MO-9410_40855_CA_IAR_20181105_Initial Abatement Action Report

4 ESP
INITIAL ABATEMENT
ACTION REPORT
10200 ARTHUR DAVIS ROAD SITE
MECKLENBURG COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO. PENDING
FACILITY ID NO. N/A
ESP PROJECT NO. E6-FN29.600
Prepared For:
North Carolina Department of Environmental Quality
Underground Storage Tank Section
Mooresville Regional Office
919 North Main Street
Mooresville, North Carolina 28115
On Behalf Of:
Mattamy Carolina Corporation
2127 Ayrsley Town Boulevard, Suite 201
Charlotte, North Carolina 28273
Prepared By:
ESP Associates, Inc.
P. 0. Box 7030
Charlotte, North Carolina 28241
November 5, 2018

4 ESP
November 5, 2018
Mr. Daniel Bowser, PG
North Carolina Department of Environmental Quality
Mooresville Regional Office - UST Section
919 North Main Street
Mooresville, NC 28115
Reference: INITIAL ABATEMENT ACTION REPORT
10200 Arthur Davis Road Site
Mecklenburg County, North Carolina
Non-Regulated/Non-Commercial UST
NCDEQ Incident No. Pending
ESP Project No. E6-FN29.600
Dear Mr. Bowser:
On behalf of Mattamy Carolina Corporation, ESP Associates, Inc. is pleased to provide the
attached Initial Abatement Action Report documenting the removal of a non-regulated/non-
commercial UST, excavation of petroleum -impacted soil, and subsequent confirmatory soil and
groundwater sampling associated with a farm 550-gallon diesel UST located at 10200 Arthur
Davis Road in an unincorporated portion of Mecklenburg County, North Carolina.
ESP recommends no further action in regards to the release. Thank you for your attention in this
matter. If you should have any questions, please do not hesitate to contact us at [phone].
Sincerely,
ESP Associates, Inc.
Franklin D. Newsom
Staff Scientist
cc: Mr. Bob Wiggins - Mattamy Carolina Corporation
Attachment - Initial Abatement Action Report
� ��p
Christopher J. Ward, PG, RSM
Department Manager
NC License No. 1600
ESP Associates, Inc.
P.O. Box 7030 Charlotte, NC 28241
1.800.960.7317 • NC: 704.583.4949, fax [phone] • SC: 803.802.2440, fax [phone]
www.espassociates.com

ESP Associates, Inc.
P.O. Box 7030 - Charlotte, NC 28241
800.960.7317 - NC:704.583.4949, fax 704.S83.49S0 - SC:803.802.2440, fax [phone]S1S
www.espassociates.com
..............................................
COPY TO:
(A) Addressee
(B) ESP Main Project File
(C) PM's Project File
LETTER OF TRANSMITTAL
ESP Project Name: 10200 Arthur Davis Road Site
ESP Project No.: E6-FN29.600
TO: NCDEQ
MRO - UST Section
919 North Main Street
Mooresville, NC 28115
Attention:
Date:
Mr. Daniel Bowser, PG
November 5, 2018
We are Sending:
Enclosed Change Order
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Report =Specifications
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Description
Initial Abatement Action Report - 10200 Arthur Davis Road Site
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OOther

1. Site Identification
C3
Date of Report:
November 5, 2018
0
Facility ID:
N/A
C3
UST Incident Number:
Pending
C3
Site Name:
10200 Arthur David Road Site
C3
Site Street Address:
10200 Arthur Davis Road
0
City/County/Zip Code:
Huntersville, Mecklenburg, 28078
C]
Description of Geographical Data Point: Approximate center of tank pit
•
Location Method:
GPS Unit
•
Latitude:
35.361464
•
Longitude:
-80.818522
C3
UST Owner:
Mike Davis (704.607.0570)
C3
UST Operator:
Mike Davis
C3
Property Owner:
Mike Davis
13001 Keith Hill Road
Huntersville, NC 28078
C3
Property Occupant:
Rose K. Davis
C3
Consultant/Contractor:
ESP Associates, Inc. - Chris Ward, PG (704.583.4949)
PO Box 7030
Charlotte, NC 28241
0
Analytical Laboratory:
Pace Analytical Services, Inc. (704.875.9092)
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
NC Certification No. 37706
• Date Discovered: October 18, 2018
• Estimated Quantity of Release: Unknown
• Cause of release: Leak from a diesel UST
• Source of Release: unregulated/noncommercial farm UST
• Size and contents of UST
system from which release occurred: Steel 550-gallon UST
4. Certification
1, Christopher J.
information coal
LM
,ist for ESP Associates, Inc., do certify that the
and accurate to the best of my knowledge.
W"u
both geology and engineering in North Carolina.
are: Geology: C-347 / Engineering: C-0587

Initial Abatement Action Report ESP Project E6-FN29.600
10200 Arthur Davis Rad Site November S, 2018
1.0 INTRODUCTION
As part of due diligence associated with the purchase of property for its planned residential
development, Mattamy Carolina Corporation contracted the removal of a steel 550-gallon farm
diesel underground storage tank (UST) located at 10200 Arthur David Road (Tax Parcel ID No.
02718103) in an unincorporated portion of Mecklenburg County, North Carolina (see Figures 1
and 2). See Tables B-1 and B-2 for specifics regarding the subject UST. A completed UST-2
form is included in Appendix A.
The Mecklenburg County Soil Survey indicates that soils at the site are classified as Mecklenburg
fine sandy loam, 2 to 8 percent slopes, well drained (MeB). Based on a review of the Geologic
Map of North Carolina, the subject site is located within the Charlotte Belt, comprised of granitic
rock formation, comprised of foliated to massive granite rock which contains hornblende. The
soils encountered in this area are the residual product of chemical weathering of rock presently
underlying the site. The soil weathering is more advanced near the surface grading with depth to
less weathered rock and finally bedrock.
Excavation of the 550-gallon diesel UST was performed on October 18, 2018, by S.M. Smith and
Sons, Inc. of Midland, North Carolina. During removal of the subject UST, obvious soil impact
was encountered as determined by a noticeable petroleum odor and elevated photoionization detector
(PID) readings. A 24-hour release notification was submitted to NCDEQ on October 19, 2018 by
CERT of Charlotte, North Carolina (see Appendix A).
The following sections detail initial abatement action performed along with subsequent confirmation
sampling.
1

Initial Abatement Action Report ESP Project E6-FN29.600
10200 Arthur Davis Rad Site November S, 2018
2.0 INITIAL ABATEMENT ACTIVITIES
2.1 October 18, 2018 Activities
On October 18, 2018, S.M. Smith and Sons, Inc. excavated soil above and around the subject 550-
gallon diesel UST as part of the tank's removal. The top of the tank was encountered at a depth of
approximately 2 feet below ground surface (ft bgs). Upon encountering apparent petroleum -
impacted soil, CERT screened soil from the excavation with a PID and encountered elevated volatile
organic compounds (VOCs) readings. A PID reading of 366 parts per million (ppm) was recorded
in soil immediately beneath the tank while PID readings of 77 ppm and 25.6 ppm were recorded at
depths of approximately 12 and 16 ft bgs within the center of the tank pit.
Once removed, the tank's dimensions were measured to be 9.5 ft x 3.2 ft corresponding to a volume
of approximately 550-gallons. Significant rust pitting and several holes associated with the UST
were observed (see photographs in Appendix Q. The UST was then loaded onto a truck and
transported off -site by CERT to a North Carolina -certified waste recycling facility (see manifest
in Appendix B).
Mattamy requested that ESP Associates, Inc. (ESP) document subsequent abatement activities
during which ESP's field scientist screened soils with a PID on October 18, 2018, and confirmed
elevated VOC readings. A release detection soil sample (designated Tank) was collected by CERT
at an approximate depth of 6 ft bgs, a depth that corresponded to the bottom of the removed UST.
Additional soil was excavated vertically from the tank pit and placed to the side of the excavation.
A second soil sample (designated Post Excavation 12') was collected by CERT from a depth of
approximately 12 ft bgs within the approximate center of the tank pit. The two soil samples (Tank
and Post Excavation 12') were delivered by CERT to Pace Analytical Services, Inc. (Pace) in
Huntersville, North Carolina by CERT to for analysis. Release detection soil sample Tank was
analyzed for total petroleum hydrocarbons -diesel range organics (TPH-DRO) and TPH-gasoline
range organics (GRO) by EPA Method 8015C. Soil sample Post Excavation 12' was analyzed for
2

Initial Abatement Action Report ESP Project E6-FN29.600
10200 Arthur Davis Rad Site November 5, 2018
VOCs by EPA Method 8260, semi -volatile organic compounds (SVOCs) by EPA Method 8270,
and for VPH/EPH by the MADEP Method.
A total of 27.51 tons of soil was placed on trucks and shipped off -site on October 18, 2018 by S.M.
Smith and Sons, under non -hazardous waste manifests, to the Environmental Soils Inc. facility in
Lattimore, North Carolina for treatment/disposal. See Appendix B for copies of the non -hazardous
waste manifests.
At the end of the day on October 18, 2018, dimensions of the tank pit excavation were measured to
be approximately 12 ft x 5 ft x 16 ft deep. It should be noted that groundwater began to seep into
the excavation as groundwater within the adjacent monitoring well (MW-UST) was measured to be
at a depth of approximately 13 ft bgs. See Figures 2 and 3 for monitoring well location.
2.2 October 22 and 23, 2018 Activities
Additional excavation of petroleum -impacted soil was performed on October 22 and 23, 2018, by
S.M. Smith and Sons, Inc. as documented by ESP field personnel. The additional soil was excavated
based on elevated PID readings; however, the vertical extent of the excavation was terminated at an
approximate depth of 13 ft bgs due to encountering groundwater.
Excavation of soil in the lateral directions was continued until non -detect or low PID readings were
encountered. The excavated soil was found to be comprised predominantly of reddish -brown
clayey silt to silty clay from the ground surface to the maximum depth of the final excavation at
approximately 13 ft bgs. Excavation at the northeast corner of the excavation was terminated due
to the potential for undermining an adjacent structure; however, PID readings in that area were
non -detect to low. Neither bedrock nor free product was encountered within the excavation;
however, groundwater was encountered at a depth of approximately 13 ft bgs. The final
dimensions of the tank pit excavation on October 23, 2018, were approximately 36 ft x 19 ft by 13
ft in depth (see Figure 3). Photographs of the UST and excavation are included in Appendix C.
3

Initial Abatement Action Report ESP Project E6-FN29.600
10200 Arthur Davis Rad Site November S, 2018
On October 22 and 23, 2018, a total of 165.69 tons of soil was excavated from the tank pit and placed
on trucks and shipped off -site by S.M. Smith and Sons, under non -hazardous waste manifests, to the
Environmental Soils Inc. facility for treatment/disposal. Therefore, a total of 193.20 tons of soil was
shipped off site on October 18, 22 and 23, 2018. See Appendix B for copies of the non -hazardous
waste manifests.
Following collection of the below confirmatory soil samples, the tank pit was backfilled with clean
fill on October 23, 2018.
3.0 CONFIRMATORY SOIL SAMPLING
On October 23, 2018, ESP collected four confirmatory soil samples, designated as West Wall,
North Wall, South Wall and East Wall, from an approximate depth of 6.5 ft bgs from the four side -
walls of the tank pit excavation as depicted on Figure 3. A bottom of excavation confirmatory soil
sample was not collected due to encountering shallow groundwater. Confirmatory soil sample
locations were selected based on field conditions including visual observations and PID readings
along with the placement and depth of the former UST.
The four confirmatory soil samples were placed in laboratory -provided containers, labeled, stored
on ice in a cooler, and hand -delivered under standard chain -of -custody procedures to Pace for
laboratory analysis. The samples were analyzed for VOCs by EPA Method 8260, SVOCs by EPA
Method 8270, TPH-DRO and TPH-GRO, and for EPH by the MADEP Method.
.19

Initial Abatement Action Report ESP Project E6-FN29.600
10200 Arthur Davis Rad Site November S, 2018
4.0 GROUNDWATER SAMPLING
Due to encountering shallow groundwater within the excavation, on October 22, 2018, ESP
collected a groundwater sample for laboratory analysis from adjacent monitoring well MW-UST
(see Figure 3). The monitoring well was installed adjacent to the former 550-gallon UST as part
of previous due diligence by others. No well tag was found inside the 2-inch diameter PVC
monitoring well's flush -mounted protective casing so the well's installation date and other
construction details are unknown.
The monitoring well was gauged with a decontaminated electronic water level indicator to have a
static water level of approximately 13.2 ft bgs while the well's total depth was recorded to be
approximately 23.1 ft bgs. Following gauging, the monitoring well was purged of three well
volumes of water using a dedicated disposable Teflon bailer. A representative groundwater
sample, designated as MW-UST, was then collected from the monitoring well using the Teflon
bailer with the water transferred into laboratory provided containers, labeled, placed on ice in a
cooler and hand -delivered under standard chain -of -custody procedures to Pace for laboratory
analysis.
Groundwater sample MW-UST was analyzed for VOCs by EPA Method 602, SVOCs plus 10
largest non -target peaks by EPA Method 625, and by MADEP for VPH and EPH.
5.0 ANALYTICAL RESULTS
5.1 Release Detection Soil Samples
As summarized on Table B-3, results of the laboratory analysis of the release detection soil sample
Tank revealed that TPH-DRO was reported at a concentration of 2,530 milligrams per kilogram
(mg/kg) while TPH-GRO was detected at a concentration of 85.8 mg/k; both above their NC action
levels of 100 and 50 mg/kg, respectively. Soil sample Post Excavation 12' collected from the
center of the excavation at a depth of approximately 12 ft bgs, revealed that all analyzed
5

Initial Abatement Action Report ESP Project E6-FN29.600
10200 Arthur Davis Rad Site November S, 2018
constituents were below reporting limits (BRLs). The Pace analytical data report is included as
Appendix D.
5.2 Confirmatory Soil Samples
As summarized on Table B-3, results of the laboratory analysis of the four confirmatory soil
samples (West Wall, North Wall, South Wall and East Wall) revealed that all analytes were below
their soil -to -groundwater maximum soil contaminant concentrations (MSCCs) with the exception
of methylene chloride. Methylene chloride was detected slightly above its soil -to -groundwater
MSCC in samples West Wall and South Wall; however, both detections were below its residential
MSCC. Methylene chloride was detected at relatively low concentrations in all four of the soil
samples and is believed to be a laboratory contaminant and not indicative of contamination. The
Pace analytical data report is included as Appendix D.
5.3 Groundwater Sample
As summarized on Table B-4, results of the laboratory analysis of groundwater sample MW-UST
revealed that all analytes were BRLs. The Pace analytical data report is included as Appendix D.
6.0 AREA RECEPTORS
On October 23, 2018, ESP performed a visual site reconnaissance to identify potential water
supply wells within an approximate 500-ft radius of the subject release site. An on -site private
water supply well (10200 Arthur Davis Road) was identified to be located approximately 250 ft
northeast and an off -site private water supply well (10330 Arthur Davis Road) located
approximately 400 ft northwest of the release site (see Figure 2).
The closest surface water bodies to the release site is an on -site pond located approximately 1,100
ft to the southeast and an off -site intermittent creek located approximately 1,400 ft west of the
2

Initial Abatement Action Report
10200 Arthur Davis Rad Site
ESP Project E6-FN29.600
November 5, 2018
release site (see Figure 1). Based on site topography, groundwater is expected to flow toward the
south-southeast.
7.0 CONCLUSIONS AND RECOMMENDATIONS
The following conclusions and recommendations have been formulated based on completion of
initial abatement activities and our review of results from the laboratory analysis of collected soil
and groundwater samples.
o On October 18, 2018, during excavation and removal of a non-regulated/non-commercial
550-gallon farm diesel UST, obvious soil impact was encountered as determined by a
noticeable petroleum odor and elevated PID readings;
o A 24-Hour Release and UST Leak Reporting Form was forwarded to NCDEQ on October
19, 2018;
o On October 18, 2018, a release detection soil sample (designated as Tank) was collected
immediately beneath the removed tank at an approximate depth of 6 ft bgs. A second soil
sample (Post Excavation 12') was collected from a depth of approximately 12 ft bgs within
the approximate center of the tank pit;
o On October 18, 2018, a total of 27.51 tons of soil was placed on trucks and shipped off -site
for permitted treatment/disposal from an excavation that measured approximately 12 ft x 5
ft x 16 ft deep at the end of the day. Neither bedrock or free product was encountered within
the excavation; however, groundwater was encountered at a depth of approximately 13 ft
bgs;
o On October 22, 2018, due to encountering shallow groundwater within the excavation, a
groundwater sample was collected for laboratory analysis from adjacent monitoring well
MW-UST;
o On October 22 and 23, 2018, a total of 165.69 tons of soil was excavated from the tank pit
and placed on trucks and shipped off -site for permitted treatment/disposal. The final
dimensions of the tank pit excavation on October 23, 2018, were approximately 36 ft x 19 ft
by 13 ft in depth with a total of 193.20 tons of soil shipped off site on October 18, 22 and 23,
2018;
7

Initial Abatement Action Report
10200 Arthur Davis Rad Site
ESP Project E6-FN29.600
November S, 2018
o On October 23, 2018, ESP collected four confirmatory soil samples, designated as West
Wall, North Wall, South Wall and East Wall, from an approximate depth of 6.5 ft bgs from
the four side -walls of the tank pit excavation;
o An on -site private water supply well (10200 Arthur Davis Road) was identified to be
located approximately 250 ft northeast and an off -site private water supply well (10330
Arthur Davis Road) located approximately 400 ft northwest of the release site;
o The closest surface water bodies to the release site is an on -site pond located approximately
1,100 ft to the southeast and an off -site intermittent creek located approximately 1,400 ft
west of the release site. Based on site topography, groundwater is expected to flow toward
the south-southeast;
o Laboratory analysis of release detection soil sample Tank revealed TPH-DRO at 2,530
mg/kg and TPH-GRO at 85.8 mg/kg; both above their NC action levels of 100 and 50
mg/kg, respectively;
o Laboratory analysis of soil sample Post Excavation 12' collected from the center of the
excavation at a depth of approximately 12 ft bgs, revealed that all analytes were BRLs;
o Laboratory analysis of the four confirmatory soil samples (West Wall, North Wall, South
Wall and East Wall), revealed that all analytes were below their NC soil -to -groundwater
MSCCs with the exception of methylene chloride. Methylene chloride was detected
slightly above its soil -to -groundwater MSCC in samples West Wall and South Wall;
however, both detections were below its residential MSCC. Methylene chloride was
detected at relatively low concentrations in all four of the soil samples and is believed to
be a laboratory contaminant and not indicative of contamination; and
o Laboratory analysis of groundwater sample MW-UST revealed that all analytes were
BRLs.
Based on above initial abatement action and results of the laboratory analysis of confirmatory soil
and groundwater samples, ESP concludes that impacted soil above standards has successfully been
abated while groundwater has been shown not to have been impacted. Therefore, ESP
recommends that no further action be performed on the subject diesel release and the release
incident issued a notice of no further action with no land use restrictions.

Initial Abatement Action Report
10200 Arthur Davis Rad Site
Attachments
ESP Project E6-FN29.600
November S, 2018
Table B-1 - Site History: UST System and Other Release Information
Table B-2 - Site History: UST Owner/Operator and Other Responsible Party
Table B-3 - Summary of Soil Sampling Results
Table B-4 - Summary of Groundwater Sampling Results
Figure 1 - USGS Topographic Site Location Map
Figure 2 - Release Location Map
Figure 3 - Final Excavation Layout and Sample Locations Map
Appendix A - 24-Hour Release and UST Leaking Reporting Form and UST-2 Form
Appendix B - Manifests
Appendix C - Site Photographs
Appendix D - Pace Analytical Data Reports
0

ATTACHMENTS

TABLES

Table B-1: Site History — UST/AST System and Other Release -Information
Revision Date: 11/1/18 Incident Number: Pending 10200 Arthur Davis Road Site Facility lD#: N/A
UST ID
Number
Current/Last
Contents*
Previous
Contents*
Capacity
(in gallons)
Construction
Details**
Tank
Dimensions
Description
of Associated
Pipingand
Pumps
Date Tank
Installed
Status of
UST***
Was release
associated
with the UST
System?
1
Diesel
Unknown
550
S-walled
steel
9.5 ft. x
3.2 ft.
none
unknown
Removed
10/ 18/ 18
Yes
Add additional records as necessary
AST ID
Number
Current/Last
Contents*
Previous
Contents*
Capacity(in
gallons)
Construction
Details**
Tank
Dimensions
Description
of Associated
Pipingand
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
Incident
Material
Date of
Description of Release
Number
Released
Release
Pending
Diesel
10/18/18
Impact encountered during excavation and removal of the 550-gallon non-regulated/non-
commercial farm UST during a real estate transaction.
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
* * Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
* * * Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Table B-2: Site History - UST/AST Owner/Operator and Other Responsible
Party Information
Revision Date: 11/1/18 Incident Number: Pending - 10200 Arthur Davis Road Site
UST ID Number
1
Facility ID Number
N/A
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/yy)
Mike Davis
Unknown to 10/18/18
Street Address
13001 Keith Hill Road
City
State
Zip
Telephone Number
Huntersville
NC
28078
704-607-0570
Name of Operator
Dates of Operation
mm/dd/ to mm/dd/
Mike Davis
Unknown to 10/18/18
Street Address
13001 Keith Hill Road
City
State
Zip
Telephone Number
Huntersville
NC
28078
704-607-0570
Incident Number
Pending
Name of Other Responsible Party
Dates of Release(s)
mm/dd/ to mm/dd/
Keith Davis
10/18/18
Street Address
13001 Keith Hill Road
City
State
Zip
Tele hone Number
Huntersville
NC
28078
704-607-0570
Add additional records for all owners, operators and responsible parties as necessary

Table B-3: Summary of Soil Sampling Results
Revision Date: 11/1/18 Incident Number: Pending - 10200 Arthur Davis Road Site Facility ID#: N/A
Analytical Method (e.g., VOC by EPA 8260) 4
MADEP
MADEP
EPH
VPH
8270
8260
8260
8260
8015
8015
Contaminant of Concern 4
44 b
tea'
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
a
a
a
°
��
2
(m/dd/yy)
(eg.
(ft BGS)
(Closure,
¢
d
¢
d
' U
Tank pit
20Day,
F�
F�
1)
LSA, etc.
Tank
10/18/18
6
Release
NA
NA
NA
NA
NA
NA
2,530
85.8
USTW
Post
Tank Pit
Excavation
10/18/18
12
Closure
BRL
BRL
BRL
BRL
BRL
BRL
NA
NA
Center
12'
Tank Pit
West Wall
10/23/18
6.5
Closure
BRL
NA
BRL
0.0295J
0.0336
BRL
BRL
BRL
W. Side
North Wall
10/23/18
Tank Pit
6.5
Closure
BRL
NA
BRL
BRL
0.0067J
0.0028J
BRL
BRL
N. Side
Tank Pit
South Wall
10/23/18
6.5
Closure
BRL
NA
BRL
0.0361J
0.0252
0.0304
BRL
BRL
S. Side
Tank Pit
East Wall
10/23/18
6.5
Closure
BRL
NA
BRL
0.0295J
0.0075J
BRL
BRL
BRL
E. Side
Soil to groundwater MSCC (mg/kg)
N/A
N/A
N/A
24
0.02
4.3
NL
NL
Residential MSCC (mg/kg)
N/A
N/A
N/A
14,000
85
1,200
NL
NL
Industrial/Commercial MSCC (mg/kg)
N/A
N/A
N/A
360,000
763
32,000
NL
NL
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface; J = Analyte was positively identified but the value is estimated below the reporting limit.
BRL = Below Reporting Limit; NA = Not Analyzed; N/A = Not Applicable; NL = Not Listed
mg/kg = milligrams per kilogram; # = Health Based Level >100%; ## = Considered immobile

Table B-4: Summary of Groundwater Sampling Results
Revision Date: 11/1/18 Incident Number: Pending 10200 Arthur Davis Road Site Facilitv ID#: N/A
Analytical Method (e.g., VOC by EPA 601)
MADEP
MADEP
4
625
602
VPH
EPH
Contaminant of Concern 4
d
d
d C
d C3
Well or
Date
Sample
Incident
SW ID
Collected
ID
Phase
(m/dd/yy)
(Closure,
20Day,
LSA, etc.
MW-1
10/22/18
UST
Closure
BRL
BRL
BRL
BRL
2L Standard (ug/1)
N/A
N/A
N/A
N/A
GCL (ug/1)
N/A
N/A
N/A
N/A
NC 213 Standard or EPA National Criteria
(ug/1)
N/A
N/A
N/A
N/A
BRL — Below Reporting Limit
Results reported in ug/1 or micrograms per liter
GCL = Gross Contamination Level
N/A = Not Applicable
NE = Not Established

FIGURES

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413
Legend
*Source: Parcel and topographic information provided
by NC Department of Public Safety (NCDPS).
PROJECT NO.
FN29.600
SHEETTITLE
FIGURE 1
ESP Associates, Inc.
Approximate Former UST Location
N
SCALE
As Shown
USGS TOPOGRAPHIC SITE LOCATION MAP
P.O. Box 7030
Charlotte, NC 28241
0 330 660 W E
Feet s
DRAWN BY
FN
PROJECT
MERIDALE BOLT ON SITE
phone [phone]
CHECKED BY
Cw
DATE 1013012018
MECKLENBURG COUNTY, NORTH CAROLINA
www.espassociates.com

Legend *Source: Parcel and topogrophic infornnotion provided
by NC Department oJPubiic Safety(NCDPS/.
Approximate Storage Tank Location N
PROJECT NO. FN29.600
SHEETTITLE FIGURE 2
RELEASE LOCATION MAP
ESP Associates, Inc.
P.O. Box 7030
SCALE As shown
Approximate Monitoring Well Sample Location 0 110 220 w E
ESP Charlotte, NC 28241
Approximate Water Supply Well Location Feet s
DRAWN BY FN
PROJECT MERIDALE BOLT ON SITE
phone [phone]
1000 Ft Radius DATE 1013012018
CHARLOTTE, NORTH CAROLINA
www.espassociates.com
CHECKED BY Cw

Legend
*Source: Parcel and topographic information provided
by NC Department of Public Safety (NCDPS).
PROJECT NO.
FN29.600
SHEETTITLE FIGURE 3
ESP Associates, Inc.
Approximate Storage Tank Location
N
SCALE
As shown
FINAL EXCAVATION LAYOUT AND SAMPLE LOCATIONS MAP
P.O. sox 7030
Charlotte, NC 28241
ESP
0 10 20 N+-E
Approximate Monitoring Well Sample Location
Feet S
DRAWN BY
FN
PROJECT MERIDALE BOLT ON SITE
phone[phone]
Q Approximate Soil Sample Location
DATE 1013012018
MECKLENBURG COUNTY, NORTH CAROLINA
www.espassociates.com
CHECKED BY cw

APPENDIX A
24-HOUR RELEASE AND UST LEAKING REPORTING FORM

, s' ':S1'
Z Hour Release and UST � " I � t�,�1 l�n•
z.Ar
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
In NC suspected release
(DWM USE ONLY)
Suspected Contamination? (Y/N) _A ----
Facility ID Number
Incident # Risk (H,I,L,U) -
Confirmed GW Contamination? (Y/N) _ 1J _
Date Leak Discover T
Received On _ Received By _-----
Confirmed Soil Contamination ?(Y/N)
Comm/Non-Commercial?
Reported by (eirrJe one): Phone, Fax or Report
Samples Taken?(Y/N) -%___
Reg/Non-regulated?
Region
Free Product? (YIN) �__ If Yes, Slate Greatest
Thickness �-
INCIDENT DESCRIPTION
Incident Name:
Address: \ZZ�Az�j r. ���� ��
County. M
� ■ � _CC,
�y,�
City/Town: ��4 \ `l Zip Code:'a0� �7
Regional Office (circle one): Asheville, Mooresville, ayetteville,
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (dedmel dagr.x):' 21',(), t 3'' j\ Longitude (AeclmW dopnnc)'����11 Y'0(2" ( L" \^j
Obtained by:
❑ GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)
❑ Topographic map
❑ GIS Address matching
Other GIAt
❑Unknown
Describe location:
0%V V —Q 1 --" C ,� ,�
, s--'7'r arL w ` �` (�5 �� .-t
l�
OC 90�` 1` .�% �?rY�
��(\v'
\)`N �S `� 1 '�vK* �q %1 v \
r
HOW RELEASE WAS DISCOVERED (Release code)
(Check one)
❑ Release Detecuon Equipment or Methods ❑ Visual/Odor ❑ Groundwater Contamination
During UST Closure/Removal ❑ Water in Tank ❑ Surface Water Contamination
Property Transfer ❑ Water Supply Well Contamination ❑ Other (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release Product Type Released
(Check one to indicate primary (Check one to indicate primary (Chock one) (Check one to indicate primary product type
source) cause) released)
Tank ❑Spill I*.troleum ❑ Gasoline/ Diesel/ ❑ Diosal/Veg. Oil
Kerosene Bland
Piping ❑ Overfill ❑ Non-Polroloum Heating Oil ❑ Vegntablo Oil 100%
❑ Dispenser orosion ❑ Both [) Other Petroleum ❑ E 10 - E20
❑ Submersible Turbine Pump ❑ Physical or Mechanical Products
❑ E21 E84
-
Damage Location ❑ Metals
❑ Delivery Problem
(Check one) [.] Other Inorganics ❑ E85 =-E99
❑
Install Problem
Organics lity 9 ❑Ethanol 10096
❑ Other ❑ ❑ ❑ Other Facility
❑ Unknown ❑ E01 - E09
❑ Unknown esitlence
Definitions presented on reverse I Definitions presented on reverse I Other
Ownership
1. Municipal 2. Military 3. Unknown �­t-5. Federal 6. County 7. State
Operation Type
1. Public Service 2 �gn-lturl. Residential 4. EducatiorVRelig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/OB) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1.
Yes 2. No Unkno n
Number of Water Supply Wells Affected ______
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Point of Contact
Address
City
State -'-,,",,"Zip
Code
Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company
Address
City
St.
Zip Code
Telephone Number
LANDOWNER AT LO TION OF UST INCIDENT
Landowner
Address
City J 1
state
KY —
Zip
TelephonetJ�umber
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident
Company C f
Telephone Number
Title �l -V\
Address C) VvV4 <n ]
1
Date
1 2 ZZ
vr•vnn v i tvcrvv) / Ova, Pago 2 of 2
�
Definitions of Sources
Tank: means the tank that stores the product and is pan of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment ( Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dislenwr to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery w the uutk. (Typical causes associated with this sour a ore spills and overfills I
Other: serves as the option to use when the release source is known but does not fit into one of the prvceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been doennined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nuzzle is rvmoved from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

E
COEOR •T
ERROLINR ENVIR09MENTRLRESPONSETERM
Emergency Response: 877-505-6799
10200 Arthur Davis Rd., Huntersville, NC
PO Box 681016
Charlotte, NC 28216
Phone: [phone]
Fax: [phone]
www.cert-usa.com
�$5 Oulu"
U'
•. o
S
Q
0 2018' ahon! Ini. i i720ft

UST-2 Site Investigation Report for Permanent Closure or Change -in -Service of UST
Return completed form to:
ware use oN Y:
The DWM Regional Office located in the area where the facility is located. Send a copy to the Central Office in Raleigh so that
to. s
the status of the tank may be changed to "PERMANENTLY CLOSED" and your tank fee account can be closed out.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
Date Rtceivea
INSTRUCTIONS READ THIS FIRST
For more than five UST systems you may attach additional forms as needed.
Permanent closure — For permanent closure, complete all sections of this form.
Change -in-service — For change -in-service where UST systems will be converted from containing a regulated substance to storing a non -regulated
substance, complete sections I, It, III, IV, and Vlll
Effective February 1, 1995, all UST closure/change-in-service reports must be submitted in the format provided in the UST-12 form. UST closure and
change -in -services must be completed in accordance with the latest version of the Guidelines for Tank Closure. A copy of the UST-12 form and the
Guidelines for Tank Closure can be obtained at www.wastenotnc.org.
You must make sure that USTs removed from your property are disposed of property. When choosing a closure contractor, ask where the tanks) will be
taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed by a qualified company. Tanks
disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment. If your tanks are disposed of improperly, you
could be held responsible for the cleanup of any environmental damage that occurs.
NOTE: If a release from the tank(s) has occurred, the site assessment portion of the tank closure must be conducted under the supervision of a P.E. or
L.G., with all closure site assessment reports bearing the signature and seal of the P.E. or L.G.
1. OWNERSHIP OF TANKS
II. LOCATION OF TANKS
Owner Name (Corporation, Individual, Public Agency, or Other Entity)
Facility Name or Company
Mike Davis
Street Address
Facility ID # (If known)
13001 Keith Hill Road
N/A
City County
Street Address
Huntersviile Mecklenburg
10200 Arthur Davis Road
State Zip Code
City County Zip Code
NC 28078
Huntersvilie Mecklenburg 28078
Phone Number
Phone Number
704-607-0570
704-607-0570
III. CONTACT
PERSONNEL
Contact for Facility:
Job Title:
Phone. No:
Mike Davis
Pro2erty Owner
704-607-0570
Closure Contractor Name:
Closure Contractor Company:
Address:
Phone. No:
Stacy Faile
SM Smith and Sons Inc.
261 NG Hwy 24 Midland, NC 28107
704-545-4177
Primary Consultant Name:
Primary Consultant Company:
Address:
Phone. No:
Chris Ward, PG
ESP Associates, Inc.
PO Box 7030 Charlotte, NC 28241
803-835-0915
IV. LIST INFORMATION
FOR REGISTERED
UST SYSTEMS
V. EXCAVATION CONDITION
Tank
Size in
Tank
Last
Last Use
Permanent
Change -in-
Water in
Free
Notableoaorommiele
ID No.
Gallons
Dimensions
Contents
Date
Close Date
Servi
ex`avan°"
Proanor
son contaminator
Yes
No
Yes
No
Yes
No
ece
Dat
❑
❑
❑
El
1:1
❑
1 ❑
❑
❑
❑
❑
VI. UST INFORMATION
FOR UNREGISTERED UST SYSTEMS
VII. EXCAVATION
CONDITION
Tank
Size in
Tank
Last
Last Use
Permanent
Tank Owner
Water in
Free
Notable odor or,mlele
ID No.
Gallons
Dimensions
Contents
Date
Close Date
Name"
inoavaaon
rodua
soil contamination
Yes
No
Yes
No
Yes
I No
1
550
9.5 x 3.2 ft
Dieisel, Diets
Not
10/18/18
Mike Davis
®
❑
❑
®
®
❑
known
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
❑
El
❑
❑
❑
❑
❑
❑
❑
If the tank owner address is different from the one listed in Section I., then enter the street address, city, state, zip code and telephone no. below:
Vill. CERTIFICATION
I certify under penalty of law that I have personally examined and am familiar with the information submitted jpAlevirstridall attached documents and that
based on my inquiry of those individuals immediately responsible for obtaining the infnnnation vr the submi ed information is true accurate and
complete.
Print name and official title of owner or owner's authorized representative
Ion ur
Date Signed
Chris ward. PG -ESP Associates, Inc. - Agent for Mattamy Carolina Cogmratio
10/31/2018
UST-2 Rev 11/2006

APPENDIX B
MANIFESTS

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 52831
Date Load Number
ENVIRONMENT 4L CONSULT 4NT
Contact:
GENERATOR:
(numbered sequentially as trucks are dispatched)
Phone: Fax:
County:.
Contact: Phone:
WASTE ORIGINATIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT4MINATION.• (ex. UST or other source)
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certfcate of Waste
Constituents. I cert fv that I am familiar with the source of contamination of the soil and further certf� the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators
TRANSPORTER:
Phone:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: - f Date: -
TRUCK #: TAG #: "µ " , r VOLUME: T-• ,
TRUCK DRIVER SIGNATURE: _ DATE:
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: D
Signature
Company Name
Date:_
Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest # 5 2 8 2 6
Date _..... _ Load Number
(numbered sequentially as trucks are dispatched)
ENVIRONMENT4L CONSULTYINT
Phone: Fax:
GENERATOR:
Address
Contact:
WASTE ORIGINATIONPOINT.• Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONEWMINATION.• (ex. UST or other source)
Counter:
Phone:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (metbods
8240 and 8270) verioing that the waste in question does not contain organic constituents other than those wbicb would
normally appear in analysis of virginpetroleumproduct residue, Iam submitting this Certificate of Waste
Constituents. I certio tbatl am familiar with the source of contamination of the soil and furtber certio the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
TRANSPORTER:
Contact:
Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #:
TRUCK DRIVER SIGNATURE:
TAG #: M /)_
rl �
VOLUME:
DATE: / '
w
DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
Date:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest # 52830
Date Load Number
(numbered sequentially as trucks are dispatched)
EjVffRONMENTAL CONSULTANT
Phone:
GENERATOR:
Contact:
WASTE ORIGINATIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION.• (ex. UST or other source)
Fax:
Comm.,:
Phone:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu ofsubmitting analytical data (metbods
8240 and 8270) verjoing that the waste in question does not contain organic constituents other than those wbicb would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certiflcate of Waste
Constituents. I cert�& that am familiar with the source of contamination of the soil and ficrtber cert o the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature:
TRANSPORTER:
Con
Phone:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
TRUCK #: e
TRUCK DRIVER SIGNATURE
TAG #: -
V,(,-VOLUME: Y 4.
DATE: /C)IA 3 /
DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 52835
Load Number
(numbered sequentially as trucks are dispatched)
ENVRONMENTAL CONSULTANT --
Contact: O;L' � iG E��r� Phone: 7_7 Fax:
GENERATOR:
�f V
WASTE ORIGIMITIONPOINT Complete Address:
Class &. Type of Contaminate in soil
SOURCE OF CONTAMINATION,• (ex. UST or other source)
County: CG
W1
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu ofsubmitting analytical data (metbods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those wbicb would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certfficate of Waste
Constituents. I cert v that I am familiar witb the source of contamination of the soil and further. certry the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: - z' Date: V,03
TRANSPORTER: r
Contact: 1'1.t� one: - f • �'?_ 7-
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate. QQ
Carrier Signature: Date:
i
TRUCK #: TAG #: 02 VOLUME: .,: 5,h
TRUCK DRIVER SIGNATURE: DATE: 10-23 -) •S
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: Date:
Signature:
Company Name
Date:
Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest # 5 ? 8 2 9
Date Lead Number
ENVIRONMENTAL CONSULTANT
Contact
GENER,4TOR:
Address:
(numbered sequentially as trucks are dispatched)
Phone: Fax:
WASTE ORIGINATIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT4MINA7I0N.• (ex. UST or other source)
County: "r .r e F
GENEX4TORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, Iam submitting this Certfficate of Waste
Constituents. I certify thatl am familiar with the source of contamination of the soil and further cert v the source, to
the best of my knowledge, contains no contaminants other than thfrt listed above.
Generators Signature: Date:
TP,4NSPORTER:
Con
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
r
TRUCK#: TAG#: -_ p�''_ VOLUME:
TRUCK DRIVER SIGNATURE: - DATE:
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
Da
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 52838
Date Load Number
(numbered sequentially as trucks are dispatched)
ENffRONMENT 4L CONSULTANT. , G �s• �
Contact: Phone::23: C•' I Fax:
GENERATOR:
pill
Address: U i &0 /� n County. v
Contact: `� ❑ r Phone:
WASTE 0RIGINATI0NP0 : Complete Address: �Ame, trs r:9 tue
Class &Type of Contaminate in soil Lr r ("'1 r r.r-
SOURCE OF CONT4MINATION.• (ex. UST or other source)
GENERATORS CERTIFIC14TIONOFWASTE CONSTITUENTS: In lieu ofsubmitting analytical data methods
8240 and 8270) verq�ing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin
petroleumproduct residue, Iam submitting this Certcate of Waste
Constituents. I cert�o that I am familiar with the source of contamination of the soil and further certq� the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Si
TRANSPORTER:
Date:i
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing tr spor•` ' n, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: !� r - Date: _ ,
TRUCK #: ..! TAG #:
TRUCK DRIVER SIGNATURE: DATE:
DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
White/Facility
I °
Canary/Invoice
Date:
Title-
Pink/Carrier
Date:
Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 -i Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest #
Date _ )" ;4' �¢ _ Load Number
(numbered sequentially as trucks are dispatched)
ENVIRONMEAMIL CONS ULE4N"I
Contact:
GENERATOR:
WASTE ORIGINATION
Fa
Phone: J A,ZC) , 7 Fax:
e County:
Phone: Zol�z 2a-�" fP--.7(
Complete Address: I
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION.• (ex. UST or other source)
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS:.In licit of s%bmitting analytical data (methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear- in analysis of z,irgin petr•oletim_iroduct r-evidrte, I am submittingtl�' Certificate of Waste
Constituents. I cent f , thatl aw familiar• with the source nf'conf amination of the soil and ftarther certify the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature:_X_ ___ _ Date: /0.7 3. JR
TRANSPORTER:
Contact:
{r) r L �-2 75
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, l):ickaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations gov''ning trapToytatiw2, and I. hereby receive this material for delivery to the
facility designate.
Carrier Signature:
TRUCK #:
TRUCK DRIVER SIGNATURE:
sr /_ z.
_-'n ` LI J y J
VOLUME: " `-I66
DATE: /,/) �
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Date: /;
Date: = '
Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest # 5 2 8 2 1
Date f . Load Number
(numbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONSULT 4NT ':..
Contact: E + —Phone:—; I Fax:
GENER 4TOR:
Address:, - - 1 .
Contact:
W,4STE ORIGINI4TIONPOINT- Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT4MINATION.• (ex. UST or other source)
County: }
Phone:
GENERf4TORS CERTIFIC,41I0N OF W,4STE CONSTITUENTS: In lieu of submitting analytical data methods
8240 and 8270) ver�fting that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certfcate of Waste
Constituents. I cert jo thatl am familiar with the source of contamination of the soil and further cert�o the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature:
TR,4NSPORTER:
Date.
Contact: A- 1 Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #: y.r' TAG #: VOLUME:
TRUCK DRIVER SIGNATURE: _ 1f" - ��Y� i t: DATE
DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: �'l;?' - - -.
Signature:
Company Name
White/Facility Canary/Invoice
Date:
Title:
Pink/Carrier
Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 52823
ENffRONMENT4L CONSULTANT
Contact:
GENERATOR:
Address:
Number
(numbered sequentially as trucks are dispatched)
Phone: Fax:
WASTE ORIGINATIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT4MINATION.• (ex. UST or other source)
Counw:
Phone: ~
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270) verjoing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleumproduct residue, Iam submitting this Certfficate of Waste
Constituents. I cert o that I am familiar with the source of contamination of the soil and further cert o the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: - Date:
TRANSPORTER:
Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #: Z_ TAG #:' ! �� '` VOLUME:
TRUCK DRIVER SIGNATURE: �`' f s� l DATE: I -
DESTINATION. Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
WhitdFacility.
Canary/Invoice Pink/Carrier
Date:.
Date:
Title:
Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 5 2- 8 2 7
oad Number
(numbered sequentially as trucks are dispatched)
ENURONMENTAL CONSULTANT
Contact:
GENERATOR:
Address
Contact.
WASTE ORMINATIONPOINT.• Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION. (ex. UST or other source)
Fax:
County:
Phone:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data methods
8240 and 8270) ver�ing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Cert#icate of Waste
Constituents. I cert�o that am familiar with the source of contamination of the soil and further cert�o the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signa
TRANSPORTER:
Contact:
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature:
TRUCK #: TAG #:
-:�rl`1U
_LL36i/ ,/
�
VOLUME:
TRUCK DRIVER SIGNATURE: .o r DATE: 7-
DESTINATION., Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
White/Facility Canary/Invoice
Date:,
Title:
Pink/Carrier
Datc:
Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest # 2 8 2 0
Date Load Number
ENURONMENT 4L CONSULT 4NT
Contact:
GENERATOR:
(numbered sequentially as trucks are dispatched)
Phone: _ Fax:
Address: County
Phone: - + . -_ 1
WASTE ORIGINATIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONT4MINATION.• (ex. UST or other source) i
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data methods
8240 and 8270) ver�ing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, Iam submitting this Certificate of Waste
Constituents. I cert�& that I am familiar with the source of contamination of the soil and further cert o the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature:
TRANSPORTER:
_1_k s}
Date: I - � .. It'R
Contact: -I - -. � Phone: ( -7 t •i) - i ( - i -� 7
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate,_f 7
Carrier Signature:. Date: 14) 1 /
TRUCK #: ? TAG #: _-Af YU-isVOLUME:_ 117,06
TRUCK DRIVER SIGNATURE: DATE:'
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature: + "� � ;. _ _ _ Date: Y,
Signature: Date: ,a . _ - {' _ -- _ _ -- . - -
Company Name �' { ~ Title:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Y
Date
Environmental Soils Inc.
Y _ PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest # 5 2 8 7 F
Load Number
(numbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONS ULTANT.•
GENERATOR:
Address:
WASTE ORIGINATIONPOINT Complete Address:
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION.• (ex. UST or other source)
Fax:
County:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270) ver�oing that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Certfcate of Waste
Constituents. I cer6� thatl am familiar with the source of contamination of the soil and further cert�o the source, to
the best of my knowledge, contains no contaminants other than that listed above,
Generators Signature:
TRANSPORTER:
Contact: Tf
Date:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #: bT_ AG #: N VOLUME: r" � I
TRUCK DRIVER SIGNATUI�F:=="�---GA--- - DATE; ZO u
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the State of North Carolina.
Facility Signature:
Signature:
Company Name
Ti
Date:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

Im
' f
Date
r � --
Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone]• Fax [phone]
Non -Hazardous Waste Manifest # 42588
Load Number
(1,111inbered sequentially as trucks are dispatched)
ENVIRONMENTAL CONSULTANT: Q.�A`
Contact: Plione: Fax:
GENERATOR:
Address:
Contact: l; �lr,,� �.•.r�
WASTE ORIGINATIONP61T? Complete
r
Class &Type of Contaminate in soil
SOURCE OF CONTAMINATION. (ex. UST or other source)
�- 73 County:
Phone:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS: In lieu of submitting analytical data (methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, Iam submitting this Certificate of Waste
Constituents. I certify that am familiar with the source of contamination of the soil and furtber certify the source, to
the best of my knowledge, contains no contaminants other than that listed above. .
Generators Signature:z�t,� �: _ Date:
TRANSPORTER:
Contact: ..� ' : ­- "­ A Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date: .
TRUCK #: -70 TAG #: P 6 P Z '^
VOLUME:
TRUCK DRIVER SIGNATURE: _ DATE: l�"?
DESTINATION.• Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Date:
Title:
White/Facility
Canary/Invoice
Pink/Carrier Goldenrod/Generator

Environmental Soils Inc.
PO Box 295 • Lattimore, NC 28089
Phone [phone] • Fax [phone]
Non -Hazardous Waste Manifest # 4 2 5 8 7
Date �� 1 Load Number �*
(numbered sequentially as trucks are dispatched)
ENVIRONMENEIL CONSULTANT
Contact: ��. z'� -.. ti , Phone: -1 ��I 3 0 9 ' ` 1 ZL Fax:
GENERATOR:
Address: "���25 �� 1 -� �'a ���. S>> ������� � Z -Z�3 County: tya t,
Contact: Phone: '70 �
WASTE ORIGIN47IONPOLV7: Complete Address: 1 k�_2ZIO AFL i (;,(N JQ
Class &Type of Contaminate in soil We
SOURCE OF CONTAMINATION. (ex. UST or,
source),, t
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS. In lieu of submitting analytical data (methods
8240 and 8270) verifying that the waste in question does not contain organic constituents other than those which would
normally appear in analysis of virgin petroleum product residue, I am submitting this Cerirtyicate of Waste
Constituents. I certify that am familiar wit$ the source of contamination of the soil and further certify the source, to
the best of my knowledge, contains no contaminants other than that listed above.
Generators Signature: Date:
TRANSPORTER:
Contact: Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials .
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby receive this material for delivery to the
facility designate.
Carrier Signature: Date:
TRUCK #:
TRUCK DRIVER SIGNATURE:
TAG#: _1- { I �70 ZS
U_ o 6
VOLUME:- a _
DATE:
DESTINATION: Environmental Soils Inc. 910 Crowder Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manne'r that has been authorized by the Sate of North Carolina.
Facility Signature:
Signature:
Company Name
Date:
Title:
Date:
White/Facility Canary/Invoice Pink/Carrier Goldenrod/Generator

APPENDIX C
SITE PHOTOGRAPHS

10200 ARTHUR DAVIS ROAD SITE
VIEW OF THE 550-GALLON DISEL UST ON 10.18.18 1 SIDE VIEW OF 550-GALLON DIESEL UST ON 10.18.18
VIEW OF UST PIT FOLLOWING REMOVAL OF THE 55-GALLON DIESEL UST ON I VIEW OF EXCAVATION OF WEST WALL OF UST PIT ON 10.22.18
10.22.18

10200 ARTHUR DAVIS ROAD SITE
VIEW OF MONITORING WELL MW-UST ADJACENT TO THE SOUTH WALL OF
THE UST PIT ON 10.22.18
VIEW OF EAST AND SOUTH WALLS OF UST PIT WITH SAMPLE LOCATIONS
ON 10.23.18
VIEW OF EAST WALL OF UST PIT AND ADJACENT STORAGE STRUCTURE ON
10.23.18
VIEW OF WEST AND NORTH WALLS OF UST PIT AND SAMPLE LOCATIONS ON
10.23.18

APPENDIX D
PACE ANALYTICAL DATA REPORTS

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
October 25, 2018
Lee Shank
Carolina Environmental Respons
5648 Daphne Drive
Charlotte, NC 28269
RE: Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Dear Lee Shank:
Enclosed are the analytical results for sample(s) received by the laboratory on October 18, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
1#�A"
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
cc: Steve Hamilton, Carolina Environmental Response Team
Cassandra Kisiah, Carolina Environmental Response
Team
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
10200 ARTHUR DAVIS
92404020
Analytes
Lab lD
Sample ID
Method
Analysts
Reported
Laboratory
92404020001
TANK
EPA8015C Modified
SEM
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92404020002
POST EVACUATION 12'
MADEP EPH
SEM
7
PASI-C
MADEP VPH
CL
6
PASI-C
EPA 8270D
PKS
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
92404020001
TAN K
EPA 8015C Modified
Diesel Range Organics(C10-C28)
2530
mg/kg
EPA 8015C Modified
Gas Range Organics (C6-C10)
85.8
mg/kg
ASTM D2974-87
Percent Moisture
21.0
%
92404020002
POST EVACUATION 12'
ASTM D2974-87
Percent Moisture
23.3
%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Report Limit Analyzed
63.9
10/23/18 16:37
9.7
10/21/18 02:57
0.10
10/18/18 17:01
0.10
10/18/18 17:02
Qualifiers
Page 4 of 40

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Carolina Environmental Response Team
Date: October 25, 2018
General Information:
1 sample was analyzed for EPA 8015C Modified. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 437441
S4: Surrogate recovery not evaluated against control limits due to sample dilution.
-TANK (Lab ID:92404020001)
• n-Pentacosane (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 5 of 40

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Method: MADEP EPH
Description: MADEP EPH NC Soil
Client: Carolina Environmental Response Team
Date: October 25, 2018
General Information:
1 sample was analyzed for MADEP EPH. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 437788
S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-
analysis).
• POST EVACUATION 12' (Lab ID: 92404020002)
• o-Terphenyl (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 6 of 40

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Method: EPA 8015C Modified
Description: Gasoline Range Organics
Client: Carolina Environmental Response Team
Date: October 25, 2018
General Information:
1 sample was analyzed for EPA 8015C Modified. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 437454
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
-TANK (Lab ID:92404020001)
• 4-Bromofluorobenzene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 7 of 40

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Method: MADEP VPH
Description: VPH NC Soil
Client: Carolina Environmental Response Team
Date: October 25, 2018
General Information:
1 sample was analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP VPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 437522
S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
• POST EVACUATION 12' (Lab ID: 92404020002)
• 4-Bromofluorobenzene (PID) (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 8 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Method: EPA 8270D
Description: 8270 MSSV Microwave
Client: Carolina Environmental Response Team
Date: October 25, 2018
General Information:
1 sample was analyzed for EPA 8270D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 9 of 40

aceAnalytical
_pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Method: EPA 8260B
Description: 8260/5035A Volatile Organics
Client: Carolina Environmental Response Team
Date: October 25, 2018
General Information:
1 sample was analyzed for EPA 8260B. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 437211
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92404033006
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 2404741)
• 2-Butanone (MEK)
• 2-Hexanone
• 4-Methyl-2-pentanone (MIBK)
• Acetone
• Diisopropyl ether
• Methyl-tert-butyl ether
• Vinyl acetate
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 10 of 40

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PROJECT NARRATIVE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Method: EPA 8260B
Description: 8260/5035A Volatile Organics
Client: Carolina Environmental Response Team
Date: October 25, 2018
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 11 of 40

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ANALYTICAL RESULTS
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Sample: TANK
Lab ID: 92404020001 Collected: 10/18/18 09:30 Received: 10/18/18 13:30 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
2530 mg/kg 63.9 10 10/20/18 12:18 10/23/18 16:37
Surrogates
n-Pentacosane (S)
0 % 33-129 10 10/20/18 12:18 10/23/18 16:37 629-99-2 S4
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
85.8 mg/kg 9.7 1 10/20/18 13:45 10/21/18 02:57
Surrogates
4-Bromofluorobenzene (S)
279 % 70-167 1 10/20/18 13:45 10/21/18 02:57 460-00-4 S5
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
21.0 % 0.10 1 10/18/18 17:01
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 40

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ANALYTICAL RESULTS
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Sample: POST EVACUATION 12'
Lab ID: 92404020002
Collected: 10/18/18
12:30
Received: 10/18/18 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Soil
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
12.9
1
10/23/18 12:18
10/24/18 23:14
N2
Aliphatic (C19-C36)
ND
mg/kg
12.9
1
10/23/18 12:18
10/24/18 23:14
N2
Aromatic (C11-C22)
ND
mg/kg
12.9
1
10/23/18 12:18
10/24/18 23:14
N2
Surrogates
Nonatriacontane (S)
72
%
40-140
1
10/23/18 12:18
10/24/18 23:14
7194-86-7
o-Terphenyl (S)
35
%
40-140
1
10/23/18 12:18
10/24/18 23:14
84-15-1
S2
2-Fluorobiphenyl (S)
56
%
40-140
1
10/23/18 12:18
10/24/18 23:14
321-60-8
2-Bromonaphthalene (S)
58
%
40-140
1
10/23/18 12:18
10/24/18 23:14
580-13-2
VPH NC Soil
Analytical Method:
MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-CO8)
ND
mg/kg
3.8
1
10/21/18 14:31
10/23/18 02:28
N2
Aliphatic (C09-C12)
ND
mg/kg
3.8
1
10/21/18 14:31
10/23/18 02:28
N2
Aliphatic(C09-C12) Adjusted
ND
mg/kg
3.8
1
10/21/18 14:31
10/23/18 02:28
N2
Aromatic (C09-C10)
ND
mg/kg
3.8
1
10/21/18 14:31
10/23/18 02:28
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
127
%
70-130
1
10/21/18 14:31
10/23/18 02:28
460-00-4
4-Bromofluorobenzene (PID) (S)
133
%
70-130
1
10/21/18 14:31
10/23/18 02:28
460-00-4
S3
8270 MSSV Microwave
Analytical Method: EPA 8270D
Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
83-32-9
Acenaphthylene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
208-96-8
Aniline
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
62-53-3
Anthracene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
120-12-7
Benzo(a)anthracene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
56-55-3
Benzo(a)pyrene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
207-08-9
Benzoic Acid
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
65-85-0
Benzyl alcohol
ND
ug/kg
858
1
10/20/18 17:46
10/21/18 13:21
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
101-55-3
Butylbenzylphthalate
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/kg
858
1
10/20/18 17:46
10/21/18 13:21
59-50-7
4-Chloroaniline
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
111-44-4
2-Chloronaphthalene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
91-58-7
2-Chlorophenol
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
7005-72-3
Chrysene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
53-70-3
Dibenzofuran
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
91-94-1
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Sample: POST EVACUATION 12' Lab ID: 92404020002 Collected: 10/18/18 12:30 Received: 10/18/18 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
2,4-Dichlorophenol
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
120-83-2
Diethylphthalate
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
84-66-2
2,4-Dimethylphenol
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
105-67-9
Dimethylphthalate
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
131-11-3
Di-n-butylphthalate
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
858
1
10/20/18 17:46
10/21/18 13:21
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
606-20-2
Di-n-octylphthalate
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
117-81-7
Fluoranthene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
206-44-0
Fluorene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
87-68-3
Hexachlorobenzene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
77-47-4
Hexachloroethane
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
193-39-5
Isophorone
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
78-59-1
1-Methylnaphthalene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
90-12-0
2-Methylnaphthalene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
15831-10-4
Naphthalene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
91-20-3
2-Nitroaniline
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
88-74-4
3-Nitroaniline
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
99-09-2
4-Nitroaniline
ND
ug/kg
858
1
10/20/18 17:46
10/21/18 13:21
100-01-6
Nitrobenzene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
98-95-3
2-Nitrophenol
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
88-75-5
4-Nitrophenol
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
108-60-1
Pentachlorophenol
ND
ug/kg
2140
1
10/20/18 17:46
10/21/18 13:21
87-86-5
Phenanthrene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
85-01-8
Phenol
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
108-95-2
Pyrene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
429
1
10/20/18 17:46
10/21/18 13:21
88-06-2
Surrogates
Nitrobenzene-d5 (S)
73
%
23-110
1
10/20/18 17:46
10/21/18 13:21
4165-60-0
2-Fluorobiphenyl (S)
69
%
30-110
1
10/20/18 17:46
10/21/18 13:21
321-60-8
Terphenyl-d14 (S)
96
%
28-110
1
10/20/18 17:46
10/21/18 13:21
1718-51-0
Phenol-d6 (S)
70
%
22-110
1
10/20/18 17:46
10/21/18 13:21
13127-88-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 40

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ANALYTICAL RESULTS
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Sample: POST EVACUATION 12' Lab ID: 92404020002 Collected: 10/18/18 12:30 Received: 10/18/18 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Surrogates
2-Fluorophenol (S)
67
%
13-110
1
10/20/18 17:46
10/21/18 13:21
367-12-4
2,4,6-Tribromophenol (S)
72
%
27-110
1
10/20/18 17:46
10/21/18 13:21
118-79-6
8260/5035A Volatile Organics
Analytical Method: EPA 8260B
Preparation Method: EPA 5035A
Acetone
ND
ug/kg
109
1
10/19/18 10:51
10/19/18 21:34
67-64-1
Benzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
71-43-2
Bromobenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
108-86-1
Bromochloromethane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
74-97-5
Bromodichloromethane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
75-27-4
Bromoform
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
75-25-2
Bromomethane
ND
ug/kg
10.9
1
10/19/18 10:51
10/19/18 21:34
74-83-9
2-Butanone (MEK)
ND
ug/kg
109
1
10/19/18 10:51
10/19/18 21:34
78-93-3
n-Butylbenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
104-51-8
sec-Butylbenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
135-98-8
tert-Butyl benzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
98-06-6
Carbon tetrachloride
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
56-23-5
Chlorobenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
108-90-7
Chloroethane
ND
ug/kg
10.9
1
10/19/18 10:51
10/19/18 21:34
75-00-3
Chloroform
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
67-66-3
Chloromethane
ND
ug/kg
10.9
1
10/19/18 10:51
10/19/18 21:34
74-87-3
2-Chlorotoluene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
95-49-8
4-Chlorotoluene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
96-12-8
Dibromochloromethane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
106-93-4
Dibromomethane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
106-46-7
Dichlorodifluoromethane
ND
ug/kg
10.9
1
10/19/18 10:51
10/19/18 21:34
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
10061-02-6
Diisopropyl ether
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
108-20-3
Ethylbenzene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
87-68-3
2-Hexanone
ND
ug/kg
54.7
1
10/19/18 10:51
10/19/18 21:34
591-78-6
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Sample: POST EVACUATION 12' Lab ID: 92404020002 Collected: 10/18/18 12:30 Received: 10/18/18 13:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8260E Preparation Method: EPA 5035A
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
98-82-8
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
99-87-6
ND
ug/kg
21.9
1
10/19/18 10:51
10/19/18 21:34
75-09-2
ND
ug/kg
54.7
1
10/19/18 10:51
10/19/18 21:34
108-10-1
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
1634-04-4
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
91-20-3
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
103-65-1
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
100-42-5
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
630-20-6
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
79-34-5
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
127-18-4
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
108-88-3
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
87-61-6
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
120-82-1
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
71-55-6
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
79-00-5
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
79-01-6
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
75-69-4
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
96-18-4
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
95-63-6
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
108-67-8
ND
ug/kg
54.7
1
10/19/18 10:51
10/19/18 21:34
108-05-4
ND
ug/kg
10.9
1
10/19/18 10:51
10/19/18 21:34
75-01-4
ND
ug/kg
10.9
1
10/19/18 10:51
10/19/18 21:34
1330-20-7
ND
ug/kg
10.9
1
10/19/18 10:51
10/19/18 21:34
179601-23-1
ND
ug/kg
5.5
1
10/19/18 10:51
10/19/18 21:34
95-47-6
109
%
70-130
1
10/19/18 10:51
10/19/18 21:34
2037-26-5
103
%
70-130
1
10/19/18 10:51
10/19/18 21:34
460-00-4
82
%
70-132
1
10/19/18 10:51
10/19/18 21:34
17060-07-0
Analytical Method: ASTM D2974-87
23.3 % 0.10 1
REPORT OF LABORATORY ANALYSIS
10/18/18 17:02
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QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
QC Batch: 437454 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92404020001
METHOD BLANK: 2405884 Matrix: Solid
Associated Lab Samples: 92404020001
Blank Reporting
Parameter Units Result Limit Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 10/20/18 12:15
4-Bromofluorobenzene (S) % 108 70-167 10/20/18 12:15
Qualifiers
LABORATORY CONTROL SAMPLE:
2405885
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50 44.1
88
70-165
4-Bromofluorobenzene (S)
%
103
70-167
MATRIX SPIKE SAMPLE:
2405886
92403886005 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 49
54.9
110
47-187
4-Bromofluorobenzene (S)
%
126
70-167
SAMPLE DUPLICATE: 2405887
Parameter
Gas Range Organics (C6-C10)
4-Bromofluorobenzene (S)
92403886007 Dup
Units Result Result
mg/kg ND ND
112 108
RPD Qualifiers
4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
QC Batch: 437522 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Associated Lab Samples: 92404020002
METHOD BLANK: 2406063
Associated Lab Samples: 92404020002
Parameter
Units
Aliphatic (C05-008)
mg/kg
Aliphatic (C09-C12)
mg/kg
Aromatic (C09-C10)
mg/kg
4-Bromofluorobenzene (FID) (S)
%
4-Bromofluorobenzene (PID) (S)
%
Matrix: Solid
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
2.5
10/22/1815:10 N2
ND
2.5
10/22/1815:10 N2
ND
2.5
10/22/1815:10 N2
96
70-130
10/22/1815:10
102
70-130
10/22/1815:10
LABORATORY CONTROL SAMPLE & LCSD:
2406064
2406065
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
14.9
14.8 14.4
99
96
70-130 3 25 N2
Aliphatic (C09-C12)
mg/kg
14.9
15.4 15.0
103
100
30-130 3 25 N2
Aromatic (C09-C10)
mg/kg
5
5.4 5.2
108
104
70-130 4 25 N2
4-Bromofluorobenzene (FID) (S)
%
108
102
70-130
4-Bromofluorobenzene (PID) (S)
%
115
108
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 40

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QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
QC Batch: 437211 Analysis Method: EPA 8260B
QC Batch Method: EPA 5035A Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92404020002
METHOD BLANK: 2404738
Associated Lab Samples: 92404020002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.2
10/19/18 12:43
1,1,1-Trichloroethane
ug/kg
ND
5.2
10/19/18 12:43
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.2
10/19/18 12:43
1,1,2-Trichloroethane
ug/kg
ND
5.2
10/19/18 12:43
1,1-Dichloroethane
ug/kg
ND
5.2
10/19/18 12:43
1,1-Dichloroethene
ug/kg
ND
5.2
10/19/18 12:43
1,1-Dichloropropene
ug/kg
ND
5.2
10/19/18 12:43
1,2,3-Trichlorobenzene
ug/kg
ND
5.2
10/19/18 12:43
1,2,3-Trichloropropane
ug/kg
ND
5.2
10/19/18 12:43
1,2,4-Trichlorobenzene
ug/kg
ND
5.2
10/19/18 12:43
1,2,4-Trimethylbenzene
ug/kg
ND
5.2
10/19/18 12:43
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.2
10/19/18 12:43
1,2-Dibromoethane (EDB)
ug/kg
ND
5.2
10/19/18 12:43
1,2-Dichlorobenzene
ug/kg
ND
5.2
10/19/18 12:43
1,2-Dichloroethane
ug/kg
ND
5.2
10/19/18 12:43
1,2-Dichloropropane
ug/kg
ND
5.2
10/19/18 12:43
1,3,5-Trimethylbenzene
ug/kg
ND
5.2
10/19/18 12:43
1,3-Dichlorobenzene
ug/kg
ND
5.2
10/19/18 12:43
1,3-Dichloropropane
ug/kg
ND
5.2
10/19/18 12:43
1,4-Dichlorobenzene
ug/kg
ND
5.2
10/19/18 12:43
2,2-Dichloropropane
ug/kg
ND
5.2
10/19/18 12:43
2-Butanone (MEK)
ug/kg
ND
103
10/19/18 12:43
2-Chlorotoluene
ug/kg
ND
5.2
10/19/18 12:43
2-Hexanone
ug/kg
ND
51.7
10/19/18 12:43
4-Chlorotoluene
ug/kg
ND
5.2
10/19/18 12:43
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
51.7
10/19/18 12:43
Acetone
ug/kg
ND
103
10/19/18 12:43
Benzene
ug/kg
ND
5.2
10/19/18 12:43
Bromobenzene
ug/kg
ND
5.2
10/19/18 12:43
Bromochloromethane
ug/kg
ND
5.2
10/19/18 12:43
Bromodichloromethane
ug/kg
ND
5.2
10/19/18 12:43
Bromoform
ug/kg
ND
5.2
10/19/18 12:43
Bromomethane
ug/kg
ND
10.3
10/19/18 12:43
Carbon tetrachloride
ug/kg
ND
5.2
10/19/18 12:43
Chlorobenzene
ug/kg
ND
5.2
10/19/18 12:43
Chloroethane
ug/kg
ND
10.3
10/19/18 12:43
Chloroform
ug/kg
ND
5.2
10/19/18 12:43
Chloromethane
ug/kg
ND
10.3
10/19/18 12:43
cis-1,2-Dichloroethene
ug/kg
ND
5.2
10/19/18 12:43
cis-1,3-Dichloropropene
ug/kg
ND
5.2
10/19/18 12:43
Dibromochloromethane
ug/kg
ND
5.2
10/19/18 12:43
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
METHOD BLANK: 2404738
Associated Lab Samples: 92404020002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
Dibromomethane
ug/kg
ND
5.2
10/19/18 12:43
Dichlorodifluoromethane
ug/kg
ND
10.3
10/19/18 12:43
Diisopropyl ether
ug/kg
ND
5.2
10/19/18 12:43
Ethylbenzene
ug/kg
ND
5.2
10/19/18 12:43
Hexachloro-1,3-butadiene
ug/kg
ND
5.2
10/19/18 12:43
Isopropylbenzene (Cumene)
ug/kg
ND
5.2
10/19/18 12:43
m&p-Xylene
ug/kg
ND
10.3
10/19/18 12:43
Methyl-tert-butyl ether
ug/kg
ND
5.2
10/19/18 12:43
Methylene Chloride
ug/kg
ND
20.7
10/19/18 12:43
n-Butylbenzene
ug/kg
ND
5.2
10/19/18 12:43
n-Propylbenzene
ug/kg
ND
5.2
10/19/18 12:43
Naphthalene
ug/kg
ND
5.2
10/19/18 12:43
o-Xylene
ug/kg
ND
5.2
10/19/18 12:43
p-Isopropyltoluene
ug/kg
ND
5.2
10/19/18 12:43
sec-Butylbenzene
ug/kg
ND
5.2
10/19/18 12:43
Styrene
ug/kg
ND
5.2
10/19/18 12:43
tert-Butyl benzene
ug/kg
ND
5.2
10/19/18 12:43
Tetrachloroethene
ug/kg
ND
5.2
10/19/18 12:43
Toluene
ug/kg
ND
5.2
10/19/18 12:43
trans-1,2-Dichloroethene
ug/kg
ND
5.2
10/19/18 12:43
trans- 1,3-Dichloropropene
ug/kg
ND
5.2
10/19/18 12:43
Trichloroethene
ug/kg
ND
5.2
10/19/18 12:43
Trichlorofluoromethane
ug/kg
ND
5.2
10/19/18 12:43
Vinyl acetate
ug/kg
ND
51.7
10/19/18 12:43
Vinyl chloride
ug/kg
ND
10.3
10/19/18 12:43
Xylene (Total)
ug/kg
ND
10.3
10/19/18 12:43
1,2-Dichloroethane-d4 (S)
%
84
70-132
10/19/18 12:43
4-Bromofluorobenzene (S)
%
101
70-130
10/19/18 12:43
Toluene-d8 (S)
%
106
70-130
10/19/18 12:43
Qualifiers
LABORATORY CONTROL SAMPLE:
2404739
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
52.6
54.2
103
74-137
1,1,1-Trichloroethane
ug/kg
52.6
53.6
102
67-140
1,1,2,2-Tetrachloroethane
ug/kg
52.6
50.3
96
72-141
1,1,2-Trichloroethane
ug/kg
52.6
55.5
105
78-138
1,1-Dichloroethane
ug/kg
52.6
52.9
101
69-134
1,1-Dichloroethene
ug/kg
52.6
57.4
109
67-138
1,1-Dichloropropene
ug/kg
52.6
58.2
111
69-139
1,2,3-Trichlorobenzene
ug/kg
52.6
55.6
106
70-146
1,2,3-Trichloropropane
ug/kg
52.6
53.5
102
69-144
1,2,4-Trichlorobenzene
ug/kg
52.6
56.9
108
68-148
1,2,4-Trimethylbenzene
ug/kg
52.6
55.9
106
74-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
LABORATORY CONTROL SAMPLE:
Parameter
2404739
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/kg
52.6
55.3
105
65-140
1,2-Dibromoethane (EDB)
ug/kg
52.6
53.7
102
77-135
1,2-Dichlorobenzene
ug/kg
52.6
54.6
104
77-141
1,2-Dichloroethane
ug/kg
52.6
53.5
102
65-137
1,2-Dichloropropane
ug/kg
52.6
56.2
107
72-136
1,3,5-Trimethylbenzene
ug/kg
52.6
56.4
107
76-133
1,3-Dichlorobenzene
ug/kg
52.6
56.5
107
74-138
1,3-Dichloropropane
ug/kg
52.6
55.7
106
71-139
1,4-Dichlorobenzene
ug/kg
52.6
56.0
106
76-138
2,2-Dichloropropane
ug/kg
52.6
53.2
101
68-137
2-Butanone (MEK)
ug/kg
105
105
100
58-147
2-Chlorotoluene
ug/kg
52.6
55.8
106
73-139
2-Hexanone
ug/kg
105
103
98
62-145
4-Chlorotoluene
ug/kg
52.6
56.0
106
76-141
4-Methyl-2-pentanone (MIBK)
ug/kg
105
102
97
64-149
Acetone
ug/kg
105
89.2J
85
53-153
Benzene
ug/kg
52.6
57.4
109
73-135
Bromobenzene
ug/kg
52.6
55.7
106
75-133
Bromochloromethane
ug/kg
52.6
53.2
101
73-134
Bromodichloromethane
ug/kg
52.6
57.9
110
71-135
Bromoform
ug/kg
52.6
54.9
104
66-141
Bromomethane
ug/kg
52.6
58.6
111
53-160
Carbon tetrachloride
ug/kg
52.6
55.9
106
60-145
Chlorobenzene
ug/kg
52.6
53.5
102
78-130
Chloroethane
ug/kg
52.6
54.2
103
64-149
Chloroform
ug/kg
52.6
55.7
106
70-134
Chloromethane
ug/kg
52.6
44.4
84
52-150
cis-1,2-Dichloroethene
ug/kg
52.6
55.3
105
70-133
cis-1,3-Dichloropropene
ug/kg
52.6
58.9
112
68-134
Dibromochloromethane
ug/kg
52.6
55.3
105
71-138
Dibromomethane
ug/kg
52.6
53.7
102
74-130
Dichlorodifluoromethane
ug/kg
52.6
50.1
95
40-160
Diisopropyl ether
ug/kg
52.6
55.0
104
69-141
Ethylbenzene
ug/kg
52.6
54.3
103
75-133
Hexachloro-1,3-butadiene
ug/kg
52.6
56.2
107
68-143
Isopropylbenzene (Cumene)
ug/kg
52.6
54.6
104
76-143
m&p-Xylene
ug/kg
105
109
104
75-136
Methyl-tert-butyl ether
ug/kg
52.6
53.7
102
68-144
Methylene Chloride
ug/kg
52.6
56.6
108
45-154
n-Butylbenzene
ug/kg
52.6
58.8
112
72-137
n-Propylbenzene
ug/kg
52.6
57.6
110
76-136
Naphthalene
ug/kg
52.6
53.6
102
68-151
o-Xylene
ug/kg
52.6
54.9
104
76-141
p-Isopropyltoluene
ug/kg
52.6
57.2
109
76-140
sec-Butylbenzene
ug/kg
52.6
58.7
112
79-139
Styrene
ug/kg
52.6
53.0
101
79-137
tert-Butyl benzene
ug/kg
52.6
52.5
100
74-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
LABORATORY CONTROL SAMPLE:
2404739
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Tetrachloroethene
ug/kg
52.6
48.0
91
71-138
Toluene
ug/kg
52.6
57.5
109
74-131
trans-1,2-Dichloroethene
ug/kg
52.6
53.8
102
67-135
trans- 1,3-Dichloropropene
ug/kg
52.6
59.4
113
65-146
Trichloroethene
ug/kg
52.6
61.3
116
67-135
Trichlorofluoromethane
ug/kg
52.6
54.2
103
59-144
Vinyl acetate
ug/kg
105
70.2
67
40-160
Vinyl chloride
ug/kg
52.6
57.5
109
56-141
Xylene (Total)
ug/kg
158
164
104
76-137
1,2-Dichloroethane-d4 (S)
%
96
70-132
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
2404741
92404033006
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
18.8
18.4
98
70-130
1,1,1-Trichloroethane
ug/kg
ND
18.8
18.1
96
70-130
1,1,2,2-Tetrachloroethane
ug/kg
ND
18.8
18.2
97
70-130
1,1,2-Trichloroethane
ug/kg
ND
18.8
16.8
89
70-130
1,1-Dichloroethane
ug/kg
ND
18.8
18.0
96
70-130
1,1-Dichloroethene
ug/kg
ND
18.8
18.6
99
49-180
1,1-Dichloropropene
ug/kg
ND
18.8
18.0
96
70-130
1,2,3-Trichlorobenzene
ug/kg
ND
18.8
13.1
70
70-130
1,2,3-Trichloropropane
ug/kg
ND
18.8
18.6
99
70-130
1,2,4-Trichlorobenzene
ug/kg
ND
18.8
14.3
76
70-130
1,2,4-Trimethylbenzene
ug/kg
ND
18.8
18.6
99
70-130
1,2-Dibromo-3-chloropropane
ug/kg
ND
18.8
18.8
100
70-130
1,2-Dibromoethane (EDB)
ug/kg
ND
18.8
17.8
95
70-130
1,2-Dichlorobenzene
ug/kg
ND
18.8
17.6
94
70-130
1,2-Dichloroethane
ug/kg
ND
18.8
17.3
92
70-130
1,2-Dichloropropane
ug/kg
ND
18.8
18.3
97
70-130
1,3,5-Trimethylbenzene
ug/kg
9.4
18.8
19.5
54
70-130
1,3-Dichlorobenzene
ug/kg
ND
18.8
18.2
97
70-130
1,3-Dichloropropane
ug/kg
ND
18.8
19.0
101
70-130
1,4-Dichlorobenzene
ug/kg
ND
18.8
17.9
95
70-130
2,2-Dichloropropane
ug/kg
ND
18.8
18.0
96
70-130
2-Butanone (MEK)
ug/kg
ND
37.5
41.9J
112
70-130 M1
2-Chlorotoluene
ug/kg
ND
18.8
19.1
102
70-130
2-Hexanone
ug/kg
ND
37.5
31.7J
85
70-130 M1
4-Chlorotoluene
ug/kg
ND
18.8
18.8
100
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
37.5
33.6J
90
70-130 M1
Acetone
ug/kg
ND
37.5
41J
109
70-130 M1
Benzene
ug/kg
ND
18.8
18.3
97
50-166
Bromobenzene
ug/kg
ND
18.8
18.2
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
MATRIX SPIKE SAMPLE:
2404741
92404033006
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/kg
ND
18.8
17.7
94
70-130
Bromodichloromethane
ug/kg
ND
18.8
17.6
94
70-130
Bromoform
ug/kg
ND
18.8
17.6
94
70-130
Bromomethane
ug/kg
ND
18.8
21.3
113
70-130
Carbon tetrachloride
ug/kg
ND
18.8
18.1
96
70-130
Chlorobenzene
ug/kg
ND
18.8
18.3
98
43-169
Chloroethane
ug/kg
ND
18.8
18.4
98
70-130
Chloroform
ug/kg
ND
18.8
17.9
95
70-130
Chloromethane
ug/kg
ND
18.8
17.4
93
70-130
cis-1,2-Dichloroethene
ug/kg
ND
18.8
17.8
95
70-130
cis-1,3-Dichloropropene
ug/kg
ND
18.8
16.9
90
70-130
Dibromochloromethane
ug/kg
ND
18.8
18.2
97
70-130
Dibromomethane
ug/kg
ND
18.8
16.6
88
70-130
Dichlorodifluoromethane
ug/kg
ND
18.8
16.8
89
70-130
Diisopropyl ether
ug/kg
ND
18.8
17.0
91
70-130 M1
Ethylbenzene
ug/kg
ND
18.8
18.7
87
70-130
Hexachloro-1,3-butadiene
ug/kg
ND
18.8
12.8
68
70-130
Isopropylbenzene (Cumene)
ug/kg
ND
18.8
18.9
100
70-130
m&p-Xylene
ug/kg
ND
37.5
36.7
89
70-130
Methyl-tert-butyl ether
ug/kg
ND
18.8
15.4
82
70-130 M1
Methylene Chloride
ug/kg
ND
18.8
14.3J
76
70-130
n-Butylbenzene
ug/kg
ND
18.8
17.6
94
70-130
n-Propylbenzene
ug/kg
ND
18.8
20.0
97
70-130
Naphthalene
ug/kg
ND
18.8
15.0
55
70-130
o-Xylene
ug/kg
ND
18.8
18.5
73
70-130
p-Isopropyltoluene
ug/kg
ND
18.8
18.2
87
70-130
sec-Butylbenzene
ug/kg
ND
18.8
19.2
102
70-130
Styrene
ug/kg
ND
18.8
17.1
91
70-130
tert-Butyl benzene
ug/kg
ND
18.8
17.8
95
70-130
Tetrachloroethene
ug/kg
ND
18.8
17.1
91
70-130
Toluene
ug/kg
ND
18.8
17.4
92
52-163
trans-1,2-Dichloroethene
ug/kg
ND
18.8
18.1
96
70-130
trans- 1,3-Dichloropropene
ug/kg
ND
18.8
16.3
87
70-130
Trichloroethene
ug/kg
ND
18.8
17.6
94
49-167
Trichlorofluoromethane
ug/kg
ND
18.8
17.4
93
70-130
Vinyl acetate
ug/kg
ND
37.5
16J
43
70-130 M1
Vinyl chloride
ug/kg
ND
18.8
20.1
107
70-130
Xylene (Total)
ug/kg
ND
56.3
55.2
98
70-130
1,2-Dichloroethane-d4 (S)
%
101
70-132
4-Bromofluorobenzene (S)
%
91
70-130
Toluene-d8 (S)
%
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
SAMPLE DUPLICATE: 2404740
Parameter
Units
92404042003
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
1,1,1-Trichloroethane
ug/kg
ND
ND
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
1,1,2-Trichloroethane
ug/kg
ND
ND
1,1-Dichloroethane
ug/kg
ND
ND
1,1-Dichloroethene
ug/kg
ND
ND
1,1-Dichloropropene
ug/kg
ND
ND
1,2,3-Trichlorobenzene
ug/kg
ND
ND
1,2,3-Trichloropropane
ug/kg
ND
ND
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2,4-Trimethylbenzene
ug/kg
ND
ND
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Dichloroethane
ug/kg
ND
ND
1,2-Dichloropropane
ug/kg
ND
ND
1,3,5-Trimethylbenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichloropropane
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
2,2-Dichloropropane
ug/kg
ND
ND
2-Butanone (MEK)
ug/kg
ND
ND
2-Chlorotoluene
ug/kg
ND
ND
2-Hexanone
ug/kg
ND
ND
4-Chlorotoluene
ug/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
Acetone
ug/kg
ND
17.1J
Benzene
ug/kg
ND
ND
Bromobenzene
ug/kg
ND
ND
Bromochloromethane
ug/kg
ND
ND
Bromodichloromethane
ug/kg
ND
ND
Bromoform
ug/kg
ND
ND
Bromomethane
ug/kg
ND
ND
Carbon tetrachloride
ug/kg
ND
ND
Chlorobenzene
ug/kg
ND
ND
Chloroethane
ug/kg
ND
ND
Chloroform
ug/kg
ND
ND
Chloromethane
ug/kg
ND
ND
cis-1,2-Dichloroethene
ug/kg
ND
ND
cis-1,3-Dichloropropene
ug/kg
ND
ND
Dibromochloromethane
ug/kg
ND
ND
Dibromomethane
ug/kg
ND
ND
Dichlorodifluoromethane
ug/kg
ND
ND
Diisopropyl ether
ug/kg
ND
ND
Ethylbenzene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Isopropylbenzene (Cumene)
ug/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
SAMPLE DUPLICATE: 2404740
Parameter
Units
92404042003
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
ND
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
85
110
4-Bromofluorobenzene (S)
%
97
82
Toluene-d8(S)
%
106
99
RPD Qualifiers
37
6
5
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
QC Batch: 437441 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92404020001
METHOD BLANK: 2405826 Matrix: Solid
Associated Lab Samples: 92404020001
Blank Reporting
Parameter Units Result Limit Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 10/22/18 15:21
n-Pentacosane (S) % 75 41-119 10/22/18 15:21
Qualifiers
LABORATORY CONTROL SAMPLE:
2405827
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
65.6 49.1
75
49-113
n-Pentacosane(S)
%
77
41-119
MATRIX SPIKE SAMPLE:
2405828
92403886001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 70.4
50.0
67 10-146
n-Pentacosane(S)
%
64 41-119
SAMPLE DUPLICATE: 2405829
Parameter
Diesel Range Organics(C10-C28)
n-Pentacosane (S)
92403886001 Dup
Units Result Result
mg/kg ND 5.5
% 66 74
RPD Qualifiers
8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
QC Batch: 437473 Analysis Method: EPA 8270D
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92404020002
METHOD BLANK: 2405957
Associated Lab Samples: 92404020002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
334
10/21/18 09:59
1,2-Dichlorobenzene
ug/kg
ND
334
10/21/18 09:59
1,3-Dichlorobenzene
ug/kg
ND
334
10/21/18 09:59
1,4-Dichlorobenzene
ug/kg
ND
334
10/21/18 09:59
1-Methylnaphthalene
ug/kg
ND
334
10/21/18 09:59
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
334
10/21/18 09:59
2,4,5-Trichlorophenol
ug/kg
ND
334
10/21/18 09:59
2,4,6-Trichlorophenol
ug/kg
ND
334
10/21/18 09:59
2,4-Dichlorophenol
ug/kg
ND
334
10/21/18 09:59
2,4-Dimethylphenol
ug/kg
ND
334
10/21/18 09:59
2,4-Dinitrophenol
ug/kg
ND
1670
10/21/18 09:59
2,4-Dinitrotoluene
ug/kg
ND
334
10/21/18 09:59
2,6-Dinitrotoluene
ug/kg
ND
334
10/21/18 09:59
2-Chloronaphthalene
ug/kg
ND
334
10/21/18 09:59
2-Chlorophenol
ug/kg
ND
334
10/21/18 09:59
2-Methylnaphthalene
ug/kg
ND
334
10/21/18 09:59
2-Methylphenol(o-Cresol)
ug/kg
ND
334
10/21/18 09:59
2-Nitroaniline
ug/kg
ND
1670
10/21/18 09:59
2-Nitrophenol
ug/kg
ND
334
10/21/18 09:59
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
334
10/21/18 09:59
3,3'-Dichlorobenzidine
ug/kg
ND
1670
10/21/18 09:59
3-Nitroaniline
ug/kg
ND
1670
10/21/18 09:59
4,6-Dinitro-2-methyl phenol
ug/kg
ND
669
10/21/18 09:59
4-Bromophenylphenyl ether
ug/kg
ND
334
10/21/18 09:59
4-ChIoro-3-methyl phenol
ug/kg
ND
669
10/21/18 09:59
4-Chloroaniline
ug/kg
ND
1670
10/21/18 09:59
4-Chlorophenylphenyl ether
ug/kg
ND
334
10/21/18 09:59
4-Nitroaniline
ug/kg
ND
669
10/21/18 09:59
4-Nitrophenol
ug/kg
ND
1670
10/21/18 09:59
Acenaphthene
ug/kg
ND
334
10/21/18 09:59
Acenaphthylene
ug/kg
ND
334
10/21/18 09:59
Aniline
ug/kg
ND
334
10/21/18 09:59
Anthracene
ug/kg
ND
334
10/21/18 09:59
Benzo(a)anthracene
ug/kg
ND
334
10/21/18 09:59
Benzo(a)pyrene
ug/kg
ND
334
10/21/18 09:59
Benzo(b)fluoranthene
ug/kg
ND
334
10/21/18 09:59
Benzo(g,h,i)perylene
ug/kg
ND
334
10/21/18 09:59
Benzo(k)fluoranthene
ug/kg
ND
334
10/21/18 09:59
Benzoic Acid
ug/kg
ND
1670
10/21/18 09:59
Benzyl alcohol
ug/kg
ND
669
10/21/18 09:59
bis(2-Chloroethoxy)methane
ug/kg
ND
334
10/21/18 09:59
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
METHOD BLANK: 2405957
Associated Lab Samples: 92404020002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
bis(2-Chloroethyl) ether
ug/kg
ND
334
10/21/18 09:59
bis(2-Ethylhexyl)phthalate
ug/kg
ND
334
10/21/18 09:59
Butylbenzylphthalate
ug/kg
ND
334
10/21/18 09:59
Chrysene
ug/kg
ND
334
10/21/18 09:59
Di-n-butylphthalate
ug/kg
ND
334
10/21/18 09:59
Di-n-octylphthalate
ug/kg
ND
334
10/21/18 09:59
Dibenz(a,h)anthracene
ug/kg
ND
334
10/21/18 09:59
Dibenzofuran
ug/kg
ND
334
10/21/18 09:59
Diethylphthalate
ug/kg
ND
334
10/21/18 09:59
Dimethylphthalate
ug/kg
ND
334
10/21/18 09:59
Fluoranthene
ug/kg
ND
334
10/21/18 09:59
Fluorene
ug/kg
ND
334
10/21/18 09:59
Hexachloro-1,3-butadiene
ug/kg
ND
334
10/21/18 09:59
Hexachlorobenzene
ug/kg
ND
334
10/21/18 09:59
Hexachlorocyclopentadiene
ug/kg
ND
334
10/21/18 09:59
Hexachloroethane
ug/kg
ND
334
10/21/18 09:59
Indeno(1,2,3-cd)pyrene
ug/kg
ND
334
10/21/18 09:59
Isophorone
ug/kg
ND
334
10/21/18 09:59
N-Nitroso-di-n-propylamine
ug/kg
ND
334
10/21/18 09:59
N-Nitrosodimethylamine
ug/kg
ND
334
10/21/18 09:59
N-Nitrosodiphenylamine
ug/kg
ND
334
10/21/18 09:59
Naphthalene
ug/kg
ND
334
10/21/18 09:59
Nitrobenzene
ug/kg
ND
334
10/21/18 09:59
Pentachlorophenol
ug/kg
ND
1670
10/21/18 09:59
Phenanthrene
ug/kg
ND
334
10/21/18 09:59
Phenol
ug/kg
ND
334
10/21/18 09:59
Pyrene
ug/kg
ND
334
10/21/18 09:59
2,4,6-Tribromophenol (S)
%
71
27-110
10/21/18 09:59
2-Fluorobiphenyl (S)
%
72
30-110
10/21/18 09:59
2-Fluorophenol(S)
%
68
13-110
10/21/18 09:59
Nitrobenzene-d5 (S)
%
71
23-110
10/21/18 09:59
Phenol-d6 (S)
%
71
22-110
10/21/18 09:59
Terphenyl-d14 (S)
%
104
28-110
10/21/18 09:59
Qualifiers
LABORATORY CONTROL SAMPLE:
2405958
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1660
1320
79
36-120
1,2-Dichlorobenzene
ug/kg
1660
1280
77
41-120
1,3-Dichlorobenzene
ug/kg
1660
1240
75
66-120
1,4-Dichlorobenzene
ug/kg
1660
1330
80
42-120
1-Methylnaphthalene
ug/kg
1660
1410
85
40-120
2,2'-Oxybis(1-chloropropane)
ug/kg
1660
1300
78
17-120
2,4,5-Trichlorophenol
ug/kg
1660
1350
81
37-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
LABORATORY CONTROL SAMPLE:
Parameter
2405958
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,6-TrichIorophenol
ug/kg
1660
1410
85
40-120
2,4-DichIorophenol
ug/kg
1660
1370
83
33-120
2,4-Dimethylphenol
ug/kg
1660
1480
89
36-120
2,4-Dinitrophenol
ug/kg
8310
6210
75
22-121
2,4-Dinitrotoluene
ug/kg
1660
1500
90
60-120
2,6-Dinitrotoluene
ug/kg
1660
1500
90
54-120
2-Chloronaphthalene
ug/kg
1660
1370
82
41-120
2-Chlorophenol
ug/kg
1660
1360
82
39-120
2-Methylnaphthalene
ug/kg
1660
1390
84
26-120
2-Methylphenol(o-Cresol)
ug/kg
1660
1350
82
41-120
2-Nitroaniline
ug/kg
3320
2740
82
45-120
2-Nitrophenol
ug/kg
1660
1350
81
35-120
3&4-Methyl phenol (m&p Cresol)
ug/kg
1660
1270
77
35-120
3,3'-Dichlorobenzidine
ug/kg
3320
2880
87
16-125
3-Nitroaniline
ug/kg
3320
2490
75
45-120
4,6-Dinitro-2-methyl phenol
ug/kg
3320
2910
88
46-120
4-Bromophenylphenyl ether
ug/kg
1660
1430
86
36-120
4-Chloro-3-methylphenol
ug/kg
3320
2840
85
37-120
4-Chloroaniline
ug/kg
3320
2530
76
35-120
4-Chlorophenylphenyl ether
ug/kg
1660
1460
88
30-120
4-Nitroaniline
ug/kg
3320
2630
79
48-120
4-Nitrophenol
ug/kg
8310
7010
84
43-120
Acenaphthene
ug/kg
1660
1370
83
46-120
Acenaphthylene
ug/kg
1660
1400
84
46-120
Aniline
ug/kg
1660
1140
69
33-120
Anthracene
ug/kg
1660
1420
85
63-120
Benzo(a)anthracene
ug/kg
1660
1500
90
61-120
Benzo(a)pyrene
ug/kg
1660
1510
91
59-120
Benzo(b)fluoranthene
ug/kg
1660
1500
90
55-120
Benzo(g,h,i)perylene
ug/kg
1660
1540
93
57-120
Benzo(k)fluoranthene
ug/kg
1660
1520
92
56-120
Benzoic Acid
ug/kg
8310
5960
72
13-120
Benzyl alcohol
ug/kg
3320
2700
81
34-120
bis(2-Chloroethoxy)methane
ug/kg
1660
1470
88
21-120
bis(2-Chloroethyl) ether
ug/kg
1660
1350
81
25-120
bis(2-Ethylhexyl)phthalate
ug/kg
1660
1390
84
56-123
Butylbenzylphthalate
ug/kg
1660
1380
83
57-120
Chrysene
ug/kg
1660
1440
87
64-120
Di-n-butylphthalate
ug/kg
1660
1350
81
58-120
Di-n-octylphthalate
ug/kg
1660
1470
88
47-121
Dibenz(a,h)anthracene
ug/kg
1660
1530
92
56-120
Dibenzofuran
ug/kg
1660
1400
84
43-120
Diethylphthalate
ug/kg
1660
1300
78
55-120
Dimethylphthalate
ug/kg
1660
1310
79
54-120
Fluoranthene
ug/kg
1660
1420
85
61-120
Fluorene
ug/kg
1660
1450
87
51-120
Hexachloro-1,3-butadiene
ug/kg
1660
1330
80
22-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 40

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
LABORATORY CONTROL SAMPLE:
Parameter
2405958
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachlorobenzene
ug/kg
1660
1360
82
53-120
Hexachlorocyclopentadiene
ug/kg
1660
1310
79
18-150
Hexachloroethane
ug/kg
1660
1290
78
39-120
Indeno(1,2,3-cd)pyrene
ug/kg
1660
1540
93
58-120
Isophorone
ug/kg
1660
1190
72
38-120
N-Nitroso-di-n-propylamine
ug/kg
1660
1270
76
30-120
N-Nitrosodimethylamine
ug/kg
1660
1580
95
32-120
N-Nitrosodiphenylamine
ug/kg
1660
1410
85
50-120
Naphthalene
ug/kg
1660
1340
80
38-120
Nitrobenzene
ug/kg
1660
1300
78
37-120
Pentachlorophenol
ug/kg
3320
2140
64
10-120
Phenanthrene
ug/kg
1660
1430
86
62-120
Phenol
ug/kg
1660
1310
79
37-120
Pyrene
ug/kg
1660
1470
88
63-120
2,4,6-Tribromophenol (S)
%
86
27-110
2-Fluorobiphenyl (S)
%
84
30-110
2-Fluorophenol(S)
%
81
13-110
Nitrobenzene-d5 (S)
%
82
23-110
Phenol-d6 (S)
%
82
22-110
Terphenyl-d14 (S)
%
103
28-110
MATRIX SPIKE SAMPLE:
Parameter
2405959
Units
92404042001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
1710
890
52
18-119
1,2-Dichlorobenzene
ug/kg
ND
1710
861
50
50-110
1,3-Dichlorobenzene
ug/kg
ND
1710
826
48
27-110
1,4-Dichlorobenzene
ug/kg
ND
1710
883
51
28-110
1-Methylnaphthalene
ug/kg
ND
1710
1000
58
24-116
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
1710
870
51
50-150
2,4,5-Trichlorophenol
ug/kg
ND
1710
1100
64
28-110
2,4,6-Trichlorophenol
ug/kg
ND
1710
1080
63
17-117
2,4-Dichlorophenol
ug/kg
ND
1710
953
56
21-128
2,4-Dimethylphenol
ug/kg
ND
1710
1040
60
10-120
2,4-Dinitrophenol
ug/kg
ND
8580
5750
67
10-107
2,4-Dinitrotoluene
ug/kg
ND
1710
1300
76
36-109
2,6-Dinitrotoluene
ug/kg
ND
1710
1250
73
32-110
2-Chloronaphthalene
ug/kg
ND
1710
959
56
30-107
2-Chlorophenol
ug/kg
ND
1710
908
53
14-106
2-Methylnaphthalene
ug/kg
ND
1710
969
56
10-135
2-Methylphenol(o-Cresol)
ug/kg
ND
1710
932
54
10-124
2-Nitroaniline
ug/kg
ND
3430
2200
64
26-116
2-Nitrophenol
ug/kg
ND
1710
910
53
28-103
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
1710
911
53
10-109
3,3'-Dichlorobenzidine
ug/kg
ND
3430
2250
66
10-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
MATRIX SPIKE SAMPLE:
2405959
92404042001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
3-Nitroaniline
ug/kg
ND
3430
2220
65
22-110
4,6-Dinitro-2-methyl phenol
ug/kg
ND
3430
2650
77
13-121
4-Bromophenylphenyl ether
ug/kg
ND
1710
1210
70
31-109
4-Chloro-3-methylphenol
ug/kg
ND
3430
2290
67
13-128
4-Chloroaniline
ug/kg
ND
3430
1730
51
18-102
4-Chlorophenylphenyl ether
ug/kg
ND
1710
1180
68
29-112
4-Nitroaniline
ug/kg
ND
3430
2340
68
16-111
4-Nitrophenol
ug/kg
ND
8580
5820
68
14-135
Acenaphthene
ug/kg
ND
1710
1030
60
26-114
Acenaphthylene
ug/kg
ND
1710
1040
61
32-108
Aniline
ug/kg
ND
1710
716
42
10-107
Anthracene
ug/kg
ND
1710
1280
74
32-111
Benzo(a)anthracene
ug/kg
ND
1710
1290
75
25-117
Benzo(a)pyrene
ug/kg
ND
1710
1310
76
25-106
Benzo(b)fluoranthene
ug/kg
ND
1710
1280
74
24-110
Benzo(g,h,i)perylene
ug/kg
ND
1710
1230
72
19-112
Benzo(k)fluoranthene
ug/kg
ND
1710
1310
76
24-114
Benzoic Acid
ug/kg
ND
8580
5180
60
10-110
Benzyl alcohol
ug/kg
ND
3430
1890
55
24-106
bis(2-Chloroethoxy)methane
ug/kg
ND
1710
959
56
13-119
bis(2-Chloroethyl) ether
ug/kg
ND
1710
888
52
10-134
bis(2-Ethylhexyl)phthalate
ug/kg
ND
1710
1280
74
10-125
Butylbenzylphthalate
ug/kg
ND
1710
1250
73
18-110
Chrysene
ug/kg
ND
1710
1260
73
30-110
Di-n-butylphthalate
ug/kg
ND
1710
1180
69
19-112
Di-n-octylphthalate
ug/kg
ND
1710
1340
78
17-105
Dibenz(a,h)anthracene
ug/kg
ND
1710
1250
73
23-111
Dibenzofuran
ug/kg
ND
1710
1110
65
35-103
Diethylphthalate
ug/kg
ND
1710
1170
68
27-113
Dimethylphthalate
ug/kg
ND
1710
1070
62
26-111
Fluoranthene
ug/kg
ND
1710
1270
74
33-109
Fluorene
ug/kg
ND
1710
1190
69
32-113
Hexachloro-1,3-butadiene
ug/kg
ND
1710
846
49
16-116
Hexachlorobenzene
ug/kg
ND
1710
1160
68
27-120
Hexachlorocyclopentadiene
ug/kg
ND
1710
756
44
10-108
Hexachloroethane
ug/kg
ND
1710
847
49
10-117
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1710
1230
72
10-122
Isophorone
ug/kg
ND
1710
843
49
28-114
N-Nitroso-di-n-propylamine
ug/kg
ND
1710
907
53
27-113
N-Nitrosodimethylamine
ug/kg
ND
1710
1030
60
10-109
N-Nitrosodiphenylamine
ug/kg
ND
1710
1180
69
10-128
Naphthalene
ug/kg
ND
1710
911
53
25-110
Nitrobenzene
ug/kg
ND
1710
911
53
18-114
Pentachlorophenol
ug/kg
ND
3430
2020
59
10-122
Phenanthrene
ug/kg
ND
1710
1250
73
30-114
Phenol
ug/kg
ND
1710
886
52
11-102
Pyrene
ug/kg
ND
1710
1320
77
25-116
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
MATRIX SPIKE SAMPLE:
Parameter
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
2405959
Units
92404042001 Spike MS MS
Result Conc. Result % Rec
% Rec
Limits
%
74
27-110
%
55
30-110
%
52
13-110
%
54
23-110
%
54
22-110
%
92
28-110
SAMPLE DUPLICATE: 2405960
Parameter
Units
92404042001
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
1-Methylnaphthalene
ug/kg
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
2,4,5-Trichlorophenol
ug/kg
ND
ND
2,4,6-Trichlorophenol
ug/kg
ND
ND
2,4-Dichlorophenol
ug/kg
ND
ND
2,4-Dimethylphenol
ug/kg
ND
ND
2,4-Dinitrophenol
ug/kg
ND
ND
2,4-Dinitrotoluene
ug/kg
ND
ND
2,6-Dinitrotoluene
ug/kg
ND
ND
2-Chloronaphthalene
ug/kg
ND
ND
2-Chlorophenol
ug/kg
ND
ND
2-Methylnaphthalene
ug/kg
ND
ND
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
2-Nitroaniline
ug/kg
ND
ND
2-Nitrophenol
ug/kg
ND
ND
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
3,3'-Dichlorobenzidine
ug/kg
ND
ND
3-Nitroaniline
ug/kg
ND
ND
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
4-Bromophenylphenyl ether
ug/kg
ND
ND
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
4-Chloroaniline
ug/kg
ND
ND
4-Chlorophenylphenyl ether
ug/kg
ND
ND
4-Nitroaniline
ug/kg
ND
ND
4-Nitrophenol
ug/kg
ND
ND
Acenaphthene
ug/kg
ND
ND
Acenaphthylene
ug/kg
ND
ND
Aniline
ug/kg
ND
ND
Anthracene
ug/kg
ND
ND
Benzo(a)anthracene
ug/kg
ND
ND
Benzo(a)pyrene
ug/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
SAMPLE DUPLICATE: 2405960
Parameter
Units
92404042001
Result
Dup
Result
Benzo(b)fluoranthene
ug/kg
ND
ND
Benzo(g,h,i)perylene
ug/kg
ND
ND
Benzo(k)fluoranthene
ug/kg
ND
ND
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
ND
ND
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
ND
ND
Fluorene
ug/kg
ND
ND
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
ND
ND
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
ND
ND
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
ND
ND
2,4,6-Tribromophenol (S)
%
71
65
2-Fluorobiphenyl (S)
%
65
63
2-Fluorophenol (S)
%
56
46
Nitrobenzene-d5 (S)
%
60
57
Phenol-d6 (S)
%
60
55
Terphenyl-d14 (S)
%
92
87
RPD Qualifiers
8
3
18
4
7
3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
QC Batch: 437788 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 92404020002
METHOD BLANK: 2407202
Matrix:
Solid
Associated Lab Samples: 92404020002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.1
10/24/18 16:24 N2
Aliphatic (C19-C36)
mg/kg
ND
10.1
10/24/18 16:24 N2
Aromatic (C11-C22)
mg/kg
ND
10.1
10/24/18 16:24 N2
2-Bromonaphthalene (S)
%
74
40-140
10/24/18 16:24
2-Fluorobiphenyl (S)
%
73
40-140
10/24/18 16:24
Nonatriacontane (S)
%
93
40-140
10/24/18 16:24
o-Terphenyl (S)
%
63
40-140
10/24/18 16:24
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2407203
Units
Spike
Conc.
2407204
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec Max
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10.1
ND ND
80
52
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.4
10.8 ND
81
54
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.5
17.2 13.5
60
48
40-140 25 50 N2
2-Bromonaphthalene (S)
%
68
72
40-140
2-Fluorobiphenyl (S)
%
69
70
40-140
Nonatriacontane (S)
%
96
67
40-140
o-Terphenyl(S)
%
62
50
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 40

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
QC Batch: 437056 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92404020001, 92404020002
SAMPLE DUPLICATE: 2404276
92402976001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 0.11 ND
SAMPLE DUPLICATE: 2404277
92404033010 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 16.9 14.9 13
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 40

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
82 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2018 05:13 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 40

aceAnalytical
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[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 10200 ARTHUR DAVIS
Pace Project No.: 92404020
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92404020001
TANK
EPA 3546
437441
EPA 8015C Modified
437600
92404020002
POST EVACUATION 12'
MADEP EPH
437788
MADEP EPH
438266
92404020001
TANK
EPA 5030B
437454
EPA 8015C Modified
437503
92404020002
POST EVACUATION 12'
MADEP VPH
437522
MADEP VPH
437772
92404020002
POST EVACUATION 12'
EPA 3546
437473
EPA 8270D
437496
92404020002
POST EVACUATION 12'
EPA 5035A
437211
EPA 8260B
437228
92404020001
TANK
ASTM D2974-87
437056
92404020002
POST EVACUATION 12'
ASTM D2974-87
437056
Date: 10/25/2018 05:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 37 of 40

Document Name:
Document Revised: February 7, 2018
11�aceAaalPical n
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Fluntersvllle ❑— Raleigh❑ Mechanicsville❑
Sample Condition Client Name:Upon Receipt . Pro ect #: WO# 92404020
�.:.,:jt, .i 1.,.i/. /,,. j� I,,
Courier: ❑Fed Ex []UPS ❑USPS []Client ❑ ❑
����
Commercial Pace ❑Other: 111 111
924040�!0
Custody Seal Present? []Yes ❑No Seals Intact? ❑Yes [:]No
i
oatellnitlels Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bumble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes -QNo ❑N/A
QIR Gun ID: 92TO45 Type aiice: I�Wet ❑Blue ❑None
Cooler Temp (°Cj: Correction Factor: Add/Subtract (°C} 1
Temp should be above freezing to 6°t
Cooler Temp Corrected ('C): 05amples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soll (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or 5C (check maps)? Old samples originate from a foreign source (internationally,
Comments/Dlscrepancy,
Chain of Custody Present?
Elves
❑No
[]N/A
1,
Samples Arrived within Hold Time?
Dyes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
[]NO
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
❑No
❑N/A
4.
Sufficient Volume?
)]Yes
❑No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
[]Yes
❑Y-es
❑No
[]No
❑N/A
❑N/A
6,
Containers Intact?
❑Yes
❑No
❑NIA
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
[]No
❑NIA
&.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
❑Yes
�!
[]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
[]Yes
❑No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
❑ io
❑No
❑N/A
❑N/A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes []NO
a -
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: �f V l Date: {�
Project Manager SRF Review: Date: l
Page 38 of 40

Document Name:
Document Revised: February 7, 2018
_ � aceAr,alytieal
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
I
F•CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples,
EKceptians: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project WO# : 92404020
PM: NMG Due Date: 10/25/18
CLIENT: 92—CERT
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_ .. _ _ — _ _ pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservedon
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will tesent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 39 of 40

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Page 40 of 40

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 01, 2018
Chris Ward
ESP Associates
3475 Lakemont Boulevard
Fort Mill, SC 29708
RE: Project: MERIDALE
Pace Project No.: 92404510
Dear Chris Ward:
Enclosed are the analytical results for sample(s) received by the laboratory on October 23, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, p
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 56

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: MERIDALE
Pace Project No.: 92404510
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
South Carolina Certification M 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification M 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 56

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: MERIDALE
Pace Project No.: 92404510
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92404510001
MW-UST
Water
10/22/18 08:25
10/23/18 14:10
92404510002
WEST WALL
Solid
10/22/18 11:05
10/23/18 14:10
92404510003
NORTH WALL
Solid
10/22/18 11:20
10/23/18 14:10
92404510004
SOUTH WALL
Solid
10/22/18 11:35
10/23/18 14:10
92404510005
EAST WALL
Solid
10/22/18 13:20
10/23/18 14:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
MERIDALE
92404510
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92404510001
MW-UST
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 625.1
BPJ
58
PASI-C
SM 6200B
CL
16
PASI-C
92404510002
WEST WALL
EPA 8015C Modified
SEM
2
PASI-C
MADEP EPH
SEM
7
PASI-C
EPA 8015C Modified
CL
2
PASI-C
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92404510003
NORTH WALL
EPA 8015C Modified
SEM
2
PASI-C
MADEP EPH
SEM
7
PASI-C
EPA 8015C Modified
CL
2
PASI-C
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92404510004
SOUTH WALL
EPA 8015C Modified
SEM
2
PASI-C
MADEP EPH
SEM
7
PASI-C
EPA 8015C Modified
CL
2
PASI-C
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92404510005
EAST WALL
EPA 8015C Modified
SEM
2
PASI-C
MADEP EPH
SEM
7
PASI-C
EPA 8015C Modified
CL
2
PASI-C
EPA 8270D
BPJ
74
PASI-C
EPA 8260E
DLK
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: MW-UST
Lab ID:
92404510001
Collected:
10/22/18 08:25
Received: 10/23/18 14:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
MADEP EPH NC Water
Analytical
Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
ug/L
96.2
96.2
1
10/27/18 12:54
10/30/18 08:25
N2
Aliphatic (C19-C36)
ND
ug/L
96.2
96.2
1
10/27/18 12:54
10/30/18 08:25
N2
Aromatic (C11-C22)
ND
ug/L
96.2
96.2
1
10/27/18 12:54
10/30/18 08:25
N2
Surrogates
Nonatriacontane (S)
49
%
40-140
1
10/27/18 12:54
10/30/18 08:25
7194-86-7
o-Terphenyl (S)
41
%
40-140
1
10/27/18 12:54
10/30/18 08:25
84-15-1
2-Fluorobiphenyl (S)
60
%
40-140
1
10/27/18 12:54
10/30/18 08:25
321-60-8
2-Bromonaphthalene (S)
61
%
40-140
1
10/27/18 12:54
10/30/18 08:25
580-13-2
VPH NC Water
Analytical
Method: MADEP VPH
Aliphatic (C05-CO8)
ND
ug/L
50.0
50.0
1
10/26/18 22:53
N2
Aliphatic (C09-C12)
ND
ug/L
50.0
50.0
1
10/26/18 22:53
N2
Aliphatic(C09-C12) Adjusted
ND
ug/L
50.0
50.0
1
10/26/18 22:53
N2
Aromatic (C09-C10)
ND
ug/L
50.0
50.0
1
10/26/18 22:53
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
99
%
70-130
1
10/26/18 22:53
460-00-4
4-Bromofluorobenzene (PID) (S)
98
%
70-130
1
10/26/18 22:53
460-00-4
625 MSSV
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-ChIoro-3-methyl phenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
Date: 11/01/2018 03:43 PM
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
ND
ug/L
4.8
0.24
1
10/24/18 10:57
10/25/18 20:06
83-32-9
ND
ug/L
4.8
0.20
1
10/24/18 10:57
10/25/18 20:06
208-96-8
ND
ug/L
4.8
0.13
1
10/24/18 10:57
10/25/18 20:06
120-12-7
ND
ug/L
4.8
0.32
1
10/24/18 10:57
10/25/18 20:06
56-55-3
ND
ug/L
4.8
0.29
1
10/24/18 10:57
10/25/18 20:06
50-32-8
ND
ug/L
4.8
0.27
1
10/24/18 10:57
10/25/18 20:06
205-99-2
ND
ug/L
4.8
0.37
1
10/24/18 10:57
10/25/18 20:06
191-24-2
ND
ug/L
4.8
0.41
1
10/24/18 10:57
10/25/18 20:06
207-08-9
ND
ug/L
4.8
0.79
1
10/24/18 10:57
10/25/18 20:06
101-55-3
ND
ug/L
4.8
0.76
1
10/24/18 10:57
10/25/18 20:06
85-68-7
ND
ug/L
4.8
3.6
1
10/24/18 10:57
10/25/18 20:06
59-50-7
ND
ug/L
9.6
0.88
1
10/24/18 10:57
10/25/18 20:06
111-91-1
ND
ug/L
4.8
0.96
1
10/24/18 10:57
10/25/18 20:06
111-44-4
ND
ug/L
4.8
0.94
1
10/24/18 10:57
10/25/18 20:06
91-58-7
ND
ug/L
4.8
1.2
1
10/24/18 10:57
10/25/18 20:06
95-57-8
ND
ug/L
4.8
0.84
1
10/24/18 10:57
10/25/18 20:06
7005-72-3
ND
ug/L
4.8
0.20
1
10/24/18 10:57
10/25/18 20:06
218-01-9
ND
ug/L
4.8
0.53
1
10/24/18 10:57
10/25/18 20:06
53-70-3
ND
ug/L
24.0
2.0
1
10/24/18 10:57
10/25/18 20:06
91-94-1
ND
ug/L
4.8
1.6
1
10/24/18 10:57
10/25/18 20:06
120-83-2
ND
ug/L
4.8
0.56
1
10/24/18 10:57
10/25/18 20:06
84-66-2
ND
ug/L
9.6
1.2
1
10/24/18 10:57
10/25/18 20:06
105-67-9
ND
ug/L
4.8
0.73
1
10/24/18 10:57
10/25/18 20:06
131-11-3
ND
ug/L
4.8
0.72
1
10/24/18 10:57
10/25/18 20:06
84-74-2
ND
ug/L
19.2
2.5
1
10/24/18 10:57
10/25/18 20:06
534-52-1
ND
ug/L
48.1
8.7
1
10/24/18 10:57
10/25/18 20:06
51-28-5
ND
ug/L
4.8
0.87
1
10/24/18 10:57
10/25/18 20:06
121-14-2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: MW-UST Lab ID: 92404510001 Collected: 10/22/18 08:25 Received: 10/23/18 14:10 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
2,6-Dinitrotoluene
ND
ug/L
4.8
0.94
1
10/24/18 10:57
10/25/18 20:06
606-20-2
Di-n-octylphthalate
ND
ug/L
4.8
0.63
1
10/24/18 10:57
10/25/18 20:06
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
4.8
0.76
1
10/24/18 10:57
10/25/18 20:06
117-81-7
Fluoranthene
ND
ug/L
4.8
0.20
1
10/24/18 10:57
10/25/18 20:06
206-44-0
Fluorene
ND
ug/L
4.8
0.20
1
10/24/18 10:57
10/25/18 20:06
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
4.8
0.90
1
10/24/18 10:57
10/25/18 20:06
87-68-3
Hexachlorobenzene
ND
ug/L
4.8
0.69
1
10/24/18 10:57
10/25/18 20:06
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
9.6
0.85
1
10/24/18 10:57
10/25/18 20:06
77-47-4
Hexachloroethane
ND
ug/L
4.8
1.1
1
10/24/18 10:57
10/25/18 20:06
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
4.8
0.28
1
10/24/18 10:57
10/25/18 20:06
193-39-5
Isophorone
ND
ug/L
9.6
0.86
1
10/24/18 10:57
10/25/18 20:06
78-59-1
Naphthalene
ND
ug/L
4.8
0.33
1
10/24/18 10:57
10/25/18 20:06
91-20-3
Nitrobenzene
ND
ug/L
4.8
1.1
1
10/24/18 10:57
10/25/18 20:06
98-95-3
2-Nitrophenol
ND
ug/L
4.8
0.88
1
10/24/18 10:57
10/25/18 20:06
88-75-5
4-Nitrophenol
ND
ug/L
48.1
3.9
1
10/24/18 10:57
10/25/18 20:06
100-02-7
N-Nitrosodimethylamine
ND
ug/L
4.8
0.88
1
10/24/18 10:57
10/25/18 20:06
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
4.8
0.95
1
10/24/18 10:57
10/25/18 20:06
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
9.6
0.96
1
10/24/18 10:57
10/25/18 20:06
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
4.8
0.91
1
10/24/18 10:57
10/25/18 20:06
108-60-1
Pentachlorophenol
ND
ug/L
9.6
4.4
1
10/24/18 10:57
10/25/18 20:06
87-86-5
Phenanthrene
ND
ug/L
4.8
0.21
1
10/24/18 10:57
10/25/18 20:06
85-01-8
Phenol
ND
ug/L
4.8
1.8
1
10/24/18 10:57
10/25/18 20:06
108-95-2
Pyrene
ND
ug/L
4.8
0.18
1
10/24/18 10:57
10/25/18 20:06
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
4.8
0.94
1
10/24/18 10:57
10/25/18 20:06
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
9.6
1.2
1
10/24/18 10:57
10/25/18 20:06
88-06-2
Surrogates
Nitrobenzene-d5 (S)
75
%
10-120
1
10/24/18 10:57
10/25/18 20:06
4165-60-0
2-Fluorobiphenyl (S)
57
%
15-120
1
10/24/18 10:57
10/25/18 20:06
321-60-8
Terphenyl-d14 (S)
34
%
11-131
1
10/24/18 10:57
10/25/18 20:06
1718-51-0
Phenol-d6 (S)
22
%
10-120
1
10/24/18 10:57
10/25/18 20:06
13127-88-3
2-Fluorophenol (S)
29
%
10-120
1
10/24/18 10:57
10/25/18 20:06
367-12-4
2,4,6-Tribromophenol (S)
63
%
10-137
1
10/24/18 10:57
10/25/18 20:06
118-79-6
602 Volatiles by Method 6200
Analytical Method: SM
6200B
Benzene
ND
ug/L
1.0
1.0
1
10/28/18 16:04
71-43-2
Chlorobenzene
ND
ug/L
1.0
1.0
1
10/28/18 16:04
108-90-7
1,2-Dichlorobenzene
ND
ug/L
1.0
1.0
1
10/28/18 16:04
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1.0
1
10/28/18 16:04
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1.0
1
10/28/18 16:04
106-46-7
Diisopropyl ether
ND
ug/L
1.0
1.0
1
10/28/18 16:04
108-20-3
Ethylbenzene
ND
ug/L
1.0
1.0
1
10/28/18 16:04
100-41-4
Isopropylbenzene (Cumene)
ND
ug/L
1.0
1.0
1
10/28/18 16:04
98-82-8
Methyl-tert-butyl ether
ND
ug/L
1.0
1.0
1
10/28/18 16:04
1634-04-4
Naphthalene
ND
ug/L
2.0
2.0
1
10/28/18 16:04
91-20-3
Toluene
ND
ug/L
1.0
1.0
1
10/28/18 16:04
108-88-3
m&p-Xylene
ND
ug/L
2.0
2.0
1
10/28/18 16:04
179601-23-1
REPORT OF LABORATORY ANALYSIS
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Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: MW-UST
Lab ID:
92404510001
Collected:
10/22/18 08:25
Received:
10/23/18 14:10 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
602 Volatiles by Method 6200
Analytical
Method: SM 6200B
o-Xylene
ND
ug/L
1.0
1.0 1
10/28/18 16:04
95-47-6
Surrogates
4-Bromofluorobenzene (S)
96
%
70-130
1
10/28/18 16:04
460-00-4
1,2-Dichloroethane-d4 (S)
105
%
70-130
1
10/28/18 16:04
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
10/28/18 16:04
2037-26-5
Sample: WEST WALL
Lab ID:
92404510002
Collected:
10/22/18 11:05
Received:
10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL DF
Prepared
Analyzed
CAS No. Qual
8015 GCS THC-Diesel
Diesel Range Organics(C10
C28)
Surrogates
n-Pentacosane(S)
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
4-Bromophenylphenyl ether
Date: 11/01/2018 03:43 PM
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
ND mg/kg 6.1 5.5 1 10/23/1817:43 10/24/1817:21
69 % 33-129 1 10/23/1817:43 10/24/1817:21 629-99-2
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
ND
mg/kg
12.3
12.3
1
10/30/18 09:45
11/01/18 08:48
N2
ND
mg/kg
12.3
12.3
1
10/30/18 09:45
11/01/18 08:48
N2
ND
mg/kg
12.3
12.3
1
10/30/18 09:45
11/01/18 08:48
N2
22
%
40-140
1
10/30/18 09:45
11/01/18 08:48
7194-86-7
S2
26
%
40-140
1
10/30/18 09:45
11/01/18 08:48
84-15-1
S2
82
%
40-140
1
10/30/18 09:45
11/01/18 08:48
321-60-8
84
%
40-140
1
10/30/18 09:45
11/01/18 08:48
580-13-2
Analytical
Method: EPA 8015C Modified Preparation Method: EPA 5030E
ND
mg/kg
8.5
8.5
1
10/24/18 02:38
10/31/18 01:47
96
%
63-130
1
10/24/18 02:38
10/31 /18 01:47
460-00-4
Analytical
Method: EPA 8270D Preparation Method:
EPA
3546
ND
ug/kg
408
94.0
1
10/24/1817:24
10/26/1819:01
83-32-9
ND
ug/kg
408
96.5
1
10/24/1817:24
10/26/1819:01
208-96-8
ND
ug/kg
408
110
1
10/24/1817:24
10/26/1819:01
62-53-3
ND
ug/kg
408
91.6
1
10/24/1817:24
10/26/1819:01
120-12-7
ND
ug/kg
408
75.5
1
10/24/1817:24
10/26/1819:01
56-55-3
ND
ug/kg
408
77.9
1
10/24/1817:24
10/26/1819:01
50-32-8
ND
ug/kg
408
70.5
1
10/24/1817:24
10/26/1819:01
205-99-2
ND
ug/kg
408
104
1
10/24/1817:24
10/26/1819:01
191-24-2
ND
ug/kg
408
80.4
1
10/24/1817:24
10/26/1819:01
207-08-9
ND
ug/kg
2040
74.2
1
10/24/1817:24
10/26/1819:01
65-85-0
ND
ug/kg
817
81.7
1
10/24/1817:24
10/26/1819:01
100-51-6
ND
ug/kg
408
74.2
1
10/24/1817:24
10/26/1819:01
101-55-3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 7 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: WEST WALL Lab ID: 92404510002 Collected: 10/22/18 11:05 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Butylbenzylphthalate
ND
ug/kg
408
86.6
1
10/24/18 17:24
10/26/18 19:01
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
817
84.1
1
10/24/18 17:24
10/26/18 19:01
59-50-7
4-Chloroaniline
ND
ug/kg
2040
114
1
10/24/18 17:24
10/26/18 19:01
106-47-8 L2
bis(2-Chloroethoxy)methane
ND
ug/kg
408
95.3
1
10/24/18 17:24
10/26/18 19:01
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
408
104
1
10/24/18 17:24
10/26/18 19:01
111-44-4
2-Chloronaphthalene
ND
ug/kg
408
80.4
1
10/24/18 17:24
10/26/18 19:01
91-58-7
2-Chlorophenol
ND
ug/kg
408
ill
1
10/24/18 17:24
10/26/18 19:01
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
408
84.1
1
10/24/18 17:24
10/26/18 19:01
7005-72-3
Chrysene
ND
ug/kg
408
54.4
1
10/24/18 17:24
10/26/18 19:01
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
408
86.6
1
10/24/18 17:24
10/26/18 19:01
53-70-3
Dibenzofuran
ND
ug/kg
408
66.8
1
10/24/18 17:24
10/26/18 19:01
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
408
109
1
10/24/18 17:24
10/26/18 19:01
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
408
92.8
1
10/24/18 17:24
10/26/18 19:01
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
408
115
1
10/24/18 17:24
10/26/18 19:01
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2040
89.1
1
10/24/18 17:24
10/26/18 19:01
91-94-1
2,4-Dichlorophenol
ND
ug/kg
408
89.1
1
10/24/18 17:24
10/26/18 19:01
120-83-2
Diethylphthalate
ND
ug/kg
408
63.1
1
10/24/18 17:24
10/26/18 19:01
84-66-2
2,4-Dimethylphenol
ND
ug/kg
408
161
1
10/24/18 17:24
10/26/18 19:01
105-67-9
Dimethylphthalate
ND
ug/kg
408
82.9
1
10/24/18 17:24
10/26/18 19:01
131-11-3
Di-n-butylphthalate
ND
ug/kg
408
66.8
1
10/24/18 17:24
10/26/18 19:01
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
817
81.7
1
10/24/18 17:24
10/26/18 19:01
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2040
66.8
1
10/24/18 17:24
10/26/18 19:01
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
408
76.7
1
10/24/18 17:24
10/26/18 19:01
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
408
85.4
1
10/24/18 17:24
10/26/18 19:01
606-20-2
Di-n-octylphthalate
ND
ug/kg
408
85.4
1
10/24/18 17:24
10/26/18 19:01
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
408
ill
1
10/24/18 17:24
10/26/18 19:01
117-81-7
Fluoranthene
ND
ug/kg
408
59.4
1
10/24/18 17:24
10/26/18 19:01
206-44-0
Fluorene
ND
ug/kg
408
84.1
1
10/24/18 17:24
10/26/18 19:01
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
408
70.5
1
10/24/18 17:24
10/26/18 19:01
87-68-3
Hexachlorobenzene
ND
ug/kg
408
52.0
1
10/24/18 17:24
10/26/18 19:01
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
408
75.5
1
10/24/18 17:24
10/26/18 19:01
77-47-4
Hexachloroethane
ND
ug/kg
408
108
1
10/24/18 17:24
10/26/18 19:01
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
408
84.1
1
10/24/18 17:24
10/26/18 19:01
193-39-5
Isophorone
ND
ug/kg
408
91.6
1
10/24/18 17:24
10/26/18 19:01
78-59-1
1-Methylnaphthalene
ND
ug/kg
408
106
1
10/24/18 17:24
10/26/18 19:01
90-12-0
2-Methylnaphthalene
ND
ug/kg
408
87.8
1
10/24/18 17:24
10/26/18 19:01
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
408
124
1
10/24/18 17:24
10/26/18 19:01
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
408
161
1
10/24/18 17:24
10/26/18 19:01
15831-10-4
Naphthalene
ND
ug/kg
408
100
1
10/24/18 17:24
10/26/18 19:01
91-20-3
2-Nitroaniline
ND
ug/kg
2040
126
1
10/24/18 17:24
10/26/18 19:01
88-74-4
3-Nitroaniline
ND
ug/kg
2040
ill
1
10/24/18 17:24
10/26/18 19:01
99-09-2
4-Nitroaniline
ND
ug/kg
817
115
1
10/24/18 17:24
10/26/18 19:01
100-01-6
Nitrobenzene
ND
ug/kg
408
ill
1
10/24/18 17:24
10/26/18 19:01
98-95-3
2-Nitrophenol
ND
ug/kg
408
99.0
1
10/24/18 17:24
10/26/18 19:01
88-75-5
4-Nitrophenol
ND
ug/kg
2040
73.0
1
10/24/18 17:24
10/26/18 19:01
100-02-7
REPORT OF LABORATORY ANALYSIS
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Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 56

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: WEST WALL Lab ID: 92404510002 Collected: 10/22/18 11:05 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
N-Nitrosodimethylamine
ND
ug/kg
408
132
1
10/24/18 17:24
10/26/18 19:01
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
408
77.9
1
10/24/18 17:24
10/26/18 19:01
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
408
121
1
10/24/18 17:24
10/26/18 19:01
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
408
109
1
10/24/18 17:24
10/26/18 19:01
108-60-1
Pentachlorophenol
ND
ug/kg
2040
74.2
1
10/24/18 17:24
10/26/18 19:01
87-86-5
Phenanthrene
ND
ug/kg
408
68.0
1
10/24/18 17:24
10/26/18 19:01
85-01-8
Phenol
ND
ug/kg
408
122
1
10/24/18 17:24
10/26/18 19:01
108-95-2
Pyrene
ND
ug/kg
408
69.3
1
10/24/18 17:24
10/26/18 19:01
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
408
79.2
1
10/24/18 17:24
10/26/18 19:01
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
408
126
1
10/24/18 17:24
10/26/18 19:01
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
408
90.3
1
10/24/18 17:24
10/26/18 19:01
88-06-2
Surrogates
Nitrobenzene-d5 (S)
80
%
23-110
1
10/24/18 17:24
10/26/18 19:01
4165-60-0
2-Fluorobiphenyl (S)
67
%
30-110
1
10/24/18 17:24
10/26/18 19:01
321-60-8
Terphenyl-d14 (S)
87
%
28-110
1
10/24/18 17:24
10/26/18 19:01
1718-51-0
Phenol-d6 (S)
62
%
22-110
1
10/24/18 17:24
10/26/18 19:01
13127-88-3
2-Fluorophenol (S)
62
%
13-110
1
10/24/18 17:24
10/26/18 19:01
367-12-4
2,4,6-Tribromophenol (S)
71
%
27-110
1
10/24/18 17:24
10/26/18 19:01
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
29.5J
ug/kg
120
12.0
1
10/24/18 09:57
10/24/18 18:02
67-64-1
Benzene
ND
ug/kg
6.0
1.9
1
10/24/18 09:57
10/24/18 18:02
71-43-2
Bromobenzene
ND
ug/kg
6.0
2.4
1
10/24/18 09:57
10/24/18 18:02
108-86-1
Bromochloromethane
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
74-97-5
Bromodichloromethane
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
75-27-4
Bromoform
ND
ug/kg
6.0
2.8
1
10/24/18 09:57
10/24/18 18:02
75-25-2
Bromomethane
ND
ug/kg
12.0
3.0
1
10/24/18 09:57
10/24/18 18:02
74-83-9
2-Butanone (MEK)
ND
ug/kg
120
3.5
1
10/24/18 09:57
10/24/18 18:02
78-93-3
n-Butylbenzene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
104-51-8
sec-Butylbenzene
ND
ug/kg
6.0
1.9
1
10/24/18 09:57
10/24/18 18:02
135-98-8
tert-Butyl benzene
ND
ug/kg
6.0
2.4
1
10/24/18 09:57
10/24/18 18:02
98-06-6
Carbon tetrachloride
ND
ug/kg
6.0
3.1
1
10/24/18 09:57
10/24/18 18:02
56-23-5
Chlorobenzene
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
108-90-7
Chloroethane
ND
ug/kg
12.0
2.9
1
10/24/18 09:57
10/24/18 18:02
75-00-3
Chloroform
ND
ug/kg
6.0
1.9
1
10/24/18 09:57
10/24/18 18:02
67-66-3
Chloromethane
ND
ug/kg
12.0
2.9
1
10/24/18 09:57
10/24/18 18:02
74-87-3
2-Chlorotoluene
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
95-49-8
4-Chlorotoluene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.0
4.3
1
10/24/18 09:57
10/24/18 18:02
96-12-8
Dibromochloromethane
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
106-93-4
Dibromomethane
ND
ug/kg
6.0
3.0
1
10/24/18 09:57
10/24/18 18:02
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.0
2.4
1
10/24/18 09:57
10/24/18 18:02
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
106-46-7
REPORT OF LABORATORY ANALYSIS
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Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: WEST WALL Lab ID: 92404510002 Collected: 10/22/18 11:05 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Dichlorodifluoromethane
ND
ug/kg
12.0
4.3
1
10/24/18 09:57
10/24/18 18:02
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.0
1.8
1
10/24/18 09:57
10/24/18 18:02
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.0
2.7
1
10/24/18 09:57
10/24/18 18:02
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.0
1.7
1
10/24/18 09:57
10/24/18 18:02
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.0
1.8
1
10/24/18 09:57
10/24/18 18:02
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.0
1.8
1
10/24/18 09:57
10/24/18 18:02
10061-02-6
Diisopropyl ether
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
108-20-3
Ethylbenzene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.0
2.4
1
10/24/18 09:57
10/24/18 18:02
87-68-3
2-Hexanone
ND
ug/kg
60.2
4.7
1
10/24/18 09:57
10/24/18 18:02
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
99-87-6
Methylene Chloride
33.6
ug/kg
24.1
3.6
1
10/24/18 09:57
10/24/18 18:02
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
60.2
4.5
1
10/24/18 09:57
10/24/18 18:02
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.0
1.8
1
10/24/18 09:57
10/24/18 18:02
1634-04-4
Naphthalene
ND
ug/kg
6.0
1.4
1
10/24/18 09:57
10/24/18 18:02
91-20-3
n-Propylbenzene
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
103-65-1
Styrene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
6.0
2.5
1
10/24/18 09:57
10/24/18 18:02
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
79-34-5
Tetrachloroethene
ND
ug/kg
6.0
2.0
1
10/24/18 09:57
10/24/18 18:02
127-18-4
Toluene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
6.0
2.7
1
10/24/18 09:57
10/24/18 18:02
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
6.0
1.9
1
10/24/18 09:57
10/24/18 18:02
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
6.0
2.5
1
10/24/18 09:57
10/24/18 18:02
79-00-5
Trichloroethene
ND
ug/kg
6.0
2.5
1
10/24/18 09:57
10/24/18 18:02
79-01-6
Trichlorofluoromethane
ND
ug/kg
6.0
2.7
1
10/24/18 09:57
10/24/18 18:02
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
6.0
1.9
1
10/24/18 09:57
10/24/18 18:02
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
6.0
2.4
1
10/24/18 09:57
10/24/18 18:02
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
6.0
2.2
1
10/24/18 09:57
10/24/18 18:02
108-67-8
Vinyl acetate
ND
ug/kg
60.2
10.6
1
10/24/18 09:57
10/24/18 18:02
108-05-4
Vinyl chloride
ND
ug/kg
12.0
2.2
1
10/24/18 09:57
10/24/18 18:02
75-01-4
Xylene (Total)
ND
ug/kg
12.0
4.3
1
10/24/18 09:57
10/24/18 18:02
1330-20-7
m&p-Xylene
ND
ug/kg
12.0
4.3
1
10/24/18 09:57
10/24/18 18:02
179601-23-1
o-Xylene
ND
ug/kg
6.0
2.3
1
10/24/18 09:57
10/24/18 18:02
95-47-6
Surrogates
Toluene-d8 (S)
100
%
70-130
1
10/24/18 09:57
10/24/18 18:02
2037-26-5
4-Bromofluorobenzene (S)
90
%
70-130
1
10/24/18 09:57
10/24/18 18:02
460-00-4
REPORT OF LABORATORY ANALYSIS
C9
L1
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Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 56

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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: WEST WALL Lab ID: 92404510002 Collected: 10/22/18 11:05 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Surrogates
1,2-Dichloroethane-d4 (S) 101 % 70-132 1 10/24/18 09:57 10/24/18 18:02 17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.6 % 0.10 0.10 1 10/23/18 17:22
Sample: NORTH WALL Lab ID: 92404510003 Collected: 10/22/18 11:20 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane(S)
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Benzyl alcohol
Date: 11/01/2018 03:43 PM
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
ND mg/kg 6.2 5.6 1 10/23/1817:43 10/24/1817:45
77
%
33-129
1
10/23/1817:43
10/24/1817:45
629-99-2
Analytical
Method: MADEP EPH Preparation Method:
MADEP EPH
ND
mg/kg
12.1
12.1 1
10/30/18 09:45
11/01/18 09:16
N2
ND
mg/kg
12.1
12.1 1
10/30/18 09:45
11/01/18 09:16
N2
ND
mg/kg
12.1
12.1 1
10/30/18 09:45
11/01/18 09:16
N2
55
%
40-140
1
10/30/18 09:45
11/01/18 09:16
7194-86-7
77
%
40-140
1
10/30/18 09:45
11/01/18 09:16
84-15-1
97
%
40-140
1
10/30/18 09:45
11/01/18 09:16
321-60-8
100
%
40-140
1
10/30/18 09:45
11/01/18 09:16
580-13-2
Analytical
Method: EPA 8015C Modified Preparation Method: EPA 5030B
ND
mg/kg
7.8
7.8 1
10/24/18 02:38
10/31/18 02:16
100 % 63-130 1 10/24/18 02:38 10/31 /18 02:16 460-00-4
Analytical Method: EPA 8270D Preparation Method: EPA 3546
ND
ug/kg
406
93.4
1
10/24/1817:24
10/26/1819:30
83-32-9
ND
ug/kg
406
95.8
1
10/24/1817:24
10/26/1819:30
208-96-8
ND
ug/kg
406
109
1
10/24/1817:24
10/26/1819:30
62-53-3
ND
ug/kg
406
90.9
1
10/24/1817:24
10/26/1819:30
120-12-7
ND
ug/kg
406
75.0
1
10/24/1817:24
10/26/1819:30
56-55-3
ND
ug/kg
406
77.4
1
10/24/1817:24
10/26/1819:30
50-32-8
ND
ug/kg
406
70.0
1
10/24/1817:24
10/26/1819:30
205-99-2
ND
ug/kg
406
103
1
10/24/1817:24
10/26/1819:30
191-24-2
ND
ug/kg
406
79.9
1
10/24/1817:24
10/26/1819:30
207-08-9
ND
ug/kg
2030
73.7
1
10/24/1817:24
10/26/1819:30
65-85-0
ND
ug/kg
811
81.1
1
10/24/1817:24
10/26/1819:30
100-51-6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 11 of 56

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: NORTH WALL Lab ID: 92404510003 Collected: 10/22/18 11:20 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
4-Bromophenylphenyl ether
ND
ug/kg
406
73.7
1
10/24/18 17:24
10/26/18 19:30
101-55-3
Butylbenzylphthalate
ND
ug/kg
406
86.0
1
10/24/18 17:24
10/26/18 19:30
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
811
83.6
1
10/24/18 17:24
10/26/18 19:30
59-50-7
4-Chloroaniline
ND
ug/kg
2030
113
1
10/24/18 17:24
10/26/18 19:30
106-47-8 L2
bis(2-Chloroethoxy)methane
ND
ug/kg
406
94.6
1
10/24/18 17:24
10/26/18 19:30
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
406
103
1
10/24/18 17:24
10/26/18 19:30
111-44-4
2-Chloronaphthalene
ND
ug/kg
406
79.9
1
10/24/18 17:24
10/26/18 19:30
91-58-7
2-Chlorophenol
ND
ug/kg
406
ill
1
10/24/18 17:24
10/26/18 19:30
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
406
83.6
1
10/24/18 17:24
10/26/18 19:30
7005-72-3
Chrysene
ND
ug/kg
406
54.1
1
10/24/18 17:24
10/26/18 19:30
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
406
86.0
1
10/24/18 17:24
10/26/18 19:30
53-70-3
Dibenzofuran
ND
ug/kg
406
66.4
1
10/24/18 17:24
10/26/18 19:30
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
406
108
1
10/24/18 17:24
10/26/18 19:30
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
406
92.2
1
10/24/18 17:24
10/26/18 19:30
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
406
114
1
10/24/18 17:24
10/26/18 19:30
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2030
88.5
1
10/24/18 17:24
10/26/18 19:30
91-94-1
2,4-Dichlorophenol
ND
ug/kg
406
88.5
1
10/24/18 17:24
10/26/18 19:30
120-83-2
Diethylphthalate
ND
ug/kg
406
62.7
1
10/24/18 17:24
10/26/18 19:30
84-66-2
2,4-Dimethylphenol
ND
ug/kg
406
160
1
10/24/18 17:24
10/26/18 19:30
105-67-9
Dimethylphthalate
ND
ug/kg
406
82.3
1
10/24/18 17:24
10/26/18 19:30
131-11-3
Di-n-butylphthalate
ND
ug/kg
406
66.4
1
10/24/18 17:24
10/26/18 19:30
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
811
81.1
1
10/24/18 17:24
10/26/18 19:30
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2030
66.4
1
10/24/18 17:24
10/26/18 19:30
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
406
76.2
1
10/24/18 17:24
10/26/18 19:30
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
406
84.8
1
10/24/18 17:24
10/26/18 19:30
606-20-2
Di-n-octylphthalate
ND
ug/kg
406
84.8
1
10/24/18 17:24
10/26/18 19:30
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
406
ill
1
10/24/18 17:24
10/26/18 19:30
117-81-7
Fluoranthene
ND
ug/kg
406
59.0
1
10/24/18 17:24
10/26/18 19:30
206-44-0
Fluorene
ND
ug/kg
406
83.6
1
10/24/18 17:24
10/26/18 19:30
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
406
70.0
1
10/24/18 17:24
10/26/18 19:30
87-68-3
Hexachlorobenzene
ND
ug/kg
406
51.6
1
10/24/18 17:24
10/26/18 19:30
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
406
75.0
1
10/24/18 17:24
10/26/18 19:30
77-47-4
Hexachloroethane
ND
ug/kg
406
107
1
10/24/18 17:24
10/26/18 19:30
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
406
83.6
1
10/24/18 17:24
10/26/18 19:30
193-39-5
Isophorone
ND
ug/kg
406
90.9
1
10/24/18 17:24
10/26/18 19:30
78-59-1
1-Methylnaphthalene
ND
ug/kg
406
106
1
10/24/18 17:24
10/26/18 19:30
90-12-0
2-Methylnaphthalene
ND
ug/kg
406
87.2
1
10/24/18 17:24
10/26/18 19:30
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
406
123
1
10/24/18 17:24
10/26/18 19:30
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
406
160
1
10/24/18 17:24
10/26/18 19:30
15831-10-4
Naphthalene
ND
ug/kg
406
99.5
1
10/24/18 17:24
10/26/18 19:30
91-20-3
2-Nitroaniline
ND
ug/kg
2030
125
1
10/24/18 17:24
10/26/18 19:30
88-74-4
3-Nitroaniline
ND
ug/kg
2030
ill
1
10/24/18 17:24
10/26/18 19:30
99-09-2
4-Nitroaniline
ND
ug/kg
811
114
1
10/24/18 17:24
10/26/18 19:30
100-01-6
Nitrobenzene
ND
ug/kg
406
ill
1
10/24/18 17:24
10/26/18 19:30
98-95-3
2-Nitrophenol
ND
ug/kg
406
98.3
1
10/24/18 17:24
10/26/18 19:30
88-75-5
REPORT OF LABORATORY ANALYSIS
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Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: NORTH WALL Lab ID: 92404510003 Collected: 10/22/18 11:20 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
4-Nitrophenol
ND
ug/kg
2030
72.5
1
10/24/18 17:24
10/26/18 19:30
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
406
131
1
10/24/18 17:24
10/26/18 19:30
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
406
77.4
1
10/24/18 17:24
10/26/18 19:30
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
406
120
1
10/24/18 17:24
10/26/18 19:30
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
406
108
1
10/24/18 17:24
10/26/18 19:30
108-60-1
Pentachlorophenol
ND
ug/kg
2030
73.7
1
10/24/18 17:24
10/26/18 19:30
87-86-5
Phenanthrene
ND
ug/kg
406
67.6
1
10/24/18 17:24
10/26/18 19:30
85-01-8
Phenol
ND
ug/kg
406
122
1
10/24/18 17:24
10/26/18 19:30
108-95-2
Pyrene
ND
ug/kg
406
68.8
1
10/24/18 17:24
10/26/18 19:30
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
406
78.6
1
10/24/18 17:24
10/26/18 19:30
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
406
125
1
10/24/18 17:24
10/26/18 19:30
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
406
89.7
1
10/24/18 17:24
10/26/18 19:30
88-06-2
Surrogates
Nitrobenzene-d5 (S)
73
%
23-110
1
10/24/18 17:24
10/26/18 19:30
4165-60-0
2-Fluorobiphenyl (S)
60
%
30-110
1
10/24/18 17:24
10/26/18 19:30
321-60-8
Terphenyl-d14 (S)
87
%
28-110
1
10/24/18 17:24
10/26/18 19:30
1718-51-0
Phenol-d6 (S)
60
%
22-110
1
10/24/18 17:24
10/26/18 19:30
13127-88-3
2-Fluorophenol (S)
59
%
13-110
1
10/24/18 17:24
10/26/18 19:30
367-12-4
2,4,6-Tribromophenol (S)
66
%
27-110
1
10/24/18 17:24
10/26/18 19:30
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
ND
ug/kg
137
13.7
1
10/24/18 09:57
10/24/18 18:41
67-64-1
Benzene
ND
ug/kg
6.8
2.2
1
10/24/18 09:57
10/24/18 18:41
71-43-2
Bromobenzene
ND
ug/kg
6.8
2.7
1
10/24/18 09:57
10/24/18 18:41
108-86-1
Bromochloromethane
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
74-97-5
Bromodichloromethane
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
75-27-4
Bromoform
ND
ug/kg
6.8
3.1
1
10/24/18 09:57
10/24/18 18:41
75-25-2
Bromomethane
ND
ug/kg
13.7
3.4
1
10/24/18 09:57
10/24/18 18:41
74-83-9
2-Butanone (MEK)
ND
ug/kg
137
4.0
1
10/24/18 09:57
10/24/18 18:41
78-93-3
n-Butylbenzene
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
104-51-8
sec-Butylbenzene
ND
ug/kg
6.8
2.2
1
10/24/18 09:57
10/24/18 18:41
135-98-8
tert-Butyl benzene
ND
ug/kg
6.8
2.7
1
10/24/18 09:57
10/24/18 18:41
98-06-6
Carbon tetrachloride
ND
ug/kg
6.8
3.5
1
10/24/18 09:57
10/24/18 18:41
56-23-5
Chlorobenzene
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
108-90-7
Chloroethane
ND
ug/kg
13.7
3.3
1
10/24/18 09:57
10/24/18 18:41
75-00-3
Chloroform
ND
ug/kg
6.8
2.2
1
10/24/18 09:57
10/24/18 18:41
67-66-3
Chloromethane
ND
ug/kg
13.7
3.3
1
10/24/18 09:57
10/24/18 18:41
74-87-3
2-Chlorotoluene
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
95-49-8
4-Chlorotoluene
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.8
4.9
1
10/24/18 09:57
10/24/18 18:41
96-12-8
Dibromochloromethane
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
106-93-4
Dibromomethane
ND
ug/kg
6.8
3.4
1
10/24/18 09:57
10/24/18 18:41
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.8
2.7
1
10/24/18 09:57
10/24/18 18:41
541-73-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: NORTH WALL
Lab ID:
92404510003
Collected:
10/22/18
11:20
Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260/5035A Volatile Organics
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
1,4-Dichlorobenzene
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
106-46-7
Dichlorodifluoromethane
ND
ug/kg
13.7
4.9
1
10/24/18 09:57
10/24/18 18:41
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.8
2.0
1
10/24/18 09:57
10/24/18 18:41
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.8
3.0
1
10/24/18 09:57
10/24/18 18:41
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.8
1.9
1
10/24/18 09:57
10/24/18 18:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.8
2.0
1
10/24/18 09:57
10/24/18 18:41
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.8
2.0
1
10/24/18 09:57
10/24/18 18:41
10061-02-6
Diisopropyl ether
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
108-20-3
Ethylbenzene
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.8
2.7
1
10/24/18 09:57
10/24/18 18:41
87-68-3
2-Hexanone
ND
ug/kg
68.3
5.3
1
10/24/18 09:57
10/24/18 18:41
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
99-87-6
Methylene Chloride
6.7J
ug/kg
27.3
4.1
1
10/24/18 09:57
10/24/18 18:41
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
68.3
5.1
1
10/24/18 09:57
10/24/18 18:41
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.8
2.0
1
10/24/18 09:57
10/24/18 18:41
1634-04-4
Naphthalene
ND
ug/kg
6.8
1.6
1
10/24/18 09:57
10/24/18 18:41
91-20-3
n-Propylbenzene
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
103-65-1
Styrene
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
6.8
2.9
1
10/24/18 09:57
10/24/18 18:41
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
79-34-5
Tetrachloroethene
ND
ug/kg
6.8
2.3
1
10/24/18 09:57
10/24/18 18:41
127-18-4 L1
Toluene
2.8J
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
6.8
3.0
1
10/24/18 09:57
10/24/18 18:41
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
6.8
2.2
1
10/24/18 09:57
10/24/18 18:41
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
6.8
2.9
1
10/24/18 09:57
10/24/18 18:41
79-00-5
Trichloroethene
ND
ug/kg
6.8
2.9
1
10/24/18 09:57
10/24/18 18:41
79-01-6
Trichlorofluoromethane
ND
ug/kg
6.8
3.0
1
10/24/18 09:57
10/24/18 18:41
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
6.8
2.2
1
10/24/18 09:57
10/24/18 18:41
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
6.8
2.7
1
10/24/18 09:57
10/24/18 18:41
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
6.8
2.5
1
10/24/18 09:57
10/24/18 18:41
108-67-8
Vinyl acetate
ND
ug/kg
68.3
12.0
1
10/24/18 09:57
10/24/18 18:41
108-05-4
Vinyl chloride
ND
ug/kg
13.7
2.5
1
10/24/18 09:57
10/24/18 18:41
75-01-4
Xylene (Total)
ND
ug/kg
13.7
4.9
1
10/24/18 09:57
10/24/18 18:41
1330-20-7
m&p-Xylene
ND
ug/kg
13.7
4.9
1
10/24/18 09:57
10/24/18 18:41
179601-23-1
o-Xylene
ND
ug/kg
6.8
2.6
1
10/24/18 09:57
10/24/18 18:41
95-47-6
Surrogates
Toluene-d8 (S)
99
%
70-130
1
10/24/18 09:57
10/24/18 18:41
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: NORTH WALL Lab ID: 92404510003 Collected: 10/22/18 11:20 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Surrogates
4-Bromofluorobenzene (S) 91 % 70-130 1 10/24/18 09:57 10/24/18 18:41 460-00-4
1,2-Dichloroethane-d4 (S) 106 % 70-132 1 10/24/18 09:57 10/24/18 18:41 17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.6 % 0.10 0.10 1 10/23/18 17:22
Sample: SOUTH WALL Lab ID: 92404510004 Collected: 10/22/18 11:35 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane(S)
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzoic Acid
Date: 11/01/2018 03:43 PM
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
ND mg/kg 6.1 5.5 1 10/23/1817:43 10/24/1817:45
66
%
33-129
1
10/23/1817:43
10/24/1817:45
629-99-2
Analytical
Method: MADEP EPH Preparation Method:
MADEP EPH
ND
mg/kg
12.4
12.4
1
10/30/18 09:45
11/01/18 09:43
N2
ND
mg/kg
12.4
12.4
1
10/30/18 09:45
11/01/18 09:43
N2
ND
mg/kg
12.4
12.4
1
10/30/18 09:45
11/01/18 09:43
N2
58
%
40-140
1
10/30/18 09:45
11/01/18 09:43
7194-86-7
63
%
40-140
1
10/30/18 09:45
11/01/18 09:43
84-15-1
88
%
40-140
1
10/30/18 09:45
11/01/18 09:43
321-60-8
90
%
40-140
1
10/30/18 09:45
11/01/18 09:43
580-13-2
Analytical
Method: EPA 8015C Modified Preparation Method: EPA 5030B
ND
mg/kg
7.2
7.2
1
10/24/18 02:38
10/31/18 02:46
97
%
63-130
1
10/24/18 02:38
10/31 /18 02:46
460-00-4
Analytical
Method: EPA 8270D Preparation Method:
EPA
3546
ND
ug/kg
413
95.1
1
10/24/18 17:24
10/26/18 20:00
83-32-9
ND
ug/kg
413
97.6
1
10/24/18 17:24
10/26/18 20:00
208-96-8
ND
ug/kg
413
ill
1
10/24/18 17:24
10/26/18 20:00
62-53-3
ND
ug/kg
413
92.6
1
10/24/18 17:24
10/26/18 20:00
120-12-7
ND
ug/kg
413
76.3
1
10/24/18 17:24
10/26/18 20:00
56-55-3
ND
ug/kg
413
78.8
1
10/24/18 17:24
10/26/18 20:00
50-32-8
ND
ug/kg
413
71.3
1
10/24/18 17:24
10/26/18 20:00
205-99-2
ND
ug/kg
413
105
1
10/24/18 17:24
10/26/18 20:00
191-24-2
ND
ug/kg
413
81.3
1
10/24/18 17:24
10/26/18 20:00
207-08-9
ND
ug/kg
2060
75.1
1
10/24/18 17:24
10/26/18 20:00
65-85-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: SOUTH WALL Lab ID: 92404510004 Collected: 10/22/18 11:35 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Benzyl alcohol
ND
ug/kg
826
82.6
1
10/24/18 17:24
10/26/18 20:00
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
413
75.1
1
10/24/18 17:24
10/26/18 20:00
101-55-3
Butylbenzylphthalate
ND
ug/kg
413
87.6
1
10/24/18 17:24
10/26/18 20:00
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
826
85.1
1
10/24/18 17:24
10/26/18 20:00
59-50-7
4-Chloroaniline
ND
ug/kg
2060
115
1
10/24/18 17:24
10/26/18 20:00
106-47-8 L2
bis(2-Chloroethoxy)methane
ND
ug/kg
413
96.4
1
10/24/18 17:24
10/26/18 20:00
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
413
105
1
10/24/18 17:24
10/26/18 20:00
111-44-4
2-Chloronaphthalene
ND
ug/kg
413
81.3
1
10/24/18 17:24
10/26/18 20:00
91-58-7
2-Chlorophenol
ND
ug/kg
413
113
1
10/24/18 17:24
10/26/18 20:00
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
413
85.1
1
10/24/18 17:24
10/26/18 20:00
7005-72-3
Chrysene
ND
ug/kg
413
55.1
1
10/24/18 17:24
10/26/18 20:00
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
413
87.6
1
10/24/18 17:24
10/26/18 20:00
53-70-3
Dibenzofuran
ND
ug/kg
413
67.6
1
10/24/18 17:24
10/26/18 20:00
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
413
110
1
10/24/18 17:24
10/26/18 20:00
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
413
93.9
1
10/24/18 17:24
10/26/18 20:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
413
116
1
10/24/18 17:24
10/26/18 20:00
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2060
90.1
1
10/24/18 17:24
10/26/18 20:00
91-94-1
2,4-Dichlorophenol
ND
ug/kg
413
90.1
1
10/24/18 17:24
10/26/18 20:00
120-83-2
Diethylphthalate
ND
ug/kg
413
63.8
1
10/24/18 17:24
10/26/18 20:00
84-66-2
2,4-Dimethylphenol
ND
ug/kg
413
163
1
10/24/18 17:24
10/26/18 20:00
105-67-9
Dimethylphthalate
ND
ug/kg
413
83.8
1
10/24/18 17:24
10/26/18 20:00
131-11-3
Di-n-butylphthalate
ND
ug/kg
413
67.6
1
10/24/18 17:24
10/26/18 20:00
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
826
82.6
1
10/24/18 17:24
10/26/18 20:00
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2060
67.6
1
10/24/18 17:24
10/26/18 20:00
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
413
77.6
1
10/24/18 17:24
10/26/18 20:00
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
413
86.4
1
10/24/18 17:24
10/26/18 20:00
606-20-2
Di-n-octylphthalate
ND
ug/kg
413
86.4
1
10/24/18 17:24
10/26/18 20:00
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
413
113
1
10/24/18 17:24
10/26/18 20:00
117-81-7
Fluoranthene
ND
ug/kg
413
60.1
1
10/24/18 17:24
10/26/18 20:00
206-44-0
Fluorene
ND
ug/kg
413
85.1
1
10/24/18 17:24
10/26/18 20:00
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
413
71.3
1
10/24/18 17:24
10/26/18 20:00
87-68-3
Hexachlorobenzene
ND
ug/kg
413
52.6
1
10/24/18 17:24
10/26/18 20:00
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
413
76.3
1
10/24/18 17:24
10/26/18 20:00
77-47-4
Hexachloroethane
ND
ug/kg
413
109
1
10/24/18 17:24
10/26/18 20:00
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
413
85.1
1
10/24/18 17:24
10/26/18 20:00
193-39-5
Isophorone
ND
ug/kg
413
92.6
1
10/24/18 17:24
10/26/18 20:00
78-59-1
1-Methylnaphthalene
ND
ug/kg
413
108
1
10/24/18 17:24
10/26/18 20:00
90-12-0
2-Methylnaphthalene
ND
ug/kg
413
88.9
1
10/24/18 17:24
10/26/18 20:00
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
413
125
1
10/24/18 17:24
10/26/18 20:00
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
413
163
1
10/24/18 17:24
10/26/18 20:00
15831-10-4
Naphthalene
ND
ug/kg
413
101
1
10/24/18 17:24
10/26/18 20:00
91-20-3
2-Nitroaniline
ND
ug/kg
2060
128
1
10/24/18 17:24
10/26/18 20:00
88-74-4
3-Nitroaniline
ND
ug/kg
2060
113
1
10/24/18 17:24
10/26/18 20:00
99-09-2
4-Nitroaniline
ND
ug/kg
826
116
1
10/24/18 17:24
10/26/18 20:00
100-01-6
Nitrobenzene
ND
ug/kg
413
113
1
10/24/18 17:24
10/26/18 20:00
98-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 56

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: SOUTH WALL Lab ID: 92404510004 Collected: 10/22/18 11:35 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
2-Nitrophenol
ND
ug/kg
413
100
1
10/24/18 17:24
10/26/18 20:00
88-75-5
4-Nitrophenol
ND
ug/kg
2060
73.8
1
10/24/18 17:24
10/26/18 20:00
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
413
134
1
10/24/18 17:24
10/26/18 20:00
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
413
78.8
1
10/24/18 17:24
10/26/18 20:00
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
413
123
1
10/24/18 17:24
10/26/18 20:00
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
413
110
1
10/24/18 17:24
10/26/18 20:00
108-60-1
Pentachlorophenol
ND
ug/kg
2060
75.1
1
10/24/18 17:24
10/26/18 20:00
87-86-5
Phenanthrene
ND
ug/kg
413
68.8
1
10/24/18 17:24
10/26/18 20:00
85-01-8
Phenol
ND
ug/kg
413
124
1
10/24/18 17:24
10/26/18 20:00
108-95-2
Pyrene
ND
ug/kg
413
70.1
1
10/24/18 17:24
10/26/18 20:00
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
413
80.1
1
10/24/18 17:24
10/26/18 20:00
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
413
128
1
10/24/18 17:24
10/26/18 20:00
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
413
91.4
1
10/24/18 17:24
10/26/18 20:00
88-06-2
Surrogates
Nitrobenzene-d5 (S)
83
%
23-110
1
10/24/18 17:24
10/26/18 20:00
4165-60-0
2-Fluorobiphenyl (S)
66
%
30-110
1
10/24/18 17:24
10/26/18 20:00
321-60-8
Terphenyl-d14 (S)
98
%
28-110
1
10/24/18 17:24
10/26/18 20:00
1718-51-0
Phenol-d6 (S)
74
%
22-110
1
10/24/18 17:24
10/26/18 20:00
13127-88-3
2-Fluorophenol (S)
70
%
13-110
1
10/24/18 17:24
10/26/18 20:00
367-12-4
2,4,6-Tribromophenol (S)
76
%
27-110
1
10/24/18 17:24
10/26/18 20:00
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
36.1J
ug/kg
112
11.2
1
10/24/18 09:57
10/24/18 19:00
67-64-1
Benzene
ND
ug/kg
5.6
1.8
1
10/24/18 09:57
10/24/18 19:00
71-43-2
Bromobenzene
ND
ug/kg
5.6
2.2
1
10/24/18 09:57
10/24/18 19:00
108-86-1
Bromochloromethane
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
74-97-5
Bromodichloromethane
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
75-27-4
Bromoform
ND
ug/kg
5.6
2.6
1
10/24/18 09:57
10/24/18 19:00
75-25-2
Bromomethane
ND
ug/kg
11.2
2.8
1
10/24/18 09:57
10/24/18 19:00
74-83-9
2-Butanone (MEK)
ND
ug/kg
112
3.2
1
10/24/18 09:57
10/24/18 19:00
78-93-3
n-Butylbenzene
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
104-51-8
sec-Butylbenzene
ND
ug/kg
5.6
1.8
1
10/24/18 09:57
10/24/18 19:00
135-98-8
tert-Butyl benzene
ND
ug/kg
5.6
2.2
1
10/24/18 09:57
10/24/18 19:00
98-06-6
Carbon tetrachloride
ND
ug/kg
5.6
2.9
1
10/24/18 09:57
10/24/18 19:00
56-23-5
Chlorobenzene
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
108-90-7
Chloroethane
ND
ug/kg
11.2
2.7
1
10/24/18 09:57
10/24/18 19:00
75-00-3
Chloroform
ND
ug/kg
5.6
1.8
1
10/24/18 09:57
10/24/18 19:00
67-66-3
Chloromethane
ND
ug/kg
11.2
2.7
1
10/24/18 09:57
10/24/18 19:00
74-87-3
2-Chlorotoluene
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
95-49-8
4-Chlorotoluene
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.6
4.0
1
10/24/18 09:57
10/24/18 19:00
96-12-8
Dibromochloromethane
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
106-93-4
Dibromomethane
ND
ug/kg
5.6
2.8
1
10/24/18 09:57
10/24/18 19:00
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
95-50-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: SOUTH WALL Lab ID: 92404510004 Collected: 10/22/18 11:35 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics Analytical Method: EPA 8260B Preparation Method: EPA 5035A
1,3-Dichlorobenzene
ND
ug/kg
5.6
2.2
1
10/24/18 09:57
10/24/18 19:00
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.2
4.0
1
10/24/18 09:57
10/24/18 19:00
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.6
1.7
1
10/24/18 09:57
10/24/18 19:00
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.6
2.5
1
10/24/18 09:57
10/24/18 19:00
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.6
1.6
1
10/24/18 09:57
10/24/18 19:00
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.6
1.7
1
10/24/18 09:57
10/24/18 19:00
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.6
1.7
1
10/24/18 09:57
10/24/18 19:00
10061-02-6
Diisopropyl ether
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
108-20-3
Ethylbenzene
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.6
2.2
1
10/24/18 09:57
10/24/18 19:00
87-68-3
2-Hexanone
ND
ug/kg
55.9
4.4
1
10/24/18 09:57
10/24/18 19:00
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
99-87-6
Methylene Chloride
25.2
ug/kg
22.4
3.4
1
10/24/18 09:57
10/24/18 19:00
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
55.9
4.1
1
10/24/18 09:57
10/24/18 19:00
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.6
1.7
1
10/24/18 09:57
10/24/18 19:00
1634-04-4
Naphthalene
ND
ug/kg
5.6
1.3
1
10/24/18 09:57
10/24/18 19:00
91-20-3
n-Propylbenzene
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
103-65-1
Styrene
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.6
2.3
1
10/24/18 09:57
10/24/18 19:00
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
79-34-5
Tetrachloroethene
ND
ug/kg
5.6
1.9
1
10/24/18 09:57
10/24/18 19:00
127-18-4
Toluene
30.4
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.6
2.5
1
10/24/18 09:57
10/24/18 19:00
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.6
1.8
1
10/24/18 09:57
10/24/18 19:00
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.6
2.3
1
10/24/18 09:57
10/24/18 19:00
79-00-5
Trichloroethene
ND
ug/kg
5.6
2.3
1
10/24/18 09:57
10/24/18 19:00
79-01-6
Trichlorofluoromethane
ND
ug/kg
5.6
2.5
1
10/24/18 09:57
10/24/18 19:00
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
5.6
1.8
1
10/24/18 09:57
10/24/18 19:00
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
5.6
2.2
1
10/24/18 09:57
10/24/18 19:00
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
5.6
2.0
1
10/24/18 09:57
10/24/18 19:00
108-67-8
Vinyl acetate
ND
ug/kg
55.9
9.8
1
10/24/18 09:57
10/24/18 19:00
108-05-4
Vinyl chloride
ND
ug/kg
11.2
2.0
1
10/24/18 09:57
10/24/18 19:00
75-01-4
Xylene (Total)
ND
ug/kg
11.2
4.0
1
10/24/18 09:57
10/24/18 19:00
1330-20-7
m&p-Xylene
ND
ug/kg
11.2
4.0
1
10/24/18 09:57
10/24/18 19:00
179601-23-1
o-Xylene
ND
ug/kg
5.6
2.1
1
10/24/18 09:57
10/24/18 19:00
95-47-6
REPORT OF LABORATORY ANALYSIS
C9
L1
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Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: SOUTH WALL Lab ID: 92404510004 Collected: 10/22/18 11:35 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260/5035A Volatile Organics
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Surrogates
Toluene-d8 (S)
100 % 70-130
1 10/24/18 09:57
10/24/18 19:00 2037-26-5
4-Bromofluorobenzene (S)
94 % 70-130
1 10/24/18 09:57
10/24/18 19:00 460-00-4
1,2-Dichloroethane-d4 (S)
105 % 70-132
1 10/24/18 09:57
10/24/18 19:00 17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
19.3 % 0.10
0.10 1
10/23/18 17:22
Sample: EAST WALL Lab ID: 92404510005 Collected: 10/22/18 13:20 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane(S)
MADEP EPH NC Soil
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
8270 MSSV Microwave
Acenaphthene
Acenaphthylene
Aniline
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Date: 11/01/2018 03:43 PM
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
ND mg/kg 6.4 5.8 1 10/23/1817:43 10/24/1818:10
62
%
33-129
1
10/23/1817:43
10/24/1818:10
629-99-2
Analytical
Method: MADEP EPH Preparation Method:
MADEP EPH
ND
mg/kg
12.7
12.7
1
10/30/18 09:45
11/01/18 10:11
N2
ND
mg/kg
12.7
12.7
1
10/30/18 09:45
11/01/18 10:11
N2
ND
mg/kg
12.7
12.7
1
10/30/18 09:45
11/01/18 10:11
N2
60
%
40-140
1
10/30/18 09:45
11/01/18 10:11
7194-86-7
45
%
40-140
1
10/30/18 09:45
11/01/18 10:11
84-15-1
56
%
40-140
1
10/30/18 09:45
11/01/18 10:11
321-60-8
59
%
40-140
1
10/30/18 09:45
11/01/18 10:11
580-13-2
Analytical
Method: EPA 8015C Modified Preparation Method: EPA 5030B
ND
mg/kg
8.8
8.8
1
10/24/18 02:38
10/31/18 03:15
103
%
63-130
1
10/24/18 02:38
10/31 /18 03:15
460-00-4
Analytical
Method: EPA 8270D Preparation Method:
EPA
3546
ND
ug/kg
417
95.9
1
10/24/18 17:24
10/26/18 20:29
83-32-9
ND
ug/kg
417
98.5
1
10/24/18 17:24
10/26/18 20:29
208-96-8
ND
ug/kg
417
112
1
10/24/18 17:24
10/26/18 20:29
62-53-3
ND
ug/kg
417
93.4
1
10/24/18 17:24
10/26/18 20:29
120-12-7
ND
ug/kg
417
77.0
1
10/24/18 17:24
10/26/18 20:29
56-55-3
ND
ug/kg
417
79.5
1
10/24/18 17:24
10/26/18 20:29
50-32-8
ND
ug/kg
417
71.9
1
10/24/18 17:24
10/26/18 20:29
205-99-2
ND
ug/kg
417
106
1
10/24/18 17:24
10/26/18 20:29
191-24-2
ND
ug/kg
417
82.0
1
10/24/18 17:24
10/26/18 20:29
207-08-9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 19 of 56

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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: EAST WALL Lab ID: 92404510005 Collected: 10/22/18 13:20 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Benzoic Acid
ND
ug/kg
2080
75.7
1
10/24/18 17:24
10/26/18 20:29
65-85-0
Benzyl alcohol
ND
ug/kg
833
83.3
1
10/24/18 17:24
10/26/18 20:29
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
417
75.7
1
10/24/18 17:24
10/26/18 20:29
101-55-3
Butylbenzylphthalate
ND
ug/kg
417
88.4
1
10/24/18 17:24
10/26/18 20:29
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
833
85.8
1
10/24/18 17:24
10/26/18 20:29
59-50-7
4-Chloroaniline
ND
ug/kg
2080
116
1
10/24/18 17:24
10/26/18 20:29
106-47-8 L2
bis(2-Chloroethoxy)methane
ND
ug/kg
417
97.2
1
10/24/18 17:24
10/26/18 20:29
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
417
106
1
10/24/18 17:24
10/26/18 20:29
111-44-4
2-Chloronaphthalene
ND
ug/kg
417
82.0
1
10/24/18 17:24
10/26/18 20:29
91-58-7
2-Chlorophenol
ND
ug/kg
417
114
1
10/24/18 17:24
10/26/18 20:29
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
417
85.8
1
10/24/18 17:24
10/26/18 20:29
7005-72-3
Chrysene
ND
ug/kg
417
55.5
1
10/24/18 17:24
10/26/18 20:29
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
417
88.4
1
10/24/18 17:24
10/26/18 20:29
53-70-3
Dibenzofuran
ND
ug/kg
417
68.2
1
10/24/18 17:24
10/26/18 20:29
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
417
ill
1
10/24/18 17:24
10/26/18 20:29
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
417
94.7
1
10/24/18 17:24
10/26/18 20:29
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
417
117
1
10/24/18 17:24
10/26/18 20:29
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2080
90.9
1
10/24/18 17:24
10/26/18 20:29
91-94-1
2,4-Dichlorophenol
ND
ug/kg
417
90.9
1
10/24/18 17:24
10/26/18 20:29
120-83-2
Diethylphthalate
ND
ug/kg
417
64.4
1
10/24/18 17:24
10/26/18 20:29
84-66-2
2,4-Dimethylphenol
ND
ug/kg
417
164
1
10/24/18 17:24
10/26/18 20:29
105-67-9
Dimethylphthalate
ND
ug/kg
417
84.6
1
10/24/18 17:24
10/26/18 20:29
131-11-3
Di-n-butylphthalate
ND
ug/kg
417
68.2
1
10/24/18 17:24
10/26/18 20:29
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
833
83.3
1
10/24/18 17:24
10/26/18 20:29
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2080
68.2
1
10/24/18 17:24
10/26/18 20:29
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
417
78.3
1
10/24/18 17:24
10/26/18 20:29
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
417
87.1
1
10/24/18 17:24
10/26/18 20:29
606-20-2
Di-n-octylphthalate
ND
ug/kg
417
87.1
1
10/24/18 17:24
10/26/18 20:29
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
417
114
1
10/24/18 17:24
10/26/18 20:29
117-81-7
Fluoranthene
ND
ug/kg
417
60.6
1
10/24/18 17:24
10/26/18 20:29
206-44-0
Fluorene
ND
ug/kg
417
85.8
1
10/24/18 17:24
10/26/18 20:29
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
417
71.9
1
10/24/18 17:24
10/26/18 20:29
87-68-3
Hexachlorobenzene
ND
ug/kg
417
53.0
1
10/24/18 17:24
10/26/18 20:29
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
417
77.0
1
10/24/18 17:24
10/26/18 20:29
77-47-4
Hexachloroethane
ND
ug/kg
417
110
1
10/24/18 17:24
10/26/18 20:29
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
417
85.8
1
10/24/18 17:24
10/26/18 20:29
193-39-5
Isophorone
ND
ug/kg
417
93.4
1
10/24/18 17:24
10/26/18 20:29
78-59-1
1-Methylnaphthalene
ND
ug/kg
417
109
1
10/24/18 17:24
10/26/18 20:29
90-12-0
2-Methylnaphthalene
ND
ug/kg
417
89.6
1
10/24/18 17:24
10/26/18 20:29
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
417
126
1
10/24/18 17:24
10/26/18 20:29
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/kg
417
164
1
10/24/18 17:24
10/26/18 20:29
15831-10-4
Naphthalene
ND
ug/kg
417
102
1
10/24/18 17:24
10/26/18 20:29
91-20-3
2-Nitroaniline
ND
ug/kg
2080
129
1
10/24/18 17:24
10/26/18 20:29
88-74-4
3-Nitroaniline
ND
ug/kg
2080
114
1
10/24/18 17:24
10/26/18 20:29
99-09-2
4-Nitroaniline
ND
ug/kg
833
117
1
10/24/18 17:24
10/26/18 20:29
100-01-6
REPORT OF LABORATORY ANALYSIS
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Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 56

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[phone]
ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: EAST WALL Lab ID: 92404510005 Collected: 10/22/18 13:20 Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Nitrobenzene
ND
ug/kg
417
114
1
10/24/18 17:24
10/26/18 20:29
98-95-3
2-Nitrophenol
ND
ug/kg
417
101
1
10/24/18 17:24
10/26/18 20:29
88-75-5
4-Nitrophenol
ND
ug/kg
2080
74.5
1
10/24/18 17:24
10/26/18 20:29
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
417
135
1
10/24/18 17:24
10/26/18 20:29
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
417
79.5
1
10/24/18 17:24
10/26/18 20:29
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
417
124
1
10/24/18 17:24
10/26/18 20:29
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
417
ill
1
10/24/18 17:24
10/26/18 20:29
108-60-1
Pentachlorophenol
ND
ug/kg
2080
75.7
1
10/24/18 17:24
10/26/18 20:29
87-86-5
Phenanthrene
ND
ug/kg
417
69.4
1
10/24/18 17:24
10/26/18 20:29
85-01-8
Phenol
ND
ug/kg
417
125
1
10/24/18 17:24
10/26/18 20:29
108-95-2
Pyrene
ND
ug/kg
417
70.7
1
10/24/18 17:24
10/26/18 20:29
129-00-0
1,2,4-Trichlorobenzene
ND
ug/kg
417
80.8
1
10/24/18 17:24
10/26/18 20:29
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
417
129
1
10/24/18 17:24
10/26/18 20:29
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
417
92.1
1
10/24/18 17:24
10/26/18 20:29
88-06-2
Surrogates
Nitrobenzene-d5 (S)
68
%
23-110
1
10/24/18 17:24
10/26/18 20:29
4165-60-0
2-Fluorobiphenyl (S)
56
%
30-110
1
10/24/18 17:24
10/26/18 20:29
321-60-8
Terphenyl-d14 (S)
78
%
28-110
1
10/24/18 17:24
10/26/18 20:29
1718-51-0
Phenol-d6 (S)
54
%
22-110
1
10/24/18 17:24
10/26/18 20:29
13127-88-3
2-Fluorophenol (S)
53
%
13-110
1
10/24/18 17:24
10/26/18 20:29
367-12-4
2,4,6-Tribromophenol (S)
64
%
27-110
1
10/24/18 17:24
10/26/18 20:29
118-79-6
8260/5035A Volatile Organics
Analytical
Method: EPA 8260B Preparation Method: EPA
5035A
Acetone
29.5J
ug/kg
110
11.0
1
10/24/18 09:57
10/24/18 19:20
67-64-1
Benzene
ND
ug/kg
5.5
1.8
1
10/24/18 09:57
10/24/18 19:20
71-43-2
Bromobenzene
ND
ug/kg
5.5
2.2
1
10/24/18 09:57
10/24/18 19:20
108-86-1
Bromochloromethane
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
74-97-5
Bromodichloromethane
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
75-27-4
Bromoform
ND
ug/kg
5.5
2.5
1
10/24/18 09:57
10/24/18 19:20
75-25-2
Bromomethane
ND
ug/kg
11.0
2.7
1
10/24/18 09:57
10/24/18 19:20
74-83-9
2-Butanone (MEK)
ND
ug/kg
110
3.2
1
10/24/18 09:57
10/24/18 19:20
78-93-3
n-Butylbenzene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
104-51-8
sec-Butylbenzene
ND
ug/kg
5.5
1.8
1
10/24/18 09:57
10/24/18 19:20
135-98-8
tert-Butyl benzene
ND
ug/kg
5.5
2.2
1
10/24/18 09:57
10/24/18 19:20
98-06-6
Carbon tetrachloride
ND
ug/kg
5.5
2.9
1
10/24/18 09:57
10/24/18 19:20
56-23-5
Chlorobenzene
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
108-90-7
Chloroethane
ND
ug/kg
11.0
2.6
1
10/24/18 09:57
10/24/18 19:20
75-00-3
Chloroform
ND
ug/kg
5.5
1.8
1
10/24/18 09:57
10/24/18 19:20
67-66-3
Chloromethane
ND
ug/kg
11.0
2.6
1
10/24/18 09:57
10/24/18 19:20
74-87-3
2-Chlorotoluene
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
95-49-8
4-Chlorotoluene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.5
4.0
1
10/24/18 09:57
10/24/18 19:20
96-12-8
Dibromochloromethane
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
106-93-4
Dibromomethane
ND
ug/kg
5.5
2.7
1
10/24/18 09:57
10/24/18 19:20
74-95-3
REPORT OF LABORATORY ANALYSIS
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Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: EAST WALL
Lab ID:
92404510005
Collected:
10/22/18
13:20
Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
8260/5035A Volatile Organics
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
1,2-Dichlorobenzene
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.5
2.2
1
10/24/18 09:57
10/24/18 19:20
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.0
4.0
1
10/24/18 09:57
10/24/18 19:20
75-71-8
1,1-Dichloroethane
ND
ug/kg
5.5
1.6
1
10/24/18 09:57
10/24/18 19:20
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.5
2.4
1
10/24/18 09:57
10/24/18 19:20
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.5
1.5
1
10/24/18 09:57
10/24/18 19:20
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.5
1.6
1
10/24/18 09:57
10/24/18 19:20
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.5
1.6
1
10/24/18 09:57
10/24/18 19:20
10061-02-6
Diisopropyl ether
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
108-20-3
Ethylbenzene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.5
2.2
1
10/24/18 09:57
10/24/18 19:20
87-68-3
2-Hexanone
ND
ug/kg
55.0
4.3
1
10/24/18 09:57
10/24/18 19:20
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
99-87-6
Methylene Chloride
7.5J
ug/kg
22.0
3.3
1
10/24/18 09:57
10/24/18 19:20
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
55.0
4.1
1
10/24/18 09:57
10/24/18 19:20
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.5
1.6
1
10/24/18 09:57
10/24/18 19:20
1634-04-4
Naphthalene
ND
ug/kg
5.5
1.3
1
10/24/18 09:57
10/24/18 19:20
91-20-3
n-Propylbenzene
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
103-65-1
Styrene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.5
2.3
1
10/24/18 09:57
10/24/18 19:20
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
79-34-5
Tetrachloroethene
ND
ug/kg
5.5
1.9
1
10/24/18 09:57
10/24/18 19:20
127-18-4 L1
Toluene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.5
2.4
1
10/24/18 09:57
10/24/18 19:20
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.5
1.8
1
10/24/18 09:57
10/24/18 19:20
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.5
2.3
1
10/24/18 09:57
10/24/18 19:20
79-00-5
Trichloroethene
ND
ug/kg
5.5
2.3
1
10/24/18 09:57
10/24/18 19:20
79-01-6
Trichlorofluoromethane
ND
ug/kg
5.5
2.4
1
10/24/18 09:57
10/24/18 19:20
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
5.5
1.8
1
10/24/18 09:57
10/24/18 19:20
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
5.5
2.2
1
10/24/18 09:57
10/24/18 19:20
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
5.5
2.0
1
10/24/18 09:57
10/24/18 19:20
108-67-8
Vinyl acetate
ND
ug/kg
55.0
9.7
1
10/24/18 09:57
10/24/18 19:20
108-05-4
Vinyl chloride
ND
ug/kg
11.0
2.0
1
10/24/18 09:57
10/24/18 19:20
75-01-4
Xylene (Total)
ND
ug/kg
11.0
4.0
1
10/24/18 09:57
10/24/18 19:20
1330-20-7
m&p-Xylene
ND
ug/kg
11.0
4.0
1
10/24/18 09:57
10/24/18 19:20
179601-23-1
o-Xylene
ND
ug/kg
5.5
2.1
1
10/24/18 09:57
10/24/18 19:20
95-47-6
REPORT OF LABORATORY ANALYSIS
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Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 56

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ANALYTICAL RESULTS
Project: MERIDALE
Pace Project No.: 92404510
Sample: EAST WALL
Lab ID: 92404510005 Collected:
10/22/18 13:20
Received: 10/23/18 14:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit
MDL DF
Prepared Analyzed
CAS No. Qual
8260/5035A Volatile Organics
Analytical Method: EPA 8260B Preparation Method: EPA 5035A
Surrogates
Toluene-d8 (S)
100 % 70-130
1
10/24/18 09:57 10/24/18 19:20
2037-26-5
4-Bromofluorobenzene (S)
90 % 70-130
1
10/24/18 09:57 10/24/18 19:20
460-00-4
1,2-Dichloroethane-d4 (S)
100 % 70-132
1
10/24/18 09:57 10/24/18 19:20
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
20.5 % 0.10
0.10 1
10/23/18 17:23
REPORT OF LABORATORY ANALYSIS
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Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 438081 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
METHOD BLANK: 2408590 Matrix: Solid
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Gas Range Organics (C6-C10) mg/kg ND 5.9 5.9 10/30/18 22:50
4-Bromofluorobenzene (S) % 92 63-130 10/30/18 22:50
LABORATORY CONTROL SAMPLE:
2408591
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
49.8 40.1
81
70-130
4-Bromofluorobenzene (S)
%
97
63-130
MATRIX SPIKE SAMPLE:
2410278
92404601005 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 49.1
38.6
77 40-155
4-Bromofluorobenzene (S)
%
87 63-130
SAMPLE DUPLICATE: 2410279
92404601008 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND ND
30
4-Bromofluorobenzene (S)
%
97 95
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 437976 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92404510001
METHOD BLANK: 2408038
Associated Lab Samples: 92404510001
Parameter
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
MDL Analyzed Qualifiers
ug/L
ND
50.0
50.0 10/26/1816:15 N2
ug/L
ND
50.0
50.0 10/26/1816:15 N2
ug/L
ND
50.0
50.0 10/26/1816:15 N2
%
121
70-130
10/26/18 16:15
%
124
70-130
10/26/1816:15
LABORATORY CONTROL SAMPLE & LCSD:
2408039
2408040
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
267
259
89
86
70-130 3 25 N2
Aliphatic (C09-C12)
ug/L
300
291
287
97
96
30-130 1 25 N2
Aromatic (C09-C10)
ug/L
100
94.1
92.8
94
93
70-130 1 25 N2
4-Bromofluorobenzene (FID) (S)
%
102
101
70-130
4-Bromofluorobenzene (PID) (S)
%
103
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 438860 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 602 by 6200B
Associated Lab Samples: 92404510001
METHOD BLANK: 2412327
Associated Lab Samples: 92404510001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2-Dichlorobenzene
ug/L
ND
1.0
1.0
10/28/18 15:31
1,3-Dichlorobenzene
ug/L
ND
1.0
1.0
10/28/18 15:31
1,4-Dichlorobenzene
ug/L
ND
1.0
1.0
10/28/18 15:31
Benzene
ug/L
ND
1.0
1.0
10/28/18 15:31
Chlorobenzene
ug/L
ND
1.0
1.0
10/28/18 15:31
Diisopropyl ether
ug/L
ND
1.0
1.0
10/28/18 15:31
Ethylbenzene
ug/L
ND
1.0
1.0
10/28/18 15:31
Isopropylbenzene (Cumene)
ug/L
ND
1.0
1.0
10/28/18 15:31
m&p-Xylene
ug/L
ND
2.0
2.0
10/28/18 15:31
Methyl-tert-butyl ether
ug/L
ND
1.0
1.0
10/28/18 15:31
Naphthalene
ug/L
ND
2.0
2.0
10/28/18 15:31
o-Xylene
ug/L
ND
1.0
1.0
10/28/18 15:31
Toluene
ug/L
ND
1.0
1.0
10/28/18 15:31
1,2-Dichloroethane-d4 (S)
%
100
70-130
10/28/18 15:31
4-Bromofluorobenzene (S)
%
90
70-130
10/28/18 15:31
Toluene-d8 (S)
%
102
70-130
10/28/18 15:31
LABORATORY CONTROL SAMPLE:
Parameter
2412328
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dichlorobenzene
ug/L
50
46.4
93
60-140
1,3-Dichlorobenzene
ug/L
50
47.0
94
60-140
1,4-Dichlorobenzene
ug/L
50
46.7
93
60-140
Benzene
ug/L
50
46.3
93
60-140
Chlorobenzene
ug/L
50
48.4
97
60-140
Diisopropyl ether
ug/L
50
51.8
104
60-140
Ethylbenzene
ug/L
50
49.4
99
60-140
Isopropylbenzene (Cumene)
ug/L
50
46.7
93
60-140
m&p-Xylene
ug/L
100
98.7
99
60-140
Methyl-tert-butyl ether
ug/L
50
45.2
90
60-140
Naphthalene
ug/L
50
46.0
92
60-140
o-Xylene
ug/L
50
46.4
93
60-140
Toluene
ug/L
50
47.3
95
60-140
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
108
70-130
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 56

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2412329
2412330
MS
MSD
92404411001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
1,2-Dichlorobenzene
ug/L
ND
20
20
18.7
17.2
93
86
60-140
8
30
1,3-Dichlorobenzene
ug/L
ND
20
20
19.1
17.8
96
89
60-140
7
30
1,4-Dichlorobenzene
ug/L
ND
20
20
19.3
17.5
97
88
60-140
10
30
Benzene
ug/L
ND
20
20
19.4
19.7
97
99
60-140
2
30
Chlorobenzene
ug/L
ND
20
20
19.3
18.5
96
93
60-140
4
30
Diisopropyl ether
ug/L
ND
20
20
17.5
16.6
87
83
60-140
5
30
Ethylbenzene
ug/L
ND
20
20
19.3
18.3
97
92
60-140
5
30
Isopropylbenzene (Cumene)
ug/L
ND
20
20
22.6
17.6
113
88
60-140
25
30
m&p-Xylene
ug/L
ND
40
40
39.2
36.5
98
91
60-140
7
30
Methyl-tert-butyl ether
ug/L
ND
20
20
17.0
16.0
85
80
60-140
6
30
Naphthalene
ug/L
ND
20
20
17.2
16.7
86
84
60-140
3
30
o-Xylene
ug/L
ND
20
20
20.9
18.3
104
91
60-140
13
30
Toluene
ug/L
ND
20
20
16.1
19.3
80
97
60-140
18
30
1,2-Dichloroethane-d4 (S)
%
101
102
70-130
4-Bromofluorobenzene (S)
%
117
88
70-130
Toluene-d8 (S)
%
87
110
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 437990 Analysis Method: EPA 8260B
QC Batch Method: EPA 5035A Analysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
METHOD BLANK: 2408079 Matrix: Solid
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.5
2.3
10/24/18 11:56
1,1,1-Trichloroethane
ug/kg
ND
5.5
2.0
10/24/18 11:56
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.5
2.1
10/24/18 11:56
1,1,2-Trichloroethane
ug/kg
ND
5.5
2.3
10/24/18 11:56
1,1-Dichloroethane
ug/kg
ND
5.5
1.6
10/24/18 11:56
1,1-Dichloroethene
ug/kg
ND
5.5
2.0
10/24/18 11:56
1,1-Dichloropropene
ug/kg
ND
5.5
1.6
10/24/18 11:56
1,2,3-Trichlorobenzene
ug/kg
ND
5.5
2.4
10/24/18 11:56
1,2,3-Trichloropropane
ug/kg
ND
5.5
1.8
10/24/18 11:56
1,2,4-Trichlorobenzene
ug/kg
ND
5.5
1.8
10/24/18 11:56
1,2,4-Trimethylbenzene
ug/kg
ND
5.5
2.2
10/24/18 11:56
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.5
3.9
10/24/18 11:56
1,2-Dibromoethane (EDB)
ug/kg
ND
5.5
2.0
10/24/18 11:56
1,2-Dichlorobenzene
ug/kg
ND
5.5
2.1
10/24/18 11:56
1,2-Dichloroethane
ug/kg
ND
5.5
2.4
10/24/18 11:56
1,2-Dichloropropane
ug/kg
ND
5.5
1.9
10/24/18 11:56
1,3,5-Trimethylbenzene
ug/kg
ND
5.5
2.0
10/24/18 11:56
1,3-Dichlorobenzene
ug/kg
ND
5.5
2.2
10/24/18 11:56
1,3-Dichloropropane
ug/kg
ND
5.5
2.1
10/24/18 11:56
1,4-Dichlorobenzene
ug/kg
ND
5.5
1.9
10/24/18 11:56
2,2-Dichloropropane
ug/kg
ND
5.5
1.9
10/24/18 11:56
2-Butanone (MEK)
ug/kg
ND
109
3.2
10/24/18 11:56
2-Chlorotoluene
ug/kg
ND
5.5
1.9
10/24/18 11:56
2-Hexanone
ug/kg
ND
54.7
4.3
10/24/18 11:56
4-Chlorotoluene
ug/kg
ND
5.5
2.0
10/24/18 11:56
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
54.7
4.0
10/24/18 11:56
Acetone
ug/kg
ND
109
10.9
10/24/18 11:56
Benzene
ug/kg
ND
5.5
1.8
10/24/18 11:56
Bromobenzene
ug/kg
ND
5.5
2.2
10/24/18 11:56
Bromochloromethane
ug/kg
ND
5.5
1.9
10/24/18 11:56
Bromodichloromethane
ug/kg
ND
5.5
2.1
10/24/18 11:56
Bromoform
ug/kg
ND
5.5
2.5
10/24/18 11:56
Bromomethane
ug/kg
ND
10.9
2.7
10/24/18 11:56
Carbon tetrachloride
ug/kg
ND
5.5
2.8
10/24/18 11:56
Chlorobenzene
ug/kg
ND
5.5
2.1
10/24/18 11:56
Chloroethane
ug/kg
ND
10.9
2.6
10/24/18 11:56
Chloroform
ug/kg
ND
5.5
1.8
10/24/18 11:56
Chloromethane
ug/kg
ND
10.9
2.6
10/24/18 11:56
cis-1,2-Dichloroethene
ug/kg
ND
5.5
1.5
10/24/18 11:56
cis-1,3-Dichloropropene
ug/kg
ND
5.5
2.0
10/24/18 11:56
Dibromochloromethane
ug/kg
ND
5.5
2.0
10/24/18 11:56
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 56

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
METHOD BLANK: 2408079 Matrix: Solid
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
Dibromomethane
ug/kg
ND
5.5
2.7
10/24/18 11:56
Dichlorodifluoromethane
ug/kg
ND
10.9
3.9
10/24/18 11:56
Diisopropyl ether
ug/kg
ND
5.5
1.9
10/24/18 11:56
Ethylbenzene
ug/kg
ND
5.5
2.0
10/24/18 11:56
Hexachloro-1,3-butadiene
ug/kg
ND
5.5
2.2
10/24/18 11:56
Isopropylbenzene (Cumene)
ug/kg
ND
5.5
2.1
10/24/18 11:56
m&p-Xylene
ug/kg
ND
10.9
3.9
10/24/18 11:56
Methyl-tert-butyl ether
ug/kg
ND
5.5
1.6
10/24/18 11:56
Methylene Chloride
ug/kg
ND
21.9
3.3
10/24/18 11:56
n-Butylbenzene
ug/kg
ND
5.5
2.0
10/24/18 11:56
n-Propylbenzene
ug/kg
ND
5.5
1.9
10/24/18 11:56
Naphthalene
ug/kg
ND
5.5
1.3
10/24/18 11:56
o-Xylene
ug/kg
ND
5.5
2.1
10/24/18 11:56
p-Isopropyltoluene
ug/kg
ND
5.5
1.9
10/24/18 11:56
sec-Butylbenzene
ug/kg
ND
5.5
1.8
10/24/18 11:56
Styrene
ug/kg
ND
5.5
2.0
10/24/18 11:56
tert-Butyl benzene
ug/kg
ND
5.5
2.2
10/24/18 11:56
Tetrachloroethene
ug/kg
ND
5.5
1.9
10/24/18 11:56
Toluene
ug/kg
ND
5.5
2.0
10/24/18 11:56
trans-1,2-Dichloroethene
ug/kg
ND
5.5
2.1
10/24/18 11:56
trans- 1,3-Dichloropropene
ug/kg
ND
5.5
1.6
10/24/18 11:56
Trichloroethene
ug/kg
ND
5.5
2.3
10/24/18 11:56
Trichlorofluoromethane
ug/kg
ND
5.5
2.4
10/24/18 11:56
Vinyl acetate
ug/kg
ND
54.7
9.6
10/24/18 11:56
Vinyl chloride
ug/kg
ND
10.9
2.0
10/24/18 11:56
Xylene (Total)
ug/kg
ND
10.9
3.9
10/24/18 11:56
1,2-Dichloroethane-d4 (S)
%
100
70-132
10/24/18 11:56
4-Bromofluorobenzene (S)
%
94
70-130
10/24/18 11:56
Toluene-d8 (S)
%
98
70-130
10/24/18 11:56
Qualifiers
LABORATORY CONTROL SAMPLE:
2408080
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
57.2
51.5
90
74-137
1,1,1-Trichloroethane
ug/kg
57.2
47.3
83
67-140
1,1,2,2-Tetrachloroethane
ug/kg
57.2
50.6
88
72-141
1,1,2-Trichloroethane
ug/kg
57.2
51.3
90
78-138
1,1-Dichloroethane
ug/kg
57.2
43.0
75
69-134
1,1-Dichloroethene
ug/kg
57.2
45.6
80
67-138
1,1-Dichloropropene
ug/kg
57.2
48.0
84
69-139
1,2,3-Trichlorobenzene
ug/kg
57.2
51.9
91
70-146
1,2,3-Trichloropropane
ug/kg
57.2
54.0
94
69-144
1,2,4-Trichlorobenzene
ug/kg
57.2
53.0
93
68-148
1,2,4-Trimethylbenzene
ug/kg
57.2
57.4
100
74-137
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
LABORATORY CONTROL SAMPLE:
Parameter
2408080
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2-Dibromo-3-chloropropane
ug/kg
57.2
57.7
101
65-140
1,2-Dibromoethane (EDB)
ug/kg
57.2
53.7
94
77-135
1,2-Dichlorobenzene
ug/kg
57.2
55.3
97
77-141
1,2-Dichloroethane
ug/kg
57.2
47.7
83
65-137
1,2-Dichloropropane
ug/kg
57.2
51.6
90
72-136
1,3,5-Trimethylbenzene
ug/kg
57.2
55.5
97
76-133
1,3-Dichlorobenzene
ug/kg
57.2
55.3
97
74-138
1,3-Dichloropropane
ug/kg
57.2
56.2
98
71-139
1,4-Dichlorobenzene
ug/kg
57.2
55.1
96
76-138
2,2-Dichloropropane
ug/kg
57.2
46.8
82
68-137
2-Butanone (MEK)
ug/kg
114
113J
98
58-147
2-Chlorotoluene
ug/kg
57.2
55.2
96
73-139
2-Hexanone
ug/kg
114
117
102
62-145
4-Chlorotoluene
ug/kg
57.2
56.0
98
76-141
4-Methyl-2-pentanone (MIBK)
ug/kg
114
115
101
64-149
Acetone
ug/kg
114
86.OJ
75
53-153
Benzene
ug/kg
57.2
49.5
86
73-135
Bromobenzene
ug/kg
57.2
52.3
91
75-133
Bromochloromethane
ug/kg
57.2
49.8
87
73-134
Bromodichloromethane
ug/kg
57.2
51.4
90
71-135
Bromoform
ug/kg
57.2
55.8
98
66-141
Bromomethane
ug/kg
57.2
44.5
78
53-160
Carbon tetrachloride
ug/kg
57.2
50.1
88
60-145
Chlorobenzene
ug/kg
57.2
51.5
90
78-130
Chloroethane
ug/kg
57.2
46.4
81
64-149
Chloroform
ug/kg
57.2
46.5
81
70-134
Chloromethane
ug/kg
57.2
50.7
89
52-150
cis-1,2-Dichloroethene
ug/kg
57.2
45.9
80
70-133
cis-1,3-Dichloropropene
ug/kg
57.2
52.4
92
68-134
Dibromochloromethane
ug/kg
57.2
55.0
96
71-138
Dibromomethane
ug/kg
57.2
48.8
85
74-130
Dichlorodifluoromethane
ug/kg
57.2
40.3
70
40-160
Diisopropyl ether
ug/kg
57.2
46.2
81
69-141
Ethylbenzene
ug/kg
57.2
52.1
91
75-133
Hexachloro-1,3-butadiene
ug/kg
57.2
50.5
88
68-143
Isopropylbenzene (Cumene)
ug/kg
57.2
52.0
91
76-143
m&p-Xylene
ug/kg
114
104
91
75-136
Methyl-tert-butyl ether
ug/kg
57.2
46.0
80
68-144
Methylene Chloride
ug/kg
57.2
43.0
75
45-154
n-Butylbenzene
ug/kg
57.2
55.6
97
72-137
n-Propylbenzene
ug/kg
57.2
56.3
98
76-136
Naphthalene
ug/kg
57.2
60.3
105
68-151
o-Xylene
ug/kg
57.2
51.7
90
76-141
p-Isopropyltoluene
ug/kg
57.2
55.3
97
76-140
sec-Butylbenzene
ug/kg
57.2
55.5
97
79-139
Styrene
ug/kg
57.2
51.4
90
79-137
tert-Butyl benzene
ug/kg
57.2
64.3
112
74-143
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
LABORATORY CONTROL SAMPLE:
Parameter
2408080
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
ug/kg
57.2
109
191
71-138 L1
Toluene
ug/kg
57.2
49.1
86
74-131
trans-1,2-Dichloroethene
ug/kg
57.2
45.3
79
67-135
trans- 1,3-Dichloropropene
ug/kg
57.2
52.7
92
65-146
Trichloroethene
ug/kg
57.2
51.1
89
67-135
Trichlorofluoromethane
ug/kg
57.2
39.6
69
59-144
Vinyl acetate
ug/kg
114
75.4
66
40-160
Vinyl chloride
ug/kg
57.2
49.2
86
56-141
Xylene (Total)
ug/kg
172
156
91
76-137
1,2-Dichloroethane-d4 (S)
%
97
70-132
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
100
70-130
MATRIX SPIKE SAMPLE:
Parameter
2408081
Units
92404379001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
13.4
8.2
61
70-130 M1
1,1,1-Trichloroethane
ug/kg
ND
13.4
7.8
58
70-130 M1
1,1,2,2-Tetrachloroethane
ug/kg
ND
13.4
10.1
75
70-130
1,1,2-Trichloroethane
ug/kg
ND
13.4
9.8
73
70-130
1,1-Dichloroethane
ug/kg
ND
13.4
7.5
56
70-130 M1
1,1-Dichloroethene
ug/kg
ND
13.4
6.7
50
49-180
1,1-Dichloropropene
ug/kg
ND
13.4
6.8
51
70-130 M1
1,2,3-Trichlorobenzene
ug/kg
ND
13.4
4.2
31
70-130 M1
1,2,3-Trichloropropane
ug/kg
ND
13.4
9.9
74
70-130
1,2,4-Trichlorobenzene
ug/kg
ND
13.4
4.5
34
70-130 M1
1,2,4-Trimethylbenzene
ug/kg
ND
13.4
8.2
61
70-130 M1
1,2-Dibromo-3-chloropropane
ug/kg
ND
13.4
11.9
89
70-130
1,2-Dibromoethane (EDB)
ug/kg
ND
13.4
9.6
72
70-130
1,2-Dichlorobenzene
ug/kg
ND
13.4
7.9
59
70-130 M1
1,2-Dichloroethane
ug/kg
ND
13.4
9.8
73
70-130
1,2-Dichloropropane
ug/kg
ND
13.4
9.1
68
70-130 M1
1,3,5-Trimethylbenzene
ug/kg
ND
13.4
7.7
58
70-130 M1
1,3-Dichlorobenzene
ug/kg
ND
13.4
7.7
47
70-130 M1
1,3-Dichloropropane
ug/kg
ND
13.4
10.5
79
70-130
1,4-Dichlorobenzene
ug/kg
ND
13.4
7.8
58
70-130 M1
2,2-Dichloropropane
ug/kg
ND
13.4
7.8
58
70-130 M1
2-Butanone (MEK)
ug/kg
ND
26.8
32.3J
121
70-130
2-Chlorotoluene
ug/kg
ND
13.4
8.5
63
70-130 M1
2-Hexanone
ug/kg
ND
26.8
21.6J
80
70-130
4-Chlorotoluene
ug/kg
ND
13.4
8.0
60
70-130 M1
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
26.8
22.8J
85
70-130
Acetone
ug/kg
36.9J
26.8
41.OJ
15
70-130 M1
Benzene
ug/kg
ND
13.4
8.0
60
50-166
Bromobenzene
ug/kg
ND
13.4
8.5
63
70-130 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
MATRIX SPIKE SAMPLE:
2408081
92404379001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/kg
ND
13.4
10.3
77
70-130
Bromodichloromethane
ug/kg
ND
13.4
8.9
66
70-130 M1
Bromoform
ug/kg
ND
13.4
9.1
68
70-130 M1
Bromomethane
ug/kg
ND
13.4
9.7
72
70-130
Carbon tetrachloride
ug/kg
ND
13.4
7.0
52
70-130 M1
Chlorobenzene
ug/kg
ND
13.4
8.3
55
43-169
Chloroethane
ug/kg
ND
13.4
6.9
51
70-130 M1
Chloroform
ug/kg
3.8J
13.4
10.5
51
70-130 M1
Chloromethane
ug/kg
ND
13.4
8.3
62
70-130 M1
cis-1,2-Dichloroethene
ug/kg
ND
13.4
8.3
62
70-130 M1
cis-1,3-Dichloropropene
ug/kg
ND
13.4
8.3
62
70-130 M1
Dibromochloromethane
ug/kg
ND
13.4
9.2
69
70-130 M1
Dibromomethane
ug/kg
ND
13.4
9.6
72
70-130
Dichlorodifluoromethane
ug/kg
ND
13.4
5.7J
42
70-130 M1
Diisopropyl ether
ug/kg
ND
13.4
9.7
73
70-130
Ethylbenzene
ug/kg
ND
13.4
7.3
55
70-130 M1
Hexachloro-1,3-butadiene
ug/kg
ND
13.4
2AJ
18
70-130 M1
Isopropylbenzene (Cumene)
ug/kg
ND
13.4
6.6
49
70-130 M1
m&p-Xylene
ug/kg
8.3
26.8
16.9
32
70-130 M1
Methyl-tert-butyl ether
ug/kg
ND
13.4
10.2
76
70-130
Methylene Chloride
ug/kg
ND
13.4
5.9J
44
70-130 M1
n-Butylbenzene
ug/kg
ND
13.4
5.1
38
70-130 M1
n-Propylbenzene
ug/kg
ND
13.4
7.5
56
70-130 M1
Naphthalene
ug/kg
ND
13.4
7.5
56
70-130 M1
o-Xylene
ug/kg
ND
13.4
7.6
49
70-130 M1
p-Isopropyltoluene
ug/kg
ND
13.4
6.1
46
70-130 M1
sec-Butylbenzene
ug/kg
ND
13.4
6.1
46
70-130 M1
Styrene
ug/kg
ND
13.4
6.7
50
70-130 M1
tert-Butyl benzene
ug/kg
ND
13.4
6.4
48
70-130 M1
Tetrachloroethene
ug/kg
ND
13.4
6.7
41
70-130 MO
Toluene
ug/kg
ND
13.4
7.5
56
52-163
trans-1,2-Dichloroethene
ug/kg
ND
13.4
7.2
54
70-130 M1
trans- 1,3-Dichloropropene
ug/kg
ND
13.4
8.0
60
70-130 M1
Trichloroethene
ug/kg
ND
13.4
6.8
51
49-167
Trichlorofluoromethane
ug/kg
ND
13.4
6.0
45
70-130 M1
Vinyl acetate
ug/kg
ND
26.8
11AJ
42
70-130 M1
Vinyl chloride
ug/kg
ND
13.4
7.9
59
70-130 M1
Xylene (Total)
ug/kg
8.3
40.2
24.5
40
70-130 MS
1,2-Dichloroethane-d4 (S)
%
112
70-132
4-Bromofluorobenzene (S)
%
87
70-130
Toluene-d8 (S)
%
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
SAMPLE DUPLICATE: 2408082
Parameter
Units
92404510002
Result
Dup
Result RPD
Max
RPD
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,1-Trichloroethane
ug/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
30
1,1,2-Trichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethane
ug/kg
ND
ND
30
1,1-Dichloroethene
ug/kg
ND
ND
30
1,1-Dichloropropene
ug/kg
ND
ND
30
1,2,3-Trichlorobenzene
ug/kg
ND
ND
30
1,2,3-Trichloropropane
ug/kg
ND
ND
30
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2,4-Trimethylbenzene
ug/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
30
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,2-Dichloroethane
ug/kg
ND
ND
30
1,2-Dichloropropane
ug/kg
ND
ND
30
1,3,5-Trimethylbenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichloropropane
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
2,2-Dichloropropane
ug/kg
ND
ND
30
2-Butanone (MEK)
ug/kg
ND
6.2J
30
2-Chlorotoluene
ug/kg
ND
ND
30
2-Hexanone
ug/kg
ND
ND
30
4-Chlorotoluene
ug/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
30
Acetone
ug/kg
29.5J
121J
30
Benzene
ug/kg
ND
ND
30
Bromobenzene
ug/kg
ND
ND
30
Bromochloromethane
ug/kg
ND
ND
30
Bromodichloromethane
ug/kg
ND
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
ug/kg
ND
ND
30
Carbon tetrachloride
ug/kg
ND
ND
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
ND
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
ND
ND
30
Dibromochloromethane
ug/kg
ND
ND
30
Dibromomethane
ug/kg
ND
ND
30
Dichlorodifluoromethane
ug/kg
ND
ND
30
Diisopropyl ether
ug/kg
ND
ND
30
Ethylbenzene
ug/kg
ND
ND
30
Hexachloro-1,3-butadiene
ug/kg
ND
ND
30
Isopropylbenzene (Cumene)
ug/kg
ND
ND
30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
SAMPLE DUPLICATE: 2408082
Parameter
Units
92404510002
Result
Dup
Result
m&p-Xylene
ug/kg
ND
ND
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
33.6
13.8J
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
ND
ND
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
ND
4AJ
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
101
107
4-Bromofluorobenzene (S)
%
90
92
Toluene-d8(S)
%
100
98
Max
RPD RPD Qualifiers
19
15
11
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 34 of 56

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 438001 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92404510001
METHOD BLANK: 2408144
Associated Lab Samples: 92404510001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
0.98
10/25/18 15:43
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
0.95
10/25/18 15:43
2,4,6-Trichlorophenol
ug/L
ND
10.0
1.3
10/25/18 15:43
2,4-Dichlorophenol
ug/L
ND
5.0
1.7
10/25/18 15:43
2,4-Dimethylphenol
ug/L
ND
10.0
1.2
10/25/18 15:43
2,4-Dinitrophenol
ug/L
ND
50.0
9.0
10/25/18 15:43
2,4-Dinitrotoluene
ug/L
ND
5.0
0.90
10/25/18 15:43
2,6-Dinitrotoluene
ug/L
ND
5.0
0.98
10/25/18 15:43
2-Chloronaphthalene
ug/L
ND
5.0
0.98
10/25/18 15:43
2-Chlorophenol
ug/L
ND
5.0
1.3
10/25/18 15:43
2-Nitrophenol
ug/L
ND
5.0
0.91
10/25/18 15:43
3,3'-Dichlorobenzidine
ug/L
ND
25.0
2.1
10/25/18 15:43
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
2.6
10/25/18 15:43
4-Bromophenylphenyl ether
ug/L
ND
5.0
0.82
10/25/18 15:43
4-Chloro-3-methylphenol
ug/L
ND
5.0
3.7
10/25/18 15:43
4-Chlorophenylphenyl ether
ug/L
ND
5.0
0.87
10/25/18 15:43
4-Nitrophenol
ug/L
ND
50.0
4.1
10/25/18 15:43
Acenaphthene
ug/L
ND
5.0
0.25
10/25/18 15:43
Acenaphthylene
ug/L
ND
5.0
0.21
10/25/18 15:43
Anthracene
ug/L
ND
5.0
0.14
10/25/18 15:43
Benzo(a)anthracene
ug/L
ND
5.0
0.33
10/25/18 15:43
Benzo(a)pyrene
ug/L
ND
5.0
0.30
10/25/18 15:43
Benzo(b)fluoranthene
ug/L
ND
5.0
0.28
10/25/18 15:43
Benzo(g,h,i)perylene
ug/L
ND
5.0
0.38
10/25/18 15:43
Benzo(k)fluoranthene
ug/L
ND
5.0
0.43
10/25/18 15:43
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
0.92
10/25/18 15:43
bis(2-Chloroethyl) ether
ug/L
ND
5.0
1.0
10/25/18 15:43
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
0.79
10/25/18 15:43
Butylbenzylphthalate
ug/L
ND
5.0
0.79
10/25/18 15:43
Chrysene
ug/L
ND
5.0
0.21
10/25/18 15:43
Di-n-butylphthalate
ug/L
ND
5.0
0.75
10/25/18 15:43
Di-n-octylphthalate
ug/L
ND
5.0
0.66
10/25/18 15:43
Dibenz(a,h)anthracene
ug/L
ND
5.0
0.55
10/25/18 15:43
Diethylphthalate
ug/L
ND
5.0
0.58
10/25/18 15:43
Dimethylphthalate
ug/L
ND
5.0
0.76
10/25/18 15:43
Fluoranthene
ug/L
ND
5.0
0.21
10/25/18 15:43
Fluorene
ug/L
ND
5.0
0.21
10/25/18 15:43
Hexachloro-1,3-butadiene
ug/L
ND
5.0
0.94
10/25/18 15:43
Hexachlorobenzene
ug/L
ND
5.0
0.72
10/25/18 15:43
Hexachlorocyclopentadiene
ug/L
ND
10.0
0.88
10/25/18 15:43
Hexachloroethane
ug/L
ND
5.0
1.1
10/25/18 15:43
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 56

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
METHOD BLANK: 2408144
Associated Lab Samples: 92404510001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
0.29
10/25/18 15:43
Isophorone
ug/L
ND
10.0
0.89
10/25/18 15:43
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
0.99
10/25/18 15:43
N-Nitrosodimethylamine
ug/L
ND
5.0
0.91
10/25/18 15:43
N-Nitrosodiphenylamine
ug/L
ND
10.0
1.0
10/25/18 15:43
Naphthalene
ug/L
ND
5.0
0.34
10/25/18 15:43
Nitrobenzene
ug/L
ND
5.0
1.1
10/25/18 15:43
Pentachlorophenol
ug/L
ND
10.0
4.6
10/25/18 15:43
Phenanthrene
ug/L
ND
5.0
0.22
10/25/18 15:43
Phenol
ug/L
ND
5.0
1.9
10/25/18 15:43
Pyrene
ug/L
ND
5.0
0.19
10/25/18 15:43
2,4,6-Tribromophenol (S)
%
72
10-137
10/25/18 15:43
2-Fluorobiphenyl (S)
%
66
15-120
10/25/18 15:43
2-Fluorophenol (S)
%
41
10-120
10/25/18 15:43
Nitrobenzene-d5 (S)
%
87
10-120
10/25/18 15:43
Phenol-d6 (S)
%
28
10-120
10/25/18 15:43
Terphenyl-d14 (S)
%
90
11-131
10/25/18 15:43
LABORATORY CONTROL SAMPLE:
Parameter
2408145
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
32.8
66
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
50
36.0
72
36-166
2,4,6-Trichlorophenol
ug/L
50
40.4
81
37-144
2,4-Dichlorophenol
ug/L
50
40.3
81
39-135
2,4-Dimethylphenol
ug/L
50
43.9
88
32-120
2,4-Dinitrophenol
ug/L
250
233
93
1-191
2,4-Dinitrotoluene
ug/L
50
41.6
83
39-139
2,6-Dinitrotoluene
ug/L
50
42.0
84
50-158
2-Chloronaphthalene
ug/L
50
34.8
70
60-120
2-Chlorophenol
ug/L
50
34.6
69
23-134
2-Nitrophenol
ug/L
50
43.7
87
29-181
3,3'-Dichlorobenzidine
ug/L
100
69.6
70
1-262
4,6-Dinitro-2-methyl phenol
ug/L
100
102
102
1-181
4-Bromophenylphenyl ether
ug/L
50
39.6
79
53-127
4-ChIoro-3-methyl phenol
ug/L
100
79.2
79
22-147
4-Chlorophenylphenyl ether
ug/L
50
36.1
72
25-158
4-Nitrophenol
ug/L
250
92.7
37
1-132
Acenaphthene
ug/L
50
35.9
72
47-145
Acenaphthylene
ug/L
50
36.4
73
33-145
Anthracene
ug/L
50
38.9
78
27-133
Benzo(a)anthracene
ug/L
50
39.0
78
33-143
Benzo(a)pyrene
ug/L
50
39.6
79
17-163
Benzo(b)fluoranthene
ug/L
50
41.5
83
24-159
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 56

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
LABORATORY CONTROL SAMPLE:
2408145
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Benzo(g,h,i)perylene
ug/L
50
34.7
69
1-219
Benzo(k)fluoranthene
ug/L
50
33.2
66
11-162
bis(2-Chloroethoxy)methane
ug/L
50
39.2
78
33-184
bis(2-Chloroethyl) ether
ug/L
50
34.2
68
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
37.3
75
8-158
Butylbenzylphthalate
ug/L
50
38.9
78
1-152
Chrysene
ug/L
50
37.8
76
17-168
Di-n-butylphthalate
ug/L
50
32.4
65
1-120
Di-n-octylphthalate
ug/L
50
45.3
91
4-146
Dibenz(a,h)anthracene
ug/L
50
35.2
70
1-227
Diethylphthalate
ug/L
50
32.4
65
1-120
Dimethylphthalate
ug/L
50
32.9
66
1-120
Fluoranthene
ug/L
50
36.5
73
26-137
Fluorene
ug/L
50
37.7
75
59-121
Hexachloro-1,3-butadiene
ug/L
50
29.3
59
24-120
Hexachlorobenzene
ug/L
50
35.1
70
1-152
Hexachlorocyclopentadiene
ug/L
50
37.6
75
25-150
Hexachloroethane
ug/L
50
28.7
57
40-120
Indeno(1,2,3-cd)pyrene
ug/L
50
38.0
76
1-171
Isophorone
ug/L
50
35.4
71
21-196
N-Nitroso-di-n-propylamine
ug/L
50
38.0
76
1-230
N-Nitrosodimethylamine
ug/L
50
26.7
53
25-150
N-Nitrosodiphenylamine
ug/L
50
38.5
77
25-150
Naphthalene
ug/L
50
33.7
67
21-133
Nitrobenzene
ug/L
50
40.3
81
35-180
Pentachlorophenol
ug/L
100
76.8
77
14-176
Phenanthrene
ug/L
50
38.2
76
54-120
Phenol
ug/L
50
14.7
29
5-120
Pyrene
ug/L
50
42.2
84
52-120
2,4,6-Tribromophenol (S)
%
86
10-137
2-Fluorobiphenyl (S)
%
73
15-120
2-Fluorophenol(S)
%
44
10-120
Nitrobenzene-d5 (S)
%
85
10-120
Phenol-d6 (S)
%
30
10-120
Terphenyl-d14 (S)
%
75
11-131
MATRIX SPIKE SAMPLE:
2408146
92404515001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
49
29.1
59
44-142
2,2'-Oxybis(1-chloropropane)
ug/L
ND
49
29.9
61
36-166
2,4,6-Trichlorophenol
ug/L
ND
49
34.1
70
37-144
2,4-Dichlorophenol
ug/L
ND
49
31.4
64
39-135
2,4-Dimethylphenol
ug/L
ND
49
3.OJ
6
32-120 M1
2,4-Dinitrophenol
ug/L
ND
245
235
96
1-191
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 56

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
MATRIX SPIKE SAMPLE:
2408146
92404515001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
ND
49
39.5
81
39-139
2,6-Dinitrotoluene
ug/L
ND
49
40.7
83
50-158
2-Chloronaphthalene
ug/L
ND
49
29.3
60
60-120
2-Chlorophenol
ug/L
ND
49
24.5
50
23-134
2-Nitrophenol
ug/L
ND
49
35.9
73
29-182
3,3'-Dichlorobenzidine
ug/L
ND
98
ND
0
1-262 M1
4,6-Dinitro-2-methyl phenol
ug/L
ND
98
99.7
102
1-181
4-Bromophenylphenyl ether
ug/L
ND
49
35.1
72
53-127
4-Chloro-3-methylphenol
ug/L
ND
98
61.7
63
22-147
4-Chlorophenylphenyl ether
ug/L
ND
49
32.8
67
25-158
4-Nitrophenol
ug/L
ND
245
91.8
37
1-132
Acenaphthene
ug/L
ND
49
30.7
63
47-145
Acenaphthylene
ug/L
ND
49
23.3
47
33-145
Anthracene
ug/L
ND
49
22.5
46
27-133
Benzo(a)anthracene
ug/L
ND
49
33.1
68
33-143
Benzo(a)pyrene
ug/L
ND
49
19.2
39
17-163
Benzo(b)fluoranthene
ug/L
ND
49
39.2
80
24-159
Benzo(g,h,i)perylene
ug/L
ND
49
36.0
73
1-219
Benzo(k)fluoranthene
ug/L
ND
49
32.5
66
11-162
bis(2-Chloroethoxy)methane
ug/L
ND
49
32.4
66
33-184
bis(2-Chloroethyl) ether
ug/L
ND
49
27.2
55
12-158
bis(2-Ethylhexyl)phthalate
ug/L
ND
49
35.2
72
8-158
Butylbenzylphthalate
ug/L
ND
49
34.8
71
1-152
Chrysene
ug/L
ND
49
34.9
71
17-168
Di-n-butylphthalate
ug/L
ND
49
31.3
64
1-120
Di-n-octylphthalate
ug/L
ND
49
45.7
93
4-146
Dibenz(a,h)anthracene
ug/L
ND
49
39.0
80
1-227
Diethylphthalate
ug/L
ND
49
32.1
65
1-120
Dimethylphthalate
ug/L
ND
49
30.3
62
1-120
Fluoranthene
ug/L
ND
49
35.6
73
26-137
Fluorene
ug/L
ND
49
33.9
69
59-121
Hexachloro-1,3-butadiene
ug/L
ND
49
25.7
53
24-120
Hexachlorobenzene
ug/L
ND
49
31.4
64
1-152
Hexachlorocyclopentadiene
ug/L
ND
49
31.8
65
25-150
Hexachloroethane
ug/L
ND
49
24.9
51
40-120
Indeno(1,2,3-cd)pyrene
ug/L
ND
49
39.2
80
1-171
Isophorone
ug/L
ND
49
29.1
59
21-196
N-Nitroso-di-n-propylamine
ug/L
ND
49
30.1
61
1-230
N-Nitrosodimethylamine
ug/L
ND
49
20.7
42
25-150
N-Nitrosodiphenylamine
ug/L
ND
49
32.0
65
25-150
Naphthalene
ug/L
ND
49
28.9
59
21-133
Nitrobenzene
ug/L
ND
49
63.8
130
35-180
Pentachlorophenol
ug/L
ND
98
72.9
74
14-176
Phenanthrene
ug/L
ND
49
34.7
71
54-120
Phenol
ug/L
ND
49
11.3
23
5-120
Pyrene
ug/L
ND
49
34.4
70
52-120
2,4,6-Tribromophenol (S)
%
78
10-137
Results presented on this
page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 56

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
MATRIX SPIKE SAMPLE:
2408146
92404515001 Spike MS MS
% Rec
Parameter
Units
Result Conc. Result % Rec
Limits Qualifiers
2-Fluorobiphenyl (S)
%
60
15-120
2-Fluorophenol(S)
%
29
10-120
Nitrobenzene-d5 (S)
%
72
10-120
Phenol-d6 (S)
%
21
10-120
Terphenyl-d14 (S)
%
35
11-131
SAMPLE DUPLICATE: 2408147
Parameter
Units
92404493001
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/L
ND
ND
30
2,4,6-Trichlorophenol
ug/L
ND
ND
30
2,4-Dichlorophenol
ug/L
ND
ND
30
2,4-Dimethylphenol
ug/L
ND
ND
30
2,4-Dinitrophenol
ug/L
ND
ND
30
2,4-Dinitrotoluene
ug/L
ND
ND
30
2,6-Dinitrotoluene
ug/L
ND
ND
30
2-Chloronaphthalene
ug/L
ND
ND
30
2-Chlorophenol
ug/L
ND
ND
30
2-Nitrophenol
ug/L
ND
ND
30
3,3'-Dichlorobenzidine
ug/L
ND
ND
30
4,6-Dinitro-2-methyl phenol
ug/L
ND
ND
30
4-Bromophenylphenyl ether
ug/L
ND
ND
30
4-Chloro-3-methylphenol
ug/L
160
137 15
30
4-Chlorophenylphenyl ether
ug/L
ND
ND
30
4-Nitrophenol
ug/L
ND
ND
30
Acenaphthene
ug/L
ND
ND
30
Acenaphthylene
ug/L
ND
ND
30
Anthracene
ug/L
ND
ND
30
Benzo(a)anthracene
ug/L
ND
ND
30
Benzo(a)pyrene
ug/L
ND
ND
30
Benzo(b)fluoranthene
ug/L
ND
ND
30
Benzo(g,h,i)perylene
ug/L
ND
ND
30
Benzo(k)fluoranthene
ug/L
ND
ND
30
bis(2-Chloroethoxy)methane
ug/L
ND
ND
30
bis(2-Chloroethyl) ether
ug/L
ND
ND
30
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
30
Butylbenzylphthalate
ug/L
ND
ND
30
Chrysene
ug/L
ND
ND
30
Di-n-butylphthalate
ug/L
ND
ND
30
Di-n-octylphthalate
ug/L
ND
ND
30
Dibenz(a,h)anthracene
ug/L
ND
ND
30
Diethylphthalate
ug/L
ND
ND
30
Dimethylphthalate
ug/L
ND
ND
30
Fluoranthene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 39 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
SAMPLE DUPLICATE: 2408147
Parameter
Units
92404493001
Result
Dup
Result
Fluorene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitroso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
132
133
Pyrene
ug/L
ND
ND
2,4,6-Tribromophenol (S)
%
0
0
2-Fluorobiphenyl (S)
%
0
0
2-Fluorophenol(S)
%
0
0
Nitrobenzene-d5 (S)
%
0
0
Phenol-d6 (S)
%
0
0
Terphenyl-d14 (S)
%
0
0
Max
RPD RPD
a
Qualifiers
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
S4
S4
S4
D3,P3,S4
S4
S4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 437890 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
METHOD BLANK: 2407704 Matrix: Solid
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Diesel Range Organics(C10-C28) mg/kg ND 5.0 4.5 10/24/18 12:53
n-Pentacosane (S) % 75 33-129 10/24/18 12:53
LABORATORY CONTROL SAMPLE:
2407705
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.9 44.4
66
43-130
n-Pentacosane (S)
%
77
33-129
MATRIX SPIKE SAMPLE:
2407706
92404303001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 85.7
71.4
82 10-130
n-Pentacosane(S)
%
89 33-129
SAMPLE DUPLICATE: 2407707
92404303002 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND ND
30
n-Pentacosane (S)
%
73 69
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 56

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 438102 Analysis Method: EPA 8270D
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
METHOD BLANK: 2408753 Matrix: Solid
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
325
63.0
10/26/18 18:02
1,2-Dichlorobenzene
ug/kg
ND
325
86.6
10/26/18 18:02
1,3-Dichlorobenzene
ug/kg
ND
325
73.8
10/26/18 18:02
1,4-Dichlorobenzene
ug/kg
ND
325
91.5
10/26/18 18:02
1-Methylnaphthalene
ug/kg
ND
325
84.6
10/26/18 18:02
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
325
86.6
10/26/18 18:02
2,4,5-Trichlorophenol
ug/kg
ND
325
100
10/26/18 18:02
2,4,6-Trichlorophenol
ug/kg
ND
325
71.8
10/26/18 18:02
2,4-Dichlorophenol
ug/kg
ND
325
70.8
10/26/18 18:02
2,4-Dimethylphenol
ug/kg
ND
325
128
10/26/18 18:02
2,4-Dinitrophenol
ug/kg
ND
1620
53.1
10/26/18 18:02
2,4-Dinitrotoluene
ug/kg
ND
325
61.0
10/26/18 18:02
2,6-Dinitrotoluene
ug/kg
ND
325
67.9
10/26/18 18:02
2-Chloronaphthalene
ug/kg
ND
325
63.9
10/26/18 18:02
2-Chlorophenol
ug/kg
ND
325
88.5
10/26/18 18:02
2-Methylnaphthalene
ug/kg
ND
325
69.8
10/26/18 18:02
2-Methylphenol(o-Cresol)
ug/kg
ND
325
98.4
10/26/18 18:02
2-Nitroaniline
ug/kg
ND
1620
100
10/26/18 18:02
2-Nitrophenol
ug/kg
ND
325
78.7
10/26/18 18:02
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
325
128
10/26/18 18:02
3,3'-Dichlorobenzidine
ug/kg
ND
1620
70.8
10/26/18 18:02
3-Nitroaniline
ug/kg
ND
1620
88.5
10/26/18 18:02
4,6-Dinitro-2-methyl phenol
ug/kg
ND
649
64.9
10/26/18 18:02
4-Bromophenylphenyl ether
ug/kg
ND
325
59.0
10/26/18 18:02
4-ChIoro-3-methyl phenol
ug/kg
ND
649
66.9
10/26/18 18:02
4-Chloroaniline
ug/kg
ND
1620
90.5
10/26/18 18:02
4-Chlorophenylphenyl ether
ug/kg
ND
325
66.9
10/26/18 18:02
4-Nitroaniline
ug/kg
ND
649
91.5
10/26/18 18:02
4-Nitrophenol
ug/kg
ND
1620
58.0
10/26/18 18:02
Acenaphthene
ug/kg
ND
325
74.8
10/26/18 18:02
Acenaphthylene
ug/kg
ND
325
76.7
10/26/18 18:02
Aniline
ug/kg
ND
325
87.5
10/26/18 18:02
Anthracene
ug/kg
ND
325
72.8
10/26/18 18:02
Benzo(a)anthracene
ug/kg
ND
325
60.0
10/26/18 18:02
Benzo(a)pyrene
ug/kg
ND
325
62.0
10/26/18 18:02
Benzo(b)fluoranthene
ug/kg
ND
325
56.1
10/26/18 18:02
Benzo(g,h,i)perylene
ug/kg
ND
325
82.6
10/26/18 18:02
Benzo(k)fluoranthene
ug/kg
ND
325
63.9
10/26/18 18:02
Benzoic Acid
ug/kg
ND
1620
59.0
10/26/18 18:02
Benzyl alcohol
ug/kg
ND
649
64.9
10/26/18 18:02
bis(2-Chloroethoxy)methane
ug/kg
ND
325
75.7
10/26/18 18:02
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
METHOD BLANK: 2408753 Matrix: Solid
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
bis(2-Chloroethyl) ether
ug/kg
ND
325
82.6
10/26/18 18:02
bis(2-Ethylhexyl)phthalate
ug/kg
ND
325
88.5
10/26/18 18:02
Butylbenzylphthalate
ug/kg
ND
325
68.9
10/26/18 18:02
Chrysene
ug/kg
ND
325
43.3
10/26/18 18:02
Di-n-butylphthalate
ug/kg
ND
325
53.1
10/26/18 18:02
Di-n-octylphthalate
ug/kg
ND
325
67.9
10/26/18 18:02
Dibenz(a,h)anthracene
ug/kg
ND
325
68.9
10/26/18 18:02
Dibenzofuran
ug/kg
ND
325
53.1
10/26/18 18:02
Diethylphthalate
ug/kg
ND
325
50.2
10/26/18 18:02
Dimethylphthalate
ug/kg
ND
325
65.9
10/26/18 18:02
Fluoranthene
ug/kg
ND
325
47.2
10/26/18 18:02
Fluorene
ug/kg
ND
325
66.9
10/26/18 18:02
Hexachloro-1,3-butadiene
ug/kg
ND
325
56.1
10/26/18 18:02
Hexachlorobenzene
ug/kg
ND
325
41.3
10/26/18 18:02
Hexachlorocyclopentadiene
ug/kg
ND
325
60.0
10/26/18 18:02
Hexachloroethane
ug/kg
ND
325
85.6
10/26/18 18:02
Indeno(1,2,3-cd)pyrene
ug/kg
ND
325
66.9
10/26/18 18:02
Isophorone
ug/kg
ND
325
72.8
10/26/18 18:02
N-Nitroso-di-n-propylamine
ug/kg
ND
325
62.0
10/26/18 18:02
N-Nitrosodimethylamine
ug/kg
ND
325
105
10/26/18 18:02
N-Nitrosodiphenylamine
ug/kg
ND
325
96.4
10/26/18 18:02
Naphthalene
ug/kg
ND
325
79.7
10/26/18 18:02
Nitrobenzene
ug/kg
ND
325
88.5
10/26/18 18:02
Pentachlorophenol
ug/kg
ND
1620
59.0
10/26/18 18:02
Phenanthrene
ug/kg
ND
325
54.1
10/26/18 18:02
Phenol
ug/kg
ND
325
97.4
10/26/18 18:02
Pyrene
ug/kg
ND
325
55.1
10/26/18 18:02
2,4,6-Tribromophenol (S)
%
56
27-110
10/26/18 18:02
2-Fluorobiphenyl (S)
%
52
30-110
10/26/18 18:02
2-Fluorophenol (S)
%
54
13-110
10/26/18 18:02
Nitrobenzene-d5 (S)
%
65
23-110
10/26/18 18:02
Phenol-d6 (S)
%
54
22-110
10/26/18 18:02
Terphenyl-d14 (S)
%
67
28-110
10/26/18 18:02
Qualifiers
LABORATORY CONTROL SAMPLE:
2408754
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1680
1560
93
36-120
1,2-Dichlorobenzene
ug/kg
1680
1220
72
41-120
1,3-Dichlorobenzene
ug/kg
1680
1190
71
66-120
1,4-Dichlorobenzene
ug/kg
1680
1250
74
42-120
1-Methylnaphthalene
ug/kg
1680
1660
99
40-120
2,2'-Oxybis(1-chloropropane)
ug/kg
1680
1240
74
17-120
2,4,5-Trichlorophenol
ug/kg
1680
1200
72
37-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
LABORATORY CONTROL SAMPLE:
Parameter
2408754
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,6-TrichIorophenol
ug/kg
1680
1280
77
40-120
2,4-DichIorophenol
ug/kg
1680
1580
94
33-120
2,4-Dimethylphenol
ug/kg
1680
1770
105
36-120
2,4-Dinitrophenol
ug/kg
8390
5300
63
22-121
2,4-Dinitrotoluene
ug/kg
1680
1300
77
60-120
2,6-Dinitrotoluene
ug/kg
1680
1370
81
54-120
2-Chloronaphthalene
ug/kg
1680
1280
77
41-120
2-Chlorophenol
ug/kg
1680
1330
79
39-120
2-Methylnaphthalene
ug/kg
1680
1700
101
26-120
2-Methylphenol(o-Cresol)
ug/kg
1680
1620
96
41-120
2-Nitroaniline
ug/kg
3360
2380
71
45-120
2-Nitrophenol
ug/kg
1680
1620
97
35-120
3&4-Methyl phenol (m&p Cresol)
ug/kg
1680
1320
78
35-120
3,3'-Dichlorobenzidine
ug/kg
3360
2120
63
16-125
3-Nitroaniline
ug/kg
3360
1690
50
45-120
4,6-Dinitro-2-methyl phenol
ug/kg
3360
2830
84
46-120
4-Bromophenylphenyl ether
ug/kg
1680
1480
88
36-120
4-Chloro-3-methylphenol
ug/kg
3360
2950
88
37-120
4-Chloroaniline
ug/kg
3360
1130J
34
35-120 L2
4-Chlorophenylphenyl ether
ug/kg
1680
1370
82
30-120
4-Nitroaniline
ug/kg
3360
1910
57
48-120
4-Nitrophenol
ug/kg
8390
5470
65
43-120
Acenaphthene
ug/kg
1680
1270
76
46-120
Acenaphthylene
ug/kg
1680
1270
76
46-120
Aniline
ug/kg
1680
677
40
33-120
Anthracene
ug/kg
1680
1330
79
63-120
Benzo(a)anthracene
ug/kg
1680
1400
83
61-120
Benzo(a)pyrene
ug/kg
1680
1320
79
59-120
Benzo(b)fluoranthene
ug/kg
1680
1350
80
55-120
Benzo(g,h,i)perylene
ug/kg
1680
1270
75
57-120
Benzo(k)fluoranthene
ug/kg
1680
1270
76
56-120
Benzoic Acid
ug/kg
8390
6030
72
13-120
Benzyl alcohol
ug/kg
3360
1860
55
34-120
bis(2-Chloroethoxy)methane
ug/kg
1680
1660
99
21-120
bis(2-Chloroethyl) ether
ug/kg
1680
1380
83
25-120
bis(2-Ethylhexyl)phthalate
ug/kg
1680
1300
77
56-123
Butylbenzylphthalate
ug/kg
1680
1300
78
57-120
Chrysene
ug/kg
1680
1400
83
64-120
Di-n-butylphthalate
ug/kg
1680
1230
73
58-120
Di-n-octylphthalate
ug/kg
1680
1390
83
47-121
Dibenz(a,h)anthracene
ug/kg
1680
1370
82
56-120
Dibenzofuran
ug/kg
1680
1290
77
43-120
Diethylphthalate
ug/kg
1680
1160
69
55-120
Dimethylphthalate
ug/kg
1680
1200
71
54-120
Fluoranthene
ug/kg
1680
1230
73
61-120
Fluorene
ug/kg
1680
1290
77
51-120
Hexachloro-1,3-butadiene
ug/kg
1680
1550
92
22-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
LABORATORY CONTROL SAMPLE:
2408754
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Hexachlorobenzene
ug/kg
1680
1480
88
53-120
Hexachlorocyclopentadiene
ug/kg
1680
1080
64
18-150
Hexachloroethane
ug/kg
1680
1260
75
39-120
Indeno(1,2,3-cd)pyrene
ug/kg
1680
1270
76
58-120
Isophorone
ug/kg
1680
1410
84
38-120
N-Nitroso-di-n-propylamine
ug/kg
1680
1250
74
30-120
N-Nitrosodimethylamine
ug/kg
1680
1430
85
32-120
N-Nitrosodiphenylamine
ug/kg
1680
1360
81
50-120
Naphthalene
ug/kg
1680
1630
97
38-120
Nitrobenzene
ug/kg
1680
1550
92
37-120
Pentachlorophenol
ug/kg
3360
1890
56
10-120
Phenanthrene
ug/kg
1680
1320
79
62-120
Phenol
ug/kg
1680
1330
79
37-120
Pyrene
ug/kg
1680
1350
81
63-120
2,4,6-Tribromophenol (S)
%
85
27-110
2-Fluorobiphenyl (S)
%
78
30-110
2-Fluorophenol(S)
%
80
13-110
Nitrobenzene-d5 (S)
%
93
23-110
Phenol-d6 (S)
%
80
22-110
Terphenyl-d14 (S)
%
92
28-110
MATRIX SPIKE SAMPLE:
2408755
92404360001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
ND
1990
954
48
18-119
1,2-Dichlorobenzene
ug/kg
ND
1990
775
39
50-110 M1
1,3-Dichlorobenzene
ug/kg
ND
1990
772
39
27-110
1,4-Dichlorobenzene
ug/kg
ND
1990
803
40
28-110
1-Methylnaphthalene
ug/kg
ND
1990
990
50
24-116
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
1990
836
42
50-150 M1
2,4,5-Trichlorophenol
ug/kg
ND
1990
727
36
28-110
2,4,6-Trichlorophenol
ug/kg
ND
1990
765
38
17-117
2,4-Dichlorophenol
ug/kg
ND
1990
947
47
21-128
2,4-Dimethylphenol
ug/kg
ND
1990
673
34
10-120
2,4-Dinitrophenol
ug/kg
ND
9970
3670
37
10-107
2,4-Dinitrotoluene
ug/kg
ND
1990
797
29
36-109 M1
2,6-Dinitrotoluene
ug/kg
ND
1990
821
41
32-110
2-Chloronaphthalene
ug/kg
ND
1990
773
39
30-107
2-Chlorophenol
ug/kg
ND
1990
789
40
14-106
2-Methylnaphthalene
ug/kg
ND
1990
994
50
10-135
2-Methylphenol(o-Cresol)
ug/kg
ND
1990
733
37
10-124
2-Nitroaniline
ug/kg
ND
3980
1560J
39
26-116
2-Nitrophenol
ug/kg
ND
1990
998
50
28-103
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
1990
662
33
10-109
3,3'-Dichlorobenzidine
ug/kg
ND
3980
808J
20
10-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
MATRIX SPIKE SAMPLE:
2408755
92404360001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
3-Nitroaniline
ug/kg
ND
3980
1080J
27
22-110
4,6-Dinitro-2-methyl phenol
ug/kg
ND
3980
1670
42
13-121
4-Bromophenylphenyl ether
ug/kg
ND
1990
822
41
31-109
4-Chloro-3-methylphenol
ug/kg
ND
3980
1810
45
13-128
4-Chloroaniline
ug/kg
ND
3980
831J
21
18-102
4-Chlorophenylphenyl ether
ug/kg
ND
1990
811
41
29-112
4-Nitroaniline
ug/kg
ND
3980
1310
33
16-111
4-Nitrophenol
ug/kg
ND
9970
3610
36
14-135
Acenaphthene
ug/kg
ND
1990
786
39
26-114
Acenaphthylene
ug/kg
ND
1990
770
39
32-108
Aniline
ug/kg
ND
1990
554
28
10-107
Anthracene
ug/kg
ND
1990
828
41
32-111
Benzo(a)anthracene
ug/kg
ND
1990
1030
44
25-117
Benzo(a)pyrene
ug/kg
ND
1990
927
40
25-106
Benzo(b)fluoranthene
ug/kg
ND
1990
996
41
24-110
Benzo(g,h,i)perylene
ug/kg
ND
1990
892
40
19-112
Benzo(k)fluoranthene
ug/kg
ND
1990
821
37
24-114
Benzoic Acid
ug/kg
ND
9970
4100
41
10-110
Benzyl alcohol
ug/kg
ND
3980
1480
37
24-106
bis(2-Chloroethoxy)methane
ug/kg
ND
1990
1050
53
13-119
bis(2-Chloroethyl) ether
ug/kg
ND
1990
868
44
10-134
bis(2-Ethylhexyl)phthalate
ug/kg
ND
1990
723
36
10-125
Butylbenzylphthalate
ug/kg
ND
1990
734
37
18-110
Chrysene
ug/kg
ND
1990
980
41
30-110
Di-n-butylphthalate
ug/kg
ND
1990
741
37
19-112
Di-n-octylphthalate
ug/kg
ND
1990
788
40
17-105
Dibenz(a,h)anthracene
ug/kg
ND
1990
809
41
23-111
Dibenzofuran
ug/kg
ND
1990
809
41
35-103
Diethylphthalate
ug/kg
ND
1990
723
36
27-113
Dimethylphthalate
ug/kg
ND
1990
722
36
26-111
Fluoranthene
ug/kg
ND
1990
1230
45
33-109
Fluorene
ug/kg
ND
1990
807
40
32-113
Hexachloro-1,3-butadiene
ug/kg
ND
1990
913
46
16-116
Hexachlorobenzene
ug/kg
ND
1990
779
39
27-120
Hexachlorocyclopentadiene
ug/kg
ND
1990
645
32
10-108
Hexachloroethane
ug/kg
ND
1990
817
41
10-117
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1990
881
40
10-122
Isophorone
ug/kg
ND
1990
890
45
28-114
N-Nitroso-di-n-propylamine
ug/kg
ND
1990
770
39
27-113
N-Nitrosodimethylamine
ug/kg
ND
1990
1010
51
10-109
N-Nitrosodiphenylamine
ug/kg
ND
1990
756
38
10-128
Naphthalene
ug/kg
ND
1990
1040
52
25-110
Nitrobenzene
ug/kg
ND
1990
963
48
18-114
Pentachlorophenol
ug/kg
ND
3980
1140J
29
10-122
Phenanthrene
ug/kg
ND
1990
1070
46
30-114
Phenol
ug/kg
ND
1990
771
39
11-102
Pyrene
ug/kg
ND
1990
1120
43
25-116
Results presented on this
page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: MERIDALE
Pace Project No.: 92404510
MATRIX SPIKE SAMPLE:
Parameter
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
2408755
Units
92404360001 Spike MS MS
Result Conc. Result % Rec
% Rec
Limits
%
39
27-110
%
40
30-110
%
40
13-110
%
51
23-110
%
40
22-110
%
44
28-110
SAMPLE DUPLICATE: 2408756
Parameter
Units
92404360002
Result
Dup
Result
Max
RPD RPD
1,2,4-Trichlorobenzene
ug/kg
ND
ND
30
1,2-Dichlorobenzene
ug/kg
ND
ND
30
1,3-Dichlorobenzene
ug/kg
ND
ND
30
1,4-Dichlorobenzene
ug/kg
ND
ND
30
1-Methylnaphthalene
ug/kg
ND
ND
30
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
ND
30
2,4,5-Trichlorophenol
ug/kg
ND
ND
30
2,4,6-Trichlorophenol
ug/kg
ND
ND
30
2,4-Dichlorophenol
ug/kg
ND
ND
30
2,4-Dimethylphenol
ug/kg
ND
ND
30
2,4-Dinitrophenol
ug/kg
ND
ND
30
2,4-Dinitrotoluene
ug/kg
ND
ND
30
2,6-Dinitrotoluene
ug/kg
ND
ND
30
2-Chloronaphthalene
ug/kg
ND
ND
30
2-Chlorophenol
ug/kg
ND
ND
30
2-Methylnaphthalene
ug/kg
ND
ND
30
2-Methylphenol(o-Cresol)
ug/kg
ND
ND
30
2-Nitroaniline
ug/kg
ND
ND
30
2-Nitrophenol
ug/kg
ND
ND
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
ND
30
3,3'-Dichlorobenzidine
ug/kg
ND
ND
30
3-Nitroaniline
ug/kg
ND
ND
30
4,6-Dinitro-2-methyl phenol
ug/kg
ND
ND
30
4-Bromophenylphenyl ether
ug/kg
ND
ND
30
4-ChIoro-3-methyl phenol
ug/kg
ND
ND
30
4-Chloroaniline
ug/kg
ND
ND
30
4-Chlorophenylphenyl ether
ug/kg
ND
ND
30
4-Nitroaniline
ug/kg
ND
ND
30
4-Nitrophenol
ug/kg
ND
ND
30
Acenaphthene
ug/kg
ND
1091
30
Acenaphthylene
ug/kg
ND
ND
30
Aniline
ug/kg
ND
ND
30
Anthracene
ug/kg
ND
489
30
Benzo(a)anthracene
ug/kg
1180
1490
23 30
Benzo(a)pyrene
ug/kg
1050
1290
20 30
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
SAMPLE DUPLICATE: 2408756
Parameter
Units
92404360002
Result
Dup
Result
Benzo(b)fluoranthene
ug/kg
1440
1690
Benzo(g,h,i)perylene
ug/kg
685
820
Benzo(k)fluoranthene
ug/kg
568
757
Benzoic Acid
ug/kg
ND
ND
Benzyl alcohol
ug/kg
ND
ND
bis(2-Chloroethoxy)methane
ug/kg
ND
ND
bis(2-Chloroethyl) ether
ug/kg
ND
ND
bis(2-Ethylhexyl)phthalate
ug/kg
ND
ND
Butylbenzylphthalate
ug/kg
ND
ND
Chrysene
ug/kg
1190
1440
Di-n-butylphthalate
ug/kg
ND
ND
Di-n-octylphthalate
ug/kg
ND
ND
Dibenz(a,h)anthracene
ug/kg
ND
ND
Dibenzofuran
ug/kg
ND
ND
Diethylphthalate
ug/kg
ND
ND
Dimethylphthalate
ug/kg
ND
ND
Fluoranthene
ug/kg
2900
3610
Fluorene
ug/kg
ND
116J
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Hexachlorobenzene
ug/kg
ND
ND
Hexachlorocyclopentadiene
ug/kg
ND
ND
Hexachloroethane
ug/kg
ND
ND
Indeno(1,2,3-cd)pyrene
ug/kg
644
781
Isophorone
ug/kg
ND
ND
N-Nitroso-di-n-propylamine
ug/kg
ND
ND
N-Nitrosodimethylamine
ug/kg
ND
ND
N-Nitrosodiphenylamine
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
Nitrobenzene
ug/kg
ND
ND
Pentachlorophenol
ug/kg
ND
ND
Phenanthrene
ug/kg
1610
1980
Phenol
ug/kg
ND
ND
Pyrene
ug/kg
2160
2710
2,4,6-Tribromophenol (S)
%
46
51
2-Fluorobiphenyl (S)
%
47
53
2-Fluorophenol(S)
%
43
50
Nitrobenzene-d5 (S)
%
62
71
Phenol-d6 (S)
%
49
54
Terphenyl-d14 (S)
%
51
54
Max
RPD RPD Qualifiers
16
18
29
19
Pia
19
20
23
9
9
14
13
9
4
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 48 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 439101 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
METHOD BLANK: 2413304
Matrix:
Solid
Associated Lab Samples:
92404510002, 92404510003,
92404510004, 92404510005
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
10.0
10.0 11/01/18 07:26 N2
Aliphatic (C19-C36)
mg/kg
ND
10.0
10.0 11/01/18 07:26 N2
Aromatic (C11-C22)
mg/kg
ND
10.0
10.0 11/01/18 07:26 N2
2-Bromonaphthalene (S)
%
71
40-140
11/01/18 07:26
2-Fluorobiphenyl (S)
%
69
40-140
11/01/18 07:26
Nonatriacontane (S)
%
57
40-140
11/01/18 07:26
o-Terphenyl(S)
%
54
40-140
11/01/18 07:26
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2413305
Units
Spike
Conc.
2413306
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec Max
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10
ND ND
40
55
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.4
ND ND
41
56
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.4
14.9 13.6
52
48
40-140 9 50 N2
2-Bromonaphthalene (S)
%
78
69
40-140
2-Fluorobiphenyl (S)
%
78
69
40-140
Nonatriacontane (S)
%
46
57
40-140
o-Terphenyl(S)
%
55
51
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 49 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 438796 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Associated Lab Samples: 92404510001
METHOD BLANK: 2412177
Associated Lab Samples: 92404510001
Parameter
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
2-Bromonaphthalene (S)
2-Fluorobiphenyl (S)
Nonatriacontane (S)
o-Terphenyl(S)
Matrix: Water
Units
Blank
Result
Reporting
Limit
MDL Analyzed Qualifiers
ug/L
ND
100
100 10/30/18 07:03 N2
ug/L
ND
100
100 10/30/18 07:03 N2
ug/L
ND
100
100 10/30/18 07:03 N2
%
58
40-140
10/30/18 07:03
%
61
40-140
10/30/18 07:03
%
87
40-140
10/30/18 07:03
%
54
40-140
10/30/18 07:03
LABORATORY CONTROL SAMPLE & LCSD:
2412178
2412179
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
ug/L
300
219
221
73
74
40-140 1 50 N2
Aliphatic (C19-C36)
ug/L
400
319
384
80
96
40-140 19 50 N2
Aromatic (C11-C22)
ug/L
850
480
647
57
76
40-140 30 50 N2
2-Bromonaphthalene (S)
%
64
85
40-140
2-Fluorobiphenyl (S)
%
63
85
40-140
Nonatriacontane (S)
%
93
92
40-140
o-Terphenyl(S)
%
63
80
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /01 /2018 03:43 PM without the written consent of Pace Analytical Services, LLC.
Page 50 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MERIDALE
Pace Project No.: 92404510
QC Batch: 437893 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92404510002, 92404510003, 92404510004, 92404510005
SAMPLE DUPLICATE: 2407710
92404442001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 21.4 22.2 4 25
SAMPLE DUPLICATE: 2407711
92404461002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 3.9 3.3 17 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 56

Pace Analytical Services, LLC
ceAnalX cal ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: MERIDALE
Pace Project No.: 92404510
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MS Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.
N2 The lab does not hold NELAC/TNI accreditation for this parameter.
P3 Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/01/2018 03:43 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 56

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
MERIDALE
92404510
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92404510002
WEST WALL
EPA 3546
437890
EPA 8015C Modified
438028
92404510003
NORTH WALL
EPA 3546
437890
EPA 8015C Modified
438028
92404510004
SOUTH WALL
EPA 3546
437890
EPA 8015C Modified
438028
92404510005
EAST WALL
EPA 3546
437890
EPA 8015C Modified
438028
92404510002
WEST WALL
MADEP EPH
439101
MADEP EPH
439746
92404510003
NORTH WALL
MADEP EPH
439101
MADEP EPH
439746
92404510004
SOUTH WALL
MADEP EPH
439101
MADEP EPH
439746
92404510005
EAST WALL
MADEP EPH
439101
MADEP EPH
439746
92404510001
MW-UST
MADEP EPH
438796
MADEP EPH
439153
92404510002
WEST WALL
EPA 5030B
438081
EPA 8015C Modified
438089
92404510003
NORTH WALL
EPA 5030B
438081
EPA 8015C Modified
438089
92404510004
SOUTH WALL
EPA 5030B
438081
EPA 8015C Modified
438089
92404510005
EAST WALL
EPA 5030B
438081
EPA 8015C Modified
438089
92404510001
MW-UST
MADEP VPH
437976
92404510001
MW-UST
EPA 625.1
438001
EPA 625.1
438332
92404510002
WEST WALL
EPA 3546
438102
EPA 8270D
438643
92404510003
NORTH WALL
EPA 3546
438102
EPA 8270D
438643
92404510004
SOUTH WALL
EPA 3546
438102
EPA 8270D
438643
92404510005
EAST WALL
EPA 3546
438102
EPA 8270D
438643
92404510001
MW-UST
SM 6200B
438860
92404510002
WEST WALL
EPA 5035A
437990
EPA 8260B
438021
92404510003
NORTH WALL
EPA 5035A
437990
EPA 8260B
438021
92404510004
SOUTH WALL
EPA 5035A
437990
EPA 8260B
438021
92404510005
EAST WALL
EPA 5035A
437990
EPA 8260B
438021
92404510002
WEST WALL
ASTM D2974-87
437893
92404510003
NORTH WALL
ASTM D2974-87
437893
92404510004
SOUTH WALL
ASTM D2974-87
437893
92404510005
EAST WALL
ASTM D2974-87
437893
Date: 11/01/2018 03:43 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 53 of 56

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page i of 2
�acekuljdidal- Document No.: Issuing Authority:
F-CAR-CS-033•Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
Huntersville ❑ Raleigh❑ Mechanicsville❑
Sample Condition Client Name:
WO# : 92404510
Upon ReceiptI.
ES
Project A
Courier: ❑
❑ Fed Ex ❑UPS ❑USPS Commercial ❑Pace ❑Other;
111 I
III 1
1
92404510
9
Custody Seal Present? ❑Yes ❑No Seals intact? Oyes
❑No
Rate/initials Person Examining Contents: 'r1}
Packing Material: ❑Bubble Wrap ❑Bubble Bags []None
❑ Other Biological Tissue Frozen?
Thermometer:
­EIGun ID: 92T045 Type of Ice: nWet
❑yes ❑NO []N/A
❑Blue ❑None
Cooler Temp J'Q _ r� Correction Factor: Add/Subtract ('C) _�
]
Cooler Temp Corrected
Temp should be above freezing to 6'C
('C):
❑Samples out of temp criteria. Samples on ice, cooling process
USDA Regulated Soil (❑ N/A, water sample)
has begun
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
❑Yes MW
including Hawaii and Puerto Rfco)? ❑Yes ❑No
Comments/Ulscreaancv:
ain of
Samples Arrived within Hold Time?
Short Hold Time Analysis (<72 hr.l?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis; Samples Field Filtered?
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matr
Headspace in VOA Vials (*-6mm)?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
lii Yes
UNo
UN/A
1.
Yes
❑No
❑N/A
2.
❑Yes
Q Tvo
❑N/A
3.
❑Yes
Di4a
❑N/A
4.
.QYes
[]No
❑N/A
S.
,ffYes
[]No
❑NIA
6.
UYes LJNo LAN/A 7,
El EjNo ❑N/A a.
QYes [-]No❑N/A 4.
❑Yes QNo
Project Manager SCURF Review:
Project Manager SRF Review: ti
N/A 10.
N/A 11.
Date/Time:
Field Data Required? []Yes ❑No
Lot 10 of split containers:
Date: 10/Z4
Date: NZ 4—
Page 54 of 56

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Recelpt(SCUR) Page 1 of 2
�� aceArtalytieal" Document No.: issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is Project # t _1P��} : 924045 045 t @ _
verified and within the acceptance range for preservation WVT`r_--
samples. pM: PTE Due Date: 10/30/18
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT: 52--ESP Assoc
"Bottom half of box is to list number of bottle
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ti
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot N
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, put of temp, incorrect containers.
Page 55 of 56

Z
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11
TEMP in 0
Received on
Ice
(YIN)
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Methanol
Other
Analyses Test 1
VOC by 8260
SVOC by 8270, EPH, ORO
GRO by 8015B
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VPH
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Page 56 of 56

Raleigh
2200 Gateway Centre Blvd.
Suite 216
Morrisville, NC 27560
919.678.1070
Columbia
2711 Alpine Rd.
Suite 200
Columbia, SC 29223
803.705.2229
4 ESP
ESP Corporate Office
3475 Lakemont Blvd.
Fort Mill, SC 29708
803.802.2440
Mailing
PO Box 7030
Charlotte, NC 28241
Greensboro Concord
7011 Albert Pick Rd. 7144 Weddington Rd., NW
Suite E Suite 110
Greensboro, NC 27409 Concord, NC 28027
336.334.7724 704.793.9855
Charleston
5900 Core Ave.
Suite 104
North Charleston, SC 29406
843.714.2040
Wilmington
211 Racine Dr.
Suite 101
Wilmington, NC 28403
910.313.6648
Lake Norman
20484 Chartwell Center Dr.
Suite D
Cornelius, NC 28031
704.649.2863
Indianapolis
8673 Bash St.
Indianapolis, IN 46256
317.537.6979
Bradenton Nashville Pittsburgh
518 13'h Street West 500 Wilson Pike Cir. One Williamsburg PI.
Bradenton, FL 34205 Suite 310 Suite G-5, Box 13
941.345.5451 Brentwood, TN 37027 Warrendale, PA 15086
615.760.8300 724.462.6606
800.960.7317
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