6001_Mecklenburg_Harrisburg_MSWLF_GW_FID1275373_20190116

I pENR USE ONLY: I I ❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
Prepare one form for each individually monitored unit.
Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Mecklenburg County Solid Waste Services
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Amber R. Grzymski, P.G. Phone: [phone]
E-mail: [e-mail]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006)
Harrisburg Road Landfill 7817 Harrisburg Road, Charlotte 60-01 .0500 December 5-6,18, 2018
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑X Detection Monitoring ❑ Assessment Monitoring ❑ Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells ❑R
Groundwater monitoring data from private water supply wells ❑
Leachate monitoring data
Surface water monitoring data ❑
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Amber R. Grzymski, P.G. Project Manager
Facility 139pr se entative Na4e LPria4-)--- f Title
1-16-2019
Date
2145 Suttle Ave, Charlotte, NC 28208
Facility Representative Address
NC PE Firm License Number (if applicable effective May 1, 2009)
980-314-3855
Code) Telephone Number
Affix NC Licc�MetWQj9j;jsional Geologist Seal
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Revised 6/2009

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MECKLENBURG COUNTY
Land Use and Environmental Services Agency
Solid Waste Services
January 16, 2019
Jaclynne Drummond
North Carolina Department of Environment
and Natural Resources
Division of Waste Management - Solid Waste Section
2090 US Highway 70
Swannanoa, NC 28778
Subject: Water Quality Monitoring Report December 2018
Harrisburg Road Landfill, Permit 60-01
Dear Ms. Drummond:
Mecklenburg County conducted semi-annual water quality monitoring at the closed
Harrisburg Road Landfill December 5 and December 6, 2018 in accordance with the
approved revised sample and analysis plan dated May 11, 2004. Samples were also
analyzed for 1,4-Dioxane and will continue to be in future sampling events. Samples
were collected from seven monitoring wells ( HBW-12B, HBW-14, HBW-17B, HBW-
20, HBW-21, HBW-22 and background well HBW-28), one potable well (MAINTE)
and, three surface -water sampling locations (HB2006, RB2008 and, HB2010).
Laboratory analytical data, field -measured data, and a table of results exceeding water
quality standards along with a preliminary explanation of the cause and significance are
included on the electronic data deliverable (EDD) submittal.
The EDD containing the monitoring data are labeled to reflect the units that are used for
reporting. Detection levels and applicable standards have been included for all sampling
locations. Surface water standards listed are the water quality standards established for
freshwater classification for aquatic life as outlined in 15A NCAC 213 "Classification and
Water Quality Standards Applicable to Surface Waters of North Carolina". Groundwater
standards listed are the standards outlined in 15A NCAC 2L "Classification of Water
Quality Standards applicable to the Groundwaters of North Carolina". If the sample is
reported in parts per billion, then the standard is also reported in parts per billion.
PEOPLE • PRIDE • PROGRESS • PARTNERSHIP
2145 Suttle Ave • Charlotte, NC 28208-5237 • [phone] • FAX [phone]
www.wipeoutwaste.com

Page 2
Surface -water samples:
Barium was detected in HB 2006, HB 2008 and HB 2010 at 28.6 ppb, 22.9 ppb and 44.3
ppb, respectively. No other analytes were detected in the surface water samples. Field -
measured parameters for surface -water samples were within the range of established
standards and are summarized in the table below.
Location
Temperature
PH
Specific
Conductivity
Dissolved
Oxygen
HB2006
9.70 C
7.3
0.167 ms/cm
11.22 mg/l
HB2008
10.20 C
7.1
0.171 ms/cm
11.40 mg/l
HB2010
9.10 C
6.8
0.246ms/cm
10.03 mg/1
Groundwater samples:
Multiple metals were detected above 21, standards. The table below summarizes metals
detections in groundwater samples.
Well ID
Ba
ug/l
Be
ug/l
Cd
ug/l
Cr
ug/l
Co
ug/l
Cu
ug/1
Ni
ug/l
Pb
ug/l
Th
ug/l
Vn
ug/l
Zn
ug/l
MAINTE
9.3
----
-----
-----
-----
86.9
-----
-----
----
5.5
46.6
HBW12B26.6
-----
-----
-----
-----
-----
-----
-----
------
11.1
-----
HB W 14
94.9
-----
-----
-----
-----
16.3
-----
-----
------
1 7.6
-----
HBW17B
63.5
-----
-----
-----
18.4
12.3
-----
-----
0.13
-----
15.7
HBW-20
7.9
-----
-----
-----
-----
----
-----
-----
------
5.2
-----
HBW-21
11.7
-----
-----
-----
-----
5.3
-----
-----
------
10.4
-----
HBW-22
35.2
-----
-----
37.8
-----
7.9
7.9
-----
-----
-----
-----
HBW-28*
32.0
-----
-----
12.0
13.4
45.8
-----
5.7
------
30.1
19.6
2L Std. ug/1
700
4
2.0
10
1
1,000
1 100
15
1 0.2
0.3
1,000
Note: Bolded results exceed 2L Standard, *Background Well
The following eight volatile organic compounds ("VOCs") were detected in the sample
collected from well HBW-17B:
VOC
Sample Result ug/l
21, Standard ug/l
Benzene
9.0
1
Tetrachloroeth lene
28.7
0.7
Trichloroeth lease
22.6
2.8
1,1-Dichloroethane
6.1
6
trans-1,2-Dichloroethane
1.3
100
1,2-Dichloro ro ane
9.4
0.6
cis-1,2 Dichloroethene
113
70-
X lens total
11.5
500
Vinyl Chloride
1.5
0.03
Note: Bolded results exceed 21, Standard
The pH was measured to be more acidic than the standard in the samples collected from
MAINTE, HBW 12B, HBW 14, HBW 17B, HBW20, HB W21, HB W22 and background
monitoring well HBW-28. Field -measured parameters for groundwater samples are
summarized in the following table:

Pai2e 3
Location
Tem erature
pH
Conductivity
HBW12B
14.9 °C
5.9
0.295 ms/cm
HBW14
15.9 °C
6.4
0.206 ms/cm
HBW17B
15.7 °C
5.0
0.058 ms/cm
HBW-20
15.9 °C
6.3
0.144 ms/cm
HBW-21
15.4 °C
5.6
0.171 ms/cm
HBW-22
16.7 °C
5.8
0.062 ms/cm
*HBW-28
15.7 °C
5.2
0.030 ms/cm
MAINTE
15.6 °C
6.4
0.063 ms/cm
Note: Bolded results are outside of the 6.5 to 8.5 S.U. range 2L Standard
*Background Well
Please call me at [phone], if you have any questions concerning this report.
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Sincerely,
A(: .1 ----a Amber R. Grzymski, P.G.
Project Manager
LUESA Solid Waste Services

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Landfill Gas Monitoring Data Form
Facility Name: Harrisburg Road Landfill Permit Number: 60-01
Date of Sampling: 12/18/2018 NC Landfill Rule (.0500 or .1600): .0500
Name and Position of Sample Collector: David E. Coleman, Environmental Specialist
Type and Serial Number of Gas Meter: Gem 2000 #GM13774
Calibration Date of Gas Meter: 8/21/2018 Date and Time of Field Calibration:12/18/18 3:11 PM
Type of Field Calibration Gas (15/15 or 35/50): _35/50_
Expiration Date of Field Calibration Gas Canister: June 2021
Pump Rate of Gas Meter: _120 Seconds _ Ambient Air Temperature: _53 Degrees
ees
Barometric Pressure: 29.26 General Weather Conditions: _Sunny, 8NE
Sample ID
Time
% LEL
% CH4
% CO2
% 02
Comments
MP-1
3:58 PM
>100
60.2
39.7
0
Methane Extraction System
MP-2
3:52 PM
>100
62.2
37.7
0
Methane Extraction System
MP-3
3:46 PM
2
0.1
0.2
21
Methane Extraction System
MP-4
3:43 PM
>100
40.1
28.8
6.4
Methane Extraction System
MP-5
4:25 PM
0
0
3.4
16.9
MP-6
4:30 PM
0
0
4.2
14.4
MP-7
4:37 PM
0
0
6.1
13
MP-8
4:44 PM
0
0
10
5.4
MP-9A
4:49 PM
0
0
0
21.3
MP-913
4:54 PM
0
0
4.9
13.3
MP-11
3:11 PM
>100
43.4
30.2
0.9
MP-12
3:23 PM
0
0
9.5
3.3
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and
attachments are true and correct. I am aware that there are significant penalties for making any false
statement, representation, or certification including the possibility of a fine and imprisonment.
IGNATURE TITLE

60-01 Harrisbura Rd Landfill Methane Wells
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aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 17, 2018
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409664
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92409664001
6001-HBW28
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409664002
6001-HBW20
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409664003
6001-HBW14
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409664004
TRIP BLANK
EPA 8260E
CL
52
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 31

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: 6001-HBW28 Lab ID: 92409664001 Collected: 12/05/18 10:45 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:14
7440-38-2
Barium
32.0
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:14
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:14
7440-43-9
Chromium
12.0
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-47-3
Cobalt
13.4
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-48-4
Copper
45.8
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-50-8
Lead
5.7
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:14
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:14
7440-28-0
Vanadium
30.1
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:14
7440-62-2
Zinc
19.6
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:14
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 20:34
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 02:39
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 02:39
107-13-1
Benzene
ND
ug/L
1.0
1
12/13/18 02:39
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 02:39
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 02:39
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 02:39
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 02:39
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 02:39
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 02:39
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 02:39
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 02:39
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 02:39
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 02:39
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 02:39
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 02:39
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 02:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 02:39
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 02:39
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 02:39
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 02:39
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 02:39
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/13/18 02:39
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 02:39
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 02:39
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 02:39
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 02:39
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 06:43 PM
without
the written consent of Pace Analytical Services, LLC.
Page 4 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: 6001-HBW28 Lab ID: 92409664001 Collected: 12/05/18 10:45 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/13/18 02:39
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 02:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 02:39
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/13/18 02:39
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/13/18 02:39
591-78-6
lodomethane
ND
ug/L
5.0
1
12/13/18 02:39
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/13/18 02:39
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/13/18 02:39
108-10-1
Styrene
ND
ug/L
1.0
1
12/13/18 02:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 02:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 02:39
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/13/18 02:39
127-18-4
Toluene
ND
ug/L
1.0
1
12/13/18 02:39
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/13/18 02:39
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/13/18 02:39
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/13/18 02:39
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/13/18 02:39
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/13/18 02:39
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/13/18 02:39
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/13/18 02:39
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/13/18 02:39
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/13/18 02:39
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/13/18 02:39
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/13/18 02:39
460-00-4
1,2-Dichloroethane-d4 (S)
88
%
70-130
1
12/13/18 02:39
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/13/18 02:39
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/07/18 18:31
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
50-150
1
12/07/18 18:31
17060-07-0
Toluene-d8 (S)
113
%
50-150
1
12/07/18 18:31
2037-26-5
Date: 12/17/2018 06:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 31

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: 6001-HBW20 Lab ID: 92409664002 Collected: 12/05/18 11:20 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:17
7440-38-2
Barium
7.9
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:17
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:17
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-48-4
Copper
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:17
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:17
7440-28-0
Vanadium
5.2
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:17
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:17
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 20:36
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 05:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 05:47
107-13-1
Benzene
ND
ug/L
1.0
1
12/13/18 05:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 05:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 05:47
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 05:47
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 05:47
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 05:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 05:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 05:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 05:47
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 05:47
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 05:47
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 05:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 05:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 05:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 05:47
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 05:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 05:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 05:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 05:47
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/13/18 05:47
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 05:47
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 05:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 05:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 05:47
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 06:43 PM
without
the written consent of Pace Analytical Services, LLC.
Page 6 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: 6001-HBW20 Lab ID: 92409664002 Collected: 12/05/18 11:20 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/13/18 05:47
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 05:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 05:47
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/13/18 05:47
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/13/18 05:47
591-78-6
lodomethane
ND
ug/L
5.0
1
12/13/18 05:47
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/13/18 05:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/13/18 05:47
108-10-1
Styrene
ND
ug/L
1.0
1
12/13/18 05:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 05:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 05:47
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/13/18 05:47
127-18-4
Toluene
ND
ug/L
1.0
1
12/13/18 05:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/13/18 05:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/13/18 05:47
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/13/18 05:47
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/13/18 05:47
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/13/18 05:47
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/13/18 05:47
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/13/18 05:47
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/13/18 05:47
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/13/18 05:47
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/13/18 05:47
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/13/18 05:47
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
12/13/18 05:47
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/13/18 05:47
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/07/18 18:50
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
50-150
1
12/07/18 18:50
17060-07-0
Toluene-d8 (S)
113
%
50-150
1
12/07/18 18:50
2037-26-5
Date: 12/17/2018 06:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 31

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: 6001-HBW14 Lab ID: 92409664003 Collected: 12/05/18 11:40 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:20
7440-38-2
Barium
94.9
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:20
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:20
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-48-4
Copper
16.3
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:20
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:20
7440-28-0
Vanadium
7.6
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:20
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:20
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 20:38
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 06:21
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 06:21
107-13-1
Benzene
ND
ug/L
1.0
1
12/13/18 06:21
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 06:21
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 06:21
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 06:21
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 06:21
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 06:21
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 06:21
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 06:21
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 06:21
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 06:21
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 06:21
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 06:21
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 06:21
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 06:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 06:21
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 06:21
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 06:21
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 06:21
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 06:21
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/13/18 06:21
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 06:21
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 06:21
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 06:21
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 06:21
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 06:43 PM
without
the written consent of Pace Analytical Services, LLC.
Page 8 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: 6001-HBW14 Lab ID: 92409664003 Collected: 12/05/18 11:40 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/13/18 06:21
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 06:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 06:21
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/13/18 06:21
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/13/18 06:21
591-78-6
lodomethane
ND
ug/L
5.0
1
12/13/18 06:21
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/13/18 06:21
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/13/18 06:21
108-10-1
Styrene
ND
ug/L
1.0
1
12/13/18 06:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 06:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 06:21
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/13/18 06:21
127-18-4
Toluene
ND
ug/L
1.0
1
12/13/18 06:21
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/13/18 06:21
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/13/18 06:21
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/13/18 06:21
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/13/18 06:21
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/13/18 06:21
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/13/18 06:21
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/13/18 06:21
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/13/18 06:21
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/13/18 06:21
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/13/18 06:21
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/13/18 06:21
460-00-4
1,2-Dichloroethane-d4 (S)
88
%
70-130
1
12/13/18 06:21
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/13/18 06:21
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/13/18 00:36
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
95
%
50-150
1
12/13/18 00:36
17060-07-0
Toluene-d8 (S)
108
%
50-150
1
12/13/18 00:36
2037-26-5
Date: 12/17/2018 06:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 31

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: TRIP BLANK Lab ID: 92409664004 Collected: 12/05/18 09:53 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/12/18 20:58
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/12/18 20:58
107-13-1
Benzene
ND
ug/L
1.0
1
12/12/18 20:58
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/12/18 20:58
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/12/18 20:58
75-27-4
Bromoform
ND
ug/L
1.0
1
12/12/18 20:58
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/12/18 20:58
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/12/18 20:58
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/12/18 20:58
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/12/18 20:58
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/12/18 20:58
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/12/18 20:58
75-00-3
Chloroform
ND
ug/L
1.0
1
12/12/18 20:58
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/12/18 20:58
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/12/18 20:58
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/12/18 20:58
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/12/18 20:58
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/12/18 20:58
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/12/18 20:58
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/12/18 20:58
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/12/18 20:58
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/12/18 20:58
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/12/18 20:58
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/12/18 20:58
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/18 20:58
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/12/18 20:58
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
12/12/18 20:58
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/18 20:58
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/12/18 20:58
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/12/18 20:58
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/12/18 20:58
591-78-6
lodomethane
ND
ug/L
5.0
1
12/12/18 20:58
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/12/18 20:58
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/12/18 20:58
108-10-1
Styrene
ND
ug/L
1.0
1
12/12/18 20:58
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/18 20:58
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/12/18 20:58
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/12/18 20:58
127-18-4
Toluene
ND
ug/L
1.0
1
12/12/18 20:58
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/12/18 20:58
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/12/18 20:58
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/12/18 20:58
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/12/18 20:58
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/12/18 20:58
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/12/18 20:58
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/12/18 20:58
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/12/18 20:58
1330-20-7
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
Sample: TRIP BLANK
Lab ID: 92409664004 Collected: 12/05/18 09:53
Received: 12/05/18 15:23 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
m&p-Xylene
ND ug/L
2.0
1
12/12/18 20:58
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/12/18 20:58
95-47-6
Surrogates
4-Bromofluorobenzene (S)
103 %
70-130
1
12/12/18 20:58
460-00-4
1,2-Dichloroethane-d4 (S)
95 %
70-130
1
12/12/18 20:58
17060-07-0
Toluene-d8 (S)
101 %
70-130
1
12/12/18 20:58
2037-26-5
Date: 12/17/2018 06:43 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
QC Batch: 446501 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92409664001, 92409664002, 92409664003
METHOD BLANK: 2447332 Matrix: Water
Associated Lab Samples: 92409664001, 92409664002, 92409664003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
12/16/18 22:20
10.0
12/16/18 22:20
5.0
12/16/18 22:20
1.0
12/16/18 22:20
1.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
10.0
12/16/18 22:20
5.0
12/16/18 22:20
10.0
12/16/18 22:20
5.0
12/16/18 22:20
10.0
12/16/18 22:20
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2447333
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
498
100
80-120
Arsenic
ug/L
500
487
97
80-120
Barium
ug/L
500
493
99
80-120
Beryllium
ug/L
500
495
99
80-120
Cadmium
ug/L
500
476
95
80-120
Chromium
ug/L
500
495
99
80-120
Cobalt
ug/L
500
484
97
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
470
94
80-120
Nickel
ug/L
500
484
97
80-120
Selenium
ug/L
500
481
96
80-120
Silver
ug/L
250
259
103
80-120
Thallium
ug/L
500
474
95
80-120
Vanadium
ug/L
500
491
98
80-120
Zinc
ug/L
500
464
93
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 31

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QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409664
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2447334
2447335
MS
MSD
92409528002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
356
341
71
68
75-125
5 M1
Arsenic
ug/L
ND
500
500
476
474
95
94
75-125
1
Barium
ug/L
122
500
500
602
596
96
95
75-125
1
Beryllium
ug/L
1.4
500
500
502
499
100
100
75-125
1
Cadmium
ug/L
ND
500
500
465
463
93
93
75-125
0
Chromium
ug/L
7.2
500
500
496
493
98
97
75-125
1
Cobalt
ug/L
11.8
500
500
490
489
96
95
75-125
0
Copper
ug/L
12.6
500
500
523
519
102
101
75-125
1
Lead
ug/L
9.2
500
500
466
464
91
91
75-125
1
Nickel
ug/L
12.2
500
500
489
487
95
95
75-125
0
Selenium
ug/L
ND
500
500
492
487
98
97
75-125
1
Silver
ug/L
ND
250
250
253
252
101
101
75-125
0
Thallium
ug/L
ND
500
500
459
457
92
91
75-125
0
Vanadium
ug/L
14.6
500
500
498
497
97
96
75-125
0
Zinc
ug/L
34.2
500
500
502
507
93
95
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
QC Batch: 446878 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92409664001, 92409664002, 92409664003
METHOD BLANK: 2449117 Matrix: Water
Associated Lab Samples: 92409664001, 92409664002, 92409664003
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Thallium ug/L ND 0.10
12/14/1819:39
LABORATORY CONTROL SAMPLE: 2449118
Spike LCS
LCS % Rec
Parameter Units Conc. Result
% Rec Limits Qualifiers
Thallium ug/L 10 9.7
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449119 2449120
MS MSD
92410006001 Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Thallium ug/L 0.062J 10 10 10.1
10.1 101 101 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
QC Batch: 447139 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92409664001, 92409664004
METHOD BLANK: 2450443
Associated Lab Samples: 92409664001, 92409664004
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/12/18 18:42
1,1,1-Trichloroethane
ug/L
ND
1.0
12/12/18 18:42
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/12/18 18:42
1,1,2-Trichloroethane
ug/L
ND
1.0
12/12/18 18:42
1,1-Dichloroethane
ug/L
ND
1.0
12/12/18 18:42
1,1-Dichloroethene
ug/L
ND
1.0
12/12/18 18:42
1,2,3-Trichloropropane
ug/L
ND
1.0
12/12/18 18:42
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/12/18 18:42
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/12/18 18:42
1,2-Dichlorobenzene
ug/L
ND
1.0
12/12/18 18:42
1,2-Dichloroethane
ug/L
ND
1.0
12/12/18 18:42
1,2-Dichloropropane
ug/L
ND
1.0
12/12/18 18:42
1,4-Dichlorobenzene
ug/L
ND
1.0
12/12/18 18:42
2-Butanone (MEK)
ug/L
ND
5.0
12/12/18 18:42
2-Hexanone
ug/L
ND
5.0
12/12/18 18:42
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/12/18 18:42
Acetone
ug/L
ND
25.0
12/12/18 18:42
Acrylonitrile
ug/L
ND
10.0
12/12/18 18:42
Benzene
ug/L
ND
1.0
12/12/18 18:42
Bromochloromethane
ug/L
ND
1.0
12/12/18 18:42
Bromodichloromethane
ug/L
ND
1.0
12/12/18 18:42
Bromoform
ug/L
ND
1.0
12/12/18 18:42
Bromomethane
ug/L
ND
2.0
12/12/18 18:42
Carbon disulfide
ug/L
ND
2.0
12/12/18 18:42
Carbon tetrachloride
ug/L
ND
1.0
12/12/18 18:42
Chlorobenzene
ug/L
ND
1.0
12/12/18 18:42
Chloroethane
ug/L
ND
1.0
12/12/18 18:42
Chloroform
ug/L
ND
1.0
12/12/18 18:42
Chloromethane
ug/L
ND
1.0
12/12/18 18:42
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/12/18 18:42
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/12/18 18:42
Dibromochloromethane
ug/L
ND
1.0
12/12/18 18:42
Dibromomethane
ug/L
ND
1.0
12/12/18 18:42
Ethylbenzene
ug/L
ND
1.0
12/12/18 18:42
lodomethane
ug/L
ND
5.0
12/12/18 18:42
m&p-Xylene
ug/L
ND
2.0
12/12/18 18:42
Methylene Chloride
ug/L
ND
1.0
12/12/18 18:42
o-Xylene
ug/L
ND
1.0
12/12/18 18:42
Styrene
ug/L
ND
1.0
12/12/18 18:42
Tetrachloroethene
ug/L
ND
1.0
12/12/18 18:42
Toluene
ug/L
ND
1.0
12/12/18 18:42
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 31

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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
METHOD BLANK: 2450443
Associated Lab Samples: 92409664001, 92409664004
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/12/18 18:42
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/12/18 18:42
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/12/18 18:42
Trichloroethene
ug/L
ND
1.0
12/12/18 18:42
Trichlorofluoromethane
ug/L
ND
1.0
12/12/18 18:42
Vinyl acetate
ug/L
ND
2.0
12/12/18 18:42
Vinyl chloride
ug/L
ND
1.0
12/12/18 18:42
Xylene (Total)
ug/L
ND
1.0
12/12/18 18:42
1,2-Dichloroethane-d4 (S)
%
92
70-130
12/12/18 18:42
4-Bromofluorobenzene (S)
%
98
70-130
12/12/18 18:42
Toluene-d8 (S)
%
100
70-130
12/12/18 18:42
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2450444
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.1
104
70-130
1,1,1-Trichloroethane
ug/L
50
49.1
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
51.0
102
70-130
1,1,2-Trichloroethane
ug/L
50
53.5
107
70-130
1,1-Dichloroethane
ug/L
50
51.7
103
70-130
1,1-Dichloroethene
ug/L
50
52.9
106
70-130
1,2,3-Trichloropropane
ug/L
50
45.8
92
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
54.8
110
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.8
102
70-130
1,2-Dichlorobenzene
ug/L
50
53.0
106
70-130
1,2-Dichloroethane
ug/L
50
48.3
97
70-130
1,2-Dichloropropane
ug/L
50
50.5
101
70-130
1,4-Dichlorobenzene
ug/L
50
51.1
102
70-130
2-Butanone (MEK)
ug/L
100
107
107
64-135
2-Hexanone
ug/L
100
106
106
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
104
104
70-130
Acetone
ug/L
100
103
103
61-157
Acrylonitrile
ug/L
250
261
104
61-143
Benzene
ug/L
50
53.3
107
70-130
Bromochloromethane
ug/L
50
53.4
107
70-130
Bromodichloromethane
ug/L
50
50.6
101
70-130
Bromoform
ug/L
50
47.5
95
70-130
Bromomethane
ug/L
50
54.6
109
38-130
Carbon disulfide
ug/L
50
53.9
108
68-130
Carbon tetrachloride
ug/L
50
49.8
100
70-130
Chlorobenzene
ug/L
50
51.0
102
70-130
Chloroethane
ug/L
50
49.4
99
37-142
Chloroform
ug/L
50
48.6
97
70-130
Chloromethane
ug/L
50
52.7
105
48-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 31

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[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
LABORATORY CONTROL SAMPLE:
2450444
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
53.0
106
70-130
cis-1,3-Dichloropropene
ug/L
50
52.4
105
70-130
Dibromochloromethane
ug/L
50
50.1
100
70-130
Dibromomethane
ug/L
50
52.3
105
70-130
Ethylbenzene
ug/L
50
51.6
103
70-130
lodomethane
ug/L
100
96.2
96
40-130
m&p-Xylene
ug/L
100
104
104
70-130
Methylene Chloride
ug/L
50
48.9
98
67-132
o-Xylene
ug/L
50
53.3
107
70-130
Styrene
ug/L
50
52.1
104
70-130
Tetrachloroethene
ug/L
50
50.3
101
69-130
Toluene
ug/L
50
50.4
101
70-130
trans-1,2-Dichloroethene
ug/L
50
52.6
105
70-130
trans- 1,3-Dichloropropene
ug/L
50
51.6
103
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
52.1
104
35-189
Trichloroethene
ug/L
50
50.9
102
70-130
Trichlorofluoromethane
ug/L
50
51.0
102
63-130
Vinyl acetate
ug/L
100
109
109
55-143
Vinyl chloride
ug/L
50
53.9
108
70-131
Xylene (Total)
ug/L
150
158
105
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
2450446
92409664001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
22.9
114
73-134
1,1,1-Trichloroethane
ug/L
ND
20
20.6
103
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
22.2
111
70-136
1,1,2-Trichloroethane
ug/L
ND
20
23.3
116
70-135
1,1-Dichloroethane
ug/L
ND
20
21.3
107
70-139
1,1-Dichloroethene
ug/L
ND
20
22.9
114
70-154
1,2,3-Trichloropropane
ug/L
ND
20
21.9
109
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
21.8
109
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
22.2
111
70-137
1,2-Dichlorobenzene
ug/L
ND
20
21.4
107
70-133
1,2-Dichloroethane
ug/L
ND
20
20.1
101
70-137
1,2-Dichloropropene
ug/L
ND
20
21.1
105
70-140
1,4-Dichlorobenzene
ug/L
ND
20
20.3
101
70-133
2-Butanone (MEK)
ug/L
ND
40
41.3
103
60-139
2-Hexanone
ug/L
ND
40
43.9
110
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
42.9
107
65-135
Acetone
ug/L
ND
40
42.2
106
60-148
Acrylonitrile
ug/L
ND
100
97.7
98
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 31

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
MATRIX SPIKE SAMPLE:
Parameter
2450446
Units
92409664001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Benzene
ug/L
ND
20
22.7
114
70-151
Bromochloromethane
ug/L
ND
20
21.6
108
70-141
Bromodichloromethane
ug/L
ND
20
22.1
111
70-138
Bromoform
ug/L
ND
20
19.6
98
63-130
Bromomethane
ug/L
ND
20
19.3
96
15-152
Carbon disulfide
ug/L
ND
20
21.2
106
69-149
Carbon tetrachloride
ug/L
ND
20
22.5
113
70-143
Chlorobenzene
ug/L
ND
20
21.9
109
70-138
Chloroethane
ug/L
ND
20
21.3
107
52-163
Chloroform
ug/L
ND
20
20.0
100
70-139
Chloromethane
ug/L
ND
20
20.9
105
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
20.9
105
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
21.4
107
70-137
Dibromochloromethane
ug/L
ND
20
20.7
104
70-134
Dibromomethane
ug/L
ND
20
23.6
118
70-138
Ethylbenzene
ug/L
ND
20
22.4
112
66-153
lodomethane
ug/L
ND
40
32.7
82
20-138
m&p-Xylene
ug/L
ND
40
45.1
113
69-152
Methylene Chloride
ug/L
ND
20
18.2
91
42-159
o-Xylene
ug/L
ND
20
22.6
113
70-148
Styrene
ug/L
ND
20
21.9
109
70-135
Tetrachloroethene
ug/L
ND
20
22.1
110
59-143
Toluene
ug/L
ND
20
21.6
108
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
21.6
108
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
21.6
108
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
18.5
92
47-135
Trichloroethene
ug/L
ND
20
22.3
111
70-147
Trichlorofluoromethane
ug/L
ND
20
22.1
111
70-148
Vinyl acetate
ug/L
ND
40
38.3
96
49-151
Vinyl chloride
ug/L
ND
20
21.7
109
70-156
Xylene (Total)
ug/L
ND
60
67.7
113
63-158
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
99
70-130
SAMPLE DUPLICATE: 2450445
Parameter
Units
92409870001
Result
Dup
Result RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
SAMPLE DUPLICATE: 2450445
Parameter
Units
92409870001
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
.28J
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
.82J
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
94
91
4-Bromofluorobenzene (S)
%
100
99
Toluene-d8 (S)
%
99
100
RPD Qualifiers
4
1
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 31

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
QC Batch: 447140 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92409664002, 92409664003
METHOD BLANK: 2450452
Associated Lab Samples: 92409664002, 92409664003
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1,1-Trichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1,2-Trichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1-Dichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1-Dichloroethene
ug/L
ND
1.0
12/13/18 05:13
1,2,3-Trichloropropane
ug/L
ND
1.0
12/13/18 05:13
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/13/18 05:13
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichlorobenzene
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichloropropane
ug/L
ND
1.0
12/13/18 05:13
1,4-Dichlorobenzene
ug/L
ND
1.0
12/13/18 05:13
2-Butanone (MEK)
ug/L
ND
5.0
12/13/18 05:13
2-Hexanone
ug/L
ND
5.0
12/13/18 05:13
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/13/18 05:13
Acetone
ug/L
ND
25.0
12/13/18 05:13
Acrylonitrile
ug/L
ND
10.0
12/13/18 05:13
Benzene
ug/L
ND
1.0
12/13/18 05:13
Bromochloromethane
ug/L
ND
1.0
12/13/18 05:13
Bromodichloromethane
ug/L
ND
1.0
12/13/18 05:13
Bromoform
ug/L
ND
1.0
12/13/18 05:13
Bromomethane
ug/L
ND
2.0
12/13/18 05:13
Carbon disulfide
ug/L
ND
2.0
12/13/18 05:13
Carbon tetrachloride
ug/L
ND
1.0
12/13/18 05:13
Chlorobenzene
ug/L
ND
1.0
12/13/18 05:13
Chloroethane
ug/L
ND
1.0
12/13/18 05:13
Chloroform
ug/L
ND
1.0
12/13/18 05:13
Chloromethane
ug/L
ND
1.0
12/13/18 05:13
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/13/18 05:13
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/13/18 05:13
Dibromochloromethane
ug/L
ND
1.0
12/13/18 05:13
Dibromomethane
ug/L
ND
1.0
12/13/18 05:13
Ethylbenzene
ug/L
ND
1.0
12/13/18 05:13
lodomethane
ug/L
ND
5.0
12/13/18 05:13
m&p-Xylene
ug/L
ND
2.0
12/13/18 05:13
Methylene Chloride
ug/L
ND
1.0
12/13/18 05:13
o-Xylene
ug/L
ND
1.0
12/13/18 05:13
Styrene
ug/L
ND
1.0
12/13/18 05:13
Tetrachloroethene
ug/L
ND
1.0
12/13/18 05:13
Toluene
ug/L
ND
1.0
12/13/18 05:13
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
METHOD BLANK: 2450452
Associated Lab Samples: 92409664002, 92409664003
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/13/18 05:13
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/13/18 05:13
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/13/18 05:13
Trichloroethene
ug/L
ND
1.0
12/13/18 05:13
Trichlorofluoromethane
ug/L
ND
1.0
12/13/18 05:13
Vinyl acetate
ug/L
ND
2.0
12/13/18 05:13
Vinyl chloride
ug/L
ND
1.0
12/13/18 05:13
Xylene (Total)
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichloroethane-d4 (S)
%
88
70-130
12/13/18 05:13
4-Bromofluorobenzene (S)
%
100
70-130
12/13/18 05:13
Toluene-d8 (S)
%
102
70-130
12/13/18 05:13
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2450453
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.1
104
70-130
1,1,1-Trichloroethane
ug/L
50
45.0
90
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.6
105
70-130
1,1,2-Trichloroethane
ug/L
50
53.5
107
70-130
1,1-Dichloroethane
ug/L
50
48.1
96
70-130
1,1-Dichloroethene
ug/L
50
47.7
95
70-130
1,2,3-Trichloropropane
ug/L
50
46.0
92
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.3
103
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.1
100
70-130
1,2-Dichlorobenzene
ug/L
50
49.7
99
70-130
1,2-Dichloroethane
ug/L
50
45.7
91
70-130
1,2-Dichloropropane
ug/L
50
50.1
100
70-130
1,4-Dichlorobenzene
ug/L
50
49.2
98
70-130
2-Butanone (MEK)
ug/L
100
92.5
93
64-135
2-Hexanone
ug/L
100
102
102
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
102
102
70-130
Acetone
ug/L
100
91.9
92
61-157
Acrylonitrile
ug/L
250
228
91
61-143
Benzene
ug/L
50
52.7
105
70-130
Bromochloromethane
ug/L
50
48.4
97
70-130
Bromodichloromethane
ug/L
50
52.7
105
70-130
Bromoform
ug/L
50
46.8
94
70-130
Bromomethane
ug/L
50
43.1
86
38-130
Carbon disulfide
ug/L
50
47.3
95
68-130
Carbon tetrachloride
ug/L
50
51.3
103
70-130
Chlorobenzene
ug/L
50
50.8
102
70-130
Chloroethane
ug/L
50
45.3
91
37-142
Chloroform
ug/L
50
45.8
92
70-130
Chloromethane
ug/L
50
42.5
85
48-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
LABORATORY CONTROL SAMPLE:
2450453
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
47.3
95
70-130
cis-1,3-Dichloropropene
ug/L
50
51.9
104
70-130
Dibromochloromethane
ug/L
50
51.0
102
70-130
Dibromomethane
ug/L
50
54.7
109
70-130
Ethylbenzene
ug/L
50
51.6
103
70-130
lodomethane
ug/L
100
94.4
94
40-130
m&p-Xylene
ug/L
100
104
104
70-130
Methylene Chloride
ug/L
50
44.9
90
67-132
o-Xylene
ug/L
50
53.7
107
70-130
Styrene
ug/L
50
52.8
106
70-130
Tetrachloroethene
ug/L
50
51.0
102
69-130
Toluene
ug/L
50
62.6
125
70-130
trans-1,2-Dichloroethene
ug/L
50
47.9
96
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.9
106
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
51.0
102
35-189
Trichloroethene
ug/L
50
51.4
103
70-130
Trichlorofluoromethane
ug/L
50
46.2
92
63-130
Vinyl acetate
ug/L
100
98.3
98
55-143
Vinyl chloride
ug/L
50
46.5
93
70-131
Xylene (Total)
ug/L
150
158
105
70-130
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
102
70-130
MATRIX SPIKE SAMPLE:
2450490
92409812005
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.5
102
73-134
1,1,1-Trichloroethane
ug/L
ND
20
19.0
95
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.8
99
70-136
1,1,2-Trichloroethane
ug/L
ND
20
20.7
103
70-135
1,1-Dichloroethane
ug/L
ND
20
19.4
97
70-139
1,1-Dichloroethene
ug/L
ND
20
19.5
97
70-154
1,2,3-Trichloropropane
ug/L
ND
20
20.9
104
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
18.9
95
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.1
95
70-137
1,2-Dichlorobenzene
ug/L
ND
20
18.8
94
70-133
1,2-Dichloroethane
ug/L
ND
20
18.1
90
70-137
1,2-Dichloropropene
ug/L
ND
20
19.2
96
70-140
1,4-Dichlorobenzene
ug/L
ND
20
18.3
92
70-133
2-Butanone (MEK)
ug/L
ND
40
38.1
95
60-139
2-Hexanone
ug/L
ND
40
40.5
101
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40.0
100
65-135
Acetone
ug/L
ND
40
40.9
102
60-148
Acrylonitrile
ug/L
ND
100
90.7
91
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
MATRIX SPIKE SAMPLE:
Parameter
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Ethylbenzene
lodomethane
m&p-Xylene
Methylene Chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans- 1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2450490
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
92409812005
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Spike
Conc.
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
40
20
20
20
20
20
20
20
20
20
20
40
20
60
MS
Result
21.0
19.7
20.4
18.4
16.4
19.0
21.0
19.7
18.3
17.6
18.0
19.3
19.2
19.6
20.6
20.5
25.3
40.3
16.1
20.6
19.8
21.0
21.3
19.8
19.5
19.4
20.8
19.8
27.9
19.0
60.9
MS
% Rec
% Rec
Limits
105 70-151
98 70-141
102 70-138
92 63-130
82 15-152
95 69-149
105 70-143
99 70-138
92 52-163
88 70-139
90 41-139
96 70-141
96 70-137
98 70-134
103 70-138
102 66-153
63 20-138
101 69-152
80 42-159
103 70-148
99 70-135
105 59-143
107 59-148
99 70-146
97 70-135
97 47-135
104 70-147
99 70-148
70 49-151
95 70-156
101 63-158
90 70-130
102 70-130
99 70-130
SAMPLE DUPLICATE: 2450489
Parameter
Units
92409664002
Result
Dup
Result RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
.78J
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 23 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
SAMPLE DUPLICATE: 2450489
Parameter
Units
92409664002
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
.34J
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
90
86
4-Bromofluorobenzene (S)
%
99
101
Toluene-d8 (S)
%
100
101
RPD Qualifiers
5
2
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 31

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
QC Batch: 446273 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92409664001, 92409664002
METHOD BLANK: 2446001
Associated Lab Samples: 92409664001, 92409664002
Parameter Units
1,4-Dioxane (p-Dioxane) ug/L
1,2-Dichloroethane-d4 (S) %
Toluene-d8 (S) %
Matrix: Water
Blank Reporting
Result Limit
Analyzed
ND 2.0
12/07/1811:26
97 50-150
12/07/1811:26
113 50-150
12/07/1811:26
Qualifiers
LABORATORY CONTROL SAMPLE: 2446002
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 17.4 87 71-125
1,2-Dichloroethane-d4 (S) % 101 50-150
Toluene-d8(S) % 114 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2446003
2446004
MS
MSD
2612158002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 16.6
17.5 82
87
50-150 5
1,2-Dichloroethane-d4 (S)
%
106
103
50-150
Toluene-d8(S)
%
117
116
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
QC Batch: 447055 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92409664003
METHOD BLANK: 2449939
Associated Lab Samples: 92409664003
Parameter
Units
1,4-Dioxane (p-Dioxane)
ug/L
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 12/12/1816:14
95 50-150 12/12/1816:14
98 50-150 12/12/1816:14
LABORATORY CONTROL SAMPLE: 2449940
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 16.9 85 71-125
1,2-Dichloroethane-d4 (S) % 97 50-150
Toluene-d8(S) % 101 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449941
2449942
MS
MSD
92409793006 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L 10.1 20
20 26.1
25.1 80
75
50-150 4
1,2-Dichloroethane-d4 (S)
%
100
102
50-150
Toluene-d8 (S)
%
111
114
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409664
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:43 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 31

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409664
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92409664001
6001-HBW28
EPA 3010A
446501
EPA6010D
446518
92409664002
6001-HBW20
EPA 3010A
446501
EPA6010D
446518
92409664003
6001-HBW14
EPA 3010A
446501
EPA6010D
446518
92409664001
6001-HBW28
EPA 3010A
446878
EPA6020B
447017
92409664002
6001-HBW20
EPA 3010A
446878
EPA6020B
447017
92409664003
6001-HBW14
EPA 3010A
446878
EPA6020B
447017
92409664001
6001-HBW28
EPA 8260B
447139
92409664002
6001-HBW20
EPA 8260B
447140
92409664003
6001-HBW14
EPA 8260B
447140
92409664004
TRIP BLANK
EPA 8260B
447139
92409664001
6001-HBW28
EPA 8260B Mod.
446273
92409664002
6001-HBW20
EPA 8260B Mod.
446273
92409664003
6001-HBW14
EPA 8260B Mod.
447055
Date: 12/17/2018 06:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 31

Document Name:
Document Revised: February 7, 2018
aceAr� Vital
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
i
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑
-Samp Client Name: WO# : 92409664
Project #:
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial note / ❑Other: 92409664
Custody Seal Present? /❑Yes Ly�fo Seals Intact? ❑Yes �V0 /z
L > Date/Initials Person Examining Contents:
Packing Material. .-1� ❑Bubble Bags ne ❑ Other
Thermome E
)—<
Nun ID: 92TO46 Type of Ice: ❑Wet ❑Blue
rs
Cooler Temp (°C): ) L' Correction Factor: Add/Subtract ('C) 0.()
Cooler Temp Corrected (°C): �r
USDA Regulated S�o'F [(<N/A, water sample)
Did samples Nv ate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
❑Yes
Biological Tiss a rozen?
❑None
[--]yeses ❑i_
No N/A
Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source li ernat'onally,
indudine Hawaii and Puerto RicoP nYes o
Comments/Discrepancy:
Chain of Custody Present?
INS
❑No
❑N/A
i.
Samples Arrived within Hold Time?
IQTi s
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Dyes
&
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
o
❑N/A
4.
Sufficient Volume?
yes
[-]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Yes
Yes
[-]No
❑No
[]N/A
❑N/A
6.
Containers Intact?
es
[-]No
[I N/A.
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
❑No
N/A
8.
Sample Labels Match COC?
Includes Date/Time/ID/Analysis Matrix:
1[Ns
"
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
❑Yes
0�0
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
5�1
Dyes
ONo
V.
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: Date:
Project Manager SRF Review: �>, Date:
Page 29 of 31

Document Name:
Document Revised: February 7, 2018
_ aCe,4na y icafo
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project IWa# : 92449664
I3M: MWB Due Dale: 12/19/18
CLIENT: 92—MECK CO
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot k
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of tern p, incorrect containers.
Page 30 of 31

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Page 31 of 31

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 17, 2018
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 06, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 40

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 40

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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409812
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92409812001
6001-HBW21
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409812002
6001-HBW22
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409812003
6001-HBW12B
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409812004
6001-HBW17B
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409812005
6001-MAINTE
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409812006
BLANK
EPA 8260E
CL
52
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 40

aceAnalytical
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW21 Lab ID: 92409812001 Collected: 12/06/18 10:55 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:38
7440-38-2
Barium
11.7
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:38
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:38
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-48-4
Copper
5.3
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:38
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:38
7440-28-0
Vanadium
10.4
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:38
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:38
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 23:52
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 09:12
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 09:12
107-13-1
Benzene
ND
ug/L
1.0
1
12/13/18 09:12
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 09:12
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 09:12
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 09:12
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 09:12
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 09:12
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 09:12
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 09:12
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 09:12
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 09:12
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 09:12
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 09:12
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 09:12
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 09:12
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 09:12
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 09:12
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 09:12
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 09:12
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 09:12
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/13/18 09:12
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 09:12
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:12
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:12
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:12
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 04:40 PM
without
the written consent of Pace Analytical Services, LLC.
Page 4 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW21 Lab ID: 92409812001 Collected: 12/06/18 10:55 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/13/18 09:12
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 09:12
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 09:12
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/13/18 09:12
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/13/18 09:12
591-78-6
lodomethane
ND
ug/L
5.0
1
12/13/18 09:12
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/13/18 09:12
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/13/18 09:12
108-10-1
Styrene
ND
ug/L
1.0
1
12/13/18 09:12
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 09:12
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 09:12
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/13/18 09:12
127-18-4
Toluene
ND
ug/L
1.0
1
12/13/18 09:12
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/13/18 09:12
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/13/18 09:12
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/13/18 09:12
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/13/18 09:12
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/13/18 09:12
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/13/18 09:12
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/13/18 09:12
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/13/18 09:12
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/13/18 09:12
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/13/18 09:12
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/13/18 09:12
460-00-4
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
12/13/18 09:12
17060-07-0
Toluene-d8 (S)
97
%
70-130
1
12/13/18 09:12
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/14/18 00:23
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
50-150
1
12/14/18 00:23
17060-07-0
Toluene-d8 (S)
110
%
50-150
1
12/14/18 00:23
2037-26-5
Date: 12/17/2018 04:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 40

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ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW22 Lab ID: 92409812002 Collected: 12/06/18 10:30 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:41
7440-38-2
Barium
35.2
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:41
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:41
7440-43-9
Chromium
37.8
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-48-4
Copper
7.9
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7439-92-1
Nickel
7.9
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:41
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:41
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:41
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:41
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 23:54
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 09:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 09:30
107-13-1
Benzene
ND
ug/L
1.0
1
12/13/18 09:30
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 09:30
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 09:30
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 09:30
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 09:30
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 09:30
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 09:30
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 09:30
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 09:30
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 09:30
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 09:30
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 09:30
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 09:30
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 09:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 09:30
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 09:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 09:30
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 09:30
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 09:30
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/13/18 09:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 09:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:30
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:30
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:30
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 04:40 PM
without
the written consent of Pace Analytical Services, LLC.
Page 6 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW22 Lab ID: 92409812002 Collected: 12/06/18 10:30 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/13/18 09:30
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 09:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 09:30
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/13/18 09:30
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/13/18 09:30
591-78-6
lodomethane
ND
ug/L
5.0
1
12/13/18 09:30
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/13/18 09:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/13/18 09:30
108-10-1
Styrene
ND
ug/L
1.0
1
12/13/18 09:30
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 09:30
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 09:30
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/13/18 09:30
127-18-4
Toluene
ND
ug/L
1.0
1
12/13/18 09:30
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/13/18 09:30
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/13/18 09:30
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/13/18 09:30
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/13/18 09:30
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/13/18 09:30
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/13/18 09:30
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/13/18 09:30
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/13/18 09:30
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/13/18 09:30
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/13/18 09:30
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/13/18 09:30
460-00-4
1,2-Dichloroethane-d4 (S)
92
%
70-130
1
12/13/18 09:30
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
12/13/18 09:30
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/13/18 23:25
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
50-150
1
12/13/18 23:25
17060-07-0
Toluene-d8 (S)
111
%
50-150
1
12/13/18 23:25
2037-26-5
Date: 12/17/2018 04:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW12B Lab ID: 92409812003 Collected: 12/06/18 11:15 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:44
7440-38-2
Barium
26.6
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:44
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:44
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-48-4
Copper
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:44
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:44
7440-28-0
Vanadium
11.1
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:44
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:44
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 23:57
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 09:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 09:47
107-13-1
Benzene
ND
ug/L
1.0
1
12/13/18 09:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 09:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 09:47
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 09:47
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 09:47
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 09:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 09:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 09:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 09:47
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 09:47
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 09:47
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 09:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 09:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 09:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 09:47
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 09:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 09:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 09:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 09:47
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/13/18 09:47
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 09:47
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 09:47
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 04:40 PM
without
the written consent of Pace Analytical Services, LLC.
Page 8 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW12B Lab ID: 92409812003 Collected: 12/06/18 11:15 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/13/18 09:47
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 09:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/13/18 09:47
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/13/18 09:47
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/13/18 09:47
591-78-6
lodomethane
ND
ug/L
5.0
1
12/13/18 09:47
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/13/18 09:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/13/18 09:47
108-10-1
Styrene
ND
ug/L
1.0
1
12/13/18 09:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 09:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/13/18 09:47
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/13/18 09:47
127-18-4
Toluene
ND
ug/L
1.0
1
12/13/18 09:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/13/18 09:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/13/18 09:47
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/13/18 09:47
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/13/18 09:47
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/13/18 09:47
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/13/18 09:47
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/13/18 09:47
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/13/18 09:47
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/13/18 09:47
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/13/18 09:47
95-47-6
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/13/18 09:47
460-00-4
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
12/13/18 09:47
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/13/18 09:47
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/14/18 00:42
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
96
%
50-150
1
12/14/18 00:42
17060-07-0
Toluene-d8 (S)
104
%
50-150
1
12/14/18 00:42
2037-26-5
Date: 12/17/2018 04:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 40

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW17B Lab ID: 92409812004 Collected: 12/06/18 12:03 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:47
7440-38-2
Barium
63.5
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:47
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:47
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-47-3
Cobalt
18.4
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-48-4
Copper
12.3
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:47
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:47
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:47
7440-62-2
Zinc
15.7
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:47
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
0.13
ug/L
0.10
1 12/12/18 03:00
12/14/18 23:59
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 13:31
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 13:31
107-13-1
Benzene
9.0
ug/L
1.0
1
12/13/18 13:31
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 13:31
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 13:31
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 13:31
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 13:31
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 13:31
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 13:31
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 13:31
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 13:31
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 13:31
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 13:31
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 13:31
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 13:31
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 13:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 13:31
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 13:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 13:31
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 13:31
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 13:31
110-57-6
1,1-Dichloroethane
6.1
ug/L
1.0
1
12/13/18 13:31
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 13:31
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 13:31
75-35-4
cis-1,2-Dichloroethene
113
ug/L
1.0
1
12/13/18 13:31
156-59-2
trans-1,2-Dichloroethene
1.3
ug/L
1.0
1
12/13/18 13:31
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 04:40 PM
without
the written consent of Pace Analytical Services, LLC.
Page 10 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-HBW17B Lab ID: 92409812004 Collected: 12/06/18 12:03 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/17/2018 04:40 PM
Analytical Method: EPA 8260E
9.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
28.7
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
22.6
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.5
ug/L
11.5
ug/L
ND
ug/L
11.5
ug/L
104 %
91 %
101 %
Analytical Method: EPA 8260E Mod
ND ug/L
96 %
101 %
1.0
1
12/13/18 13:31
78-87-5
1.0
1
12/13/18 13:31
10061-01-5
1.0
1
12/13/18 13:31
10061-02-6
1.0
1
12/13/18 13:31
100-41-4
5.0
1
12/13/18 13:31
591-78-6
5.0
1
12/13/18 13:31
74-88-4
1.0
1
12/13/18 13:31
75-09-2
5.0
1
12/13/18 13:31
108-10-1
1.0
1
12/13/18 13:31
100-42-5
1.0
1
12/13/18 13:31
630-20-6
1.0
1
12/13/18 13:31
79-34-5
1.0
1
12/13/18 13:31
127-18-4
1.0
1
12/13/18 13:31
108-88-3
1.0
1
12/13/18 13:31
71-55-6
1.0
1
12/13/18 13:31
79-00-5
1.0
1
12/13/18 13:31
79-01-6
1.0
1
12/13/18 13:31
75-69-4
1.0
1
12/13/18 13:31
96-18-4
2.0
1
12/13/18 13:31
108-05-4
1.0
1
12/13/18 13:31
75-01-4
1.0
1
12/13/18 13:31
1330-20-7
2.0
1
12/13/18 13:31
179601-23-1
1.0
1
12/13/18 13:31
95-47-6
70-130 1
70-130 1
70-130 1
2.0 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/13/18 13:31 460-00-4
12/13/18 13:31 17060-07-0
12/13/18 13:31 2037-26-5
12/14/18 01:01 123-91-1
12/14/18 01:01 17060-07-0
12/14/18 01:01 2037-26-5
Page 11 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-MAINTE Lab ID: 92409812005 Collected: 12/06/18 11:40 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:50
7440-38-2
Barium
9.3
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:50
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:50
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-48-4
Copper
86.9
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:50
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:50
7440-28-0
Vanadium
5.5
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:50
7440-62-2
Zinc
46.6
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:50
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/15/18 00:01
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/13/18 10:04
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/13/18 10:04
107-13-1
Benzene
ND
ug/L
1.0
1
12/13/18 10:04
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/13/18 10:04
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/13/18 10:04
75-27-4
Bromoform
ND
ug/L
1.0
1
12/13/18 10:04
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/13/18 10:04
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/13/18 10:04
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/13/18 10:04
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/13/18 10:04
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/13/18 10:04
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/13/18 10:04
75-00-3
Chloroform
ND
ug/L
1.0
1
12/13/18 10:04
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/13/18 10:04
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/13/18 10:04
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/13/18 10:04
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/13/18 10:04
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/13/18 10:04
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 10:04
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/13/18 10:04
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/13/18 10:04
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/13/18 10:04
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/13/18 10:04
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/13/18 10:04
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 10:04
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/13/18 10:04
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 04:40 PM
without
the written consent of Pace Analytical Services, LLC.
Page 12 of 40

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ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: 6001-MAINTE Lab ID: 92409812005 Collected: 12/06/18 11:40 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
2-Hexanone
lodomethane
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
8260 MSV SIM
1,4-Dioxane (p-Dioxane)
Surrogates
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 12/17/2018 04:40 PM
Analytical Method: EPA 8260E
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
99 %
91 %
99 %
Analytical Method: EPA 8260E Mod
ND ug/L
95 %
97 %
1.0
1
12/13/18 10:04
78-87-5
1.0
1
12/13/18 10:04
10061-01-5
1.0
1
12/13/18 10:04
10061-02-6
1.0
1
12/13/18 10:04
100-41-4
5.0
1
12/13/18 10:04
591-78-6
5.0
1
12/13/18 10:04
74-88-4
1.0
1
12/13/18 10:04
75-09-2
5.0
1
12/13/18 10:04
108-10-1
1.0
1
12/13/18 10:04
100-42-5
1.0
1
12/13/18 10:04
630-20-6
1.0
1
12/13/18 10:04
79-34-5
1.0
1
12/13/18 10:04
127-18-4
1.0
1
12/13/18 10:04
108-88-3
1.0
1
12/13/18 10:04
71-55-6
1.0
1
12/13/18 10:04
79-00-5
1.0
1
12/13/18 10:04
79-01-6
1.0
1
12/13/18 10:04
75-69-4
1.0
1
12/13/18 10:04
96-18-4
2.0
1
12/13/18 10:04
108-05-4
1.0
1
12/13/18 10:04
75-01-4
1.0
1
12/13/18 10:04
1330-20-7
2.0
1
12/13/18 10:04
179601-23-1
1.0
1
12/13/18 10:04
95-47-6
70-130 1
70-130 1
70-130 1
2.0 1
50-150 1
50-150 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
12/13/18 10:04 460-00-4
12/13/18 10:04 17060-07-0
12/13/18 10:04 2037-26-5
12/14/18 01:20 123-91-1
12/14/18 01:20 17060-07-0
12/14/18 01:20 2037-26-5
Page 13 of 40

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ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: BLANK Lab ID: 92409812006 Collected: 12/06/18 10:17 Received: 12/06/18 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/16/18 01:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/16/18 01:47
107-13-1
Benzene
ND
ug/L
1.0
1
12/16/18 01:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/16/18 01:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/16/18 01:47
75-27-4
Bromoform
ND
ug/L
1.0
1
12/16/18 01:47
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/16/18 01:47
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/16/18 01:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/16/18 01:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/16/18 01:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/16/18 01:47
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/16/18 01:47
75-00-3
Chloroform
ND
ug/L
1.0
1
12/16/18 01:47
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/16/18 01:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/16/18 01:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/16/18 01:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/16/18 01:47
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/16/18 01:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 01:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 01:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/16/18 01:47
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/16/18 01:47
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/16/18 01:47
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/16/18 01:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 01:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 01:47
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
1
12/16/18 01:47
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 01:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 01:47
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/16/18 01:47
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/16/18 01:47
591-78-6
lodomethane
ND
ug/L
5.0
1
12/16/18 01:47
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/16/18 01:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/16/18 01:47
108-10-1
Styrene
ND
ug/L
1.0
1
12/16/18 01:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 01:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 01:47
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/16/18 01:47
127-18-4
Toluene
ND
ug/L
1.0
1
12/16/18 01:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/16/18 01:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/16/18 01:47
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/16/18 01:47
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/16/18 01:47
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/16/18 01:47
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/16/18 01:47
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/16/18 01:47
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/16/18 01:47
1330-20-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 40

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
Sample: BLANK
Lab ID: 92409812006 Collected: 12/06/18 10:17
Received: 12/06/18 14:10 Matrix: Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
m&p-Xylene
ND ug/L
2.0
1
12/16/18 01:47
179601-23-1
o-Xylene
ND ug/L
1.0
1
12/16/18 01:47
95-47-6
Surrogates
4-Bromofluorobenzene (S)
99 %
70-130
1
12/16/18 01:47
460-00-4
1,2-Dichloroethane-d4 (S)
90 %
70-130
1
12/16/18 01:47
17060-07-0
Toluene-d8 (S)
100 %
70-130
1
12/16/18 01:47
2037-26-5
Date: 12/17/2018 04:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 40

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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
QC Batch: 446501 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92409812001, 92409812002, 92409812003, 92409812004, 92409812005
METHOD BLANK: 2447332 Matrix: Water
Associated Lab Samples: 92409812001, 92409812002, 92409812003, 92409812004, 92409812005
Blank Reporting
Parameter Units Result Limit Analyzed
Antimony
ug/L
ND
5.0
12/16/18 22:20
Arsenic
ug/L
ND
10.0
12/16/18 22:20
Barium
ug/L
ND
5.0
12/16/18 22:20
Beryllium
ug/L
ND
1.0
12/16/18 22:20
Cadmium
ug/L
ND
1.0
12/16/18 22:20
Chromium
ug/L
ND
5.0
12/16/18 22:20
Cobalt
ug/L
ND
5.0
12/16/18 22:20
Copper
ug/L
ND
5.0
12/16/18 22:20
Lead
ug/L
ND
5.0
12/16/18 22:20
Nickel
ug/L
ND
5.0
12/16/18 22:20
Selenium
ug/L
ND
10.0
12/16/18 22:20
Silver
ug/L
ND
5.0
12/16/18 22:20
Thallium
ug/L
ND
10.0
12/16/18 22:20
Vanadium
ug/L
ND
5.0
12/16/18 22:20
Zinc
ug/L
ND
10.0
12/16/18 22:20
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2447333
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
498
100
80-120
Arsenic
ug/L
500
487
97
80-120
Barium
ug/L
500
493
99
80-120
Beryllium
ug/L
500
495
99
80-120
Cadmium
ug/L
500
476
95
80-120
Chromium
ug/L
500
495
99
80-120
Cobalt
ug/L
500
484
97
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
470
94
80-120
Nickel
ug/L
500
484
97
80-120
Selenium
ug/L
500
481
96
80-120
Silver
ug/L
250
259
103
80-120
Thallium
ug/L
500
474
95
80-120
Vanadium
ug/L
500
491
98
80-120
Zinc
ug/L
500
464
93
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 40

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409812
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2447334
2447335
MS
MSD
92409528002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
356
341
71
68
75-125
5 M1
Arsenic
ug/L
ND
500
500
476
474
95
94
75-125
1
Barium
ug/L
122
500
500
602
596
96
95
75-125
1
Beryllium
ug/L
1.4
500
500
502
499
100
100
75-125
1
Cadmium
ug/L
ND
500
500
465
463
93
93
75-125
0
Chromium
ug/L
7.2
500
500
496
493
98
97
75-125
1
Cobalt
ug/L
11.8
500
500
490
489
96
95
75-125
0
Copper
ug/L
12.6
500
500
523
519
102
101
75-125
1
Lead
ug/L
9.2
500
500
466
464
91
91
75-125
1
Nickel
ug/L
12.2
500
500
489
487
95
95
75-125
0
Selenium
ug/L
ND
500
500
492
487
98
97
75-125
1
Silver
ug/L
ND
250
250
253
252
101
101
75-125
0
Thallium
ug/L
ND
500
500
459
457
92
91
75-125
0
Vanadium
ug/L
14.6
500
500
498
497
97
96
75-125
0
Zinc
ug/L
34.2
500
500
502
507
93
95
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 40

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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
QC Batch: 446879 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92409812001, 92409812002, 92409812003, 92409812004, 92409812005
METHOD BLANK: 2449121 Matrix: Water
Associated Lab Samples: 92409812001, 92409812002, 92409812003, 92409812004, 92409812005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Thallium ug/L ND 0.10 12/14/18 23:02
LABORATORY CONTROL SAMPLE: 2449122
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 9.9 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449123 2449124
MS MSD
92409256007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Thallium ug/L ND 10 10 10.2 10.0 102 100 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
QC Batch: 447140 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92409812001, 92409812002, 92409812003, 92409812005
METHOD BLANK: 2450452 Matrix: Water
Associated Lab Samples: 92409812001, 92409812002, 92409812003, 92409812005
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1,1-Trichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1,2-Trichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1-Dichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,1-Dichloroethene
ug/L
ND
1.0
12/13/18 05:13
1,2,3-Trichloropropane
ug/L
ND
1.0
12/13/18 05:13
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/13/18 05:13
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichlorobenzene
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichloroethane
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichloropropane
ug/L
ND
1.0
12/13/18 05:13
1,4-Dichlorobenzene
ug/L
ND
1.0
12/13/18 05:13
2-Butanone (MEK)
ug/L
ND
5.0
12/13/18 05:13
2-Hexanone
ug/L
ND
5.0
12/13/18 05:13
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/13/18 05:13
Acetone
ug/L
ND
25.0
12/13/18 05:13
Acrylonitrile
ug/L
ND
10.0
12/13/18 05:13
Benzene
ug/L
ND
1.0
12/13/18 05:13
Bromochloromethane
ug/L
ND
1.0
12/13/18 05:13
Bromodichloromethane
ug/L
ND
1.0
12/13/18 05:13
Bromoform
ug/L
ND
1.0
12/13/18 05:13
Bromomethane
ug/L
ND
2.0
12/13/18 05:13
Carbon disulfide
ug/L
ND
2.0
12/13/18 05:13
Carbon tetrachloride
ug/L
ND
1.0
12/13/18 05:13
Chlorobenzene
ug/L
ND
1.0
12/13/18 05:13
Chloroethane
ug/L
ND
1.0
12/13/18 05:13
Chloroform
ug/L
ND
1.0
12/13/18 05:13
Chloromethane
ug/L
ND
1.0
12/13/18 05:13
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/13/18 05:13
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/13/18 05:13
Dibromochloromethane
ug/L
ND
1.0
12/13/18 05:13
Dibromomethane
ug/L
ND
1.0
12/13/18 05:13
Ethylbenzene
ug/L
ND
1.0
12/13/18 05:13
lodomethane
ug/L
ND
5.0
12/13/18 05:13
m&p-Xylene
ug/L
ND
2.0
12/13/18 05:13
Methylene Chloride
ug/L
ND
1.0
12/13/18 05:13
o-Xylene
ug/L
ND
1.0
12/13/18 05:13
Styrene
ug/L
ND
1.0
12/13/18 05:13
Tetrachloroethene
ug/L
ND
1.0
12/13/18 05:13
Toluene
ug/L
ND
1.0
12/13/18 05:13
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
METHOD BLANK: 2450452 Matrix: Water
Associated Lab Samples: 92409812001, 92409812002, 92409812003, 92409812005
Blank Reporting
Parameter Units Result Limit
Analyzed
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/13/18 05:13
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/13/18 05:13
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/13/18 05:13
Trichloroethene
ug/L
ND
1.0
12/13/18 05:13
Trichlorofluoromethane
ug/L
ND
1.0
12/13/18 05:13
Vinyl acetate
ug/L
ND
2.0
12/13/18 05:13
Vinyl chloride
ug/L
ND
1.0
12/13/18 05:13
Xylene (Total)
ug/L
ND
1.0
12/13/18 05:13
1,2-Dichloroethane-d4 (S)
%
88
70-130
12/13/18 05:13
4-Bromofluorobenzene (S)
%
100
70-130
12/13/18 05:13
Toluene-d8 (S)
%
102
70-130
12/13/18 05:13
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2450453
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.1
104
70-130
1,1,1-Trichloroethane
ug/L
50
45.0
90
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.6
105
70-130
1,1,2-Trichloroethane
ug/L
50
53.5
107
70-130
1,1-Dichloroethane
ug/L
50
48.1
96
70-130
1,1-Dichloroethene
ug/L
50
47.7
95
70-130
1,2,3-Trichloropropane
ug/L
50
46.0
92
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.3
103
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.1
100
70-130
1,2-Dichlorobenzene
ug/L
50
49.7
99
70-130
1,2-Dichloroethane
ug/L
50
45.7
91
70-130
1,2-Dichloropropane
ug/L
50
50.1
100
70-130
1,4-Dichlorobenzene
ug/L
50
49.2
98
70-130
2-Butanone (MEK)
ug/L
100
92.5
93
64-135
2-Hexanone
ug/L
100
102
102
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
102
102
70-130
Acetone
ug/L
100
91.9
92
61-157
Acrylonitrile
ug/L
250
228
91
61-143
Benzene
ug/L
50
52.7
105
70-130
Bromochloromethane
ug/L
50
48.4
97
70-130
Bromodichloromethane
ug/L
50
52.7
105
70-130
Bromoform
ug/L
50
46.8
94
70-130
Bromomethane
ug/L
50
43.1
86
38-130
Carbon disulfide
ug/L
50
47.3
95
68-130
Carbon tetrachloride
ug/L
50
51.3
103
70-130
Chlorobenzene
ug/L
50
50.8
102
70-130
Chloroethane
ug/L
50
45.3
91
37-142
Chloroform
ug/L
50
45.8
92
70-130
Chloromethane
ug/L
50
42.5
85
48-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
LABORATORY CONTROL SAMPLE:
2450453
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
47.3
95
70-130
cis-1,3-Dichloropropene
ug/L
50
51.9
104
70-130
Dibromochloromethane
ug/L
50
51.0
102
70-130
Dibromomethane
ug/L
50
54.7
109
70-130
Ethylbenzene
ug/L
50
51.6
103
70-130
lodomethane
ug/L
100
94.4
94
40-130
m&p-Xylene
ug/L
100
104
104
70-130
Methylene Chloride
ug/L
50
44.9
90
67-132
o-Xylene
ug/L
50
53.7
107
70-130
Styrene
ug/L
50
52.8
106
70-130
Tetrachloroethene
ug/L
50
51.0
102
69-130
Toluene
ug/L
50
62.6
125
70-130
trans-1,2-Dichloroethene
ug/L
50
47.9
96
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.9
106
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
51.0
102
35-189
Trichloroethene
ug/L
50
51.4
103
70-130
Trichlorofluoromethane
ug/L
50
46.2
92
63-130
Vinyl acetate
ug/L
100
98.3
98
55-143
Vinyl chloride
ug/L
50
46.5
93
70-131
Xylene (Total)
ug/L
150
158
105
70-130
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
103
70-130
Toluene-d8 (S)
%
102
70-130
MATRIX SPIKE SAMPLE:
2450490
92409812005
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.5
102
73-134
1,1,1-Trichloroethane
ug/L
ND
20
19.0
95
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.8
99
70-136
1,1,2-Trichloroethane
ug/L
ND
20
20.7
103
70-135
1,1-Dichloroethane
ug/L
ND
20
19.4
97
70-139
1,1-Dichloroethene
ug/L
ND
20
19.5
97
70-154
1,2,3-Trichloropropane
ug/L
ND
20
20.9
104
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
18.9
95
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.1
95
70-137
1,2-Dichlorobenzene
ug/L
ND
20
18.8
94
70-133
1,2-Dichloroethane
ug/L
ND
20
18.1
90
70-137
1,2-Dichloropropene
ug/L
ND
20
19.2
96
70-140
1,4-Dichlorobenzene
ug/L
ND
20
18.3
92
70-133
2-Butanone (MEK)
ug/L
ND
40
38.1
95
60-139
2-Hexanone
ug/L
ND
40
40.5
101
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40.0
100
65-135
Acetone
ug/L
ND
40
40.9
102
60-148
Acrylonitrile
ug/L
ND
100
90.7
91
64-147
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
MATRIX SPIKE SAMPLE:
Parameter
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Ethylbenzene
lodomethane
m&p-Xylene
Methylene Chloride
o-Xylene
Styrene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans- 1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
2450490
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
92409812005
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Spike
Conc.
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
40
40
20
20
20
20
20
20
20
20
20
20
40
20
60
MS
Result
21.0
19.7
20.4
18.4
16.4
19.0
21.0
19.7
18.3
17.6
18.0
19.3
19.2
19.6
20.6
20.5
25.3
40.3
16.1
20.6
19.8
21.0
21.3
19.8
19.5
19.4
20.8
19.8
27.9
19.0
60.9
MS
% Rec
% Rec
Limits
105 70-151
98 70-141
102 70-138
92 63-130
82 15-152
95 69-149
105 70-143
99 70-138
92 52-163
88 70-139
90 41-139
96 70-141
96 70-137
98 70-134
103 70-138
102 66-153
63 20-138
101 69-152
80 42-159
103 70-148
99 70-135
105 59-143
107 59-148
99 70-146
97 70-135
97 47-135
104 70-147
99 70-148
70 49-151
95 70-156
101 63-158
90 70-130
102 70-130
99 70-130
SAMPLE DUPLICATE: 2450489
Parameter
Units
92409664002
Result
Dup
Result RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
.78J
1,1-Dichloroethene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC.
Qualifiers
Page 22 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
SAMPLE DUPLICATE: 2450489
Parameter
Units
92409664002
Result
Dup
Result
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromochloromethane
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon disulfide
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dibromomethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
lodomethane
ug/L
ND
ND
m&p-Xylene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
o-Xylene
ug/L
ND
ND
Styrene
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans- 1,3-Dichloropropene
ug/L
ND
ND
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
.34J
Vinyl acetate
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
Xylene (Total)
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
90
86
4-Bromofluorobenzene (S)
%
99
101
Toluene-d8 (S)
%
100
101
RPD Qualifiers
5
2
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
QC Batch: 447145 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92409812004
METHOD BLANK: 2450496
Associated Lab Samples: 92409812004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/13/18 05:30
1,1,1-Trichloroethane
ug/L
ND
1.0
12/13/18 05:30
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/13/18 05:30
1,1,2-Trichloroethane
ug/L
ND
1.0
12/13/18 05:30
1,1-Dichloroethane
ug/L
ND
1.0
12/13/18 05:30
1,1-Dichloroethene
ug/L
ND
1.0
12/13/18 05:30
1,2,3-Trichloropropane
ug/L
ND
1.0
12/13/18 05:30
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/13/18 05:30
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/13/18 05:30
1,2-Dichlorobenzene
ug/L
ND
1.0
12/13/18 05:30
1,2-Dichloroethane
ug/L
ND
1.0
12/13/18 05:30
1,2-Dichloropropane
ug/L
ND
1.0
12/13/18 05:30
1,4-Dichlorobenzene
ug/L
ND
1.0
12/13/18 05:30
2-Butanone (MEK)
ug/L
ND
5.0
12/13/18 05:30
2-Hexanone
ug/L
ND
5.0
12/13/18 05:30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/13/18 05:30
Acetone
ug/L
ND
25.0
12/13/18 05:30
Acrylonitrile
ug/L
ND
10.0
12/13/18 05:30
Benzene
ug/L
ND
1.0
12/13/18 05:30
Bromochloromethane
ug/L
ND
1.0
12/13/18 05:30
Bromodichloromethane
ug/L
ND
1.0
12/13/18 05:30
Bromoform
ug/L
ND
1.0
12/13/18 05:30
Bromomethane
ug/L
ND
2.0
12/13/18 05:30
Carbon disulfide
ug/L
ND
2.0
12/13/18 05:30
Carbon tetrachloride
ug/L
ND
1.0
12/13/18 05:30
Chlorobenzene
ug/L
ND
1.0
12/13/18 05:30
Chloroethane
ug/L
ND
1.0
12/13/18 05:30
Chloroform
ug/L
ND
1.0
12/13/18 05:30
Chloromethane
ug/L
ND
1.0
12/13/18 05:30
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/13/18 05:30
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/13/18 05:30
Dibromochloromethane
ug/L
ND
1.0
12/13/18 05:30
Dibromomethane
ug/L
ND
1.0
12/13/18 05:30
Ethylbenzene
ug/L
ND
1.0
12/13/18 05:30
lodomethane
ug/L
ND
5.0
12/13/18 05:30
m&p-Xylene
ug/L
ND
2.0
12/13/18 05:30
Methylene Chloride
ug/L
ND
1.0
12/13/18 05:30
o-Xylene
ug/L
ND
1.0
12/13/18 05:30
Styrene
ug/L
ND
1.0
12/13/18 05:30
Tetrachloroethene
ug/L
ND
1.0
12/13/18 05:30
Toluene
ug/L
ND
1.0
12/13/18 05:30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
METHOD BLANK: 2450496
Associated Lab Samples: 92409812004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/13/18 05:30
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/13/18 05:30
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/13/18 05:30
Trichloroethene
ug/L
ND
1.0
12/13/18 05:30
Trichlorofluoromethane
ug/L
ND
1.0
12/13/18 05:30
Vinyl acetate
ug/L
ND
2.0
12/13/18 05:30
Vinyl chloride
ug/L
ND
1.0
12/13/18 05:30
Xylene (Total)
ug/L
ND
1.0
12/13/18 05:30
1,2-Dichloroethane-d4 (S)
%
91
70-130
12/13/18 05:30
4-Bromofluorobenzene (S)
%
102
70-130
12/13/18 05:30
Toluene-d8 (S)
%
99
70-130
12/13/18 05:30
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2450497
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
52.6
105
70-130
1,1,1-Trichloroethane
ug/L
50
46.6
93
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.5
105
70-130
1,1,2-Trichloroethane
ug/L
50
53.4
107
70-130
1,1-Dichloroethane
ug/L
50
47.5
95
70-130
1,1-Dichloroethene
ug/L
50
49.0
98
70-130
1,2,3-Trichloropropane
ug/L
50
45.3
91
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.8
104
70-130
1,2-Dibromoethane (EDB)
ug/L
50
51.0
102
70-130
1,2-Dichlorobenzene
ug/L
50
51.8
104
70-130
1,2-Dichloroethane
ug/L
50
45.5
91
70-130
1,2-Dichloropropane
ug/L
50
49.4
99
70-130
1,4-Dichlorobenzene
ug/L
50
52.0
104
70-130
2-Butanone (MEK)
ug/L
100
91.5
91
64-135
2-Hexanone
ug/L
100
101
101
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
101
101
70-130
Acetone
ug/L
100
91.0
91
61-157
Acrylonitrile
ug/L
250
231
92
61-143
Benzene
ug/L
50
53.2
106
70-130
Bromochloromethane
ug/L
50
48.8
98
70-130
Bromodichloromethane
ug/L
50
52.5
105
70-130
Bromoform
ug/L
50
47.2
94
70-130
Bromomethane
ug/L
50
46.4
93
38-130
Carbon disulfide
ug/L
50
48.4
97
68-130
Carbon tetrachloride
ug/L
50
50.9
102
70-130
Chlorobenzene
ug/L
50
51.1
102
70-130
Chloroethane
ug/L
50
44.9
90
37-142
Chloroform
ug/L
50
46.7
93
70-130
Chloromethane
ug/L
50
43.9
88
48-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
LABORATORY CONTROL SAMPLE:
2450497
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
49.0
98
70-130
cis-1,3-Dichloropropene
ug/L
50
51.8
104
70-130
Dibromochloromethane
ug/L
50
52.2
104
70-130
Dibromomethane
ug/L
50
53.4
107
70-130
Ethylbenzene
ug/L
50
52.0
104
70-130
lodomethane
ug/L
100
94.2
94
40-130
m&p-Xylene
ug/L
100
105
105
70-130
Methylene Chloride
ug/L
50
45.9
92
67-132
o-Xylene
ug/L
50
53.7
107
70-130
Styrene
ug/L
50
53.0
106
70-130
Tetrachloroethene
ug/L
50
51.6
103
69-130
Toluene
ug/L
50
51.6
103
70-130
trans-1,2-Dichloroethene
ug/L
50
48.8
98
70-130
trans- 1,3-Dichloropropene
ug/L
50
51.7
103
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
49.8
100
35-189
Trichloroethene
ug/L
50
52.5
105
70-130
Trichlorofluoromethane
ug/L
50
46.1
92
63-130
Vinyl acetate
ug/L
100
100
100
55-143
Vinyl chloride
ug/L
50
46.5
93
70-131
Xylene (Total)
ug/L
150
159
106
70-130
1,2-Dichloroethane-d4 (S)
%
89
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2450498
2450499
MS
MSD
92409793004
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
18.3
19.2
92
96
73-134
4
1,1,1-Trichloroethane
ug/L
ND
20
20
20.0
20.9
100
104
82-143
4
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
17.8
19.3
89
97
70-136
8
1,1,2-Trichloroethane
ug/L
ND
20
20
19.2
19.0
96
95
70-135
1
1,1-Dichloroethane
ug/L
ND
20
20
19.8
20.3
99
101
70-139
3
1,1-Dichloroethene
ug/L
ND
20
20
20.3
19.5
102
97
70-154
4
1,2,3-Trichloropropane
ug/L
ND
20
20
17.8
18.4
89
92
71-137
4
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
17.3
17.7
87
89
65-134
2
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
17.7
19.2
89
96
70-137
8
1,2-Dichlorobenzene
ug/L
ND
20
20
18.7
19.1
93
95
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
19.2
19.4
96
97
70-137
1
1,2-Dichloropropane
ug/L
ND
20
20
19.8
19.7
99
98
70-140
0
1,4-Dichlorobenzene
ug/L
ND
20
20
18.5
19.2
92
96
70-133
4
2-Butanone (MEK)
ug/L
ND
40
40
38.4
40.8
96
102
60-139
6
2-Hexanone
ug/L
ND
40
40
32.2
35.2
80
88
65-138
9
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
35.8
36.1
89
90
65-135
1
Acetone
ug/L
ND
40
40
34.5
35.0
86
87
60-148
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 40

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2450498
2450499
MS
MSD
92409793004
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Acrylonitrile
ug/L
ND
100
100
96.6
97.9
97
98
64-147
1
Benzene
ug/L
ND
20
20
21.0
20.4
105
102
70-151
3
Bromochloromethane
ug/L
ND
20
20
19.3
20.3
97
102
70-141
5
Bromodichloromethane
ug/L
ND
20
20
18.8
18.3
94
92
70-138
3
Bromoform
ug/L
ND
20
20
14.0
14.8
70
74
63-130
6
Bromomethane
ug/L
ND
20
20
16.1
16.9
81
84
15-152
5
Carbon disulfide
ug/L
ND
20
20
19.2
19.7
96
99
69-149
2
Carbon tetrachloride
ug/L
ND
20
20
19.6
19.6
98
98
70-143
0
Chlorobenzene
ug/L
ND
20
20
18.3
19.1
92
96
70-138
4
Chloroethane
ug/L
ND
20
20
18.5
20.2
93
101
52-163
9
Chloroform
ug/L
ND
20
20
20.7
20.5
103
103
70-139
1
Chloromethane
ug/L
ND
20
20
18.2
17.4
91
87
41-139
4
cis-1,2-Dichloroethene
ug/L
3.9
20
20
24.9
24.9
105
105
70-141
0
cis-1,3-Dichloropropene
ug/L
ND
20
20
19.6
18.7
98
93
70-137
5
Dibromochloromethane
ug/L
ND
20
20
17.1
18.2
85
91
70-134
7
Dibromomethane
ug/L
ND
20
20
19.2
18.6
96
93
70-138
3
Ethylbenzene
ug/L
ND
20
20
18.8
19.7
94
99
66-153
5
lodomethane
ug/L
ND
40
40
18.2
22.2
45
55
20-138
20
m&p-Xylene
ug/L
ND
40
40
38.8
39.8
97
100
69-152
3
Methylene Chloride
ug/L
ND
20
20
19.4
19.0
97
95
42-159
2
o-Xylene
ug/L
ND
20
20
18.6
19.4
93
97
70-148
4
Styrene
ug/L
ND
20
20
19.0
19.3
95
96
70-135
1
Tetrachloroethene
ug/L
ND
20
20
18.6
19.1
93
96
59-143
3
Toluene
ug/L
ND
20
20
19.3
19.0
97
95
59-148
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
19.5
18.7
97
93
70-146
4
trans- 1,3-Dichloropropene
ug/L
ND
20
20
19.5
18.8
97
94
70-135
3
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
18.0
17.2
90
86
47-135
4
Trichloroethene
ug/L
ND
20
20
21.8
21.1
109
106
70-147
3
Trichlorofluoromethane
ug/L
ND
20
20
19.9
19.7
100
99
70-148
1
Vinyl acetate
ug/L
ND
40
40
40.4
42.0
101
105
49-151
4
Vinyl chloride
ug/L
ND
20
20
21.1
21.2
105
106
70-156
0
Xylene (Total)
ug/L
ND
60
60
57.4
59.3
96
99
63-158
3
1,2-Dichloroethane-d4 (S)
%
96
91
70-130
4-Bromofluorobenzene (S)
%
101
102
70-130
Toluene-d8(S)
%
101
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
QC Batch: 447864 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92409812006
METHOD BLANK: 2453789
Associated Lab Samples: 92409812006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1,1-Trichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1,2-Trichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1-Dichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1-Dichloroethene
ug/L
ND
1.0
12/16/18 00:56
1,2,3-Trichloropropane
ug/L
ND
1.0
12/16/18 00:56
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/16/18 00:56
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichlorobenzene
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichloropropane
ug/L
ND
1.0
12/16/18 00:56
1,4-Dichlorobenzene
ug/L
ND
1.0
12/16/18 00:56
2-Butanone (MEK)
ug/L
ND
5.0
12/16/18 00:56
2-Hexanone
ug/L
ND
5.0
12/16/18 00:56
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/16/18 00:56
Acetone
ug/L
ND
25.0
12/16/18 00:56
Acrylonitrile
ug/L
ND
10.0
12/16/18 00:56
Benzene
ug/L
ND
1.0
12/16/18 00:56
Bromochloromethane
ug/L
ND
1.0
12/16/18 00:56
Bromodichloromethane
ug/L
ND
1.0
12/16/18 00:56
Bromoform
ug/L
ND
1.0
12/16/18 00:56
Bromomethane
ug/L
ND
2.0
12/16/18 00:56
Carbon disulfide
ug/L
ND
2.0
12/16/18 00:56
Carbon tetrachloride
ug/L
ND
1.0
12/16/18 00:56
Chlorobenzene
ug/L
ND
1.0
12/16/18 00:56
Chloroethane
ug/L
ND
1.0
12/16/18 00:56
Chloroform
ug/L
ND
1.0
12/16/18 00:56
Chloromethane
ug/L
ND
1.0
12/16/18 00:56
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/16/18 00:56
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/16/18 00:56
Dibromochloromethane
ug/L
ND
1.0
12/16/18 00:56
Dibromomethane
ug/L
ND
1.0
12/16/18 00:56
Ethylbenzene
ug/L
ND
1.0
12/16/18 00:56
lodomethane
ug/L
ND
5.0
12/16/18 00:56
m&p-Xylene
ug/L
ND
2.0
12/16/18 00:56
Methylene Chloride
ug/L
ND
1.0
12/16/18 00:56
o-Xylene
ug/L
ND
1.0
12/16/18 00:56
Styrene
ug/L
ND
1.0
12/16/18 00:56
Tetrachloroethene
ug/L
ND
1.0
12/16/18 00:56
Toluene
ug/L
ND
1.0
12/16/18 00:56
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 40

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
METHOD BLANK: 2453789
Associated Lab Samples: 92409812006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/16/18 00:56
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/16/18 00:56
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/16/18 00:56
Trichloroethene
ug/L
ND
1.0
12/16/18 00:56
Trichlorofluoromethane
ug/L
ND
1.0
12/16/18 00:56
Vinyl acetate
ug/L
ND
2.0
12/16/18 00:56
Vinyl chloride
ug/L
ND
1.0
12/16/18 00:56
Xylene (Total)
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichloroethane-d4 (S)
%
84
70-130
12/16/18 00:56
4-Bromofluorobenzene (S)
%
100
70-130
12/16/18 00:56
Toluene-d8 (S)
%
100
70-130
12/16/18 00:56
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2453790
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
70-130
1,1,1-Trichloroethane
ug/L
50
49.1
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.7
105
70-130
1,1,2-Trichloroethane
ug/L
50
54.8
110
70-130
1,1-Dichloroethane
ug/L
50
50.8
102
70-130
1,1-Dichloroethene
ug/L
50
52.2
104
70-130
1,2,3-Trichloropropane
ug/L
50
45.9
92
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.0
106
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.3
101
70-130
1,2-Dichlorobenzene
ug/L
50
48.6
97
70-130
1,2-Dichloroethane
ug/L
50
48.2
96
70-130
1,2-Dichloropropane
ug/L
50
50.0
100
70-130
1,4-Dichlorobenzene
ug/L
50
47.9
96
70-130
2-Butanone (MEK)
ug/L
100
96.4
96
64-135
2-Hexanone
ug/L
100
97.2
97
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
97.8
98
70-130
Acetone
ug/L
100
96.3
96
61-157
Acrylonitrile
ug/L
250
246
98
61-143
Benzene
ug/L
50
53.8
108
70-130
Bromochloromethane
ug/L
50
56.8
114
70-130
Bromodichloromethane
ug/L
50
52.8
106
70-130
Bromoform
ug/L
50
49.1
98
70-130
Bromomethane
ug/L
50
40.7
81
38-130
Carbon disulfide
ug/L
50
53.8
108
68-130
Carbon tetrachloride
ug/L
50
51.3
103
70-130
Chlorobenzene
ug/L
50
51.0
102
70-130
Chloroethane
ug/L
50
48.4
97
37-142
Chloroform
ug/L
50
49.2
98
70-130
Chloromethane
ug/L
50
45.6
91
48-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
LABORATORY CONTROL SAMPLE:
2453790
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
51.2
102
70-130
cis-1,3-Dichloropropene
ug/L
50
53.8
108
70-130
Dibromochloromethane
ug/L
50
51.5
103
70-130
Dibromomethane
ug/L
50
56.9
114
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
lodomethane
ug/L
100
90.0
90
40-130
m&p-Xylene
ug/L
100
104
104
70-130
Methylene Chloride
ug/L
50
44.4
89
67-132
o-Xylene
ug/L
50
54.2
108
70-130
Styrene
ug/L
50
52.6
105
70-130
Tetrachloroethene
ug/L
50
50.8
102
69-130
Toluene
ug/L
50
51.3
103
70-130
trans-1,2-Dichloroethene
ug/L
50
51.5
103
70-130
trans- 1,3-Dichloropropene
ug/L
50
54.3
109
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
47.9
96
35-189
Trichloroethene
ug/L
50
54.4
109
70-130
Trichlorofluoromethane
ug/L
50
51.0
102
63-130
Vinyl acetate
ug/L
100
99.9
100
55-143
Vinyl chloride
ug/L
50
51.7
103
70-131
Xylene (Total)
ug/L
150
158
105
70-130
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2453791
2453792
MS
MSD
92410469002
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
23.0
23.0
115
115
73-134
0
1,1,1-Trichloroethane
ug/L
ND
20
20
21.1
21.3
106
107
82-143
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.9
22.0
109
110
70-136
0
1,1,2-Trichloroethane
ug/L
ND
20
20
23.1
23.2
115
116
70-135
1
1,1-Dichloroethane
ug/L
ND
20
20
21.3
21.6
107
108
70-139
1
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.7
107
108
70-154
1
1,2,3-Trichloropropane
ug/L
ND
20
20
21.8
23.7
109
118
71-137
8
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.6
21.0
108
105
65-134
3
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.9
21.1
109
106
70-137
3
1,2-Dichlorobenzene
ug/L
ND
20
20
19.9
19.2
100
96
70-133
4
1,2-Dichloroethane
ug/L
ND
20
20
21.1
20.7
106
104
70-137
2
1,2-Dichloropropane
ug/L
ND
20
20
20.8
21.0
104
105
70-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
19.6
20.0
98
100
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
40.8
39.7
102
99
60-139
3
2-Hexanone
ug/L
ND
40
40
41.9
40.9
105
102
65-138
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
40.8
42.0
102
105
65-135
3
Acetone
ug/L
ND
40
40
43.4
43.8
108
110
60-148
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 40

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2453791
2453792
MS
MSD
92410469002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Acrylonitrile
ug/L
ND
100
100
96.9
97.0
97
97
64-147
0
Benzene
ug/L
ND
20
20
23.3
22.9
116
115
70-151
2
Bromochloromethane
ug/L
ND
20
20
23.6
23.6
118
118
70-141
0
Bromodichloromethane
ug/L
ND
20
20
21.8
22.3
109
112
70-138
2
Bromoform
ug/L
ND
20
20
19.7
18.8
98
94
63-130
5
Bromomethane
ug/L
ND
20
20
15.3
16.7
76
84
15-152
9
Carbon disulfide
ug/L
ND
20
20
21.5
20.4
108
102
69-149
5
Carbon tetrachloride
ug/L
ND
20
20
23.1
23.2
115
116
70-143
0
Chlorobenzene
ug/L
ND
20
20
22.0
21.5
110
107
70-138
2
Chloroethane
ug/L
ND
20
20
21.3
20.5
106
103
52-163
4
Chloroform
ug/L
ND
20
20
20.9
20.8
104
104
70-139
0
Chloromethane
ug/L
ND
20
20
16.8
16.8
84
84
41-139
0
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.6
21.4
108
107
70-141
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.3
22.0
106
110
70-137
4
Dibromochloromethane
ug/L
ND
20
20
21.0
20.8
105
104
70-134
1
Dibromomethane
ug/L
ND
20
20
23.1
23.8
116
119
70-138
3
Ethylbenzene
ug/L
ND
20
20
22.2
21.6
111
108
66-153
3
lodomethane
ug/L
ND
40
40
23.4
32.5
59
81
20-138
32 R1
m&p-Xylene
ug/L
ND
40
40
45.1
43.8
113
110
69-152
3
Methylene Chloride
ug/L
ND
20
20
17.3
17.5
86
87
42-159
1
o-Xylene
ug/L
ND
20
20
23.0
21.9
115
110
70-148
4
Styrene
ug/L
ND
20
20
22.7
21.3
114
107
70-135
6
Tetrachloroethene
ug/L
ND
20
20
22.4
21.4
112
107
59-143
4
Toluene
ug/L
ND
20
20
21.7
22.4
109
112
59-148
3
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.9
22.2
109
111
70-146
1
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.6
22.7
108
113
70-135
5
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
15.6
15.1
78
75
47-135
3
Trichloroethene
ug/L
ND
20
20
23.5
23.9
117
119
70-147
2
Trichlorofluoromethane
ug/L
ND
20
20
22.0
21.3
110
107
70-148
3
Vinyl acetate
ug/L
ND
40
40
28.7
28.4
72
71
49-151
1
Vinyl chloride
ug/L
ND
20
20
19.5
19.8
97
99
70-156
2
Xylene (Total)
ug/L
ND
60
60
68.0
65.8
113
110
63-158
3
1,2-Dichloroethane-d4 (S)
%
91
92
70-130
4-Bromofluorobenzene (S)
%
104
102
70-130
Toluene-d8(S)
%
97
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 40

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
QC Batch: 447350 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92409812002
METHOD BLANK: 2451417
Associated Lab Samples: 92409812002
Parameter
Units
1,4-Dioxane (p-Dioxane)
ug/L
1,2-Dichloroethane-d4 (S)
%
Toluene-d8 (S)
%
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 12/13/1815:41
95 50-150 12/13/1815:41
108 50-150 12/13/1815:41
LABORATORY CONTROL SAMPLE: 2451418
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane(p-Dioxane) ug/L 20 15.7 79 71-125
1,2-Dichloroethane-d4 (S) % 97 50-150
Toluene-d8(S) % 108 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2451420
2451421
MS
MSD
92409812002 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 15.3
15.0 76
75
50-150 1
1,2-Dichloroethane-d4 (S)
%
100
96
50-150
Toluene-d8(S)
%
112
109
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
QC Batch: 447353 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92409812001, 92409812003, 92409812004, 92409812005
METHOD BLANK: 2451437
Matrix:
Water
Associated Lab Samples:
92409812001, 92409812003, 92409812004, 92409812005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
12/13/18 15:21
1,2-Dichloroethane-d4 (S)
%
96
50-150
12/13/18 15:21
Toluene-d8 (S)
%
108
50-150
12/13/18 15:21
LABORATORY CONTROL SAMPLE: 2451438
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 15.2 76 71-125
1,2-Dichloroethane-d4 (S) % 101 50-150
Toluene-d8 (S) % 111 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2451439
2451440
MS
MSD
92409812005 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L ND 20
20 17.5
17.9 87
90
50-150 2
1,2-Dichloroethane-d4 (S)
%
92
92
50-150
Toluene-d8(S)
%
81
79
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409812
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 04:40 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 40

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409812
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92409812001
6001-HBW21
EPA 3010A
446501
EPA6010D
446518
92409812002
6001-HBW22
EPA 3010A
446501
EPA6010D
446518
92409812003
6001-HBW12B
EPA 3010A
446501
EPA6010D
446518
92409812004
6001-HBW17B
EPA 3010A
446501
EPA6010D
446518
92409812005
6001-MAINTE
EPA 3010A
446501
EPA6010D
446518
92409812001
6001-HBW21
EPA 3010A
446879
EPA6020B
447018
92409812002
6001-HBW22
EPA 3010A
446879
EPA6020B
447018
92409812003
6001-HBW12B
EPA 3010A
446879
EPA6020B
447018
92409812004
6001-HBW17B
EPA 3010A
446879
EPA6020B
447018
92409812005
6001-MAINTE
EPA 3010A
446879
EPA6020B
447018
92409812001
6001-HBW21
EPA 8260B
447140
92409812002
6001-HBW22
EPA 8260B
447140
92409812003
6001-HBW12B
EPA 8260B
447140
92409812004
6001-HBW17B
EPA 8260B
447145
92409812005
6001-MAINTE
EPA 8260B
447140
92409812006
BLANK
EPA 8260B
447864
92409812001
6001-HBW21
EPA 8260B Mod.
447353
92409812002
6001-HBW22
EPA 8260B Mod.
447350
92409812003
6001-HBW12B
EPA 8260B Mod.
447353
92409812004
6001-HBW17B
EPA 8260B Mod.
447353
92409812005
6001-MAINTE
EPA 8260B Mod.
447353
Date: 12/17/2018 04:40 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 35 of 40

Document Name:
Document Revised: February 7, 2018
Page 1 of 2
m
Sample Condition Upon
Receipt(SCUR)
aceAnalyticai
Document No.:
issuing Authority:
Pace Carolinas Quality Office
F-CAR-CS-033-Rev.06
r
Laboratory receiving samples:
Asheville ❑ Eden❑
Greenwood ❑
Huntersville Raleigh❑ Mechanicsville�l
118
Name:
0 : 92409812
SampleClient
Project
°LUSh�Q�elllllll
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-�
Courier:
Fed Ex❑U ❑
❑ Commercial ❑pace
❑Other:
+�74Q981.2
Custody Seal Present? [-]Yes Egdo/
Seals Intact? Dyes
DKO�
�} J Z
Date/Initials Person Examining Contents b
Packing Material: ❑Bubble Wrap
❑bubble Bags one
❑ Other
BialogicaiTissue Frozen?
❑Yes to ❑N/A
Thermometer: �ZTi7�6
IR Gun ID:
Type of Ice: [wet
❑Blue
❑None
a
CL
C
Cooler Temp (°C): 3 Correction Factor: Add/Subtract (°C}
�
(),�
Temp should be above freezing #0 6°C
�
�
`{
Cooler Temp Corrected S°C ►:
❑Samples out of temp criteria Samples on tce, cooling process
a
a
has begun
USDA Regulated Soil Q N/A, water sample)
Did samples vrigi to in a quarantine zone within
the United States: CA, NY, or SC
(check maps)?
Old samples originate from a foreign source (internationaliy,
including Hawaii and Puerto Rico)? [--]Yes ❑No
O
a
�
❑Yes No
Comments/Discrepancy:in
Chain of Custody Present?
il3�� ❑No
[]N/A
I.
Samples Arrived within Hold Time?
0`res [:]No
❑N/A
Z•
Short Hold TimeAnalysis (<72 hr.)?
13Z ❑No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes Na
[]N/A
4•
Sufficient Volume?
es ❑No
❑N/A
5.
Correct Containers Used?
❑❑No
[I NIA
6.
-Pace Containers Used?
�4
Yes No
N/A
Containers Intact?
i3Ye5 [-]No
❑N/A.
7,
Dissolved analysis: samples Field Filtered?
❑Yes I2No
❑N/A
S.
Sample Labels Match COO
, es [:]No
❑NIA
9.
-includes Date/Time/€D/Analysis Matrix: V v 1
Headspace in VOA Vials (>5-6mm)? ❑Y 01(. ❑N/A 10,
Trip Blank Present? Qfes ❑No ❑N/A 11.
Trin BlankCustodv Seals Present? ❑Yes ❑No ❑N/A
Field Data Required? Dyes []NO
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
I
Person contacted: Date/Timei
Date:
Project Manager SCURF Review:
Project Manager 5RF Review: Date. _ I
Page 36 of 40

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m
Document Name:
Sample Condition Upon Receipt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
F-CAR-CS-033-Rev.06
Issuing Authority:
Pace Carolinas Quality Office
aceAnalXicai
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville [ Raleigh[] Mechanicsviller-1
SampleClient Name: 10 924p9812
- . � , � Project
M(� IV 1 rt S l h'-� �w llll�t Courier: Fed Ex ❑U ❑USP ❑ Tent��1"
❑ Commercial ❑Pace ❑Other: !320981.7
Custody Seal Present? Des Leo Seals Intact? Des ❑K6 `)
Date/initials Person Examining Contents:)
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑9 ne ❑ Other Biological❑
T'ssue Fro
mzen?.
Thermoeter ❑Yes EMo N/A
Q'iR Gun ID;
92TO46
Type of Ice: Wet []Blue []None
Cooler Temp (°C): �Correction Factor: Add/Subtract (°C) 0.0
Cooler Temp Corrected (°C): '
USDA Regulated Soil ( N/A, water sample)
Did samples origji 6to in a quarantine zone within the United States: CA, NY, or SC (check maps)?
n,.o, Ifni.,
Temp should be above freezing to VC
[]Samples out of temp criteria. Samples on ice, cooling process
has hegun
Did samples originate from a foreign source (internationally,
inchidine Hawaii and Puerto Ricol? ❑Yes []No
Comments/Discrepancy:
Chain of Custody Present?
[]NO
El N/A
1,
des
Samples Arrived within hold Time?
' Ves
❑No
❑NIA
2.
Short Hold Time Analysis (<72 hr.)?
es❑_,,NN.
❑N/A
3.
Rush Turn Around Time Requested?
]Yes
(�No
❑N/A
4.
Sufficient Volume?
EKs
❑No
❑N/A
S.
Correct Containers Used?
EjY
❑No
❑N/A
6.
-Pace Containers Used?
Yews
❑No
❑NIA
Containers Intact?
®Ye5
[IN.
El N/A.
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
E3 o
❑N/A
8.
Sample Labels Match COC?
Q(es
❑No
❑N/A
9.
AncludesDate/Tirne/ID/Analysis Matrix: V V
!
lieadspace in VOA Vials (55-6mm)?
❑Y
ro
❑N/A
10.
Trip Blank Present?
es
[:]No
[]N/A
11.
Trip Blank Custody Seals Present?
❑yes
lido
❑N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time: _
Project Manager SCURF Review:
Project Manager SRF Review: / r
Field Data Required? ❑Yes [-]NO
Date: ? f
Date: S
Page 38 of 40

Document Name; Document Revised: February 7, 2018
m Sample Condition Upon Receipt(SCUR) Page 1 of 2
5,qlceAnapical Document No.: Issuing Authority:
f F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
_ . A
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project IWo# : 92409U 14
Due Date: 12/20/18
12M : MWB
CLIENT:
92—thECK CO
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot p
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Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a Copy Of this form will he sent to the North Carolina DEHNR Certification Office OA
Out of hold, interred preservative, out of temp, incorrect containers.
Page 39 of 40

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Page 40 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
December 17, 2018
Amber Grzymski
Mecklenburg County Solid Waste
2145 Suttle Avenue
Charlotte, NC 28208
RE: Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Dear Amber Grzymski:
Enclosed are the analytical results for sample(s) received by the laboratory on December 05, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 22

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 22

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409667
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92409667001
6001-HB2006
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409667002
6001-HB2008
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
92409667003
6001-HB2010
EPA 6010D
SH1
15
PASI-A
EPA 6020E
SER
1
PASI-A
EPA 8260E
CL
52
PASI-C
EPA 8260B Mod.
DLK
3
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 22

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Sample: 6001-HB2006 Lab ID: 92409667001 Collected: 12/05/18 12:55 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:23
7440-38-2
Barium
28.6
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:23
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:23
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-48-4
Copper
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:23
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:23
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:23
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:23
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 20:46
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/16/18 03:30
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/16/18 03:30
107-13-1
Benzene
ND
ug/L
1.0
1
12/16/18 03:30
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/16/18 03:30
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/16/18 03:30
75-27-4
Bromoform
ND
ug/L
1.0
1
12/16/18 03:30
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/16/18 03:30
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/16/18 03:30
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/16/18 03:30
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/16/18 03:30
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/16/18 03:30
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/16/18 03:30
75-00-3
Chloroform
ND
ug/L
1.0
1
12/16/18 03:30
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/16/18 03:30
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/16/18 03:30
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/16/18 03:30
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/16/18 03:30
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/16/18 03:30
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 03:30
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 03:30
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/16/18 03:30
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/16/18 03:30
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/16/18 03:30
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/16/18 03:30
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 03:30
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 03:30
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 06:44 PM
without
the written consent of Pace Analytical Services, LLC.
Page 4 of 22

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Sample: 6001-HB2006 Lab ID: 92409667001 Collected: 12/05/18 12:55 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/16/18 03:30
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 03:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 03:30
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/16/18 03:30
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/16/18 03:30
591-78-6
lodomethane
ND
ug/L
5.0
1
12/16/18 03:30
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/16/18 03:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/16/18 03:30
108-10-1
Styrene
ND
ug/L
1.0
1
12/16/18 03:30
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 03:30
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 03:30
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/16/18 03:30
127-18-4
Toluene
ND
ug/L
1.0
1
12/16/18 03:30
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/16/18 03:30
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/16/18 03:30
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/16/18 03:30
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/16/18 03:30
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/16/18 03:30
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/16/18 03:30
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/16/18 03:30
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/16/18 03:30
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/16/18 03:30
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/16/18 03:30
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/16/18 03:30
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
12/16/18 03:30
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
12/16/18 03:30
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/13/18 00:55
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
50-150
1
12/13/18 00:55
17060-07-0
Toluene-d8 (S)
109
%
50-150
1
12/13/18 00:55
2037-26-5
Date: 12/17/2018 06:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 22

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Sample: 6001-HB2008 Lab ID: 92409667002 Collected: 12/05/18 13:07 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:26
7440-38-2
Barium
22.9
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:26
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:26
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-48-4
Copper
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:26
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:26
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:26
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:26
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 20:48
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/16/18 03:47
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/16/18 03:47
107-13-1
Benzene
ND
ug/L
1.0
1
12/16/18 03:47
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/16/18 03:47
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/16/18 03:47
75-27-4
Bromoform
ND
ug/L
1.0
1
12/16/18 03:47
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/16/18 03:47
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/16/18 03:47
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/16/18 03:47
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/16/18 03:47
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/16/18 03:47
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/16/18 03:47
75-00-3
Chloroform
ND
ug/L
1.0
1
12/16/18 03:47
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/16/18 03:47
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/16/18 03:47
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/16/18 03:47
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/16/18 03:47
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/16/18 03:47
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 03:47
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 03:47
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/16/18 03:47
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/16/18 03:47
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/16/18 03:47
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/16/18 03:47
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 03:47
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 03:47
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 06:44 PM
without
the written consent of Pace Analytical Services, LLC.
Page 6 of 22

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Sample: 6001-HB2008 Lab ID: 92409667002 Collected: 12/05/18 13:07 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/16/18 03:47
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 03:47
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 03:47
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/16/18 03:47
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/16/18 03:47
591-78-6
lodomethane
ND
ug/L
5.0
1
12/16/18 03:47
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/16/18 03:47
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/16/18 03:47
108-10-1
Styrene
ND
ug/L
1.0
1
12/16/18 03:47
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 03:47
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 03:47
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/16/18 03:47
127-18-4
Toluene
ND
ug/L
1.0
1
12/16/18 03:47
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/16/18 03:47
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/16/18 03:47
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/16/18 03:47
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/16/18 03:47
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/16/18 03:47
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/16/18 03:47
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/16/18 03:47
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/16/18 03:47
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/16/18 03:47
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/16/18 03:47
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/16/18 03:47
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
12/16/18 03:47
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
12/16/18 03:47
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/13/18 01:14
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
99
%
50-150
1
12/13/18 01:14
17060-07-0
Toluene-d8 (S)
109
%
50-150
1
12/13/18 01:14
2037-26-5
Date: 12/17/2018 06:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 22

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Sample: 6001-HB2010 Lab ID: 92409667003 Collected: 12/05/18 11:55 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-36-0
Arsenic
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:35
7440-38-2
Barium
44.3
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-39-3
Beryllium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:35
7440-41-7
Cadmium
ND
ug/L
1.0
1
12/08/18 03:15
12/16/18 23:35
7440-43-9
Chromium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-47-3
Cobalt
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-48-4
Copper
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-50-8
Lead
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7439-92-1
Nickel
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-02-0
Selenium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:35
7782-49-2
Silver
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-22-4
Thallium
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:35
7440-28-0
Vanadium
ND
ug/L
5.0
1
12/08/18 03:15
12/16/18 23:35
7440-62-2
Zinc
ND
ug/L
10.0
1
12/08/18 03:15
12/16/18 23:35
7440-66-6
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Thallium
ND
ug/L
0.10
1 12/12/18 03:00
12/14/18 20:51
7440-28-0
8260 MSV Low Level Landfill
Analytical Method: EPA 8260E
Acetone
ND
ug/L
25.0
1
12/16/18 04:04
67-64-1
Acrylonitrile
ND
ug/L
10.0
1
12/16/18 04:04
107-13-1
Benzene
ND
ug/L
1.0
1
12/16/18 04:04
71-43-2
Bromochloromethane
ND
ug/L
1.0
1
12/16/18 04:04
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
12/16/18 04:04
75-27-4
Bromoform
ND
ug/L
1.0
1
12/16/18 04:04
75-25-2
Bromomethane
ND
ug/L
2.0
1
12/16/18 04:04
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
12/16/18 04:04
78-93-3
Carbon disulfide
ND
ug/L
2.0
1
12/16/18 04:04
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
1
12/16/18 04:04
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
12/16/18 04:04
108-90-7
Chloroethane
ND
ug/L
1.0
1
12/16/18 04:04
75-00-3
Chloroform
ND
ug/L
1.0
1
12/16/18 04:04
67-66-3
Chloromethane
ND
ug/L
1.0
1
12/16/18 04:04
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
1
12/16/18 04:04
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
12/16/18 04:04
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
12/16/18 04:04
106-93-4
Dibromomethane
ND
ug/L
1.0
1
12/16/18 04:04
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 04:04
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
12/16/18 04:04
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
1
12/16/18 04:04
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
1
12/16/18 04:04
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
1
12/16/18 04:04
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
1
12/16/18 04:04
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 04:04
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
1
12/16/18 04:04
156-60-5
REPORT OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 12/17/2018 06:44 PM
without
the written consent of Pace Analytical Services, LLC.
Page 8 of 22

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
Sample: 6001-HB2010 Lab ID: 92409667003 Collected: 12/05/18 11:55 Received: 12/05/18 15:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level Landfill Analytical Method: EPA 8260E
1,2-Dichloropropane
ND
ug/L
1.0
1
12/16/18 04:04
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 04:04
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
1
12/16/18 04:04
10061-02-6
Ethylbenzene
ND
ug/L
1.0
1
12/16/18 04:04
100-41-4
2-Hexanone
ND
ug/L
5.0
1
12/16/18 04:04
591-78-6
lodomethane
ND
ug/L
5.0
1
12/16/18 04:04
74-88-4
Methylene Chloride
ND
ug/L
1.0
1
12/16/18 04:04
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
1
12/16/18 04:04
108-10-1
Styrene
ND
ug/L
1.0
1
12/16/18 04:04
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 04:04
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
1
12/16/18 04:04
79-34-5
Tetrachloroethene
ND
ug/L
1.0
1
12/16/18 04:04
127-18-4
Toluene
ND
ug/L
1.0
1
12/16/18 04:04
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
1
12/16/18 04:04
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
1
12/16/18 04:04
79-00-5
Trichloroethene
ND
ug/L
1.0
1
12/16/18 04:04
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
12/16/18 04:04
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
1
12/16/18 04:04
96-18-4
Vinyl acetate
ND
ug/L
2.0
1
12/16/18 04:04
108-05-4
Vinyl chloride
ND
ug/L
1.0
1
12/16/18 04:04
75-01-4
Xylene (Total)
ND
ug/L
1.0
1
12/16/18 04:04
1330-20-7
m&p-Xylene
ND
ug/L
2.0
1
12/16/18 04:04
179601-23-1
o-Xylene
ND
ug/L
1.0
1
12/16/18 04:04
95-47-6
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/16/18 04:04
460-00-4
1,2-Dichloroethane-d4 (S)
90
%
70-130
1
12/16/18 04:04
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/16/18 04:04
2037-26-5
8260 MSV SIM
Analytical Method:
EPA 8260E Mod.
1,4-Dioxane (p-Dioxane)
ND
ug/L
2.0
1
12/13/18 01:34
123-91-1
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
50-150
1
12/13/18 01:34
17060-07-0
Toluene-d8 (S)
107
%
50-150
1
12/13/18 01:34
2037-26-5
Date: 12/17/2018 06:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 22

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[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
QC Batch: 446501 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92409667001, 92409667002, 92409667003
METHOD BLANK: 2447332 Matrix: Water
Associated Lab Samples: 92409667001, 92409667002, 92409667003
Blank Reporting
Parameter Units Result Limit
Antimony
ug/L
ND
Arsenic
ug/L
ND
Barium
ug/L
ND
Beryllium
ug/L
ND
Cadmium
ug/L
ND
Chromium
ug/L
ND
Cobalt
ug/L
ND
Copper
ug/L
ND
Lead
ug/L
ND
Nickel
ug/L
ND
Selenium
ug/L
ND
Silver
ug/L
ND
Thallium
ug/L
ND
Vanadium
ug/L
ND
Zinc
ug/L
ND
Analyzed
5.0
12/16/18 22:20
10.0
12/16/18 22:20
5.0
12/16/18 22:20
1.0
12/16/18 22:20
1.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
5.0
12/16/18 22:20
10.0
12/16/18 22:20
5.0
12/16/18 22:20
10.0
12/16/18 22:20
5.0
12/16/18 22:20
10.0
12/16/18 22:20
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2447333
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
498
100
80-120
Arsenic
ug/L
500
487
97
80-120
Barium
ug/L
500
493
99
80-120
Beryllium
ug/L
500
495
99
80-120
Cadmium
ug/L
500
476
95
80-120
Chromium
ug/L
500
495
99
80-120
Cobalt
ug/L
500
484
97
80-120
Copper
ug/L
500
512
102
80-120
Lead
ug/L
500
470
94
80-120
Nickel
ug/L
500
484
97
80-120
Selenium
ug/L
500
481
96
80-120
Silver
ug/L
250
259
103
80-120
Thallium
ug/L
500
474
95
80-120
Vanadium
ug/L
500
491
98
80-120
Zinc
ug/L
500
464
93
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 22

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409667
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2447334
2447335
MS
MSD
92409528002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Antimony
ug/L
ND
500
500
356
341
71
68
75-125
5 M1
Arsenic
ug/L
ND
500
500
476
474
95
94
75-125
1
Barium
ug/L
122
500
500
602
596
96
95
75-125
1
Beryllium
ug/L
1.4
500
500
502
499
100
100
75-125
1
Cadmium
ug/L
ND
500
500
465
463
93
93
75-125
0
Chromium
ug/L
7.2
500
500
496
493
98
97
75-125
1
Cobalt
ug/L
11.8
500
500
490
489
96
95
75-125
0
Copper
ug/L
12.6
500
500
523
519
102
101
75-125
1
Lead
ug/L
9.2
500
500
466
464
91
91
75-125
1
Nickel
ug/L
12.2
500
500
489
487
95
95
75-125
0
Selenium
ug/L
ND
500
500
492
487
98
97
75-125
1
Silver
ug/L
ND
250
250
253
252
101
101
75-125
0
Thallium
ug/L
ND
500
500
459
457
92
91
75-125
0
Vanadium
ug/L
14.6
500
500
498
497
97
96
75-125
0
Zinc
ug/L
34.2
500
500
502
507
93
95
75-125
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 22

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
QC Batch: 446878 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92409667001, 92409667002, 92409667003
METHOD BLANK: 2449117 Matrix: Water
Associated Lab Samples: 92409667001, 92409667002, 92409667003
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
Thallium ug/L ND 0.10
12/14/1819:39
LABORATORY CONTROL SAMPLE: 2449118
Spike LCS
LCS % Rec
Parameter Units Conc. Result
% Rec Limits Qualifiers
Thallium ug/L 10 9.7
97 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449119 2449120
MS MSD
92410006001 Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Thallium ug/L 0.062J 10 10 10.1
10.1 101 101 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 22

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
QC Batch: 447864 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level Landfill
Associated Lab Samples: 92409667001, 92409667002, 92409667003
METHOD BLANK: 2453789 Matrix:
Associated Lab Samples: 92409667001, 92409667002, 92409667003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1,1-Trichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1,2-Trichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1-Dichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,1-Dichloroethene
ug/L
ND
1.0
12/16/18 00:56
1,2,3-Trichloropropane
ug/L
ND
1.0
12/16/18 00:56
1,2-Dibromo-3-chloropropane
ug/L
ND
2.0
12/16/18 00:56
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichlorobenzene
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichloroethane
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichloropropane
ug/L
ND
1.0
12/16/18 00:56
1,4-Dichlorobenzene
ug/L
ND
1.0
12/16/18 00:56
2-Butanone (MEK)
ug/L
ND
5.0
12/16/18 00:56
2-Hexanone
ug/L
ND
5.0
12/16/18 00:56
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
12/16/18 00:56
Acetone
ug/L
ND
25.0
12/16/18 00:56
Acrylonitrile
ug/L
ND
10.0
12/16/18 00:56
Benzene
ug/L
ND
1.0
12/16/18 00:56
Bromochloromethane
ug/L
ND
1.0
12/16/18 00:56
Bromodichloromethane
ug/L
ND
1.0
12/16/18 00:56
Bromoform
ug/L
ND
1.0
12/16/18 00:56
Bromomethane
ug/L
ND
2.0
12/16/18 00:56
Carbon disulfide
ug/L
ND
2.0
12/16/18 00:56
Carbon tetrachloride
ug/L
ND
1.0
12/16/18 00:56
Chlorobenzene
ug/L
ND
1.0
12/16/18 00:56
Chloroethane
ug/L
ND
1.0
12/16/18 00:56
Chloroform
ug/L
ND
1.0
12/16/18 00:56
Chloromethane
ug/L
ND
1.0
12/16/18 00:56
cis-1,2-Dichloroethene
ug/L
ND
1.0
12/16/18 00:56
cis-1,3-Dichloropropene
ug/L
ND
1.0
12/16/18 00:56
Dibromochloromethane
ug/L
ND
1.0
12/16/18 00:56
Dibromomethane
ug/L
ND
1.0
12/16/18 00:56
Ethylbenzene
ug/L
ND
1.0
12/16/18 00:56
lodomethane
ug/L
ND
5.0
12/16/18 00:56
m&p-Xylene
ug/L
ND
2.0
12/16/18 00:56
Methylene Chloride
ug/L
ND
1.0
12/16/18 00:56
o-Xylene
ug/L
ND
1.0
12/16/18 00:56
Styrene
ug/L
ND
1.0
12/16/18 00:56
Tetrachloroethene
ug/L
ND
1.0
12/16/18 00:56
Toluene
ug/L
ND
1.0
12/16/18 00:56
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 22

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
METHOD BLANK: 2453789 Matrix:
Associated Lab Samples: 92409667001, 92409667002, 92409667003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
trans-1,2-Dichloroethene
ug/L
ND
1.0
12/16/18 00:56
trans- 1,3-Dichloropropene
ug/L
ND
1.0
12/16/18 00:56
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
12/16/18 00:56
Trichloroethene
ug/L
ND
1.0
12/16/18 00:56
Trichlorofluoromethane
ug/L
ND
1.0
12/16/18 00:56
Vinyl acetate
ug/L
ND
2.0
12/16/18 00:56
Vinyl chloride
ug/L
ND
1.0
12/16/18 00:56
Xylene (Total)
ug/L
ND
1.0
12/16/18 00:56
1,2-Dichloroethane-d4 (S)
%
84
70-130
12/16/18 00:56
4-Bromofluorobenzene (S)
%
100
70-130
12/16/18 00:56
Toluene-d8 (S)
%
100
70-130
12/16/18 00:56
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2453790
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.6
103
70-130
1,1,1-Trichloroethane
ug/L
50
49.1
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
52.7
105
70-130
1,1,2-Trichloroethane
ug/L
50
54.8
110
70-130
1,1-Dichloroethane
ug/L
50
50.8
102
70-130
1,1-Dichloroethene
ug/L
50
52.2
104
70-130
1,2,3-Trichloropropane
ug/L
50
45.9
92
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.0
106
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.3
101
70-130
1,2-Dichlorobenzene
ug/L
50
48.6
97
70-130
1,2-Dichloroethane
ug/L
50
48.2
96
70-130
1,2-Dichloropropane
ug/L
50
50.0
100
70-130
1,4-Dichlorobenzene
ug/L
50
47.9
96
70-130
2-Butanone (MEK)
ug/L
100
96.4
96
64-135
2-Hexanone
ug/L
100
97.2
97
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
97.8
98
70-130
Acetone
ug/L
100
96.3
96
61-157
Acrylonitrile
ug/L
250
246
98
61-143
Benzene
ug/L
50
53.8
108
70-130
Bromochloromethane
ug/L
50
56.8
114
70-130
Bromodichloromethane
ug/L
50
52.8
106
70-130
Bromoform
ug/L
50
49.1
98
70-130
Bromomethane
ug/L
50
40.7
81
38-130
Carbon disulfide
ug/L
50
53.8
108
68-130
Carbon tetrachloride
ug/L
50
51.3
103
70-130
Chlorobenzene
ug/L
50
51.0
102
70-130
Chloroethane
ug/L
50
48.4
97
37-142
Chloroform
ug/L
50
49.2
98
70-130
Chloromethane
ug/L
50
45.6
91
48-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 22

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
LABORATORY CONTROL SAMPLE:
2453790
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
cis-1,2-Dichloroethene
ug/L
50
51.2
102
70-130
cis-1,3-Dichloropropene
ug/L
50
53.8
108
70-130
Dibromochloromethane
ug/L
50
51.5
103
70-130
Dibromomethane
ug/L
50
56.9
114
70-130
Ethylbenzene
ug/L
50
51.0
102
70-130
lodomethane
ug/L
100
90.0
90
40-130
m&p-Xylene
ug/L
100
104
104
70-130
Methylene Chloride
ug/L
50
44.4
89
67-132
o-Xylene
ug/L
50
54.2
108
70-130
Styrene
ug/L
50
52.6
105
70-130
Tetrachloroethene
ug/L
50
50.8
102
69-130
Toluene
ug/L
50
51.3
103
70-130
trans-1,2-Dichloroethene
ug/L
50
51.5
103
70-130
trans- 1,3-Dichloropropene
ug/L
50
54.3
109
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
47.9
96
35-189
Trichloroethene
ug/L
50
54.4
109
70-130
Trichlorofluoromethane
ug/L
50
51.0
102
63-130
Vinyl acetate
ug/L
100
99.9
100
55-143
Vinyl chloride
ug/L
50
51.7
103
70-131
Xylene (Total)
ug/L
150
158
105
70-130
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2453791
2453792
MS
MSD
92410469002
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
23.0
23.0
115
115
73-134
0
1,1,1-Trichloroethane
ug/L
ND
20
20
21.1
21.3
106
107
82-143
1
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
21.9
22.0
109
110
70-136
0
1,1,2-Trichloroethane
ug/L
ND
20
20
23.1
23.2
115
116
70-135
1
1,1-Dichloroethane
ug/L
ND
20
20
21.3
21.6
107
108
70-139
1
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.7
107
108
70-154
1
1,2,3-Trichloropropane
ug/L
ND
20
20
21.8
23.7
109
118
71-137
8
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
21.6
21.0
108
105
65-134
3
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.9
21.1
109
106
70-137
3
1,2-Dichlorobenzene
ug/L
ND
20
20
19.9
19.2
100
96
70-133
4
1,2-Dichloroethane
ug/L
ND
20
20
21.1
20.7
106
104
70-137
2
1,2-Dichloropropane
ug/L
ND
20
20
20.8
21.0
104
105
70-140
1
1,4-Dichlorobenzene
ug/L
ND
20
20
19.6
20.0
98
100
70-133
2
2-Butanone (MEK)
ug/L
ND
40
40
40.8
39.7
102
99
60-139
3
2-Hexanone
ug/L
ND
40
40
41.9
40.9
105
102
65-138
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
40.8
42.0
102
105
65-135
3
Acetone
ug/L
ND
40
40
43.4
43.8
108
110
60-148
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 22

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2453791
2453792
MS
MSD
92410469002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Acrylonitrile
ug/L
ND
100
100
96.9
97.0
97
97
64-147
0
Benzene
ug/L
ND
20
20
23.3
22.9
116
115
70-151
2
Bromochloromethane
ug/L
ND
20
20
23.6
23.6
118
118
70-141
0
Bromodichloromethane
ug/L
ND
20
20
21.8
22.3
109
112
70-138
2
Bromoform
ug/L
ND
20
20
19.7
18.8
98
94
63-130
5
Bromomethane
ug/L
ND
20
20
15.3
16.7
76
84
15-152
9
Carbon disulfide
ug/L
ND
20
20
21.5
20.4
108
102
69-149
5
Carbon tetrachloride
ug/L
ND
20
20
23.1
23.2
115
116
70-143
0
Chlorobenzene
ug/L
ND
20
20
22.0
21.5
110
107
70-138
2
Chloroethane
ug/L
ND
20
20
21.3
20.5
106
103
52-163
4
Chloroform
ug/L
ND
20
20
20.9
20.8
104
104
70-139
0
Chloromethane
ug/L
ND
20
20
16.8
16.8
84
84
41-139
0
cis-1,2-Dichloroethene
ug/L
ND
20
20
21.6
21.4
108
107
70-141
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
21.3
22.0
106
110
70-137
4
Dibromochloromethane
ug/L
ND
20
20
21.0
20.8
105
104
70-134
1
Dibromomethane
ug/L
ND
20
20
23.1
23.8
116
119
70-138
3
Ethylbenzene
ug/L
ND
20
20
22.2
21.6
111
108
66-153
3
lodomethane
ug/L
ND
40
40
23.4
32.5
59
81
20-138
32 R1
m&p-Xylene
ug/L
ND
40
40
45.1
43.8
113
110
69-152
3
Methylene Chloride
ug/L
ND
20
20
17.3
17.5
86
87
42-159
1
o-Xylene
ug/L
ND
20
20
23.0
21.9
115
110
70-148
4
Styrene
ug/L
ND
20
20
22.7
21.3
114
107
70-135
6
Tetrachloroethene
ug/L
ND
20
20
22.4
21.4
112
107
59-143
4
Toluene
ug/L
ND
20
20
21.7
22.4
109
112
59-148
3
trans-1,2-Dichloroethene
ug/L
ND
20
20
21.9
22.2
109
111
70-146
1
trans- 1,3-Dichloropropene
ug/L
ND
20
20
21.6
22.7
108
113
70-135
5
trans-1,4-Dichloro-2-butene
ug/L
ND
20
20
15.6
15.1
78
75
47-135
3
Trichloroethene
ug/L
ND
20
20
23.5
23.9
117
119
70-147
2
Trichlorofluoromethane
ug/L
ND
20
20
22.0
21.3
110
107
70-148
3
Vinyl acetate
ug/L
ND
40
40
28.7
28.4
72
71
49-151
1
Vinyl chloride
ug/L
ND
20
20
19.5
19.8
97
99
70-156
2
Xylene (Total)
ug/L
ND
60
60
68.0
65.8
113
110
63-158
3
1,2-Dichloroethane-d4 (S)
%
91
92
70-130
4-Bromofluorobenzene (S)
%
104
102
70-130
Toluene-d8(S)
%
97
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 22

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
QC Batch: 447055 Analysis Method: EPA 8260B Mod.
QC Batch Method: EPA 8260E Mod. Analysis Description: 8260 MSV SIM
Associated Lab Samples: 92409667001, 92409667002, 92409667003
METHOD BLANK: 2449939
Matrix:
Water
Associated Lab Samples:
92409667001, 92409667002, 92409667003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,4-Dioxane (p-Dioxane)
ug/L
ND
2.0
12/12/18 16:14
1,2-Dichloroethane-d4 (S)
%
95
50-150
12/12/18 16:14
Toluene-d8 (S)
%
98
50-150
12/12/18 16:14
LABORATORY CONTROL SAMPLE: 2449940
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,4-Dioxane (p-Dioxane) ug/L 20 16.9 85 71-125
1,2-Dichloroethane-d4 (S) % 97 50-150
Toluene-d8(S) % 101 50-150
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2449941
2449942
MS
MSD
92409793006 Spike
Spike MS
MSD MS
MSD
% Rec
Parameter
Units Result Conc.
Conc. Result
Result % Rec
% Rec
Limits RPD Qual
1,4-Dioxane (p-Dioxane)
ug/L 10.1 20
20 26.1
25.1 80
75
50-150 4
1,2-Dichloroethane-d4 (S)
%
100
102
50-150
Toluene-d8 (S)
%
111
114
50-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 22

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HARRISBURG RD LANDFILL PERMIT
Pace Project No.: 92409667
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/17/2018 06:44 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 22

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HARRISBURG RD LANDFILL PERMIT
92409667
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92409667001
6001-HB2006
EPA 3010A
446501
EPA6010D
446518
92409667002
6001-HB2008
EPA 3010A
446501
EPA6010D
446518
92409667003
6001-HB2010
EPA 3010A
446501
EPA6010D
446518
92409667001
6001-HB2006
EPA 3010A
446878
EPA6020B
447017
92409667002
6001-HB2008
EPA 3010A
446878
EPA6020B
447017
92409667003
6001-HB2010
EPA 3010A
446878
EPA6020B
447017
92409667001
6001-HB2006
EPA 8260B
447864
92409667002
6001-HB2008
EPA 8260B
447864
92409667003
6001-HB2010
EPA 8260B
447864
92409667001
6001-HB2006
EPA 8260B Mod.
447055
92409667002
6001-HB2008
EPA 8260B Mod.
447055
92409667003
6001-HB2010
EPA 8260B Mod.
447055
Date: 12/17/2018 06:44 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 22

Document Name:
Document Revised: February 7, 2018
J aceArral lca1�
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples: _
Asheville ❑ Eden❑ Greenwood ❑ Huntersv�lle Raleigh❑ Mechanicsville❑
Sample Condition Client Name: WV# : 924Q9667
Upon Receipt
,r . 1 /'/ Project #
Courier: Der x ❑UPS ❑LISPS ❑Client
❑ Commercial '� ace ❑Other: 9 09667
Custody Seal Present? ❑Yes o- Seals Intact? ❑Yes �o
C�
Packing Material: ❑Bubble Wrap ❑Bubble Bagsornne- ❑ Other
Thermometer: Type of Ice: let ❑Blue
-;OIR Gun ID: 92TO46
Cooler Temp (°C): 3 '6 Correction Factor: Add/Subtract (°C) 0.()
Cooler Temp Corrected (°Cj:
USDA Regulated Soil N/A, water sample)
Did sample riginate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
nYes IQNn
Date/Initials Person Examining Contents lG I
Biological TisFA
et1?
❑Yes ❑No
[:]None
Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples originate from a foreign source {intkaticnally,
includinE Hawaii and Puerto Ricol? nYes o
Comments/Discrepancy:
Chain of Custody Present?
'NYes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
s
El No
❑NIA
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
Na
El NIA
3.
Rush Turn Around Time Requested?
❑Yes
No
❑N/A
4.
Sufficient Volume?
hes
Cho
[]NIA
5.
Correct Containers Used?
byes
❑No
❑N/A
6.
-Pace Containers Used?
es
[]No
❑NIA
Containers Intact?
s
[:]No
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
N/A
8.
Sample Labels Match COC?
Yes
❑No
[]N/A
9.
-includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)?
Des
0Q
❑N/A
10.
Trip Blank Present?
[�es
❑N/A
11.
Trip Blank Custody Seals Present?
[]Yes
No
❑N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Field Data Required? ❑Yes ❑No
Project Manager SCURF Review: Date: �T^jam
Project Manager SRF Review: i - Date: I .Z
Page 20 of 22

Document Name:
Document Revised: February 7, 2018
;ZeAnal1Cc31
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project: WO# : 92409667
ISM: MWS Due Date: 12/19/18
CLIENT: 92—MECK CO
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot 9
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 21 of 22

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