1 11/27/18 18:40 67-66-3 Chloromethane ND ug/L 1.0 1 11/27/18 18:40 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/27/18 18:40 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/27/18 18:40 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 11/27/18 18:40 106-93-4 Dibromomethane ND ug/L 1.0 1 11/27/18 18:40 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/27/18 18:40 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/27/18 18:40 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 1 11/27/18 18:40 110-57-6 Dichlorodifluoromethane ND ug/L 1.0 1 11/27/18 18:40 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 11/27/18 18:40 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/27/18 18:40 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/27/18 18:40 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/27/18 18:40 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/27/18 18:40 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/27/18 18:40 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/27/18 18:40 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 1.0 1 11/27/18 18:40 10061-02-6 Ethylbenzene ND ug/L 1.0 1 11/27/18 18:40 100-41-4 2-Hexanone ND ug/L 5.0 1 11/27/18 18:40 591-78-6 lodomethane ND ug/L 5.0 1 11/27/18 18:40 74-88-4 Methylene Chloride ND ug/L 1.0 1 11/27/18 18:40 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/27/18 18:40 108-10-1 Styrene ND ug/L 1.0 1 11/27/18 18:40 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/27/18 18:40 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/27/18 18:40 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/27/18 18:40 127-18-4 Tetrahydrofuran ND ug/L 10.0 1 11/27/18 18:40 109-99-9 Toluene ND ug/L 1.0 1 11/27/18 18:40 108-88-3 1,1,1-Trichloroethane ND ug/L 1.0 1 11/27/18 18:40 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/27/18 18:40 79-00-5 Trichloroethene ND ug/L 1.0 1 11/27/18 18:40 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/27/18 18:40 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/27/18 18:40 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/27/18 18:40 108-05-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 68 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: TRIP BLANK Lab ID: 92408417021 Collected: 11/27/18 00:00 Received: 11/27/18 16:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV Low Level Landfill Analytical Method: EPA 8260E Vinyl chloride ND ug/L 1.0 1 11/27/18 18:40 75-01-4 m&p-Xylene ND ug/L 2.0 1 11/27/18 18:40 179601-23-1 o-Xylene ND ug/L 1.0 1 11/27/18 18:40 95-47-6 Surrogates 4-Bromofluorobenzene (S) 96 % 70-130 1 11/27/18 18:40 460-00-4 1,2-Dichloroethane-d4 (S) 106 % 70-130 1 11/27/18 18:40 17060-07-0 Toluene-d8 (S) 98 % 70-130 1 11/27/18 18:40 2037-26-5 8260 MSV SIM Analytical Method: EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1 12/03/18 12:26 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 102 % 50-150 1 12/03/18 12:26 17060-07-0 Toluene-d8 (S) 107 % 50-150 1 12/03/18 12:26 2037-26-5 Date: 12/14/2018 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 69 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR Pace Project No.: 92408417 Sample: MW-3R Lab ID: 92408417022 Collected: 12/11/18 10:46 Received: 12/11/18 17:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Date: 12/14/2018 09:55 AM Analytical Method: EPA 8270D Preparation Method: EPA 3510C ND ug/L 10.0 1 12/12/18 16:19 12/14/18 03:09 56-55-3 ND ug/L 10.0 1 12/12/18 16:19 12/14/18 03:09 218-01-9 ND ug/L 10.0 1 12/12/18 16:19 12/14/18 03:09 53-70-3 ND ug/L 6.0 1 12/12/18 16:19 12/14/18 03:09 117-81-7 ND ug/L 10.0 1 12/12/18 16:19 12/14/18 03:09 193-39-5 64 % 13-130 1 12/12/18 16:19 12/14/18 03:09 4165-60-0 58 % 13-130 1 12/12/18 16:19 12/14/18 03:09 321-60-8 67 % 25-130 1 12/12/18 16:19 12/14/18 03:09 1718-51-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 70 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444850 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013 METHOD BLANK: 2439371 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 11/30/1810:26 LABORATORY CONTROL SAMPLE: 2439372 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.7 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439373 2439374 MS MSD 92408597001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 2.6 2.8 103 110 75-125 7 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 71 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444851 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Associated Lab Samples: 92408417014, 92408417016, 92408417017, 92408417018, 92408417019, 92408417020 METHOD BLANK: 2439375 Matrix: Water Associated Lab Samples: 92408417014, 92408417016, 92408417017, 92408417018, 92408417019, 92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 11/30/1811:30 LABORATORY CONTROL SAMPLE: 2439376 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.4 96 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439377 2439378 MS MSD 92408417014 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 2.3 2.4 91 92 75-125 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 72 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444350 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013,92408417014, 92408417016,92408417017,92408417018,92408417019,92408417020 METHOD BLANK: 2437215 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013,92408417014, 92408417016,92408417017,92408417018,92408417019,92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Antimony ug/L ND 5.0 11/30/18 05:02 Arsenic ug/L ND 10.0 11/30/18 05:02 Barium ug/L ND 5.0 11/30/18 05:02 Beryllium ug/L ND 1.0 11/30/18 05:02 Cadmium ug/L ND 1.0 11/30/18 05:02 Chromium ug/L ND 5.0 11/30/18 05:02 Cobalt ug/L ND 5.0 11/30/18 05:02 Copper ug/L ND 5.0 11/30/18 05:02 Iron ug/L ND 50.0 11/30/18 05:02 Lead ug/L ND 5.0 11/30/18 05:02 Manganese ug/L ND 5.0 11/30/18 05:02 Nickel ug/L ND 5.0 11/30/18 05:02 Selenium ug/L ND 10.0 11/30/18 05:02 Silver ug/L ND 5.0 11/30/18 05:02 Sodium ug/L ND 5000 11/30/18 05:02 Tin ug/L ND 5.0 11/30/18 05:02 Vanadium ug/L ND 5.0 11/30/18 05:02 Zinc ug/L ND 10.0 11/30/18 05:02 LABORATORY CONTROL SAMPLE: Parameter 2437216 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Antimony ug/L 500 483 97 80-120 Arsenic ug/L 500 454 91 80-120 Barium ug/L 500 522 104 80-120 Beryllium ug/L 500 520 104 80-120 Cadmium ug/L 500 481 96 80-120 Chromium ug/L 500 489 98 80-120 Cobalt ug/L 500 472 94 80-120 Copper ug/L 500 507 101 80-120 Iron ug/L 5000 5150 103 80-120 Lead ug/L 500 463 93 80-120 Manganese ug/L 500 474 95 80-120 Nickel ug/L 500 477 95 80-120 Selenium ug/L 500 458 92 80-120 Silver ug/L 250 246 98 80-120 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 73 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 LABORATORY CONTROL SAMPLE: 2437216 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Sodium ug/L 5000 5240 105 80-120 Tin ug/L 500 475 95 80-120 Vanadium ug/L 500 488 98 80-120 Zinc ug/L 500 444 89 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437217 MS 92408417001 Spike Parameter Units Result Conc. Antimony ug/L ND 500 Arsenic ug/L ND 500 Barium ug/L 36.0 500 Beryllium ug/L ND 500 Cadmium ug/L ND 500 Chromium ug/L ND 500 Cobalt ug/L ND 500 Copper ug/L ND 500 Iron ug/L 42AJ 5000 Lead ug/L ND 500 Manganese ug/L 4.OJ 500 Nickel ug/L ND 500 Selenium ug/L ND 500 Silver ug/L ND 250 Sodium ug/L 8300 5000 Tin ug/L ND 500 Vanadium ug/L ND 500 Zinc ug/L ND 500 Qualifiers 2437218 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 500 474 481 95 96 75-125 1 500 451 455 90 91 75-125 1 500 549 554 103 104 75-125 1 500 514 520 103 104 75-125 1 500 476 481 95 96 75-125 1 500 483 491 96 98 75-125 2 500 461 467 92 93 75-125 1 500 496 500 99 100 75-125 1 5000 5160 5240 102 104 75-125 2 500 455 460 91 92 75-125 1 500 472 478 94 95 75-125 1 500 470 476 94 95 75-125 1 500 465 472 93 94 75-125 2 250 242 243 97 97 75-125 0 5000 13500 13500 104 105 75-125 0 500 474 480 95 96 75-125 1 500 480 486 96 97 75-125 1 500 447 455 89 90 75-125 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Qual Page 74 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444283 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417014,92408417015,92408417021 METHOD BLANK: 2436999 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417014,92408417015,92408417021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/27/18 18:06 1,1,1-Trichloroethane ug/L ND 1.0 11/27/18 18:06 1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/27/18 18:06 1,1,2-Trichloroethane ug/L ND 1.0 11/27/18 18:06 1,1-Dichloroethane ug/L ND 1.0 11/27/18 18:06 1,1-Dichloroethene ug/L ND 1.0 11/27/18 18:06 1,2,3-Trichloropropane ug/L ND 1.0 11/27/18 18:06 1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/27/18 18:06 1,2-Dibromoethane (EDB) ug/L ND 1.0 11/27/18 18:06 1,2-Dichlorobenzene ug/L ND 1.0 11/27/18 18:06 1,2-Dichloroethane ug/L ND 1.0 11/27/18 18:06 1,2-Dichloropropane ug/L ND 1.0 11/27/18 18:06 1,4-Dichlorobenzene ug/L ND 1.0 11/27/18 18:06 2-Butanone (MEK) ug/L ND 5.0 11/27/18 18:06 2-Hexanone ug/L ND 5.0 11/27/18 18:06 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 11/27/18 18:06 Acetone ug/L ND 25.0 11/27/18 18:06 Acrylonitrile ug/L ND 10.0 11/27/18 18:06 Benzene ug/L ND 1.0 11/27/18 18:06 Bromochloromethane ug/L ND 1.0 11/27/18 18:06 Bromodichloromethane ug/L ND 1.0 11/27/18 18:06 Bromoform ug/L ND 1.0 11/27/18 18:06 Bromomethane ug/L ND 2.0 11/27/18 18:06 Carbon disulfide ug/L ND 2.0 11/27/18 18:06 Carbon tetrachloride ug/L ND 1.0 11/27/18 18:06 Chlorobenzene ug/L ND 1.0 11/27/18 18:06 Chloroethane ug/L ND 1.0 11/27/18 18:06 Chloroform ug/L ND 1.0 11/27/18 18:06 Chloromethane ug/L ND 1.0 11/27/18 18:06 cis-1,2-Dichloroethene ug/L ND 1.0 11/27/18 18:06 cis-1,3-Dichloropropene ug/L ND 1.0 11/27/18 18:06 Dibromochloromethane ug/L ND 1.0 11/27/18 18:06 Dibromomethane ug/L ND 1.0 11/27/18 18:06 Dichlorodifluoromethane ug/L ND 1.0 11/27/18 18:06 Ethylbenzene ug/L ND 1.0 11/27/18 18:06 lodomethane ug/L ND 5.0 11/27/18 18:06 m&p-Xylene ug/L ND 2.0 11/27/18 18:06 Methylene Chloride ug/L ND 1.0 11/27/18 18:06 o-Xylene ug/L ND 1.0 11/27/18 18:06 Styrene ug/L ND 1.0 11/27/18 18:06 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 75 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 METHOD BLANK: 2436999 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417014,92408417015,92408417021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Tetrachloroethene ug/L ND 1.0 11/27/18 18:06 Tetrahydrofuran ug/L ND 10.0 11/27/18 18:06 Toluene ug/L ND 1.0 11/27/18 18:06 trans-1,2-Dichloroethene ug/L ND 1.0 11/27/18 18:06 trans- 1,3-Dichloropropene ug/L ND 1.0 11/27/18 18:06 trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/27/18 18:06 Trichloroethene ug/L ND 1.0 11/27/18 18:06 Trichlorofluoromethane ug/L ND 1.0 11/27/18 18:06 Vinyl acetate ug/L ND 2.0 11/27/18 18:06 Vinyl chloride ug/L ND 1.0 11/27/18 18:06 1,2-Dichloroethane-d4 (S) % 104 70-130 11/27/18 18:06 4-Bromofluorobenzene (S) % 97 70-130 11/27/18 18:06 Toluene-d8 (S) % 99 70-130 11/27/18 18:06 LABORATORY CONTROL SAMPLE: Parameter 2437000 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 50.1 100 70-130 1,1,1-Trichloroethane ug/L 50 49.0 98 70-130 1,1,2,2-Tetrachloroethane ug/L 50 47.1 94 70-130 1,1,2-Trichloroethane ug/L 50 47.4 95 70-130 1,1-Dichloroethane ug/L 50 46.1 92 70-130 1,1-Dichloroethene ug/L 50 47.9 96 70-130 1,2,3-Trichloropropane ug/L 50 48.8 98 70-130 1,2-Dibromo-3-chloropropane ug/L 50 50.2 100 70-130 1,2-Dibromoethane (EDB) ug/L 50 49.7 99 70-130 1,2-Dichlorobenzene ug/L 50 48.8 98 70-130 1,2-Dichloroethane ug/L 50 49.1 98 70-130 1,2-Dichloropropane ug/L 50 46.6 93 70-130 1,4-Dichlorobenzene ug/L 50 47.4 95 70-130 2-Butanone (MEK) ug/L 100 105 105 64-135 2-Hexanone ug/L 100 108 108 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 108 108 70-130 Acetone ug/L 100 106 106 61-157 Acrylonitrile ug/L 250 249 100 61-143 Benzene ug/L 50 46.8 94 70-130 Bromochloromethane ug/L 50 49.3 99 70-130 Bromodichloromethane ug/L 50 50.8 102 70-130 Bromoform ug/L 50 48.7 97 70-130 Bromomethane ug/L 50 60.9 122 38-128 Carbon disulfide ug/L 50 43.9 88 68-130 Carbon tetrachloride ug/L 50 49.0 98 70-130 Chlorobenzene ug/L 50 48.2 96 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 76 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 LABORATORY CONTROL SAMPLE: 2437000 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloroethane ug/L 50 46.0 92 37-142 Chloroform ug/L 50 48.0 96 70-130 Chloromethane ug/L 50 41.8 84 48-120 cis-1,2-Dichloroethene ug/L 50 47.2 94 70-130 cis-1,3-Dichloropropene ug/L 50 48.1 96 70-130 Dibromochloromethane ug/L 50 50.6 101 70-130 Dibromomethane ug/L 50 49.6 99 70-130 Dichlorodifluoromethane ug/L 50 35.9 72 53-134 Ethylbenzene ug/L 50 48.7 97 70-130 lodomethane ug/L 100 99.4 99 40-124 m&p-Xylene ug/L 100 96.7 97 70-130 Methylene Chloride ug/L 50 49.9 100 67-132 o-Xylene ug/L 50 48.7 97 70-130 Styrene ug/L 50 47.7 95 70-130 Tetrachloroethene ug/L 50 45.8 92 69-130 Tetrahydrofuran ug/L 500 519 104 62-128 Toluene ug/L 50 45.5 91 70-130 trans-1,2-Dichloroethene ug/L 50 47.1 94 70-130 trans- 1,3-Dichloropropene ug/L 50 49.6 99 70-130 trans-1,4-Dichloro-2-butene ug/L 50 63.3 127 35-189 Trichloroethene ug/L 50 47.1 94 70-130 Trichlorofluoromethane ug/L 50 48.4 97 63-126 Vinyl acetate ug/L 100 102 102 55-143 Vinyl chloride ug/L 50 41.9 84 70-131 1,2-Dichloroethane-d4 (S) % 103 70-130 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 98 70-130 MATRIX SPIKE SAMPLE: 2437002 92408417010 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 21.4 107 73-134 1,1,1-Trichloroethane ug/L ND 20 21.5 108 82-143 1,1,2,2-Tetrachloroethane ug/L ND 20 20.1 101 70-136 1,1,2-Trichloroethane ug/L ND 20 20.7 103 70-135 1,1-Dichloroethane ug/L ND 20 20.4 102 72-139 1,1-Dichloroethene ug/L ND 20 21.6 108 81-154 1,2,3-Trichloropropane ug/L ND 20 20.4 102 71-137 1,2-Dibromo-3-chloropropane ug/L ND 20 22.4 112 65-134 1,2-Dibromoethane (EDB) ug/L ND 20 20.5 102 72-137 1,2-Dichlorobenzene ug/L ND 20 21.1 106 70-133 1,2-Dichloroethane ug/L ND 20 20.7 104 73-137 1,2-Dichloropropane ug/L ND 20 20.1 101 79-140 1,4-Dichlorobenzene ug/L ND 20 20.8 104 70-133 2-Butanone (MEK) ug/L ND 40 45.4 114 60-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 77 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 MATRIX SPIKE SAMPLE: 2437002 92408417010 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Hexanone ug/L ND 40 46.0 115 65-138 4-Methyl-2-pentanone (MIBK) ug/L 0.65J 40 44.8 110 65-135 Acetone ug/L ND 40 58.1 145 60-148 Acrylonitrile ug/L ND 100 106 106 64-147 Benzene ug/L 0.55J 20 20.7 101 72-151 Bromochloromethane ug/L ND 20 21.9 109 77-141 Bromodichloromethane ug/L ND 20 21.2 106 76-138 Bromoform ug/L ND 20 19.3 97 63-130 Bromomethane ug/L ND 20 19.2 96 15-152 Carbon disulfide ug/L ND 20 19.3 97 69-149 Carbon tetrachloride ug/L ND 20 21.9 109 70-143 Chlorobenzene ug/L ND 20 21.3 106 70-138 Chloroethane ug/L ND 20 20.2 101 52-163 Chloroform ug/L ND 20 20.6 103 74-139 Chloromethane ug/L ND 20 18.8 94 41-139 cis-1,2-Dichloroethene ug/L ND 20 21.1 106 77-141 cis-1,3-Dichloropropene ug/L ND 20 19.0 95 74-137 Dibromochloromethane ug/L ND 20 21.0 105 70-134 Dibromomethane ug/L ND 20 21.7 108 76-138 Dichlorodifluoromethane ug/L ND 20 16.6 83 47-155 Ethylbenzene ug/L ND 20 21.0 105 66-153 lodomethane ug/L ND 40 41.2 103 20-138 m&p-Xylene ug/L ND 40 43.0 107 69-152 Methylene Chloride ug/L ND 20 21.5 108 42-159 o-Xylene ug/L 0.53J 20 21.6 105 73-148 Styrene ug/L ND 20 20.6 103 70-135 Tetrachloroethene ug/L ND 20 21.6 108 59-143 Tetrahydrofuran ug/L 169 200 394 112 70-133 Toluene ug/L 0.26J 20 19.2 95 59-148 trans-1,2-Dichloroethene ug/L ND 20 20.5 102 76-146 trans- 1,3-Dichloropropene ug/L ND 20 20.0 100 71-135 trans-1,4-Dichloro-2-butene ug/L ND 20 21.1 106 47-135 Trichloroethene ug/L ND 20 21.2 106 77-147 Trichlorofluoromethane ug/L ND 20 22.8 114 76-148 Vinyl acetate ug/L ND 40 38.2 96 49-151 Vinyl chloride ug/L ND 20 19.5 97 70-156 1,2-Dichloroethane-d4 (S) % 106 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 97 70-130 SAMPLE DUPLICATE: 2437001 92408402007 Dup Parameter Units Result Result RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 1,1,1-Trichloroethane ug/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 78 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 SAMPLE DUPLICATE: 2437001 Parameter Units 92408402007 Result Dup Result 1,1,2,2-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,2,3-Trichloropropane ug/L ND ND 1,2-Dibromo-3-chloropropane ug/L ND ND 1,2-Dibromoethane (EDB) ug/L ND ND 1,2-Dichlorobenzene ug/L ND ND 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND ND 1,4-Dichlorobenzene ug/L ND ND 2-Butanone (MEK) ug/L 12.2 12.8 2-Hexanone ug/L ND 0.56J 4-Methyl-2-pentanone (MIBK) ug/L ND 1.3J Acetone ug/L 82.9 85.7 Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND 0.18J cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Dichlorodifluoromethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND m&p-Xylene ug/L ND ND Methylene Chloride ug/L ND ND o-Xylene ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Tetrahydrofuran ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND RPD Qualifiers 5 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 79 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 SAMPLE DUPLICATE: 2437001 92408402007 Dup Parameter Units Result Result RPD Qualifiers Vinyl chloride ug/L ND ND 1,2-Dichloroethane-d4 (S) % 106 105 0 4-Bromofluorobenzene (S) % 99 97 2 Toluene-d8 (S) % 98 97 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 80 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444286 Analysis Method: EPA 8260B QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill Associated Lab Samples: 92408417011, 92408417012, 92408417013, 92408417016, 92408417017, 92408417018, 92408417019, 92408417020 METHOD BLANK: 2437012 Matrix: Water Associated Lab Samples: 92408417011, 92408417012, 92408417013, 92408417016, 92408417017, 92408417018, 92408417019, 92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 11/27/18 18:23 1,1,1-Trichloroethane ug/L ND 1.0 11/27/18 18:23 1,1,2,2-Tetrachloroethane ug/L ND 1.0 11/27/18 18:23 1,1,2-Trichloroethane ug/L ND 1.0 11/27/18 18:23 1,1-Dichloroethane ug/L ND 1.0 11/27/18 18:23 1,1-Dichloroethene ug/L ND 1.0 11/27/18 18:23 1,2,3-Trichloropropane ug/L ND 1.0 11/27/18 18:23 1,2-Dibromo-3-chloropropane ug/L ND 2.0 11/27/18 18:23 1,2-Dibromoethane (EDB) ug/L ND 1.0 11/27/18 18:23 1,2-Dichlorobenzene ug/L ND 1.0 11/27/18 18:23 1,2-Dichloroethane ug/L ND 1.0 11/27/18 18:23 1,2-Dichloropropane ug/L ND 1.0 11/27/18 18:23 1,4-Dichlorobenzene ug/L ND 1.0 11/27/18 18:23 2-Butanone (MEK) ug/L ND 5.0 11/27/18 18:23 2-Hexanone ug/L ND 5.0 11/27/18 18:23 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 11/27/18 18:23 Acetone ug/L ND 25.0 11/27/18 18:23 Acrylonitrile ug/L ND 10.0 11/27/18 18:23 Benzene ug/L ND 1.0 11/27/18 18:23 Bromochloromethane ug/L ND 1.0 11/27/18 18:23 Bromodichloromethane ug/L ND 1.0 11/27/18 18:23 Bromoform ug/L ND 1.0 11/27/18 18:23 Bromomethane ug/L ND 2.0 11/27/18 18:23 Carbon disulfide ug/L ND 2.0 11/27/18 18:23 Carbon tetrachloride ug/L ND 1.0 11/27/18 18:23 Chlorobenzene ug/L ND 1.0 11/27/18 18:23 Chloroethane ug/L ND 1.0 11/27/18 18:23 Chloroform ug/L ND 1.0 11/27/18 18:23 Chloromethane ug/L ND 1.0 11/27/18 18:23 cis-1,2-Dichloroethene ug/L ND 1.0 11/27/18 18:23 cis-1,3-Dichloropropene ug/L ND 1.0 11/27/18 18:23 Dibromochloromethane ug/L ND 1.0 11/27/18 18:23 Dibromomethane ug/L ND 1.0 11/27/18 18:23 Dichlorodifluoromethane ug/L ND 1.0 11/27/18 18:23 Ethylbenzene ug/L ND 1.0 11/27/18 18:23 lodomethane ug/L ND 5.0 11/27/18 18:23 m&p-Xylene ug/L ND 2.0 11/27/18 18:23 Methylene Chloride ug/L ND 1.0 11/27/18 18:23 o-Xylene ug/L ND 1.0 11/27/18 18:23 Styrene ug/L ND 1.0 11/27/18 18:23 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 81 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 METHOD BLANK: 2437012 Matrix: Water Associated Lab Samples: 92408417011, 92408417012, 92408417013, 92408417016, 92408417017, 92408417018, 92408417019, 92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Tetrachloroethene ug/L ND 1.0 11/27/18 18:23 Tetrahydrofuran ug/L ND 10.0 11/27/18 18:23 Toluene ug/L ND 1.0 11/27/18 18:23 trans-1,2-Dichloroethene ug/L ND 1.0 11/27/18 18:23 trans- 1,3-Dichloropropene ug/L ND 1.0 11/27/18 18:23 trans-1,4-Dichloro-2-butene ug/L ND 1.0 11/27/18 18:23 Trichloroethene ug/L ND 1.0 11/27/18 18:23 Trichlorofluoromethane ug/L ND 1.0 11/27/18 18:23 Vinyl acetate ug/L ND 2.0 11/27/18 18:23 Vinyl chloride ug/L ND 1.0 11/27/18 18:23 1,2-Dichloroethane-d4 (S) % 101 70-130 11/27/18 18:23 4-Bromofluorobenzene (S) % 97 70-130 11/27/18 18:23 Toluene-d8 (S) % 98 70-130 11/27/18 18:23 LABORATORY CONTROL SAMPLE: Parameter 2437013 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 49.3 99 70-130 1,1,1-Trichloroethane ug/L 50 46.4 93 70-130 1,1,2,2-Tetrachloroethane ug/L 50 46.1 92 70-130 1,1,2-Trichloroethane ug/L 50 48.1 96 70-130 1,1-Dichloroethane ug/L 50 44.6 89 70-130 1,1-Dichloroethene ug/L 50 46.3 93 70-130 1,2,3-Trichloropropane ug/L 50 48.6 97 70-130 1,2-Dibromo-3-chloropropane ug/L 50 49.3 99 70-130 1,2-Dibromoethane (EDB) ug/L 50 48.3 97 70-130 1,2-Dichlorobenzene ug/L 50 47.8 96 70-130 1,2-Dichloroethane ug/L 50 45.9 92 70-130 1,2-Dichloropropane ug/L 50 46.0 92 70-130 1,4-Dichlorobenzene ug/L 50 47.1 94 70-130 2-Butanone (MEK) ug/L 100 100 100 64-135 2-Hexanone ug/L 100 106 106 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 70-130 Acetone ug/L 100 103 103 61-157 Acrylonitrile ug/L 250 242 97 61-143 Benzene ug/L 50 46.2 92 70-130 Bromochloromethane ug/L 50 48.2 96 70-130 Bromodichloromethane ug/L 50 49.9 100 70-130 Bromoform ug/L 50 47.8 96 70-130 Bromomethane ug/L 50 59.4 119 38-128 Carbon disulfide ug/L 50 42.7 85 68-130 Carbon tetrachloride ug/L 50 48.3 97 70-130 Chlorobenzene ug/L 50 47.4 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 82 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 LABORATORY CONTROL SAMPLE: 2437013 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloroethane ug/L 50 43.5 87 37-142 Chloroform ug/L 50 45.9 92 70-130 Chloromethane ug/L 50 41.0 82 48-120 cis-1,2-Dichloroethene ug/L 50 45.5 91 70-130 cis-1,3-Dichloropropene ug/L 50 47.6 95 70-130 Dibromochloromethane ug/L 50 50.5 101 70-130 Dibromomethane ug/L 50 50.2 100 70-130 Dichlorodifluoromethane ug/L 50 33.3 67 53-134 Ethylbenzene ug/L 50 46.8 94 70-130 lodomethane ug/L 100 99.6 100 40-124 m&p-Xylene ug/L 100 96.2 96 70-130 Methylene Chloride ug/L 50 47.9 96 67-132 o-Xylene ug/L 50 48.0 96 70-130 Styrene ug/L 50 47.4 95 70-130 Tetrachloroethene ug/L 50 44.9 90 69-130 Tetrahydrofuran ug/L 500 503 101 62-128 Toluene ug/L 50 46.1 92 70-130 trans-1,2-Dichloroethene ug/L 50 45.4 91 70-130 trans- 1,3-Dichloropropene ug/L 50 48.2 96 70-130 trans-1,4-Dichloro-2-butene ug/L 50 63.1 126 35-189 Trichloroethene ug/L 50 46.6 93 70-130 Trichlorofluoromethane ug/L 50 45.6 91 63-126 Vinyl acetate ug/L 100 98.5 98 55-143 Vinyl chloride ug/L 50 40.4 81 70-131 1,2-Dichloroethane-d4 (S) % 104 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 99 70-130 MATRIX SPIKE SAMPLE: 2437014 92408417019 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 21.4 107 73-134 1,1,1-Trichloroethane ug/L ND 20 21.4 107 82-143 1,1,2,2-Tetrachloroethane ug/L ND 20 20.8 104 70-136 1,1,2-Trichloroethane ug/L ND 20 21.4 107 70-135 1,1-Dichloroethane ug/L 1.3 20 22.3 105 72-139 1,1-Dichloroethene ug/L ND 20 21.8 109 81-154 1,2,3-Trichloropropane ug/L ND 20 20.7 104 71-137 1,2-Dibromo-3-chloropropane ug/L ND 20 21.6 108 65-134 1,2-Dibromoethane (EDB) ug/L ND 20 21.5 108 72-137 1,2-Dichlorobenzene ug/L ND 20 20.5 103 70-133 1,2-Dichloroethane ug/L ND 20 21.6 108 73-137 1,2-Dichloropropane ug/L ND 20 20.3 101 79-140 1,4-Dichlorobenzene ug/L ND 20 21.5 108 70-133 2-Butanone (MEK) ug/L ND 40 44.7 112 60-139 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 83 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 MATRIX SPIKE SAMPLE: 2437014 92408417019 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 2-Hexanone ug/L ND 40 44.5 111 65-138 4-Methyl-2-pentanone (MIBK) ug/L ND 40 46.5 116 65-135 Acetone ug/L ND 40 47.4 118 60-148 Acrylonitrile ug/L ND 100 105 105 64-147 Benzene ug/L 0.37J 20 21.4 105 72-151 Bromochloromethane ug/L ND 20 22.6 113 77-141 Bromodichloromethane ug/L ND 20 21.2 106 76-138 Bromoform ug/L ND 20 20.5 103 63-130 Bromomethane ug/L ND 20 17.6 88 15-152 Carbon disulfide ug/L ND 20 19.4 97 69-149 Carbon tetrachloride ug/L ND 20 22.8 114 70-143 Chlorobenzene ug/L ND 20 21.6 108 70-138 Chloroethane ug/L ND 20 22.3 112 52-163 Chloroform ug/L ND 20 21.3 106 74-139 Chloromethane ug/L ND 20 18.0 90 41-139 cis-1,2-Dichloroethene ug/L 0.86J 20 21.5 103 77-141 cis-1,3-Dichloropropene ug/L ND 20 19.8 99 74-137 Dibromochloromethane ug/L ND 20 21.2 106 70-134 Dibromomethane ug/L ND 20 22.6 113 76-138 Dichlorodifluoromethane ug/L ND 20 17.5 88 47-155 Ethylbenzene ug/L ND 20 21.3 106 66-153 lodomethane ug/L ND 40 38.4 96 20-138 m&p-Xylene ug/L 1.11 40 44.4 108 69-152 Methylene Chloride ug/L 5.7 20 26.5 104 42-159 o-Xylene ug/L 0.591 20 21.6 105 73-148 Styrene ug/L ND 20 21.0 105 70-135 Tetrachloroethene ug/L ND 20 21.3 106 59-143 Tetrahydrofuran ug/L 50.5 200 269 109 70-133 Toluene ug/L ND 20 20.2 101 59-148 trans-1,2-Dichloroethene ug/L ND 20 21.3 107 76-146 trans- 1,3-Dichloropropene ug/L ND 20 20.8 104 71-135 trans-1,4-Dichloro-2-butene ug/L ND 20 22.4 112 47-135 Trichloroethene ug/L ND 20 21.7 109 77-147 Trichlorofluoromethane ug/L 1.2 20 24.1 115 76-148 Vinyl acetate ug/L ND 40 37.1 93 49-151 Vinyl chloride ug/L ND 20 19.1 96 70-156 1,2-Dichloroethane-d4 (S) % 107 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8 (S) % 99 70-130 SAMPLE DUPLICATE: 2437015 92408417020 Dup Parameter Units Result Result RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 1,1,1-Trichloroethane ug/L ND ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 84 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 SAMPLE DUPLICATE: 2437015 Parameter Units 92408417020 Result Dup Result 1,1,2,2-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,2,3-Trichloropropane ug/L ND ND 1,2-Dibromo-3-chloropropane ug/L ND ND 1,2-Dibromoethane (EDB) ug/L ND ND 1,2-Dichlorobenzene ug/L ND ND 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND ND 1,4-Dichlorobenzene ug/L ND ND 2-Butanone (MEK) ug/L ND ND 2-Hexanone ug/L ND ND 4-Methyl-2-pentanone (MIBK) ug/L ND ND Acetone ug/L ND ND Acrylonitrile ug/L ND ND Benzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon disulfide ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Dichlorodifluoromethane ug/L ND ND Ethylbenzene ug/L ND ND lodomethane ug/L ND ND m&p-Xylene ug/L ND ND Methylene Chloride ug/L ND ND o-Xylene ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Tetrahydrofuran ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans- 1,3-Dichloropropene ug/L ND ND trans-1,4-Dichloro-2-butene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND RPD Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 85 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 SAMPLE DUPLICATE: 2437015 92408417020 Dup Parameter Units Result Result RPD Qualifiers Vinyl chloride ug/L ND ND 1,2-Dichloroethane-d4 (S) % 106 107 2 4-Bromofluorobenzene (S) % 95 95 0 Toluene-d8 (S) % 97 97 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 86 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444962 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009 METHOD BLANK: 2439583 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 11/30/18 18:12 1,2-Dichloroethane-d4 (S) % 103 50-150 11/30/18 18:12 Toluene-d8 (S) % 105 50-150 11/30/18 18:12 LABORATORY CONTROL SAMPLE: 2439584 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 17.5 87 71-125 1,2-Dichloroethane-d4 (S) % 104 50-150 Toluene-d8 (S) % 105 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439585 2439586 MS MSD 92408402001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 18.0 18.5 90 92 50-150 3 1,2-Dichloroethane-d4 (S) % 103 101 50-150 Toluene-d8(S) % 103 105 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 87 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444963 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 92408417010, 92408417012, 92408417013, 92408417014, 92408417015 METHOD BLANK: 2439593 Matrix: Water Associated Lab Samples: 92408417010, 92408417012, 92408417013, 92408417014, 92408417015 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 11/30/18 17:53 1,2-Dichloroethane-d4 (S) % 102 50-150 11/30/18 17:53 Toluene-d8 (S) % 105 50-150 11/30/18 17:53 LABORATORY CONTROL SAMPLE: 2439594 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 18.3 92 71-125 1,2-Dichloroethane-d4 (S) % 102 50-150 Toluene-d8(S) % 105 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439595 2439596 MS MSD 92408410001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 40 40 35.9 35.5 90 89 50-150 1 1,2-Dichloroethane-d4 (S) % 98 98 50-150 Toluene-d8(S) % 104 103 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 88 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 445241 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 92408417011, 92408417016, 92408417017, 92408417019, 92408417020, 92408417021 METHOD BLANK: 2441278 Matrix: Water Associated Lab Samples: 92408417011, 92408417016, 92408417017, 92408417019, 92408417020, 92408417021 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 12/03/18 12:07 1,2-Dichloroethane-d4 (S) % 99 50-150 12/03/18 12:07 Toluene-d8 (S) % 106 50-150 12/03/18 12:07 LABORATORY CONTROL SAMPLE: 2441279 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.1 95 71-125 1,2-Dichloroethane-d4 (S) % 97 50-150 Toluene-d8(S) % 103 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2441280 2441281 MS MSD 92408417011 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 18.9 19.5 91 93 50-150 3 1,2-Dichloroethane-d4 (S) % 104 104 50-150 Toluene-d8(S) % 108 108 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 89 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 445243 Analysis Method: EPA 8260B Mod. QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM Associated Lab Samples: 92408417018 METHOD BLANK: 2441286 Associated Lab Samples: 92408417018 Parameter Units 1,4-Dioxane (p-Dioxane) ug/L 1,2-Dichloroethane-d4 (S) % Toluene-d8 (S) % Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 12/03/1811:47 95 50-150 12/03/1811:47 104 50-150 12/03/1811:47 LABORATORY CONTROL SAMPLE: 2441287 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 16.4 82 71-125 1,2-Dichloroethane-d4 (S) % 103 50-150 Toluene-d8(S) % 105 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2441288 2441289 MS MSD 92408417018 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 17.4 17.7 83 85 50-150 2 1,2-Dichloroethane-d4 (S) % 102 105 50-150 Toluene-d8(S) % 108 110 50-150 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 90 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444391 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Associated Lab Samples: 92408417010, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017, 92408417019 METHOD BLANK: 2437288 Matrix: Water Associated Lab Samples: 92408417010, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017, 92408417019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 4,4'-DDD ug/L ND 0.050 11/30/18 16:58 4,4'-DDT ug/L ND 0.050 11/30/18 16:58 Aldrin ug/L ND 0.050 11/30/18 16:58 alpha-BHC ug/L ND 0.050 11/30/18 16:58 delta-BHC ug/L ND 0.050 11/30/18 16:58 Endosulfan I ug/L ND 0.050 11/30/18 16:58 Endosulfan 11 ug/L ND 0.050 11/30/18 16:58 Endrin ug/L ND 0.050 11/30/18 16:58 Endrin aldehyde ug/L ND 0.050 11/30/18 16:58 Heptachlor ug/L ND 0.050 11/30/18 16:58 Heptachlor epoxide ug/L ND 0.050 11/30/18 16:58 Methoxychlor ug/L ND 0.15 11/30/18 16:58 Decachlorobiphenyl (S) % 85 10-130 11/30/18 16:58 Tetrachloro-m-xylene (S) % 70 10-130 11/30/18 16:58 LABORATORY CONTROL SAMPLE: Parameter 2437289 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 4,4'-DDD ug/L 0.25 0.21 85 49-130 4,4'-DDT ug/L 0.25 0.25 99 45-130 Aldrin ug/L 0.25 0.20 78 25-130 alpha-BHC ug/L 0.25 0.20 81 53-130 delta-BHC ug/L 0.25 0.20 81 54-130 Endosulfan I ug/L 0.25 0.23 94 43-130 Endosulfan II ug/L 0.25 0.21 86 64-130 Endrin ug/L 0.25 0.21 86 56-130 Endrin aldehyde ug/L 0.25 0.24 97 59-130 Heptachlor ug/L 0.25 0.22 89 37-130 Heptachlor epoxide ug/L 0.25 0.21 84 56-130 Methoxychlor ug/L 0.75 0.76 101 46-130 Decachlorobiphenyl (S) % 89 10-130 Tetrachloro-m-xylene (S) % 72 10-130 1•r_�r:�►�y�1:��.9�t•1»�zS�f��Z�l 92408417012 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 4,4'-DDD ug/L ND 0.25 0.20 80 28-130 4,4'-DDT ug/L ND 0.25 0.28 112 11-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 91 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 MATRIX SPIKE SAMPLE: Parameter 2437290 Units 92408417012 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers Aldrin ug/L ND 0.25 0.19 75 10-130 alpha-BHC ug/L ND 0.25 0.21 84 27-130 delta-BHC ug/L ND 0.25 0.21 83 44-130 Endosulfan I ug/L ND 0.25 0.22 89 10-139 Endosulfan II ug/L ND 0.25 0.24 97 36-130 Endrin ug/L ND 0.25 0.21 86 26-130 Endrin aldehyde ug/L ND 0.25 0.22 90 19-160 Heptachlor ug/L ND 0.25 0.21 83 25-130 Heptachlor epoxide ug/L ND 0.25 0.19 76 18-130 Methoxychlor ug/L ND 0.75 0.69 92 10-130 Decachlorobiphenyl (S) % 126 10-130 Tetrachloro-m-xylene (S) % 78 10-130 SAMPLE DUPLICATE: 2437291 Parameter Units 92408417013 Result Dup Result RPD Qualifiers 4,4'-DDD ug/L ND ND 4,4'-DDT ug/L ND ND Aldrin ug/L ND ND alpha-BHC ug/L ND ND delta-BHC ug/L ND ND Endosulfan I ug/L ND ND Endosulfan II ug/L ND ND Endrin ug/L ND ND Endrin aldehyde ug/L ND ND Heptachlor ug/L ND ND Heptachlor epoxide ug/L ND ND Methoxychlor ug/L ND ND Decachlorobiphenyl (S) % 242 229 5 S5 Tetrachloro-m-xylene (S) % 86 84 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 92 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444238 Analysis Method: EPA 8270D QC Batch Method: EPA 3510C Analysis Description: 8270 Water MSSV RVE Associated Lab Samples: 92408417011, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017 METHOD BLANK: 2436738 Matrix: Water Associated Lab Samples: 92408417011, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 11/28/18 13:24 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 11/28/18 13:24 Chrysene ug/L ND 10.0 11/28/18 13:24 Dibenz(a,h)anthracene ug/L ND 10.0 11/28/18 13:24 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 11/28/18 13:24 2,4,6-Tribromophenol (S) % 69 10-137 11/28/18 13:24 2-Fluorobiphenyl (S) % 58 13-130 11/28/18 13:24 2-Fluorophenol (S) % 58 10-130 11/28/18 13:24 Nitrobenzene-d5 (S) % 67 13-130 11/28/18 13:24 Phenol-d6 (S) % 49 10-130 11/28/18 13:24 Terphenyl-d14 (S) % 67 25-130 11/28/18 13:24 LABORATORY CONTROL SAMPLE: 2436739 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 39.7 79 50-130 bis(2-Ethylhexyl)phthalate ug/L 50 41.7 83 50-130 Chrysene ug/L 50 39.2 78 50-130 Dibenz(a,h)anthracene ug/L 50 43.8 88 40-130 Indeno(1,2,3-cd)pyrene ug/L 50 43.2 86 40-130 2,4,6-Tribromophenol (S) % 78 10-137 2-Fluorobiphenyl (S) % 61 13-130 2-Fluorophenol (S) % 58 10-130 Nitrobenzene-d5 (S) % 68 13-130 Phenol-d6 (S) % 52 10-130 Terphenyl-d14 (S) % 67 25-130 MATRIX SPIKE SAMPLE: 2436740 92408417012 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L ND 50 42.2 84 50-130 bis(2-Ethylhexyl)phthalate ug/L ND 50 43.6 87 50-130 Chrysene ug/L ND 50 41.7 83 50-130 Dibenz(a,h)anthracene ug/L ND 50 46.9 94 40-130 Indeno(1,2,3-cd)pyrene ug/L ND 50 45.7 91 40-130 2,4,6-Tribromophenol (S) % 83 10-137 2-Fluorobiphenyl (S) % 63 13-130 2-Fluorophenol(S) % 60 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 93 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 MATRIX SPIKE SAMPLE: 2436740 92408417012 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrobenzene-d5 (S) % 72 13-130 Phenol-d6 (S) % 53 10-130 Terphenyl-d14 (S) % 67 25-130 SAMPLE DUPLICATE: 2436741 92408417013 Dup Parameter Units Result Result RPD Qualifiers Benzo(a)anthracene ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Chrysene ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Indeno(1,2,3-cd)pyrene ug/L ND ND 2,4,6-Tribromophenol (S) % 77 77 1 2-Fluorobiphenyl (S) % 57 59 4 2-Fluorophenol (S) % 55 56 2 Nitrobenzene-d5 (S) % 66 66 1 Phenol-d6 (S) % 50 50 1 Terphenyl-d14 (S) % 66 62 6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 94 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 446768 Analysis Method: EPA 8270D QC Batch Method: EPA 351 OC Analysis Description: 8270 Water MSSV RVE Associated Lab Samples: 92408417022 METHOD BLANK: 2448629 Matrix: Water Associated Lab Samples: 92408417022 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 12/13/18 10:39 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 12/13/18 10:39 Chrysene ug/L ND 10.0 12/13/18 10:39 Dibenz(a,h)anthracene ug/L ND 10.0 12/13/18 10:39 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 12/13/18 10:39 2,4,6-Tribromophenol (S) % 58 10-137 12/13/18 10:39 2-Fluorobiphenyl (S) % 53 13-130 12/13/18 10:39 2-Fluorophenol (S) % 51 10-130 12/13/18 10:39 Nitrobenzene-d5 (S) % 55 13-130 12/13/18 10:39 Phenol-d6 (S) % 44 10-130 12/13/18 10:39 Terphenyl-d14 (S) % 78 25-130 12/13/18 10:39 LABORATORY CONTROL SAMPLE: 2448630 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 43.2 86 50-130 bis(2-Ethylhexyl)phthalate ug/L 50 39.2 78 50-130 Chrysene ug/L 50 44.1 88 50-130 Dibenz(a,h)anthracene ug/L 50 49.0 98 40-130 Indeno(1,2,3-cd)pyrene ug/L 50 47.8 96 40-130 2,4,6-Tribromophenol (S) % 79 10-137 2-Fluorobiphenyl (S) % 60 13-130 2-Fluorophenol (S) % 60 10-130 Nitrobenzene-d5 (S) % 65 13-130 Phenol-d6 (S) % 56 10-130 Terphenyl-d14 (S) % 75 25-130 MATRIX SPIKE SAMPLE: 2448631 92410046001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L ND 50 39.5 79 50-130 bis(2-Ethylhexyl)phthalate ug/L ND 50 35.7 71 50-130 Chrysene ug/L ND 50 40.1 80 50-130 Dibenz(a,h)anthracene ug/L ND 50 42.1 84 40-130 Indeno(1,2,3-cd)pyrene ug/L ND 50 41.3 83 40-130 2,4,6-Tribromophenol (S) % 2 10-137 SO 2-Fluorobiphenyl (S) % 42 13-130 2-Fluorophenol(S) % 1 10-130 SO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 95 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 MATRIX SPIKE SAMPLE: 2448631 92410046001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Nitrobenzene-d5 (S) % 46 13-130 Phenol-d6 (S) % 8 10-130 SO Terphenyl-d14 (S) % 72 25-130 SAMPLE DUPLICATE: 2448632 92410057002 Dup Parameter Units Result Result RPD Qualifiers Benzo(a)anthracene ug/L ND ND bis(2-Ethylhexyl)phthalate ug/L ND ND Chrysene ug/L ND ND Dibenz(a,h)anthracene ug/L ND ND Indeno(1,2,3-cd)pyrene ug/L ND ND 2,4,6-Tribromophenol (S) % 69 54 24 2-Fluorobiphenyl (S) % 66 51 26 2-Fluorophenol(S) % 61 44 32 Nitrobenzene-d5 (S) % 71 53 29 Phenol-d6 (S) % 57 41 33 Terphenyl-d14 (S) % 82 68 18 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 96 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444412 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Associated Lab Samples: 92408417001, 92408417002 METHOD BLANK: 2437373 Matrix: Water Associated Lab Samples: 92408417001, 92408417002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 11/28/18 15:41 LABORATORY CONTROL SAMPLE: 2437374 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 51000 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437375 2437376 MS MSD 92408543001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 31.3 50000 50000 82100 81800 102 101 80-120 0 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437770 2437771 MS MSD 92408413007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 69.8 50000 50000 123000 122000 106 104 80-120 1 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 97 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444413 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Associated Lab Samples: 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008, 92408417009, 92408417010,92408417011,92408417012,92408417013,92408417014,92408417016,92408417017, 92408417018,92408417019,92408417020 METHOD BLANK: 2437379 Matrix: Water Associated Lab Samples: 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008, 92408417009, 92408417010,92408417011,92408417012,92408417013,92408417014,92408417016,92408417017, 92408417018,92408417019,92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 11/28/18 18:48 LABORATORY CONTROL SAMPLE: 2437380 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 51300 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437381 2437382 MS MSD 92408417003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 67100 50000 50000 120000 121000 106 108 80-120 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437383 2437384 MS MSD 92408417013 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Alkalinity, Total as CaCO3 ug/L 573000 50000 50000 587000 603000 28 61 80-120 3 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 98 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444490 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008 METHOD BLANK: 2437735 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 11/28/18 15:13 LABORATORY CONTROL SAMPLE: 2437736 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 248000 99 90-110 SAMPLE DUPLICATE: 2437738 92408554002 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids ug/L 125 mg/L 120000 4 SAMPLE DUPLICATE: 2438176 92408543001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids ug/L 79.0 mg/L 77000 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 99 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444602 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Associated Lab Samples: 92408417009, 92408417010, 92408417011, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017,92408417018,92408417019,92408417020 METHOD BLANK: 2438224 Matrix: Water Associated Lab Samples: 92408417009, 92408417010, 92408417011, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017,92408417018,92408417019,92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 11/29/18 01:14 LABORATORY CONTROL SAMPLE: 2438225 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 246000 98 90-110 SAMPLE DUPLICATE: 2438226 92408417009 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids ug/L 236000 239000 1 SAMPLE DUPLICATE: 2438227 92408417019 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids ug/L 171000 163000 5 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 100 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444804 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013,92408417014, 92408417016,92408417017,92408417018,92408417019 METHOD BLANK: 2439095 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013,92408417014, 92408417016,92408417017,92408417018,92408417019 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 100 11/29/1818:53 LABORATORY CONTROL SAMPLE: 2439096 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 507 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439097 2439098 MS MSD 92408417001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 520 552 103 109 80-120 6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439099 2439100 MS MSD 92408413007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 534 546 106 109 80-120 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 101 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444805 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Associated Lab Samples: 92408417020 METHOD BLANK: 2439101 Matrix: Water Associated Lab Samples: 92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfide ug/L ND 100 11/29/1819:15 LABORATORY CONTROL SAMPLE: 2439102 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 536 107 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439103 2439104 MS MSD 92408417020 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 546 558 108 111 80-120 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2439105 2439106 MS MSD 92408731008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfide ug/L ND 500 500 563 573 112 114 80-120 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 102 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444332 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92408417001, 92408417002, 92408417003 METHOD BLANK: 2437139 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 1000 11/28/1812:45 LABORATORY CONTROL SAMPLE: 2437140 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 52800 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437141 2437142 MS MSD 92408543001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate ug/L 3.4 50000 50000 55000 54000 103 101 90-110 2 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437143 2437144 MS MSD 92408568001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate ug/L 2.8 50000 50000 53700 53700 102 102 90-110 0 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 103 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444333 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Associated Lab Samples: 92408417004, 92408417005, 92408417006, 92408417007, 92408417008, 92408417009, 92408417010, 92408417011,92408417012,92408417013,92408417014,92408417016,92408417017,92408417018, 92408417019,92408417020 METHOD BLANK: 2437145 Matrix: Water Associated Lab Samples: 92408417004, 92408417005, 92408417006, 92408417007, 92408417008, 92408417009, 92408417010, 92408417011,92408417012,92408417013,92408417014,92408417016,92408417017,92408417018, 92408417019,92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Sulfate ug/L ND 1000 11/28/1822:01 LABORATORY CONTROL SAMPLE: 2437146 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 54500 109 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437147 2437148 MS MSD 92408417004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate ug/L 20700 50000 50000 73600 73800 106 106 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437149 2437150 MS MSD 92408417014 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Sulfate ug/L ND 50000 50000 52500 52900 105 106 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 104 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 445157 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008 METHOD BLANK: 2440904 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 12/02/1816:40 LABORATORY CONTROL SAMPLE: 2440905 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 19400 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2440906 2440907 MS MSD 92408294004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 29.4 10000 10000 38900 38900 96 95 90-110 0 mg/L MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2440908 2440909 MS MSD 92408943002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 131 10000 10000 132000 133000 12 22 90-110 1 M6 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 105 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 445158 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Associated Lab Samples: 92408417009, 92408417010, 92408417011, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017,92408417018,92408417019,92408417020 METHOD BLANK: 2440910 Matrix: Water Associated Lab Samples: 92408417009, 92408417010, 92408417011, 92408417012, 92408417013, 92408417014, 92408417016, 92408417017,92408417018,92408417019,92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride ug/L ND 1000 12/02/1817:25 LABORATORY CONTROL SAMPLE: 2440911 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 19900 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2440912 2440913 MS MSD 92408417009 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 24800 10000 10000 34400 34200 96 94 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2440914 2440915 MS MSD 92408417020 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride ug/L 15100 10000 10000 25100 25100 100 100 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 106 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444379 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013 METHOD BLANK: 2437258 Matrix: Water Associated Lab Samples: 92408417001, 92408417002, 92408417003, 92408417004, 92408417005, 92408417006, 92408417007, 92408417008,92408417009,92408417010,92408417011,92408417012,92408417013 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 8.0 11/29/18 09:18 LABORATORY CONTROL SAMPLE: 2437259 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 109 109 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437260 2437261 MS MSD 92407809001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L ND 100 100 96.8 101 92 97 80-120 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437262 2437263 MS MSD 92408291004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L 0.0044J 100 100 112 110 108 106 80-120 2 mg/L Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 107 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR Pace Project No.: 92408417 QC Batch: 444381 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Associated Lab Samples: 92408417014, 92408417016, 92408417017, 92408417018, 92408417019, 92408417020 METHOD BLANK: 2437264 Matrix: Water Associated Lab Samples: 92408417014, 92408417016, 92408417017, 92408417018, 92408417019, 92408417020 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Cyanide ug/L ND 8.0 11/29/18 09:43 LABORATORY CONTROL SAMPLE: 2437265 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 106 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2437266 2437267 MS MSD 92408417014 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Cyanide ug/L ND 100 100 107 108 103 104 80-120 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 108 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: OSR Pace Project No.: 92408417 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. SO Surrogate recovery outside laboratory control limits. S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis). REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 109 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR Pace Project No.: 92408417 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92408417010 MW-10 EPA 3510C 444391 EPA 8081 B 445013 92408417012 MW-4R EPA 3510C 444391 EPA 8081 B 445013 92408417013 MW-2R EPA 3510C 444391 EPA 8081 B 445013 92408417014 EQUIPMENT BLANK EPA 3510C 444391 EPA 8081 B 445013 92408417016 MWA R EPA 3510C 444391 EPA 8081 B 445013 92408417017 MW-15 EPA 3510C 444391 EPA 8081 B 445013 92408417019 MW-7 EPA 3510C 444391 EPA 8081 B 445013 92408417001 MW-8 EPA 3010A 444350 EPA 6010D 444632 92408417002 MW-9 EPA 3010A 444350 EPA 6010D 444632 92408417003 MW-14 EPA 3010A 444350 EPA 6010D 444632 92408417004 MW-11 EPA 3010A 444350 EPA 6010D 444632 92408417005 MW-12 EPA 3010A 444350 EPA 6010D 444632 92408417006 MW-13 EPA 3010A 444350 EPA 6010D 444632 92408417007 SW-1 EPA 3010A 444350 EPA 6010D 444632 92408417008 SW-3 EPA 3010A 444350 EPA 6010D 444632 92408417009 SW-4 EPA 3010A 444350 EPA 6010D 444632 92408417010 MW-10 EPA 3010A 444350 EPA 6010D 444632 92408417011 SW-2 EPA 3010A 444350 EPA 6010D 444632 92408417012 MW-411 EPA 3010A 444350 EPA 6010D 444632 92408417013 MW-2R EPA 3010A 444350 EPA 6010D 444632 92408417014 EQUIPMENT BLANK EPA 3010A 444350 EPA6010D 444632 92408417016 MWA R EPA 3010A 444350 EPA 6010D 444632 92408417017 MW-15 EPA 3010A 444350 EPA 6010D 444632 92408417018 MW-311 EPA 3010A 444350 EPA 6010D 444632 92408417019 MW-7 EPA 3010A 444350 EPA 6010D 444632 92408417020 MW-5R EPA 3010A 444350 EPA 6010D 444632 92408417001 MW-8 EPA 7470A 444850 EPA 7470A 444862 92408417002 MW-9 EPA 7470A 444850 EPA 7470A 444862 92408417003 MW-14 EPA 7470A 444850 EPA 7470A 444862 92408417004 MW-11 EPA 7470A 444850 EPA 7470A 444862 92408417005 MW-12 EPA 7470A 444850 EPA 7470A 444862 92408417006 MW-13 EPA 7470A 444850 EPA 7470A 444862 92408417007 SW-1 EPA 7470A 444850 EPA 7470A 444862 92408417008 SW-3 EPA 7470A 444850 EPA 7470A 444862 92408417009 SW-4 EPA 7470A 444850 EPA 7470A 444862 92408417010 MW-10 EPA 7470A 444850 EPA 7470A 444862 92408417011 SW-2 EPA 7470A 444850 EPA 7470A 444862 92408417012 MW-4R EPA 7470A 444850 EPA 7470A 444862 92408417013 MW-2R EPA 7470A 444850 EPA 7470A 444862 92408417014 EQUIPMENT BLANK EPA 7470A 444851 EPA 7470A 444863 92408417016 MWA R EPA 7470A 444851 EPA 7470A 444863 92408417017 MW-15 EPA 7470A 444851 EPA 7470A 444863 92408417018 MW-3R EPA 7470A 444851 EPA 7470A 444863 92408417019 MW-7 EPA 7470A 444851 EPA 7470A 444863 92408417020 MW-5R EPA 7470A 444851 EPA 7470A 444863 92408417011 SW-2 EPA 3510C 444238 EPA 8270D 444471 92408417012 MW-4R EPA 3510C 444238 EPA 8270D 444471 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 110 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR 92408417 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92408417013 MW-2R EPA 3510C 444238 EPA 8270D 444471 92408417014 EQUIPMENT BLANK EPA 3510C 444238 EPA 8270D 444471 92408417016 MWA R EPA 3510C 444238 EPA 8270D 444471 92408417017 MW-15 EPA 3510C 444238 EPA 8270D 444471 92408417022 MW-3R EPA 3510C 446768 EPA 8270D 447313 92408417001 MW-8 EPA 8260B 444283 92408417002 MW-9 EPA 8260B 444283 92408417003 MW-14 EPA 8260B 444283 92408417004 MW-11 EPA 8260B 444283 92408417005 MW-12 EPA 8260B 444283 92408417006 MW-13 EPA 8260B 444283 92408417007 SW-1 EPA 8260B 444283 92408417008 SW-3 EPA 8260B 444283 92408417009 SW-4 EPA 8260B 444283 92408417010 MW-10 EPA 8260B 444283 92408417011 SW-2 EPA 8260B 444286 92408417012 MW-4R EPA 8260B 444286 92408417013 MW-2R EPA 8260B 444286 92408417014 EQUIPMENT BLANK EPA 8260B 444283 92408417015 TRIP BLANK EPA 8260B 444283 92408417016 MWA R EPA 8260B 444286 92408417017 MW-15 EPA 8260B 444286 92408417018 MW-3R EPA 8260B 444286 92408417019 MW-7 EPA 8260B 444286 92408417020 MW-5R EPA 8260B 444286 92408417021 TRIP BLANK EPA 8260B 444283 92408417001 MW-8 EPA 8260B Mod. 444962 92408417002 MW-9 EPA 8260B Mod. 444962 92408417003 MW-14 EPA 8260B Mod. 444962 92408417004 MW-11 EPA 8260B Mod. 444962 92408417005 MW-12 EPA 8260B Mod. 444962 92408417006 MW-13 EPA 8260B Mod. 444962 92408417007 SW-1 EPA 8260B Mod. 444962 92408417008 SW-3 EPA 8260B Mod. 444962 92408417009 SW-4 EPA 8260B Mod. 444962 92408417010 MW-10 EPA 8260B Mod. 444963 92408417011 SW-2 EPA 8260B Mod. 445241 92408417012 MW-4R EPA 8260B Mod. 444963 92408417013 MW-2R EPA 8260B Mod. 444963 92408417014 EQUIPMENT BLANK EPA 8260B Mod. 444963 92408417015 TRIP BLANK EPA 8260B Mod. 444963 92408417016 MWA R EPA 8260B Mod. 445241 92408417017 MW-15 EPA 8260B Mod. 445241 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 111 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR 92408417 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92408417018 MW-3R EPA 8260B Mod. 445243 92408417019 MW-7 EPA 8260B Mod. 445241 92408417020 MW-5R EPA 8260B Mod. 445241 92408417021 TRIP BLANK EPA 8260B Mod. 445241 92408417001 MW-8 SM 2320B-2011 444412 92408417002 MW-9 SM 2320B-2011 444412 92408417003 MW-14 SM 2320B-2011 444413 92408417004 MW-11 SM 2320B-2011 444413 92408417005 MW-12 SM 2320B-2011 444413 92408417006 MW-13 SM 2320B-2011 444413 92408417007 SW-1 SM 2320E-2011 444413 92408417008 SW-3 SM 2320E-2011 444413 92408417009 SW-4 SM 2320E-2011 444413 92408417010 MW-10 SM 2320B-2011 444413 92408417011 SW-2 SM 2320E-2011 444413 92408417012 MW-4R SM 2320B-2011 444413 92408417013 MW-2R SM 2320B-2011 444413 92408417014 EQUIPMENT BLANK SM 2320B-2011 444413 92408417016 MWA R SM 2320E-2011 444413 92408417017 MW-15 SM 2320B-2011 444413 92408417018 MW-3R SM 2320B-2011 444413 92408417019 MW-7 SM 2320B-2011 444413 92408417020 MW-5R SM 2320B-2011 444413 92408417001 MW-8 SM 2540C-2011 444490 92408417002 MW-9 SM 2540C-2011 444490 92408417003 MW-14 SM 2540C-2011 444490 92408417004 MW-11 SM 2540C-2011 444490 92408417005 MW-12 SM 2540C-2011 444490 92408417006 MW-13 SM 2540C-2011 444490 92408417007 SW-1 SM 2540C-2011 444490 92408417008 SW-3 SM 2540C-2011 444490 92408417009 SW-4 SM 2540C-2011 444602 92408417010 MW-10 SM 2540C-2011 444602 92408417011 SW-2 SM 2540C-2011 444602 92408417012 MW-4R SM 2540C-2011 444602 92408417013 MW-2R SM 2540C-2011 444602 92408417014 EQUIPMENT BLANK SM 2540C-2011 444602 92408417016 MWA R SM 2540C-2011 444602 92408417017 MW-15 SM 2540C-2011 444602 92408417018 MW-3R SM 2540C-2011 444602 92408417019 MW-7 SM 2540C-2011 444602 92408417020 MW-5R SM 2540C-2011 444602 92408417001 MW-8 SM 4500-S2D-2011 444804 92408417002 MW-9 SM 4500-S2D-2011 444804 92408417003 MW-14 SM 4500-S2D-2011 444804 92408417004 MW-11 SM 4500-S2D-2011 444804 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 112 of 174 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR Pace Project No.: 92408417 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92408417005 MW-12 SM 4500-S2D-2011 444804 92408417006 MW-13 SM 4500-S2D-2011 444804 92408417007 SW-1 SM 4500-S2D-2011 444804 92408417008 SW-3 SM 4500-S2D-2011 444804 92408417009 SW-4 SM 4500-S2D-2011 444804 92408417010 MW-10 SM 4500-S2D-2011 444804 92408417011 SW-2 SM 4500-S2D-2011 444804 92408417012 MW-4R SM 4500-S2D-2011 444804 92408417013 MW-2R SM 4500-S2D-2011 444804 92408417014 EQUIPMENT BLANK SM 4500-S2D-2011 444804 92408417016 MW-1R SM 4500-S2D-2011 444804 92408417017 MW-15 SM 4500-S2D-2011 444804 92408417018 MW-3R SM 4500-S2D-2011 444804 92408417019 MW-7 SM 4500-S2D-2011 444804 92408417020 MW-5R SM 4500-S2D-2011 444805 92408417001 MW-8 EPA 300.0 Rev 2.1 1993 444332 92408417002 MW-9 EPA 300.0 Rev 2.1 1993 444332 92408417003 MW-14 EPA 300.0 Rev 2.1 1993 444332 92408417004 MW-11 EPA 300.0 Rev 2.1 1993 444333 92408417005 MW-12 EPA 300.0 Rev 2.1 1993 444333 92408417006 MW-13 EPA 300.0 Rev 2.1 1993 444333 92408417007 SW-1 EPA 300.0 Rev 2.1 1993 444333 92408417008 SW-3 EPA 300.0 Rev 2.1 1993 444333 92408417009 SW-4 EPA 300.0 Rev 2.1 1993 444333 92408417010 MW-10 EPA 300.0 Rev 2.1 1993 444333 92408417011 SW-2 EPA 300.0 Rev 2.1 1993 444333 92408417012 MW-4R EPA 300.0 Rev 2.1 1993 444333 92408417013 MW-2R EPA 300.0 Rev 2.1 1993 444333 92408417014 EQUIPMENT BLANK EPA 300.0 Rev 2.1 1993 444333 92408417016 MWA R EPA 300.0 Rev 2.1 1993 444333 92408417017 MW-15 EPA 300.0 Rev 2.1 1993 444333 92408417018 MW-3R EPA 300.0 Rev 2.1 1993 444333 92408417019 MW-7 EPA 300.0 Rev 2.1 1993 444333 92408417020 MW-5R EPA 300.0 Rev 2.1 1993 444333 92408417001 MW-8 SM 4500-CI-E-2011 445157 92408417002 MW-9 SM 4500-CI-E-2011 445157 92408417003 MW-14 SM 4500-CI-E-2011 445157 92408417004 MW-11 SM 4500-CI-E-2011 445157 92408417005 MW-12 SM 4500-CI-E-2011 445157 92408417006 MW-13 SM 4500-CI-E-2011 445157 92408417007 SW-1 SM 4500-CI-E-2011 445157 92408417008 SW-3 SM 4500-CI-E-2011 445157 92408417009 SW-4 SM 4500-CI-E-2011 445158 92408417010 MW-10 SM 4500-CI-E-2011 445158 92408417011 SW-2 SM 4500-CI-E-2011 445158 92408417012 MW-4R SM 4500-CI-E-2011 445158 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 12/14/2018 09:55 AM without the written consent of Pace Analytical Services, LLC. Page 113 of 174 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR Pace Project No.: 92408417 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92408417013 MW-2R SM 4500-CI-E-2011 445158 92408417014 EQUIPMENT BLANK SM 4500-CI-E-2011 445158 92408417016 MWA R SM 4500-CI-E-2011 445158 92408417017 MW-15 SM 4500-CI-E-2011 445158 92408417018 MW-3R SM 4500-CI-E-2011 445158 92408417019 MW-7 SM 4500-CI-E-2011 445158 92408417020 MW-5R SM 4500-CI-E-2011 445158 92408417001 MW-8 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417002 MW-9 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417003 MW-14 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417004 MW-11 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417005 MW-12 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417006 MW-13 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417007 SW-1 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417008 SW-3 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417009 SW-4 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417010 MW-10 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417011 SW-2 SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417012 MW-4R SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417013 MW-2R SM 4500-CN-E-2011 444379 SM 4500-CN-E-2011 444616 92408417014 EQUIPMENT BLANK SM 4500-CN-E-2011 444381 SM 4500-CN-E-2011 444617 92408417016 MWA R SM 4500-CN-E-2011 444381 SM 4500-CN-E-2011 444617 92408417017 MW-15 SM 4500-CN-E-2011 444381 SM 4500-CN-E-2011 444617 92408417018 MW-3R SM 4500-CN-E-2011 444381 SM 4500-CN-E-2011 444617 92408417019 MW-7 SM 4500-CN-E-2011 444381 SM 4500-CN-E-2011 444617 92408417020 MW-5R SM 4500-CN-E-2011 444381 SM 4500-CN-E-2011 444617 Date: 12/14/2018 09:55 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 114 of 174 CHAIN-0 -CUSTODY Analytical Request Document ;. aceAnalytical Chain -of- ustody is a LEGAL DOCUMENT - Complete all relevent fields Company: 4 DBilling Information: � Report To: Email To: Copy To: Site Collection Info/Address: Customer Project Name/Number: OSP State: County/City: Time Zone Collected: / [ ]PT[ ]MT[ ]CT [ JET Phone: Email: Site/Facility ID #: Compliance Monitoring? [ ] Yes [ ] No Collected By (print): lrn1El\ MQ Purchase Order Quote #: # DW PWS ID #: DW Location Code: al [C, ct y (signature)-' Turnaround Date Required: Immediately Packe on Ice: [ ] Yes [ ] No ple Disposal: [ ] Dispose as appropriate [ ] Return } ] Archive- [ } Hold: Rush: [ ] Same [ ] 2 Day [ (Expedite Day [ ] Next Day ] 3 Day [ ] 4 Day [ ] 5 Day Charges Apply) Field Filtered {if applicable): [ ] Yes [ ] No Analysis: * Matrix Codes (Insert in Matrix box below): Drinking Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air Water (DW), Ground Water (GW), Wastewater (WW), AR), Tissue (TS), Bioassay {B), Vapor (V), Other (OT) Customer Sample ID Matrix * C mp / Grab Collected (or Composite Start) Composite End Res Cl # of Ctns Date I Time Date Time at [� W r` 10 Zv b^' h,1411.9 133o l W - w - 1112&. t03 r2 1A11<f� W O • 924084 1 lurn7rer r ` 92408427 - ! �, Container Preservative T . e "• Cab 4'Co]eeelYla�ager u U »« Preservative Types: (1) nitric acid, 2) su furic acid, (3) hydrochloric acid, (4) sodium hydroxide, (S) zinc acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other '--11 Analyses Lab BiufilivLine. ;; tq pfj ' v 1 U MW4 2 GW `/ / E2 Y.: Nr w-13 G 60 303 �C.`YPa Customer Remarks Special Conditions Possible Haz rds T".YPe of Ice Usgd et Blue ] rDry [None SHORT HOLDS PRESENT[<7z hours) Y ',,,>N N/ Lab5arrip]eTemperature Info P krhg Material Used Lab;Tra, :...g# Temp Blank Received Y ©NA 3179 Therm ID# Cooler IT llpon Receipt i oC Radchem samp[e[s) screened �e500 cpm); Y ]V NA `. Sarrkples received vi 3 Cooler 1 Therrn Corr Factor oC fJ;DEX UPS Aclient Courier ce Courie Cooler 1 Corre.cted Teff mp R I' quis ed Company: (Signature) Date/Time: Received by/Company: ignature) Date/Time: MTJL LAB Comments i ALE l���G/� !q 30 /% ; � � p �! � �( i � O {V � TabJe � elinquished by/Company: (Signature) Date/Time: Received by/Co p y: (Signature) Date/Time: AcctnU m Template =Blank Ret:etved Y hf rNA Preldgln HCL McQH; TSP < Other;. Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: p Non'Con€otm °"e(s} Page: of: CRAM -CIF -CUSTODY Analytical Request Document Analytical - Chain -of -,Custody is a LEGAL DOCUMENT- Complete all relevent fields f t .ti --21 Billing Information: 2 •�1e i W� 408417 M pM: KL}{1 Due Date: 9�- NDFt CLIENT : Container Preservative Type "*"ccy La[aProfectManager LJEFT—o (Jl l,l Report To: Email To: ** Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate, (6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (13) ammonium sulfate, Copy To: Site Collection Info/Address: (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (o) Other Customer Pro' ct N / b Analyses Lab Peotile/Erne le1Vum er: State: County/City: Time Zone Collected: ]PT[ ]MT[ ]CT [ ]ET Phone: Site/Facility ID # Compliance Monitoring? Email: [ ] Yes [ ] No NZ Collected By (print): 1-T(9 *;9kF Purchase Order Quote #: : DW PWS ID #: DW Location Code: Cole y (sig ture): Turnaround Date Required: Immediately Packed on Ice: ISKmPle [ ] Yes [ ] No Dis osal: ] ] Dispose as appropriate [ ] Return Rush:p [ ] 5am Day ( ] Next Da Field Filtered (if applicable): y ] ] Archive: Y [ ] es t ] No Hold: 11 2 Day [ 1 3 Day j] 4 Day [ 1 5 Day Analysis:kn [ ] : (Expedite Charges Apply) * Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (GW), Wastewater (WW), 3' Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other OT;: $ , Customer Sample ID Matrix * Comp / Grab Collected (or Composite Start) Composite End Res Cl Iftf-7 Ctns Date Time Date Time Cie N 2G/, o Awn 1a ,:'ti/` J Customer Remarks / Special Conditions / Possible IHaz rds: . yiI aFy: Pignawre jDateeTime: Received q30 Relinquished by/Company: (Signature) Date/Time: Reaeged Relinquished by/Company: (Signature) Date/Time: Received (Signatu Date/Time: 1I-Z-1 4 Date/Ti me: Page: of: CHAIN-O-CUSTODY Analytical Request Document Cha,n,f-C study is a LEGAL DOCUMENT Complete all relevent fields Company: +}-'J , ` D � Billing Information: Address: Report To: Email To: Copy To: Site Collection Info/Address: '653(0 OL-D SAll6& Raad Customer Project ffNaame/N ber: li 1� State: ounty/City: Time Zone Collected: �`/ly1S��A IPmI ] PT I ] MT I ] CT [LT Phone: Email: Site/Facility ID #: Compliance Monitoring? [ ] Yes [ ] No Collected By (print): 651C S �� Purchase Order t Quote #: DW PWS ID #: DW Location Code: Colle d y (signature): Turnaround DateRequired: Immediately Packed on Ice: [ ] Yes [ ] No Sample Disposal: [ ] Dispose as appropriate [ ] Return [ ] Archive: [ ] Hold: Rush: [ ] Same Day [ ] 2 Day [ ] 3 (Expedite [ ] Next Day Day [ ] 4 Day [ ] 5 Day Charges Apply) Field Filtered (if applicable): [ ] Yes [ ] No Analysis: * Matrix Codes (Insert in Matrix box below): DrinkingWater Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), (DW), Ground Water (GW), Wastewater (WW), Tissue (TS), B(oassay (B), Vapor (V), Other (OT) Customer Sample ID Matrix * Camp/ Grab Collected (or Composite Start) Composite End Res Cl #of Ctns Date Time Date Time w ri/ Wq2 I — 5V, aW //; ._ II0S — a v,y - a //4(/ 0 ` ,9 w- Is GW { Customer Remarks / Special Conditions / Possible Haz; PM: KLH1 Dale Date: 12/11/18 CLIENT: 92-NDR �(6) Preservative Types: (1) nitric acid, {2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate, methanol, (7) sodium bisulfate, (9) sodium thiosulfate, (9) hexane, (A) ascorbic acids (B) ammonium sulfate, C) ammonium hydroxide, (D)TSP, (U) Unpreserved, (0) Other `b pr-ot ;fie Analyses Lab Peofi]e1L�ne. r Relinquished Company: [Signature) Date/Time: Received by/Company: (Signature) Date/Time: MTJLaAe USE ONLY --,•- Comments ) j t ( Relinquished by/Company: (Signature Date/Time: Received by/Company; (ignature) Date/Time: Acetnu m Template Hp Blank Received N NA P.relogin (L ' McOH TSP ;' Other `• Relinquished by/Company: (Signature) Date/Time: Received by/Company: (Signature) Date/Time: PM Non Cohforrnance(s) Page: YES / NO; of: CHAIN -OF -CUSTODY Analytical Request Document aceAna1y4ica1 Chain -of -Custody is a LEGAL DOCUMENT- Complete all relevent fields Company: Billing Information: Report To: Email To: Copy To: Site Collection Info/Address: Customer Project Name/Number: State: County/City: Time Zone Collected: / [ ]PT[ ]MT[ ]CT [ ]ET Phone: Site/Facility ID #: Compliance Monitoring? Email: [ ] Yes [ ] No Collec By (pri�t•): Purchase Order #: DW PWS ID #: uq Quote #: DW Location Code: Colle By (signature): Turnaround Date Required: Immediately Pace on ice: ( [ ] Yes [ ] No Sample Disposal: Rush: Field Filtered (if applicable): ( ) Dispose as appropriate [ ] Return [ ] Same Day [ ] Next Day [ ] Yes [ ] No [ ] Archive: [ ] 7 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day [ ] Hold: (Expedite Charges Apply) Analysis: * Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water (Gift Wastewater (WW), Product (P), Soil/Solid (SL), Oil (O ), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT) Comp / Collected (or Res # of Customer Sample ID Matrix * Grab Composite Start) Composite End Cl Ctns Date Time I Date I Time G W 121ii/,Q 1 101Via -- _'_)L iPi$L15 WO# . 924084/7 3m7teror ; KLH1 Due Date: 12/11/18 p V �. j CLIENT: 92-MDR r � m Container , rzarvnuve i y pe - %db Project Ma ^ er ,• rr' Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5 zinc acetate, (6) methanol, (7) sodium bisulfate, [8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate, (C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other Customer Remarks / Special Condit onr / Possible Hazards: TKpe of icie.U' Wet Blue O'. None SHORT kOLDS PRESENT {<72 hours) Y N N La samp[e Temperatureinfo Q Packing Material Used Lab Trackm # g tt�� /� pp Gi-F��Q Temp Blank Received Y :NA ThermlD# Cooler 1 Temp Upon Receopt�oC Radchem samples) screened (<500 cpm) Y N NA' Samples received via Capler 1 Therm Cvrr Factor oC FEDEX .:::. UPS Client Courser : Pace Couder ". Gooler T Corrected Temp oC Relinquis d by Company: (Signature) Date Time: ��f[�/,'s'?J Received bV/Company: (Signature} Date/T(ime j MTJi LAB TkLY Comments Table# �GF JZiJ _ lL Relinquished by/Company: (Signat re) Date/Time: 7 /I Received by/ pang: (ignature) L Date/Time: pcctnum Template i Try :Blank Received Y Nq p: Rrelog(n HCL.' McQ}1 TSP ; Other. Relinquished by/Company: (Signat re) Date/Time: Received by/Company: (Signature) Date/Time: pj� Non Conformarice(s}. Page: ..;tYFS /•.NO. - Of: O �FaceAnalytical o National Center for Testing & Innovation P a ANALYTICAL REPORT December 05, 2018 Pace Analytical - Huntersville, NC Sample Delivery Group: L1047537 Samples Received: 11/28/2018 Project Number: 92408417 Description: OSR Report To: Kevin Herring 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Entire Report Reviewed By: �vUnn v�,, �. L111-� Nancy McLain Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. V It 49 it 152 of 174 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Fn Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 FS MW-4R L1047537-01 5 [Cn] MW-2R L1047537-02 6 EQUIPMENT BLANK L1047537-03 7 Fr Qc: Quality Control Summary 8 Chlorinated Acid Herbicides (GC) by Method 8151 8 RC GI: Glossary of Terms 9 F Al: Accreditations & Locations 10 Sc: Sample Chain of Custody 11 rAl FSC Page 153 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047537 12/05/18 05:51 2 of 12 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time MW-4R L1047537-01 GW 11/26/1814:55 11/28/1808:15 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Chlorinated Acid Herbicides (GC) by Method 8151 WG1203496 1 11/30/18 09:24 12/03/1818:42 KLM Collected by Collected date/time Received date/time M MW-2R L1047537-02 GW 11/26/1814:52 11/28/1808:15 [Cn] Method Batch Dilution Preparation Analysis Analyst date/time date/time Acid Herbicides (GC) by Method 8151 WG1203496 1 11/30/18 09:24 12/03/1818:56 KLM FSrChlorinated Collected by Collected date/time Received date/time sQC EQUIPMENT BLANK L1047537-03 GW 11/26/1808:40 11/28/1808:15 Method Batch Dilution Preparation Analysis Analyst GI date/time date/time Chlorinated Acid Herbicides (GC) by Method 8151 WG1203496 1 11/30/18 09:24 12/03/1819:09 KLM FAI FSC Page 154 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, NC 92408417 L1047537 12/05/18 05:51 3 of 12 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. VV VV� � �t La�'_ Nancy McLain Project Manager FP1 FTC FSS FSr FC-1 F, FAI FSC Page 155 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047537 12/05/18 05:51 4 of 12 ONE LAB. NATIONWIDE. MW-4R SAMPLE RESULTS - 01 Collected date/time: 11/26/18 14:55 L1047537 Chlorinated Acid Herbicides (GC) by Method 8151 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time 2,4-D IJ 0.744 2.00 1 12/03/2018 18:42 WG1203496 Dalapon J 1.04 2.00 1 12/03/2018 18:42 WG1203496 2,4-DB IJ 0.775 4.00 1 12/03/2018 18:42 WG1203496 Dicamba J 0.813 2.00 1 12/03/2018 18:42 WG1203496 Dichloroprop IJ 0.778 2.00 1 12/03/2018 18:42 WG1203496 Dinoseb J 0.795 2.00 1 12/03/2018 18:42 WG1203496 MCPA IJ 13.1 200 1 12/03/2018 18:42 WG1203496 MCPP J J4 7.15 200 1 12/03/2018 18:42 WG1203496 2,4,5-T IJ 0.843 2.00 1 12/03/2018 18:42 WG1203496 2,4,5-TP (Silvex) IJ 0.845 2.00 1 12/03/2018 18:42 WG1203496 (S)2,4-Dichloropheny/Acetic 76.7 14.0-158 121031201818.42 WG1203496 Acid ACCOUNT: PROJECT: SDG: DATE/TIME: Pace Analytical - Huntersville, INC 92408417 L1047537 12/05/18 05:51 Fp] FTc FSS 4 Cn Fc 7G1 FAI FSC Page 156 of 174 PAGE: 5of12 MW-2R SAMPLE RESULTS - 02 Collected date/time: 11/26/18 14:52 L1047537 Chlorinated Acid Herbicides (GC) by Method 8151 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time 2,4-D IJ 0.744 2.00 1 12/03/2018 18:56 WG1203496 Dalapon J 1.04 2.00 1 12/03/2018 18:56 WG1203496 2,4-DB IJ 0.775 4.00 1 12/03/2018 18:56 WG1203496 Dicamba J 0.813 2.00 1 12/03/2018 18:56 WG1203496 Dichloroprop IJ 0.778 2.00 1 12/03/2018 18:56 WG1203496 Dinoseb J 0.795 2.00 1 12/03/2018 18:56 WG1203496 MCPA IJ 13.1 200 1 12/03/2018 18:56 WG1203496 MCPP J J4 7.15 200 1 12/03/2018 18:56 WG1203496 2,4,5-T IJ 0.843 2.00 1 12/03/2018 18:56 WG1203496 2,4,5-TP (Silvex) IJ 0.845 2.00 1 12/03/2018 18:56 WG1203496 (S)2,4-Dichloropheny/Acetic 70.4 14.0-158 121031201818:56 WG1203496 Acid ONE LAB. NATIONWIDE. Fp] FTc FSS 4 Cn Fc 7G1 FAI FSC Page 157 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047537 12/05/18 05:51 6 of 12 EQUIPMENT BLANK SAMPLE RESULTS - 03 Collected date/time: 11/26/18 08:40 L1047537 Chlorinated Acid Herbicides (GC) by Method 8151 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time 2,4-D IJ 0.744 2.00 1 12/03/201819:09 WG1203496 Dalapon J 1.04 2.00 1 12/03/201819:09 WG1203496 2,4-DB IJ 0.775 4.00 1 12/03/2018 19:09 WG1203496 Dicamba J 0.813 2.00 1 12/03/201819:09 WG1203496 Dichloroprop IJ 0.778 2.00 1 12/03/201819:09 WG1203496 Dinoseb J 0.795 2.00 1 12/03/201819:09 WG1203496 MCPA IJ 13.1 200 1 12/03/201819:09 WG1203496 MCPP J J4 7.15 200 1 12/03/201819:09 WG1203496 2,4,5-T IJ 0.843 2.00 1 12/03/201819:09 WG1203496 2,4,5-TP (Silvex) IJ 0.845 2.00 1 12/03/201819:09 WG1203496 (S)2,4-Dichloropheny/Acetic 69.6 14.0-158 121031201819.09 WG1203496 Acid ONE LAB. NATIONWIDE. Fp] FTc FSS 4 Cn Fc 7G1 FAI FSC Page 158 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, NC 92408417 L1047537 12/05/18 05:51 7 of 12 WG1203496 Chlorinated Acid Herbicides (GC) by Method 8151 Method Blank (MB) (MB) R3365161-1 12/03/18 17:46 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I 2,4-D U 0.744 2.00 Dalapon U 1.04 2.00 2,4-DB U 0.775 4.00 Dicamba U 0.813 2.00 Dichloroprop U 0.778 2.00 Dinoseb U 0.795 2.00 MCPA U 13.1 200 MCPP U 7.15 200 2,4,5-T U 0.843 2.00 2,4,5-TP (Silvex) U 0.845 2.00 (S)2,4-Dichloropheny/Acetic 69.0 14.0-158 Acid QUALITY CONTROL SUMMARY 1-1047537-01,02,03 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3365161-2 12/03/1818:00 • (LCSD) R3365161-3 12/03/1818:14 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % 2,4-D 5.00 3.41 3.93 68.2 78.6 50.0-120 14.2 20 Dalapon 5.00 3.35 3.92 67.0 78.4 32.0-120 15.7 20 2,4-DB 5.00 3.55 4.04 71.0 80.8 53.0-140 12.9 20 Dicamba 5.00 3.35 3.76 67.0 75.2 51.0-120 11.5 20 Dichloroprop 5.00 4.41 5.14 88.2 103 55.0-127 15.3 20 Dinoseb 5.00 2.89 3.02 57.8 60.4 36.0-134 4.40 20 MCPA 50.0 24.6 31.5 49.2 63.0 10.0-160 24.6 40 MCPP 50.0 209 242 418 484 10.0-160 E J4 P E J4 P 14.6 23 2,4,5-T 5.00 3.60 4.08 72.0 81.6 54.0-120 12.5 20 2,4,5-TP (Silvex) 5.00 3.58 4.08 71.6 81.6 50.0-125 13.1 20 (S)2,4-Dichloropheny/Acetic 63.6 71.0 14.0-158 Acid ONE LAB. NATIONWIDE. FP1 FTc FSS 4 Cn FSr 7G1 FAI [Sc Page 159 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, NC 92408417 L1047537 12/05/18 05:51 8 of 12 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report ONE LAB. NATIONWIDE. The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions CP IP FTC MDL Method Detection Limit. RDL Reported Detection Limit. FSS Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. [Cn] Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. FSr U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes Fc reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or FAI duplicated within these ranges. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and FSC potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL). J4 The associated batch QC was outside the established quality control range for accuracy. P RPD between the primary and confirmatory analysis exceeded 40%. Page 160 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047537 12/05/18 05:51 9 of 12 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T 104704245-17-14 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T ID T WI NY SD WY MI NV T NE IA OH T PA T f IL Ills WV vA UT T CA�� T KS MO KY W 11110 � NM O� AR N Sc T MS A`7L GA T TX * LA T AK T T q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: Pace Analytical - Huntersville, NC 92408417 L1047537 12/05/18 05:51 ME Page 161 of 174 PAGE: 10 of 12 i Chain of Custody o 4 ceAnal #r #* Workorder; 92�108 17 Wor Report f InvaIce To Kevin Herring Pace Analytical Charlotte SKO Kincey Avo. SLute 100 hluntorsville. NC 28078 Phone1(704)875-9092 Email: kevin-herring@Welabs.com State of Sample Origin, NC' item Sample ID 1 k!VJ-;R 12 MUV-2R F4EOUIPMEW BLANK 4 - a Transfers Released 13y 2 3 CooIer TemDerature on Receiot Q -Name: OSR S Ll t}c ontract T4 DatefTime Lab lB Md#rix t I1t2&2C161A-.55 f32406417012 Wale, rtSr2MO1014-52 9240841710t3 Water i 11i2612018 08-40 92408417014 Water 17a[afrme Received Fay N - °C I CustodySeal Y or jhft RAD SCREM- .5 rnl f Results R"uested By' 1211112018 � 3 R"ucsted AnTMI i Containers MENEEMMI I101 N �Mwm R:.txilTlmr2 zQ If{f r7= Received oil Ice Y or N 31q z2,07� v cc&'`: r'"e Bampte5 Intact LAB USE ONI-Y 07 0 Tueway, Novamher 27, 2018 10-40,02 AM Fk:1T-A�L•C•002re++.00 24t118rGh�UU9 Page of F#41 I Page 163 of 174 O �FaceAnalytical o National Center for Testing & Innovation P a ANALYTICAL REPORT December 05, 2018 Pace Analytical - Huntersville, NC Sample Delivery Group: L1047714 Samples Received: 11/28/2018 Project Number: 92408417 Description: OSR Report To: Kevin Herring 9800 Kincey Avenue, Suite 100 Huntersville, NC 28078 Entire Report Reviewed By: �vUnn v�,, �. L111-� Nancy McLain Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace National is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. V it 164 of 174 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page 1 Fn Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 FS MW-1R L1047714-01 5 [Cn] MW-15 L1047714-02 6 Qc: Quality Control Summary 7 Fr Chlorinated Acid Herbicides (GC) by Method 8151 7 GI: Glossary of Terms 8 RC Al: Accreditations & Locations 9 F, Sc: Sample Chain of Custody 10 FAI FSC Page 165 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047714 12/05/18 05:54 2 of 11 M W-1 R L1047714-01 GW SAMPLE SUMMARY Collected by ONE LAB. NATIONWIDE. Collected date/time Received date/time 11/27/18 09:37 11/28/18 09:15 FP1 Method Batch Dilution Preparation Analysis Analyst date/time date/time FTC Chlorinated Acid Herbicides (GC) by Method 8151 WG1203496 1 11/30/18 09:24 12/03/1819:51 KLM Collected by Collected date/time Received date/time M MW-15 L1047714-02 GW 11/27/1811:47 11/28/1809:15 Method Batch Dilution Preparation Analysis Analyst [Cn] date/time date/time Acid Herbicides (GC) by Method 8151 WG1203496 1 11/30/18 09:24 12/03/18 20:06 KLM FSrChlorinated RC F, FAI FSC Page 166 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, NC 92408417 L1047714 12/05/18 05:54 3 of 11 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. VV VV� � �t La�'_ Nancy McLain Project Manager FP1 FTC FSS FSr FC-1 F, FAI FSC Page 167 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047714 12/05/18 05:54 4 of 11 MW-1R SAMPLE RESULTS - 01 Collected date/time: 11/27/18 09:37 L1047714 Chlorinated Acid Herbicides (GC) by Method 8151 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time 2,4-D IJ 0.744 2.00 1 12/03/201819:51 WG1203496 Dalapon J 1.04 2.00 1 12/03/201819:51 WG1203496 2,4-DB IJ 0.775 4.00 1 12/03/201819:51 WG1203496 Dicamba J 0.813 2.00 1 12/03/201819:51 WG1203496 Dichloroprop IJ 0.778 2.00 1 12/03/201819:51 WG1203496 Dinoseb J 0.795 2.00 1 12/03/201819:51 WG1203496 MCPA IJ 13.1 200 1 12/03/201819:51 WG1203496 MCPP J J4 7.15 200 1 12/03/201819:51 WG1203496 2,4,5-T IJ 0.843 2.00 1 12/03/201819:51 WG1203496 2,4,5-TP (Silvex) IJ 0.845 2.00 1 12/03/201819:51 WG1203496 (S)2,4-Dichloropheny/Acetic 62.6 14.0-158 121031201819.51 WG1203496 Acid ONE LAB. NATIONWIDE. Fp] FTc FSS 4 Cn Fc F, FAI FSC Page 168 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047714 12/05/18 05:54 5 of 11 ONE LAB. NATIONWIDE. MW-15 SAMPLE RESULTS - 02 Collected date/time: 11/27/18 11:47 L1047714 Chlorinated Acid Herbicides (GC) by Method 8151 Result Qualifier MDL RDL Dilution Analysis Batch Analyte ug/I ug/I ug/I date / time 2,4-D IJ 0.744 2.00 1 12/03/2018 20:06 WG1203496 Dalapon J 1.04 2.00 1 12/03/2018 20:06 WG1203496 2,4-DB IJ 0.775 4.00 1 12/03/2018 20:06 WG1203496 Dicamba J 0.813 2.00 1 12/03/2018 20:06 WG1203496 Dichloroprop IJ 0.778 2.00 1 12/03/2018 20:06 WG1203496 Dinoseb J 0.795 2.00 1 12/03/2018 20:06 WG1203496 MCPA IJ 13.1 200 1 12/03/2018 20:06 WG1203496 MCPP J J4 7.15 200 1 12/03/2018 20:06 WG1203496 2,4,5-T IJ 0.843 2.00 1 12/03/2018 20:06 WG1203496 2,4,5-TP (Silvex) IJ 0.845 2.00 1 12/03/2018 20:06 WG1203496 (S)2,4-Dichloropheny/Acetic 70.2 14.0-158 121031201820:06 WG1203496 Acid ACCOUNT: PROJECT: SDG: DATE/TIME: Pace Analytical - Huntersville, INC 92408417 L1047714 12/05/18 05:54 Fp] FTc FSS 4 Cn Fc 7G1 FAI FSC Page 169 of 174 PAGE: 6of11 WG1203496 Chlorinated Acid Herbicides (GC) by Method 8151 Method Blank (MB) (MB) R3365161-1 12/03/18 17:46 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I 2,4-D U 0.744 2.00 Dalapon U 1.04 2.00 2,4-DB U 0.775 4.00 Dicamba U 0.813 2.00 Dichloroprop U 0.778 2.00 Dinoseb U 0.795 2.00 MCPA U 13.1 200 MCPP U 7.15 200 2,4,5-T U 0.843 2.00 2,4,5-TP (Silvex) U 0.845 2.00 (S)2,4-Dichloropheny/Acetic 69.0 14.0-158 Acid QUALITY CONTROL SUMMARY L1047714-01,02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3365161-2 12/03/1818:00 • (LCSD) R3365161-3 12/03/1818:14 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % 2,4-D 5.00 3.41 3.93 68.2 78.6 50.0-120 14.2 20 Dalapon 5.00 3.35 3.92 67.0 78.4 32.0-120 15.7 20 2,4-DB 5.00 3.55 4.04 71.0 80.8 53.0-140 12.9 20 Dicamba 5.00 3.35 3.76 67.0 75.2 51.0-120 11.5 20 Dichloroprop 5.00 4.41 5.14 88.2 103 55.0-127 15.3 20 Dinoseb 5.00 2.89 3.02 57.8 60.4 36.0-134 4.40 20 MCPA 50.0 24.6 31.5 49.2 63.0 10.0-160 24.6 40 MCPP 50.0 209 242 418 484 10.0-160 E J4 P E J4 P 14.6 23 2,4,5-T 5.00 3.60 4.08 72.0 81.6 54.0-120 12.5 20 2,4,5-TP (Silvex) 5.00 3.58 4.08 71.6 81.6 50.0-125 13.1 20 (S)2,4-Dichloropheny/Acetic 63.6 71.0 14.0-158 Acid ONE LAB. NATIONWIDE. FP1 FTc FSS 4 Cn FSr �GI FAI [Sc Page 170 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, NC 92408417 L1047714 12/05/18 05:54 7 of 11 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report ONE LAB. NATIONWIDE. The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Abbreviations and Definitions CP IP FTC MDL Method Detection Limit. RDL Reported Detection Limit. FSS Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. [Cn] Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. FSr U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes Fc reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or FAI duplicated within these ranges. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and FSC potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL). J4 The associated batch QC was outside the established quality control range for accuracy. P RPD between the primary and confirmatory analysis exceeded 40%. Page 171 of 174 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Pace Analytical - Huntersville, INC 92408417 L1047714 12/05/18 05:54 8 of 11 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T 104704245-17-14 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T ID T WI NY SD WY MI NV T NE IA OH T PA T f IL Ills WV vA UT T CA�� T KS MO KY W 11110 � NM O� AR N Sc T MS A`7L GA T TX * LA T AK T T q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: Pace Analytical - Huntersville, NC 92408417 L1047714 12/05/18 05:54 ME Page 172 of 174 PAGE: 9ofll This page intentionally left blank. Chair of Custody 0 ;,7?ceAna1j4ics Workorder: 92408417 Workorder Name OBR Rep OFT j InU01CO T;, _ _ sutrcr;n!rr .ct To Kevin Hereing Pace An2l.Oiral Charlotte a ,�(` , , � Po-j .A � ��' _ � 9800 Kincey Ave. Suite 100 F— Huntersville, SIC: 2W7B r4 T Phone 1{704)875-9092 Email kevin herringoapacetabs,wm State of ample Origin: NC item Sample IQ Called datfrinxe Lab ID 11 l20l20 i 8 14:55 9240-94170 4 �rLMervetl contaitie rs T1 k' Matrix 4 ?AV.11R ii12 01$ 44 37 924D64t7016 Malec 5 14 s5 11+271,741811:47 92408417017 Water Transfers Released ay � Daturin a Received By — 7 "1 �- 2 Cooler Tem perature on Recei t 1. " gC CU5tQdVSeal Y or - I �AL-- •rF ? S H-E , ,0.5 M- -Ir I pafefTimp Resuits Requested By: 321910018 RL'quesN_d AnpIV'si P It Received on Ice or N L4 V1,W5 uov»iv LAB USE ONLY —a- C*rnmatlltS ales Intact (Y� or N ,rveuiay, 44ouembet z7, 70184.a4 5A pm FMT-ALL-002rev.0024U2rch2009 P44 3f73 of 174 Pa ce An on • r Testin • & I n n f Cooler•Form Lz liE�3r; SDGw 0()glI� CL)oICF Receivrd10pemxi On. Z1a+ '� 118 Temperature Kcccivcd By- A,Iam Burns Sign ature, _ Receipt Check List NP Yes No C.00 Seal Present / Intact? COC Signed / Accurate? Bottles arrive intact? f Correct bottles used? Sufficient volume sent? z If Applicable UDA Zero headspace? Preservation Correct j Checked? Page 174 of 174 Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix C — Field Data Appendix C — Field Data Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix C — Field Data This page intentionally left blank. Document Name: Field data Sheet Date Issued: July 28, 2016' R Pa e: l of Document Nuutl F CAI;-FLD-001-rev.01 Issuing Authority: Pace Ifimtemille Quality Office I Name and AEliation Name and Affiliation Well ID: I Well Diameter: Total Well Depth: i ft Static Water Level: ft� Height of Water Columrt:. — ft Purge Information M osp Well Locked: ( YES / NO) Construction: (PVC/Steel/Stainless Steel) Multi Pactor•- ('(Radius/12)2 x 3.14 x 7.48] Casing Volume: gallons CaL 3 Volumes: — gallons Pump Intake: — it Date Purged:/ / Start : Pi:nish: — Purge Rate: Purging Method- Total Volume Purged: '— (gallons/mis) Sampling Information Date Collected: * Time Collected: a/ 05 (am/0 Sampling Equipment Used: Instrument ID: V S'r-t*�FT a(§ F Sz e �1 f�dt �t �doo Bottle TypePreservation Analysis Required rPw - 4F6V,0 VOA 14Q9 oxan2 I-saD rS2 % a-�/so,-•.a �''o/I n�. "1-135� c6(nn� Sit F� /a(rc (21010 / 74;zc Field Measurements/Observations Sample Temp CC): Time: 2� 5 Turbidity (ntu): /5, 3 Time: /005� llflf�r n w'g DissOxy.(mg/L:�•� Time: /)OS Fe2+mg/ L: —" Time: Specific Cond. (uS): 1a S. I Time: 0 0 5 Res. Cl (mg/L)/(µg/L): Time: Sample pH (s.u.): (0.0 Time: / ,;'0 S Odor: N 01V E ! Time: ] �05 ReDox(utV): 4N,2 Time: .1 05 Appearance: Mr Time; 1205 ReDox (EH value):YSI ProP]us +200mV Other: General/WeatherObservations: Sampler Signature Stabilization Test Time- Temp. S ff) Wind flz�iS(mph) i �ARfa7yfical ' Document Name: Field data Sheet Date issued: July 28, 2016 Page. tof Docamem Number: F-CAR-FLD-001-rev.01 Issuing Authority: Pace Hunteraville Quality Office Well ID: ` Well Diameter: Total Well Depth: 441,8 Static Water Level: ft a Height of Water Column-.— ft Purse Information Well Locked: ( YES / NO) Construction: (PVC/Steel/Stainless Steel) MultiFactor- — r(Radius/12)2 x 3.14 x 7.48J Casing Volume: gallons Cal 3 Volumes: gallons Pump Intake: ft Date Purged: _// Staxt: Finish: Purge Rate: ^ Purging Method: Total Volume Purged: (gallons/mis) Sampling Information Date Collected: % ( /a�/ 1 Time Collected: )3 15 (am Sampling Equipment Used: 9)2 hl 8 Instrument ID:. y-`1 It-yw'Pm d IZ5 Ill rScrcAfTX0s170g0 Bottle Type Preservation Analysis Required 1n 4/o�,Q VOA . 0 15Drn0 Field Measurements/Observations M /VOnC� f{NOg Nno1{ AIA04 1 gl Acek* A- look Gk"s — $�forJ li'f /JioxoNP Ch(orc�¢ su)i..t Ailc 6010 Fg40 4-a Sa I �` 2 Neva - Sd�p Sample Temp (°C): l 1, I Time: 3N Turbidity (ntu): 15' Time: 13' 15 Diss Oxy.(mg/L): 7, m2 Time: J 345 Pe 2+ mg/L: Time: Specific Cond. (uS): 003.q Time: )3:15 Res. Cl (mg/L)/(µg/L): — Time- Sample pH (s.u.): (p • Time: ) 345 Odor: SU I LO Yt0 Time: 13:1 S ReDox (mV): " 2 H Time:. I T) 5 Appearance: M u�TTime: 13:15 ReDox (EH value):YSI ProFlus +200mV f j8, q Other: Time: --- General/Weather Observations: -S W- 2 Temp.SV(OF) Wind St/S (mph) Sampler Signatufe Stabilization Test Time Purged Temp. (aC) Diss Oxy. (mg/L) Spec. (us) . pH (s.u.) ReDox (mV) Turbidity (ntu) ' Volume (gallons removed Other Water level (ft) r me: Field data Sheet ^ Date Issued: July 28 2016 Fageil l ot.i 14 hv- Name and Af]i]ation (Sampler(s): Field Bata Sheet ration WAS-$h(e..ddt .Project#; Ua7t - ACC - Name and Affiliation (Inspector): A/1 AC Well Information Well M Well Locked: ( YES / NO) Well Diameter: -- Construction: (PVC/Steel/Stainless Steel) Total Well Depth: - ft Multi }?actor*: [*(radius/12)2x3r14x7.48] Static Water Level: ft Casing Volume: �— gallons Height of Water Column '— ft Cal. 3 Volumes: gallons r Pump hitake: ft Purge Information Date Purged, — / Start•: — Finish: Purge Rates Purging Method: Total Volume Purged: (gallons/mis) Sampling Information Date Collected: Time Collected: Sampling Equipment Used:... �� Instrument ID: �/5X o2Va'Pro R/ ��{e$er�t e Bottle Type Preservation Analysis Required��5 p q, /-,tzo a -asa o: /�OTI F 7D5 ck ley Alk l- l.:Is..-e Af-Aoq /-- Ias-).Q A(Ao>•F i M )4e ehF(G - ik lAic .. Field Measurements/Observations Sample Temp, eC): Time: _Turbidity(ntu): /0:7 Time: /Gy,5 Diss Oxy (mg/L): Time: /57f S Fe 2+ mg/L: �Time: Specific Cond (uS): 3-T&, 0 Time: 1915- .lies. Cl (mg/L)/(µg/L): "—' Time: '—' Sample pH (s u.): is , 5 Time: / S4-5 Odor: uS� ( Time: _ / S V 5 ReDox (mV): s.% Time: l/ a!e rZ /5 Appearance: Time; /ems ReDox (EH value):YSI ProPlus +2oomV 1 rf Other; d �qr — Time: ` Genera]/Weather Observations:- .61-J-3 sunn /cloudy/rainy) Temp. So CF) Wind &/,5 (mph) Sampler Sigi MM ®®®/—W2L on PENN ®pi®®®mwlll - Document Name: Field data Sheet Date Issued: July 28, 2016 _ CCRIk?/yllCaI - .. -Pa e: 1ofj Issuing Document Nuinber: P-CAR-PLD-001-rev.01 Authority: Pace Fruntersville Quality Office Field Data Sheet Name and Afiliation Nance and Afiliation (Inspector):_ N1A Well ID: Well Diameter: Total Well Depth: Static Water Level: ft Y Height of Water Column: ft Well Locked: ( YES / NO) Construction: (PVC/Steel/Stainless Steel) Multi Factor": (•(Radius/12)2 x 3.14 x 7.48] Casing Volume: gallons Cal. 3 Volumes: gallons Pump Intake: ft Purge Information Date Purged: /__/ -- Start: Finish: Purge Rate: Purging Method: Total Volume Purged: (gallons/mis) Sampling information Date Collected'. 11 A/L9_ Time Collected: I W5- (aIItZg Sampling Equipment Used: gA(, —Instrument ID: ys_ hsZdH SC1,A-4-'VId4Pg0 Bottle Type Preservation Analysis Required f1It{DpXVAA 14 Le $)-b0 92,w/,,/-p7XAn4 �x12-;zS0 lym-2 7 61�n�tiQ/ Su��+lir� �lC /_ast1nfl f-/>tlp� /-lases �✓r4ri�-F � � 1—IaS sao /�o}nc� Field Measurements/Observations- Sample Temp (°C): --(I.—Time: W45' Turbidity (ntu): _ Time: A/913- Diss Oxy.(mg/L): �7.. 5 Time: �—' Fe 2+ mg/L: Time: Specific Cond. (uS): � � Time: A� Res. Cl (mg/L)/(µg/L): - Time: Sample pH(s.u.): Time: //�'5 Odor: N0/J� Time: ReDox (mV): `J FO, ( Time: lgg5 Appearance: C (A✓ Time: I qV5- ReDox (EH value):YSI ProPlus +200mV 5q,) Other: — Time: General/WeatherObservations: cloudy/raiiny) Temp. (°F) WindnLL5—(mph) Sampler Signature: 44, A Date:�ll/ aG//y Stabilization Test Time Purged Temp. (IC) Diss Oxy. (mg/L) Spec. Cond. pH (s.u.) ReDox (mV) Turbidity (ntu) Volume (CBreemo / ) Water level (ft) Other r ZRn Ytkaf` Document Name: Field data Sheet I Date Issued: July 28, 2016 Pa e: I of I Document Number: F-CAR-FLD-001-mv.01 Issuing Authority: Face HuntersvitleQuality Office Name and Afilietion Name and Afilfation Well ID: MW- 11% ^ Well Diameter: 0 Total Well Depth: 60 ft Static Water Level: 35.3I {t: Height of Water Column: 2*0 ft M OSR Well Locked: (Y�E / NO) Construction: (OSteel/Stainless Steel) MultiFactor*: 0413 (•(Radias/12)2 x 3.19 x 7.48] Casing Volume: q. o2 gallons CaL 3 Volumes: 12.00 gallons Puntp Intake: 5-7-5 ft Purge Information At, Date Purged: 1) / 27 i I8n Start: 0919 Finish: 043li PurgeRate:Igo 1-1 Purging Method: R1addEr K"j? Total Volume Purged: 21Qfl (gallons/jo Sampling Informati Date Collected: I 1 / 27/ 1$ Time Collected: O 9 37 (6/pth) Sampling Equipment Used: Bladder' POLMP InstrumentlD: )(SI Pt•0• ?II,CS a1764 /7'PI Bottle Type Preservation alysis Required -500 ML 2-25oML None Tbs Cs,lortde salf%h Alk I_250 n.L •I -I Og 6010 -74-10 2 - I ZS ML NaoH Ali O •t 2, ei4e. oand a soWat (^ yO ML oA .Hc SUP UP I i,4 J;6VQt1o.. 2 ILAP4ers jq - IDUL None 82'90, go81, 8151 Field Measurement servations SampleTemp(oC): 13.6 Time: og37 Turbidity(ntu): 2 8 Time:, 0437 DissOxy.(mg/L): oy Time: 0937 Fe2+mg/L: Nb Time: 0437 Specific Cond. (uS) 218.7 Time: 0937 Res. Cl (mg(L)/(µ''g/L): Time: � SamplepH(s.u.): 11 SyTime: o437 Odor: MtAs• ( Time: 0437 ReDox(mV): - I35.3 Time: 6g37 Appearance: Clear Time: 0937 ReDox (EH value):YSI ProPlus +200mV 9 • 1_ _ Other: Time: General/Weather Observations: D/cloudy/rainy) Temp.38 (°F) Wind 8 (mph) Sampler Signature: Date: 11 I27/18 Stabilization Test *2150, Time Purged Temp. (C) Diss Oxy. (mg/L) Spec. Cond. (US) pH (s.u.) ReDox (mV) Turbidity (ntu) e removed (gallons/®1 Water level (ft) Other 0922 13.2 1.1 229.6 5.4 -1y1.5 2•.-1 y20 1. 3.9 - 0 2.5 3.4 0.•7 22'0.4 5A -13y:S 2.'4 SO 36.25 - 0428 13.6 0:5 z18.8 5,14 •-141.3 2.7 12s0 3C.24 - 0931 12.9 0 . q 21 .7 S. q-190• I 2.'1 16 80 3 .30 me 0134 13.2 0.Ll 218.0 5.4 -137.y ''2.? 210.0 Y, ,, CCARaJ'yllGa/ i Document Name: Field data Sheet Date Issued: July 28, 2016.Pa e: 1-oH� .. Document Numbs[: P-CAR-FLD-001-rev.01 -Issuing Authority: Pace Humersville Quality Office Name and AffiJation Name and Aflliation Well ID: N1W - a R Well Diameter: � i A Total Well Depth: 21 ft Static Water Level: "7 . q 3 ft Height of Water Column: I� osR Well Locked: (l`D / NO) Construction: ( V�/Steel/Stainless Steel) Multi Factor-: O • I S3 r(Radius/12)2 x 3.14 x 7.48J Casing Volume: /2.2 gallons Cal. 3 Volumes: 6 . G 3 gallons Pump Intake: i 9 ft Purge Information Date Purged: l / 26 / I ? Start : 13.58 Finish: (4 4 e1 Purge Rate: L5OMIMI Purging Methad: 81 ow el' oR a t- 9!t P . Total Volume Purged: m C (gallons/49 Sampling Information DateCollected:-1 /2C/ l8-'1 , Time Collected: N52 (am/10) Sampling Equipment Used: U 1 a ti t� t r Pcx m a Instrument ID: yST_- PPo 'PI t 5 tr17 C q/T-P= * 356g Bottle a Preservation 1-SooML.72--ZS0mi- lone TDS I-Z50 Au NNo 2-1215 M1, W oN t^ te4ak- 6- No Mt V( •NCI S-1L nhts iW-IOD«E A►W NoA4 — ieI—d Measurements/Observations ialysis Required (ul" CAlamae ft oto �{-10 'atni a Sal�`Pdd �O lil{ a(iexgne Sample Temp (°C): l y • O Time: LI� S2 Turbidity (ntu): 6 . Tune: 14 S 2 Diss Oxy (mg/L): I . G Time: N 52 Fe 2+ mg/L: I . S Timms (4 52 Specific Cond. (uS): 1145 Time: 1 q 52 Res. CI (mg/L)/(µg/L): `mime: Sample pH (s.u.): 6.3 Time: 1 y S 2 Odor: M to S-� Y Time: 14 5.2. ReDox(mV): -W3•Z Time: (452 Appearance:6r6+6 41±14 Time: ,Iy52- ReDox (EH value):YSI ProPlus +200mV I S 6 • $ Other: Time: - 4 -- Generai/Weather Observations: Qimi /cloudy/rainy) Temp.T'O (OF) Wind-j_Q_(mph) Sampler Signature: 1(d'- Stabilization Test Time Temp. Dias Oxy. Cond. pH (s.u.) ReDox Turbidity mmo ume Water Other Purged (C) (mg/L) (US) (mV) (ntu) (gallons/ level (it) J401. 15.0 S. 1428 6.3 -35.5 --- N50 7. L13 -' 81o.d er- GM Kul Ac 1 IZe of zs 1y28 .6 I IS.7 I G -q -31• I 1 S.? 72c 8 .G5 1 1Za4u l ly3rI q.,q 1 2.-? 1 usr 1 0 -$4.0 .3 410 8.8q-- I43y I jq.-7 I 2.3 I Ilya I G.3 1-3s.17.,2 12Co 9.qq I--- 01Y Document Nain.e: DocumentJuly 28, 2016 ��• PieldData:Sh6gt Paged'ofo7 Document NuMber: F-CAR-FLD-001.rev,01 Issueing Authority: Pace Huntersville.Quality Office Location:__ WAS+On- SOdCM, jJC. Project: OS R Well. ID:"1W�aR r a Stabilization Test a•i<:lL�®�� •M;M ,caAnalylicaf' I Document Name: Field data Sheet I -Fame: I of Document Number: F-CAR-FLD-001-rev.01 Name and Afdiation (Sampler(s): • �%lS Name and Afiliation (Inspector) f\t r Well Diameter: Construction: (PVC/Steel/Stainless Steel) Total Well Depth: s-� 't-'' ft Multi Factor*: � [•(Radius/12)2 x 3.14 x 7.481 Static Water Level:. L ft Casing Volume: I. 1:7 %�i gallons . Height of Water Column: ft CeL 3 Volumes: ^ l ' gallons Pump Intake: 1i Ctt ft Purge Information Date Purged: Start, . ' %lt, Finish:{) (; Purge Rate: 6-ctr. ')" Purging Method: l "3L ' . - Total Volume Purged:. (gallons/#Is)�.,1 Sampl ing Information Date Collected: / Time Collected:` (un)pm) Sampling Equipment Used: E J') f ;/rt.y hutrument ID: J.<1i t "1 " ° %{ Bottle Type Preservation Analysis Required ! --Sz;nl - PfI s}.7 Now, I C>S i a !m L kol -7elk Sample Temp (eC): a , NelC17 /�lUr}e3Y1 %Zn ltQi Ctlon��� }i�.�.. - A(�f'�, �SiE(7i-'iHd%p�$Zd;c`+ 55 !`N • I ,.;�' c�.a^x, e�.., Turbidity (ntu): j. Time: Diss Oxy (mg/L): Time: i' '` / eE ' _ Fe 2+ mg/L. Time: — Specilic Cond. (uS): Timed >` ic1 Res. Cl (mg/L)/(ug/L): - Time Sample pH (s.u.): 6.3 Time:: �');.N Odor: 1, x.i.Z L-3ime: ReDox (mV): > c7 - � Time: ` Appearance: Time:(, -` t / Z. ReDox (EH value):YSI ProPlus +200mV _ ! k Other: Time: General/WeatherObservations: m.. tsunn cloud rain Tem . �) [ 'F Wind t3' i n ( Y/) Y/ Y) F ( ) Stabilization Test Time Temp. Diss Oxy. Spec. Cond. pH (s.u.) ReDox Turbidity Volume removed Water Other Purged a (C) (mg/L) (US) (mV) (ntu) (gallons/. '^f level (ft) Nit t'mot :-Y,v `%s"1 ' i7 19 xf, � 6, ci -- 020 9 f,, I TT— " -7 oc) ... �r t, T ✓ 0 1'Z11 !(.. tl ./"ho .l t-It+-�- 6E'- .`Jr. f7 L '1. P Document Name: Field Data sheet Document'Issued. July 28, 2016 Page f y Document Number: F-CAR-FLD-001.rev,01 Issuein$:Authorlty: Pace Huntersvllle.Quality Office Client: —,�l , i i`, Location: r� Project: Well10:iUV ` a Stabilization Test Time' Pur`ed` B Temp. °C ( ) Diss Oxy. ,(mg/L) " Spec. Cond. (us) pH (s.u:) ReDox (my) (ntu) Volue mTurbidity Removed . (gallons/mis);. circle one Water level. ft ( 1 Other Jl IL/ 1,9 ZljC L, j SG> c 1 ` 9 o 5 70o tl -0c Document Name: Field data Sheet Date Issued: July 28, 2016 1 1 .. rage:, of Q Document Nu nber: F=CAR-MDAel-rev.ol IssuingAuthors Pace iluntersvffie uaH 4 ty ��AR81 _ pie . Name and Aflliation Name and Afiliation Well ID: YVI W" 3 Well Diameter: u Total Well Depth: ft Static Water Level: 11' oR 0 ft Height of Water Column: #: aSiZ re5Aof6 2 Well Locked: aY / NO) Construction: P�/Steel/Stainless Steel) MultiFactor*: 0• /— S r(Radius/12)2 x 3.14 x 7.48] Casing Volume: 1 i (7 gallons Cal 3 Volumes: qi gallons Pump Intake: ft Purge Information Date Purged:.. 1� l� i Start : J (0 22 Finish: / 0 Purge Rate: — Purging Method: 4J illddtr h'&—. Total Volume Purged: a(OD (gallons/gO Sampling Information Date Collected: 12 /-U / 9 Sampling Equipment Used: I1 B Bottle Type Field Measurements/Observations Time Collected: / 0 `t pat) ;�P InstrumentID: YSr-1tD;ZIo pr-aojiiS&(3L-t-,7Ia1.. Preservation Analysis Required Alone Sample Temp (°C): i � ' I Time: I Q'if o Turbidity (ntu): 14,1 Time: / 0# 6 DissOxy.(mg/L): (3 Time: 0-'4 Fe2+mg/L: =Time: Specific Cond. (us): 3S 4 3 Time: Jo t(% Res. Cl (mg/L)/(µg/L): Time: Sample pH (s.0 ): iP, Time: I o 46 Odor: N0 i/ Time: / 0 1 q& ReDox(mV): Time:. 10`f& Appearance: tv Time: /0:1(6 ReDox (EH value):YSI ProPlus +200mV I0V3 Other: —, Time: General/WeatherObservations: VYIUJ 3� Temp.�(7 (°F) WindS/o/0 (mph) Stabilization Test Time Purged Temp. (aC) Dias Oxy. (s Ox Spec. Cam' pH (s.u.) ReDox (mV) Turbidity (nm) Volume (g��ved ,� Water level (ft) Other t0?5 qS .2 361, �t� - 08 i.7-.6 hoc) /T 3o p a9 -78,6 (0 C964a 30 -GG.� �CIJO t1, oi3� /So I.�191 9.0 !-�V0 !�-30 Document Name: Document issued: July 28, 2016 Field Data Sheet Page,2.of,�k . /��MAMWN f Document Number: F-CAR-FLD-001.rev.01 l5sueing Authority: Pace Huntersville Quality Office Client: pv F Location: Project: _ DMA2411 Well ID: . M W—W Stabilization Test 1.2 OVM 1.625 (LIM 4 asap Turbidity (ntu) �J Document Neme: Field data Sheet Date Issued: July 28, 2016 . Page: 1 of -2- Document Number: F-CAR-FLD-001-rev.01 e Issuing Authority Pace Huntersvi0uali Quality Office - Name and Affiliation Name and Aflliation (Inspector):_ AI A Well ID: N Well Diameter: Total Well Depth: a C) ft Static Water Level:9•�ft, Height of Water Column: 1 •^I'1- #: OSA Well Locked: d5 / NO) Construction: I�/Steel/Stainless Steel) Multi Factor*:o•�(s3 [•(Radius/12)2x3.14x7.481 Casing Volume: 1.41 gallons Cal. 3 Volumes: -7 gallons Pump Intake: I I ft Purge Information Date Purged: 1I / �(,� 1 I D Stara : I y 1 Finish: 14 S l Purge Rate: I D o M /1'r7N Purging Method: ('14l if r ? V-6 Total Volume Purged: 3 90 0 (gallons/Og Samoline Information Date Collected: _/ / I Time Collected: 14 SS (am/(g&) Sampling Equipment Used:�I R 1� V». f Instrument ID:� 51 1't (aS ITP1a � b8y Bottle Type a I L;k, "rsl4-I00.1 ",5 Preservation No hQ Amalysis Required 97-ID Mel W1 Sl , fn -4VD L VDA 11C1 82tf20 TFK + �LDF /-Soo,.L None 1VDr e TOS C tev:6c Sv a}f Kok, ,I-aVD.�L I Sro . L 2.-12Sn t. Field Measurements/Observations H/VD1 L0010, U ZD-74i10 NA04t/Nvtol++Z.KAt41*1e PSul4e Sample Temp (aC): (l'%1 Time: t `1 SS Turbidity (ntu): 7 ( Time: 1 K SS Diss Oxy (mg/L): 0• 0fyTime: l `I5S Fe 2+ mg/L: — Time: — Specific Cond. (uS): (p 71 Time: Res. Cl (mg/L)/(µg/L): — Time: Sample pH (s.u.): _ (p .3 Time: I `I SS Odor: rl D N2 Time: (K ReDox (mV): LlZ D Time: 1 y rss Appearance: flea✓ Time- t NSS ReDox (EH value).YSI ProPlus +200mV 9490 Other: — Time: General/Weather Observations: /cloudy/rainy) Temp. So (OF) Wind--p(mph) Sampler Signature: e:A Date: 111 210 1 I g Stabilization Test Time Purged Temp. (C) Diss Oxy. (mg/L) Cond. (US) pH (s.u.) ReDox (mV) Turbidity (nth) Vol removed (gallons/410 Water level (ft) Other 1 I S I •7 9 b .3 6.4 -1 .3 3 300 $ 28 `II 1 .q. 3 f•-1 G. -D•S $ 3 (o06 2 4d1 1 l .9 2. 3"181 63 1, 10.9 Too 9.29 1` 7-q 1 14.1f• 6*5 9• .0 Iaoo 8.2It IK2.� 1 •01 1.3 87• .3 1 as! .9 I Isuo 2- Document Naive: Documentlssµed: July 28, 2016 • ' Md.Data :Sheet Pagg2of 2_ DocumentNUnber: IssueingAuthbrlty: f F-CAR-FLD-001.rev,01 Pace Huntersvlll'e.Quallty pffice Location: Li. %s4yr- Satan MC Project: o S (� Well ID: Mw _qA rrsrora Stabilization Test Volume Removed drdeone � 1 Document Name: Field data Sheet .. Date Issued: July 28, 2016 Pale. 1 of .. - Document Number: P=CAR-FLD-001-rev.01e .Issuing Authority: Pace Huntersville Quality . c .. Project #: O S e Name and Affiliation (Sampler(s): rj Q - P 1:1C E Name and Afiliation (Inspector):_ A Well 1D: Well Diameter: Total Well Depth: 3 0 ft Static Water Level: I D.�( ft Height of Water Column: f R' 03 ft WellLacked: Y�/ NO) Construction: V�Steel/Stalnless Steel) MultiFactor': n - 1(,3 [(Radius/M2 x 3.14 x 7.48] CasingVoiume: 311 gallons Cal 3 Volumes: 913 gallons Pump Intake: ft Purge Information Date Purged: ) / /_ Start: 103Finish: / D; Ste% Purge Rate: Db n Purging Methods Deck blddbv- rn� lO Total Volume Purged:=Q_(gallons/ s) Sampling Information Date Collected: ai'/_ IS !! Time Collected: D6 pat) SamplingEquipment Used: 0elA 6�a�lclPrIR.k Instrument ID:y5#'0210 prupla-sk(se'en,'Tplo —ram— I # �✓� U Bottle Type' Preservation Analysis Required I_V0 1-500 w,p'1 ;9 n P f-asn w�Q )'I�Sti-P l-1%5w�Q Field Measurements/0bserv499,ns GAL NONE. >f410 A(A-oif i !✓AOrF� B� ;ke--Aec 60� io ne S 46/OrZ srIA6 . Rl(c -. %©/U FY D . Su/ Sample Temp Cq: 13. R Time: 11; K Turbidity (ntu): 0.575 Time: 1 / OS DissOxy.(mg/L): Time: ji-Mr Fe2+mg/L: Time: — Specific Cond. (us): 1 a-e 1 Time: 11: 05 Res. Cl (mg/L)/(µg/L): — Time: Sample pH (s.u.): aZ Time: 14:05 Odor: /J ON9 ReDox (mV): 19 Time:. W 05 Appearance: C" Ipd v Time: //' 05 ReDox (EH value):YSI ProPlus +200mV L E . oZ Other: Time: — GeneraVWeather Observations : 111 W - 512 /rainy) Temp. 35' (°F) Winds/a/5 (mph) SamplerSignatuie: I (Lli •�( Stabilization Test .. U .......... Time Purged Temp. (°C) Dias Oxy. (mg/L) Spec. Cond.PH (s.u.) ReDox (mV) Turbidity (ntu) — Volume (gallonsemoved D Water level (ft) Other �4 13,9 tFl 6,a 1'83. b.&9 &00 a 1111.22eyy 0041 3;4- g 170,1 k',1,2 — i�f,3i 5 i 1�o G,a 191,.8 0,�o SOv 1L25 me 0 i Document Name: Field Data Sheet Document Issued: July 28, 2016 Page aof,2 Document Number: F-CAR-FLD-001.rev.01 Issueing Authority: Pace Huntersville Quality Office Client: r f b Location:SAItOW,WC, Project: Well ID: iYI W—sl� Stabilization Test wen Dtasneta miaipicabm raetoe i 0.O4OB 1.2 O.OM 1.6m OAM 2 0.3630 3 03674 4 Q6M 6 1-45S4 s 2.61w • •. Turbidity t • Document Name: Field data Sheet Pam_ Z ,., I., ,1!7�WCOAW&aw, 1 1 Of AuthoriPace Ut Document Number: F-CAR-ITLD-001-mv.01 issuing ty: I I I Office Name and Afffiation (Sarnpler(s): �11) /_1 r1r, Name and Afiliation (Inspector): N A Well Information Well Diameter: ;_ — Construction: #: US K Steel) Total Well Depth: it Multi Factor*: a [*(Radius/l2)2x3.14x7.48l Static Water Level: - _5f; ft, Casing Volume: gallons Height of water Colunm:ILft' Cal. 3 Volumes: 5. gallons Pump Intake: 00 ft Pura Information Date Purged.-_LL_/_� / Start: /0 ;0 Finish: /0 Z/ Purge Rate: .�_,Lo�mt/vk PurgingMetbod: �J, _h_' ' C Total Volume (gallons/14o,.) r _Aj Sampling Information Date Collected: / Time ColIec.ted:(a4pjn) Sampling Equipment Used, �.1;11,n u),n Instrument ID: ''.&1 *V/t`1E 4//7j27B4—a0z 3 a­O'toftle Type Preservation Analysis Required �n L A!r2p il Alod f b) Ac e f3t�, 6,Am,�-,L /3,; if r- C- ZU &J 15, 1, l el j Field Measurernents/Observations Sample Temp ('C):_�7 �.Jirne: ill (I Turbidity (ntu): S. Time: 2() Diss Oxy (mg/L): a Time: [() q Fe 2+ SpecificCand.(uS): -3;5,_& Time: Sample pH(su)- Time: ReDox (mV): '30 Time: ReDox (EH value).YSI ProPlus +200inv. General/Weather Observations: Sampler Signature Stabilization Test Res. Cl (xng/L)/(gg/L)- —'Time: Odor: N jr) Time: Appearance: ( (e ,4 Time: Other: I Time: — Time Temp. Diss OXY. Spec. Cond. pH (s.u.) ReDox Turbidity Volume removed Water Other Purged ('C) (mg/L) (US) (MV) (ntu) (gallcms/ml � level (ft) 10 3 Li IT-T— 777 �� tic) 0Z ON 6 f q 10 73 L� 7 0 Cl I C),G S }~� Document Name: Field data Sheet Date Issued: July 28, 2016- 1 �aaefttlal kW' . Pa Iof j " - Document Number P=CAR-CAR-001-rev.01 . Issuing Authority: Face Huntersville Quality Office Name and Af]liation Name and Aflliation (Inspector): ' AIA Well ID: Well Diameter: Total Well Depth: 27 h Static Water Level: `l•-1� ft. Height of Water Column:12.2 ft Field Data Sheet T Well Locked: tfi8W/ NO) Construction: f�W/Steel/Stainless Steel) Multi Factor": d• 1 to 3r(Radius/12)2 x 3.14 x 7.48] Casing Volume: I. q 1 q gallons Cal. 3 Volumes: 5 t-7 gallons Pump Intake: 'ZU ft Purge Information L/ Date Purged: I I / 2 / . (t_ Start: (O D5 Finish: 1 O Z O Purge Rate: 10 0 Purging Method: r3 1kI It r PVL— Total Volume Purged: (5-0 0 (gallons/tQ Samvlin¢ Information Date Collected: ((- /2- p/ 19 Time Collected: 10 Sampling Equipment Used: B(adelcr• Query Instrument ID: iSI 1-7 5—ITiow*bdY Bottle Type preservation Analysis Required ! '.iSOw,l. I{y�D (oOID 02 �1`i'lp —.laS...L N,t0H /16cOH4.2h AcF<{P Cyat,;de/sit �dQ Field Measurements/Observations Sample Temp (aC): 1 tLo Time: I 0 2-s Turbidity (ntu): i • I Time: 1 O'2. s Diss Oxy (mg/L): Time: 10 2S Fe 2+ mg/L: — Time: Specific Cond. (uS): S`I-I Time. 10? S' Res. Cl (mg/L)/(µg/L): : Timer Sample pH (s.u.): S 7 Time: IO2S Odor: Ndhi? Time: 10ZS ReDox(mV): I'{S=0 Time: 10 Appearance: cLCtr Time: lags ReDox (EH value):YSI ProPlus +200mV •3`'LS O Other: — Time: '— General/Weather Observations: M w (sunny/ r y/rainy) Temp. 5 (OF) Wind o(mph) Stabilization Test Time Purged Temp. (°C) Dies Oxy. (mg/L) Spec. Cond. � • pH (s.u.) ReDox (mV) Turbidity (ntu) Volume (gallons ed JQ Water level (it) Other PSI— 14-(a �•7 (,3.�1 5� )Ss8 D.y 300 ly.'.2 loft 14-5 ty,2 557.1 r7 157.0 0.5- roDD fy•9& lol4 LY•S 5-1 5M 1 5'-7 1q6,& 1•to too IC(. L l01'7 L4•W q.1 I 5-q•2 5.: I4(q 0 0.9 1 l20o I b 1020 1 NIP 5•1 jrvP IL11410 2ARNY&Caf' Document Name: Field data Sheet Date Issued: July N, 2016- Page,1-of1. - DocumentNumber F-CAR-FLD-001-mv.01 - - - - Issuing Authority: Face Huntersville Quality Office Field Data Sheet Client: hl D R Location: w; n1+0N S tt em, N C Project #: (J 5 2 Name and Af]liation (Sampler(s): JLMS M G (Z P,1.L# Name and Af Nation (Inspector): ti / A- Wel] ID: AV - 9 Well Diameter: 2. , i1 Total Well Depth 6 r) ft Static Water Level: S 7�. 4 S ft Height of Water Column: b •S 7-ft Well Locked: Construction: NO) Steel) Multi Factor*: 01b r(Radius/12)2 x 3.14 x 7.48] Casing Volume: I , O b gallons CaL 3 Volumes: K/ • 1 gallons Pump Intake: S 7, S O ft Purge Information Date Purged: I 1 /-LL/ ) g Start: la S% Finish I�� Purge RateJOOM I S/M%/1 Purging Method: 81 ^a al f.- 4 K /•'t P Total Volume Purged: _ 10 0 (gallons mis) Samgling_Information Date Collected: l ( / Lb/ 14 Time collected: I I z i) amam j in SamplingEquipment Used: BlAd61rfLAMr Instrument ID: YSLJA$e9a/now ba&q Bottle Type Preservation Analysis Required Soar. / 2-2SaML None TD4/6tAfj:*q/.44r��rr:�/ 1.2SoML NN0� (w 6'02.e/ �4y4 Z-12.SML N&01-1/No,& fA^-rid ^t4IC.'[e Lim 4a,%& VoA _ NL1_ 82Le+Tlt1+OGbF Field Measurements/Observations Sample Temp (ac): 14 , 5 --Time.-ILL a Turbidity (ntu): 01 - H_ Time: 1 l 2' Diss Oxy (mg/L): 6. 7 Time: 112 4 Fe 2+ mg/L: Time: Specific Cond. (us): I S Z-' Time: t 12 O Res. Cl (mg/L)/(µg/L): Time: Sample pH (s.u.): 5,7 Time: 1) 2 0 Odor: Time: 11 L Q ReDox (mV): 1 5 g• a Time:. t 12 0 Appearance: L 1 2 P. Time: 1 J 2 0 ReDox (EH value):YSI ProPlus +200mV 316 •9 Other: ^^ Time: General/Weather Observations: (sunny cloud rainy) Temp, i Z (OF) Wind 4- S (n Sampler Signature: a Y qn B YVI- f Date: t 1 /Z 6/ 18 Stabilization Test . Time Purged Temp. (C) Diss Oxy. (mg/L) Cond. (u$) pH (s.u.) ReDox (mV) Turbidity (nm) Volume eved (gallons Water level (ft) Other loSb ILt.b 1 6 S, Soo 1. OO S1.48 10 S q 14. 7 . 7. 4 151.3 5.7 154.2 7.6 6000PAR SIAS 1102 1 111.6 -7.1 1112.71 5. 1 b.) it Lk 400 1 S . tlo S I Iy. 7.1 1 (52.Ot I S.7 156.S 1)3 Izvo 111,Ltal ►1 0 S 1 I1-1. b 1 b . 9 1152.41 S. 7 141S7.2 117A l Soo I TV.4 8 ag 4wa f Document Name: Field Data :Sheet Docuuient'lsaped: July 28, 2D16 Page�ofg Document Nuiliber: F-CAR-FLD-001.rev,01 hsueing Authority: Pace Hunters 1110.Quality Office Location: w;tiSton. S°.ILM, N L ?a a.exs Project: 0 5 lk ) 2 ' s 4 Well ID; Mw-q Es " I s Stabllizat(on Test Time Temp. Diss Oxy: Spec. Cond. pH (s.u.) ReDox (mV) Turbidity Volume Remov Water level. Other Purged (°C) (mg/L) (us) (ntu) _ (gallon mis) (n) circle ona - tt S. 1804 S1.49 tl IA 1y.7_ .6.94 141.7' t SC S I °I.IE 1 2 loin S% eta Document Name: Field data Sheet Date Issued: July 28, 2016 Page: 1-of Z. �' _,,�Alutiirffcal Issuing Authority: Pace Hunteravllle Quality Document Number: P-CAR-FLD-001-rev.01 Office Field Data Sheet Client: 1^I O R Location —';At0/�6,kif g t+l Pioject#: 00 (� Name and Af iation (Sampler(s): .S! n. 8 MER Pac L Name and Affiliation (Insnectorl: /A WeIlID: M W-1 0 Well Diameter: I" ' r� Total Well Depth: 7- . 010 ft Static Water Level: 11 , 5 13 ft a Height of Water Column:—%-,�-_ft Well Locked: Construction: NO) Steel) Multi Factor*: Q• 141 [•(Radius/12)2 x 3.14 x 7.481 Casing Volume: :. S S gallons Cal. 3 Volumes: Nt b S gallons Pump Intake: 6 . S ft Purge Information Date Purged: \� l6. Start, I Z N 3 Finish: 326 tP�ur�geR,ate: t oe m1 i /�+%^ Purging Method: 81iA Mite Q A, rn i Total Volume Purged: _ (galkmso Sampling Information Date Collected: '0 00 Time Collected: I O (am/6 Sampling Equipment Used: I ad d l P tti m P Instrument ID: Y $7 17 61 / Tf W 6 OS 4 Bottle Type Preservation Analysis Required (.400ML/1.1f4fA NaAt TOf/Uira+C/rttKlcaar;� t-2SoJAL. WNA3 (Polo/1POZ03 4> Srn L Na, O H / H OHi'%PteAug GYati•del matt: df 1O-yOda L VoA _ WCL 4a6o4tr f-+OUF �• - 19gr^L fi•lahf0.M6[r >`I owl A p? Tom' 4+061 Field Measurements/Observations Sample Temp (*C): 13 .0 Time: 13 3 Q Turbidity (ntu): 7 . I Time: 1 3 3 a Diss Oxy (mg/L): O. L1Time: Ian Pe 2+ mg/L: "" Time: ` Specific Cond. (uS): 194 (7 6 Time: 13110 Res. Cl (mg/L)/(µg/L): Time: Sample pH (s.u.): Time: 1.33 4 Odor3t. Stet f:wr Time: 13 3 ReDox (mV): — ! ! S . 7 Time: %13 4 Appearance: d (e T Time: t 3 3 ReDox (EH value).YSI ProPlus +200mV 2-4.1 Other: Time: General/Weather Observations Temp.CF) Wind 0- S (mph) Sampler Signature: Ryan Date: t l/ 2 6 / 16 Stabilization Test- . __ Time Purged Temp. (°C) Diss O (mg/L) Spec. (S) pH(s.u.) ReDox (mV) Turbidity (nm) Volume (gllonsed Water level (it) Other i1H6 ) .6 1bti b. -125 Z.o 'too 05L i24°1 ►3.5 3 .4 1941 6 S >Z -q &Q'0 tl 12 S2. 1 •4 2.0 iMob 1 0.5 •-116.7 1 V7 440 it 1Z 11.3 %A IVY= I h-5 1 %k. 2 IZoo 11.51 LL3-0j 13,1 o.q liam 1 0.5 -14 %7 2Zoo %07 Document Name: Document'Usued July 28, 2016 FWd Data Sheet PIRelpf j . Document Number: Issuein$ Authority: f F-tAR-FLD-001.rev.01 Pace Huntersvlile.Quality Office Location: W i A S+on . 5 &ld.A, N( 1.2 %AM pSR 2 Project: s Well ID-, -b . Stabilize on Test Turbictity Volume RemoVedo circle one - I mo InMOMw[=w�-M �Mv Document Name: Field data Sheet Date Issued: July 28, 2016. Page: lofal /y__,��+,�7 "'"" �R �' f' Document Number: P-CAR-FLD-001-rev.01 Issuing Authority!Pace Huntersville uali 8 4 ty die • Name and Aidiation Name and Affiliation Well ID: 11►k tl Well Diameter: 2;A Total Well Depth: d 0 Static Water Level: 3.29 ft,, Height of Water Column: '1 Z ft #: oSR Well Locked: (tF / NO) Construction: (10/Steel/Stainless Steel) Multi Factor*: 0.1 98 r(Radius/12)2 x 3.14 x 7.481 Casing Volume: 2.73 gallons Cal. 3 Volumes: B.11 gallons Pump Intake: 17.5 ft Purge Information 4A Date Purged: l� 2� J$ Start: 101'Z Finish: 01 33 Purge Rate: S ^ Purging Method:'S &446f pNMe Total Volume Purged: 3350 (gallons/ tls Sampling Information Date Collected: II / ZS/ 18 Time Collected: 103 6 (l'pm) SemplingEquipmentUsed: Rldkid.Jer- Pi*"l InstrumentID:YSS.Pfo P603*I%CHITYL f�26r� Bottle T e Preservation Analvais Required 1,500mL V?,50,NL Field Measurements/Observations N) 00 e -r 03 o a oM t Zo Ac 4 4e NGl SampleTemp (oc): 13.11 Time: 103s Turbidity(ntu): b•G Time: 1036 Diss Oxy.(mg/L): O • S Time: 10 3 Pe 2+ mg/L: 4.5 Time: 103 6 Specific Cond. (us): 3 y G. 4 Time: 1036 Res. CI1 - Time: Sample pH (s.u.): S.9 Time: 103C J(m�g1/L)/(µg/L): Odor:{Ii/vTt�$ulluc Time: 1036 ReDox(mV): -5S.8 Time:. 1036 Appearance: Clem Time: 103C ReDox (EH value):YSI ProPlus +200mV q t4.2 Other: Time: - General/Weather Observations: (1 Stabilization Test . k Temp.62 ff) Wind 10(mph) Time Purged Temp. (C) Diss Oxy. (mg/L) c. Coed. (US) pH (s.u.) ReDox (mV) Turbidity (ntu) r mo d (gallons/i& Water level (ft) Other loll 13.3 9 333.1. 5.47 -M.6 .8.0 480 3.840 10 18 13.6 1.2 338• 5.,j - No•1 11.S o 3..40 - 1021 1 5 3Ni.2 5.8 - 44.1 I I N.6 o 3:4o 1oe4 13: 0.8 343.,3 5.8 -qT 10.3 1920 3.yo - l02'7 13.6 0.6 345.3 1 5.8 1 -So..N 1 2 S 2400 3,.140 Document Naine: Documenthpoid July 28, 2016 �MY PieldData, Sheet Pageaofa Document Number: IssueingAufhority: F-CAR-FLD-ool.rev,ol Pace Hunteriville Quality Office Location: G1+n5ion� Sa�CM NC Project: OSR . Well ID: Stabilizatl no Test . .vn l�eeee• x, oaos. %.2 oneis . iaza o.2oeo 2 3 026" 4 .6.653. 6 1. M a 2AM MIN M... Volume • 0 �UMEM ff� OW&M mum� ®�®M-MM-WERPEM�® ®®®®®®®®rem � Document Name: Field data Sheet Date Issued: July 28, 2016 -Na e: 1-ofiR / aaeAfialyffGal Document Number: P-CAR-FLD-001-rev.01 Issuing Authority: Pace Huntersville Quality office Client: HDR Locati ;Wins}on^SAlert.,Nc�Ioject#: 05R Name and Afrliation (Sampler (s): RSK PA C e Name and Afllfation (Inspector): MIA' _ Well ID: ✓u1/� ^1 Z Well Locked: (QF s / NO) Well Diameter: 21.1 Construction: (1 V�/Steel/Stainless Steel) Total Well Depth 6,07 ft Multi Factor*: O- ICS r(Radius/12)2 x 3.14 x 7.48) Static Water Level: 4. yg ft Casing Volume: 1. 33 gallons . Height of Water Column: Ii •ZZ ft Cal. 3 Volumes: 5-M. gallons Pump Intake: 13 ft Purge Information prL Date Purged::( QQ/? 6 18 start: 1(35 Finish: 1 (S 6 Purge Rate, o Purging Method: P (e` J d e t` Pw M Q Total Volume Purged: 1100 (gallons/rq Samuline Information Date Collected: I I / 26/ I S Time Collected: I I S9 &-Pm) Sampling Equipment Used: 13le.do(Cr ?"f InstrumentlD..YSI Pro Plasik1764�7P= Bottle Typ Preservation talysis Required 1. 5004- 2-25o s.1. (None S so%Me moriae Alk L 2,15 6 MML 6010 74'70 2-125 ML ID aoN -tZ„ "t Gl�antde "sul�tdt: A 1,4 dlt,lcao Field Measurements/Observations Sample Temp (eC): N • $ Time: 1151, Turbidity (ntu): 3. N Time: I I V 9 Diss Oxy (mg/L): 1.0 Time: I t 59 Fe 2+ mg/L: AD Time: I1 Sal Specific Cond. (uS): U26.0 Time: I 1 59 Res. Cl (mg/L)/(µg/L): � Time: — Sample pH (s.u.): S• 4 Time: 1159 Odor: N one Time: 11 SA ReDox(mV): -31:G Time:. 11Sot Appearance: C.Iegr Time: 1159 ReDox (EH value).YSI ProPlus +200mV l 64 • H Other: — Time: General/Weather Observations: /rainy) Temp5 14 (°F) Wind I0 (mph) Sampler Signature Stabilization Test *2563 Time Purged Diss Oxy. (mg/L) Cond. (US) pH (s.u.) ReDox (mV) Turbidity (ntu) Volume oved (gallons/(s Water level (ft) Other 1138 6Temp. 2. US.4 5.8 -14.3 A.S 30o N.S2 1141 I . �I rr•s 5- -zs.2 � . 00 -94N�t (.0 Nz1.2 S. -aS.o 3 0o 4.9q — I1 14,'1 (.G 01,o 5.1 =30.3 3.-7 1200 4.G — T150 It(.'1 L I zq•o .9 -334 C.0 I5OO y.6 Document Naine: Document Usued. Nly 28, 2016 FieldData.Sheet Pa&eo?of� Document Number: F-CAR-FLD-001.rev,O1 Issueing Authority: Pace Huntersville.Quality Office won Paelec' Location: W tr%s+on — S al em f NC 1.2 O.naiB . teat' uaoeo OSR : oars.. Project: _ mw — �Z 4. Well ID-, s iseea Stabilize ion Test Time Purged Temp. lot) Diss Oxy. :(mg/L) .. Spec. Cond. (us) pH (s.u.) ReDox (mV) (ntu) Volue mTurbidity Removed (gallons/�). circle ane - Water level. (ft) Other Il 3 t4. 1.0 C.6 5.q 19010 ...' 4.54 1155 4.8. I.I t(25.5 -%3.6 3.3 2100 q.cq E■ ■■ Document Name: Field data Sheet Date Issued: July 28, 2016 lof I ceRlialYf 1` Pape: - Issuing Authority: Pace Huntersville Quality Document Number: F-CAR-FLD-001-mv.01 Office Name and Affiliation Name and Affiliation Well ID: P'lW i Well Diameter: Total Well Depth:. 20 ft Static Water Level: • q ft z Height of Water Column: I2.1 Q ft #: OSR Well Locked: (ffi/ NO) Construction: (lt VO/Steel/Stainless Steel) MultiFactor*: - 0.16 3 1+(Radius/12)2 x 3.14 x 7.48] Casing Volume: 1.17 gallons . Cal. 3 Volumes: 5.91 gallons Pump Intake: 17.5 ft Purge Information Date Purged: 1( / 2 Start : Finish: 13 O0 Purge Rate: Purging Method: 1310 fltl@r- PuwTotal Volume Purged: 1190 (gallons/r@ Sampling Information Date Collected: 1� 26/ 18 Time Collected: 3� 03 (am/4 J p yss ere p1t.s1t1?G4 -rPS 4zses Sampling Equipment Used: 81 e• �Cr tiw. p Instrument ID: Bottle Type Preservation alysis Required 50oa.t,_( 2450ML f1ione /AIK I - 250 ML wjos 010 -1470 2- 125 ML• t0 0 t2.Ao6A c tlmide soliide 6- 40o-- VOA SAGS 826o t 4 4;*);Qne Field Measurements/Observations Sample Temp (oC): 2 Time:. 1303 Turbidity (ntu): - 3.3 Time: 1303 Diss Oxy (mg/L): 3 • S Time: 13 03 Fe 2+ mg/L: Time: l 3 0 3 Specific Cond. (uS): I2y• 8 Time: 1303 Res. CI (mg/L)/(gg/L): Time: Sample pH (s.u.): 5- 5 Time: 1303 Odor: None Time: 31 o3 ReDox (mV): - 2•w7• 7 Time: 1303 Appearance: C 10-%r Time: 1303 ReDox (EH value):YSI ProPlus +200mV 1•72.3 Other: I Time. I GeneraVWeather Observations: Temp.53 (OF) Wind 10(mph) Sampler Signature Stabilization Test Time Purged Temp. (C) Diss Oxy. (mg/L) c. Cod. (US.) pH (s.u.) ReDox (m� Turbidity (n ) Y Volume (gallons/i@ Water level (ft) Other 1Z51 g q,o 1Z5.3 5• -2R.o 3, o ,24 0.4e:)0 i254 15.0 3.S IZy.8 5.5 _22.6 3.y 73o .? - (26'1 ► iA 3. i C25.7 5.5 -24.5 3,6 logo 3.3 - 300 0 3.6 )25.3 5.5 =21.1 3.1 380 32 - Date Issued: July 2P, 2016 Document Name: Field data Sheet -Pa e: I'll . o - Issuing Authority: Pace tIuntersville Quality Document Number: F-CAR-FLD-001-rev.01 office Name and Afiliation Name and Afflfation Well ID: MIN - I N n Well Diameter: Total Well Depth (a 0 ft Static Water Level: $ I • 15 ft.` Height of Water Colun: t m #: bSt- Well Locked: YE / NO) Construction: �^'V�1 �.nrSteel/Stainless Steel) Multi Factor*:� r(Radius/12)2 x 3.14 x 7.48) Casing Volume: 31 gallons CaL 3 Volumes: 3 `13 gallons Pump Intake: ft Puree Information Date Purged: I k 2lu /. t Start: I I I Finish: 1 1 S Purge Rate: 1 0 0 M n Purging Method; B.141-rur pvt,.�Total Volume Purged: 1800 (gallons®) Sampling Information DateCollected: Time Collected: 120 S (am/p SamplingEquipmentUsed: J514 1,f-r I � Instrument ID: 'Isl l'I�S�TPW�k(pDB`i Bottle Type aSOv.L VoA Field Measurements/Observations Preservation N er.t M4D4/Na04 t7-hA 14 U Analysis Required', I 1 7%1SY14•4P / Alk, (W ovrOP (AM01 I.b1n l "1M17)- Sample Temp (eC): 1 3• Le Time: 110 S Turbidity (ntu): 5 7 Time: 1 20 S Diss Oxy (mg/L): 3.15 Time: 120 S Fe 2+ mg/L-.Time: Specific Cond. (us): 1-1S.0 Time: I ZO$ Res. a (mg/L)/(µg/L): Time: Sample pH (s.u.): S.`I Time: 12019 Odor: Pf ne Time: 1205- ReDox(mV): 1(03•9 Time: 12°S Appearance: lea/ Time: 120S- ReDox (EH value):YSI ProPlus+200mV _X03-K Other: Time: General/WeatherObservations: Kw - I4 (sunny/ ou4/rainy) Temp. -EC, (°F) Wind C (mph) Sampler Signature Stabilization Test Time Purges Temp. (C) Diss Oxy. (mg/L') Cond. (Ur) pH (s.u.) ReDox (MV) Turbidity (ntu) removed ume (gallons/9 61evel [Other ligq I. • 1.5 I'l4.5 U-3 14S.0 a-U 300 T<.t-I I.5 Covn II90 0014 3 11 1. Z 5'1 I51.8 aV 9GC . Ir 1153 114.3 7.0 t l-g 5.7 I(ol• '7.3 1 )ZVO 57.95 115 13.8 1 3.5 I -It. 3 57.1 11,2.1 1 S1 1 100 sLyS il5'9 13•Ls 3.5 1-11.1 5.7 11,3•9 l...n Igau stsZ ¢� Document Name: Field data Sheet Date Issued: Jlotsuly 28, 2016 Pa a /CaRlk7tytfCBt .Issuing Authority: Pace Huntersville Quality Document Number: P=CAR-CAR-001-rev.01 Office Client: OR Location: W i A S{ o nStA14 r trC i'dject S M1 Name and AGliatlon (Sampler(s): 3K . / P A e 2 _ Name and Afiliation (Inspector): W Q Well ID: M W - 15 Well Locked: (0E / NO) Well Diameter: Pin Construction: (R /Steel/Staintess Steel) Total Well Depth 418 it Multi Factor*:0.163 [*(Radius/12)2 x 3.14 x 7.481 Static Water Level: 38.74 ftt Casing Volume: 1.5I gallons Height of Water Column: Q •26 ft Cal.3 Volumes: 4.53 gallons Pump Intake: N ? ft Purge Information Date Purged: I I 27 / 'a � Start: 1102 Finish: I I q 4 Purge Rate: 900 A/M•01 / . Purging Method: V&N%C IC Se4- Sofi~S*IeTotal Volume Purged: $4106 (gallons/( Sampling Information Date Collected: I I / 27/ I ? Time Collected: 11 7 (4&pm) Sampling EquipmentUsed.Vaf• Spd• SubMQfsib CInstrumentID:Y51 Pro 91WS tk170/T-Fx- #s,50% Bottle Tye Preservation ApaIysisRequired 1-500M1r 2-2So,»l, None Tn S I chioeo 4suWa+e flIk 1- 2s0 ^1. ; INo3 010 0 2-.125Mt- NeoH Mao" +Z, Acg.Fa cyanide u(flde C= NoM1_ VOA HCl 82t;o 1 d�oxsne i= Am6er5R.I00# , R&+&5 N one Sz7o, 8o81, 8151. Field Measurements/Observations Sample Temp (aC): 15.S 4'Z Time: 11 q7 Turbidity (ntu): 3.2 Time: tl Diss Oxy (mg/L): Time: I i Fe 2+ mg/L: -- Time: 'I��'K Specific Cond. (uS): r0 Time: I i 41 Res. Q (mg/L)/(µg/L):--=-Time: - Sample pH (s.u.): re • I Time: 1147 Odor: NOAC Time: 114 ReDox (mV): 'Sq•'7 Time- 1%41 Appearance: C 1 e Q i- Time: 1141 ReDox (EH value):YSI ProPlus +200mV 1l0.3 Other: Time: General/Weather Observations (�/cloudy/rainy)Temp. L13 (OF) Wind 10 (mph) Sampler Signature Stabilization Test 02'7. Time Purged Temp. (C) Dias Oxy. (mg/L) Cond. (US.) pH (s.u.) ReDox (m� Turbidity (.to) removeed (gallons/t t�) Water level (ft) Other Ito's 13.4 8•Z i61 6•° -48•I 3.4 coo 3 .0- -- Io8 13.8 ^ 8• o IG4 •0 •-0., 3>6, IZoo' 34.25 1 l i r 13. P -TA -7G5 6. 0- -qa.3 ' 3.3 1800 39.26 Ittq 13.0 8.3 75R' 6.0 -'TI.S 3.8 2400 4.30 1117 13:5 7,5 1Ws .0 -NO,a{ 3oeio 3q. 3 - /�8�� (' Document. Name: PieldData:$heet Documentlesued. July 28, 2016 PaBeaof a Document Number: F-CAR-FLD-001.rev.01 IssueingAuthority: Pace Huntersville Quality Offlce Location: W �ns%on - S�.lem NC a 1.2 ooioa. O.b616 , s 62s osoeo Project: OSR z 3 oa6so 096T0 Well ID• 5 i 4 6 06G90 ,AM0 • I a 2AM Stabilize Ion Test Time' Purged Temp. (°C) Diss Oxy: :(mg/(-) Spec. Cond. (us) pH (s.u:) RepOx (mV) Turbidity (ntu) Volume Remoded (gallon s/rEq Water level. Other It2o 13.9 7.5 7 a I . 40.5.. 3:-H -3oo ..: 39.33 1t23 , l3. 6.S 732 ) -41. 1 3. 200 39.,3 1t26 ( .0 6.� 7z5 6•I.. -41.0 q 1soo. 39.36 A2°! 5. 8 ?24 6.1 -Uo.8.. 3.0 00. 39.46 1132 IS.I !09 6 1 - N6• 3.7 Sooc> 31.51 11.35 15.8 5.0. 703 6• I -5.2:3". . Z.�: 600 11f 1138 IG-0 1 4.5 102 C.I -55'.S 2.7 7200 '34.50 11 1 6.1 4.4:. ?04 6.1 -67.4 IZw 300 .34.4f. (144 t5.5 4..3 '703 I -54.3 3.2 8400 39.46 Document Name: Field data Sheet Date Issued: July 28, 2016 • Pa e: IN �' —'" "�� 1 Issuing Authority: Pace Huntersville Quality i Document Number: F-CAR-FLD-001-rev.01 Office Field Data Sheet \ Client: HDR Loeation:WiAS+%A-SOW, NG. Project#: OcS/Sp We(l Develor/Kepi 1 Name and AHliation (Sampler(s): _?SK . Name and Well ID: MW 1 S Well Locked: ES / NO) Well Diameter: oZ r, Construction: (n/Steel/Stainless Steel) Total Well Depth: M 8 ft Multi Factor*: 0- I G S ['(Radius/12)2 x 3.14 x 7.481 Static Water Level: 38•14 fta Casing Volume: 1.51 gallons Height of Water Column:�ft Cal. 3 Volumes: gallons Pump Intake: N 7. S ft Puree Information I l 28 l8 Ml Date Purged: 11 / 2� / I $ Start, 1 2 3 S posh: G��? 3 Purge Rate:112 D 0 M, A Purging Method:Ve,0uAlt Se. S-AmtrSi616TotalVolume Purged: /06.418 (gallons/19 Samplinglnformation Sampling ulDmentlla d Instrument ID: y31 Pro Pt'Ax#1754 TPI VT'M P � g E4 �.�_ Bottle Type Preservation An sis Required RedtU2le�enF (h` fen — PASS 11 27). ��} HatY che<,1� C'F4SS�11��8, Sample Temp (,q: Time:_ Diss Oxy (mg/L): Specific Cond. (uS): Time: Sample pH (s.u.): Time: _ ReDox (mV): Turbidity (ntu): Time: Fe 2+ mg/L: Time: Cl (mg/L)/(ug/L): Time: Time:. Appearance: ReDox (EH value):YSI ProPlus +200mV, General/Weather Observations: Lik Sampler Signature Stabilization Test r Cu Time Purged Diss Oxy. (mg/L) Spec. Cond. (US) pH (s.u.) ReDox (mV) Turbidity (nm) Volume removed (gallons/t&s Water level(ft) Other SURGE1.8 VtTemp. 01 C•0 -41.4 339•S 000 y1./3 SURGE • 705 .3 -43.4 1 3.5 21000 y2.74 SURGE -So. 3 MS. 36000 1 LWT.GH SURGE 1S00 6.5 1•o All. 9 1 6,0 -sy.2 19.8 GG000 T.C.P. SURGE Wail an dr 4e %X+reasek 4b Io M;n. Rai a 1��a Document. Name: ReidDatasheet DocumentIsstted. July 28, 2016 .Page loft Document Nuiiiber: F-CAR-FLD-001.rev,D1 Issueing'Autho'rity: Pace Huntersvill,'e.QualityOffice Location: W'nSfon - Sa�eM� NG Project: OS ILJ211 DMID 6Ai' .z i a MW — 15 Well ID: s Stabilization Test MMIMMM�., RemovedVolume 9I circle one ������ • a • .. a �- OSR Methane Readings Temp = 50F BP = 28.68 in. meter BP = 28.82 in. Well ID CH4 % co2% o2% Balance% MM-1 0.00 4.4 18.0 77.6 MW-1R 00.0 00.1 20.2 79.7 MW-2R 00.0 00.6 22.6 76.8 M W -13 0.00 00.2 19.9 79.9 MW - 15 00.0 00.2 19.8 79.8 2�E tiNfflS�evl_�fa12N11 �� �l��f'Jl U . ,i� •NBt-k o8mh f� This page intentionally left blank. Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix D — Electronic Files Appendix Electronic rtable Document Format (PDF) of this Report ectronic Data Deliverable (EDD) of Groundwater Winston-Salem City/County Utilities I Assessment Monitoring Report ��� Appendix D — Electronic Files This page intentionally left blank. FN HDR Engineering, Inc. of the Carolinas 440 S Church Street, Suite 1000 Charlotte, NC 28202-2075 704.338.6700 NC License F0116 hdrinc.com © 2019 HDR, Inc., all rights reserved