22074_Gathing Motor_Soil Cleanup Report 20161031

Correspondence:Amec Foster Wheeler Environment & Infrastructure, Inc.2801 Yorkmont Road, Suite 100Charlotte, North Carolina 28208Tel[phone]Fax[phone]Licensures: NC Engineering F-1253, Geology C-247
www.amecfw.com
October 31, 2016
Mr. Terry Finch, Director of OperationsSpectrum Properties, Inc.
201 South Tryon Street, Ste. 550Charlotte, North Carolina 28202
Subject:Soil Cleanup Report
Former Gathings Motor CompanyTax Parcel 073-073-071216/1220 South Tryon Street
Charlotte, North CarolinaAmec Foster Wheeler Project:6228-16-0369
Dear Mr.Finch:
Amec Foster Wheeler Environment & Infrastructure, Inc.(Amec Foster Wheeler)is pleased
to submit this Soil Cleanup Report for the above-referenced site.The activities were
performed in general accordance with our proposal (Prop16chltev315, dated September 2,
2016) as authorized by Spectrum Properties, Inc. on September 20, 2016.
Project Background Information
The subject site is located along the northwest side of South Tryon Street in Charlotte, North
Carolina (Figure 1).Amec Foster Wheeler (as MACTEC) performed a Phase I
Environmental Site Assessment (ESA) and additional work on behalf of the former property
owner in 2006 and 2007. Three Underground Storage Tanks (USTs) and one Oil/Water
Separator (OWS) were removed by Amec Foster Wheeler’s subcontractor in late 2006 and
early 2007.The USTs were reportedly last used by Gathings Motor Company in the 1960’s
and 1970’s.Amec Foster Wheeler completed the following reports for work performed at
the property:
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte,North Carolina
Amec Foster Wheeler Project: 6228-16-0369
2
Title of Report Project Number Date
Phase I ESA 6228-05-3261 Oct. 28, 2005
Phase II ESA 6228-06-3932 Feb. 2, 2007
Report of Asbestos Survey 6228-06-3932 Dec. 11, 2006
UST Closure Report 6228-06-3932 Feb. 5, 2007
Phase I Limited Site Assessment 6228-06-3932 May 31, 2007
Tank 1 is the subject of this report and was removed on December 21, 2006 (Figure 2).The
tank was reportedly used to store fuel oil for a boiler that was located inside the building just
northeast of the former tank location.The soil surrounding and beneath the tank exhibited
greenish-gray discoloration and strong odor which was considered evidence of a petroleum
release.The excavation dimensions for the 1,000-gallon tank were approximately 16 feet
by 10 feet with a depth of approximately 8.5 feet. Tank 1 was buried approximately 4 feet
below grade and measured approximately 10.5 feet long and 4 feet in diameter. The product
supply and return lines were observed approximately 2 feet below the ground surface
between the tank and the building.
TankNumber
InstallationDate ApproximateSize in
Gallons
TankDimensions LastContents
1 unknown 1,000 10.5’ x 4’Fuel Oil
for a boiler
After receiving laboratory results for soil samples at the UST removal (see Table 1),Amec
Foster Wheeler and our subcontractor returned to the site on January 11 and 12, 2007 to
excavate additional soil affected by the petroleum release and collect confirmation soil
samples for analysis. The soil remediation activities were summarized in the UST Closure
Report referenced above.Approximately 270 tons of petroleum-affected soil was removed
from the area of Tank 1 and disposed of at Environmental Soils, Inc.in Lattimore, North
Carolina.
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte, North Carolina
Amec Foster Wheeler Project: 6228-16-0369
3
The results of the confirmation analyses indicated that petroleum-affected soil (C9-C22
Aromatics and C9-C18 Aliphatics)with concentrations exceeding the Residential and
Maximum Soil Contaminant Concentrations (MSCCs)remained beneath the building
foundation (represented by sample BD-3).These results are summarized in Table 2.
Since re-development of the property was planned that may possibly include residential
land use,Amec Foster Wheeler recommended that the remaining soil at location BD-3 be
excavated and disposed following demolition of the site building.Amec Foster Wheeler also
recommended that confirmation sampling and analysis be performed to verify that no
affected soil with hydrocarbon concentrations exceeding the residential MSCCs remain.
In 2015, the former property owners transferred ownership of the property to Spectrum
Properties (Spectrum). Spectrum is presently involved in redevelopment of the property and
recently retained Lanier Site Services to demolish the building nearest former Tank 1 and
to perform excavation, hauling and disposal of the remaining affected soil. Spectrum
requested that Amec Foster Wheeler oversee the cleanup of the remaining soil at the rear
of the 1216/1220 building.
Soil Cleanup Activities
On September 30, 2016, following completion of the building demolition,Amec Foster
Wheeler personnel and Spectrum’s contractor,Lanier Site Services, Inc. (Lanier) met at the
property to excavate affected soil near the location of former Tank 1.Mr. John Maas of
Amec Foster Wheeler provided direction to Lanier to assist in the excavation of petroleum-
affected soil at this location.The purpose of the excavation was to remove and dispose the
soil likely affected by historic release(s)of petroleum.The excavation was initiated at grade
at the approximate former location of soil sample BD-3 (Figure 2)and was extended
laterally in three directions.The final excavation base ranged from a minimum depth of four
feet to a maximum depth of approximately 11 feet below grade. The petroleum-affected soil
was removed from the excavation with a trackhoe and loaded into dump trucks for disposal
at a permitted facility.
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte, North Carolina
Amec Foster Wheeler Project: 6228-16-0369
4
Mr. Maas observed the excavation activities and collected samples of soil from the sidewalls
and base of the excavation for visual,olfactory and field screening using a Photoionization
Detector (PID)The excavation continued laterally and vertically based on visual (stained
soil was noted) and PID screening until the visible stained soil was removed and PID
readings indicated that confirmation samples should be collected.A photographic log of the
excavation activities is included as Attachment A.Amec Foster Wheeler did not observe
evidence of groundwater in the excavation during the soil excavation activities.
The final limits of the irregular-shaped excavation are shown on Figure 2.A total of 90.48
tons of soil was removed during the excavation and disposed at Environmental Soils in
Lattimore, North Carolina.On the same date as the excavation activities,Lanier backfilled
the excavation with imported fill dirt.Copies of waste disposal manifests for the soil are
included as Attachment B to this report.
Confirmation samples (S-1 (base), S-2 through S-5 (sidewalls))were taken from the base
and the sidewalls of the excavation to confirm the effectiveness of the remedial effort
(Figure 2).Table 3 provides the sample depth information.Each sample was collected
directly from the backhoe bucket using a new pair of disposable gloves, placed into
laboratory-prepared sample containers, and stored on ice. The samples were delivered
under chain-of-custody protocol to Prism Laboratories, Inc.in Charlotte, North Carolina.The
laboratory analyzed the confirmation soil samples for risk-based parameters including
volatile organic compounds (EPA Method 8260/5035B), semi-volatile organic compounds
(EPA Method 8270), and volatile petroleum compounds (VPH) and extractable petroleum
hydrocarbons (EPH) according to the methods of the Massachusetts Department of
Environmental Protection.
Results
No concentrations of petroleum hydrocarbons were identified that exceeded the applicable
MSCCs.Copies of the laboratory analytical data reports are provided in Attachment C.
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte,North Carolina
Amec Foster Wheeler Project: 6228-16-0369
TABLES
TPH-GRO TPH-DRO
(mg/kg)(mg/kg)
T1A 8 890 17,000
T1B 8 420 14,000
(2006)State Action Level --10 10
Note:
Bold Font indicates that the concentration exceeded the State Action Level
Sample Number
Depth of
Sample
(ft bgs)
Table 1
Tank Closure Soil Analytical Results (2006)
Former Gathings Motor Company
1216/1220 South Tryon Street
Charlotte, North Carolina
Amec Foster Wheeler Project 6228-16-0369
Compound T-1
Bottom T-1 North T-1 South T-1 East T-1 West BD-2 BD-3 BD-4 BD-5
Soil-to-
Water
MSCC
Residential
MSCC
Depth in feet >13 7 7 7 7 15 5-6 6 6 --
Acetone < 0.002 <0.0018 < 0.002 0.028 <0.0017 <0.0016 <0.86 <.0016 <.0016 24 940
Aliphatics, C5-C8 <2.59 <1.97 <2.09 <2.15 <2.25 <1.93 205 <2.74 <2.84 68 939
Aliphatics, C9-C18 5.49 2.49 J 2.47 J 2.65 J 4.09 J 2.25 J 6310 <2.74 <2.84 540 1500
Aliphatics, C19-C36 <4.84 <4.79 <4.99 <4.58 <4.24 <4.24 24.9 <2.74 <2.84 ##31000
Aromatics, C9-C22 <7.74 <7.76 <7.98 <7.33 <6.79 <6.78 2565 <2.74 <2.84 31 469
Sec-Butylbenzene 0.0011 J <0.00098 <0.0011 0.0046 J <0.00096 <0.00087 21 <0.00092 <0.00092 3.3 626
Tert-Butylbenzene <0.0011 <0.00098 <0.0011 0.0014 J <0.00096 <0.00087 4.8 <0.00092 <0.00092 3.4 626
Ethylbenzene <0.0012 <0.0011 0.0170 J <0.001 <0.0011 <0.00095 0.740 J <0.001 <0.001 4.9 1560
Fluorene <0.016 <0.015 0.0429 <0.015 <0.016 <0.015 0.106 J <0.015 <0.015 47 620
Isopropylbenzene <0.00089 <0.00078 <0.00089 <0.00075 <0.00077 <0.00069 4.6 <0.00074 <0.00074 1.7 1564
p-Isopropyltoluene <0.0016 <0.0014 <0.0016 <0.0013 <0.0014 <0.0012 28 <0.0013 <0.0013 0.12 100
2-Methylnaphthalene <0.016 <0.014 <0.016 <0.014 <0.015 <0.014 0.440 J <.014 <.014 3.6 63
Naphthalene <0.0013 <0.0012 <0.0013 <0.0011 <0.0012 <0.0010 20.4 <0.0011 <0.0011 0.16 313
Phenanthrene <0.017 <0.016 <0.018 <0.016 <0.017 <0.016 0.143 J <0.016 <0.016 56 469
n-Propylbenzene <0.0011 <0.0049 <0.0011 <0.00094 <0.00096 <0.00087 10 <0.00092 <0.00092 1.7 626
1,2,4-
Trimethylbenzene <0.0016 <0.00098 <0.0016 <0.0013 <0.0014 <0.0012 120 <0.0013 <0.0013 8.5 782
1,3,5-Trimethylbenzene <0.0017 <0.0015 <0.0017 <0.0014 <0.0014 <0.0013 95 <0.0014 <0.0014 8.3 782
Xylenes (total)<0.0032 <0.0028 <0.0032 <0.0027 <0.0028 <0.0025 4.27 <0.0046 <0.0046 4.6 3129
Notes:
1. All results shown in mg/kg (milligrams per kilogram)
2. MSCC = Maximum Soil Contaminant Concentration Prepared/Date:RCF 2-5-07
3. J = Estimated result < PQL and ≥ MDL Checked/Date:LMM 9-1-16
5. ## = considered immobile
6. NC DEQ Soil-to-water MSCCs and Residential Soil Cleanup Levels rev. 4/16/2012
Table 2
Confirmation Soil Analytical Results
Former Gathings Motor Company
1216/1220 South Tryon Street
Charlotte, North Carolina
Amec Foster Wheeler Project 6228-16-0369
4. --- Bold font indicates MSCC was exceeded
Compound S-1 S-2 S-3 S-4 S-5 Soil-to-Water
MSCC
Residential Soil
Cleanup Levels
(mg/kg)
Depth in feet >11 6 6 6 6
Acetone 0.020 J 0.0099 J 0.031 J 0.020 J 0.0099 J 24 14000
Aliphatics, C5-C8 <25 <22 <24 <21 <25 68 939
Aliphatics, C9-C18 <59 <54 <58 <57 <56 540 1,500
Aliphatics, C19-C36 <34 <32 <34 <36 <31 ##31,000
Aromatics, C9-C22 <38 <35 <37 0.53 J <37 31 469
Sec-Butylbenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 3.3 626
Tert-Butylbenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 3.4 626
Ethylbenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 4.9 1,560
Fluorene <0.44 <0.42 <0.44 <0.47 <0.41 47 620
Isopropylbenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 1.7 1,564
p-Isopropyltoluene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 0.12 100
2-Methylnaphthalene <0.44 <0.42 <0.44 <0.47 <0.41 3.6 63
Naphthalene <0.015 <0.012 <0.013 <0.014 <0.012 0.16 313
Phenanthrene <0.44 <0.42 <0.44 <0.47 <0.41 56 469
n-Propylbenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 1.7 626
1,2,4-Trimethylbenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 8.5 782
1,3,5- Trimethylbenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 8.3 782
Xylenes (Total)<0.023 <0.019 <0.019 <0.021 <0.019 4.6 3,129
1,2- Dichlorobenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 0.23 1,400
1,3- Dichlorobenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 7.6 460
1,4- Dichlorobenzene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 0.099 110
Toluene <0.0077 <0.0062 <0.0063 <0.0069 <0.0062 4.3 1,200
Acenaphthylene <0.44 <0.42 <0.44 <0.47 <0.41 11 469
Benzo(a)pyrene <0.44 <0.42 <0.44 <0.47 <0.41 0.096 0.088
Benzo(b)fluoranthene <0.44 <0.42 <0.44 <0.47 <0.41 1.2 0.880
Benzo(g,h,i)perylene <0.44 <0.42 <0.44 <0.47 <0.41 6400 469
Benzo(k)fluoranthene <0.44 <0.42 <0.44 <0.47 <0.41 12 9
Chrysene <0.44 <0.42 <0.44 <0.47 <0.41 39 88
Fluoranthene <0.44 <0.42 <0.44 <0.47 <0.41 290 620
Pyrene <0.44 <0.42 <0.44 <0.47 <0.41 270 469
Prepared/Date: LMM 10/19/16
Notes:Checked/Date: JRM 10/19/16
1. Samples collected on 9/30/2016
2. J-Detected but below the Reporting limit; therefore, result is an estimated concentration (CLP J-Flag).
3. All results show in mg/kg (milligrams/kilogram)
4. MSCC=Maximum Soil Contaminant Concentration
5. ## = considered immobile.
6. Analytical detections and selected compounds shown. See laboratoy analytical report for a complete list of compounds analyzed.
7. NC DEQ Soil-to-Water MSCCs and Residential Soil Cleanup Levels rev. 4/16/2012
Table 3
Confirmation Soil Analytical Results (2016)
Former Gathings Motor Company
1216/1220 South Tryon Street
Charlotte, North Carolina
Amec Foster Wheeler Project 6228-16-0369
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte, North Carolina
Amec Foster Wheeler Project: 6228-16-0369
FIGURES
PREPARED BY: JMS DATE: 10/26/2016 CHECKEDBY: RCF DATE: 10/26/2016 JOB NUMBER FIGURE 16228-16-0369
VICINITY MAPFORMER GATHINGS MOTOR COMPANY1216 & 1220 S. TRYON STCHARLOTTE, NORTH CAROLINA
¯SITE
0 400 800200 Feet
Service Layer Credits: © OpenStreetMap (and) contributors, CC-BY-SASources: Esri, HERE, DeLorme, USGS, Intermap, increment P Corp.,NRCAN, Esri Japan, METI, Esri China (Hong Kong), Esri (Thailand),MapmyIndia, © OpenStreetMap contributors, and the GIS UserCommunity
!!
!
!
!
!
!
!
!
!
!
!!
!
!!!
!.
S-5
T-1EAST
T1A
S-1S-2
S-3
S-4
T-1SOUTH
T-1WEST
BD-4
BD-5
BD-3
BD-2 BD-1 T-1 NORTH
T-1 BOTTOM
T1B ¯0 10 20 Feet
FORMER 1216 BUILDING
APPROXIMATE LIMITS OF SEPTEMBER 2016 EXCAVATION
APPROXIMATE LIMITS OF JANUARY 2007 EXCAVATION
NOTES: LOCATIONS OF FEATURES SHOWN ARE APPROXIMATE
PREPARED BY: JMS CHECKED BY: RCF PROJECT NO: 6228-16-0369 FIGURE NO: 2
SAMPLE LOCATION MAPFORMER GATHINGS MOTOR COMPANY1216 & 1220 S. TRYON STREETCHARLOTTE, NORTH CAROLINA
DATE: 10/31/2016 DATE: 10/31/2016
POWER POLE IN PARKING LOT
PARKING AREASOUTH
!December 2006 UST Closure Soil Sample Location
!January 2007 Confirmation Soil Sample Location
!September 2016 Confirmation Soil Sample Location
Power Pole
Former Site Building
Former Tank 1
Approximate Limits of September 2016 Excavation
Approximate Limits of January 2007 Excavation
Property Line
!.
FORMER BACKDOOR
FORMER BOILER AREA
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte, North Carolina
Amec Foster Wheeler Project: 6228-16-0369
APPENDIX APHOTOGRAPHIC LOG
PHOTOGRAPHIC LOG
Project:
1216/1220 South Tryon St
Site Location:
Charlotte, NC
Project No.
6228-16-0369
Photo1 Sept.2016
Direction of Photo
Northwest
Description:
View of the site and
demolition activities.
Photo2 Sept.
2016
Direction of Photo:
n/a
Description:
View of typical soil and
fill layers within theexcavation.
Excavationlocation
PHOTOGRAPHIC LOG
Project:
1216/1220 South Tryon St
Site Location:
Charlotte, NC
Project No.
6228-16-0369
Photo3 Sept.2016
Direction of Photo
North
Description:
View of excavated soil
and debris.
Photo4 Sept.
2016
Direction of Photo:
Northeast
Description:
View of the partially
backfilled excavation.
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte, North Carolina
Amec Foster Wheeler Project: 6228-16-0369
APPENDIX B
WASTE MANIFESTS FOR SOIL
Former Gathings Motor Company October 31, 20161216/1220 South Tryon StreetCharlotte, North Carolina
Amec Foster Wheeler Project: 6228-16-0369
ATTACHMENT CLABORATORY REPORT
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
10/06/2016
AMEC Foster Wheeler (Charlotte)
Rob Foster
2801 Yorkmont Rd. #100
Charlotte, NC 28208
Project: Spectrum S. Tryon
Project No.: 6228160369
Lab Submittal Date: 09/30/2016
Prism Work Order: 6090524
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
President/Project Manager
Reviewed ByRobbi A. Jones Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 42
Sample Receipt Summary
10/06/2016
Prism Work Order: 6090524
Client Sample ID MatrixLab Sample ID Date Sampled Date Received
6090524-01 09/30/16S-1 09/30/16Solid
6090524-02 09/30/16S-2 09/30/16Solid
6090524-03 09/30/16S-3 09/30/16Solid
6090524-04 09/30/16S-4 09/30/16Solid
6090524-05 09/30/16S-5 09/30/16Solid
Samples were received in good condition at 2.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 42
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 6090524
10/06/2016
Summary of Detections
0.020 J mg/kg dry6090524-01 S-1 Acetone 8260B
0.0099 J mg/kg dry6090524-02 S-2 Acetone 8260B
0.031 J mg/kg dry6090524-03 S-3 Acetone 8260B
0.020 J mg/kg dry6090524-04 S-4 Acetone 8260B
0.53 J mg/kg dry6090524-04 S-4 C9-C10 Aromatics MADEP VPH
0.0099 J mg/kg dry6090524-05 S-5 Acetone 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-1
Prism Sample ID: 6090524-01
Prism Work Order: 6090524
Time Collected: 09/30/16 10:30
Time Submitted: 09/30/16 13:50
6228160369
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P6J003113410/5/16 17:13 ZRCmg/kg dry 1.4C9-C18 Aliphatics
BRL MADEP EPH P6J003113410/5/16 17:13 ZRCmg/kg dry 2.7C19-C36 Aliphatics
BRL MADEP EPH P6J003111310/5/16 17:13 ZRCmg/kg dry 1.8C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14062 %1-Chlorooctadecane
40-14060 %o-Terphenyl
40-14085 %2-Fluorobiphenyl
40-140100 %2-Bromonaphthalene
General Chemistry Parameters
74.0 *SM2540 G P6J003010.100 10/3/16 16:34 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0691,2,4-Trichlorobenzene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0681,2-Dichlorobenzene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0631,3-Dichlorobenzene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0651,4-Dichlorobenzene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0861-Methylnaphthalene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0832,4,6-Trichlorophenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0862,4-Dichlorophenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0682,4-Dimethylphenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0622,4-Dinitrophenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0542,4-Dinitrotoluene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0592,6-Dinitrotoluene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0642-Chloronaphthalene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0632-Chlorophenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0712-Methylnaphthalene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0572-Methylphenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0812-Nitrophenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0883,3’-Dichlorobenzidine
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0553/4-Methylphenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0674,6-Dinitro-2-methylphenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0764-Bromophenyl phenyl ether
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0624-Chloro-3-methylphenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0544-Chloroaniline
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0584-Chlorophenyl phenyl ether
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.0694-Nitrophenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.061Acenaphthene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.064Acenaphthylene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.072Anthracene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.059Azobenzene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.058Benzo(a)anthracene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.048Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-1
Prism Sample ID: 6090524-01
Prism Work Order: 6090524
Time Collected: 09/30/16 10:30
Time Submitted: 09/30/16 13:50
6228160369
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.052Benzo(b)fluoranthene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.049Benzo(g,h,i)perylene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.058Benzo(k)fluoranthene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.037Benzoic Acid
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.059Benzyl alcohol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.077bis(2-Chloroethoxy)methane
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.063Bis(2-Chloroethyl)ether
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.076Bis(2-chloroisopropyl)ether
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.066Bis(2-Ethylhexyl)phthalate
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.063Butyl benzyl phthalate
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.056Chrysene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.054Dibenzo(a,h)anthracene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.068Dibenzofuran
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.061Diethyl phthalate
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.059Dimethyl phthalate
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.063Di-n-butyl phthalate
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.055Di-n-octyl phthalate
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.057Fluoranthene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.064Fluorene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.071Hexachlorobenzene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.080Hexachlorobutadiene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.079Hexachlorocyclopentadiene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.075Hexachloroethane
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.051Indeno(1,2,3-cd)pyrene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.060Isophorone
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.072Naphthalene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.063Nitrobenzene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.070N-Nitroso-di-n-propylamine
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.068N-Nitrosodiphenylamine
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.053Pentachlorophenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.058Phenanthrene
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.066Phenol
BRL 8270D P6J002910.44 10/4/16 18:59 JMVmg/kg dry 0.059Pyrene
Surrogate Recovery Control Limits
39-13264 %2,4,6-Tribromophenol
44-11561 %2-Fluorobiphenyl
35-11564 %2-Fluorophenol
37-12255 %Nitrobenzene-d5
34-12160 %Phenol-d5
54-12761 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000631,1,1,2-Tetrachloroethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000371,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-1
Prism Sample ID: 6090524-01
Prism Work Order: 6090524
Time Collected: 09/30/16 10:30
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000521,1,2,2-Tetrachloroethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000681,1,2-Trichloroethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000211,1-Dichloroethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000341,1-Dichloroethylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000421,1-Dichloropropylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000441,2,3-Trichlorobenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000981,2,3-Trichloropropane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000571,2,4-Trichlorobenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000591,2,4-Trimethylbenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000311,2-Dibromoethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000361,2-Dichlorobenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000461,2-Dichloroethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000481,2-Dichloropropane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000581,3,5-Trimethylbenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000511,3-Dichlorobenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000391,3-Dichloropropane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000301,4-Dichlorobenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000372,2-Dichloropropane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000402-Chlorotoluene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000464-Chlorotoluene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.000374-Isopropyltoluene
0.020 8260B P6J001910.077 10/4/16 2:01 ANGJmg/kg dry 0.0019Acetone
BRL 8260B P6J001910.0046 10/4/16 2:01 ANGmg/kg dry 0.00045Benzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00064Bromobenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00042Bromochloromethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00043Bromodichloromethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00087Bromoform
BRL 8260B P6J001910.015 10/4/16 2:01 ANGmg/kg dry 0.00095Bromomethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00038Carbon Tetrachloride
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00041Chlorobenzene
BRL 8260B P6J001910.015 10/4/16 2:01 ANGmg/kg dry 0.00064Chloroethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00056Chloroform
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00052Chloromethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00033cis-1,2-Dichloroethylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00026cis-1,3-Dichloropropylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00032Dibromochloromethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00035Dichlorodifluoromethane
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00030Ethylbenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00031Isopropyl Ether
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00046Isopropylbenzene (Cumene)
BRL 8260B P6J001910.015 10/4/16 2:01 ANGmg/kg dry 0.00071m,p-Xylenes
BRL 8260B P6J001910.077 10/4/16 2:01 ANGmg/kg dry 0.00070Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6J001910.15 10/4/16 2:01 ANGmg/kg dry 0.00070Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-1
Prism Sample ID: 6090524-01
Prism Work Order: 6090524
Time Collected: 09/30/16 10:30
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.077 10/4/16 2:01 ANGmg/kg dry 0.00066Methyl Isobutyl Ketone
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00043Methylene Chloride
BRL 8260B P6J001910.015 10/4/16 2:01 ANGmg/kg dry 0.00025Methyl-tert-Butyl Ether
BRL 8260B P6J001910.015 10/4/16 2:01 ANGmg/kg dry 0.00024Naphthalene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00039n-Butylbenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00046n-Propylbenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00032o-Xylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00037sec-Butylbenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00046Styrene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00026tert-Butylbenzene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00037Tetrachloroethylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00044Toluene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00046trans-1,2-Dichloroethylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00040trans-1,3-Dichloropropylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00050Trichloroethylene
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00050Trichlorofluoromethane
BRL 8260B P6J001910.038 10/4/16 2:01 ANGmg/kg dry 0.0011Vinyl acetate
BRL 8260B P6J001910.0077 10/4/16 2:01 ANGmg/kg dry 0.00037Vinyl chloride
BRL 8260B P6J001910.023 10/4/16 2:01 ANGmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12997 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P6J00381002510/5/16 18:12 ANGmg/kg dry 0.76C5-C8 Aliphatics
BRL MADEP VPH P6J00381002510/5/16 18:12 ANGmg/kg dry 2.9C9-C12 Aliphatics
BRL MADEP VPH P6J00381002510/5/16 18:12 ANGmg/kg dry 0.24C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130118 %2,5-Dibromotoluene (PID)
70-130103 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-2
Prism Sample ID: 6090524-02
Prism Work Order: 6090524
Time Collected: 09/30/16 10:35
Time Submitted: 09/30/16 13:50
6228160369
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P6J003113210/5/16 17:49 ZRCmg/kg dry 1.4C9-C18 Aliphatics
BRL MADEP EPH P6J003113210/5/16 17:49 ZRCmg/kg dry 2.6C19-C36 Aliphatics
BRL MADEP EPH P6J003111310/5/16 17:49 ZRCmg/kg dry 1.7C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14065 %1-Chlorooctadecane
40-14065 %o-Terphenyl
40-14084 %2-Fluorobiphenyl
40-14099 %2-Bromonaphthalene
General Chemistry Parameters
78.7 *SM2540 G P6J003010.100 10/3/16 16:34 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0651,2,4-Trichlorobenzene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0631,2-Dichlorobenzene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0591,3-Dichlorobenzene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0611,4-Dichlorobenzene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0811-Methylnaphthalene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0782,4,6-Trichlorophenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0812,4-Dichlorophenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0642,4-Dimethylphenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0582,4-Dinitrophenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0592-Chlorophenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0672-Methylnaphthalene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0542-Methylphenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0762-Nitrophenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0833,3’-Dichlorobenzidine
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0634,6-Dinitro-2-methylphenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0724-Bromophenyl phenyl ether
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0504-Chloroaniline
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.0644-Nitrophenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.057Acenaphthene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.061Acenaphthylene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.067Anthracene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.055Azobenzene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.045Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-2
Prism Sample ID: 6090524-02
Prism Work Order: 6090524
Time Collected: 09/30/16 10:35
Time Submitted: 09/30/16 13:50
6228160369
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.055Benzo(k)fluoranthene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.055Benzyl alcohol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.059Bis(2-Chloroethyl)ether
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.071Bis(2-chloroisopropyl)ether
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.062Bis(2-Ethylhexyl)phthalate
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.053Chrysene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.051Dibenzo(a,h)anthracene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.064Dibenzofuran
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.058Diethyl phthalate
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.055Dimethyl phthalate
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.059Di-n-butyl phthalate
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.051Di-n-octyl phthalate
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.053Fluoranthene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.060Fluorene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.066Hexachlorobenzene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.075Hexachlorobutadiene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.075Hexachlorocyclopentadiene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.070Hexachloroethane
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.048Indeno(1,2,3-cd)pyrene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.057Isophorone
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.067Naphthalene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.059Nitrobenzene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.066N-Nitroso-di-n-propylamine
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.049Pentachlorophenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.054Phenanthrene
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.062Phenol
BRL 8270D P6J002910.42 10/4/16 19:22 JMVmg/kg dry 0.055Pyrene
Surrogate Recovery Control Limits
39-13265 %2,4,6-Tribromophenol
44-11559 %2-Fluorobiphenyl
35-11563 %2-Fluorophenol
37-12255 %Nitrobenzene-d5
34-12157 %Phenol-d5
54-12762 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000511,1,1,2-Tetrachloroethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000301,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-2
Prism Sample ID: 6090524-02
Prism Work Order: 6090524
Time Collected: 09/30/16 10:35
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000421,1,2,2-Tetrachloroethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000551,1,2-Trichloroethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000791,2,3-Trichloropropane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000461,2,4-Trichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000481,2,4-Trimethylbenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000371,2-Dichloroethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000391,2-Dichloropropane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000471,3,5-Trimethylbenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000411,3-Dichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000374-Chlorotoluene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.000304-Isopropyltoluene
0.0099 8260B P6J001910.062 10/4/16 2:29 ANGJmg/kg dry 0.0015Acetone
BRL 8260B P6J001910.0037 10/4/16 2:29 ANGmg/kg dry 0.00036Benzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00052Bromobenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00034Bromochloromethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00071Bromoform
BRL 8260B P6J001910.012 10/4/16 2:29 ANGmg/kg dry 0.00077Bromomethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00033Chlorobenzene
BRL 8260B P6J001910.012 10/4/16 2:29 ANGmg/kg dry 0.00052Chloroethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00045Chloroform
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00042Chloromethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00024Ethylbenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00037Isopropylbenzene (Cumene)
BRL 8260B P6J001910.012 10/4/16 2:29 ANGmg/kg dry 0.00057m,p-Xylenes
BRL 8260B P6J001910.062 10/4/16 2:29 ANGmg/kg dry 0.00056Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6J001910.12 10/4/16 2:29 ANGmg/kg dry 0.00056Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-2
Prism Sample ID: 6090524-02
Prism Work Order: 6090524
Time Collected: 09/30/16 10:35
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.062 10/4/16 2:29 ANGmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00035Methylene Chloride
BRL 8260B P6J001910.012 10/4/16 2:29 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6J001910.012 10/4/16 2:29 ANGmg/kg dry 0.00020Naphthalene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00026o-Xylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00037Styrene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00036Toluene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00040Trichloroethylene
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00040Trichlorofluoromethane
BRL 8260B P6J001910.031 10/4/16 2:29 ANGmg/kg dry 0.00085Vinyl acetate
BRL 8260B P6J001910.0062 10/4/16 2:29 ANGmg/kg dry 0.00030Vinyl chloride
BRL 8260B P6J001910.019 10/4/16 2:29 ANGmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123101 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P6J00381002210/5/16 18:43 ANGmg/kg dry 0.66C5-C8 Aliphatics
BRL MADEP VPH P6J00381002210/5/16 18:43 ANGmg/kg dry 2.6C9-C12 Aliphatics
BRL MADEP VPH P6J00381002210/5/16 18:43 ANGmg/kg dry 0.21C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130118 %2,5-Dibromotoluene (PID)
70-130101 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-3
Prism Sample ID: 6090524-03
Prism Work Order: 6090524
Time Collected: 09/30/16 10:40
Time Submitted: 09/30/16 13:50
6228160369
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P6J003113410/5/16 18:25 ZRCmg/kg dry 1.4C9-C18 Aliphatics
BRL MADEP EPH P6J003113410/5/16 18:25 ZRCmg/kg dry 2.8C19-C36 Aliphatics
BRL MADEP EPH P6J003111310/5/16 18:25 ZRCmg/kg dry 1.8C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14067 %1-Chlorooctadecane
40-14065 %o-Terphenyl
40-14082 %2-Fluorobiphenyl
40-14096 %2-Bromonaphthalene
General Chemistry Parameters
74.0 *SM2540 G P6J003010.100 10/3/16 16:34 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0691,2,4-Trichlorobenzene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0681,2-Dichlorobenzene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0631,3-Dichlorobenzene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0651,4-Dichlorobenzene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0861-Methylnaphthalene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0832,4,6-Trichlorophenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0862,4-Dichlorophenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0682,4-Dimethylphenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0622,4-Dinitrophenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0542,4-Dinitrotoluene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0592,6-Dinitrotoluene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0642-Chloronaphthalene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0632-Chlorophenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0712-Methylnaphthalene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0572-Methylphenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0812-Nitrophenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0883,3’-Dichlorobenzidine
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0553/4-Methylphenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0674,6-Dinitro-2-methylphenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0764-Bromophenyl phenyl ether
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0624-Chloro-3-methylphenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0544-Chloroaniline
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0584-Chlorophenyl phenyl ether
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.0694-Nitrophenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.061Acenaphthene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.064Acenaphthylene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.072Anthracene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.059Azobenzene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.058Benzo(a)anthracene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.048Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-3
Prism Sample ID: 6090524-03
Prism Work Order: 6090524
Time Collected: 09/30/16 10:40
Time Submitted: 09/30/16 13:50
6228160369
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.052Benzo(b)fluoranthene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.049Benzo(g,h,i)perylene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.058Benzo(k)fluoranthene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.037Benzoic Acid
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.059Benzyl alcohol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.077bis(2-Chloroethoxy)methane
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.063Bis(2-Chloroethyl)ether
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.076Bis(2-chloroisopropyl)ether
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.066Bis(2-Ethylhexyl)phthalate
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.063Butyl benzyl phthalate
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.056Chrysene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.054Dibenzo(a,h)anthracene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.068Dibenzofuran
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.061Diethyl phthalate
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.059Dimethyl phthalate
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.063Di-n-butyl phthalate
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.055Di-n-octyl phthalate
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.057Fluoranthene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.064Fluorene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.071Hexachlorobenzene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.080Hexachlorobutadiene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.079Hexachlorocyclopentadiene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.075Hexachloroethane
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.051Indeno(1,2,3-cd)pyrene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.060Isophorone
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.072Naphthalene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.063Nitrobenzene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.070N-Nitroso-di-n-propylamine
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.068N-Nitrosodiphenylamine
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.053Pentachlorophenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.058Phenanthrene
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.066Phenol
BRL 8270D P6J002910.44 10/4/16 19:45 JMVmg/kg dry 0.059Pyrene
Surrogate Recovery Control Limits
39-13269 %2,4,6-Tribromophenol
44-11570 %2-Fluorobiphenyl
35-11569 %2-Fluorophenol
37-12259 %Nitrobenzene-d5
34-12166 %Phenol-d5
54-12770 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000521,1,1,2-Tetrachloroethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000311,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-3
Prism Sample ID: 6090524-03
Prism Work Order: 6090524
Time Collected: 09/30/16 10:40
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000431,1,2,2-Tetrachloroethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000561,1,2-Trichloroethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000181,1-Dichloroethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000281,1-Dichloroethylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000351,1-Dichloropropylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000361,2,3-Trichlorobenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000811,2,3-Trichloropropane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000471,2,4-Trichlorobenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000481,2,4-Trimethylbenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000301,2-Dichlorobenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000381,2-Dichloroethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000391,2-Dichloropropane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000481,3,5-Trimethylbenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000421,3-Dichlorobenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000321,3-Dichloropropane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000251,4-Dichlorobenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000302,2-Dichloropropane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000332-Chlorotoluene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000384-Chlorotoluene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.000314-Isopropyltoluene
0.031 8260B P6J001910.063 10/4/16 2:57 ANGJmg/kg dry 0.0015Acetone
BRL 8260B P6J001910.0038 10/4/16 2:57 ANGmg/kg dry 0.00037Benzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00053Bromobenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00035Bromochloromethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00072Bromoform
BRL 8260B P6J001910.013 10/4/16 2:57 ANGmg/kg dry 0.00078Bromomethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00032Carbon Tetrachloride
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00034Chlorobenzene
BRL 8260B P6J001910.013 10/4/16 2:57 ANGmg/kg dry 0.00053Chloroethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00046Chloroform
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00043Chloromethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00027cis-1,2-Dichloroethylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00026Dibromochloromethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00029Dichlorodifluoromethane
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00024Ethylbenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00026Isopropyl Ether
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00038Isopropylbenzene (Cumene)
BRL 8260B P6J001910.013 10/4/16 2:57 ANGmg/kg dry 0.00058m,p-Xylenes
BRL 8260B P6J001910.063 10/4/16 2:57 ANGmg/kg dry 0.00057Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6J001910.13 10/4/16 2:57 ANGmg/kg dry 0.00057Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-3
Prism Sample ID: 6090524-03
Prism Work Order: 6090524
Time Collected: 09/30/16 10:40
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.063 10/4/16 2:57 ANGmg/kg dry 0.00054Methyl Isobutyl Ketone
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00036Methylene Chloride
BRL 8260B P6J001910.013 10/4/16 2:57 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6J001910.013 10/4/16 2:57 ANGmg/kg dry 0.00020Naphthalene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00038n-Propylbenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00026o-Xylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00031sec-Butylbenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00038Styrene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00030Tetrachloroethylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00036Toluene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00038trans-1,2-Dichloroethylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00041Trichloroethylene
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00041Trichlorofluoromethane
BRL 8260B P6J001910.032 10/4/16 2:57 ANGmg/kg dry 0.00087Vinyl acetate
BRL 8260B P6J001910.0063 10/4/16 2:57 ANGmg/kg dry 0.00031Vinyl chloride
BRL 8260B P6J001910.019 10/4/16 2:57 ANGmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123105 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P6J00381002410/5/16 19:13 ANGmg/kg dry 0.75C5-C8 Aliphatics
BRL MADEP VPH P6J00381002410/5/16 19:13 ANGmg/kg dry 2.9C9-C12 Aliphatics
BRL MADEP VPH P6J00381002410/5/16 19:13 ANGmg/kg dry 0.23C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130129 %2,5-Dibromotoluene (PID)
70-130112 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-4
Prism Sample ID: 6090524-04
Prism Work Order: 6090524
Time Collected: 09/30/16 10:45
Time Submitted: 09/30/16 13:50
6228160369
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P6J003113610/5/16 19:02 ZRCmg/kg dry 1.5C9-C18 Aliphatics
BRL MADEP EPH P6J003113610/5/16 19:02 ZRCmg/kg dry 2.9C19-C36 Aliphatics
BRL MADEP EPH P6J003111410/5/16 19:02 ZRCmg/kg dry 1.9C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14067 %1-Chlorooctadecane
40-14067 %o-Terphenyl
40-14082 %2-Fluorobiphenyl
40-14097 %2-Bromonaphthalene
General Chemistry Parameters
69.9 *SM2540 G P6J003010.100 10/3/16 16:34 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0731,2,4-Trichlorobenzene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0711,2-Dichlorobenzene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0661,3-Dichlorobenzene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0691,4-Dichlorobenzene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0911-Methylnaphthalene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0882,4,6-Trichlorophenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0912,4-Dichlorophenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0722,4-Dimethylphenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0662,4-Dinitrophenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0572,4-Dinitrotoluene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0632,6-Dinitrotoluene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0682-Chloronaphthalene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0672-Chlorophenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0752-Methylnaphthalene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0602-Methylphenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0862-Nitrophenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0933,3’-Dichlorobenzidine
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0583/4-Methylphenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0714,6-Dinitro-2-methylphenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0814-Bromophenyl phenyl ether
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0664-Chloro-3-methylphenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0574-Chloroaniline
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0614-Chlorophenyl phenyl ether
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.0734-Nitrophenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.064Acenaphthene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.068Acenaphthylene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.076Anthracene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.062Azobenzene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.062Benzo(a)anthracene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.051Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-4
Prism Sample ID: 6090524-04
Prism Work Order: 6090524
Time Collected: 09/30/16 10:45
Time Submitted: 09/30/16 13:50
6228160369
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.055Benzo(b)fluoranthene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.052Benzo(g,h,i)perylene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.062Benzo(k)fluoranthene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.040Benzoic Acid
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.062Benzyl alcohol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.082bis(2-Chloroethoxy)methane
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.066Bis(2-Chloroethyl)ether
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.080Bis(2-chloroisopropyl)ether
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.070Bis(2-Ethylhexyl)phthalate
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.067Butyl benzyl phthalate
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.059Chrysene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.057Dibenzo(a,h)anthracene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.072Dibenzofuran
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.065Diethyl phthalate
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.062Dimethyl phthalate
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.067Di-n-butyl phthalate
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.058Di-n-octyl phthalate
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.060Fluoranthene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.068Fluorene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.075Hexachlorobenzene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.085Hexachlorobutadiene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.084Hexachlorocyclopentadiene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.079Hexachloroethane
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.054Indeno(1,2,3-cd)pyrene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.064Isophorone
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.076Naphthalene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.067Nitrobenzene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.074N-Nitroso-di-n-propylamine
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.072N-Nitrosodiphenylamine
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.056Pentachlorophenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.061Phenanthrene
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.069Phenol
BRL 8270D P6J002910.47 10/4/16 20:08 JMVmg/kg dry 0.062Pyrene
Surrogate Recovery Control Limits
39-13268 %2,4,6-Tribromophenol
44-11564 %2-Fluorobiphenyl
35-11564 %2-Fluorophenol
37-12257 %Nitrobenzene-d5
34-12158 %Phenol-d5
54-12768 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000571,1,1,2-Tetrachloroethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000331,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-4
Prism Sample ID: 6090524-04
Prism Work Order: 6090524
Time Collected: 09/30/16 10:45
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000471,1,2,2-Tetrachloroethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000611,1,2-Trichloroethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000191,1-Dichloroethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000311,1-Dichloroethylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000381,1-Dichloropropylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000391,2,3-Trichlorobenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000881,2,3-Trichloropropane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000511,2,4-Trichlorobenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000531,2,4-Trimethylbenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000281,2-Dibromoethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000321,2-Dichlorobenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000411,2-Dichloroethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000431,2-Dichloropropane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000521,3,5-Trimethylbenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000461,3-Dichlorobenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000351,3-Dichloropropane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000271,4-Dichlorobenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000332,2-Dichloropropane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000362-Chlorotoluene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000414-Chlorotoluene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.000334-Isopropyltoluene
0.020 8260B P6J001910.069 10/4/16 3:24 ANGJmg/kg dry 0.0017Acetone
BRL 8260B P6J001910.0041 10/4/16 3:24 ANGmg/kg dry 0.00040Benzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00058Bromobenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00038Bromochloromethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00039Bromodichloromethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00078Bromoform
BRL 8260B P6J001910.014 10/4/16 3:24 ANGmg/kg dry 0.00085Bromomethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00034Carbon Tetrachloride
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00037Chlorobenzene
BRL 8260B P6J001910.014 10/4/16 3:24 ANGmg/kg dry 0.00058Chloroethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00050Chloroform
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00046Chloromethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00029cis-1,2-Dichloroethylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00023cis-1,3-Dichloropropylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00028Dibromochloromethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00031Dichlorodifluoromethane
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00027Ethylbenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00028Isopropyl Ether
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00041Isopropylbenzene (Cumene)
BRL 8260B P6J001910.014 10/4/16 3:24 ANGmg/kg dry 0.00064m,p-Xylenes
BRL 8260B P6J001910.069 10/4/16 3:24 ANGmg/kg dry 0.00062Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6J001910.14 10/4/16 3:24 ANGmg/kg dry 0.00062Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-4
Prism Sample ID: 6090524-04
Prism Work Order: 6090524
Time Collected: 09/30/16 10:45
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.069 10/4/16 3:24 ANGmg/kg dry 0.00059Methyl Isobutyl Ketone
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00039Methylene Chloride
BRL 8260B P6J001910.014 10/4/16 3:24 ANGmg/kg dry 0.00022Methyl-tert-Butyl Ether
BRL 8260B P6J001910.014 10/4/16 3:24 ANGmg/kg dry 0.00022Naphthalene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00035n-Butylbenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00041n-Propylbenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00028o-Xylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00033sec-Butylbenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00042Styrene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00023tert-Butylbenzene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00033Tetrachloroethylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00040Toluene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00041trans-1,2-Dichloroethylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00036trans-1,3-Dichloropropylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00045Trichloroethylene
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00045Trichlorofluoromethane
BRL 8260B P6J001910.035 10/4/16 3:24 ANGmg/kg dry 0.00095Vinyl acetate
BRL 8260B P6J001910.0069 10/4/16 3:24 ANGmg/kg dry 0.00033Vinyl chloride
BRL 8260B P6J001910.021 10/4/16 3:24 ANGmg/kg dry 0.0013Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
84-123104 %Dibromofluoromethane
76-12997 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P6J00381002110/5/16 19:44 ANGmg/kg dry 0.66C5-C8 Aliphatics
BRL MADEP VPH P6J00381002110/5/16 19:44 ANGmg/kg dry 2.6C9-C12 Aliphatics
0.53 MADEP VPH P6J00381002110/5/16 19:44 ANGJmg/kg dry 0.20C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130122 %2,5-Dibromotoluene (PID)
70-130105 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-5
Prism Sample ID: 6090524-05
Prism Work Order: 6090524
Time Collected: 09/30/16 10:50
Time Submitted: 09/30/16 13:50
6228160369
Extractable Petroleum Hydrocarbons by GC/FID
BRL MADEP EPH P6J003113110/5/16 19:38 ZRCmg/kg dry 1.3C9-C18 Aliphatics
BRL MADEP EPH P6J003113110/5/16 19:38 ZRCmg/kg dry 2.5C19-C36 Aliphatics
BRL MADEP EPH P6J003111210/5/16 19:38 ZRCmg/kg dry 1.7C11-C22 Aromatics
Surrogate Recovery Control Limits
40-14063 %1-Chlorooctadecane
40-14067 %o-Terphenyl
40-14081 %2-Fluorobiphenyl
40-14095 %2-Bromonaphthalene
General Chemistry Parameters
80.0 *SM2540 G P6J003010.100 10/3/16 16:34 JLB% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0631,2-Dichlorobenzene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0581,3-Dichlorobenzene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0791-Methylnaphthalene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0772,4,6-Trichlorophenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0802,4-Dichlorophenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0632,4-Dimethylphenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0582,4-Dinitrophenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0502,4-Dinitrotoluene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0552,6-Dinitrotoluene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0602-Chloronaphthalene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0662-Methylnaphthalene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0532-Methylphenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0752-Nitrophenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0813,3’-Dichlorobenzidine
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0513/4-Methylphenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0624,6-Dinitro-2-methylphenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0714-Bromophenyl phenyl ether
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0584-Chloro-3-methylphenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0504-Chloroaniline
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0544-Chlorophenyl phenyl ether
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.0644-Nitrophenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.056Acenaphthene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.060Acenaphthylene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.066Anthracene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.054Benzo(a)anthracene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.045Benzo(a)pyrene
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-5
Prism Sample ID: 6090524-05
Prism Work Order: 6090524
Time Collected: 09/30/16 10:50
Time Submitted: 09/30/16 13:50
6228160369
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.048Benzo(b)fluoranthene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.054Benzo(k)fluoranthene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.035Benzoic Acid
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.072bis(2-Chloroethoxy)methane
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.061Bis(2-Ethylhexyl)phthalate
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.059Butyl benzyl phthalate
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.052Chrysene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.063Dibenzofuran
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.057Diethyl phthalate
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.059Di-n-butyl phthalate
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.051Di-n-octyl phthalate
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.053Fluoranthene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.059Fluorene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.074Hexachlorobutadiene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.074Hexachlorocyclopentadiene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.069Hexachloroethane
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.056Isophorone
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.059Nitrobenzene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.065N-Nitroso-di-n-propylamine
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.063N-Nitrosodiphenylamine
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.049Pentachlorophenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.054Phenanthrene
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.061Phenol
BRL 8270D P6J002910.41 10/4/16 20:31 JMVmg/kg dry 0.055Pyrene
Surrogate Recovery Control Limits
39-13269 %2,4,6-Tribromophenol
44-11565 %2-Fluorobiphenyl
35-11567 %2-Fluorophenol
37-12258 %Nitrobenzene-d5
34-12162 %Phenol-d5
54-12766 %Terphenyl-d14
Volatile Organic Compounds by GC/MS
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000511,1,1,2-Tetrachloroethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000301,1,1-Trichloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-5
Prism Sample ID: 6090524-05
Prism Work Order: 6090524
Time Collected: 09/30/16 10:50
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000421,1,2,2-Tetrachloroethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000551,1,2-Trichloroethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000171,1-Dichloroethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000271,1-Dichloroethylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000341,1-Dichloropropylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000351,2,3-Trichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000791,2,3-Trichloropropane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000461,2,4-Trichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000471,2,4-Trimethylbenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000251,2-Dibromoethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000291,2-Dichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000371,2-Dichloroethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000381,2-Dichloropropane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000471,3,5-Trimethylbenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000411,3-Dichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000311,3-Dichloropropane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000241,4-Dichlorobenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000292,2-Dichloropropane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000322-Chlorotoluene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000374-Chlorotoluene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.000304-Isopropyltoluene
0.0099 8260B P6J001910.062 10/4/16 3:52 ANGJmg/kg dry 0.0015Acetone
BRL 8260B P6J001910.0037 10/4/16 3:52 ANGmg/kg dry 0.00036Benzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00052Bromobenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00034Bromochloromethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00035Bromodichloromethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00070Bromoform
BRL 8260B P6J001910.012 10/4/16 3:52 ANGmg/kg dry 0.00076Bromomethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00031Carbon Tetrachloride
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00033Chlorobenzene
BRL 8260B P6J001910.012 10/4/16 3:52 ANGmg/kg dry 0.00052Chloroethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00045Chloroform
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00042Chloromethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00026cis-1,2-Dichloroethylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00021cis-1,3-Dichloropropylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00025Dibromochloromethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00028Dichlorodifluoromethane
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00024Ethylbenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00025Isopropyl Ether
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00037Isopropylbenzene (Cumene)
BRL 8260B P6J001910.012 10/4/16 3:52 ANGmg/kg dry 0.00057m,p-Xylenes
BRL 8260B P6J001910.062 10/4/16 3:52 ANGmg/kg dry 0.00056Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P6J001910.12 10/4/16 3:52 ANGmg/kg dry 0.00056Methyl Ethyl Ketone (2-Butanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 42
Laboratory Report
10/06/2016
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
2801 Yorkmont Rd. #100 Project No.:
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Sample Matrix: Solid
Client Sample ID: S-5
Prism Sample ID: 6090524-05
Prism Work Order: 6090524
Time Collected: 09/30/16 10:50
Time Submitted: 09/30/16 13:50
6228160369
BRL 8260B P6J001910.062 10/4/16 3:52 ANGmg/kg dry 0.00053Methyl Isobutyl Ketone
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00035Methylene Chloride
BRL 8260B P6J001910.012 10/4/16 3:52 ANGmg/kg dry 0.00020Methyl-tert-Butyl Ether
BRL 8260B P6J001910.012 10/4/16 3:52 ANGmg/kg dry 0.00020Naphthalene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00032n-Butylbenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00037n-Propylbenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00025o-Xylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00030sec-Butylbenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00037Styrene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00021tert-Butylbenzene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00029Tetrachloroethylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00036Toluene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00037trans-1,2-Dichloroethylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00033trans-1,3-Dichloropropylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00040Trichloroethylene
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00040Trichlorofluoromethane
BRL 8260B P6J001910.031 10/4/16 3:52 ANGmg/kg dry 0.00085Vinyl acetate
BRL 8260B P6J001910.0062 10/4/16 3:52 ANGmg/kg dry 0.00030Vinyl chloride
BRL 8260B P6J001910.019 10/4/16 3:52 ANGmg/kg dry 0.0012Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
84-123108 %Dibromofluoromethane
76-12998 %Toluene-d8
Volatile Petroleum Hydrocarbons by GC/PID/FID
BRL MADEP VPH P6J00381002510/5/16 20:15 ANGmg/kg dry 0.78C5-C8 Aliphatics
BRL MADEP VPH P6J00381002510/5/16 20:15 ANGmg/kg dry 3.0C9-C12 Aliphatics
BRL MADEP VPH P6J00381002510/5/16 20:15 ANGmg/kg dry 0.24C9-C10 Aromatics
Surrogate Recovery Control Limits
70-130123 %2,5-Dibromotoluene (PID)
70-130105 %2,5-Dibromotoluene (FID)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0019 - 5035
Blank (P6J0019-BLK1)Prepared: 10/03/16 Analyzed: 10/04/16
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0019 - 5035
Blank (P6J0019-BLK1)Prepared: 10/03/16 Analyzed: 10/04/16
Methylene Chloride mg/kg wetBRL0.0050
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.7
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.6
ug/L 50.00 76-129Surrogate: Toluene-d8 10050.0
LCS (P6J0019-BS1)Prepared: 10/03/16 Analyzed: 10/04/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0436 0.0050 0.05000 72-11587
1,1,1-Trichloroethane mg/kg wet0.0416 0.0050 0.05000 67-13183
1,1,2,2-Tetrachloroethane mg/kg wet0.0442 0.0050 0.05000 56-12688
1,1,2-Trichloroethane mg/kg wet0.0432 0.0050 0.05000 70-13386
1,1-Dichloroethane mg/kg wet0.0429 0.0050 0.05000 74-12786
1,1-Dichloroethylene mg/kg wet0.0409 0.0050 0.05000 67-14982
1,1-Dichloropropylene mg/kg wet0.0391 0.0050 0.05000 71-13078
1,2,3-Trichlorobenzene mg/kg wet0.0454 0.0050 0.05000 68-13091
1,2,3-Trichloropropane mg/kg wet0.0430 0.0050 0.05000 60-13786
1,2,4-Trichlorobenzene mg/kg wet0.0451 0.0050 0.05000 66-12590
1,2,4-Trimethylbenzene mg/kg wet0.0436 0.0050 0.05000 69-12987
1,2-Dibromoethane mg/kg wet0.0478 0.0050 0.05000 70-13296
1,2-Dichlorobenzene mg/kg wet0.0458 0.0050 0.05000 72-12392
1,2-Dichloroethane mg/kg wet0.0432 0.0050 0.05000 68-12886
1,2-Dichloropropane mg/kg wet0.0415 0.0050 0.05000 73-13083
1,3,5-Trimethylbenzene mg/kg wet0.0436 0.0050 0.05000 69-12887
1,3-Dichlorobenzene mg/kg wet0.0430 0.0050 0.05000 71-12086
1,3-Dichloropropane mg/kg wet0.0421 0.0050 0.05000 75-12484
1,4-Dichlorobenzene mg/kg wet0.0432 0.0050 0.05000 71-12386
2,2-Dichloropropane mg/kg wet0.0420 0.0050 0.05000 50-14284
2-Chlorotoluene mg/kg wet0.0440 0.0050 0.05000 67-12488
4-Chlorotoluene mg/kg wet0.0426 0.0050 0.05000 71-12685
4-Isopropyltoluene mg/kg wet0.0431 0.0050 0.05000 68-12986
Acetone mg/kg wet0.0896 0.050 0.1000 29-19890
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0019 - 5035
LCS (P6J0019-BS1)Prepared: 10/03/16 Analyzed: 10/04/16
Benzene mg/kg wet0.0434 0.0030 0.05000 74-12787
Bromobenzene mg/kg wet0.0448 0.0050 0.05000 73-12590
Bromochloromethane mg/kg wet0.0450 0.0050 0.05000 72-13490
Bromodichloromethane mg/kg wet0.0446 0.0050 0.05000 75-12289
Bromoform mg/kg wet0.0448 0.0050 0.05000 66-13590
Bromomethane mg/kg wet0.0433 0.010 0.05000 20-18087
Carbon Tetrachloride mg/kg wet0.0401 0.0050 0.05000 64-14380
Chlorobenzene mg/kg wet0.0436 0.0050 0.05000 74-11887
Chloroethane mg/kg wet0.0431 0.010 0.05000 33-14986
Chloroform mg/kg wet0.0427 0.0050 0.05000 73-12785
Chloromethane mg/kg wet0.0450 0.0050 0.05000 45-14390
cis-1,2-Dichloroethylene mg/kg wet0.0445 0.0050 0.05000 76-13489
cis-1,3-Dichloropropylene mg/kg wet0.0446 0.0050 0.05000 71-12589
Dibromochloromethane mg/kg wet0.0449 0.0050 0.05000 73-12290
Dichlorodifluoromethane mg/kg wet0.0390 0.0050 0.05000 26-14678
Ethylbenzene mg/kg wet0.0418 0.0050 0.05000 74-12884
Isopropyl Ether mg/kg wet0.0443 0.0050 0.05000 59-15989
Isopropylbenzene (Cumene)mg/kg wet0.0415 0.0050 0.05000 68-12683
m,p-Xylenes mg/kg wet0.0845 0.010 0.1000 75-12484
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0477 0.050 0.05000 J61-15795
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0475 0.10 0.05000 J63-14995
Methyl Isobutyl Ketone mg/kg wet0.0500 0.050 0.05000 57-162100
Methylene Chloride mg/kg wet0.0430 0.0050 0.05000 74-12986
Methyl-tert-Butyl Ether mg/kg wet0.0462 0.010 0.05000 70-13092
Naphthalene mg/kg wet0.0471 0.010 0.05000 57-15794
n-Butylbenzene mg/kg wet0.0425 0.0050 0.05000 65-13585
n-Propylbenzene mg/kg wet0.0420 0.0050 0.05000 67-13084
o-Xylene mg/kg wet0.0423 0.0050 0.05000 74-12685
sec-Butylbenzene mg/kg wet0.0406 0.0050 0.05000 66-13181
Styrene mg/kg wet0.0464 0.0050 0.05000 77-12193
tert-Butylbenzene mg/kg wet0.0399 0.0050 0.05000 67-13280
Tetrachloroethylene mg/kg wet0.0386 0.0050 0.05000 68-13077
Toluene mg/kg wet0.0428 0.0050 0.05000 71-12986
trans-1,2-Dichloroethylene mg/kg wet0.0426 0.0050 0.05000 73-13285
trans-1,3-Dichloropropylene mg/kg wet0.0441 0.0050 0.05000 68-12388
Trichloroethylene mg/kg wet0.0439 0.0050 0.05000 75-13388
Trichlorofluoromethane mg/kg wet0.0409 0.0050 0.05000 44-14682
Vinyl acetate mg/kg wet0.0488 0.025 0.05000 85-16198
Vinyl chloride mg/kg wet0.0406 0.0050 0.05000 48-14781
Xylenes, total mg/kg wet0.127 0.015 0.1500 74-12685
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.4
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 76-129Surrogate: Toluene-d8 9848.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0019 - 5035
LCS Dup (P6J0019-BSD1)Prepared: 10/03/16 Analyzed: 10/04/16
1,1,1,2-Tetrachloroethane mg/kg wet0.0437 0.0050 0.05000 2072-11587 0.3
1,1,1-Trichloroethane mg/kg wet0.0402 0.0050 0.05000 2067-13180 3
1,1,2,2-Tetrachloroethane mg/kg wet0.0422 0.0050 0.05000 2056-12684 5
1,1,2-Trichloroethane mg/kg wet0.0424 0.0050 0.05000 2070-13385 2
1,1-Dichloroethane mg/kg wet0.0427 0.0050 0.05000 2074-12785 0.4
1,1-Dichloroethylene mg/kg wet0.0393 0.0050 0.05000 2067-14979 4
1,1-Dichloropropylene mg/kg wet0.0384 0.0050 0.05000 2071-13077 2
1,2,3-Trichlorobenzene mg/kg wet0.0447 0.0050 0.05000 2068-13089 2
1,2,3-Trichloropropane mg/kg wet0.0433 0.0050 0.05000 2060-13787 0.7
1,2,4-Trichlorobenzene mg/kg wet0.0432 0.0050 0.05000 2066-12586 4
1,2,4-Trimethylbenzene mg/kg wet0.0426 0.0050 0.05000 2069-12985 2
1,2-Dibromoethane mg/kg wet0.0479 0.0050 0.05000 2070-13296 0.1
1,2-Dichlorobenzene mg/kg wet0.0464 0.0050 0.05000 2072-12393 1
1,2-Dichloroethane mg/kg wet0.0430 0.0050 0.05000 2068-12886 0.5
1,2-Dichloropropane mg/kg wet0.0429 0.0050 0.05000 2073-13086 3
1,3,5-Trimethylbenzene mg/kg wet0.0425 0.0050 0.05000 2069-12885 3
1,3-Dichlorobenzene mg/kg wet0.0430 0.0050 0.05000 2071-12086 0.2
1,3-Dichloropropane mg/kg wet0.0413 0.0050 0.05000 2075-12483 2
1,4-Dichlorobenzene mg/kg wet0.0431 0.0050 0.05000 2071-12386 0.3
2,2-Dichloropropane mg/kg wet0.0412 0.0050 0.05000 2050-14282 2
2-Chlorotoluene mg/kg wet0.0434 0.0050 0.05000 2067-12487 1
4-Chlorotoluene mg/kg wet0.0418 0.0050 0.05000 2071-12684 2
4-Isopropyltoluene mg/kg wet0.0414 0.0050 0.05000 2068-12983 4
Acetone mg/kg wet0.0850 0.050 0.1000 2029-19885 5
Benzene mg/kg wet0.0427 0.0030 0.05000 2074-12785 2
Bromobenzene mg/kg wet0.0439 0.0050 0.05000 2073-12588 2
Bromochloromethane mg/kg wet0.0441 0.0050 0.05000 2072-13488 2
Bromodichloromethane mg/kg wet0.0445 0.0050 0.05000 2075-12289 0.1
Bromoform mg/kg wet0.0435 0.0050 0.05000 2066-13587 3
Bromomethane mg/kg wet0.0416 0.010 0.05000 2020-18083 4
Carbon Tetrachloride mg/kg wet0.0409 0.0050 0.05000 2064-14382 2
Chlorobenzene mg/kg wet0.0428 0.0050 0.05000 2074-11886 2
Chloroethane mg/kg wet0.0392 0.010 0.05000 2033-14978 9
Chloroform mg/kg wet0.0426 0.0050 0.05000 2073-12785 0.3
Chloromethane mg/kg wet0.0432 0.0050 0.05000 2045-14386 4
cis-1,2-Dichloroethylene mg/kg wet0.0439 0.0050 0.05000 2076-13488 1
cis-1,3-Dichloropropylene mg/kg wet0.0459 0.0050 0.05000 2071-12592 3
Dibromochloromethane mg/kg wet0.0438 0.0050 0.05000 2073-12288 2
Dichlorodifluoromethane mg/kg wet0.0364 0.0050 0.05000 2026-14673 7
Ethylbenzene mg/kg wet0.0403 0.0050 0.05000 2074-12881 4
Isopropyl Ether mg/kg wet0.0446 0.0050 0.05000 2059-15989 0.7
Isopropylbenzene (Cumene)mg/kg wet0.0398 0.0050 0.05000 2068-12680 4
m,p-Xylenes mg/kg wet0.0820 0.010 0.1000 2075-12482 3
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0441 0.050 0.05000 20 J61-15788 8
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0433 0.10 0.05000 20 J63-14987 9
Methyl Isobutyl Ketone mg/kg wet0.0466 0.050 0.05000 20 J57-16293 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P6J0019 - 5035
LCS Dup (P6J0019-BSD1)Prepared: 10/03/16 Analyzed: 10/04/16
Methylene Chloride mg/kg wet0.0430 0.0050 0.05000 2074-12986 0.02
Methyl-tert-Butyl Ether mg/kg wet0.0458 0.010 0.05000 2070-13092 1
Naphthalene mg/kg wet0.0458 0.010 0.05000 2057-15792 3
n-Butylbenzene mg/kg wet0.0406 0.0050 0.05000 2065-13581 5
n-Propylbenzene mg/kg wet0.0404 0.0050 0.05000 2067-13081 4
o-Xylene mg/kg wet0.0418 0.0050 0.05000 2074-12684 1
sec-Butylbenzene mg/kg wet0.0394 0.0050 0.05000 2066-13179 3
Styrene mg/kg wet0.0447 0.0050 0.05000 2077-12189 4
tert-Butylbenzene mg/kg wet0.0388 0.0050 0.05000 2067-13278 3
Tetrachloroethylene mg/kg wet0.0389 0.0050 0.05000 2068-13078 0.7
Toluene mg/kg wet0.0416 0.0050 0.05000 2071-12983 3
trans-1,2-Dichloroethylene mg/kg wet0.0424 0.0050 0.05000 2073-13285 0.4
trans-1,3-Dichloropropylene mg/kg wet0.0438 0.0050 0.05000 2068-12388 0.6
Trichloroethylene mg/kg wet0.0435 0.0050 0.05000 2075-13387 0.8
Trichlorofluoromethane mg/kg wet0.0388 0.0050 0.05000 2044-14678 5
Vinyl acetate mg/kg wet0.0461 0.025 0.05000 2085-16192 6
Vinyl chloride mg/kg wet0.0384 0.0050 0.05000 2048-14777 6
Xylenes, total mg/kg wet0.124 0.015 0.1500 2074-12683 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.5
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10050.0
ug/L 50.00 76-129Surrogate: Toluene-d8 9949.4
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
Blank (P6J0029-BLK1)Prepared & Analyzed: 10/04/16
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
Blank (P6J0029-BLK1)Prepared & Analyzed: 10/04/16
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.327 39-132Surrogate: 2,4,6-Tribromophenol 832.75
mg/kg wet 1.663 44-115Surrogate: 2-Fluorobiphenyl 751.25
mg/kg wet 3.327 35-115Surrogate: 2-Fluorophenol 732.44
mg/kg wet 1.663 37-122Surrogate: Nitrobenzene-d5 651.07
mg/kg wet 3.327 34-121Surrogate: Phenol-d5 692.29
mg/kg wet 1.663 54-127Surrogate: Terphenyl-d14 761.27
LCS (P6J0029-BS1)Prepared & Analyzed: 10/04/16
1,2,4-Trichlorobenzene mg/kg wet1.09 0.33 1.665 34-11866
1,2-Dichlorobenzene mg/kg wet1.04 0.33 1.665 33-11763
1,3-Dichlorobenzene mg/kg wet0.980 0.33 1.665 30-11559
1,4-Dichlorobenzene mg/kg wet0.988 0.33 1.665 31-11559
1-Methylnaphthalene mg/kg wet1.06 0.33 1.665 40-11964
2,4,6-Trichlorophenol mg/kg wet1.20 0.33 1.665 39-12672
2,4-Dichlorophenol mg/kg wet1.15 0.33 1.665 40-12269
2,4-Dimethylphenol mg/kg wet1.41 0.33 1.665 30-12784
2,4-Dinitrophenol mg/kg wet0.968 0.33 1.665 27-12958
2,4-Dinitrotoluene mg/kg wet1.13 0.33 1.665 48-12668
2,6-Dinitrotoluene mg/kg wet1.13 0.33 1.665 46-12468
2-Chloronaphthalene mg/kg wet1.44 0.33 1.665 41-11486
2-Chlorophenol mg/kg wet1.13 0.33 1.665 34-12168
2-Methylnaphthalene mg/kg wet1.06 0.33 1.665 38-12263
2-Methylphenol mg/kg wet1.10 0.33 1.665 32-12266
2-Nitrophenol mg/kg wet1.07 0.33 1.665 36-12364
3,3’-Dichlorobenzidine mg/kg wet1.11 0.33 1.665 22-12167
3/4-Methylphenol mg/kg wet1.09 0.33 1.665 34-11966
4,6-Dinitro-2-methylphenol mg/kg wet1.17 0.33 1.665 29-13270
4-Bromophenyl phenyl ether mg/kg wet1.16 0.33 1.665 46-12469
4-Chloro-3-methylphenol mg/kg wet1.25 0.33 1.665 45-12275
4-Chloroaniline mg/kg wet0.939 0.33 1.665 17-10656
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
LCS (P6J0029-BS1)Prepared & Analyzed: 10/04/16
4-Chlorophenyl phenyl ether mg/kg wet1.09 0.33 1.665 45-12165
4-Nitrophenol mg/kg wet1.23 0.33 1.665 30-13274
Acenaphthene mg/kg wet1.09 0.33 1.665 40-12366
Acenaphthylene mg/kg wet1.15 0.33 1.665 32-13269
Anthracene mg/kg wet1.25 0.33 1.665 47-12375
Azobenzene mg/kg wet1.19 0.33 1.665 39-12571
Benzo(a)anthracene mg/kg wet1.18 0.33 1.665 49-12671
Benzo(a)pyrene mg/kg wet1.20 0.33 1.665 45-12972
Benzo(b)fluoranthene mg/kg wet1.17 0.33 1.665 45-13270
Benzo(g,h,i)perylene mg/kg wet1.18 0.33 1.665 43-13471
Benzo(k)fluoranthene mg/kg wet1.32 0.33 1.665 47-13279
Benzoic Acid mg/kg wet0.427 0.33 1.665 10-8326
Benzyl alcohol mg/kg wet1.01 0.33 1.665 29-12261
bis(2-Chloroethoxy)methane mg/kg wet0.956 0.33 1.665 36-12157
Bis(2-Chloroethyl)ether mg/kg wet0.901 0.33 1.665 31-12054
Bis(2-chloroisopropyl)ether mg/kg wet0.894 0.33 1.665 33-13154
Bis(2-Ethylhexyl)phthalate mg/kg wet1.17 0.33 1.665 51-13371
Butyl benzyl phthalate mg/kg wet1.16 0.33 1.665 48-13270
Chrysene mg/kg wet1.28 0.33 1.665 50-12477
Dibenzo(a,h)anthracene mg/kg wet1.18 0.33 1.665 45-13471
Dibenzofuran mg/kg wet1.20 0.33 1.665 44-12072
Diethyl phthalate mg/kg wet1.29 0.33 1.665 50-12477
Dimethyl phthalate mg/kg wet1.24 0.33 1.665 48-12474
Di-n-butyl phthalate mg/kg wet1.37 0.33 1.665 51-12882
Di-n-octyl phthalate mg/kg wet1.27 0.33 1.665 45-14076
Fluoranthene mg/kg wet1.27 0.33 1.665 50-12776
Fluorene mg/kg wet1.16 0.33 1.665 43-12570
Hexachlorobenzene mg/kg wet1.28 0.33 1.665 45-12277
Hexachlorobutadiene mg/kg wet1.17 0.33 1.665 32-12370
Hexachlorocyclopentadiene mg/kg wet1.24 0.33 1.665 32-11774
Hexachloroethane mg/kg wet1.04 0.33 1.665 28-11763
Indeno(1,2,3-cd)pyrene mg/kg wet1.20 0.33 1.665 45-13372
Isophorone mg/kg wet1.05 0.33 1.665 30-12263
Naphthalene mg/kg wet1.07 0.33 1.665 35-12364
Nitrobenzene mg/kg wet1.09 0.33 1.665 34-12265
N-Nitroso-di-n-propylamine mg/kg wet0.973 0.33 1.665 36-12058
N-Nitrosodiphenylamine mg/kg wet1.15 0.33 1.665 38-12769
Pentachlorophenol mg/kg wet1.22 0.33 1.665 25-13373
Phenanthrene mg/kg wet1.25 0.33 1.665 50-12175
Phenol mg/kg wet1.12 0.33 1.665 34-12167
Pyrene mg/kg wet1.21 0.33 1.665 47-12772
mg/kg wet 3.330 39-132Surrogate: 2,4,6-Tribromophenol 782.60
mg/kg wet 1.665 44-115Surrogate: 2-Fluorobiphenyl 711.19
mg/kg wet 3.330 35-115Surrogate: 2-Fluorophenol 712.37
mg/kg wet 1.665 37-122Surrogate: Nitrobenzene-d5 641.07
mg/kg wet 3.330 34-121Surrogate: Phenol-d5 632.11
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
LCS (P6J0029-BS1)Prepared & Analyzed: 10/04/16
mg/kg wet 1.665 54-127Surrogate: Terphenyl-d14 681.13
LCS Dup (P6J0029-BSD1)Prepared & Analyzed: 10/04/16
1,2,4-Trichlorobenzene mg/kg wet1.10 0.33 1.667 2034-11866 1
1,2-Dichlorobenzene mg/kg wet1.00 0.33 1.667 2033-11760 4
1,3-Dichlorobenzene mg/kg wet0.978 0.33 1.667 2030-11559 0.2
1,4-Dichlorobenzene mg/kg wet1.01 0.33 1.667 2031-11561 2
1-Methylnaphthalene mg/kg wet1.03 0.33 1.667 2040-11962 2
2,4,6-Trichlorophenol mg/kg wet1.27 0.33 1.667 2039-12676 6
2,4-Dichlorophenol mg/kg wet1.15 0.33 1.667 2040-12269 0.01
2,4-Dimethylphenol mg/kg wet1.40 0.33 1.667 2030-12784 0.7
2,4-Dinitrophenol mg/kg wet0.908 0.33 1.667 2027-12954 6
2,4-Dinitrotoluene mg/kg wet1.20 0.33 1.667 2048-12672 6
2,6-Dinitrotoluene mg/kg wet1.19 0.33 1.667 2046-12472 5
2-Chloronaphthalene mg/kg wet1.50 0.33 1.667 2041-11490 4
2-Chlorophenol mg/kg wet1.13 0.33 1.667 2034-12168 0.6
2-Methylnaphthalene mg/kg wet1.07 0.33 1.667 2038-12264 1
2-Methylphenol mg/kg wet1.10 0.33 1.667 2032-12266 0.3
2-Nitrophenol mg/kg wet1.10 0.33 1.667 2036-12366 3
3,3’-Dichlorobenzidine mg/kg wet1.14 0.33 1.667 2022-12168 2
3/4-Methylphenol mg/kg wet1.12 0.33 1.667 2034-11967 3
4,6-Dinitro-2-methylphenol mg/kg wet1.05 0.33 1.667 2029-13263 11
4-Bromophenyl phenyl ether mg/kg wet1.16 0.33 1.667 2046-12469 0.2
4-Chloro-3-methylphenol mg/kg wet1.26 0.33 1.667 2045-12276 0.6
4-Chloroaniline mg/kg wet0.906 0.33 1.667 2017-10654 4
4-Chlorophenyl phenyl ether mg/kg wet1.16 0.33 1.667 2045-12170 7
4-Nitrophenol mg/kg wet1.20 0.33 1.667 2030-13272 2
Acenaphthene mg/kg wet1.11 0.33 1.667 2040-12367 2
Acenaphthylene mg/kg wet1.17 0.33 1.667 2032-13270 2
Anthracene mg/kg wet1.27 0.33 1.667 2047-12376 1
Azobenzene mg/kg wet1.19 0.33 1.667 2039-12571 0.3
Benzo(a)anthracene mg/kg wet1.26 0.33 1.667 2049-12676 7
Benzo(a)pyrene mg/kg wet1.24 0.33 1.667 2045-12974 3
Benzo(b)fluoranthene mg/kg wet1.19 0.33 1.667 2045-13271 2
Benzo(g,h,i)perylene mg/kg wet1.20 0.33 1.667 2043-13472 1
Benzo(k)fluoranthene mg/kg wet1.35 0.33 1.667 2047-13281 2
Benzoic Acid mg/kg wet0.407 0.33 1.667 2010-8324 5
Benzyl alcohol mg/kg wet1.02 0.33 1.667 2029-12261 0.9
bis(2-Chloroethoxy)methane mg/kg wet0.939 0.33 1.667 2036-12156 2
Bis(2-Chloroethyl)ether mg/kg wet0.916 0.33 1.667 2031-12055 2
Bis(2-chloroisopropyl)ether mg/kg wet0.886 0.33 1.667 2033-13153 0.9
Bis(2-Ethylhexyl)phthalate mg/kg wet1.23 0.33 1.667 2051-13374 4
Butyl benzyl phthalate mg/kg wet1.22 0.33 1.667 2048-13273 5
Chrysene mg/kg wet1.26 0.33 1.667 2050-12476 0.9
Dibenzo(a,h)anthracene mg/kg wet1.22 0.33 1.667 2045-13473 3
Dibenzofuran mg/kg wet1.24 0.33 1.667 2044-12074 3
Diethyl phthalate mg/kg wet1.33 0.33 1.667 2050-12480 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
LCS Dup (P6J0029-BSD1)Prepared & Analyzed: 10/04/16
Dimethyl phthalate mg/kg wet1.31 0.33 1.667 2048-12478 6
Di-n-butyl phthalate mg/kg wet1.42 0.33 1.667 2051-12885 4
Di-n-octyl phthalate mg/kg wet1.30 0.33 1.667 2045-14078 2
Fluoranthene mg/kg wet1.28 0.33 1.667 2050-12777 0.7
Fluorene mg/kg wet1.20 0.33 1.667 2043-12572 3
Hexachlorobenzene mg/kg wet1.31 0.33 1.667 2045-12279 2
Hexachlorobutadiene mg/kg wet1.13 0.33 1.667 2032-12368 4
Hexachlorocyclopentadiene mg/kg wet1.20 0.33 1.667 2032-11772 4
Hexachloroethane mg/kg wet1.03 0.33 1.667 2028-11762 1
Indeno(1,2,3-cd)pyrene mg/kg wet1.24 0.33 1.667 2045-13375 3
Isophorone mg/kg wet1.05 0.33 1.667 2030-12263 0.4
Naphthalene mg/kg wet1.07 0.33 1.667 2035-12364 0.3
Nitrobenzene mg/kg wet1.06 0.33 1.667 2034-12264 3
N-Nitroso-di-n-propylamine mg/kg wet0.944 0.33 1.667 2036-12057 3
N-Nitrosodiphenylamine mg/kg wet1.14 0.33 1.667 2038-12768 0.6
Pentachlorophenol mg/kg wet1.16 0.33 1.667 2025-13370 5
Phenanthrene mg/kg wet1.25 0.33 1.667 2050-12175 0.09
Phenol mg/kg wet1.08 0.33 1.667 2034-12165 3
Pyrene mg/kg wet1.23 0.33 1.667 2047-12774 2
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 772.57
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 691.16
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 672.23
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 601.00
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 622.08
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 671.11
Matrix Spike (P6J0029-MS1)Prepared & Analyzed: 10/04/16 Source: 6090524-01
1,2,4-Trichlorobenzene mg/kg dry1.22 0.44 2.246 BRL 34-11854
1,2-Dichlorobenzene mg/kg dry1.14 0.44 2.246 BRL 33-11751
1,3-Dichlorobenzene mg/kg dry1.08 0.44 2.246 BRL 30-11548
1,4-Dichlorobenzene mg/kg dry1.12 0.44 2.246 BRL 31-11550
1-Methylnaphthalene mg/kg dry1.18 0.44 2.246 BRL 40-11953
2,4,6-Trichlorophenol mg/kg dry1.31 0.44 2.246 BRL 39-12658
2,4-Dichlorophenol mg/kg dry1.30 0.44 2.246 BRL 40-12258
2,4-Dimethylphenol mg/kg dry1.51 0.44 2.246 BRL 30-12767
2,4-Dinitrophenol mg/kg dry1.18 0.44 2.246 BRL 27-12953
2,4-Dinitrotoluene mg/kg dry1.33 0.44 2.246 BRL 48-12659
2,6-Dinitrotoluene mg/kg dry1.34 0.44 2.246 BRL 46-12460
2-Chloronaphthalene mg/kg dry1.65 0.44 2.246 BRL 41-11474
2-Chlorophenol mg/kg dry1.30 0.44 2.246 BRL 34-12158
2-Methylnaphthalene mg/kg dry1.22 0.44 2.246 BRL 38-12254
2-Methylphenol mg/kg dry1.25 0.44 2.246 BRL 32-12256
2-Nitrophenol mg/kg dry1.29 0.44 2.246 BRL 36-12357
3,3’-Dichlorobenzidine mg/kg dry1.02 0.44 2.246 BRL 22-12145
3/4-Methylphenol mg/kg dry1.23 0.44 2.246 BRL 34-11955
4,6-Dinitro-2-methylphenol mg/kg dry1.34 0.44 2.246 BRL 29-13259
4-Bromophenyl phenyl ether mg/kg dry1.27 0.44 2.246 BRL 46-12457
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
Matrix Spike (P6J0029-MS1)Prepared & Analyzed: 10/04/16 Source: 6090524-01
4-Chloro-3-methylphenol mg/kg dry1.37 0.44 2.246 BRL 45-12261
4-Chloroaniline mg/kg dry0.985 0.44 2.246 BRL 17-10644
4-Chlorophenyl phenyl ether mg/kg dry1.23 0.44 2.246 BRL 45-12155
4-Nitrophenol mg/kg dry1.39 0.44 2.246 BRL 30-13262
Acenaphthene mg/kg dry1.24 0.44 2.246 BRL 40-12355
Acenaphthylene mg/kg dry1.32 0.44 2.246 BRL 32-13259
Anthracene mg/kg dry1.42 0.44 2.246 BRL 47-12363
Azobenzene mg/kg dry1.35 0.44 2.246 BRL 39-12560
Benzo(a)anthracene mg/kg dry1.36 0.44 2.246 BRL 49-12661
Benzo(a)pyrene mg/kg dry1.34 0.44 2.246 BRL 45-12960
Benzo(b)fluoranthene mg/kg dry1.37 0.44 2.246 BRL 45-13261
Benzo(g,h,i)perylene mg/kg dry1.29 0.44 2.246 BRL 43-13457
Benzo(k)fluoranthene mg/kg dry1.56 0.44 2.246 BRL 47-13269
Benzoic Acid mg/kg dry0.602 0.44 2.246 BRL 10-8327
Benzyl alcohol mg/kg dry1.23 0.44 2.246 BRL 29-12255
bis(2-Chloroethoxy)methane mg/kg dry1.09 0.44 2.246 BRL 36-12148
Bis(2-Chloroethyl)ether mg/kg dry1.05 0.44 2.246 BRL 31-12047
Bis(2-chloroisopropyl)ether mg/kg dry1.02 0.44 2.246 BRL 33-13145
Bis(2-Ethylhexyl)phthalate mg/kg dry1.35 0.44 2.246 BRL 51-13360
Butyl benzyl phthalate mg/kg dry1.36 0.44 2.246 BRL 48-13261
Chrysene mg/kg dry1.46 0.44 2.246 BRL 50-12465
Dibenzo(a,h)anthracene mg/kg dry1.33 0.44 2.246 BRL 45-13459
Dibenzofuran mg/kg dry1.37 0.44 2.246 BRL 44-12061
Diethyl phthalate mg/kg dry1.46 0.44 2.246 BRL 50-12465
Dimethyl phthalate mg/kg dry1.46 0.44 2.246 BRL 48-12465
Di-n-butyl phthalate mg/kg dry1.56 0.44 2.246 BRL 51-12870
Di-n-octyl phthalate mg/kg dry1.39 0.44 2.246 BRL 45-14062
Fluoranthene mg/kg dry1.45 0.44 2.246 BRL 50-12765
Fluorene mg/kg dry1.32 0.44 2.246 BRL 43-12559
Hexachlorobenzene mg/kg dry1.43 0.44 2.246 BRL 45-12264
Hexachlorobutadiene mg/kg dry1.25 0.44 2.246 BRL 32-12356
Hexachlorocyclopentadiene mg/kg dry1.16 0.44 2.246 BRL 32-11751
Hexachloroethane mg/kg dry1.09 0.44 2.246 BRL 28-11748
Indeno(1,2,3-cd)pyrene mg/kg dry1.12 0.44 2.246 BRL 45-13350
Isophorone mg/kg dry1.21 0.44 2.246 BRL 30-12254
Naphthalene mg/kg dry1.20 0.44 2.246 BRL 35-12353
Nitrobenzene mg/kg dry1.19 0.44 2.246 BRL 34-12253
N-Nitroso-di-n-propylamine mg/kg dry1.10 0.44 2.246 BRL 36-12049
N-Nitrosodiphenylamine mg/kg dry1.31 0.44 2.246 BRL 38-12758
Pentachlorophenol mg/kg dry1.05 0.44 2.246 BRL 25-13347
Phenanthrene mg/kg dry1.42 0.44 2.246 BRL 50-12163
Phenol mg/kg dry1.27 0.44 2.246 BRL 34-12156
Pyrene mg/kg dry1.38 0.44 2.246 BRL 47-12761
mg/kg dry 4.492 39-132Surrogate: 2,4,6-Tribromophenol 582.62
mg/kg dry 2.246 44-115Surrogate: 2-Fluorobiphenyl 591.32
mg/kg dry 4.492 35-115Surrogate: 2-Fluorophenol 572.57
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
Matrix Spike (P6J0029-MS1)Prepared & Analyzed: 10/04/16 Source: 6090524-01
mg/kg dry 2.246 37-122Surrogate: Nitrobenzene-d5 541.20
mg/kg dry 4.492 34-121Surrogate: Phenol-d5 542.44
mg/kg dry 2.246 54-127Surrogate: Terphenyl-d14 571.28
Matrix Spike Dup (P6J0029-MSD1)Prepared & Analyzed: 10/04/16 Source: 6090524-01
1,2,4-Trichlorobenzene mg/kg dry1.32 0.45 2.248 BRL 2034-11859 8
1,2-Dichlorobenzene mg/kg dry1.25 0.45 2.248 BRL 2033-11756 9
1,3-Dichlorobenzene mg/kg dry1.16 0.45 2.248 BRL 2030-11551 7
1,4-Dichlorobenzene mg/kg dry1.20 0.45 2.248 BRL 2031-11553 7
1-Methylnaphthalene mg/kg dry1.30 0.45 2.248 BRL 2040-11958 9
2,4,6-Trichlorophenol mg/kg dry1.50 0.45 2.248 BRL 2039-12667 14
2,4-Dichlorophenol mg/kg dry1.45 0.45 2.248 BRL 2040-12264 11
2,4-Dimethylphenol mg/kg dry1.62 0.45 2.248 BRL 2030-12772 7
2,4-Dinitrophenol mg/kg dry1.12 0.45 2.248 BRL 2027-12950 5
2,4-Dinitrotoluene mg/kg dry1.43 0.45 2.248 BRL 2048-12664 7
2,6-Dinitrotoluene mg/kg dry1.40 0.45 2.248 BRL 2046-12462 4
2-Chloronaphthalene mg/kg dry1.82 0.45 2.248 BRL 2041-11481 10
2-Chlorophenol mg/kg dry1.39 0.45 2.248 BRL 2034-12162 7
2-Methylnaphthalene mg/kg dry1.32 0.45 2.248 BRL 2038-12259 8
2-Methylphenol mg/kg dry1.41 0.45 2.248 BRL 2032-12263 12
2-Nitrophenol mg/kg dry1.39 0.45 2.248 BRL 2036-12362 7
3,3’-Dichlorobenzidine mg/kg dry1.35 0.45 2.248 BRL 20 D22-12160 28
3/4-Methylphenol mg/kg dry1.35 0.45 2.248 BRL 2034-11960 9
4,6-Dinitro-2-methylphenol mg/kg dry1.35 0.45 2.248 BRL 2029-13260 1
4-Bromophenyl phenyl ether mg/kg dry1.39 0.45 2.248 BRL 2046-12462 9
4-Chloro-3-methylphenol mg/kg dry1.52 0.45 2.248 BRL 2045-12267 10
4-Chloroaniline mg/kg dry1.12 0.45 2.248 BRL 2017-10650 13
4-Chlorophenyl phenyl ether mg/kg dry1.39 0.45 2.248 BRL 2045-12162 12
4-Nitrophenol mg/kg dry1.52 0.45 2.248 BRL 2030-13268 9
Acenaphthene mg/kg dry1.36 0.45 2.248 BRL 2040-12361 9
Acenaphthylene mg/kg dry1.44 0.45 2.248 BRL 2032-13264 9
Anthracene mg/kg dry1.50 0.45 2.248 BRL 2047-12367 6
Azobenzene mg/kg dry1.42 0.45 2.248 BRL 2039-12563 5
Benzo(a)anthracene mg/kg dry1.51 0.45 2.248 BRL 2049-12667 10
Benzo(a)pyrene mg/kg dry1.50 0.45 2.248 BRL 2045-12967 12
Benzo(b)fluoranthene mg/kg dry1.40 0.45 2.248 BRL 2045-13262 2
Benzo(g,h,i)perylene mg/kg dry1.41 0.45 2.248 BRL 2043-13463 9
Benzo(k)fluoranthene mg/kg dry1.58 0.45 2.248 BRL 2047-13270 2
Benzoic Acid mg/kg dry0.569 0.45 2.248 BRL 2010-8325 6
Benzyl alcohol mg/kg dry1.33 0.45 2.248 BRL 2029-12259 8
bis(2-Chloroethoxy)methane mg/kg dry1.19 0.45 2.248 BRL 2036-12153 10
Bis(2-Chloroethyl)ether mg/kg dry1.21 0.45 2.248 BRL 2031-12054 14
Bis(2-chloroisopropyl)ether mg/kg dry1.13 0.45 2.248 BRL 2033-13150 11
Bis(2-Ethylhexyl)phthalate mg/kg dry1.50 0.45 2.248 BRL 2051-13367 11
Butyl benzyl phthalate mg/kg dry1.45 0.45 2.248 BRL 2048-13264 6
Chrysene mg/kg dry1.52 0.45 2.248 BRL 2050-12468 5
Dibenzo(a,h)anthracene mg/kg dry1.45 0.45 2.248 BRL 2045-13464 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P6J0029 - 3546
Matrix Spike Dup (P6J0029-MSD1)Prepared & Analyzed: 10/04/16 Source: 6090524-01
Dibenzofuran mg/kg dry1.51 0.45 2.248 BRL 2044-12067 9
Diethyl phthalate mg/kg dry1.60 0.45 2.248 BRL 2050-12471 9
Dimethyl phthalate mg/kg dry1.56 0.45 2.248 BRL 2048-12469 6
Di-n-butyl phthalate mg/kg dry1.66 0.45 2.248 BRL 2051-12874 6
Di-n-octyl phthalate mg/kg dry1.49 0.45 2.248 BRL 2045-14066 7
Fluoranthene mg/kg dry1.52 0.45 2.248 BRL 2050-12768 5
Fluorene mg/kg dry1.48 0.45 2.248 BRL 2043-12566 11
Hexachlorobenzene mg/kg dry1.55 0.45 2.248 BRL 2045-12269 8
Hexachlorobutadiene mg/kg dry1.43 0.45 2.248 BRL 2032-12364 13
Hexachlorocyclopentadiene mg/kg dry1.37 0.45 2.248 BRL 2032-11761 17
Hexachloroethane mg/kg dry1.30 0.45 2.248 BRL 2028-11758 18
Indeno(1,2,3-cd)pyrene mg/kg dry1.51 0.45 2.248 BRL 20 D45-13367 30
Isophorone mg/kg dry1.33 0.45 2.248 BRL 2030-12259 9
Naphthalene mg/kg dry1.29 0.45 2.248 BRL 2035-12358 8
Nitrobenzene mg/kg dry1.30 0.45 2.248 BRL 2034-12258 9
N-Nitroso-di-n-propylamine mg/kg dry1.19 0.45 2.248 BRL 2036-12053 8
N-Nitrosodiphenylamine mg/kg dry1.41 0.45 2.248 BRL 2038-12763 8
Pentachlorophenol mg/kg dry1.27 0.45 2.248 BRL 2025-13356 19
Phenanthrene mg/kg dry1.50 0.45 2.248 BRL 2050-12167 5
Phenol mg/kg dry1.39 0.45 2.248 BRL 2034-12162 9
Pyrene mg/kg dry1.54 0.45 2.248 BRL 2047-12768 11
mg/kg dry 4.497 39-132Surrogate: 2,4,6-Tribromophenol 693.10
mg/kg dry 2.248 44-115Surrogate: 2-Fluorobiphenyl 661.47
mg/kg dry 4.497 35-115Surrogate: 2-Fluorophenol 652.90
mg/kg dry 2.248 37-122Surrogate: Nitrobenzene-d5 561.26
mg/kg dry 4.497 34-121Surrogate: Phenol-d5 602.69
mg/kg dry 2.248 54-127Surrogate: Terphenyl-d14 621.40
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Batch P6J0038 - MADEP VPH (S)
Blank (P6J0038-BLK1)Prepared: 10/04/16 Analyzed: 10/05/16
C5-C8 Aliphatics mg/kg wetBRL5.0
C9-C12 Aliphatics mg/kg wetBRL5.0
C9-C10 Aromatics mg/kg wetBRL5.0
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (PID)10210.9
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (FID)889.37
LCS (P6J0038-BS1)Prepared: 10/04/16 Analyzed: 10/05/16
C5-C8 Aliphatics mg/kg wet35.9 5.0 32.00 70-130112
C9-C10 Aromatics mg/kg wet11.8 5.0 10.67 70-130110
C9-C12 Aliphatic mg/kg wet33.7 5.0 32.00 70-130105
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (PID)10110.8
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (FID)889.38
LCS Dup (P6J0038-BSD1)Prepared: 10/04/16 Analyzed: 10/05/16
C5-C8 Aliphatics mg/kg wet34.7 5.0 32.00 5070-130108 4
C9-C10 Aromatics mg/kg wet11.6 5.0 10.67 5070-130108 2
C9-C12 Aliphatic mg/kg wet32.8 5.0 32.00 5070-130102 3
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (PID)10210.9
mg/kg wet 10.67 70-130Surrogate: 2,5-Dibromotoluene (FID)899.52
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P6J0031 - 3546
Blank (P6J0031-BLK1)Prepared: 10/04/16 Analyzed: 10/05/16
C9-C18 Aliphatics mg/kg wetBRL25
C19-C36 Aliphatics mg/kg wetBRL25
C11-C22 Aromatics mg/kg wetBRL10
mg/kg wet 1.990 40-140Surrogate: 1-Chlorooctadecane 751.49
mg/kg wet 1.990 40-140Surrogate: o-Terphenyl 711.40
mg/kg wet 3.980 40-140Surrogate: 2-Fluorobiphenyl 823.28
mg/kg wet 3.980 40-140Surrogate: 2-Bromonaphthalene 953.79
LCS (P6J0031-BS1)Prepared: 10/04/16 Analyzed: 10/05/16
C9-C18 Aliphatics mg/kg wet30.6 25 59.88 40-14051
C19-C36 Aliphatics mg/kg wet61.1 25 79.84 40-14077
C11-C22 Aromatics mg/kg wet13010 169.7 40-14076
mg/kg wet 1.996 40-140Surrogate: 1-Chlorooctadecane 721.44
mg/kg wet 1.996 40-140Surrogate: o-Terphenyl 761.52
mg/kg wet 3.992 40-140Surrogate: 2-Fluorobiphenyl 893.56
mg/kg wet 3.992 40-140Surrogate: 2-Bromonaphthalene 983.90
LCS Dup (P6J0031-BSD1)Prepared: 10/04/16 Analyzed: 10/05/16
C9-C18 Aliphatics mg/kg wet31.1 25 59.94 5040-14052 2
C19-C36 Aliphatics mg/kg wet56.1 25 79.92 5040-14070 9
C11-C22 Aromatics mg/kg wet12210 169.8 5040-14072 6
mg/kg wet 1.998 40-140Surrogate: 1-Chlorooctadecane 741.47
mg/kg wet 1.998 40-140Surrogate: o-Terphenyl 741.49
mg/kg wet 3.996 40-140Surrogate: 2-Fluorobiphenyl 863.44
mg/kg wet 3.996 40-140Surrogate: 2-Bromonaphthalene 963.85
Matrix Spike (P6J0031-MS1)Prepared: 10/04/16 Analyzed: 10/05/16 Source: 6090524-01
C9-C18 Aliphatics mg/kg dry35.8 34 80.78 BRL 40-14044
C19-C36 Aliphatics mg/kg dry68.1 34 107.7 BRL 40-14063
C11-C22 Aromatics mg/kg dry14713 228.9 BRL 40-14064
mg/kg dry 2.693 40-140Surrogate: 1-Chlorooctadecane 651.76
mg/kg dry 2.693 40-140Surrogate: o-Terphenyl 681.82
mg/kg dry 5.386 40-140Surrogate: 2-Fluorobiphenyl 914.89
mg/kg dry 5.386 40-140Surrogate: 2-Bromonaphthalene 995.32
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Batch P6J0031 - 3546
Matrix Spike Dup (P6J0031-MSD1)Prepared: 10/04/16 Analyzed: 10/05/16 Source: 6090524-01
C9-C18 Aliphatics mg/kg dry36.1 34 80.78 BRL 5040-14045 0.7
C19-C36 Aliphatics mg/kg dry68.5 34 107.7 BRL 5040-14064 0.6
C11-C22 Aromatics mg/kg dry17013 228.9 BRL 5040-14074 15
mg/kg dry 2.693 40-140Surrogate: 1-Chlorooctadecane 671.80
mg/kg dry 2.693 40-140Surrogate: o-Terphenyl 681.84
mg/kg dry 5.386 40-140Surrogate: 2-Fluorobiphenyl 935.03
mg/kg dry 5.386 40-140Surrogate: 2-Bromonaphthalene 1035.54
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 42
10/6/16
Level II QC Report
2801 Yorkmont Rd. #100 Project No: 6228160369
Project: Spectrum S. TryonAMEC Foster Wheeler (Charlotte)
Charlotte, NC 28208
Attn: Rob Foster
Prism Work Order: 6090524
Time Submitted: 9/30/2016 1:50:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P6J0030 - Solids, Dry Weight
Duplicate (P6J0030-DUP2)Prepared & Analyzed: 10/03/16 Source: 6090524-01
% Solids % by Weight74.0 0.100 74.0 200.04
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 42
Sample Extraction Data
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P6J00316090524-01 10/04/16 11:4510.04 2g mL
P6J00316090524-02 10/04/16 11:4510.01 2g mL
P6J00316090524-03 10/04/16 11:4510.03 2g mL
P6J00316090524-04 10/04/16 11:4510.05 2g mL
P6J00316090524-05 10/04/16 11:4510.09 2g mL
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P6J00306090524-01 10/03/16 16:3430 30g g
P6J00306090524-02 10/03/16 16:3430 30g g
P6J00306090524-03 10/03/16 16:3430 30g g
P6J00306090524-04 10/03/16 16:3430 30g g
P6J00306090524-05 10/03/16 16:3430 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P6J00296090524-01 10/04/16 11:4530.06 1g mL
P6J00296090524-02 10/04/16 11:4530.12 1g mL
P6J00296090524-03 10/04/16 11:4530.1 1g mL
P6J00296090524-04 10/04/16 11:4530.13 1g mL
P6J00296090524-05 10/04/16 11:4530.01 1g mL
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P6J00196090524-01 10/03/16 8:524.39 5g mL
P6J00196090524-02 10/03/16 8:525.11 5g mL
P6J00196090524-03 10/03/16 8:525.33 5g mL
P6J00196090524-04 10/03/16 8:525.18 5g mL
P6J00196090524-05 10/03/16 8:525.05 5g mL
Prep Method: MADEP VPH (S)
Lab Number Batch Date/TimeInitialFinal
P6J00386090524-01 10/04/16 13:024.13 16g mL
P6J00386090524-02 10/04/16 13:024.42 16g mL
P6J00386090524-03 10/04/16 13:024.16 16g mL
P6J00386090524-04 10/04/16 13:025.03 16g mL
P6J00386090524-05 10/04/16 13:023.72 16g mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 42
Page 42 of 42